InfraCal TOG/TPH Analyzer TOG/TPH Analyzer

InfraCalInfraCal TOG/TPH AnalyzerTOG/TPH AnalyzerCalibrationCalibration

www.WilksIR.comwww.WilksIR.com

Calibration OilCalibration Oil

�� Heavy hydrocarbon Heavy hydrocarbon

�� No volatilesNo volatiles�� No volatilesNo volatiles

�� No AdditivesNo Additives

Mixing Standards Mixing Standards –– Volume/volumeVolume/volume

ppm ppm OilOil SolventSolvent

400400 40ul40ul 10 ml10 ml

300300 30ul30ul 10 ml10 ml300300 30ul30ul 10 ml10 ml

200200 20ul20ul 10 ml10 ml

100100 10 ul10 ul 10 ml10 ml

First Standard: First Standard: 100 ppm100 ppm

�� Add 10Add 10--ml of solvent to ml of solvent to the 10the 10--ml graduated ml graduated cylindercylinder

First Standard: First Standard: 100 ppm100 ppm

� Add 10-ml of solvent to the 10-ml graduated cylinder

�� Using the syringe add Using the syringe add 10 10 microlitersmicroliters of oil to 10of oil to 10--ml of solvent in the ml of solvent in the ml of solvent in the ml of solvent in the graduated cylinder graduated cylinder

First Standard: First Standard: 100 ppm100 ppm

�� Add 10Add 10--ml of solvent to ml of solvent to the 10the 10--ml graduated ml graduated cylindercylinder

�� Using the syringe add Using the syringe add 10 10 microlitersmicroliters of oil to 10of oil to 10--ml of solvent in the ml of solvent in the ml of solvent in the ml of solvent in the graduated cylinder graduated cylinder

�� Pour this standard into Pour this standard into a vial labeled “100 a vial labeled “100 ppmppm””

First Standard: First Standard: 100 ppm100 ppm

�� Add 10Add 10--ml of solvent to ml of solvent to the 10the 10--ml graduated ml graduated cylindercylinder

�� Using the syringe add Using the syringe add 10 10 microlitersmicroliters of oil to 10of oil to 10--ml of solvent in the ml of solvent in the ml of solvent in the ml of solvent in the graduated cylinder graduated cylinder

�� Pour this standard into Pour this standard into a vial labeled “100 a vial labeled “100 ppmppm””

��Shake to mixShake to mix

Second Standard: Second Standard: 50 ppm50 ppm

� Pour 5Pour 5--ml of the 100 ml of the 100 ppmppm standard back into the standard back into the 1010--ml graduated cylinderml graduated cylinder

Second Standard: Second Standard: 50 ppm50 ppm

�� Pour 5Pour 5--ml of the 100 ml of the 100 ppmppm standard back into the standard back into the 1010--ml graduated cylinderml graduated cylinder

�� Fill the cylinder to 10Fill the cylinder to 10--ml with clean solventml with clean solvent

Second Standard: Second Standard: 50 ppm50 ppm

�� Pour 5Pour 5--ml of the 100 ml of the 100 ppmppm standard back into the standard back into the 1010--ml graduated cylinderml graduated cylinder

�� Fill the cylinder to 10Fill the cylinder to 10--ml with clean solventml with clean solvent

�� This will cut the 100 This will cut the 100 ppmppm standard in half to be 50 standard in half to be 50 ppmppm

�� Pour this standard into a vial labeled “50 Pour this standard into a vial labeled “50 ppmppm””

�� Shake to mixShake to mix

Third Standard: Third Standard: 25 ppm25 ppm

�� Pour 5Pour 5--ml of the 50 ml of the 50 ppmppm standard back into the standard back into the 1010--ml graduated cylinderml graduated cylinder

�� Fill the cylinder to 10Fill the cylinder to 10--ml with clean solventml with clean solvent

Third Standard: Third Standard: 25 ppm25 ppm

�� Pour 5Pour 5--ml of the 50 ml of the 50 ppmppm standard back into the standard back into the 1010--ml graduated cylinderml graduated cylinder

�� Fill the cylinder to 10Fill the cylinder to 10--ml with clean solventml with clean solvent

�� This will cut the 50 This will cut the 50 ppmppm standard in half to be 25 standard in half to be 25 ppmppm

�� Pour this standard into a vial labeled “25 Pour this standard into a vial labeled “25 ppmppm””

Calibration to Prepared StandardsCalibration to Prepared Standards

�� Make sure Make sure InfraCalInfraCal has been on for has been on for

1 hour1 hour

�� Make sure sample plate is cleanMake sure sample plate is clean�� Make sure sample plate is cleanMake sure sample plate is clean

�� Zero Zero InfraCalInfraCal

Cleaning the Cleaning the InfraCalInfraCalHATRHATR--T2 Trough CrystalT2 Trough Crystal

�� Add enough solvent to Add enough solvent to cover crystalcover crystal

�� Wipe slowly across the Wipe slowly across the �� Wipe slowly across the Wipe slowly across the crystal in crystal in one directionone direction, , wiping back and forth wiping back and forth tends to spread residual tends to spread residual oiloil

�� For high TOG/TPH For high TOG/TPH levels, repeat cleaning levels, repeat cleaning

2 or 3 times2 or 3 times

ZeroingZeroing

�� Press and hold the Press and hold the ZEROZERO button until the button until the display reads display reads bALbAL..

RecallZEROCAL

RUN

bAL

ZeroingZeroing

�� A multiplier value to 3 decimal places will be A multiplier value to 3 decimal places will be displayed when zero is established. The actual displayed when zero is established. The actual value is only of interest when reporting value is only of interest when reporting problems to the factoryproblems to the factory

RecallZEROCAL

RUN

1.267

ZeroingZeroing

�� Press Press RUNRUN. The display should read 00 . The display should read 00 ++ 02 02 If not, repeat the zero processIf not, repeat the zero process

RecallZEROCAL

RUN

00

Calibration to Prepared StandardsCalibration to Prepared Standards

�� Run each standard at least 3 times on the Run each standard at least 3 times on the

InfraCalInfraCal

�� Average results for each standardAverage results for each standard

�� Enter averaged results under the “A” in the Enter averaged results under the “A” in the

manual on page 13 or 14 and the manual on page 13 or 14 and the

corresponding calibration value in the C corresponding calibration value in the C

columncolumn

Example Calibration TableExample Calibration Table

AA

AbsorbanceAbsorbance

CC

Calibration Calibration

StandardStandard

AO1= 42AO1= 42 CO1= 25CO1= 25

AO2= 81AO2= 81 CO2= 50CO2= 50

AO3= 149AO3= 149 CO3= 100CO3= 100

Entering Values into EDIT programEntering Values into EDIT program

Make sure Cal Lock switch on the back of the InfraCal is in the “I” position

+

Made In U.S.A.

EN 61010-1

EN 55022 Class B

EN 50082-1

Serial #

�� Press the Press the CALCAL button for two seconds, button for two seconds, until until CAL CAL appears on the displayappears on the display

CAL

RecallZEROCAL

RUN

�� Press Press RECALLRECALL until until EditEdit is displayedis displayed

Edit

RecallZEROCAL

RUN

3

�� Press Press CAL CAL and the display will read and the display will read n= n=

for a short timefor a short time

n=3

RecallZEROCAL

RUN

n=

3

�� Set Set n= n= to the number standards using the to the number standards using the up and down arrowsup and down arrows

n=3

RecallZEROCAL

RUN

n=

3

�� Set Set n= n= to the number standards using the to the number standards using the up and down arrows up and down arrows (for our example it (for our example it will be 3)will be 3)

33

RecallZEROCAL

RUN

3

�� Press CAL and the display will read Press CAL and the display will read A01=A01=for a short time for a short time

A01

RecallZEROCAL

RUN

A01

AbsorbanceAbsorbance Calibration Calibration

StandardStandard

AO1= 42AO1= 42 CO1= 25CO1= 25

� Using the up and down arrows, scroll to the first absorbance value (for our example it will be 42)

AO1= 42AO1= 42 CO1= 25CO1= 25

AO2= 81AO2= 81 CO2= 50CO2= 50

AO3= 149AO3= 149 CO3= 100CO3= 100

42

� Using the up and down arrows, scroll to the first absorbance value (for our example it will be 42)

RecallZEROCAL

RUN

42

�� Press Press CALCAL again and the display will read again and the display will read C01=C01=

C01

RecallZEROCAL

RUN

C01

AbsorbanceAbsorbance Calibration Calibration

StandardStandard

AO1= 42AO1= 42 CO1= 25CO1= 25

�� Using the up and down arrows, scroll to the first Using the up and down arrows, scroll to the first calibration value calibration value (for our example it will be 25)(for our example it will be 25)

CO1= 25CO1= 25

AO2= 81AO2= 81 CO2= 50CO2= 50

AO3= 149AO3= 149 CO3= 100CO3= 100

25

�� Using the up and down arrows, scroll to the first Using the up and down arrows, scroll to the first calibration value calibration value (for our example it will be 25)(for our example it will be 25)

RecallZEROCAL

RUN

25

InfraCalInfraCal TOG/TPH AnalyzerTOG/TPH AnalyzerCalibrationCalibration

For questions please contact us at:For questions please contact us at:[email protected]@WilksIR.com, or 203, or 203--855855--91369136