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1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: J 200A, LFJ602003C Product #: J 200A, LFJ602003C Issue Date: September 1, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the J 200A RoHS-Compliant series products manufactured by Littelfuse, Inc. Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 RemarksForm 585-047 Rev. A 2/21/06
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Page 1: New ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse... · 2013. 9. 28. · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: J 200A, LFJ602003C Product #: J 200A, LFJ602003C

Issue Date: September 1, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the J 200A RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks:

Form 585-047 Rev. A 2/21/06

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2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 N/A Base – Epoxy BMC FTI 400 3-8 2 N/A Phenolic Board FR-4 9-19 3 Al 6061-T5 Aluminum - Terminal 20-24 4 Al 6061-T5 Aluminum - Set screws 20-24 5 N/A 65Mn - Clip 25-28 6 N/A Copper Alloy T3 - Clamp 29-33 7 H65 Rivet - Brass 34-37 8 N/A Zinc Plated Steel - Screw Terminal 38-42 9 N/A Zinc Plated Steel - Flange 38-42 10 N/A Zinc Plated Steel – Hexagon Screw 38-42 11 N/A Tin Plating 43-46

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_scsTest Report No. SH10090106/ CHEM Date: S€o. 9. 2010 Page 1 of 6

JIAGANG SYNTHETIC MATERIALS CO,,LTD OF JIAXING159# XINDA ROAD, XIUZHOU INDUSTRY GARDEN OF JIAXING

The following sample(s) was/were submitted and identified by/on behalf of the ctienl as: EpOXy POTT|NG MATERIAL

: 10384398-2: 618(618-2y9001:JIAGANG SYNTHETIC I.|ATERIALS CO.,LTD OFJIAXING

SGS Ref No.Model No.Supplier

Dato ol Sample ReceivedTesting Pe od

Test Method

Test Result(s)

Conclusion

sEP 04,2010sEP 04, 2010 TO SEP 09, 2010

Please refer to nexl page(s).

: Please reter to nexl page(s).

Based on lhe performed tests on submitted sample(s), the results complywith the RoHS Directive 200295/EC and its subsequent amendments.

Signed tor and on behall ofSGS-CSTC Chemical Laboralory

,..Qr,'-Fan Jingjie, JJApproved Signatory

8&'s.k0*.Ytu Roa4sndid,chrE 2@233 E&E 06-2rrr!4PS3 ',$l 113-?r)6{55796 o5er HL66-205150{ds3 6 lsdfreF$d

Monb.ronh€scsGrcup (scss^)

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Test Report No. SH10090106/ CHEM Date: Sep.9,2010

Test Results:Descriplion lor specimen 1 : Black mate al

Page 2 of 6

A: RoHS Direclivo m02/95/EC

Tesl ltem(s)Cadmium (Cd)Lead (Pb)Itilercury (Hg)Hexavalent Chromium (CrVl) byalkaline extractionSum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl etherDibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl 6therP€ntabromodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl elherOctabromodiphenyl etherNonabromodiphenyl eth€rDecabromodiphenyl ether

Test lllethod (Ref erence)

IEC 62321: 2008, ICP-OESIEC 62321: 2008, ICP-OESIEC 62321: 2008, ICP-OES

IEC 62321:2008, UV-Vis

IEC 62321:2008, GC-MSIEC 62321:2008, GC'MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321: iD08, GC-MSIEC 62321:2008, GC-MSIEC 62321: 2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-MS

IEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321: 2008, GC-lt4SIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321;2008, GC-lrSIEC 62321: 2008, GC-lllSIEC 62321 : 2008, GC-I,S

Unit

mgKgmgKgmgKgmS/kg

ms/KsmgKgmS/kgmS/kgmsI(smg/kgmg/kgmgikgmg/kgmgikgmg/kgmsrgmg/kgmdkgm[yKgmdkgmgKgMEKgMEKqmgK9mgKgMEKg

Besult

N.D.N.D.N.D.

N,D.

N,D.N.D.N.D.N,D,N,D,N,D,N,D,N.D,N.D.N.D.N.D.N.D.N,D,N,D,N.D.N.D.N,D.N,D.N,D.N.D.N.D.N.D.

l,/lDL Limit

2 1002 10002 1000

2 1000' 1000

55555

5555555555- 10005555

Note:1. mgukg = ppm2. N.D. = Not Detected (< [,lDL)3. MDL = Method Detection Limit4. '-" = Not regulateds.The maximum permissible limit is quoted from the document 2005/618/EC am€nding RoHS dn€dtv€ 200295/EC

r i: 13! Bjrr'lird.s,\?s Rod'gs{btcnN 200231 E E:(06-l')slr@l63 rrE{$ 2rl6rq,$re

Mrmb.r ofi h. sos ooup (sGs sA)

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Test Report No. SH10090106/ CHEM Dare: S€p. 9,2010

B: PAHS (Polvnucl€ar Aromatlc HvdrocarbonslTesl ltem(s) Unil Tesl Method

zEK 01.2-08, GC-|4SzEK 01.2-08, GC-ltilSzEK 01.2-08, GC-I,SzEK 01.2-08, GC-I,SzEK 01.2-08, GC-[,|SzEK 01.2-08, GC-IjSzEK 01.2-08, GC-[,|SzEK 01.2-08, GC-t\,tSzEK 01.2-08, GC-MSZEK 01.2.08, GC-MSzEK 01.2-08, GC-t\rSzEK 01.2,08, GC-MSzEK 01.2-08, GC-|\4SzEK 01.2-08, GC-|\.4SzEK 01.2-08, GC-MSzEK 01.2-08, GC-MS

Page 3 of 6

Results l\,4DLN.D. 0.2N.D. O.2N.D. 0.2N.D. 0.2N.D. 0.2N.D. 0.2N.D_ 0.2N.D. O.2N.D. O.2N.D. 0.2N.D. 0.2N.D. 0.2N.D. 0.2N.D. 0.2N.0. o.2N.D. O.2N.D,

Naphthalene (NAP) mS/kgAcenaphthylene (ANY) mg/kgAcenaphthene (ANA) mdkgFluorene (FLU) mS/kgPhenanthreno (PHE) mdkgAnlhracene (ANT) mS/kgFluoranthene (FLT) mS/kgPyrene (PYR) m94<SBenzo{a)anthracene (BaA) mgikSChrysene (CHR) mgikgBenzo(b)fluoranthene (BbF) mdkSBenzo(k)fluoranthene (BkD mgr'kgBenzo(a)pyrene (BaP) mS/kglnd€no(1-,2,3-c,d)pyrene(lPY) mS/kgDibenzo(a,h)anthracene(DBA) mg/kgBenzo(g,h,i)perylene {BPE) mg/kgLim ol 16 PAHS acc. US EPA mg/kgNote:1. mg,4g = ppm2. N-D. = Not Detected (< MDL)3. MDL = l,rethod Detection Limit

ZEK 01.2-08 : Festrainino maxlmum valuea for products

Remark:"= Only PAH substanc€s >0,2 mg/kg are tak€n into account while calculating the sum of PAHS"' = ln case lhat the maximum values exceed the limits of category 1, but are within the limit6 of category 2,

one may confirm the suitabilily of the tesled material which indented lo be put in the mouth by additionalspecitic migralion tests ol PAH componenls based on DIN EN 1186ft and S64 LFGB 80.30-1. The conclusionof the migration test results must be made based on lood law criteria.

Theso tests were subconlracted to scs Gz CHEM LAB (G21009102625), (Date of testing: 2010/09/04-09/09).

" lh&E{be,tuMl9Eb,6N ?00233 mE:(16-r)5lttn!53 ErE:(s6rrl$e5!6?!

Parameter Calegory 1 Category 2 Category 3

aierial indented to be pul irhe mouth or matedalforoys with normal skin contaclor children aged < 36nonlhs

,latedals those are notncluded in Category 1, withnedictable conlact with lherkin longerthan 30 s. {long.erm skin contacl)-

vlaterials lhose are notncluded in Category 1 or 2,ffith prediclable skin conlactrpto 30 s (shon-term skin)ontact).

lenzolalpyrene (mg/kg) <MDL (<0.2)" ' 20

lum of 16 PAH (US EPA)mg/kg)" <MDL (<0.2)" ' 1 0 200

rnldlt*emaK@ 4 id.eeut6&.t ift.*.rh Fe E.

ir.mbd or rh. s6s G.@p ($Gs sA)

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SGSTest Report Page 4 ol 6No. SHl0090106/ CHEM Date: Sep. 9, 2010

ATTACH ENTSRoHS Testinq Ftow Chart

1) Name ol the person who made testing: Belta Wang / Cutey Yu / Ross Zhan2) Name ol the person in charge of testing: Adams Yu / Ryan Yang

Sample l\reasurement

Acid djgestion withmicrowave/ hotplate

Heating to90-95t forextraction

1)Alkal i Fusion /Dry Ashing

2) Acid todissolve

Filtralion andpH adjustment

Adding 1,5-diphenylcabazidefor color

Adding 1,5-diphenylcabazide

development indicates the

Pb/Cd/Hg PBBs,/PBDEs

Positive

Negative

hnd'Driw{,<a,orht 3.!rnd rbrM ^ei!rJ..!..r6tr. Indsrd dnih.ndid.lrd jr,drM,& mrtri,xdh:--rtuanm.E6.

ioqttNm m}lr*.rtr dn b. irdoi M rdrho d tuL ibtu.rrr'lr.hr ori. @riaiP.rtsxre olrlra ohhi! ds. lirDt! tr i6 h

?0nr3 trl!0t2tilr@5$ €tE66-20d19$679

Monbdot rh. sos ooup (9Gs 5A)

.Li j3dsrcd's,kF,Ydu Ro.4srE''r!,cih

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Test Report No. SH10090106/ CHEM Date: Sep.9,2010

ATTACHIiIENTS

Page 5 of 6

1) Name of the person2) Name ol lhe person

PAHST6sting Flow Chart

who made testing: Cutey Yuin charge of testing: Ryan Yang

M ^!mrior..!.:n b s. rmdb d

. h. / ! in.ddrhrd!.{rb. !dd&! ihnrd 6a!r o

lbub $qi hd't, rld{rrciLr b

seBMsYM Rod s',@,chlE ?00?33 f&f:l&-2r)Brt2!$ ltrE$6-rll6{s530n

Sample cutting / preparation

Sample Measuremenl

Solvenl extraction

Concentration/Dilution

Lr.hb., ot ihs SGS GrouD ISGS SAI

'Il rt

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scsTest Report No. SH10090106/ CHEM Date: Sep. 9,2010

Sample pholo :

kBlb'g'eIs]!lto|Ro.d'gE''lrlchiu f &EtN6-2r) 61{ra5$ lE rF (t6-2r)641167rlr@5e{ rn (36-4)!450q$ 1q.ll]Igf ga--,.

Page 6 of 6

SGS aulhenticate the photo on original report only

"" End of Repon "'

Mambdonh6 sGs Group (scs sA)

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Test Report

ZHUHA SEZ HARBOUR INDUSTRIAL LAMINATE LTD4,XINGGUO STREET,NANKENG INDUSTRIAL ZONE,ZHUHAJ CITYCHINA

The following sample(s) wasi,vere submitted and identified on behatf of the clients as :FR4(Z)

SGS Job No.SGS Intemsl Reference No.Date of Sample ReceivedTesting Period

Test Requested

Test M€thod

Test Results

Conclusion

No. CANEC1102810201 Date:27 Jul2011 Page 1 of 11

13260645 - SZ3.120 J!l201120 Jul 2011 - 27 Jul 2011

Selecl€d test(s) as reqlested by client.

Ple€se refer to next page(s).

Pl€ase refer to next page(s).

A: Bas€d on lhe peafomed tests on submitted samples, the results of Lead,Ivercury, Cadmium, Hexavalent chromium, Polybrominat€d biphenyls (pBB),Polybrominated diphenyl ethers (PBDE) comply with the limits as set byRoHS Diredive 201'1/65/EU Annex ll; recasting 2002y95/EC.

!y b s...fror.G) rdd .

Signed for and on behalf ofSG$CSTC Ltd.

Almay GaoApproved Signatory

! ! t - r -{s 3@ 6'!&!M4!-qlsm'Dolq^b d tr.oce!llr'! e do

;;n.d; ^N tud' d sr &dfldr r. rdvtrd tidi66in"-oiEi-it;ttiairafitia6

,.LDJdFbs.nn|condhld.or3.rubld b rrfr Id hdeB tu Ei.tunk Dolq^b d '!!lrrsa r! r! e doer dl

drhin rh. ffiL d drmrt i6Mmr.ri.hbotcr'mr 'flhelor. r.d dmrh Drrie! ro I hld.dd,;;.;,ii6Gii;idnsahruid.'idcun.nd rik6dn.n6rb,i,.'

r9(dr@sdndrP'rtu9uEdsnl1nir.lLdqdhqtuF{4th 51c@ I (36-E)3?155665 I B6-r)8a75113 ffid rq. @m

+l ,_rli &tt+fpEe+fli{tlls6€ |,|i51o633 I fe-432165566 t {sl0)€4075113 0 46cNitgtFs

Mohb6rolthoSGS Group1SGS SA)

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Test Report

Test Results:

lD for specimen 1Doscription for specimen I

A RoHS Dir€.dh 201 t/8siEu

Test ltem(s)Cadmium (Cd)Lead (Pb)Merdrry (Hs)Hexavalent Chromium (C l) byalkaline exlractionSum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabromobiphenylDecabromobiphenyl

Monobbmodiphenyl etherDib.oinodiphenyl elherTribromodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl etherHexabromodiphenyl etherHeptiabromodiphenyl etherOclabromodiphenyl etherNonabromodiphenyl elherDecabromodiphenyl elher

Note:1. mg/kg = ppm2. N.D. = Not Detec{ed (< MDL)3. MDL = Method Detection Limit4. "-" = Not regulated

No. CANEC11028'10201Dalet2T Jul2011 Page2 of 11

cANl1-028.102.001Lt-grey sheet w/ red printing

UnitmgKgmgKgmgrcmg/kg

mg/(gmS/kSmS/kSms/Ksm9Kgmg/Kgmg/Kgml|/Kgmg/KgmgKgmg/x9mg/Kgmg/Kgmg/Kgmg/K9mg/Kgmg/Kgmg/Kgms/Kgms/kgmgKsmgKs

ResultN.D.

5N.D.N.D,

N . D ,N , D ,N . D .N,D.N,D.N.D-N , D ,N , D ,N,D.N , D ,N , D .N , D ,N . D ,N . D .N , D ,N , D ,N . O .N . D .N.D,N.D.N.D.N.D.

IVlDL2222

55

55555

5

:

555555555

Limit100100010001000

1000

Test Method (Reference)IEC 62321:2008, ICPOESIEC 62321:2008, ICPOESIEC 62321:2008, ICP-OESIEC 62321:2008, UV-Vis

IEC 62321:2008, GC-ltlSIEC 62321:2008, GGMSIEC 62321:2008, GGMSIEC 62321:2008, GGMSIEC 62321:2008, ceMSIEC 62321:2008, GGMSIEC 62321:2008, GGMSIEC 62321:2008, GGltlSIEC 62321:2008, GGMSIEC 62321:2008, GGMS

IEC 62321:2008, GGMSIEC 62321 :2008, cc-L,lsIEC 62321:2008, GGMSIEC 62321:2008, GGMSIEC 62321:2008, GC-MSIEC 62321:2008, GC-[,|SIEC 62321:2008, GC-IIS1EC62321:2008, GC-NISIEC 62321:2008, GC-MSIEC 62321:2008, GCMS

1000

s d((${3dd! tu4!.ebn! '4-!a4!N

M.id' 'o|.|.fu'c|od!leun.1nni.dbr.iE|i.co1.ioTl.lEbd!I.Ddn.dn!!I ' !r4!]!!!!-g!!!rmildi.ft.ro" -d Edde' u Ei .r! 1.. srtr ' ̂ t rordd d h ! dcLNd b.dd'd d.tlnr*trtno' @h | & $ n f u c $ i { h i n f u n n l b n y L 6 b c l | . d . i d f t n . o c ! m . i t d o .i i i i i f f $ d r f d i F r r " i n i . i t t i " ' s ; ( b " i i . . ' , d , . ' l Y ' . b 6 c r . d | r d l h t r d o . J T . i t d o .tffJl.Hlnq .rllariochh .nd obl1fftr;.;'l;;ij .Ldh\i". '.o.., ;rdiM06i d 'B @dd' q ap..'

ry6rh.:rmpr'(3)r0dod

l$rcd!fr4li'ndhori9le$.llddrqr0dhFEr&ripldnoir 510663 r {86-a0)3?1s66 I (36-20)d207tn3 M.@ r93.M

+E ./_,1i .&*trrileq*+fli4*f 1${ t1.510663 I (36-20)u1s555s I @20}2075'13 " 1613€9 *

M.nber otlhoSGSGrcuo ISGS SA)

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Test Report

B: Phhelete(s)

Test ltem(6)

Dimethyt Phthatate (DMP)Diethyl Phthalate (DEP)Dibutyt Phthatate (DBP)aenzylbutyl Phthatale (BBP)Di-(2-€thylhexyl) Phthalate(DEHP)Diisononyl Phthalate (otNP)Di-n-oclyl Phthatale (DNoP)Diisodecyl Phthalate (DIDP)Diiso butyl Phtharate (DiBP)Dinonyl Phthatate (DNP)Diisoodyr Pharalate (DloP)Dipropyl Phthalate (DPrP)Dicydohexyl Phthalate (DCHP)Dipentyl Pt{halate (DPP)Dibenzyl Phthalate (DBZP)Diphenyl Phthalale (DPhP)Di-n-hexyl phthalato (DNHP)

Note :

No. CANEC1102810201DaIe:27 Jul2011 Page 3 of 1'l

Unit

% lwtwl% (wtuv)

Test Method (Reference)

EN14372:2004, GGMSEN14372:2004, GC-MSEN14372:2004, GGMSEN14372:2004, GC-MSEN14372:2004, GC-LlS

EN14372:2004, GC-[,4SEN14372: 2004, GC-[4SEN14372: 2004, GC,MSEN14372: 2004, GC-MSEN14372:2004, GGI,SEN14372:2004, GC-[4SEN14372:2004, GGMSEN14372:2004, GGMSEN14372:2004, GGMSEN14372:2004, GGMSEN143721 2004, GCiVSEN14372:2004, GC-[.4S

Result l\4DL

N.D. 0.003N.D. 0.003N.D. 0.003N.D_ 0.003N.D. 0.003

N.D. 0.01N.D. 0.m3N.D. 0.01N.D. 0.003N.D. 0.003N.D. 0.01N.D. 0.003N.D. 0.003N.D. 0.003N.D. 0.003N.D. 0.003N.D_ 0.003

1. mg/kg = ppm;0.1% = 1000ppm2. N.D. = Not Deteded (< MDL)3. MDL = Method Detedion Limit

For refeence:Entry 51/52 of Regulation (EC) No 5522009 €mending Annex XV of REACH Regulation (EC) No 1907/2006(previously restricted under Directive 2005/84/EC):FoT DBP. BBP. DEHP(1)Shall not be us€d as substances or in mixtures, in @ncentrations greater than 0,1 % by weight of theplasticised matedal, in toys and d$ldcare articles.(2) Toys and cfiildcare articles containing hese phthalates in a concent€tion greater than 0,1 % by weight of theplasticised mate.ial shall not be placed on the market.For DINP. DNOP. DIDP(1) Shall not be used as substanc€s or in mixtures, in concenbations greater than 0,1 % by weight of theplasticis€d material, in toys and childc€re articles which can be placed in the mouth by chitdren.(2) Such ioys and childcare articles containing thes€ phthalates in a concentration greater than O, 1 % by w€ightof the plasticised material shall not be placed on the ma*et.

y atl.d b [! c.ie.r coidndt oi s. 4t q &65 b o d hi'/tu e. @mbh' md-6.d[drr,bb.' ldJd'!!!fui|clcd.ldcu.nt'ub].dbr..m.ndcoid[bi,fuE|dod.Dem.6r1q4L"!s4!4!4Eq4ry

|' l .bbcn.d|idlhLd!c!n.i ldd.i dm!m.nk. rrib ddn./i lenioi b.

ryb'h'$hp.G)16d.d

rsl@lid{ldtd'Prdd[dntftlnrri.owEttdt0rdq0n 5106fi r (36-20)321ss55s r (36-5)3207sr13 "w,ci.sos,@h

. + E .J-ill .&tarittE**n***193+ ltl| 510663 I (36-10)32154a65 t (tF10)320r5113 e qBdlr€qF m

M.nb.rolrh. sGsGrouo (scssa)

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Test Report

G PFqS { Porflrdooclane sulfortab6 }

No. CANEC1102810201 Dare: 27 Jut 201 1 Page 4 of 1'1

Test ltem(s)

Perfl uorooclane sulfonales(PFOS)PFOS AcidPFOS Metal SaltPFOS Arnide

Nole:

Test ltem(s)

Naphthalene

Phenanthrene

Unit

mg/Kg

Test Method (Refe.ence)

EPA 3550C: 2007, LGMS

ResUIt MDL

N.D. 10

1. mg/kg = ppm2. N.D. = Not Detected (< l,roL)3. MDL = lrethod Detection Limit

Fo. reference: commission regulation (Eu) No 75712010 amending regul€tion (EC) No gSO/2004:(1 ) Fo. the purposes of this entry, Anide 4(1 ) (b) shatt apply to concentrations of PFOS equat to or below I 0mgikg (0,001 % by weight) when it occurs in subsiances or in preparations.(2) For the purposes of this entry, Anide 4( 1 ) (b) shall appty to concentrations of PFOS in s€mi-fnished productsor arlicles, or parts thereol if the concentration of PFOS is tower than 0,1 % by \,€ight catcdated with referenceto the mass of sAucturally or micro-structurally distinct parts that contain PFOS or, for texliles or other coatedmaterials, if the amount of PFOS is lower than 1 Ug /m, of the coated material.

D: TBBP.A aT€frabffbbl6oh€nol A)

Test ltem(s) unit Test Method (Reference)

Tetrabromobisphenol A mgks EPA 3550C:20O7, GGMS&LC-MS(TBBP.A)

Note:1. mg/kg = ppm2. N.D. = Not Detecled (< MDL)3. MDL = Method Detedion Limit

E: PAlls (Potynudo€r Aomelb FhdEcarborB)

Result

N,D,

MDL

1 0

Unit

mgKsmgKsmg/Kgmg/Kgmg/Kgmg'l(smsftsmgKg

Result

N.D.N.D.N.D.N . D .N,D,N.D,N.D.N.O.

l\,1DLo.2o.2o.20.20.2o.2o.2o.2

Test Method

ZEK 01,2{8, GGMSzEK 01.2{8, GG|USzEK 01.2-08, GC]VISzEK 01 .2-08, GC-tltSzEK 01.2-08, GC-MSzEK01.2-08, GGMSzEK 01_2-08, GGMSzEK 01.2{8, GGtttS

{ o' a qdd' d hdP i* e!e!l!!!!-31!-!g!:!!qM.nd.!or.r.tunlc b i i.r e!m.i

. deul r b.disd 6.r6ltndoi @ffi'qfiii,.'::8fifii$F$lifl'J"S#ilT,#i"1}ffiiiffi$trili:{di'i"ff.?i$ili["ffi:ili#f$$.i'jj#l]iifij'"'ii"irjii]io.i-iiG;;u:i;;i;;;i,i;';;;ii';fi"i,-n'Eduad..d.|'|*hL(qo,b'q.ryt'.ki'aro"dri.6nGmo

rv6rh'.,npb{i)bdld

&l6rb&rtdhoidoadfrtid @D.r.qllr0fitudrr0il 310663 t (86-20e155556 1186-482075113 lw.cu !g.om+E .ffi .&*AritftEfl,t!N*4f8196i ll: 5r0@ t {!6-20)0fl!6666 | €0-20182075113 . !FdrB€s0!.d

M6mb6f of $o SGSG.ouo ISGSSA)

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T€st ReDort

Test ltem(s)

Benz(a)anthraceneChrysen€Benzo(b)fuorantheneBenzo(k)fuorantheneBenzo(a)pyreneIndeno(1,2,}cd)pyreneDibenzo(a,h)anthraceneBenzo(g,h,i)peryleneSum of 1 6 PAHS acc. L,S EPA

Note:

Benzolalpyrcne(msn<s)Sum 16 PAH (US EPA)(msfts)"

No. CANEC110281020'1 Dale. 27 Jul 2011 Pag€ 5 of 11

Result l,rOL

N.D- O.2N.D. O.2N_D. O.2N.D. O.2N_D. 0.2N.D. O.2N.D. O.2N.D. O.2N.D.

Unit

mg/Kgmg/xgmg/kgmg/kgmg/Kgmg/Kgmg/KgmS/kgm9Kg

Test l/lethod

ZEK 01 .2-08, GC]\,|SZEK 01.2-08, GC]\ilSzEK 01.2-08, GC-|VSZEK 01.2-08, GC-l\,lSzEK 01.2-08, GC-l\rlSZEK 01.2-08, GC-l\ilSZEK 01.2-08, GC-lt/tSzEK 01.2-08, GC-t\4S

1. mg/kg = ppm2. N.D. = Not Detected (< MDL)3. IIDL = Method Detec{ion Limit

ZEK 0l .2{}8 : R€streinlm maximum vdur6 for productE

Calegory 1 Calegory 2Matedal indenled to b€ put in Maledals those are not Maledats those are notlhe mouth or material for toys included in Category 1 , with included in Category 1 or 2,with normal skin contact for predictiabte contact with the with prediclabte skin contactc}lildrcn aged < 36 nonths skin longerthan 30 s. up 10 30 s (short-term skin

(tong-tetm skin conlact). conl,act).

<MDL (<0.2)'-'

<MDL (<0.2)..'

Category 3

200

20

1 0

Rema* : _ = Only PAH substances >0.2 mg/kg are taken into account white catcltating the sum of PAHS"'= In case that the maximum values exceed the limits of category 1, but are within the limits of

category 2, one may @nfirm the suitability of the tested material which indented to be put in themouth by additional specifc migration tests of PAH components bas€d on DIN EN 1186ff and564 LFGB 80.30-1. The conclusion of the migration test results must be made based on foodlaw criteria,

rybs..!rr.(.)iond

$lcdlbtiddr|rs!&lldtnnldndgcnihsEt0lfi0lrgll0n 510663 I t+a)3al9€6!.5 I @-20)8,!75113 'w'cn'!gl 6m

+l J_ e*tri*lE{+n#**lss? t* 5!06s I {r.-?0)0ft55555 | (36-20)3,oali3 ' sschh!€lr3m

d l d & 6 6 b . d t n p l e & 4 \ ' i q

#;;i;d;d" b,;d @d" n.rid b t.- m! 6drd! b r'6.{ou!q!j!{ ^{1er ! &*i s-i;rdrroa ''

ffil;:{ili,{i.t1#,:ffiil1il#.i:g.lii'ffnl'*il1}-fl#i1ili:1ff:ijji*:}i :+}'F.i#

M€nb.rolrho scs Gloup (scssA)

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scsTest Report

ATTACI{ M EiITS

1) Nane otthe perron who made tesing: Be a \rhnq / Cdey yu,t Ross Zhan2) Name otthe person in chage of testing: Adams yu / Ryan yangiJ) _r h€se sampes wsre drssotvad totatly by pr€-conditionhg method according to below flow chfi

(Cr8+ and PBB8/PBDES test method Bxctudeo

No. CANECl102810201 Oate 27 Jut 2011

RoHS T.3thi Flow Ch.rt

Page 6 of 11

d' d *G.. o 3 d iip rM &! coTr!!!!r4=9E9t!Drr,orD ri,br r.dor rond eLrfn,ut|d b r.m .nd 6idr'or I b Ebdrenc omf.d d .!4t !t!s!4!q!!!e4!agMd-i i--td;" tu ; M.db" .;;ddBd trd.ri ^ id@' dh i do.er'+ ts rd! id heiiioiMr or @;'.;em$}6d*;;i;' i 'n.olc'st'.hdfu|'|iin'hconF1i!ro[asN|b''|lylldllc;;6'F;;.iiindi{';i;;ao']ig;d;"i'.&lfuhruifu'idgnd1d'r;'.6fu.-|4"di.apd!.-.

j l$l(drto{ld.hr!{tuC$E rdtrdidob.lqrr0ii|06Cl1on s10663 t {!6-rq321s5656 I (86-6)66talIt lwct 6sr.d: 4t.l-i{ .a*frtantE**tl,t*l1s3B bl: sto663 i @9q8456666 r €&432075113 . ro3dn€.6.6,

Bample Preparatlon

Sample Meagurement

Atld digestion withmicrowave.i hotslate

Sample solvente)draction

lVetallicmaterial

Concentraticn/Oilution of effactlon

9olLrtionAdding digestion

reagent

Heeting toS0-95'C forertraction

Boiling waterextrection

'l) Alkeli Fusion /DryAshing

2) Acid todiasolve

Filretion endpH adjustment

Adding 1,5-diphenylcaltazidefor colordev€lopment

Adding 1,5-diphEnylcelbazidefor colordevelopment

A rsd colorindicetBs thepresence of cF..lf necegaary

Fb/CdHt PBB!'/FBOET

Positjve

egetive

M.mb.roltho scs Goup (SGSSA)

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T€st Report

ATTACI{II ENTS

Name of the persmName of the persm

Ptlhdates Testirg Flcv Chatt

who made testhg: Tina Zheoin chage dtesting: Ryen Yang

No. CANEC1102810201Oatet 27 Jul2011 Page 7 of 11

r )

d q u.s,D s.r rnr /le qLq 19!1!l!!:.y lLdm.M.d.'o,..ch c b;d do.un.d.dbld r bnr md 6duor t r rkac oar '$ n {P44!4!ErSs-*""* i'E:91 11":1-lil1" ':T:l:11

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;,;;i.l;'r;;d; oiih: ;;;i;;p;.di- ordr! do-.-r b *b"1ui ,.d ondo. mry b F6add b.hom ilhier..,.oon'6t.'Mttos..rnp.(.)r.dd

lStrd!R.4hdrharu!tu@llldnao06*rrrllfr oldrlot| 5163+q.r'ill *t&tti?E*,F!ailit*1s8$ Al:s106€3

r (8ts&)321ss5s I {d&i!)020n113 wd 3!.,@nl (36-20)&15S56 r (86.10)@6113 s [email protected]

Sample cutinq / pr€pardion

Sampl€ Measurem6nt

Solvent ertrection

Conc€nfetbn/Dilution

Mehbe.ollh6SGS Group (SGS SA)

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Test R€port No. CANEC1102810201 Dal' tr:27 Jul2011 Page I of 11

ATTACI{MENTS

PFOA t PFOS Testirg FloY Ctrart

1) Name 0tthe person rho made tesing: Cindy Huang2) Name 0l the person In chage dE3ting: Rysn yang

y&ri.dro r' c.mn coidrio.! or5. sror i.rt* b e d!!!Jri'!ry 4!:qedl!!4!l!4*4I!q1i6;;;;';i;;;i;;.&f"i.;i 'hdbT.*-d.*a[h*t,Ebdricoai.drl!y!,:!c!9d&4s}@-..-.!4.4(;!]:}:!!.l1|91]..'93::-1:]jT!lg1

fi:ffiid"r*,*u:ilijrlr"*Cr.:,,*'r*';:5sti'*f ;ffi:;fii-"Tmet"?ji$1*lmi,-ji.rll"'i*$i.!]J-fllt-j;,!Jf;;;;i|1iiN'|ii;;;'gi.6.i;d'd.lmieldrunmlir:[6run.i.mdi[6Dd!ct

lolcdb&rdrPdda[idlddNlli.nrs0.dsBrDidc]r$nrotu 610663 t (lC?0)&156656 I 186-4)82075113 {w.6.3gs eh

sE .r_ill '&trAA*&E*+n&4*1$q br* slo€63 I {36-&)82155555 I (36-20)32075113 ! s$ cl'iit€ss3 M

Sample cuting / pr@erdion

Samole Measu16ment

Sotvent extractim

Concentra(ErVDilution

M6mb€rolthe SGS Grouo (SGSSA)

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scsTest Report No. CANEC1102810201 Dai€t 27 Jut 2011

ATTACI{MENTS

TBBP-ATe*gFlovCH

Name of the pe.sm rho made testing: Cuby yuName ofthe persm ln chage oftestlng: Ryan Yang

Page 9 of 11

1 )

Sample cutting / prepsretion

Sempl6 Measurement

SolvBnt extractim

Liquid-liquid extrectim

ConcBnkatiorvDilution

GC+,IS & HPLCMS

fl(adblctdtntuCledtnrkntry0dqErDddoldlroh 510663 t (8t20)02'5666 ' p6-20)32075113 rw'cr'ssr'tr

1E a'l :9ftlt4tEfl*raflli*1s3s t|: tloo& I {r5_2qe4nt565 I €t20)32075113 ' !Fdr'''o'$ m

M6mb€rollhe scs Grou! (scs3A)

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T€st Report

ATTACHHENTS

l) Name of the person2) Name of the person

lv lo 1r'..rmor.G) b(d

PAHS Testtg Flqv CfErt

who made testing: cuEy Yuin chage dtesting: R/an Yang

rs(dlEsrdlPdcrFsEcreeEi&h&rr0ll4sdc&gir 510663 I (06;r)e156665 I le20)82q75111 w d qe @n+l .J_tl .g!lfi,if,tE**tll4*&1s39 6l:510€€3 I {36_20)821s5t55 | {3to&0t5113 0 !!!'riF@FM

No. CANEC1102810201 DaEi27 Jul2011 Page 10 of 11

Sample cuting / prepar*ion

Samgl€ Mee6ur€ment

Solv€nt extractim

Concentratirry'Dilution

Filtration

GC-MS

DATA

YUbi*r ro irs G(fl caddo^r'rS'bh !d,ro d.dfrrc 'omd &;6 'i

'Dtr 01cq"*' d *rt$ 0. dr!rFs:4!:qe4!4!r!!lgd{br

.6;iifiidh'irdild6i rtr

i:;j;;i ;ii;d;-';;".6;d;.;d.-ii,;d;;h:;td"io'i,.''o{!ry oihhndron or rh! 6icni.

lY lo ('..rmor.G) b(d

Menbs. olth!sGS OrcurlsGS SA)

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Test R€pod

Sample photo:

No. CANEC1 10281020'1 Date: 27 Jul2011 Page 1'1 of 11

cAN11-028102.001

SGS authenticate the photo on odginal report only'*' End of Report '*

tbsr..npr.(.)r.dd

d q '@ub{.' tfe _hm &' dry!q4!-l!!-++s1

h-dN;a*r;- .d r'i&d"" rt; d*d hd. ary idd' d F ! .ocr4.1 L d$d t i, ;6nd on @;'#;r$,{*i>{;hi",Lr'* d crvt'r rd"'h.. riry tucon;ZlF;:';;;iitN;;;;; ;;;;;;i.;;d;, i; -;;;;d*...n riL ddar. dmori. '.D-!-.

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r (36-20)32r5a555 i f64)l?075113 *w,cr,sgs,@mI (3d20)@15$$ I €n-20)82075113 0 !s3diE€!s3.m

MBmbor of rhe SGS Glo'ro ISGS SA)

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Test Report Number : TWNC00216857

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse Inc. Date : Jul 25, 2011 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Aluminum Material Date Sample Received : Jul 19, 2011 Date Test Started : Jul 19, 2011

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

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Number : TWNC00216857

Test Conducted

Page 2 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Silvery Metal

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 19, 2011 Test Period : Jul 19, 2011 To Jul 25, 2011

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

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Number : TWNC00216857

Test Conducted

Page 3 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method:

Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

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Number : TWNC00216857

Test Conducted

Page 4 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Remarks: *1: List Of Appropriate Acid:

Material Acid Added For Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sampling/grinding or cutting

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved

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Number : TWNC00216857

Test Conducted

Page 5 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

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Test Report Number : TWNC00216856

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse Inc. Date : Jul 25, 2011 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Copper Alloy Date Sample Received : Jul 19, 2011 Date Test Started : Jul 20, 2011

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

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Number : TWNC00216856

Test Conducted

Page 2 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Coppery Metal

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 46 Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative(< 0.02)(#)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample

surface of 10 cm2 was used and the dilution factor was adjusted accordingly.

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 19, 2011 Test Period : Jul 20, 2011 To Jul 25, 2011

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

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Number : TWNC00216856

Test Conducted

Page 3 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method:

Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 32: New ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse... · 2013. 9. 28. · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product

Number : TWNC00216856

Test Conducted

Page 4 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Remarks: *1: List Of Appropriate Acid:

Material Acid Added For Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sampling/grinding or cutting

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved

Page 33: New ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse... · 2013. 9. 28. · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product

Number : TWNC00216856

Test Conducted

Page 5 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

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Test Report Number : TWNC00216854

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse Inc. Date : Jul 27, 2011 LIMA Technology Center, Lipa City,

Malvar, Batangas.

Sample Description: One (1) group of submitted samples said to be : Part Description : Steel Date Sample Received : Jul 19, 2011 Date Test Started : Jul 19, 2011

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

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Number : TWNC00216854

Test Conducted

Page 2 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item (1) (2)

Heavy Metal

Cadmium (Cd) content ND ND Lead (Pb) content ND ND Mercury (Hg) content ND ND

Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)

Negative (< 0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample

surface of 10 cm2 was used and the dilution factor was adjusted accordingly.

Tested Components (1) Black Plating Layer (2) Silvery Metal Base Material

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jul 19, 2011 Test Period : Jul 19, 2011 To Jul 27, 2011

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 40: New ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse... · 2013. 9. 28. · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product

Number : TWNC00216854

Test Conducted

Page 3 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method:

Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 41: New ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse... · 2013. 9. 28. · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product

Number : TWNC00216854

Test Conducted

Page 4 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

Page 42: New ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse... · 2013. 9. 28. · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product

Number : TWNC00216854

Test Conducted

Page 5 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

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