-
This report shall not be reproduced, unless in its entirety,
without written approval from Kaycha Labs. This report isan Kaycha
Labs certification. The results relate only to the material or
product analyzed. Test results areconfidential unless explicitly
waived otherwise. Void after 1 year from test end date. Cannabinoid
content of batchmaterial may vary depending on sampling error.
IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not
Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per
Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ)
are terms used to describe the smallest concentration that can be
reliably measured byan analytical procedure. RPD=Reproducibility of
two measurements. Action Levels are State determined thresholdsfor
human safety for consumption and/or inhalation. The result >99%
are variable based on uncertainty ofmeasurement (UM) for the
analyte. The UM error is available from the lab upon request.The
"Decision Rule" for thepass/fail does not include the UM. The
limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # 97164
___________________
Signature
10/05/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA
Kaycha LabsCBD Cooling Rub Peppermint
N/AMatrix: Derivative
Certificateof Analysis
Sample:GA00723001-001Harvest/Lot ID: CBD RUB 1000MG
Seed to Sale #N/ABatch Date :N/A
Batch#: CBD RUB 1000MGSample Size Received: 60 ml
Retail Product Size: 60Ordered : 07/23/20Sampled : 07/23/20
Completed: 08/03/20 Expires: 08/03/21Sampling Method: SOP Client
Method
Aug 03, 2020 | Southern Sun11613 SW 234th StArcher, FL, 32618,
US
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.039%THC/Container :23.682 mg
Total CBD
1.492%CBD/Container :895.212 mg
Total Cannabinoids
1.643%Total Cannabinoids/Container:986.088 mg
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA
0.052% ND 0.040% ND ND 0.018% ND ND 1.492% 0.039% ND
0.520mg/g ND
0.400mg/g ND ND
0.180mg/g ND ND
14.920mg/g
0.390mg/g ND
LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001
0.0001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date :
Extracted By :508 3.0091g 07/24/20 09:07:10 650
Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On -
07/28/20 16:51:33 Batch Date : 07/24/20 08:43:01Analytical Batch
-GA014256POT Instrument Used : GA-HPLC-001 2030C Plus Running On
:
Reagent Dilution Consums. ID
042720.09 400 280670882072020.R29 VAV-09-1020 Lot#
947.077072120.R02 6970145500298
19062406016466-042
Full spectrum cannabinoid analysis utilizing High Performance
Liquid Chromatography with UV detection (HPLC-UV). (Method:
SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method
SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSEDAnalyzed By Weight Extraction date LOD(ppm)
Extracted By650 NA 07/23/20 650
Analysis Method -SOP.T.40.013 Batch Date : 07/23/20
16:32:25Analytical Batch -GA014249FIL Reviewed On - 07/28/20
14:09:04Instrument Used : GA-Filth/Foreign Material
MicroscopeRunning On :
This includes but is not limited to hair, insects, feces,
packaging contaminants, and manufacturing wasteand by-products. An
SH-2B/T Stereo Microscope is use for inspection.
-
This report shall not be reproduced, unless in its entirety,
without written approval from Kaycha Labs. This report isan Kaycha
Labs certification. The results relate only to the material or
product analyzed. Test results areconfidential unless explicitly
waived otherwise. Void after 1 year from test end date. Cannabinoid
content of batchmaterial may vary depending on sampling error.
IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not
Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per
Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ)
are terms used to describe the smallest concentration that can be
reliably measured byan analytical procedure. RPD=Reproducibility of
two measurements. Action Levels are State determined thresholdsfor
human safety for consumption and/or inhalation. The result >99%
are variable based on uncertainty ofmeasurement (UM) for the
analyte. The UM error is available from the lab upon request.The
"Decision Rule" for thepass/fail does not include the UM. The
limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # 97164
___________________
Signature
10/05/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA
Kaycha LabsCBD Cooling Rub Peppermint
N/AMatrix : Derivative
Certificate of Analysis PASSEDSouthern Sun
11613 SW 234th StArcher, FL, 32618, USTelephone: (954)
336-1166Email: [email protected]
Sample : GA00723001-001Harvest/LOT ID: CBD RUB 1000MGBatch# :
CBD RUB1000MGSampled : 07/23/20Ordered : 07/23/20
Sample Size Received : 60 mlCompleted : 08/03/20Expires:
08/03/21Sample Method : SOP Client Method
Page 2 of 4
Pesticides PASSEDPesticides LOD Units Action Level
ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3
NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01
ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3
NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm
0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3
NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1
NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE
0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1
NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS
0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5
NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE
0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2
NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01
ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1
NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm
0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL
0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5
NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL
BUTOXIDE 0.1 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 ND
Pesticides LOD Units Action Level ResultPROPICONAZOLE 0.01 ppm 1
NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02
ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPIROMESIFEN 0.01 ppm 3
NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1
NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM
0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0 PPM 20 ND
TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3
NDTRIFLOXYSTROBIN 0.01 ppm 3 NDCHLORDANE * 0.01 PPM 0.1
NDPENTACHLORONITROBENZENE(PCNB) *
0.01 PPM 0.2 ND
PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 3
NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 1
NDCYPERMETHRIN * 0.01 PPM 1 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By635 , 1541
0.9950g 07/27/20 02:07:49 635 , 1541Analysis Method - SOP.T.30.065,
SOP.T.40.065 ,SOP.T.30.065, SOP.T40.070Analytical Batch -
GA014315PES , GA014391VOL Reviewed On- 07/28/20 14:09:04Instrument
Used : GA-LCMS-001 Pes , GA-GCMS-003 Triple Quad PestRunning On
:Batch Date : 07/27/20 14:02:46
Reagent Dilution Consums. ID072320.R12 10 280670882070620.R17
6970145500298071320.R01 VAV-09-1020 (947.077) / ALK-09-1412
(9291.179)
P734631 / P7411895
Pesticide screen is performed using LC-MS which can screen down
to below single digit ppb concentrations forregulated Pesticides.
Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060
Sample Preparation forPesticides Analysis via LCMSMS and
SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). *
VolatilePesticide screening is performed using GC-MS which can
screen down to below single digit ppb concentrationsfor regulated
Pesticides. Analytes marked with an asterisk were tested using
GC-MS.
-
This report shall not be reproduced, unless in its entirety,
without written approval from Kaycha Labs. This report isan Kaycha
Labs certification. The results relate only to the material or
product analyzed. Test results areconfidential unless explicitly
waived otherwise. Void after 1 year from test end date. Cannabinoid
content of batchmaterial may vary depending on sampling error.
IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not
Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per
Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ)
are terms used to describe the smallest concentration that can be
reliably measured byan analytical procedure. RPD=Reproducibility of
two measurements. Action Levels are State determined thresholdsfor
human safety for consumption and/or inhalation. The result >99%
are variable based on uncertainty ofmeasurement (UM) for the
analyte. The UM error is available from the lab upon request.The
"Decision Rule" for thepass/fail does not include the UM. The
limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # 97164
___________________
Signature
10/05/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA
Kaycha LabsCBD Cooling Rub Peppermint
N/AMatrix : Derivative
Certificate of Analysis PASSEDSouthern Sun
11613 SW 234th StArcher, FL, 32618, USTelephone: (954)
336-1166Email: [email protected]
Sample : GA00723001-001Harvest/LOT ID: CBD RUB 1000MGBatch# :
CBD RUB1000MGSampled : 07/23/20Ordered : 07/23/20
Sample Size Received : 60 mlCompleted : 08/03/20Expires:
08/03/21Sample Method : SOP Client Method
Page 3 of 4
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND
2-PROPANOL 50 ppm 500 PASS ND
ACETONE 75 ppm 750 PASS ND
ACETONITRILE 6 ppm 60 PASS ND
BENZENE 0.1 ppm 1 PASS ND
BUTANES (N-BUTANE) 500 ppm 5000 PASS ND
CHLOROFORM 0.2 ppm 2 PASS ND
DICHLOROMETHANE 12.5 ppm 125 PASS ND
ETHANOL 500 ppm PASS ND
ETHYL ACETATE 40 ppm 400 PASS ND
ETHYL ETHER 50 ppm 500 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
HEPTANE 500 ppm 5000 PASS ND
METHANOL 25 ppm 250 PASS ND
N-HEXANE 25 ppm 250 PASS ND
PENTANES (N-PENTANE) 75 ppm 750 PASS ND
PROPANE 500 ppm 5000 PASS ND
TOLUENE 15 ppm 150 PASS ND
TOTAL XYLENES 15 ppm 150 PASS ND
TRICHLOROETHYLENE 2.5 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By508 .0239g
07/27/20 01:07:20 508
Analysis Method -SOP.T.40.032Analytical Batch -GA014302SOL
Reviewed On - 07/29/20 14:54:38Instrument Used : GA-GCMS-001
Headspace SolventRunning On :Batch Date : 07/27/20 12:29:02
Reagent Dilution Consums. ID
24154107164282-100279984
Residual solvents screening is performed using GC-MS which can
detect belowsingle digit ppm concentrations. Currently we analyze
for 21 Residualsolvents.(Method: SOP.T.40.032 Residual Solvents
Analysis via GC-MS).
-
This report shall not be reproduced, unless in its entirety,
without written approval from Kaycha Labs. This report isan Kaycha
Labs certification. The results relate only to the material or
product analyzed. Test results areconfidential unless explicitly
waived otherwise. Void after 1 year from test end date. Cannabinoid
content of batchmaterial may vary depending on sampling error.
IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not
Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per
Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ)
are terms used to describe the smallest concentration that can be
reliably measured byan analytical procedure. RPD=Reproducibility of
two measurements. Action Levels are State determined thresholdsfor
human safety for consumption and/or inhalation. The result >99%
are variable based on uncertainty ofmeasurement (UM) for the
analyte. The UM error is available from the lab upon request.The
"Decision Rule" for thepass/fail does not include the UM. The
limits are based on F.S. Rule 64-4.310.
Jeremy CampbellLab Director
State License # CMTL-0001ISO Accreditation # 97164
___________________
Signature
10/05/2020
___________________Signed On
2444 NE 1st Blvd Suite 700Gainesville, FL, 32609, USA
Kaycha LabsCBD Cooling Rub Peppermint
N/AMatrix : Derivative
Certificate of Analysis PASSEDSouthern Sun
11613 SW 234th StArcher, FL, 32618, USTelephone: (954)
336-1166Email: [email protected]
Sample : GA00723001-001Harvest/LOT ID: CBD RUB 1000MGBatch# :
CBD RUB1000MGSampled : 07/23/20Ordered : 07/23/20
Sample Size Received : 60 mlCompleted : 08/03/20Expires:
08/03/21Sample Method : SOP Client Method
Page 4 of 4
Microbials PASSED
Analyte LOD ResultASPERGILLUS_FLAVUS not present in 1
gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER
not present in 1 gram.ASPERGILLUS_TERREUS not present in 1
gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1
gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043 / SOP.T.40.044Analytical Batch
-GA014214MIC Batch Date : 07/23/20Instrument Used : GA-093
PathogenDx ScannerRunning On :
Analyzed by Weight Extraction date Extracted By1748 0.9422g
07/27/20 1748
Dilution10Microbiological testing for Fungal and Bacterial
Identification via Polymerase Chain Reaction (PCR) methodconsisting
of sample DNA amplified via tandem Polymerase Chain Reaction (PCR)
as a crude lysate which avoidspurification. (Method SOP.T.40.043)
If a pathogenic Escherichia Coli, Salmonella, Aspergillus
fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus
terreus is detected in 1g of a sample, the sample fails
themicrobiological-impurity testing.
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002
ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND
0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND
0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch
-GA014316MYC | Reviewed On - 07/29/20 09:44:43Instrument Used :
GA-LCMS-001 MYCRunning On :Batch Date : 07/27/20 14:03:17
Analyzed by Weight Extraction date Extracted By635 0.9950g
07/27/20 02:07:58 635
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using
LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065
Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb).
Aflatoxin B1, B2, G1, and G2 must individually be