0 GelmanSciences
Gelman Sciences Inc. 642 South Wagner Road Ann Arbor, MI 48103 734.436.4025 phone 734.436.4040 fax
CASE NARRATIVE Monthly Data Gelman Sciences Project: 1,4-Dioxane Remediation Date: April 2022
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition, all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
Gelman Sciences Inc. attests to the validity of the laboratory data generated by Gelman Sciences Ann Arbor, Michigan Environmental Laboratory facilities reported herein. All analyses performed by Gelman Science's Environmental Laboratory facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. Gelman Science's Environmental group has reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
At the end of the month some of the 1,4-dioxane samples were sent to Ann Arbor Technical Services for analysis due to a reproducibility problem. The balance of the samples was analyzed for 1,4-dioxane at Gelman Science's Environmental Laboratory. All bromate samples were analyzed by Gelman Science's Environmental Laboratory. The test results in this report meet all NELAP requirements for parameters for which accreditation are required or available. Any exceptions to NELAP requirements are noted in this report. All exceptions are noted per laboratory standard operating procedure based on EPA Method 1624c. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results. The odd even rule is used for rounding. Holding times were met for all samples analyzed. Proper preservation was observed on all samples unless otherwise detailed in the individual sections below. Samples MW-54d, 72d, and 71 were recollected due to questionable results.
RECEIPT/ STORAGE
The samples were received on the days noted in the report for the Month; the samples arrived in good condition, properly preserved and on ice when necessary. Samples that require 1,4-dioxane analysis are collected in hydrochloric HCI acid-preserved vials to a pH of ≤2, except for the Pall ozone treatment samples. These samples have chemicals that, when mixed with the HCI acid, cause interferences and trap damage. Every attempt is made to analyze these samples within 24 hours of receipt.
Samples that require Bromate analysis are collected and preserved in the laboratory with ethylene di-amine and refrigerated.
Samples that are delivered to the laboratory the same day as they are collected are likely not to have reached a fully chilled temperature. This is acceptable as long as there is evidence that chilling has begun. All samples are iced or refrigerated at 4°C (±2°C) from the time of collection until sample preparation or analysis.
1,4-Dioxane (GC-MS)
All ground water and treated water samples were analyzed for 1,4-Dioxane (GC-MS) in accordance with EPA 1624C, which has been modified to enhance detection limits. Samples that were diluted to bring them within the calibrated range of the instrument are noted with a "D" under the Qualifier Code section of the data report. Reporting limits were adjusted based on each dilution.
April 2022 Page 1 of 8
0 GelmanSciences Reporting limit for undiluted samples is 1ppb (part per billion, micrograms per liter, µg/L). All quality control parameters were within the acceptance limits for reported samples unless indicated.
Bromate (Ion Chromatography)
All surface water and treated samples were analyzed for Bromate (Ion Chromatography) in accordance with EPA 300.1. Surrogates are added to all samples. All quality control parameters were within the acceptance limits with the balance of sample analyzed.
The reporting limit for treated samples is 5.0ppb and for surface samples is 2.0ppb.
Barium
A composite Outfall001 sample was sent to Ann Arbor Technical Services (ATS) for total barium analysis in accordance with EPA 200.7. Barium samples are analyzed quarterly in compliance with PLS NPDES permit. This sample is preserved with nitric acid and refrigeration. The results were less than the permitted level of 440µg/L at 160µg/L.
Qualifiers
1,4-Dioxane Qualifier Codes:
Qualifier Code Description nd: The compound was analyzed for, but not detected at or above the detection limit indicated. D: Analyte value quantified from a dilution; reporting limit is raised to reflect dilution. E: The compound result is greater than the upper quantitation limit in the associated calibration curve, reported as estimate. B: The sample vials contained air bubbles larger than 5mm, which may affect compound results. J: The compound was positively identified; the associated numerical value is the approximate concentration. M: Matrix effects, sample required dilution.
R: The reported value is unusable and rejected due to variance from quality control criteria.
V: The reported value is considered estimated due to variance from quality control criteria. H: Sample was analyzed past 14-day hold time, but within 45 days. 0: Samples analyzed in outside laboratory.
S: Samples split with DEQ.
Bromate Qualifier Codes:
Qualifier Code Description nd: The compound was analyzed but was not detected at or above the detection limit indicated. E: The compound result is greater than the upper quantitation limit in the associated calibration curve. J: The compound was positively identified; the associated numerical value is the approximate concentration. R: The reported value is unusable and rejected due to variance from quality control criteria. V: The reported value is considered estimated due to variance from quality control criteria. H: Sample was analyzed past 28-day hold time
Analyst: Gage M. Trendel
Report Checked by: Ray Woods
Date:
April 2022 Page 2 of 8
m 477/> GelmanSciences Sample Analysis Report
April, 2022 642 South Wagner Road Ann Arbor, MI 48103-9019 US 734.436.4025 phone
Analyst Initials: eft - T-Date: 5lici-70
Sample Name - Date/Time Sampled 1,4-Dioxane Results (ppb) R.L. (ppb) Bromate Results (ppb) R.L. (ppb) Bromide Results (ppb) R.L. (ppb) Comments Qualifier(s)
Extraction Wells
C3
DOLPH-04-18-22-12:25-1 130 10 O,O
TW-10-04-18-22-12:10-1 970 10 O,D
TW-20-04-18-22-12:05-1 560 10 O,D
TW-24-04-29-22-12:25-1 2500 40 O,O
TVV-25-04-07-22-15:00-1 4000 80 O,D
TW-25-04-18-22-12:00-1 4000 80 O,D
D2
LB-4-04-18-22-10:05-1 450 10 O,O
TW 21 04 18 22 10:30 1 240 10 O,O
TW-5-04-18-22-11:45-1 760 20 O,O
E
TW-17-04-18-22-11:55-1 59 5 O,O
TW-18-04-18-22-10:35-1 250 10 O,O
TW-23-04-18-22-10:10-1 420 10 O,O
TW 29 04 18 22 10:15 1 330 10 O,D
SW
TW-22-04-18-22-12:15-1 420 10 O,O
TW-28-04-18-22-12:20-1 450 10 O,O
Monitoring Wells
Sample Name - Date/Time Sampled 1,4-Dioxane Results (ppb) R.L. (ppb) Bromate Results (ppb) R.L. (ppb) Bromide Results (ppb) R.L. (ppb) Comments Qualifier(s)
C3
MW-1 Replacement-04-21-22-14:20-1 1600 80 O,O
MW-105s-04-19-22-10:59-1 370 10 O,D
MW-32-04-28-22-14:52-1 14 1.0 O
DO
MW-142s-04-25-22-10:49-1 nd 1.0 O
MW-143s-04-25-22-12:22-1 nd 1.0 O
MW-53d-04-04-22-09:02-1 nd 1.0 O
MW-53i-04-04-22-11:38-1 36 1.0 O
MW-53s-04-04-22-10:22-1 nd 1.0 O
D2
175 Jackson Plaza-04-04-22-13:50-1 1200 40 O,D
2819 Dexter Rd-04-19-22-12:34-1 160 10 O,O
MW-107-04-19-22-14:10-1 580 10 O,O
MW-113-04-26-22-13:19-1 180 4 O,O
MW-120s-04-18-22-14:15-1 nd 1.0 O
MW-121s-04-18-22-09:36-1 nd 1.0 O
MW-92-04-26-22-11:55-1 87 4 O,O
MW-BE-1d-04-22-22-12:23-1 500 10 O,O
MW-BE-1s-04-22-22-13:50-1 570 40 O,O
E
MW-101-04-07-22-14:36-1 90 10 O,D
MW-103d-04-11-22-12:55-1 6 1.0 O
MW-103s-04-01-22-12:35-1 83 1.0 O
MW-104-04-07-22-12:06-1 30 1.0 O
MW-105d-04-19-22-09:49-1 130 10 O,O
Sample Name - Date/Time Sampled 1,4-Dioxane Results (ppb) R.L. (ppb) Bromate Results (ppb) R.L. (ppb) Bromide Results (ppb) R.L. (ppb) Comments Qualifier(s)
MW-106s-04-26-22-14:55-1 280 20 O,D
MW-108d-04-21-22-11:17-1 510 10 O,D
MW-108s-04-21-22-10:01-1 220 10 O,O
MW-110-04-07-22-13:22-1 120 10 O,O
MW-112d-04-11-22-10:26-1 2 1.0 O
MW-112i-04-11-22-11:35-1 9 1.0 O
MW-112s-04-11-22-09:16-1 3 1.0 O
MW-119-04-26-22-09:04-1 37 1.0 O
MW-120d-04-18-22-12:56-1 nd 1.0 O
MW-121d-04-18-22-10:45-1 2 1.0 O
MW-142d-04-25-22-09:38-1 nd 1.0 O
MW-143d-04-24-22-15:16-1 nd 1.0 O
MW-143i-04-25-22-13:31-1 nd 1.0 O
MW-71-04-21-22-12:43-1 1100 20 O,O
MW-76i-04-12-22-10:55-1 110 5 O,O
MW-76s-04-12-22-12:05-1 310 5 O,O
MW-79d-04-07-22-09:26-1 nd 1.0 O
MW-79s-04-07-22-10:38-1 290 10 O,O
MW-81-04-26-22-10:31-1 150 4 O,D
MW-84s-04-12-22-09:14-1 320 10 O,O
MW-85-04-12-22-13:28-1 420 40 O,O
Surface Water
Not Applicable
HC/HR-04-01-22-12:45-1 nd 2.0
HC/HR-04-04-22-09:50-1 nd 2.0
HC/HR-04-05-22-11:00-1 nd 2.0
HC/HR-04-06-22-09:50-1 nd 2.0
Sample Name - Date/Time Sampled 1,4-Dioxane Results (ppb) R.L. (ppb) Bromate Results (ppb) R.L. (ppb) Bromide Results (ppb) R.L. (ppb) Comments Qualifier(s)
HC/HR-04-07-22-10:20-1 nd 2.0
HC/HR-04-08-22-10:40-1 nd 2.0
HC/HR-04-11-22-10:40-1 nd 2.0
HC/HR-04-12-22-09:20-1 nd 2.0
HC/HR-04-13-22-09:45-1 nd 2.0
HC/HR-04-14-22-10:00-1 nd 2.0
HC/HR-04-15-22-09:50-1 nd 2.0
HC/HR-04-18-22-09:30-1 nd 2.0
HC/HR-04-19-22-11:00-1 nd 2.0
HC/HR-04-20-22-11:30-1 nd 2.0
HC/HR-04-21-22-09:40-1 nd 2.0
HC/HR-04-22-22-09:05-1 nd 2.0
HC/HR-04-25-22-13:30-1 nd 2.0
HC/HR-04-26-22-09:00-1 nd 2.0
HC/HR-04-27-22-09:10-1 nd 2.0
HC/HR-04-28-22-13:15-1 nd 2.0
HC/HR-04-29-22-12:00-1 nd 2.0
Treatment System
OUTFALL-04-03-22-1 6 1.0 O
OUTFALL-04-03-22-2 6.2 5.0
OUTFALL-04-04-22-1 6 1.0 O
OUTFALL-04-04-22-2 8.0 5.0
OUTFALL-04-05-22-1 5 1.0 O
OUTFALL-04-05-22-2 7.2 5.0
OUTFALL-04-06-22-1 5 1.0 O
OUTFALL-04-06-22-2 8.8 5.0
OUTFALL-04-07-22-1 5 1.0 O
Sample Name - Date/Time Sampled 1,4-Dioxane Results (ppb) R.L. (ppb) Bromate Results (ppb) R.L. (ppb) Bromide Results (ppb) R.L. (ppb) Comments Qualifier(s)
OUTFALL-04-07-22-2 7.4 5.0
OUTFALL-04-10-22-1 8 1.0 O
OUTFALL-04-10-22-2 11 5.0
OUTFALL-04-11-22-1 8 1.0 O
OUTFALL-04-11-22-2 8.4 5.0
OUTFALL-04-12-22-1 7 1.0 O
OUTFALL-04-12-22-2 8.0 5.0
OUTFALL-04-13-22-1 7 1.0 O
OUTFALL-04-13-22-2 7.2 5.0
OUTFALL-04-14-22-1 8 1.0 O
OUTFALL-04-14-22-2 8.3 5.0
OUTFALL-04-17-22-1 6 1.0 O
OUTFALL-04-17-22-2 8.2 5.0
OUTFALL-04-18-22-1 6 1.0 O
OUTFALL-04-18-22-2 11 5.0
OUTFALL-04-19-22-1 5 1.0 O
OUTFALL-04-19-22-2 11 5.0
OUTFALL-04-20-22-1 6 1.0 O
OUTFALL-04-20-22-2 12 5.0
OUTFALL-04-21-22-1 5 1.0 O
OUTFALL-04-21-22-2 10 5.0
OUTFALL-04-24-22-1 6 1.0 O
OUTFALL-04-24-22-2 8.8 5.0
OUTFALL-04-25-22-1 5 1.0 O
OUTFALL-04-25-22-2 10 5.0
OUTFALL-04-26-22-1 6 1.0 O
OUTFALL-04-26-22-2 11 5.0
Sample Name - Date/Time Sampled 1,4-Dioxane Results (ppb) R.L. (ppb) Bromate Results (ppb) R.L. (ppb) Bromide Results (ppb) R.L. (ppb) Comments Qualifier(s)
OUTFALL-04-27-22-1 5 1.0 O
OUTFALL-04-27-22-2 13 5.0
OUTFALL-04-28-22-1 7 1.0 O
OUTFALL-04-28-22-2 13 5.0
Red Pond-04-01-22-09:00-1 400 10 O,O
Red Pond-04-04-22-06:40-1 360 40 O,O
Red Pond-04-05-22-07:35-1 360 10 O,O
Red Pond-04-06-22-07:55-1 420 40 O,O
Red Pond-04-07-22-07:00-1 580 40 O,O
Red Pond-04-08-22-07:20-1 530 40 O,O
Red Pond-04-11-22-07:20-1 590 40 O,O
Red Pond-04-12-22-07:05-1 530 40 O,D
Red Pond-04-13-22-07:15-1 470 10 O,O
Red Pond-04-14-22-07:35-1 520 40 O,D
Red Pond-04-15-22-07:33-1 520 40 O,O
Red Pond-04-18-22-07:10-1 480 40 O,O
Red Pond-04-19-22-09:05-1 510 40 O,O
Red Pond-04-20-22-07:10-1 490 40 O,O
Red Pond-04-21-22-07:20-1 360 40 O,O
Red Pond-04-22-22-07:10-1 560 40 O,O
Red Pond-04-26-22-07:20-1 450 40 O,D
Red Pond-04-27-22-07:15-1 550 10 O,O
Red Pond-04-28-22-07:25-1 510 40 O,O
Red Pond-04-29-22-07:35-1 420 40 O,D
i
WM/780R TF :UNICA SE RIETS
290 South Wagner Road Ann Arbor. Michigan 48143 Tel. 7341996-0995 Fax- 734/996-3731 NlIchlgan Laboratory ID: 9504 Wisconsin Laboratory ID: 996321720
Data Transmittal Cover Page
Project Name: Pall Corporation
ATS Project Number: G001-002
ATS Report Number(s): Inorg_SRF_0411221 Client PO Number: 4505179649
Project Description: This data report contains the results of 1 water sample, received by ATS on April 11, 2022 to be analyzed for Barium.
We certify that the sample analyses for this report have been conducted in accordance with guidelines provided
in the referenced standard test method, and are consistent with detailed procedures described in a written Standard Operating Procedure specific to the ATS Laboratories, as required by USEPA. Laboratory data sheets, SOPs, and QA/QC information are available for inspection and audit at the laboratory upon request. Unless specifically noted on the data report, all applicable sample preservation and holding time requirements have been met.
Recipient: Mr. Gage Trendel
No. of Pages (including cover pg.): 10
From:
Email:
FAX Number:
claw trendel oall.com
Sarah Stubblefield Email: [email protected]
Senior Chemist / Lab Manager FAX Number: 734-995-3731
Additional Message: Copy report to: Patterson, Keith ([email protected]), Brode, Jim ([email protected])
Katie Strohauer ([email protected]), [email protected], Peters, Sue Peters ([email protected])
Amanda Isabella ([email protected])
Date: 4/18/22 Signed:
IF YOU DO NOT RECEIVE ALL PAGES OF THIS TRANSMITTAL, PLEASE CALL 734-995-0995.
This material is intended only for the use of the individual or entity to whom it is addressed, and may contain information that is privileged and
confidential. If you are not the intended recipient or the agent responsible for delivering this material to the intended recipient, you are hereby
notified that any dissemination, distribution or copying of this communication is strictly prohibited. If you have received this communication in
error, please notify us immediately by telephone. Thank you.
XAG001-002.221Data_Transmittal_Cover_Page SLS
ANN ARBOR TECHNICAL SERVICES INC.
INORGANIC ANALYSIS Barium by ICP-AES
USEPA 200.7
ATS Project Number: G001-002.22
ATS SDG: 0411221
Prepared By: Ann Arbor Technical Services, Inc.
290 South Wagner Road Ann Arbor, MI 48103
ANN ARBOR TECHNICAL SERVICES INC.
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: G001-002 Report Date: 4/18/22 SRF / SDG Number(s): 0411221 Client PO Number: 4505179649
Case Narrative Summary
This case narrative applies to the following sample that was received at Ann Arbor Technical Services, Inc. (ATS) on 4/11/22, and associated matrix-specific QA/QC:
Sam les
Client Sample Identification Sample Date Requested Turn Around Time Analysis Matrix
Received 4/11/22
Outfall Grab 4/9/22 Standard Barium Water
Upon receipt, samples were scheduled for the following analyses:
Analysis Number of Samples
• Metals Digestion by US EPA 200.7 • 1 Sample + 1 Matrix Spike + 1 Matrix Spike Duplicate
• Select Metals by US EPA 200.7 (Barium) • 1 Sample + 1 Matrix Spike + 1 Matrix Spike Duplicate
Sample Receipt, Chain of Custody Records, and Holding Times
Samples were delivered directly to ATS by Pall Corporation staff. Samples were received with proper chain of custody records included. Samples were preserved to a pH of <2 at the time of sample receipt. Sample condition and anomalies, if any, are presented in the "Sample Receipt" section of this report. All samples were prepared and analyzed within the holding times cited in the corresponding analytical methods with the following exceptions:
• None
Data Review and Approval
All data contained in this report have been generated in accordance with guidelines provided in the referenced standard test method, and are consistent with detailed procedures described in a written standard operating procedures (SOPs) specific to the ATS Laboratory, as required by US EPA. All data are peer and management reviewed to ensure compliance with the above referenced SOP's and project specifications. In addition, all data conform to the laboratory's Quality Assurance / Quality Control Manuals.
A single QA/QC batch is defined as no more than 20 samples excluding method blanks (MB, LRB), fortified blanks (BS, LFB, LCS), matrix spikes (MS, SPK), and duplicates whether spiked or native (MSD, SPK DUP, DUP, LR).
G001-002.22/CN0411221.doc
Consultants in Chemist?), & Environmental Science 290 South Wagner Road, Ann Arbor, Michigan 48103 Tel 734/995-0995 Fax 734/995-3731
Data Deliverables
This data package constitutes a Level II package; other data report packages (Level I, Level IV DVP, EPA R5 EDD) are available upon request. There were no hardcopy data summary sheets generated for this project.
Sample Preparation
Samples were digested in accordance with US EPA method 200.7 (Determination of Metals and Trace Elements in Water and Wastes by Inductively Coupled Plasma-Atomic Emission Spectrometry).
Anomalies Noted: • None
Sample Analysis
Samples were analyzed in accordance with US EPA method 200.7 (Determination of Metals and Trace Elements in Water and Wastes by Inductively Coupled Plasma-Atomic Emission Spectrometry). An initial calibration with at least five levels was used to quantitate individual metals. Samples were reported to project specific reporting limits as mg/L.
Anomalies Noted: • None
Sample Dilutions
Samples containing compounds at concentrations above the initial calibration curve were diluted and reanalyzed for those compounds. The following samples were diluted for barium.
• None
Analytical QA/QC Summary
Calibration Verification
Method calibration was verified through the analysis of a mid-level initial calibration verification (CV) standard at a frequency of every ten samples. All verification standards met the acceptance criteria with the following exceptions:
• None
Instrument Blanks
Low system background was demonstrated through the analysis of instrument blanks at a minimum of every ten samples. All instrument blanks met the acceptance criteria with the following exceptions:
• None
G001-002.22/CN_0411221.doc
QA/QC Batch Summary
Laboratory Reagent Blanks
A laboratory reagent blank (LRB) was analyzed with the QA/QC batch. The LRB met the acceptance criteria with the following exceptions:
• None
ACCURACY
Laboratory Fortified Blanks (LFB/OPR) Laboratory Control Samples - Accuracy
A laboratory fortified blank (LFB) was analyzed as part of the QA/QC batch. The LFB met the acceptance criteria with the following exceptions:
• None
Matrix Spikes and Matrix Spike Duplicates - Accuracy
A matrix spike (MS) and matrix spike duplicate (MSD) was analyzed as part of the QA/QC batch. The MS/MSD's met the acceptance criteria with the following exceptions:
• None
G001-002.22/CN_0411221.doc
PRECISION
Matrix Spike and Matrix Spike Duplicates - Precision
A matrix spike (MS) and matrix spike duplicate (MSD) was analyzed as part of the QA/QC batch. The replicates met the acceptance criteria with the following exceptions:
• None
//azmff,76' / April 18, 2022
Mark T. DeLong (Quality Assurance Coordinator)
/ April 18, 2022 Philip B. Simon (Laboratory Director)
G001-002.22/CN0411221.doc
; 230 South Wagner Road Ann Arbor, Michigan 48103 Tol. 7341995-0995 Fax. 734/995-3731 Michigan Laboratory ID: 9904 Wisconsin Laboratory ID: 998321720 VLINIUMOR TECMSCA.t. SERVICES
PROJECT ID / NUMBER
Pall / 0001-002
SAMPLE CUSTODIAN (Pfint tc,p.tuie)
Gage Trendel ([email protected])
RELINQUISHED BY (Prim L .;,:itac)
cl .............___
CHAIN OF CUSTODY RECORD
Client Purchase Authorization (Purchase Order)
PO# 4505179649
DATE / TIME
4/11/22 9:30
RECEIVED BY CP. Ju L '
3.-;
SHIPPING INFORMATION: SHIPPER (Check one) / TRACKING applicable)
Date Fed Ex UPS
Dale Fed Ex UPS
Date Fed Ex UPS Number
Dale Fed Ex UPS
DA E 7 /W RELINQUISHED BY (Print r. S., Inut4
a 01
RELIND SHED BY prat SIgnamo) DATE / TIME REC. JED BY Trull L rognam 4) DATE / TIME RELINQUISHED BY (pr.t.c,,,,,c)
COMMENTS (Preservation. etc.)
Oudall/Eff->Unpreserved All others.>HCI preserved
0
1.
2.
3.
4.
5.
8.
_ABGRAToRY ,LIENTIFICATION (AID Use Only) "ME Samoa Identificauan
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1 \ - 4/10/2022 r ,a X Outfall 1 1 X
i 4/11/2022 7:20 X Red Pond 1 1 X
4/11/2022 7:25 X Eff-OC-la 1 1 X
4/11/2022 7:25 X Eff-OC-2a 1 1 X
4/11/2022 7:30 X Outfall Grab 1 1 X
4/9/2022 n/a % 6 --Berrairr CAA \9'
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, Page 1
NUMBER(S) (If
DHL Courier Tracking Number
DHL Courier Tracking Number
DHL Courier Tracking
DHL Courier Tracking Number
DATE! TIME RECEIVED BY rmmt sc-,,,Jr.) DATE /TIME
DATE / TIME RECEIVED BY rpm, t .r,,,,,,,o DATE /TIME
LYSIS • •
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Water
Water
Water
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11.
12.
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14.
15
16.
17.
18.
19.
20
* - Requested Turn-Around Time Priority Number Key: 1 = Urgent 2 = Rush 3 = Standard
ANN ARBOR TECHNICAL SERVICES INC
For: Mr. Gage Trendel Pall Corporation 642 South Wagner Road Ann Arbor, MI 48103
290 South Wagner Road Ann Arbor, Michigan 48103 Tel. 734/995-0995 Fax. 734/995-3731 Michigan Laboratory ID: 9604 Wisconsin Laboratory ID: 998321720
Sample Identification: Outfall Grab
Sample Date: 4/9/22 Sample Time: na
Sampled By: Client Laboratory Receipt Date: 4/11/22 Sample Matrix: Water
ATS Project: Pall Corporation Report Date: 4/18/22
ATS SRF: 0411221
Inorganic Analysis Data Summary Sheet
#G001-002
Reporting Limit Analysis Analysis Analyzed
Parameter Method Units Result Date Time By
Metals Analysis
Metals Digestion EPA 200.7 Yes - 4/13/22 10:20 DMS
Total Barium EPA 200.7 mg/L 0.16 0.001 4/14/22 12:24 DMS
Comments All methods reference USEPA methods unless otherwise noted.
na - Indicates not available / not applicable.
XAG001-002.221April Samples\Ballnorg_SRF_041122 rev. 4/18/22
ANN ARBOR 7ECHNICAL SERVICES INC
290 South Wagner Road Ann Arbor, Michigan 48103 Tel. 734/995-0995 Fax. 734/995-3731 Michigan Laboratory ID: 9604 Wisconsin Laboratory ID: 998321720
QC Batch Number: OCINORG0413221
Parameter: Barium (US EPA 200.7)
REPLICATE ANALYSIS
#G001-002
Outfall Grab Matrix Spike 1.8 mg/L 1.8 mg/L 1.8 mg/L 4.3
Quality Assurance / Quality Control Data Summary
ATS Project: Pall Corporation #G001-002
Report Date: 4/18/22
Results of QA Samples run concurrently with project samples
Sample Replicate #1 Replicate #2 Mean Relative Range
(percent)
SPIKES and/or QC CHECK SAMPLES
Sample/Analyte
#G001-002
Known Concentration
Spike Concentration
Analyzed Concentration
Recovery (percent)
Laboratory Fortified Blank <0.001 mg/L 1.6 mg/L 1.7 mg/L 104.1
Outfall Grab Matrix Spike 0.16 mg/L 1.6 mg/L 1.8 mg/L 104.2
Outfall Grab Matrix Spike Duplicate 0.16 mg/L 1.6 mg/L 1.8 mg/L 99.4
BLANK ANALYSIS Sample Analyzed Concentration QC Decision
#G001-002
Laboratory Reagent Blank <0.001 mg/L Acceptable
Comments: Calculations performed prior to rounding.
Control Limits: Recoveries
Laboratory Fortified Blank (85 - 115 %)
Matrix Spike (75 - 125 %)
Relative Range
Replicates ( <20%)
X:\O001-002.221April Samples\Banorg_SRF_041122 rev. 4/18/22
Etf:X-44ft.= Data Transmittal Cover Pogo
Project Noma: Pull Corporation ATS Project Number. 6001.002
AM Ronan Numbor(o): InorAZ i 0404Z21 CIIoM PO Number: 450
project Thla des super, mash, the rowan of wuMr sau., maim! A.M./WW1 4, 202210W ans.] ke 1.4
We candy Name adnanle and. brOlasa.1. bow conaessel m mcortwncs us. ...nes new., sift Mumps., stmassa tar monat and ow Danubian. vain armed unmans assent. In. sum. GYM. Opwanna, Paw s', la .ATO Lam., umraiMIUMPA, wows,* nsweA. MN, aNOC Men* arab* Whine. rawdOrlM Ishainimupon lunout low
(OW an no
Reelplant Mc Trendel
No. of On, iinoloolna cover MMI 18
Preen:
[mil: tum_benaclitealessaFAX ',neon
So. Shata.13 !mad: 1313ILS10301•11ellaMlAtUOCIMUDIC311.1.3e34.1Awawaswestu m.o., FAX Number. 73443,3731
Addl....pc Cody upon le Pons's, Knol,AUIpllosenevalLcans), &Wax.. Um broduQ0MY.P) Knee SPOOduor petrol suou,sA3 don,. rwooda(M•opeinuawmearn. Pala, Sue Pelona cwlers4palltan) Amanda ROMA (seosida IsubaikapaLcam)
Oats: 4/31/22 Signed:
IF YOU DO NOT RECENE ALL PACED OF TOD TRANDIA3174. PLEASE CALL 73400,0901.
I...
5omnle
Samples containing compounds al camer,. Mos limn tfs rata oalibniuo• oarwi ucte clawed sod teasulrxd fa diem compounds. The follows. ample wean diluwd kw 1,4•Dlossue:
a. liawdYVR
MON.
1,0bornIA, Renrent Nlpnkc
Iaus..Y..g...kai..... ,Y=d Q.0 1.14. Tim LRO me lo ompuisce cram.,
non"i:. tI,:.:inntocoponnt
IntrDlel Stnndnrch, Sortoentro • OnanilIodmi
71us Inclbad Mlluu Imenual Sunda. aoly, rot Sump. Wane •landarts an. and seumuaa tames and dos eseeMaixd star wtth du klbmng enapUoem
• Moe
derl1RACY
Lnborn tore Fortified Flinn. ILFIM, PRITAboratory Cnnlrnl Smnelen • Attorney
A 3sterslory fon, Dal Munk (1.31130PR) wraulyMMup.ufnu PA3C,C bac, Tha L1,140PR metdotliceeplams camium... folloymp
• Mine
Maine Solar% And M Rhin Snlbr Aceurncv
A moms spike (MS) and mans ipsie dupt•cals (AM, was analysed m penal' the QA/QC huh. M.VMS1:70 ma the saws, sa es.. esuena with the following extepilues:
• Mae
cza:acatucn,01.1314.
JialL
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0404221
Prepared By: Ann Arbor Tothrtionl Sonekcs. Inc.
200 South Wo)mor Rood See Arbor. MI 40103
PRECISInN
Mnttly Solar end Metrlo Snake PrteltInn
A mattes span (MThand =Ma 'pike duplicate (PASD3was analysed as pad of cheQA/QC bnul. ThM4M4S15% men. gootolonatotonott condo wtth ao fonororgenttotiont
• Nest
7)7a.aZ41.
Mad T. Damp (Quaky Montano Contd..,
Tgullp D. Sumo (Lstoralosy NAY.,
Osele0333A31,w3LDsAu
, AntalL202.2
/Affil II ?Or
I
B O
S
=oar
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: C001-002 Report Date: 4/11/22 SRF / SDG Number(s): 0404221 Client PO Number: 4505179649
rale NORIO IVr
Thls use tom. oppLes le Rho Wanes dwnpk. the wu men. al Ann &bee Techascsl Swim, (5731 m .1.321. and lissuustsd inurla.Me36e 0NQC
Onetarajdf.adIndinn 11,, wen,
I...4 Tata. Awn. Minn
00.001I I 4.11,*•••••din Pad .NM 1,1••••• Wawa
bfl, n thin, 11 I MN. ion W•nwtan, thaws 1,3 ,www. Woe,
-930 01/32 I Iwo* 1.4-3/1•••••,Dt••••• wow
Upon mem sample...en, scheduled Rothe fol.,. ma..
pus,. • 1,4-131auum ROM, Urnant TAT • 3 Snudles • I Marne Suds • I Musa 5,U Dupl. • 1,413Liune RISCPA 16341- Mad. TAT • I Semi.les
notnnte Rectint. eltmln ntClMml, Record.. and finklinn Timm
Samples warn delivered dimedy so ATS by Pali Corpus,. ale!: Samples was real+.with peeper dale of auk* W.. lochs. Sunnis eandidae nod suonnadie, if any. are mbar promoted IA du Itecelp, Nell. of Ihts repart or r din mmnmrw Irdneldual dila sheets. All samples woe peepsad and analyzed wuhln 43 days vgth !Ns fullowlnal extepslonc
00310. .11.i.040011.
...au. in Chemi, boorwlensidlSoeure MS. Ware.. AM 340,10chips, 41.13 UM/MOM Fan 7340.3731
ER IIII
MIINIIIIIIIMINIIIIIIIIIIIII
'Ant IA 1 EEE [III ,
i
'I §
i I
, -
,
=
p
In IIIIIIIIIIIII IIIIIIIRIIIIIIIII
III II II
IIIIIIIIIIRIIIIIIII •lloiiiiiillullIIIIII IIIIIIRIENNIIIIIIIIII IMIOrta
MI li
r
IIIIIIIIIIIIIII
IIIIIIIIIIIIIII
III
Emiasin 11111 lin il - :
pi ii • '
4
z
Boa. Review and Aonnwnt
All ...annul. an dm Keen have bone amended in aceadam.mth..Mares pr.:Aided us the rammed staadsAlbt usesod,u1 weaWunl with deluded proasPoo deseribol Mawr. mudded apenned preoedures (SOPU speed-onto. ATS Loam,. as iyquwed by MEP&AD gar am paw sad nousuaniens reviewed le enure complus. with the allow rekrenced SOP's ssulprosen specifleasord. Is rata.. dace confonn loan laboratory, Quaky Meows. CbuIlly Control Musa..
A magi. QNQC I...LW um mon dun 20 mammies excluding nwelind kalsoks (MD, LAD, fuddled Math (RS, MUM, flume spikes (MS, SPX), sal duplIcsass whether se.. 040, NPR OUP, DUP, SR,
ys
O S
>i yy
polo Ounlifitotirtnn.SnteldnItionn. and TtchnItol Narrstion
Thuttm vatlavvub. otv .nm
- the aelibrulat, nal. the mclka -rr taken am sampls dalunon
- samewlesslan reueneed bemuse dm libenuory.turnau detesuilned Meth. Duralue WM, (MDLYUnill Of Detection (LOD, .3 the PracInsl0usAldnunn MU.. Of QuuMnelwn 0401 VolDLY- concetunsine repots. brow doe IstoubstyAstrunisau Method Oelection Lund (MDLYLInut
Quanlitstion (1001 mod die IALNOWn. Stem/ To Mum Rom MAO et aunnlelmmelY IOU -tr - duly* oxicentrslial anclhod blank exceeds reputing NMI
-aeolyin not detscanaboye MOL / L0D -•"_IMinln✓mlylehu s33Pase1M heta maPPle WY. QM0C wl,tnl b. "M' -White mutt Inserfaanes '7- lobo. ion naiad:ow= IS and 30,cotpunce RJR. - ltd.. ion foneasouiels 10, ancepusice window and result It Ms Reporwd
A an& QA/QC bath a dentod on on num wn201ompl0 ottludont Mahal taaso IMO. LIM, Med. blob Ills. tn. LCS), own% nono(LF14. MS. SKI. not 4.05tno, MoolItt DM DUP..,
pole Petlerrable.
Medals peeks, costilindes • Lovell' primp; edict der repeat package% (Loul 1,14.1 TV DV% EPA RS HDO1 mu nubble upset num. Than wen we haulm, dui unwary shoal generated toed,. pro=
5atenlr AnahNt.
1.50inoono,tudonliBICLIdS1 Srdldu notononhottl by ootoonad top OCALS in oaconnoco wad USDA method 1634 (Vela. Mime Compounds by hoops DIkulee Om Chronwinuraphy - Mass Spectrorneuy3 An Waal eallbsollon WM al leant... was used b gum.. 1.4.11401•Ae. Semple. woe tenoned lo prtuset spunk reporting ling. Swedes wire
Anomalies Nark,
E I-
O
` m
.%Z • 5
I
3
LIE
1
oy
is
4,41 #.1L E-Z-r.
Data Transmittal Cover Pape
Prop:. Nome: Pall Corporation
ATS Project Rumba,: 0001.002
ATS Report Nurnbor(a):
1 "S 0 * 71-701 4" '21Cita nt PO Number. 4
Project Douription: ThO data report...3bn . mums or ew.ta awn PC. rood.. by ATS on April
S. 2.022 m bo andyzed for 1, Deno.
We wet/ Out Iv ona,•• lug me ftport So. Per pro.toot
tt piletemodOsneua wt monad, w we.naaaa PI,OrpOodpio0.0wasas.ne.a A•uosien
Oponnny Preco.e• spout° to the ATS tastorum at rso..1 Iry IRICSA. to oratorpilota •P•61.. InlemerNo ntoectio,r. ...al .1 P. 0001 nsposat Ll.a•
ote.boely rood on nadat..scon..lnoolcsoess,re wear-awed roan,. wonsola neve open
Roelolent Nis Gana Trandal
PAX Number.
No. of Pape* (Including <owe S., 20
0.12P tignoltbot.00rn
From: S.Ar.tutt ,cf4O3AirArtoTc,IrKalSclYrx: orD
Srdata.pstitaill.soP FAX Num.: Tae-005-3731
Aebiltlonal Wane: f mand to. Panomon... (Moth_eottemcalInpolcoml, bale. An rpm bonotaponcom)
lOdlo Sbohooar hatngsnoon(ahonpoeen). r000dollnlvapeeoeoraccon. Peters, Sue Peen Noe patoreapatcon,
,rods habeas (amarela mobonadOponoom)
Dow 4/1102 Signed:
If YOU DO NOT RECEIVE ALL PAGES OF THIS TRANSMITTAL PLEASE CALL /3400,00,5,
bwssed•O ma* rows.*
mdtpfin. .po......o. ,....P.sosoronnssolums.....troNo.lisa so* ram p
Kv..opa02
4°
3
C
p
I
3
ANN ARBOR TF.NICAL SERVICES NC
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0405221
Prepared By: Ann Arbor Technical Service ,
290 South Wagon,. Rood
Ann Arbor, MI 48103
11
3
"4-{(t
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: G001-002 Report Date: 4/1122 SRF / SDC Number(s): 0405221 Client PO Number: 4505179649
Cote Nnrrn1Ivc Summnry
.(I;IN )or. norluvo4/501,
ztzttl: folloeva7grrs on: st Ana Mar Teclmaal Sorel.; Inc.
Itaaratt
kmt 7wT4Lt_mn"e
Arno., 41V12
aeons M.
paraMPpl eaUp
SP 4/4),
PreOe-ls ulM e•Pls. welt(_
PreOft-S. ova Onset o.
1.1.11d 411.72 ft on43,1 1,4iNPsw WPn
afW.SIs 0.177
ufM MAL I .f.fhwon• w:w4,40T enrol
than wool sonata were adalaled fur the re:lomat; analyse.
ANL,. the-,cculSatmlo
• I...Daum rUSP.PA US, - tb,at TAT • S...
• I,I.O.onsas fUSIIPA Ia=41-Yer.Wd TAT • • Sneaks • I Amur. Spree•I tastro.Spko ptrylmra
cymni, tt,•crlor, elmln of Cuatnolv Rernrth. and I Inbline
Samolcs were delivard directly to ATS by Pall Cuporataoath Somplo were 'ceased wIN papa damn of
custody mord. metaled Sample conatilleo and lemmata, If any, ue taker prmaord M Pa 'Sample Rouge
section of Nis moon. mdse commons on Mind.] data thou. All wales were prepared and analr-nd wain
43 days lath the follow..., <seepage,:
0011.0 ....010UZIlea
200 Soon Wo r 2.7trAtter.11467.4107 " Te173."=Eaa 7 31.7..173I
3
3
I
Pr. Resit"' p04 A nn rnvo
All datecomalned Is this report love ban ',mud occordenpp wren ,osplcIPM PsP00. 0 in 0..... 00. 1.1apeapl tost nielod, and are corms., wasp dented mow.o desert. on • wrmen standard oPerabnC procedures (SON, specific to the ATS Laboratory. as mowed by L.IP.PA. Mean are par and numeetneat
taviorod to anurc calsolunco rdlt eve above refooneol SOP'. um pro, ypeclinntionn. m ad.houn, all data
wawa, 10 the Iowa/ay, Peelny Aso.. / Owls, Control Mame,.
('ZVAZ.1:::::`,Z(Irs',===:,Z"L't.bytte.4;:gg:=V." pot, SperlficotInn, and Tech n km! Norratir,
The fel:Naos an qualdler ducnottons Nu rosy be tool throur.00t eau SOO and us pros.. with Oulz
auce....ed ma. on etch SIX lawn o sporopnue.
• - c.c.s Ne calaration ru:, of No method 13. - mull when from sample &lawn
• -r -concentmlue. ',mud between the labonnoryAnsounantdesonened Method Oetecnon Limit (MDLyll.330 Of Duectan (Lou). and the Practical ..anhotios Orponotanoo
100) - conceandson ...not below the labonanynna.nent htestad Detection Limit NOI,Lonic
Of Ca...aloe (1.0(?) and the instrumenl Signal To None Num (WWI appnulnately
'0' - enalac eonceinranao nand Wok tamed. topmast broil - annlyte rote...tot above MOL / LOD
- walicaleanzelyte intsednd b.. of us* Qn/QC adastea me. wafer..
- uskalot rallo between IS and 30 54, accentanoe wad..
adleal. an rata aural& 30,3coepunee and ren, la Na Repotted
A sl am OM:SC.11 ft./mod.. more dun 20 samples culud, method Mani:A(54, LAU), (unified b.>
OIS ICS, nutria cod,. (LPN, /..910). and Juptaales ...raga. or native (LPMD, alS0,14
OUP, DUP, LR).
Dam Oeliverphim
Thu nave peeks. Cans.. • 1.4.1 II package, other data report pods, (Level I. Lc.I N OVP, IPA RS ROD)
are oralLable upon ream.. Tbsn was sat...coy data summary the. genera.. for Nu project
. /unnir Anal.
09100 method 142ANohdle Oriente Conaouncla by Isotope Dilution GM Ctrommoulaby - Alan Spectrometry) An
mwa callbodba wiN least live levels wsa tool to quantitate I.e.Dat.tans. Samples were reputed to pro,
spectra repMmgbmrLL Sampin P.m ft,orted
otnenaGnt Nonni: 0,214o1r-P0,0410=11..
.1
AN
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AL
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RV
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.
AN
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RB
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RV
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.
AN
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.
-114111011,,,-61:13.171=211
QUALITY ASSURANCE I QUALITY CONTROL SUL. VARY
UBORAIORY ACCURACY SUM VARY
10,41 USEPALU • OWC Ba.N.rar. CC040.5221 630 .1,121 Ita001.1Jato. 033103222 /100010ar 41138/22
taborrl, P.a. RUM (LF8)/ taboirsbry Control Sample (LC S)I OnAleing 1,161,on PM Amin, (OPR)
Iur up. I Arvo coo I my...* korms.ars 810.1•12 8401,19 081011 1.•41s..
Ev- z-541;417;;;;:a;—
1 - 1,=1=1=.-.4-1-1=-41 L. I. I - I tam 01, 80 01581 set Me IN 10 111
-1111151- ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANC E/ QUALITY CONTROL SLAV VARY
LABORATORY ACCURACY SUM VA RY
aMnaT MU, 301
o..0C Sr. Rear C0340.312:21 .3 C.0.221
0321.128 Fnct Des 1.1.022
11.1. SOH (MS)
I L.) irro• o I Amrskeaki P.r.hurra or. 0.2it4r3 Wt.@ 4610
02041041.
-AWL
artat US0,1131
CAOC Pr. our.: Want
Pcfal Kerr, 0:01.0.22 8,0.(ler 4.1.222
ILI. Spit. ChrpReate (USD)
1 1 - 1.4=-.1=1=-1,„1-(=,1 - V.:U.S.> 041.2:82 4441 1.0aur el. 6.2 .0 O 1D
I — ICI A.a 1=1 — — — I — 1 Ma sat Ma la 08.1
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONI ROL SUL, VARY
UtIORATORY ACCURACY SUM VARY
ANN ARBOR TECHNICAL SERVICES, INC.
UA UTY ASSURANCE I QUALITY CONTROL SLAV VARY
LABORATORY PRECISION SUUVARY
1.0811,1121 CV% r .3 Pa.016,E, G03162222 Rear116. 6,112.02
U.strtx Sptko (US) I IbUtt Sp))) WOW) (USD)
.1a,r. 0 610ta... WAIL, .4111 tar 1.681, 4.3 4.2. 1.11 1 &Oars
I,•• Cvv AL,
E arc
CE
11
eV
AO& L'.-Ettc. CHAP) OF CUSTODY RECORD
%TY ••••••ft. rlZe,a,,, w t S“ ••• ••••1
fryl-61Domi L; Ar0 -ip-5SIS r,25,01)n...,.3.,.,1,61. -- - IiroheafrPs•ar”
0.
Wt. 1.06.A112. GOG /1:84r. 0308.362421 SOS mint
woman Rao, Dar 41.322
ubontoy Rose. stint NMI (41.)
I la 4,00 lAnas• fru IA., Tyr korai Mr,* Oa I r.. tar lip.. I Yaw Gramm Uri ar.brOasur Uri I.P.61•671 Una. waa 1.0am Marti OS1
73S
rcgal to 1131) 0
4:WV GEL
x K x
"-53$ a Alf S31
nr -Eal./1, 2A S
L,5
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONTROL SUL, VARY
LABORATORY BEAUX SU \WARY
4i44111-,-ATZ=O:= Data HMO", and ADM..,
Data Transmittal Cover Pogo
Project Remo: Poll Corporation
ATS Project Number. G001-002
ATS Report Number(.):
41 "5 0 51 79647." "21CliOnt PO Number:
Project DoatriptiOn: Inc nokra r000n mood. Ion moth of S wale, aanao,ccoNed by ATS on AOt nob.. le, IA 0a m.
Wow" WI lb* we. ono,. arm o ptwantars.00nmam
lan0.4 oat manpp ad w eandslent.$0.1•1•41 aourrooa in • ...son OlArdeal OporotopPotc.eare moo. io No AT* leasakom. •• mot by USW", iabonaory
oat ',b oor..Nowa tab. .poled, no.0 wtlw dna ...W.A.... ...Po mu.. end noogro woo 11.1111"....1
R.... Mr. Cops Om.
No. or Popes (India.. cow pp): 17
From:
Ensolt Ogio_POOSIOISOIACOM
FAX Number.
loan 9.nadld Coos: ...51.141.1.111.1,C2MAISM.1.22M
734.0.3731
Addmowl Amman Copy moon to Po/union... polin lionorooneipollcong. ad. Jim girrijorodoOPoiloo.) .aortouwerhoriocernI. woodoni3Oparallonacom. Peters. Sus Polon lu
Amanda tube. (a.m. looborto0,poLCOrn)
Mao: 4/11= Signed:
IF YOU ISO NOT RECEIVE ALL PACES OF TH. PONS/ARTA, PLEASE CALL 114-00,0006.
1.....yeks • ••••••1 War ccoodem, • .maw on.** er oonboof me*. 11,.....010.101.UW.O.
gnomic Oliotio.•
Savo,le anbkmg comp000ds si co...roos Wow lh. Wool od.nago .rve wale 44.4 and towlyaid far
sloe .npaoola The folloo.c.moka
• Rul Anat..=
Jo...Mr, !Arvind Blank,
A Woo., nagail monk Pia) was anal.. as port of Oa PAPC bads Ow LAN met .c aorosarco.lario "Ms. fol... amp..
• No.
Infernal Stanrinrch smISurrountri - OuantltallnQ
no robed n., ....st .thorl . Z ronZto.. ..:.:16nneenns ...ono tondo& .not nna mown :sus mot.
• N..
ACCURACY
Jmbnralnry FortifIrd Ithinks fLFItIOPIDlaborneorr Con:rnl Samnien - Accornev
A I.xsoory hoe. blank O.FOgPNlwrodyodm Poo or. OARX Tt. e....nee crwswb. bationng =spoor.
. No.
Mobil Seiko, and MOM< Selke Duni:met -Accoracv
A roma sp. OAS, ad mans oaoya.. rat orua QA, Qc bash nen... mt..: won, aacpa.aeae.wiu..a following
I *WNW 1 IN I
Otel<03110,040•StlAs
...N. I
ORGANIC ANALYSIS 1,4-Dioxane by GC/MS
USEPA 1624
ATS Project Number:0001-002.22
ATS SDG: 0406221
Prepared By: Ann Arbor Technical Services Inc.
290 South Wagner Road
Ann ArbordA I 48101
PRECISION
MACH, Rollie and Mxtris Solke Dnaliellten • POT id,
Amonour. NS) sod = spilit„doplkou (MSD) woo sealyriA as pm, of .QAMC boo. The NISRASOis
mei!. To d. occripla mien fellow. compile. ..
Mo,. Oolong (QuAly Mawr. Coonh.ol)
Philip U. Samoo 0.4.nowy Lam./
GOOI.L.12..0,C4121.k.
FAO...22
/Anal 11 i922
AWL
B
S
O
LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: C001-002
Report Date: 4111/22
SAE / SDC Number(s): 0406221
Client PO Number: 4505179649
case Nam.. Nom.,
TAW ow amt. looks to J. kllowp3 nooks Pow. mai. r Aso Arbor Toc.losi Saw. I. (ATS) on 4/.22..4.o.alisil obiatoopeddo OrVOCI
orn,laivoloWnviacia. Norninial Tun Amon:Moo AaMla
Rorn-, onoz OW., MI
Ned PIN 46712 1.11.10 'Mao una WN
4.7 Wow
ro.cr-tt ORM Ilrmnl Wen
Own.. 4.2 to.r1.••• Wig
Up. nrcaino Loran.a wens labodulod k.11c follow as sembses.
&nit tbadassflamont
• ',Daum fUSLI, lo., -11..a TAT • S Ilrke • I M.o.. Dooliale
tiortiMe Rtrrint. Cnnin at ColInOV Rm... and !told' no Timm
Sopa. on. dr/lowed Okada to ATS by Poll Coo... oraff. Sonvilas woe ...rod with,. dinio of custody Iwo. included. Somploorodloon and anon... If ony. ano MO. prescnbrd In doo •Samplo Rcoclpr limbo °ratio oeport or . doom on IMMOal data accts. All InOtplin VIVO prorated and anal.. att. AS "
N ... I. M fotkriona outgun.
0001•014.1.1,9,0LIN.Y4
tladrsnom CAN.. d. 293 ScsatiWagworliost Ann Artot Lhasa. FlaCO 1117WROOOS Fax OIASSJ731
HM IM
I!
1 41i ,I /111 1
I
I ii i41in
I ;
110,1 1 i 1 ; s s gi 1
I l 3333).., L I s_ 7 -- - - - - -
I 1 -- w^6.—
1 i I I Elf Lg.
i il
IT I
C4.„.
, 4 ; 65a
I I I ii i I 1 I Ii ii
i hl-
\-5
2
TI I
If
Ii
- - • - .„2t!!
;,...,,,,,,...1. li.............A
Is ITo
--• -------- .. . 3 ,,.,,.
P
5;
All due moo.. this .v• boa gosenrica iosoconleace wIN guidcluicsprov.d in gor rokromat mochool.sail aro rondos with... poi... doom. u •wriaco.ndard ono..
promhires (SOP) ap0C4. In MATS 1..411101,11.....bY MIO.Ved 10 engUro Compilanix Mtd. oho Wow M.15On and pope, axone... In Damon. alldW coofoon lo rho laboratory, Qoalip Assonove /Onolioy Con.: Meow.
A sin& QAIQC both r dem* ultimo. than SS amp. cank.ro roc.. blinks PAP LUX foto. Wan. RAS. SOO. and donlan....or pad. woo RASO SPX DUP. DUP. LIO
Bala OunlMen non, Sneci nentInn, and Technical Snrrntina
Ito OM.. aro g m.0odsapltoa aW maybe rod Ihroughota Oda SOO and an presaged.. Ono summed sorroka in soh SIX woo. aa aporopr.o.
• FE. -caccob. calibration rang. of . mead • "Ir Won from sample dilWico • -r -corresneratIoncapotudbefteews labonaoryfroinonsni damn.. Mohod Onaction
CADWIAnia Of Doom. ODD, and J. PMkel Quanta.. Loon (VOLVO.. Orido.Otabon
0.0/ . 11ADL• -.woo.. repo. Woo. bbontorygnaninant Method Doo.on Of QLLIIIIIMISOR (L001 tad be Sig. To No. RAP (SYR, of soproonvidy Id I
- onvontrabon in coolant WM .crods sporting law 'U" -molt'. not dearoacil obove SOL / LOD •••• wan. onalyto .cceded taildi a...Flo ...lac •M• - inaab moula 'Y"-bdiena ion ratio lo.o.io IS sod 30 %amp.. window -Mr- node,.. Ion rabo ou.k. worn.. ...sal nava NS. Rao..
A morale QAJOC boob a dormant as an mama Ow sake random ot.hoil blanks (MP Lan, faunal b.,. On. LED. La). nom op., (UM. MS. DUP, DUP, Lit,
Data Dr ll, croales
• ow, am R5 IDD) ale aviulablo open rural Tboo woo no bank,/ data wrn, ..s gouge for Mb pion.
;;ample Anodyne
1.010.tataaillabsoLCCOCO: Sonolo won analyad by pago ao. aspOUMSk sew.. oe,pA
meNed Orolobla Or.. Como.. by Isogon., Cilloanoo Goo Cloonoinpophy - Maas Soorawrisoryr. An mood ...on ad. a. Ia. No awls tau ot.d In quo.. I.4•Dooxano. Untoda woo report. to project spalOt reporwo langs. San"la win nipootod ao raga.
Awash. Nese,
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Data Transmittal Covor Page
Profs. Marna, Pall Corporation
ATS ProJact Number, 0001.002
ATS ROport MUntisarD0I 10°,01'6_0402221 Cllant PO MUMMY: 4505179640
prejout Opupeptipp; lees dela to, Nee. lha rmrg otSamer sample. emaNail N ATS 7,22 la be ansNad ler 1,4 ilk*.
W • cone,. O. ouoipIe a...los...mot.. ern...ow In ,.par. mnpwra. pas. in ea *masa *Sad ag an raAWm all** mor.mmes mina, m • mina.
Owes, Proua.e apcSla ID MATS Lseantion...../Insa try trx,.. Later*Mume.u. CO, tend OACCIlau.lon •••• Isom, woo /*quest Wilms
DmIalleat Mr. C., 'Iran.
FAX Num,:
No. al P•poto IlndUOICIO mmrp0.1: ti
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M0IUortal \Coup. Cop/ mood MC Potter,. Keen Parb_paIlmemeliPaLauut. Oracle. lm llaullIMSPubranN Kim Dunham, Meirarteuar...rmoornt, maossMeocoeralimurotn. Pe,. Sue Pon
Nnenclo leoWll, remerde ImbetaMpallcoml
Data; W11/72 3Mnedt
IF YOU DO NOT RECEIVE ALL PAOES OF 'Dili TRANSLUR, PLEASE CALL 73.055-0(30
1...arbII• ...a soy in....I..noosularoory• ram It% mon no to...wade...A
Mirerstoro.mlai. cameo.. I• I1,w hr l•.a.w0e womn
3
ORGANIC ANALYSIS 1,4-Dioxane by GC/MS
USEPA 1624
ATS Project Number: 0001-002.22
ATS SDG: 0407221
Prepared By: Ann At Tethriltai Service; Ix
290 South Wagner Road Ann Arbor, Mt 48103
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LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: C001.002 Report Dote: 4/11/22 SRP / SDG Number(s): 0407221 Client PO Number: 4503179649
erg NaMIllYr Sunman,
MN ease ourolroo avpSu b tbrollarriag 5 lamp.. via. =raved M Asa Arbor Tedmleel Soma,. (ATS) On 417/.. ed aurevared meele.specille QA/DC,
CfaitgaeLlotamillmme
q•1.0 ref Ile ya m
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Us. meals «unpin woes... kJ Mr lig MUowing analyse..
IrTll
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aalbaLs DasteuaiStmels. • I,443imme (DSO, Urtiea TAT • 5 Slagle.. Nana 3.• • IMAM SplLe OuplIon.
I
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Mt dela *mewed in Ulna. have beta mammal 1,1 accordance ...nil pulelim pro.. in Lk cereencal eroded le meth.* end me rondo. rim drawled placed, Plumbed m • wrinea mum. avers., prooralerca (SON) emulIc la ih. ATS Loborsiory,regoIrof hf =PA. All deg ere peer mad armament temewal co snare ragekente* dm Maim reamed SOP.. end PuIPMeemirlautaaa adalnani mat, so Outlay Amaral. /Om* Crewel MsmgIL
• I:IAIOC be. ...A e, ea more ilion2Cmamek• meludins nelbl biaeim (44 Lan), (eM.4 blab UMLFII. La), mote cam (MS, MIK, arid dmillom siiktbrr se. or maw (M50, SPX DIJI, DUI, LP).
if
11
pm. OH alifiratione. Sneelncntinn, and TetbnlYal
The ...lee, an queltDa drial5Lem tan may be awl 00000000.WsSDO and ere paisealwati their u.4004 same.. in each SDO e. appropriate,
• - sum. theeldwedontemeserate method • `TY- mall tam fienmangle Mutton • -eanGentretlaa repotted bcPram the lebotmetyPearaeneat clesamlned Method IldecInn lama
(MDLyLlaui ...Drum (LOD, aed the Pramual Queelltedos (POLYLusuOrClumaguae (LW: ▪ - mamas, 'evened lebomoryloommothIctlecd Dc von Ln.MIADLYLimic Or Qualms, (LW, mil. mum, Nalm Neaa
'mime =noon., el method Weak *Ms reporung Dien •LPI melete not argued above MOL / LOD . ...-Indmme a., has aoudad both or sample spec. QNQCoo•Irot limns ▪ - Welke. amnia taierfenace N'-Id.. ma mite bug, IS end 50 14 mar., ine,
era nu out, aeorpu, ardor mad melt b Nor Reputed
A .100 PA/CC 000 .2 deficoda no mere Om to amp. ceded... method 01mtles (140, 1100), Eau. Menlo In LED. LCD, mum mtkes (LEM. MS, SPKLad due,. whether waked or native (MID, MSD, SPX DUP, DUI% LPL
psis noivmslOrt
eemole Rrcelct.thabt ere-moldy Record, 4,4 tielillneTlmo Tim dog pedemornMees • Level n package; otha dale mpon Rama (Level L Level IV DVP, EPA RS EDO, an rentable upen rtgaral Tam* no lunkapy dale memory Mau awc 44tar01.paten.
Samples were Mlle.. dusty to ATS by Poll Capers= Math. Sample. west rend wi0 PraPur UM. a,eagerly regards InMerled. Son* aadilaon en4 enornalls, Keay, ere saber pram,' te Pe ̀ Semple Receipt' maga artha report er la the ousamete as larbyklmild.e. Madre All maglia* ampersand waived yr* 45 drys 01010 Wawa. emeation0
• Noe
O,31.61O.11,64OMiam
la A Efflo* 220 ScutriWMNa RoarL Ara klaw.Ledattal 41(0 T4172411.0045 Fat 734090.373I
gPTRIf Analvele
4-Dimene Annh.1.(CKINar San/plow= enslynd by purge and trap DOM o won:Lao ' ,nth U.SLPA method 16245000103 Organic Campo,. by hemp Dilation Oa. °earn...imply/ - Mess Spain...ay, An galls' calibration... Icest Eve alma web used ia queen, I,4.13.5msta Suns. ram reported le pee, mpaf neporties Maim Somalm was reported es ine-
Arronolior
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ANN FLISCIVIS I GUI-MM./1,
QUALITY ASSURANCE/ QUALITY CONTROL SU M VARY
LABORATORY ACCURACY SUMMARY
1,1.33 USIIPA1Laa cus)C.ssrs•-. Esc. OsUrs AT,. NslOv CCG. iet Pram Mar 4:1‘7,2
Labor., EWA.) RUM (LEIS)/ Labs., Control Sam* (LCS)/0.0olng PeocIsion soul AteuraCy (OPT)
muss:se Losfu as I sTsess.sl......s. I I I
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3.044.733 W.= XXXI I *Ow. XXX ttICI k 1.4 /. IS II,
Lye. LAVAL. CLUXILWLI/rlr OCC,L0SKSI .0 0.7t1t XxvIIWW. G.1.1.72
P.* Drs 4.14.112
Use. Spa* (US)
I LOY,. ID I /././.12031X.X.411•6103.....• OXV73. u.4n 1.4.0.•••
LAILLeeL UEFA CucC OCCRD, M. sots coral
Fss,Des. 311S33
Ustrts SFS...Outs (USD)
•o IA.1I..on XXXI. Owed N. 4. t It l Xx3
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONTROL SUMMARY
LABORATORY ACCURACY SUMMARY
- I - I - I - I 03, COI IX .01. w.1 0/.1
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/ QUALITY CONTROL SUM VARY
LABORATORY ACCURACY S UV VARY
teR111 tax X./ x11 XXXI 1.311../.•
hL
MPS 1124 (AOC Sasssso. occot000ral SCO OsCrat su,susnean CSASSet22 IteX10.1 sm.)
Ustrts Spits (US)/ LW. Spike Dupls. (US D)
I 130.13.01. 1403,30/31.3/13x1WeItay../I GP= x
031.111,.. souses au= us...
113.031 03/ PBX IX X.2 a ID
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALILY CONTROL SW/ VARY
LABORATORY PRECISION SUL, VARY
us I ti., I WA l rrle•41 Iso OA.,I3X31 XXI ./ 1.31 tb 14. 3001. w. tau
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ANN ARBOR TECHNICAL SERVICES, INC.
QUA UT( ASSURANCE / QUALITY CONTROL S UV VARY
LABORATORY BLANK SUMMARY
110.1 LIMA sill LIACICOL•AfieLte: CC0.510711
corm 0,3144.2
PoTIOVt. 41‘12.12
Labs., Reagent clank (USEI) / Uslhosi Blank (MB)
.13w o C. I 1 Pwil LOW I 1.1. I XXX Xxx313-4,,,,tr33.. 3, I 3,01,301 XI IP If 1.403.... 303 11. (.1
. 4,1= '
_441-411- Data Review and APPrevel
Data Transmittal Cover Page
Project Nome: Pall Corporation
ATS Project Number: G001-002
ATS Report Numb:at* inorg_SRF_040.221 Client PO Number. 4505179649
Project Description: Ikea doss moat contains the moults or et odor sant., tocovod by ATS on Apra 0. 2.022 to be analyzed los I A donoa
we odor mat Ma sande asap. ad eta moan tam tom Gadded a •cootans Mood. ..maned a Po mama. modem mon000kana w comm. otostatatoS weroadosdaaadd m •wIlda Mad. Otaardai Pamdam adaY0.w ATO LabanStilaa at Mod. lay OM, tdoreassysata Wow SOP, eat DA. add* , am dam. ...eon ad soda a ad todnowydno was... War aposiikary noted on. ad INN, uaPprsw wondo presovaoca ant Nana tose nand. new Nan
Redolent Mt Cops Monad
tie. et Papas (lode.. *ever ppp 23
From: Sarah
FAX Number:
OkSeLltorskITIONI.COM
CNN.: SION.SIstaNTRUDON$ANDORoMmtklaVdardellFAX Ronda: 734-005-3131
Additional bleaangsa Copy report la Parham, KOMModh.pallonsanitoolcorn). Broad.. OnsbrodoepaLoaml
Kobe StroNdarfogrohaterfblvarvastok r000da0Msopondkoocod Pours. Om Palm (ase.potareakpateaml
Amanda Wham (emu. laabollaNadkdo)
Dad 4/11/23 91$2oad
IF YOU DO NOT RECEIVE ALL PACIES OF THLS TRANSMITTAL. PLEASE GLL 73.-90.005.
tr. 4444 • 4404 Mak, •I• st a•••41411 de •Pem al t aId • y *ha Vo =Osa.nrrbti rand
Satanic Plinth,.
Samples toad, condom& et comenkettontabnee snits.: calibrates, corm odd dilutedand teanalynd dote compound. TN Nile., tamp. ova Coto] fa IA-Diode.
• bed Palen • 11Y,1 Adak • laWavIfIra
• MW-i warm • MW-101 Oa=
j.obantlary Rade.' Plank.
A Waandory rug. blaak arafleod as pm of Me QA/QC bash The Lail ma Oa ...ace wM Wkibnea roaspOong
• Naas
Jetrrnel Slender& end Serroraire
Tha malsod mama Internal Sanded only. net Sindsgabtaw lalsmal sanded emu and monad timm met die dap.. aorta milt the Mow, camphors:
• Nate
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toboratori Fortified Menlo 0.1,11/0PRI I.ntioret0, Control Swale. - Accent,
A laboratory fart,. btu* (LRAM.) WU ...Wyatt as pastor. QA/QC bad. The LEVORR met the Namarao amass wall do Mame. compares:
• Naos
MION't and Meld* Salk, Ditellralee Aecurocy
A amok spa. (IN) and mama spike dads. DASD) vat analysed at parlor Mc 0$40C batch. Me WAND, ma Me dew, soapsuds anent loth Me Tullosang mamma
• Now
0001.12301,01111 ad
1/ 44L—
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number:O001-002.22
ATS SDG: 0408221
Prepared By: Ann Arbor Technical Samoa,
290 South Wa,sner Rand AIM Add, td 148101
yaveisolN
Moldy Spike and Meld, Sallie Duplicate.- Preel.l.
mmemalaba 0.1tind mods dike duplicate NISINwas...4,4.,...ra.ouOmaah. t4soem. ..athpmciOuudcoepusce anima ma, th. lamp mamas.:
• Root
Mot T. Delo. (90. Assaf aom Coordinator,
Philip D. Simon Nabondory Doak,
ONNaknoCrt.maratoa
/A,sdl II 2D0
IANILL:417` S 8
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LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: 0001-002 Report Dote: 4/11/22 SRF / SDC Number(s): 0408221 Client PO Number: 4505179649
Cade Narrative SIIIIIMII,
Thu ur ostradw opal. to Oss Tokamak l l samoks tNe was Neared at Ave Arbor Team.' Sada; IN. IATS, on 4422. awactsted natal-spoon< QA/QC:
,,,r....8. Maalkal. So al• pf I,,Lta,,,,e2m,,,,,,a q. IA.,
444444 44,1
(44.11411 NM UMW 1 411*ma Woo
lad Pad 11127 4.. i...n... wa.
Or,..I. utri, Um. Lords.. Wake
PIT$DC-2• 4,11,1 llama t..3intovr Woes
0.,Se. a .r.en um. I..-P... W.,-INAIS 4///M Ibmaml 140* Wm.
MW-set 4/172 SUmara I 44onast Wear
MW-Tea 4.," Wad IA-11..q Wads
Marla .7111__ ad. IA.Omma Nom
Marl le 4,14 4444,4 1,40444 Min
Isamu. akal tosataa I 4.IIImmo Wan
Upon labial land. way utako00 rot dye folk.. analyse.
/ad. NONIALSURILS • lAdiodae DORM ltdd llama TAT • S ...aka • I 'Alm Sadu • I Maria Sp. Polk.
• ',Osamu DISEPA Sunda TAT • a Sao..
jiemair Reerint. Chitin arrested.. Retort!, end Roblin. TIT,
&rooks woe &lowed dreedy MATS by Pal Corpordoo oNT. Samples ware received wod$ Naar chador custody moods tncludod. Sample e.t.a and anomalies. If soy, another roasted IN die,mple Readpr Kann alba aped MM do memo. ea InstnAsNal au Amts. Ati morale. wan peered eedalabzdwrl0n aSday•wla the follmang
• Rao*
.0140121.01.0•10711Am
ia akauslo,1 f n* low 230 So. War, Road. Alm Artor. Whom 4IE3 TO 73051406 Fax 714/92,373t
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An data waded to Ma INw have hem gmaralaal w eamedrea wear 4puWma madded $n od seaman, standard tea Incthod..od as coodtati old added pada.. ckaaded Me onueo standard Nero, procedural (SON) Noel. to the ATS LaNtratory,./neared by MEM. All dam maw and management reamed to masa oomphance watt the dove alarmed SOP, and roam speaRrations. la damn. al data condos. to the Laboratory, Quad Avalon. / OW. Control Mum..
A soak (MVQC bad Is deRoad as mmore Mao 20 mop. eschtdog mahod blanks (A, LIMN fondled Iambs OrS, LCS), matrix sides SPK), and thulium. abettor spiked or odd OAS, SPX DOT, DO, LS,
Onto ODOUR. ND, SISNUMatkale. and Ted Iltdfld Narration
The Wooing are qualifier deo:maim Mat may Nosed diroughnot am SDO and are predated old Ike mosciarod amok. el each SOO dada as dor *pad.
'E'-acad. the dIllwado range or. meMad •D, meek lam from Notate &korai ":" -691Kaannoll mooned have. the Sabonstoryikommati skieroursol Medd Daemon Lam (PIDLYIkok Of Damon (U305 and do Nankai Quarandon LoolUNDLYbandOTOdaddeam (LOO) IMDL, - mamas. loaded below do khwatarynnsoesnent Naked Dawson t.....oLyu.d ON}Notalaso SLOB and tha irottomost 05.07. Node Rs1W (JT20.1ofappoxmpaoh:0:: 'O• eadaandeo n method bbole exwods midland had lr -.nal,. detected dove &SOL/ LOD
INN.. anal, has exceeded batch or sample speeltk (NA1C contort hods 'M'- ingrates mark soh:Kama "r- ioalutIa len la. barmen IS end 30 t, acceptance ...Saw
- iodates ion am outside 30.seNotonce sand. and molt uNa Reponed
Atingle 04.,Qc bath ee eeee thee to wet. eutotoo msmodbo. ota...).....4ba4a to(OS, LEN LCS),NOts DI, SRK). and MINI. ..dead ',dor 05140. MS, SPX DUP, DUP, LS).
I 8
pain Dellverehle.
TN. data Nelms. Nod.. • LW 1l wham: attack. rePaa Packages (Lev41.4011V ovr. ITA N IMS) are addable upon rarest. That was no N:copy data ammo, Nom generated lee Nada.
Damp. ANNYM•
1.±BitemAaalxoefIT-M1, 8. 40.....eoreet br lanes. dap CIONIS eeeemeoce .oes use, /std. I t,,,VaLgalo °rpm Compatuato by homed 0.4ta Gape...y.0y -gun Spa...7h A. MLR addranem wt. at 'Nat...dam dal to quota. I.dDloome. Sampled was moaned to proMet speak rapotanc Ian. Sampler rem "potted wog,
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QUALITY ASSURANCE / QUALITY CONTROL UNWARY
LABORATORY ACCURACY SUILBIARY
LW. WI. 1223
<ACC 6.42,63 , OCCOW.,332221
$03 0.121
*a123-3, .3140222
0.53 41.7022
LabOcalogy ForBtoll Mont (LFB) / Laboratory C./1/13.We (LCS)/OntaNg Protlabc /usu., (OPR)
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ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/ QUALITY CONTROL SULIVARY
LABORATORY ACCURACY SUILLUJIY
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ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/ QUALITY CONTROL SUUVARY
LABORATORY ACCURACY SUILVARY
m 03
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ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/QUALITY CONTROL SUMMARY
LABORATORY PRECISION SULLVARY
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w.
3•n. ID
000103222 0402201
04002114
VNW
0400040 411.1...1(1.1111,4, ,ugg pa, ...a
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by GC/MS Sh«I
04/0,20221.00.
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MEMEME033 Dala DellVerablm Data Transmittal Cover Page
ProJoct Name: Pall Caporallon
ATS Prole. Number. 0001402
ATS Report Humberto): Inor._SFtf_0411221 Client PO Number. 4505170649
Project porodpdon: llos deb prport poresans. ram. of 1.1p sample. waived by Arr. cm AMI111,322 10 to onerme0 for Itaaan.
Wash Mat ma wars arobsas tor. moon haw men commee In mardamearar marraram omoaad b min sloarbal.Mollma and me meNbNvet,MIMd a Mem oorenbor
OOPa and emart0 mama. ob mamba lor memralon and mot el mmeamomy troommaam. Umm• Woo. rotor on ar Oa noon. M apMableunpbprryorm rd bap Yoe moaternonb Maas. met
Ommtap Pmtr.Omw moo. .ATS Laboreroms. es Mma, torM0CFA uenrrry dom...
RecIplant Mr. Camer Darr. GPM hum nardelitoole. PAX Number
Na al Papas (Including now pg.): 10
P.Or Sarah ...UM [mall: )10M0 StratMerMfoAnataboda,nmeeThemloes com v.. m.o. moaao FM( Number. 711-0PS...1731
Addllionsl Mmeapc Coq, re, he Promo, Kam (Mal moweiruppoiloom1 8.4.. An Om MoNlapatoond Mlie pralrammarrirmogaom). moodefeamperalleamoom P.m Su. Palm Isla polarMapalleorn) Amon. Isabono Mann. habolla.pallaam)
Oaten 4/1002 Stoned:
IF YOU CO NOT RECENE ALL PAGES OF THIS IPAHSSUIT, PLEASE CALL 23441954(615.
Moor.. awl
omnr Botch Slumps
Lobsadacara
A laboratory amen, WA (Lail) two rtstwod rs.640M0C beak Tin LAP mot be marg.. <Maio with to folio.......",
• Nom
Acrouncr
JAhnrotneo Fortified ithinkt (I,FIvolilti ',liberator/ Control Snmtdot - Actor.,
A laboratory wino: WNW (LFB) was ansly.1 a. pan of. 0MQC barb. TM LPN let ...prom alum with. rollorlog amp..
• Nees
Middy Snikm nod Marla Sake Otiollmlm • ?term,
A mama spike (MS) and mein sp. duplicate (MSD) vm.mlyzed:nom of Or QNQC Mich 11. MO/Man art. smote ern olionam. the tallowinaoroPkinm
• Nom
.1.1...,,C4,1•111.11
INORGANIC ANALYSIS
Barium by ICP-AES
USEPA 200.7
ATS Project Number: G001-002.22
ATS SDG: 0411221
Prepared By: Ann Arbor ToMmicial Savicon.
290 South Wooner Road Ann Arbor, Mt 48103
Par:croon:
), aria Stilke and Manly UM,. - Procidon
A mama soda (MS) and mama mike duplicsto (MSC).. may/ad to. pm of Ma ClAn3C trioh.1.a topirdos me Ow amepainoe me min the follow/. campuoiss:
• Nom
ANYT. DelAng (Quality Maumee Coorderatod
Phil. U. Simon (Laboratory Director)
bolioSuO,oraMI
1A.1118.20.
,8801.11.2022
O
8
I
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: C001-002 Report Date: 4/18/22 SRC / SDG Number(s): 0411221 Client PO Number: 4505179649
Car Mural.. SIMON',
lius run ninallre ppllabgw foUOWI. sample lbot ma remnant at Mn Arbor Tochnral MM.. Ina. FATS) on 41122. sod ass000tad minnormak OMOC:
Clant,err •
P.... WM,
Omfall OAlr
Pa,..ord Tara Aramollbar Ambm
nrlwt
Upon mopi samples ran mo:bled foetho followitm snotty:me
blab= • Malls nlprnm Min ITA2[O.7 • I • I flui• Sp... I Mo. Stile . ...I., • I S.,. • I Wan Spibir • I Mena SO....
camnle Reerint.Cbein nrCeueady Rot., and Ilold1118TImeo
Sampla rue delocred ue5e ATS by Poll Comrstion Sampan war roma. mob proper drama( manly records Include, Sample were omen., le • MI of <2 el Ore Mos ormarplcrommt. Sample ...lion sad anomalies. irony,. prom. In ...Semple Reeene roman of tbie report. Altmann. wart papa. oral analysed maul Loa Wt.( lima and In thecorteepondmpamlyilal /who. mat Mr comptloac
• Neer
Ditto Reeks. end Aoarovid
AN dal comalar1 In Ms mama haw bun mormal to month= with widellna provoled In dm nlooral standant at mathad.md as oanantant wilk doodad mokrdeloo Mamba in • Wince abduct wonting peocedums MOM) speci0o is die ATS labomory, tom. by OS 82A. Mill. end ..do mom compliance with dm a.. refaranal SOP, red pro, speerkstrona la W., Pala conk. ado laboratory, Oarbly Manama 1 Quality Con.' Maw..
A rool• QA/PC batch r hand r rm moor Man 20 samara eacturbna anabod Manka (MB, LILOL (MOW blot. LCS)..... sp4es (43.61911. and dupbum M.er mMed om.no )(SD. 52K DUP. 002.11 )
tromoamMumian
no :awn itl,trafiZiVir==''Fe.:aornoni
mom
War
l' ; 5 di!. ; 111111
WO IIIII
iiilla
ir--* ilia
l I igUi
i
a im
,
ii
1
'
i I
I a
— - c.v...
..... ...
7...7. • • • • E,
-.9,_,,I. .., . • - .
lip, -.g a .7.; - • • - r i
ii J
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LI0
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71
...M.P... ...ma • tawl0 Pmbate-rmtmr.m.m0PabarafLeral L Level IV DVIL EPA Its CM as evadable upon rape. Then were no WA.. 44. maw, shaw pnaded for Gin.
Oomole Pronarolln8
Samara war dimned b accontanco rub US EPA method 2007 Pacrtninabon able. and Tao Clemenm. Water and Wm. by ...ratty Oambal Plesnanaturnie eeuAaa SpIC...).
Ana.abet Aunt
• N.,.
Sim.) Anatol',
&maim woo sirlyrid In acconarnmanets US CPA matbal 200.7 (Dream.. or Met. sad Tram 13arreata an WW as Meara by Indoctbaly Coupled PhommAromie I.Mioo Sportnanary). Aa Inalalmhbranorsmith as lean rho lamb was m puma. Indirldual =Pia temp. Was repUted 10 pro, spec. mamma timlb
meal.
Anowofru Nam,:
csmolo Dilutions
Soniales centianr. co:moan, at metawnown Mow the sorl CoMOMOI: mroo vac 8loted rd ratirtyted for MOM amp:Am. Thokilowna Ampus wens dAhtled ice bantam
• None
Anelvilrel On/Dr: Silteslers
celibration WM-ice:ion Method mlitomon vs. vadfled Omagh Ow mat*. of • mld-ln. Neal mlibmbon Yon:Hawn IC, ow.aa at a Ilapancyorrecry vamp.. All sonfintion atan.rda ate the ammo.. ono. rah Ma follomito memo..
• ,,
lnanmuntIbaaks
Low gym:, backgyound Wad demonstrated through be may. of aurnman Monks ot • Mo.. arm. Ire samplea IIrarnall MMsmomnnoc era.. with. meeplarnm I
. None
COSI.11.O4.61,12114.
Dm Bradley
'Rondo( Gar, agape_MorklOpall.coma Sons Mcoday, April 18. 20221:19 PM To: Jan Bred.y Suldoct RE Poll eCOC 4/15/2022
les an Outfall Ora. Wo should call trOuttallGral, iruteadoRtartom too. So no oampodte.
Thanks ler Minh. this te my attention!' assumed the label that was on tt westb way les dooms been labeled. Justkeep everything In line with how Ks ham done .the pad.
gt°4;`,'" "PLY OPERA I IOML AM)) 14 Z. MC:0,42 C. Wagner Road Ann Adraf I j rares 0: 0/0.077.10001 0: 419.787.51411F: 016.077.1)35
From: Bradley oilm.bredleyemnaitortethnkalsoroloos.00mo Sent Monday, ARM IR 2072 1.4 PM TorRendol, Gm. opietrendolVm1Nriono SubRite RS: Pall eCOC 4/15f2022
Me Menage Is From an RateMei Sender TIM me.., mime hem ouleldayourorpenlatam Um mike atematord00
Cu, Ma. OrMaralnp the rayons from last brook. The taldinn sample Iwo sample mimeo/ Barium... aernMe
date of 4/12/12. tt doesn't have an IndicaUon of whether Ws • grab or • composite. Do you want to keep the mote sample name, and Is It a composite et sm./
i nota.d the sample from April 9on was an at hill areb sample
Jim
From: Wen., Gap ougosuwial&uo Net Monday. AMU 18.2022 8:15 AM TO:Soroh Stubblefield o3raHaulddrfeehlf1arnarborledinkahmktommo, Mark Datong 43adatilon(Paonarboottohnloolserdon coup Cc WM Stubble/We/a. StobtOnlieldPannodinymohntralrmirm mg,. Bradley elpithfadlernaaortarborlochnIcalMarbms COM. Subject PM .000 4/15/2022
ll ,
li I.,
• .
g gg
Ru
sh
3 •
Sta
a.r
d
Inorganic Analysis Data Summary Shoot
ESL: mr Quality Assurance / Quality Control
Data Summary
Sopa Trnvol Cerousw•
41110
Semple Identtncialon: armor
',sorra Trod My: caw
Yeteq7acnot Daly' ir.7 Y.,o Net,
A. S",..0. Pell C75,O77,..
.074 Om.. oleo AT3 SAN omits
NW. p• „„,, Peppering LPN,
mat :7„ pmt
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: C001-002 Report Date: 4/18/22 SRF /SDG Number(s): 0.411221 Client PO Number: 4505179649
rue Nerrellve Sammery
This use wrath,' applies re die folk...Stomp. that wee to.lved at Ann Arbor Talitteal Sm., Inc (ATS) ea Pit/22,0W woos. nuerraneeeitic ()NOG
A.:F .... Ante An .1 17 r
en302 enealt
CC &MO Number, OCINORG041322$ ATS Projod: Pall CW(Welion
parameter: roman (US EPA MD., Roo. DAN: 1,02
Ras. of OA Sample run concurrentiradin Prole. aomplea
REPLICATE ANALYSIS Project Name: Pall CorporetIon
o0001.002
Data Transmittal Cover Page ZEZ6COMMEJEZZEBIZEIII
Sample Replicate 01 Replluts 02 Mean Rater.) Range
ATS Project Number: G001-002 ATS Report ...arts):
Client PO Number, 4TO if70R %9""
AG00,0= pr.*, Doen,lotion, The deb moon contains o. cavils of Stonier lune.. ince, ed lye,. on
wow there Wee epee tamat la met 1.0 mon. A0411,022 lo be analyzed for I, Dimano. ORGANIC ANALYSIS 1,4-Dioxane by GC/MS
10. ON: We wary mob Me en,. am/ewe Ice no mood hew lwewenthAlAd ...en. Wei thedefena Weed., USEPA 1624 Mee Mei II Ow hi*. named tea nwtnee...d am opeontontreln dewed vector. rOtiCeibod n•anthem
Soindeed Opernonp Pn.conon, N.V. home All Yeuayne.,w n•II,end b/wCPA Latheekry Oath COP, end °AOC Peonnaon eve end.. Pr ropaclun an, welt al the ',Atha, won !wore bile.
Wel on rte aatertoen edecolcatnt nerece• perm., e.,lw.vy men, tun* been
lon•Irterterliallon 011/1)
noifJ1 eel
Naar.
A
Preorais Defoe.*
annel•Dsta
en.
NI IDS
gre•arril AmaWTW
umnl Mem
Ihren,
Upue Prosier *unpin we scheduled foe Ma rdlowaS anelysoe.
NicrdeLillsorales • r.e...ne OPILPA - Unroo TAT • S Sono:es • ...SP....
LA-Diereee 1..D.esne
1 ii-gtonsiu
Semnle Petrie,. Chain nren•indr Recent, end 1 InIdln, Tlmre
Sompio wee &loved &reedy to ATS by P.M Corponom eta. Srnpo. were Iceelwe with we, elan of mouldy made exhaled. Sen. condition end wawa., deny, re claw piesrmed in rhe `Semple Arse, semen of taus report or In the comments not indtoldual died.. AU camp. wore preen/Ward azialyved within CS days wt. Me following eareporma
WW/I
We. Wen
lava Warr
UnII.111.7.0.00 'Dieu
SPIKES and. OC CHECK SAtIPL£S own
SoerlprolAnalyte ConKc".•=tIon Conc=orlon
00001.0.2 Weeweety lone,* Meek
white an we. 116th
0.4 C.. Mere :ewe theeeee
BLANK ANALYSIS
00001.2 Wrenn., Nem. r Meut -Veal now,. Accept.%
•0 ntd.
anteot nryl
Analyzed Concentration
le met
!recovery (percserl
.1
iO4.7
ee A
..amps Analyzed Concentration OC Oeclelon
RocIplent: Ur, Cog.) Th.. Out: soze co,n PAX Number:
No. of Pagel pnaluding cow, pa.,
Sarah ...Warlord Emelt •re•rap'ewNgllrin,'LA9nArn•TMinICP,7, -• , cram
n••••• O.., ten loam. FAX Number: 734005.3731
ATS Project Number: 0001-002.22 Add.. Yuuse: Copy moan Pertersondkoth Peaces pagers.M.Senst/i....d.0.
Nona Shone., rsabohnuenflAnon..0 S. Petro (Sine P.../P.SsamS ATS SDG: 0411221 Amon., Isabella lama. laabobapoSna.l
Dare: a1 rter Signed:
IF Y. 70 NOT NLCEIVE ALL PAGES OF THIS TRAPCMITTAL PLEASE CALL 734005-OM Comments: Control Unite: oneanna
Prepared By: lebeefeey knead era 1.4.11411 IA•cal. fare [75 OP 14 Arm Arbor Tnchnoc, Sun.:, Inc.
tovaa v•coe.rnivomrr wonerem•con•wronounrroo.•ae•••••.,.............nt.••••.* P.n. run. :SO Sour, WeRncr Road Awed ereyeewneewwa•Ve.ww.wwee AI 1W ce•••e•Ka.,m, • war y *Ow, • Nap.. f•:0,X) Ann Arbor, MI PI I 03
iocoowea.27*,_
pale ReMeW end ADP thWIII
All dare wowined ie dd. report love ban gemmed in vcwdanu will guidelines pip,. the refecrteJ
eiondard teat meMnd, and are consistent wade J.. princedom ow in A Welt. ste, Ael Cew mu:donna(SOP.)',MCnLie AIM Lebocalory. u sognool by USFJ'A. All dote etc peer end m evlcweiw anuic emotion...I the above referenced SOra and pineat anceircatiore. In nihlitien., ell See
oanfnnn ro the laboratory's O..esliry AMM.< /Qtrely Conn. Motiols.
(US. LFU, 1.417, mane splku (AL4. SI'KL ad duerlren wLaber oplked w nave (M5O, SPK DUI•, UUP, LfQ.
Pete On entire nem Smirker., end Tech n reel Herren,
Tito folio...it are moldier deccriptont Jot nosy to used through. this SDO not no Pre.mled suneured remora in each SDG accrion as apeman..
- °muds rho calibrimon range of the method •U•-root taken from sample Silurian
- cononarauon mooned WINK. Mc laborsanryAnstrument determined Method !Mecum lam, NOLYLImal Of DmeNon (IDD), end the hoaxer Goanbiannn Lenin (POLY,. Of Osleatitation
IL00) `MM. — eon:num. reported bekor ihoraturynosmmient Method Detection Una,' (MDLYilenit
Quutlfauen (W0I and r. 'tunnel.. Signal To None Ira. (V1O of eprimuntoldy IO: Inalpro canunaorion in method Monk exceed* RPM,. Inn.
•LF. snolyle mtdcicgcd Above PADL/ LOIS Y..- indicate. snalyte luaaeedd belch of sor,lo specifier:0.'0C connolUmlp
enalna iiitufwence -r - indiceree Ion raw...v. IS ud %sue,. endow
- mike. ion moo outride 30,4 weapon. 0ndmie acid molt re Not Reported
tigal15=i,:=1Z,V,;:1171=-tr:IttztN7.?:s'.T.tr""
fiat: Delluerntilm
This dim pact:ego canna.. • Level II picker,: ocher too mix'', packages Revel I. /cool IV DV, SPA RS EDO) ere available up= mot.. There won no turdcopy data summary deco Ernereted for dm preynes
Sem. Anelvsla
1-1-11inserr-Aislynell1QMS): Snon he rem ruined by nwne and cane °CMS I...enhance with USEPA method l n24 tVolidde Orgamc Compounds by Isotope Dilution Cos Cluninstomprry SPoclroneeNY) An initial calibration with al land five levels woo uNd n qoatintate I,Otozone. Sernplcs woe reported to preout opecIfIc repatung timiu. Semrinuva rcporled .4 rag,
nomulles Nor, • None
oonnea.M.Y.oil
eetheWile.liee,•••Wa.thww.I.epe.“
cernnie Dlbnlnnn
Samples containing enenmonds et ennui..arts show the ',lig ulibrelion curve wee ddiacd se. =rod,. foe those once:node The following samPirauvred,itt. (car ,Thezeci
• Ited l,n1 1/22
Prevent Mon.
A rebore, nape. Musk O.RI1) woo rely . es pen of the QAf.b•tch. 'Frio WI a. Om accept.. alloie with. fellow, ceprptlooep
!menu.. Steed ergin and Surrecere. - 0 ilentlrefinn
Thu Mahrld risiluesw,In:etzlLiads.rd, =, ,:t ,Serropues. Internal tontlirds vent and fewmon Unwired the
• None "
AretioAry
1,enn rem, Fortified Tile. (1,FIVOPRI i nnentirern Centre] Sinnott., men
A redo., a..., Wank oximarith...../.... es. ....WC b.... weeptancn money. Jo Nano% eseeptrone
• None
Pletrly Seine, end Matrix Spine Penllentel - ACCIrror,
1 d.r .:Prk. NS) end nutt=tdzIra(ASD)soas anslyted as min ago QA/QC botch. MSAiSON eaPtPticns,
00.03123.
Merrix SnIkr end Merril SPU. DrIPliThres -Perching
A mum unlit DAS) and mono mike dunk.. (tat)) was 'only.] 64, of Ile OA, OC kuao The MSAISD, nut the pieciuon accept.. antenna. Ms fol.ving amnons:
• None
hterieT.DeLeen (Quality Noumea Co00...1
c . 7 D,
Philip IL Simon (Labor., Med*,
0011.0e1..04,112erew
. `r=
.
i
I P
.P.
10Y
...1
.1....0
tCO
Z
QUALITY ASSURANCE / QUALITY CONTROL SUMMARY
LABORATORY ACCURACY SIN VARY
1.11A 104
0 1.0C OCOACONT22,
W6 NITS.
P-4•211,44, 6N.0222
PAro10u. 41.1222
WOW Sp. OM
tuu....esp.A.
x
L. L.. (.402:1.41.0 1.41.9 VI.. /3
I - I :.-.1=I-1-Izz41 - I - I - I .41.1 ULF eta Na la
ANN ARBOR TECHNICAL SERVICES, INC.
otmury AS SURMW E I QUALITY CONTROL SU VVARY
LABORATORY ACCURACY SLIVVARY
PAros MESA WM
0.1.C. EV41 1,..or OCC.481124
Ri C.1.21
1.1402.12
.00 .101.
Whit Sp. Chiseksle (LISD)
I us ...se IAP.1emen so+ 41.1.14, W.= 1.4 1,0••••• - I — 1
Issim'ii'kt
.61.1 C14, II/
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONTROL SUPVARY
LABORATORY PRECISION SUPLIARY
Usu. ICU
OM% 6.02rter. 0001.,01211
SJO 11141
0.111 44
F.P.4.16 4/11.ffit
Ruble SOU On)/ Ms. Spite MOW., (USD)
I 'A., I kr.. I 11.• I MD I w I 0a.
010111.1103 11..11
Nv.R. 1.4
j
Fc
.51, nv
t V IN •-•• 131
0 , 11 42.1 - 1
... I — It 4.2=2
4.1.=
asIS=1
41,154
129
7.6
14
;ill 1
3 E
• Requseitd Turns. ra nelems Madly Numbs, K, 1 • Russet 2 Rush Se Mmes.
si
5
13
1
CI
rj;
l
ANN ARBOR TECHNICAL SERVICES, INC.
SWAM ASSURANCE /QUALITY countot.SUMARY
LABORATORY SUNK SUMMARY
1
WLPA •
1114.5.=0. -.• CCCORG:11122I
U. f.41141
P.c.farc aser_au
laborabsy Reagent SUM ORM/ elsthod Stunk (MB)
Imo,. se. Ism. rs.lussuel CAS ., 11..r. I 66.11......e1.11144.,...mint 0.14.1122 tall= nee. 1,101..• .6 UN 041
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONTROL SU., WRY
LABORATORY ACCURACY SU LI VARY
VKaa 1.64.A1421
00.1.41141
U. CA11211
C101044
tr122/2
Labotelay Festned Stank MS)/ Laboratory C0/11/01Ssenp. (LCS)/Ontioang Penis.. end Ames, (OPR)
Isms. .leuhees, .leures us, aweless se. = Rau .Kea
I - 1,4:r-4= - I - 14441 fgt. 4.4.1. 11r W u 11
1 4- 1 4 0j iLi,_
LI:=011311 Polo Review and Antlanotd Snod, Iblutinno
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number:0001-002.22
ATS SDG: 0412221
LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: 0001-002
Report Date: 4/18/22 SRF / SDG Number(u): 0412221
Client PO Number: 4505179649
Cr. Narrative SsittlIdar,
Dos ma 11•17.11., &nabob, tiro following ...pka dun woe dashed as Nos Arbor Takeo...vices Inc. (ATS)a.,02/22, anal soaoclalot atartauP.S. 0,100
Os. Inant• /Ono. .04,
Oinroll ml Rot hie
ranc.2.
OW.07. MW-I lit
ul /0:
us2RZ
erl IRS
4n Ira VI ICS 4/10/3
d7
Tana Aroona TMw
shorn
tam.
Itmo shawl UT.
M1,4.4
Swann.
Upon merit vamp. were achattakd for do following saaly.
drub. blabaddStaudn • ,A-0...000PA Ws. TAT • S Suroln • 114s. 5.41 • I Mom Spas P.n.
• l...4kosaa CUM, 1420- doodad TAT • d.b.a.
Wo LWorm
Warn Won
Warn
WwM Won
I ulnas. IA-Nwn•
I,40inotor
Ad dun consaml le NW upon low bons gonnaal la mno.. on. guidelines anwukd in Lb. Warmed auWN ou embed, atut are amiss. anduktalkd pracadide. Mot. in • *Mat so.. mem. Ploordwa.(SOPs) goggle so 'MATS Lab..., as took. by MU, M Poo and senµnoml revitavd to more compluncc with . micro reformed SOrs and peojcatmedlooloau le WM.. an data uniform at the laboratory's Q.. Anurar. / Coal, Coobal • Rod noulanSir.
A redid 0 , 0C touir o aorous r no on. don SO ossnplca nod. IMO. 0dll. lAU1.faroflWbkcte(IIS. LH, LCS), nom spike. (MS, SPK), and dupl.. whalbsrmluid or Eat. 0.1SD. II, DM tit, j.ohorntory Rea.. Manko
Santa. oontoIrdnd caonp000ds at mamma.. above the Waal <Libra. corm woo diluted and nuaalysol fa Noy aumlrW Tbr Collow.a utopias wen diluted fa 1,4).ane:
Prat. 0onliclardlona. Snocificennno. and TtOhn Red Narration
The following ate godlike Mao.. dud noy ba used throve. Gs MO and an prooskof with thew a.m. ramp. in mt. Slur moon as racoon.
cam. Ito contention range of do =Jo! "D"-• mob wk. In. urn. 04.a
• "Y-tmwo.rgrm reported knivon labonuoryftrognunad Mar.. Motod Onternaa Limit 0d0IXLInal Of DOM. 0.0D, sof Na Hooka, Quodibuion Loot IPS,Lyttinit Of 0tiondauo•
•15ADI, - ooncranall. nip. Mow the lobotolorynoatrunscal Medod Debullon Land 0.4DLYI..ne Mum.. (100) and Oa inonment Snout To Nona Rob (SNI0oforsommoiS InI "Ir rouble cancan. lion in mhad blank npsning tuna
an dakoloS kora see
anal, hos eaneduf bath. amok opecdic QA/P0oonloot idols i• - end.. manta NMI. ran
1-- I.. Ion bean. IS and Wralaw "NW. - ko Dols. 30, a weionac soolow out molt n Na Sao..
sleek QAJQC ba. to ...as ao moca than 20 musks esekdias resod blanks CM. LAB, fond. Moth (K., MS), InalhS took. (um, MS, SPAT, mad Just.. wbador spinal to anti. RFM17), MSD, SCR DUP, DI, Lk,
pere nolloarahlip
Tw dm rodd.....• • lo.t: ri news. Mr.! Li.. N DV1, ore ...biz upon req.. TA.uctero h.., J. moron, do.. patented Walla
Sam,* An.volt
Somme Receipt. (NMI or Cottody Record, owl HoMlne Timm LtbaucteAcoMilatatabl: Mockn woocoUvot by P.P. hap 00744 in occonlan. wall MUM enahod io2A(Vcdotikdpau Compoon. by Ago. Mot. Or Chrotnotognauy - M.S....A A.
Samples way tkUnvad thready to ATS by Pa0 Corpondon .R. Sono. were loc.... proper.. or we. ea... rub at keg five loses vwu tn. la qua.. I,Dimac Sop. won reported wormer malady moods tack.. Sample condition and anomalies..., ant al. preacnted In ...Son* Ikon.. spank moon. lands. Samp. woo essonaMtnte,anctko of Oda report a dse mom. as laskvkbasl data alms. wasp45 days.. Nor folloompeae..ona A noftahu Noted:
Prepared By: • N... • N... Ann Arbor Technical Semmes, Inc.
290 South Wag., Road 000.6210,0412321. Ann Arbor, M I 48103 4.146127O4.01ITIII.
PRRXISION
$0,,IT Sulk, and %Uric:4Oe Poolleoter rreebina
A mans sp. RAS) and nut. bp....e(MSD, coat anal... polargre 0Ad2C Mich The MS/AISO, matt. peer. Borrow. aka. wita the following eacepitoou
• No.
trod:ay.,
Mgt T.... (Quality Mamma Coodanator)
Aral to 2022 PhIbp U. Swots (Labor.. Oisteto)
00111.11.010IIMIOs.
I
O
B
I
COUtidruo. IN Mews y. tottnowonwil Sance 290 mat mom Mot mo iota. worm 40103 To 734,tolSCOOS F.7349054731
f,. I Olii 1/1111111
I I I0111 11
I1 i
1 111h
in -0i ssit
1 S gt Si
_
—
i ...0
....
I ,g. ;.
1 I I I IS: 1 "...=, . - . . • . . . ..
I
/
li 19 II
1 Ig lii iIi ja
Illi
i .;
1 I 1 1 1 1 11
11"al ;', il ; 99 7 ! 1"
— —.
F :saa 1;71
gHl Mg
i 1.7(timA,..44-,- l —
... ....
; 11 [ *,
•—:
B
1
Ir
5g O
0
3
iVigt ;
I
I
3
a
It
1
3
bil
A labongory rums blank ILItI0 was analysed es pod ele a QA/QC buck The um,. the swot.. ante. .0 du 1011a.,<Itarllaft:
• None
;mem:a Stototorth and Sorrocotr.- 0ommtelou
Tin notbod abb. boor. Stand.. Ws, M Sno.. Imor.al shindela arm and RI.. 4.31. reel the sox,.met, w. Me followna oaopduaW
• No.
ACCURACY
Almrenry Fn rt I fl ett Rlenka R.FRIOPR, Idharstory Cantrell Somntm - Accuracy
A ...my fordtled Wok 02B/01M) was unload a. port of de QA/0C bated Th. UTOOPFt MCI do etono atth do follow, moutons,
• Ntio•
01pIrlo Salk. awl Mutate Sol. 0ad9e n - AOODMOO
A moon spite MS) and moth optic cloak. (AISD) was ...dyad as pan of the QA,C N. The hISMSD's not do accuracy amplanco mom with Oa folloonag couptio.
441aL JtaL
3E
a 7
if
I
3
a
AN
N A
RB
OR
TE
CH
NIC
AL
SE
RV
ICE
S, I
NC
.
AN
N A
RB
OR
TE
CH
NIC
AL
SE
RV
ICE
S, I
NC
.
g
os
is
O
27
3
1
ORGANIC ANALYSIS 1,4-Dionne by GC/MS
USEPA 1624
ATS Project Number:O001-002.22
ATS SDC: 0413221
Prepared By: A. Arbor Thchnieal Service, Inc.
290 South Wagncr Road Ann Arbor, MI 48103
CIMIAILU.04,041.1.1.
O
O
-El — Igkgligp
3
10!
1C4 1 011i i
LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: C001-002
Report Dote: 4/18/22
SRF / SDG Number(s): 0413221
Client PO Number: 4505179649
row Norm'Ire SIImmnry
Tbss cow nano, applies so the following 9 =nolo pre were row.. at Ann Alban Techment Samerajne. (ATS) on 4/I. • and unaided nuthe.opeOCCOMOC
C.. ..f. kn. A
nvLanf 0 I47 0. I onl 4. ••••
NM 0 Ow.. W.K.
■ 5 I. Ill II ... w
2 II as 4.D mane W
0I .A. W..
. vela
W.WA 01' li.M. I .I. s Wow
r4vAs5 7/11 wunl 4- one W
01,411 VIM , en• W
Upo meant nuncio rue ...led for the NI. as .a.,scs.
Ansbx• NralbscoLlauclo • 1,•-n.••••.(LNI:PA Lae. TAT • S Sam.. • I Maas Sp,. • Se•nu Slate Um;la•
• ((ISM I n24) - Sand., TAt • 4 S.n.pb
cortmle Baehr, ('hula Meo.I040 Record.. PIA tlnldlne Tiler.
5 O
Ce
3
3 99
rhorR Review and At•Pros, 4
AU data ocoluoal In thls report hews been generated in ea...In. guadellase provided in Ilse referenced Wads. kit thelbad.sod are omitted ...is. procedures described In a omiten standard °paging powders.. (SOPs) .peenie as the ATS Laboratory, an mooned by US PA. All data mn rcer and management rer.red b ensure compliance outh the above referenced SOP's sad proyea speeolkutthrts. le 44.1thon. all this <adorn. sa the Lthanoo's Push, Aroannee / Qua!, Camel Mows,
sax LFD, Lp7, nun(. apleaa (Mx SPK). W hRWold wheva spdd a roue. (MSD, S1aX our. our. I.N).
Polo OttollfleotIon,SocelflentIon,
The fottrng qualalertlipOr that root' to rod thrapbout this SOO and nee Presented air. Melt
•e•-• meals the calthothon mn. of the method • 13. - fault taken (mm weak tidal.; • alliccaralion mowed between the Isbumsarylattrument Lkienatned Mahal Doecueo Limn
1.01-YLimot Of De ection 0.013). W Ow Prams., Quo... tom (POLYUmr, 01.0.. ,,mao
"DAD, concrntnium reported bebw the laborabry,olsurnent Method Detecaon Limit (MDL,Lanul 0(0a...on (LW) and tha thonanent Sa,nal To Nome Rano (SNR) of coprourostey It I
-orinlyieccountr.n mellied blank exceeds repulse. In. snslyte rot dowsed above MIX. LOD
••••- analyte me. batch or sample speak QA.VC control Inn os Isr - Indlealts Inaba Alam-Mt
indicstet Ion rad° Lem, IS and 3071 ...pio...thda. - mica. ion Tab ans. JOS....nee wine,. end res. k Nol
A.mgt QA/QC bonds la del0Mu ro mon than 20 samples cad...method blanks 041,11), bir. spike
DUP,UP.IJO.
5101, nrilvernbl,
Tare= =71‘:= 1 :at nt=:= 7t:ek
flrnnic. AnOy•ls
11,.olaus.,..cab,tha.C.,): Samples were anal,. try purge and , OdMSm mmba. with USP.PA method ION Violable cte...,e br Ca, Cl,reaublOnaby - Mau Speararneny)
Sate,let wen ..lead drawly n ATS by Pall Carp,. MIL Sample wax teemed with proper Own of walla ealthrsoon ...Al al bur (Ivo levels son and to quenth. L4.Dussent- Samples were reported to plead
custody rem. leebded. Sun. comb., and anum.a, if any, are ad.t presented in the ,turthle IleecipC speenle reponsng tenon. Seta,. wax '<portd al ay./L
wedge of the report or $n the coalmen/son thdroduel daft theca, AU sartlislet were prepared sod ..lyted wallet AS days Vhtlie Follosvin,,execpbons, Anemia.," Non,
CAnnnn• Lmtnnuenial Senna r ooOtourottoolvItoot.mokbot.tit000n 44103 T•1711,12.60W3 Fee 73493.731
Data Transmittal Covor Pogo
Project Nemo: Pell Corporation
ATS Project Number: 0001.002
ATS Report Number(e): Org_SRF_0113221 ClIentleO Number: 4505170610
Project D000dptlon: thb data loped ...At the tosalla of b voMer sample, roan. by AT1 On Awe Ia lo the arthSpod for 1, Chown.
Wn sway owl . sem. ay.,. far the woo Mow au. wads, la ...ow .wap ox,. now retquaue sone. Wan...0W me taWdemwm.eWd tracneknn Oman. n Salad Cowman usual...* epaulets the ATP ate; ^-- ea re., by ULU& taloa*, Ora thee. CON.. CIVOC rAyenston am.M.Inb , opeason and mule 0 the tabor., open no,. Wag. •that eaty mob:. neat ell ..leatle somas Co.monaaaad IwaL. uro...a"... N.. be.
Reelplant Mr. Ca, Tee.,
No. of Papa. (Inetodtoo eov.r pp.): 21
From so.h 9WbNdeM comet
FAX Number.
e`lf
nnor (now m.o...an PAX Number: 734.04.731
Aeklillooal Massage: Coot' Pa... , KO. Owth 5,00a. Jim gen 0/001003050/ gabs SI/above, OXIMItheces,Noni coen1 notoosgerv.opormion.corn. Pews... Pokes (suo ploors.polLsxn) Anthreb Nabob (armada rabetheopall corn)
Date, altar, Slunotl:
IF YCeJ DO NOT RECEIVE ALL PACES OF MIS TRANSMITTAL. PLEA. CALI. 734.02S4,05.
rans.u. e.imn n wo a.. 0.
r4s
Coln. I, 11,,Innt
Snruplat <mummy; compouult lennee0Uebom above tLa wiluldavadon currc 'nee Jawed Lod cerrulyted foe those eompourds. The follow...lc snmpks were dilated kr L.nunee:
• Rol Peal 011/L2
• 1.1W,I 01=
• LIW.N.I012in
• MW.44.4/.2,4
• alW4L101.
TAbornto,Reprent Meek,
A LthemosYreerlent blank NUN., eard,ed as pan of. QA, OC WK5. rto with the followthzateepUww:
• None
Intern'', S..... and Surrnentrr - OWN, ' IbrInn
This raelbod cares Imenul Stannanlo rely, rot Maropra. (mane' wader. arem and retenuen uthea met the scuounce aim was the Sulbann.eseenboiss:
Arootney
Leheretery Fort' nrd Ripe. a .F11,0PRI Lubenttery emigre, Serenle. Accerecv
A lubora, forldirel Went (LIquOPIO•o• e•mtlynd cm, of the QA/PC batch To brATAI.Z: lena
trIT SnIkes on4 Motrir Cnikr Poolleotri Ace:more
A noble spike (MS) end moon spike deptlessa (MSD) was sms.`yred as pert orthe QAQC turd.. The /AVMS0•, reel the atom, aeceotanea course rob the following eseeptions:
• None
AN
N A
RB
OR
TE
CH
NIC
AL
SE
RV
ICE
S,
INC
.
AN
N A
RB
OR
TE
CH
NIC
AL
SE
RV
ICE
S,
INC
.
QUALITY ASSURANCE / QUALITY CONTROL SUMMARY
LABORATORY ACCURACY SUMMARY
Lat. I. 0.0 O. KelIal 0.3.11I21
1,ollOacr. 063.02,1 nr.10.
Matrix SpDT (Mg
4,112022
0.1.72 On. C.. I - -I-I - I
ISO C. 10. W9 we IA
fp
weat MG/. C.COMONIO-bo,.1.00 WWI
RyolOri. 4/15=2
Maul[ Spas DvpScala (USD)
I ma /ma.. n I Aws./... I AaM••••••• ion. 14C...a
_AWL
1.50,1U4 OC.1.111221
SOO WWI Pry/<a arta: 0:0)././2 Ann, can /Alma
ILI. Sp4 (IS)/ Malslt Spike Dup... (ISO)
l..../allaa-sdara
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE /QUALITY CONTROL SUMMARY
LABORATORY ACCURACY SUMMARY
i/14,1 O. I. 111 n. VI • la
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/QUALITY CONTROL SUMMARY
LABORATORY PRECISION SUUMARY
.3=1.0 4•1~H16a .1.02
°MO ,ISIO
I •a.~s•„Y
a 1
I 0 RI I
41 I I 1/. I IL. I An. I Oa I I nl
9.1.0 000. .00...
0.192.000019
, -1 09.4
oq,,i1 ea./
I fi,12rrl,
Arc* 4,11.1
.01.1.1101
40 9
Int
?A
II
CKANI OF CUSTODY RECORD
a/n.
MI
0440ed ate
S
Er. I I 1
• - Remmatsi Tern-Around Tine Mee, Numb', IC, I . Urgtnt 2 =Rath 3. Stand.
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONTROL SUV1AARY
LABORATORY BLANK SUMMARY
meal /AOC se ./4/4, ./ tOD
LEO, ICI
Rya, l" Drar Z''' U'
Labe/May Rosman/ Blank (LRB)/ Method Blank DIED
Ana A I Ie.,/a Cos 1,•4.11-• 10.-A ••-• Rai 1.4,1.• I M. oann P.. I
O
Or a
L
Lat.
am,
ANN ARBOR TECHNICAL SERVICES, INC.
OUAUTY ASSURANCE /QUALITY CONTROL SUMMARY
LABORATORY ACCURACY SUMMARY
003..11211 ZOO NOV,
4:11,272
Laboratory Fa/t/ .1 BUM (LEO)! Laboratory Co... Swap. (LCS)/OnLoing PatIsbn and Auvracy (OPR)
I las a•ax 1.161. 0.1.. IMO
.10
I o. uz. sc, Da/. I a. SO II
°B
ed
J0
A0
O I
MU
JS
UC
JI M
CC
Data ROoleW find APOlaVRI SemnIe Muth.,
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number: 0001-002.22
ATS SDG: 0414221
LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: 0001-002
Report Dote: 4/18/22
SRF / SDC Number(s): 0414221
Client PO Number: 4505179649
14nr.lve Sworn,
T. ow norrono a.a to gat followne ...SW v.... so A.A.. Tahnnol Wows Inc. (An) oo U14/A. ind Guch. maussopecifk QAIQC:
CliwnSonnl• 14.1koon W.wa
Nil. MI
Rol 1.4
Off4W-1• PITA, C ow6nu.
WA, Dan tnworilT.Anonl Tim
4/1 len
4/14,22
MAIN
YIN) 11,,
UUT4Um.
Upon realolsornoles was whodulal for gro fol./ fig
embus Mittact2ms. • SAVA Uqw, TAT • 5gnpin•I 1.41.1x go. • I Mono gr....
lon
Wow
60 do/soon/W. lo thoe repo. low two scoot. in accaidonoo tollowildolown powwow. refuse o4 otandaid iou mum,.l we colahtelli pr000dwen Clownboiln • wilion Wed. woo.' ...as (SOPA) speific male ATS Loboroory.swoogrod by USLWA. All dean am porn. row.. Memo colophon. on. Wt.. ro famord SOP, and prow. waifkatIona MrddWn, a/1 dolo conform M tobowory,Quahly Assume/ Coat. Wm.,. • Rol 11.14,14/22
A on& QM:1C kw. Is deka ao no mot O. 20 ...excluding mot. 01.10,(MII. UM, fortlfwd blanks (0.,1,191, LCS). =MR "Wei (MS, SPKl, end dupl.. ...sp.' or wow (INSO.STIC DUP, Johnrolnro Rotronf Mon.
Sample cadoinang compowds Gconomoolom snow du ii.olool.ralion cow woe ails. nod mwelynol fo. Tlo felbwing Gawks woe MTh. for 1,1-Doonne.
pate and Tectonic.' Nnmition
This following.. qualifordesolotont dot moyW sad dimogboul WO SOO and ,* wadd willed. wwondod tample an oath SDO satiooaa appro...
11B11- encoodwto callbrOloo gunge ado ft.. -D•-raWrIYm Iron arm. 11 - rep.. m. latorotory/loonowoo dom.. Slottol A Limit (MDLYLonil Of Docthon (LOD, mgt. ProcOml pow.. Lno01)134.o. Qowoowo 0.001 1/401.,- concontimloo mooned.. go labonowyfinstromoni Method DCICCOMI Low lAIDL14.1mIt Of Ownlotalloo CIAO wol d0 mom...pal To Nol. Na110 1SNR) of appouiroOtly Ilk I ArerntAcT 111. - concontrouon s method blank won. mporung1.4
arolyla no4 dew. go. MDL / LOD
A Won, tweml WNW wc owpcb., The010060006500000600. .6 the follow, am oo.:
• Nan.
Internal Stand.. and SIWW/Ontol • Ongnitig Min
Tbh mctiolc==..14 . 7 ,1;a4Sorrogoto Otani slaw.. Gan end on. motile
• Nnn
1,4111.1., s . " - indl000rs only. An wacdol lowhorsomok Noodle QA/QC cannot WO Ind.. mono h.... I.ohorWory Fortlfirfl Maul. MFTWOTR1 Lahonlory Control Nimes. - A ce..ro
11...no•ne Woo -r- Ion ...owe 15 and 70 % w.pwrce Wog. •Nk. - InAtocwon rwo amok WA wow.. .4. owl romIllogARcoartol A Wnomory Ong. blank (I.PlOOPR) we.mbewol as pon of ib• QAQC NUS TNLFlVOrksetg0
woo.. mom woll .loan napliaw • Norio
Mr, DUP..).
Drlivenhh,
Mk doss package tannage. Leval II poclogC11111.11,... robin (/awl L Is. ry DV, is, 515 RUM Spores Recent. Chian eu.dv Rnordg. mud 116I4Ine Timm wow ropom‘ Thor wit no hodcopywo Onn, she. 'wowed for Or proso.
Samples woo deluaeddaaAy0 Ass by Poll Cmporoteouraff. Soc la ono. whw0 wllh pmperohun ofcon* a4.odwd. Wept,: on.U. and woralloof my. we dam. prpagal Ino5onole Racipr sc.. of gm rtilorl or lo Illacommagt on 041044 ldoe6c00 All ornpla wow popool.Joulpal wig. 45 dayo with Wir fol., m.o..
• Nam
l‘mnIc Muhl?,
1...tDiovuxdostalagIGNSI teeN wlo ww?..q puma ad Yap am is..... ww, usorn en.. 1674 (VO. Orin. Co eme.byknap Dtlumn Cos ChnononpoWS - Wow SP....7)- Ao
wen Iwo Inv knob w.0e4 maunw 01A•Owun. Sample was rtpened WWI,/ apftll, rep., Now St/rola.* mom. woes
Anomdw Prepared By: • N.•
Ann Arbor Technical Susi., Inc. 290 South Wagner Road
.01.103.1101,410.11. Ann Arbor, MI 0103 01019elawCH,14221.1. Clorwlwart Chewist“ EmOnworroolSno.
100 $.IfloomoRen0..,1406A1AOlgan WM TY 73.9541910 Fir 734/7.3131
55001910N
Maier tiollw and Moirl, Snike Dontlentea - rrttliloq
A sum .1. (MS) and nol..ple dupl•ak (AISD) was mulyeof at poor 0A,IC both. The AlSO4SCro ma pm.loon weep.. ono. woln Oc WIlowag «cp..
• Sow
Mule T. DoLtwe tQwwimwwwwCw...:w1
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A mou spike (A1S1 and nut. wiko dopbroo (MSD1ww mewed. pot of Oa QA/QC Wok. 0 MSO4S01. oat go row., ...cc mono w11h go following cakopt.t.
• Now
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5 r. Data Transmittal Cover Pogo
Project Nemo: Pan Corporation ATS Project Nurnbon G001-002
iC
3
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3
ORGANIC ANALYSIS 1,4-Dioxane by GC/NIS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0415221
Prepared By: Ann Arbor Technical Savior, Inc.
290 South Wagner Road Ann Arbor. MI 40103
„i 683
3 5
4
I
3
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: G001-002 Report Date: 4/18/22 SRF/ SDG Number(s): 0415221 Client PO Number: 4505179649
Caw Nocrailve Stuntman,
Ihn wsa oarrome sop.% so the S umpin dot woe received at Am Arhoe Terholost Seneca Mc (ATS)one/I502. rod ...sod ma..epeole Q/VOC
pool dagY
'Ron,:rIVI"'"I '
40000.0... sm v.: tv......47lnp M•m.
nor II. all tAmna 1.4eutae War
Errjl wp ,1I/. I IA-u--.- Woo
Ilni1C. • 07100 Um., L.......... ...,
_jstnez. own l.e. L041 Wan
MP... oral Moo I...Insow Woo
Upo teems maples were scheduled tor Meld...me analyses.
eduilystl MaabcalS .lP • Irroni TAT • 5 So... • t Morisse a.I Moots Sp. Dunham
11
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Data Review WI Apnrnonl
3 B ed
1 3
JJ
pA
01
Si
lb
All d•racontsliied m tho mood have been generated In montome wt. modems pnrodod In do referenced standard shot method, end we consistent m. denoted precede= dosarbol Mn a win. oiodaid operering preoedsors (SON mcifte so Me ATS LAborsteey, as opium. by USEPA. All dm w end monmmont ...at tomer< <motion. with . above reformed SOP's wd promo aprofirsuctos. In odd. ,sad.. omfonw m Mhor.mT,Ottohly AMMO. ovary cowl, Maws,
tilVi l. Q. 1%. ."=9Thr ,Z.717,7e;:n:lirsr==ro dr'rt trb,1:=. ftiPI-KRNIU 1 3.lr
Pitta Ounlinea non, tincrincntion, and Trchnkal siert-anon
The following are qualikce Law-option, iatt nwy soot throughout ooh SOO arid wo presented with their resecie.t samples a cote sty] scant. as epproonste.
• -cam& Ma ullbe.Mn ranee or the inetbal • -D. - reside 'liken front sample diturion • `7" -0nm reported between . Ishorateryhrollunent determined Method Deloettoo Limit
(MDLytanit Of Moshe. CLOD, end Ma Neches' QUM 'Wan Lonntl(POLYL.I. (LOCI
earcnIIIIIAIn 0eporw below der loherwayhnonment MOI.1 ',Notion Lout (MOLAJmit Of Quanntstice (L001.4 the wove.. To Nona Rano (SNR) approslostcly
coneenostrun in method bleat mem. mponme ion "U" snelyt: M dolootol ohm., NIDL /LOD
Indicates snslym hsa mardod Mach cc ...note spook 0A/PC control Imola its.sto cowls Into ference
-r retro between IS sod SO TC meets.< widow `,sir- huhu. Ion ratio etude 30% sdoep.co window Arel rook w Not Itepor.1
A sonic PAIOC banli in denied os nu mom than 20 samples exch., method liAnks(hM. IJ10, folioed Nooks CBS, LAI, LQ.0..0. spikes (10, hp, SPK). and dupl.. whather spiked or n.bws (LEM, MSD, SPK OUP, DUP. LAN
Dal 0rticrrnMea
• Low, If p.0gr, odor den read! WU des axed 1, Ind tv ay, ens RS r.om Sample It cri•Int. of Ctittadv Rrronia. and IlnidInn Timis arc iinaa norm.,. There woe so bode*, dim sown, elms moored kw ads pro,
SillInAs Waif ,IIVertdilinstly to MS by Pen Comunitron ustf. Soup. woe m.om with prone:echoingf custody, eceeNs included Sample con.. rod sninahm, if en, we other amend nn the 'Sett,. Receipt' cgmnIr Anglo., mune of lbw moon or on Ow Comments on rodirsdusl dam sine.!. All temple. were motored ord mlyerd wldwi 45 days wail the followed ...P.m: ,.. lhos ie,,,nelsys f0ca..), Sample were mlyred by pume sod woo MS in math, wt. USP.PA
• Ns. meshes! 1624 (Volutle Orwinte Compounds by 'tempo Drha.on Oa OromotoffulMy - hfoss Ns...OVA An and cslibmoon with 0 lout live In. wet mod to qesnlitge I A.Diosene. .iii4es woe weeded to moymt
spook reporting Molts Semple. were 'meted ne mntl.
270 Sor0 Wddner Road. Am Ma, LIO*Mn 411C.3 10100010490 FaeTWY0473I
Onni-41/12/04,,II.
ATS Report Nurnbor(s). 0, 17 4Client PO Numbon 4 5 OS
04 15221 0
Projoct Description, Mks deb report Contolno rtssUts of S.., urnelo. gowned by ATS on April., =to. rno/ymn leg I.4 Murano.
via wary Owl . mem tor Ns moon no... w.n 02....4 In anpann,.. am fp.i.ron pr../ In . nnoenOvIl anentara teal natl., frkI nne n ...I. atm. °omen, Lb ....TO LaWn.ne, a nInvend try iracnn. SOF, wo CM.00 reo•noun Pr otencm.s auto +too lubeNbN won iwtsAse Urmss
now on ewe. nlooft, shoot.. sr, . pentaval..nd Naomi rem ....Arm,. moo hoer ,al
Recline,. Pc. Coco 0000
No. of Poo. ftricludlisp cows pad: 17
Moon: 7 ,1^.—O•wd"12:9,, ,
FAX NUMMI'.
From: SMM Stubbtalleld EMAIL Spoon SturriicIaltaanriatnicrtCnrinclanirin oainnowittairinatai FA/felons.: 734-00,373I
Add.Moolineownlint COW wrOcet lee Pad<r<0R XotthrkalM_pocsrumiloar ooml Orede. Arn nirn twode(Ioodorml Keno Strehouer Mo.noweloNeo.com, rroarartinwapancionacani. Pomm.r.ruo palnn Men,poMmelpollownl
AM/. Isabelle lemon. leabolaftoollown)
Oats: 411,41.72
IF YOU 00 NOT RECEIVE ALL PACES OF D1IS IRAN: MTV, PLCASE CALL 734-09,0005.
m.o.. w mow.... .1 ......rmmosesso• o en wow memo. weer, ors mowid•.swrowl*"......
cent.ni Mm.mwwam I. M. lakes *.ed V.. rows *way hr wwseow. Monter
Shr11,44, MOM,. compounds at concor/allots shove the mlusl od.brulen curve weia 41:00.1 resnalyro5 for clop compotrwle. The fol.', maples wort dewed for 1.4.0.onw
• Pm N...150:
Reacrin Rlnnke
A tabor., reacon Wank Minn wss ar,yrot al, of Na OMQC Mkh. TM Latin. 04W:falai. WPM wall non folio mg meow:or.
• None
Informed SSapdnnio rend Sorrnestes Ito tIon
Ilaa mattxwl ualuel !Kemal St...March only. not Swap .. lam.. wandank area end MUM,. h., Met Me occoptonce omens with the fnUewing eacomons.
• None
AeCtIRACY
I.nhnmtns F.rl I n crt Itlank• ft,91.09R1 lanai...Iry Control Satan. - AeroMICY
A lobentory Willed blank ILFTVOPIO was anshqed as pot of the PAlQC NW. The LIM,OPR met the acceptance miens with the fathom, mop...
Mnic(c SM." and Motels Snikr Ditnlicatra Arcurner
A nwoot spare 04S) and moms mks 7,504. (MSO) was anal,ed as pan of Me QAVC Mach. The NISMSD's met de accesacyasseptime attain will thercillawIng campbon,
4.1402/10.1.0.0.231.1.
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QUALITY ASSURANCE auAtny CONTROL SUIOAARY
LABORATORY ACCURACY SUMMARY
MM.)
1..C1601:14,,r OCCAU.3711
SCO
Pawl NS-a_ fiJ01aN11 4.167)22
lEstrkSpRe (US)
3
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONTROL SULWARY
LABORATORY ACCURACY SU/APART
$04
0.0C ...Le., OCAV.1).211
SOD WM,
QOL1IX121
R4,DNY 4,14571
WM0 Spam Oupault (IASO)
I ...se. II,....+114,00C , 41>.-ara - 4 I - 1=1.1 = I= I - I I -I -I - I .0. VS, N.= it .0 ,1 In K Ave IN 03
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / OUAUTY CONTROL SUR...AY
LABORATORY PRECISION SULWARY
ueros WO. tut CCOACNIMI
10,3 WWI
0301,..12
.40 ,100C
SW. spa. (as),
I Le co I ern. kw. I L., 10•441 r. I 1. 1 I a=c= NMI,. WM= td-Oars 0335. p. nee
+5= it U. I U3.4. 41 740 el. 4),
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4• , 044-40
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.yrsax-3
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4414611,1-
4•11.
•uans 723
.e.re 73.1
T.
CRON OF CUSTODY RECORD
:79
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4.0.4
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V
11
• REQ.sttd Turn-Around 11./a PRottO limbos K, 1 =Urgent 2= Rush 3 • Stan:3rd
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE / QUALITY CONTROL SUIWARY
LABORATORY BUNK SU..RE
LYMbet DIVA 2.4
CILVOC 0005.4$5711
1100 01.21
0.1-001.12
4.11.21
Laboratory Reagent BUnk RAD)/ 101hed Btu. (U8)
LA 04,0 14,..t.f.4,4•Tne1C,...-• I C. I 04. N.T. Nu. I40.... +I) NL net
Gearant
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/ QUALITY CONTROL SUMMARY
LABORATORY ACCURACY SUMMARY
MU/. %IN
sot NUM
Ita-te• 0.01.0.12
4.117721
laboratory FodiRed es.. 0.F mtLaberalay Contra/ ST.* ILCS“
0 I Au.s red
LR-14+512 WS= .4 'AO.. tU1e1 CO. I. 6,5 1.3
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04112214
Witiu 04/11,102 720
hibmi WIMP MOCPAI DOCPA 1404 nu«Ya11e0 [UMW U3CPA 104
boiall Num. OCOMMI11.1
12101.1
000,0 17µ004100N m 1411.041, YYYm« 40,22
11.0. IMO 1100
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basis
GOO aCA.
04/110001
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1.1f171^72,12,'" 11.4.1011..ic b ODO Meer .1 Manp M
berolerf....0
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marollon11010•NMPA.I OUP., 10, :004411 Mumps 001.100412271
GOO 1.41.1
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r" IMOInolnon 11.4.1
Pl. Valium CooM • 00 004000 Pm.
Cale Vfol °olio mpl
'hypos.. Dela 04/12,.222
Moly. Dar 04/120022 201020
POL Owl
LOX
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0114. P24.0010,011 Pr: 714000.1131
ATs PleMb 14.0. An Moo xvmba 04.00 00001. D
Libencloey Illoopplo ID
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1.4.42cara
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Lamour, Baimlo
GO,O=M
0412221
041=1-0
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Pampas GU 04n1/202:1110
Molybosl14411.1000, COMA 104 Pnarawn 4441.10120, 1I U PA 10N
00 Balch Numb. 010000412211
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Deb... 0.0 1.000
1001.0. 6011 SOLOWM% Fasla 1 Deals Wel
Trot P41µ410,1.22 D. 04412CD22 Anarysis Dow 04/120172140212
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accie 00.
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z=4 blololuro 100.0 ,0,01220422 2 4/410
I0L1 0000 final Volu. MCI 1000
GNa W.
Probacallaa DIM Now. Ariorysio Gb 001,20222102.1
Owl
03102.731C0110010 Vac i01010,17)1
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0.602 7; POL awl
ATM Prelool Nwea
AT0 0041 Muaves. 0
Yr. "0001.0
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Paionu4er
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000140222 04171,.
041=1, N al
0017/20,27..
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Labotaary itaimlo ID .1.7421.0 Liable
5.4..• Da* 0011,20. 1716 Amlyibal 0160PAI LIMP/ Me Pnson401.1•4nedlUSOPA.1 LIMP/ 'al 00 GIM Woo., 0004100417F1
Mbum
MM, MOa r.ahaw 04«1400, 1.r
D.µan 4610
zr,44•41 Malmo. Ina
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almi WM.* [VW 1000
MM. kola 40
boals
Ua. 00 22
p,. arollanClala 00120022 M.o.,. Deb 04412/1272 14.4110
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Om 00.
at.0.10.4040
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CAM
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omo, Maisloto
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LIMN
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Wel
2206
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Owl
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M0 ODD bum., 041272 21011
Mary Sample ID 2212, Laosocilewb.ple ID 041=14 Wlxo Woo
04.4 Delo
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A26•554.50.1.4 00.0029
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Maul. W.4
WON.. la. A.4.1441lhowe IVO Vwl .CPA ‘021 11.4/Wen 241744 fO5Val 450. in24 04114141,15.1. 02.54411.1
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04.15...0
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0413221
041=14
Valet 11.0 044..514
moms., um. N., LIDL.IQIWw.mdkm VAI 1JODPA 2229 c< Dm. Mum., 00.10051.1
ATO PrOMOMMIMW 0001401.. 521111. 4.0.4
0.1 Om...
Lamm., Immal.
Kam.
r.wm.MDmm
Aw,110.114.1.2 .1¢P.
Pr•prll.r 14.1040 21111,.9 U•.SPA 1624
041.1
alma
5410.211.1
WNW
4.142022.
MOM 1051
0025001.21
11.0.0.5444•.4: 11.4 0054 b. 11V
'2 :044.4. 041 1.0 00.1 Va.... 5410
10
Unm 99142 10.0.400.0. 0411.1. 999,9 Dal. way.. MOOD,
CAL MOL MIL
.1.014 422 ad
1.4c;T:L%'Lb,,,:g1US IWO
5000 150•.91/19.40011 0.0
F..
Ww
OW. pt
1,00..11. .14 WU..
M.. NY MM. 1045.
Roman
1.4440.0. 12151-1 6500 61.1
dal
Owl
"Tr,
ffitrztitic: Data Transmittal Cotow Papa
Project Name: Pon Corporation
ATS ProJact Number: 5001•002 ATS Roport Numbor(a): Orp_SRF_04113221
Client PO Number: 4505179840
pr.*, ...,eipoon: rsa sess moan wedelns No tom. of 5 worm sample, nroornd by A71 cm
M.2022 m maly. for 1.4 (Magma
We oer0lrvlatM.wm0•1. •nap•, ban .000•11. boon 00.0600 .0000.00000..0000
im 0.000) 0.00 ono 0:00.11. 0.1.6.00101•001. 300.10.000 1.008.0410 0 MI ATO Labor., ow owes.
10, and WAD ..won ra• work.. worm. ma war rl w Monday upon wawa OW. nowo on Memo rooal on mm. woo. wwwww "ow nom
col
elplono Mr. O000 Trandol Gwlk 0•30 ni,•51 410,1 tom
of Pope SooA2n0.aver po.1: 17
DM:
FAX MM.,:
Swim Stobtkerold ,.rabSkttreW(LArOAgyrTorhTTral5e.01m,mpp
0.0 CIM..00•00. , FAX Number. 7140054731
Idltbrod Itooampor Caw royal lo: Palrnno. Nell OMII: polunianirripatirom, Biota, J. Orm tomeetpummoi .0 firrahrew potrolwartifthono.00mb 00000.1.0.001000, Maur, Soo Pew. (wo
Mooch laatiallo (onus. loalkil... 041.11
SA-%93-s: sto: 40522 Ironed:
IF WU DO NOT RECEIVE ALL PAM OF IMISTRAMSMITTAL PLEASE CALL 7344004001
rpmwY brew. •M000.0 *M. P.Mo 00.60.00.0.
1.00
MOODIML7700,100040.0...01AM
SamnIr minnows
Sample, wow. warrAmdt al conecalrworir above dm nerd abbr.., ro e voor ... owl maroly703 for
awe coarpouods. The Waiving ro.la ...Wed fee lkDionone.
• Rod P.M VIII=
I,oboralory
A bilkomory magent bk. (UW1 war wily. so rot of Ow134, ber. Tbe 1.101 rm On.mcepmwealien,
WI, on 0.04000
• None
Jolter.' Stan d,141 sad Surr000lt, • Onontitollon
Them ethod .dim Imam% SW4aids sly, of Sorrowt lnlenwl mama. mew sod retenoon Om. men rho
mtg... cow... the rallowmgcaccroons.
• None
ACCURACY
Laboratory ForrifIrd 1.0 ,1 (I,FRIoPRI Vabnroront enorroi Samoirs - Accurst,
A lab., belled Nook (LFILO7R)wm analywil as pal oft. QA/QC tow. 11,41.141/0PR am Ow ...not coral...nark folkowlnyouplionsi
• None
platrir Sollon sod MAIM Solke Doi:Drain - Acenrsre
A wine spike (A41Thed miano oaks doplonte µ1S0) ala malyea1m pan of. QA/QC be,. Th. MS/MSD,
MI Ow mammy wept.. wk. WI, the fallowing csoordaw
• None
0)0103322/0,111121.0
ANN ARBOR TECHNICAL SERVICES MC
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0418221
Prepared By: Ann Arbor Technical Semi., loc.
290 South Wagner Road Ann Arbor, MI 411103
yairisary
Mairle Sate sod Shirk Snikr rionlfratet - 17Thfl•inr1
Amon orikefli1S1w4 es.(, op. doplitiole (MSD1 gulped in pan on. 12 SC sees The mn thrp.lmn raga. okrw worth No follow. =p.m
• Na.
1/74/_a.g.ev
Mai, T. DoL000 (Oman, Ammo Coordlostol)
NUM B. Selo (Wags, Donlan
Ca0140.0,001..
/5,1M 70,
/ Anr1131.2322
4444I4L
I
8
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Rol
=MI
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: C001-002 Report Dote: 4/25/22 SRF SDC Number(s): 0410221 Client PO Number: 4505179649
COW Narrative Sommer,
The mmanarrMArt oms. w 0. fol/awl. 5 wimple 0. 0 mare 40000 ol Ann Arbor Technical Nark,
Ii573/ on 4/11/11.“55 mom. moom•lomitie OAAN,
So NMI,.
iL,S7
1re1,44
hRk aisl
Ff40,1 14
0.144.•
Mann reed
,mro carat.,wordw
onin
V•7
0.47
00X01
Upon tacos somples went mboilakd for the Wool. molyse•
andtto tandocoilasmka • I.O.I.(115117A 1,:01-worn TAT • 5 garspk• • 1 Meta Op.•I..Ma 501. I/Wow
Thew Unr.
I Irvin
mow
Thum
70m Aalyl
1.0•00
1,11mm•
00iman
1.4µmme Orwe
i•-P,••• Man
Mom
Woo wow
WPr
onto Redeye end Approval
MI dm& conlalmil in dor report /wee born genenkel in sow.. with yodel.% provided in Ne rokorneed
wad. WI.... end 00 0000.1 with derailed procedures dwabod la • won.M.M MO:mod Nam.. (501, wicine to Oro A71114borvary, o mow. UstlA. All darn ott par sod ...woof mirrored to mum warn.. on. the above miaowed SOP', and perm, erectIkdron• la...a. mild.
"'farm 10 the IsboratoDy's Qualay Ammo. ()wady Corned Mundt.
A eragla OA/QC botch to Wined 20 wool. emludas0 awn. blanks (M(L forMisd
al, VI, LL,), tram wk. (511,153 sod Walks. Midler en.. or news (M40,1PK DU7. DUP. LA).
Polo 011ollnenflane..SPedflThrlans. and Treholesi Narration
Thor followl. qualifier demotion. Ow .y be owl Waugh. Ns SOO +Adam pi...kJ wt. Ogre
•0000.1mmpla 0. SW.. as sworn.-
• qr . -.cads the colibrarian ram. *fine method • "1r- owls Wren from work &Woo
• 'l -comments. mowed taw.. biborMary/inanonenliktenninof Method Dew. Limit
DADLThank Of Dotectior(L0313 a. Ow Pratt.] OwntaThon Larot B`OLYL.witit Of Qiwoution 0.0(r)
'AWL' -cowenawon nrpormThelow tsbenntraynwoonent Method Own. Lunn (54D130....
Of Qum... (LOP) and Ow Instrument Simul To Nam Palm ‘37:111 of anprommoiely 101
wflYk am. -nterdion n method Monk ores. roparting
1̂1' oulym nor deka. above MDL/ LOD
- indaThlasnslyle hoz mow. b... or somrk gook OA/PC.00bl lien.
Th1. - bdkaks.ema laterfemeree
- ma retie between 15 and 70% meepome window
'NV- indica. roe rwo 0/01M 3crx umptamswmdawmJ lsalt u Not ItepaM4
Aar slo QA/OCbakk In.nd or no more Oisis awns...Mo.. method broJcs (M11, LA111. f.onedbSoA
4.3 LC31.Thoo0 moth. 0,94.MS.SP14.mdOolients wisest @pace or Wave MSS, ars PUP, DUP,
Polo71sladWrackese coward.. Lewd D rem, some. mom Meberre(14.11, Good NOM PPAR3 BOD)
somole ReteMt. Chian of Commis Record,. IMMI Holdlne Tim, me OW Po. arvan requeiL Ilue wow no ...yd. wow, slues gemmed for Ike proJem
Sonspla wore ...al growl, ATS by roil OmporMoo Malt. Serrip. wee waved with prop. tholoaf
woody rook. lowladad. Sark condition and encoulles, awry. an. ailed. mosented in Me • Somple Rowse Samole onelvm. 00 0 (5001000 so sampler sue 'mond imi emir. me. 45 day.... Mom. ram000m: 1_,:liayontnoabsig.(OCOMSJ: Snort. or. mooad by pap mil bop OCOAS in moon:Low wth USEPA
mallwel 1450010.1110 Copalc Camrowds by borapo DOMM.Owenerrormalry - M.O. SpeerromeuTh Aa . N..
WWI colibooranwh nt low five keels vow usethe crumb.. L4.13ormine. Simples.. 'owned lo project
morine moor,. Ion. Sampler ...Wed in mg.
0001.10.130,040221om
ennorfronoro rt tmoo....rolSonme 200 SouP Wagner Road..kboOkioaan Td7340,0015 For ...MI
ifu !ii--, ,,t,1 i 1 ;scti 1
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1 1 4
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01.00.01,001017.
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3
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44.4.111—
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9
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Data Transmittal Cover Pago
Project Name: Pall Corporation
ATS Project Number. t3001-002
ATS Report Number(e): 0,3RF_0410221
Client PO Number. 4505179640
Project Deeeriptlen: Thbdeo moon matins results of 20m..... Nob. try ATS on Noll
10, 2072 to sea snel)Tel br 1, Morons.
w weir y snalypro M be lopplharel..
▪ T.61•18..Cad MM. WV mhotl.4.1 mil ...WO Wmaww solsawllM
SYtNN OperullnaProuulaw anortablM AU Labonelb., at ruwl,WI by USW, Lonor...... 604, rout QACCodorooson pa AM. brtn... baaaa SW Immo, mom.. Unms
spool., now on. arm Nom A spoorobb sob. prom.. ms hole. Wm nquinniatas
R.Iplent W.Oepe Tronds, On. or. , orryklds.Psom
FAX Numborr.
No.otP.•• 0oVer .4: 33
From Soon 11.0161.1 !NM .prantAntAbfloNsilorylOrtcyT•cMyen•rocmorn
4..”...ran....yr FAX Nom.: 734•00.73I
Addltionsl bosuns: Copy moon lo: Colloroan, MAn RA. pellammi.atcorn). Made. Jim pim Oroctodbudloon.1
Ka. S.M./ Ondrohauw.tvorliamen, nooad•Ww.oparueatwoorn. Palm. Sue Polars Imo
Amanda Isaballe (anon. Isabollattsblootn)
0.: MSA,
IF MU 00 NOT MCFJVC ALL PACES OF THIS TRAMLAITAI.. PLEASE CALL 734.0.0905.
n o muse Mo.*, erylw .t•••11,••••••••••••••••••••••.••••••*••••.¢.1........
II,o,•••••.,*•••••••••••••.••••0.1•Ass•Roa•lw•p•••..... ,••••••••awSr•as..,••••••*
reirol•Vorya•••••••do,loneWne•owe. •Iime•••••••••...Taypar/Vad her•no•MON•cemew.g.ami•
••••,,, ••••••••...*••••••/W T••••
xsual, 46,...._11.4••••••••_C••••_,.,
il-IR
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3
6
3
elf
!
ORGANIC ANALYSIS 1,4-Dioxane by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0419221
Prepared By: Mn Arbor Technical Screlect.
290 South Wegricr Road
Ana Arbor. MI 40103
11
a
3
P.
1
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number. 6001-002 Report Date: 4/25/22 SRF / SDG Number(s): 0419221 Client PO Number. 4505179649
Cate Nen-eller Summary
Ter nee nentret urplit• to the following :0 samplo dun was recalmt a Awl A40 Swvitc2, Inc
MIS/ on 009027. sod bumbled nummpAlric 0AR:M
klemifien Ds.
R.cre..4 VIS12
s,yor•INO1
AM M1wl
in MO
LOA
.71
TY, N1
TAAI
TW•IX
TWA
TW•I7
TW.2,
TWA
TWO
-72
Mt?.
irt
MWMod
1.11biNh
001.02.0,61IRCIA.
AWN
N1017
Awn
VITT,
u tV77
uiWS
✓ISAS
UIMJ
+11.71
MSC/
ARM
ARM
MK:
T. Am,MN That
Ilrvm
Arms
SaeW
rtsrotml
our..
Yosrlu4
lwranl
MnA.
bbrhol
WNW
14410.1•• sm.
11,1.,• /••••
tronmms Wm*
Coma. rw Clormoy E rownnotent.dSarnee 290 SodOrWspoelkod, MnAdrmIldbton 10103 TOW.. Fora 734/7054731
1... W.
I 4.1•.••• Wen
I Wm,
41Morro woo
1 FA.. WA.,
I.Lfbn•w Won
1,41...••••• Ww
14r1•••••• Warr
1444•.9 Wm.
1,4414.... Won,
IIDMw WO,
I ,4 1•••••o WO,
bk... soon
4.ineLee Worn
Ie
—7/ 5
3
9
gQ
i
!I
!if 41
Upon ANrpt sompirs woo schodukd M rho rollowbo Nub..
AosIbls ItunkuaLtssoks
• 1,-0•sum MOM - Ursort TAT • .00la• I Mum SNI• • I Mart Sods W..
• 1.4•Olmoe RSISPA 1, 211-.MATAT • N...
11.1PlY RYYPInl. d'hoIn of Custody ROYOTRInond ItnlAlnr Timm
Samples were eethetcedaectly b ATS by Nil Comonebe ear. Swop. win Ruhwd woh pee. Maloof Iscank,...41. Sam. cond.. W anonrob. Amy, ore Mho prom. in . Son. Reasor
baba of Mb manor to the oommcAbm indm0.1 dab shosto Alt books moo prem. and amlpod 0000 15 dorysw: az Maw, acceptor*:
PM. Rre1rec um/ A.m.'
An Asa cone.bd In this moon Imo b. Amos. In bombs= wohjuldelum pt.. In be teracoad lat NANA. est aro yormommosh bolkd /usts= A.R. on • rodum /M d opens.
peon:dem PPM Ns:4kb. ATS Labostory, royArol by mem All art pea fad management
...lowed to ensure omralWlec urib stave rokrtncal SOP/sand project sposilkoln. lo ARM. all data
conform to lho Isbontory's Qualify Am../ QMluy Canhal Man.s.
A ANA. OAR1C bola a defined os ea mos Ada II mop. ossludimg nisbod blanks (MD. LRIR Nu. OR, LH, MS, fro. /p.m RAS. SPK), onr1 dupl.. Mortar Spiked or auw 4930. SPK OUP. DIM. LAL
pMP Onalitto Nen, Sneetnearinne. end Teeenieel Nam Nee
The folleense we qualifier demotions.. boy boo•d tbourphout Zhu NOG sod moms.td mb bar saracubd umplu be. NOG wt. Y apprepnalp.
- orzetd. the calkbraU. Snipe of the method 'D--molt tam horn um. diktioo
- cormstro. Nom. bubo.. bboratoryfoutromont bums. Merbod OstmloolMilt (MOLY.. Of Dersolon ROD, AA .1 1.1.1Q•substran Lunit (POL)LAMO(C....
/WO ommatiz000 boor. below Iha Isboatoryloosubsuro MM. Dom. Ural, (MOLY..
Of Quomboon (LOO, sod . PO dArtl Stms1 To Naas RAN ,SNR, of Amos/m.1y lb I sablylis commundloo itt method blsok morals Nominal.,
111- onal)le Mn dOsoNd above /LAD analyse has mended ho. or sample rpm. OAKX eostrol bons
indm. nuois Interforenco `V- m.o. rem b. berm. IS sod 30 1.m.mar mad. 1.121r - rod.. W m.o.. MG Acquonce nab. sod mutt Not Repos.
A si 0c QA/QC hatch rs &Mod os m mon than 3. bombs rocludang nothod blanks 0•111.1.1111). /Mt. blaolo (11,1,11. LCSL Norm op.. Rd, MS. SPK, and dn... MINIM s,ted or mum (LEND. MID. SI. DUI DUP. LI.
‘011.041...04,434116.•
AN
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ANN ARBOR TECHNICAL SERVICES, INC.
QUALM ASSURANCE / QUALITY CONTROL SUL/WRY
LABORATORY BLANK SUIAIARY
urn, USU. sua
aloe Sou Moue Doca.tuat
SOO mem
1.0.01.1000 csoaccoos
Rue Dess
Laboratory Reagent Want (LAB)/ Method Blank (VB)
6 S
1.201.110 1.1.1.250 1.51. 1.0.5.• II.02010.11,5•15NI0.0.05. Lel I R.. I 515121222•10.110.2.1221I .....•002,00. cur.
.9t 001 oat
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE f QUAUTY CONTROL SUILVARY
LABORATORY ACCURACY SUIJUARY
4.2.1 125£11.11-. 111,....12ce. axe,. 021
.0211 P-0.14.-. /10.001 1,252.1 Laboratory fcrified Blank REM / Laboratory Control Sample (LCS)/ OnOotng Pied.. and Accuracy (DPR)
us...0 1.00 rulnernaT.I.2.= 1111.0'72 .15222 242214 I...-. 0.51
12.2.1 W.120
OM... 11,2e- 000.1.01121 503 .11211
112.111.2.2 4311.221 112.1 0. .5.21 Wt./ Spina (US)
. 05.. 0 I...2. In......sloreau. 10110 216 .11=t 1101.1
4111-441L
au. um* 1511 CV0C ErzUreet 0,20,5111111 203 2200111..-2.1
.1YO1
0.1.222Yuman, .5.22Ilatrts SpRa Crypt,. (MSG)
ANN ARBOR TECHNICAL SERVICES, INC.
OUALRY ASSURANCE /QUALITY CONTROL SUUVARY
LABORATORY ACCURACY SUILUARY
(100 131 F. el 0
ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/ DUALITY CONTROL SULIVARY
LABORATORY ACCURACY SULWARY
lauat2•012,021.10.-...-•.•1211212. .15120 120 0 121 rat 1521 • 10
If EL;
a
0.121.0121
IO2
Oqii a AY- 405=1 555.1
•
1,
t(
v<f:
4.701
15.00
0.520
00001
5152.
551200 20.1 .11,104,
50201
40.2 2.55.1
01=
.101:1 Kee
15.
011
1.1
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000
1201 1211 110
Iq
d
CHARS OF CUSTODY RECORD
:F
0.1
5 R' • ti
it
II E5 Ig
3
O
r.• 1.01, 11.
15
001 MO.
rwR
100
1110
Xt.
• Requested T, Amoral Thee PrbrIty !Unbar Nays I = Urya 2 • Ftush 3 = Standard
CtiAD/ Of CUSTODY RECORD
7.01.2 201,51.0.1.0
4002 0ZI
uue
00.0550.5.50 .105.21.5.2.
0.0.00 el 00 IV 1
1.6
1.2 10.10.11.1.
Is g
1.0
220
0`1(2011-t1 v.= 100 . 1 0001
14 5000 •3I 051. 10.
251772 012 54511111
ao 4111.1 110101 121.
01721 05 1. 15..
;
• Riquested Tum-Around Thu Priortry Number Key: 1=Urgent 2 Rush 3•Sbndard
.40 641 „,_
O
8
5
2
tie
5 6.
p. RM. RINI Alsnr0•01
All dun ma ne. in mk egrwf hrre been generated in accord.= W4pubklkw promdoS in Oa referenced
standard ten merhud, dad art etuumtem rash demiledpeocedare• daubed In a mince nandod opera:mg
prenedonts (SON) epomfm a M ATS required by =PA. All dam me pow end numpreanot
renewed to more compliance abow Wenn. SOrs Nod propeomonf.... In addl./mad date
conform to the lebocory,Kolity Ammo= / Palmy Control Ma ear.
Date On al Mentions. Snecifleetinn, and Technical Narrating
To foam* ant qualifier devermlicoe Mat rosy be mad thioughom dos SDO and me =eared with M.
.ueentel um. I. Gnu, SDO.rbon m
• E• -• =c.d. Dea... marmotthe method
•11. - ...tains rt. ample =Moon • • J• conenstraelon reponal Nom= Pm 14onaromyriamonan drionnlool M.. Dere.. Lioni
IMOLA:on Of Degt. (LOD,. and the D.J. QumM.dm Lonit (P0LYLI. Of Quentillatleo
PAR . 1/401.• - cononamorm reported below the labormoryhnanaumniMmhod D... LAM OdDLycom Of Quanoinion (DM and the ammo. Swell To Nene Pane aNa) ernPaaaJmarelY
o.Yk mrrooealan pn method Work =needs repo.. la.
• 1Y. embed tam dewed Aare mDL/1.0D ... .ord.. me/. Mu erica. bath or urn* =cork OA/QC ongrul
Mr- Johann whit oderferenee • 1• - los re. bd.. IS and. mom.. win..
- indiums I. ratio outride JO% acorpmace •odoor and boat ie Not Reponed
A eagle Ou0C b....WM. as .mon don 10 temle. =eluding meth. b.. O....). fondled bads
NIS. LIM. LCD. p.m sedan (.FM, MS, SPID, a/01.10.1k.svfoodsr.pdged Wire (MAD, MSD.SPK
DUP. l•RS
Darn Dellvernble,
• lard u P..: eau.. .ryas Poet a. Le. I. Levet ry DV, EPA RS EDO,
arc mutbr. up. =gout Thee wan oolurdeopydabmormary =Ws goon. for the porta
;inmate Arian!,
J An.= tOts.”0: aeool....uneulvarabYmett• And me Oaers ...e.e.e.ne.s•nbUSP2A rme..d 1010Nefebla One.. Compounds by Moto. Doi.. Om aueourogrermy - Mms Specoomorys An odor ea.*. was Mean= In... toed to quroUtste I.1.13loamie. Samples.. reported reneelect monde repo.. llmica. ....way reported as
Ando.= Nona-. N...
=0I.11104.0.2012I
Project Name:
ATS Project Number.
ATS Rapper Number(e): Client PO Number:
Data Tranarnittal Cover Pago
Pall Corporation
0001.002
•?;fl itS7Irtr: (1"1
pepleemeaceippon: Rtr data men ...Om rawls era sonar same.. too.. by ATS on Amt 20, 2CO2 m be nnopao lor to Oloxene.
Vi• coney nor to ...to anon. he MIS ropenissiv•beol order. in MO. .=
mtwana1.... WI mutate, an I an cae.....terlpoo.no deuce. Nowa...ft .000.C....00 P.M.. speedo lo M ATS Lat0.0.00.r n0.10011 by O.., das 0010..maCINOC Worn.. ee• awAlvtd• ourousonaw ewe ot ins ..haroa0 wenn,* UMma
upd0.a/.a..tabu 0,00.. 00 Wk. , 0.000.00borml...01.01Ing Imo eogiAnentob nu. ban
Redolent: ...Q. T...
No. of Pao. (Inebellng oey.reg.,
Fro= Sondo Shorgele.
21
Dna:
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FAX Numbed
I FAX Number: 73.1Ard..3731
AddltIonel Do, mponb PuttorSen, K000 M. ,
Kato M.A., pretrohaire4Momgdom). twooduf.mopenolionown. P.M Sue Posers (aun peierelgoolleorn)
Mune. ko.ta Meow. matempenacen,
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t....1.0a , YIN. 401.ryt• wNa.rl mn .00.0.•••••I OM.",
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Smote Dilootnn.
Sample co.., compounds al orneenu..s above Ma Aral ealrbrolart cane ...surd end money. for
grow compeurett. The Wool. nano. was dr.. foci...oar
• Rol rode/X.3 • heW.I04 MM.
• AlW.IOUVIO/22 • Mint Dower Rd WIN.
• MYMICITMIOD3
'alimentary Reeeent Rlenkr
A Women. megot blank pea,. analyzed m pen of the 0NQC Web. To DUI nun the amp.= anon
Wm MfWlowry exceptions:
• No.
Internal Stand RH, and Serowe. -Onanritallen
Tab meted nelon:1=7 ,17:Lonly. a:Sunapee. Internal Mao.. mat and Mullion Unto incl the
• Nese
AroiRAcv
Jatherelnry Pori I Der! Blank, (11.FTIMPR) !Ahern ter, Control Same]." • Avelino,
A Monk, fondled blank OSIDOMO was s.lyaed ....of De OM. Neck The Lrwork.d the acatplanCe CnIe• elm M folbabp aseeptkor
• Nene
Matrix Snike, And Metric Soler DunlIcates - Action=
aum. ntain rat. and nutnn•peectueoe Nam .... adnputofine QAMC hoick To MS/SASIK•
nom the room= memom. cobra rills. fallowing todepturnar • Naos
0031.011.1.00.021.44
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number:O001-002.22
ATS SDG: 0420221
Prepared By: Ann Mbar Technical Services, Inc.
290 South Wagner Road Mn Arbor. M1411103
pRECISION
JafaMc Snlke and Moiety Salk,. Dentin.- Perching
A main, spike 0.1. rued matte epika drolleale (1... nee modyn.d ea pen oftheQAMO h. ,. The ...SD ,met do pardon Kuplanevallatairldi M fdlor.u.g cu...
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, Atan 2, 2022
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LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: G001-002 Report Dote: 4/25/22 SRF / SDC Number(s): 0420221 Client PO Number: 4505179649
Sane No rr. Ivr SIIPIMPrY
Thla Cate rutnI0Va 0p$K1 b 0.4 WO, 0 Nilapits Mt war Woherd el Ann Mar Techmol Service, lm. (ATS) on .20:2. and asunieled nunnaoneadc
RN acrd
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mw.rom
2210 Mw 074
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Upon mon. utopias were ackehrled fort. following aorlyse.
Anabon CluratonLIng.
• I.aaawrUfirw MM. Um. TAT • S Som. • I Mane Soilo • I Mont
• lbOseerna (MITA IC4,5“..TAT • aSawla
1,10‘w r
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Smote Recant. Chain of Cult... RrmrMs ond Dateline Thne•
Simples w.rdsvered directly to ATS by MI Comoro. snit Sm.. were =awed .4 proper ch. of malady rerroNs barren Semple ecaddion and anomelnet. Waco, are eltbee preened In M•Sopk smold" nem. of Mut tenon or in Mt conmenra oa mdtvi.al dam them. All monks wen prepped end analyzed .thin
doy• rlu Or forlo.agareep.str
New
C001.1.04,01.316.
Curnaim. Chemo ry tomornneoena Sew., 290 UM Worm Roan. Pon Anse.blithdon 4103 TO31109,01IS Fan 711005.3731
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Project Namo: Pall Corporation ATS Project Number: 0001-002
ATS Report Nurnbarydr Orp_SRF_0421221 Client PO Number: 4505170.9
project...Malan: TAB Oato report co... me too. or 5.slor son,to. roc.. by AM./.
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ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Projcct Number: G001-002.22
ATS SDG: 0421221
Prepared By: Ann Arbor Technical Services, Inc.
290 South Wagner Read Ann Arbor. M148103
3
I
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LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number. GOOI-002 Report Date: 4/25/22 SRF / SDG Number(s): 0421221 Client PO Number: 4505179649
Cale Narrative Summary
Res mamma. speller to the PI...5 owe. Wt.. ...awn Akar Teduncal Sem. W. IATSI ea O21/22.ad roar.. .0.00 03(0 QM)C
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Upon semi, sunplo Wat sch0.100:1 for the Woo., rodywo
Maxt.lfloroks • I,aOwr (MEM - Urge:NUT • • 1 •
Ramnis Recelni. Oman of nntrxtv Record, and 'Midler Time.
Saw.. woe ddivord ATS by PO Caryenuan
corIcely rtcordo Winded Swale mdllw ondmornthekiropy, reeldapro.cd la thelemplo Ro.p. •
lk eNam.0a ndoidual data gwoo All Nngln avepeepald adN0cI00 Ihd 45d, wlb.Nronowa...plloor
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AS dose ammo/ in Yes report Arm bean gemmed to aorcedsore with soulehsto promded Ow rehmscod want. mat muss, wel as snesteuwlthdrmld poomelom demobs,' in • Wilke otendred mend, pm:educes (SON) meats bibs ATS Lobotomy,. mucked by USDA. And. me pseud marMlemest reviewed to mom compliance mat .4 ohms Maenad SOI, end omen oponfamiirons Weddlnuo, NI Jets morons to tho hbermory,mlity Amorous/ Quality Costml tdasuato.
Ample (htdOC Nacho dermal at so mom Mix 10 amp!. moludisg shothed blanks (OML IIL fondled Monks MS, LK, LCS),uutm smsen0SS.SPKINstdoPlimeswbether t9thrd Lit).
Pals Oustillestism,tiorelliestions. and Teehnksl N0m1Non
The rolkmog n quid. deoctiptioos dont my be toted throughout Sus SOO and vs pmts.! with their snoeude4 temples on each SIXI lesson •• opornonate.
mcoododte estlbeasomonge seek method •D- -mask hams Min sunpla Won. ttr - eamstration mooned betwem the leborolorynomonwet dosmatned blethod Del.= Limit (MOLYLortilt Or Daemon (LOIN, otst (MM. OMOSIMMO ur. (I.0Q) lAtDet - commends= mooned bolow the lahromoryhmertment Method Detect. Limn (14014ollout Of Qmottlatios (I.0Q)aud the lestromeot Sigma To Noise /WM (SNR) of oppmlmately101•D•-auk, conoestranon in method bleak tee*. IMMO. Wall
- molyte sot detected shove AWL / LOD indicates wslyte hos...DOW tomb or sun* smarm QA/QC metro, limits
9T'-Weals mats Menem. indicate. ca. between IS and 1014 smote'. morSow
'Mr - 'MMus lm num molded. meow. *Mow Rod snider Na Repotted
A woes QA/QC bstolo w defined au so mots ohm 20 waste. amiudong mod. blan. (MD, Utll, raddled blanks (DS. L.,:tS), 'Wm... (UM, PAS. Stqa DU, DUP, Lk.
Pad Dellrersidr.
titrt, o, ritsorstsstosts.1. 4,.. mobs.: sr. , rt.. Roo. R... Or.' I.11ea11V iwr. nt, R1 in, oval.Me upon memos Them sows no Stordcopy dos summary Awns gaterms4 for Ws popes
%mole Asst.,
.LEDvs, ...OR. ...so...Sr mot sod ',GUMS umccedtrcawltk USIIPA method 104 (Volatile Onomlo Compounds by lump INionmoemChromotoPPOSY-M•••.Pmmtm,Mh tnittal estibrallos with et MN Am keels wu ussd tomosture 1.4•Butsone. Sample. were repohd Wong. maga ...mine's.. Sasslet mos smarted m
Anen:4,74.Nolol.•
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Labors tory Resort', Plonks
A Mimi, msg. 66'44a/11N wtssatlyred a portal's' QAPQC Web. The IAN sins the steep...tem with the MlawIng campus.
• Nom
Internal SOlId 05 and Stterooste.- OuinflistIon
This method outlets Memel Stands. only, not Sono.... Internal wads.' meal and menhos ume• met the ...Mors miens rid, des follownR comps°.
• Nom
ACCAIRACY
!Abort' tort Fortified Plonks 0 tFIROPRI T,shorstsrr Control Soon...Accuracy
A Lawn, WOW blank , PRlwusayed m port of the OM0C beck Ile ltIYOPNro. Keenness Mats ugh nn follow, mamma:
• Moe
fast& tinikel and Mstris SnIke Danllrntre -Arettrney
A mons spike (Slit ml mou.tpiks dupe. (USN MU analysed stoma. QA)PC WM. lho NISAISCre nambe mammy omit.. mum odds that MMus. °mottos..
• Nom
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mum No' ter rely'nd as port of Rs QA,OR met. mecoloommgams Monts with the follomm stammer
• None
Mark T. Doles. ((Motley Maumee Gargiulo.)
c
Moho D. Semen °Adana, throne,
1100141912.01, 211....
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AAA- Eggigt:.. Data Transmittal Cover Pago AMY:M.0R 7ECHNICAL SERVICES INC
E 4
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All dus coalsmod in OM,. have born gemmed in mu... guideline pow. In Oner e/mud suouterd tau method, and am fouls.,..... p,ndnro deato. M • mtban mudard °W.% pro.no. (SON) op.. .tope ATS Litbonatory, on required by USEPA Alldw me pew tad mtte... reviewed no come comploa. wuh etc abo. rekrmreJ SOP, au:loc.°, smell... In addl., aU data conform to. laboratory, Quality Maumee / Q.ulity Control Msotiett
A eagle ()MOO bane dernod m no mom .20 samples ...hiding method blanks (MR. LW), fon. Mionk. LSD. mem spikes NS. SPK, and ...unto wk., oinked or na. (MSC, SPI, DUP, DUI, LR).
;
2 2
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nnrn O. • IfflenlInne. SPeelflenlInnv. end Teehnleel Morn.,
The following ant qualifier ckornettuos dot may be mod ...bout mu WO and arc prem. told. Men samptes to each SOO met. as morocco..
- mord. calibration rupee( the method - rush taker. Item sample
, - conominalm reputed ben. the labonswytonsinonentdoennenoi Method Mutton Limn (AIDLYLiniit Of Dcrectaon ILODL mod the Prechul Quantatton lams (POLYLunn Of 0unindaton (LC.,
ontentnmon rmaru.l baler .lebor.ryinunoment Moth.1 DC.I.L Limit (MDLYLImit Of Ounbtatico (LOP) and me inatontou Signal To Moue Rohe ISNR, of epponsonelely 91- -aadyn conostraten metbod blank amecds repotting Ito.
analyte no. dewed.. AML / LOD Wings aal, tuauecodol hewn or sample :Kok OA/QC...I llmlu
Tr . - WK. mum ituestount IndiCalm an re. between 15 and )0 It aucemace window
eabcatm not mho wt.& 10% ourptence *Ind. and ruull u Na Rencded
(‘11., " ? "C =Irl iaZZIZ17PI I:=Ifer ' s=rn 'aUTV,t). ).:SV, TI4b,"DUP
Dpfn DrIlternblet
1, date pmloote caul.. o Level II packs, otha data ncive packed. (Level 1, Leval IV DVP, EPA R5 RDD) me 6. oiLabla upon rein.. There wan no h.., dou winnwry shecu ',curator tee nito pmtoce
Smote Anolvsl,
LEDramogAnab..CICAL/t. Samples woe .Mein by pun.. and hop GC.,MS &e.t.a. with USEPA mo., 1424 (Volude (quint compound. by I., DINA. Gta ChrornolotroPhY - Mae SPeetmene.i. An Natal ultbratbn tn. et L. Ave levels ...to wed tumunr. Sunplos were reported to project meant 'coon. limits. Streaks were upon. on
C001401...,041.21.L.
PrOJoet Nemo: Pelt Corporation
ATS Project Number 0001.002
ATS Report Number(sE Org_SRF_042.2221 Client PO Number. 4505170640
Project Description: The data roe. cot. Po mt. of 0 wnle, cam.. roe. by ATS on Aonl 21•:0310 . enoSsood Inc 1.4 Dean
Wa *may.. 0w.ampb mot. to, tna 'mot non. ottoman• tom paean. roo.el orb moue voodoo) log mt., snl Con.1.1 vin ins wt.
Occoglool Opormoo Proomomp•orlo to ma m moon. ty U.CPA. Lawn.. astama. ons ONO. vnamson ....a to, tammon steno. Me IAA., wan imoint LKna
M.., ram co Ma dare mat an mut.. U.1.4 V.41,1101 and no1My ems nog ermne hoe Dorn
Redolent Mr. Cann Trended
FAX Numb.:
No. or Popov (Inelodlno tow,.
From: SetenSusbble. [man: Sarnn
t•mor O.aYartr mom., FAX Numb. 73.95.3711
AdWeional Meamoje: Cony,. to: Pam... (kolth_pootaroundlleontoom)..... 0bb bmdo.P.L.) PUP., SlrmuwM (allohmmen(0.req.coml. noodsdlkropastbm eon, Palma Sus Para (nos porcuallpolloorn)
Amanda Isabella (or.. lubonnetpollecinl
De. 4.5/22 Slorwd:
IF YOU DO NOT RECEIVE .1. PAGE. OF THIS TRANCMITTAL. PLEASE CALL 73440.4005.
emu
Imlutionq
San,. faelmillui, corms.. st convent...vit. NnW caltbusion cure were diluted got mangy cod roc thaw coryulMids.T1te tolknving sand. war obluted roc IA-Dquee.
• Rol Not 402,42
• lAw.R.44.,22 . mo/..
• MW-Ittal 441,4]
• mw-ltenna
!Allot-Won Renew Monk,
A tsborat, rodent blank (litEhmt easIyzed a.pnaIOoQMQCbats, The LAB net th oecepl•mt ernerss voth the following =uproot
Innernnl Sin nderdr andSnrrnents n.rml rminn
Tin inched mains Internal Stoodards only. not Swot:stet Imental aundo‘ds emu ond rotontIon toms met tic acceptance entenawldt. folkway mutt...
ArrimArY
J.eivootory Fortified Bien. (I,FR/OPRI 1,nhorelory Control Semidry Acen roc,.
A lobo., Nettled bLank (LIDADPR) nu malyud es poratsa.QMQC batch. The ',RO (mc1 . ...nu.... wills the following a«poona.
• None
Matrix Spike. n net hI n SPIke Uunllnlrl - A crOrm,
• None
OB01.111.4.M.11121.1.
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number: G00I-002.22
ATS SOC. 0422221
Prepared By:
Ann Mbar Technical Services, Inc. 290 South Wegner Road
Ann Arbor, MI 48'03
PRECISION
Malt Sol. owl SUM', Snike Preel•lon
met nq ruo town de mnawMg a<grlow
N kT. DeLont (NAY Aosorence
PhIbp U. Strom (Laboulor/D.o.
oontml.2.O,04.11to.
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LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: G001-002
Report Date: 4/25/22
SRF/ SDG Number(s): 0422221
Client PO Number: 4505179649
rem- No rend', Somton ry
ilea cue nano. µlobes so ....log 9 umplea Put wens Norio. et Ann Arbor Technics/ Sent.. Inc. (ATS)esAr.,..2. and med.! nmero.lpecific QAMC:
Clint Somok&noincam r.a.T.
Sony,' AC.,
P.I.11 rot
Rod P.M
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4/0/22
4/22/22
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4/21/22
mom.
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Snood, Receipt. Chnin of CuMotiv Record.. nod lioldint Time,
Samples were delivered dkMlya ATS by Pall Corpondson &WE Samples was received wt. proou dun, of custody monk Included. Sample con.. and manna, du, ere ettherprmuled In the -.Me Rau, &WI, of dd. mi. or M me commute on mdtvoduel due sbuto. All samples were prepared im1 andynd wIthin 45 dem roth . fdlowmd mceptions:
00012W21O+,042,I3 k
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QUALITY ASSURANCE / QUALITY CONTROL SUL/ VARY
LABORATORY ACCURACY 8.11/ VARY
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CA2122I Was<02A2
P+P.A Wt 42.2.22
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ANN ARBOR TECHNICAL SERVICES, INC. 44604.14-
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QUA/ EN ASSURANCE / QUALITY CONTROL SUVVARY QUALITY ASSURANCE /QUALITY CONTROL SW: VARY
LABORATORY PRECISION SULWARY LABORATORY BLANK SU V VARY
Wow/ LMENE 1121
ONOC 0XV.012.1 SAO CA2222I P. Par..: 0:01.0211 E.A.O.r alsan
Mex. /ABA 1122 CA02 Lg. Nrlx OCOAGO/22221 SOO 0.2121 1-..jeci rAwn O1c 472.22/2
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Li• Ian. 0 1.,..10..11.410....••• NYS.. WWII V. .L=1 q.311.3 I.Aagura
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LABORATORY ACCURACY SULWARY
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4.4 11-Dm Summary 22176-01 1,4-010X0170 by GC1MS Dala Summary ShGI 0114 229000011 17661 ry + ̀ Dale Summary Shvat
All Projw Numbs, 41001001.
ASO SOO Nuo09 GIG= Con1119.01•114 LOA
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NoloWl WOW (GEM)
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0130.0111401
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11.101.•
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C.,1081.1.
wsl 11.1. pt
0.11101312
0.1. 0.010800031.111
114:)..LI:ZZOs 1,4 DIoxone by GC/MS DOID Summary Sheol
Pat
7 ̀ : ;Ill =1'
AT111.01.1 Mu.* OCODC44.. Al0 800 0.11021
1..70 1...ralory.... ID 01000.12
02.11 0.1. NM.= MOD
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1.4.01Now
err ~~Ar~rrror
CABO
131111.1
114711m• 1630
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11.1.
001
0,7100120020111
MAL POL
001
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AT{ Propel 8.808r 000103222
13110.1 TW.10
u.m.y 13.801 to 010=1.13
WO. mPY Cm. 0101•0032 010
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Ann ,131313, uNppn ut0
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011.1108
11•w
Unft• mot
01. 040070.2 ADO,. Dm.
„aciitaLL-1.4,f,t1,:=2„T's 1,4~loxano by GC/MS
Data Summary Sheat
0:01011.28 1030 1311010029 1000 ATO 31.1.311 MD... 0101403. ATO Prq.e1 Mum.. 0071.01XLV ono .13.000
GCl„=.1;0110=1 AT8 800 0.10:21 01111.1 7.00
" WPC. 1300...1.0.1 DOM can 10 0.883 =1:::$17 041 L01.1311. ..11011 18. 10.0.....03 6111.311.1. 600 00.111
Pina1Volum..01 1.1300 08110.1-10 01821,0 111.1101,08.1.L1 13030 0.43 LADonbory 0. 1111. 04.01.11•100. 0110781-10 SAO
011.00...m. WM. 10 DOD. INC.. 10 0088 Wadat 031.008
TO 000 Dumb, 0110301
TAM 0000
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.00
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(1.0CPA1 '7..0" r "" 07,01' 070C11 MOCPA ULU 3..8...1100 Dal 13.000(22 L010,1410. WOO= USCPA 1000 01010...2 Pr.pan.8.0•1. .OVA ICA 0.00030
IC 13.1.10..... O. C 13.01, N.M./ OC 13.148 Numb. 000.061111201 A...1. DMA 00200120,10.3 OCOR00.10011 An•Iru OW 01/20/X011020020 0.31100.10371 010300.133131,18
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MAU not 1802. Da. 00.1
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0.020271101 101
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KM Num. Gk., . M MOM
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nelo•
coy. eCt owl CAL f= 12101.1 0462 1.01.1 nV 0001 1,4.411
I134,1-1 11401
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0.1442.n
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Dom Summary SAeot
Pea•mlbelemm 100.4 An trolml kooker
AID 000 Mumo.r Clu.Iar.W 10
ONO.
flamo% Dm.
myo.; word Woe, .
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1000
Lote elk
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MAKI.
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Noe. 4. Odl
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1,4-Dloxono by GC/MS Data Summary Shoot .4130 Summary Sheot '4;Ta:= = Is
.AciaL
1'4 GCIMS2,17:41.1Z reMel komle 000140127 hunt M.. MO ProMlNumar 0001407.1: eas 40.1.10-22 1000 Pm. eloklum 1000
0470.1. 7KV ATS BOO 1.04. DOOM ma r°042.91 ATI 000 lkimbe
0201.01;412JI
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NOG Dodo MI 0.804.0 KeeMere. ..0 0126/214 1141Veleme.1.1 •000
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Weer 0.14 feme 10 MOOK WOlor Data. rm. IS000.
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OCO.1004.34OK. UN
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a OmanKM tot 01441030410241
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1•41.111*
Mn AA4T4.14MNnWa, 1044.
AM., Mgnb•n 11101
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14•1•14 Wu, Om. Dam 040x00227.10 AP41.4041041144011.0 40,1 USCPA IOU Pmpanal•n114100411.114144 ohop,o,om
000404110.04mo OCOP001=41
000140217
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1,40.04444
Mn Patm•T•MwleM 0•41444.10. 200 IMO W•00•111000 tort. /04.11. 1403
ta irft0 nlIl ig :21 4
114/44A1144141044
CASS 17101.1 Ola 001
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.1310 Prsp4m1146 DM* 01/01420.4 Munnl• OM. 04.200.711n*
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PCIL owl
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414.1.101 RIM Volum•CmU 30001141mian F.*/134414 UMW Pok ImmmnPlap13414 01121=77 A441,14044 IMMO= 0254 n0
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D0t0 Summary ATI1,4-Dlozone by " 444.41 T''"" 1030 Ala ha4•m
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1.tanc:24Ac.Irs 04010011..00r01
MOO
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7.44411oOlum 140.11 }NOV
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0341 rnwrMwlo ou—snon
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polo/m.144
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C~eOY 4444+.044
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Data Transmittal Cover Pogo
Project Norm, Poll Corporation ATS PrOlott Number. G001-002
ATS Report NOMborfal, 40;SL:77 04 25221 40Client PO NM.. 4505 170840
(10aerIptIon: Tha dour re, contolro the moos of 3 nada,amnos,nomMadM ATS on Artell 23. 2022 to Pe nrayPod Ica 1, Mu,.
Wa panty mat Won.. stInc, rest ma,. war. Papa,. • rallea
rameta1Coradro Fraranum.ark a. ATP. Lesnlary a.. OOP, •ne °ACC Mon sum a pa taw*, rpm cep. moo, nand on ma eau mom at applaa.... paw., and Poldna ta. naaamana ••••• sows mat
Alml pls. Mr. Cale ',pedal .,PNIP4PCPI, PPM
No. of Papu (IndyilIng la
From: Sarah Stutatleriekl
FAXNumber-
r41Mlt careen SitIttermmllannamorTernrchey,,, con,
FAX MAIM, 7340033731
MM... M.., Copy moan,: K.m9.0 paPso...14,), Omde, 4. Ern bodes mteom) Ram stroomr norahnonniPhond.4 moodoadwqmo......... S. P... P.. ...P ....) Amor. Mt. famenclu Plabetlufp.l.axn)
ORGANIC ANALYSIS 1,4-Dioxane by GC/NIS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0425221
LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: G001-002 Report Elate: 5/2/22 SRF/ SDG Numbcr(s): 0425221
Cheat PO Number: 4505179649
elite NatTallVe SUMMON
This cam per.. applies lo etc (Wk., 3 Nano. that woe mein. at Ann Arbor Tor oral Santis Ins CATS) on V2.122, and esseci.d outruopeeirto OAF0C
annalm CTrr Smuol• Monona.,
14.77 4n4/22 arIVO
MV/411,4.
Am.. Ten Arno, 11. Am. Man.
Wand Won
Wand
rpm Isoapt sapp4m a...4,4,W for Ilse follomnd mires
601. XullneLDLYGNa • 1.4..• (MITA .2•1 - Up. TAT . t man. ',Pa • I M.... lauecuu • 1,Dnunt Irdal - TAT
All Gm mooed on dm loon have been ono. rn amordtom crab oidclbroo porn. In ...nerd eumtard tau moil., and art amnia. voth Madre deacribed •n • written standard operating proce.M..,SON) spot,. m the ASS Laboratory, az req.. by USU., All J. am per ard roamed co ensure compliance with Or Mere rekrotted SOP, and pro, seeciflobona In ,n0 Aatamaw= to lubutm,89,Q98,t9 Auaaw,ca 7Q. .7Conaol Mm o4,
Rls, Leo, Loh m.tm<.p:w [Ms, six), omdrplmta. wfrrma pit. a m4ra 11.ISD, 51'X Dur, our. uQ.
rant 9.O kaftan.. and Trrh plot Nitro.,
The fonowiegmc gondolier descriptions Out may Muted throughout this SOO and ore emoted with Mau nomad samp. m earla SDG unto as appropnan
• -Er -ex slaw eal,lson ranee of Mr hod - Am, took= faun mom, Minion
• -ennuamtaan model batmen Ma Ishrautryf.muncra determined Method Dm. Lmut OfDLPLuna (OD, and the Pmettol Quanotaban Luau rPOLYOnto Of Quantmetton
: ASS eamentratron roan.. MI. Joe hbordorybnortuncat Mehad De retion Loot NOLVLinsol
OtQuaoloatten (1.0Q) sml the mono. Stout To Nom Rano (SNR)of aormorantely IC, I analyte romodrom tro rrnthad blank cm.. reach, limit
-arulyu nMdcleciod aborc MDL/ LOD 'F. - indica. lady, Iw asooSed bad or tamp, spathe QAMC <Meal !Oita
- Mtmta minx total.. 9"- Lu1,mles son ratio balsam IS and la %Km.. ann.. "NA' - rod.. an ram mot.
Am pie QAUQCMd is def.ed as no morp 0.70 mortal otoluding method blanks(MO.LRph moire.. Wanks (RS EMI, LC,. mama mikes (LFM, MS, SPX, and duplicates whechor sotked or mans GPM, kW% SP,: DUP. DU, LAS
note nellurrahlo
Slsonnir itrreinf. (-nolo or (Tory,. Soft tfohltne Ttor, Thu das pmlam mu... • Level II pmk.te;o4., deternetod MOM. God L L060 IV DV, LTA RS COW . made. can reeved There nom no borkomd. hammy shoo coos.. for dna pro,
Samples same delivered olmeIly ATS by Poll Corporatun Butt Same. wort moned with moor dud of custody rocooda included Sample eon...n and anensaho Ira, .tiler . her presented on the "Sample Race, motion alai...on or in iM comma. on cruhvutuald..0.. All samples woe prepared and analysed within 43 4sys .11, stet follnatn,
Sitnillir Analyst,
L.1,1b.onadodysaaffraS, Smirsk, were analymd by puma and trap GCIMS In moardancc want LISLTA Oslo: S/2/72 ahtnad: method CVO (Valuate Oros. Compounds by hobo Glutton Gas Cloomumnaphy - Mau Spectrometry). An
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From: kende, Gage <gage_tromelobpollsan” Sane Mond,. Apnl 25.2022 3121 Om T Jon Bradley Subject eCOC 4/25/2822
Typo. My mistake. The two roonnorIng wells [ant today are standard turnaround.
lboblah mutt was not co.ected. if the result cornea back 6 00 m uw won, w. bavo to Uwe with that result.
Gage gitt,r r°"d°' tatahl, alONa MUG tar.A.MENI.
tTillf.rogr,:1;r4=4:117.,. 1,0.8, fin, 13,a88,4o, ImadloYeannarborlachnlealserelooccon,Sant: Monday, AO 25, 2022 2:48 PM To:In:m.1,0ga teagetr.delOpall.00r. Subject RE: Pan eCOC4/25/2022
This Maass. Is From an EMMA/ Sander TO, ammo arm (ter am4. your ...OM. Use eadkon urban OP.FO
Gape, I have o candle of questions for you.
You Irdloted urgent turn for MW-BE-1d and MW.DE.Is that tine,And my records Indloto that MW.BE-ldthould be around 94.0 I mad an ',Intel result of around SOCppb. I am
N/TMIlly ILIVM•rg another dilution, Is Pats sornethIrd acto oautd coot,
Thanks Jim
From: Tramiel, Gana eras, trendrilenalsome Sant Monday, April PS, 2022 855 AM To: Sarah Strobblafteldejorah StoMM•flentommarbort•dIntrattonares Acme; Mark Paton, 6500 0.1.8faa....tos.k.11.9v1,, ,.. Cc David Stubblefield <n... OuhldneeldfannnathenerMdra,mvIrns end,
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ATS Project Number: G001.002
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ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0426221
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ORGANIC ANALYSIS 1,4-Dioxane by GC/MS
USEPA 1624
LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: C001-002 Report Date: 5/2/22 SRF / SDG Number(s): 0427221 Client PO Number: 4505179649
Cn•r Narrative Summary
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Pro). N.M. Pall Corporation ATS Proloct Number. G001-002
ATS Report Numbar(a): Client PO Number. :g77649-4 " 21
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IF YOU DO NOT RECEIVE ALL PAGES OF THIS TRANSMITTAL, PLEASE GU. T34.096120DS.
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ORGANIC ANALYSIS 1,4-Dioxane by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0428221
Prepared By: AAA Arbor Technical Salaam, Inc.
290 S.. Wagner Road Ann Arbor. MI 48103
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LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: C001-002 Report Date: 5/2/22 SRI' / SDG Number(s): 0428221 Client PO Number: 4505179649
Cate Narrative Simms, ro
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woody ream. included. Sample medium ooil mambo, iroy, on elew remand in ...note Itinalpr .ratione(0:.eronortoe,e ammo. en indryidusl ea* Win. All unpin, wax plgv 4rdsubs.. within
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QUALITY ASS U.NC E/ DUALITY CONTROL SU V VA RY TAB ORATORY BLANK SUL/ VARY
PPS MICA I224
OlPC CaPL/Par CCOR.S2122I
SCO 0411221
CXICC222
Arc:AC.0r 522/112
Laboratory Repent BUM (LAB)/ W Bad BYnk(UB)
Ye Imps 0 IA.aN.OaIAa Plialia•pc.r. cm I rw. La. la.. I after mar... I am., c.. um I cara. I P 11114:1.72 PISe9 Our I.Pana
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ANN ARBOR TECHNICAL SERVICES, INC.
O UA LITY ASS URM/C E / QUALITY CONTROL SUV VARY
LABORATORY AC C UI.CY SU,/ VARY
PPS USEP IS.21
O.4 SuPal OCOAC.2l22I
SCG C.4.221
ApcIParte, 002,402.22
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Laboratory Faatifiad Blank (ISM I Labalattay Cont/ol Sample &CS)/ Onto.. Poschlan and Accuracy (OPR)
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QUALITY ASSURANC E /QUALTY CORI ROL SUMMARY
LABORATORY ACCURACY SUL/ MARY
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ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASSURANCE/ QUALITY CONTROL SUMMARY
U./WORT ACCURACY SUVYAAY
Mdse CUM Val
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000100222 CP., Bat 12.2
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IPI 1,111 0 I P.1.411.1111..P.P.I..P.P.• 1411121141.7 PISS. .115$ 1.411.1.0 .41.1 .111 tea 41.1. .14 O. III 14
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ATS Project Number.
ATS Report Number(s):
Client PO Number:
Data Transmittal Covor Page
Poll Corporation
G001.002
° 2 i17fa8"7 rt "2214
Prole. Dageplpslop; Thn deto repeat collates. noets. of 15 wt. , same., received by ATS On 4420.2022 to be analyzed far 1.4 Daum
We coney theleweawca• aninphis lee yes mend nn. Pews onnopsted in aertions• nn canhonea neathel tn. anemone ens•denl wet rase. and me cannehrit sehOchineap,neeelmideserthlein• vein WandertICC•AffnOPPOW.• ...ID To ArllAtAndou,•• A.A•A ery ULM. tenordisep.aalwes. CON.. CARIC latennden snIsta• noe ...la at tow More. spates.. Ww
now s n sale ear newt ad ...We u• l• presemslIcA•AO ream Mme wit.* h.. mat
Recipient MP Oew Tete.
MR of Page. Itneluellno cover POI 27
Ernst wee Imn0,lainn , ...
FAX Number,
Frew Sam Stubbbllekl Death Swan ,,,r11+.1.1,,,Ann,,,,,,,,,,h101, •••T thnowes.c•usds *Ayr PAX Num.: nt-oa-ani
MOM. Weeps: Coopepeet to: Pothsesent. (teenspennesealaSpoleons). Made, Ant broda0pancoin,
Rolle Strohm Amanda laAnalle (amen. inebotedIcsalleern)
0.1e. 5f202 Maned:
If YOU 00 NOT RECEIVE ALL PAGES Cf DOMAN:40T, PLEASE CALL 73.00,0006.
Teem haaw•ews,...ese inaweau w *on wen«.1 am ...swam Menem imnownhpie•ow swPwcwit •wie••••.../...........werwhh we*. tow .was os• nnwhenc*pw wow seetecturance•••••nwasosereasaser wepspeeen * ma..vwaayP.IW6 npaowne.A•0*•
*ie. M.. melon. taneensretvaweeena Thawso•
WonnOWSIT7AII,1••••••ahl,•••,..00.•
Semn.b. Retch. Chain efCmtmtvRrcnrdr. and I I °Inlet Timm sem. AnnIvgit
Semple wets.'divert.'&replya ATS by Pall Corpora.. daft 5sinples hem cached with p.p....of cmi sec.. low h., :ample condition end.mrallet.daoY..n 0thee inesewnot1 the, SceisitIeRn501,section of lbws cep. at the onsennadit ow individual diesel.. AO samples were papered end an vnthle
aye with the followit. ace*. • Rene
note REVIeve nnA Annmvel
All et. contained in dn. new Meehan generated le seceselan“ with nusklines provided b the teferained denten' tese method, and are wanton whit detail.' pro“dutoodesembtal in emcee etandanlopessunn picadors. (SON) specific to the ATS Lalsontioty, es teenoted by MEP& All...eau pea widen...Iasi teviawed to en* unnellance with the show refwercad SOP, end pm, specifications. In widen, all tlitia conform to the leteratety, Quality Menne. /()any Cannel MUM..
A mini. CAR/Clutch is dared as no noose Mae. week. escludiwg methed blurb OAR LAD, fondled blanks (ER LIR, RCS, ususts spit. (AIS. SPX), and duplgetca whether spiked or caw OAS, SMC DUP. DUI. 1.50
pate Onellncerlone. SnrsincatInns. end Technkal Narration
11.6 fallowing era qualifier deeenptiont del may be used thfoughout Otis SW endue pnwental wt. Men associated sampled le ems SOO when se percipient
area doe oh brat. nap.. method • - mu/tuba Os= week dokonen • ..1. -cenceenonon evened bows. the lalsopenoyAnstranced duermirowl Method N.J. Lima
0•101,Riasit Of S.M. (LOD), and the Practical QwNMIon Limit (POLVLIinit Of C.w.o..
0 05 15.400. - toncannitIon repotted babw p. lobonatoeynowereencon Method Deaden (AIDI,Lonolt 0 10. 00Pan MOO:and. lesi.nent Sipa To Rohe Re. 0700 of einnecisnaWIY 10:111. -analyte ceaceelnitssit too method blank cm.. moorhen look V -.sable need... abase >COL/ LOD
ladgesen ma/. he cm:0.41N. or temple specific 0 , QC ssonnol ire. •M•-brdlalo inane inexicoence `r- Indiana oon sello between 15 and 50 IS acceptance window `NV- indica. ion mile Meade 3055 acceplancs window and meek ia Not Repassed
A ueeirQA,QC ewe tad.... no mono then 20 temples auto.. method Nate (Mb, LOB, loralled blanks laR LP11. LOU metros RIO. (UM. MR Sr K)...1 Pond.ata whet., eeSsed ere n0. (t1.0 ROSS. S01,DUI, DUP. IA).
1..411mancAmivelfnCAIII, Samples were enaYivd by 'wee top CONI5 in ...dance st0 OREM mashed 1624 Notstile Oran. Campo. by Isotope Dilution Gee Cleanueoppaphy - Mum Spectrometry). An inWW calibrehen with et knot five 'cycle was wood to quantitate 1.4•Diesene. Rune. wens repo. le project .nrcifiereporeng Well.. Steeples see repnd ae mpL
olaornalx • Nana
Semple Mad,
Sonse wenn..a compets& sn concentrennen above. maul cobbling, cur. woe clamed ndeanlyadfa thou isonspounds. The folkwing millets:twat diluted for 1,1hosaese:
• Itaill5w4.0102
jebnmiert Rearent Meek,
A loonies, mien, blInk (ISUO woe enalyved ea pert of the ONOC batch The LAI3 ten the imcepensec enteral with the femme, eacnelenc
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Ti.4 method valuer letermi Stenennis ce/y. not Sump,. !atonal andante out and Mennen Wt. mat On iitteptabOeCriftria with the following exceplAnx
Arrlitt ACV
I aluornten. Fortified Plank, (En/C/1. M I eboriano, Central Senn,In • AM .,
A Lamm, fortified blank ttrwomo una analyted .1, Ida QMQCM.1 The IYWOrIt ma dm worphiree ottuw web . Woven uncistime
• New
rantrl‘ Seiko and Mat. Snit,. Duplicate,- A rcurno,
Nita Rrlivereblm A SAM spike (510)seld MOM spike dophoese (.450) was enelyad u patent INCA= bald. Mc hISRASD,nett the seamy iwcaphiAN win the following anyhow:
Misdate pack. come.. a Level II ph:14.g other data typed pelmet:ea.. I. Level IV DV1, EPA R5 EDI0 • None
sae esvil.bla mean regent These was no haroloopy data mown, sheens nenaethl fa ate pwjeW.
Coet.01.0,oestutew 06010,11.01,41.1 AA
ORGANIC ANALYSIS 1,4-Dioxanc by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0429221
Prepared By:
Ann Arbor Technical Services. Inc. 290 South Wegner Reed
Ann Arbor, M145101
PRECISION
Matriv , nlke and Metric Snlire nonfinite.- Precis',
A ma= NA. (PAS)*Al nuamepAegluilho. 0010 was ens0scif apwtof as 0 , 0Ohetch. The ...SO ,net the precluoa m.p.g.:aliens with. folbesng execrate.
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LABORATORY OPERATIONS
CASE NARRATIVE
ATS Project Number: C001-002
Report Date: 5/2/22
SRI: / SDC Number(s): 0429221
Client PO Number: 4505179649
Cr, Narrative Snmmery
'Miscast mural. sophist to . Weaving 15 amok, that wen mowed alAnn Actor 1.4shakal Sermes Is (ATM on A., and emaciated InalnassPeclac QMQ0
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Upn receipt samples wasacheddedfar the fol/owing mat,.
Astaats SicelnetSetreba • io•eenetusrPA itao - Uwe V, • , S.e.ne• • i.e.m Fei.b•em • 1,e0waeneROEPA I650-12man TAT • Suple.
• 1.411shane (MEM ION,-Slang TAT • ..P.•
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Project Name: Pall Corporation
ATS Project Number. 0001.002
ATS Report No.:10qm): Org_SRF_0S02221
Client PO Number: 4505170840
peningtOnncriptIgn: Thn dale npen contain, too matt. of 0 water onemine,neon. ATT, 02. :OM b be 'Indy:altar IA Cram..
We envy Pm. a.. analyses b me neon p.ueoeen eon*, M etecedenee nInevid•One• Dawn.
Mew nneeanoul mann.10 ton onenee,n1 eensbeenlann dended vow.. *son. M•eMerOW./ cnendeg tonne ION AID Laaseelenee.m et.. by USW& Let*. au *ft, 60Ps. W CIACIC Idomelen N wed.. bmaMbned eedtel..banneeeneenrenenL Urkao epodnean,ree.0 on Ow dm. new, WI...tie •ovele exam. end Nang *me net**.Item been fra.
Rachman W. Cepa Teem.
No. of No.'s (Inducting...0>LO: 10
From Soren owebiadd es..
Caulk aNnt_IMelenetbre
FAX Number:
_Soren SuNeellitamarmanencelenu•tmm FAX Nuenbec 13406,3731
AddltIonol Copy recent*: Pederson. l(eilh dlen.gallortonegpatcom, Mode. Jen Om bradeelnelLo, nq Nett fib.naml (ItanhnunritIvonn.com), neacdalSe.,.......drAPPIP, Su. Pelee fw•pq•nmpamm)
Amanda Mane. wow. ealaniaetpat cone
Dale: acre Signed:
IF YOU 00 NOT RECEIVE ALL PA0E3 OF TNIS TRANCAIITI, PLEASE CALL 734.00-0995.
TMn,.bar veintose,e ..ta• ono ire* •neern•nnen es.* we wean,. ran.. new per... ream ...I OM av .....r."04.4.42.0a.6. VW.* rvevnew ......•PAt.ine•on4enelneencne TM1014..
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ORGANIC ANALYSIS 1,4-Dioxane by GC/MS
USEPA 1624
ATS Project Number: G001-002.22
ATS SDG: 0502221
Prepared By: Ann Arbor Tectnical Services, loc.
290 South Wagner Road Ann Arbor, M140103
11
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LABORATORY OPERATIONS CASE NARRATIVE
ATS Project Number: 0001-002 Report Date: 5/922 SRF / SDC Number(s): 0502221 Client PO Number: 4505179649
Cele NerretIve Summery
oase wee. applies doe following 6 sunpla (An, an 5: ed aunceded mania-speofkQNQC
F4mPL tae'.I le Wn•efoc,,___
nu:errata Ann Aker Techiaad Seneca, Inc
Rest...en A.ned Tien An.. Mum
Ilee.o. 54,27
Ondale0I leen. Le-ne••• Wenr•
Redraw., Inn3
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tare I 44Nenee Wne•
5,2, t1
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Pv.:e
Upon receipt sampka 'me sdkedeled fee Ibe PAU.. Early..
6gebsu EINSWALILMX0 • Le-Dienane RPXPA Urger., TAT • S Samples • I Men. Fp.. I Manx Sp. nuelnr•
• I.e.lanune (LIM - SuAlud TAT • I S..
cgmple RrtrinL Chain nf rnaIrody ROAM., end .Olding
Semple were debvered domed, a ATS by Pell Connived= AWL Sample. were 'calved Inth pm, chain of nintody am, Included. Semple an.. and mambo. If any. me alba peceental dle - Sample Recap• ember, of Ow report or u. the wenn. on mirmianaua nun, All sample rot peepaged and analysed neon
days rie. Ibe Collmnag excerdanc • Nene
glnaens.0/0,430.0Ixec
CannAkewhe. CAerenn,f Lamonneent/Sarnee 2110SWIP Wegner Reed,Me Arme. WA. 4,03 147114005.09)6 coe 73.6.3731
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_AUL_ ANN ARBOR TECHNICAL SERVICES, INC.
QUALITY ASS URANC E QUALITY CONTROL 5U V VARY
LABORATORY BLANK SU // VARY
ltnat MMUS! Gam eateroaroar 0CCX40002221 LOX 0561721 Palma/Ka. GOOKCITZI R•pxt Dar WeZ2.2
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QUALITY ASSUMIX E !QUALITY CONTROL SUBUARY
LABORATORY ACCURACY 5UV VARY
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QUALITY ASSURABLE I QUALITY CONTROL SU V VARY
LABORATORY ACCURACY SUYVARY
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QUALITY ASS URA/ICE! QUALM CONTROL SU SWART
LABORATORY ACCURACY 5 U LWARY
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ATS Raped Numbor(a): Client PO Number:
Project TMs data rap. omlalro em MIA1. Of 0 WI. aampa.. M. 0..1 1,.. 1.10Y CO, 202210 be 011allyoul lor Douro.
WA *4y...I um. .01yeas for .01111.• b•. 0./..11, Onsn.1 In Ma rearm. mdan3 amoonehlard Nnn elal.ell poor.. bud. henna SW.. Open.; MS .A0.1001. 40 00...040Cmbroollon aro ...• far amme. and atoll. labooNalytmon Lwow
nollad co Ma deb noot einpocem.cem iromeamo eltl bdona hem... wL
Fierbeent Mr. Ooqo 'holdall Coot .qyir tmadmIll,II "Om
FAX Num.,
Na M Peon (Including corer pg.): 18
Foam: Senn Stubbled. Emil: Soo, .11m
woe...sir to. mnom FAX Number: 734-0013731
Aadwonol Mom.: Corm mood to: Poorson... COO pariartonftoollzorK Brod, Jr. Qs) bro.fOrollcom)
IWO StmMra Orstramuertemmqoam/......0.................-0...O...I Amanda lea.. ta/nanda laa..19.111n,
OW: ARS22 Slane.
IF YOU 00 NOT RECEIVE ALL PAC. OF THIS TRANSMITTAL. PLEASE CALL 734-07,000S.
An. p o. wens m......aans. Thant.
man osugooLmoorm.......
Dab Summery Sbeet
Data Transmittal Covor PagoAra mato N..'
=Lae 10
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Pall Corporation Labonory Senses) 0.1.210 ▪ CoLl occo OA MCC 1.2
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