J56861-1 Std Tal L2 Final Report - MDEQ€¦ · The test results in this report meet NELAP requirements for parameters for which accreditation is required or ... Method(s) 3546: Many

ANALYTICAL REPORT

Job Number: 680-56861-1

Job Description: Hattiesburg Sludge Total APR 2010

For:Ashland Inc.

500 Hercules RoadWilmington, DE 19894

Attention: Nancy Berrios

_____________________________________________

Approved for release.Lidya GuliziaProject Manager I5/11/2010 4:12 PM

Lidya GuliziaProject Manager I

[email protected]/11/2010

cc: Craig Derouen

The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This reportmay not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to theperson who signed this report.

Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; AZ: AZ0741; CA: 03217CA;CO; CT: PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KYUST; LA DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV:GA00006; NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244;SC: 98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WVDHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q

TestAmerica Laboratories, Inc.

TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404

Tel (912) 354-7858 Fax (912) 352-0165 www.testamericainc.com

Page 1 of 238

mailto:[email protected]

http://www.testamericainc.com

Job Narrative

680-56861-1

Receipt

Pre-preserved vials for volatiles analysis were not submitted for sample IBS-5-NS (680-56861-7). The volatiles analysis was perfomed on

a subsample taken from the bulk sample container.

All other samples were received in good condition within temperature requirements.

GC/MS VOA

Method(s) 8260B: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that

one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for four analytes to recover outside criteria for

this method when a full list spike is utilized. The LCS/LCSD associated with batch 166185 had one analyte outside control limits;

therefore, re-analysis was not performed. These results have been reported and qualified.

Method(s) 8260B: The continuing calibration verification (CCV) for pentachloroethane recovered above the upper control limit. The

samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.

Method(s) 8260B: The trip blank associated with these samples contained a detection above the method detection limit (MDL) for the

following analyte: acetone.

Method(s) 8260B: The field blank associated with these samples contained a detection above the reporting limit (RL) for toluene and a

detection above the method detection limit (MDL) for 2-butanone, acetone, ethylbenzene, and xylenes. The field blank was re-analyzed

with concurring results; the first set of data has been reported.

Method(s) 8260B: The rinse blank associated with these samples contained a detection above the reporting limit (RL) for toluene and a

detection above the method detection limit (MDL) for 2-butanone and acetone. The rinse blank was re-analyzed with concurring results;

the first set of data has been reported.

Method(s) 8260B: Due to the level of dilution required for the following sample(s), surrogate recoveries are not reported: IBS-1-LS

(680-56861-1), IBS-3-NS (680-56861-2), IBS-3-US (680-56861-6), IBS-4-NS (680-56861-4), IBS-6-NS (680-56861-10), IBS-6-US

(680-56861-13), IBS-7-LS (680-56861-15), IBS-7-US (680-56861-16), IBS-4-US (680-56861-9), IBS-1-US (680-56861-20), IBS-2-LS

(680-56861-22), IBS-2-NS (680-56861-21), IBS-2-US (680-56861-23), IBS-5-LS (680-56861-8), IBS-5-US (680-56861-12), IBS-7-NS

(680-56861-14), IBS-8-US (680-56861-19), IBS-3-LS (680-56861-3), IBS-4-LS (680-56861-5), IBS-6-LS (680-56861-11), IBS-8-LS

(680-56861-18).

Method(s) 8260B: Surrogate recovery for the following sample(s) was outside control limits: IBS-5-NS (680-56861-7). Re-extraction

and/or re-analysis was performed with concurring results. The original analysis has been reported.

No other analytical or quality issues were noted.

GC/MS Semi VOA

Method(s) 3546: Many of the project samples would not concentrate to the desired final volume of 1.0 ml. Samples were concentrated to

various final volumes from 5.0 ml to 20 mls and 1.0 ml was delivered to the analysis group for analysis.

Method(s) 8270C: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that

one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for 4 analytes to recover outside criteria for this

method when a full list spike is utilized. The LCSD associated with batch 166243 had 3 analytes outside control limits; therefore,

re-extraction/re-analysis was not performed. These results have been reported and qualified.

Method(s) 8270C: The laboratory control sample (LCS) for batch 166243 exceeded control limits for the following analyte(s):

1,4-Napthoquinone, 1-Napthylamine, alpha,alpha-dimethylphenethylamine, famphur, methyl methansulfonate,

o,o,-triethyphosphorothioate has been identified as a poor performing analyte when analyzed using this method; therefore,


Method(s) 8270C: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that

one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for 4 analytes to recover outside criteria for this

method when a full list spike is utilized. The LCS associated with batch 166243 had 3 analytes outside control limits; therefore,


Method(s) 8270C: The laboratory control sample (LCS) for batch 166243 exceeded control limits for the following analyte(s):

1-napthylamine, alpha,alpha, dimethylphenthylamine, methapyri;ene, methyl methansulfonate, o,o,o-triethylosphorothioate has been

identified as a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed. These

results have been reported and qualified.

Method(s) 8270C: The following samples were diluted due to the nature of the sample matrix: IBS-1-LS (680-56861-1), IBS-3-LS

(680-56861-3), IBS-3-NS (680-56861-2), IBS-3-US (680-56861-6), IBS-4-LS (680-56861-5), IBS-4-US (680-56861-9), IBS-5-NS

Page 2 of 238

(680-56861-7), IBS-2-US (680-56861-23), IBS-1-US (680-56861-20), IBS-4-NS (680-56861-4), IBS-5-US (680-56861-12), IBS-6-LS

(680-56861-11), IBS-6-NS (680-56861-10), IBS-6-US (680-56861-13), IBS-7-LS (680-56861-15), IBS-7-NS (680-56861-14), IBS-7-US

(680-56861-16), IBS-8-LS (680-56861-18), IBS-8-NS (680-56861-17), IBS-8-US (680-56861-19), IBS-2-LS (680-56861-22, IBS-2-NS

(680-56861-21) and the associated MS/MSD samples (680-56861-21 MS and 680-56861-21 MSD). As such, surrogate recoveries are

not reported, and elevated reporting limits (RLs) are provided.

Method(s) 8270C: Sample IBS-4-NS (680-56861-4) was diluted due to the abundance of target analytes. As such, surrogate recoveries

are not reported, and elevated reporting limits (RLs) are provided.

Method(s) 8270C: The laboratory control sample (LCS) for batch 166147 exceeded control limits for the following analytes that have been

identified as poor performer. The following analytes have been identified, in the reference method and/or via historical data, to be poor

and/or erratic performers: Famphur, 1,4-Napthaquinone, Methane sulfonate, Benzaldehyde, 1-naphthylamine, 2-naphthylamine,

p-Dimethylamino azobenzene, p-phenylenediamine, a,a-dimethylphenethylamine, Methapyriline, 2-picoline (2-methylpyridine),

3,3’-dimethylbenzidine, 3,3’-dichlorobenzidine, Benzidine, Benzaldehyde, Benzoic acid, Dinoseb, Hexachlorophene,

Hexachlorocyclopentadiene, o,o,o-triethylphosphoro-thioate.

Method(s) 8270C: Matrix spikes for batch 166138 could not be recovered due to sample matrix interferences which required sample

dilution. The associated laboratory control sample (LCS) met acceptance criteria.

Method(s) 8270C: The laboratory control sample (LCS) for batch 166138 exceeded control limits for one or more of analytes identified as

poor performers. The following analytes have been identified, in the reference method and/or via historical data, to be poor and/or erratic

performers: Famphur, 1,4-Napthaquinone, Methane sulfonate, Benzaldehyde, 1-naphthylamine, 2-naphthylamine, p-Dimethylamino

azobenzene, p-phenylenediamine, a,a-dimethylphenethylamine, Methapyriline, 2-picoline (2-methylpyridine), 3,3’-dimethylbenzidine,

3,3’-dichlorobenzidine, Benzidine, Benzaldehyde, Benzoic acid, Dinoseb, Hexachlorophene, Hexachlorocyclopentadiene,

o,o,o-triethylphosphoro-thioate. Re-extraction was not performed.


Metals

No analytical or quality issues were noted.

General Chemistry

No analytical or quality issues were noted.

VOA Prep

Method(s) 5035: The pre-preserved volatile sample vials submitted for the following sample(s) contained significantly less than 5 grams:

IBS-1-LS (680-56861-1), IBS-4-LS (680-56861-5), IBS-8-US (680-56861-19). Reporting limits in these samples have been elevated

based on the analysis weight.


Comments

No additional comments.

Page 3 of 238

METHOD SUMMARY

Job Number: 680-56861-1Client: Ashland Inc.

Preparation MethodMethodLab LocationDescription

Matrix: Solid

SW846 8260BVolatile Organic Compounds (GC/MS) TAL SAV

SW846 5030ATAL SAVPurge and Trap

SW846 5035TAL SAVClosed System Purge and Trap

SW846 8270CSemivolatile Compounds by Gas Chromatography/Mass

Spectrometry (GC/MS)

TAL SAV

SW846 3546TAL SAVMicrowave Extraction

SW846 6010BMetals (ICP) TAL SAV

SW846 3050BTAL SAVPreparation, Metals

SW846 7471AMercury (CVAA) TAL SAV

SW846 7471ATAL SAVPreparation, Mercury

Matrix: Water

SW846 8260BVolatile Organic Compounds (GC/MS) TAL SAV

SW846 5030BTAL SAVPurge and Trap

SW846 8270CSemivolatile Compounds by Gas Chromatography/Mass

Spectrometry (GC/MS)

TAL SAV

SW846 3520CTAL SAVLiquid-Liquid Extraction (Continuous)

SW846 6010BMetals (ICP) TAL SAV

SW846 3010ATAL SAVPreparation, Total Metals

SW846 7470AMercury (CVAA) TAL SAV

SW846 7470ATAL SAVPreparation, Mercury

Lab References:

TAL SAV = TestAmerica Savannah

Method References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Savannah

Page 4 of 238

METHOD / ANALYST SUMMARY

Client: Ashland Inc. Job Number: 680-56861-1

Method Analyst Analyst ID

Lanier, Carolyn CLSW846 8260B

Sokolin, Eleina ESSW846 8260B

Haynes, Carion CRHSW846 8270C

Bland, Brian BCBSW846 6010B

Eaton, Cliff CESW846 7470A

Eaton, Cliff CESW846 7471A


Page 5 of 238

SAMPLE SUMMARY


Client Sample IDLab Sample ID Client Matrix

Date/Time

Sampled

Date/Time

Received

04/14/2010 0950 04/17/2010 1045IBS-1-LS680-56861-1 Solid

04/14/2010 1245 04/17/2010 1045IBS-3-NS680-56861-2 Solid

04/14/2010 1255 04/17/2010 1045IBS-3-LS680-56861-3 Solid

04/14/2010 1715 04/17/2010 1045IBS-4-NS680-56861-4 Solid

04/14/2010 1735 04/17/2010 1045IBS-4-LS680-56861-5 Solid

04/15/2010 0845 04/17/2010 1045IBS-3-US680-56861-6 Solid

04/15/2010 0950 04/17/2010 1045IBS-5-NS680-56861-7 Solid

04/15/2010 1005 04/17/2010 1045IBS-5-LS680-56861-8 Solid

04/15/2010 1100 04/17/2010 1045IBS-4-US680-56861-9 Solid

04/15/2010 1105 04/17/2010 1045IBS-6-NS680-56861-10 Solid

04/15/2010 1110 04/17/2010 1045IBS-6-LS680-56861-11 Solid

04/15/2010 1145 04/17/2010 1045IBS-5-US680-56861-12 Solid

04/15/2010 1415 04/17/2010 1045IBS-6-US680-56861-13 Solid

04/15/2010 1505 04/17/2010 1045IBS-7-NS680-56861-14 Solid

04/15/2010 1520 04/17/2010 1045IBS-7-LS680-56861-15 Solid

04/15/2010 1525 04/17/2010 1045IBS-7-US680-56861-16 Solid

04/15/2010 1600 04/17/2010 1045IBS-8-NS680-56861-17 Solid

04/15/2010 1615 04/17/2010 1045IBS-8-LS680-56861-18 Solid

04/15/2010 1620 04/17/2010 1045IBS-8-US680-56861-19 Solid

04/15/2010 1700 04/17/2010 1045IBS-1-US680-56861-20 Solid

04/16/2010 0840 04/17/2010 1045IBS-2-NS680-56861-21 Solid

04/16/2010 0850 04/17/2010 1045IBS-2-LS680-56861-22 Solid

04/16/2010 0930 04/17/2010 1045IBS-2-US680-56861-23 Solid

04/15/2010 1735 04/17/2010 1045FB-1680-56861-24FB Water

04/16/2010 0945 04/17/2010 1045FB-2680-56861-25FB Water

04/14/2010 0000 04/17/2010 1045TB-1680-56861-26TB Water

04/15/2010 0000 04/17/2010 1045TB-2680-56861-27TB Water

04/16/2010 1000 04/17/2010 1045RB-1680-56861-28RB Water


Page 6 of 238

SAMPLE RESULTS


Page 7 of 238

Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix: % Moisture: 53.4

680-56861-1

Solid

Date Sampled: 04/14/2010 0950

Date Received: 04/17/2010 1045

8260B Volatile Organic Compounds (GC/MS)

Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 1854

1000000

8260B Analysis Batch: 680-166686

Prep Batch: 680-166108

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

m0466.d

2.8 g

5 g

5035

MSM

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

190000000 U 19000000042000000Acetone

770000000 U 770000000160000000Acetonitrile

380000000 U 38000000092000000Acrolein

380000000 U 380000000130000000Acrylonitrile

19000000 U 190000002800000Benzene

19000000 U 190000005700000Bromoform

19000000 U 190000005700000Bromomethane

96000000 U 9600000092000002-Butanone (MEK)

19000000 U 190000004200000Carbon disulfide

19000000 U 190000003200000Carbon tetrachloride

19000000 U 190000003700000Chlorobenzene

19000000 U 1900000080000002-Chloro-1,3-butadiene

19000000 U 190000006500000Chlorodibromomethane

19000000 U 1900000010000000Chloroethane

19000000 U 190000004200000Chloroform

19000000 U 190000003800000Chloromethane

19000000 U 1900000084000003-Chloro-1-propene

19000000 U 190000003200000cis-1,3-Dichloropropene

38000000 U 38000000170000001,2-Dibromo-3-Chloropropane

19000000 U 190000006500000Dibromomethane

19000000 U 190000003700000Dichlorobromomethane

19000000 U 190000003600000Dichlorodifluoromethane

19000000 U 1900000042000001,1-Dichloroethane


19000000 U 1900000057000001,1-Dichloroethene

19000000 U 1900000033000001,2-Dichloropropane

19000000 U 190000005000000Ethylbenzene

19000000 U 190000005700000Ethylene Dibromide

19000000 U 1900000013000000Ethyl methacrylate

96000000 U 96000000130000002-Hexanone

19000000 U 190000006900000Iodomethane

770000000 U 770000000200000000Isobutyl alcohol

380000000 U 38000000088000000Methacrylonitrile

19000000 U 190000003800000Methylene Chloride

38000000 U 3800000017000000Methyl methacrylate

96000000 U 96000000160000004-Methyl-2-pentanone (MIBK)

96000000 U 9600000024000000Pentachloroethane

380000000 U 380000000100000000Propionitrile

19000000 U 190000003600000Styrene

19000000 U 1900000092000001,1,1,2-Tetrachloroethane


19000000 U 190000007300000Tetrachloroethene

160000000 190000003200000Toluene

38000000 U 3800000011000000trans-1,4-Dichloro-2-butene

19000000 U 190000002400000trans-1,2-Dichloroethene

19000000 U 190000003300000trans-1,3-Dichloropropene

TestAmerica Savannah Page 8 of 238

Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS


680-56861-1

Solid

Date Sampled: 04/14/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 1854

1000000





Lab File ID:

Instrument ID:

m0466.d

2.8 g

5 g

5035

MSM


19000000 U 1900000023000001,1,1-Trichloroethane


19000000 U 190000005000000Trichloroethene

19000000 U 190000004600000Trichlorofluoromethane

19000000 U 1900000092000001,2,3-Trichloropropane

38000000 U 380000009600000Vinyl acetate

19000000 U 190000005700000Vinyl chloride

38000000 U 380000004200000Xylenes, Total

Surrogate %Rec Acceptance LimitsQualifier

0 65 - 124D4-Bromofluorobenzene

0 65 - 124DDibromofluoromethane

0 65 - 132DToluene-d8 (Surr)


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-NS


680-56861-2

Solid

Date Sampled: 04/14/2010 1245



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 1917

1000





Lab File ID:

Instrument ID:

m0467.d

5.7 g

5 g

5035

MSM


56000 U 5600012000Acetone

220000 U 22000046000Acetonitrile

110000 U 11000027000Acrolein

110000 U 11000038000Acrylonitrile

2500 J 5600810Benzene

5600 U 56001700Bromoform

5600 U 56001700Bromomethane

28000 U 2800027002-Butanone (MEK)



5600 U 56001100Chlorobenzene



5600 U 56003000Chloroethane

5600 U 56001200Chloroform

5600 U 56001100Chloromethane

5600 U 560025003-Chloro-1-propene










5600 U 56001400Ethylbenzene



28000 U 2800037002-Hexanone

5600 U 56002000Iodomethane







110000 U 11000029000Propionitrile

5600 U 56001000Styrene




190000 5600940Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-NS


680-56861-2

Solid

Date Sampled: 04/14/2010 1245



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 1917

1000





Lab File ID:

Instrument ID:

m0467.d

5.7 g

5 g

5035

MSM







11000 U 110002800Vinyl acetate

5600 U 56001700Vinyl chloride

11000 U 110001200Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 0930

20000





Lab File ID:

Instrument ID:

m0508.d

3.5 g

5 g

5035

MSM


3100000 U 3100000670000Acetone

12000000 U 120000002500000Acetonitrile

6100000 U 61000001500000Acrolein

6100000 U 61000002100000Acrylonitrile

55000 J 31000045000Benzene

310000 U 31000092000Bromoform


180000 J 15000001500002-Butanone (MEK)






310000 U 310000170000Chloroethane

310000 U 31000067000Chloroform


310000 U 3100001300003-Chloro-1-propene













1500000 U 15000002000002-Hexanone

310000 U 310000110000Iodomethane



530000 31000060000Methylene Chloride




6100000 U 61000001600000Propionitrile

310000 U 31000057000Styrene




6800000 31000051000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 0930

20000





Lab File ID:

Instrument ID:

m0508.d

3.5 g

5 g

5035

MSM







610000 U 610000150000Vinyl acetate


610000 U 61000067000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-NS


680-56861-4

Solid

Date Sampled: 04/14/2010 1715



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2004

1000





Lab File ID:

Instrument ID:

m0469.d

5.2 g

5 g

5035

MSM


55000 U 5500012000Acetone


110000 U 11000026000Acrolein


37000 5500800Benzene



27000 U 2700026002-Butanone (MEK)






















27000 U 2700036002-Hexanone









5500 U 55001000Styrene




150000 5500920Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-NS


680-56861-4

Solid

Date Sampled: 04/14/2010 1715



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2004

1000





Lab File ID:

Instrument ID:

m0469.d

5.2 g

5 g

5035

MSM















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 0953

50000





Lab File ID:

Instrument ID:

m0509.d

3.2 g

5 g

5035

MSM


9900000 U 99000002200000Acetone

40000000 U 400000008100000Acetonitrile

20000000 U 200000004700000Acrolein

20000000 U 200000006700000Acrylonitrile

990000 U 990000140000Benzene

990000 U 990000300000Bromoform

990000 U 990000300000Bromomethane

480000 J 49000004700002-Butanone (MEK)






990000 U 990000530000Chloroethane

990000 U 990000220000Chloroform


990000 U 9900004300003-Chloro-1-propene










990000 U 990000260000Ethylbenzene



4900000 U 49000006500002-Hexanone

990000 U 990000360000Iodomethane



740000 J 990000190000Methylene Chloride




20000000 U 200000005100000Propionitrile

990000 U 990000180000Styrene




13000000 990000170000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 0953

50000





Lab File ID:

Instrument ID:

m0509.d

3.2 g

5 g

5035

MSM







2000000 U 2000000490000Vinyl acetate


2000000 U 2000000220000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US


680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2052

5000





Lab File ID:

Instrument ID:

m0471.d

3.2 g

5 g

5035

MSM


1600000 U 1600000350000Acetone

6400000 U 64000001300000Acetonitrile

3200000 U 3200000770000Acrolein

3200000 U 32000001100000Acrylonitrile

160000 U 16000023000Benzene

160000 U 16000048000Bromoform


800000 U 800000770002-Butanone (MEK)







160000 U 16000035000Chloroform


160000 U 160000710003-Chloro-1-propene













800000 U 8000001100002-Hexanone

160000 U 16000058000Iodomethane







3200000 U 3200000840000Propionitrile

160000 U 16000030000Styrene




2000000 16000027000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US


680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2052

5000





Lab File ID:

Instrument ID:

m0471.d

3.2 g

5 g

5035

MSM







320000 U 32000080000Vinyl acetate


320000 U 32000035000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-NS


680-56861-7

Solid

Date Sampled: 04/15/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/25/2010 2115

04/25/2010 2115

40




Lab File ID:

Instrument ID:

m0472.d

5.1 g

5 mL

5030A

MSM


2100 J 2600570Acetone


5100 U 51001200Acrolein


260 U 26038Benzene



1300 U 13001202-Butanone (MEK)






















1300 U 13001702-Hexanone









260 U 26048Styrene




1100 26043Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-NS


680-56861-7

Solid

Date Sampled: 04/15/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/25/2010 2115

04/25/2010 2115

40




Lab File ID:

Instrument ID:

m0472.d

5.1 g

5 mL

5030A

MSM











75 65 - 1244-Bromofluorobenzene

56 65 - 124XDibromofluoromethane

66 65 - 132Toluene-d8 (Surr)


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1754

20000





Lab File ID:

Instrument ID:

m0507.d

3.0 g

5 g

5035

MSM


5200000 U 52000001100000Acetone

21000000 U 210000004300000Acetonitrile

10000000 U 100000002500000Acrolein

10000000 U 100000003500000Acrylonitrile

520000 U 52000076000Benzene

520000 U 520000160000Bromoform

520000 U 520000160000Bromomethane

2600000 U 26000002500002-Butanone (MEK)






520000 U 520000280000Chloroethane

520000 U 520000110000Chloroform


520000 U 5200002300003-Chloro-1-propene










520000 U 520000140000Ethylbenzene



2600000 U 26000003400002-Hexanone

520000 U 520000190000Iodomethane







10000000 U 100000002700000Propionitrile

520000 U 52000097000Styrene




9800000 52000087000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1754

20000





Lab File ID:

Instrument ID:

m0507.d

3.0 g

5 g

5035

MSM







1000000 U 1000000260000Vinyl acetate


1000000 U 1000000110000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US


680-56861-9

Solid

Date Sampled: 04/15/2010 1100



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/23/2010 1641

1000





Lab File ID:

Instrument ID:

m0396.d

3.6 g

5 g

5035

MSM


310000 U 31000069000Acetone

1200000 U 1200000260000Acetonitrile

620000 U 620000150000Acrolein


31000 U 310004600Benzene

31000 U 310009400Bromoform


160000 U 160000150002-Butanone (MEK)









31000 U 31000140003-Chloro-1-propene













160000 U 160000210002-Hexanone









31000 U 310005800Styrene




1100000 310005200Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US


680-56861-9

Solid

Date Sampled: 04/15/2010 1100



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/23/2010 1641

1000





Lab File ID:

Instrument ID:

m0396.d

3.6 g

5 g

5035

MSM















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-NS


680-56861-10

Solid

Date Sampled: 04/15/2010 1105



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2202

400





Lab File ID:

Instrument ID:

m0474.d

5.2 g

5 g

5035

MSM


24000 U 240005300Acetone


48000 U 4800012000Acrolein


2400 U 2400350Benzene



12000 U 1200012002-Butanone (MEK)






















12000 U 1200016002-Hexanone









2400 U 2400450Styrene




33000 2400410Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-NS


680-56861-10

Solid

Date Sampled: 04/15/2010 1105



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2202

400





Lab File ID:

Instrument ID:

m0474.d

5.2 g

5 g

5035

MSM















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS


680-56861-11

Solid

Date Sampled: 04/15/2010 1110



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 1017

20000





Lab File ID:

Instrument ID:

m0510.d

3.3 g

5 g

5035

MSM


3700000 U 3700000820000Acetone

15000000 U 150000003100000Acetonitrile

7500000 U 75000001800000Acrolein

7500000 U 75000002500000Acrylonitrile

370000 U 37000054000Benzene

370000 U 370000110000Bromoform

370000 U 370000110000Bromomethane

1900000 U 19000001800002-Butanone (MEK)






370000 U 370000200000Chloroethane

370000 U 37000082000Chloroform


370000 U 3700001600003-Chloro-1-propene













1900000 U 19000002500002-Hexanone

370000 U 370000130000Iodomethane







7500000 U 75000001900000Propionitrile

370000 U 37000069000Styrene




14000000 37000063000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS


680-56861-11

Solid

Date Sampled: 04/15/2010 1110



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 1017

20000





Lab File ID:

Instrument ID:

m0510.d

3.3 g

5 g

5035

MSM







750000 U 750000190000Vinyl acetate


750000 U 75000082000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US


680-56861-12

Solid

Date Sampled: 04/15/2010 1145



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1312

2000





Lab File ID:

Instrument ID:

m0495.d

3.2 g

5 g

5035

MSM


910000 U 910000200000Acetone

3600000 U 3600000740000Acetonitrile

1800000 U 1800000430000Acrolein

1800000 U 1800000620000Acrylonitrile

91000 U 9100013000Benzene

91000 U 9100027000Bromoform


450000 U 450000430002-Butanone (MEK)







91000 U 9100020000Chloroform


91000 U 91000400003-Chloro-1-propene













450000 U 450000600002-Hexanone








1800000 U 1800000470000Propionitrile

91000 U 9100017000Styrene




980000 9100015000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US


680-56861-12

Solid

Date Sampled: 04/15/2010 1145



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1312

2000





Lab File ID:

Instrument ID:

m0495.d

3.2 g

5 g

5035

MSM







180000 U 18000045000Vinyl acetate


180000 U 18000020000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US


680-56861-13

Solid

Date Sampled: 04/15/2010 1415



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2313

2000





Lab File ID:

Instrument ID:

m0477.d

3.5 g

5 g

5035

MSM


830000 U 830000180000Acetone

3300000 U 3300000680000Acetonitrile

1700000 U 1700000400000Acrolein

1700000 U 1700000560000Acrylonitrile

83000 U 8300012000Benzene

83000 U 8300025000Bromoform


410000 U 410000400002-Butanone (MEK)







83000 U 8300018000Chloroform


83000 U 83000360003-Chloro-1-propene













410000 U 410000550002-Hexanone








1700000 U 1700000430000Propionitrile

83000 U 8300015000Styrene




1800000 8300014000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US


680-56861-13

Solid

Date Sampled: 04/15/2010 1415



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/25/2010 2313

2000





Lab File ID:

Instrument ID:

m0477.d

3.5 g

5 g

5035

MSM







170000 U 17000041000Vinyl acetate


170000 U 17000018000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-NS


680-56861-14

Solid

Date Sampled: 04/15/2010 1505



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1359

2000





Lab File ID:

Instrument ID:

m0497.d

6.2 g

5 g

5035

MSM


97000 U 9700021000Acetone


190000 U 19000047000Acrolein


110000 97001400Benzene



49000 U 4900047002-Butanone (MEK)






















49000 U 4900064002-Hexanone









9700 U 97001800Styrene




70000 97001600Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-NS


680-56861-14

Solid

Date Sampled: 04/15/2010 1505



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1359

2000





Lab File ID:

Instrument ID:

m0497.d

6.2 g

5 g

5035

MSM















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS


680-56861-15

Solid

Date Sampled: 04/15/2010 1520



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 0000

20000





Lab File ID:

Instrument ID:

m0479.d

3.4 g

5 g

5035

MSM


5000000 U 50000001100000Acetone

20000000 U 200000004100000Acetonitrile

10000000 U 100000002400000Acrolein

10000000 U 100000003400000Acrylonitrile

500000 U 50000073000Benzene

500000 U 500000150000Bromoform

500000 U 500000150000Bromomethane

2500000 U 25000002400002-Butanone (MEK)






500000 U 500000270000Chloroethane

500000 U 500000110000Chloroform


500000 U 5000002200003-Chloro-1-propene










500000 U 500000130000Ethylbenzene



2500000 U 25000003300002-Hexanone

500000 U 500000180000Iodomethane







10000000 U 100000002600000Propionitrile

500000 U 50000093000Styrene




5900000 50000084000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS


680-56861-15

Solid

Date Sampled: 04/15/2010 1520



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 0000

20000





Lab File ID:

Instrument ID:

m0479.d

3.4 g

5 g

5035

MSM







1000000 U 1000000250000Vinyl acetate


1000000 U 1000000110000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US


680-56861-16

Solid

Date Sampled: 04/15/2010 1525



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 0024

10000





Lab File ID:

Instrument ID:

m0480.d

3.3 g

5 g

5035

MSM


2900000 U 2900000630000Acetone

12000000 U 120000002400000Acetonitrile

5800000 U 58000001400000Acrolein

5800000 U 58000002000000Acrylonitrile

290000 U 29000042000Benzene

290000 U 29000086000Bromoform


1400000 U 14000001400002-Butanone (MEK)






290000 U 290000160000Chloroethane

290000 U 29000063000Chloroform


290000 U 2900001300003-Chloro-1-propene













1400000 U 14000001900002-Hexanone

290000 U 290000100000Iodomethane







5800000 U 58000001500000Propionitrile

290000 U 29000054000Styrene




2800000 29000048000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US


680-56861-16

Solid

Date Sampled: 04/15/2010 1525



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 0024

10000





Lab File ID:

Instrument ID:

m0480.d

3.3 g

5 g

5035

MSM







580000 U 580000140000Vinyl acetate


580000 U 58000063000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-NS


680-56861-17

Solid

Date Sampled: 04/15/2010 1600



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 1040

200





Lab File ID:

Instrument ID:

m0511.d

5.2 g

5 g

5035

MSM


13000 U 130002900Acetone


27000 U 270006400Acrolein


390 J 1300190Benzene



840 J 66006402-Butanone (MEK)






















6600 U 66008802-Hexanone









1300 U 1300250Styrene




17000 1300220Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-NS


680-56861-17

Solid

Date Sampled: 04/15/2010 1600



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 1040

200





Lab File ID:

Instrument ID:

m0511.d

5.2 g

5 g

5035

MSM












77 65 - 124Dibromofluoromethane



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS


680-56861-18

Solid

Date Sampled: 04/15/2010 1615



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 1104

20000





Lab File ID:

Instrument ID:

m0512.d

3.1 g

5 g

5035

MSM


6600000 U 66000001400000Acetone

26000000 U 260000005400000Acetonitrile

13000000 U 130000003100000Acrolein

13000000 U 130000004500000Acrylonitrile

660000 U 66000096000Benzene

660000 U 660000200000Bromoform

660000 U 660000200000Bromomethane

3300000 U 33000003100002-Butanone (MEK)






660000 U 660000350000Chloroethane

660000 U 660000140000Chloroform


660000 U 6600002900003-Chloro-1-propene










660000 U 660000170000Ethylbenzene



3300000 U 33000004300002-Hexanone

660000 U 660000240000Iodomethane



610000 J 660000130000Methylene Chloride




13000000 U 130000003400000Propionitrile

660000 U 660000120000Styrene




14000000 660000110000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS


680-56861-18

Solid

Date Sampled: 04/15/2010 1615



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/27/2010 1104

20000





Lab File ID:

Instrument ID:

m0512.d

3.1 g

5 g

5035

MSM







1300000 U 1300000330000Vinyl acetate


1300000 U 1300000140000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US


680-56861-19

Solid

Date Sampled: 04/15/2010 1620



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1509

1000





Lab File ID:

Instrument ID:

m0500.d

3.2 g

5 g

5035

MSM


570000 U 570000130000Acetone

2300000 U 2300000470000Acetonitrile

1100000 U 1100000270000Acrolein

1100000 U 1100000390000Acrylonitrile

57000 U 570008300Benzene

57000 U 5700017000Bromoform


290000 U 290000270002-Butanone (MEK)







57000 U 5700013000Chloroform


57000 U 57000250003-Chloro-1-propene













290000 U 290000380002-Hexanone








1100000 U 1100000300000Propionitrile

57000 U 5700011000Styrene




810000 570009600Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US


680-56861-19

Solid

Date Sampled: 04/15/2010 1620



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1509

1000





Lab File ID:

Instrument ID:

m0500.d

3.2 g

5 g

5035

MSM







110000 U 11000029000Vinyl acetate


110000 U 11000013000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US


680-56861-20

Solid

Date Sampled: 04/15/2010 1700



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1533

2000





Lab File ID:

Instrument ID:

m0501.d

3.4 g

5 g

5035

MSM


390000 U 39000087000Acetone

1600000 U 1600000320000Acetonitrile

790000 U 790000190000Acrolein


55000 390005700Benzene

39000 U 3900012000Bromoform


200000 U 200000190002-Butanone (MEK)









39000 U 39000170003-Chloro-1-propene













200000 U 200000260002-Hexanone









39000 U 390007300Styrene




820000 390006600Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US


680-56861-20

Solid

Date Sampled: 04/15/2010 1700



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1533

2000





Lab File ID:

Instrument ID:

m0501.d

3.4 g

5 g

5035

MSM















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-NS


680-56861-21

Solid

Date Sampled: 04/16/2010 0840



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1556

2000





Lab File ID:

Instrument ID:

m0502.d

6.3 g

5 g

5035

MSM


93000 U 9300020000Acetone


190000 U 19000045000Acrolein


17000 93001400Benzene



46000 U 4600045002-Butanone (MEK)


14000 93001500Carbon tetrachloride





2100 J 93002000Chloroform















46000 U 4600061002-Hexanone









9300 U 93001700Styrene




290000 93001600Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-NS


680-56861-21

Solid

Date Sampled: 04/16/2010 0840



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1556

2000





Lab File ID:

Instrument ID:

m0502.d

6.3 g

5 g

5035

MSM















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS


680-56861-22

Solid

Date Sampled: 04/16/2010 0850



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1620

50000





Lab File ID:

Instrument ID:

m0503.d

3.3 g

5 g

5035

MSM


11000000 U 110000002500000Acetone

46000000 U 460000009300000Acetonitrile

23000000 U 230000005500000Acrolein

23000000 U 230000007800000Acrylonitrile

1100000 U 1100000170000Benzene

1100000 U 1100000340000Bromoform

1100000 U 1100000340000Bromomethane

5700000 U 57000005500002-Butanone (MEK)



1100000 U 1100000220000Chlorobenzene



1100000 U 1100000620000Chloroethane

1100000 U 1100000250000Chloroform

1100000 U 1100000230000Chloromethane

1100000 U 11000005000003-Chloro-1-propene










1100000 U 1100000300000Ethylbenzene



5700000 U 57000007500002-Hexanone

1100000 U 1100000410000Iodomethane







23000000 U 230000005900000Propionitrile

1100000 U 1100000210000Styrene




9400000 1100000190000Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS


680-56861-22

Solid

Date Sampled: 04/16/2010 0850



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1620

50000





Lab File ID:

Instrument ID:

m0503.d

3.3 g

5 g

5035

MSM







2300000 U 2300000570000Vinyl acetate

1100000 U 1100000340000Vinyl chloride

2300000 U 2300000250000Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US


680-56861-23

Solid

Date Sampled: 04/16/2010 0930



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1643

1000





Lab File ID:

Instrument ID:

m0504.d

3.2 g

5 g

5035

MSM


370000 U 37000081000Acetone

1500000 U 1500000300000Acetonitrile

730000 U 730000180000Acrolein


12000 J 370005400Benzene

37000 U 3700011000Bromoform


180000 U 180000180002-Butanone (MEK)









37000 U 37000160003-Chloro-1-propene













180000 U 180000240002-Hexanone









37000 U 370006800Styrene




640000 370006200Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US


680-56861-23

Solid

Date Sampled: 04/16/2010 0930



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/19/2010 1610

04/26/2010 1643

1000





Lab File ID:

Instrument ID:

m0504.d

3.2 g

5 g

5035

MSM















Analytical Data


Client Sample ID:

Lab Sample ID:

FB-1

Client Matrix:

680-56861-24FB

Water

Date Sampled: 04/15/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1451

04/20/2010 1451

1.0




Lab File ID:

Instrument ID:

p0101.d

5 mL

5 mL

5030B

MSP

Analyte Result (ug/L) Qualifier MDL RL

8.4 J 255.0Acetone


20 U 207.4Acrolein

20 U 207.2Acrylonitrile

1.0 U 1.00.25Benzene

1.0 U 1.00.50Bromoform

1.0 U 1.00.80Bromomethane

1.5 J 101.02-Butanone (MEK)

2.0 U * 2.00.60Carbon disulfide

1.0 U 1.00.50Carbon tetrachloride

1.0 U 1.00.25Chlorobenzene

1.0 U 1.00.302-Chloro-1,3-butadiene

1.0 U 1.00.10Chlorodibromomethane

1.0 U 1.01.0Chloroethane

1.0 U 1.00.14Chloroform

1.0 U 1.00.33Chloromethane

1.0 U 1.00.203-Chloro-1-propene

1.0 U 1.00.11cis-1,3-Dichloropropene

1.0 U 1.00.441,2-Dibromo-3-Chloropropane

1.0 U 1.00.20Dibromomethane

1.0 U 1.00.25Dichlorobromomethane

1.0 U 1.00.25Dichlorodifluoromethane

1.0 U 1.00.251,1-Dichloroethane


1.0 U 1.00.111,1-Dichloroethene

1.0 U 1.00.131,2-Dichloropropane

0.18 J 1.00.11Ethylbenzene

1.0 U 1.00.25Ethylene Dibromide

1.0 U 1.00.25Ethyl methacrylate

10 U 101.02-Hexanone

5.0 U 5.01.0Iodomethane


20 U 203.3Methacrylonitrile

5.0 U 5.01.0Methylene Chloride

1.0 U 1.00.48Methyl methacrylate

10 U 101.04-Methyl-2-pentanone (MIBK)

5.0 U 5.01.2Pentachloroethane

20 U 204.6Propionitrile

1.0 U 1.00.11Styrene

1.0 U 1.00.331,1,1,2-Tetrachloroethane


1.0 U 1.00.15Tetrachloroethene

2.7 1.00.33Toluene

2.0 U 2.00.50trans-1,4-Dichloro-2-butene

1.0 U 1.00.20trans-1,2-Dichloroethene

1.0 U 1.00.21trans-1,3-Dichloropropene


Analytical Data


Client Sample ID:

Lab Sample ID:

FB-1

Client Matrix:

680-56861-24FB

Water

Date Sampled: 04/15/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1451

04/20/2010 1451

1.0




Lab File ID:

Instrument ID:

p0101.d

5 mL

5 mL

5030B

MSP


1.0 U 1.00.501,1,1-Trichloroethane


1.0 U 1.00.13Trichloroethene

1.0 U 1.00.25Trichlorofluoromethane

1.0 U 1.00.411,2,3-Trichloropropane

2.0 U 2.00.28Vinyl acetate

1.0 U 1.00.18Vinyl chloride

0.39 J 2.00.20Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

FB-2

Client Matrix:

680-56861-25FB

Water

Date Sampled: 04/16/2010 0945



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1521

04/20/2010 1521

1.0




Lab File ID:

Instrument ID:

p0103.d

5 mL

5 mL

5030B

MSP


7.7 J 255.0Acetone


20 U 207.4Acrolein
























0.14 J 1.00.11Ethylbenzene
















2.5 1.00.33Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

FB-2

Client Matrix:

680-56861-25FB

Water

Date Sampled: 04/16/2010 0945



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1521

04/20/2010 1521

1.0




Lab File ID:

Instrument ID:

p0103.d

5 mL

5 mL

5030B

MSP









0.40 J 2.00.20Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1

Client Matrix:

680-56861-26TB

Water

Date Sampled: 04/14/2010 0000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1551

04/20/2010 1551

1.0




Lab File ID:

Instrument ID:

p0105.d

5 mL

5 mL

5030B

MSP


5.0 J 255.0Acetone


20 U 207.4Acrolein





10 U 101.02-Butanone (MEK)



















1.0 U 1.00.11Ethylbenzene
















1.0 U 1.00.33Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1

Client Matrix:

680-56861-26TB

Water

Date Sampled: 04/14/2010 0000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1551

04/20/2010 1551

1.0




Lab File ID:

Instrument ID:

p0105.d

5 mL

5 mL

5030B

MSP









2.0 U 2.00.20Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2

Client Matrix:

680-56861-27TB

Water

Date Sampled: 04/15/2010 0000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1621

04/20/2010 1621

1.0




Lab File ID:

Instrument ID:

p0107.d

5 mL

5 mL

5030B

MSP


25 U 255.0Acetone


20 U 207.4Acrolein













































Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2

Client Matrix:

680-56861-27TB

Water

Date Sampled: 04/15/2010 0000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1621

04/20/2010 1621

1.0




Lab File ID:

Instrument ID:

p0107.d

5 mL

5 mL

5030B

MSP















Analytical Data


Client Sample ID:

Lab Sample ID:

RB-1

Client Matrix:

680-56861-28RB

Water

Date Sampled: 04/16/2010 1000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1652

04/20/2010 1652

1.0




Lab File ID:

Instrument ID:

p0109.d

5 mL

5 mL

5030B

MSP


9.5 J 255.0Acetone


20 U 207.4Acrolein








































1.3 1.00.33Toluene





Analytical Data


Client Sample ID:

Lab Sample ID:

RB-1

Client Matrix:

680-56861-28RB

Water

Date Sampled: 04/16/2010 1000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1652

04/20/2010 1652

1.0




Lab File ID:

Instrument ID:

p0109.d

5 mL

5 mL

5030B

MSP















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS


680-56861-1

Solid

Date Sampled: 04/14/2010 0950


8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)

Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1733

10

8270C Analysis Batch: 680-167447


Injection Volume:



Lab File ID:

Instrument ID:

g1006.d

30.04 g

10 mL

1 uL

3546

MSG


71000 U 710008800Acenaphthene

71000 U 710007700Acenaphthylene

71000 U 710006000Acetophenone

71000 U 7100060002-Acetylaminofluorene

14000000 U 14000000580000alpha,alpha-Dimethyl phenethylamine

71000 U 7100079004-Aminobiphenyl

140000 U 1400007300Aniline

71000 U 710005400Anthracene

71000 U 7100012000Aramite, Total

71000 U 710005800Benzo[a]anthracene

71000 U 7100011000Benzo[a]pyrene

71000 U 710008100Benzo[b]fluoranthene

32000 J 710004700Benzo[g,h,i]perylene

71000 U 7100014000Benzo[k]fluoranthene

71000 U 710007100Benzyl alcohol

1100000 7100060001,1'-Biphenyl

71000 U 710008400Bis(2-chloroethoxy)methane

71000 U 710009600Bis(2-chloroethyl)ether

71000 U 710006400bis(chloroisopropyl) ether

71000 U 710007100Bis(2-ethylhexyl) phthalate

71000 U 7100077004-Bromophenyl phenyl ether

71000 U 710005600Butyl benzyl phthalate

140000 U 140000110004-Chloroaniline

71000 U 7100075004-Chloro-3-methylphenol

71000 U 7100084002-Chloronaphthalene

71000 U 7100086002-Chlorophenol

71000 U 7100079004-Chlorophenyl phenyl ether

71000 U 710004500Chrysene

71000 U 7100036000Diallate

34000 J 710005100Dibenz(a,h)anthracene

71000 U 710007100Dibenzofuran

71000 U 7100079001,2-Dichlorobenzene



140000 U 14000060003,3'-Dichlorobenzidine

71000 U 7100075002,4-Dichlorophenol


71000 U 710007500Diethyl phthalate

27000 J 710005400Dimethoate

71000 U 7100036007,12-Dimethylbenz(a)anthracene

360000 U 3600001800003,3'-Dimethylbenzidine

71000 U 7100094002,4-Dimethylphenol

71000 U 710007300Dimethyl phthalate

71000 U 710006400Di-n-butyl phthalate

71000 U 7100051001,3-Dinitrobenzene

360000 U 360000360004,6-Dinitro-2-methylphenol


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS


680-56861-1

Solid

Date Sampled: 04/14/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1733

10



Injection Volume:



Lab File ID:

Instrument ID:

g1006.d

30.04 g

10 mL

1 uL

3546

MSG


360000 U 3600001800002,4-Dinitrophenol

71000 U 71000100002,4-Dinitrotoluene


71000 U 710006200Di-n-octyl phthalate

71000 U 7100034000Dinoseb

71000 U 71000260001,4-Dioxane

71000 U 710003600Disulfoton

71000 U 710006600Ethyl methanesulfonate

71000 U 710004700Ethyl Parathion

71000 U * 710006200Famphur

71000 U 710006900Fluoranthene

71000 U 710007700Fluorene

71000 U 710008400Hexachlorobenzene

71000 U 710007700Hexachlorobutadiene

71000 U 710008800Hexachlorocyclopentadiene

71000 U 710006000Hexachloroethane

36000000 U 360000002800000Hexachlorophene

71000 U * 710006200Hexachloropropene

32000 J 710006000Indeno[1,2,3-cd]pyrene

71000 U 710007100Isophorone

71000 U 710005100Isosafrole

14000000 U 14000000180000Methapyrilene

71000 U 7100088003-Methylcholanthrene

71000 U * 710003600Methyl methanesulfonate

21000 J 7100081002-Methylnaphthalene

71000 U 710005600Methyl parathion

71000 U 7100058002-Methylphenol

12000 J 7100092003 & 4 Methylphenol

8000 J 710006400Naphthalene

71000 U * 7100036001,4-Naphthoquinone

71000 U * 71000140001-Naphthylamine

71000 U 7100073002-Naphthylamine

360000 U 36000096002-Nitroaniline

360000 U 36000099003-Nitroaniline

360000 U 360000100004-Nitroaniline

71000 U 710005600Nitrobenzene

71000 U 7100088002-Nitrophenol

360000 U 360000710004-Nitrophenol

710000 U 7100001800004-Nitroquinoline-1-oxide

71000 U 710005600N-Nitro-o-toluidine

71000 U 710006000N-Nitrosodiethylamine

71000 U 7100026000N-Nitrosodimethylamine

71000 U 710005100N-Nitrosodi-n-butylamine

71000 U 710006900N-Nitrosodi-n-propylamine

71000 U 710007100N-Nitrosodiphenylamine

71000 U 710005400N-Nitrosomethylethylamine


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS


680-56861-1

Solid

Date Sampled: 04/14/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1733

10



Injection Volume:



Lab File ID:

Instrument ID:

g1006.d

30.04 g

10 mL

1 uL

3546

MSG


71000 U 710005800N-Nitrosomorpholine

71000 U 710004500N-Nitrosopiperidine

71000 U 710003900N-Nitrosopyrrolidine

20000 J * 710008600o,o',o''-Triethylphosphorothioate

71000 U 710004100p-Dimethylamino azobenzene

71000 U 710005400Pentachlorobenzene

71000 U 710004500Pentachloronitrobenzene

360000 U 36000071000Pentachlorophenol

71000 U 710007100Phenacetin

6800 J 710005800Phenanthrene

71000 U 710007300Phenol

71000 U * 710004700Phorate

71000 U 7100036002-Picoline

360000 U * 360000180000p-Phenylene diamine

71000 U 710005100Pronamide

71000 U 710005800Pyrene

71000 U 710006200Pyridine

71000 U 710005100Safrole, Total

71000 U 710004300Sulfotepp

71000 U 7100066001,2,4,5-Tetrachlorobenzene

71000 U 7100047002,3,4,6-Tetrachlorophenol

71000 U 710004900Thionazin

71000 U 7100075002-Toluidine

71000 U 7100066001,2,4-Trichlorobenzene

71000 U 7100075002,4,5-Trichlorophenol


71000 U 71000360001,3,5-Trinitrobenzene


0 34 - 130D2,4,6-Tribromophenol

0 34 - 130D2-Fluorobiphenyl

0 30 - 130D2-Fluorophenol

0 39 - 130DTerphenyl-d14

0 30 - 130DPhenol-d5

0 27 - 130DNitrobenzene-d5


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS


680-56861-1

Solid

Date Sampled: 04/14/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/10/2010 1028

100



Injection Volume:



Lab File ID:

Instrument ID:

g1155.d

30.04 g

10 mL

1 uL

3546

MSG


2500000 71000073000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-NS


680-56861-2

Solid

Date Sampled: 04/14/2010 1245



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1758

10



Injection Volume:



Lab File ID:

Instrument ID:

g1007.d

30.05 g

1.0 mL

1 uL

3546

MSG


770 J 4200520Acenaphthene






8400 U 8400430Aniline






910 J 4200280Benzo[g,h,i]perylene



51000 42003601,1'-Biphenyl












4200 U 4200270Chrysene

4200 U 42002200Diallate

800 J 4200300Dibenz(a,h)anthracene

510 J 4200420Dibenzofuran







470 J 4200440Diethyl phthalate

4200 U 4200320Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-NS


680-56861-2

Solid

Date Sampled: 04/14/2010 1245



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1758

10



Injection Volume:



Lab File ID:

Instrument ID:

g1007.d

30.05 g

1.0 mL

1 uL

3546

MSG


22000 U 22000110002,4-Dinitrophenol




4200 U 42002000Dinoseb

4200 U 420015001,4-Dioxane




4200 U * 4200370Famphur


500 J 4200460Fluorene







720 J 4200360Indeno[1,2,3-cd]pyrene



850000 U 85000011000Methapyrilene






1600 J 42005503 & 4 Methylphenol





22000 U 220005702-Nitroaniline















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-NS


680-56861-2

Solid

Date Sampled: 04/14/2010 1245



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1758

10



Injection Volume:



Lab File ID:

Instrument ID:

g1007.d

30.05 g

1.0 mL

1 uL

3546

MSG





1200 J * 4200510o,o',o''-Triethylphosphorothioate







4200 U 4200430Phenol

4200 U * 4200280Phorate

4200 U 42002202-Picoline


4200 U 4200300Pronamide

4200 U 4200340Pyrene

4200 U 4200370Pyridine


4200 U 4200250Sulfotepp



4200 U 4200290Thionazin

4200 U 42004402-Toluidine













Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-NS


680-56861-2

Solid

Date Sampled: 04/14/2010 1245



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/10/2010 1052

100



Injection Volume:



Lab File ID:

Instrument ID:

g1156.d

30.05 g

1.0 mL

1 uL

3546

MSG


140000 420004300Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1822

10



Injection Volume:



Lab File ID:

Instrument ID:

g1008.d

30.06 g

10 mL

1 uL

3546

MSG


10000 J 710008800Acenaphthene






140000 U 1400007300Aniline






71000 U 710004700Benzo[g,h,i]perylene



1000000 7100060001,1'-Biphenyl












71000 U 710004500Chrysene

71000 U 7100036000Diallate

71000 U 710005100Dibenz(a,h)anthracene

7900 J 710007100Dibenzofuran

















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1822

10



Injection Volume:



Lab File ID:

Instrument ID:

g1008.d

30.06 g

10 mL

1 uL

3546

MSG


360000 U 3600001800002,4-Dinitrophenol




71000 U 7100034000Dinoseb

71000 U 71000260001,4-Dioxane




71000 U * 710006200Famphur


71000 U 710007700Fluorene







71000 U 710006000Indeno[1,2,3-cd]pyrene



14000000 U 14000000180000Methapyrilene






71000 U 7100092003 & 4 Methylphenol





360000 U 36000096002-Nitroaniline

360000 U 36000099003-Nitroaniline

360000 U 360000100004-Nitroaniline



360000 U 360000710004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1822

10



Injection Volume:



Lab File ID:

Instrument ID:

g1008.d

30.06 g

10 mL

1 uL

3546

MSG





71000 U * 710008600o,o',o''-Triethylphosphorothioate







71000 U 710007300Phenol

71000 U * 710004700Phorate

71000 U 7100036002-Picoline


71000 U 710005100Pronamide

71000 U 710005800Pyrene

71000 U 710006200Pyridine


71000 U 710004300Sulfotepp



71000 U 710004900Thionazin

71000 U 7100075002-Toluidine













Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/10/2010 1116

100



Injection Volume:



Lab File ID:

Instrument ID:

g1157.d

30.06 g

10 mL

1 uL

3546

MSG


2400000 71000073000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-NS


680-56861-4

Solid

Date Sampled: 04/14/2010 1715



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1506

100



Injection Volume:



Lab File ID:

Instrument ID:

g1016a.d

30.10 g

1.0 mL

1 uL

3546

MSG








75000 U 750003900Aniline









360000 3800032001,1'-Biphenyl












38000 U 380002400Chrysene

38000 U 3800019000Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-NS


680-56861-4

Solid

Date Sampled: 04/14/2010 1715



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1506

100



Injection Volume:



Lab File ID:

Instrument ID:

g1016a.d

30.10 g

1.0 mL

1 uL

3546

MSG


190000 U 190000940002,4-Dinitrophenol




38000 U 3800018000Dinoseb

38000 U 38000140001,4-Dioxane




38000 U 380003300Famphur


38000 U 380004100Fluorene






38000 U 380003300Hexachloropropene






38000 U 380001900Methyl methanesulfonate

38000 U 3800043002-Methylnaphthalene



38000 U 3800049003 & 4 Methylphenol

38000 U 380003400Naphthalene

38000 U 3800019001,4-Naphthoquinone



190000 U 19000051002-Nitroaniline

190000 U 19000052003-Nitroaniline

190000 U 19000056004-Nitroaniline



190000 U 190000380004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-NS


680-56861-4

Solid

Date Sampled: 04/14/2010 1715



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1506

100



Injection Volume:



Lab File ID:

Instrument ID:

g1016a.d

30.10 g

1.0 mL

1 uL

3546

MSG





38000 U 380004600o,o',o''-Triethylphosphorothioate






38000 U 380003100Phenanthrene

38000 U 380003900Phenol

38000 U 380002500Phorate

38000 U 3800019002-Picoline

190000 U 19000095000p-Phenylene diamine

38000 U 380002700Pronamide

38000 U 380003100Pyrene

38000 U 380003300Pyridine


38000 U 380002300Sulfotepp



38000 U 380002600Thionazin

38000 U 3800040002-Toluidine













Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-NS


680-56861-4

Solid

Date Sampled: 04/14/2010 1715



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/10/2010 1140

200



Injection Volume:



Lab File ID:

Instrument ID:

g1158.d

30.10 g

1.0 mL

1 uL

3546

MSG











Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1910

10



Injection Volume:



Lab File ID:

Instrument ID:

g1010.d

30.05 g

20 mL

1 uL

3546

MSG








330000 U 33000017000Aniline

170000 U 17000013000Anthracene

170000 U 17000029000Aramite, Total


170000 U 17000026000Benzo[a]pyrene





1600000 170000140001,1'-Biphenyl










170000 U 170000200002-Chlorophenol


170000 U 17000011000Chrysene

170000 U 17000086000Diallate










170000 U 17000013000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1910

10



Injection Volume:



Lab File ID:

Instrument ID:

g1010.d

30.05 g

20 mL

1 uL

3546

MSG


860000 U 8600004200002,4-Dinitrophenol




170000 U 17000081000Dinoseb

170000 U 170000610001,4-Dioxane

170000 U 1700008600Disulfoton



170000 U * 17000015000Famphur


170000 U 17000018000Fluorene








170000 U 17000017000Isophorone

170000 U 17000012000Isosafrole

34000000 U 34000000420000Methapyrilene





170000 U 170000140002-Methylphenol

170000 U 170000220003 & 4 Methylphenol

170000 U 17000015000Naphthalene


170000 U * 170000330001-Naphthylamine


860000 U 860000230002-Nitroaniline

860000 U 860000230003-Nitroaniline

860000 U 860000250004-Nitroaniline


170000 U 170000210002-Nitrophenol

860000 U 8600001700004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1910

10



Injection Volume:



Lab File ID:

Instrument ID:

g1010.d

30.05 g

20 mL

1 uL

3546

MSG










170000 U 17000017000Phenacetin


170000 U 17000017000Phenol

170000 U * 17000011000Phorate

170000 U 17000086002-Picoline


170000 U 17000012000Pronamide

170000 U 17000014000Pyrene

170000 U 17000015000Pyridine

170000 U 17000012000Safrole, Total

170000 U 17000010000Sulfotepp



170000 U 17000012000Thionazin

170000 U 170000180002-Toluidine













Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/10/2010 1203

50



Injection Volume:



Lab File ID:

Instrument ID:

g1159.d

30.05 g

20 mL

1 uL

3546

MSG


5200000 83000086000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US


680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1934

10



Injection Volume:



Lab File ID:

Instrument ID:

g1011.d

30.02 g

15 mL

1 uL

3546

MSG








410000 U 41000021000Aniline

200000 U 20000015000Anthracene

200000 U 20000035000Aramite, Total


200000 U 20000032000Benzo[a]pyrene





340000 200000170001,1'-Biphenyl










200000 U 200000250002-Chlorophenol


200000 U 20000013000Chrysene

200000 U 200000100000Diallate










200000 U 20000015000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US


680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1934

10



Injection Volume:



Lab File ID:

Instrument ID:

g1011.d

30.02 g

15 mL

1 uL

3546

MSG


1000000 U 10000005100002,4-Dinitrophenol




200000 U 20000099000Dinoseb

200000 U 200000740001,4-Dioxane

200000 U 20000010000Disulfoton



200000 U * 20000018000Famphur


200000 U 20000022000Fluorene








200000 U 20000020000Isophorone

200000 U 20000015000Isosafrole

41000000 U 41000000510000Methapyrilene





200000 U 200000170002-Methylphenol

200000 U 200000270003 & 4 Methylphenol

200000 U 20000018000Naphthalene


200000 U * 200000410001-Naphthylamine


1000000 U 1000000280002-Nitroaniline

1000000 U 1000000280003-Nitroaniline

1000000 U 1000000300004-Nitroaniline


200000 U 200000250002-Nitrophenol

1000000 U 10000002000004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US


680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1934

10



Injection Volume:



Lab File ID:

Instrument ID:

g1011.d

30.02 g

15 mL

1 uL

3546

MSG










200000 U 20000020000Phenacetin


200000 U 20000021000Phenol

200000 U * 20000014000Phorate

200000 U 200000100002-Picoline


200000 U 20000015000Pronamide

22000 J 20000017000Pyrene

200000 U 20000018000Pyridine

200000 U 20000015000Safrole, Total

200000 U 20000012000Sulfotepp



200000 U 20000014000Thionazin

200000 U 200000220002-Toluidine





1100000 20000021000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-NS


680-56861-7

Solid

Date Sampled: 04/15/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1958

10



Injection Volume:



Lab File ID:

Instrument ID:

g1012.d

30.12 g

1.0 mL

1 uL

3546

MSG








8600 U 8600440Aniline









4300 U 43003701,1'-Biphenyl













4300 U 43002200Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-NS


680-56861-7

Solid

Date Sampled: 04/15/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1958

10



Injection Volume:



Lab File ID:

Instrument ID:

g1012.d

30.12 g

1.0 mL

1 uL

3546

MSG






4300 U 43002100Dinoseb

4300 U 430016001,4-Dioxane




4300 U * 4300380Famphur


4300 U 4300470Fluorene





















3500 J 220005902-Nitroaniline















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-NS


680-56861-7

Solid

Date Sampled: 04/15/2010 0950



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 1958

10



Injection Volume:



Lab File ID:

Instrument ID:

g1012.d

30.12 g

1.0 mL

1 uL

3546

MSG












4300 U 4300440Phenol

4300 U * 4300290Phorate

4300 U 43002202-Picoline



4300 U 4300350Pyrene





















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 2022

10



Injection Volume:



Lab File ID:

Instrument ID:

g1013.d

30.02 g

10 mL

1 uL

3546

MSG








210000 U 21000011000Aniline

100000 U 1000007800Anthracene

100000 U 10000018000Aramite, Total


100000 U 10000016000Benzo[a]pyrene





940000 10000087001,1'-Biphenyl










100000 U 100000120002-Chlorophenol


100000 U 1000006500Chrysene

100000 U 10000053000Diallate










100000 U 1000007800Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 2022

10



Injection Volume:



Lab File ID:

Instrument ID:

g1013.d

30.02 g

10 mL

1 uL

3546

MSG


530000 U 5300002600002,4-Dinitrophenol




100000 U 10000050000Dinoseb

100000 U 100000370001,4-Dioxane

100000 U 1000005300Disulfoton



100000 U * 1000009000Famphur


100000 U 10000011000Fluorene








100000 U 10000010000Isophorone

100000 U 1000007500Isosafrole

21000000 U 21000000260000Methapyrilene





100000 U 10000084002-Methylphenol

100000 U 100000130003 & 4 Methylphenol



100000 U * 100000210001-Naphthylamine


530000 U 530000140002-Nitroaniline

530000 U 530000140003-Nitroaniline

530000 U 530000150004-Nitroaniline


100000 U 100000130002-Nitrophenol

530000 U 5300001000004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 2022

10



Injection Volume:



Lab File ID:

Instrument ID:

g1013.d

30.02 g

10 mL

1 uL

3546

MSG










100000 U 10000010000Phenacetin


100000 U 10000011000Phenol

100000 U * 1000006900Phorate

100000 U 10000053002-Picoline


100000 U 1000007500Pronamide

100000 U 1000008400Pyrene

100000 U 1000009000Pyridine

100000 U 1000007500Safrole, Total

100000 U 1000006200Sulfotepp



100000 U 1000007200Thionazin

100000 U 100000110002-Toluidine













Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/10/2010 1227

50



Injection Volume:



Lab File ID:

Instrument ID:

g1160.d

30.02 g

10 mL

1 uL

3546

MSG


2800000 51000053000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US


680-56861-9

Solid

Date Sampled: 04/15/2010 1100



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 2046

10



Injection Volume:



Lab File ID:

Instrument ID:

g1014.d

30.11 g

5.0 mL

1 uL

3546

MSG








150000 U 1500007600Aniline









180000 7400063001,1'-Biphenyl












74000 U 740004700Chrysene

74000 U 7400038000Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US


680-56861-9

Solid

Date Sampled: 04/15/2010 1100



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 2046

10



Injection Volume:



Lab File ID:

Instrument ID:

g1014.d

30.11 g

5.0 mL

1 uL

3546

MSG


380000 U 3800001900002,4-Dinitrophenol




74000 U 7400036000Dinoseb

74000 U 74000270001,4-Dioxane




74000 U * 740006500Famphur


74000 U 740008100Fluorene










15000000 U 15000000190000Methapyrilene






74000 U 7400096003 & 4 Methylphenol





380000 U 380000100002-Nitroaniline

380000 U 380000100003-Nitroaniline

380000 U 380000110004-Nitroaniline



380000 U 380000740004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US


680-56861-9

Solid

Date Sampled: 04/15/2010 1100



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/03/2010 2046

10



Injection Volume:



Lab File ID:

Instrument ID:

g1014.d

30.11 g

5.0 mL

1 uL

3546

MSG












74000 U 740007600Phenol

74000 U * 740004900Phorate

74000 U 7400038002-Picoline


74000 U 740005400Pronamide

74000 U 740006000Pyrene

74000 U 740006500Pyridine


74000 U 740004500Sulfotepp



74000 U 740005200Thionazin

74000 U 7400078002-Toluidine














Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-NS


680-56861-10

Solid

Date Sampled: 04/15/2010 1105



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1442

50



Injection Volume:



Lab File ID:

Instrument ID:

g1015a.d

30.03 g

1.0 mL

1 uL

3546

MSG








41000 U 410002100Aniline









290000 2100018001,1'-Biphenyl












21000 U 210001300Chrysene

21000 U 2100011000Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-NS


680-56861-10

Solid

Date Sampled: 04/15/2010 1105



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1442

50



Injection Volume:



Lab File ID:

Instrument ID:

g1015a.d

30.03 g

1.0 mL

1 uL

3546

MSG


110000 U 110000520002,4-Dinitrophenol




21000 U 2100010000Dinoseb

21000 U 2100075001,4-Dioxane




21000 U 210001800Famphur


21000 U 210002300Fluorene
















21000 U 2100027003 & 4 Methylphenol





110000 U 11000028002-Nitroaniline

110000 U 11000029003-Nitroaniline

110000 U 11000031004-Nitroaniline



110000 U 110000210004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-NS


680-56861-10

Solid

Date Sampled: 04/15/2010 1105



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1442

50



Injection Volume:



Lab File ID:

Instrument ID:

g1015a.d

30.03 g

1.0 mL

1 uL

3546

MSG












21000 U 210002100Phenol

21000 U 210001400Phorate

21000 U 2100011002-Picoline


21000 U 210001500Pronamide

21000 U 210001700Pyrene

21000 U 210001800Pyridine


21000 U 210001300Sulfotepp



21000 U 210001400Thionazin

21000 U 2100022002-Toluidine













Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-NS


680-56861-10

Solid

Date Sampled: 04/15/2010 1105



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/10/2010 1250

200



Injection Volume:



Lab File ID:

Instrument ID:

g1161.d

30.03 g

1.0 mL

1 uL

3546

MSG











Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS


680-56861-11

Solid

Date Sampled: 04/15/2010 1110



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1021

10



Injection Volume:



Lab File ID:

Instrument ID:

g1016.d

30.05 g

20 mL

1 uL

3546

MSG








320000 U 32000017000Aniline

160000 U 16000012000Anthracene

160000 U 16000028000Aramite, Total


160000 U 16000026000Benzo[a]pyrene





800000 160000140001,1'-Biphenyl










160000 U 160000200002-Chlorophenol


160000 U 16000010000Chrysene

160000 U 16000084000Diallate










160000 U 16000012000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS


680-56861-11

Solid

Date Sampled: 04/15/2010 1110



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1021

10



Injection Volume:



Lab File ID:

Instrument ID:

g1016.d

30.05 g

20 mL

1 uL

3546

MSG


840000 U 8400004100002,4-Dinitrophenol




160000 U 16000079000Dinoseb

160000 U 160000590001,4-Dioxane

160000 U 1600008400Disulfoton



160000 U 16000014000Famphur


160000 U 16000018000Fluorene








160000 U 16000016000Isophorone

160000 U 16000012000Isosafrole

33000000 U 33000000410000Methapyrilene





160000 U 160000130002-Methylphenol

160000 U 160000210003 & 4 Methylphenol

160000 U 16000015000Naphthalene




840000 U 840000220002-Nitroaniline

840000 U 840000230003-Nitroaniline

840000 U 840000240004-Nitroaniline


160000 U 160000200002-Nitrophenol

840000 U 8400001600004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS


680-56861-11

Solid

Date Sampled: 04/15/2010 1110



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1021

10



Injection Volume:



Lab File ID:

Instrument ID:

g1016.d

30.05 g

20 mL

1 uL

3546

MSG










160000 U 16000016000Phenacetin


160000 U 16000017000Phenol

160000 U 16000011000Phorate

160000 U 16000084002-Picoline


160000 U 16000012000Pronamide

160000 U 16000013000Pyrene

160000 U 16000014000Pyridine

160000 U 16000012000Safrole, Total

160000 U 1600009800Sulfotepp



160000 U 16000011000Thionazin

160000 U 160000170002-Toluidine





2500000 16000017000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US


680-56861-12

Solid

Date Sampled: 04/15/2010 1145



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1045

10



Injection Volume:



Lab File ID:

Instrument ID:

g1017.d

30.18 g

10 mL

1 uL

3546

MSG








380000 U 38000020000Aniline

190000 U 19000014000Anthracene

190000 U 19000033000Aramite, Total


190000 U 19000030000Benzo[a]pyrene





160000 J 190000160001,1'-Biphenyl










190000 U 190000230002-Chlorophenol


190000 U 19000012000Chrysene

190000 U 19000098000Diallate










190000 U 19000014000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US


680-56861-12

Solid

Date Sampled: 04/15/2010 1145



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1045

10



Injection Volume:



Lab File ID:

Instrument ID:

g1017.d

30.18 g

10 mL

1 uL

3546

MSG


980000 U 9800004800002,4-Dinitrophenol




190000 U 19000092000Dinoseb

190000 U 190000690001,4-Dioxane

190000 U 1900009800Disulfoton



190000 U 19000017000Famphur


190000 U 19000021000Fluorene








190000 U 19000019000Isophorone

190000 U 19000014000Isosafrole

39000000 U 39000000480000Methapyrilene





190000 U 190000160002-Methylphenol

190000 U 190000250003 & 4 Methylphenol

190000 U 19000017000Naphthalene




980000 U 980000260002-Nitroaniline

980000 U 980000260003-Nitroaniline

980000 U 980000280004-Nitroaniline


190000 U 190000240002-Nitrophenol

980000 U 9800001900004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US


680-56861-12

Solid

Date Sampled: 04/15/2010 1145



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1045

10



Injection Volume:



Lab File ID:

Instrument ID:

g1017.d

30.18 g

10 mL

1 uL

3546

MSG










190000 U 19000019000Phenacetin


190000 U 19000020000Phenol

190000 U 19000013000Phorate

190000 U 19000098002-Picoline


190000 U 19000014000Pronamide

190000 U 19000016000Pyrene

190000 U 19000017000Pyridine

190000 U 19000014000Safrole, Total

190000 U 19000012000Sulfotepp



190000 U 19000013000Thionazin

190000 U 190000200002-Toluidine














Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US


680-56861-13

Solid

Date Sampled: 04/15/2010 1415



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1108

10



Injection Volume:



Lab File ID:

Instrument ID:

g1018.d

30.07 g

10 mL

1 uL

3546

MSG








380000 U 38000020000Aniline

190000 U 19000014000Anthracene

190000 U 19000033000Aramite, Total


190000 U 19000030000Benzo[a]pyrene





140000 J 190000160001,1'-Biphenyl










190000 U 190000230002-Chlorophenol


190000 U 19000012000Chrysene

190000 U 19000098000Diallate










190000 U 19000014000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US


680-56861-13

Solid

Date Sampled: 04/15/2010 1415



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1108

10



Injection Volume:



Lab File ID:

Instrument ID:

g1018.d

30.07 g

10 mL

1 uL

3546

MSG


980000 U 9800004800002,4-Dinitrophenol




190000 U 19000092000Dinoseb

190000 U 190000690001,4-Dioxane

190000 U 1900009800Disulfoton



190000 U 19000017000Famphur


190000 U 19000021000Fluorene








190000 U 19000019000Isophorone

190000 U 19000014000Isosafrole

39000000 U 39000000480000Methapyrilene





190000 U 190000160002-Methylphenol

190000 U 190000250003 & 4 Methylphenol

190000 U 19000017000Naphthalene




980000 U 980000260002-Nitroaniline

980000 U 980000270003-Nitroaniline

980000 U 980000280004-Nitroaniline


190000 U 190000240002-Nitrophenol

980000 U 9800001900004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US


680-56861-13

Solid

Date Sampled: 04/15/2010 1415



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1108

10



Injection Volume:



Lab File ID:

Instrument ID:

g1018.d

30.07 g

10 mL

1 uL

3546

MSG










190000 U 19000019000Phenacetin


190000 U 19000020000Phenol

190000 U 19000013000Phorate

190000 U 19000098002-Picoline


190000 U 19000014000Pronamide

190000 U 19000016000Pyrene

190000 U 19000017000Pyridine

190000 U 19000014000Safrole, Total

190000 U 19000012000Sulfotepp



190000 U 19000013000Thionazin

190000 U 190000200002-Toluidine














Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-NS


680-56861-14

Solid

Date Sampled: 04/15/2010 1505



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1132

10



Injection Volume:



Lab File ID:

Instrument ID:

g1019.d

30.02 g

1.0 mL

1 uL

3546

MSG








7900 U 7900410Aniline









18000 40003401,1'-Biphenyl













4000 U 40002000Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-NS


680-56861-14

Solid

Date Sampled: 04/15/2010 1505



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1132

10



Injection Volume:



Lab File ID:

Instrument ID:

g1019.d

30.02 g

1.0 mL

1 uL

3546

MSG






4000 U 40001900Dinoseb

4000 U 400014001,4-Dioxane

410 J 4000200Disulfoton



4000 U 4000350Famphur






































Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-NS


680-56861-14

Solid

Date Sampled: 04/15/2010 1505



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1132

10



Injection Volume:



Lab File ID:

Instrument ID:

g1019.d

30.02 g

1.0 mL

1 uL

3546

MSG












4000 U 4000410Phenol

4000 U 4000260Phorate

4000 U 40002002-Picoline



490 J 4000320Pyrene





















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS


680-56861-15

Solid

Date Sampled: 04/15/2010 1520



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1156

10



Injection Volume:



Lab File ID:

Instrument ID:

g1020.d

30.15 g

10 mL

1 uL

3546

MSG








220000 U 22000012000Aniline

110000 U 1100008500Anthracene

110000 U 11000019000Aramite, Total


110000 U 11000018000Benzo[a]pyrene





620000 11000095001,1'-Biphenyl










110000 U 110000140002-Chlorophenol


110000 U 1100007100Chrysene

110000 U 11000058000Diallate










110000 U 1100008500Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS


680-56861-15

Solid

Date Sampled: 04/15/2010 1520



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1156

10



Injection Volume:



Lab File ID:

Instrument ID:

g1020.d

30.15 g

10 mL

1 uL

3546

MSG


580000 U 5800002800002,4-Dinitrophenol




110000 U 11000054000Dinoseb

110000 U 110000410001,4-Dioxane

110000 U 1100005800Disulfoton



110000 U 1100009800Famphur


110000 U 11000012000Fluorene








110000 U 11000011000Isophorone

110000 U 1100008100Isosafrole

23000000 U 23000000280000Methapyrilene





110000 U 11000092002-Methylphenol

25000 J 110000150003 & 4 Methylphenol

110000 U 11000010000Naphthalene




580000 U 580000150002-Nitroaniline

580000 U 580000160003-Nitroaniline

580000 U 580000170004-Nitroaniline


110000 U 110000140002-Nitrophenol

580000 U 5800001100004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS


680-56861-15

Solid

Date Sampled: 04/15/2010 1520



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1156

10



Injection Volume:



Lab File ID:

Instrument ID:

g1020.d

30.15 g

10 mL

1 uL

3546

MSG










110000 U 11000011000Phenacetin


110000 U 11000012000Phenol

110000 U 1100007500Phorate

110000 U 11000058002-Picoline


110000 U 1100008100Pronamide

110000 U 1100009200Pyrene

110000 U 1100009800Pyridine

110000 U 1100008100Safrole, Total

110000 U 1100006800Sulfotepp



110000 U 1100007800Thionazin

110000 U 110000120002-Toluidine





2100000 11000012000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US


680-56861-16

Solid

Date Sampled: 04/15/2010 1525



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1219

10



Injection Volume:



Lab File ID:

Instrument ID:

g1021.d

30.02 g

15 mL

1 uL

3546

MSG








380000 U 38000019000Aniline

190000 U 19000014000Anthracene

190000 U 19000033000Aramite, Total


190000 U 19000030000Benzo[a]pyrene





230000 190000160001,1'-Biphenyl










190000 U 190000230002-Chlorophenol


190000 U 19000012000Chrysene

190000 U 19000097000Diallate










190000 U 19000014000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US


680-56861-16

Solid

Date Sampled: 04/15/2010 1525



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1219

10



Injection Volume:



Lab File ID:

Instrument ID:

g1021.d

30.02 g

15 mL

1 uL

3546

MSG


970000 U 9700004700002,4-Dinitrophenol




190000 U 19000091000Dinoseb

190000 U 190000680001,4-Dioxane

190000 U 1900009700Disulfoton



190000 U 19000017000Famphur


190000 U 19000021000Fluorene








190000 U 19000019000Isophorone

190000 U 19000014000Isosafrole

38000000 U 38000000470000Methapyrilene





190000 U 190000150002-Methylphenol

190000 U 190000250003 & 4 Methylphenol

190000 U 19000017000Naphthalene




970000 U 970000260002-Nitroaniline

970000 U 970000260003-Nitroaniline

970000 U 970000280004-Nitroaniline


190000 U 190000230002-Nitrophenol

970000 U 9700001900004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US


680-56861-16

Solid

Date Sampled: 04/15/2010 1525



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1219

10



Injection Volume:



Lab File ID:

Instrument ID:

g1021.d

30.02 g

15 mL

1 uL

3546

MSG










190000 U 19000019000Phenacetin


190000 U 19000019000Phenol

190000 U 19000013000Phorate

190000 U 19000097002-Picoline


190000 U 19000014000Pronamide

190000 U 19000015000Pyrene

190000 U 19000017000Pyridine

190000 U 19000014000Safrole, Total

190000 U 19000011000Sulfotepp



190000 U 19000013000Thionazin

190000 U 190000200002-Toluidine














Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-NS


680-56861-17

Solid

Date Sampled: 04/15/2010 1600



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1243

10



Injection Volume:



Lab File ID:

Instrument ID:

g1022.d

30.03 g

1.0 mL

1 uL

3546

MSG








9100 U 9100470Aniline









4600 U 46003901,1'-Biphenyl













4600 U 46002300Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-NS


680-56861-17

Solid

Date Sampled: 04/15/2010 1600



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1243

10



Injection Volume:



Lab File ID:

Instrument ID:

g1022.d

30.03 g

1.0 mL

1 uL

3546

MSG






4600 U 46002200Dinoseb

4600 U 460017001,4-Dioxane




4600 U 4600400Famphur


















4600 U 46005903 & 4 Methylphenol




















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-NS


680-56861-17

Solid

Date Sampled: 04/15/2010 1600



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1243

10



Injection Volume:



Lab File ID:

Instrument ID:

g1022.d

30.03 g

1.0 mL

1 uL

3546

MSG












4600 U 4600470Phenol

4600 U 4600300Phorate

4600 U 46002302-Picoline



4600 U 4600370Pyrene












700 J 4600470Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS


680-56861-18

Solid

Date Sampled: 04/15/2010 1615



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1307

10



Injection Volume:



Lab File ID:

Instrument ID:

g1023.d

30.00 g

10 mL

1 uL

3546

MSG








270000 U 27000014000Aniline

130000 U 13000010000Anthracene

130000 U 13000023000Aramite, Total


130000 U 13000021000Benzo[a]pyrene





760000 130000110001,1'-Biphenyl










130000 U 130000160002-Chlorophenol


130000 U 1300008500Chrysene

130000 U 13000069000Diallate










130000 U 13000010000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS


680-56861-18

Solid

Date Sampled: 04/15/2010 1615



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1307

10



Injection Volume:



Lab File ID:

Instrument ID:

g1023.d

30.00 g

10 mL

1 uL

3546

MSG


690000 U 6900003400002,4-Dinitrophenol




130000 U 13000065000Dinoseb

130000 U 130000490001,4-Dioxane

130000 U 1300006900Disulfoton



130000 U 13000012000Famphur


130000 U 13000015000Fluorene








130000 U 13000013000Isophorone

130000 U 1300009800Isosafrole

27000000 U 27000000340000Methapyrilene





130000 U 130000110002-Methylphenol

130000 U 130000170003 & 4 Methylphenol

130000 U 13000012000Naphthalene




690000 U 690000180002-Nitroaniline

690000 U 690000190003-Nitroaniline

690000 U 690000200004-Nitroaniline


130000 U 130000170002-Nitrophenol

690000 U 6900001300004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS


680-56861-18

Solid

Date Sampled: 04/15/2010 1615



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1307

10



Injection Volume:



Lab File ID:

Instrument ID:

g1023.d

30.00 g

10 mL

1 uL

3546

MSG










130000 U 13000013000Phenacetin


130000 U 13000014000Phenol

130000 U 1300008900Phorate

130000 U 13000069002-Picoline


130000 U 1300009800Pronamide

15000 J 13000011000Pyrene

130000 U 13000012000Pyridine

130000 U 1300009800Safrole, Total

130000 U 1300008100Sulfotepp



130000 U 1300009400Thionazin

130000 U 130000140002-Toluidine





2500000 13000014000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US


680-56861-19

Solid

Date Sampled: 04/15/2010 1620



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1331

10



Injection Volume:



Lab File ID:

Instrument ID:

g1024.d

30.04 g

10 mL

1 uL

3546

MSG








480000 U 48000025000Aniline

240000 U 24000018000Anthracene

240000 U 24000042000Aramite, Total


240000 U 24000038000Benzo[a]pyrene





33000 J 240000200001,1'-Biphenyl










240000 U 240000290002-Chlorophenol


240000 U 24000015000Chrysene

240000 U 240000120000Diallate










240000 U 24000018000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US


680-56861-19

Solid

Date Sampled: 04/15/2010 1620



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1331

10



Injection Volume:



Lab File ID:

Instrument ID:

g1024.d

30.04 g

10 mL

1 uL

3546

MSG


1200000 U 12000006100002,4-Dinitrophenol




240000 U 240000120000Dinoseb

240000 U 240000880001,4-Dioxane

240000 U 24000012000Disulfoton



240000 U 24000021000Famphur


240000 U 24000026000Fluorene








240000 U 24000024000Isophorone

240000 U 24000018000Isosafrole

49000000 U 49000000610000Methapyrilene





240000 U 240000200002-Methylphenol

240000 U 240000310003 & 4 Methylphenol

240000 U 24000022000Naphthalene




1200000 U 1200000330002-Nitroaniline

1200000 U 1200000340003-Nitroaniline

1200000 U 1200000360004-Nitroaniline


240000 U 240000300002-Nitrophenol

1200000 U 12000002400004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US


680-56861-19

Solid

Date Sampled: 04/15/2010 1620



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1331

10



Injection Volume:



Lab File ID:

Instrument ID:

g1024.d

30.04 g

10 mL

1 uL

3546

MSG










240000 U 24000024000Phenacetin


240000 U 24000025000Phenol

240000 U 24000016000Phorate

240000 U 240000120002-Picoline


240000 U 24000018000Pronamide

240000 U 24000020000Pyrene

240000 U 24000021000Pyridine

240000 U 24000018000Safrole, Total

240000 U 24000015000Sulfotepp



240000 U 24000017000Thionazin

240000 U 240000260002-Toluidine





110000 J 24000025000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US


680-56861-20

Solid

Date Sampled: 04/15/2010 1700



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1354

10



Injection Volume:



Lab File ID:

Instrument ID:

g1025.d

30.02 g

10 mL

1 uL

3546

MSG








180000 U 1800009100Aniline









230000 8800075001,1'-Biphenyl












88000 U 880005600Chrysene

88000 U 8800045000Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US


680-56861-20

Solid

Date Sampled: 04/15/2010 1700



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1354

10



Injection Volume:



Lab File ID:

Instrument ID:

g1025.d

30.02 g

10 mL

1 uL

3546

MSG


450000 U 4500002200002,4-Dinitrophenol




88000 U 8800043000Dinoseb

88000 U 88000320001,4-Dioxane




88000 U 880007800Famphur


88000 U 880009600Fluorene










18000000 U 18000000220000Methapyrilene






88000 U 88000110003 & 4 Methylphenol





450000 U 450000120002-Nitroaniline

450000 U 450000120003-Nitroaniline

450000 U 450000130004-Nitroaniline


88000 U 88000110002-Nitrophenol

450000 U 450000880004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US


680-56861-20

Solid

Date Sampled: 04/15/2010 1700



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 2315

05/04/2010 1354

10



Injection Volume:



Lab File ID:

Instrument ID:

g1025.d

30.02 g

10 mL

1 uL

3546

MSG












88000 U 880009100Phenol

88000 U 880005900Phorate

88000 U 8800045002-Picoline


88000 U 880006400Pronamide

88000 U 880007200Pyrene

88000 U 880007800Pyridine


88000 U 880005300Sulfotepp



88000 U 880006100Thionazin

88000 U 8800094002-Toluidine














Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-NS


680-56861-21

Solid

Date Sampled: 04/16/2010 0840



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

05/04/2010 1529

50



Injection Volume:



Lab File ID:

Instrument ID:

g1026.d

30.08 g

1 mL

1 uL

3546

MSG








38000 U 380002000Aniline








5900 J 190001900Benzyl alcohol

33000 1900016001,1'-Biphenyl












19000 U 190001200Chrysene

19000 U 190009900Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-NS


680-56861-21

Solid

Date Sampled: 04/16/2010 0840



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

05/04/2010 1529

50



Injection Volume:



Lab File ID:

Instrument ID:

g1026.d

30.08 g

1 mL

1 uL

3546

MSG






19000 U 190009300Dinoseb

19000 U 1900070001,4-Dioxane




19000 U 190001700Famphur


19000 U 190002100Fluorene
















19000 U 1900025003 & 4 Methylphenol










99000 U 99000190004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-NS


680-56861-21

Solid

Date Sampled: 04/16/2010 0840



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

05/04/2010 1529

50



Injection Volume:



Lab File ID:

Instrument ID:

g1026.d

30.08 g

1 mL

1 uL

3546

MSG





8600 J 190002300o,o',o''-Triethylphosphorothioate







19000 U 190002000Phenol

19000 U 190001300Phorate

19000 U 190009902-Picoline


19000 U 190001400Pronamide

19000 U 190001600Pyrene

19000 U 190001700Pyridine


19000 U 190001200Sulfotepp



19000 U 190001300Thionazin

19000 U 1900020002-Toluidine














Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS


680-56861-22

Solid

Date Sampled: 04/16/2010 0850



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

05/04/2010 1553

10



Injection Volume:



Lab File ID:

Instrument ID:

g1027.d

30.11 g

20 mL

1 uL

3546

MSG








400000 U 40000020000Aniline

200000 U 20000015000Anthracene

200000 U 20000034000Aramite, Total


200000 U 20000031000Benzo[a]pyrene





470000 200000170001,1'-Biphenyl










200000 U 200000240002-Chlorophenol


200000 U 20000013000Chrysene

200000 U 200000100000Diallate










200000 U 20000015000Dimethoate









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS


680-56861-22

Solid

Date Sampled: 04/16/2010 0850



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

05/04/2010 1553

10



Injection Volume:



Lab File ID:

Instrument ID:

g1027.d

30.11 g

20 mL

1 uL

3546

MSG


1000000 U 10000005000002,4-Dinitrophenol




200000 U 20000096000Dinoseb

200000 U 200000720001,4-Dioxane

200000 U 20000010000Disulfoton



200000 U 20000017000Famphur


200000 U 20000022000Fluorene








200000 U 20000020000Isophorone

200000 U 20000014000Isosafrole

40000000 U 40000000500000Methapyrilene





200000 U 200000160002-Methylphenol

200000 U 200000260003 & 4 Methylphenol

200000 U 20000018000Naphthalene




1000000 U 1000000270002-Nitroaniline

1000000 U 1000000280003-Nitroaniline

1000000 U 1000000290004-Nitroaniline


200000 U 200000250002-Nitrophenol

1000000 U 10000002000004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS


680-56861-22

Solid

Date Sampled: 04/16/2010 0850



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

05/04/2010 1553

10



Injection Volume:



Lab File ID:

Instrument ID:

g1027.d

30.11 g

20 mL

1 uL

3546

MSG










200000 U 20000020000Phenacetin


200000 U 20000020000Phenol

200000 U 20000013000Phorate

200000 U 200000100002-Picoline


200000 U 20000014000Pronamide

200000 U 20000016000Pyrene

200000 U 20000017000Pyridine

200000 U 20000014000Safrole, Total

200000 U 20000012000Sulfotepp



200000 U 20000014000Thionazin

200000 U 200000210002-Toluidine





1400000 20000020000Diphenyl ether









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US


680-56861-23

Solid

Date Sampled: 04/16/2010 0930



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

04/23/2010 1826

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7044.d

30.10 g

20 mL

1 uL

3546

MSN








62000 U 620003200Aniline









55000 3100026001,1'-Biphenyl












31000 U 310002000Chrysene

31000 U 3100016000Diallate



















Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US


680-56861-23

Solid

Date Sampled: 04/16/2010 0930



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

04/23/2010 1826

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7044.d

30.10 g

20 mL

1 uL

3546

MSN


160000 U 160000780002,4-Dinitrophenol




31000 U 3100015000Dinoseb

31000 U 31000110001,4-Dioxane




31000 U * 310002700Famphur


31000 U 310003400Fluorene





16000000 U * 160000001200000Hexachlorophene











31000 U 3100040003 & 4 Methylphenol





160000 U 16000042002-Nitroaniline

160000 U 16000043003-Nitroaniline

160000 U 16000046004-Nitroaniline



160000 U 160000310004-Nitrophenol










Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US


680-56861-23

Solid

Date Sampled: 04/16/2010 0930



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/20/2010 1628

04/23/2010 1826

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7044.d

30.10 g

20 mL

1 uL

3546

MSN












31000 U 310003200Phenol

31000 U 310002100Phorate

31000 U 3100016002-Picoline


31000 U 310002200Pronamide

5000 J 310002500Pyrene

31000 U 310002700Pyridine


31000 U 310001900Sulfotepp



31000 U 310002200Thionazin

31000 U 3100033002-Toluidine














Analytical Data


Client Sample ID:

Lab Sample ID:

RB-1

Client Matrix:

680-56861-28RB

Water

Date Sampled: 04/16/2010 1000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/21/2010 1423

04/25/2010 0023

1.0



Injection Volume:



Lab File ID:

Instrument ID:

g0754.d

1060 mL

1 mL

1 uL

3520C

MSG


9.4 U 9.40.72Acenaphthene

9.4 U 9.40.80Acenaphthylene

9.4 U 9.40.54Acetophenone

9.4 U 9.41.52-Acetylaminofluorene

1900 U * 190033alpha,alpha-Dimethyl phenethylamine

9.4 U 9.41.14-Aminobiphenyl

19 U 192.0Aniline

9.4 U 9.40.65Anthracene

9.4 U 9.40.86Aramite, Total

9.4 U 9.40.52Benzo[a]anthracene

9.4 U 9.40.67Benzo[a]pyrene

9.4 U 9.42.5Benzo[b]fluoranthene

9.4 U 9.40.82Benzo[g,h,i]perylene

9.4 U 9.41.1Benzo[k]fluoranthene

9.4 U 9.41.0Benzyl alcohol

9.4 U 9.40.551,1'-Biphenyl

9.4 U * 9.40.89Bis(2-chloroethoxy)methane

9.4 U 9.41.0Bis(2-chloroethyl)ether

9.4 U 9.40.74bis(chloroisopropyl) ether

9.4 U 9.41.5Bis(2-ethylhexyl) phthalate

9.4 U 9.40.734-Bromophenyl phenyl ether

9.4 U 9.41.1Butyl benzyl phthalate

19 U 192.14-Chloroaniline

9.4 U 9.40.944-Chloro-3-methylphenol

9.4 U 9.40.752-Chloronaphthalene

9.4 U 9.40.822-Chlorophenol

9.4 U 9.40.794-Chlorophenyl phenyl ether

9.4 U 9.40.48Chrysene

9.4 U 9.40.74Diallate

9.4 U 9.40.94Dibenz(a,h)anthracene

9.4 U 9.40.75Dibenzofuran

9.4 U 9.40.501,2-Dichlorobenzene




9.4 U 9.41.02,4-Dichlorophenol

9.4 U 9.40.692,6-Dichlorophenol

9.4 U 9.40.83Diethyl phthalate

9.4 U 9.40.71Dimethoate

9.4 U 9.41.17,12-Dimethylbenz(a)anthracene

19 U 199.43,3'-Dimethylbenzidine

9.4 U 9.43.82,4-Dimethylphenol

9.4 U 9.40.93Dimethyl phthalate

9.4 U 9.40.78Di-n-butyl phthalate

9.4 U 9.40.571,3-Dinitrobenzene

47 U 479.44,6-Dinitro-2-methylphenol


Analytical Data


Client Sample ID:

Lab Sample ID:

RB-1

Client Matrix:

680-56861-28RB

Water

Date Sampled: 04/16/2010 1000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/21/2010 1423

04/25/2010 0023

1.0



Injection Volume:



Lab File ID:

Instrument ID:

g0754.d

1060 mL

1 mL

1 uL

3520C

MSG


47 U 479.42,4-Dinitrophenol

9.4 U 9.41.12,4-Dinitrotoluene

9.4 U 9.41.02,6-Dinitrotoluene

9.4 U 9.41.3Di-n-octyl phthalate

9.4 U 9.44.7Dinoseb

9.4 U 9.43.21,4-Dioxane

9.4 U 9.40.75Disulfoton

9.4 U 9.40.91Ethyl methanesulfonate

9.4 U 9.41.2Ethyl Parathion

9.4 U * 9.41.0Famphur

9.4 U 9.40.70Fluoranthene

9.4 U 9.40.91Fluorene

9.4 U 9.40.75Hexachlorobenzene

9.4 U 9.40.58Hexachlorobutadiene

9.4 U 9.42.4Hexachlorocyclopentadiene

9.4 U 9.40.72Hexachloroethane


9.4 U * 9.41.3Hexachloropropene

9.4 U 9.40.94Indeno[1,2,3-cd]pyrene

9.4 U 9.40.85Isophorone

9.4 U 9.40.47Isosafrole

1900 U * 19002.5Methapyrilene

9.4 U 9.41.33-Methylcholanthrene

9.4 U * 9.40.57Methyl methanesulfonate

9.4 U 9.40.742-Methylnaphthalene

9.4 U 9.40.83Methyl parathion

9.4 U 9.40.842-Methylphenol

9.4 U 9.41.23 & 4 Methylphenol

9.4 U 9.40.66Naphthalene

9.4 U * 9.40.581,4-Naphthoquinone

9.4 U * 9.41.01-Naphthylamine

9.4 U 9.41.42-Naphthylamine

47 U 471.22-Nitroaniline



9.4 U 9.40.69Nitrobenzene

9.4 U 9.40.722-Nitrophenol

47 U 471.84-Nitrophenol

19 U 199.44-Nitroquinoline-1-oxide

9.4 U 9.41.4N-Nitro-o-toluidine

9.4 U 9.40.88N-Nitrosodiethylamine

9.4 U 9.42.6N-Nitrosodimethylamine

9.4 U * 9.40.91N-Nitrosodi-n-butylamine

9.4 U 9.40.68N-Nitrosodi-n-propylamine

9.4 U 9.40.87N-Nitrosodiphenylamine

9.4 U 9.43.1N-Nitrosomethylethylamine


Analytical Data


Client Sample ID:

Lab Sample ID:

RB-1

Client Matrix:

680-56861-28RB

Water

Date Sampled: 04/16/2010 1000



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/21/2010 1423

04/25/2010 0023

1.0



Injection Volume:



Lab File ID:

Instrument ID:

g0754.d

1060 mL

1 mL

1 uL

3520C

MSG


9.4 U 9.40.79N-Nitrosomorpholine

9.4 U 9.40.83N-Nitrosopiperidine

9.4 U 9.40.94N-Nitrosopyrrolidine

9.4 U * 9.40.94o,o',o''-Triethylphosphorothioate

9.4 U 9.40.75p-Dimethylamino azobenzene

9.4 U 9.40.49Pentachlorobenzene

9.4 U 9.40.74Pentachloronitrobenzene

47 U 471.9Pentachlorophenol

9.4 U 9.41.3Phenacetin

9.4 U 9.40.73Phenanthrene

9.4 U 9.40.78Phenol

9.4 U 9.40.82Phorate

9.4 U 9.41.32-Picoline

1900 U 19009.4p-Phenylene diamine

9.4 U 9.40.84Pronamide

9.4 U 9.40.59Pyrene

47 U 472.2Pyridine

9.4 U 9.40.75Safrole, Total

9.4 U 9.40.50Sulfotepp

9.4 U 9.40.721,2,4,5-Tetrachlorobenzene

9.4 U 9.40.682,3,4,6-Tetrachlorophenol

9.4 U 9.40.86Thionazin

9.4 U 9.41.32-Toluidine

9.4 U 9.40.531,2,4-Trichlorobenzene

9.4 U 9.41.12,4,5-Trichlorophenol

9.4 U 9.40.802,4,6-Trichlorophenol

9.4 U 9.41.91,3,5-Trinitrobenzene


96 40 - 1392,4,6-Tribromophenol

78 50 - 1132-Fluorobiphenyl

73 36 - 1102-Fluorophenol

101 10 - 121Terphenyl-d14

77 38 - 116Phenol-d5

83 45 - 112Nitrobenzene-d5


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS


680-56861-1

Solid

Date Sampled: 04/14/2010 0950


6010B Metals (ICP)

Method: 6010B Analysis Batch: 680-166538 Instrument ID:

Preparation: Prep Batch: 680-166337 Lab File ID: N/A

Dilution: 1.0 Initial Weight/Volume: 1.10 g

Date Analyzed: 04/23/2010 0555 Final Weight/Volume: 100 mL

Date Prepared: 04/21/2010 1618

3050B

ICPD

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

1.5 J 3.91.2Arsenic

37 1.90.58Barium

0.24 J 0.970.19Cadmium

13 1.90.97Chromium

120 1.91.0Lead

4.9 U 4.91.9Selenium

0.30 J 1.90.19Silver

7471A Mercury (CVAA)

Method: 7471A Analysis Batch: 680-167080 Instrument ID:


Dilution: 10 Initial Weight/Volume: 0.60 g



7471A

LEEMAN1


3.8 0.360.15Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-NS


680-56861-2

Solid

Date Sampled: 04/14/2010 1245


6010B Metals (ICP)






3050B

ICPD


2.1 U 2.10.62Arsenic

4.0 1.10.32Barium

0.53 U 0.530.11Cadmium

1.6 1.10.53Chromium

2.9 1.10.56Lead


1.1 U 1.10.10Silver







7471A

LEEMAN1


0.012 J 0.0240.0098Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255


6010B Metals (ICP)






3050B

ICPD


2.5 J 3.61.1Arsenic

22 1.80.55Barium

0.27 J 0.910.18Cadmium

16 1.80.91Chromium

41 1.80.96Lead


0.62 J B 1.80.17Silver







7471A

LEEMAN1


0.66 0.0370.015Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-NS


680-56861-4

Solid

Date Sampled: 04/14/2010 1715


6010B Metals (ICP)






3050B

ICPD



3.5 1.00.31Barium

0.51 U 0.510.10Cadmium

1.5 1.00.51Chromium

0.95 J 1.00.54Lead


0.10 J B 1.00.098Silver







7471A

LEEMAN1


0.020 U 0.0200.0081Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735


6010B Metals (ICP)






3050B

ICPD


2.1 J 4.71.4Arsenic

16 2.30.70Barium

0.40 J 1.20.23Cadmium

13 2.31.2Chromium

59 2.31.2Lead


0.41 J B 2.30.22Silver







7471A

LEEMAN1


0.26 0.0470.019Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US


680-56861-6

Solid

Date Sampled: 04/15/2010 0845


6010B Metals (ICP)






3050B

ICPD


2.8 J 7.72.3Arsenic

13 3.81.2Barium

0.38 J 1.90.38Cadmium

11 3.81.9Chromium

40 3.82.0Lead


3.8 U 3.80.37Silver







7471A

LEEMAN1


0.24 0.0790.032Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-NS


680-56861-7

Solid

Date Sampled: 04/15/2010 0950


6010B Metals (ICP)






3050B

ICPD


2.0 J 2.40.70Arsenic

120 1.20.35Barium

0.18 J 0.590.12Cadmium

18 1.20.59Chromium

12 1.20.63Lead


0.15 J B 1.20.11Silver







7471A

LEEMAN1


0.024 U 0.0240.010Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005


6010B Metals (ICP)






3050B

ICPD


2.5 J 5.31.6Arsenic

23 2.60.79Barium

0.55 J 1.30.26Cadmium

24 2.61.3Chromium

75 2.61.4Lead


0.42 J B 2.60.25Silver







7471A

LEEMAN1


0.40 0.0530.022Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US


680-56861-9

Solid

Date Sampled: 04/15/2010 1100


6010B Metals (ICP)






3050B

ICPD


3.3 J 8.32.4Arsenic

27 4.11.2Barium

0.77 J 2.10.41Cadmium

23 4.12.1Chromium

49 4.12.2Lead

10 U 104.1Selenium

0.42 J B 4.10.40Silver







7471A

LEEMAN1


1.1 0.0760.031Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-NS


680-56861-10

Solid

Date Sampled: 04/15/2010 1105


6010B Metals (ICP)






3050B

ICPD



150 1.20.36Barium

0.59 U 0.590.12Cadmium

13 1.20.59Chromium

7.6 1.20.63Lead


1.2 U 1.20.11Silver







7471A

LEEMAN1


0.021 U 0.0210.0087Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS


680-56861-11

Solid

Date Sampled: 04/15/2010 1110


6010B Metals (ICP)






3050B

ICPD


1.3 J 4.31.3Arsenic

16 2.10.64Barium

0.31 J 1.10.21Cadmium

17 2.11.1Chromium

51 2.11.1Lead


0.53 J B 2.10.21Silver







7471A

LEEMAN1


0.43 0.0480.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US


680-56861-12

Solid

Date Sampled: 04/15/2010 1145


6010B Metals (ICP)






3050B

ICPD


3.6 J 103.1Arsenic

18 5.21.6Barium

0.52 J 2.60.52Cadmium

27 5.22.6Chromium

28 5.22.8Lead

13 U 135.2Selenium

5.2 U 5.20.50Silver







7471A

LEEMAN1


0.25 0.110.043Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US


680-56861-13

Solid

Date Sampled: 04/15/2010 1415


6010B Metals (ICP)






3050B

ICPD


3.4 J 113.2Arsenic

18 5.41.6Barium

0.61 J 2.70.54Cadmium

15 5.42.7Chromium

43 5.42.9Lead

14 U 145.4Selenium

0.52 J B 5.40.52Silver







7471A

LEEMAN1


0.33 0.0970.040Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-NS


680-56861-14

Solid

Date Sampled: 04/15/2010 1505


6010B Metals (ICP)






3050B

ICPD



18 1.00.31Barium

0.52 U 0.520.10Cadmium

7.3 1.00.52Chromium

2.6 1.00.55Lead


1.0 U 1.00.10Silver







7471A

LEEMAN1


0.023 U 0.0230.0093Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS


680-56861-15

Solid

Date Sampled: 04/15/2010 1520


6010B Metals (ICP)






3050B

ICPD


3.1 J 6.01.8Arsenic

18 3.00.91Barium

0.47 J 1.50.30Cadmium

31 3.01.5Chromium

27 3.01.6Lead


0.30 J 3.00.29Silver







7471A

LEEMAN1


0.52 0.0610.025Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US


680-56861-16

Solid

Date Sampled: 04/15/2010 1525


6010B Metals (ICP)






3050B

ICPD


2.6 J 7.12.1Arsenic

12 3.61.1Barium

0.48 J 1.80.36Cadmium

24 3.61.8Chromium

32 3.61.9Lead


3.6 U 3.60.34Silver







7471A

LEEMAN1


0.59 0.0690.028Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-NS


680-56861-17

Solid

Date Sampled: 04/15/2010 1600


6010B Metals (ICP)






3050B

ICPD



120 1.20.37Barium

0.61 U 0.610.12Cadmium

15 1.20.61Chromium

13 1.20.65Lead


1.2 U 1.20.12Silver







7471A

LEEMAN1


0.022 U 0.0220.0091Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS


680-56861-18

Solid

Date Sampled: 04/15/2010 1615


6010B Metals (ICP)






3050B

ICPD


3.3 J 7.82.3Arsenic

37 3.91.2Barium

0.67 J 2.00.39Cadmium

54 3.92.0Chromium

100 3.92.1Lead


0.51 J 3.90.38Silver







7471A

LEEMAN1


0.86 0.0640.026Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US


680-56861-19

Solid

Date Sampled: 04/15/2010 1620


6010B Metals (ICP)






3050B

ICPD


14 U 144.3Arsenic

15 7.22.2Barium

3.6 U 3.60.72Cadmium

23 7.23.6Chromium

38 7.23.8Lead

18 U 187.2Selenium

7.2 U 7.20.69Silver







7471A

LEEMAN1


0.48 0.130.054Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US


680-56861-20

Solid

Date Sampled: 04/15/2010 1700


6010B Metals (ICP)






3050B

ICPD


3.0 J 4.71.4Arsenic

28 2.30.70Barium

0.33 J 1.20.23Cadmium

22 2.31.2Chromium

24 2.31.2Lead


0.24 J 2.30.22Silver







7471A

LEEMAN1


0.72 0.0480.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-NS


680-56861-21

Solid

Date Sampled: 04/16/2010 0840


6010B Metals (ICP)






3050B

ICPD



4.2 1.10.32Barium

0.53 U 0.530.11Cadmium

1.1 U 1.10.53Chromium

1.7 1.10.56Lead


1.1 U 1.10.10Silver







7471A

LEEMAN1


0.012 J 0.0210.0086Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS


680-56861-22

Solid

Date Sampled: 04/16/2010 0850


6010B Metals (ICP)






3050B

ICPD


3.4 J 5.31.6Arsenic

39 2.70.80Barium

0.46 J 1.30.27Cadmium

23 2.71.3Chromium

41 2.71.4Lead


0.88 J 2.70.26Silver







7471A

LEEMAN1


1.1 0.0590.024Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US


680-56861-23

Solid

Date Sampled: 04/16/2010 0930


6010B Metals (ICP)






3050B

ICPD


2.5 J 8.42.5Arsenic

23 4.21.3Barium

0.51 J 2.10.42Cadmium

19 4.22.1Chromium

36 4.22.2Lead

10 U 104.2Selenium

4.2 U 4.20.40Silver







7471A

LEEMAN1


1.1 0.0840.034Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

RB-1

Client Matrix:

680-56861-28RB

Water

Date Sampled: 04/16/2010 1000


6010B Metals (ICP)



Dilution: 1.0 Initial Weight/Volume: 50 mL



3010A

ICPD


20 U 204.6Arsenic

2.8 J 102.3Barium

5.0 U 5.02.0Cadmium

10 U 101.2Chromium

10 U 104.0Lead

20 U 206.4Selenium

10 U 100.89Silver




Dilution: 1.0 Initial Weight/Volume: 50 mL



7470A

LEEMAN1


0.20 U 0.200.091Mercury


DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

GC/MS VOA

Indicates the analyte was analyzed for but not detected.U

LCS or LCSD exceeds the control limits*

Result is less than the RL but greater than or equal to the MDL

and the concentration is an approximate value.

J

Surrogate is outside control limitsX

Surrogate or matrix spike recoveries were not obtained

because the extract was diluted for analysis; also compounds

analyzed at a dilution may be flagged with a D.

D

GC/MS Semi VOA


LCS or LCSD exceeds the control limits*

MS or MSD exceeds the control limitsF

MS, MSD: The analyte present in the original sample is 4 times

greater than the matrix spike concentration; therefore, control

limits are not applicable.

4

Result exceeded calibration range.E



J

RPD of the LCS and LCSD exceeds the control limits*

Surrogate or matrix spike recoveries were not obtained

because the extract was diluted for analysis; also compounds

analyzed at a dilution may be flagged with a D.

D

Metals

Compound was found in the blank and sample.B




J


Page 167 of 238

QUALITY CONTROL RESULTS


Page 168 of 238

Quality Control Results


QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

GC/MS VOA


SolidIBS-1-LS 5035680-56861-1 T

SolidIBS-3-NS 5035680-56861-2 T

SolidIBS-3-LS 5035680-56861-3 T

SolidIBS-4-NS 5035680-56861-4 T

SolidIBS-4-LS 5035680-56861-5 T

SolidIBS-3-US 5035680-56861-6 T

SolidIBS-5-LS 5035680-56861-8 T

SolidIBS-4-US 5035680-56861-9 T

SolidIBS-6-NS 5035680-56861-10 T

SolidIBS-6-LS 5035680-56861-11 T

SolidIBS-5-US 5035680-56861-12 T

SolidIBS-6-US 5035680-56861-13 T

SolidIBS-7-NS 5035680-56861-14 T

SolidIBS-7-LS 5035680-56861-15 T

SolidIBS-7-US 5035680-56861-16 T

SolidIBS-8-NS 5035680-56861-17 T

SolidIBS-8-LS 5035680-56861-18 T

SolidIBS-8-US 5035680-56861-19 T

SolidIBS-1-US 5035680-56861-20 T

SolidIBS-2-NS 5035680-56861-21 T

SolidIBS-2-LS 5035680-56861-22 T

SolidIBS-2-US 5035680-56861-23 T

Analysis Batch:680-166185

Lab Control Sample Water 8260BLCS 680-166185/6 T

Lab Control Sample Duplicate Water 8260BLCSD 680-166185/7 T

Method Blank Water 8260BMB 680-166185/9 T

WaterFB-1 8260B680-56861-24FB T

WaterFB-2 8260B680-56861-25FB T

WaterTB-1 8260B680-56861-26TB T

WaterTB-2 8260B680-56861-27TB T

WaterRB-1 8260B680-56861-28RB T


Lab Control Sample Solid 8260BLCS 680-166615/6 T

Lab Control Sample Duplicate Solid 8260BLCSD 680-166615/7 T

Method Blank Solid 8260BMB 680-166615/8 T

Solid 680-166108IBS-4-US 8260B680-56861-9 T


Page 169 of 238





Report

Basis

GC/MS VOA





Solid 680-166108IBS-1-LS 8260B680-56861-1 T

Solid 680-166108IBS-3-NS 8260B680-56861-2 T

Solid 680-166108IBS-4-NS 8260B680-56861-4 T

Solid 680-166108IBS-3-US 8260B680-56861-6 T

SolidIBS-5-NS 8260B680-56861-7 T

Solid 680-166108IBS-6-NS 8260B680-56861-10 T

Solid 680-166108IBS-6-US 8260B680-56861-13 T

Solid 680-166108IBS-7-LS 8260B680-56861-15 T

Solid 680-166108IBS-7-US 8260B680-56861-16 T





Solid 680-166108IBS-5-LS 8260B680-56861-8 T

Solid 680-166108IBS-5-US 8260B680-56861-12 T

Solid 680-166108IBS-7-NS 8260B680-56861-14 T

Solid 680-166108IBS-8-US 8260B680-56861-19 T

Solid 680-166108IBS-1-US 8260B680-56861-20 T

Solid 680-166108IBS-2-NS 8260B680-56861-21 T

Solid 680-166108IBS-2-LS 8260B680-56861-22 T

Solid 680-166108IBS-2-US 8260B680-56861-23 T





Solid 680-166108IBS-3-LS 8260B680-56861-3 T

Solid 680-166108IBS-4-LS 8260B680-56861-5 T

Solid 680-166108IBS-6-LS 8260B680-56861-11 T

Solid 680-166108IBS-8-NS 8260B680-56861-17 T

Solid 680-166108IBS-8-LS 8260B680-56861-18 T

Report Basis

T = Total


Page 170 of 238





Report

Basis

GC/MS Semi VOA


Lab Control Sample Solid 3546LCS 680-166138/12-A T

SolidIBS-2-NS 3546680-56861-21 T

Matrix Spike Solid 3546680-56861-21MS T

Matrix Spike Duplicate Solid 3546680-56861-21MSD T

SolidIBS-2-LS 3546680-56861-22 T

SolidIBS-2-US 3546680-56861-23 T


Lab Control Sample Solid 3546LCS 680-166147/22-A T

Method Blank Solid 3546MB 680-166147/21-A T

SolidIBS-1-LS 3546680-56861-1 T

SolidIBS-3-NS 3546680-56861-2 T

SolidIBS-3-LS 3546680-56861-3 T

SolidIBS-4-NS 3546680-56861-4 T

SolidIBS-4-LS 3546680-56861-5 T

SolidIBS-3-US 3546680-56861-6 T

SolidIBS-5-NS 3546680-56861-7 T

SolidIBS-5-LS 3546680-56861-8 T

SolidIBS-4-US 3546680-56861-9 T

SolidIBS-6-NS 3546680-56861-10 T

SolidIBS-6-LS 3546680-56861-11 T

SolidIBS-5-US 3546680-56861-12 T

SolidIBS-6-US 3546680-56861-13 T

SolidIBS-7-NS 3546680-56861-14 T

SolidIBS-7-LS 3546680-56861-15 T

SolidIBS-7-US 3546680-56861-16 T

SolidIBS-8-NS 3546680-56861-17 T

SolidIBS-8-LS 3546680-56861-18 T

SolidIBS-8-US 3546680-56861-19 T

SolidIBS-1-US 3546680-56861-20 T


Lab Control Sample Water 3520CLCS 680-166243/8-A T

Lab Control Sample Duplicate Water 3520CLCSD 680-166243/9-A T

Method Blank Water 3520CMB 680-166243/7-A T

WaterRB-1 3520C680-56861-28RB T


Lab Control Sample Solid 680-1661388270CLCS 680-166138/12-A T


Solid 680-166138IBS-2-US 8270C680-56861-23 T


Lab Control Sample Water 680-1662438270CLCS 680-166243/8-A T


Page 171 of 238





Report

Basis

GC/MS Semi VOA


Lab Control Sample Duplicate Water 680-1662438270CLCSD 680-166243/9-A T

Method Blank Water 680-1662438270CMB 680-166243/7-A T


Water 680-166243RB-1 8270C680-56861-28RB T


Lab Control Sample Solid 680-1661478270CLCS 680-166147/22-A T

Method Blank Solid 680-1661478270CMB 680-166147/21-A T

Solid 680-166147IBS-1-LS 8270C680-56861-1 T

Solid 680-166147IBS-3-NS 8270C680-56861-2 T

Solid 680-166147IBS-3-LS 8270C680-56861-3 T

Solid 680-166147IBS-4-LS 8270C680-56861-5 T

Solid 680-166147IBS-3-US 8270C680-56861-6 T

Solid 680-166147IBS-5-NS 8270C680-56861-7 T

Solid 680-166147IBS-5-LS 8270C680-56861-8 T

Solid 680-166147IBS-4-US 8270C680-56861-9 T


Solid 680-166147IBS-4-NS 8270C680-56861-4 T

Solid 680-166147IBS-6-NS 8270C680-56861-10 T

Solid 680-166147IBS-6-LS 8270C680-56861-11 T

Solid 680-166147IBS-5-US 8270C680-56861-12 T

Solid 680-166147IBS-6-US 8270C680-56861-13 T

Solid 680-166147IBS-7-NS 8270C680-56861-14 T

Solid 680-166147IBS-7-LS 8270C680-56861-15 T

Solid 680-166147IBS-7-US 8270C680-56861-16 T

Solid 680-166147IBS-8-NS 8270C680-56861-17 T

Solid 680-166147IBS-8-LS 8270C680-56861-18 T

Solid 680-166147IBS-8-US 8270C680-56861-19 T

Solid 680-166147IBS-1-US 8270C680-56861-20 T

Solid 680-166138IBS-2-NS 8270C680-56861-21 T

Matrix Spike Solid 680-1661388270C680-56861-21MS T

Matrix Spike Duplicate Solid 680-1661388270C680-56861-21MSD T

Solid 680-166138IBS-2-LS 8270C680-56861-22 T


Solid 680-166147IBS-1-LS 8270C680-56861-1 T

Solid 680-166147IBS-3-NS 8270C680-56861-2 T

Solid 680-166147IBS-3-LS 8270C680-56861-3 T

Solid 680-166147IBS-4-NS 8270C680-56861-4 T

Solid 680-166147IBS-4-LS 8270C680-56861-5 T

Solid 680-166147IBS-5-LS 8270C680-56861-8 T

Solid 680-166147IBS-6-NS 8270C680-56861-10 T


Page 172 of 238





Report

Basis

Report Basis

T = Total


Page 173 of 238





Report

Basis

Metals


Lab Control Sample Water 7470ALCS 680-166266/7-B T

Method Blank Water 7470AMB 680-166266/6-B T

WaterRB-1 7470A680-56861-28RB T

Matrix Spike Water 7470A680-56861-28MS T

Matrix Spike Duplicate Water 7470A680-56861-28MSD T


Lab Control Sample Water 3010ALCS 680-166297/19-A T

Method Blank Water 3010AMB 680-166297/18-A T

WaterRB-1 3010A680-56861-28RB T


Lab Control Sample Water 680-1662976010BLCS 680-166297/19-A T

Method Blank Water 680-1662976010BMB 680-166297/18-A T

Water 680-166297RB-1 6010B680-56861-28RB T


Lab Control Sample Solid 3050BLCS 680-166337/24-A T

Method Blank Solid 3050BMB 680-166337/23-A T

SolidIBS-1-LS 3050B680-56861-1 T

SolidIBS-3-NS 3050B680-56861-2 T


Lab Control Sample Water 680-1662687470ALCS 680-166266/7-B T

Method Blank Water 680-1662687470AMB 680-166266/6-B T

Water 680-166268RB-1 7470A680-56861-28RB T

Matrix Spike Water 680-1662687470A680-56861-28MS T

Matrix Spike Duplicate Water 680-1662687470A680-56861-28MSD T


Page 174 of 238





Report

Basis

Metals




SolidIBS-3-LS 3050B680-56861-3 T

SolidIBS-4-NS 3050B680-56861-4 T

SolidIBS-4-LS 3050B680-56861-5 T

SolidIBS-3-US 3050B680-56861-6 T

SolidIBS-5-NS 3050B680-56861-7 T

SolidIBS-5-LS 3050B680-56861-8 T

SolidIBS-4-US 3050B680-56861-9 T

SolidIBS-6-NS 3050B680-56861-10 T

SolidIBS-6-LS 3050B680-56861-11 T

SolidIBS-5-US 3050B680-56861-12 T

SolidIBS-6-US 3050B680-56861-13 T

SolidIBS-7-NS 3050B680-56861-14 T

Matrix Spike Solid 3050B680-56861-14MS T

Matrix Spike Duplicate Solid 3050B680-56861-14MSD T


Lab Control Sample Solid 7471ALCS 680-166534/24-A T

Method Blank Solid 7471AMB 680-166534/23-A T

SolidIBS-3-LS 7471A680-56861-3 T

SolidIBS-4-NS 7471A680-56861-4 T

SolidIBS-4-LS 7471A680-56861-5 T

SolidIBS-3-US 7471A680-56861-6 T

SolidIBS-5-NS 7471A680-56861-7 T

SolidIBS-5-LS 7471A680-56861-8 T

SolidIBS-4-US 7471A680-56861-9 T

SolidIBS-6-NS 7471A680-56861-10 T

SolidIBS-6-LS 7471A680-56861-11 T

SolidIBS-5-US 7471A680-56861-12 T

SolidIBS-6-US 7471A680-56861-13 T

SolidIBS-7-NS 7471A680-56861-14 T

Matrix Spike Solid 7471A680-56861-14MS T

Matrix Spike Duplicate Solid 7471A680-56861-14MSD T


Lab Control Sample Solid 680-1663376010BLCS 680-166337/24-A T

Method Blank Solid 680-1663376010BMB 680-166337/23-A T

Solid 680-166337IBS-1-LS 6010B680-56861-1 T

Solid 680-166337IBS-3-NS 6010B680-56861-2 T


Page 175 of 238





Report

Basis

Metals


Lab Control Sample Solid 7471ALCS 680-166757/20-A T

Method Blank Solid 7471AMB 680-166757/19-A T

SolidIBS-1-LS 7471A680-56861-1 T

SolidIBS-3-NS 7471A680-56861-2 T

SolidIBS-7-LS 7471A680-56861-15 T

SolidIBS-7-US 7471A680-56861-16 T

SolidIBS-8-NS 7471A680-56861-17 T

SolidIBS-8-LS 7471A680-56861-18 T

SolidIBS-8-US 7471A680-56861-19 T

SolidIBS-1-US 7471A680-56861-20 T

SolidIBS-2-NS 7471A680-56861-21 T

SolidIBS-2-LS 7471A680-56861-22 T

SolidIBS-2-US 7471A680-56861-23 T

Matrix Spike Solid 7471A680-56861-23MS T

Matrix Spike Duplicate Solid 7471A680-56861-23MSD T




SolidIBS-7-LS 3050B680-56861-15 T

SolidIBS-7-US 3050B680-56861-16 T

SolidIBS-8-NS 3050B680-56861-17 T

SolidIBS-8-LS 3050B680-56861-18 T

SolidIBS-8-US 3050B680-56861-19 T

SolidIBS-1-US 3050B680-56861-20 T

SolidIBS-2-NS 3050B680-56861-21 T

SolidIBS-2-LS 3050B680-56861-22 T

SolidIBS-2-US 3050B680-56861-23 T


Page 176 of 238





Report

Basis

Metals




Solid 680-166528IBS-3-LS 6010B680-56861-3 T

Solid 680-166528IBS-4-NS 6010B680-56861-4 T

Solid 680-166528IBS-4-LS 6010B680-56861-5 T

Solid 680-166528IBS-3-US 6010B680-56861-6 T

Solid 680-166528IBS-5-NS 6010B680-56861-7 T

Solid 680-166528IBS-5-LS 6010B680-56861-8 T

Solid 680-166528IBS-4-US 6010B680-56861-9 T

Solid 680-166528IBS-6-NS 6010B680-56861-10 T

Solid 680-166528IBS-6-LS 6010B680-56861-11 T

Solid 680-166528IBS-5-US 6010B680-56861-12 T

Solid 680-166528IBS-6-US 6010B680-56861-13 T

Solid 680-166528IBS-7-NS 6010B680-56861-14 T

Matrix Spike Solid 680-1665286010B680-56861-14MS T

Matrix Spike Duplicate Solid 680-1665286010B680-56861-14MSD T


Lab Control Sample Solid 680-1665347471ALCS 680-166534/24-A T

Method Blank Solid 680-1665347471AMB 680-166534/23-A T

Solid 680-166534IBS-3-LS 7471A680-56861-3 T

Solid 680-166534IBS-4-NS 7471A680-56861-4 T

Solid 680-166534IBS-4-LS 7471A680-56861-5 T

Solid 680-166534IBS-3-US 7471A680-56861-6 T

Solid 680-166534IBS-5-NS 7471A680-56861-7 T

Solid 680-166534IBS-5-LS 7471A680-56861-8 T

Solid 680-166534IBS-4-US 7471A680-56861-9 T

Solid 680-166534IBS-6-NS 7471A680-56861-10 T

Solid 680-166534IBS-6-LS 7471A680-56861-11 T

Solid 680-166534IBS-5-US 7471A680-56861-12 T

Solid 680-166534IBS-6-US 7471A680-56861-13 T

Solid 680-166534IBS-7-NS 7471A680-56861-14 T

Matrix Spike Solid 680-1665347471A680-56861-14MS T

Matrix Spike Duplicate Solid 680-1665347471A680-56861-14MSD T


Page 177 of 238





Report

Basis

Metals


Lab Control Sample Solid 680-1667577471ALCS 680-166757/20-A T

Method Blank Solid 680-1667577471AMB 680-166757/19-A T

Solid 680-166757IBS-1-LS 7471A680-56861-1 T

Solid 680-166757IBS-3-NS 7471A680-56861-2 T

Solid 680-166757IBS-7-LS 7471A680-56861-15 T

Solid 680-166757IBS-7-US 7471A680-56861-16 T

Solid 680-166757IBS-8-NS 7471A680-56861-17 T

Solid 680-166757IBS-8-LS 7471A680-56861-18 T

Solid 680-166757IBS-8-US 7471A680-56861-19 T

Solid 680-166757IBS-1-US 7471A680-56861-20 T

Solid 680-166757IBS-2-NS 7471A680-56861-21 T

Solid 680-166757IBS-2-LS 7471A680-56861-22 T

Solid 680-166757IBS-2-US 7471A680-56861-23 T

Matrix Spike Solid 680-1667577471A680-56861-23MS T

Matrix Spike Duplicate Solid 680-1667577471A680-56861-23MSD T




Solid 680-166825IBS-7-LS 6010B680-56861-15 T

Solid 680-166825IBS-7-US 6010B680-56861-16 T

Solid 680-166825IBS-8-NS 6010B680-56861-17 T

Solid 680-166825IBS-8-LS 6010B680-56861-18 T

Solid 680-166825IBS-8-US 6010B680-56861-19 T

Solid 680-166825IBS-1-US 6010B680-56861-20 T

Solid 680-166825IBS-2-NS 6010B680-56861-21 T

Solid 680-166825IBS-2-LS 6010B680-56861-22 T

Solid 680-166825IBS-2-US 6010B680-56861-23 T

Report Basis

T = Total


Page 178 of 238



Surrogate Recovery Report


Client Matrix: Solid

Lab Sample ID Client Sample ID

BFB DBFM TOL

%Rec %Rec %Rec

680-56861-1 IBS-1-LS 0D 0D 0D

680-56861-2 IBS-3-NS 0D 0D 0D

680-56861-3 IBS-3-LS 0D 0D 0D

680-56861-4 IBS-4-NS 0D 0D 0D

680-56861-5 IBS-4-LS 0D 0D 0D

680-56861-6 IBS-3-US 0D 0D 0D

680-56861-7 IBS-5-NS 75 56X 66

680-56861-8 IBS-5-LS 0D 0D 0D

680-56861-9 IBS-4-US 0D 0D 0D

680-56861-10 IBS-6-NS 0D 0D 0D

680-56861-11 IBS-6-LS 0D 0D 0D

680-56861-12 IBS-5-US 0D 0D 0D

680-56861-13 IBS-6-US 0D 0D 0D

680-56861-14 IBS-7-NS 0D 0D 0D

680-56861-15 IBS-7-LS 0D 0D 0D

680-56861-16 IBS-7-US 0D 0D 0D

680-56861-17 IBS-8-NS 96 77 75

680-56861-18 IBS-8-LS 0D 0D 0D

680-56861-19 IBS-8-US 0D 0D 0D

680-56861-20 IBS-1-US 0D 0D 0D

680-56861-21 IBS-2-NS 0D 0D 0D

680-56861-22 IBS-2-LS 0D 0D 0D

680-56861-23 IBS-2-US 0D 0D 0D

MB 680-166615/8 104 92 100

MB 680-166686/8 113 93 108

MB 680-166737/8 122 97 122

MB 680-166861/9 121 103 112

LCS 680-166615/6 101 96 98

LCS 680-166686/6 91 79 88

Surrogate Acceptance Limits

BFB = 4-Bromofluorobenzene 65-124

DBFM = Dibromofluoromethane 65-124

TOL = Toluene-d8 (Surr) 65-132


Page 179 of 238







BFB DBFM TOL

%Rec %Rec %Rec

LCS 680-166737/6 103 78 95

LCS 680-166861/7 113 104 103

LCSD 680-166615/7 94 85 94

LCSD 680-166686/7 94 80 92

LCSD 680-166737/7 103 80 94

LCSD 680-166861/8 106 92 93






Page 180 of 238





Client Matrix: Water


BFB DBFM TOL

%Rec %Rec %Rec

680-56861-24 FB-1 100 91 103

680-56861-25 FB-2 99 93 100

680-56861-26 TB-1 99 90 102

680-56861-27 TB-2 98 93 102

680-56861-28 RB-1 94 92 103

MB 680-166185/9 100 100 105

LCS 680-166185/6 99 99 111

LCSD 680-166185/7 99 102 107






Page 181 of 238







TBP FBP 2FP TPH PHL NBZ

%Rec %Rec %Rec %Rec %Rec %Rec

680-56861-1 IBS-1-LS 0D 0D 0D 0D 0D 0D

680-56861-1 IBS-1-LS 0D 0D 0D 0D 0D 0D

680-56861-2 IBS-3-NS 0D 0D 0D 0D 0D 0D

680-56861-2 IBS-3-NS 0D 0D 0D 0D 0D 0D

680-56861-3 IBS-3-LS 0D 0D 0D 0D 0D 0D

680-56861-3 IBS-3-LS 0D 0D 0D 0D 0D 0D

680-56861-4 IBS-4-NS 0D 0D 0D 0D 0D 0D

680-56861-4 IBS-4-NS 0D 0D 0D 0D 0D 0D

680-56861-5 IBS-4-LS 0D 0D 0D 0D 0D 0D

680-56861-5 IBS-4-LS 0D 0D 0D 0D 0D 0D

680-56861-6 IBS-3-US 0D 0D 0D 0D 0D 0D

680-56861-7 IBS-5-NS 0D 0D 0D 0D 0D 0D

680-56861-8 IBS-5-LS 0D 0D 0D 0D 0D 0D

680-56861-8 IBS-5-LS 0D 0D 0D 0D 0D 0D

680-56861-9 IBS-4-US 0D 0D 0D 0D 0D 0D

680-56861-10 IBS-6-NS 0D 0D 0D 0D 0D 0D

680-56861-10 IBS-6-NS 0D 0D 0D 0D 0D 0D

680-56861-11 IBS-6-LS 0D 0D 0D 0D 0D 0D

680-56861-12 IBS-5-US 0D 0D 0D 0D 0D 0D

680-56861-13 IBS-6-US 0D 0D 0D 0D 0D 0D

680-56861-14 IBS-7-NS 0D 0D 0D 0D 0D 0D

680-56861-15 IBS-7-LS 0D 0D 0D 0D 0D 0D

680-56861-16 IBS-7-US 0D 0D 0D 0D 0D 0D

680-56861-17 IBS-8-NS 0D 0D 0D 0D 0D 0D

680-56861-18 IBS-8-LS 0D 0D 0D 0D 0D 0D

680-56861-19 IBS-8-US 0D 0D 0D 0D 0D 0D

680-56861-20 IBS-1-US 0D 0D 0D 0D 0D 0D

680-56861-21 IBS-2-NS 0D 0D 0D 0D 0D 0D

680-56861-22 IBS-2-LS 0D 0D 0D 0D 0D 0D


TBP = 2,4,6-Tribromophenol 34-130

FBP = 2-Fluorobiphenyl 34-130

2FP = 2-Fluorophenol 30-130

TPH = Terphenyl-d14 39-130

PHL = Phenol-d5 30-130

NBZ = Nitrobenzene-d5 27-130


Page 182 of 238









680-56861-23 IBS-2-US 0D 0D 0D 0D 0D 0D

MB 680-166147/21-A 94 81 76 99 81 78

LCS 680-166138/12-A 80 60 57 69 62 60

LCS 680-166147/22-A 101 82 70 95 79 74

680-56861-21 MS IBS-2-NS MS 0D 0D 0D 0D 0D 0D

680-56861-21 MSD IBS-2-NS MSD 0D 0D 0D 0D 0D 0D









Page 183 of 238









680-56861-28 RB-1 96 78 73 101 77 83

MB 680-166243/7-A 102 88 75 103 82 90

LCS 680-166243/8-A 110 95 80 103 87 92

LCSD

680-166243/9-A

103 87 79 100 85 91









Page 184 of 238



WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/20/2010 1251

Method Blank - Batch: 680-166185

Date Prepared:

Instrument ID:

Lab File ID:



Analysis Batch: 680-166185

Prep Batch: N/A

04/20/2010 1251

pq093.d

5 mL

5 mL

Units: ug/L

Method: 8260B

Preparation: 5030B

MSPMB 680-166185/9

Analyte Result Qual MDL RL

25 U 255.0Acetone


20 U 207.4Acrolein






2.0 U 2.00.60Carbon disulfide






































WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/20/2010 1251


Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A

04/20/2010 1251

pq093.d

5 mL

5 mL

Units: ug/L

Method: 8260B

Preparation: 5030B

MSPMB 680-166185/9













Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 100 75 - 120

Dibromofluoromethane 100 75 - 121

Toluene-d8 (Surr) 105 75 - 120




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/20/2010 1041

04/20/2010 1111

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 680-166185

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/L

04/20/2010 1041

Prep Batch: N/A


pq085.d

5 mL

5 mL

pq087.d

5 mL

5 mL

ug/L

04/20/2010 1111


Prep Batch: N/A

Method: 8260B

Preparation: 5030B

MSP

MSP

LCS 680-166185/6

LCSD 680-166185/7

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

132128 17 - 175 3 50Acetone

106112 77 - 119 5 30Benzene

9392 62 - 133 1 30Bromoform

107138 12 - 184 26 50Bromomethane

110109 33 - 157 0 302-Butanone (MEK)

142137 55 - 131 4 30 * *Carbon disulfide

120128 71 - 135 6 30Carbon tetrachloride

102103 85 - 116 1 30Chlorobenzene

102104 75 - 133 2 30Chlorodibromomethane

12397 40 - 165 24 50Chloroethane

111108 82 - 120 3 30Chloroform

141133 48 - 142 6 50Chloromethane

116123 76 - 126 6 30cis-1,3-Dichloropropene

95100 49 - 140 5 301,2-Dibromo-3-Chloropropane

108116 78 - 119 7 30Dibromomethane

112119 78 - 127 6 30Dichlorobromomethane

151145 34 - 154 4 30Dichlorodifluoromethane

111107 74 - 127 4 301,1-Dichloroethane

114121 66 - 132 6 301,2-Dichloroethane

9995 62 - 141 4 301,1-Dichloroethene

114117 73 - 124 3 301,2-Dichloropropane

103107 86 - 116 3 30Ethylbenzene

101103 80 - 121 2 30Ethylene Dibromide

103109 34 - 161 5 302-Hexanone

112115 70 - 125 3 30Methylene Chloride

110120 40 - 151 9 304-Methyl-2-pentanone (MIBK)

99104 82 - 122 5 30Styrene

103107 81 - 128 3 301,1,1,2-Tetrachloroethane


101104 76 - 126 3 30Tetrachloroethene

106110 81 - 117 4 30Toluene

10198 72 - 131 3 30trans-1,2-Dichloroethene

115127 73 - 128 10 30trans-1,3-Dichloropropene




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/20/2010 1041

04/20/2010 1111

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/L

04/20/2010 1041

Prep Batch: N/A


pq085.d

5 mL

5 mL

pq087.d

5 mL

5 mL

ug/L

04/20/2010 1111


Prep Batch: N/A

Method: 8260B

Preparation: 5030B

MSP

MSP

LCS 680-166185/6

LCSD 680-166185/7


% Rec.

118127 76 - 127 8 301,1,1-Trichloroethane


100108 84 - 115 8 30Trichloroethene

133132 58 - 149 1 50Trichlorofluoromethane

9393 70 - 130 0 301,2,3-Trichloropropane

131129 10 - 217 1 30Vinyl acetate

113111 59 - 144 2 50Vinyl chloride

102107 84 - 118 4 30Xylenes, Total

Surrogate LCS % Rec LCSD % Rec Acceptance Limits

4-Bromofluorobenzene 99 99 75 - 120

Dibromofluoromethane 99 102 75 - 121

Toluene-d8 (Surr) 111 107 75 - 120




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/23/2010 1128


Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A mq219.d

5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166615/8


2000 U 2000440Acetone


4000 U 4000960Acrolein


200 U 20029Benzene

























1000 U 10001302-Hexanone









200 U 20037Styrene




200 U 20034Toluene




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/23/2010 1128


Date Prepared:

Instrument ID:

Lab File ID:





5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166615/8




















Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/23/2010 0954

04/23/2010 1018

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq216.d

5 g

5 mL

mq217.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166615/6

LCSD 680-166615/7


% Rec.

8492 16 - 202 9 50Acetone

9499 63 - 130 5 50Benzene

98102 66 - 127 4 50Bromoform

8594 54 - 146 10 50Bromomethane

8997 19 - 192 9 502-Butanone (MEK)

8698 46 - 134 13 50Carbon disulfide


9396 77 - 120 4 50Chlorobenzene


6184 26 - 166 32 50Chloroethane

8897 68 - 127 10 50Chloroform

101111 46 - 137 9 50Chloromethane






8897 65 - 130 10 501,1-Dichloroethane

9498 62 - 140 5 501,2-Dichloroethane

7183 59 - 137 15 501,1-Dichloroethene


96101 77 - 121 6 50Ethylbenzene


9298 47 - 151 6 502-Hexanone



97104 75 - 123 7 50Styrene




9398 67 - 132 6 50Toluene






Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/23/2010 0954

04/23/2010 1018

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq216.d

5 g

5 mL

mq217.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166615/6

LCSD 680-166615/7


% Rec.






8397 10 - 254 15 50Vinyl acetate

92102 56 - 139 10 50Vinyl chloride

9498 76 - 122 4 50Xylenes, Total




Toluene-d8 (Surr) 98 94 65 - 132




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/25/2010 1531


Date Prepared:

Instrument ID:

Lab File ID:





5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166686/8


2000 U 2000440Acetone




200 U 20029Benzene

























1000 U 10001302-Hexanone









200 U 20037Styrene




200 U 20034Toluene




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/25/2010 1531


Date Prepared:

Instrument ID:

Lab File ID:





5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166686/8




















Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/25/2010 1420

04/25/2010 1444

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq235.d

5 g

5 mL

mq236.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166686/6

LCSD 680-166686/7


% Rec.

7776 16 - 202 0 50Acetone

8784 63 - 130 3 50Benzene

9598 66 - 127 3 50Bromoform

8279 54 - 146 4 50Bromomethane

8087 19 - 192 8 502-Butanone (MEK)





6152 26 - 166 17 50Chloroethane

7979 68 - 127 0 50Chloroform

8251 46 - 137 47 50Chloromethane






7777 65 - 130 1 501,1-Dichloroethane

9695 62 - 140 1 501,2-Dichloroethane

8688 59 - 137 3 501,1-Dichloroethene


9491 77 - 121 2 50Ethylbenzene


9196 47 - 151 6 502-Hexanone



9493 75 - 123 1 50Styrene




9188 67 - 132 4 50Toluene






Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/25/2010 1420

04/25/2010 1444

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq235.d

5 g

5 mL

mq236.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166686/6

LCSD 680-166686/7


% Rec.






7880 10 - 254 3 50Vinyl acetate

7379 56 - 139 7 50Vinyl chloride

9187 76 - 122 4 50Xylenes, Total




Toluene-d8 (Surr) 88 92 65 - 132




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/26/2010 0946


Date Prepared:

Instrument ID:

Lab File ID:





5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166737/8


2000 U 2000440Acetone




200 U 20029Benzene

























1000 U 10001302-Hexanone









200 U 20037Styrene




200 U 20034Toluene




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/26/2010 0946


Date Prepared:

Instrument ID:

Lab File ID:





5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166737/8




















Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/26/2010 0835

04/26/2010 0859

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq241.d

5 g

5 mL

mq242.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166737/6

LCSD 680-166737/7


% Rec.

8598 16 - 202 14 50Acetone

8991 63 - 130 2 50Benzene

111119 66 - 127 7 50Bromoform

7766 54 - 146 15 50Bromomethane

9296 19 - 192 5 502-Butanone (MEK)





5856 26 - 166 2 50Chloroethane

8486 68 - 127 3 50Chloroform

7879 46 - 137 1 50Chloromethane






8082 65 - 130 2 501,1-Dichloroethane

99102 62 - 140 3 501,2-Dichloroethane

7877 59 - 137 1 501,1-Dichloroethene


101101 77 - 121 0 50Ethylbenzene


107112 47 - 151 5 502-Hexanone



104103 75 - 123 1 50Styrene




9495 67 - 132 1 50Toluene






Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/26/2010 0835

04/26/2010 0859

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq241.d

5 g

5 mL

mq242.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166737/6

LCSD 680-166737/7


% Rec.






7681 10 - 254 7 50Vinyl acetate

7069 56 - 139 1 50Vinyl chloride

9998 76 - 122 1 50Xylenes, Total




Toluene-d8 (Surr) 95 94 65 - 132




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/27/2010 0903


Date Prepared:

Instrument ID:

Lab File ID:





5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166861/9


2000 U 2000440Acetone




200 U 20029Benzene

























1000 U 10001302-Hexanone









200 U 20037Styrene




200 U 20034Toluene




SolidClient Matrix:

40Dilution:

Date Analyzed:

Lab Sample ID:

04/27/2010 0903


Date Prepared:

Instrument ID:

Lab File ID:





5 g

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

MSMMB 680-166861/9




















Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/27/2010 0753

04/27/2010 0816

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq259.d

5 g

5 mL

mq260.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166861/7

LCSD 680-166861/8


% Rec.

92105 16 - 202 14 50Acetone

96106 63 - 130 10 50Benzene

94103 66 - 127 9 50Bromoform

8193 54 - 146 14 50Bromomethane

95105 19 - 192 10 502-Butanone (MEK)





6465 26 - 166 2 50Chloroethane

95106 68 - 127 11 50Chloroform

102125 46 - 137 20 50Chloromethane






94107 65 - 130 12 501,1-Dichloroethane

8898 62 - 140 10 501,2-Dichloroethane

94112 59 - 137 18 501,1-Dichloroethene


95104 77 - 121 9 50Ethylbenzene


8491 47 - 151 8 502-Hexanone



9198 75 - 123 8 50Styrene




96105 67 - 132 9 50Toluene






Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/27/2010 0753

04/27/2010 0816

Lab Control Sample/


40

40

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

mq259.d

5 g

5 mL

mq260.d

5 g

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

MSM

MSM

LCS 680-166861/7

LCSD 680-166861/8


% Rec.






93107 10 - 254 15 50Vinyl acetate

103126 56 - 139 20 50Vinyl chloride

93102 76 - 122 8 50Xylenes, Total




Toluene-d8 (Surr) 103 93 65 - 132




Solid

1.0

04/22/2010 2329Date Analyzed:

Lab Control Sample - Batch: 680-166138

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

n7005.d

04/20/2010 1628



30.07 g

1 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSNLCS 680-166138/12-A

Analyte QualLimit% Rec.ResultSpike Amount

3330 2060 62 37 - 130Acenaphthene

3330 2130 64 37 - 130Acenaphthylene

3330 1560 47 22 - 130Acetophenone

3330 2720 82 10 - 1302-Acetylaminofluorene

16600 14700 88 J E10 - 130alpha,alpha-Dimethyl phenethylamine

3330 362 11 10 - 1304-Aminobiphenyl

3330 1570 47 13 - 130Aniline

3330 2340 70 39 - 130Anthracene

3330 2970 89 10 - 130Aramite, Total

3330 2400 72 40 - 130Benzo[a]anthracene

3330 2500 75 43 - 130Benzo[a]pyrene

3330 2450 74 35 - 130Benzo[b]fluoranthene

3330 2230 67 37 - 130Benzo[g,h,i]perylene

3330 2300 69 34 - 130Benzo[k]fluoranthene

3330 2040 61 25 - 130Benzyl alcohol

3330 2070 62 31 - 1301,1'-Biphenyl

3330 2750 83 30 - 130Bis(2-chloroethoxy)methane

3330 1980 60 16 - 130Bis(2-chloroethyl)ether

3330 2100 63 15 - 130bis(chloroisopropyl) ether

3330 2620 79 38 - 130Bis(2-ethylhexyl) phthalate

3330 2370 71 35 - 1304-Bromophenyl phenyl ether

3330 2800 84 41 - 130Butyl benzyl phthalate

3330 2000 60 23 - 1304-Chloroaniline

3330 2400 72 36 - 1304-Chloro-3-methylphenol

3330 2050 62 35 - 1302-Chloronaphthalene

3330 1990 60 32 - 1302-Chlorophenol

3330 2330 70 40 - 1304-Chlorophenyl phenyl ether

3330 2330 70 43 - 130Chrysene

3330 2410 72 10 - 130Diallate

3330 2350 71 36 - 130Dibenz(a,h)anthracene

3330 2120 64 38 - 130Dibenzofuran

3330 1710 51 27 - 1301,2-Dichlorobenzene



3330 2840 85 28 - 1303,3'-Dichlorobenzidine

3330 2150 65 35 - 1302,4-Dichlorophenol

3330 2170 65 10 - 1302,6-Dichlorophenol

3330 2420 73 42 - 130Diethyl phthalate

3330 2260 68 10 - 130Dimethoate

3330 2570 77 10 - 1307,12-Dimethylbenz(a)anthracene

3330 1700 15 U10 - 1303,3'-Dimethylbenzidine

6650 4250 64 31 - 1302,4-Dimethylphenol

3330 2360 71 43 - 130Dimethyl phthalate




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

n7005.d

04/20/2010 1628



30.07 g

1 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSNLCS 680-166138/12-A


3330 2630 79 39 - 130Di-n-butyl phthalate

3330 2660 80 10 - 1301,3-Dinitrobenzene

3330 2870 86 22 - 1304,6-Dinitro-2-methylphenol

3330 3190 96 10 - 1372,4-Dinitrophenol

3330 2610 79 36 - 1302,4-Dinitrotoluene

3330 2510 75 38 - 1302,6-Dinitrotoluene

3330 2550 77 37 - 130Di-n-octyl phthalate

3330 2760 83 10 - 130Dinoseb

3330 627 19 10 - 1301,4-Dioxane

3330 2710 82 10 - 130Disulfoton

3330 1800 54 10 - 130Ethyl methanesulfonate

3330 2990 90 10 - 130Ethyl Parathion

3330 205 6 J *10 - 130Famphur

3330 2370 71 40 - 130Fluoranthene

3330 2220 67 38 - 130Fluorene

3330 2170 65 40 - 130Hexachlorobenzene

3330 1940 58 29 - 130Hexachlorobutadiene

3330 1740 52 10 - 130Hexachlorocyclopentadiene

3330 1700 51 23 - 130Hexachloroethane

16600 170000 5 U *10 - 130Hexachlorophene

3330 330 0 U *10 - 130Hexachloropropene

3330 2430 73 34 - 130Indeno[1,2,3-cd]pyrene

3330 1940 58 30 - 130Isophorone

3330 2350 71 10 - 130Isosafrole

3330 3240 97 J10 - 130Methapyrilene

3330 1650 50 10 - 1303-Methylcholanthrene

3330 180 5 J *10 - 130Methyl methanesulfonate

3330 2050 62 35 - 1302-Methylnaphthalene

3330 2850 86 10 - 130Methyl parathion

3330 2150 65 32 - 1302-Methylphenol

3330 2170 65 31 - 1303 & 4 Methylphenol

3330 1880 57 32 - 130Naphthalene

3330 18.0 1 J *10 - 1301,4-Naphthoquinone

3330 81.2 2 J *10 - 1301-Naphthylamine

3330 758 23 10 - 1302-Naphthylamine

3330 2380 71 29 - 1302-Nitroaniline

3330 2260 68 30 - 1303-Nitroaniline

3330 2520 76 32 - 1304-Nitroaniline

3330 1890 57 24 - 130Nitrobenzene

3330 2130 64 31 - 1302-Nitrophenol

3330 2750 83 18 - 1304-Nitrophenol

3330 2510 75 J10 - 1304-Nitroquinoline-1-oxide

3330 2190 66 10 - 130N-Nitro-o-toluidine




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

n7005.d

04/20/2010 1628



30.07 g

1 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSNLCS 680-166138/12-A


3330 1910 58 10 - 130N-Nitrosodiethylamine

3330 1810 54 11 - 130N-Nitrosodimethylamine

3330 2370 71 10 - 130N-Nitrosodi-n-butylamine

3330 2380 72 26 - 130N-Nitrosodi-n-propylamine

3330 2460 74 43 - 130N-Nitrosodiphenylamine

3330 1940 58 10 - 130N-Nitrosomethylethylamine

3330 2320 70 10 - 130N-Nitrosomorpholine

3330 2070 62 10 - 130N-Nitrosopiperidine

3330 2130 64 10 - 130N-Nitrosopyrrolidine

3330 3760 113 10 - 130o,o',o''-Triethylphosphorothioate

3330 2610 78 10 - 130p-Dimethylamino azobenzene

3330 2210 67 10 - 130Pentachlorobenzene

3330 2500 75 10 - 130Pentachloronitrobenzene

3330 2770 83 26 - 130Pentachlorophenol

3330 2600 78 10 - 130Phenacetin

3330 2270 68 38 - 130Phenanthrene

3330 1950 59 31 - 130Phenol

3330 2320 70 10 - 130Phorate

3330 1340 40 10 - 1302-Picoline

16600 2390 14 10 - 130p-Phenylene diamine

3330 2520 76 10 - 130Pronamide

3330 2300 69 40 - 130Pyrene

3330 991 30 10 - 130Pyridine

3330 2230 67 10 - 130Safrole, Total

3330 2280 68 10 - 130Sulfotepp

3330 2020 61 10 - 1301,2,4,5-Tetrachlorobenzene

3330 2520 76 10 - 1302,3,4,6-Tetrachlorophenol

3330 2620 79 10 - 130Thionazin

3330 1070 32 10 - 1302-Toluidine

3330 1830 55 30 - 1301,2,4-Trichlorobenzene

3330 2260 68 38 - 1302,4,5-Trichlorophenol


3330 2880 87 10 - 1301,3,5-Trinitrobenzene


2,4,6-Tribromophenol 80 34 - 130

2-Fluorobiphenyl 60 34 - 130

2-Fluorophenol 57 30 - 130

Terphenyl-d14 69 39 - 130

Phenol-d5 62 30 - 130

Nitrobenzene-d5 60 27 - 130




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/04/2010 1617

05/04/2010 1641

Solid

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 680-166138

50

50

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Instrument ID:

Lab File ID:



Injection Volume:




04/20/2010 1628

04/20/2010 1628



g1028.d

30.03 g

1 mL

1 uL

g1029.d

30.09 g

1 mL

1 uL

Method: 8270C

Preparation: 3546

MSG

MSG

680-56861-21

680-56861-21

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

0 0 37 - 130 NC 50 U F U FAcenaphthene

56 0 37 - 130 NC 50 J U FAcenaphthylene

44 0 22 - 130 NC 50 J U FAcetophenone

0 43 10 - 130 NC 50 U F J2-Acetylaminofluorene

NC NC 10 - 130 NC 50 U Ualpha,alpha-Dimethyl phenethylamine

0 0 10 - 130 NC 50 U F U F4-Aminobiphenyl

0 0 13 - 130 NC 50 U F U FAniline

69 52 39 - 130 27 50 J JAnthracene

0 0 10 - 130 NC 50 U F U FAramite, Total

68 60 40 - 130 13 50 J JBenzo[a]anthracene

0 0 43 - 130 NC 50 U F U FBenzo[a]pyrene

59 0 35 - 130 NC 50 J U FBenzo[b]fluoranthene

62 57 37 - 130 8 50 J JBenzo[g,h,i]perylene

0 0 34 - 130 NC 50 U F U FBenzo[k]fluoranthene

-59 -61 25 - 130 2 50 J F J FBenzyl alcohol

-224 -248 31 - 130 4 50 4 41,1'-Biphenyl

79 0 30 - 130 NC 50 J U FBis(2-chloroethoxy)methane

0 0 16 - 130 NC 50 U F U FBis(2-chloroethyl)ether

66 52 15 - 130 23 50 J Jbis(chloroisopropyl) ether

87 65 38 - 130 30 50 J JBis(2-ethylhexyl) phthalate

71 55 35 - 130 26 50 J J4-Bromophenyl phenyl ether

91 78 41 - 130 16 50 J JButyl benzyl phthalate

0 0 23 - 130 NC 50 U F U F4-Chloroaniline

0 0 36 - 130 NC 50 U F U F4-Chloro-3-methylphenol

61 0 35 - 130 NC 50 J U F2-Chloronaphthalene

0 0 32 - 130 NC 50 U F U F2-Chlorophenol

0 59 40 - 130 NC 50 U F J4-Chlorophenyl phenyl ether

69 63 43 - 130 10 50 J JChrysene

NC NC 10 - 130 NC 50 U UDiallate

63 55 36 - 130 14 50 J JDibenz(a,h)anthracene




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/04/2010 1617

05/04/2010 1641

Solid

Matrix Spike/


50

50

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Instrument ID:

Lab File ID:



Injection Volume:




04/20/2010 1628

04/20/2010 1628



g1028.d

30.03 g

1 mL

1 uL

g1029.d

30.09 g

1 mL

1 uL

Method: 8270C

Preparation: 3546

MSG

MSG

680-56861-21

680-56861-21


% Rec.

63 60 38 - 130 5 50 J JDibenzofuran

59 0 27 - 130 NC 50 J U F1,2-Dichlorobenzene

0 0 25 - 130 NC 50 U F U F1,3-Dichlorobenzene

57 0 26 - 130 NC 50 J U F1,4-Dichlorobenzene

0 0 28 - 130 NC 50 U F U F3,3'-Dichlorobenzidine

0 0 35 - 130 NC 50 U F U F2,4-Dichlorophenol

0 0 10 - 130 NC 50 U F U F2,6-Dichlorophenol

84 69 42 - 130 20 50 J JDiethyl phthalate

50 45 10 - 130 11 50 J JDimethoate

0 31 10 - 130 NC 50 U F J7,12-Dimethylbenz(a)anthracene

NC NC 10 - 130 NC 50 U U3,3'-Dimethylbenzidine

0 0 31 - 130 NC 50 U F U F2,4-Dimethylphenol

0 52 43 - 130 NC 50 U F JDimethyl phthalate

102 92 39 - 130 11 50 J JDi-n-butyl phthalate

0 0 10 - 130 NC 50 U F U F1,3-Dinitrobenzene

NC NC 22 - 130 NC 50 U U4,6-Dinitro-2-methylphenol

NC NC 10 - 137 NC 50 U U2,4-Dinitrophenol

0 0 36 - 130 NC 50 U F U F2,4-Dinitrotoluene

0 0 38 - 130 NC 50 U F U F2,6-Dinitrotoluene

83 66 37 - 130 24 50 J JDi-n-octyl phthalate

NC NC 10 - 130 NC 50 U UDinoseb

NC NC 10 - 130 NC 50 U U1,4-Dioxane

63 0 10 - 130 NC 50 J U FDisulfoton

0 0 10 - 130 NC 50 U F U FEthyl methanesulfonate

2530 0 10 - 130 NC 50 F U FEthyl Parathion

49 0 10 - 130 NC 50 J U FFamphur

68 56 40 - 130 20 50 J JFluoranthene

57 0 38 - 130 NC 50 J U FFluorene

66 0 40 - 130 NC 50 J U FHexachlorobenzene

67 0 29 - 130 NC 50 J U FHexachlorobutadiene




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/04/2010 1617

05/04/2010 1641

Solid

Matrix Spike/


50

50

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Instrument ID:

Lab File ID:



Injection Volume:




04/20/2010 1628

04/20/2010 1628



g1028.d

30.03 g

1 mL

1 uL

g1029.d

30.09 g

1 mL

1 uL

Method: 8270C

Preparation: 3546

MSG

MSG

680-56861-21

680-56861-21


% Rec.

0 0 10 - 130 NC 50 U F U FHexachlorocyclopentadiene

75 53 23 - 130 36 50 J JHexachloroethane

NC NC 10 - 130 NC 50 U UHexachlorophene

0 0 10 - 130 NC 50 U F U FHexachloropropene

59 56 34 - 130 6 50 J JIndeno[1,2,3-cd]pyrene

58 0 30 - 130 NC 50 J U FIsophorone

62 0 10 - 130 NC 50 J U FIsosafrole

NC NC 10 - 130 NC 50 U UMethapyrilene

0 0 10 - 130 NC 50 U F U F3-Methylcholanthrene

0 0 10 - 130 NC 50 U F U FMethyl methanesulfonate

61 0 35 - 130 NC 50 J U F2-Methylnaphthalene

0 0 10 - 130 NC 50 U F U FMethyl parathion

0 0 32 - 130 NC 50 U F U F2-Methylphenol

0 0 31 - 130 NC 50 U F U F3 & 4 Methylphenol

63 51 32 - 130 21 50 J JNaphthalene

0 0 10 - 130 NC 50 U F U F1,4-Naphthoquinone

NC 0 10 - 130 NC 50 U U F1-Naphthylamine

0 0 10 - 130 NC 50 U F U F2-Naphthylamine

0 449 29 - 130 NC 50 U F J F2-Nitroaniline

0 0 30 - 130 NC 50 U F U F3-Nitroaniline

0 0 32 - 130 NC 50 U F U F4-Nitroaniline

0 0 24 - 130 NC 50 U F U FNitrobenzene

0 0 31 - 130 NC 50 U F U F2-Nitrophenol

NC NC 18 - 130 NC 50 U U4-Nitrophenol

NC NC 10 - 130 NC 50 U U4-Nitroquinoline-1-oxide

0 0 10 - 130 NC 50 U F U FN-Nitro-o-toluidine

0 0 10 - 130 NC 50 U F U FN-Nitrosodiethylamine

NC NC 11 - 130 NC 50 U UN-Nitrosodimethylamine

0 45 10 - 130 NC 50 U F JN-Nitrosodi-n-butylamine

57 0 26 - 130 NC 50 J U FN-Nitrosodi-n-propylamine




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/04/2010 1617

05/04/2010 1641

Solid

Matrix Spike/


50

50

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Instrument ID:

Lab File ID:



Injection Volume:




04/20/2010 1628

04/20/2010 1628



g1028.d

30.03 g

1 mL

1 uL

g1029.d

30.09 g

1 mL

1 uL

Method: 8270C

Preparation: 3546

MSG

MSG

680-56861-21

680-56861-21


% Rec.

54 51 43 - 130 7 50 J JN-Nitrosodiphenylamine

0 0 10 - 130 NC 50 U F U FN-Nitrosomethylethylamine

0 0 10 - 130 NC 50 U F U FN-Nitrosomorpholine

57 45 10 - 130 24 50 J JN-Nitrosopiperidine

0 0 10 - 130 NC 50 U F U FN-Nitrosopyrrolidine

12 -58 10 - 130 36 50 J J Fo,o',o''-Triethylphosphorothioate

41 42 10 - 130 2 50 J Jp-Dimethylamino azobenzene

67 54 10 - 130 21 50 J JPentachlorobenzene

0 0 10 - 130 NC 50 U F U FPentachloronitrobenzene

NC NC 26 - 130 NC 50 U UPentachlorophenol

0 0 10 - 130 NC 50 U F U FPhenacetin

63 55 38 - 130 13 50 J JPhenanthrene

0 0 31 - 130 NC 50 U F U FPhenol

55 0 10 - 130 NC 50 J U FPhorate

0 0 10 - 130 NC 50 U F U F2-Picoline

NC NC 10 - 130 NC 50 U Up-Phenylene diamine

57 49 10 - 130 16 50 J JPronamide

61 55 40 - 130 11 50 J JPyrene

0 0 10 - 130 NC 50 U F U FPyridine

59 45 10 - 130 27 50 J JSafrole, Total

96 84 10 - 130 13 50 J JSulfotepp

0 0 10 - 130 NC 50 U F U F1,2,4,5-Tetrachlorobenzene

50 41 10 - 130 21 50 J J2,3,4,6-Tetrachlorophenol

57 0 10 - 130 NC 50 J U FThionazin

0 0 10 - 130 NC 50 U F U F2-Toluidine

58 48 30 - 130 20 50 J J1,2,4-Trichlorobenzene

0 0 38 - 130 NC 50 U F U F2,4,5-Trichlorophenol

0 0 36 - 130 NC 50 U F U F2,4,6-Trichlorophenol

NC NC 10 - 130 NC 50 U U1,3,5-Trinitrobenzene

-1020 -1120 10 - 130 6 50 4 4Diphenyl ether




Surrogate MS % Rec MSD % Rec Acceptance Limits

2,4,6-Tribromophenol 0 0 34 - 130D D

2-Fluorobiphenyl 0 0 34 - 130D D

2-Fluorophenol 0 0 30 - 130D D

Terphenyl-d14 0 0 39 - 130D D

Phenol-d5 0 0 30 - 130D D

Nitrobenzene-d5 0 0 27 - 130D D




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/03/2010 1645


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/20/2010 2315

g1004.d

30.11 g

1.0 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSGMB 680-166147/21-A








660 U 66034Aniline









330 U 330281,1'-Biphenyl












330 U 33021Chrysene

330 U 330170Diallate


















SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/03/2010 1645


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/20/2010 2315

g1004.d

30.11 g

1.0 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSGMB 680-166147/21-A









330 U 330160Dinoseb

330 U 3301201,4-Dioxane




330 U 33029Famphur


330 U 33036Fluorene
















330 U 330433 & 4 Methylphenol
















SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/03/2010 1645


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/20/2010 2315

g1004.d

30.11 g

1.0 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSGMB 680-166147/21-A


















330 U 33034Phenol

330 U 33022Phorate

330 U 330172-Picoline



330 U 33027Pyrene

330 U 33029Pyridine











330 U 33034Diphenyl ether






Phenol-d5 81 30 - 130





Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

g1005.d

04/20/2010 2315



30.08 g

1.0 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSGLCS 680-166147/22-A


3320 2710 82 37 - 130Acenaphthene

3320 2890 87 37 - 130Acenaphthylene

3320 2010 61 22 - 130Acetophenone

3320 3260 98 10 - 1302-Acetylaminofluorene

16600 16700 100 J E10 - 130alpha,alpha-Dimethyl phenethylamine

3320 423 13 10 - 1304-Aminobiphenyl

3320 1090 33 13 - 130Aniline

3320 3260 98 39 - 130Anthracene

3320 2900 87 10 - 130Aramite, Total

3320 3670 111 10 - 130Aramite, Total

3320 3780 114 10 - 130Aramite, Total

3320 3100 93 40 - 130Benzo[a]anthracene

3320 3200 96 43 - 130Benzo[a]pyrene

3320 3270 98 35 - 130Benzo[b]fluoranthene

3320 2830 85 37 - 130Benzo[g,h,i]perylene

3320 3460 104 34 - 130Benzo[k]fluoranthene

3320 2650 80 25 - 130Benzyl alcohol

3320 2850 86 31 - 1301,1'-Biphenyl

3320 3400 102 30 - 130Bis(2-chloroethoxy)methane

3320 2440 73 16 - 130Bis(2-chloroethyl)ether

3320 2660 80 15 - 130bis(chloroisopropyl) ether

3320 3620 109 38 - 130Bis(2-ethylhexyl) phthalate

3320 3240 97 35 - 1304-Bromophenyl phenyl ether

3320 3600 108 41 - 130Butyl benzyl phthalate

3320 1220 37 23 - 1304-Chloroaniline

3320 2860 86 36 - 1304-Chloro-3-methylphenol

3320 2830 85 35 - 1302-Chloronaphthalene

3320 2600 78 32 - 1302-Chlorophenol

3320 3060 92 40 - 1304-Chlorophenyl phenyl ether

3320 3360 101 43 - 130Chrysene

3320 3040 91 10 - 130Diallate

3320 2840 85 36 - 130Dibenz(a,h)anthracene

3320 2810 85 38 - 130Dibenzofuran




3320 3190 96 28 - 1303,3'-Dichlorobenzidine

3320 2550 77 35 - 1302,4-Dichlorophenol

3320 2720 82 10 - 1302,6-Dichlorophenol

3320 3220 97 42 - 130Diethyl phthalate

3320 2140 64 10 - 130Dimethoate

3320 3380 102 10 - 1307,12-Dimethylbenz(a)anthracene

3320 1700 13 U10 - 1303,3'-Dimethylbenzidine




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

g1005.d

04/20/2010 2315



30.08 g

1.0 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSGLCS 680-166147/22-A


6650 5190 78 31 - 1302,4-Dimethylphenol

3320 3050 92 43 - 130Dimethyl phthalate

3320 3460 104 39 - 130Di-n-butyl phthalate

3320 3250 98 10 - 1301,3-Dinitrobenzene

3320 3650 110 22 - 1304,6-Dinitro-2-methylphenol

3320 3360 101 10 - 1372,4-Dinitrophenol

3320 3160 95 36 - 1302,4-Dinitrotoluene

3320 3140 95 38 - 1302,6-Dinitrotoluene

3320 3770 113 37 - 130Di-n-octyl phthalate

3320 3700 111 10 - 130Dinoseb

3320 1020 31 10 - 1301,4-Dioxane

3320 3440 103 10 - 130Disulfoton

3320 2130 64 10 - 130Ethyl methanesulfonate

3320 3620 109 10 - 130Ethyl Parathion

3320 135 4 J *10 - 130Famphur

3320 3120 94 40 - 130Fluoranthene

3320 3030 91 38 - 130Fluorene

3320 2950 89 40 - 130Hexachlorobenzene

3320 2730 82 29 - 130Hexachlorobutadiene

3320 1070 32 10 - 130Hexachlorocyclopentadiene

3320 2420 73 23 - 130Hexachloroethane

16600 170000 36 U10 - 130Hexachlorophene

3320 330 0 U *10 - 130Hexachloropropene

3320 2850 86 34 - 130Indeno[1,2,3-cd]pyrene

3320 2380 72 30 - 130Isophorone

3320 2820 85 10 - 130Isosafrole

3320 3060 92 J10 - 130Methapyrilene

3320 2000 60 10 - 1303-Methylcholanthrene

3320 207 6 J *10 - 130Methyl methanesulfonate

3320 2650 80 35 - 1302-Methylnaphthalene

3320 3040 92 10 - 130Methyl parathion

3320 2750 83 32 - 1302-Methylphenol

3320 3520 106 31 - 1303 & 4 Methylphenol

3320 3310 100 32 - 130Naphthalene

3320 330 0 U *10 - 1301,4-Naphthoquinone

3320 330 1 U *10 - 1301-Naphthylamine

3320 764 23 10 - 1302-Naphthylamine

3320 2590 78 29 - 1302-Nitroaniline

3320 1930 58 30 - 1303-Nitroaniline

3320 2630 79 32 - 1304-Nitroaniline

3320 2240 68 24 - 130Nitrobenzene

3320 2610 79 31 - 1302-Nitrophenol

3320 3080 93 18 - 1304-Nitrophenol




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

g1005.d

04/20/2010 2315



30.08 g

1.0 mL

1 uL

Units: ug/Kg

Method: 8270C

Preparation: 3546

MSGLCS 680-166147/22-A


3320 1900 57 J10 - 1304-Nitroquinoline-1-oxide

3320 1820 55 10 - 130N-Nitro-o-toluidine

3320 2520 76 10 - 130N-Nitrosodiethylamine

3320 2290 69 11 - 130N-Nitrosodimethylamine

3320 3890 117 10 - 130N-Nitrosodi-n-butylamine

3320 3120 94 26 - 130N-Nitrosodi-n-propylamine

3320 3400 102 43 - 130N-Nitrosodiphenylamine

3320 2300 69 10 - 130N-Nitrosomethylethylamine

3320 3160 95 10 - 130N-Nitrosomorpholine

3320 2620 79 10 - 130N-Nitrosopiperidine

3320 3060 92 10 - 130N-Nitrosopyrrolidine

3320 4760 143 *10 - 130o,o',o''-Triethylphosphorothioate

3320 3000 90 10 - 130p-Dimethylamino azobenzene

3320 2800 84 10 - 130Pentachlorobenzene

3320 3340 101 10 - 130Pentachloronitrobenzene

3320 3720 112 26 - 130Pentachlorophenol

3320 3150 95 10 - 130Phenacetin

3320 3030 91 38 - 130Phenanthrene

3320 2390 72 31 - 130Phenol

3320 4490 135 *10 - 130Phorate

3320 587 18 10 - 1302-Picoline

16600 1700 4 U *10 - 130p-Phenylene diamine

3320 3220 97 10 - 130Pronamide

3320 3040 91 40 - 130Pyrene

3320 1460 44 10 - 130Pyridine

3320 2870 86 10 - 130Safrole, Total

3320 3090 93 10 - 130Sulfotepp

3320 2720 82 10 - 1301,2,4,5-Tetrachlorobenzene

3320 2990 90 10 - 1302,3,4,6-Tetrachlorophenol

3320 3220 97 10 - 130Thionazin

3320 606 18 10 - 1302-Toluidine

3320 2450 74 30 - 1301,2,4-Trichlorobenzene



3320 1960 59 10 - 1301,3,5-Trinitrobenzene

3320 2760 83 10 - 130Diphenyl ether






Phenol-d5 79 30 - 130









WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/24/2010 1924


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/21/2010 1423

g0748.d

1000 mL

1 mL

1 uL

Units: ug/L

Method: 8270C

Preparation: 3520C

MSGMB 680-166243/7-A


10 U 100.76Acenaphthene

10 U 100.85Acenaphthylene

10 U 100.57Acetophenone

10 U 101.62-Acetylaminofluorene


10 U 101.24-Aminobiphenyl

20 U 202.1Aniline

10 U 100.69Anthracene

10 U 100.91Aramite, Total

10 U 100.55Benzo[a]anthracene

10 U 100.71Benzo[a]pyrene

10 U 102.6Benzo[b]fluoranthene

10 U 100.87Benzo[g,h,i]perylene

10 U 101.2Benzo[k]fluoranthene

10 U 101.1Benzyl alcohol

10 U 100.581,1'-Biphenyl

10 U 100.94Bis(2-chloroethoxy)methane

10 U 101.1Bis(2-chloroethyl)ether

10 U 100.78bis(chloroisopropyl) ether

10 U 101.6Bis(2-ethylhexyl) phthalate

10 U 100.774-Bromophenyl phenyl ether

10 U 101.2Butyl benzyl phthalate

20 U 202.24-Chloroaniline

10 U 101.04-Chloro-3-methylphenol

10 U 100.802-Chloronaphthalene

10 U 100.872-Chlorophenol

10 U 100.844-Chlorophenyl phenyl ether

10 U 100.51Chrysene

10 U 100.78Diallate

10 U 101.0Dibenz(a,h)anthracene

10 U 100.79Dibenzofuran

10 U 100.531,2-Dichlorobenzene




10 U 101.12,4-Dichlorophenol

10 U 100.732,6-Dichlorophenol

10 U 100.88Diethyl phthalate

10 U 100.75Dimethoate

10 U 101.27,12-Dimethylbenz(a)anthracene


10 U 104.02,4-Dimethylphenol

10 U 100.99Dimethyl phthalate




WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/24/2010 1924


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/21/2010 1423

g0748.d

1000 mL

1 mL

1 uL

Units: ug/L

Method: 8270C

Preparation: 3520C

MSGMB 680-166243/7-A


10 U 100.83Di-n-butyl phthalate

10 U 100.601,3-Dinitrobenzene



10 U 101.22,4-Dinitrotoluene

10 U 101.12,6-Dinitrotoluene

10 U 101.4Di-n-octyl phthalate

10 U 105.0Dinoseb

10 U 103.41,4-Dioxane

10 U 100.79Disulfoton

10 U 100.96Ethyl methanesulfonate

10 U 101.3Ethyl Parathion

10 U 101.1Famphur

10 U 100.74Fluoranthene

10 U 100.96Fluorene

10 U 100.79Hexachlorobenzene

10 U 100.62Hexachlorobutadiene

10 U 102.5Hexachlorocyclopentadiene

10 U 100.76Hexachloroethane


10 U 101.4Hexachloropropene

10 U 101.0Indeno[1,2,3-cd]pyrene

10 U 100.90Isophorone

10 U 100.50Isosafrole

2000 U 20002.7Methapyrilene

10 U 101.43-Methylcholanthrene

10 U 100.60Methyl methanesulfonate

10 U 100.782-Methylnaphthalene

10 U 100.88Methyl parathion

10 U 100.892-Methylphenol

10 U 101.33 & 4 Methylphenol

10 U 100.70Naphthalene

10 U 100.621,4-Naphthoquinone

10 U 101.11-Naphthylamine

10 U 101.52-Naphthylamine




10 U 100.73Nitrobenzene




10 U 101.5N-Nitro-o-toluidine




WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/24/2010 1924


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/21/2010 1423

g0748.d

1000 mL

1 mL

1 uL

Units: ug/L

Method: 8270C

Preparation: 3520C

MSGMB 680-166243/7-A


10 U 100.93N-Nitrosodiethylamine

10 U 102.8N-Nitrosodimethylamine

10 U 100.96N-Nitrosodi-n-butylamine

10 U 100.72N-Nitrosodi-n-propylamine

10 U 100.92N-Nitrosodiphenylamine

10 U 103.3N-Nitrosomethylethylamine

10 U 100.84N-Nitrosomorpholine

10 U 100.88N-Nitrosopiperidine

10 U 101.0N-Nitrosopyrrolidine

10 U 101.0o,o',o''-Triethylphosphorothioate

10 U 100.79p-Dimethylamino azobenzene

10 U 100.52Pentachlorobenzene

10 U 100.78Pentachloronitrobenzene

50 U 502.0Pentachlorophenol

10 U 101.4Phenacetin

10 U 100.77Phenanthrene

10 U 100.83Phenol

10 U 100.87Phorate

10 U 101.42-Picoline


10 U 100.89Pronamide

10 U 100.63Pyrene

50 U 502.3Pyridine

10 U 100.80Safrole, Total

10 U 100.53Sulfotepp

10 U 100.761,2,4,5-Tetrachlorobenzene

10 U 100.722,3,4,6-Tetrachlorophenol

10 U 100.91Thionazin

10 U 101.42-Toluidine

10 U 100.561,2,4-Trichlorobenzene

10 U 101.22,4,5-Trichlorophenol

10 U 100.852,4,6-Trichlorophenol

10 U 102.01,3,5-Trinitrobenzene





Terphenyl-d14 103 10 - 121

Phenol-d5 82 38 - 116





Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/25/2010 2044

04/24/2010 2059

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/L

04/21/2010 1423



g0794.d

1000 mL

1 mL

1 uL

g0752.d

1000 mL

1 mL

1 uL

ug/L

04/21/2010 1423



Method: 8270C

Preparation: 3520C

MSG

MSG

LCS 680-166243/8-A

LCSD 680-166243/9-A


% Rec.

8998 45 - 117 9 40Acenaphthene

91100 51 - 112 9 40Acenaphthylene

7883 25 - 110 6 40Acetophenone

105103 69 - 123 2 402-Acetylaminofluorene

221197 10 - 158 11 40 J E * J E *alpha,alpha-Dimethyl phenethylamine

2432 10 - 130 28 404-Aminobiphenyl

7876 10 - 114 2 40Aniline

93100 52 - 116 7 40Anthracene

114102 10 - 150 3 40Aramite, Total

99102 10 - 150 3 40Aramite, Total

99102 10 - 150 3 40Aramite, Total

114117 10 - 150 3 40Aramite, Total

99117 10 - 150 3 40Aramite, Total

99117 10 - 150 3 40Aramite, Total

11496 10 - 150 3 40Aramite, Total

9996 10 - 150 3 40Aramite, Total

9996 10 - 150 3 40Aramite, Total

100101 49 - 124 1 40Benzo[a]anthracene

100102 48 - 120 2 40Benzo[a]pyrene

106101 46 - 126 5 40Benzo[b]fluoranthene

9999 51 - 117 0 40Benzo[g,h,i]perylene

101106 47 - 126 5 40Benzo[k]fluoranthene

9192 34 - 113 1 40Benzyl alcohol

94101 47 - 112 8 401,1'-Biphenyl

124130 50 - 112 5 40 * *Bis(2-chloroethoxy)methane

9496 43 - 110 2 40Bis(2-chloroethyl)ether

9697 42 - 110 1 40bis(chloroisopropyl) ether

122118 47 - 134 3 40Bis(2-ethylhexyl) phthalate

96103 42 - 110 8 404-Bromophenyl phenyl ether

121123 52 - 135 2 40Butyl benzyl phthalate

9091 10 - 110 1 404-Chloroaniline

9298 46 - 118 6 404-Chloro-3-methylphenol

94101 47 - 110 7 402-Chloronaphthalene




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/25/2010 2044

04/24/2010 2059

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/L

04/21/2010 1423



g0794.d

1000 mL

1 mL

1 uL

g0752.d

1000 mL

1 mL

1 uL

ug/L

04/21/2010 1423



Method: 8270C

Preparation: 3520C

MSG

MSG

LCS 680-166243/8-A

LCSD 680-166243/9-A


% Rec.

8486 47 - 110 2 402-Chlorophenol

97105 46 - 114 8 404-Chlorophenyl phenyl ether

98101 51 - 123 4 40Chrysene

98108 36 - 145 10 40Diallate

100100 46 - 124 0 40Dibenz(a,h)anthracene

9099 50 - 112 10 40Dibenzofuran

7475 39 - 110 1 401,2-Dichlorobenzene



107103 10 - 113 3 403,3'-Dichlorobenzidine

8689 46 - 115 4 402,4-Dichlorophenol

8689 46 - 130 3 402,6-Dichlorophenol

103112 51 - 119 8 40Diethyl phthalate

88100 28 - 142 12 40Dimethoate

9392 39 - 130 2 407,12-Dimethylbenz(a)anthracene

2218 10 - 130 17 40 J3,3'-Dimethylbenzidine

8993 36 - 110 5 402,4-Dimethylphenol

99108 50 - 116 9 40Dimethyl phthalate

108113 49 - 123 5 40Di-n-butyl phthalate

10594 53 - 136 11 401,3-Dinitrobenzene

119100 29 - 167 17 404,6-Dinitro-2-methylphenol

135112 10 - 189 18 402,4-Dinitrophenol

108104 49 - 128 4 402,4-Dinitrotoluene

100103 45 - 131 3 402,6-Dinitrotoluene

122122 44 - 134 0 40Di-n-octyl phthalate

10988 50 - 144 21 40Dinoseb

5968 11 - 110 14 401,4-Dioxane

111116 40 - 130 4 40Disulfoton

7577 32 - 130 3 40Ethyl methanesulfonate

106102 60 - 140 4 40Ethyl Parathion

718 10 - 130 90 40 J *Famphur

9498 50 - 120 4 40Fluoranthene

95101 50 - 115 6 40Fluorene




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/25/2010 2044

04/24/2010 2059

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/L

04/21/2010 1423



g0794.d

1000 mL

1 mL

1 uL

g0752.d

1000 mL

1 mL

1 uL

ug/L

04/21/2010 1423



Method: 8270C

Preparation: 3520C

MSG

MSG

LCS 680-166243/8-A

LCSD 680-166243/9-A


% Rec.

9299 48 - 119 7 40Hexachlorobenzene

8083 40 - 110 3 40Hexachlorobutadiene

4439 10 - 110 10 40Hexachlorocyclopentadiene

7575 33 - 110 0 40Hexachloroethane

6948 10 - 130 36 40 J JHexachlorophene

00 10 - 130 NC 40 U * U *Hexachloropropene

9899 40 - 126 1 40Indeno[1,2,3-cd]pyrene

8794 50 - 111 8 40Isophorone

8996 37 - 130 8 40Isosafrole

101142 10 - 130 34 40 J * JMethapyrilene

6464 62 - 130 1 403-Methylcholanthrene

77 10 - 130 1 40 J * J *Methyl methanesulfonate

8589 46 - 110 4 402-Methylnaphthalene

106104 51 - 146 3 40Methyl parathion

9291 46 - 110 1 402-Methylphenol

9394 43 - 110 2 403 & 4 Methylphenol

8386 41 - 110 3 40Naphthalene

911 10 - 130 22 40 J *1,4-Naphthoquinone

22 10 - 130 5 40 J * J *1-Naphthylamine

3032 10 - 130 6 402-Naphthylamine

100103 45 - 122 3 402-Nitroaniline

9297 30 - 116 6 403-Nitroaniline

98103 36 - 125 5 404-Nitroaniline

8889 46 - 110 1 40Nitrobenzene

9288 42 - 120 4 402-Nitrophenol

102111 30 - 122 8 404-Nitrophenol

7861 10 - 151 24 404-Nitroquinoline-1-oxide

8788 45 - 130 1 40N-Nitro-o-toluidine

9391 48 - 130 2 40N-Nitrosodiethylamine

100105 33 - 110 5 40N-Nitrosodimethylamine

138140 41 - 130 1 40 * *N-Nitrosodi-n-butylamine

110110 45 - 112 1 40N-Nitrosodi-n-propylamine

105111 47 - 119 6 40N-Nitrosodiphenylamine




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/25/2010 2044

04/24/2010 2059

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Date Prepared:

Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/L

04/21/2010 1423



g0794.d

1000 mL

1 mL

1 uL

g0752.d

1000 mL

1 mL

1 uL

ug/L

04/21/2010 1423



Method: 8270C

Preparation: 3520C

MSG

MSG

LCS 680-166243/8-A

LCSD 680-166243/9-A


% Rec.

9090 47 - 130 0 40N-Nitrosomethylethylamine

108107 35 - 130 1 40N-Nitrosomorpholine

9197 53 - 130 6 40N-Nitrosopiperidine

106102 50 - 130 4 40N-Nitrosopyrrolidine

177183 23 - 162 3 40 * *o,o',o''-Triethylphosphorothioate

10892 29 - 169 16 40p-Dimethylamino azobenzene

8794 52 - 130 8 40Pentachlorobenzene

9799 52 - 130 3 40Pentachloronitrobenzene

111111 37 - 132 1 40Pentachlorophenol

103104 62 - 130 2 40Phenacetin

97101 52 - 117 4 40Phenanthrene

8285 39 - 110 3 40Phenol

105111 29 - 181 5 40Phorate

7782 10 - 130 6 402-Picoline

3434 10 - 130 0 40 J Jp-Phenylene diamine

97103 64 - 134 5 40Pronamide

100102 52 - 125 2 40Pyrene

6975 10 - 110 9 40Pyridine

8993 39 - 130 4 40Safrole, Total

97105 44 - 130 8 40Sulfotepp

8188 41 - 130 9 401,2,4,5-Tetrachlorobenzene

8993 38 - 130 4 402,3,4,6-Tetrachlorophenol

102112 48 - 135 10 40Thionazin

5355 27 - 130 3 402-Toluidine

8081 41 - 110 0 401,2,4-Trichlorobenzene

8994 47 - 122 5 402,4,5-Trichlorophenol

9096 46 - 120 6 402,4,6-Trichlorophenol

9665 10 - 200 39 401,3,5-Trinitrobenzene


2,4,6-Tribromophenol 110 103 40 - 139

2-Fluorobiphenyl 95 87 50 - 113

2-Fluorophenol 80 79 36 - 110





Terphenyl-d14 103 100 10 - 121

Phenol-d5 87 85 38 - 116

Nitrobenzene-d5 92 91 45 - 112




WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/21/2010 1906


Date Prepared:

Instrument ID:

Lab File ID:





04/21/2010 1215

50 mL

50 mL

Units: ug/L

Method: 6010B

Preparation: 3010A

N/A

ICPDMB 680-166297/18-A


20 U 204.6Arsenic

10 U 102.3Barium

5.0 U 5.02.0Cadmium

10 U 101.2Chromium

10 U 104.0Lead

20 U 206.4Selenium

10 U 100.89Silver

Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/21/2010 1215



50 mL

50 mL

Units: ug/L

Method: 6010B

Preparation: 3010A

N/A

ICPDLCS 680-166297/19-A


2000 1970 98 75 - 125Arsenic

2000 2090 104 75 - 125Barium

50.0 51.7 103 75 - 125Cadmium

200 204 102 75 - 125Chromium

500 506 101 75 - 125Lead

2000 2050 102 75 - 125Selenium

50.0 50.1 100 75 - 125Silver




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1427


Date Prepared:

Instrument ID:

Lab File ID:





04/21/2010 1618

1.00 g

100 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

N/A

ICPDMB 680-166337/23-A



1.0 U 1.00.30Barium

0.50 U 0.500.10Cadmium


1.0 U 1.00.53Lead


1.0 U 1.00.096Silver

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/21/2010 1618



1.00 g

100 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

N/A

ICPDLCS 680-166337/24-A


200 192 96 75 - 125Arsenic

200 206 103 75 - 125Barium

5.00 5.08 102 75 - 125Cadmium

20.0 20.4 102 75 - 125Chromium

50.0 50.2 100 75 - 125Lead

200 197 99 75 - 125Selenium

5.00 4.93 99 75 - 125Silver




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/26/2010 2021


Date Prepared:

Instrument ID:

Lab File ID:





04/23/2010 1017

1.00 g

100 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

N/A

ICPDMB 680-166528/23-A



1.0 U 1.00.30Barium

0.50 U 0.500.10Cadmium


1.0 U 1.00.53Lead


0.133 J 1.00.096Silver

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/23/2010 1017



1.00 g

100 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

N/A

ICPDLCS 680-166528/24-A


200 184 92 75 - 125Arsenic

200 195 98 75 - 125Barium

5.00 4.75 95 75 - 125Cadmium

20.0 19.4 97 75 - 125Chromium

50.0 47.8 96 75 - 125Lead

200 185 92 75 - 125Selenium

5.00 4.84 97 75 - 125Silver




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/26/2010 2247

04/26/2010 2252

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/23/2010 1017

04/23/2010 1017



1.16 g

100 mL

1.16 g

100 mL

Method: 6010B

Preparation: 3050B

N/A

N/A

ICPD

ICPD

680-56861-14

680-56861-14


% Rec.

95 94 75 - 125 1 20Arsenic

102 102 75 - 125 1 20Barium

97 96 75 - 125 0 20Cadmium

103 102 75 - 125 1 20Chromium

98 98 75 - 125 0 20Lead

93 92 75 - 125 0 20Selenium

100 98 75 - 125 1 20Silver




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/28/2010 2226


Date Prepared:

Instrument ID:

Lab File ID:





04/27/2010 0909

1.00 g

100 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

N/A

ICPDMB 680-166825/22-A



1.0 U 1.00.30Barium

0.50 U 0.500.10Cadmium


1.0 U 1.00.53Lead


1.0 U 1.00.096Silver

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/27/2010 0909



1.00 g

100 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

N/A

ICPDLCS 680-166825/23-A


200 197 99 75 - 125Arsenic

200 211 106 75 - 125Barium

5.00 5.07 101 75 - 125Cadmium

20.0 20.7 103 75 - 125Chromium

50.0 49.8 100 75 - 125Lead

200 200 100 75 - 125Selenium

5.00 5.03 101 75 - 125Silver




WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1115


Date Prepared:

Instrument ID:

Lab File ID:





04/21/2010 1021

50 mL

50 mL

Units: ug/L

Method: 7470A

Preparation: 7470A

N/A

LEEMAN1MB 680-166266/6-B


0.20 U 0.200.091Mercury

Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/21/2010 1021



50 mL

50 mL

Units: ug/L

Method: 7470A

Preparation: 7470A

N/A

LEEMAN1LCS 680-166266/7-B


2.50 2.33 93 80 - 120Mercury

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 1233

04/22/2010 1236

Water

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/21/2010 1021

04/21/2010 1021



50 mL

50 mL

50 mL

50 mL

Method: 7470A

Preparation: 7470A

N/A

N/A

LEEMAN1

LEEMAN1

680-56861-28

680-56861-28


% Rec.

89 89 80 - 120 0 20Mercury




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/27/2010 1322


Date Prepared:

Instrument ID:

Lab File ID:





04/23/2010 1046

0.50 g

50 mL

Units: mg/Kg

Method: 7471A

Preparation: 7471A

N/A

LEEMAN1MB 680-166534/23-A


0.020 U 0.0200.0082Mercury

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/23/2010 1046



0.50 g

50 mL

Units: mg/Kg

Method: 7471A

Preparation: 7471A

N/A

LEEMAN1LCS 680-166534/24-A


0.250 0.236 94 80 - 120Mercury

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/27/2010 1447

04/27/2010 1450

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/23/2010 1046

04/23/2010 1046



0.53 g

50 mL

0.54 g

50 mL

Method: 7471A

Preparation: 7471A

N/A

N/A

LEEMAN1

LEEMAN1

680-56861-14

680-56861-14


% Rec.

88 83 80 - 120 8 20Mercury




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/28/2010 1844


Date Prepared:

Instrument ID:

Lab File ID:





04/26/2010 1535

0.51 g

50 mL

Units: mg/Kg

Method: 7471A

Preparation: 7471A

N/A

LEEMAN1MB 680-166757/19-A


0.020 U 0.0200.0080Mercury

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/26/2010 1535



0.51 g

50 mL

Units: mg/Kg

Method: 7471A

Preparation: 7471A

N/A

LEEMAN1LCS 680-166757/20-A


0.245 0.254 103 80 - 120Mercury

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/28/2010 1931

04/28/2010 1933

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/26/2010 1523

04/26/2010 1523



0.56 g

50 mL

0.56 g

50 mL

Method: 7471A

Preparation: 7471A

N/A

N/A

LEEMAN1

LEEMAN1

680-56861-23

680-56861-23


% Rec.

101 94 80 - 120 2 20Mercury


Page 236 of 238

Page 237 of 238

Login Sample Receipt Check List


Login Number: 56861

Question T / F/ NA Comment

Creator: Daughtry, Beth

List Source: TestAmerica Savannah

List Number: 1

Radioactivity either was not measured or, if measured, is at or below

background

N/A

The cooler's custody seal, if present, is intact. True

The cooler or samples do not appear to have been compromised or

tampered with.

True

Samples were received on ice. True 6 coolers rec'd 4/17/10; 7th cooler rec'd on 4/19

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 4/17 Rcpt - 0.8, 1.4, 0.9, 0.6, 1.9, 2.0 C; 4/19

recpt @ 0.2 C

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and

the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. False Client labeled outside baggie on soil containers

had to place on containers

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in

diameter.

True

If necessary, staff have been informed of any short hold time or quick TAT

needs

True

Multiphasic samples are not present. N/A

Samples do not require splitting or compositing. N/A

Is the Field Sampler's name present on COC? True

Sample Preservation Verified True


Page 238 of 238

J56861-1 Std Tal L2 Final Report - MDEQ€¦ · The test results in this report meet NELAP requirements for parameters for which accreditation is required or ... Method(s) 3546: Many

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