7/27/2019 Thesis_2.doc
1/37
Chapter 2
In-Plant Testing of HydroFloat Separator in Phosphate Industry
2.1 Introduction
2.1.1 General
Teeter bed technologies can only be applied to mineral systems that have a particle size range
and density differences are within acceptable limits. The CrossFlow separator requires a
moderately large difference in particle densities. The unit inherently accumulates low density
coarse particles at the top of the teeter bed, which are too light to penetrate the bed, but at the
same time, too heavy to be carried by the rising water into the overflow. As a result,
misplacement of low-density, coarse particles to the high-density underflow can occur. This
inefficiency can be partially corrected by increasing the elutriation water, to try to carry the low
density coarse particles into the overflow however this can sometimes cause the fine, high-
density particles to also report to the overflow instead of penetrating the teeter bed. !ndustry
representatives identified the need to develop an air assisted hydraulic concentrator that would
combine the fle"ibility of a flotation process with the high capacity of a density separator to
overcome the inefficiencies of the CrossFlow separator.
The limitations of the CrossFlow separator were recognized and overcome through the design of
the #ydroFloat separator. The #ydroFloat can theoretically be applied to any mineral
classification system where differences in apparent density can be created by the selective
attachment of air bubbles. !t incorporates a flotation process with the high capacity of a density
separator. Figure $.% is a schematic of the #ydroFloat separator.
%
7/27/2019 Thesis_2.doc
2/37
#igh &ensity
'ow &ensity
(ubbles
Teeter (ed
!nterface
Float
)roduct
*ater
Addition
Float
+e,ect
&ewatering
Cone
-eparation
Chamber
Feed
Circulation
'oop
.lutriation
/etwo r0
Figure 2.1. Schematic draing of HydroFloat separator
The device operates similar to a traditional CrossFlow separator with the feed settling against an
upward current of fluidization water. 1nli0e the CrossFlow, the #ydroFloat utilizes compressed
air and a small amount of frothing agent in the fluidization water to produce fine air bubbles.
+eagentized feed is introduced into the top of the separator where the feed particles are allowed
to settle based on their size and2or density. )reviously treated with a collector to ma0e one or
more of the minerals hydrophobic, the particles within the separation chamber attach to the small
bubbles, reducing their effective density. These lighter bubble-particle aggregates rise through
the separation chamber, through the teeter bed and overflow the top of the #ydroFloat separator
$
7/27/2019 Thesis_2.doc
3/37
into the product launder. The hydrophilic particles move down through the teeter bed and are
eventually discharged through the control valve at the bottom of the separator.
2.1.2 !d"antages of a Hydraulic separator o"er con"entional froth flotation cells
The use of a fluidized bed over conventional flotation significantly improves the recovery of
particles by 3i4 reducing turbulence, 3ii4 enhancing buoyancy, 3iii4 increasing particle retention
time, and 3iv4 improving bubble-particle contact.
The presence of the high-solids teeter bed reduces the turbulence commonly associated in
traditional flotation units and therefore enhances the buoyancy of the particles. The teetering
effect of the hindered-bed relinquishes the need for bubble-particle aggregates to have sufficient
buoyancy to rise to the top of the cell. The low density agglomerates can easily overflow into the
product launder, where as the hydrophilic particles move through the teeter bed and eventually
discharge through the control valve at the bottom of the separator.
5ther benefits of the #ydroFloat separator versus traditional froth flotation cells include
increases in particle retention time by producing a counter-current flow of particles settling in a
hindered state against an upward rising current of water, and the increased probability of bubble-
particle contacting in the teeter-bed due to the high-solids content. A higher production rate is
possible with the #ydroFloat separator than in traditional froth flotation cells due to the high
percent solids in the compact teeter bed.
6
7/27/2019 Thesis_2.doc
4/37
The #ydroFloat separator is ideally suited to recover coarse particles that traditional froth
flotation cells cannot efficiently recover for several reasons. 5ne reason for the improved
recovery of coarse particles is the upward flow of elutriation water in the #ydroFloat separator
helps lift the larger particles into the product launder. econd, the teeter bed produces ideal
conditions for bubble-particle interactions by maintaining high solids content and quiescent flow
conditions. !n addition, the high solids content within the teeter-bed separator ma0es it possible
to treat large tonnages in a very compact volume as compared to conventional flotation
separations which are conducted at very low solids contents using large volume cells.
2.1.# Pro$ect %ustification
5ne of the driving forces behind the #ydroFloat separator is the phosphate industry7s need to
recover coarse particle phosphate 38$9 " 6:; size fraction4 from the feed matri". !t is estimated
that %?.:-%: million of
revenues.
As in the coal industry, the energy benefits of the #ydroFloat over conventional equipment are
related to the reduction in pumping requirements and water usage which is a direct result of the
higher feed ton rate. The lower operating and maintenance cost per ton of product is
significantly reduced with the #ydroFloat versus conventional equipment. 5verall, the
implementation of the #ydroFloat separator will allow operations to become more profitable and
@
7/27/2019 Thesis_2.doc
5/37
more competitive by utilizing reserves more effectively, reducing waste and increasing
productivity.
:
7/27/2019 Thesis_2.doc
6/37
2.2 &iterature 'e"ie
2.2.1 General
The recovery of minerals by flotation is one of the most versatile mineral-processing techniques
used in industry today. Flotation methods are utilized throughout the mining industry to treat
sulfide ores such as copper, lead and zinc, o"ide ores such as hematite and cassiterite and non-
metallic ores such as phosphate and coal 3*ills, %$4. ince its inception in the early %
7/27/2019 Thesis_2.doc
7/37
reduction in the flotation rate of the particles 3Bameson, %??4. !t can be seen that the efficiency
of the froth flotation process deteriorates rapidly when operating in the e"tremely fine or coarse
particle size ranges, which is considered between %
7/27/2019 Thesis_2.doc
8/37
The variety of flotation machines available on the mar0et today can be classified into two
distinct groupsG pneumatic and mechanical machines 3*ills, %$4. )neumatic machines
commonly utilize air that is blown in or induced, where it must be dissipated through a series of
baffles or some form of permeable base within the cell. ince air is used not only to produce the
froth and create aeration but also to maintain the suspension and to circulate it, an e"cessive
amount is usually introduced 3*ills, %$4. Complications directly related to the e"cessive
amount of air limited the use of pneumatic machines until the development of the flotation
column.
;echanical flotation machines are the most common and widely used flotation machine on the
mar0et today. The units are characterized by a mechanically driven impeller which agitates the
slurry and disperses the incoming air into small bubbles 3*ills, %$4. Air addition into the cell
can either be forced through an e"ternal blower, or self-aerating. Typically most mechanical
flotation cells are set up in a series of Jban0sK, where several cells will allow free flow from one
cell to the ne"t down the ban0.
)erformance is generally based on three factors includingG 3i4 ;etallurgical performance, i.e.,
product recovery and grade, 3ii4 Capacity, and 3iii4 5perating and maintenance costs 3*ills,
%$4. An analysis of the effectiveness of the various types of flotation machines was made by
Loung 3%9$4, who discusses performance with regard to the basic obectives of flotation, which
are the recovery of the hydrophobic species into the froth product, while still achieving a high
selectivity by retaining as much as the hydrophilic species as possible in the slurry. +ecovery is
directly related to particle-bubble attachment and requires quiescent conditions, which is not
9
7/27/2019 Thesis_2.doc
9/37
found in conventional mechanical flotation devices. The mechanical impellers found in typical
flotation cells are not ideal for particle-bubble contact, which has led the industry to utilize
column cells for a variety of mineral applications that, up until the past decade or two, was
unheard of.
Column cells are considered to be ideal displacement machines, where as mechanical cells are
ideal mi"ers 3*ills, %$4. A column cells improves recoveries by minimizing turbulence within
the cell and froth washing. !n %%@, .;. Callow patented the first apparatus with air sparging
through a porous false bottom, 3+ubinstein, %:4, which would become the basis for future
column cell designs. (y %%, ;. Town and . Flynn had developed the first design involving a
countercurrent of slurry and air within a column. And while pneumatic Callow apparatuses were
very popular in the early %$
7/27/2019 Thesis_2.doc
10/37
2.2.# Phosphate Flotation
)hosphate beneficiation plants are designed to process run-of-mine ore, typically called the ore
matri", into a sellable product for use in either the fertilizer mar0et or as an integral part or the
production of phosphoric acid. The ore matri" is upgraded by separating the phosphate grains
from other impurities such as clay and silica. (eneficiation plants in the outheastern 1nited
tates 3Florida and /orth Carolina4 generally use sizing and classification processes to
concentrate the phosphate roc0 and separate it from impurities.
Florida beneficiation plants typically wash and deslime the ore matri" at %:< mesh. The material
finer than %:< mesh is considered tailings and is pumped to settling ponds. Appro"imately 6
7/27/2019 Thesis_2.doc
11/37
The industry, however, has ta0en other approaches to circumvent the problem of low floatability
of coarse particles. For instance, such approaches are e"emplified by the use of gravitational
devices such as spirals, tables, launders, sluices and belt conveyors modified to perform a Ns0in
flotationN of the reagentized pulp. Although a variable degree of success is obtained with these
methods, they have to be normally supplemented by scavenger flotation. !n addition, some of
them require e"cessive maintenance have low capacity or high operating costs. Their
performance is less than satisfactory and in certain cases their use has been discontinued.
)revious laboratory and pilot-scale testing of the #ydroFloat separator has proven its capabilities
as an effective flotation device for recovering fine and coarse phosphate. The unit has especially
proven successful in the 86: mesh fraction of the phosphate ore matri" in Florida. This size
fraction was previously discarded to the tailings when detachment and buoyancy limitations in
traditional flotation methods failed to recover the material.
%%
7/27/2019 Thesis_2.doc
12/37
2.# In-Plant Testing at Phosphate Plant ! (I)C*
The )hase ! field-testing of the #ydroFloat separator involved 3i4 equipment setup, 3ii4
sha0edown testing, and 3iii4 detailed testing at the )hosphate )lant A. The goal of this effort was
to compare the unit to e"isting conventional cells in several different areas of the plant by
analyzing the anticipated product grade and recovery, insol content, reagent consumption, and
feed capacity at, and above, design feed rates of the unit. The three areas of the plant where the
#ydroFloat separator was tested included the fine feed, amine flotation and coarse feed circuits.
The main obective of the fine and coarse phosphate testing was to demonstrate the potential of
the unit as a candidate for the process equipment in a proposed plant design with both fine and
coarse circuits. The main obective of the amine flotation testing was to demonstrate the
feasibility of using the unit for silica flotation and to develop data to determine its potential
application for use in the amine flotation circuit at )hosphate )lant A. Appro"imately months
was allocated to this tas0.
!ndividuals from riez ;agnetics and Iirginia Tech participated in the testing at )hosphate )lant
A with cooperation from 0ey personnel at the processing plant. Additional tests were conducted
by )hosphate )lant A representatives to e"pand the data base for evaluating the potential of
incorporating the #ydroFloat separator into proposed circuit upgrades.
%$
7/27/2019 Thesis_2.doc
13/37
2.#.1 +,uipment Setup
2.#.1.1 Fine Circuit
This tas0 focuses on the installation of the pilot-scale unit in the fine feed circuit at )hosphate
)lant A. The separator was transported from the riez ;agnetics Central +esearch 'ab in rie,
)A to the processing plant. *ith cooperation from the operators and mechanics at the plant, the
%9-inch diameter, pilot-scale #ydroFloat separator was installed at the fine circuit at )hosphate
)lant A as shown in Figure $.$. +eagentized feed was supplied to the #ydroFloat separator
through a two-inch line connected to the e"isting plant conditioning tan0s. Concentrate and
tailings streams were discharged into floor sumps.
The unit was operated asa column flotation cell, utilizing the #ydroFloat separator air sparging
system. The test unit included 6 compartments that allowed more water and air to be added 3up
to < gpm water and %< cfm air4. There was no teeter-bed required in this system. )lant
compressed air and %%: volt electrical power were connected to the separator for the automated
control system. The separator was automatically controlled through the use of a simple )!&
control loop which includesa pressure sensor mounted on the side of the separator to measure
the relative pressure 3level4, a single loop )!& controller, and a pneumatic pinch valve to control
the underflow discharge to maintain a constant bed pressure 3level4.
%6
7/27/2019 Thesis_2.doc
14/37
Figure 2.2. 1-inch iameter Pilot-Scale HydroFloat Separator Test Circuit
2.#.1.2 !mine Circuit
The same separator used in the fine circuit was also used in the amine flotation circuit. *ith
cooperation from the operators and mechanics at the plant, the %9-inch diameter, pilot-scale
#ydroFloat separator was installed in the amine circuit at )hosphate )lant A. +eagentized feed
was supplied to the #ydroFloat separator through a two-inch line connected to the e"isting plant
conditioning tan0s. Concentrate and tailings streams were discharged into floorsumps.
%@
7/27/2019 Thesis_2.doc
15/37
The unit was operated as acolumn flotation cell, utilizing the #ydroFloat separator air sparging
system. The test unit included 6 compartments that allowed more water and air to be added 3up
to < gpm water and %< cfm air4. There was no teeter-bed required in this system. )lant
compressed air and %%: volt electrical power were connected to the separator for the automated
control system. The separator was automatically controlled through the use of a simple )!&
control loop which includesa pressure sensor mounted on the side of the separator to measure
the relative pressure 3level4, a single loop )!& controller, and a pneumatic pinch valve to control
the underflow discharge to maintain a constant pressure 3level4.
2.#.1.# Coarse Circuit
The same separator used in the fine and amine flotation circuits was also used in the coarse
circuit, with one modification. The center compartment was removed from the unit, so as to
allow the unit to operate with a typical teeter-bed 3a total of $ compartments4. *ith cooperation
from the operators and mechanics at the plant, the %9-inch diameter, pilot-scale #ydroFloat
separator was installed in the coarse circuit at )hosphate )lant A. +eagentized feed was supplied
to the #ydroFloat through a two-inch line connected to e"isting plant conditioning tan0s.
Concentrate and tailings streams were discharged into floorsumps.
)lant compressed air and %%: volt electrical power were connected to the separator for the
automated control system. The separator was automatically controlled through the use of a
simple )!& control loop which includesa pressure sensor mounted on the side of the separator to
measure the relative pressure, a single loop )!& controller, and a pneumatic pinch valve to
control the underflow discharge to maintain a constant bed pressure.
%:
7/27/2019 Thesis_2.doc
16/37
2.#.2 Sha/edon Testing
After completing the installation of the test #ydroFloat unit, preliminary sha0edown testing was
conducted to resolve any une"pected operational problems that could arise. These tests are
normally necessary to resolve any problems that may have been overloo0ed in the initial
engineering and to confirm that feed capabilities, pipe sizes, electrical supplies, control systems,
etc., are adequate. An average of si" sha0edown tests per circuit was conducted with the unit.
2.#.# etailed Testing
Two series of detailed test programs were conducted using the pilot-scale test unit. The first
series of test were performed to investigate the effects of the 0ey design variables on separator
performance and to simultaneously define the overall grade and recovery curve.
The #ydroFloat separatoris designed for feed rates of $ tph2ft$and % tph2ft$rougher concentrate,
which allows the test unit to operate at @ tph feed and $ tph concentrate, respectively. The initial
testing in the fine and coarse circuit evaluated the unit at loading rates much higher than design
to establish the recovery fall-off. The design rates for the amine flotation circuit were not
precisely 0nown going into the testing, but were thought to be similar to those for rougher
flotation. )art of the amine testing program was devoted to determining the design rates and
evaluating the #ydroFloat separator performance across the board, both at the design rate and
above.
%
7/27/2019 Thesis_2.doc
17/37
*ith the recovery fall-offdetermined for each circuit and unit configuration, the subsequent
series of testing was used to investigate the effects of 0ey operating parameters. Tests were
conducted to establish reagent consumption 3fatty acid, surfactant, amine and diesel oil4, to
investigate the bed levels and sparger water required for the best unit operation and to investigate
the variability associated with the overall system. For each test, samples were ta0en from the
feed, concentrate and tailings streams after conditions were stabilized. The samples were
analyzed for ()', ;g5 and insol.
2.#.0 Process +"aluation
To ensure the test data was reliable and self-consistent, all as-received results were analyzed and
adusted using a commercially available mass-balance program. "perimental values that were
deemed by the mass balance routines to be unreliable were removed from the data set. The
participating mining company used the compiled data to establish the metallurgical
improvement, operating savings and economic paybac0 that may be realized by implementing
the proposed high-efficiency technologies.
The process evaluation has been divided into three sections including 3i4 fine feed circuit, 3ii4
amine flotation circuit, and 3iii4 the coarse feed circuit.
2.#.0.1 Fine Circuit
Fifty-three tests were conducted during the fine circuit testing at )hosphate )lant A. Testing in
the fine circuit produced an average of %
7/27/2019 Thesis_2.doc
18/37
#ydroFloat separator and plant tails percent ()' for each test. The plant *emco cells averaged
only about
7/27/2019 Thesis_2.doc
19/37
Figure 2.0. 'ougher Concentrate Grade of HydroFloat Separator "ersus Plant Cells
&uring testing, several attempts were made to obtain final grade concentrates 3?= insol4 with
one stage of flotation. The results show that insol concentrates between -%
7/27/2019 Thesis_2.doc
20/37
recovered 9
7/27/2019 Thesis_2.doc
21/37
+eagent dosages were affected by the poor water quality and e"cessive slimes in the feed during
the testing program. The fatty acid dosagein the plant ranged from
7/27/2019 Thesis_2.doc
22/37
2.#.0.2 !mine Circuit
Twenty-four tests were conducted during the amine flotation circuit testing at )hosphate )lant A.
#ydroFloat separator testing in the amine flotation circuit produced an average of %.6= higher
insol concentrate and recovered about 9= less insol to the amine tailings than in the )lant
*emco Cell. Figure $. displays the concentrate grade for the #ydroFloat separator and the
plant for each test. The plant *emco cells averaged only about
7/27/2019 Thesis_2.doc
23/37
Figure 2.3. !mine Concentrate Grade Comparison of HydroFloat Separator
"ersus Plant Cells
$6
7/27/2019 Thesis_2.doc
24/37
Figure 2.4. 5P& 'eco"ery Comparisons HydroFloat Separator "ersus Plant Cells
5ne of the most important operating parameters to consider for amine flotation is the ability of
the process equipment to recover coarse silica without recovering phosphate. Comparison testing
of the #ydroFloat separator with the *emco Cell produced promising results. As shown in
Figure $.9, the #ydroFloat separator had ust slightly less recoveries than the plant for all of the
size fractions e"cept the 6: mesh, where it had a nearly = increase in ()' recovery than the
plant.
$@
7/27/2019 Thesis_2.doc
25/37
Figure 2.. Comparison of Test 'esults for !mine Phosphate (Plant Circuit 2*
+eagent dosages were affected by the poor water quality and e"cessive slimes in the feed during
the testing program. The surfactant dosage for the #ydroFloat separator ranged from
7/27/2019 Thesis_2.doc
26/37
*hile the operation of the #ydroFloat separator for amine flotation was difficult to optimize due
to various outside variables affecting the system, a significant number of tests were conducted at
differing operating variables undervarying operating conditions to achieve optimum operating
conditions. The optimum conditions for the #ydroFloat separator for use in amine flotation as
defined by this testing program areG 6 compartment sections, with bed level between ?
7/27/2019 Thesis_2.doc
27/37
from $.
7/27/2019 Thesis_2.doc
28/37
Figure 2.17. 'eco"ery Comparison of HydroFloat Separator "ersusPlant Cells
Figure 2.11. Grade Comparison of HydroFloat Separator "ersus Plant Cells
$9
7/27/2019 Thesis_2.doc
29/37
The ability of the unit to recover coarse material into an acceptable concentrate proved to be
successful during the testing program. 5ne test achieved an overall ()' of $= at a feed rate of
6.$ tph 39= of design4 and a concentrate overflow froth rate of %.: tph 3?9= of design4. The
associated concentrate grade was %= ()'.
creen and chemical analyses were conducted on selected tests to determine the recovery
coefficients for various mesh sizes. The #ydroFloat separator recovery coefficients are
considered to be e"cellent asshownin Figure $.%$.
Figure 2.12. Comparison of Test 'esults for Coarse Phosphate (Plant Circuit 1*
)ercent solids in the tailings averaged ?:.9= for all tests. The #ydroFloat separator was
configured with$ compartments, with bed levels between 9$ and 9?, and with a recommended
$
7/27/2019 Thesis_2.doc
30/37
level of 9:. This resulted in optimum condition ofG froth depths between %: and $< inches,
sparger water near $< gpm, and air flow at :.< cfm. The measured recovery coefficients and
concentrate grade at these design rates were acceptable. (ased on this data, the #ydroFloat can
successfully be implemented into the )hosphate )lant A coarse flotation circuit.
2.#. Sample !nalysis
&etailed analysis was conducted on each of the samples collected during the testing program.
The analyses were performed in accordance with AT; procedures onsite at the )hosphate )lant
A. +epresentative samples were collected around the pilot-scale unit. lurry flow rates for the
feed, concentrate and tailings streams were directly measured using a stopwatch and a calibrated
container. The mass and liquid flow rates were then calculated from the measured slurry flow
rates and the sample assays using the two-product formula.
2.#.3 Future 8or/
*hile the results of the testing loo0 promising, the proect has been put on hold until the
company finishes a reorganization proect.
6
7/27/2019 Thesis_2.doc
31/37
2.0 In-Plant Testing at Phosphate Plant 5 (Cargill*
The )hase ! field-testing of the #ydroFloat separator involved 3i4 equipment setup, 3ii4
sha0edown testing, and 3iii4 detailed testing at the )hosphate )lant (. The goal of this effort was
to compare the unit to e"isting conventional cells by analyzing the anticipated product grade and
recovery, insol content, reagent consumption and feed capacity at, and above, design feed rates
of the unit. The main obective of testing was to determine if the #ydroFloat separator could
achieve higher recoveries of the coarse particles than the conventional cells. Appro"imately %$
months was allocated to this tas0. !ndividuals from riez ;agnetics and Iirginia Tech
participated in the testing at )hosphate )lant ( with cooperation from 0ey personnel at the
processing plant.
2.0.1 +,uipment Setup
The separator was transported from the riez ;agnetics Central +esearch 'ab in rie, )A to the
processing plant. *ith cooperation from the operators and mechanics at the plant, the %-foot
diameter, pilot-scale #ydroFloat separator was installed in the coarse circuit at )hosphate )lant
( as shown in Figure $.%6. +eagentized feed was supplied to the #ydroFloat separator through a
two-inch line connected to the e"isting plant conditioning tan0s. Concentrate and tailings
streams were discharged into floorsumps.
)lant compressed air and %%: volt electrical power were connected to the separator for the
automated control system. The separator was automatically controlled through the use of a
simple )!& control loop which includesa pressure sensor mounted on the side of the separator to
measure the relative pressure 3level4, a single loop )!& controller, and a pneumatic pinch valve
6%
7/27/2019 Thesis_2.doc
32/37
to control the underflow discharge to maintain a constant bed pressure 3level4. Clarified water
was connected to the separator to create the fluidized teeter bed of solids.
Figure 2.1#. Pilot-Scale HydroFloat Separator Test Circuit
2.0.2 Sha/edon Testing
After completing the installation of the test #ydroFloat unit, preliminary sha0edown testing was
conducted to resolve any une"pected operational problems that could arise. These tests are
normally necessary to resolve any problems that may have been overloo0ed in the initial
engineering and to confirm that feed capabilities, pipe sizes, electrical supplies, control systems,
etc., are adequate.
6$
7/27/2019 Thesis_2.doc
33/37
2.0.# etailed Testing
Two series of detailed test programs were conducted using the pilot-scale test unit. The first
series of test were performed to investigate the effects of the 0ey design variables on separator
performance and to simultaneously define the overall grade and recovery curve.
The #ydroFloat separator is designed for feed rates of $ tph2sqft and % tph2sqft rougher
concentrate, which allows the test unit to operate at @ tph feed and $ tph concentrate,
respectively. The initial testing in the coarse circuit evaluated the unit at loading rates much
higher than design, to establish the recovery fall-off.
*ith the recovery fall-offdetermined for each circuit and unit configuration, the subsequent
series of testing was used to investigate the effects of 0ey operating parameters. Tests were
conducted to establish reagent consumption 3fatty acid, surfactant, and diesel oil4, to investigate
the bed levels and sparger water required for the best #ydroFloat separator operation, and to
investigate the variability associated with the overall system. For each test, samples were ta0en
from the feed, concentrate and tailings streams after conditions were stabilized. The samples
were analyzed for ()', ;g5, and insol.
2.0.0 Process +"aluation
To ensure the test data was reliable and self-consistent, all as-received results were analyzed and
adusted using a commercially available mass-balance program. "perimental values that were
deemed by the mass balance routines to be unreliable were removed from the data set. The
participating mining company used the compiled data to establish the metallurgical
66
7/27/2019 Thesis_2.doc
34/37
improvement, operating savings and economic paybac0 that may be realized by implementing
the proposed high-efficiency technologies. Test results were previously summarized and
reported in preceding documentation and will not be covered in detailed in this report.
2.0. Sample !nalysis
&etailed analysis was conducted on each of the samples collected during the testing program.
The analyses were performed in accordance with AT; procedures onsite at the )hosphate )lant
(. +epresentative samples were collected around the pilot-scale unit. lurry flow rates for the
feed, underflow and overflow streams were directly measured using a stopwatch and a calibrated
container. The mass and liquid flow rates were then calculated from the measured slurry flow
rates and the sample assays using the two-product formula.
2.0.3 Future 8or/
)ilot-scale testing at )hosphate )lant ( in Florida proved to be successful, and the company has
agreed to purchase a prototype #ydroFloat separator for testing against e"isting flotation cells in
the coarse recovery circuit. !nstallation of the prototype is e"pected during eptember $
7/27/2019 Thesis_2.doc
35/37
2. Conclusion
%. 5ne of the goals of this proect is to successfully prove the technology in a sufficient
period of time to minimize the financial ris0 that will be ta0en by industry. The previous
years test wor0 has eliminated the uncertainties associated with the #ydroFloat separator
by proving plant scale units do in fact wor0. This can be seen by the fact that industry
leaders have submitted purchase requests for full scale units in their preparation plants.
(ased on the successful installation of these full scale units, further implementation of
additional units can be utilized in a broad spectrum of companies and industries.
$. Hey design and operating variables have been established based on the performance
capabilities of the #ydroFloat separator. From here, proof-of-concept 3)5C4 tests using a
production-scale unit can be implemented at the various test locations where full scale
prototypes are being installed. The )5C-scale tests will identify critical scale-up criteria
for the design of industrial applications. The )5C-scale tests will also be used to define
the performance capabilities of the high-efficiency processes in an industrial setting and
to fully demonstrate the potential economic benefits that can be realized with the
#ydroFloat separator.
6:
7/27/2019 Thesis_2.doc
36/37
2.3 'eferences
Florida !nstitute of )hosphate +esearch, )ublication /o.
7/27/2019 Thesis_2.doc
37/37
/orth Carolina tate ;inerals +esearch 'aboratory, )ublication /o. $-$@-), %$, J)reliminary
&esliming Tests w2 /C )hosphate 1sing a )ilot-cale 'inate" #ydrosizer,K )repared (yG
chlesinger, '. and #utwel0er, B.
+ubinstein, B.(., %:. Column FlotationG )rocesses, &esigns and )ractices. ordon and (reach
cience )ublishers, 1nited tates.
oto, #. and (arbery, ., %%, JFlotation of Coarse )articles in a Counter-Current Column
Cell,K ;inerals and ;etallurgical )rocessing, Iol. 9, /o. %, pp. %-$%.
*ills, (arry A., %$. ;ineral )rocessing Technology :thdition. )ergamon )ress. Tarrytown,
/ew Lor0.
Loung, )., %9$, JFlotation ;achines,K ;inerals ;agazine, Iol. %@, /o. %, pp. 6:.