UNITED STATES ENVIRONMENTAL PROTECTION AGE rttUblVEO OCTKM991 SECTION REGION 7 25 FUNSTON ROAD KANSAS CITY, KANSAS 66115 OCT Date: MEMORANDUM SUBJECT: Data 'Transmittal for Activity #: Site -Desciption: K^ /s^^^v ^ FROM: Andrea Jirka Chief, Laboratory Branch, ENSV TO: ATTN: Robert Morby Chief, Superfund Branch, WSTM Attached is the data transmittal for the above referenced site. This should be considered a Partial or Complete data transmittal (completes transmittal of / ). If you have have any questions or comments, please contact Dee Simmons at 551-5129. Attachments cc: Data Files NOTE: Please see Mary Gerken, SPFD-WSTM, if you want-an -- ..._—.„ ^ electronic copy of the data. • :• hltaa~?>f) i -J>.- *•••£ I ...... ID a a cOfnua ncrCLRi mm
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25 FUNSTON ROAD KANSAS CITY, KANSAS 66115 OCTKM991 · UNITED STATES ENVIRONMENTAL PROTECTION AGE rttUblVEO OCTKM991 SECTION REGION 7 25 FUNSTON ROAD KANSAS CITY, KANSAS 66115 OCT
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UNITED STATES ENVIRONMENTAL PROTECTION AGE
rttUblVEO
OCTKM991SECTION
REGION 725 FUNSTON ROAD
KANSAS CITY, KANSAS 66115
OCTDate:
MEMORANDUM
SUBJECT: Data 'Transmittal for Activity #:Site -Desciption: K^ /s ^ v
FROM: Andrea JirkaChief, Laboratory Branch, ENSV
TO:
ATTN:
Robert MorbyChief, Superfund Branch, WSTM
Attached is the data transmittal for the above referenced
site. This should be considered a Partial or
Complete data transmittal (completes transmittal of/
). If you have have any questions or
comments, please contact Dee Simmons at 551-5129.
Attachments
cc: Data Files
NOTE: Please see Mary Gerken, SPFD-WSTM, if you want-an -- ..._—.„ ^electronic copy of the data. • :• hltaa~?>f)i-J>.- *•••£ I
. . . . . . ID aa cOfnua ncrCLRi mm
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CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII <2)/
NAME OF SURVEY OR ACTIVITY
ONTH YEAR
CONTENTS OF SHIPMENT
SAMPLENUMBER
TYPE OF CONTAINERS
BOHLEVOA SET
(2 VIALS EA)
NUMBERS OF CONTAINERS PER SAMPLE NUMBER
SAMPLED MEDIA RECEIVING LABORATORY
REMARKS/OTHER INFORMATION(condition ol samples upon receipt.
older sample numbers, etc 1
^X d£Xa y
XX
DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
CONSISTING OF.
. ICE CHEST(S); OTHER
. BOX(ES) -fca COMMERCIAL CARRIER:
.COURIER
SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)
PER/0>JNEL CUSTODY RECORDDATE TIME RECEIVED_BY
UNSEALED
REASON FOR CHANGE OF CUSTODY
TfiSrUNQUISHED BY
1 SEALED
DATE TIME W//9/REASON FOR CHANGE OF CUSTODY
UNSEALED [~ UONSEALED \
RELINQUISHED BY DATE TIME ECEIVED BY REASON FOR CHANGE OF CUSTOD
"ISEALED UNSEALEDf" "1SEALED UNSEALED f"
CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII
ACTIVITY LEADEft(Print) NAME OF SURVEY OR ACTIVITY,
jifcaDATE OF COLLJpK
DAY MONTH'
SHEET
CONTENTS OF SHIPMEN
SAMPLENUMBER CUBITAINER
TYPE OF CONTAINERS
BOHLE BOniEVOA SE r
(2 VIAL3 EA)
NUMBERS OF CONTAINERS PER SAMPLE NUMBER
SAMPLtD MEDIA
otherRECEIVING LABORATORY
REMARKS.-OTHER INFORMATION(condition of samples upon receipt.
These data were reviewed primarily according to the"Laboratory Data Validation Functional Guidelines for EvaluatingInorganic Analyses," July 1988 revision with changes given in theRegion VII Inorganic Data Review Training Manual and EPAmemorandums.
The following comments and attached data sheets are a resultof the'ESAT review, according to EPA policies, of the followingdata from the contract laboratory.
CASE NO.: 16873SITE: Mississippi River PoolREVIEWER: Kevin Ludwikoski
This data review assignment covers NINE WATER samples analyzedfor TOTAL METALS and SIX SOIL samples analyzed for TOTAL METALSfor case number 16873. There was one PE sample, one field blank,one rinsate blank and one field duplicate for Total Metals inwater. There was one field duplicate for Total Metals in soilincluded with this assignment. Sample ISXP8001D was used as alaboratory duplicate sample for the analysis. As a result, thissample is refered to in this document and reported in the datasheets as ISXP8001L.
1. Technical Holding Times / Preservation
A. Technical holding times were observed for a1!! analytes.
B. Technical holding times are not specified for soil samples.
2. Initial and Continuing Calibration
A. All percent recoveries were within control limits for watersamples.
B. All percent recoveries were with control limits for soilsamples.
3. Blanks
Several analytes were detected in the blanks. Correspondingsample results were qualified according to the blank rule usingfive times the highest blank value. Sample results requiringmodification are reported as non-detect on the attached datasheets.
Fe, Mg, and Pb were found in the rinsate blank (ISXP8109F) ;however, no data were qualified due to this sample. Due to the highconcentration of these analytes, the user is encouraged to usecareful judgement in utilizing associated data.
B. TOTAL METALS(SOIL)
5 x HighestAnalvte Blank (mq/kq) Qualified Samples
Pb 1.4 None qualified
4. ICP interference Check
Recoveries of solution AB analytes were within control limitsfor Total Metals. Sb, K, and Na were found but not present in theICS solution. All absolute values for these analytes were below theCRDL; therefore, no data were qualified by the ICP interferencecheck sample.
5. Laboratory control Standard (LCS)
A. LCS results were within established control limits forTotal Metals in water samples.
B. LCS results were within established control limits forTotal Metals in soil samples.
6. Duplicates
A. The RPD for all analytes were within control limits forTotal Metals in water samples.
B. The RPD for Cu and Fe exceeded control limits for TotalMetals in soil. The sample results that were coded J are listedbelow.
TOTAL METALS(SOIL)
Analyte Samples Qualified Code
Cu ISXP8101, -102, -103, -103D, -104, J-104S, -105, -901C
Fe ISXP8101, -102, -103, -103D, -104, J-105, -901C
Note: All samples listed above with the exception of ISXP8104Swere also "J" coded for Cu due to the spike rule.
7. Matrix Spike Sample
A. Cd, Pb, and Tl were out of range for matrix spike recoveryfor Total Metals in water. The samples that had data qualified arelisted below.
-104L, -105, -901CNote: Cu in samples ISXP8101, -102, -103, -103D, -104, -105 and901C were previously "J" coded due to the duplicate rule.
s. ICP Serial Dilution
A. The ICP serial dilution results for Total metals in waterwere within control limits.
B. The ICP serial dilution results for Total Metals in soilwere within control limits with the exception of Cu (13.9 %RPD).Samples ISXP8101, -102, -103, -103D, -104, -104L, -104S, -105, and-901C were qualified by ICP serial dilution rules. These sampleshad been previously "J" coded due to either the spike or duplicaterules.
9. Furnace Atomic Absorption/
A. No MSA's were performed on Total Metals in water.
B. The analytical scheme was followed for Furnace AA analysisfor Total Metals in soil. MSA correlation coefficients wereacceptable for As in samples ISXP8104 and ISXP8104L (cc=.9949 and.9981 respect ively).
10. PE Sample
All analytes present in the PE Sample were found at acceptablelevels with the exception of Al and Hg (160% and 149% recoveries,respectively).
11. summary
A. Two analytes had samples that were qualified by the blankrule and three by the spike rule for Total Metals in water.
B. Four analytes were qualified by the spike rule, two by theduplicate rule and one by serial dilution outliers for Total Metalsin soil. '«'
ENVIRONMENTAL SERVICES ASSISTANCE TEAM - ZONE H
ICF Technology Incorporated
NSI Technology services Corp.
The Bionetics Corp.
ESAT Region VIINSI Tech. Serv. Corp.25 Funston RoadKansas City, KS 66115(913) 551-5000
These data were reviewed primarily according to the "LaboratoryData Validation Functional Guidelines for Evaluating OrganicAnalyses," February 1990.
The following comments and attached data sheets are a result ofthe ESAT review, according to EPA policies, of the following datafrom the contract laboratory.
CASE NO.: 16873SITE: Mississippi River PoolREVIEWER: David J. Hickev
This data review assignment covers 11 WATER and 7 SOIL samplesanalyzed for VOLATILES; 9 WATER and 6 SOIL samples analyzed forSEMIVOLATILES: and 9 WATER and 6 SOIL samples analyzed forPESTICIDES/PCBs for Case number 16873. For the volatiles, therewere five field blanks (including trip and rinsate), six methodblanks, two field duplicates, and one performance evaluation sampleincluded with this assignment. For the semivolatiles, there weretwo field blanks, five method blanks, two field duplicates, and oneperformance evaluation sample included with this assignment. Forthe pesticides/PCBs, there was two field blanks, two fieldduplicates, one performance evaluation sample, four method blanks,and six instrument blanks included with this assignment.
1. Holding Times and Preservation
Volatiles;
Several water samples exceeded the specified Aromatic holdingtimes for volatiles by 2 days or less but no qualification wasrequired. No holding times have been established for soil samples.
Semivolatiles;
Two water samples exceeded extraction holding times by two daysor less but no qualification was required. Analysis of the watersfor semivolatiles was completed within the specified time limit. Noholding times have been established for soil samples.
Pesticides/"PCBs:
Two water samples exceeded extraction holding times by two daysor less but no qualification was required. Analysis of the waterswas completed within the specified time limit. No holding timeshave been 'established for soil samples.
2. GC/MS Tuning
All relative ion abundances were within the established controllimits.
3. initial and Continuing Calibration
Volatiles;
All %RSD's were within control limits on the initialcalibration. All RRF values were within control limits on both theinitial and continuing calibrations. %D was out of control forChloromethane, Chloroethane, Acetone, 2-Butanone,Dibromochloromethane, and Bromoform. Since associated data wereeither non-detect or qualified by other rules, no data werequalified by the volatile continuing calibrations.
Semivolatiles;
All %RSD's were withiofi' control limits on the initial
calibrations. All RRF values were within control limits on both theinitial and continuing calibrations.%D was out of control forHexachlorocyclopentadiene, 2-Methylphenol, 2,2'-Oxybis(l-Chloropropane), N-Nitroso-Dipropylamine, 4-Nitrophenol, Carbazole,3-Nitroaniline, 2,4-Dinitrophenol, 4-Nitroaniline, 4,6-Dinitro-2-Methylphenol, N-Nitrosodiphenylamine, and Bis(2-Ethylhexyl)Phthalate. As a result, the following samples were J-coded: ISXP8102S, ISXP8102W, ISXP8104S, and ISXP8104W for N-Nitroso-Dipropylamine; ISXP8102S, ISXP8102W, ISXP8104S, andISXP8104W for 4-Nitrophenol; ISXP8103, ISXP8103D, ISXP8104,ISXP8104S, and ISXP8104W for Carbazole.
Pesticides/PCBs;
All samples were within quality control limit requirements forretention time windows and percent relative standard deviation onthe initial calibration. All samples were within quality controllimit requirements 'for analytical sequence and relative percentdifference on the continuing calibration. Almost every sample hadcompounds that did not meet quality control limit requirements forpercent difference between the concentrations between columns(quantitation column within 25% of confirmation column). Since allcompounds were less than the contract required quantitation limit(CRQL), no data were qualified.
4. GC/ECD Instrument Performance
The pesticide resolution check mixture was within qualitycontrol limit requirements. The pesticide performance evaluationcheck was within quality control limit requirements for retentiontime windows, relative percent difference of the performanceevaluation mixtures and individual mixes, and percent breakdown ofEndrin and 4,4'-DDT.
5. Internal Standard Response
Volatiles;
Sample ISXP8102 and its reanalysis were outside of controllimits (high) for Chlorobenzene. Since all compounds quantitatedfrom Chlorobenzene were non-detect for this sample, no qualificationwas necessary.
Semivolatiles;
Sample ISXP8103 and the diluted analysis were outside ofcontrol limits (low) for Acenaphthene-dlO and Phenanthrene-dlO(original analyses only), Crysene-dl2 and Perylene-12. As a result,all positive compound results quantitated from Crysene-dl2 andPerylene-dl2 were J-coded for that sample. Sample ISXP8103D and thediluted analysis were outside of control limits for Acenaphthene-dlOand Phenanthrene-dlO (original analyses only), Crysene-dl2 andPerylene-12. As a result, all positive compound results quantitatedfrom Acenaphthene-dlO, Phenanthrene-dlO, Crysene-dl2, and Perylene-d!2 were J-coded for that sample. Samples ISXP8104, ISXP8104S, andISXP8104W were outside of control limits (low) for Acenaphthene-dlO,Phenanthrene-dlO, Crysene-di2, and Perylene-dl2. These samples were
not reanalyzed. As a result, all positive compound resultsquantitated from Acenaphthene-dlO, Phenanthrene-dlO, Crysene-dl2,and Perylene-dl2 were J-coded for those samples. Samples ISXP8102,ISXP8102S, and ISXP8102W were outside of control limits (low) forPerylene-dl2. These samples were not reanalyzed. As a result, allpositive compound results quantitated from Perylene were J-coded forthose samples.
5. Pesticide Clean-up Checks
The percent recoveries for the florisil cartridge were withinquality control limit requirements with the exception of Endrin. Nodata were qualified.
6. Blanks
Volatiles:
Methylene Chloride was found in two of the water method blanksat levels below the CRQL. No samples were qualified as a result ofmethod blank contamination. Methylene Chloride, Acetone, andToluene were found in the water field blanks, qualifying samplesISXP8006F, ISXP8009F, and ISXP8926P with a U-code for Acetone.Acetone in the soil field blank (ISXP8108F) qualified samplesISXP8101, ISXP8102, ISXP8103D, ISXP8104, ISXP8105, ISXP8104S, andISXP8104W with a U-code.
Semivolatiles:
Bis(2-Ethylhexyl)Phthalate was found in two of the soil methodblanks, qualifying samples ISXP8103D and ISXP8104 with a U-code forthat compound. Diethylphthalate, Bis(2-Ethylhexyl)Phthalate, andDi-N-Butylphthalate were found in the water field blanks, qualifyingsample ISXP8001D with a U-code for Bis(2-Ethylhexyl)Phthalate.
Pesticides/PCBs;
All four method blanks were free of contamination. Allinstrument blanks were free of contamination.
7. Surrogate Recovery
Volatiles;
Surrogate compound recoveries were outside control limits (low)for l,2-Dichloroethane-d4 in sample ISXP8102. Upon reanalysis ofthe sample, all surrogate compound recoveries were within controllimits. There was no qualification of sample data based on thereanalysis results.
Semivolatilesi
Surrogate compound recoveries for 2-Fluorobiphenyl and 2,4,6-Tribromophenol were above control limits in several samples.However, no samples were qualified.
Pesticides/PCBs^*
Surrogate compound recoveries for both Tetrachloro-m-Xylene andDecachlorobiphenyl were below control limits in several samples.Surrogate compound recoveries for Tetrachloro-m-Xylene was abovecontrol limits in the dilution of one sample. Surrogate compoundrecoveries for Decachlorobiphenyl were 0% recovery in severalsamples. As a result of these outliers, all positive results forsamples ISXP8001, ISXP8001D, ISXP8004, ISXP8005, ISXP8109F,ISXP8101, ISXP8102, ISXP8104, ISXP8104S, ISXP8104W, and ISXP8105were J-coded; the high concentrations of some analytes seen in manysoil samples should be seen as lower estimates of the trueconcentrations. All non-detect values for these samples should beviewed as estimated detection limits.
8. Matrix spike/Matrix Splice Duplicate Recovery
Volatiles:
The Matrix spike/Matrix spike duplicate recoveries for bothmatrices were within control limits. All RPDs for both matriceswere within control limits. Contamination of Acetone in the waterMS/MSD; and Methylene Chloride, Acetone, and 2-Butanone in the soilMS/MSD did not result in the gualification of any sample data. Notethat for LAST purposes, the MS and MSD are listed as ISXP8001S andISXP8001W, even though they originated from sample ISXP8001D.
Semivolatiles;
The Matrix spike/Matrix spike duplicate recoveries were out ofcontrol for one compound in the water matrix. The MS/MSD recoverieswere out of control for two compounds in the medium-level soilmatrix, and out of control for one compound in the low-level soilmatrix. The RPD for the water matrix was within control limits,while both level soil matrix MSD's each had one RPD out of controllimits. Ho samples were qualified based on MS/MSD recoveries orRPD's. Note that for LAST purposes, the MS and MSD for the watermatrix are listed as ISXP8001S and ISXP8001W, even though theyoriginated from sample ISXP8001D.
Pesticides/PCBs:
The Matrix spike/Matrix spike duplicate recoveries were out ofcontrol for three compounds in the water matrix. The Matrixspike/Matrix spike duplicate recoveries were out of control for tencompounds in the soil matrix. The RPDs for both the water and soilmatrices were within control limits. No samples were qualifiedbased on MS/MSD recoveries. Note that for LAST purposes, the MS andMSD for the water matrix are listed as ISXP8001S and ISXP8001W, eventhough they originated from sample ISXP8001D.
9. Performance Evaluation Sample
Volatiles;
Recovery of spiked analytes was very good. Acetone, which wasalso present in one of the/.field blanks, was the only additional
compound found in the performance sample. No data were qualifiedbased on performance evaluation sample recoveries.
Semivolatiles;
Recovery of spiked analytes was very poor. None of the targetanalytes were recovered from the performance sample. The reason forno recovery is thought to exist in the performance spiking solution,as similar results (no recovery) were obtained from two otherperformance samples unrelated to this project. As a result, thespiking solution is no longer being used in performance evaluation.
Pesticides/PCBs:
Recovery of spiked analytes was very poor. None of the targetanalytes were recovered from the performance sample. The reason forno recovery is unknown.
10. Duplicates
Volatiles;
Good agreement existed between the duplicates in both matricesand their respective original samples.
Semivolatiles;
Good agreement existed between the duplicates in both matricesand their respective original samples. However, two phthalates weredetected in sample ISXP8001D that were not detected in the originalsample. Additionally, a phthalate was reported in sample ISXP8103which was not present in the duplicate.
Pesticides/PCBs;
Good 'agreement existed between the duplicates in both matricesand their respective original samples. Note that Endrin wasdetected in the duplicate of ISXP8003, but just below the CRQL.
11. Compound Identification and Quantitation
Due to the requested review level, results listed on thesummary forms were used for the review. These results were notchecked against the raw data for accuracy, and calculations were notverified. All positive results found below the CRQL were raised tothe CRQL and coded U. Samples ISXP8104S and ISXP8104W in theSemivolatiles, which exceeded the calibration range of theinstrument for Fluoranthene, were not diluted and reanalyzed. Hadthe samples not been qualified for other QC outliers, they wouldhave been J-coded.
12. summary
Volatiles:
The lab was instructed to analyze the water and soil samplesfor VOA analytes. Calibration outliers were found for many
compounds, however, sample results were either non-detect or werequalified by other rules. Methylene Chloride was found in two ofthe three water method blanks, but since samples were non-detect forthis compound, no coding was necessary. All soil method blanks werefree of contamination. Field blank contamination resulted in thequalification of three water samples for one compound, and sevensoil samples for one compound. Poor internal standard compoundrecovery in a sample and its reanalysis did not result in any sampledata qualification since no quantitated compounds were affected.All other QC was acceptable.
Semivolatiles;
The lab was instructed to analyze the water and soil samplesfor Semivolatiles analytes. Calibration outliers were found formany compounds, resulting in data for seven soil samples being J-coded. One common laboratory contaminant was found in two of thethree soil method blanks and three common laboratory contaminantswere found in both vof the water field blanks, qualifying threesamples with a U-code for Bis(2-Ethylhexyl)Phthalate. All watermethod blanks were free of contamination. Poor surrogate compoundrecovery did not result in the qualification of any positive sampledata. Poor internal standard compound recovery in eight samples(six of which were not reanalyzed) resulted in the qualification ofall positive sample data which were quantitated from those internalstandard compounds that were out of control with a J-code. Allother QC was acceptable.
Pesticides/PCBs:
All quality-control limit requirements were met for bothinitial and continuing calibrations. All instrument performancechecks met quality control limit requirements except for onecompound in the clean-up check, but that outlier did not result inthe qualification of any sample data. All blanks were free ofcontaminafion. Severe surrogate recovery outliers led to thequalification of all positive results with a J-code for twelvesamples. All other QC was acceptable.
S P F D
ANALYSIS REQUEST REPORT
FOR ACTIVITY: ISXP8
10/10/91 16:08:b2
PRELIMINARY DATASUBJECT TO REVISION
ALL REAL SAMPLES AND FIELD .Q.C.
* LABO APPROVED
FY: 91 ACTIVITY: ISXP8
LABO DUE DATE IS 10/ 1/91.
INSPECTION DATE: 8/ 1/91
DESCRIPTION: MISSISSIPPI RIVfR POOL #15 LOCATION: DAVENPORT
STATUS: ACTIVE TYPE: SAMPLING - CONTRACT LAB ANALYSIS ' PROJECT:
EXPLANATION! OF CODES AND INFORMATION ON ANALYSIS REQUEST DETAIL REPORT
SAMPLE INFORMATION:
SAMP. NO. = SAMPLE IDENTIFICATION NUMBER (A 3-DIGIT NUMBERWHICH IN COMBINATION WITH THE ACTIVITY NUMBERAND QCC, PROVIDES AN UNIQUE NUMBER FOR EACH SAMPLEFOR IDENTIFICATION PURPOSES)
QCC = QUALITY CONTROL CODE I A ONE-LETTER CODE USED TODESIGNATE SPECIFIC QC SAMPLES. THIS FIELD WILL BEBLANK FOR ALL NON-QC OR ACTUAL SAMPLES):A = TRUE VALUE FOR CALIBRATION STANDARDB = CONCENTRATION RESULTING FROM DUPLICATE LAB SPIKEC = MEASURED VALUE FOR CALIBRATION STANDARDD = MEASURED VALUE FOR FILED DUPLICATEF = MEASURED VALUE FOR FIELD BLANK ;
G = MEASURED VALUE FOR METHOD STANDARDH = TRUE VALUE FOR METHOD STANDARDK = CONCENTRATION RESULTING FROM DUPLICATE FIELD
SPIKEL = MEASURED VALUE FOR LAB DUPLICATEM = MEASURED VALUE FOR LAB BLANKN = MEASURED VALUE FOR DUPLICATE FIELD SPIKEP = MEASURED VALUE FOR PERFORMANCE STANDARDR = CONCENTRATION RESULTING FROM LAB SPIKES = MEASURED VALUE FOR LAB SPIKET = TRUE VALUE OF PERFORMANCE STANDARDW = MEASURED VALUE FOR DUPLICATE LAB SPIKEY = MEASURED VALUE FOR.FIELD SPIKEZ = CONCENTRATION RESULTING FROM FIELD SPIKE
M = MEDIA CODE (A ONE-LETTER CODE DESIGNATING THEMEDIA OF THE SAMPLE):A = AIRH = OTHER (DOES NOT FIT ANY OTHER CATEGORY)S = SOLID (SOIL. SEDIMENT. SLUDGE)T = TISSUE (PLANT & ANIMAL)W = WATER (GROUND WATER. SURFACE WATER. WASTE
WATER, DRINKING WATER)DESCRIPTION = A SHORT DESCRIPTION OF THE LOCATION WHERE SAMPLE
WAS COLLECTEDAIRS/STORET LOC. NO. = THE SPECIFIC LOCATION IDENTIFICATION
NUMBER FOR EITHER OF THESE NATIONALDATABASE SYSTEMS, AS APPROPRIATE
DATE/TIME INFORMATION = SPECIFIC INFORMATION REGARDING WHEN THESAMPLE WAS COLLECTEDBEG DATE = DATE SAMPLING WAS STARTEDBEG. TIME = TIME SAMPLING WAS STARTEDEND DATE - DATE SAMPLING WAS COMPLETEDEND TIME = TIME SAMPLING WAS COMPLETEDNOTE: A GRAB SAMPLE WILL CONTAIN ONLY
BEG. DATE/TIMEA TIMED COMPOSITE SAMPLE WILLCONTAIN BOTH BEG AND END DATE/TIMETO DESIGNATE DURATION OF SAMPLECOLLECTION
ANALYTICAL RESULTS/MEASUREMENTS INFORMATION:
COMPOUND = MGP (MEDIA-GROUP-PARAMETER) CODE AND NAME OFTHE MEASURED CONSTITUENT OR CHARACTERISTICOF EACH SAMPLE
UNITS = SPECIFIC UNITS IN WHICH RESULTS ARE REPORTED:C = CCtJTIGRADC (CELSIUS) DEGRtcSCFS = CUBIC FEET PER SECONDGPM = GALLONS PER MINUTEIN = INCHESI.D. = SPECIES IDENTIFICATIONKG -•• = KILOGRAML = LITERLB = POUNDSMG =.MILLIGRAMS (1 X 10-3 GRAMS)MGD ; = MILLION GALLONS PER DAYMPH = MILES PER HOURMV = MILLIVOLTM/F = MALE/FEMALEM2 = SQUARE METERM3 = CUBIC METERNA = NOT APPLICABLENG = NANOGRAMS (1 X 10-9 GRAMS)NTU = NEPHELOMETRTC. TURBIDITY UNITSPC/L = PICO (1 X 10-12.) TUPRIES PER LITE1?PG = PICOGRAMS (1 X 10-12 GRAMS)P/CM2 = PICOGRAMS PER SQUARE CENTIMETERSCM = STANDARD CUBIC METER (1 ATM, 25 C)SQ FT = SQUARE FEETSU = STANDARD UNITS (PH)UG = MICROGRAMS (1 X 10-6 GRAMS)UMHOS = MICROMHOS/CM (CONDUCTIVITY UNITS)U/CC2 = MICROGRAMS PER 100 SQUARE
CENTIMETERSU/CM2 = MICROGRAMS PER SQUARF CENTIMETER1000G = 1000 GALLONS+/- = POSITIVE/NEGATIVE# = NUMBER
DATA QUALIFIERS = SPECIFIC CODES USED IN CONJUNCTIONWITH DATA VALUES TO PROVIDE ADDITIONALINFORMATION ON THE REPORTED RESULTS. OR USEDTO EXPLAIN THE ABSENCE OF A SPCIFIC VALUE:BLANK = IF FIELD IS BLANK. NO REMARKS OR
QUALIFIERS ARE PERTINENT. FOR FIN A LREPORTED DATA. THIS MEAMS THAT THEvALUEs HAVE BEEN REVIEWED AND FOUNDTO BE ACCEPTABLE FOR USE.
I = INVALID SAMPLE/DATA - VALUE WOT REPORTEDj = DATA REPORTED BUT NOT VALID BY APPROVED
QC PROCEDURESK = ACTUAL VALUE OF SAMPLE IS < VALUE REPORTEDL = ACTUAL VALUE OF SAMPLE IS > VALUE REPORTEDM = DETECTED BUT BELOW THE LEVEL OF REPORTED
VALUE FOR ACCURATE QUANTIFICATION0 = PARAMETER NOT ANALYZEDU = ACTUAL VALUE OF SAMPLE IS < THE
MEASUREMENT DETECTION LIMIT (REPORTEDVALUE)
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 001 0010 002 003 004
WM01 SILVER BY ICAP
WM02 ALUMINUM, TOTAL. BY ICAP
WM03 ARSENIC. TOTAL, BY ICAP
WM04 BARIUM, TOTAL, BY ICAP
WM05 BERYLLIUM. TOTAL, BY ICAP
WM06 CADMIUM. TOTAL. BY ICAP
WM07 COBALT, TOTAL, BY ICAP
WM08 CHROMIUM, TOTAL. BY ICAP
WMO9 COPPER. TOTAL, BY ICAP
WM10 IRON. TOTAL, BY ICAP
WM11 MANGANESE, TOTAL. BY ICAP
WM12 MOLYBDENUM BY ICAP
WM13 NICKEL BY ICAP
WM14 LEAD. TOTAL. BY ICAP
WM15 ANTIMONY, TOTAL. BY ICAP
WM16 SELENIUM BY ICAP
WM17 TITANIUM BY ICAP
WM18 THALLIUM BY ICAP
WM19 VANADIUM BY ICAP
l\'M?0 I?UJO BY ICAP
WK21 CALCIUM. TOTAL BY Ii'.AP
WM22 MAGNESIUM. TOTAL BY ICAP
WM23 SODIUM. TOTAL BY ICAP
WM24 POTASSIUM, TOTAL BY ICAP
WM34 MERCURY BY COLD VAPOR AA
WP17 PCB-1016
:. UG/l.
••UG/L
:UG/L
:UG/L:.UG/L
:UG/L
:UG/L
•UG/L
:UG/L
•UG/L
•UG/L
: UG/L
•'UG/L
•UG/L
!UG/L
:UG/L
: UG/L
:UG/L
:UG/L
•UG/L
•MG/L
!MG/L:MG/L
:MG/L
:UG/L
;UG/L
• 10
•420
: 10
:200
Is.o\5.0
•so!lO
:25
M200
:430
':N/A
:40
\4.8
•60
:5.0
•N/A
: 10
^50
: 32
^53
: 15
•41
•5.0
•0.20
:1 .0
u
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U
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uuuu0
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:'10
•420
: 10
:200
':5.0
•5.0:.50
: 10
:25
: 1200
•430
:N/A
•40
^5.2
•60
•5.0
•N/A
: 10
•50
•33
•53
: 15
•40:5.0
•0.20
•1.0
U
U
U
U
U
U
U
u
0
uuuu0
uu
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•1C
.:230
MO
:200
:5.0
'•5.0'
•50
: 10
:25
:370
•250
iN/A
':40:3 0
:60
•5.0
:N/A
: 10
•50
^20
'.73
•32
^20
•5.0
: 0 . 20
':1.0
u
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U
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0
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" C
1200
10
200
5.0
5.0
50
10
25
250
60
N/A
40
3.0
60
5.0
N/A
10
50
29
60
23
19
5.0
0.20
1 .0
u
U
U
U
U
U
uu
0
uuII
u0
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i 0
: 1 3000
: 10
•200
•5.0:.5.0
:50
•12
^25
: 2600
•500
•N/A
•40:.6.9:60
!5.0
:N/A
•10
•50
••11;67
:22
: 16
'.5.0
•0.20
:1 .0
U
U
U
U
U
u
u
0
uuuu0
uu
uuu
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 001 00 ID 002 003 004
WP18 PCB-1221 -UO/L
WP19 PCB-1232 :UG/L
WP20 PCB-1242 :UG/L
WP21 PCB-1248 :UG/L
WP22 PCB-1254 : UG/L
WP23 PCB-1260 :UG/L
WS01 PHENOL :UG/L
WS03 ETHER, BIS(2-CHLOROETHYL) . BY GC/MS \ UG/L
W-S04 2-CHLOROPHENOL : UG/L
WS05 1 ,3-DICHLOROBENZENE : UG/L
W50G 1 ,4-DICHLOROBENZENE :UG/L
WS07 BENZYL ALCOHOL : UG/L
WS08 1 .2-DICHLOROBENZENE : UG/L
WS09 2-METHYLPHENOL (0-CRESOL) :UG/L
WS10 ETHER. BIS(2-CHLOROISOPROPYL). BY GC/MS':UG/L
WS11 4-METHYLPHENOL IP-CRESOL) :UG/L
WS12 N-NITROSO-DIPROPYLAMINE : UG/L
WS13 HEXACHLOROETHANE.BY GC/MS :UG/L
WS14 NITROBENZENE ': UG/L
Wf,15 rc.OPHORON/E.BV GC/MS :UG./L
V.'SIG 2-NITROPHENOL : UG/L
WS17 2 .4-D1METHYLPHENOL : UG/L
WS18 BENZOIC ACID. BY GC/MS : UG/L
WS19 METHANE, BISC2-CHLOROETHYOXY) . BY GC/MS^UG/L
WS20 2.4-DICHLOROPHENOL :UG/L
WS21 1 ,2.4-TRICHLOROBENZENE :.UG/L
1.0 U
2.0 U
1 .0 U
1.0 ,- U
1 .0 U
1 .0 U
10 U
10 U
10 U
10 U
10 U
N/A 0
10 U
10 U
N/A 0
10 U
10 U
10 U
10 U
10 IJ
10 U
10 U
N/A 0
10 U
10 U
10 U
1.0 U
2.0 U
1.0 U
1.0 U
1.0 U
1 .0 U
10 U
10 U
10 U
10 U
10 U
N/A 0
10 U
10 U
': N/A 0
: 10 U
: 10 U
•10 U
• 10 U
•1C U
•10 U
: 10 U
•N/A 0
MO U
• 10 U
•10 U
1 . G U '.
2.0 U
1.0 U
1 .0 U
1.0 U
1 .0 U
10 U
10 U
10 U
10 U
10 U
N/A 0
10 U
10 U
N/A 0
10 U
10 U
10 U
10 U
'.W iJ
10 U
10 U
N/A 0
10 U
10 U
10 U
" . 0 u .
2.0 U
1.0 U
1.0 U
1 .0 U
1 .0 U
10 U
10 U
10 U
10 U
10 LI
N/A 0
10 U
10 U
N/A 0
10 U
10 U
10 U
10 IJ
10 U
1 0 U
10 U
N/A 0
10 U
10 U
10 U
1.0 u
2.0 U
1 .0 U
1 .0 U
1 .0 U
1.0 U
10 U
10 U
10 U
10 U
10 U
N/A 0
10 U
10 U
M/A ij
10 U
10 U
10 U
10 U
i 0 i '
iG i.i
1 0 U
N/A 0
10 U
10 U
10 U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 001 0010 002 003 004
W522 NAPHTHALENE
WS23 4-CHLOROANILINE
WS24 HEXACHLOROBUTADIENE.BY GC/MS
WS25 4-CHLORO-3-METHYLPHENOL
WS26 2-METHYLNAPHTHALENE
WS27 HEXACHLOROCYCLOPENTADIENE.BY GC/MS
WS28 2.4.6-TRICHLOROPHENOL
WS29 2.4.5-TRICHLOROPHENOL
MJG/L
••UG/L
•UG/L
•UG/L
•UG/L
:UG/L
iUG/L
:UG/L
W530 2-CHLORONAPHTHALENE \ UG/L
WS31 2-NITROANILINE (ORTHO NITROANILINE )
WS32 PHTHALATE. DIMETHYL. BY GC/MS
WS33 ACENAPHTHYLENE. BY GC/MS
WS34 3-N1TROANILINE
WS35 ACENAPHTHENE. BY GC/MS
WS36 2,4-DIUITROPHENOL
WS37 4-WITROPHENOL
•UG/L
•UG/L
•UG/L
:UG/L
•.UG/L
: UG/L
•UG/L
WS38 DIBENZOFURAN • UG/L
WS39 2.4-DINITROTOLUENE !UG/L
WS40 2,6-DINITROTOLUENE ! UG/L
WS-11 PHTHALATE. DIETHYL. BY GC/MS
WS42 4-CHLOROPHENYL PHEWYL ETHER
WS'13 FLUORENE.BY GC/MS
WS-14 4-NITROAN1LINE
WS45 4.6-DIWITRO-2-METHYLPHENOL
•UG/L
•UG/L
• UG/L
•UG/L
•UG/L
WS46 N-WITROSODIPHENYLAMINE :UG/L
WS47 4-BROMOPHENYL PHENYL ETHER •UG/L
10
10
10
10
10
10
10
25
10
25
10
10
25
10
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ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 001 001D 002 003 004
WS-18 HEXACHLORGBEMZENE.BY iif./MS
WS49 PENTACHLOROPHENOL
WS50 PHENANTHRENE
WS51 ANTHRACENE, BY GC/MS
WS52 PHTHALATE. DI-N-BUTYL-. BY GC/MS
WS53 FLUORAMTHENE.BY GC/MS
WS54 PYRENE
WS55 PHTHALATE, BUTYL BEN2YL
US66 3.3'-DICHLOROBENZIDINE
WS57 ANTHRACENE. BEWZOiAi. BY GC/MS
WS58 PHTHALATE. BISi 2-ETHYLHEXYL J . BY GC/MS
WS59 CHRYSENE, BY GC/MS
WS60 PHTHALATE, DI-N-OCTYL-. BY GC/MS
WS61 FLUORANTHENE. BENZO(B), BY GC/MS
WS62 FLUORAMTHEME. BENZSGi K.) . BY GC/MS
WSG3 PYRENE, BENZGiA;, BY GC/MS
WS64 INDENOl 1 . 2 . 3-CD JPYRENE
WS65 ANTHRACENE. DI BENZOI A . H) . BY GC/MS
WS66 PERYLENE. BENZOI G.H. I ). BY GC/MS
Wf,r,7 riRRATvii.r
WV03 CiiLCRGWETHrtl-jC . BV i'v-.-MS.
WVO'i BROMGMt THANE . BY GC/MS
WVOb V J N Y L CHLORIDE
WV06 CHLOROETHANE, BY GC/MS
WV07 METHYLENE CHLORIDE
WV08 1 . 1-DICHLOROETHENE
• i if;/!. ^
:UG/L
: UG/L
•UG/L
: UG/L
:UG/L
: UG/L
:UG/L
•UG/L
:UG/L
•UG/L
•UG/L
: UG/L
•UG/L: UG/L
: UG/L
•UG/L
10
25
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
'UG/L -10
•UG/L ho
JJC/L : 10
in1, /i. •. in
•HG/L :10
•UG/L -10
•UG/L :10
•UG/L :10
•UG/L -10
M
uuuuuuuuuuuuuuuuuuij
IJ
uuuuu
• 10:25
: 10
MO
:10
:10
•10
': 15
: 10
: 10
• 1 1
•10
•!io•10
: 10
•10
: 10:. 10:10: 10
•1C
•10:. 10
•10
: 10
•10
uuuuuuu
uuu
uuuuuuuIJuuuuuuu
10
25
10 .
10
10 , v10
10
10
10
10
10
10
10
1.0
10
10
10
10
10
10
10
10
uuuuuuuuuuuuuuuuuuuLI
uIJ
240
10
10
10
uuu
1C
25
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
uuuuuu0
uuuuIJuuI)uuuuuuu
uuu
':10
•25
ho;. 10:. 10:. 10:. 10
•10
ho
: 10
•10
•10
ho
ho
: 10
•10
•TO
•10
:10
': 10
; 10•10
•10
':]0
• 10
•10
U
U
U
uuuuuuuIJ
uuuuuuuuuU
uuuuu
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 001 001D 002 003 004
WV09 1 . 1-DICHLOROETHANE . mVU
WV10 1 .2-DICHLOROETHENE. TOTAL i UG/L
WV11 CHLOROFORM, BY GC/MS : UG/L
WV12 1 ,2-DICHLOROETHANE :UG/L
WV13 1 ,1 .1-TRICHLOROETHANE • : UG/L
WV14 CARBON TETRACHLORIDE . BY GC/MS : UG/L
WV15 BROMODICHLOROMETHANE. BY GC/MS !uG/L
WV16 1 .2-DICHLOROPROPANE '.UG/L
•ti\n7 BENZENE, BY GC/MS ': UG/L
WV19 TRICHLOROETHENE :UG/L
WV20 DICHLORGPROPENE. CIS-1.3-, BY GC/MS :UG/L
WV21 DIBROMOCHLOROMETHANE. BY GC/MS : UG/L
WV22 1 , 1 .2-TRICHLOROETHANE : UG/L
WV24 BROMOFORM, BY GC/MS ': UG/L
WV25 TETRACHLOROETHEME :LUVL
WV26 TOLUENE ;. UG/L
WV27 1 . 1 ,2,2-TETRACHLOROETHANE ': UG/L
WV28 CHLOROBEN2ENE. BY GC/MS : UG/L
WV29 ETHYL BEN2ENE . BY GC/MS ': UG/L
WV30 ACETONE. BY GC/MS :l.i:.-.."_
WV31 CARBON DISULfTRE. BY dr. /MS :U '.>/!.
WV32 2-BUTANONE : llf./L
WV33 VINYL ACETATE : UG/L
WV34 2-HEXANONE • UG/L
WV35 4-METHYL-2-PENTANONE : UG/L
WV36 STYRENE ! UG/L
in i.i
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
. •> M j ;I ','
1 0 '-'
•"10 i.i
: M/A 0
: 10 U
•10 U
: 10 U
10 I1
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
U
1C 'J
; 10 I!
; N/A 0
: 10 U
•10 U
•10 U
10 U
1600
10 U
10 U
10 • U
10 U
10 U
10 U
10 U
190
10 U
10 U
10 U
10 U
2800
10 U
10 U
: 10 U
: 10 U
: 10 U
:o u': 1 0 'J
: N/A 0
,: 1 o . u: 10 U
: 10 U
10 U
86
44
10 U
10 U
10 U
10 U
10 U
10 U
4R
10 U
10 U
10 U
10 U
160
10 U
10 U
: 10 U
: 10 U
•10 U
.'iO U
: 1 0 U
•N/A 0
: 10 U
•10 U
: 10 U
10 U
30
71
10 U
10 U
10 U
10 U
10 U
10 U
12
10 U
10 U
10 U
10 U
35
10 U
10 U
10 U
10 U
10 U
10 U
10 U
N/A 0
10 U
10 U
10 U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 001 001D 002 003 004
WV37
WV40
Z201
2202
XYLENES. TOTAL
TRANS-1 ,3-DICHLOROPROPENE
SAMPLE NUMBER
ACTIVITY CODE
• iif.;/i_ .
•UG/L
:NA
:NA
j 1(?
•10
•001
:ISXP8
u • i n
U : 10
•001
•ISXP'8
ii . i r\U - i o
U : 10
•002
:ISXP8
II t /-vU . 1 U
u hoioos•ISXP8
U
u: 10
: 10
•004
:ISXP8
U :
U :
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008F. 009F 101
SM01 SILVER BY I CAP
SM02 ALUMINUM. TOTAL. BY ICAP
SM03 ARSENIC. TOTAL. BY JCAP
SM04 BARIUM. TOTAL, BY ICAP
SM05 BERYLLIUM, TOTAL, BY ICAP
SM06 CADMIUM. TOTAL. BY ICAP
SM07 COBALT. TOTAL. BY ICAP
SM08 CHROMIUM, TOTAL. BY ICAP
S&S9 COPPER, TOTAL. BY ICAP
SM10 IRON, TOTAL, BY 1C.AP
SM11 MANGANESE. TOTAL BY ICAP
SMI 2 MOLYBDENUM BY ICAP
SMI 3 NICKEL BY ICAP
SMI 4 LEAD, TOTAL. BY ICAP
SM15 ANTIMONY, TOTAL. BY ICAP
SM1G SELENIUM BY ICAP
SM17 TITANIUM BY ICAP
SM18 THALLIUM BY ICAP
SMI 9 VANADIUM BY ICAP
SM20 2Ifir BY I CAP
SM21 CALCIUM. TOTAL. BY KAP
SM22 MAGNESIUM. TOTAL. BY ICAP
SM23 SODIUM BY ICAP
SM24 POTASSIUM BY ICAP
SM34 MERCURY BY COLD VAPOR AA
SP17 PCB-1016
•Mr, /krv
: MG/KG:
:MG/KG.
:MG/KG: :.
:MG/KG:
: MG/KG:
: MG/KG:
.MG/KG:
: MG/KG:
: MG/KG:
: MG/KG:
: MG/KG:
: MG/KG:
: MG/KG:
:Mfj/Mj:
: MG/KG:
:MG/KG:
: MG/KG:
: MG/KG:: M'.,. •>->,:
• MI , / 1: i : •
•MG/Kf, !
•MG/KG:
•MG/KG:
: MG/KG ':;UG/KG:
i.: 2. 6
•8300
•2.8
•72
•1.4
•1.4
: 14
: 18
•53
: 1 3000
':260
:N/A
: 18
•39: M/A
•1.4
:N/A
•2.8
•21
'. 110
: 36000
: 1 3000
: 1 400
• 1400
•0.14
•51
U
U
U
U
U
J
J
J
0
oU
0 :
U
U
U
U
U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F 009F 101
SP18 PCB-1221
SP19 PC6-1232 :
SP20 PCB-1242
SP21 PCB-1248 !
SP22 PCB-1254 :
SP23 PCB-1260 :
SS01 PHENOL
SS02 CARBAZOLE
•SSO3 ETHER, BIS(2-CHLOROETHYL) , BY GC/MS
SS04 2-CHLOROPHENOL
SS05 1 ,3-DICHLOROBENZENE
SS06 1 ,4-DICHLOROBENZENE
SS07 BENZYL ALCOHOL
SS08 1 .2-DICHLOROBENZENE
SSOQ 2-METHYLPHENOL (0-CRESOLJ
SS10 WTHER. BIS(2-CHLOR01SOPROPYL). BY GC/MS
SS11 4-METHYLPHENOL IP-CRESOL)
SS12 N-NITROSO-DIPROPYLAM1WE
SSI 3 HEXACHLOROETHANE.BY GC/MS
SSI 4 NITROBENZENE
SSI 5 1SOPHORONE. BY GC/MS
SSI 6 2-N1TROPHENOL
SSI 7 2.4-D1METHYLPHENOL
SS18 BEMZ01C ACID, BY GC/MS
SS19 METHANE. BIS(2-CHLOROETHYOXY) . BY GC/MS
SS20 2,4-DICHLOROPHENOL
UC-./KG:
UG/KG:
UG/KG:
UG/KG: ;•
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/KG :
UG/KG:
UG/KG:
UG/KG:
UG/KG:
UG/I--0:
UG/CG:
•UG/KG:; UG/KG :
: UG/KG :
•UG/KG:
: UG/KG :
'5',
; 100
!51
•940
151
151
•5100
•5500
^5100
: c' 1 00
:5100
•5100
•N/A:.5100
: T-1 GO
IN/ A:5100
•5100
:5100
I-': C'O
: b 'i 00
• :51CO
': ':5100
• !N/A• :5100
: ! 5 1 00
U :
U
U
J
U
U
U
U
U
1,1
U
0
U
i l
0
U
U
U
1 1
I I
U
U
0
U
U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F 009F 101
SS21 1 . 2.4-TR1CHLGROBENZENE
SS22 NAPHTHALENE
SS23 4-CHLOROANILINE
SS24 HEXACHLOROBUTADIENE.BY GC/MS
SS25 4-CHLORO-3-METHYLPHENOL
SS26 2-METHYLNAPHTHALENE
SS27 HEXACHLOROCYCLOPENTADIENE.BY GC/MS
SS28 2.4.6-TRICHLOROPHENOL
S£29 2.4,5-TRICHLOROPHENOL
SS3G 2-CHLOROMAPHTHALENE
SS31 2-NITROANILINE
SS32 PHTHALATE. DIMETHYL. BY GC/MS
SS33 ACENAPHTHYLENE, BY GC/MS
SS34 3-NITROANILINE
SS35 ACEKAF-HTHENE . BY GC/MS
3336 2.4-DlNlTRGPH£NuL
SS37 4-NITRGPHENOL
5S38 DIBENZOFURAN
SS39 2.4-DIN1TROTOLUENE
S''-1C) 2 fi-niM!TROTOH''!:''!F
SS-II PiiTiiALATE. DIETV-iVi . 6 1 i-.i'..-'M~,
SS-12 .-i-ilhLORuF'HE'N/L PHENYL El HER
SS43 HLUOREME .(JL/MS
SS44 4-N1TROANILINE
SS45 /1.6-DINITRO-2-METHYLPHENOL
SS46 N-NITROSODIPHENYLAMINE
•MO/KG^
•-UG/KG:
:UG/KG:
: UG/KG.
:UG/KG:
:UG/K.G:
:UG/KG:
:UG/K.G:
:UG/KG:
: uG/K-C:
• UG/KG:
:UG/KG:
:UG/KG:
!UG/KG:
• UG/MJ-
:UG/KG:
:UG/KG.:
•UG/KG:
:UG/KG:
ll'.i.-t-!;-
• I I I - /" I. .
•UG/KG': UG/KG:
: UG/KG :
: UG/KG:
•UG/KG:
: o i 00
^5100
:5100
^5100
15100:.5100
:5100
^5100
: 1 2000
•5100
: 1 2000
•5100
•5100
: 1 2000
:5100
: 1 2000
': 1 2000
^5100:.5100
; 5 1 oo:.5100
•5100
•5100
: 1 2000
: : 1 2000
: :5100
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F' 009 F 101
SS47 4-BRGMOPHEWYL PHENYL ETHER
SS48 HEXACHLOROBENZENE.BY GC/MS
SS49 PENTACHLOROPHENOL
SS50 PHENANTHRENE
SS51 ANTHRACENE, BY GC/MS
SS52 PHTHALATE. DI-N-BUTYL-. BY GC/MS
SS53 FLUORANTHENE.BY GC/MS
SS54 PYRENE
S555 PHTHALATE. BUTYL BENZYL
3556 3.3'-DICHLOROBEN2IDINE
SS57 ANTRACENE. BENZO(A) , BY GC/MS
SS58 PHTHALATE. BIS12-ETHYLHEXYL) , BY GC/MS
SS59 CHRYSENE. BY GC/MS
SS60 PHTHALATE, DI-N-OCTYL-. BY GC/MS
SS61 FLUORANTHEME. BEMZO(B) . BY GC/MS
SS62 FLUORAMTHENE. BENZOvK) . BY GC/MS
SS63 PYRENE, BENZO(AJ. BY GC/MS
SS64 INDEWOl 1 . 2 . 3-CD) PYRENE
SS65 ANTHRACENE. DIBEWZO( A , H) . BY GC/MS
SSee PERYLEME. BEMZOf.G H I>. BY GC/MS
GVG3 CliLOROMETHAME . BY Gf./MS
SV04 BROMOME THANE . BY GC/MS
iVOB VINYL CHLORIDE
SV06 CHLOROETHANE. BY GC/MS
SV07 METHYLENE CHLORIDE
SV08 1 . 1-DICHLOROETHYLENE
•UG/KG.:
•UG/KG:
: UG/KG:
•.UG/KG:
:' UG/KG :
: UG/KG:
: UG/KG :
•UG/KG:
:UG/KG:-
:UG/KG:
: UG/KG :
: UG/KG:
•UG/KG:
: UG/KG:
: UG/KG:
: UG/KU:
•UG/KG:
•UG/KG:
: UG/KG:
: IJG/T-.G:
: UG/KG;
• UG/KG :
•UG/KG:
: UG/KG :
•UG/KG:
: UG/KG :
•: D i 00
^5100
: 1 2000
: 1 9000
':5100
^5100
: 28000
: 26000
•5100
: 5100
: 1 5000
•5100
: 1 9000
•5100: 1 8000
:5100: 1 3000
• 5400
: 5 1 00
. 5500: 15
. 15
880
15
15
15
0
U
U
U
U
U
U
U
U
U
U
l l
II\ I
U
U
U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F 009F 101
SV03 1 . 1-D1CHLOROETHANE -iir;/KG :
SV10 TRANS-1 ,2-DICHLOROETHYLENE : UG/KG :
SV11 CHLOROFORM. BY GC/MS : UG/KG:
SV12 1 ,2-DICHLOROETHANE :UG/KG:
SV13 1 .1 .1-TRICHLOROETHANE :UG/KG:
SV14 CARBON TETRACHLORIDE . BY GC/MS \ UG/KG :
SV15 BROMODICHLOROMETHANE , BY GC/MS : UG/KG:
SV16 1 ,2-DICHLOROPROPANE :UG/KG:
"SV17 BENZENE, BY GC/MS : UG/KG:
SV18 TRAMS-i . 3-DICHLOROPROPEWE :UG/KG:
SV1S TRICHLOROETHYLENE -UG/K.G:
SV20 DICHLOROPROPENE. CIS-1,3-. BY GC/MS : UG/KG :
SV21 DIBROMOCHLOROMETHANE, BY GC/MS -UG/K.G:
SV22 1 , 1 ,2-TRICHLOROETHANE : UG/KG :
SV24 BROMOFORM, BY GC/MS iiJG/KG:
SV25 1 . 1 .2,2-TETRACHLGFtOETHENE : UG/KG:
SV26 TOLUENE ': UG/KG .:
SV27 1 . 1 . 2.2-TETRACHLOROETHANE -UG/K.G:
SV28 CHLOROBENZENE, BY GC/MS : UG/KG:
SV29 ETHYL BEMZEME.BY G-"/M? '•.>.'<,"<:'
SV30 ACETOWE. BY GC/MS : '>."'.-. 'f- •: :
SV31 CARBON DISULFIOE. BY bC/MS . : UC,./MV
SV32 2-BUTANONE : UG/KG.
SV33 V7NYL ACETATE : UG/KG:
SV34 2-HEXANONE : UG/KG :
SV35 4-METHYL-2-PENTANONE :' UG/KG :
15 u
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
15 U
1 5 . 1 )
1 7 I I
15 U
15 U
N/A 0
15 U
15 U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F' 009 F 101
SV36 STYRENE
SV37 XYLENES. TOTAL
WM01 SILVER BY ICAP
WM02 ALUMINIUM. TOTAL, BY ICAP
WM03 ARSENIC. TOTAL, BY ICAP
WM04 BARIUM. TOTAL. BY ICAP
WM05 BERYLLIUM. TOTAL. BY ICAP
WM06 CADMIUM. TOTAL. BY ICAP
Wto€>7 COBALT. TOTAL. BY ICAP
WMCS CHROMIUM. TOTAL. BY ICAP
WM09 COPPER. TOTAL. BY ICAP
WM10 IRON. TOTAL. BY ICAP
WM11 MANGANESE, TOTAL. BY ICAP
WM12 MOLYBDENUM BY ICAP
WM13 NICKEL BY ICAP
WM14 LEAD. TOTAL. BY ICAP
WM15 ANTIMONY, TOTAL, BY ICAP
WM16 SELENIUM BY ICAP
WM17 TITANIUM BY ICAP
WM1S THALLIUM BY ICAP
WM13 VANADIUM BY ICAP
WM20 ZINC BY ICAP
WM^1 CALCIUM. TOTAL BY ICAP
WM22 MAGNESIUM, TOTAL BY ICAP
WM23 SODIUM. TOTAL BY ICAP
WM24 POTASSIUM, TOTAL BY ICAP
• I.IG/KGJ•-UG/K.G:
:UG/L :10
:UG/L :370
:UG/L :10
:UG/L :200
:UG/L :5.0
!UG/L 5.0
:UG/L :50
:UG/L :10
:UG/L :25
:UG/L :320
:UG/L .400
:UG/L :N/A
:UG/L :40
:UG/L .;15
:UG/L ':60
:UG/L :5.0
:UG/L :N/A
•UG/L -10
:U'J/L :50
• UG/I. -20
:MC/L : 120
:MG/L :48
:MG/L :820
•MG/L :7.1
U
/
U
U
U
U
U
U
U
0
U
U
U
U
0
U
U
U
:10
•200
= 10 . •
•200
'•.5.0
'•s.o:.50
• 10•25
•100
•15
:N/A
:40
:3.0
^60
!s.o!N/A: !0
:'SC:.20
!s.o!s.o!s.o:5.0
U
U
U
U
U
U
U
I)
U
U
U
0
U
U
U
U
0
U
U
U
U
U
U
U
15 U :
IB U :.
-
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F 009F 101
WM34 MERCURY BY C.OLD VAPOR AA :"«VU
WP1 7 PCB-1016 :UG/L
WP18 PCB-1221 :UG/L
WP19 PCB-1232 ':UG/L
WP20 PCB-1242 !UG/L
WP21 PCB-1248 :'UG/L
WP22 PCB-1254 ': UG/L
WP23 PCB-1260 :UG/L
•WSrOI PHENOL :UG/L
WS03 ETHER. BIS( 2-CHLOROETHVL ) , BY fit /MS : UG/L
WS04 2-CHLOROPHENGL :UG/L
WS05 1 ,3-DlCHLOROBENZENE : UG/L
WS06 1 ,4-DICHLOROBENZENE :UG/L
WS07 BEN2YL ALCOHOL : UG/L
WS08 1 .2-DICHLOROBENZENE :Ub/L
WS09 2-METHYLPHENOL lO-CRESOL.) : UG/L
WS10 ETHER. BIS(2-CHLOROISOPROPYL) . BY GC/MS:UG/L
WS11 1-METHYLPHENOL (P-CRESOL.) : UG/L
WS12 N-NITROSO-DIPROPYLAMIME : UG/L
v,'c. n nrxAr.ni nRnFTMii.]r pv r,r ..•(,'. c. :'i,.-^
W31-1 NITRGBEUZEIJE :i.M.-.'L
WS15 1SOPHORONE .BY L)C/MS : UG/L
WS16 '^-WITROPHEWOL :l)G/L
W517 2.4-DIMETHYLPHENOL : UG/L
WS18 BENZOIC ACID, BY GC/MS : UG/L
WS19 METHANE. BIS( 2-CHLOROETHYOXY ) . BY GC/MS: UG/L
0 20 '.' :
1.0 U
1 .0 U
2.0 ,r U
1 .0 U
1 .0 U
1 .0 U
1 .0 U
10 U
10 U
10 U
10 U
10 U
N/A 0
10 U
10 U
N/A 0
10 U
10 U
• '0 U
• 1 0 U
'•10 U
:10 U:. 10 U
: N/A 0
: 10 U
0.52
1.0 U
1.0 U
2.0 U
1.0 • .. U
1.0 U
1 .0 U
1.0 U
10 U
10 U
10 U
10 U
10 U
N/A 0
10 U
10 U
N/A 0
10 U
10 U
10 • U
10 U
10 U
10 U
10 U
N/A 0
10 U
.
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F 009 F 101
WS20 2.4-DICHLOROPHENOL :n<VU
WS21 1 ,2.4-TRICHLOROBENZENE ' : UG/L
WS22 NAPHTHALENE : UG/L
WS23 4-CHLOROANILINE : UG/L
WS24 HEXACHLOROBUTADIENE.BY GC/MS : UG/L
WS25 4-CHLORO-3-METHYLPHENOL : UG/L
WS26 2-METHYLUAPHTHALENE : UG/L
WS27 HEXACHLOROCYCLOPENTADIEUE.BY GC/MS : UG/L
-tf928 2.4.6-TRICHLOROPHENOL :. UG/L
WS29 2.4.5-TRICHLOROPHENOL :UG/L
WS30 2-CHLORONAPHTHALENE ! UG/L
WS31 2-NITROANILINE (ORTHO NITROANILINE ) : UG/L
WS32 PHTHALATE. DIMETHYL. BY GC/MS : UG/L
WS33 ACENAPHTHYLENE, BY GC/MS : UG/L
WS34 3-NITROANILINE : UG/L
WS35 ACENAPHTHENE. BY GC/MS • UG/L
WS36 2.4-DINITROPHENOL ! UG/L
WS37 4-NITROPHENOL . !uG/L
WS38 DIBENZOFURAN • UG/L
WS39 2.4-DINITROTOLUENE :UG/L
WS-10 2.C-DINITROTOLUEWE : 00/L
WS41 PHTHALATE. DIETHYL. BY GC/MS : UG/L
W542 4-CHLOROPHENYL PHENYL ETHER : UG/L
WS43 FLUORENE.BY GC/MS ': UG/L
WS44 4-N1TROANILINE : UG/L
WS45 4.6-DINITRO-2-METHYLPHENOL :. UG/L
i n i i -
10 U \
10 U
10 / U
10 U
10 U
10 U
10 U
10 U
25 11
10 U
25 U
10 U
10 , U
25 U
10 U
25 U
25 U
10 U
1 G U
10 U
10 U
10 U
10 U
25 U
25 U
10 U .
10 U
10 U
10 U
10 . •.., U
10 U
10 U
10 LI
10 U
25 U
10 U
25 U
10 U
10 U
25 |!
10 U
25 U
25 U
10 U
} 0 :.:
'.',0 U
• 10 '.'
: 10 U
•10 U
•25 U
':2S U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 005 006 F 008 F. 009F 101
WS4G Ki-KilTROSGDlf'HENVLAMINE 'iiG/L^:
WS47 4-BROMOPHENYL PHENYL ETHER 'iuG/L :
WS48 HEXACHLOROBENZENE.BY GC/MS ' : UG/L :
WS49 PENTACHLOROPHENOL : UG/L :
WS50 PHENANTHRENE : UG/L :
WS51 ANTHRACENE. BY GC/MS : UG/L
WS52 PHTHALATE, DI-N-BUTYL-, BY GC/MS : UG/L
WS53 FLUORAMTHENE.BY GC/MS : UG/L
W554 PYRENE : UG/L
WS55 PH1HALATE, BUTYL BENZYL : UG/L
WS5G 3.3'-DICHLOROBENZIDINE : UG/L
WS57 ANTHRACENE. BENZO(A), BY GC/MS : UG/L
WS58 PHTHALATE. BISC2-ETHYLHEXYL) , BY GC/MS ': UG/L
WS59 CHRYSENE. BY GC/MS : UG/L
WS6C PHTHALATE. DI-M-OCTYL-. BY GC/MS -UG/L
WS61 FLUGRANTHElML, BENZOL), BY GC/MS :UG/L
WS62 FLUORANTHENE. BENZSO(K). BY GC/MS ! UG/L
WS63 PYRENE. BEN?0<A). BY GC/MS : UG/L
WS64 INDENOU . 2 . 3-CD) PYRENE : UG/L
V,'c-,(rtr. iMTHR.-.r.nii: D J BEfv.TO' A . M? . fiV GC/MS :ijG/L
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 108F 109F
WSG6 PERYLENE . BENZOI G.H . I > . BY Gf./MS '• UC./L
WS67 CARBAZOLE ' : UG/L
WV03 CHLOROMETHANE . BY GC/MS : UG/L
WV04 BROMOMETHANE . BY GC/MS :.UG/L
WV05 VINYL CHLORIDE : UG/L
VA/06 CHLOROETHANE . BY GC/MS ':UG/L
WV07 METHYLENE CHLORIDE : UG/L
WV08 1 ,1-DICHLOROETHENE : UG/L
'V?y09 1 ,1-DICHLOROETHANE ":UG/L
WV10 1 .2-DICHLOROETHENE. TOTAL : UG/L
WV11 CHLOROFORM. BY GC/MS :UG/L
WV12 1 ,2-DICHLOROETHANE : UG/L
WV13 1 . 1 , 1-TRI CHLOROETHANE • UG/L
WV14 CARBON TETRACHLORIDE . BY GC/MS : UG/L
WV15 BROMODICHLOROMETHANE, BY GC/MS • UG/L
WV16 1 .2-DICHLOROPROPANE -UG/L
WV17 BENZENE. BY GC/MS : UG/L
WV19 TRICHLOROETHENE -UG/L
WV20 DICHLOROPROPENE. CIS-1,3-. BY GC/MS : UG/L
WV21 DIBRQMOCHLOROMETHAWE. BY GC/MS : UC/L
WV22 1 , 1 ,2-TR I CHLOROETHANE :UG/L
WV2'1 BROMOFORM. BY. GC/MS : UG/L
WV2b TETRACHLOROETHENE :UG/L
WV26 TOLUENE : UG/L
WV27 1 , 1 ,2,2-TETRACHLOROETHANE : UG/L
WV28 CHLOROBENZENE, BY GC/MS ' : UG/L
10 'J :
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
•10 U
•1C U
•10 II
• 10 U
: 18
: 10 U
•10 U
ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION
COMPOUND UNITS 108F 109F
WV29 ETHYL BENZENE. BY GC/MS :HG/L^.
WV30 ACETONE, BY GC/MS :UG/L
WV31 CARBON DISULFIDE. BY GC/MS ! UG/L
WV32 2-BUTANONE :. UG/L
WV33 VINYL ACETATE : UG/L
WV34 2-HEXANONE :UG/L
WV35 4-METHYL-2-PENTANONE : UG/L
WV36 STYRENE ! UG/L
fotfB? XYLENES.. TOTAL :UG/L
WV40 TRAWS-1 ,3-DICHLOROPROPENE : UG/L
2201 SAMPLE NUMBER ': MA
2202 ACTIVITY CODE : NA
. 'i r\ M
: 10 U
: 10 U
•10 U
IN/A o•10 U
:10 U
: 10 U
:10 U:. 1 0 U
108 :109
ISXP8 :ISXP8
PRELIMINARY DATASUBJECT TO REVISION
ACTIVITY ISXP8 MISSISSIPPI RIVER POOL #15
THE PROJECT LEADER SHOULD CIRCLE ONE - STORET, AIRS, OR ARCHIVE.
CIRCLE ONE: STORET AIRS ARCHIVE
•s
DATA APPROVED BY LABO FOR TRANSMISSION TO PROJECT LEADER ON) 10/10/91 16:08:52 BY
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: isxpSLAB: AATSCASE: 16873
ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: WATER DATA COMPLETED: 10/10/91
PARAMETERS
SILVERALUMINUMARSENICBARIUMBERYLLIUMCADMIUMCOBALTCHROMIUMCOPPERIRONMANGANESEMOLYBDENUMNICKELLEADANTIMONYSELENIUMTITANIUM •THALLIUMVANADIUMZINCCALCIUMMAGNESIUMSODIUM,,POTASSIUMMERCURY BY COLD VAPOR AA
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: isxpSLAB: AATSCASE: 16873
ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: isxpSLAB: AATSCASE: 16873
ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: WATER DATA COMPLETED: 10/10/91
PARAMETERS
SILVERALUMINUMARSENICBARIUMBERYLLIUMCADMIUMCOBALTCHROMIUMCOPPERIRONMANGANESEMOLYBDENUMNICKELLEADANTIMONYSELENIUMTITANIUMTHALLIUMVANADIUMZINCCALCIUMMAGNESIUMSODIUMPOTASS JCUMMERCURY BY COLD VAPOR AA
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS03900MATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS03900MATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS03900MATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: VOLATILES METHOD: CS03900MATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: AATSCASE: 16873
ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: SEDIMENT DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: AATSCASE: 16873
ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: SEDIMENT DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS03900MATRIX: SEDIMENT DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL #15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS03900MATRIX: SEDIMENT DATA COMPLETED: 10/10/91
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91
PARAMETERS
CHLOROMETHANEBROMOMETHANEVINYL CHLORIDE .-CHLOROETHANEMETHYLENE CHLORfDE1,1-DICHLOROETHYLENE1,1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENECIS-1, 3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORM1,1,2,2-TETRACHLOROETHENETOLUENE1,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON BISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTAL
EPA #SAMPLEDID #SMO #
UNITS
UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG
N UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG
E UG/KGUG/KGUG/KGUG/KGUG/KGUG/KG
E UG/KGUG/KG
E UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: VOLATILES METHOD: CS03900MATRIX: SEDIMENT DATA COMPLETED: 10/10/91
EPA #SAMPLEDID #SMO #
ISXP8103D07/31/910#3 A#2GL369
ISXP810407/31/910#4 A#17GL370
ISXP810507/31/910#5 A#lGL371
PARAMETERS UNITS
CHLOROMETHANEBROMOMETHANEVINYL CHLORIDE .CHLOROETHANEMETHY-LENE CHLORIDE1,1-DICHLOROETHYLENE1,1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORM1,1,2,2-TETRACHLOROETHENETOLUENE71,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON BISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTAL
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION
SITE: MISSISSIPPI RIVER POOL # 15
ACTIVITY: ISXP8LAB: PNELICASE: 16873
ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91
EPA #SAMPLEDID #SMO #
PARAMETERS UNITS
CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDE1,1-DICHLOROETHYLENE1,1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORM1,1,2,2-TETRACHLOROETHENETOLUENE,1,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON DISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTAL
U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION