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ANALYSIS TYPE: SEMIVOLAT1LES-PAGE 1
TLE: WATERLOO AB: TMA/NORCAL
COAL GAS MATRIX:METHOD:
SEDIMENT9303M02
UNITSCASE:
UG/KG11157
SAMPLE PREP: ANALYST/ENTRY: 1PLC REVIEWER: arny______ DATE : 02/02/8!
SAMPLES TK9B8001
DATA FILE :
TK9B8002
P64
TK9B8003 TK9B8004
PHENOL 12000 U 12000 U 11000 U 12000 UBIS(2-CHL0R0ETHYL) ETHER 12000 U 12000 U 11000 u 12000 U2-CHL0R0PHEN0L 12000 U 12000 U 11000 U 12000 u1.3 DICHLOROBENZENE 12000 U 12000 U 11000 U 12000 u1,4 DICHLOROBENZENE 12000 U 12000 U 11000 U 12000 uBENZYL ALCOHOL 12000 U 12000 U 11000 U 12000 u1.2 DICHLOROBENZENE 12000 U 12000 U 11000 u 12000 u2-METHYLPHENOL 12000 U 12000 U 11000 U 12000 uBIS <2-CHLOROISOPROPYL)ETHER 12000 U 12000 U 11000 U 12000 U4-METHYLPHENOL 12000 u 12000 U 11000 U 12000 uN-N1TROSO-DIPROPYLAMINE 12000 u 12000 U 11000 U 12000 uHEXACHLOROETHANE 12000 u 12000 U 11000 U 12000 uN1TROBENZENE 12000 u 12000 U 11000 U 12000 uISOPHORONE 12000 u 12000 U 11000 U 12000 u2-NITRGPHENOL 12000 u 12000 U 11000 U 12000 u2.4-DIMETHYLPHENOL 12000 u 12000 U 11000 U 1 2000 uBENZOIC ACID 60000 u 57000 U 53000 U 59000 u
(2-CHLOROETHOXY) METHANE DICHLOROPHENOL
12000 u 12000 U 11000 U 12000 u12000 u 12000 U 11000 U 12000 u
1,2.4-TRI CHLOROBENZENE 12000 u 12000 U 11000 U 12000 uNAPHTHALENE 1300 M 770 M 11000 U 3800 M4-CHLOROANILINE 12000 u 12000 U 11000 u 12000 uHEXACHLOROBUTAD1ENE 12000 u 12000 U 11000 u 12000 u4-CHLORO-3-METHYLPHENOL 12000 u 12000 U 11000 u 12000 u2-METHYLNAPHTHALENE 2400 M 12000 U 11000 u 9600 MHEXACHLOROCYCLOPENTADIENE 12000 U 12000 U 11000 u 12000 u2.4,6-TRICHLOROPHENOL 12000 U 12000 U 11000 u 12000 u2,4,5-TRICHLOROPHENOL 60000 U 57000 U 53000 u 59000 u2-CHLORONAPHTHALENE 12000 u 12000 U 11000 u 12000 u2-NITROANILINE 60000 u 57000 U 53000 u 59000 uDIMETHYLPHTHALATE 12000 u 12000 u 11000 u 12000 uACENAPHTHYLENE 3300 M 1200 M 11000 u 1 2000 u3-NITROANILINE 60000 U 57000 U 53000 u 59000 uACENAPHTHENE 12000 U 12000 U 11000 u 3300 M2.4-DINITR0PHEN0L 60000 U 57000 U 53000 u 59000 u4-NITROPHENOL 60000 U 57000 U 53000 u 59000 uDlBENZOFURAN 12000 u 12000 U 11000 U 1500 M2. 4-DINITROTOLUENE 12000 u 12000 u 11000 u 12000 U
ANALYSIS TYPE: SEMIVOLATILES-PAGE 2
FlTLE: WATERLOO COAL GAS
LAB: TMA/NORCALSAMPLE PREP: ANALYST/ENTRY
MATRIX: SEDIMENT METHOD: 9303M02
PLC REVIEWER: ,~,_r_nvDATA FILE : P65
UNITS: UG/KG CASE: 11157DATE: 02/03/89
SAMPLES TK9B8001 TK9B8002 TK9B8003 TK9B8004
2.6-DINITROTOLUENE 12000 U 12000 U 11000 U 12000 UDIETHYLPHTHALATE 12000 U 12000 U 11000 U 12000 U4-CHLOROPHENYL PHENYL ETHER 12000 U 12000 U 1 1000 U 12000 UFLUORENE 2300 M 12000 U 11000 U 6800 M4-NITROANILINE 60000 U 57000 U 53000 U 59000 U4.6-DINITR0-2-METHYLPHEN0L 60000 U 57000 U 53000 U 59000 UN-NITROSODIPHENYLAMINE 12000 U 12000 U 11000 U 12000 U4-BROMOPHENYL PHENYL ETHER 12000 U 12000 U 11000 U 12000 UHEXACHL0R0BEN2ENE 12000 U 12000 U 11000 U 12000 UPENTACHLOROPHENOL 60000 U 57000 U 53000 U 59000 UPHENANTHRENE 11000 M 830 M 11000 U 61000ANTHRACENE 1900 M 12000 U 11000 U 12000 UDI-N-BUTYLPHTHALATE 12000 U 12000 U 11000 U 12000 UFLUORANTHENE 5800 M 1500 M 650 M 6900 MPYRENE 10000 M 3800 M 6500 M 1 1000 MBUTYL BENZYL PHTHALATE 12000 U 12000 U 11000 U 12000 U3.3’ DICHLOROBENZIDINE 25000 U 24000 U 22000 U 24000 U^^JZO ( A ) ANTHRACENE 12000 U 12000 U 11000 U 12000 U
(2-ETHYLHEXYL)PHTHALATE 12000 U 12000 u 11000 u 12000 UCHRYSENE 4200 M 2100 M 1700 M 14000 JDI -N- OCTYL PHTHALATE 12000 U 12000 U 11000 U 12000 UBENZO(B)FLUORANTHENE 1600 M 1500 M 860 M 6300 MBENZO(K)FLUORANTHENE 2500 M 2200 M 590 M 4500 MBENZO(A;PYRENE 2800 M 2100 M 980 M 5300 MINDENO(1.2,3-CD)PYRENE 12000 U 12000 U 11000 U 2100 MD1BENZO(A.H)ANTHRACENE 12000 U 12000 U 11000 U 12000 UBENZO(G,H.I)PERYLENE 1400 M 12000 U 11000 U 12000 U
PHENOL 24000 U 24000 u 13000 u 24000 UBIS(2-CHL0R0ETHYL) ETHER 24000 U 24000 U 13000 u 24000 u2-CHLOROPHENOL 24000 U 24000 U 13000 u 24000 U1.3 DICHLOROBENZENE 24000 U 24000 U 13000 U 24000 u1,4 DI CHLOROBENZENE 24000 U 24000 U 13000 u 24000 uBENZYL ALCOHOL 24000 U 24000 U 13000 u 24000 u1.2 DICHLOROBENZENE 24000 U 24000 u 13000 U 24000 u2-METHYLPHENOL 24000 U 24000 u 13000 U 24000 uBIS(2-CHL0R0ISOPROPYL)ETHER 24000 U 24000 U 13000 U 24000 u4-METHYLPHENOL 24000 U 24000 U 13000 U 24000 uN-N1TROSO-DIPROPYLAMINE 24000 U 24000 U 13000 u 24000 uHEXACHLOROETHANE 24000 U 24000 U 13000 u 24000 uNITROBENZENE 24000 U 24000 u 13000 u 24000 uISOPHORONE 24000 U 24000 U 13000 u 24000 u2-NITROPHENOL 24000 U 24000 U 13000 u 24000 u2.4-DIMETHYLPHENOL 24000 U 24000 U 13000 u 24000 uBENZOIC ACID 120000 u 120000 U 62000 u 110000 u
2-CHL0R0ETH0XY ) METHANE 24000 u 24000 U 13000 u 24000 uDICHLOROPHENOL 24000 U 24000 U 13000 u 24000 u
1,2.4-TRI CHLOROBENZENE 24000 u 24000 U 13000 u 24000 uNAPHTHALENE 51000 13000 M 13000 u 1300004-CHLOROANILINE 24000 U 24000 U 13000 u 24000 uHEXACHLOROBUTADIENE 24000 u 24000 u 13000 u 24000 u4-CHLORO-3-METHYLPHENOL 24000 u 24000 U 13000 u 24000 u2-METHYLNAPHTHALENE 22000 M 9900 M 13000 u 170000HEXACHLOROCYCLOPENTADIENE 24000 U 24000 U 13000 u 24000 u2.4,6-TRICHLOROPHENOL 24000 u 24000 u 13000 u 24000 u2,4,5-TRICHLOROPHENOL 120000 U 120000 u 62000 u 110000 u2-CHL0R0NAPHTHALENE 24000 u 24000 U 13000 u 24000 u2-NITROANILINE 120000 u 120000 U 62000 u 110000 uDIMETHYLPHTHALATE 24000 u 24000 u 13000 u 24000 uACENAPHTHYLENE 34000 77000 13000 u 24000 u3-NITROANILINE 120000 u 120000 U 62000 u 110000 uACENAPHTHENE 24000 u 1900 M 13000 u 15000 M
2,4-DIN1TROPHENOL 120000 u 120000 U 62000 u 110000 u4-NITROPHENOL 120000 u 120000 U 62000 u 110000 uDIBENZOFURAN 3600 M 2400 M 13000 u 12000 M
2,4-DINITROTOLUENE 24000 u 24000 u 13000 u 24000 u
2,6-DINITROTOLUENE 24000 U 24000 U 13000 U 24000 UDIETHYLPHTHALATE ' 24000 U 24000 U 13000 U 24000 U4-CHLOROPHENYL PHENYL ETHER 24000 U 24000 U 13000 U 24000 UFLUORENE 7800 M 4800 M 13000 U 330004-NITROANILINE 120000 U 120000 U 62000 U 1 10000 U4.6-DINITR0-2-METHYLPHEN0L 120000 U 120000 U 62000 U 110000 UN-NITROSODIPHENYLAMINE 24000 U 24000 U 13000 U 24000 U4-BR0M0PHENYL PHENYL ETHER 24000 U 24000 U 13000 U 24000 uHEXACHLOROBENZENE 24000 U 24000 U 13000 U 24000 uPENTACHLOROPHENOL 120000 U 120000 U 62000 U 1 10000 uPHENANTHRENE 98000 J 35000 J 13000 U 690.00ANTHRACENE 24000 U 24000 U 13000 U 4600 MD 1 -N-BUTYLPHTHALATE 24000 U 24000 u 13000 U 24000 UFLUORANTHENE 97000 68000 13000 U 4600 MPYRENE 220000 J 150000 J 1800 M 8000 MBUTYL BENZYL PHTHALATE 24000 U 24000 u 13000 U 24000 U3.3’ DICHLOROBENZIDINE 48000 U 48000 u 25000 U 47000 U^feJZO(A)ANTHRACENE 160000 J 24000 u 13000 U 4200 M1R ( 2-ETHYLHEXYL ) PHTHALATE 5700 M 24000 u 13000 U 24000 UCHRYSENE 24000 U 140000 J 1200 M 4400 MDI -N-OCTYL PHTHALATE 24000 U 24000 u 13000 U 24000 UBENZO(B)FLUORANTHENE 75000 69000 13000 U 2600 MBENZO(K)FLUORANTHENE 56000 J 59000 J 13000 U 24000 UBENZO(A)PYRENE 69000 89000 13000 U 24000 UI NDENO(1.2,3-CD)PYRENE 32000 J 47000 J 13000 U 24000 UDIBENZO(A.H)ANTHRACENE 24000 U 24000 u 13000 U 24000 UBENZO(G,H.I)PERYLENE 57000 J 140000 J 13000 u 24000 U
PHENOL 23000 U 24000 U 24000 U 23000 UBISC2-CHL0R0ETHYL) ETHER 23000 U 24000 U 24000 U 23000 U2-CHL0R0PHEN0L 23000 U 24000 U 24000 U 23000 U1.3 DICHLOROBENZENE 23000 U 24000 U 24000 U 23000 U1,4 DICHLOROBENZENE 23000 U 24000 U 24000 U 23000 UBENZYL ALCOHOL 23000 U 24000 U 24000 U 23000 U1.2 DICHLOROBENZENE 23000 U 24000 U 24000 U 23000 U2-METHYLPHENQL 23000 U 24000 U 24000 U 23000 UBIS(2-CHL0R0ISOPROPYL)ETHER 23000 U 24000 U 24000 U 23000 U4-METHYLPHENOL 23000 U 24000 U 24000 U 23000 UN-NITROSO-DIPROPYLAMINE 23000 U 24000 U 24000 U 23000 UHEXACHLOROETHANE 23000 U 24000 U 24000 U 23000 UNITROBENZENE 23000 U 24000 U 24000 U 23000 UISOPHORONE 23000 U 24000 U 24000 U 23000 U2-N1TROPHENOL 23000 U 24000 U 24000 U 23000 U2.4-DIMETHYLPHENOL 23000 U 24000 U 24000 U 23000 UBENZOIC ACID 110000 U 120000 U 110000 U 110000 U
(2-CHL0R0ETH0XY) METHANE 23000 U 24000 U 24000 U 23000 U1R D I CHLOROPHENOL 23000 U 24000 U 24000 U 23000 U1.2,4-TRI CHLOROBENZENE 23000 U 24000 U 24000 U 23000 UNAPHTHALENE 23000 U 24000 U 24000 U 23000 u4-CHLOROANILINE 23000 U 24000 U 24000 U 23000 uHEXACHLOROBUTADIENE 23000 U 24000 U 24000 U 23000 u4-CHL0R0-3-METHYLPHEN0L 23000 U 24000 U 24000 U 23000 u2-METHYLNAPHTHALENE 23000 U 24000 U 24000 U 23000 uHEXACHLOROCYCLOPENTADIENE 23000 U 24000 U 24000 u 23000 u2.4,6-TR1CHLOROPHENOL 23000 U 24000 U 24000 u 23000 u2,4.5-TRICHLOROPHENOL 110000 u 120000 u 110000 u 110000 u2-CHLORONAPHTHALENE 23000 u 24000 u 24000 u 23000 u2-NITROANILINE 110000 u 120000 u 110000 u 110000 uDIMETHYLPHTHALATE 23000 u 24000 u 24000 u 23000 uACENAPHTHYLENE 670 M 24000 u 1400 M 23000 u3-NITROANILINE 110000 U 120000 u 110000 U 110000 uACENAPHTHENE 23000 U 24000 u 24000 U 23000 u2,4-D1NITROPHENOL 110000 U 120000 u 110000 u 110000 u4-NITROPHENOL 110000 U 120000 u 110000 u 110000 uDIBENZOFURAN 23000 u 24000 u 24000 u 23000 u2,4-DINITROTOLUENE 23000 u 24000 u 24000 u 23000 u
2.6-DINITR0T0LUENE 23000 U 24000 U 24000 U 23000 UD!ETHYLPHTHALATE 23000 U 24000 U 24000 U 23000 U4-CHLOROPHENYL PHENYL ETHER 23000 U 24000 u 24000 U 23000 UFLUORENE 23000 U 24000 u 24000 U 23000 u4-NITROANILINE 110000 U 120000 u 110000 U 110000 u4,6-DINITR0-2-METHYLPHEN0L 110000 U 120000 u 110000 U 110000 uN-N1TROSODI PHENYLAM INE 23000 U 24000 u 24000 U 2300 0 u4-BROMOPHENYL PHENYL ETHER 23000 U 24000 u 24000 U 23000 uHEXACHL0R0BEN2ENE 23000 u 24000 u 24000 U 23000 uPENTACHLOROPHENOL 110000 u 120000 u 110000 U 1 10000 uPHENANTHRENE 23000 u 24000 u 1300 M 23000 uANTHRACENE 23000 u 24000 u 24000 U 23000 uDI-N-BUTYLPHTHALATE 23000 u 24000 u 24000 U 23000 uFLUORANTHENE 860 M 24000 u 1800 M 23000 uPYRENE 1000 M 1800 M 3300 M 23000 uBUTYL BENZYL PHTHALATE 23000 U 24000 u 24000 U 23000 u3.3’ DICHLOROBENZIDINE 47000 U 48000 u 47000 U 47000 u4felZO ( A ) ANTHRACENE
(2-ETHYLHEXYL)PHTHALATE23000 U 1200 M 24000 U 23000 u23000 U 24000 U 24000 U 23000 u-
CHRYSENE 1200 M 24000 U 2500 M 23000 uDI -N- OCTYL PHTHALATE 23000 U 24000 U 24000 U 23000 uBENZO(B)FLUORANTHENE 23000 U 24000 U 24000 U 23000 uBENZO CK>FLUORANTHENE 23000 U 24000 u 24000 U 23000 uBENZO(A)PYRENE 23000 U 24000 u 24000 U 23000 uINDENO(1,2,3-CD)PYRENE 23000 U 24000 u 24000 U 23000 uDIBENZO(A,H)ANTHRACENE 23000 U 24000 u 24000 U 23000 uBENZO(G,H,I)PERYLENE 23000 U 24000 u 24000 U 23000 u
PHENOL 23000 U 25000 u 25000 U 23000 UBIS(2-CHL0R0ETHYL) ETHER 23000 U 25000 u 25000 U 23000 u2-CHL0R0PHEN0L 23000 U 25000 u 25000 U 23000 U1.3 DICHLOROBENZENE 23000 U ^ 25000 u 25000 U 23000 U1,4 DICHLOROBENZENE 23000 U 25000 u 25000 U 23000 UBENZYL ALCOHOL 23000 U 25000 u 25000 U 23000 U1.2 DICHLOROBENZENE 23000 U 25000 u 25000 U 23000 U2-METHYLPHENOL 23000 U 25000 u 25000 U 23000 UBIS(2-CHLOROISOPROPYL)ETHER 23000 U 25000 u 25000 U 23000 U4-METHYLPHENOL 23000 U 25000 u 25000 U 23000 UN-NITROSO-DIPROPYLAMINE 23000 U 25000 u 25000 U 23000 UHEXACHLOROETHANE 23000 u 25000 u 25000 U 23000 uNITROBENZENE 23000 u 25000 u 25000 U 23000 UISOPHORONE 23000 u 25000 u 25000 U 23000 u2-NITROPHENOL 23000 u 25000 u 25000 u 23000 u2.4-DIMETHYLPHENOL 23000 u 25000 u 25000 U 23000 uBENZOIC ACID 110000 u 120000 u 120000 u 110000 u
(2-CHL0R0ETH0XY) METHANED I CHLOROPHENOL
23000 u 25000 u 25000 U 23000 u23000 u 25000 u 25000 U 23000 u
1,2,4-TRI CHLOROBENZENE 23000 u 25000 u 25000 U 23000 uNAPHTHALENE 23000 u 25000 u 25000 U 2200 M4-CHLOROANILINE 23000 u 25000 u 25000 u 23000 UHEXACHLOROBUTADIENE 23000 u 25000 u 25000 u 23000 U4-CHLORO-3-METHYLPHENOL 23000 u 25000 u 25000 u 23000 u2-METHYLNAPHTHALENE 23000 u 25000 u 25000 u 23000 uHEXACHLOROCYCLOPENTADIENE 23000 u 25000 u 25000 u 23000 u2.4,6-TRICHLOROPHENOL 23000 u 25000 u 25000 u 23000 u2.4.5-TR1CHLOROPHENOL 110000 u 120000 u 120000 u 110000 u2-CHL0R0NAPHTHALENE 23000 u 25000 u 25000 u 23000 u2-N1TROANILINE 110000 u 120000 u 120000 u 110000 uDIMETHYLPHTHALATE 23000 u 25000 u 25000 u 23000 uACENAPHTHYLENE 23000 u 25000 u 1700 M 1600 M3-NITROANILINE 110000 u 120000 u 120000 u 110000 UACENAPHTHENE 23000 u 25000 u 25000 u 23000 u2,4-DINITR0PHEN0L 110000 u 120000 u 120000 u 110000 u4-NITROPHENOL 110000 u 120000 u 120000 u 110000 uDIBENZOFURAN 23000 u 25000 u 25000 u 23000 u2,4-DINITROTOLUENE 23000 u 25000 u 25000 u 23000 u
ANALYSIS TYPE: SEMIVOLAT1LES-PAGE 2
ITLE: WATERLOO AB: TMA/NORCAL
COAL GAS MATRIX:METHOD:
SEDIMENT9303M02
UNITS CASE :
UG/KG 1 1157
SAMPLE PREP: ANALYST/ENTRY: PLC REV I EWER: p rrw DATE: 02/03/iDATA FILE P65
SAMPLES TK9B8013 TK9B8014 TK9B80 15 TK9B8016
2,6-DIN1TROTOLUENE 23000 U . 25000 U 25000 U 23000 UDIETHYLPHTHALATE 23000 U 25000 U 25000 U 23000 U4-CHLOROPHENYL PHENYL ETHER 23000 U 25000 U 25000 U 23000 UFLUORENE 23000 U 25000 U 25000 U 23000 u4-N1TROANILINE 110000 U 120000 U 120000 U 110000 u4.6-DIN ITR0-2-METHYLPHEN0L 110000 U 120000 U 120000 U 110000 uN-NITROSODI PHENYLAM INE 23000 U 25000 U 25000 U 23000 u4-BROMQPHENYL PHENYL ETHER 23000 U 25000 U 25000 U 23000 uHEXACHLOROBENZENE 23000 U 25000 U 25000 U 23000 uPENTACHLOROPHENOL 110000 U 120000 U 120000 U 1 10000 uPHENANTHRENE 23000 u 25000 U 25000 U 23000 uANTHRACENE 23000 u 25000 U 25000 U 2200 MD I -N-BUTYLPHTHALATE 23000 u 25000 U 25000 U 23000 UFLUORANTHENE 650 M 25000 U 2600 M 2400 MPYRENE 1100 M 1000 M 3400 M 4700 MBUTYL BENZYL PHTHALATE 23000 U 25000 U 25000 U 23000 U3.3’ DICHLOROBENZIDINE 47000 U 50000 U 50000 U 47000 U^ksIZO ( A ) ANTHRACENE 23000 U 25000 U 25000 U 3400 M^Ps (2-ETHYLHEXYL)PHTHALATE
23000 U 25000 U 25000 U 23000 UCHRYSENE 23000 U 25000 U 3400 M 3500 MDI -N-OCTYL PHTHALATE 23000 U 25000 U 890 M 23000 UBENZO(B)FLUORANTHENE 23000 u 25000 U 1900 M 2800 MBENZO(K)FLUORANTHENE 23000 u 25000 U 1900 M 2800 MBENZO(A)PYRENE 23000 u 25000 U 1400 M 2200 MINDENO(1.2.3-CD)PYRENE 23000 u 25000 U 25000 U 3200 MDIBENZO(A,H)ANTHRACENE 23000 u 25000 U 25000 U 23000 UBENZO(G.H,I)PERYLENE 23000 u 25000 U 25000 U 23000 U
ANALYSIS TYPE: SEMIVQLATILES-PAGE 1
^■TLE: WATERLOO COAL GAS MATRIX: SEDIMENT^XAB: TMA/NORCAL
METHOD: 9303M02SAMPLE PREP: ANALYST/ENTRY: PLC REV I EWER ; I'T, c n x
DATA FILE : >64
SAMPLES TK9B8017 TK9B8018 TK9B8019
PHENOL 23000 U 26000 U 22000 UBIS(2-CHL0R0ETHYL) ETHER 23000 U 26000 U 22000 U2-CHLOROPHENOL 23000 U 26000 u 22000 u1,3 DICHLOROBENZENE 23000 U 26000 u 22000 U1,4 DICHLOROBENZENE 23000 U 26000 u 22000 UBENZYL ALCOHOL 23000 U 26000 u 22000 U1,2 DI CHLOROBENZENE 23000 U 26000 u 22000 u2-METHYLPHENOL 23000 u 26000 u 22000 UB1S(2-CHL0R01SOPROPYL)ETHER 23000 u 26000 u 22000 U4-METHYLPHENOL 23000 u 26000 u 22000 uN-N1TROSO-DIPROPYLAMINE 23000 u 26000 u 22000 UHEXACHLOROETHANE 23000 u 26000 u 22000 UNITROBENZENE 23000 u 26000 u 22000 UISOPHORONE 23000 u 26000 u 22000 U2-NITROPHENOL 23000 u 26000 u 22000 U2,4-DIMETHYLPHENOL 23000 u 26000 u 22000 UBENZOIC ACID 110000 u 130000 u 110000 UaK(2-CHL0R0ETH0XY) METHANE 23000 u 26000 u 22000 UV* DICHLOROPHENOL 23000 u 26000 u 22000 U1,2,4-TRI CHLOROBENZENE 23000 u 26000 u 22000 UNAPHTHALENE 5900 M 26000 u 22000 U4-CHLOROANILINE 23000 u 26000 u 22000 uHEXACHLOROBUTAD1ENE 23000 u 26000 u 22000 u4-CHLORO-3-METHYLPHENOL 23000 u 26000 u 22000 u2-METHYLNAPHTHALENE 4500 M 26000 u 22000 uHEXACHLOROCYCLOPENTADIENE 23000 U 26000 u 22000 u2,4,6-TRICHLOROPHENOL 23000 u 26000 u 22000 u2,4,5-TRICHLOROPHENOL 110000 u 130000 u 110000 u2-CHLORONAPHTHALENE 23000 u 26000 u 22000 u2-NITROANILINE 110000 u 130000 u 110000 uDIMETHYLPHTHALATE 23000 u 26000 u 22000 uACENAPHTHYLENE 54000 26000 u 22000 u3-NITROANILINE 110000 u 130000 u 110000 uACENAPHTHENE 23000 u 26000 u 22000 u2,4-DINITROPHENOL 110000 u 130000 u 110000 u4-NITROPHENOL 110000 u 130000 u 110000 uDIBENZOFURAN 2600 M 26000 u 22000 u2,4-DINITROTOLUENE 23000 U 26000 u 22000 u
UNITS CASE : DATE:
UG/KG1115702/02/89
ANALYSIS TYPE: SEMIVOLATILES-PAGE 2
UNITS CASE : DATE:
SAMPLES TK9B8017 TK9B8018 TK9B80 19
2.6-DINITR0T0LUENE 23000 U 26000 U 22000 UDIETHYLPHTHALATE 23000 U 26000 U 22000 U4-CHLOROPHENYL PHENYL ETHER 23000 U 26000 U 22000 UFLUORENE 3900 M 2100 M 22000 U4-NITROANILINE 110000 U 130000 U 110000 U4,6-DINITRO-2-METHYLPHENOL 110000 U 130000 U 110000 UN-NITROSODI PHENYLAM INE 23000 U 26000 U 22000 u4-BROMOPHENYL PHENYL ETHER 23000 U 26000 U 22000 uHEXACHLOROBENZENE 23000 U 26000 U 22000 uPENTACHLOROPHENOL 110000 U 130000 U 110000 uPHENANTHRENE 37000 J 9700 M 1900 MANTHRACENE 23000 U 26000 U 22000 uDI-N-BUTYLPHTHALATE 23000 U 26000 U 22000 UFLUORANTHENE 88000 J 37000 2500 MPYRENE 200000 J 93000 J 3300 MBUTYL BENZYL PHTHALATE 23000 U 26000 u 22000 U2^3’ D1CHLOROBENZIDINE 47000 U 52000 u 44000 UHZO (A) ANTHRACENE 23000 U 26000 u 22000 UWs (2-ETHYLHEXYL)PHTHALATE
23000 U 26000 u 22000 UCHRYSENE 85000 J 50000 J 22000 UDI-N-OCTYL PHTHALATE 23000 U 26000 u 22000 UBENZO(B)FLUORANTHENE 57000 17000 M 22000 U
BENZO(K)FLUORANTHENE 41000 J 20000 M 1300 MBENZO(A)PYRENE 69000 23000 M 22000 UINDENO(1.2,3-CD)PYRENE 28000 15000 M 22000 UDIBENZO(A.H)ANTHRACENE 23000 U 26000 U 22000 UBENZO(G.H,I)PERYLENE 96000 J 49000 J 22000 U
* THIS IS A CRUDE ESTIMATION BASED ON RESPONSE RELATIVE TO AN INTERNAL STANDARD. AN AUTHENTIC STANDARD HAS NOT BEEN RUN.
** THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH ROUTINE AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY COMPOUND MASS SPECTRA AND RETENTION TIMES.
TENTATIVELY IDENTIFIED COMPOUNDS
TITLE: WATERLOO COAL GAS LAB: TMA/NORCAL ANALYST/ENTRY: PLC
* THIS IS A CRUDE ESTIMATION BASED ON RESPONSE RELATIVE TO AN INTERNAL STANDARD. AN AUTHENTIC STANDARD HAS NOT BEEN RUN.
*# THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH ROUTINE. AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY COMPOUND MASS SPECTRA AND RETENTION TIMES.
ANALYSIS TYPE: SEMIVGLATILE5-PA6E i
TITLEi WATERLOO COAL GAS matrix: WATER UNITSAAB! EPA REGION VII Kfc method: 6251W00 /)/ case:SAMPLE PREP: _ ANALYST /'ENTRY l MLG REVIEWER t date:
* THIS IS A CRUDE ESTIMATION BASED ON RESPONSE RELATIVE TO AN INTERNA-.. STANDARD. AN AUTHENTIC STANDARD HAS NOT BEEN RUN.
** THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH ROUTINE.. AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY COMPOUND NASS SPECTRA AND RETENTION TINES.
ANALYSIS TYPE: VOLATILES
'ITLE: SEDIMENT FOR VOLATILES MATRIX: SEDIMENT„AB: REGION VII ERA METHOD: 6241S00SAMPLE PREP: " ANALYST/ENTRY: DME REVIEWER:
CHLOROMETHANE 12 U 12 LI 12 U 60 UBROMOMETHANE U nn U -C. -iL LI 1 10 UVINYL CHLORIDE 14 U 14 IJ 14 U 70 UCHLOROETHANE 14 U 14 U 14 U 70 UMETHYLENE CHLORIDE 30 U 10 U 10 LI 50 L.lACETONE 10 U 10 U 1 0 IJ 50 IJCARBON DISULFIDE 5. 0 1.) 5. 0 U 5.0 U : r.::'
jL-—1 IJ1,1-DICHLUROETHENE 5. 0 IJ 5. 0 U 5. 0 U ur U1,1 DICHLOROETHANE 5.0 IJ 5. 0 U 5. 0 U ir; L.I1.2,-DICHLOROETHENE 5.0 U 5.0 u 5.0 IJ •—i ::r
-:’l •. J uCHLOROFORM 5. 0 U 5.0 IJ 5. 0 U 2 3 U1,2.DICHLOROETHANE 5.0 IJ 5.0 IJ 5.0 U 23 U2-BUTANONE 10 u 10 IJ 10 U 5 u1,1,1-TRICHLOROETHANE 5.0 IJ 5.0 u 5.0 U IJCARBON T E T R A C HL 0RIDE 5.0 u 5. 0 LI 5. 0 U in:; I..JVINYL ACETATE 10 IJ 10 LI 10 IJ 50 uBRGM0DI ChiL.OROMETHANE 5. 0 IJ 5.0 U 5.0 U cr IJ
2—D I CHLOROPROPAME ^Pl.S-1.3-DICHL0R0PR0PENE
5.0 IJ 5.0 IJ 5.0 U 25 Li5. A U 5.0 U 5.0 IJ 23 I...I
TRICHLOROETHENE 5.0 LI 5. 0 LI 5. 0 U •~I fVJ-.ill IJ
BENZENE 500 5. 0 U 5. 0 u 620DIBROMQCHLOROMETHANE 5. 0 IJ 5.0 U 5.0 IJ u1,1,2-TRICHLOROETHANE 5. 0 IJ 5.0 IJ 5.0 u cr I...ITRANS-1,3-DICHLOROF'ROPENE 5. 0 U 5.0 IJ 5.0 IJ i::.~
oi. wJ LIBROMOFORM 5. g U 5. 0 U 5.0 u . nr IJ
4-METHYL-2-PENTAN0NE 10 Ll 10 IJ 10 u 50 IJ2--HEX ANONE 10 U 10 IJ 10 u 50 L.l1,1,2,2-TETRACHL0R0ETHANE 5. 0 IJ 5.0 U 5.0 IJ •—» ur
/.._i IJ
TETRACHLOROETHENE 5. 0 U 5. 0 IJ 5. 0 u ■—i cr UTOLUENE 87 5.0 U 5.0 LI T i'7'jCHLOROBENZENE 5. 0 U 5. 0 LI 5. 0 IJ ■~i rr
oiL -..J IJETHYL BENZENE 65 5.0 U 5.0 IJ 13200STYRENE 5. 0 U 5. 0 IJ 5.0 LI rr; IJTOTAL XYLENES 19 5.0 U 5. 0 U 770
ANALYSIS TYPE: VOLATILES
|T I TLE : SEDIMENT FOR VOLATILESLAB; REGION VII EPASAMPLE PREP; ANALYST/ENTRY:
MATRIX: SEDIMEN METHOD: 624 IS®0
DME REVIEWER: __DATA FILE : D10
UNITS; UG/CASE; *' UJ°
DATE; 12/14/88
SAMPLES TK9B31009 TK9B8010 TK9B8011 1 K 9 B o 0 1 *•'
‘r •CHLOROMETHANE 12 U 12 U 12 U 12 UBROMOMETHANE U *L. Xi. U IJ ••“•l •” UVINYL CHLORIDE 14 u 14 U 14 U 14 UCHLOROETHANE 14 u 14 U 14 IJ 14 LiMETHYLENE CHLORIDE 10 u 10 U 15 U 12 Uacetone 10 u 10 U 10 U 10 IJCARBON DISULFIDE 5.0 u 5.0 LI 5.0 U 5.0 U1„1-DICHLOROETHENE 5. 0 IJ 5. 0 U 5.0 IJ 5. 0 U1„1 DICHLOROETHANE 5. 0 u 5. 0 LJ 5. 0 IJ 5 „ 0 LJ1,2,~DICHLOROETHENE 0.0 !J 5.0 IJ 5.0 IJ 5.0 IJCHLOROFORM 5. 0 IJ 5.0 U 5. 0 IJ 5. 0 U1,2,DICHLOROETHANE 5. 0 u 5.0 U 5.0 IJ 5. 0 IJ2-BUTANONE 1 0 u 1 0 IJ 10 u 1 0 i.jI,!,1-TRICHLOROETHANE 5.0 IJ 5. 0 Ll 5.0 IJ 5. 0 IJC A R B 0 N T El T FS A L H L GRIDE 5.0 LI 5. 0 IJ 5,0 u 5. 0 IJVINYL ACETATE 10 U 10 U 10 Ll 10 IJB R 0 r 10 D I C H L 0 R 0 M E T H A N E 5. 0 IJ 5. 0 LJ- 5. 0 Ll 5 0 u
2 —DICHLGROPROPANE 5.0 u 5. 0 LJ 5.0 U cr •_J D uS-1,3 -D ICHLOROPROPENE 0. 0 IJ 5. 0 Ll 5.0 U . I'-;'-1 U
IRICHLOROETHENE 5.0 LI 5.0 U 5.0 Ll 5.0 IJBENZENE 5. 0 LJ 5. 0 U 5.0 U 5.0 uDIBROMOCHLOROMETHANE 5. 0 IJ 5.0 L! 5.0 U 5, 0 LJ1,1.2--TR I CHLOROETHANE 5. 0 IJ 5.0 IJ 5.0 U 5. 0 LJTRANS-1,3-D ICHLOROPROPENE 5.0 U 5.0 U 5. 0 U 5. 0 LJBROMOFORM 5. 0 LI 5. 0 U 5. 0 IJ 5.0 LJ4-METHYL-2-PENTANONE 10 LI 10 U 10 U 10 LJ2-HEXANOME 10 U 10 U 10 U 10 IJ1,1,2,2-TETRACHL0R0ETHANE 5. 0 U 5.0 U 5.0 U 5. 0 LJTETRACHLORQETHENE 5. 0 IJ 5. 0 IJ 5. 0 U 5.0 LiTOLUENE 9. 0 5,0 U 5.0 U 5. 0 LJCHLOROBENZENE 5. 0 Ll 5. 0 U 5. 0 U 5.0 UETHYL BENZENE 49 5. 0 U 5.0 U 5. 0 uSTYRENE 5. 0 U 5. 0 U 5. 0 U 5. 0 uTOTAL XYLENES 16 5.0 IJ 5.0 Ll 5. 0 u
ANALYSIS TYPE: VOLATILES
'ITLE: SEDIMENT FOR VOLATILES rLAB: REGION VII ERA
CHLOROMETHANE 12 U 12 U 12 LI 12 UBROMOMETHANE U U 'T' •**? U uVINYL CHLORIDE 14 U 14 IJ 14 U 1-1 UCHLOROETHANE 14 U 14 u 14 U 1 4 UMETHYLENE CHLORIDE 14 U 14 u 14 IJ 14 UACETONE 10 U 10 IJ 10 LI 10 IJCARBON DISULFIDE 5. 0 U 5. 0 u 5. A U b „ 0 U1 , 1-DICHLORGETHENE 5-0 U 5.0 LI 5 „ 0 U b. I-:!-' LJ1,1 DICHLOROETHANE 5.0 IJ 5.0 IJ 5. 0 IJ b. 0 !J1,2,-DICHLORGETHENE 5.0 IJ 5. 0 IJ 5. 0 U 5. 0 IJCHLOROFORM 5- 0 U 5. 0 U 5.0 IJ 5 - 0 IJ1,2,DICHLOROETHANE 5.0 IJ 5. 0 U 5.0 IJ 5. 0 u2-BUTAHONE 10 LI 10 IJ 10 U 10 IJ1,1,1-TRICHLOROETHANE 5 „ 0 U 5. 0 u 5.0 IJ 5. 0 IJCARBON TETRACHLORIDE 5- 0 U 5« 0 IJ 5. 0 u 5.0 uVINYL ACETATE 10 U 10 LI 10 u 1 0 IJBROMODICHLOROMETHANE 5. 0 U 5. 0 IJ 5. 0 u 5. 0 IJ
2—DICHLOROPROPANE 5. 0 U 5. 0 IJ 5.0 LI 5. O uWts-1,3-DICHL0RDPR0PEME 5.0 U 5. 0 U 5. 0 U 5. 0 uTRICHLORGETHENE 5. 0 U 5.0 U 5 - 0 LI 5. 0 uBENZENE 5. 0 IJ 5. A U 5. 0 U 5.0 uDIBRGMOCHLOROMETHANE 5. 0 U 5.0 IJ 5.0 U 5,0 IJ1,1,2-TRICHLOROETHANE 5. 0 LI 5.0 LI 5.0 U 5. 0 uTRANS -1,3--DICHL0R0PR0PENE 5 - 0 U 5.0 U 5. 0 U 5. 0 IJBROMOFORM 5. 0 U 5.0 LI 5.0 u 5.0 U4—METHYL—2—F’ENT ANONE 10 IJ 10 U 10 u 10 U2—HEXANDNE 10 U 10 U 1 0 IJ 10 IJ1 , 1,2,2-TETRACHL0R0ETHANE 5.0 IJ 5.0 IJ 5.0 IJ 5. 0 ijTETRACHLOROETHENE 5.0 U 5.0 LI 5. 0 u 5.fJ UTOLUENE , 5.0 LI 5. 0 U 5.0 u 5.0 LlCHLOROBENZENE 5. 0 LI 5.0 IJ 5.0 u 5.0 UETHYL BENZENE 5. 0 LI b. k) IJ 5.0 IJ 5.0 IJSTYRENE 5. 0 U 5. 0 U 5.0 IJ 5. 0 IJTOTAL XYLENES 5.0 U 5.0 u 5. 0 u 5.0 LJ
ANALYSIS TYPE: VOLATILES
ITLE: SEDIMENT FOR LAE: REGION VII EPA
SAMPLE F’l
'OLATILES MATRIX: SEDIMENTMETHOD: 6241S00
ANALYST/ENTRY: DME REVIEWER:DATA FILE : D 1 0 -.2 j.
SAMPLES TK9B8:017 TL:9B801S TK9B8019
CHLQROMETHANE 12 U 12 U 12 UBROMOMETHANE jL. U 2- jL. U UVINYL CHLORIDE 14 IJ 14 IJ 14 UCHLQROETHANE 14 u 14 u 14 UM E T H Y l.. E N E C H L 0 RID E 10 u 10 u 10 UACETONE 1 0 u 10 Ll 1 0 UCARBON DISULFIDE 5.0 u 5. 0 U 5. 0 u1 , 1-DICHL.ORQETHENE 5.0 u 5.0 U 5. 0 IJ1.1 DICHLQROETHANE 5. 0 IJ 5. 0 IJ 5.0 u1.2. --DICHLOROETHENE 5.0 u 5. 0 IJ 5.0 uCHLOROFORM 5.0 IJ 5 - !i-‘ LI 5. 0 u1,2.DICHLOROETHANE 5.0 u 5.0 Ll 5.0 u2-BUTANONE 10 u 10 IJ 10 IJ1,1,1-TRICHLOROETHANE 5.0 u 5. 0 U 5.0 LlCARBON TETRACHLORIDE 5. 0 IJ 5.0 IJ 5. 0 UVINYL ACETATE 10 u 10 IJ 1 0 U
BROMODICHLOROMETHANE 5. 0 u 5.0 U 5.0 U^2 — DICHLOROPROPANE 5.0 LI 5. 0 U 5. 0 Llls-1.3-DICHL0RDPR0PENE 5, 0 u 5. 0 U 5. 0 LlTCICHLOROETHENE ■ 5.0 u 5. 0 U 5.0 U
BENZENE 5. 0 IJ 5. 0 U 5. 0 UDIBRDMOCHLOROMETHANE 5. 0 LI b » ! ■: u 5. 0 Ll1,1,2-TP ICHLOROETHANE 5.0 U 5. 0 Ll 5. 0 UTRANS-1.3- D ICHLOROPROPENE 5.0 U b. it ' u 5. 0 U
BROMOFORM 5. 0 U 5.0 Ll 5.0 U
4 - M E T H Y L. - 2 -PE N T A N 0 N E 10 LI 10 U 10 U
2—HEXANONE 10 LI 10 U 10 IJ1,1,2,2-TETRACHL0R0ETHANE 5,0 U 5. 0 U 5.0 UTETRACHLOROETHENE 5.0 U 5.0 IJ 5.0 uTOLUENE 5.0 IJ 5.0 Ll 5.0 IJ
CHLOROBENZENE 5. 0 LI 5. 0 IJ 5. 0 IJ
ETHYL BENZENE 5. 0 U 5. 0 U b. U) Ll
STYRENE 5. 0 LI 5.0 IJ 5.0 Ll
TOTAL XYLENES 5.0 IJ 5.0 Ll 5.0 U
UNITS: UG/(C.k CASE;DATE: 12/14/E
ANALYSIS TYPE: VOLATILES
TITLE: WATER FOR VOLATILES MATRIX: WATER UNITSLAB: REGION VII ERA METHOD: 62 41 W00 CASE:SAMPLE PREP: ANALYST/EN" 'RY: DME REVIEWER:
DATA FILE : DllDATE:
SAMPLES TK9B8102 TK9BB1 05 F
CHLOROMETHANE 12 Ll 12 U ABROMOMETHANE r-i /—.»L. all. U UVINYL CHLORIDE 14 U 14 LICHLOROETHANE 14 U 14 UMETHYLENE CHLORIDE 10 U 10 U
ACETONE 10 U 10 UCARBON DISULFIDE 5.0 U 5.0 U1 . 1 - D I C H L. 0 R 0 E T H E N E 5.0 U 5. 0 U
1,1 D1CHLOROETHANE 5. 0 U 5.0 IJ
1,2,-DICHLOROETHENE 5. 0 U 5.0 U
CHLOROFORM 5.0 U 5.0 U1,2,DICHLOROETHANE 5.0 u 5. 0 U
2—BUT A NON El 10 U 10 U1,1,1~TRICHLOROETHANE 5 KI 0 U 5.0 IJC A R B 0 N T E T R A C H i... 0 RIDE 5. 0 L.I 5.0 U
VINYL ACETATE 10 LI 10 U
BRGMODICHLOROMETHANE 5.0 LI 5.0 u
1,2-DICHL0R0PR0PANE 5,0 U 5. 0 LI
CIS-1„3-DICHL0R0PR0PENE 5.0 U 5.0 U
TRICHLOROETHENE 5.0 IJ 5.0 LI
^enzene 5.0 u 5.0 U
B R 0 M 0 C H L 0 R 0 M E T14 A N E 5.0 U 5.0 IJ
T,1,2-TRICHLOROETHANE 5.0 LJ 5. 0 LITRANS-1,3-DICHL0R0PRQPENE 5.0 IJ 5.0 IJBROMOFORM 5. 0 IJ 5, 0 U4—M E T H Y L—2—P E N T A N 0 N E 10 u 10 U
2-HEXANONE 10 IJ 10 U
1,1,2,2-TETRACHL0R0ETHANE 5.0 u 5.0 LI
T E! T R A C H L 0 R 0 E T H E N E 5.0 IJ 5 - 0 U
TOLUENE 5.0 IJ 5.0 IJ
CHLOROBENZENE 5. 0 u 5. 0 U
ETHYL. BENZENE 5.0 IJ 5. 0 u
STYRENE 5. 0 IJ 5. 0 u
TOTAL XYLENES 5.0 u 5.0 LI
' , ■
'"Hi"
•
UG/L
12/14/88
ecology and environment, inc.CLOVERLEAF BUILDING 3, 6405 METCALF, OVERLAND PARK, KANSAS 66202, TEL. 913/432-9961
International Specialists in the Environment
MEMORANDUM
TO: Andrea Jirka, PhD, Chief, LABOTHRU: Paul Doherty, DPO
FROM: Peggy Cox, TATTHRU: Audra Gier, ATATLO^^
Joe Chandler, TATI^?
DATE: February 2, 1989
SUBJECT: Review of data for WATERLOO COAL GAS TDD# T07-8810-044 PAN# T07-Z054-QSG
These data were reviewed according to the "Laboratory Data Validation Functional Guidelines for Evaluating Organic Analyses," February 1, 1988 revision and the "Laboratory Data Validation Functional Guidelines for Evaluating Pesticides and PCBs."
The following comments and attached data sheets are a result of Ecology & Environment, Inc.'s review of the above mentioned data from the contract laboratory.
CASE NO.: 11157 LABORATORY: TMA/NORCALCONTRACT NO.: 68-W8-0009 METHOD NO.: 9303M02SITE: WATERLOO COAL GAS EPA ACTIVITY : TK9B8REVIEWER: P. COX MATRIX: SOIL
Case 11157 contained 19 soil samples analyzed for base/neutrals and acids at the medium level concentration. Laboratory did not report tentatively identified compounds (TICS) on Form IF for several samples. Since identification and concentrations of the tentatively identified compounds were not known, instruction was to report them wifeh^fiothing significant 'found.
HOLDING TIMES and PRESERVATION
No technical holding times or required preservation are specified for soil samples.
GC/MS TUNING
All GC/MS tunings and mass calibrations were within quality control limits for all associated data.
INITIAL and CONTINUING CALIBRATION
Pyrene, benzo(a)anthracene, chrysene, indeno(1,2,3-cd)pyrene along with other compounds were outside quality control limits for percent relative standard deviation (%RSD) on the initial calibration. Several compounds including phenanthrene, anthracene, benzo(k)fluoranthene, dibenz(a,h)anthracene, and benzo(g,h,i)perylene were outside quality control limits for percent difference (%D) on the continuing calibrations. All sample data was qualified by the calibration rules.
INTERNAL STANDARD RESPONSE
All internal standard response areas were within a factor of 2 when comparing samples and their associated continuing calibration response areas.
BLANKS
Two method blanks were analyzed for base/neutrals and acids and no compounds were reported.
SURROGATE RECOVERY
All compounds were recovered within quality control limit requirements.
2
MATRIX SPIKE/MATRIX SPIKE DUPLICATE
A matrix spike/matrix spike duplicate was analyzed for base/neutrals and acids and 2,4-dinitrotoluene was outside quality control limit requirements for percent recovery on the matrix spike and matrix spike duplicate and 2-chlorophenol was outside control limits for percent recovery on the matrix spike. Uo data was qualified by the matrix spike/matrix spike duplicate.
PERFORMANCE EVALUATION SAMPLE
No performance evaluation sample was submitted to the laboratory for analysis.
COMPOUND IDENTIFICATION and QUANTITATION
All samples were correctly identified by mass spectra submitted for each positive sample response.