Data Pengujian CaCO3'

7/26/2019 Data Pengujian CaCO3'

1/26

Hasil Evaluasi Uji Standarisasi

No Ulangan

1 1 0.1036

0.1033

3 0.1033

4 0.10!

"#rata

1 0.100$

0.100!

3 0.1000

4 0.101"#rata

3 1 0.1000

0.100$

3 0.1003

4 0.1014

"#rata

4 1 0.1031

0.10%3 0.1008

4 0.100$

"#rata

! 1 0.103!

0.10%

3 0.101%

4 0.1031

"#rata6 1 0.10!4

0.1018

3 0.1013

4 0.1006

"#rata

% 1 0.103

0.1011

3 0.10034 0.101

"#rata

&o'ot (sa)O*salat + gra)


2/26

"#rata -otal

Ulangan

1 0.1031 8.40

0.10% 8.40

3 0.100$ 8.0

4 0.101% 8.30

! 0.1010 8.0

6 0.101! 8.!

% 0.100! 8.0

"#rataS

/"S

&o'ot (sa) O*salat+ gra)

olu)# KMnO4+ )L


3/26

Larutan KMnO4 O,18 N

N KMnO4

8.!! 0.180!

8.!! 0.1800

8.!! 0.1800

8.!0 0.1%$6

0.1800

8.30 0.1811

8.! 0.1814

8.! 0.180!

8.40 0.1%$40.1806

8.40 0.1%%3

8.4! 0.1%%$

8.40 0.1%%8

8.4! 0.1%8%

0.1779

8.40 0.188

8.40 0.1818.! 0.180

8.0 0.1833

0.1825

8.!0 0.1814

8.40 0.181

8.30 0.18!

8.40 0.188

0.18228.%0 0.1804

8.3! 0.1816

8.30 0.1818

8.30 0.180!

0.1811

8.!0 0.1808

8.30 0.1814

8.30 0.18008.40 0.1811

0.1808

olu)# KMnO4+ )L


4/26

0.180%

N KMnO4

0.188

0.181

0.1833

0.18!

0.1834

0.180

0.18!

0.186


5/26

Hasil Evaluasi Uji Standarisasi L

&a*u ri)#r 2 Natriu) O*salat

Ulangan

1 0.1031 8.40

0.10% 8.40

3 0.100$ 8.0

4 0.101% 8.30

! 0.1010 8.0

6 0.101! 8.!

% 0.100! 8.0

"#rata

S

/"S

&o'ot Natriu)O*salat +gra)

olu)#KMnO4 +)L


6/26

rutan KMnO4 O,18 N

N KMnO4

0.$$8 0.188

0.$$8 0.181

0.$$8 0.1833

0.$$8 0.18!

0.$$8 0.1834

0.$$8 0.180

0.$$8 0.18!

0.186

0.$8

Kemurnian Natrium

Oksalat

!,44310


7/26

Hasil Evaluasi Uji Standarisasi La

No Ulangan

1 1 0.!000 0.!006

3 0.!003

"#rata

1 0.!18$

0.!040

3 0.!1!0

"#rata

3 1 0.!01 0.!014

3 0.!0

"#rata

4 1 0.4$$4

0.4$$8

3 0.!011

"#rata

! 1 0.!03

0.!01

3 0.!043

"#rata

6 1 0.!186

0.!338

3 0.!340

"#rata

% 1 0.!%88

0.4$$8

3 0.4$$6

"#rata

"#rata -otal

&o'ot 5a5O3 Standar+ gra)


8/26


9/26

Hasil Evaluasi Uji Standarisasi Larutan EDTA ,

#aku $rimer % Kalsium Kar&'nat

Ulan(an )*

1 +"11 1+- 1

! +"18 !+"" 1

. +"- 1+" 1

4 +"4 !+" 1

" +"!! 1+- 1

- +48 1+"" 1

/ +"1" !+! 1

0erata

SD

0SD

#'&'t 2a2O.

Standar 3(ram

5'lume EDTA

3mL


10/26


11/26

Hasil Evaluasi Uji $resisi $eneta*an Kadar 2a2O

K'de Sam*el % #D # 1-!!1

Ulan(an

1 +"8/ ""+-

! +"." "4+

. +"/ "4+

4 +"!" ""+

" +"!. "4+8

- +"18 "4+1

/ +".! "4+40erata

SD

0SD

#'&'t Sam*el 2a2O.

3(

5'lume KMnO4 ,18

N 3mL


12/26

dalam Ka*ur Se7ara SN

2aO

+18!- ""+-

+18!- ""+8.

+18!- ""+!!

+18!- "-+4

+18!- ""+8-

+18!- ""+!

+18!- ""+"-""+--

+.4-

+-!1"

N KMnO4


13/26

Hasil Evaluasi Uji $resisi $eneta*an Kadar 2a2O. d

K'de Sam*el % #D # 1-!!1

Ulan(an

1 , "! 1, 8

! , "11 1, /

. , ".4 1, -

4 , "1" 1, -

" , ""! 1, 8

- , "" 1, -

/ , ""8 1, 80erata

SD

0SD

#'&'t Sam*el 2a2O.

3(

5'lume EDTA Hasil

Standarisasi 3mL


14/26

lam Ka*ur 3 Met'de EDTA

M EDTA )$ 2aO

+!"! 1 "", /4

+!"! 1 "", "-

+!"! 1 "", !

+!"! 1 "", !.

+!"! 1 "", .

+!"! 1 "", .4

+!"! 1 "", .!""+./

+!."

+41-4


15/26

Hasil Evaluasi Uji Akurasi $eneta*an Kadar 2aO d

K'de Sam*el % #D # 1-!!1

Ulan(an#erat 2aO Sam*el 9 S*ike 3(ram

1 +!//" +4111

! +!/8 +4!4

. +!8- +414!

4 +!/-" +418.

" +!81 +4!4

- +!// +41!/

/ +!84- +414/0erata

#erat 2aO Sam*el

3(ram


16/26

lam Ka*ur Se7ara SN

#erat Standar 3(ram 0e7'ver:

+14 "+4-

+14 14+!8

+14 4+.

+14 11+!8

+14 1!+/8

+14 -+.

+14 !+.8+!4


17/26

Hasil Evaluasi Uji Akurasi $eneta*an Kadar 2a2O.

K'de Sam*el % #D # 1-!!1

Ulan(an

1 +!/ +4!11

! +!/1 +41-

. , !/1 +4!18

4 +!/84 +41

" +!81! +4!1

- +!// +41/

/ +!8" +410erata

#erat 2a' Sam*el

3(ram

#erat 2a' Sam*el 9 S*ike

3(ram


18/26


19/26

Hasil Evaluasi Uji Akurasi Penetapan Kadar CaO dalam Kapur Metode SNI 15!"#$1$$

Ulan%an

&ata Penim'an%an &ata Penitaran ml E&(A &ata kadar 'erat CaO

1 0.!006 0,!008 0,!01 0.!01 !4,0 )L 80,30 )L 0.%%! 0.4111

0.!010 0,!018 0,!06 0.!06 !4,30 )L 8,80 )L 0.%80 0.440

3 0.!0!6 0,!0!! 0,!00 0.!00 !!,0 )L 80,$0 )L 0.806 0.414

4 0.!0! 0,!0!$ 0,!04 0.!04 !4,00 )L 81,%0 )L 0.%6! 0.4183

! 0.!00 0,!0$ 0,!0 0.!0 !4,%0 )L 8,80 )L 0.801 0.440

6 0.!01 0,!018 0,!0 0.!0 !4,10 )L 80,60 )L 0.%%0 0.41%

% 0.!0$6 0,!0$1 0,!00 0.!00 !!,60 )L 80,40 )L 0.846 0.414%

Rerata

#erat sam*el

3(ram

#erat sam*el 9

s*ike 3(ram

#erat Standar

3(ram

5'lume KMnO4

sam*el

5'lume KMnO4

sam*el 9 s*ike

#erat 2aO sam*el

3(ram

#erat 2aO sam*el 9

s*ike 3(ram


20/26

) *e+over,

0.1400 $!.46/

0.1400 104.8/

0.1400 $4.03/

0.1400 101.8/

0.1400 10.%8/

0.1400 $6.$3/

0.1400 $.$3/

98.24%

#erat 2aO Standar

3(ram


21/26

Hasil Evaluasi Uji Akurasi Penetapan Kadar CaCO- dalam Kapur Metode In House

Ulan%an

&ata Penim'an%an &ata Penitaran ml E&(A &ata kadar 'erat CaO

1 +"! ,"1 9 ,!"1 +!"1 1,8 mL !,8 mL +!/ +4!11

! +"1/ ,"11 9 ,!" +!" 1,/" mL !," mL +!/1 +41-

. +"1" ,"1/ 9 ,!"! +!"! 1,/" mL !,8" mL , !/1 +4!18

4 +"- ,"" 9 ,!" +!" 1,/ mL !,-" mL +!/84 +41" +"." ,". 9 ,!" +!" 1, mL !,/" mL +!81! +4!1

- +"" ,"" 9 ,!"4 +!"4 1,- mL !,/ mL +!// +41/

/ +"!- ,"! 9 ,!" +!" 1,8" mL !,-" mL +!8" +41

*erata

#erat sam*el

3(ram

#erat sam*el 9 s*ike

3(ram

#erat Standar

3(ram

5'lume EDTA

sam*el

5'lume EDTA

sam*el 9 s*ike

#erat 2aO sam*el

3(ram

#erat 2aO sam*el 9

s*ike 3(ram


22/26

) *e+over,

+14 1+"

+14 8+4!

+14 1!+"

+14 1+4.+14 +4.

+14 1!+.

+14 8+.

1"".-!)

#erat 2aO Standar

3(ram


23/26


24/26

gan Natriu) O*salat

7astian 'a*u


25/26

Hasil Evaluasi Uji $resisi $eneta*an Kadar 2a2O. dalam Ka*ur 3 Met'de EDTA

K'de Sam*el % #D # 1-!!1

Ulan(an

#'&'t Sam*el 2a2O. 3(

M EDTA )$

1 , "! 1, 8 +!"! 1! , "11 1, / +!"! 1

. , ".4 1, - +!"! 1

4 , "1" 1, - +!"! 1

" , ""! 1, 8 +!"! 1

- , "" 1, - +!"! 1

/ , ""8 1, 8 +!"! 1

0erata

SD

0SD

Hasil Evaluasi Uji $resisi $eneta*an Kadar 2a2O. dalam Ka*ur 3Met'de SN

K'de Sam*el % #D # 1-!!1

Ulan(an

#'&'t Sam*el 2a2O. 3( 5'lume KMnO4 ,18 N 3mL

N KMnO4 2aO

1 +"8/ ""+- +18!- ""+-

! +"." "4+ +18!- ""+8.

. +"/ "4+ +18!- ""+!!

4 +"!" ""+ +18!- "-+4" +"!. "4+8 +18!- ""+8-

- +"18 "4+1 +18!- ""+!

/ +".! "4+4 +18!- ""+"-

0erata ""+--

SD +.4-

0SD +-!1"

5'lume EDTA Hasil Standarisasi

3mL


26/26

2aO

"", /4"", "-

"", !

"", !.

"", .

"", .4

"", .!

""+./

+!."

+41-4

Data Pengujian CaCO3'

Documents