ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse...1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: Pico Product #: 473L

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: Pico

Product #: 473L Series

Issue Date: August 29, 2013

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,

2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

<Global EHS Specialist>

(1) Parts, sub-materials and unit parts

This document covers the Pico RoHS-Compliant series products manufactured by

Littelfuse, Inc.

＜ Raw Materials Used

Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1

Remarks：

Pb (lead) contained in the high temperature melting solder > 85% and is categorized as

exempt under section 7a of the RoHS Annex.

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 SIKOR 410 (909-371) Ceramic Tube - Body 3-31

2 082xxx-001 Element – Cu99.9MSn 32-35

3 RK-3-K71 (692320) Solder 36-41

4 910-xxx (910-271) Caps & Lead Assay 42-47

5 648102 Yarn 48-54

6 648106-001 Yarn 55-62

7 648112-001 Yarn 63-70

8 087234

(old part number 087340) Epoxy Powder (HF Gold) 71-80

No. : CE/2013/13197D e.2O13lO1l22 Page: 1 of 29

MULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE 1 5' 91207 LAUF

SignaturetidFor QuePlease with scs

m

t lllllllllll

Tho following sample(s) wae/were submitted and identifiod by/on behalf of the client as:

Test RePortCERAMTEC GMBHGESCHAFTSBEREICH

Sample DescriptionStyle/ltem No.Sample Receiving DateTesting Period

CERAMICstKoR c41020131111420131 1 l1 4 r o 2013101 122

Please rcfer to next Page(s)

Bas€d on th€ perfomed tes15 on submitted-samples the test results of CaTilt: llf Iill."". i"riuur""t cnromium cr(vt), pBBs and PBDES comply with the limits as set Dy'*iilt

5]rJJ" ior'trcsiEu Annex ll: recastins 200295/Ec

TeBt R€6ult(s)

Concluslon

{tsrw4)

glnd f!. r|d oatlsatst|Iwal{ LlD.

Test RePort No.: CE/2013/'13197 Dale,2113101122 Page:2 d 29

3E$HIFf#R|'",.. MULTTFUNKTT.NSKERAMTK,LuTTPoLD.TMBE 15' e1207 I-AUF

Te3t Result(s)

PART I'IAME No.1 LT.GRAY CERAMIC

ltr] r[ll]llllrlll

lethod MDLR€6ult Limit

Ts€t ltem(s) Unit No.1

2 n.d. 1006admiumlcdt mg/Kg ,\rith reference to lEu bzrzt zvvo 4l

oerformed bv ICPAES2 69 1000

aead (Pb) mgikg with reference to lEu bzrz r. uuuooerformed bv ICP-AES

2 n.o. 1000Mercury (Hg) mg/Rg With reference to IEU bztz tt zwo 4l

.edormed bv ICP-AES.2 n.d. 1000

Fidavater* ctrromium Cr(vt) mg/Kg With reference to IEU oz.rz I zuuo

Derfomed bY W-VIS

Wii6EEi6E6€N- 1 4322. Analysisms oerformed bv GC/MS.

0.003 n.d.EEF iE6zyt uLrtYt Ptuaute) (cesNo.:8548-7) 0.003 n.d.dEFiP (Di- (2-€thylheryl)phthalate) (CAS No: 117-81-7)

vo with reference to EN t45lz. ^tt11'l

,nas Dedormed bY GC/MS0.01 n.d.

o-i6'f ioiisooecyt ptttnatae) (cnsNo.:267614G0)

with €felence to EN rar/2. Arrcrvrl

wa6 oerformed bY GC/MS0.01 n.d.

-tNp (Di-rsononyl phthalate) (cASNo.:28553-124)

o/o With reference to EN l'+r/z Îrdrvrrr

was Derfomed bY GC/MS0.003 n.d.

6NdF (Di-n-octyl Phthalate) (cAsNo.:11744-0)

% With reference ro EN l'rJZ ^rrcrv'''sr:s o€rfomed bY GC/MS.

0.003 n . d .S6FlDibutyt phthalate) (cAs No :u-74-2\

% With rclelence rc EN r4o'' ^r'rt''e

was o€rformed bY GC/MS.'10 n.d.

F;dluorooc'lane sulf onates(PFOS-Acid, Metal Salt' Amide)

mg/Kg /Vith rcbrence rc un ErA oorw'ZOO7. Analysis was Perfomed bY

1 0 n.o.FF6A (A (cAs No.: 335€7-1) mg/xg with €lerence Io uD EF^ eJrv!

2007. Analysis was Perfomed bYI c/Ms

0.5 n,o.F6ii6fr!6rinateo giphenvts (pces)(CAS No.: 1336363)

mgKg With relelence ro ur Er^ rF""

method. Analysis was Performed bYGC/MS.

ffi trffi ffiru*ffi ,$ffi ffi*trffi ffi ffi ffi:ffi ffi Tffi $-*.,---,-,*',',1,1i;:;'i:: l lrn:m::::r';n:M*::l;"*nr::vrJ"*"""^"

.-j--lil l --

Test RePort No. rCE/201313197 O€lle 2O131O1t22 Page: 3 of 29

3E$ilIFfSUR!'"- MuL'FUNKTToN.KERAMTK'LUTTP.LD.TRABE 15' e1207 LAUFr flMllllllll

t ethod MDLResultNo.1

LimitTest ltem(s) Unit

0.5 n.d.Fiilifr Ic,rinatedTerPhenYls(PCTs)

mgKg With r€ference to uu ErA Joauemethod. Analysis was Performed bYGC/MS.

5 n.d.fllorinatodNaPf thatene(PCNs)

mg/kg With rclerence to uD Er^ rlruvmethod. Analysi6 was Performed bYGC/MS

100 n.d.Alkanes, c10-'13, chloro (shortChain Chlodnated Parafiins) (C'ASNo.:8553*41)

mg./Kg With retelence Io ur ErA r*evmethod. Analy6is was Performed bYGC/MS

NegativePVC Analysi9 was Penormeo oY r I r^ a'

FLAME Test.3 n.d.

F6if,EiGfri3e (cr5 t'lo : so-ooo) mg/Kg With reteren@ rc l5u tlzza't\zwe)

Analvsis was p€rformed by HPLC/DAD0.5 n.d.

fi6i6mahyt dibromodiPnenYtmethane (DBBT)

mgKg With retelence Io uJ ErA oz' v"method. Analysis was Performed bY

0.5 n.d.fi 6i6me-m'etnytdictrtorodiptenytmethane (Ugilec121)

mg/kg With reierence rc us Er^ o''""method. Analysis was Pedormed bYGC/MS

wilh refelence to ub Er^ oztue

method. Analysis was Perfomed bY

GC/MS,

0.5 n.d.M6fi 66Eifrll tetrachlorodlpnenylmethane (Ugilec141)

mg/Kg

l.lelooen 50 n,o.ffi areiFnjffi(D (cAs No : I ms/ks14762-94-8) |

With referenc€ to BS EN 14582t2oo7 '

Analysis was Performed bY lC

wrh '"f""C t" DlNaS4o?'1 3 '-

Analysis w€s Pedormed bY GC/FPD

50 n.d.Fa-ifiEild6torine (ct) (cns t.'|o :22537-15-t)

mg/kg

50 n.d.F6ifrGiE6frine 1e4 lcns no :100€7 -32-2\

mgKg

50 n,o-tia-6lEili&ine 1t1 lces No :143f244-8\

mg/Kg

oE-rntc.trn ctlnlgylg:mg/Kg

0.03 n.d.fiib-iEi rinllBn 0.03 n.d.ilfiEnyiT-"(rF mgKg

ffiffi gmffi ffi $ffi,nffi ffi *nffi *$:ffi rffi ffi iitr"-"-''n"*',':ii..llllili: l i'iH:1il#:!il11611#j$i"l$*lfrL;11i1""""""'-

Test Report No. : CE12O13/13197 Dale :20131O1t22 Page: 4of 29

l|r]|||r] l|lrllCERAMTEC GMBHGESCI.TAFTSBEREICHMULTIFUNKTIONSKERAMIK'LUITPOLDSTRABE'1 5' 91 207 tAUF

method MOLResult Limit

Test ltem(s) Unit No.1

Asb€6toe NegativeAdii6trte lcns Ho.: zzs36+e-a; ./"

With reference to EPA 600/R-93i 116method. Analysis '.tas pertormed byStereo Microscope (SM)' Di6pe6ionStaining Polarized Light lMicroscope(DS-PLM) and X-€Y DiffractionSpec'tometer (XRD)

NegativeffiGGleASIor217?-7ql %

NegativeA;ifr;phy ite (CAs No.: 7t536€7- D/o

Negativedi[6iG Pas no.: t zoot -zg-s) ./"

Negatived6ii6iGlds tto:'i zoot-za4 oa

Negative-emolite (cAs No.: 77536-689 %

AZO 3 n.d.ij:.4.AMrNoDl PHENYL (cAs No.92$7-1)

mgftg With reference to Ll-uE ol uz-zAnalvsis was P€rfomed bY GC/MS-

3 n.d.2rlEEIlzrDrtlE (cAS No.: 92-87- mgKg With relerence to LFso oz uz_Z.

Analvsis vras Performed bY GC/MS3 n .d .

5i-cHLoRo-o-ToLUIDINE(CAS No.: 95€9-2)

mg/kg With reference to LFGb uz.uz-zAnalysis was Perfomed bY GC/MS

3 n.o.4}2-NAPHTHYLAMINE (CASNo.:91-59-8)

mg/Kg Nith €i€rence to LFlto 6z.uz_2.\nalveis w€s Performed bY GC/MS

3 n.d.6jmlNoAzoroLUENE (cASNo.:97-56-3)

mg/kg y'Vith reference to Ll_Gb 62 ur-zAnalvsis was Per{omed bY GC/MS

Wiih reference to LFGB 82.(2-2Analvsis was D€rfomed bY GC/MS

3 n.d-6ilfr tvtiNo-q-NlrnorolueNe(CAS No.: 99-55-8)

mg/K9

3 n.d.TjlF:eHLoRoANlLlNE (cAs No.:10647-8)

m9Kg With reference to Ll-uE !z uz_Z.Analvsis e€6 Performed bY GC/MS

3 n.d.E -TSiIMtNoANlsoLE (cAsNo.:615-05-4)

mg/Kg With refelence to Ll_uit oz uz-zAnalvsis was Performed bY GC/MS

3 n.d.9): 4,4-drll,tntoot pHeuvLl,tEtHArue(CAS No.: 101-779

mS/kS With reference to LFrrn oz uz-z

Analysis was Perfomed bY GC/MS

3 n.d.i6t3SotcFtoRoBENzlDlNE(CAS No.: 91-941)

mg/Kg wth €telence ro Lr\rD oz v._''anrlvsis was oerformed bY GC/MS

3 n.d.iili .a'-omelroxrgerlztotre(CAS No.: 119-904)

mgi Kg With relerence ro Lr\rD o. va_''analvsis was oerformed bY GC/MS

3 n.d.ilf

-53io-ifi ernwgevtotne(CAS No.: 119-93-7)

mgKg With reterenc€ Io Lr\rD 04 uz_z'

Analysis ,,vas Per{ormed bY GCiMS

Test RePort No. : CE/20'1:|/13197 Oate 2013101t22 Page: 5 of 29

!:] lrllllllllfllCERAMTEC GMBHGESCHAFTSBEREICHMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5' 91207 LAUF

Method MDLR€6ult Limlt

T6t ltem(5) Unlt No.t3 n.d.

iF)..33LDrMETHYL4,4-DIAMINODIPHENYLMETHANE(CAS No.: 838-88-0)

mg/Kg With refelence to Lf(,t dz uz_zAnalysis was Performed bY GC/MS

3 n.d.fitTcREstDlNE (2-METHoxY-gi,tElHYLeNtLtNo (cns No.,120-71-8)

mg/kg With reteFnce to LruB oz uz-zAnalysis wa6 Performed bY GC/MS

3 n.d.iSITTLMETHYLENE-Bls- (2-CHLOROANILINE) (CAS No.:101-1441

mg/Kg With retelence to Lrsit oz uz-z

Analysis was Per{ormed bY GC/MS

n.d.'16):

No.:4/A'-oXYDIANILINE (CAS10140-4)

mgKg With reference to LFUE !z uz_zAnalvsis ',!as performed by Gc/Ms

3 n .d .rzr-21:+Srl.toonntuuelcnsNo.:139651)

mg/kg With reference lo LFutt or'uz_zAnalysis was Perfomed bY GC/MS-

3 n.d.iEj oLl.JlDlNE (cAs No.r 95-53{)

mgKg With reference to Ll-uE bz uz_zAnalvsis was Performed bY Gc/Ms

3 n.d-IIiZIToLUYLENEDIAMINE(CAS No.: 95-80-7)

mg/kg With rclerence to LFutt oz.uz-zAnalvsis wa6 Performed bY GC/MS'

3 n.d.tdiltTS-TRTMEiHYLANI Ll NE(CAS No.: t3717-7)

mg/Kg With Gterence to Lr(,tt oz.uz-u'Analvsi6 was Performed bY GC/MS'

n.d.@nrstotNe (cls tto.: so04-0)

mg/Kg With reference io LFUE sz uz_Z.Analvsis was Performed bY GC/MS'

3 n.d.ttT-AMtNoAzoBENZENE(CAs No.: 60-09-3)

mgftg with rcFrence to Lr\tD oz uz-.Analvsis was Dedormed bY GC/MS

3 n.d.-2j-xYLrD[.lE (cAs No.: 95-6&1)

mg/Kg With relerence rc LFstt oz.vz_z'Analvsis was Perfomed bY GC/MS'

3 n.d.'AIZEXYLIDINE (cAs No : 87-62-7)

mg/Kg with reference lo Ll_utt oz,uz-z.Analvsi6 w€s Performed bY GC/MS'

cFc'3 ((;nloror|uorcEaruvrr',

Group I n.d.Efri-rdtuorocarton-tt lcAs t'to :75694)

mgKg With retelence rc u! Er^ ou' 'method. Analysis was Per{ormed bYGC/MS.

1 n.d.dfi66iluorocarbon-'12 (CnS uo :75-71€)

mg/Kg With lelelence ro uD ErA ouz '

method. Analysis was P€rformed bY

GC/MS,

sir;r3:i#irr:ryr5's,,"''riirfl{]ii;fim:ilH;,;|f;TTild,j;'li*'ii'flfiffiffi1;;ilffi#.ffidffi1l;!#t{iil'i#,;r.r''$*utru,rfu+ii*i'*l+li.+uli*l,pqa+,r*i?l'ff*li'fr#f+#*ir#"*i1,;*i,,":ffilla${#}iffiltt}*illffi.Ttrffi"r r:",,,:-.li'i;:;tfri:,ti$f?*r*trf$*"$''{i1i:*ijs fl fl trJn"':ll,ilx;'$'l :li,Hff#jilffiitf,'$"1i+4il*;#f,iffrf$i"'J$ffft*r"ffimi#r:*F"ffilm*l'**':;'gin$uii"****;m:r""ru;wr'gs;

Test Report No.:CE/2013/'13197Oale :2013101122 P a g e : 6 o f 2 9

Itr|l[ttl]lll[lllCERAMTEC GMBHeEsCHliiseEnercFt t/tuLTtFUNKTIoNsKERAMIK,LUITPoLDaTRABE 15, 91207 LAUF

T€al ltem(s) Unit Mdhod MDLResull LimitNo.1

Florof luorocarbon-1 1 3 ICAS No :76-13-1)

mg/kg fv n-reference to US EPA 502'1method. Analysis was Performed bYGC/MS.

n.d.

ehbrofluorocalbon-1 14 (CAs No.:76-1+2\

dhf 6ror1id;46fi:i15id5-Nt76-15-3)

mg/Kg With reference to US EPA 5021method. Analy€is wa6 Perfomed bYGC/MS.

n.d.

Wittr reference to Us EPA 5021method. Analysis was Pedormed bYGC/MS,

't n.d.mg/Kl

e#i;a-"--aim"--75-724'

wth referenc€ to us EPA 5021method. Analysis wEs Performed bYGC/MS.

1 n.d.mg/Kg

Chlorofluorocarbon-11 1 (CAS No :3545e3)

mg/kg With reference to US EPA 5021method. Analysis wes Performed bYGC/MS.

n.d.

ffiroRuorocaroon-t t 2 (CnS No :76-12-0)

mgftg WilFreference to US EPA 5021method. Analysis \Aras Pedormed bYcc/Ms.

n.d.

eFi;-rolhlorofl uorocarbon-211(cAsNo:422-784)

mg/K9 With ieference to US EPA 5021method. Analysis $/as Performed bYGC/MS.

1 n,o.

-hlorofl uorocarbon-212(cAsNo3182-2Cl )

mg/kg WiG;;i;Ence to us EPA 5021 | 1method. Analysi6was Perfomed bY IGC/t S. I

n.d.

n-d.dSrodiio'ocarbdtaaTcAs No : I ms/ks2354-06-5) |

with reference to us EFA ouz Imethod. Analysis was Perfomecl bYGC/MS.

'1 n.d.dfiloffiior'o;rborl-rl4 (cAs No r I mgikg2925531-0) I

With retelence to un Er^ ouz Imethod. Analysis was Performed bYGC/MS.

I n.d.6fri66iluorocarton-215 lCAs No.:425943-2)

mg/Kg With referenc€ to us El"A cul Imethod. Analysis was P€rformed bYGC/MS.

effiffi ffi *ffi ffi ffi hffi$xrgffi m'*s,r..i,$1'1,!r!Fs.i

l@ _-

*;;;;;;_-

Test Report No.:CE/201313197 Dale:2013101122 Page: 7 of 29

CERAMTEC GMBHGESCHAFTSBEREICH

[]Lllllllllllllll

MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5, 91207 LAUF

Test ltem(3) unit Method MDLR€sult LimitNo.'ln-d.

Ctrtorottuorocarlon-Z t 6 lCnS No :ael-97-2)

mgKg With €lerence to us EFA ouz Imethod- Analysis was perfonned byGC/MS.

1 n.d.dfri;rofl uorocarbon-217 (cAs No.:422-88-6)

mgKg Wlth reference to uu Et'A suz Imethod. Analysis was Perfomecl bYGC/MS.

HCFCs{Hvdrochlo,ofl uorccabons}iiffig{) with reference to us EPA 5021


1 n.o.mtyKg

n.d.FtcFG22 (CAS No.: 75-45€) m9Kg With €lerence to us EFA ouz I

method. Analysis wa6 Pedomed bYGC/MS.

1 n.d.FEFElgt (ces No.: s9+zM)

frEFdr7il6esMlasa-145

mgKg With reference to us El'A cuz Imethod. Analysis was Performed bYGC/MS.Wttr reference to US EPA s02tmethod. Analy6is was Perfomed bYGC/MS.

1 n.d.mgKg

Wiitr reference to US EPA 5021m€thod- Analysis was Perfoamed bYGC/MS.

I n.d.FEffi-tzz (ces Ho.: as+-zl'z) m9Kg

n.o.ncr-e-tzg (cns uo.: :00-gg-z) mo/kq lwith reference to ub Ei'A ouz I

lmethod. Analysis was performed bylGc/Ms.

1 n.d.FdF6liZ (c,qS Ho, zg3z+s-o) mo/ko lwith reference to us Er/A cuz I-

lmethod. Analysiswas performed bylecnts.

1 n.d.FEml tcAS No.: 359-28-4) mo/ko lwith reference to us Er/A cuzl- -

lmetJtod Analysis was performed by

n .d .ftFdl32FCl32b (CAS No.: 1649-08-7)mo/ko lwith reference to us El'A cuz I

lmethod. Analysi6 wEs performed byIGC/MS.

pffi immffi ffiffi *gffi ffi$ffi gnrtffi trmhffi'.-ffi,;irr; tru1riri _,__*,__lhe5cs;;--

Test RePort No.: CE/2013/13197 Dale:2o13to1122 Page: 8 of 29

CERAMTEC GMBHGESCFIAFTSBEREICH

r l[tll llllllll

MULTIFUNKTIONSKERAMIK,LUITPOLOSTRABE'1 5, 91 207 LAUF

Tesl ltom(s) Unit Method | [loLR€ult LimitNo.l

1 n.o.Ftc-fl-t:ga (ces no.: zs-aa-z) mg/Kg With eference to us EPA 5uz I

m€thod. Analysis was Pe ormed bYGC/MS.

HCFC-141b (CAS No.: 1717-00€) m9Kg with refere.nce to us EPA 5021method- Analysis was Pedomed bYGC/MS.

I n.d.

HCFC-142b (CAS No.: 7S8-3) mg/Kg WlFreference to Us EPA 5021method. Analysis was Pedomed bYGC/rrs.

1 n.d.

HCFG22i (CAS No.: 422-264) mg/Kg Wlth reference to US EPA 5021method. Analysi6 w€s Performed bYGC/MS.

n.d.

HCFC-222 (CAS No.: 422-491 ) mg/kg Wittr reference to US EPA 502 1method. Analysis uras per{orm€d byGC/MS,

n.d.

FEFe-zx (cas uo.: +z-s2€)

trcrr-rl-4@SI6i"tEj-

FeFea2sA]fiSTo:At@

mgi Kg W-lth ref€rence to US EPA 5021method. Analysis was Performed bYcc/Ms.

I n.d.

mgKg Wr1fr reterence to US ePA Sozlmethod. Analysis was Performed bYGC/MS.

I n-d.

mgKg WiifErence to us EPA 5021m€thod- AnalFis was Performed bYGC/MS.

1 n-d.

n.d.FEFe-22sco (cns no.: soz-s+t) mgKg With reference to us EPA cuz I

method. Analy6is was Pedormed bYGC/MS.

1 n.d.HCFG226 (CAS No.: 431-87-8) msyKg With refelence to ub El'A ouz I

method. Analysis uras performed byGC/MS.

1 n.d.FEFe-zat lceS No.: 4zt-91-:1 mg/kg with reference to u5 ErA ouz I

method. Analysis wa6 Perfomed bY

GC/MS.n.d.

;EFe-232 (cAs No.: 460-89-9) mgKg With reference to us EPA 5uz Imethod. Analy6is was Perfomed bYGC/MS,

e$ffi *!ffi iffi rmmffilmm*ffi Nmrursnffi,!!1e||)$.,i i , "

| ,.so2sr2,, +$6102r,,sr,! ' *"q'i"

;;;;.;;;;;;;;;

Test RePort No.:CE/201313197 Datet2113rc1f22 Page: I of 29

3t$ilfti#RE,"t MULTTFuNKTToNsKEôMTK'LUrrPoLDsr*oBE 1 5' el 207 LAUF!]L[lrl]llllll|l

lr.thod MDLR66ult Limit

Test lt6m(8) Unit No.l

Wii[EEnce to us EPA 5021method. Analysis was Performed bYGC/MS.

1 n.d.HcF-c-233 (cAs No.: 7125-84-0) mgKg

WiifrErence to us ePn soztmethod. Analysis w€s Pedormed bYGC/MS.

1 n,o.FEFcTgl (caS ruo.: +zs-9a-s) mg/K9

n . d .-G235(cAsNo.:460-924)

F-crJ--i@Hdi67z5

mg/kg With lelerence to uJ Er^ ouz 'method. Analysis was Performed bYGC/MS.with referenc€ to us EFA cuz Imethod. Analy6is was Performed bYGC/MS.

1 n.d.mgKg

with refe€nce to us EFA ouz Imethod. Analysis was Pe orm€d bYGC/MS.

1 n.d.FicFCZz (crS t'to.: +eo6lg) mg/Kg

1 n.d.HCFC-243 (CAS No : 460-69-5) mg/lg With reterence lo uD Er ovzI


n.d.lCFC-244 mg/Kg Nith reference to us Er^ ouz I

nethod. Analysis lvas Pedormed bYsc/Ms.

I n.d.fcrJ:idE-No-.4r1 a1{) I ms/ks With rcference to us Et'A cuz I

method. Analysis was Pedorm€d bYGC/MS.

1 n.d.FdFe-25G252 (cAs No.; E19-ool) mgftg With €ference to u! ErA euz '

method. Analysis was Perfomed bYGC/MS.

n.o.FdFdzsg (cls r'lo.: aoo-gs-s) mg/Kg With reference to us Et'^ cuz I

method. Analysis was Performed bYcc/Ms.

I n.d.F6FdET tcAs llo : +20-e7'3) m9/Kg With reielence lo uo ErA ou' I

method. Analysis was Perfomecl bYGC/MS.Wii6E6rence to us ePe sozlmethod. Analysis was Performed bYGC/MS.

1 n.d.F6F.lldifces No : azr{z-o3) mg/kg

fl ir,,ffi #irllflTrri+*$i#{1fr#ffr ,#ff fi,Hil]ffill]ffi S,ffi"ffi{#ni#;#'r*."Hx x:r"I'-fi.";iH.",f,::T"?i:$:,ls"i iiiil{#i}#ff.s"i""#l'}r*sti"fF;f "rF+#ilq-fl;'h,ffi t{.li:*r#in$i1i':*i$;".ffi "+'""ry;*;l*r'rlx*r!rri&"tlî:i':i:i**-*':s:. l;:s'.*;*l'1":,s-i:ifiiir'*.t$ffiir*',$i,[Ffffii#l.Tf"ffi'$ rs's"{:}F*!#$iffi#i'l'l;[s,rsrffi "s,:ffi x1l'1i]ffisll'g;

Test Report No. : CE/2013/13197 D.f(e : 2013101122 Page : 10 of 29


l|][llllllllllfll

MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE'I 5, 91207 LAUF

Test ltem(a) Unit lrethod MOLResult LlmitNo.l

HCFC-271 (CAS No.: 430-55-7) mg/Kg Wttr reference to us EPA 5021method. Analy6is was Performed bYGCiMS.

n.d.

HalonsHalnn-1211 (CAS No.: 353-59-3) m9Kg With r€ference to US EPA 5021

method. Analysis was Performed bYGC/MS,

n.d.

1 n.d.Halon-'1301(CAS No : 7563-8) mg/Kg

1 n.o.Fi,alon-2402 (CAS No.r 124-7+a mgKg

eHcs (chlorlnato hydrocarbon)1J J 2-Tetrachloroethane (CASNo.:630-20$)

mg/kg With reference to US EPA 5021method. Analysis ,r/as Pedormed bYGC/MS.

'1 n.d.

1 Jl,1-Trichloroethane (CAs No :71-55€)

mgKg Wttr rete.rence to US ePn SOZImethod. Analy6is wa6 Perfomed bYGC/MS,

1 n.d.

m!yKg Wittr reference to US EPA 5021method. Analy6is wa6 Perfomed bYGC/MS.

n.d.lF-Tetrachloroethane(cAsNo.:7&34-5)

m-Trichloroethane (CAs No :79-00-5)

m9Kg w-lth reference to us EPA 5021method. Analysis was Performed bYcc/Ms.

n.d.

l75i-cnooettlane lcns uo.: z+34-3)

fr@lWith reference to Us EPA 5021lmethod. Analysis was Performed bylecnls.

1 n.d.

1 n-d.iJ5ictriDictrloroettrene (CAs No. : zs-354)

mg/r(g with ref€€nce to u5 EFA suz Imethod. Analysis was Performed bYGC/MS.

n.o.i toropopene (cnS Ho:56&5&6)

mg/kg With retelence to us ErA ouz Imethod. Analysis was Performed bYGC/MS.

1 n.d.TllSTrichloropropane (CAS No :96-18-4)

iFdEffiffihan-NGl5Til107{&2)

m9Kg With refelence to us EFA cuz Imethod. Analysis was Perfomed bYGC/MS.WiifrErence io Us EPA 5021method. Analysis was Performed bYGC/MS.

1 n,o.mg/Kg

itt,f#,iiil[ffi ii1il:" l#fr ,lii:d;.,H[TJ"fii*ird--*-+t.":##gtr*k;ti:Hffi s#,r{l*tr*B!ff 'f:lF*r'r*:, ild:.s*ltl;u"*i[*,fl1:nr{L{1#*rl"ill1il'FiiH:f{HH$ti#il?:i.$iffiiii#.Fffifiil}il{ri*;ir***:r,lii$id***:**iffi r #"#r!tr['iL1 rii!!''if. liitn:Lp*s rofi.:1.#xr*r"?j,#i"*:ii*ili;B:$idfu q; #::;r;ir."" ;i#m$:Ci*''mis.":1cffi:lF"# y15,:n"r*$'#twiiru;srjiir; ilia'"Hirr"i;; ;ni

scsI

Test Report No. : CE/2013,/13'197 Dale : 2013101122 Page : 11 of 29

tlltl[tlllllllllllCERAMTEC GMBHeEl-Cirniiseinercn MulrtFuNKTIoNSKERAMlK,LUlrPoLDsrMBE ls' e1207 LAUF

Test ltem(6)

It6ichi"rop'opane@El6l78€7-5)

unlt Mothod MDLRe6ult LimltNo.t

mg/Kg Witfr reference to US EPA 5021method. Analysis was Performed bYGC/MS.

n.d.

1.lDi-chloroprcpane (CAS No :142-28-S)

mg/kg WilFE-ference to Us EPn 502tmethod. Analysis was Performed bYGC/MS.

1 n.d.

22Dichloropropane (CAS No.:594-2O-7)

caffiG.chr#ae-i6ESN".-56-23-5)

6f,Eroeiffild5l6'l7tdo-:5

mg/Kg With reference to US EPA 502 1method- Analysis v€s Performed bYGC/MS.

I n.d.

m9Kg Wiif, r*erence io us EPn so2tmethod. Analysis was Performed bYGC/MS.

1 n.d.

Wittr reterence to US EPn S021method. Analysis was Perforned bYcc/Ms.

n.d.mgKg

n.d.dfrlorolorm (cAS No.: 67€6-3)

ehioofiaffiefJ-?dSI6i?6i3)

mgKg With reference to Us El'A 5uzrmethod. Analy8is was Perfomed bYGC/MS.Wlrreference to uS EPA 502'lmethod- Analysis wa6 Pedomed bY

GC/MS.

1 n.d.mgKg

1 n.d.FTZDicfiloroethe'ie (cAS No : I mg/kg15S59-2) |

Nith €lerence to uu ErA 3uz Inethod. Analysis lvas performed by3C/MS.

n.d-fll3orchtrcropropene(cAsNo.:1 0061 -0't -s)

mgftg uvith reference to uu EPA cuz Imethod. Analysis was Performed bYcc/Ms.

1 n.d.FEiicn-orooutaoiene(cnsno.,8748-3)

mgKg With retelence ro u! ErA ouz Imethod. Analy6is was Perfomed bY(tc/Ms.

1 n,o.M-alt;;e cNoride (cAs No.: 75-09-2)

mg/kg With lelelence rc un Er ouz Imethod. Analysi6 was Performed bYGCruS

n.d.GiilZfi6Eiene Prs Ho: tzz-184)

myKg With aeference to uu El'A cuz Imethod. Analysis was Perfomed bYcc/Ms.

u;,;rrTiljjtfil*Htj,$lm:rrHirilsTTj."rllT'ili.iifiilffiffi*&'#iilffi;ffiffi;rilil,i[trs$ ilI*.'J.",3#!f iAf"sFlii',{{iir*}fii;F#n**i*r ;rm,"# +:r*":',"xr4i;rF*iiJJfr *#"#*ir*i: *i +fi]",ftfi;;, " 6,"d trh€ c.m

#ru;ri ; i,:"; li,:.* ii:"ii :s *.r1iti.tri$'fi1'sft+iFr'-'d#-1ii*,ffif;#$ft*,*r*rl!ff ,H#,i"1'l"lirjli:;i#l+:i:ffi.Fitr$,$"l;riutmoiiv ' 'o e "gP","o

'tY i'

H**flTiffi$::,ffi1s};*#i-ffit*dil"Yftii*,###H#i*,s"ffi[r*r"xr'*iii:""xru#,xn:,*u:tru:r*"!i5;T- *'fl g":,r" :lr,"^:x S'l 9;,

Test Report No.: CE2O13/13197 Dale 2013101122 Page | 12 of 29

CERAMTEC GMBHeEsiHnprseenetcH MULTIFUNKTIoNSKERAI/IlK'LUITPoLDSTMBE 1s, 91207 LAUF

|ll|rullllllllllll

Te3t ltem(s) Unit ir.thod MOLRoault LimitNo.l

tran+1,2-Dichloroethene (CASNo.: 156$0-5)

mg/Kg !{tith reference to US EPA 5021method. Analy8is wa6 Perfomed bYGC/MS.

n.d.

iEiI13-Dichloropropene(cASNo.:10061-02€)

mdks With reterence to US EPA 5021method. Analysis was Perfo.med bYGC/MS.

n-o.

Trichloroethylene (CAS No.: 7$01"6)

mg/Kg With reference to US EPA 5021method. Analysis was Perfomed bYGC/MS.

1 n.d.

sum ot PBB8 msyKg5

n.o, 1000n.d.

Monoblomobiphenyl m!yKg

Dibromobiphenyl mg/kg n.d.

5 n.d.Tribromobiphenyl m9Kg

fet€bromobiPhenyl mg/kg 5 n.d.n.d.

PentabrcmobiPhenyl mgKgn.d.

Hexabromobiphenyl mg/Kg

Heptabromobiphenyl mg/kg 5 n.o.5 n.d.

Octabrornobiphenyl mgKg5 n.d.

NonabromobiPhenYl mg/Kgn.d.

Oecabromobiphenyl mg/kgn.d. '1000

surn of PBDES mgKg5 n.d.

Monobromodiphenyl ether mgKg5 n.d.

Dibrcmodiphenyl ether mg/Kg5 n.d-

iribromodiphenyl ether mgikg5 n-o.

TetrabromodiPhenYl ether mg/K95 n.d.

Pentabromodiphenyl ether mgKg5 n.d.

HexabromodiPhenyl ether mdkg5 n.d.

FeDtabromodiphenyl ether mgKg5 n.d.

Octabromodiphenyl ether mg./Kg5 n.d-

FonabromodiPhenylether mg/Kg5 n.d.

becabrornodiPhenyl ether mgftg

i$ii-&1ff;ri'#F,[liilH.fi;,"]:f,ff:tury'jiH:TTi:Tii:::liiiifffi[ff"*ffi;.iffi.ffi'll#;ffiiil;j#Tl"sj:il+ffi-##*i1ffi k"#;l"{:ffi i:i*$#,H*tr#;iF'll'ilex;It j{i,Hrilils",}ff hi:#ri j,*e#ji:T#.["I#td";iLf f p.mmq:,ffi :lr*p.l:jrugmffi,*r,r,-;iit*"i'*,**rffi,[$,$:Ai idi!#S'r]iitii;"i$',S*#$ge{ii::silFlltF+€i}'sT'$Si#,dtttulllll;#iiilB;;"rir"*r.i#:xii;'J**:#ur5""pffr*c:N4fuiFi . l /Tdw.dl l j

i;;p.ni tuy -*'ho-d,b.d- be'"/-

Test RePort No. : CE201 3/1 31 97 DaIe | 2O13lUn2 Page : 1 3 of 29

lll| tl]llllllllCERAMTEC GMBHGESCHAFTSBEREICH

Noto :

PFOS Refercnce Information : POPS - (EU) 7572010

Outlawtng PFOS as substances or preparations inadicles o; oarts at a tevel above 0 1%('1000ppm)

MULTIFUNKTIONSKEMMIK,LUITPOLDSTMBE 15, 91207 LAUF

concentrations above O OOIo/o (1Oppm)' in semi-finished producls or

in textiles or other coatgd materials above 1Fg/m'

1. mg/kg = ppm : 0.1wt% = 1000PPm

2. n.d. = Not Detected3. MOL = Method Detection Limit

4 . " - "=No tRegu la ted5. '* = Qualitative analysis (No Unit)

6. Negative = Undetectable / Positive = Detectable

z. f"Jting |."ng" ot ""u"sto€

qualitative analysis i6 from less than O 1olo to 1OO% The judgment criterion: asbestos fibers'u"ingio*d' i""n**"s"Posit ive';asbestosfibersnotbeingfoundisshownas"Negative'-

!$i,il4jirT:..[fi1jiHtj#1ffi*l]i:*H;1',:ili"Jilktrif"i'.,i:,:J#;,'ffiil;'*ruiJ:,il#J*'li[if*r{#H*fr;#.i'r+ri:+iAii*['';i;ti*Fgftii$.*""w"lssffi:'jii+-p#;-YE:l*;q,,'i"ii*t#"fl'#ir';"r:;l;rin"+q"r+'d:;i""*1il'iiii:r:hf:t!,'i*i;.t, :1i+'.tr.:$.x;: ilils,i':iliiei:ilfr!ff .ffii!ri#*#*{t:l';".sr::E}t ?ii{'S!i':*T*., ii'i;l$,*Tf.tr':#ii{'i*$ii*}Tii}ilq##;'i#,{#"s},*:*1f"'l##iiiB:#ir;*+*ii*i::$'*:r;r"":rs;""#'nr'gr;i;;p;ry ev

"n.dhod.d ar.'dim

Test Report No.:CE/2013i/13197 Oetrie:2O13t01122 Page: '14 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK'LUITPOLDSTMBE 1 5, 91 207 LAUF

It] lltrlllllllll

1 ) Thes€ samples were clissolved totally by pre_conditioning mdhod accofding to belo'e flow chart( cr& test method excluded )

Name of the peFon who made measurement: Climbgreat YangName of the pergon in charge of measurement: Troy Chang

2)3)

Sample Material Diqe6tion Acid

$eel. copper, aluminum, solder Aoua reoia. HNO3, HCl, HE H2O,

Glasl HNO3/HF

Gold, platinum, palladium, ceramic Aqu€ regia

Silver HN03

Plastic HzSOr, HzOz, HNos, HC!

Others Added appropdate reagent to totaldig$tion

Note.' : (1) For nonfietallic material,(2) For rEtallic mat€rial' add

add alkaline dige6tion reagent and heat to 9$'95"C '

oure weter and heat to bciling

Add appropriate amountof digestion reagent

Micror/ave digestion wlthHNO3iHCI/HF

Acid dige6tion by suitable aciddepended on difieFnt samPlematerial (as below hble)

Heat to appropriatetgnperature to e)dract

Cool, filter digestatethrough filter1) Alkal iFusion

2) HClto dissolve

Add diphenyl-calbazidefor color development

measurc the absorbanceat 540 nm bY W-VIS

ffi*'trffi#ffiffffi'---t,,-.-*:rl|i 'dt.aE:r)t I'i"ji

I t's60?r,@" f+s6l0.2q" ww4nw -

*.*;;;*

Test Report No.; CE/2013/13197Dale: 2o13101D2 Page : 15 of 29

I]l[ttl]llllllllCERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15, 91207 LAUF

PFOA/PFOS analytical flov, chert of Uliresonic extraction {LC/MS} prcceduro

t Name of the Derson lvho made measurement: Roman WongI Name of the peron in charge of measurement: Troy chang

ffi ff ffi ffi $ffi ffi *r ffi ffiffi ffi ffi#"--ffi ffi.!*:!;,r1!r'it;i|!T:l i,M1or2"^''@o,,,4" !W4nw -;;;**;-

Conc€ntratdDilute Extracted solution

Analysis was performed bY LC/MS

Test Report No. :CE201313197Oale:2013101122Page : 16 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

PCTs analytical flow chart

I Name ofthe person who made m€asurement Barry Tseng! Name of the person in charge of measurement Troy Chang

Data

l[|r[tr] l|llll

,gffiffiffiffiffi$ffimffiffiffi*mffi,!5:*:t l] l la' i i trri: - -----;;; loflhecc'o

Test Report No.: CE/2013/13197 Datet2013lo1l22 Page: 17 of 29

CERAMTEC GMBHcEscxerrseeaetcFr MULTtFUNKTIoNsKEnnMIK'LUITPoLDSTRABE 1 5, 91207 LAUF

PBB,PBOE analytical FLOW CHART

I Name ofthe per6on who made measurcment Rornan Wong

I Name of the pe6on in oharge of measurement Troy chang

It|||lt]llllllll

Fil6t testing process -----'

Optional screen Process ..'.

Confirmation process - .>

: f s.r*n ,nerv*is | !t l

r . . , , . . . . . . . . . 1 . . . ' ' ' . . . . ' ' r

Sample extraction/Soxhlet method

I

ConcentrateJDiluteExtracted solution

Screen analysis

lssue Repod

I Filter I--'_1+

I Analysis by GCTMS I|--..-----------

ffi l$$ffi,f $ffi ffi"m*Nffi siffi ft m*t**-*--ffi- -,__

*,;;;,

Test Report No. : CE/2013i/13'197 O€trle .2013101122 Page | 18 of 29

Itl||lllllllI|lllllCERAMTEC GMBHeEsCH,errsaenercH MuLTtFUNKTIoNSKERAITIK'LUlrPoLDsrRABE l5' 91207 IAUF

PCBS analytical flow chart

I Name ofthe Derson who made measurement: Balry TsengI Name of the berson in charge of measurement Troy Chang

ittr"ffi I;ii:1TRii;ilTl:ld;ilfi*fr*ilitfi $ltHi}5,ri+lllHiff"ili[iffi ;#*##.ft[mffi;l;;*d n "-.d

bv he c"h

$i.i"..r""t#*-n;:rf"i*S,**$$"!iy1ffii;?*ft#6;"i11trdg#;h*14;bii:*ir;;;*"r:::"'*;;r;":i:,"j l,l:.,t1 r r,*,o-"ro.r4ri'.idsdrPa'!-{$nFtqrrwdi/Li

i ' i ri.!ir I riflrt

,*irflF#1Htr":,#ilhffii'#'#r"ft'.1i"tr'*Lq$iii:'H t'ffi*,ffi$;:ff l,:lt^1ffi*,'i^l;t*1T.fr s

Test Report No.: CE/2013/13197 D?'Le:2013101122 Page: 19 of 29


II

Chlorinded Paraffins analytical flow chart

Name of the person who made measurement: Barry TsengName of the person in charge of measurement: Troy Chang

tr|flIllllflrlllllMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5' 91207 LAUF

Data

ffi wmttsffiNffi$rmffi*t--**m':mffi.)!'t:rrtrlt t;".:

Test Report No.: CE/2013/13197 D.f(e 2013101122 Page: 20 of 29


Analysis flow chart for detemination of A3bestog

I Name ofthe peEon who made measurement Victor Kao

r Name of the pe6on in charge of measurement: Wendy Wd

I Rofe]snce method: EPA 600/R-9U1161

Containing Asbestos/Positiv6 Not containing AsbostoyNegatrve

rJl|Ilr]|||llllll


Continue when ploblerns are encountared withD$PLM ancuot for quality assurance pumoses

Asbestos idenffcalron bY X_|aYdiff €ctjon speclrcmetat (XRD)Asbestos identfic€lion by dispersion staining

polaized light micrcscop€ (OS_PLM)

ffi m*mtrffi#ffi ,ruN'w$n'm'sp*mw'm-ffil c4'it..:, j | l i '

Test Report No. : CE/2013/13197 Dale " 2O13lO1n2 Page : 21 of 29


!

t

Analytical flow chart of Organlc'Tin conteni

Name ofthe person who made measurement: Ginny Chen

rrlu[llllllllllllMULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15, 91207 LAUF

Name of the person in charge of measurement: Troy Chang

Da€

ffiiffi#ffiffififfi.ffiffi$Hitr$ffiffin i r l t r i i '

" l r r r f l i 3 r l t

ji*r; ,tNjrr !jtJ

Test Report No. : CE2O1?,/13197 D'l,e t 2013101122 Page : 22 ol 29

CEMMTEC GMBHGESCHAFTSBEREICH

II

PCNS analytical tlow charl

Name ofthe person who made measuremenl: Barry TsengName ofthe;erson in charge of mea6u€menl: Troy Chang

f,]rIltl]llllllll


Data

msrysm;mtffi#ffir ts4tin*Er1ii:t;r;:I i+M€,rprp rrsero,),4" ssFs --- .---#

Test Report No.: CE2013/13197 Dalo 2013101122 Page | 23 of 29

CERAMTEC GMBHGESCI-I,AFTSBEREICH MULTIFUNKTIONSKERA[TIK,LUITPOLDSTRABE '15' 91207 LAUF

Analytical flow chart of phthalato content

I Name of the Derson \lvtlo made measurementl Roman WongI Name of the person in charge of measurement: Troy Chang

1r] [ll: lllllll

Data

m*ffi*w*tn;N{

Test Report No. : CE/2013i/13197 Oate, 2O1A01l22 Peae : 24 of 29

CERAMTEC GMBHGESCHAFTSBEREICH I\4ULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE'1 5, 9'1 207 LAUF

Forflaldehyde anaMical flow chart

I Name of the person who made measurcment Scott Kur Name ofthe person in chaqe d measurement Trcy Chang

( T€6t Method : Us EPA 8315A ' ISO 17226-1 )

Data

ffi ,g+ffi"ffiffi}$gp-ffi *$ii-*,fr$**n'*#$

Sample extraclion

Dedved by DNPH ConcentratdDilute Extractedsolution

Test Report No. rCE/201313197 Dalet201A0122 Paoe : 25 of 29

CEFAMTEC GMBHGESCHAFTSBEREICH

Analysis flow chart for determination of PVc in malerial

t

IName of the person who made mea6urement: Ginny ChenName of the person in chaqe of measu.ement: Troy Chang

MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

UAta

f t ' l ' , : I ; -" , . ; "* . .1. . . ; , . .* ," ;**" . ; i " . ,1 '"") ; ' ' "**;"" ' ' ""- i . , - , ' "" ' "" ' ! "o, .dor** 'h,aa"*q!€-Fi i,ii6iniii;i"in-.n'"i,*.me;;Fnb'i*'ancod@*.,FbdTn'-oo@ft*dM.!!@_'€finisLo;c.dw 'o-'t '." *d in$dr ,$u.5 de ldhe'e. a.v lo@ dr'ffitm ' tadls- "i'crh'co' prv\'rdrssal

miie o r ' 'a*"nq -tv * *hi tr€,m'Bd. r*nraMs tn' F"corr?"so'.6,@1rh'i - ] " i . " " " m ' * e o s t r E , r - ' , q ' o 1 o c J F n . i E o m 1 @ . r oi;;;;;; ;;;ifdd;tr;i;d: 'd!"t ;ii;i;6d* .r h. -ed

". i , r { . r r f r ; 3 3 \ . j

Samole ore-trealment

Sample analyzed by FTIR

Check wave-numbea of C-Clbonding

Test RePortCERAIiITEC GMBHGESCHAFTSBEREICH

No. : CE/201313197Dale :2013101122 Page : 26 of 29

MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15' 91207 LAUFLrm[ llllllllllll

II

DBBT analytlcal flot,v chart

Name of the person who made measurcment: Roman Wongi.iame ot ini berson in cnarge of measuremenl: Troy chang

Data

**$"ir;+:*rsi,*q*'q"rlffi r**fr fgri-dif*rit*;;a;r:iffi t-gffe;*#'-t':';':**,ii$,itji.i"ll*'-*i'*:"tr-;::; :"""K:r;jr?i*".;i#;s"s:"'l#jjJ"'i!'qji:isjqjj:l;

Sample extraction by soxhlet method

ConcentratdDilute Extracled solution

Test Report No.:CE/2013/13197Dal.e:2013101122Page:27 ol 29

CERAMTEC GMBHGESCIIAFTSBEREICH I,1ULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5, 91 207 LAUF

Analytical flow chart of halogen cont€nt

1) Name ofthe Derson who made measu€ment:Rita Chen2) Name of the person in charge of measurement Troy Chang

rl|fittl ttlll

Sample pretreatment / Separation

Weighting and putting 6ample in cell

Orygen Bomb Combustion / Absorption

Dilution to fixed volume

Analysis wa6 per{ormed by lC

ifr '"""$"".,.";,""-."'""**..'I".""i**.'. i"l;:i".f;Ti'"T,lir:;r+s:"r#{*ra.:::l;.l1!",::t:.'a*l;;.?i'.;'L: -v'r;T;;i."1ffii.1::;its:"ft""f.:D"$;;3'ir:i;t* .:ti i ; ; ; i ; ; , ; ; 1 . ; ; . ' ; 1 ; ; n ' j t r eabdc€a t , n . [ do ' ' i ; t . t conp , j / . ' o "? ' r c -o ' 1' - ?d , r @@-m. :biJiii, ']d".i,^;'r'"i ' 'doi.rr"'"t-ib@;''hisfcat-dLha@;b.;i;,66neol'hisdo4mmlism|*/flaiaonderybep]o3eodediob

Test Report No. : CEl2013/13197Oale:2013101n2 Page : 28 of 29

CEMMTEC GMBHGESCHAFTSBEREICH IVULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5, 91 207 LAUF

Analytical flow chart of volatile organic compounds (VOcs)

I Name of the person who made measurement : Chun Wur Name of the pe6on in chafge of measurement : Shinjyh Chen

(Reference method : US EPA 5021)

I|][tl] lllllll

umss o'se *rd so a:J b ].o"f, n' j: 4m re.'d m.ry ! ya ".l* * - .

: :: -*l

:Il:.:::T::l:: I "ihF;odr n,!.srd a Fe cor 'i i.;l "'"-ffil"i,"iil,I,iiiii to-iiiotii,i'ii t",:ar tnoi;. uble. a'fta,ouondid'ro FMo

;t*:'"m*u*;;r'l+*#*;.'*d*q":il;-J *t'dJ"*';:jl;;*xlril!"m;"j,gi'T -";fi?:l:*.":"trF1'"":l'i1\'j, . ' ;;;;i'.d;;;-;;r ji

"d :'n ' n* 'nd or* oa' n' o"

N4r . i F . r v I l i em / i i : , r : . : r . r r : ; 1 i 5N3U

Sample pretreatment

Take sample and put it intoheadspace glasswale.

Bake the sample in the c /en

Analysis was performed by GO/IIS

Test Report No. : CE201913197Date .2013101122Page | 29 of 29

CEMMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAIVIK,LUITPOLDSTRABE'1 5, 91207 LAUF

* The tested sample / pa is marked by an aftow it ifs thown on the photo. '

"' End of Report *'

|l] ttt][]ttt|l

" "RT?: :k . . ' " ,+ " ; " ' i . . ; " " ; " * ; *n"c - . , i . * * " . '5c f rep ' | 'adoF,€dd€ iJb |soL lAJi,J 6,iijni,jî,,nmrooc *,s *riedb .m"roccoFrn; 6;n''odm.{ a' lw {q 6r '.r"n! aT cdd o'!r€'

iil*l:ifl1,"**"r""rr"r::f"*l'++:ii:h,lir.';;"9:no.;u"";',nx"s:l:i;"'"t,1'r'.;' ii llilri4l%leni li:iLflrilT{ie'i;";:b;" r#;.""'s

" hd,'

ii;;fi c; l"ii-n.;i- i;:"f ';e;t;b-i1s morbs6-ero

,i i; i r'ltilrrrFj

L3L97

Test Report Number： SHAH00361401

Authorized by： For intertek testing services Ltd., Shanghai

Jacob Lin General Manager

Page 1 Of 4 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

Applicant： LITTELFUSE,INC. Date： JAN 16, 2013 800 E. NORTHWEST HWY Attn： A.DIVIETRO/D.UNTIEDT

Sample Description： One (1) submitted sample said to be Grey Wire. Item Name ： Wire Tin Plated Cu. Part No. ： Element.

************************************************************************************************************************************************************ Tests Conducted：

As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************

To be continued


Tests Conducted





(Ⅰ) Test Result Summary： Testing Item R esult (ppm)

(1) Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg With 50cm2) Negative (< 0.02)

Testing Item R esult (ppm)

(2) Heavy Metal Cadmium (Cd) content / Plating ND Lead (Pb) content / Plating 60 Mercury (Hg) content / Plating ND Chromium VI (Cr6+) content (mg/kg With 50cm2) / Plating Negative (< 0.02)

Remarks： ppm = parts per million = mg/kg

ND = not detected @ = Due to the insufficient sample area, reduced total sample surface of 10 cm2 was used and the dilution factor

was adjusted accordingly. mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre

Tested components：

(1)Substrate. (2)Plating. Responsibility of Chemist: Dent Fang / Ken He

(Ⅱ) RoHS Requirement：

Restricted substances Limits Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)

The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.

(Ⅲ) Test Method：

Testing item T esting method R eporting limit

Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in Annex B, by boiling water extraction and determined by UV-VIS Spectrophotometer.

0.02 mg/kg with 50cm2

Remark：Reporting limit = Quantitation limit of analyze in sample Date Sample Received：Jan.9, 2013 Testing Period：Jan.9, 2013 to Jan.14, 2013

************************************************************************************************************************************************************ To be continued


Tests Conducted





(Ⅳ) MEASUREMENT FLOWCHART: Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents Reference standard: IEC 62321 edition 1.0:2008 REMARKS： *1: LIST OF APPROPRIATE ACID：

MATERIAL ACID ADDED FOR DIGESTION Polymers HNO 3,HCl,HF,H2O2,H3BO3 Metals HNO 3,HCL,HF Electronics H NO3,HCL,H2O2,HBF4

*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED. ************************************************************************************************************************************************************

To be continued

Sampling/grinding or cutting

Weigh sample and for different material,

digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized water and add Diphenyl-

carbazide solution

Cr6+

Weigh sample andadd organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Negative*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes


Tests Conducted





***********************************************************************************************************************************************************

End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Test Report Number : TWNC00294413

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0294413* Page 1 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jan 17, 2013 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Solder Part Number : 692320 Date Sample Received : Jan 11, 2013 Date Test Started : Jan 11, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Number : TWNC00294413

Test Conducted

*THJ0294413* Page 2 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary: Result

Test Item Unit Test Method Silvery metal

RL

Heavy Metal

Cadmium (Cd) content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) content ppm


882771 2

Mercury (Hg) content ppm


ND 2

Chromium VI (Cr6+) content mg/kg with 50 cm2

With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.

Negative 0.02

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter

Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result.

Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 11, 2013 Test Period : Jan 11, 2013 To Jan 16, 2013


Test Conducted

*THJ0294413* Page 3 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅱ) RoHS Limits: Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm)

Lead (Pb) content 0.1% (1000ppm)

Mercury (Hg) content 0.1% (1000ppm)

Chromium VI (Cr6+) content 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.


Test Conducted

*THJ0294413* Page 4 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008


For different material, digest the sample with appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution


Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved


Test Conducted

*THJ0294413* Page 5 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List of Appropriate Acid： Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as

detected.

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.


Test Conducted

*THJ0294413* Page 6 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo


Authorized by: On Behalf of Intertek Testing Services Taiwan Limited


*THJ0289672* Page 1 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Dec 20, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Caps & Leads Part Number : 910-271 Date Sample Received : Dec 06, 2012 Date Test Started : Dec 13, 2012

Test Conducted :



Test Conducted

*THJ0289672* Page 2 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item (1) (2) (3) (4)

Heavy Metal

Cadmium (Cd) content ND ND ND ND

Lead (Pb) content ND 115 ND ND Mercury (Hg) content ND ND ND ND Chromium VI (Cr6+) content (mg/kg with 50cm2)

Negative (< 0.02)

Negative (< 0.02)

Negative (< 0.02)

Negative (< 0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Tested Components (1) Coppery metal base material (Lead) (2) Silvery plating layer (Lead) (3) Gunmetal metal base material (Cap) (4) Silvery plating layer (Cap)

Responsibility of Chemist :Irene Chiou / Kevin Liu

Date Sample Received : Dec 06, 2012 Test Period : Dec 13, 2012 to Dec 19, 2012

(Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.


Test Conducted

*THJ0289672* Page 3 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content


2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample


Test Conducted

*THJ0289672* Page 4 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008



Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

Cr6+


Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating


Test Conducted

*THJ0289672* Page 5 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List Of Appropriate Acid：

Material Acid Added For Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report



Test Conducted

*THJ0289672* Page 6 of 6



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo

Is!49p94

Applicant IITELFUSE,lNC.8OO E. NORTHWEST HWYAlin: J.DIIIIGLASAN / A.CESISTA JR

One (1) piee of submitted samples eid to be: Whlb yarnPaft Desiplion : INX-DEEPYELLOWPan Number : 818102

Nunbor: I307O207ESHA{102

Oate:Aus.01,2013

As requesred by the applicant, ior dslails €lel to attached page(s).

! hth rcferenc€ to lest melhod of IEC 62321 Edilion 1and maximum conc€nhalion tinits quoted from RoHS20r1l65/EU

8e!{l0:2008 Pass

For Inlenek lesling s€Me Lld., shanghai

1n 7/,"Joy Znou

Inteitek T*tlng Sewic€ Ltd., ShanghalBb* s, Jinlim sdin.s sqEE No.30l vSM Ro!d, sh.nqh.i chha. 20o2s3

tbtr#Fisfr&lrERz\;lt&dBrlrl*8o1 stA&61**EB s 200233

Page '1 of 7

1. Tesl Esuh of RoHS Da€ctive:

Numb6r: l30702O76SHA{02

Elgllib4 E9!!l!

Cadmium {Cd) contsnt (dtg.itg) NO

Lead (Pb) codent (msn(s) NO

Msrcury (Hs) @tenl (mg/kg) ND

chrcmium (Vl) Gra conient (ms/ksxlor non-meta0 ND

Polybrcminaied bjpn€nyls(PBBg) (nE^s)

monobrcmo biphsny's (MonoBB) ND

Dibromo biphenyls (DiBB) NOIdbrcho biphenrs (TdBB) ND

TerEbrcmo biphenyls (IstnBB) NO

Pedabromo biphenYe (PenraBB) ND

Hexabrcmo biphenyls (HexaBB) ND

Heplrbronr biphenYs (HeplaBB) ND

od€brcmo biphenylG (oclaBB) NO

Nonabmmo biphenyb (NonaBB) NO

Decabrcmo biphenyl {D€caBB) NO

PolybrchimGd diphenyl eiheu (PBDES) (nE/kg)

Monobrcmo diphenyl elh€€ (MonoBDE) ND

Dibmmo dipnsnyl elher€ (D|BDE) ND

T.ibrcmo diphenyl eiheF {IriBDE) ND

Tebabrcrb diphenyl ehell (TehBDE) ND

Penlablomodiphenyl elheE(PentaBDE) ND

Hc,€brcmo diphent ef'ers (HexaBDE) ND

Hepiabromo diph€rryl elhe.s (HephBDE) ND

octabromo diphenyl etheB (octaBoE) ND

Nonabrcmo diphenyl €lh€rs (NonaBDE) NO

Oec€brcmo diphenyl elher (D€.aBDE) ND

Remark: ND. not delecied

Intertek Testing Service3 Ltd., sh.nghaisrod B. Jinring Bulins$ squ.€, ib.3or Ysh€n Rood, shanohal, ctitu. 2m233

f.i&*tfP4&tt&taFA;ll&ft€rrrii301 *.tRdlrfiEB r* 200233

P a g e 2 d T

I99CA9E4 Number: l30702O78SHA{02

Tns abovs limits $/€r€ quot€d f.om RoHS Oi.edive 201 1r'6tEu ior homogeneous matedal.

Intertek T$tng Service6 Ltd., shanghaiErod( B, Jd'no 38ro3 sqls, M1 3or Y'Shan Ro/d stulE , Ch@ 200?33

ti&'i*f,E&JlilEllfFa "lt*frerr$8or llG&AraAgB @ 200233

Telophd.: +33 21 3120 6050 F&im

wih reblen€e ro lEc 62321 Ediiion 1.0:2008, by aciddigeslion unlil lh€ lesled sample was tolally dissolved, and

Wf' lebrEnoe lo IEC 62321 Ediiion 1 .0: 2008. bv aciddigestion unril rhe reGred 8€mple was torally di$olved, and

\4fth refeene io IEC 62321 Edition 1 .0: 2008, by aciddigeEtion unlil lhe tested sarnple was lolally dEsolved, anddelennined bv ICPOES.

Wth relelence to |EC62321 Ednron 1.0:2008, by slkalnedrgeslion and delemined by UV-VIS Speclrophotomeler.

Wlh rebrence lo IEC 62321 Edilion 1 .0: 2008, bv solventextraclion and dsbmin€d by Gc/Ms and tunher HPLo@nlimalion when nee66ary.

Polybrcminared biphen9s(PBBS)& polybrominEleddiphenyl elh€E (PBDES)

Page 3 of 7

E4-Esp94 Numb€r: 1107020784HA{02

(D) Messurement ff orchad:

Test for Cd/Pb/Hg/q (V|)/PBA3/PBDE6 @nlenlsReferenca slandad, lEC6232i Edilion 1.0: 2008

Weigh sample and fordifeEnt m.bnal, digesl

Make up wilh deionized walerand add diphenyl-caoazide

"1: list of appropdale acid,

2, lf lhe €sult of root tesl is posilive, Chrcmium Vl $ould be delemined as deleded.

Intertsk Te3ling Servlcos Ltd., ShanghaiBrod( B. .Iiriig Buriid squ.B, irr.Pol YsMn Rord, shanohal, chlno 240233

rEi*qd&fm&teA-rliErtiB Lrrrr301 *e&d$frr,B rl 20033

T.r.phomr +€6 21 6120 6060 F.ermiro: +35 21 61t 9740

P a g e 4 d T

T€.t R.!on

L Test Gsult summary

t{umbor: 130702078SH4-002

I€lino ilem lesuhrppmlND1{O,,tD,,to

Remffk: PPB = Pans p€l million - mg/kgNO = Nd deie.led

Remad(s: Repoding limil - Auanritation limit of analyte in sampte

Dsle campler@iEd: Ju|.26,2013Test ing pedod: Jd.26,2013ToAug.01,2013

T$tino iiem Testino melhod Rebortino limii

Halosen (F, Cl, Br, l) @nient lMth reference 10 EN 14582:2007 bv combustion in a calodmetdc bomband decmi.ed by ion chromarog€phy

InGrtek lesting Services Ltd., ShanghaiBbd s, Jinriro B6im$ s!sE. N0.301 Yrshdi Rdd, sbnshai. chin. 200233

li4xlff;Etfld&*aRAdtsfrEuq€o1 ntE6itr4B ts 200233

T.|.phd.:+3521512060G0Fdim

Page 5 of 7

E4-BePe4

MessuredEni fowchart:

Test for Hglogen @nrenl

Reference nEd'od: EN 14582, 2007

Numbor: 130702078SHA{'02

Sampling/grinding or Cutting

Add absorbent in a Calonmetric bomb & Placeweighed sample In bomb

Fillthe Calorimetric Bomb wilh oxygen

lgnite then leave the Bomb al room lemperature

Any test gpecimen in theCalorimetric Bomb?

TEnsferthe absodent into a Volumetdc flask

Make uo with deionized water

Analyzed by ion Chromatography

Intedek T€ting Se.vice6 Ltd., ShanghalBrod( B, Jinnn! Burhos squarc No aor Ysb |d, shansh'i chiru. 200233

L&id44&fedaFa\.1li4 dE'lrit8o1 3fr EF$*qB& 200233

Page 6 of 7


Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited


*THJ0285760* Page 1 of 8


全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Nov 19, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648106-001 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012

Test Conducted :



Test Conducted

*THJ0285760* Page 2 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test Item White Yarn

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND


Test Conducted

*THJ0285760* Page 3 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test Item White Yarn

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Nov 12, 2012 Test Period : Nov 13, 2012 To Nov 15, 2012

(Ⅱ) RoHS Limits:


Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)



Test Conducted

*THJ0285760* Page 4 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method:

Test Item Test Method Reporting Limit



2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm



Test Conducted

*THJ0285760* Page 5 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation




For non-metal part For metal part


Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample


Negative *2

Substrate Plating




Cr6+



Cd/Pb/Hg

Analyzed by ICP-OES



Test Conducted

*THJ0285760* Page 6 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid：

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4



Test Conducted

*THJ0285760* Page 7 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582

End of Report


Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask



Analyzed by ion chromatography


Test Conducted

*THJ0285760* Page 8 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo




*THJ0285761* Page 1 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Nov 19, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648112-001 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012

Test Conducted :



Test Conducted

*THJ0285761* Page 2 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test Item Submitted Samples

Heavy Metal





Test Conducted

*THJ0285761* Page 3 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test Item Submitted Samples

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND



Date Sample Received : Nov 12, 2012 Test Period : Nov 13, 2012 To Nov 15, 2012

(Ⅱ) RoHS Limits:





Test Conducted

*THJ0285761* Page 4 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method:

Test Item Test Method Reporting Limit



2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm



5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm


50 ppm



Test Conducted

*THJ0285761* Page 5 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410





PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation






Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample


Negative *2

Substrate Plating




Cr6+



Cd/Pb/Hg

Analyzed by ICP-OES



Test Conducted

*THJ0285761* Page 6 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid：




Test Conducted

*THJ0285761* Page 7 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582

End of Report










Test Conducted

*THJ0285761* Page 8 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo




*THJ0289667* Page 1 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Dec 13, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Epoxy Powder - Gold HF

(Old part number is 087340) Part Number : 087234-HF Date Sample Received : Dec 06, 2012 Date Test Started : Dec 06, 2012

Test Conducted :



Test Conducted

*THJ0289667* Page 2 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test Item Yellow powder

Heavy Metal




Halogen Content Fluorine (F) ND Chlorine (Cl) 336 Bromine (Br) ND Iodine (I) ND


Test Conducted

*THJ0289667* Page 3 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test Item Yellow powder

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND



Date Sample Received : Dec 06, 2012 Test Period : Dec 06, 2012 to Dec 11, 2012

(Ⅱ) RoHS Limits:





Test Conducted

*THJ0289667* Page 4 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410




2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm



5 ppm

Polybrominated DiphenylEthers (PBDEs)


5 ppm


Test Conducted

*THJ0289667* Page 5 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410



50 ppm

Phthalates With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.

50 ppm

Hexabromocyclododecane (HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined by GC-MS.

10 ppm



Test Conducted

*THJ0289667* Page 6 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Remarks: *1: List of Appropriate Acid：






PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation






Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample


Negative *2

Substrate Plating




Cr6+



Cd/Pb/Hg

Analyzed by ICP-OES



Test Conducted

*THJ0289667* Page 7 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard：EN 14582









Test Conducted

*THJ0289667* Page 8 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test For Phthalates Contents Reference Method: EN 14372: 2004



By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD


Test Conducted

*THJ0289667* Page 9 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C

End of Report




By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD


Test Conducted

*THJ0289667* Page 10 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo

ICP Test Report Certification Packet - Littelfuse/media/files/littelfuse...1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: Pico Product #: 473L

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