Transcript
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Sue FergusonLab Director
State License # n/aISO Accreditation #
17025:2017___________________Signature
03/12/2021
___________________Signed On
10427 Cogdill Road, Suite 500Knoxville, TN, 37932, US
Kaycha LabsNorthern Lights D8
N/AMatrix: Derivative
Certificateof Analysis
Sample:KN10308007-003Harvest/Lot ID: NLTS-D8-01
Seed to Sale #N/ABatch Date :03/04/21
Batch#: NLTS-D8-01Sample Size Received: 10 gram
Total Weight/Volume: N/ARetail Product Size: 1 gram
Ordered : 03/04/21sampled : 03/04/21
Completed: 03/12/21 Expires: 03/12/22Sampling Method: SOP Client Method
Mar 12, 2021 | Evolved, LLC61875 Broken Top Dr. #26Bend, OR, 97702, US
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsNOT TESTED
MycotoxinsNOT TESTED
ResidualsSolventsPASSED
FilthNOT TESTED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.267%Total CBD
0.043%Total Cannabinoids
80.279%
CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA
ND ND 0.015% ND 0.043% 0.015% 0.037% 0.267%79.889% 0.011% ND
ND ND0.150mg/g ND
0.430mg/g
0.150mg/g
0.370mg/g
2.670mg/g
798.890mg/g
0.110mg/g ND
LOD 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :113 0.2035g 03/10/21 09:03:27 113Analysis Method -Expanded Measurement of Uncertainty: Flower Matrixd9-THC:12.7%, THCa: 9.5%, TOTAL THC 11. 1%. These uncertaintiesrepresent an expanded uncertainty expressed at approximately the 95%confidence level using a coverage factor k=2 for a normal distribution.
Reviewed On -03/10/2116:42:03 Batch Date : 03/09/21 11:51:54
Analytical Batch -KN000539POT Instrument Used : HPLC E-SHI-008
Reagent Dilution Consums. ID
120320.R02 40 00298878031021.R01 200331059030321.R01 947.217Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis.). *Based on FL action limits.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Sue FergusonLab Director
State License # n/aISO Accreditation #
17025:2017___________________Signature
03/12/2021
___________________Signed On
10427 Cogdill Road, Suite 500Knoxville, TN, 37932, US
Kaycha LabsNorthern Lights D8
N/AMatrix : Derivative
Certificate of Analysis PASSEDEvolved, LLC
61875 Broken Top Dr. #26Bend, OR, 97702, USTelephone: 9493387078Email: evolved.bend@gmail.com
Sample : KN10308007-003Harvest/LOT ID: NLTS-D8-01Batch# : NLTS-D8-01Sampled : 03/04/21Ordered : 03/04/21
Sample Size Received : 10 gramTotal Weight/Volume : N/ACompleted : 03/12/21Expires: 03/12/22Sample Method : SOP Client Method
Page 2 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.05 ppm 0.3 NDACEPHATE 0.05 ppm 3 NDACEQUINOCYL 0.05 ppm 2 NDACETAMIPRID 0.05 ppm 3 NDALDICARB 0.05 ppm 0.1 NDAZOXYSTROBIN 0.05 ppm 3 NDBIFENAZATE 0.05 ppm 3 NDBIFENTHRIN 0.05 ppm 0.5 0.202BOSCALID 0.05 ppm 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.05 ppm 0.1 NDCHLORANTRANILIPROLE 0.05 ppm 3 NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDCHLORPYRIFOS 0.05 ppm 0.1 NDCLOFENTEZINE 0.10 ppm 0.5 NDCOUMAPHOS 0.05 ppm 0.1 NDCYPERMETHRIN 0.05 ppm 1 NDDAMINOZIDE 0.05 ppm 0.1 NDDIAZANON 0.05 ppm 0.2 NDDICHLORVOS 0.05 ppm 0.1 NDDIMETHOATE 0.05 ppm 0.1 NDDIMETHOMORPH 0.10 ppm 3 NDETHOPROPHOS 0.05 ppm 0.1 NDETOFENPROX 0.05 ppm 0.1 NDETOXAZOLE 0.05 ppm 1.5 NDFENHEXAMID 0.05 ppm 3 NDFENOXYCARB 0.05 ppm 0.1 NDFENPYROXIMATE 0.05 ppm 2 NDFIPRONIL 0.05 ppm 0.1 NDFLONICAMID 0.05 ppm 2 NDFLUDIOXONIL 0.05 ppm 3 NDHEXYTHIAZOX 0.05 ppm 2 NDIMAZALIL 0.05 ppm 0.1 NDIMIDACLOPRID 0.05 ppm 3 NDKRESOXIM-METHYL 0.05 ppm 1 NDMALATHION 0.05 ppm 2 NDMETALAXYL 0.05 ppm 3 NDMETHIOCARB 0.05 ppm 0.1 NDMETHOMYL 0.05 ppm 0.1 NDMEVINPHOS 0.05 ppm 0.1 NDMYCLOBUTANIL 0.05 ppm 3 NDNALED 0.05 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.05 ppm 0.1 NDPERMETHRINS 0.05 ppm 1 NDPHOSMET 0.05 ppm 0.2 ND
Pesticides LOD Units Action Level ResultPIPERONYL BUTOXIDE 0.05 ppm 3 NDPRALLETHRIN 0.05 ppm 0.4 NDPROPICONAZOLE 0.05 ppm 1 NDPROPOXUR 0.05 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.10 ppm 3 NDSPINETORAM 0.05 ppm 3 NDSPIROMESIFEN 0.05 ppm 3 NDSPIROTETRAMAT 0.05 ppm 3 NDSPIROXAMINE 0.05 ppm 0.1 NDTEBUCONAZOLE 0.05 ppm 1 NDTHIACLOPRID 0.05 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL SPINOSAD 0.02 ppm 3 NDTRIFLOXYSTROBIN 0.05 ppm 3 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By143 0.5006g 03/08/21 03:03:23 143Analysis Method - SOP.T.30.060, SOP.T.40.060 ,Analytical Batch - KN000528PESInstrument Used : E-SHI-125 PesticidesRunning On : 03/08/21 11:12:55 Batch Date : 03/08/21 08:47:29
Reagent Dilution Consums. ID022221.R20 5 P7364369022521.R11 00302193030821.R01030821.R02
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 57 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.060 Procedure for Pesticide Quantification Using LCMS).Analytes ISO pending. *Based on FL action limits. *
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Sue FergusonLab Director
State License # n/aISO Accreditation #
17025:2017___________________Signature
03/12/2021
___________________Signed On
10427 Cogdill Road, Suite 500Knoxville, TN, 37932, US
Kaycha LabsNorthern Lights D8
N/AMatrix : Derivative
Certificate of Analysis PASSEDEvolved, LLC
61875 Broken Top Dr. #26Bend, OR, 97702, USTelephone: 9493387078Email: evolved.bend@gmail.com
Sample : KN10308007-003Harvest/LOT ID: NLTS-D8-01Batch# : NLTS-D8-01Sampled : 03/04/21Ordered : 03/04/21
Sample Size Received : 10 gramTotal Weight/Volume : N/ACompleted : 03/12/21Expires: 03/12/22Sample Method : SOP Client Method
Page 3 of 4
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
PROPANE 500 ppm 5000 PASS ND
BUTANES (N-BUTANE) 500 ppm 5000 PASS ND
METHANOL 25 ppm 3000 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
PENTANES (N-PENTANE) 75 ppm 750 PASS ND
ETHANOL 500 ppm 5000 PASS ND
ETHYL ETHER 50 ppm 500 PASS ND
1.1-DICHLOROETHENE 0.8 ppm 8 PASS ND
ACETONE 75 ppm 750 PASS ND
2-PROPANOL 50 ppm 500 PASS ND
ACETONITRILE 6 ppm 60 PASS ND
DICHLOROMETHANE 12.5 ppm 125 PASS ND
N-HEXANE 25 ppm 250 PASS ND
ETHYL ACETATE 40 ppm 400 PASS ND
CHLOROFORM 0.2 ppm 2 PASS ND
BENZENE 0.1 ppm 1 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND
HEPTANE 500 ppm 5000 PASS ND
TRICHLOROETHYLENE 2.5 ppm 25 PASS ND
TOLUENE 15 ppm 150 PASS ND
XYLENES-M&P (1,3&1,4-DIMETHYLBENZENE)
10 ppm 150 PASS ND
XYLENES-O (1,2-DIMETHYLBENZENE)
5 ppm 150 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By138 0.02108g 03/10/21 02:03:56 138
Analysis Method -SOP.T.40.032Analytical Batch -KN000547SOL Reviewed On - 03/12/21 16:12:28Instrument Used : E-SHI-106 Residual SolventsRunning On : 03/11/21 11:21:04Batch Date : 03/10/21 10:27:26
Reagent Dilution Consums. ID
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 22 residual solvents.(Method: SOP.T.40.032 Residual Solvents Analysis via GC-MS). Analytes ISOpending. *Based on FL action limits.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Sue FergusonLab Director
State License # n/aISO Accreditation #
17025:2017___________________Signature
03/12/2021
___________________Signed On
10427 Cogdill Road, Suite 500Knoxville, TN, 37932, US
Kaycha LabsNorthern Lights D8
N/AMatrix : Derivative
Certificate of Analysis PASSEDEvolved, LLC
61875 Broken Top Dr. #26Bend, OR, 97702, USTelephone: 9493387078Email: evolved.bend@gmail.com
Sample : KN10308007-003Harvest/LOT ID: NLTS-D8-01Batch# : NLTS-D8-01Sampled : 03/04/21Ordered : 03/04/21
Sample Size Received : 10 gramTotal Weight/Volume : N/ACompleted : 03/12/21Expires: 03/12/22Sample Method : SOP Client Method
Page 4 of 4
Heavy Metals PASSED
Reagent Dilution Consums. ID022321.07030121.R30011521.R01020921.R14012221.R14
50 7226/0030021201015060
Metal LOD Unit Result Action Level (PPM)
ARSENIC-AS 0.04 ppm ND 1.5CADMIUM-CD 0.04 ppm ND 0.5MERCURY-HG 0.04 ppm ND 3LEAD-PB 0.04 ppm ND 0.5
Analyzed by Weight Extraction date Extracted By12 0.2655g 03/12/21 12:03:24 12
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -KN000542HEA | Reviewed On - 03/12/21 12:34:06Instrument Used : Metals ICP/MSRunning On :Batch Date : 03/09/21 14:11:35
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS. Analytes ISO Pending. *Based on FL action limits.
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