Geohydrological Report, Phase II Uncontrolled Waste Site ...

GEOHYDROLOGICAL REPORT, PHASE II

UNCONTROLLED WASTE SITE INVESTIGATION

DIAMOND VOGEL PAINTS

MAURICE, IOWA

TCI JOB #884719

BOOK 2

30305944111111

Superfund

APPENDIX D

RAW LAB RESULTS

TABLE 1

VOLATILE ORTANIC ANALYSIS (VOA)

DATA SUMMARY

Client: pjt-J

n’:ond—yqgoJ_ -_HDR Sample I.D.: thi.i

Sample Mate ix: Soil Date Collected: 8/28/84

Method No.: DIRECT SPARGE Date Received by Lab:9/1/84

Date Analyzed: 11/6/84

_____j- '/h.g_ ug/hg•: 12.5 B romoine t h an < 11.0 Benzene

______ iJAiP.____Chlcrciiie thane < 15.0 ■ Chlorobenzene5.5 B rcrnodi ch 1 orome thane * 15.0 Toluene

. > c Dibromochlorcmethane < 18.0 Ethylbenzene7.0 Methylene Chloride 12.5 Acrolein

< 11.2 B romofo rm < 12.5 Acrylonitrile

6.8 ___ Ch 1 o ro fo rm * 85.3 Methyl Ethyl iv 7.0 Carbon Tetrachloride 118 Acetone< 12.5 Trich1c ro f1uo romethane

< 12.5 Chloroe thane

< 7.0 1,1 -Dichioroethane

< 7.C 1,2-Dichloroethane

< 5.5 1,1,1-Trichloroethanp

< 12.5 1 ,1 ,2-TrichloreethariP

< 17.3 1,1,2,2-Tetrachloroethanp

< 12.5 Vinyl Chloride

< 7. C 1,1 -Dich1oroethenp

< 4.0 ___ Trans-1,2-Dich1oroethene

< 4.3 Trichlorcethene

•: 10.3 Tet rach1oroethenp

< 12.5 2-Ch1orcethylvinvIpthpr

< 15.0 1,2-Dich1oropropane

•: 12.5 CIS - 1,3-Dich1 cropropene ‘ u

< 12.5 Trans-1,3-Dichlornprnppnp

VOL AT I LE OATAMC ANALYSIS (VOA)

L A i A S 3 M M /; LY

tlient:__ Djaillprid Vogel - HDD____ Sample I.D.:_ (_23-70302-2) TCI 1-2

Sample Matrix:___ Soi 1____________ Date Collected: 8/29/S4

Method No. : DIRECT SPARGE_____ Date Recc-i ved by Lab : 9/1/84


----------‘j.9

< 12.5 E roniomethane

c 12.5 Chloromethane

5.5 B r o m o d i c h 1 o r o; t i e t h a n e

< 7.8 Dib rcmoch1o rometh are

*-■ 7.0 Methylene Chloride

< 11.3 B rorro t g nn

^ 4.0 _ Ch 1 o ro fo mi

< 7.0 Carbon Tetrachloride

- 12.5 T rich1 ore fluoromethane


< 7.0 1,1- Di chi o roe thane

< 7.0 1,2-Dichloroethane

< 9.5 1,1,1-Trichloroethane

< 12.5 1,1,2-Trich1orcethane

< 17.3 1,1,2,2-Tetrachloroethane


< 7.0 1 ,1-Di chloroethene

«: 4.0 T rans-1,2-Dich1oroethene

< 4.3 T rich1c roet hene

< 10.3 Teteach loroethene

< 12.5 2-Ch1oroe thy 1 vinyl ether


< 12.5 .CIS - 1 ,3- Di ch 1 orooropene

< 12.5 Trans-1,3-Dich1oropropene

Benzene

Chlorobenzene

To 1uene

Ethylbenzene

Acrolein

Ac ry 1 on i t r i 1 e

Methyl Ethyl Ketone

Acetone

‘ ‘ u

u 9 / -" a

< 11.0

15.0

< 15.0

■- 1 ; . 0

- 12.5

< 12.5

129

VOLATILE CRT AN 1C ANALYSIS (VOA)

DATA SUMMARY

Client:: Diamond Vogel - HOR

Semple Matrix: Soil

Method No.: DIRECT SPARGE

/

Sample l.p.: (23-70302-3) TC11-4

Date Collected:8/29/84__________ __

Date Received by Lab: 9/1/84

Date Analyzed: 11/6/84_________

ug/Rg pq/Kg

< 12.5 B roino methane <11.0< 12.5 Chloromethane < 15.0

< 5.5 B roniodi ch 1 crometha.ne < 15.0

< 7.8 Dibrc ochloronethane < 1 8. C

< 7.0 Methylene Chloride < 12.5

< 11.6 Bromoform < 12.5

< J.O Cli 1 o rc fo rm < 25.0

< 7.0 Carbon Tetrachloride 9

< 12.5 Trichlorofluoromethane

< 12.5 Chloroethane

< 7.0 1 ,1 -Dichloroethane


< 9.5 1 ,1,1-Trichloroethane

<12.5 1,1,2-Trichioroethane

< 17.3 1 ,1 ,2,2-Tetrachloroethane


< 7.0 1 ,1-Dichloroethene

< 4.0 Trans-1 ,2-Dichioroethene

< 4.8 T rich1oroethene

< 10.3 Tetrachloroethene

< 12.5 2-Ch1oroethv1viny1 ether


< 12.5 CIS - 1 ,3-Dich1oropropene u

< 12.5 Trans-1 ,3-Dich1oropropene

Benzene

Ch1crcbenzene

Toluene

Ethy1 benzene

Acrolein

Acry1 onitrile

Methyl Ethyl

Acetone


DATA SUMMARY

Client: Diamond Vogel - HDR Samp 1 e I .D. : (23-70302-4) TCI 1-5

Sample Matrix: Soil Date Collected: 8/29/84

Method No.: DIRECT SPARGE Date Received by Lab: 9/1/84


pc/Kg ua/Ka

•: 12.5 E rcmoine thane ______ < 11.0 Benzene

■: 12.5 Chloromethane 15.0 Chlorobenzene

______JLA _ Brc-modi chloromethane < 15.0 Toluene

• 7.8 Di br-: mcchloroinechane < 18.0 Ethylbenzene

< 7.0 Me .hylene Chloride <12.5 Acrolein

______jjj3 B romo fc nn < 12.5 Aery Icnitri1e

•• A.O Chloro fcr:n < 25.0 Methyl Ethyl

< 7.0 Carbon Tetrachloride 278 Acetone

< 12.5 T rich1cro f1uo rome thane

< 12.5 Ch1oroethane

< 7.0 1 ,1 -Diehl oroethane

•- 7.0 1,2-Dichioroethane

< 9.5 1,1,1-Trichioroethane

< 12.5 1,1,2-Trich1oroethane

< 17.3 1 ,1,2,2-Tetrachloroethane

<12.5 Vinyl Chloride

or--.V

i111,1-Dichloroethene

< 4.0 Trans-1,2-Dich1oroethene

4.3 T rich1oroethene

< 10.3 Tet rach1oroethene


< 15.0 1 ,2-Dichloropropane

< 12.5 CIS - 1 ,3-Dich1oropropene

< 12.5 Trans-1 , 3-Dich1oropropene

VOL AT ILF OrTmiC P-! i A L Y S I5 (VGA)

LL\ I A L R \

Client: Diamond Vogel - HDR

Samp 1e Matrix: Soil

Method fio.: DIRECT SPARGE

s«»:e I.D.; U3-TO3Q2-5) TCI 1-7

Date Collected:__ 8/29/84

Date Received bj Lab: 9/1/84


ug/*g

1 2 . b B remomethane

•: 12.5 Chlo romethane

< 5.5 Bromcdich1oremetnane

< 7.8 D i b r o mo c h 1 o r o me l h a r. e

< 7.0 Methylene Chloride

< 11.8 Ercmcform

< -4 J Ch lore form

-• 7.0 Carbon letrachloride

< 12.5 T rich1cro f1uoromethane





<12.5 1,1,2-Trichlorcethane


•: 12.5 Vinyl Chloride

< 7.0 1,1 -Dichloroethene

< 4.0 Trans -1,2-Dich1oroethene

< 4. S T rich1oroethene

- 10.3 Tetrachlorcetnene

< 12.5 2 - Ch 1 o roe th v 1 v i ny 1 e t h e r


< 12.5 CIS - 1 , 3-Dich1oropropere


;iO/j'a____

< ll.G Benzene

15.0

< 15 . C

Ch1orobenzene

i o 1 u e n e

< 1 3. C

< 12,5

< 12.5

< 25 .C

< 25.0

145

Ethylbenzene

Acrolein

Aerylonitrile

Methyl Ethyl Ke

Acetone

Total Xylenes

VOLATILE ORTAN IC ANALYSTS (VGA)

DATA SUMMARY

Client: Diamond Vogel HDR

Sample Matrix: Soil

Method No.: DIRECT SPARGE

J

Sample I.D.: (23-70302-6) TC11-8

Date Collected:__8/29/84


Date Analyzed:11/6/84

• 12.5 B romomethane

' 12.5 Chloromethane

C! KJ . Bromcdichloromethane

< 7.8 Dib rcmochlo romethane

•• 7.0 Methylene Chloride

' 11.8 8romofor:a

5 c------------— ^ »• •Ch lore form

•: 7.0 Carbon Tetracn1 oride

< 12.5 Trichloro fluoromethane

, <12.5 Cliloroethane

< 7.0 1 ,1 -Di chloroetnar.e

< 7.0 1 ,2-Dichloroethane

< 9.5 1 ,1 ,1 -Trich1oroethane


< 17.3 1,1 ,2,2-Tetrach1orcethane



< 4.0 Trans - 1 ,2-Dich1oroethere

< 4.3 Trich1oroethene

< 10.3 Tetrach1oroethene

< 12.5 2-Ch1oroethy 1 vinyl ether

•- 15.0 1,2-Dichloropropane

< 12.5 CIS - 1,3-Dichloropropene

< 12.5 Trans-1,3-Dichloropropene

r 9/ ••9

•' 11.0____ Benzene

15.0__Chlorobenzene

< 15.0____ T o 1 u e n e

1 S. 0 Ethylbenzene

< 1 2 ■ 5____ Ac ro 1 e i n

< 12.6 __ Acrylenitrile

< 25.C___ Methyl Ethyl r'.et

<25.0 Acetone

VOLATILE ORTANIC ANALYSIS (VGA)

DATA SUMMARY

Cl ient : Die;; ■Odd Vogel - HDR Sample 1.0. : ( 23- 70302-7) TC12-2

So; pie Mat rix : Soil Date Collected: D/29/84

Me thod No. : DIRECT SPARGE Date Roceived by Lab : 9/1/84

Date Analyzed : 11/7/84

V ia / Y. a n a / K q

12.5 Bromcinethane 11.0 Benzene

12.5 Ch lo roiiie thane 15.0 . Ch1orobenzene

< 5.5 B romodi ch 1orcmethane 15.0 Toluene

•c 7.8 Di b roinoch 1 o rcmethane < 18.0 Ethy1 benzene

39.7 Methylene Chloride r' 12.5 Acrolein

•c 11.8 B romcform < 12.5 Acrvionitri le

S n Ch loro fern < 25.0 Methyl Ethyl Ketone

7.0 Carbon Tetrachloride 70.3 Acetone

< 12.5 Trich1oro flnorcmethane

< 12.5 Ciilo roe thane

7.0 1 ,1 -Dichloroethane

7.0 1,2-Dichloroethane

9.5 1,1,1-Trichloroethane

12.5 1,1,2-Trich1croe thane

1 7. 3 1,1,2,2-Tetrachloroethane


< 7.0 1,1-Dichloroethene

< 4.0 Trans - 1,2-Dich1oroethene

< 4.8 T rich1oroethene

10.3 Tetrach1oroethene

< 12.5 2-Chloroethylvinyl ether

< 15.0 1 ,2-DichloropropaneMethylene chloride ■

u< 12.5 CIS - 1 ,3-DichloropropeneNote:,.

X 12.5 Trans-1,3-Dichloropropenesuspected to be a

VOLATILE' ORTAillC DIALYSIS (VOA)

DATA SUMMARY

Client:: Di ctinond Vocjel-H[iR Sample I.D.: ( 23-70302-8) TC12-5

Sample Mat ri x: Soil Date Collected: 8/29/34

Method No. : DIRECT SPARGE Date Received by Lab :11/7/84

Date Analyzed:

r*;/Kq ___ _____ ud/Kq

< 12.5 8 romofiiethane < 11.0 Benzene

12.5 Chloromethane < 15.0 ' Chlorobenzene

<• 5.5 Broincdichlorcme thane < 15.0 To 1uene

<• 7.8 Dibromcchlcrcrrethane 1S.C Ethylbenzene

25.5 Methylene Chloride 12.5 Acrolein

11.8 B romc f o rn: •- 12.5 Aery 1 on i tri 1 e

4. C Chloroform < 25.0 Methyl Ethyl Ketone

7.0 Carbon Tetrachloride • 72.5 Acetone

12.5 T richlorofluoromethane

12.5 Chloroe thane

7.0 1 ,1 -Di chloroethane

7.0 1 ,2-Di chloroethane

9.5 1,1,1-Trichloroethane


< 17.3 1 ,1 ,2 ,2-Tet rachloroethane

12.5 Vinyl Chloride


< 4.0 Trans-1 ,2-Dich1oroethene NOTE- Methylene chloride is suspected to be a< 4.8 Trichloroethene

•c 10.3 Tet each 1orcethenelaboratory contaminan

< 12.5 2- Ch 1 crcetliy 1 vi nyl ether


< 12.5 CIS - 1 ,3-Dich1oropropene u

s 12.5 Trans-1,3-Dich1oropropene

volatile: ortanic ANALYSIS (VOA)

DATA SUMMARY

I Duplicate

Cl i ent : f)i a;:iiond Vooel-HDR Sample I.D.: ( 23- 70302-8) TC12-5

S cl!np ] G Mat rlx : Soil Date Collected: 8/29/84

Mothod Mo. : DIRECT SPARSE Date Received by Lab : 9/1/84


U ‘3 / K G/ ■ “ uq/Kq

12.5 Gromomethane •: 11.0 Benzene

< 12.5 Chloromethane < 15.C Chlorobenzene

<\ 5.5 Bromodi chi orotne thane 15.C To 1uene

< 7.3 Di b romoch loromethane < 12.0 Ethylbenzene

29.5 __ Methylene Chloride •' 12.5 Ac ro1e i n

11.3 Eromo forn 12.5 Aery 1 on i:: r i 1 e

r' 4.0 Ch 1 o ro fo rm < 25.0 Methyl EthvT Ketone

< 7.0 Carbon Tetrachloride 137 Acetone

< 12.5 Trich1oro f1uoromethane

12.5 Ch1oroe thane

<r% 7.0 1 ,1 -Di chloroethane


< 9.5 1 ,1 ,-l-Tri chloroethane

< 12.5 1 ,1 ,2-Trichloroethane

< 17.3 1 ,1,2,2-Tetrachlcroethane



< 4.0 Trans -1 ,2-Dich1oroethene

< 4.3 T rich1oroethene NOTE: Methylene chloride is suspected to be a laboratory contaminantv 10.3 Tetrachloroethene

12.5 2-Ch1oroe thy 1 vinyl ether

< lr .0 1,2-Dichloropropane

12.5 CIS - 1,3-Dich1oropropene ' ‘ u

< 12.5 Trans -1,3-Dich1oropropene


DATA SUMMARY

Client:____Diamond Vogel-H DR

S amp 1 e Mat r i x : Soil_______

Method No.: QIPECT SPARGE

JSample I.D.: (23-70302-9) TCI2-6

Date Collected: 8/29/84_________

Date Received by Lab:9/1/84


pa/ .-.a

< 12.5 B remomethane

< 12.5 Chloromethane

r 5.5 __ Bromodich1oromethane

< 7.8 0 i b r o mo c h 1 o r c me t h a n e

rr 0 Methvlene Chloride

< 11.8 B rc-mc form

, t'* . J Chloroform

< 7.0 Carbon Tetrachloride

< 12.5 Trichloro fluorometnane

< 12.5 Ch 1 o roc-thane

< 7.0 1,1 -Dich1oroethane

< 7.0 1 ,2-Cichloroethane


< 12.5 1 ,1 ,2-Tri ch I o roe t.harm



[ A 1 1 1.^ o 1 ,1 - Di chloroethene

< 4. q Trans-1,2-Dich1oroethene

< A. 3 Trichloroethene

10.3 Tetrachloroethene


< 15.0 1,2-Dichloropropane

< 12.5 CIS - 1,3-Dich1oropropene


____< 11.0 Benzene

< 15.0 Chlorobenzene

< 15.0

< 13.0

< 12.5

•: 12.5

< 25.0

Gh.R

Toluene

Ethylbenzene

Acrolein

Aery 1 onitri1e

Methyl Ethyl Ketone

Acetone

NOTE: Methylene chloride is

suspected to be a laboratory

contaminant


DATA SUMMARY

Client: Diamond-Vogel - HORJ

Sample I.D. : (23-70 302-10) TCI 2-10

Sample Mat rix : Soil Date

Method No. : DIRECT SPARGE Date

Date

q/Tg

12.5 B rorno methane

12.5 Chloromethane

< 5.5 Brcimcdi chioromethane

■- 7.3 . Dib rcmochlo romethane

13.3 Methylene Chloride

< 11.3 Brcmoform

4.0 Ch 1 oro fc rm

7.0 Carbon Tetrachloride

< 12.5 T rich1oro f1ucromethane

< 12.5 Ch1oroe thane

7.0 1 ,1 -Dichloroethane




< 17.3 1 ,1 ,2 ,2-Tetrachloroethane

12.5 Vinyl Chloride


4.0 T rans-1 ,2-Dich1oroethene

4.8 Trichloroethene

10.3 Tetrachlorcethene

• : 12.5 2-Ch1oroethy 1viny1 ether


12.5 CIS - 1 ,3-Dichioropropene

12.5 Trans-1 , 3-Dich1oropropene

Collected : 8/29/8-1_______

Recei ved by Lab : 9/1/84

An a 1 y 2 e d :]

ej / K a

jc_U . 0

< 15.0

< 15.0

92.0

< 12 ,_5_

< 12.5

< 25. C

31 .S

28 3

Benzene

Ch1orobenzene

To 1uene

Ethylbenzene

Acrolein'

Aery Ionitrile

Methyl Ethyl K.etcr.e

Acetone

Total Xylenes

NOTE: Methylene chloride is suspected to be a laboratory contaminant

VOLATILE ORTAN I C ANALYSIS (VOA)

DATA SUMMARY

/

Client: loncI-Vogel HDR Samplc I-D>; ( 23-70302--11) TCI 3-1

Sample Matrix : Soil Date Collected: 8/29/84

Method fio. : DIRECT SPARGE Date Received by Lab: 9/1/84

Date Analyzed: ]177/84

V- 5: 9 pg/Tg

- 12.5 B rcmomethane •: 11.0 Benzene

< 12.5 Ch loroinethane •: 15.0 Chlorobenzene

< o. 5 B romodTchlorcmethane •: 15.0 Toluene

< 7.8 Dibromochlorcmethane < 18.0 Ethylbenzene

i 5.5 Methylene Chloride < 12.5 Acrolein

- 11.8 B romoform ■: 12.5 Acry1 onitrile

-i.O Ch 1 o ro fo rm < 25.0 Methyl Ethyl Ketone

■: 7.0 Carbon Tetrachlcride < 25.0 Acetone

< 12.5 Trich1oro f1uoromethane

< 12.5 Chloroethane

< 7.0 1 ,1 - Di chi oroethane

< 7.0 1 ,2-Dichlorcethane


12.5 1 ,1 ,2-Trich1oroethane

< 17.3 1,1,2,2 -Tetrach1oroethane


■- 7.0 1,1-Dichloroethene

< 4.0 Trans-1,2-Dich1oroethene

< -. 8 Trichloroethene

10.3 Tet rach 1 o rce thc-.ne

< 12.5 2- Ch 1 oroetriy 1 vi nyl etherNOTE: Methylene chloride is

< 15.0 1 ,2-Dichloropropane suspected to be a laboratory

< 12.5 CIS - 1 ,3-Dich1oropropene contanu nant

< 12.5 Trans-1 ,3-Dichloropropene

VOLATILE OKI MIC ANALYSIS (VOA)

OAT A SUMMARY

/

Cl ient,: ni =j»:ir>r.H Vnnel-HDR_______ Sample 1.0. : ( 23-70302-1 2)TC1 -1-2

Sample Matrix:_______________ Date Collected; 8/29/84

Method No. :___ DIRECT SPARGE______ Date Received by Lab: q/1/flZj

Da t e Analyzed :___ jjl IJ.I.2A__________

V 12.5 E r'omomethane

12.5 Chloromethane

5.5 Brcmcdichlorc ethane

7 r. Dibromochlorornethane

< 7.0 Methylene Chloride

11.8 Brcmofcrm1 fl

— . -JCh 1 o ro : rm

7.C Carbon let racii 1 ori de

< 12.5 Tri ch 1 orof. 1 uorcmethane


< 7.0 1,1 -Dichioroethane

< 7.0 1,2-Dicnlorcethane

< 9.5 1 ,1,1-Trichlorcethane

12.5 1 ,1 ,2-Trichlorcethane

< 17.3 1 ,1 ,2,2-Tetrachioroethane

12.5 Vinyl Chloride


< 4.0 Trans-1 ,2-Dichloroethene

<,1 O

** . o T rich1oroethene

< 10.3 Tet rach1oroethene

< 12.5 2-Ch1oroethy 1 vinyl ether

15.0 1,2-Dichloropropane

12.5 CIS - 1 ,3-Dichloropropene

12.5 Trans-1,3-Dich1oropropene

n o / K a

< 11.0 Eenzene

Ai 1 L

1'! o Ch1orobenzene

< 15.0 Tc1none

< 18.0 Ethy1 benzene

< 12.5 Ac ro1e i n

< 12.5 Ac ry 1 on i t r i 1 e

< 25.0 Methyl Ethyl Ketone

<25.0 Ace t one


DATA SUMMARY

Client : Diamond Vooel-HDR Sample I.D. : (23-70 302-1 3) TC13-G


Method No.: DIRECT SPARGE Date Received by Lab: 9/1/34


-a/Kg yg/i'g

«: 12.5 B romomethane 11.0 Benzene

•: 12.5 Chloromethane 15.0 ■ Chlorobenzene

< 5.5 Brcmcci ch 1 oron'ethane < 15.0 Toluene

< 7.8 Di b r o mo ch 1 o r orne t h a n e < 18.0 Ethylbenzene

•: 7.0 Methylene Chloride 12.5 Ac rol e i n

< n.s E rorno f o rm 12.5 Acrylonitrile

< 4.0 Ch 1 o rc fo rm < 25.0 Metnyl Ethyl

< 7.0 Carbon Tetrachloride < 25.0 Acetone

< 12.5 Trich1oro fluoromethane

<• 12.5 Cli 1 oroethane

< 7.0 1 ,1 -Di chi oroethane

< 7.0 1,2-Dich1oroethane

■' 9.5 1,1,1 -Trich1oroethane


<17.3 1,1,2,2-Tetrachloroethane


< 7.0 1,1 -Dich1oroethene

< 4.0 Trans-1,2-Dichloroethene

< 4.8 T richloroethene

< 10.3 Tet:ach1oroethene

< 12.5 2-Ch1oroe thy 1vinylether


< 12.5 CIS - 1,3-Dich1oropropene ' - u


VOLATILE ORTANIC ANALYSIS (VCA)

DATA SUMMARY

Cli-nt: Diamond Vogel HDR_____ Sample I.D.: (23-70302-14)TCI3-87


Method No.: DIRECT SPARGE Date Received by Lab: 9/V84

Date Ar.a lyzed : 11/7/84

. - JiSiula_____ _____vq/ K g

•: 12.5 Bromcmethane - 11.0 Benzene< 12.5 Ch1o romethane < 15.0 ’ Ch1orobenzene< 5.5 Bromodichlororr.ethane < 15.0 Tolueie< 7.8 Di b romochlo rometh anc- < 18.0 Ethylbenzene< 7.0 Methylene Chloride < 12.5 Acrolein

< 11.8 Brcmo form < 12.5 Ac ry 1 on i t r i 1 e< 4.0 Ch 1 o ro fo rm < 25.0 Methyl Ethyl Keton< 7.0 Carbon Tetrachloride < 25.0 Acetone< 12.5 Trich1oro f1uoromethane 71 .0 Total Xylenes< 12.5 Chloroethare

•' 7.0 1 ,1 -Dichloroethane




< 17.3 1 .1,2,2-Tetrach1oroethane



< 4.0 Trans-1 ,2-Dich1oroethene


< 10.3 Tetracliloroethene

< 12.5 2-Chlcroethvlvinyl ether


CIS - 1 ,3-Dich1cropropene

Trans-1,3-Dich1cropropene

vclat ilf: oktanic a;jalvs is (voa)

DATA SUMMARY

Cl ient: Di arr.oncl Vogel -HDR

Sap 1 e M ac r i x :_Sen 1

Metiicd fie. : DIRECT SPARGE

Sample l.p.: (23-7Q30Z-15) TC14-1

Date Collected: 8/29/84 * 1


Date Analyzed:ll/7/84______________

yG;g

l 2 • 5 B roinoine thane

< 12.5 Chloromc- thane

__ '•5.5 Brcincdich1oromethane

< / . 0 Dib remoehloromethane

•: 7.0 Methylene Chloride

'11° B remeform

1 O. <J Ch 1 o ro fo rrc

< 7.0 Carbon Tetrachlo<-i de

< 12.5 Tri ch 1 ore f 1 uoronie thane

< 12.5 Ch1orcethane

< 7.0 1 ,1 -Di chloroethane



< 12.5 1,1,2-Tricn1croe thane




< 4.0 Trans-1,2-Dichloroethene

< 4.3 Trichloroethene

•• 10.3 Tet rach1oroethene



< 12.5 CIS - 1 ,3-Dich1oropropene

< 12.5 Trans-1 ,3-Dichloropropene

uq/Ka____

< 11.Q___ Eenzone

1 -• • 0 ’_ Chlorobenzene

'■ IS.9 Toluene

62.5

Ethylbenzene

Acrolein

Aery 1 on i t ri 1 e

Methyl Ethyl Ketone

Acetone

u

atile cr:a:i; c analys i s (vga.)

DATA SUMMARY

Cl ierr. : Di amendVocel-HPR Sample 1.0. : ( 23-70302-1 7)TCI4A-1 _

Sample Mat rix : Soil Date Collected: 8/29/84

Method Do. : C! FEC7 c-PAR 1-- Date Received by Lad: 9/1/84_____ _

Date Analvzed: 11/12/84

. r> • V

U_.::____

O/C

F.-nrcmocnane < 11.0 Benzene

f.h In rennet hare 15. C . Chic-rcoenzene

Brcinccicr. lorsmetr.ane ■■ 17.0 Toluene

- ■; D i b rr. nr, c r. lcromethane < 13.0 Ethylbenzene

6-1.0 }.i* *'; /1 c!■.e Ch 1 z r i ce •• ! £. - <-.c rc i e t n

1 1 . £ p ro:;:c rc r:n < 12.5 Ac ry 1 on * t •* i i e

-. 0 Ch 1 o rc- fc r:?. ^ -■*- - -* * j* ■ £-^7 1

7.0 Carbon Tetrachlcride < 25.0 Acetone

< 12.5 7ri chicrofl jcro~.ethane

< 12.5 Chlorcetnane

7 rv 1 ,1 - Di chlorcethane

< 7.0 1 ,2- Di ch 1 oroethar.e

■ , c 5 1,i,1-Trichlorcethane

< 12.5 1,1,2-Tricnloroe th ane

17.3 1 ,1 ,2 ,2-Tetrachlore-ethane


< / . 'J 1 ,1 -Dich1orcethene

A. 0 Trans -1 ,2- Di c.o 1 croethene

• o Trichlorcethene

10.3 Tetrachlorcethene

s 12.5 2-Chl oroethyl vir.ylether NOT-: Methvlene chloride is

15.0 1,2-Di ch1cropropane suspected to be a laboratory

< 12.5contaminant

C:S - 1 ,3-Dich1cropropene


II

VOt.AT r LE o:'7A?;:c A'. Ai. y si

data summary

(YCA)

Cl ienr : Diamond Vogel-HDR

- -‘‘"pit Mat ri / :SoiJ[

thc-c! mO . : DIRECT SPARGE

Sornp]c 1. 0. (_23-70302-J 8) TC14A-2

Date Collected:___8/29/84

Late- Received by Lab:__9/1/84


• c ' n

1 L , "J 5 ro::;o:i:et'iane

■ 12.5 Chio romethane

5.5 B rcmccich1cr ernethane

- L i b r o nc cnlorc rr.e t h a n e

35.8 Me t ri v1en e Chic ride

< B rc.T.o fc- rr;i

Ch It rare rrr,

7.0 Ca rten let rach 1 r ri •£«

12.5 : r 1 ch 1 oro f 1 uc rorne thane

12.5 Cm : oi'Oc triemg

•; *? ■>.• . w 1,1- Di cn 1 oroethane

7.0 1 ,2-Dich1oroethane

o _ 5 1 ,1,1 -Trichioroethane

< 1 ? ^ 1 ,1,2-Trich:oroetnane

17. 3 1 ,1 ,2 ,2-let rach lcroer.nar.p


7.0 1 ,1 -Dich1o roethene

< 4.0 Trans -1,2-Dich1oroethene

< 4.3 Trich1orcethene

1 A 1• :j < Tot rach 1 oroet.nerte

12.5 2-Ci 1 orcethv 1 vinyl et.hrr

v 15.0 1 ,2-Di ch 1 c rcc-rooane

< 12.5 CIS - 1 , 3-Dich1cropropenp

12.5 Trans - 1 , 3-Chch1 a roprooene

U'ri: *-n

11.0

< 15.0

l £. C

< 12.0

I ... 3

12.5

2 5 n

oenzene

Chloranenzene

To 1 uene

Er, y 1 t-enzc-nc*

Ac rcIe i n

Aeryicni:rile

Acetone

NOTE: Methylene chloride is suspected to be a laboratory contami riant

DuplicateVC1-AT i in OR7/Vi I C ANALYSIS (VGA)

[.'AT r, 5 U"TVr,A {

Diamond Vogel-HDR c . , n (23-70302-18)TC14A-2L ■ 1 *-•__ J Samp 1 e I . D. :

S amp!o Mat rix ;____ Soil Date Collected:. 8/29/84

Method Ac . : DIRECT SPARSE Date Received by Lab: 9/1/84

i1 a 10 Analyzed: 11/12/84

» f' / r> e 0 / Y 012.5 Bro.Tioir.e thane ■■ 11.0 Benzene

■■ 12.5 Chloromethare _____ y 15.0 Ch1orobenzeoe

5.5 B rcnodi ch 1: ron:e thane •' 15.0 Toluene

_ 7 Q Di l rcmcch 1 roir.e thane _____ ' 13.0 Ethylbenzene

4 5 _ Methylene Chloride < 12.5 Acrolein

_____ y_J 1 . 5 B no mo •' 0 rm •r 12.5 "Aery 1 cn i t r i ■ a

i ,7 Chi ore form 25.0 Met.hvl Etnyl he tor,

< / . 0 Careen letrach10ride •• 25. C Acetone

■* 12.5 irich1 ore fl00 cores thane

< 12.5 Chlorcethane

- 7.0 1 ,1 -Dichlorcethane

< 7.0 1,2-Cicnlorcethano

1 ,1 ,1 -7ricn1;rcetnane

- 12.5 1 ,1 ,2-Tricnicroetnane

< 17.3 1,1,2,2-Tetrachlcroethane

A f'O t T | Viny1 Chi oride

„ *7 r, 1 ,1 - Di ch 1 orcetherte

11l

°\T

Trans -1,2- Di ch 1 oroc-ther.e NOTE: Methylene chloride '< ■'. S Tri chi0roether.e suspected to be a laboratoi

1 r. 7 contaminant’• 1 w . J Tetrachloroethenc-

12.5 2 - Ch 10rce thy 1 v i .0 v 1 e the r

< 15.0 1 ,2-Dichlcropropane

•- 12.5 _ CIS - 1 , 3-Dich1croprcpene ' ' u

< 12.5 i rans -1 , 3- Di c.h 10 ropropene

Organic Analysis Data Sheet\

Cl i en t: Jâmqncl_Boge_l -HDR Samp lei. D. T~23- 7030~2-T9T~TCT4A- 3 Da 11v Co 11ected: ’8/29/84 Date Received by 'LabTJ/j'/ST"'

Sample Matrix: __Soi1Date Extracted/ P re pa r & d' ~Method ho: EPA 8240 I'iethonol _Ex tractDate Analyzed-: TT/1L78/4

6.3

r _ 6_/l

< __ 2_.8

< 3.9

r

| lo!

i1

< 2.0

< ___3Ji

< 6.3

< 6.3

3.5< 3.5

< 4.8

< 6.3

8.6

6.3

3.5

s 2.0

< 2.4

< 5.1

s 6.3< 7.5< 6.3< 6.3

Vo 1 a t i le Compo unds

Brcir.ome thane

Ch 1 orome thane

Brcr.odi chloromethane

Di b romoch loron:e thane

Methylene Chloride

Brcrnc form

Chloroform

Carbon Tetrsch1oride

T r i ch 1 o ro f 1 uo rcrr.e th a n e

Ch1oroethane

’-9/L or|MJ/KoN)

__ 7_.5

JJL4

356 _

_jA3

6.3

Volatile Compounds

Eeocene

Ch1orobenzene

Toluene

Ethyl benzene

Ac f'o 1 sin

Aoryloni tri le

615 Xy 1 c-nes

1ii-Dichlorcethane

1.2- Dichlcroethane

1 ,1 ,1 -Tri chi oroethane

1.1.2- Trichloroethane

1 ,1 ,2,2-Tetrach1oroethane

Vinyl Chloride

1,1 -Dich1oroethene

Trans-1,2 - D i c h 1 c ro e ch e r e

T ri ch 1 oroethene

Tetrach1oroethere

2-Chloroethylvinyiether

1,2-Dichloropropane

CIS - 1 ,3-Dicr. 1 oropropene

T pans-1:3-Dich1oropropene

Organic Analyc- is Data Sheet Duplica te

Client: Diamond Bogel HDRs a mp i e i. d .II£7cr3a?_-r9TTCT4^ 3Da te Coll ectedl_ jjs72978TTDate Received by" Lab: ""97T787~

Sample Matrix:__ SoijDate Extracted/Prepared:___ ~Method No: _EPA_8?40 Methanol Extract Da te Ana 1 y'zed : T17V97q4

(Circl'Volatile CoaiDound Volatile Ccmoounds

< 6.3 B romomethane < 5.5 Benzene

< _6_13___ Chiorcmethane < 7.5 Chlorobenzene

< 2.8 B romodich1oromethane < 12.5 Toluene

3.9 Dib romoch1oromethane 402 Ethyl benzene

< 3.5 Methylene Chloride < 6.3 Acrolein

< 5.S B romoform < 6.3 Aery lord tri 1 e2.0 Ch1orofcrm 13.0 2-3,-none

< 3.5 Carbon Tetrachloride < 13.0 Accicp.-j

< 6.3 T ri c!i lorofl uoronie thane 704 Xylenes

6.3 Chi oroethar.e

< 3.5 1 ,1 -Dichloroethar.e


4.8 1 ,1 ,1 -Tri chloroethane


8.6 1 ,1 ,2,2-Tetrachiorcetnane


< 3.5 1,1-Dichloroechene

2.0 Trans-1,2-Dichlorcethene

s 2.4______ Tri ch 1 oroetnene

/ 5.1 Tetrach1oroe there

< 6.3 2-Chicroe thy 1 vinyl ether

7.5 1,2-Oichlorocropane

6.3 CIS - 1 ,3-Bicriiorcpropene ‘ ' u

< 6.3 Trans-1,3-Dichlorcprcpene

Organic Analysis Data Sheet

C ! ; e 111: D i a no n d_Bo g_e 1 - H D R Saj 1 e I. D. (22- 70302-2Cfj TCM A-4Dt e Collected: 8/29JS4 _Date Received by Lab I’9/1/84

Sample Matrix:_ Soil Date Extracted/Prep-fr ed :

Re1110d Mo: ERA fi?.40_Methanol extractDa te Ana ly zed : 11/1~6/84 ~

':._J J5

5.9

: 2 0

"l 3. 5

5.3

‘L_ 3.5

' a __

3.6

< 6.3

< 3.5

2.0

'' 7.5

_ tL.3

h. 3

Vola ti1e Comp0anas

Broii;c methane

Chi 0 rone thane

B romc d i cl; 1 c rone th a nc-

Dibrone di 1 crone the re

Methylene Chlo-mde

B ro.mo f 0 nr,

Ch 10 rc fo rill

^ 1 o ■ • i ^ - r a c i 110 r t d e

Tri chi ore flue roir.e th are

Chioroethane

.<___ 7.5

.r__„28J5.

-_9.Z6.ifL

_<___ 6.3

< 6.3

< 13.0

< __ L3A

1 ,711__

1.1- Diehloroethane

1.2- Dichlcroethane

1 ,1 ,1-Trichloroethane

1 jl,2-1richioroethane

1.1.2.2- Tetrachloroethane

Volatile Compounds

Benzene

Ch1orcbenzene

Tol uer.e

Ethylbenzene

Acrolein

Acryloni trile

2-Beta non e

Aceccr.e

Xyl e.nes

Vinyl Chloride

1,1-Dichloroethene

Trans-1,2-Dichloroethene

Trichioroetnene

Tetrachloroethene

2- Ch 10 ro e thy 1 v i ny 1 e th e r

1,2-Dichloropropane

CIS - 1,3-Dichioropropene

Trans-1,3-Dichloropropene

a

Organic Analysis Data Shee

Client: Diamond-Vogel HDR _Scr.pl o I7p7"]>"3^70302-2^X'TC 14A-6!a. te Col 1 t-cifco :_8729/S4____Detc Received by labV 9/1/84"’

Sample Matrix:__.Soi 1____ (Date Extracted/Prepared: Method No:__ EPA 82-10 Methanol extractDate Analyzed: Tl/16/34

(Circle oiioj

< 6.3

VqJjp ti_l Compounds

E rcmoi.e thane

o/L or Key Vql a tile Compound;

Benzene

6.3 Ch 1 c rciiietna no ______7 dp___ __ Chlorobenzene

2.8 E remedi ci'i 1 orc:ne thane __7^_5_____ i o 1 u e r. e

•f *3 Gw! . J Diercmcchl oromc-thane 49^5_____ Etnyloen.zene

< 3.5 Methylene Chloride < 6.3 Acrolein.

1 ,7 n

j , :> _________E ro:;:ci‘or,T; __ 6_._3____________ Acryl cr.i tr i 1 e

V o n Ch1 ore form , 13.0 2-5jtanone

3.5 Carbon Tetrachloride .- 13.0 Acetone

6.3 Trich'iorofl uoromc-thane 84.1 Xylenes

< 6.3 Chioroethane

< 3.5 1 ,1-Dichloroethane< 3.5 1 ,2-Dichloroethane

4.8 1 ,1 ,1-Trichloroethane

< 6.3 1 ,1 .2-Trichiorcethane< 8.6 1 ,1 ,2,2-Tetrac.hloroethane


< 3.5 1 ,1 - Di chi oroethene

2.0 Trans-1,2-Di ch 1 oroethene

2.4 Trichl oroethene<; 5.1 Tetradil oroethene

< 6.3 2-Chloroethylvinylether

7.5

6.3

6.3

1 ,2-Dicnloroprcpane

CIS - 1 ,3-Dichioropropene

Trans-1,3-Dich1oropropene

am;c a; SIS (VGA)

cat a

Client : Diamond Vogel-HDR

S ar:a I o M£t r i *: _ Soi T__

Method No. : DIRECT SPARGE

Scfr.{!I c- 1. 0. : _(_2_3_- 70302-24 )TC14A-0

Da tc- Co 1 i e c:: c- d _ S/_29 /84

Dote Received 1/ lac: 9/1/84

Dote Ana 1/zee: 11/12/84

uc.'12.5 8 rr-r:'>

_ .________ ____• 12.5 Chic romethar e

■ 5.5 E roitoci chl ~ tr one

Ditrcmccr k '-rett-v

1 7.3 Methviene Chi o'-ice

1 i E rOm'O *crrn

1 Ch it.ro ft rrn

*7 Carter, 7et re ch 11 r i ce

12.5 . M cM ore t , ■jeroHitthant

■r 12.5 CM I c rce thane

7.0 1,1- Di ch. 1 croethene

c 7.0 1,2-Dichioroetnene

C C 1 ,1,l-7richlcroethane

<, 12.5 1,I,2-7richloroethane

1 7. 3 i,I,2,2-7etrachloroethane

12.5 Vir.vl Chloride

7.0 1 ,1 -Dich1orcethene

V 4.0 Trans-1 ,2-Di ch 1 oroethe.ne


V 10.3 Tc-t rach1 oroe thene

12.5 2 -Ch To rcethv1vin v1e t h e r

< 15.0 1 ,2-Dichlcrcorooane

12.5 CIS - I,3-Dich1cropropene

Trans-1,3-Dich1orcprccene< 12.5

1 ■ n Ci,

fr 1r.' orotencens

1 89

J1JL

12. S

!33

Et.ny 1 cencene

Ac no 1 c- i r.

'Ac -y 1 cn i t •• i i e

Methyl Ethy; he-

Acetone

Xy 1 e-nes


II

a

VCLA7 ! LE CRT AN: C ANALYSIS (VOA

DAI

—diet: Diamond Vogel-HDR . r r. (23- 70302-26)7X1 5-3

I £ ; . J . :

S trip le Matri ? : Soil Date Col iocted: 8/29/84

— Method No.: Di[f'ECT SPARGE Do to F:e ce i ved by Lao: 9/1/84

_

Cate Anal;/.tea: 11/12/84

_

• . /■* •’ r\

_____ lAL^L___ E romonc-thane < 11.0 Ber.cene

■ 12.5 Cri lerometr. trie <13.0 Chlorobenzene

—5 . 5 BrcmcdichIcromethane 15.0 Toluene

•- 7.5 Si b rente ch 1 c rcmethane lc.C Ethylbenzene

— __.... 24 Metny 1 ene Chloride 12.5 Ac rc 1 e i n

- 11.2 E rcir.o fo :"r < 12.5 Aery knit ri ;e

—•: -1.0 Ch lore fcr:.i < 2c.O Met::/; Etcvl Ketone

■: 7.0 Carbon Tetrachloride 63.3 Ace.3Re

—r : 2 .5 Tri ch 1 cro f 1 torc-ir.ethane

< 12.5 C.h 1 orce thane

—^ 7 n' . . V»‘ 1,1- Di ch 1 oroethane

< 7.0 1 ,2-Dichlcrcethane

—< 9.5 1 ,1,1-Trichlcrcethane

< 12.5 1 ,1,2-Trichlcroethane

_< 17.3 1 ,1 ,2,2 -Tecrach 1 crcethar.e


—< 7.0 1 ,1 -Dich1croethene NOTE: Methylene chloride is

< 4.0 T r;ns-1,2-Dich1crcethene suspected to be a laboratorycontaminant

—< -. s : r: cl: 1 oroethene

•: 10.3 let each1crcethene

_•- 12.5 2-Chic roe thy 1viny1e t h e r

•: 15.0 1,2-Dichlcrpprcpane

_•: 12.5 CIt - 1,3-Dich1orepropene ‘ ‘ u

< 12.5 irans-1,3-Dich1oropropene

n

VOL A. IL. E. 08 7 AN I C /VIA .YSIS (VCA)

—DATA SUM MAIM

,

—Client

Sample

:__Dla.tnof'

Matri x :

d Vogel 1 [DR______ Samp

Soi1 Date

e I. D. : ( 23-70302-27) TCI 5-4

Collected: 8/29/84

Method 110 . ! w. Ir.ZCT SPARGE Date Received by Lab: 9/1/84


—* / * ^ 0 0 V'c

_J.L.L. Brcmcr.iethar.e ___ < 17.0 Benzene

______ _CP lororne thane _ _ -'15.0 Ch 1 o r cfc e r z e r e

5 . v Brc.T.c-di ch 1 crcjnetnane ■ IE.C Toluene

7 Ei 5 r omcchloromethane i -C . 0 r * ft y * £ A r £ c r d

1 8. 8 Methylene Chloride - 12.5 Acrolein

1 7 B rcrno form < 12.5 Acrv 1 or. i; ri 1 e

* Ch 1 c rc fo rm ■- 25.0 Meon/l Ethyl he tone

< t . J Carocr: Tet re cn 1 o ri :e 25.0 Acetone

: o -. T richlerofiuo rome tnaoe 48.3 Xylenes

12. E Chloroethane

■r. 7.0 1 ,1 -Di ch 1 orce-thane

i . 0 1,2-Dich1c roe thane

r . " 1 ,1 ,1-Trich lorcetnar.e

i p r 1 ,1 ,2-7rich1orce:r,ar:«

17.3 1 ,1 ,2 ,2-Tetrachloroet.sane

i? E Vinyl Chloride

< 7.0 1,1 -Dich1croethene

< -1.0 Trans-1 ,2-Dichicroethene

4. fi Trich1orcethene

■* n ->I J . .7et rach1croetheneROTE: Methylene chloride is

2-Ch1oroe thy 1vinylether1 .< . 0 suspected to be a laboratory—

< 15.0 1,2-Dich1oropreoane contaminant

1 ? ~ CIS - 1 , 3-Di ch 1 croprepen-'

12.5 Trans -1,3-Dich1c ropreoene

VOLAT : IE Gr.T ,Vi 1 c At, AL. i ; S ( V ... •.)

• v• v

Cl ier.t : Diamond Vogel HDR

Sa:■; 0 Me! t r i / : ___Soi 1

Met1,,:: •: ho. : DIRECT SPARGE

Semple I.D.: ( 23-70302-28) TCI 5-6

Date Collected:____ 8/29/84_______

Dote F.ecei/£-■:! by-Lai: 9/1/84

Date At.a lyze j :_JJ /l_2/84

\

■ 12.5 Brcrcomet:; one < i I . 0 Benzene .

Chlcrornet rare - 15.0 . Ch lorcbenzer.e

r £ rp.T.cci ch iorpii'.etnare 15.2 To 1 uc-re

7 ;. Ci b rcn-.cc:; Icrcinethene Eth vIbenzene

21.3 Methylene Ch I c ri ce < 12.5 Ac ro 1 e i n

, : y Bromoform <12.5 •Aery 1 onitri 1e

' *• . Chi;rotor- Me t n •/1 Eth v I i

7 • ’ C c f* 7 C tl . 6 7 r j C r'i '.Of', C 6 50.3 r c c* t o n z

12. Tr’I chlcrc-1 cere-methane

Ch Icrcetr.ar.e

- 7. G i ,1 -Di ch 1 orcethar.e

< 7.0 1 ,2-Dichlcroethane

7 r 1 ,1 ,1 -7ricn 1 c rce-thane

1 •*» rI - . 7 1 ,1 ,2-Tri chi orcetr.are

x 17.3 1 ,1 ,2,2-Tetrachleroethane

< 12.5 Vinyl Chic ride

•• 7.0 1,1 -Dich1orcethene

< -i.O Trans -1,2-Dich1oroe thene

v- 4 o Trichloroechene

- 10.3 Tec rach 1 orcether.e

12.5 2- Ch 1 crcethy 1 vi ny I etne r

13.0 1 ,2-Di c.hl oropropane

NOTE: Methylene chlorideis suspected to be a laboratory contaminant

li ch I orop roper,e

•: 12.5 ch 1 oropropene-

uCIS - 1

Trans -1

\> r<# p AT! LE OEiAMIC ANALYSIS (VGA)

DATA S UMMAAY

Ci-en:: Diar::ond Vogel-HDR

People Matrix: Soil

Method No. : DIRECT SPARGE

Sarnie I.D. ;_( 23- 70302-29)TC15-7

Date Collected: 8/29/84

Dote Received by Lab: 9/1/84

Oa t o An a 1 y z e d :11/12/84

42.5

11..?

■t _1

•c i ;■>

> 8. ■

■c } ?

7 . j

—j ->■

■: 9 ,, 5

■- P

V j . 3

’ o _

n■ . '■j

J . n

c

t. row: metric fie

C n : c ro me t r. a n c

6 r c :r-c ci chic rc-mezn a r. e

Di b rcmocr.lorcmethcne

Methylene Chi trice

E '■ccic fc rTi

Co 1 o ro ft re

Carocn letrach1oride

; ri c.n loro f; uoromethane

Ch 1 orce tnane

1 ,1 -Dichlcrcethane

1.2- Dichlorcethane

1.1, 1 - Tri ch1oroethane


1.1, a,2-;et rach1o roethane

Vinyl Chloride

1 ,1-Cichloroethene

Trans - 1 ,2-9ich1oroethene

Tn ch1oroethene

i o t rach 1 orte trier, e

2 - Ch 1 o rc e t hy 1 v i ny 1 e t r, e r

1,2-Dichic ropropane

CIS - 1 ,3-Di c.n 1 oropropene

*rans- I,2-Dich1oreprorene

l: C /y C

- 1 1 . C

______: iv . . Cn1occbencene

* i . ' Toluene

22.5 Ethy 1 benzene

12.5 Ac rclein

p . 5 'At r. 1 or i t ri1e

Mot PI Etnvl i

35 .-8 Acetone

55.5 Xy 1 e.nes

NOTE: Methylene chloride is suspected to be a laboratory contami nant

V’-: a: > if or tani c analysis (yoa;

data summary

C; io-.t :

Mo-: hoc!

Diamond Vogel -1!DR

' :___Sp 1 ]

: 2!E C T SPA PGR

Sample

Date Collected:

( 23 - 70 302-30 )TCI G -1

8/29/94

Ca:e Pece i ved L/ La!): 9/1/84

Cate Analyzed^ 11/12/84

28.3

. u

1 7. 2

±QJ

1 9 n

15.0

12.5

Chi-; rcêths.ne

l r ;i ch : : --'methare

10 y . e-r. e C r i ~ r : de-

O’.U . 6troC'"i ; C f* 1 06Trichlorofl ucroniethar.e

Ciilcroethcfie

1.1- Si ch 1 orcetha.ne

1.2- Sich1crcethare

1 ,1 ,1 -7r! cr.lorcethare

ci ch : o rceth are

1,1,2 ,2-Tee each Icrcetr.ane

Vinyl Chloride

1.1- 2ich1c roethene

Trane-1 ,2-Dichloroethene

• ri ch 1 o roet here

■ e t ra ch1o roe t he ne

2-Ch ’ oroeehy1viny]ether

1.2- Dich1o repropane

C:5 - 1 . 2-Cr ch 1 croproper,e

Trane -1,a-jich1oreprepene

2 I b.

Benzene

Ch 1 o '■ c c e n c e r. e

To 1 ,ene

Etny 1 zerz ere

Ac rc 1 e i .n

Aery : cr, i e r i 1 e

Ace t or. o


vcl a: . i -w t' i r.L

DATA SUMMARY

Cl ion•.: _D_i arr.onc! Vogel-HDR _

Sa-r.o 1 e Matrix:___Soil_____

Me:‘-.oo No. : TTI P£CT SPARGE

Sample ; ;( 23-70302-31 )TC16-3

Coti Co 1 lected : _B[j_ /BA

batc- r:ecei ved L/ Lab: 9/1 /84

Late Analyzes: 11/12/84

12 E tix trie thane

i a . r z

90.3

co icro'.MOtone

5 romcd*! ch 1 c ''o:r.e thane

Dib rcôcnr c r cine'.nan c-

M.e tv 11 rI e Cn i c r: a e

r::;

•: 11.0___ Benzene

•• 15.0 Cn 1 orooenzer.e

7J_. 3 Ethylbenzene

12.5____ .Acrolein

Jjt.J____ Aery Ion itrile

25 . C Me z r./1 E tr < 1 e t c .o e

•• / . J oc men .et rato;c r:ce

- 12.: Trich1c ro f1uo rone there

12.5 Cii 1 crcetric.ne

r 7,0 1 ,1 - Di chloroethar.e

< 7.0 1 ,2-Di chic re-ethane

.; ? . 5 1 ,1 ,1-Tri cnl orcethare

'j s - 1 ,1 ,2-Tri cnl oroetna.ne

< 1 / . 0 1 ,1 ,2 ,2 -Tet rac.h ■ c roe thane

] •> r; y i r, y 1 Chi o r i d 6

•- 7.0 1,1 -Dich1c roe t here

< A. 0 Trans - 1 ,2-Dicn1 or tetnene

... 1 0 T rich1o rcethene

■■ 10.3 Te t each 1oroe there

12.5 2- Ch 1 orcethy 1 v i.nylethe r

< 15.0 1,2-Dichlcropropane

•: 12.5 CIS - 1 , 3-Dich1oropropene

• 12.5 Trans-1 ,3-Cichloropropene

191 Acetone

132 Xylenes

NOTE: Methylene chloride issuspected to be a laboratory contaminant

' ‘ u

V.

DATA SUMMARY

Diamond Voeel HDR r - .....J a :i![y le I.D.: ( 23-70302-32)TCI 7-1

;acri/: Soil Date Co lice ted: 8/29/84

0.: DIRECT SPARGE Date Receiver b/ tat: 9/1/84

L 0 Z £ Ana:/:oc: 11/12/84

£ -'t ~;ch are

Chlerc:nstfi2ne

B rc-n cc i chic- romethane

me c.n ;: r anahi

c

c mr

re *■:

< o

/.0

Q

: o -j

15.0

• 12.5

Careen Tetrach ’Gride

• r: c.n 1 era *; -jcroniethane

C.h 1 c rcetnene

1 , i - Di eh 1 orcet.har.e

1,2 - Dichic roethane

I,1,i-Triehloroechane

1.1,2-■ i ri c.n I oroethane

1,1,2, 'etrachlcroethane

Viny I Chi or i de

1 ,1-Di eh 1 oroetnene

* f aHS - 1 01 i -* - Di c.n 1 orcethene

T r i c:i I G r 2 e t h e r, e

Tetrac.h 1 tree there

2- Ch:c roe thy 1viny!ethe r

1,2-Dichloropropane

CIS - 1.2-Dich1orepropene

Trar.s-1 ,3- Di ch 1 orepropene

36.3 Xylenes

uNOTE: Methylene chloride is suspected to be a laboratory contaminant

VOLATILE ORTANiC DIALYSIS (VOA)

DATA SUMMARY

Cl ient Diamond Booel-IIDR Sample I.D.: (23-70302-34 ) TCI 7-5

Sample Matrix : ôil Date Collect ed: 8/29/34

Method No. : DIRECT SPARGE Date Received by Lab: 9/1/84


j/Kq yg/Kn

< 12.5 Bromoiiiethane < 11.0 Eenzene

12.5 Chlcromethane < 15.0 . Chlorobenzene

< r *-0 . D Brcrnodi chi oromethane < 15.0 Toluene

< 7.8 Di bromochloromethar.e < 18.0 Ethylbenzene

7. C Methylene Chloride < 12.5 Acrolein

< 11.8 Eromoform < 12.5 Aery 1 onitri1e

4.0 Ch 1 o ro fo rm < 25.0 Methyl Ethyl Ket

< 7.0 Carbon Tetrachloride <25.0 Acetone

s 12.5 Trich1oro f1uoromethane 27.8 Xylenes




< 9.5 1 ,1 , 1-Tri chloroethane

12.5 1 ,1 ,2-lrichloroethane



s 7.0 1 ,1 -Dich1oroethene

< 4.0 Trans-1 ,2-Dichioroethene

4.8 Trichloroethene

10.3 Tetrach1oroethene



< 12.5 CIS - 1 ,3-Dich1oropropene ’ ' u


VOLATILE ORE AN IC ANALYSIS (VOA)

DATA SUMMARY

Cl ient : Diamond Boqel HDP. Sample I.D.: (23-70 302-35) TC 17-6

Sample Mat rix : Soil Date Co 11ected : 8/29/84

Method Mo. : DIRECT SPARGE Date Received by Lab: 9/1/84


u c/Lg uo/Kq

12.5 E romomethane < 11.0 Benzene

12.5 Ch loromethane < 15 . C Chlorobenzene

•: 5.5 Brcmodichlorcmethane < 15.0 Toluene

7.3 Dibromochloromethane < 18.0 Ethylbenzene

7.0 Methylene Chloride < 12.5 Acrolein

11.8 Bromc-form < 12.5 Acrvlcnit riIe

< 4. G Ch loro form < 25.0 Me t h y 1 E t n y i a r

< 7.0 , Carbon Tetrachloride < 25.0 Acetone

< 12.5 Tri ch 1 ore fl ucromethane

< 12.5 Chlorcethane

< 7.0 1 ,1 -Dic.hlorGet.hane

7.0 1 ,2- Di c.h loroethane

< 9.5 1,1 ,1-Trichloroethane

< 12.5 1,1,2-Trich1oroe thane

17.3 1,1,2,2-Tetrachloroethane

12.5 Vinyl Chloride


4.0 Trans-1 ,2-Dichloroethene

< 4.3 Tri ch 1 orcet.hene

10. 3 Tetrach1oroethene


15.0 1 ,2-Di c.h loropropane

12.5 CIS - 1 ,3-Dich1oropropene ‘ ' u


Cl ic-nt : Diamond Boqel-HDR S a mp1e I.D.: (23-70302-35) TC17-6

Samp1e Matrix: Soil Date Collecte d: 8/29/84

Met .nod No.: DIRECT SPARGE Date Received by Lab: 9/1/84


* i ■n / n ? ' • V pa/Eg

12.5 B romofiie thane < 11.0 Benzene

12.5 Ch lc rcmethar.e < 15.0 Chlorobenzene

5,5 Bromocichlorcmethane < 15.0____ Toluene

7.8 D i b r o n i c c h 1 o r c m e t h a n e < 18.0 Ethylbenzene

7.G Methylene Chloride < 12.5 Acrolein

11.8 B rcnio form < 12.5 Acry 1 on i t ri 1 e

-.0 Chlcrofc I'm < 25.0 Methyl Ethyl

7.0 Carbon Tetrachloride < 25.0 Acetone

< 12.5 Tri ch 1 oro fi uoromethane

12.5 Chloroethane

7.0 1 ,1 -DichIoroethane

< 7.0 1 ,2-Di chloroethane

< 9.5 1 ,1 ,1-Tri chloroethane

< 12.5 1 ,1 ,2-Trichioroethane

< 17.3 1 ,1,2,2-Tetrach1oroethane


7.0 1,1-Dichic roethene

4.0 Trans-1,2-Dichioroethene

< 4.8 Trich1orcethene

10.3 Tetrachloroethene

< 12.5 2-Ch1oroe thy 1vinylether

s.' 15.0 1 ,2-Dichloropropane

12.5 CIS - 1 ,3-Dichloropropene

*s 12.5 Trans-1 , 3-Dich1oropropene


DATA SUMMARY

Client: Diamond Vogel-HDR

Sample Matrix: Soil

Method No.:___ DIRECT SPARGE

Sample I.D.: (23-70302-3o) TCI 7-6

Date Collected: 8/29/84



ne/J.a_

< I - • 5__ Brofiicme thane

1 - • 5 Ch lorome thane

L ____ B romod i chic rome t h an e

< 7-s Dib romochloromethane

< /• Q____ Methylene Chloride

^ 11 • d___ Bromofcrm

■- 4.0

■- 7.0

< 12.5

< 12.5

< 7.0

s 7.0

< 9.5

< 12.5

< 17.3

< 12.5

< 7.0

< 4.0

< 4.S

•: 10.3

< 12.5

< 15.0

< 12.5

< 12.5

Ch 1 o ro fc rm

Carbon Tetrachloride

Tri c.n 1 oro f 1 uorcinethane

Chlorcethane

1 .1 -Dichloroethane

1 ,2-Dich1o roe thane

1 >1,1-Trichloroethane



Vinyl Chloride

1,1 -Dich1orcethene

Trans -1 ,2-Dichloroethene

Trich1o roethene

Tet each 1orcethene

2 - Ch 1 o roe thy 1viny1e the r

1 i2-Dichloropropane

CIS - 1,3-Dich1oropropene


jig/hq

< 11.0

< 15,0

8.0

< 12.5

< 12,5

< 25.0

< 25.0

Benzene

Ch1orcbenzene

Toluene

Ethylbenzene

Ac ro1e i n

Aery 1 on11 ri1e

Methyl Ethyl Ketone

Ace t one

' u

Cl ic-r.t :__pi among Vogel HDR

Simple Mat ri :<: Soil___

•vcthcc tio , ; ul r£CT jFAr.G:

1 9 C,

5.5

7.2

7.0

1 ' '2

r

i r.

< 12. S

12.5

< 7.0

< 7.0

< 9.5

< 12.5

17.3

12.5

< 7.0

< 4. C

< J c

•: 10.3

< 12.5

s 15.0

< 12.5

< 12.5

E rcncinetharit;

Cnloromethane

Brcmcci chlorcaietharc-

Dibrctnoch lorcrr-e there

f-'ethyleno C’-lorice

B •~orr.'? rerrr,

Ch 1 o ro f c rm

Career. Tetrachloride

i rich1oref1eoromet.hare

Cii 1 c roe thane

1 ,1 - Di chi orcethane

1,2-Dich loreet.hane

1 ,1 ,1-Tri ch icroethane

1 ,1 ,2-Tri ch 1 eroe trane

1 ,1 ,2 ,2-Tetrachlcroetr.ane

Vinyl Chloride

1,1-Dichloroe there

Trans -1 ,2- [■: ch 1 oroethene

Trich1oroethene

Tetrach1 ores there

2-Ch1oroethy 1viny1ethe r

1 ,2 - Di ch 1 o rop ropane

CIS - 1 ,3-Dich1oropropene

Trans -1,3-Dich1o rop repene

. AM A: V r.K (

S a rr p'! e t . : .

Solti Coll e.c

D Ci t e Piecei v

Cc L C: Af. o l y c1

—

(23-70302-38) TC20-1

i a . e

Bentone

Ch 1 o '-cbontene

. 0 I 'J Q r: c

Et::/1 Dorênc-

Ac rc 1 ! r.

9 C

9 C n

V: :V:vi Ke

V G L AT ! L [ 0P.T AG i c AN AL VS IS ( V CA)

DA;A SUMMARY

C-1 lcr-t :._.Dj.ciîond_ Vqae_l_-_HDR_ _

S^plo Matrix:$pjJ

MotGo J Ac. : DIRECT SPARGE

Sample l.D. : _(23-70302-39)TC20-3

Date Co 1 lecteri8/29/84_

Date Receive:! by Lab:_9/l/84


t n zi:...

' ■? r

- *-cnicr:ether.e

C.h 1 o r :>me: nan e

Borncci ch ■ orcmetnano

D: c rr-r-ccr. !c rcmetnane

P •’ 0 __

•: 11. 0 t; e r,: e r, -*

/. e

11i’itt.'i /1one- Ch

b rc.r.c: err::

;ri ce 18.5

7.0

c =.

4.0

■: 10.2

- 12.5

< 15.0

12.:

Ccrocr. . e t rach 1 o r. ce

■ r: cr. 1 c re r i uo come th are

C;i 1 orcet bane

1 ,1-01 ch 1 oroethar.e

1 »— - Ca ch 1 o roe thane

1 »^ * * * • r i c h 1 o r o e t h a n e

1 ,1,2-Tricnlcroethane

i ,1 ,2 ,2 -1 e t ra ch 1 o roe thane

Vi r.y 1 Ch 1 ori a'e

1 ,1 - Di ch 1 c rcether.e

Trans-1 ,2-Di c.h 1 croetnene

T r? ch 1 c rce ther.e

Tec rach1oroethene

a -Cr1orcethy 1viny1 ether

1 ,2-Dich1o repropane

t:3 - 1,3-Dich1cro'propene

i nans -1 , 3- D', ch 1 o ropropene

< a d . L

Cn1c rccencene

i c 1 j e r. c

Ethy 1 oer.cene

Acrol c- i n

'Aery len : t ri 1 e

Vc * n y ] Z - ^ , 1

Acetone-

ii

i 0!. A i i L F G r; T A'. 1 C A.,' i A L V 5 j $ ( V 0 A}

DATA SUMMARY

Ci ient : pia Hjpji d_Vo ge ]_-H DR S a mp

Sample Matr i >': Soil Cate

Me-choc1 fie. : DIRECT SPARGE Date

Date

A'L •• 9

______:îLL___ Brcrccmethane

< 12.5 Cr. io rometh are

-• 5.5 £ remodich1o rometh are

r 7.3 £ i b rerro ch 1 c '-cine t n a r:

7 _ r: Me t h y 1 e ;i e Ch 1 o ri ce

^ ? E reme fc rm

4.0 Ch ’ o re fo r:a

*• / . u Caroon let race i c r: he

c 12.5 . n ch ! c ro f 1 (jo rorv.f-1h anp

^ i - . Ch 1orce thane

< 7. C 1 s 1 - D i c h 1 o ro c ti h n n <9

< 7.0 1,2-D.ch10 roethane

9.5 1 ,1 ,1-Tri chlorcetr,ar.e

< 12.5 1 1 * i^ * Tri ch i c r0c thnnp

< 17.3 1,1,2 ,2-Tet rachloropthsr.e

•' 12.5 Vinyl Chloride

- 7.0 1,1 -Dich1orcethene

< 4.0 Tcans- 1 .2- Di ch 1 ornprher.e

•: 4 . S Tri ch 1 orcet hc-r.e

•: 10. 3 Tet ra ch1oroethere

< 12.5 2 - Ch 1 oroe tii v 1 v i n v 1 e t h e r

A Cn o 1,2-Dichloropropane

< 12.5 - 1 ,3-Di ch 1 cropropc-ne

< 12.5 Trans-1,3-Dich1oroprnnenp

8/29/84

11/18/84

0 0'/ 0

. i . i.’

■ 1 5 . C

•'_15 . C

< 12.0

£: .

•• 25. G

tenzc-r-e

Cn ] c ret enter,e

. 0 I j •z f; c

Acrolein

Ac ry 1 cr. i l rile

.-.cetore

cn

n

volati lr c'<ic analysis (voa)

lata summary

Client: Oiuiiinod Vogel-HDR

-jamp ie Mja ri x : Soil

t-'e t h c d No. : DIRECT SPARGE

Sa.-nple TC20-7

0-ale Collected: . 8/29/84

Da te Receive d by Lad: 9/1/84

Date Analysed: 11/15/84

b ro.nofiieth ane

Ch lcrorret har.o

£ rorr.cdi ch I or on::ethane

Di 5 rcncc'i loro'tethane

Me thy 1 ene Ch 1 o ride

Brcrnofcrrn

Ch 1 rc fc r.Ti

Carbon Tetrach1 oride ■

• r1' cn 1 c rc f 1 uc rorcethare

Ch 1 croe thane

1 >1 - Di ch 1 oroethane

1,2-Dichloroethane

1 11, 1 - Tri ch1oroethane

1»1 ,2-Trich1oroethane

1 .1,2,2-Tetrachloroethane

Vinyl Chloride

1 ,1 - Di ch 1 orc-ethene

Trans -1,2-Dich1oroethene

Trich1oroethene

Te t rach1orce thene

2 -Ch1o roe t hyIviny1e t he r

1.2-Dichlcropropane

CIS - 1,3-Dich1croprcpene

i r ans -1 , 3- Di ch 1 o rep rope tieu

1 L r CRT a: i I c AN A L Y S ! S ( V 0 A)

DATA SUMMARY .

Sample 1. 0. : (23-70302-42)__TC22-1

Da t e Collected: 8/29 / 84_

Date Received ty Lao :__9/_]/84

Date Analyzed: _JJ / J_5/ 84___________

C110n: ;.J4j.?A:noo.Ooii£JdM_...

Sa-oio Mat : x :____ S.CLiJ________

Molted No. : e! RCCT SPARGE

------ ---------- L’ G *.

—--- .* " B f o iTtG - lit I. n e 1 r.

____ __» p '• Ch1c romethace ... 1 r r,

______ -_d.____ E-c:tcdi cm 1 oro;;;e:hane ,. 1 -

—*7 ;. L: o re freer. 1 c ron-c-mare : 1 -

.■__ 7.C Methylene Chic’'ice

i L_ . f

_- __ .

• 11.8 5 f'G‘rnG 7 0 rr;;-

. .J r Chloroform < 7 -

• *' . -J Cc r. or. . £ * ;’a Cri i 0 r' 1 Cc •r 7 Z■ 12. S i r: ch 1 crc f: -jo rene thane

12.5 Chio roe thane

•r. 7.0 1 , i -Dich1oroetnane

--- ..7.0 1,2 -Dicm 1c roe thane

9.5 1 J ,1-Tri cr. lorcethane

, 1 ? - -. ■. *■. —---------- -

i,■,2 -ir:chioroe t nane

-17.3 1,1,2,2-TetrachIcrcethane

12.5 Vinyl Chloride

< 7. G 1 ,1 -Dich1o roet hene

4.0 irant -1,2-Dich1oroethene

< A. 8 Tri c h 1 o r o e t h e n e

__10. 3 Te t r a c h1oroethene

12.5 a-Cnio roe thy 1vinyiethe r

15.0 1,2-Dich1oroprepane

12.5 C-S - 1,3-Dich1 croprepene‘ u

< 12.5 Trans-1 , c- Di ch 1 croprooer.e

CCm : crctericene

To 1 uene

Ethylbenzene

Ac r o1e i n

Aery Ionitriie

Me thy 1 5thvl YetC'^

Ace tone

VOLATILE CRT AM IC ANALYSIS (VGA.

LATA SUMMARY

Cl lent :___Diamond Vogel-HDR_

SaiRDle Matrix:___SoiJ

Mc-thcd Me.: DIRECT SPARGE

S a :rtp 1 e I. D. :__(2 3- 70 30 2_- £4) TC2 2 - 5

Dato Co 1 lectc-ci: 8/29/84_____

Data Received by Lab: 9/1/84

Date Analysed : 11/15/84

wo u", '■

i ?

/. \j

1 : .

b ron:o;:;etnane

Ch i o r or;o t n a .n e

B roriodl ch Ic-rometh ane

Di b rcrnoch 1c rc:t;et bane

Methylene Chloric?

E retro for':;

r. 15

12Cr 0 r::i

& e n z e r.

Ch 1 c rot-era ere

: 1 jer.C:

Acrolein

Acrylcr itrile

Metny: Ethyl het:

12.5

12.5

7.0

/. u

■>I - .

Caroon 7e t rach1c rice

7r, ch 1 c rc f 1 ec remethane

Ch i oroethane

1 ,1 -Ci chloroethane

1,2-Dichloroethane

1.1.1- Trichlcroetnane


•: 17.2 I, .2:2-7e t rach1c roethane

< 12.5

<. u

in

12.5

15.0

12.5

12.5

Vinyl Chloride

1.1- Dichloroethene

Trans -1,2-Dich1croet hene

Trich1oroethene

Tet rach 1 oroethc-ne

2-Ch1orcethyiviny1e the r

1.2- Dichloropropane

CIS - 1,3-D:ch1oroprepene

Trans-1,3-Dich1oroprepene

VOLATILE CRT AN IC ANALYSIS (VGA)

DATA SUMMARY

CnenL: Dianiond Vogel HDR

Sample Matrix:__ SojJ

Ms-hod No.: DIRECT SPARGE

Sample I • C. :_(f 3-70302-45) TC22-7

DaLe Co 11 c* c t e d : _ 8/29/84

Date Received by Lab:____9/1/84

Date Ar.alybc-c: 11/15/84

—______ji_2 _._5 ____ 5 rci'r.ernetharo

‘ *“ * Ch 1 o rc:neth ar.e

— ----- *' * " fcreraodi ch loromethar.*

' * ui b rcmoch 1 c romethene

— ——----------- 1_1___.. Methylene Chloride

< 11.0 B rorac form

_•: 4.0 Ch 1 o ro f o nn

< / . 0 Carben Tetrachloride

_<• 12.5 Tr i ch i o ro f 1 uo reniethane

< 12.5 Ch1oroe thane

7 r," ( • V. 1,1- Di ch 1 crcetnsne

.r J O 1,2-Dichlorcethane

•- 9.5 1 ,1 ,1-7 richloroethane

•- 12.5 1,1,2-Tricn1oroethane

< 17.3 1 ,1 ,2 ,2-Tetrachloroetha.ne

' 12.5 Vinyl Chloride

_< 7.0 1,1 -Dichloroethene

< 4. C T rans- 1,2-DichIorcethene

a _ 0 Trich1oroethene

< i !J . J Te t ra ch 1 o roe t lien e

< 12.5 2 - Ch 1 o roe thy 1 v i ny 1 e the r

< 15 . Q 1 ,2-Dichloroprcpane

< 12.5 CIS - 1 ,3-Dich1orepropene

< 12.5 Trans-1 , 3-Dich Toroprcpene

2 O.'i 0

13.0

75 .0

< 25. r». 'J

Chicrcoereene

Tc1jene

EthyIbeneene

Ac ro1e I r

jfc: r\ r.r' c

u

A.NALY i! CAL TECHNOLOGIES , INC. I-D. 70302

RESULTS of epa quality control samples

WP 127S , VOLATILE ORGANICS

PARAMETER X

EPA DATA

S 55i C . 1.3

SAMPLE

11-

RESUL

-6-84

1 ,2-dichi orcethan.e ^ ' ^13.7 2.5 8.7-18.7 10.7

C hi pro form v ^63.3 14.9 33.5-98.1 61.2

1,1 ,1-trichlorcethcne ^ ^8.1 4.2 MOL-16.5 8.1

1,1,2-trichlorcethene ^ ^10.7 8.1 MDL-26.3 9.2

- ■ , t-)Career . etrachl or I :'e v ' 13.2 *) 7

^ • *5 . £ - 2 G . 5 14.7

1,1,2,2-TetrachIorcethene ' ^3.6 2.4 4.8-14.4 8.6

Sremodichi creme thane ^ ^11.2 2.7 5.8-16.5 12.5

Ci bromochl oromethane ‘ S. 2 2.7 4 .0-14.4 1 U . u

, -brcmOTorm ■ ' 14.0 3.0

ooCM

1

oCO

16.2

Results of EPA Interlabcratory comparison Studies.

Results of QC Materials Run Concurrently with Samples.

5 95 Percent Confidence Interval.

70 307!/-.ii I 1C/*.L. i LCHi.JiOoI Eo j i NC .

RESULTS OF ERA QUALITY CONTROL SAMPLES

WP 1278, VOLATILE ORGANICS

PARAMETER y

1,2-dichioroothar:e ' 13.7

Chi orofcr". CO

CO

1.1.1-trichlcrcethane ^ 'S.l

/ "• '1,1,2-trichloroethene v ^ 10.7

Career, Tetrachloride î j . c

1,1,2,2-Tetrachlorcethene *• ^9.6

.. . , 4 u (MR)2rc~.0GK.nlcromethane v ‘ 11.2

( -i \Dibrcmcchlcromethane '• 1 5.2

Brcmoform ^ ^14.0

ERA DATA 1 SAMPLE RESULTS5 95M C.T.3 11-7-84

2.5 8.7-13.7 . 11.7

14.9 38.5-98.1 58.6

4.2 KSL-16.5 . 7.6

6.1 MDL-26.8 9.3

3.7 5.0-20.C 13.7

o »

a. 4 4.8-14.4 7.8

2.7 5.8-16.5 12.1

2.7 4.0-14.4 9.9

3. C 8.0-20.0 15.6

Results of EPA Interlaboratory comparison Studies.


3 95 Percent Confidence Interval.

i. 23-70302

RESULTS OF EPA QUALITY CONTROL SAMPLES

OP 1270, VOLATILE 0 ROAN ICS

n ; v ? •* z y r r» XEPA DATA 1 SAMPLE RESULTS

t .*• , _ i t.f\ S 95:f C.l.-- 11/16/84

1,2-di chic roe thane 'i;>] 3.7 2.5 8.7-13.7 12.4

1 \ .1 \Chi oreform ’ J C5.3 1.9 *>o r. co t 71 .21.; .l-triar.lcroc-thar.c- ^ ’ 1

S.l *:1 . (L MjL-16.5 8.3, . . 12 ) i, i, a-ir chi crcethene v ; i C. 7 c.l MPL-2t..S 10.2careen Tetrachlorids ^ 1

13.2 j , i r. c; 9 r -v. .;. - £ u . V.- 14.21 ,i ,1: ,--Tetrechlcrcethene ' ^

9.6 2.4 fl 0 ■* i .: 9.7/ i c \E'romccichioremethane '• '1 11.2 2.7 5.8-16.6 12.0f 7 u ^Pibrcmcchloremethane v- 1 9.2 2.7 4 .0-14 .4 ■8.5

/ 2 5 'Promo form v 1 14.0 3.0 8.0-20.0 11.8

."«Ssults of ErA Interlaboratory comparison Studies..

Results of QC Materials Run Concurrently with Samples

• 55 Percent Confidence Interval.

m

RE MLI Ct Lif i; CAL! T V COM ACL SAMPLES i

—

107:/ VOLATILE CF GAM CL

f i *. *■. m 1—r r-f r.~ rs.L I r.r. XCPA DAT S 95c'

0 1 n ~C . I.

SAMPLE RESULT 11-15-84

1 , 2 - i c n lore a ta n e ‘ ^13.7 o r b . / - 1 O . i 7.3

t : )C:il oroTorm ' ‘ 68.3 14.9 't? r C - -. J * -- x . * 37.1

. ( • "3 ,: ,:- tr i:n i oroetr.a r.c- G l ^ . 2 V *'■ t i ^ 5.2

-1,1 ,2-tricM oroethene ^

1C.7 S. 1 MLL-M.E 5.3

Carbon Tetrachlcricc- ' ^13.2 3.7 r c 't- 7.9

i ,1,2,2-Tetrachl croether.e ' ' S. 6 2.4 4 .3 -1 4 .4 4.5

—lli\

Eromccic.nl o rente tharse v- 1 11.2 2.7 r n t r <"b . G - * 0 . C 7.3

(2±)

Lh urcMOcn icromethane ' c _ 2 2.7 .1 f> 1 1 ,1” u. ~t , n 5.5

(-■-]

troiriorcrm 14.0 3.0 o n 5 n a^ “ C J . «-• 8.4

Results of CPA Interlaboratory comparison Studies.


; 25 Percent Confidence Interval.

Client: DuSample ITd'u Cate Coiled

Da t e R e c c-1 v a

« Recovery

57.9

68.5

7EM

63,7

63.1

Organic Analysis Data SheetSjn_ke

•.n.ond Vogel HDR

2.3.-.703Q2.-Ji3)IC2Q -1■eG';il/23./id______:d by Lab: 9/1/84

Sample Matrix:Date Cxtracted/Pre

Soi 1

.-a redKe th oa No: _ qj re.cUSna me Date Analyzed: 11/15/84

Volatile Co;r.prounds tRecoveryVo 1 a t i 1 e Corrsp o u n d

5 rcirometh are ____ 64,1 BenzeneCl: loro.-;e thane Chlorobenzene

C rcmcdich1 oromethane 66.0 Tolnene

Dibrc.-r.och lorosme tnane EthylbenzeneMethylene Chioride AcrcleinE roinoforri

'Acrvlonitri 1 eCh 1 ore ferns . 2-Beta noreCaro on Tetrad: 1 ori de Acetone!richlorofiooronethane

C.'11 o rce tn a no

1 ,1-Dichlcroetnane

1 ,2-Dichloroethane

1,1 ,1 -T ri chloroetnane


.1,1,2,2-Tetrachloroethane

Vinyl Chloride

1 ,1-Dichloroethene


Trichloroethene

Tetrachl oroethe.ne

2-Chloroethylvinyl ether

1,2-Dichloropropane

CIS - 1 ,3-Dichloropropene


i • A-'. i,\. i;,Sjnke

C11£nt; _Dia;t,ond Bogel-ljDRSan:pl e I Sb ~"(’23- 70 30"2 - 22 j"f CT4'A- 6 Oats Collected: Ji/29/84 Date Received by LCii; T9/j/7J4

Sofr;p 1 c Ma t r i x: Soi 1 _Datc- E>-tracted/-PrepaFedT" Method No: EPA_824Q __Date Analyzed: "Tl? I 6?'8 4 '

P.ecov'erx.

O

95.9

102.0

105.6

99.0

Vo 1 a ti1e Compounds ^Lftecovery

Brcmome thane 96.1

Ch1orcmethane

B rcmodi :;i 1 o rcme th a ne __ 94.7

Cabrcrr.ccn i 0r catst.nano

‘•!ethy 1 ere Chi 1 onde

r.- ron.c T o rF

Ch 10 rc f 0 rp

Carbon Tetraciiloride

T rich10 ro fiuo rcme th a ne

Chiorcethane

1 ,1-Dich10 roe thane

1 ,2-Dicnloroethane

1 .1 ,1 -Tri ch 10 roe thane

1 ,1 ,2-Trichlcroethane

1 ,1 ,2,2-Tetrachloroethane

Vinyl Chloride

1,1-Dichloroethene

Trans-1,2-Dichloroetnene

T richloroethene

Vo 1 a ti l_e_Ccrnpour.ds

Benzene

Ch i orober.zene

Tolucne

Ethylbenzene

AeroIein

Aery 1 oni tri 1 e

2-5ut« none

Acetone

Tetrachloroethene

2- Ch 10 rc e tny 1 v i ny 1 e th e r

1,2-Dichloroprcpane

CIS - 1,3-Dichioroprepene

Trans-1,3-Dichlorcpropene


Client: _Diamond-Bogel_HD_R Sair.ple 1.0."[23-70302~-TTpf CD Date Collected': 8/29/84 Date Received by Lab~:9/l/84 •

SPJ_KE

Sample Matrix:___ Soi 1Date Extracted/Prepared ' Method No: Direct Sparqe Date Analyzed': "1177/84

A Recovery

US___

3 7.7

112

116.4

109

119

Vo 1 a ti1e Comooends Recovery

Dro mo me thane 105

Chloromethane _________

B roxodi ch 1 o ro:r.e th are ___ 101.1

01 b r o: so chloromet h a n e

Me try 1 ene Chi crice-

B remoter::;

Ch 1 a ro fo np.

Careen Tetrachloride _________

Trichlorofl uoremethane___________

Chlorcethane

1 ,1-Diehlcroethane

1 ,2-Dichioroethane

1 ,1 ,1-Trichloroetnane


■ 1.1 ,2,2-Tetracn 1 oroethane

Vinyl Chloride

1.1- Dichloroethene

T rans -1 ,2- D i ch 1 o roe th ene

Trich1croech ene

:e trach1o roe ch ene

2 - Ch 1 c rc e thy ] v i ny 1 e th e r

1.2- Dich1orocropane

CIS - 1,3-Dichloropropene


' ‘ u

Volatile Comcoun.

Benzene

Chlorobenzene

To! uc-ne

Ethylbenzene

Acrolein

/“.v.: y i bfi i ■.! i ! _

Organic Analysis Data Sheet Spi kc

Cl i en t: Q-jai;iond_Vo_geL-t|DR _ Sa-p'ie Iii... 12.3 -ia;i02-25TLC15-1i ■ a. c e Ccllecieo: 8/29 /j>4 Date Recei ved oy Lao 9/1/84

Samp 1 e fto tri x SojJ______Da te Extracted/Rropared:Method No:__ Direct SpargeD a t e A n a 1 y z e a:11/12/84

;• Recovery

____ LH_

109.6

109^5

109

ML1

Volatile Compour.ds

B roc;o;i:o thane

Ch 1 c ror.etha ne

B rc-iiiO dichlo rome tn a ne

Dio reito.ch 1 o rone th a ne

Methylene Chloride

Broinoform

Chi ore fori?:

Caroon Tetrachloride

T r i ch 1 o rc f 1 uo rcfte th a n e

Chloroethane

1 ,1-Dichloroethane

1 ,2-Dichlorcethane

1 ,1 ,1-Tri chloroethane


1 ,1 ,2,2-Tetrachl orcettiane

Vinyl Chloride

1.1- Dichloroethene


Trichioroetnene

Tetrachlcroethene

2- Ch 1 o ro e thy 1 v i ny 1 e th e r

1.2- Dichloropropane

CIS - 1,3-Dichloropropene


«Recovery

__1.14J__

_J00V7__

Volatile Comp

Benzene

Chlorobenzene

Tol uer.e

Etnyloenzene

Acrclein

Aery Ionitri1e

2-Sutenor.e

Acetone

ANALYTICAL TECHNOLOGIES, INC. I . D. 01-001145

TCP. v 2TCP7'f ••

-•

TC8r *4

? 5TC8 ?; 6TC8 aSTC8 r8 (Duplii

EPA PRIORITY POLLUTANTS TESTED FOR BY GC/ECD METHOD NO. 608

PESTICIDES, PCB's (water)

A1drina-BHCb-BHCd-BHCg-BHCChlordane4,4'-DDD4,4'-DDE4,4'-DDTDieldrinEndosulfan IEndosulfan IIEndosulfan sulfateEndrinEndrin aldehyde Heptachlor Heptachlor epoxide Toxaphene Methoxychlor

PCB -1016 PCB -1221 PCB -1232 PCB -1242 PCB -1248 PCB -1254 PCB -1260 PCB -1262

LIMIT OF DETECTION (ug/g)

43 6 94

1410

5 .10

3101060

620

sj

30240

60

7575757575757575

u

I.D. * *01-001145

Decanic Analysis Delta Sheet

_________ Sample Matrix:_________ Date Extracted/_________ Method No. 356-12-84 Date Analyzed?"

Pesticides and PC3 1 s

(Ci rc 1 e one.). sg/L orô/Kqy

*______________ Aid rin

_______________ Alpha - BriC

IBeta - EMC

-------------------------Gamma - 3HC (Lindane)

...Delta - BHC

■k______________ Chlordane*4,4' - DDD

!4,4' - DDE

!_____________ 4,4' - DDT

★____ Dieldrin

*Endosulfan I

--------- *_______ Endosulfan II

---------*Endosulfan Sulfate

*____________ Endrin

-------- *_______ Endrin Aldehyde

-------- *_______ Endrin Ketone

........ *Heptachlor

k---------------------- Heptachlor Epoxide

TMethoxych lor

____ 1_______ Toxaphene

____ *_______ Aroclor 1016

* _______ Aroclor 1221

* _______ Aroclor 1232

* _______ Aroclor 1242

____*_______ Aroclor 1248

___ *_______ _ Aroclor 1254

- . * Aroclor 1250

* None Detected

Client: HDR .4884706 Sample T7d?"tC8?2 Date Samp I ed ?_6-7-84 Date Received by Lab:

Soi 1

'Prepa red : 6-2f-8? 50/8080

6-23-84

u

I.D. r01-0011

'JrQcMiic Ana lys if. L.]; a Sheet:

Client: HOP. -884706ba-sip! e !. D. TC8-3Date S a nip 1 edrjr7j^~~IIIDa:e Received by Lao: ~6^]YES4

Scinpl (; lia tr'i •<; SoilDat e Ex trac ted/ivTpar e d~ 6~-T?T-'84Method No.____ 3550/8080 ....Date Analyzed: 6-23-84

Pes ticides and PCB‘s

[ Circle one)""'.

•-9/D 0t? cq/Ku •

★

*

*

*

*

*

*

*•

*

A1 dri n

Alpha - BHC

Beta - BHC

Gamma - BHC (Lindane)

Delta - BHC

Ch1ordane

4,4! - DDD

4,4' - DDE

4,4' - DDT

Di el dri n

Endosulfan I

Endosulfan il

Endosulfan Sulfate

Endrin

Endrin Aldehyde

Endrin Ketone

Heptachlor

Heptachlor Epoxide

Methoxychlor

Toxaphene

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

u

★ None Detected

D.

Orua/ric Analysis D-rta Sheet

c! ^ _HDR *'884706damp is i . D. TC8*4Da te S a flip led: ~6-7-84Date Received by Lab: 6AET2~T84~

SampI e 'la tri x : Soi lDate Extracted/Prepa red :Method No...........3550/8080Date Analyzed: 6-23-84"

Pesticides and PCB's

( C i rc I e .en-e-}-.

A1 d r i n

Alpha - BHC

★

★

★

★

*

*

*

X

X

X

X

X

X

X

X

X

X

X

X

X

Beta - BHC


Delta - BHC

Ch1ordane

4,4' - ODD

4,4' - DDE

4,4' - DDT

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan Sulfate

Endrin

Endrin Aldehyde

Endrin Ketone

Heptach1 or

Heptachi or Epoxide

Methoxych 1 or

Toxaphene

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

u

* None Detected

I.D. •■••01-001145

- o •

Client: HDR-f884706Sample I. ^~Tc8d[~Da te Samp 1 ed __6-7-84Date Received by Lab:

Pesticides and PCB ‘s

(Circle one]:_q/L od To/Kg

*______________ Aldrin

------------------------- A l pi)a - BHC

_______ Beta - BHC

---------- Z-------------Gamma - BHC (Lindane)

______IDei ta - BHC

*Chlordane

_____ !________ 4,4' - DDD

1_______________ 4,4' - DDE

* 4,4' - DDT

*_____________ Dieldrin

*. Endosulfan I

_____ 1_____ _ Endosulfan II

-------- *_______ Endosulfan Sulfate

ZEndrin

--------*________ Endrin Aldehyde

--------------------------- Endrin Ketone

____1. Heptachlor

★—-----------—___ heptachlor Epoxide

-------HMethoxychlor

*.____________ Toxaphene

—_*________ -Aroclor 1016

Organic Analysis Data Sheer

* A rod or 1221Vr Arocl or 1232Hr Aroclor 1242Hr

Aroclor 1248

* Aroclor 1254

* Arocl or 1260

6-21-84

Sample Matrix:____SoilDate Extracted/Prepared: Method No.3550/8080 Date Analyzed: 6-23-84

6-21-84

* None Detected

l.J. =01-001145

ur^fjui c Ana !ys i s Sheet

C1 i en r.: HDR =884706Samp 1 e i'Td TCB7o* Da te Samp 1 ed": 6=7=81Date Received by Lab: 6=17=84“

Sample Matrix: __SoilDate Extracted/Prepared: 5171-84Hetnod No.3550/8080 Date Ana 1 vzed : 6~- x J -84


(Circ1e one)•-9/L arflg/Kg.'

*Aldrin

'_____________ Alpha - BHC

_____I________ Beta - BHC

r. Gamma - BHC (Lindane)

!_____________ Delta - BHC

★ _________ Chlordane* ________ 4,4' - DDD

- ________ 4,4' - DDE

________ 4,4' - DDT

★:___________ __ Di e 1 d r i n*______________ Endosulfan I

* ________ Endosulfan II

*Endosulfan Sul fate

ic__ ________ Endrin

*_____________ . Endrin Aldehyde

*______ _ Endrin Ketone

*_____________ Heptachlor

*---------------------- Heptachlor Epoxide★____________ Methoxychlor

• *

________ ____ Toxapnene

* ________ Aroclor 1016

_ *___________Aroclor 1221

* ________ Aroclor 1232

* ________ Aroclor 1242

____________ Aroclor 1248

___*_____________Aroclor 1254

___ *_____ Aroclor 1260

I.D. -01-001 145

li ' ■na ivsis Data ;net.

Clien t: Sample iToT

HDR -7884706

~7C8*8 T-7T8rDate Sampled: _ .

Date Recc-i ved^bTTaF] Ur2TT!Tzr

Sampl e Ma tri x : SoilDate Extracted/Pripared*: Method No. 35S0/8080 Date Ana 1 yzedT"^Z7Wr~

5T7T-84

Pesticides and RGB's

(Circle cn-aJU. j-.S/L or'uQiK.q}

Aldrin

Alpha - 8HC

Beta - BHC


Delta - BHC

Ch1ordane

4,4’ - ODD

4,4' - DDE

4,4' - DDT

Dieldrin

Endosul fan. I

Endosulfan II

Endosulfan Sulfate

Endrin

Endrin Aldehyde

Endrin Ketone

Heptachlor

Heptachlor Epoxide

Methoxych1 or

Toxaphene

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

* None Detected

i.0. =01-001145

Client: DDR =884706Sample i .1).

Organic Analysis Ddta Sheet.

Sample Matrix: So i 1

Date Sampled:TC8=o Duplicate

Date Received by'Lab: 6-12-8^

Date Extracted/Prepared Method No. 3550/8080

5-21-84

Date Analyzed:_ 6-23-84


(Circle one) cg/L Qiymc/Kq".;i

A1 d r i n

Alpha - BHC

Beta - BHC


Delta - BHC

Chlordane

4,4' - DDD

4,4' - DDE

4,4' - DDT

Diel dri n

Endosulfan I

Endosulfan II

Endosulfan Sul fate

Endrin

Endrin Aldehyde

Endrin Ketone

Heptachlor

. Heptachlor Epoxide

Methoxychlor

Toxaphene

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

* None Detected

n

n. w . Oi-001145

Sample I.D.: _TC8 42 10'-11.5'

Date Collected:_____6-7-84

Date Received by Lab: 6-12-84

Date Analyzed: 6-22-84

VOLAT I II OP. r Arne AT; A!. VO if- ( V'OA)

DA?'A SUMMARY

pq/Kq ag/ho- 12.5 Bromomethane < 11.0 Benzene< 12.5 Cmloromethane < 15.0 Chlorobenzene •< 5.5 Broinodi chioromethane - 15.0 To 1uene< 7.3 Oibromochloromethane < 18.0 Ethy 1 benzene

38.8 Methylene Chloride - 12.5 Ac ro 1 e i n< 11.8 B romo form < 12.5 AcryIonitrile< 4.0 Chlorofo rm < 25.0 Methyl Ethyl Ketone< 7.0 Carbon Tetrachloride < 25.0 Acetone< 12.5 Tri ch 1 orofluoromethane

< 12.5 Ch1oroethane





< 1 7. 3 1,1,2,2-Tet rach1oroethane

12.5 Vinyl Chloride

- 7.0 1,1 -Dich1oroethene

■v 4.0 1rans-1 ,2-Dich1oroethene

- * n^ H . O Trichioroethene

_____«J0.3 iet rach1oroethene

<12.5 2-Chlcroethylvinyl ether


< 12.5 CIS - 1,3-Dich1oropropene ' a

< 12.5 irans- 1,3-Dich1o rop ropene

C? ientHDR -884706___

Sample Matrix:__ Soil

Method No.: 5030/8240

i.D. 01-001145

VOLATILE OPT AM 1 C ANALYSIS (VOA)

DAEA SUMMARY

Client:_HDf^_A_884706

Sample Matrix:___ Soil

Method No. : 5030/8240

Sample I.D.: TC8 ;!2 1.5 1 -16.5'

Date Collected: 6-7-84



pg/Kg

12.5

< 12.5

5.5

< 7.8

< 7,0

<11.8

< 4.0

< 7,0

< 12.5

< 12.5

< 7.0

7.0

•: 9.5

8 romome thane

Cnloromethane

Bromodi ch1oromethane

Dibromochloromethane

Methylene Chloride

Bromoform

Ch 1 o ro fo rm


Trich1oroflnoromethane

Ch1oroethane

1.1- Dichloroethane

1.2- Dichloroethane

1 ,i ,1-Trichloroethane

‘—5 1 ,1 ,2-Trichloroethane

—-1 7• 3.____1 J ,2 ,2-Tetrachloroethane

< 12.5____ Vinyl Chloride

< J•"__ 1,1-Dichloroethene

2—Q Trans-1,2-Dichloroethene

< ^. S Trichloroethene

< 10.3

< 12,5

< 15.0

< 12.5

< 12.5

Tet eachloroethene

2 - Cm 1 o roe t hy I v i ny 1 e t h e r

1,2-Dich1oropropane


Trans-l,3-Dich1oropropene

ug/i'.g ___

11.0 Benzene

< 15.0 Chlorobenzene

*'• 15 ,Q Toluene

18-0 Ethylbenzene

12.5 Acrolein

< 12,5 ___ Ac ry1 onit ri1e

< 25.0____ Methyl Ethyl Ketone

< 25,0 Acetone

‘ u

I.D. 01-001145

-12-

C1 ienr _____ HDR jj384706_________ Sample I . D. : TCS_?4_ 20' -21.5 ‘

Sample Matrix:Soil________ Date Collected: 6-7-84

Method No.: 5030/8240Date Received by Lab: 6-12-84


V0LA7 ! LE OPT AN 1C ANALYSIS (VOA)

DATA SUMMARY

ng/Kg

< 12.5

r: 12.5

c r. J

•- 7.8

27.5

< 11.8

< 4.0

< 7.0

< 12.5

12.5

< 7.0

7.0

< 9.5

< 12.5

17.3

12.5

< 7.0

4.0

1S.1

< 10,3

•: T2.5

< 15.0

< 12,5

< 12.5

8 romometnane

Chloromethane-

8 roiiiodi ch 1 oromethane

Dibromochloroinethane

Methylene Chloride

Bromoform

Ch lorofo rm


Trich1oro f1uoromethane

Chloroethane

1.1 -Dich1oroethane

1.2- Dichloroethane

1.1 , 1 -Trich1oroethane

1J ,2-Trichloroethane

1.1.2.2- Tetra chioroethane

Vinyl Chloride

1.1- Dich1oroethene

i cans - 1 ,2 - Di c.h 1 oroethene

Trichloroethene

Tet rach1oroethene

2-Chloroetnylvinyl ether

1.2- Dich1orcpropane


Trans-1,j-Dichloropropene

__ ug/Kg

11.0 Benzene

•' 15,0 Chlorobenzene

16,800______ Toluene

^ ’ 1^^______ Ethylbenzene

' < 12,5_____ Acrolein

__12.5 Acrylcn i t r i 1 e

. < 25,0 Methyl Ethyl Ketone

< 25,0 Acetone

' u

J.0, 03-001145

VOL AT i LE OR I AN I C AN At “'S !iV(iA;

LAVA SUMMARY

Client:HOP. «884706___

Sample Matrix:____ Soil

Method No.: 5030/3240

Sample I.D.:__TC8 #5 25‘-26.51

Date Collected: _ G-7-84



>9/Kg

■ 12.5

< 5,5

< 7.8

138

< 11.8

< -1.0

< 7,0

< 12.5

< 12,5

< 7,0

7Jl_

-• 9.5

< 12,5

< 17,3

< 12.5

< 7,0

___18.6

___59.7

•• 10.3

< 12.5

< 15,0

< 12.5

< 12.5

Bromometnane

Chloromethane

E romodich1oromethane

Dib romoch1o romethane

Methylene Chloride

E romoform

Ch loro form


Tri ch 1 orofl uoromethane

Chloroethane

1.1- Di chi oroethane

1.2- Dichloroethane

1J ,1-Trichloroethane

1.1.2- Trich1oroethane


Vinyl Chloride

1,1 -Dich1oroethene

!nans-1,2-Dich1oroethene

irich1oroethene

Tetrachloroethene

2-Chloroethy1vinylether

1.2- Dich1oropropane



wg/ Rq

0

- 15.0

3230

< 18.0

< 12.5

< 12,5

507__

206

335

866

513

Benzene

Chlorcbenzene

Toluene

Ethylbenzene

Acrolein

Ac ry1 onit r i 1 e

Methyl Ethyl Ketone

Acetone

Trichlorotrifluoroethane

Methyl Isobutyl Ketone

Methyl Cyclohexane

/

NOTE: Sample was loaded with

hydrocarbons, i.e. mineral

spirits, lacquer thinner.‘ u

I.D. 01-001145

OF 7Am IC ANALYSIS (VOA

7AT A SUMMARY

Client:^?Lf884706

Sample Matrix: Soil

Method Mo. : 5030/8240

Sample I . D. :___ 7C_8 .46 30‘-31.5*


Date Received by Lab:___6-12-84


t; iC / (,']

1 't ?■—___ _

; u . j

12.5

5.5

< 7.8

76.5

< 11.8

< 4.0

< 7.0

< 12.5

12.5

7.0

< 7.0

< S. 5

< 12.5

< 17.3

< 12.5

7.0

4.0

< 4.8

< 10.3

< 12.5

< 15,0

< 12.5

< 12.5

B romouie thane

Chloromethane

8 rornodi ch 1 orcmethane

Dibromochloromethane

Me thy ie.ne Chloride

BrodiOform .

Ch 1 o ro fo rm


Tri ch 1 orofl uoromethane

Ch1oroe thane

1 ,1 -Oi chi oroethane

1 ,2-Dich1oroethane

1 ,1 ,1-Trich1oroethane


1 ,1,2,2-Tetrach1oroethane

Vinyl Chloride

1,1 -Dichloroethene

T rans- 1,2-Dich1oroethene

i ri ch 1 croetherie

! e t rach1oroethene

2-Ch1oroethy 1vinylether

1,2-Dich1o ropropane

CIS - 1 ,3- Di ch 1 oroproperie

irans-1,3-Dich1oropropene

I 1.0___ Benzene

15.0 Ch 1 c robenzene

639___ Toluene

1628______ Ethylbenzene

12.5 Ac r o 1 e i n

12.5 Aery I on i t r i 1 e

25.0 Metnyl Ethyl Ketone

< 25.0 Acetone

MOTE: Sample loaded with hydro

carbons, i.e. mineral spirits,

lacquer thinner.

I.D. 01-001145

VOL AT 1 Lf CRT AN i C AN AI^YS I S (VGA)

HATA SUMMARY

c l i er.t __HDR_£ 8S4 706

Sample Matrix:Soil

.Method Me.: 5030/8240

Sample i.D.: fCS 48 40 ! -41.5'




:i ronioinet hane

Chloromethene

o. 5

40.0

11.3

< 4,0

<■ 7.0

< 12.5

<12,5

< __ 7 J0_

'■ 7.0

B rc-modi chi c r c m e t h a n e

uib ronicchio romethane

Methylene Chloride

Broinoform

Ch 1 o ro fo rm


Tri ch lorof 1 uoroinethane

Ch1oroethane

1 ,1 -Dich1oroethane

1,2-Dich1oroethane

i . i ,1-Trichloroethane

12.5

< 17.3

- 12.5

7.0

< 4 . G

4.3

< 10.3

< 12,5

< 15.0

< 12.5

•: 12.5

!,1-2-Trich1oroethane

1.1.2.2- Tet rach1oroethane

Vinyl Chloride

1,1 -Dich1oroe thene

Trans-1,2-Dich1oroethene

Tricnloroethene

Tet rach1oroethene

2-Chloroethylvinylether

1.2- Dich1o ropropane

C1- - 1,3-Dich1oropropene

icans-1,3-Dich1oropropene

-9/Tq

11-0____ Benzene

_z 15.0___ Chlorobenzene

•- 11.0 T o i u e n e

•5 Ethylbenzene

12.5 Acrolein

12.5 __ Ac ry 1 on i t r i 1 e

< 25,0____ Methyl Ethyl Ketone

•' 25.0____ Acetone

NOTE: Sample loaded with hydro

carbons, i.e. mineral

spirits, lacquer thinner

J.D. -01-001145

i

inorônic Ana ! v-. i1

Client: HDR ,?884706Sample T.D. TC8?T102'n".'oT““.....Date Collected7 _ ' 6-7-84 Date Received by Lab: fc-12-82'

(Circle one) mg/L or^rriq/Kq;

<2.5

'^triv:.... .....So _ ___Date fmv.cted/Preparea: 7\cid Digested Method ,Nc.3050 ' ‘i“Date Analyzed: ~ o-TfUlli)

(Circle one) ni£/L_ or mg/Kg

12.1

1 .

14.9

= 5.0

Antimony CalciumArs eni c

MagnesiumBarium Phosphorous

B e ry 11 i um

Boron—

Potassium

SiliconCaamium TinChromium (Total)

Chr'omium (hexavalent)

Cobait

Copper

I ron

6.9

= 0.1

_25_._9

<2.5

: 2.5

<2.5

67.3

Lead (Total)

Lead (organic)

Manganese

Mercury

Molybdenum

Nickel

Sel&niurn

Si 1ver

Sodiurn

Thai 1ium

Vanadium

Zi ric

l.D. =0]-00114b

Inorganic Ana I'/si P ♦ • r • . . , i L d j t) t.- •

Client: HDR ^884706bample iTDr~Tc'8>3 1 5 1 -1 6 .IT7 pate Collected: 6-7-84Date Received by~TaFflFT2~i34

Sample Matrix: SoilDate Extracted/Prepared: ScuTDTaestionMethod No.___ ___ 3050 “Dote Analyzed?- 6-2T-'B4----------------

(C i rc 1 e mq/L onf mq/Kq

-1.0

<0.5

7.3

<5.0

6.1

<0.1

10.3

(Circle one) mq/L or mq/Kq

Antimony CalciurnArseni c

MagnesiumBarium PhosphorousBery 11 i um

PotassiumBoron

Si 1 iconCadmium

i i n .Chromium (Total)

Chromium (hexavalent)

Cobalt

Copper

Iron

Lead (Total)

Lead (organic)

Manganese

Mercury

Molybdenum

Nickel<2.5

<2.5Seleniurn

Silver

Sodiurn

Thai 1ium

16.8Vanadium

Zi nc u

' • D. -'01-001145

1 -

: no rqa ni Analysis Data Sheet

Cilent: _ HPR *884706 iaifip le I. D. T Cpa"PTT fi? f~Da r.e Coll ec tea : ^7 -84 Date Received by Lab: ~6^l 2-84

Sample Matrix:____ SoilDa te Extracted/PreparedT-Method No_.___ 3050 —Date Analyzed: ~6-25^7^4

Acid Digestion

(Circle ong) mq/L o»niq/Kq

Antimony

Arsenic

(Circle one)

.'iiq/L or mg/Kg

<1.0

<0,5

7.2

<5.0

5.2

<0.1

Bari urn

Beryllium

Boron

Cadmiurn

Chromium (Total)


Cobalt

Copper

I ron

Lead (Total)

Lead (organic)

Manganese

Mercury

10.4

<2.5

<2.5

Molybdenum

Nickel

Seleniurn

Silver

Sodi uiii

Ca lei urn

Magnes i urn

Phosphorous

Potassiurn

Si 1 icon

Tin .

15^

Thal l i uin

Vanadium

Zi nc

.D. ;;01 -O'.

i norga r, ’ i c I y < Da •eoi

Client: HDR *884706 Sample T.ThDate Col lected? 6-7-84 Date Received by'

TCS?5' 25'-26.5

Lab: 6-12-84

Sanipl e taU'i x : -*oi 1Date Lxtracted/Prepared: Acid Digestion Method Ko. 3050 " ‘Date Analyzed": 6-25-84

(C i rc 1 eôtie)— inq/L of- iiiq/Kq

(Circle one) mq/L or mo/Ko

<2.5

6.2

--1 .0

<0.5

ITT

Antimony

Arsenic

Sari urn

B e ry 11 i urn

Boron

Cadmiurn

Chromium (Total)

Chromium (hexavalerit)

<5.0

6.7

<0.1

15.5

<2.5

<777

<2.5

26.2

Cobalt

Copper

I ron

Lead (Total)

Lead (organic)

Manganese

Mercury

Molybdenum

Nickel

S e1eniurn

Silver

Sodiurn

Thallium

Vanadium

Zi nc

Calcium

Magnesium

Phosphorous

Potassium

Si 1 icon

Tin

' u

I.D. -01-001145

C

riient: HDR ^884706 Sample M^tr-Sample I ■ D-__TC8j[6~30T~31\ 5^ Date Extracted:Oate Collected: 6-7-84 _ Method Mo.Date Received by Tab : Tl 2T4 ~ Date Analyzed:"

Inorganic 'Analysis lj(, u

(C i rc 1 e oofrpT. iTic/L Q-Tmq/Kq )

7.8

Antimony

Ars eni c

can um

Bery 11 i um

(Circle one) incj/L or m_g/_Kq

Boren

Cadmium

Chromium (Total)


Cobalt

Copper

I ron

5.2

<0.1

14.5

<5.0<2?5

<5.0

24.5

Lead (Total)

Lead (organic)

Manganese

Mercury

Molybdenum

Nickel

Sel en i urn

Si1ver

Sodium

Tha11ium

Vanadium

Zi nc

....~Jo.ilPrepared Acid Digestion

3050 6-25-84

Calcium

Mag ties i um

Phosphorous

Po tas sium

Si 1icon

Tin

u

Inorganic Analysis . Oar.a She

C i itutHOk -• 834 70bSample f.D.' TC *S"TlT'To‘r-TrFr“ Date Collected": 6-7-84’’"Date Received by Lab: ~1>^T2-2A

Sample Matrix: SoilDate Extracted/Prepared: oMethod No. _305Q .Date Analyzed": (T-25-84

(Circle mq/L or

<2.5

12.1

<1.0

<0.5

14.9

(Circle one) mq/L or rng/Kq

Antimony

Art eni c

Eari um

Beryllium

Boron

Cadmium

Chromium (Total)


Cobalt

<5.0____ Copper

6.9

<0.1

25.9

<2,5

<2.5

<2.5

67.3

J ron

Lead (Total)

Lead (organic)

Manganese

Mercury

Molybdenum

Nickel

Selenium

Si 1ver

Sodium

Thai 1ium

Vanadium

Zi nc

Calciurn

Maones i urn

Phosphorous

Potass i uni

Si 1 icon

Tin

u

TZ^Wf

Inorganic Analysis Data Sheet

Client: HDR A884706Sample 'I.D. TCS A3 151 -16.51 Date Collected: 6-7-84Date Received by Lab: G8~4

Sample Matrix:Soi 1Date Extracted/Prepared: 6-22-84Method No. 3050Date Analyzed: 6-25-84

i£L5

JL3_

6J

<0.1

JLfl.,.3.

.5

(Circle one) nig/L or mg/Kq

Antimony

Arseni c

Sari urn

Bery 11 i urn

Boron

Cadmi uni

Chromium (Total)


Cobalt

Copper

I ron

Lead (Total)

Lead (organic)

Manganese

Mercury

Molybdenum

Nickel

Seleniurn

Si1ver

Sodium

Thallium

________ Vanadium

15.8 Zinc

Cal ci urn

Msgnes i uni

Phosphorous

Potassium

Si 1icon

Tin

‘ u

iiiorociiic Analytic p,aia c!ieet-

C1ient: Pi DR -834 706Sample I.D. rCU Date Collected: Date Received by"

Saii:p 1 e Ma cr i x: i 1Date Extracted/Pt'epaT'e’di 5-22-84'Method No. 3050Date Analyzed: ' ~6-To:~S~

(C i re: 1 e qjw) inq/L or fmiq/Kq)

____ <2^5

4.8

■ 1.0

<0.5

7.2

<5.0

5.2

(Circle one)mcj/L or mg/Ka

Antimony Ca 1 ci uni

Arsenic Mag lies i um

Barium Phos pnorous

Bery 11 i um Potassium

Boron Si 1icon

Cadmium

Chromium (Total)


Cobalt

Copper

I ron

Lead (Total)

Lead (organic)

Tin

<0.1

10.4<275

7?7'5

Manganese

Mercury

Molybdenum

Nickel

Sel c-ni urn

S i 1ver

Sodiurn

Thai!ium

15.5Vanadium

Zi ncu

Inorganic Analysis D.ii.a Sheet

Client: _HDj^ ^88470^______Sample l.D. TCS ?5'~257-26'.57Da te Co 11 ected’: 6^7-84Da te Rece i ved by- Lab riTTJC'sT"

Sample Matrix: ~01!Date Extracted/repared: 6-12;■ 1 eth od No. _ 3050Date Analyzed: 6-20-84

(Circle pjie^mq/L orfma/KoJ

------------<8.5

6.2.

Antimony

Arseni c

(Circle one) mq/L or mg/Kg

<5.0

Bari urn

B e ry 11 i um

Boron

Cadmium

Cnromium (Total)


Cobalt

Copper

I ron

Lead (Total)

Lead (organic)

Manganese

Mercury

Molybdenum

Nickel

Selenium

Si 1ver

Sodium

Thai 1ium

26. OCVanadium

Zi nc

Calcium

Ma onesiurn

Phosphorous

P 0 t u S S "i U IT!

Si 1 icon

Tin

u

HOP. •-■884 70C'• TC8 ^8"40‘ -4i .5' tec': 6-7-84

6-12-84p 4 r f\ r*.c le /-r / 2 i-* f

Soil■' r'‘'ec erec7" ~6 3050~’6r25"-84

i.

'c.z>

a. /

<l.n

<GL5

14,2

<5.0

<0.1

12.5

^ O v P c

36.1

tn ro

■_f;ror:' u :■ ' vc

:■.= '"Oory

MciyDuern

Nickel

Seieni u;:

i v e •'

.10 01 .

varioî u i!'

Zi no

rc 1 or- _! . o r

\-C » 1 ;jr.i

Magnc-r. i o--

Pnc< to

P-P T - C c; |

S1} i c rt

11 n

■ ' u

I f\j

VOL AT I Lf ORT/V!! C ANALYSIS (VOA;

DAI A SUMMARf

Cl ient HDR 4884706

Sample Matrix:______Soil

Method No.: 5030/8240

Sample i.0.: TC8 ? & 40'-41.51




uq,- f.cj

- 12.5

< 12.5

■■ 5,5

7.8

40.0

< 11.8

< 4,0

< 7.0

< 12.5

< 12,5

-■ 7,0

_<__ 7.0

-- 9,5

<- 12.5

< 17.3

s 12.5

< 7.0

B romomethane

Ch loro.me thane

Brornodichlaroinethane

Di b rcmoch 1 o roine thane

Methylene Chloride

B romoform

Ch 1 o ro fo rm


T ri ch 1 crofl uo roine thane

Ch1oroethane

1,1 -Dich1oroethane

1 ,2-Di chloroethane

1 >i,1-Trichloroethane

1.1.2- Trichioroethane


Vinyl Chloride

1,1-Dichioroethene

4.0

< 4.8

•: 10.3

12.5

«: 15.0

< 12.5

< 12.5


T rich1oroethene

Tet rach1oroethene

2-Ch1oroethylv i nylether

1 ,2-Di ch Icropropane



< 11 . 0

< 15,0 •

< 15.0

35.5

12.5

< 12.5

< 25,0

< 25.0

Benzene

Ch1orobenzene

Toluene

tthy1 benzene

Acrolein

Aery Ion itrile

Methyl Ethyl Ketone

Acetone

NOTES:

1; Sample loaded with hydrocarbons

i-e. - mineral spirits, lacquer

thinner.

2) Methylene Chloride is suspected

to be a laboratory contaminant.

-29-

VGLATI Lf; ORTAfMC ANALYSIS (V OA;

DATA SUMMARY

— Client; HDR f884706 Sample I.[ j.; TC8 ? 3 15'-16.51u/!ip 16 Mdr. r i x .. Soil Date Co 11 ected; 6-7-84

— Method No. : 5030/8240 Date Received bv lab- 6-12-84

Date Analy zed; 6-22-84

oq:Ko oq/Kg

— 12.5 8 romomethane ■: 11.0 Benzene•: 12.5 Ch loroniethane •• 15.0 ' ChIerobenzene

— 5.5 BroffiodichIoromethane =■ 15.0 To 1uene7 ^ Dib romoch1o romethane < 18.0 Ethylbenzene

— •; /. 0 Methylene Chloride < 12.5 Acrolein< 11.3 B romo form < 12.5 Acrylonitri le

—< 4.0 Chlorofo rm < 25.0 Methyl Ethyl Ketone< 7.0 Carbon Tetrachloride < 25.0 Acetone

—< 12.5 Trich1orofiuoromethane

•- 12.5 Ch1oroethane

—■- 7.0 1,1 -Dich1oroethane

“» r*/ . U 1,2-Dichioroethane

—< 9.5 1 ,1 ,1-Trich1oroethane

•; 12.5 1 ,1 ,2-Trichioroethane

—17.3 1 ,1 ,2,2-Tetrachioroethane



^.0 Trans-1,2-Dich1oroethene

4.8 T ricn1oroethene

< 10.3 Tet racii 1 oroethene

__< 12.5 2-Chloroetnyivinyl ether

< 15.0 i,2-Dichloropropane

•: 12.5 CIS - 1 ,3-Dich1oropropene ' ' U

1 ") ~ T rans-1,3-Dich1oropropene

—

BU

LL tank: ana:i

TAT A, SUMMARY

■ • ‘--n tHDR •- 334706

S uii ij ] e Mc31 r j v ; £(, -j i

Method No.: 5030/3340

Sample _____ TC8 ?2 10'- 1 ] . 5 *

Date Colloctea: 6-7-84



pg/l'-q

12.

Jo ,

•' 11.8

< 4.0

< 12,5

< 12,5

< 7.0

•: 12.5

Broinome. thane

Ch 1 o roaiezn ane

B ronioci c.h 1 o roc-ethane

D'i bronioch loromethane

Methylene Chloride

Broinoform

Ch 1 o ro fo rm


Trichlorofluoromethane

Ch1croethane

1,1 -Dich1oroethane

1,2-Dichloroethane

1,1 ,1-Trichloroethane

1 >1 .2-Trichloroethane

1,1 ,2,2-Tetrach1oroethane

Vinyl Cnloride

y 10,3

< 12,5

< 15,0

< 12.5

• , 1 -Dich1oroethene

Trent-1,2-Dich1oroethene

T rich1oroethene

ie t rach1oroethene

a - Ch ) o roe thy 1 v i ny 1 etiie r

1,2-Dich1oroprcpane

CIS - I , 3-Dichloropropene

Tran s- 1,j-Dicnloropropene

ua/Kc

11.0____benzene

13•Q____ Chlorobenzene

.C o1uene

< 12.5

< 12.5

25.0

< 25.0

Ethyl be rizene

Ac ro 1 e i r:

Acrylonitrile

Methyl Ethyl he

Acetone

ne

NOTE: Methylene Chloride is

suspectea to be a laboratory

contaminant.

a

-3 i

VOL AT ILE OR:'/v::r; analyt

DAI A SUMMARY

Cl i ent :HDR *884706

Sample Matrix:___ Soil

Method ho. : 5030/82*40

Sample I.D.: 1C8 ~ 6 30*-31.5‘

Date Collected: 6-7-S4

L'ate Received by Lab: 6-12-84


nq/Ag

< 12.5

12.5

5.5

V 7.8

76.5

< 11.8

< 4.0

< 7.0

12.5

Bromometnane

Chioromethane

Brcmodi chloromethane

Dibromochlorcmethane

Methylene Chloride

Bromoform

Ch 1 o ro form


Tri cm ! orof 1 uoromethane

••• 11.0

15.0

689

1628

< 12,5

< 12.5

< 25.0

< 25.0

Benzene

Ch1orobenzene

To 1uene

Ethylbenzene

Ac ro1e i n

Aery Ion it ri le

Methyl Ethyl Ketone

Acetone

< 12,5

< 7,0

< 7,0

< 9,5

< 12.5

< 17.3

■- 12.5

< 7.0

< 4.0

10.3

' 12.5

<15,0

< 12.5

< 12.5

Ch1oroethane

1 .1 -Di chloroethane

1 ,2-Dichloroethane

1 .1 ,1-Trichloroethane

1,1,2-Trichloroethane

1 ,1 ,2,2-Tetrachloroethane

Vinyl Chloride

1 ,1 -Dich1oroethene


T richloroethene

letrach1oroethene

2-Ch1oroethy 1 vinyl ether

1,2-Dich1cropropane

CiS - i,3-Dich1oropropene


NOTE:

1/ sample loaded with hydrocarbons

i.e. - mineral spirits, lacquer

thinner



32-

V0LA7ILE' ORTAMiC AfJALYSIS

ih'\ i i\ SUMMARY

( Y QA)

Cl lent :HDR ? 884706

Sample Matrix: Soil

Method flo.: 5030/8240

Sample I.D.: TC8 A5 25‘-26.5'



Date Aria ] y z e d : 6-22-84

pc, r.Q

B rcmcmsthane

Ch1o romethane

__j__ 5.5

< 7.8

138

< 11.8

4_0_

_r__ 7.0_

< 12.5

< 12.5

< 7.0

7.0

• ■ 5,5

•• 12,5

< 17,3

< 12.5

< 7,0

18.6

B rcmocichloromethane

Dib comechloromethane

Methylene Chloride

Bromoform

Cn lore form

Carbon êtrachloride

T richlorofluoromethane

Ch1oroethane

1,1 -Dich1oroethane

1 ,2-Dich1oroethane

1 .1 ,1 -Trich1oroethane

1 ,1 ,2 -Trichioroethane

1 , i ,2 ,2-Tetrach1oroethane

Vinyl Cnloride

1 ,1 - .01 ch 1 oroethene


59.7___ Trichioroethene

____ Tetrach 1 oroethene

^^____ 2-Cn i orcethy 1 vi nj' 1 ether

—^ 1 ,2-Di ch loropropane

------- CIS - I , 3- Di ch 1 oropropene

— ~ D Trans -1,3-Dich1oropropene

li r. i Q

.0 Benzene

3230__

12.5

< 1? s

507

206

335

866

513

Ch1orobenzene

Toluene

Ethylbenzene

Acrolein

Aery Ionitrile

Methyl Ethyl Ketone

Acetone

Trichl orotrif1uoroeth

Methyl isobutyl keton

Methyl Cyclohexane

NOTE:

1) sample was loaded with hydro

carbons i.e. - mineral spirits,

lacqu'br thinner



SEM: - VOL. AT L F ORGANIC/\J i h.

DATA SHEET

Client.’:__ HDR

Sample I. D. 01-001 146 :TCc

Sample Matrix: Soil

Method Wo.: FPA 8270

Date Sampled: 6-7-84


Date extracted/prepared: 6-20-84

Date Analyzed: 7-j1-84

___mg/Kc

< 0,80

< 0.33

< 0.98

< 0.27

< 0.30

<0.36

< 0.94

< 2.4

<0.36

< 0.24

< 4.2

< 0.19

< 0.35

< 4.4___

< 0.2 d

< 0,22 . r\ r- „< U . 04

mq/Kq .

Phenol■ 0.37 Inceno (l,2,3-c,d;s Pyrene

Benzo (g,h,i; perylene

Benzo (a) Pyrene

2-Chlorophenol < 0.412 ,4- Di ch 1 oropheriol " 0.252,4,6-Trich1orophenol

4-Chloro-3-methylphenol (p

Peritach 1 orepheno 1-chloro-m-cresol)

2 ,4-Dimethyl phenol

2-methy1 - 4,6-dinit ropheno1

2-Wit rophenol(4,6-dinitro- o-cresol)

4-Nitrophenol

2,4-Dinit rophenol

Acenapthene

Acenaphthylene

Benzidine

Chrysene

Isophorcne

Pnenanth rene

< 0.19

—< 0.78

< 0.25

< 0. 19

< 0.22

< 0.25

< 0.25

< 0.19

Anth racene

ben-c- (a) anthracene

Dibenzo (a,r.) anthracene

Fluorene

FI uoranthene

Benzo (b) fluoranthene

Benzo (k) fluoranthene

Pyrene

a

VOLATILE Of-:fA‘I C ANALVS IT

UMMAR

C1ient : HDR ^384706

Sample Matrix: Soil

Method No.: 5030/8240

Sample I.D.: TC8 ? 4 20‘-21.5'

Sate Collected: 6-7-84


Date Analysed: , 6-22-84

B rcmomethane

Chloromethane

Bromcdichloromethane

7 Q/ . u27.5

n .a

< 4.0

< 7.0

< 12.5

< 12.5

Dib romoch1oromethane

Metnylene Chloride

Brcmoform

Ch lore form


Trich1oro fluoromethane

Chloroethane

< 7,0

< 7,0

< 9.5

< 12.5

< 17.3

< 12.5

< 7,0

-■ 4,0

___18,1

-■ 10.3

< 12.5

< 15.0

•- 12,5

< 12.5

1 ,1 -Di ch 1 oroethane

1 ,2-Dichloroethane

1 >■,1-Trichioroethane



Vinyl Chloride

1 ,1-Dichloroethene


Tri ch 1 o roetherie

Tetrach1orcethene

2-Chloroethy 1vinyiether

1 ,2-Dich1oropropane

CIS - 1 ,3-Dich1oropropene

Trans-1,3-Dich1o rop ropene

11.0

if n

Benzene

Cn 1 orobenzene

72,140

__ < 12.5

-■ 12.5

< 25.0

- 25.0

Toluene

Ethy Ibenze.oe

Acrolein

Aery 1 onit ri1e

Methyl Ethyl Ketone

Acetone

N01 cc: Methylene Chloride is

suspected to be a

1aboratory contaminant.

u

- ;-h -

SEMI-VOLATILE 0 R GAN IC AN A L Y SIS

DATA SHEET

Client:_____HDR

Sample I. D. (TC8 ?i )

Sample Mat rix:__ So i 1

Method No. : EPA 32 70

_ Date Sampled:___ 6-7-84

Date Received by Lab:____6-12-84

_ Date Extracted/Prepared: 6-20-84


jnq/Kq

< D•19_____ Hexach1orobenzene

0.19

0.19

< 0.44

0.19

1.7

0.57

0.25

0.25

0.19

< 0.25

< 2.20.16

0.25

0.25

1. 7

0.57

< 0.5 7

<0.42

< 0.53

0.19

0.16

< 0.09

MIC9/ Kg

_ Nitrobenzene

__ 1 >2-Dich1orobenzene

_ 1>3-Dich1orobenzene

_ 1,4-Dichlorobenzene

_ 1 >2,4-Tr:ch1orobenzene

_ 3,3-Dichlorobenzidine

_ 2,4-Dinitrote 1uene

_ 2,6-Qinitrotoluene

_ N-Nit ros odimethy1 amine

... N-Ni trosodi phenyl ami ne

_ trosodi-n-propylamine

_ Diethyl Phthalate,

_ Dimethyl Phthalate

_ Di-n-butyl Phthalate

_ Butyl benzylphathalate

- Gis '• 2-ethyl hexyl) phthalate

. Dis (2-chloroethyl) ether

. Bis (2-chloroisopropy1) ether

4-Chlorophenyl-phenyl ether

Bis (2-chloroethoxv) methane

4-Broinophenyl-pheny 1 ether

Hexachloroethane

Hexachlorobutadierie

:. 16

0.19

0.57

Hexach1orocyclopentadiene

Napthalene

2-Chloronapthalene

1 ',2- Di pheny 1 hy d raz i ne

Di-n-Octyl Phthalate

SFKT - VOLA" i LE GkGAf.'! C ANA[

data sheet

Client h’DR

Sample i. D. : 01-001145 (TC8 ^2)

Sample Matri x: So i 1

Method No. : EPA 8270

Date Sampled: 6-7-S4

Date Receivec by Lab: 6-12-84

Date Extracted/?repa re d 6-20-84


SPIKE

",mg/Kgmq/Kc

____84.8

< 0.33

< 0.98

< 0.27

<0.30

39.2

85.4

< 2.4

<0.36

< 0.24

< 4.2

< 0.19

<0.35

<4.4

< 0.25

< 0.22

129.5

< 0.19

<0,78

< 0.25

116,4

< 0.22< 0.25

< 0.25

< 0.19

Phenol

2-Chlorophenol

2 ,4-Dich1orophenol

2>4 ,6-irich1oropheno1

4-Chloro-3-methy 1 phenol (p

Pentach1orophenol


2-methy1 - 4,6-di n i t rophenol

2-N!trophenol

4-Nitrophenol

2 ,4-Dinit rophenol

Acenapthene

Acenaphthy1ene

Benzidine

Ch rysene

Isophorone

Indeno (l,2,3-c,d) Pyr&n

Benzo (g,h,i) perylene

Benzo (a) Pyrene

-chloro-m-cresol)

(4 ,6-diriitro-o-cresol)

Phenanth rene

Anth racene

Benzo {aj anthracene

Dibenzo (a,h) anthracene

FI uorene

FI uorantnene



Pyrene

SEMI-VOLATILE ORGANIC At/SIS

DATA SHEET

covery

0.25

< 0.25

101.0

0.5

0.42

0.53

125.9

0.16

121.2

Butylbenzylphathalate

Bis (2-ethylhexyl) phthalate

_ P,1S (2-chloroethyl) ether

__ Bis (2-ch 1 oroisopropy 1) ether

_ 4-ChTorophenyl-phenyl ether

_ Bis (2-chloroethoxy) methane

_ 4-Brornophenyl-phenyl ether

Hexach1oroethane

Hexachlorobutadiene

Cl i ent‘: HDR Date Sampled:Sample 1.0.: 01-001145 (TC8 42) Date Received by LabSample Matrix: Soi 1 Date Extracted/PrepaMethod No.: EPA 8270 Cate Analyzed: 7-1

- ;n 3/Kg mq./Kg

< 0.19 Hexach1orobenzene 0.2598.2 Nit robenzene < 0.16

< 0.19 1 ,2-Dichlorobenzene < 0.19< 0.19 1,3-Oichlorobenzene < 0.5779.4 1,4-Dichlorobenzene 92.9

118.9 1>2,4-Trichlorobenzene

< 1.7 3,3-Dichiorobenzidine

97.8 2,4-Dinitrotoluene

< 0.25 2,6-Dinit rotoluene

< 0.25 N-Nitrosodimethyl amine

< 0.19 N-Ni t ros odiphenyl amine

81.7 N-Nitresodi-n-propyl amine

< 2.2 Diethyl PhthalateoV

Dimethyl Phthalate

< 0.25 Di-n-butyl Phthalate

6-7-84

6-12-84

6-20-84

lexachlcrocyclopentadien

Napthalene

SEMI -VOLA:iLE ORGAN IC ANAL VS IS

DATA. SHEET

Cl i ent':_______ HDR

Sample i.D.:OI-OQ]145 {TC8 *3)

Sample Matrix:______ Soil

Me tiled No. ; EPA 32 70



Date Extracted/Prepared: 6-20-84


rnp/Ka------VZ____ jf. nig/Kq

< 0. SO

< 0.33

< 0.98

< 0.27

<0.30

< 0.36

< 0.94

< 2.4

<0.36

< 0.24

< 4,2

< 0.19

< 0.35

< 4.4

< 0.25

< 0.22

< 0.54

< 0.19

< 0,76

< 0.25

< 0.19

< 0.22

< 0.25

< 0.25

< 0.19

Phenol < 0.37 Indeno (1 ,2,3-c.d)2-Ch1orophenc1 < 0.41 Benzo (g,h,il pery2,4-Dichlorophenoi 0.25 Benzo (a) Pyrene2,4,6-Trichlorophenoi

4-Chloro-3-methyl phenol (p-chloro-m- cresol)Pentachlorophenol

2 ,4-Dimethylphenol

2-methyl-4,6-dinitrophenol (4,6-dinitro-o-cresol)

2-Nit hd phenol

4-Nitrophenol

2,4-Dinitrophenol

Acenapthene

Acenaphthylene

Benzidine

Chrysene

Isopnorone

Phenanth rene

Anth racene

Benzo (a) anthracene

Dibenzo (a,n) anthracene

FI uorene

FIuoranthene



Pyrene

Pyrene

!c-ne

it Mi - V0LA7 I i_T ORGAN I C Af J A i. V S ] $

DATA SHLL7

Cll'ent':________HDR

Sample I. D.: 01-001145 TCft ?3

Sample Matrix:501i

Method No. : £p^ 2.270

Date

Date

Date

Date

Sampled: 6-7-.R4

Received by Lab: 6-12-84

Lxoracted/Prepared; n-?0-84

Analyzed: 7-11-84

mq/Kq

< 0.19

< 0.19

< 0.19

< 0.19

< 0,44

< 0.19

< 1.7

< 0.57

< 0.25

< 0.25

•- 0.19

< 0.25

< 2.2

< 0. 16

< 0.25

< 0.25

2.0

< 0.57

< 0.5 7___

<0.42

< 0.53

< 0.19

< 0.16

< 0.09

. 2,4-Dinitrotoluene

2,6-Dinit roto1uene

N-Nit rosodimethyl amine

N-Nit ros odiphenyI amine

mq/Kq

Hexach 1 orobenzerie< 0.25

Nit rcbenzene< 0. 16

1,2-Dichlorobenzene< 0.19

1,3-Dichlorobenzene< 0.57

1 >4-Dich1orobenzene< 0.25

i.2,4-Trichlorobenzene

3,3-Dichlorobenzidine

N-Nit rosodi-n-propyl amine

Diethyl Phthalate

Dimethyl Phthalate

Di-n-butyl Phthalate

. Butyl benzylphathalate

Bis (z-ethylhexyl) phthalate

Bis (2-ch1oroethy1) ether

Bis (2-ch1orcisopropy1) ether

4-Ch1orophenyl-phenyl ether

Bis (2-chloroethoxy) methane

4-Bromcphenyl-phenyl ether

Hexach1oroethane

Hexachlorobutadiene

Hexach1orocyclopenta diene

Napthalene•

2-Chloronapthalene

1 ,2-Diphenylhydrazine


SEMI-VOLATILE ORGAN!£ ANALYSIS

BATA SHEET

Client:_ HOP,

Sample I. D. :___ 01-00114 5 (TCS ^sT

Sample Mat ri x :___ c0]

Method No. : £p/\





____ mg ,/Kg

< 0.80

<0.33

< 0.98

< 0.27

__ <0.30

__ < 0.36

<0.94

< 2.4

< 0.36

< 0.24

< 4.2

< 0.19

< 0.35

< 4.4

< 0.25

< 0.22

< 0.54

< Q.19

< 0. 78

< 0.25

< 0.19

< 0.22

< 0.25

< 0.25

< 0.19

niq/Kq

Phenol

2-Chlorophenol

2,4-Dicn1orophenol

2,4,6-Trich1orophenol

0.37

0.41

< 0.25

Indeno (1,2,3-c.d; p:

Benzo (g.h.i) peryler

Benzo (a) Pyrene

4-Ch1o ro-3-methy1pheno1 (p-chioro-m-c res o1)

Pentach1orophenol


2-methy1 -4,6-dinit ropheno1 (4 ,6-dinit ro-o-creso1)

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol

Acenapthene

Acenaphthylene

Benzidine

Ch rysene

Isopnorone

Phenantnrene

Ant!) racene



FIuorene

Fluoranthene



Pyrene

ene

' ’ tMJ- V 01. AT I L E OR G AN' p C AN ALYSIS

DATA SHEET

Cl Tent

Sample

Sample;

Method

:_____ HDk______

1 • D- •'__ 01-003 145 (TC8 451

Kat n’ x Soil

,)0- •'EPA 82 70

Date Sampled; 6-7-84



Date Analyzed; 7-12-84

mc/Kfjriuj/K q

r\ i r\u . « 9 ____ Hexach 1 oroberzene< 0.25

___ < 0.19 N'i t robenzenp< 0.16.

< 0.19 ____ ' .2-Dich1crobenzene< 0.19

< 0.19 1,3-Dich1orobenzene< 0.5 7

0.44 1,4-Dichlorobenzene< 0.25

< C. 19 1>2 ,4-Trich1orobenzene

< 1.7 3,3-Dich1orobenzidine

< 0.57 2,4-Dinitrotoluene

< 0.25 2,6-Dinit roto1uene

< 0.25 N-Nitrosodimethyl amine

< 0.19 N-Nit rosodiphenyl amine

< 0.25 N-Nitrosodi-n-propylamine

<2.2 Diethyl Phthalate

< 0.16 Dimethyl Phthalate

< 0.25 Di-n-butyl Phthalate

< 0.25 ButylbenzyIphathalate

5.3 Bis (2-ethy1 hexyl) phthalate

___ < 0.57 Bis (2-chl oroethy 1} ethe*-

.__ 0.5 / — Bis (2-chloroisopropyl) ether

__ < 0.42 4-Ch1orophenyl-phenyl ether

< 0.53 — Bis (2-chloroethoxy) methane

< 0-19 - 4-Bromopnenyl-phenyl ether

< 0.16 Hexach1oroethane

< 0.09 Hexachlorobutadiene

Hexachlorocyclopentaciene

Napthalene

2-ChlorGnapthalene

1- ,2- Di pheny 1 hydraz ine


•\ I • -

: ..... .....i.1 CP___' ■ _i?J;.003 245 'TCS'ÔT

i e j :___ 0-7-C4 ... ........-■;ei 'ey G-i?_-84'

So i

■ \ • ^ •270

/ 1 O lL~

1 i 0 v.C!

r -■

n ;

0.57

< "0725

T“272“

<~74

i 0.33

....0.33

0.29

-■ 0.33

i

c:i i r-roosr.z i ui no

r.Uro toluene

r,'! ■ ‘7

< 0.21

•• 0_. 33

■- 0.33

_'2.3

0.74

• 0.7-3

0.55

■ 0.09

■; 0.25• clff

07l2~

■: o’. 33*

ToTl"

0'.25"

•" o'. 74”

.. -------

?■ i ■i \ -

1 1

: c-s'.y 1 -;,nony 1 e

O-jA^ch lorrc-tncr.o

Kt-vocii 1 orODutad i ene

hexach1orocyc1 open ta diene

Oc: p.’i t.-'ici 1 ene

2-Cr. 1 c ro n e p th a 1 e n e

1 .2-pi er-eny 1 hydrae i ne

1 Ft. the late

u

ICO

tEMi - vula: ;le organ!( anal/sis 1

DATA SHEET

Date Sampled : 6-7-84

Date1 Recei ved by Lab : 6-12-84

Date E/t racted/Prepa red : 6-20-84


Client: hDK

Sample I.D.:__0_j -001145 (70. Ml

Sample Matrix: Soil


< 0.33

< 0.98

< 0.2 7

< 0.30

< 0.36

< 0.94

< 2,4

<0.36

< 0.24

< 4.2

< 0.19

< 0.35

<4.4

< 0.25

< 0,22

< 0.54

< 0.19

< 0.78

< 0.25

< 0.19

< 0.22

< 0.25

< 0.25

< 0.19

Phenol

mg/t.q .

Inaeno (l,2,3-c,d1 pyr. ..2-Ch1orophenol U . h i Benzo (g,h,i) perylene

2 ,4-Dich1orophenol

2 .4 ,5-Trich1orophenol

'• 0.25 Benzo (a) Pyrene

4-Chloro-3-methyl phenol (p-chloro-m-cresol)

Pe.ntachlorophenol


2-methyl-4,6-dinitrophenol•(4,6-dinitro-o-cresol)

2-Nit rophenol

4-fli t rophenol

2 ,4-Dinitrophenol

Acer, apt here

Acenaphthylene

Benzidine

Ch rysene

Isophorcne

Phenanthrene

Anth racene



Eluorene “

Elucranthene



Py re n e

ene

SEMI-VOLATILE ORGANIC ARAL/S 13

DATA SHEET '

Clienr : HOP

Samp 1e I.D.: 01-001H5 (TC8 ^4)

Sample Matrix: ôil

Method f,'o. : EPA 82 70

„ Date Sampled: f-7-8*1

_ Date Received by Lao: 6-12-84

Date Extracted/Prepared: 6-20-P4

Date Analyzed: /_ i -p _ 04

mg/Kg

0.19

0.19

< 0.19

< 0.19

0.19

1. 7

0.57

0.25

0.2!

0.19

0.25

< ?

0. 16

0.3

0.25

60. D /

0.5 7

0.42

0.5:

0.19

4l9/££_

0. 16

__ Hexacn1orobenzene

__ nitrobenzene

__1 >2-Dichlorobenzene

__ 1 .3-Dichlorobenzene

__ I >4-Dichlorobenzene

_ 1>2.4-Trichlorobenzene

_ 3,3-Dich1orobenzidine

_ 2,4-Dinitrotoluene

_2 ,6-= Di n i t rot01 uene

_ N-Nitrosodimethylamine

__ N-Nit rosodiphenyl amine

- n-Nit rosodi-n-propyl amine

_ Diethyl Phthalate

_ Dimethyl Phthalate

_ Di-n-butyl Phthalate

_ Butyl benzylphathalate

. Bis (2-et.hylhexyl) phthalate

- 2is (2-chlorcethyl) ether

.. Bis (2 - ch 10 roi s op ropy 1) ether

- ‘’“Ch 1 orophenyl-phenyl ether

Bis (2-chloroethoxyJ methane

4-8romophenyl-phenyl ether

Hexachloroethane

0.25

0.19

0.57

0.25

_____ Hexach1orobutadiene

_ Hexachl crocyclopentadi e.n

_ Rapthalene

_ 2-Ch lorcnapthalene

1 >-^ - Di pheny 1 hydraz ine

_ Di-n-Octyl Phthalate

-4 5-

SEMI-VOLATILE ORGAN TO ANAL

DATA SHEET

Client:____ HDk

Sample I.D.: Ol-OQl]45 (TC8

Sample Matrix: SoilMethod No. :____ EPA 87to~ "





__ mg/Kg

- 0.80

< 0,33

< 0.95

< 0.27

<0.30

<0.36

< 0.94

< 2.4

<0.36

_< 0.24

<4,2

< 0.19

Phenol

2-Chlorophenol

2 ,4- Di ch 1 orophenol

2 .4 ,6-Trichlorophenol

mg/Kg

1_0_._37

< 0.41

*= 0.25

I n de n o v 1 , 2 , o- c, d) Pv re ne


Benzo (a) Pyrene

4- Ch loro- 3-methyl phenol (p-chloro-rn-cresol)

Pentach1orophenol


2-methyl-4,6-dinitrophenol (4 ,6-dinitro-o-cresol)

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol

Acenapthene< 0.35

< 4.4

< 0.25

< 0.22

< 0.54

< 0,19

< 0. 78

< 0.19

_< 0.22

< 0.25

< 0.25

<0.19

Acenaphthylene

Benzidine

Ch rysene

Isophorone

Pherianthrene

Anthracene


Dibenzo (a,n) anthracene

FIuorene

FIuoranthene



Pyrene

u

Date Sampled:____ ___6-7-8h

Date Received by Lab:__ 6-12-84



'.•CM!- VOLATILE 0;-:G/Y,!C ANAL/SIS

DATA SHEET

Client:HDD

Sample I. D. : 01-001 146 1TC8 •-•■ft :■

Sample Matrix:____ Soil

Method Do.: spa g?70

o. IVI Q

0.19

C. 19

0.19

< 0.44

0.19

1.7

0.57

< 0.25

< 0.25

< 0.19

0.25

<2.2

0. 16

< 0.25

0.57

< 0.57

0.42

0.53

0.19

0.16

0.09

He/.acn ;ore-benzene

Nitrobenzene

i >2- Di ch 1 oI'obenzene

1.3- Dichlorobenzene


1.2.4- Trichlorobenzene

3.3- Dichlorobenzidine

2.4- Dinitrotoluene

2,6-Dinitrotoluene

N-Nit ros odimethyl amine

N-Ditrosodiphenyl amine

H-Di trosodi-r.-propyl amine

Diethyl Phthalate

Dimethyl Phthalate

Di-n-butyi Phthalate

Q--5_____ Butylbenzylphatnal ate

. Bis (2-ethylhexyl) phthalate

Bis (2-chloroethyl) ether

Bis (2-chloroisopropyl) ether

4-Chlorophenyl-phenyl ether


4-Bromcphenyl-phenyl ether

Hexachloroethane

Hexach1orebutadiene

0.25

0.16

0.19

< 0.57

< 0.25

Hexachlorocyclopentad

Napthalene

2 - Ch 1 o ron a pt h a 1 e ne

1;2-Dipheny1hydrazine


i ene

DATA SHEET

Cl i eat :

Sample I.O.:

Sample Matri

Method Mo. :

HDR Date Sampled:.in-001145 trc« »«. Date

fa-.

So i 1

EPA 8270Date Extracted/Prepared: fa

Date Analyzed: 7 _ t v _ c ■

-fi

__ iHfaila.

.■ 0 00'J . O'-

-■ 0.33

< C. 58

< 0.27

<0.30

< 0.36

< 0.94

< 2.4

<0.36

< 0.24

< 0,19

< 0. 35

<4.4

Phenol

2-Ch1oropheno1

2,4-Dich1orophenol

2 ,4 ,6-Trichlorophenol

mg/Kg

'■ 0.37

'• 0.4 1

< 0.25

Indeno (1 ,2,3-c.d} Pyr

Benzo (g,h,i; perylene

Benzo [&j Pvr£n&

4-Chloro-3-methyl phenol (p-chloro-m-cresol)

Pentach1oropheno1


2-methyl-4,6-di„itrophenol (4,6-di„itro-o-cresol)

2-Nitrophenol

4-Nitrophenol

2 ,4-Dinitrophenol

Acenapthene

Acenaphthylene

Benzidine< 0.25

< 0.22

•- 0.54

_y 0.19

< 0.78

< 0.25

< 0.19

< 0.22

< 0.25

•• 0.25

< 0.19

Ch rysene

Isophorone

Phenantn re:ie

Anthracene


Di benzo (a,h) anthracene

FI uorene

FI uoranthene



Pyrene

u

Client:---------------- H5.l'Date Sampled:6-7-84DUPLICATE

Sample I.D. : 0I-Q0114S (TCP, *?,) Date Received by Lab: 5-12-84

Sample Matrix:So i 1Date Ext racted/Prepa red : 6-20-84

Method No.:_EPA 8270 Date Analyzed: 7-12-84

SEMI-VOLATILE ORGANIC ANALYSIS ;

DATA SHEET

mq/Kq

< 0.19

< 0.19

< 0.19

< 0.19

<0.44

< 0.19

< 1.7

< 0.57

< 0,25

< 0.25

< 0.19

< 0.25

< 2.2< 0.16

< 0.25

< 0.25

2.6

< 0.57

< 0.57

<0.42

< 0.53

< 0.19

< 0.16

< 0.09

Hexach1orobenzene

Nit robenzene

1 ,2-Dichlorobenzene

1.3- Diehlorobenzene



3,3-Dichiorobenzidine

_ 2,4-Dinitrotoluene

2,6-Dinitrotoluene

N-Nitrosodimethyl amine

N-Ni trosodiphenyl amine

N-Nit rosodi-n-propy1 amine

Diethyl Phthalate

Dimethyl Phthalate


Butylbenzylphathalate

Bis (2-ethylnexyl) phthalate

Bis (2-chloroethyl) ether


4-Chloropheny1-phenyl ether


4-Bromophenyl-phenyl ether

Hexach1oroethane

Hexachlorobutadiene

mq/Kq_____

< 0-25_____ Hexachlorocyclopentadien

< 0• 16_____ Napthalene

< 0-19 2-Chloronapthalene

< 0-57_____ 1,2-Diphenylnydrazine

< Q-25____ Di-n-Octyl Phthalate

' ‘ u

TABLE 2

SERCO

1//-AS~-JV^

Sanitary Engineering Laboratories, Inc. 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBER

Monitoring Well Water Analysis

Client: Terracon Consultants, Inc.Attn: Mr. John Hartwell P.O. Box 37582 Omaha, NE 68137

Date Sampled: 10/3/84

Date Received: 10/5/84

Sample Identity: BOS Well

Analysis

Toluene <1 ug/1Xylene 2 ug/1Ethylbenzene <1 ug/1Methyl Ethyl Ketone <5 ug/1Total Organic Carbon 7 mg/1Total Organic Halogen 14 ug/1

<means less than

October 31, 1984nh 1147N#25

Prepared and Submitted by SERCO

David W. HavickSenior Chemist

SERGOSanitary Engineering Laboratories, Inc.1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone:(319) 277-2401

__________________________ _____________________________________ ________________________________________________________________ MEMBER





Sample Identity: Monitoring Well 3 #1

Analysis

TolueneXyleneEthylbenzene Methyl Ethyl Ketone Total Organic Carbon Total Organic Halogen

<1 ug/1 <1 ug/1 <1 ug/1 <5 ug/1 3 9 mg/1 28 ug/1

<means less than

October 31, 1984nh 1147N#20

Prepared and Submitted bySJ3RCO


SERCOSanitary Engineering Laboratories, Inc. 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBER






Analysis


<1 ug/1<1 ug/1<1 ug/1<5 ug/18 mg/1

25 ug/1

<means less than

October 31, 1984nh 1147N#21



SERCOSanitary Engineering Laboratories, Inc. 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone:(319) 277-2401

MEMBER





Sample Identity: Monitoring We11 3 #3

Analysis

Toluene <1 ug/1Xylene <1 ug/1Ethylbenzene <1 ug/1Methyl Ethyl Ketone 5.4 ug/1Total Organic Carbon 44 mg/1Total Organic Halogen 24 ug/1

<means less than

October 31, 1984 nh 1147N #22


David W. Havick Senior Chemist

ii


MEMBER






Analysis


< means less than

< 1 ug/1< 1 ug/1< 1 ug/1< 5 ug/145 mg/1

340 ug/1

October 31, 1984bh 1147N#17



A----- 7

Jt&££fc&d

SERCOSanitary Engineering Laboratories, Inc. 1922 Main Street, P.0. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBER






Analysis


<1 ug/1 <1 ug/1 <1 ug/1 <5 ug/1 14 mg/1 55 ug/1

<means less than


October 31, 1984nh 1147N#18


SERCOSanitary Engineering Laboratories, Inc 1922 Main Street, P.O. Box 625 Cedar Falls. Iowa 50613 Phone: (319) 277-2401

relied

//-/S- fa S-L- I


Client: Terracon Consultants, Inc. Attn: Mr. John Hartwell P.O. Box 37582 Omaha, NE 68137




Analysis

TolueneXylene <1 ug/1Ethylbenzene <1 ug/1Methyl Ethyl Ketone <1 ug/1Total Organic Carbon 6.4 ug/1Total Organic Halogen 27

39mg/1ug/1

<means less than

Prepared and Submitted bySERCO

October 31, 1984 1147N

#19


SERCO?nooa/y En9meering Laboratories, Inc. 1922 Mam Street, P.0, Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBCR


Client: Terracon Consultants, Inc. Attn: Mr. John HartwellP.O. Box 37582 Omaha, NE 68137



Sample Identity: TC1D

Analysis

TolueneXylene 4,900 ug/1Ethylbenzene 34,000 ug/1Methyl Ethyl Ketone 9,100 ug/1Total Organic Carbon 9,300 ug/1Total Organic Halogen 92 mg/1

46 ug/1

Prepared and Submitted bvSERCO

Octobernh#26

31, 1984 1147N


SERCOSanitary Engineering Laboratories Inc 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

n-tx-S4*t~

MEMBER






Analysis


3,000 ug/18,200 ug/12,400 ug/1

700 ug/16 8 mg/189 ug/1

October 31, 1984 nh 1147N #27

Prepared and Submitted SERCO

David W. Havick Senior Chemist

by

u


MEMBER





Sample Identity: TC3

Analysis


13.000 ug/147.000 ug/114.000 ug/11,400 ug/1

26 mg/1250 ug/1


October 31, 1984nh 1147N#28


’• V .7 :• <l«-sccJiui Vjtiaiit.V fc; -jv t

Ulz'A'-tL^ iSERCO

Sanilary Engineering Laboratories Inc 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401______________________________________________________________________________ __MEMB6H






Analysis


16.000 ug/159.000 ug/115.000 ug/1

890 ug/170 mg/1

110 ug/1

October 31, 1984nh 1147N#29


COxsZ-^J


IkLS.-WS't- I

SERGOSanitary Engineering Laboratories, Inc. 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBER

Monitoring Well Mater Analysis





Analysis


\20 ug/183 ug/123 ug/123 ug/18 mg/1

47 ug/1

October 31, 1984nh 1147N#30

Prepared and Submitted ERCO


by

SERCO?noo . / En9'neering Laboratories. Inc 1922 Mam Street, P.0. Box 625 Cedar Falls, Iowa 50613 Phone:(319) 277-2401



Date Sampled: - - -


Sample Identity: TC6S

Analysis


3.4 ug/115 ug/14.0 ug/1

1-9 ug/122 mg/110 ug/1

October 31, 1984nh 1147N#32

P^^PS-^sd and Submitted bySERCO


SERGOSanitary Engineering Laboratories, Inc 1922 Main Street. P.O. Box 625 Cedar Falls, Iowa 50613 Phone:(319) 277-2401

//-/5 j

MEMBER



Date Sampled: - - -



Analysis


3,700 ug/139,000 ug/1

2. 4 ug/1110 ug/12 7 mg/1

170 ug/1

October 31, 1984nh 1147N#31


J


! H-/S

SERCO—j

Sanitary Engineering Laboratories, Inc. 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBER



Date Sampled: - - -



Analysis

-TolueneXyleneEthylbenzene Methyl Ethyl Ketone Total Organic Carbon Total Organic Halogen

22 ug/1320 ug/116 ug/115 ug/15 7 mg/1HO ug/1


October 31, 1984nh 1147N#33




('A A* »

1 ■V'VV'-'V-■ u..______________

J-QrcOS

•Ai


Date Sampled: - - -


Sample Identity: TC8 Dup.

Analysis

Tpluene 4,900 ug/1Xylene 30,000 ug/1Ethylbenzene 8,300 ug/1Methyl Ethyl Ketone <5 ug/1Total Organic Carbon 38 mg/1Total Organic Halogen 91 ug/1

<means less than



October 31, 1984nh 1147N#34

SERCO

Sanitary Engineering Laboratories, Inc,1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone:(319) 277-2401——____________ _____ _____________________________________________________________________________________ MEMBER


Client: Terracon Consultants, Inc. ciAttn: Mr. John Hartwell 1P.O. Box 37582 Omaha, NE 68137

Date Sampled: - - -


Sample Identity: None Given

Analysis


300 ug/15,300 ug/11,700 ug/13,800 ug/1

101 mg/116 ug/1


October 31, 1984nh 1147N#35


SERCOSanitary Engineering Laboratories Inc 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone:(319) 277-2401

MEMBER



Date Sampled: - - -



Analysis


4.1 ug/194 ug/15.3 ug/1

450 ug/12 9 mg/177 ug/1

October 31, 1984nh 1147N#36

Prepared and Submitted SERCO

by


SERCOSanitary Engineering Laboratories Inc 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

—_______________ _______________ ______ ________________________._______________ _____ _________________________________________________________ ________________________________________ MEMBER



Date Sampled: - - -



Analysis


1.5 ug/115 ug/11.0 ug/1

12 ug/129 mg/1

110 ug/1


October 31, 1984nh 114 7N#37


SERCOSa™tafy Engineering Laboratories, Inc 1922 Main Street, P.0. Box 625Cedar Falls, Iowa 50613 Phone: (319) 277-2401



Date Sampled: - - -



Analysis


<means less than

<1 ug/1<1 ug/i<1 ug/l9.7 ug/1

11 mg/152 ug/1

October 31, 1984nh 1147N#38


<%Zcs2.jZiJ*


SERCOSanitary Engineering Laboratories. Inc 1922 Main Street. P.O. Box 625 Cedar Falls. Iowa 50613 Phone:(319) 277T2401

Monitoring Well Mater Analysis


Date Sampled: - - -



Analysis

TolueneXyleneEthylbenzene Methyl Ethyl Ketone Total•Organic Carbon Total Organic Halogen

1,100 ug/111,000 ug/1

620 ug/11,100 ug/1

6 7 mg/181 ug/1

October 31, 1984nh 1147N#39



II

SERCO?ooota// .En9'neering Laboratories, Inc 1922 Main Street, P.O. Box 625Cedar Falls, Iowa 50613 Phone: (319) 277-2401



Date Sampled: - - -


Sample Identity: TC14A Deep

Analysis


1,100 ug/134.000 ug/112.000 ug/118.000 ug/1

126 mg/1

120 ug/1

Octobernh#40

31, 1984 1147N

Prepared and Submitted bv SERCO *


SERCOEn9ineering Laboratories, Inc.

1922 Mam Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

UJz/S:/i/>4___ j

Well Water Analysis

Client: Terracon Consultants, Inc. Attn: Mr. John HartwellP.O. Box 37582 Omaha, NE 68137

Date Sampled: - - -



Analysis


10.000 ug/163.000 ug/113.000 ug/11,800 ug/1

3 6 mg/19 ug/1

October 31, 1984nh 1147N#41



SERGOSanitary Engineering Laboratories, Inc 1922 Main Street. P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBER



Date Sampled: - - -



Analysis


11.000 ug/152.000 ug/114.000 ug/14,300 ug/1

98 mg/1340 ug/1


October 31, 1984nh 1147N#42


SERCOSanitary Engineering Laboratories, Inc 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMOIR



Date Sampled: - - -



Analysis


2.9 ug/119 ug/12.8 ug/1

89 ug/1396 mg/118 ug/1


October 31, 1984nh 1147N#44


Sanitary Engineering Laboratories, Inc. 1922 Main Street, P.O. Box 625 Cedar Falls, Iowa 50613 Phone:(319)277-2401

SERCO

MEMBER



Date Sampled: - - -



Analysis

: Toluene XyleneEthylbenzene

' Methyl Ethyl Ketone Total Organic Carbon Total Organic Halogen

6.200 ug/120,000 ug/17.200 ug/1

550 ug/14 4 mg/186 ug/1


October 31, 1984nh 1147N#43


SERCOSanitary Engineering Laboratories, Inc. 1922 Main Street, P.O. Box 625 Cedar Falls. Iowa 50613 Phone: (319) 277-2401

MEMBER



Date Sampled: - - -



Analysis

Toluene 1.7 ug/1Xylene 11 ug/1Ethylbenzene 1 ug/1Methyl Ethyl Ketone •15 ug/1Total Organic Carbon 6 mg/1Total Organic Halogen 9 ug/1


October 31, 1984nh 1147N#45


iff-l‘\ .... . l-'gHii'Sv'S

! MS-14 M-


MEMBER






Analysis


<1 ug/1<1 ug/1<1 ug/1<5 ug/1

258 mg/163 ug/1

<means less than


October 31, 1984nh 1147N#24


SERCO

•eceBYfeC;

IHS-N >L-

Sanitary Engineering Laboratories, Inc. 1922 Main Street, P.0. Box 625 Cedar Falls, Iowa 50613 Phone: (319) 277-2401

MEMBER






Analysis


<1 ug/1<1 ug/1<1 ug/17.4 ug/1

5 0 mg/110 ug/1

<means less than


October 31, 1984 David W. Havicknh 1147N Senior Chemist#23

TABLE 3

1

VOLATILE ORGANIC ANALYSIS {VOA) DATA SUMMARY

Client: Diamond Vogel Phase II

Sample Matrix: Mater


Sample I. D. : 01-001536 HI (TC8D)


Date Received by.Lab: 10-4-84Date Analyzed: 10-8-84

uq/L

< 5.0

< 5.0< 2.2

< 3.1

417< 4.7< 1.6

< 2.8

< 5,0

< 5.0

< 2.8

< 2.8

< 3,8

< 5.0

< 6.9

< 5.0< 2.8

< 1.612,7

< 4.1

< 5.0

68.2< 5.0

< 5.0

Bromomethane

Chloromethane

BromodichloromethaneDibromochloromethane

Methylene Chloride

BromoformCh loro form


Tri chlorofl uoromethane

Chloroethane

1,1 -Di chloroethane

1,2-Di chloroethane

1.1,1-Tri chloroethane

1,1 ,2-Trichloroethane

1,1,2 ,2-Tetrachloroethane

Vinyl Chloride

1 »l-Dichloroethene

Trans-1,2-Di chloroethene

Trichloroethene

Tetrachloroethene

2-Chi oroethyl vinyl ether 1,2-Di chloropropane

CIS - 1,3-Di ch 1 oropropene

Trans-1 ,3-Dichloropropene

ug/L

— 108.8 < 6.0

< 6.0

< 7,2

< 5.0< 5,0

3484

280

620

Benzene

Chlorobenzene

Toluene

Ethylbenzene

Ac ro1ein

Acrylonitrile

Methyl Ethyl Ketone

Acetone

4-Methyl -2-Pentanone

2

VOLATILE ORGANIC ANALYSIS (VGA)

DATA SUMMARY

Client: Diamond Vogel Phase II

Sample Matrix: Water


Sample I.D.: 01-001536 (#2 Trip Blank)


Date Received by Lab: 10-4-84Date Analyzed:_____ 10-8-84

uq/L

< 5.0

< 5,0

< 2.2

< 3.1< 2.8

< 4.7< 1,6

< 2.8

< 5.0

< 5.0< 2,8

< 2.8

< 3,8

< 5,0

< 6.9< 5,0< 2.8

< 1.6

< 1.9

<4,1< 5.0< 6.0

< 5,0

< 5.0

ug/L

Bromomethane <4.4

Chloromethane < 6.0

Bromodichloromethane < 6.0

Dibromochloromethane < 7.2

Methylene Chloride < 5.0

Bromoform <5.0 Chloroform <10 0

Carbon Tetrachloride <10.0Tri chlorofl uoromethane

Chloroethane

1 ,1 -Dichloroethane

1,2-Oichloroethane

1.1.1- Trichloroethane-


1,1,2,2 - Tet rach lo roe thane

Vinyl Chloride

1.1- Di chloroethene

Trans-1,2-Di chloroethene

Trichloroethene

Tetrachloroethene 2-Chloroethyl vinyl ether

1.2- Di ch 1 oropropaneCIS - 1,3-Dichloropropene


Benzene

Chlorobenzene

Toluene

Ethylbenzene

Acrolein

Aery Ion i tri le

Methyl Ethyl Ketone

Acetone

3

Organic Analysis Data S.'ieot

Client: Diamond VogelSample 01-ddr536 (TC8D)"Date Sampled:""" TG^Z^&T ~ Date Received by Lat>: HPFOT

Sample Matrix.: Water_ * 1Date ExtracteC'/Treoared: rd-S-84Method No:_ _EPA 625Date Analysed: IO"-nPB4

ie one;11 or ..g/Kg

Semi-Volatile Compounds

Hexachlorobenzene

Nitrobenzene

l • 2-Pichlorobenzene

i ,3-Dichiorobenzene< 4.7

< 2.0

<17.5

< 6.0

< 2,7

< 2.7

< 2.0

< 2.7

<23.3

< 1.7

< 2,7< 2.7

< 2.7

< 6.0

< 6.0

< 4.5

< 5.6

< 2,0

< 1.7< 1.0

< 2.7

< 1.7

< 2.0 < 6.0

< 2.7



3.3- Dichlorobenzidine2.4- Dinitrotoluene

2,6-Di ni trotol uene

N-Ni trosodimethyl amine N-Nitrosodiphenylamine

N-Ni trosodi - n-propyl ami ne Diethyl Phthalate Dimethyl Phthalate

Di-n-butyl Phthalate Butyl benzyl phthalateBis (2-ethylhexyl) phthalate Bis (2-chloroethyl) ether


4-Chlorophenyl-phenyl ether Bis (2-cnloroethoxy) methane 4-Bromophenyl-phenyl ether

Hexachloroethane Hexach1orobutadiene

Hexach1orocycl opentadiene

Naphthalene2-Chloronapthalene1 ,2-Diphenylhydrazine


U

■■r r.ir, i c Ana h; i s ; ■. -hr oet

c 1 i en t:__Pjaiiiorid Voqe 1-3ir4’le I ■ 0 • „JLL-P0_1536'TfC80jL);:te ?a;--p > ed10-2-84 ~

received Dv'Lc-l)':

^Circle one) (tVUor ■. g, Ka

__ijjj____

< 3.5

__ <10.4___ _

<2.9

3.2

3.8

54.5

<25.4

< 3.8

< 2.5

<44.5< 2.0

..10_-4_-8j

-Volatile Compoun:s

5ai!ip I e \-\b trix :____Wateri-'ute ox traded / Preoared:Method ho:__ EPA_625____"Da * e A n a i y: :i:__ lp -14 - 84~

Phenol

2-Cr, lcrop.henol

-d ch 1 Gi'cphenol2

7 a e_-

• ul. : L.ny ; pfi&no | p-z

Pen tecr. 1 orophenol

2 ,4-~ir.ethylphencl

2- me thy 1 - 4 ,6-cinitrophenol (■

2-fii trophenol

4-Ni trophenol

2,4-Dimtrophenol

Aoeraerihene

a; ol;

■oinitrc-o-c res

< 3.7

<46.6< 2.7

< 2,3

< 5.7< 2,0

< 8.3

< 2.7

< 2.0

< 2.3

< 2.7 2. 7~

<2-0

< 3-9

< 4-3

2.7

Aten;on thy lore

Benzidine

Chrysene

Isophorone

Phenanth rone

Anthracene

Beneo (a) anthracene

Dibento (a,h) anthracene

FI uorc-ne

Fluoranthene


Bento (k) fluoranthene

Pyrene

Indeno (1,2,3-c.d) pyrene


Bento (a) Pyrene

-io.ta.-a4

5


Client.: _ Diamond Vogel __ ___ _Simple !. D.__ 01-001536~ (TC8D)Dace Sampled: 10-2-84Date Received by Labi ~TqP~4-84

Semple Mi t ri >::___ Water_______Date- Extracted, Prepared: 10-8-E'eshod No:EPA 625________ ___._2Cate Analyzed:^Q-14-84_ "

Semi-Volatile Compounds

C_ Recovery

50.4

4_7_._7

53.3

67.2

46.7

57.6

44.7

Kexachlorobenzene

Mitrobenzene

1.2- Dichlorcbenzene

1 , 3-Di chlorobenzene

1 ,4- Si ch 1 orobenzene

1 ,2,4-Trichlorobenzene

3.3- Dichlorobenzidine2.4- Dinitrotoluene

2.5- Dini trctcl uene

M trosodimethyl ami ne

N-Ni trosodiphenyl amine

N-N i: res odi-r-propyl amine

Diethyl Phthalate

Dimitry] Phthalate


Eutylbenzylpr.thalate

Bis (2-ethy 1 hexyl) phthalate

Eis (2-cnloroethyl) ether


4 - C h 1 o ro ph e ny T - ph eny 1 e th e r

Eis (2-ciiloroethoxy) methane

4-3romophenyl-phenyl ether

Hexachloroethane

Hexach1orobutadiene

Hexachl orocycl open tadi ene

Naphthalene

2-Chloronapthalene

1 >2-Diphenylhydrazine


_ SPIKE84

0

Organic Analys is Da ta Sheet

Client:__Diamond Vogel_____ ___ Sample Matrix: Mater_ ___Sample l.D. 01-001536 (TC8D)__ Date Extracted /PreparedflO-TaTCate Sampled:__10-2-84________ Method Mo: __EPA 625 ____Sate Received oy Lab:___10-4jc84_ Date Analyzed:10-14-84

Sc-rri -Volatile Compounds

Recovery

12.8

66.3

57.6

58.2

58.3

Phenol

2-Chlorophenol

2.4- Di chi orophenol

2,4 ,6-Tri chi orophenol

4-Chloro-3-methylphenol (p-chl oro-m-cresol)

Pen tacnl orophenol

2.4- Dime thyl phenol

2-ir.ethy 1 - 4,6-dini trqphenol (4 ,6-dini tro-o-cresol)

2-Mitrophenol

4-Mitrophenol

2.4- Dinitrophenol

Acer.aph there

Acenaphthylene

Benzidine

Chrysene

lsophorone

Phenanthrene

Anth racene



FI uorene

FI uoranthene



Pyrene

Indeno (1,2,3-c.d) Pyrene


Benzo (a) Pyrene

SPIKE

APPENDIX E

CUSTODY DOCUMENTS

Technologies, Inc

i.d. 01-001145

November 27, 1984received

HDS8404 Indian Hills Drive 0:naha, fit 68114

Attention: Mike Harris

FILE COPYDiamond Vogel, Project No. 884706

fUt "“If'?1 technologies, Inc. received a total of here ieiied'S ““««<«». •«* ™ selected soils

- thirteen (13) selected priority pollutant metals priority pollutant volatile organicspriority pollutant base/neutral and acid organics

- chlorinated pesticides y

The results are listed in the attached tables.

Attachments

u

AnalylicalTechnoIogies Jnc.Corpoiulo Olllcos: 1Corpoiulo Olllcos:225 W. 30lh Sliool Notional City. CA 92050 619-4//-41/3

PROJECT NO.RmT-o G

I SAMPLERS: (Signature)

"project NAME

TMarv>.eY\^ V0o>c\

0Xcrv**7(

STATIONNUMBER DATE TIME STATION LOCATION

Rom ^1fL •j.j-s.o'

Rcm H2-%N»\ A.m.

A.vh.

A.nV

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$b/v\

Vim

& w** -irJ ^*(

- XoTGM, Him fi.V*.

kcM ^SZlM A.w

KcmSJiM

>)}&(

A-»^ *P n ÎlCH **5

■*«•£-no* -

1385 iji/

RECEIVED BY; ISignsiu^l

nEL OUlSMLi; BY: tSig'»lu>rl . DAT E/TIME RECEIVED IIY: (Sign.iimc)

(METHOD OF SHIPMENT:SHIPPED OY: (S»g'»8lu»r)

Gen

era!

Inor

gani

c

i i

Chain of Custody Record

*4

SAMPLE TYPES OTHER

U.£o*^ IU CC 7* LU — CD2 tis

REMARKS

r.•v

\z"I—

QJ(An0*6

rfj

o

o*ucTO>u

8cTO»7>6

ycTOu>Oc

yoto

vsOETOo>6

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k

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TOT OF C

A I. NUMBER ONTAINERS

/£^»HI

REL'NOUISHED BY: ISiBnalu.el

RtLIMOUI5IIED BY: isiynmuirf

COURIER: (SiBn.-ituf e)

DATE/TIME

oaie/iime

RECEIVED BY: ISignsiurrl

RECEIVED BY: lsiBni>tu.«l

DAir/riMF

^ 1

(

AnalylicalTechnoiogiesJnc.

Coipoialo Olllcos:' Coipoialo Olllcos:

225 W. 3fllh Sltool Nollonal City. CA 92050619-477-4173

PROJECT NO

pZ'-j-y.ocI SAMPLERS: (Signature)

PROJECT NAME

Dl'cr^^nJ) VOae.)

Chain of Custody Record

SAMPLE TYPES OTHER

STATIONNUMBER DATE

17~TIME STATION LOCATION

TCc £J$/z P.A

1 Tc 6 2- '/r/B*! €>•0-9*3"TC 6 -**3 “Zr/gy 13.-I4-.5" ^

TCC #>.W.|t£* *s <

ZfVgy P./VT. 2 3-24.iT ÎtC£ ^4

Am, 2g-lM.c; <

Tc<f *"7 s/r/fl* -£^Ll 33-?^.r

miTC ^ **3 2£7^ 43-44.T ^

TCfi f/6lTM ti m j/j:

fijkrrorTT

4s-4U^T ^

nCUNbUISHED UY:(SignilLrii

I ME rIIOD OF SHIPMENT:

- uctou«oc

*? V,^ TOC •" *u CJe> :>

10c«JDz

0)n«»a6

a>*o'cIQ>u O

rgan

ics

UctoC71Octo*o

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tile

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anic

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OJDU_ 6

<UCa;Uis.X"*5

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U.£O^T.WLUn:r.UJ —m < ? I-*8

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4A 1 \

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4

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£< *si

•*{'Kt

/fa' ||TOTAL NUMnrn

wm&sm

REUNOUISHED BY- icirOF C ONTAINE RS lo

OATE/TIME ITECEIVEO UY; ISignntine) HEUNUUISIIED BY: ISigna^clOATE/TIME

SHIPPED UY: (Signahirr) poicoumcn: (Signature)

REMARKS

RECEIVED BY; (Signature!

uatehime

c//>A / /*/

(

AnalyticalTechnologies,lnc Cotpcroto Oliices, ?t'5 W 30m Siseei Nanono: City. CA 9;.,Q60 619 477-41

I.D. 01-001536

H D R8404 Indian Hills Drive Omaha, NE 68114

November 27, 1984

file copyProject Number: 884719 -Diamond Vogel Phase II


On October 4, 1984 Analytical Technologies, Inc. received one (1) water sample for analysis of volatile organics (EPA Method 624), and base/neutral/acids (EPA Method 625). Samples were taken on October 2, 1984, iced immediately, and shipped on October 3, 1984. Only station TC8D was sampled, the other station was dry (from note on chain of custody record).

Attached are the test results.

ML:mat

Attachments

NOTE: Samples from this project will be disposed of in thirty (30)days from the date of this report, unless we are informed otherwise.

ReviewedTechnical Associate

U

(

J^.AndyjicolTechnologiesJnc Cc'CO»a:e OKices 225 W 30rn Sweet Notional City. CA 92050 619 47

I.D.tf 23-70302

t

Moveniber 28, 1984

HDR8404 Indian Hills Drive Omaha, HE 68114


FILE COPY

RE: Diamond Vogel

On September 1, 1984 Analytical Technologies, Inc., Tempe, AZ received 45 soils from the Diamond Vogel site; the samples were archived in cold storage. On October’ll, 1SS4 Mr. Mike Harris

requested that the soils be shipped to the ATI National City, CA laboratory for analysis of volatile organics by GC/M5. The analyses were done according to EPA Method 8240 using direct sparge (where possible) in order to attain the lowest possible limits of detection for GC/MS.

The results are listed in the attached tables. If there are any questions please call (619) 477-4173.

M.</br

Enclosures

NOTE: Samples from this project will be disposed of in thirty (30)days from the date of this report, unless we are informed otherwise.

HU D LNGINELKING AND TLSTING U.IAK IA1.I.S l. l.DAK KAI'IUS DA VI NI'IJK'I DLS MOINES. IOWA

Kansas city wiciiita. KansasOKLAHOMA CITY TULSA, OKLAHOMA

23

070302

Location of Sampling:

Collector's Sample ~C \6 A I

~C \6TC1 \AZL£__£_iL4_

CHAIN OF CUSTODY RECORD

Producer Hauler _Disposal Site

.Other; ^\q ,w, \ - ■/ ; , Sample: "

Shipper Name: //7^> A—

Address: .... (7'lie 2>r /La,/..NumberStreet-------

Collector's Name: ,/Signature

Ci ty State Zip Code

Telephone: 3 3d '

Date Sampled /g ^___ Time Sampled

Type of Process Producing Wastehours

Field Information ,S : ■ <>/,■ , ,____Lee 7 < c:e^~

t-£' > (■— V* I t uv ;■ • —l

nAND ItMiNu

*NC analysis and reports

CONSTRUCTION SERVICES

MELD ENGINEERING AND TESTING

TERRACON CONSULTANTS, INC.CEDAR FALLS CEDAR RAPIDS DAVENPORT DES MOINES. IOWA

KANSAS CITY WICHITA. KANSAS OKLAHOMA CITY TULSA. OKLAHOMA j

“L

Collector's Sample Set MiU.j

CHAIN OF CUSTODY RECORD

Location of Sampling: Producer Hauler Disposal Site

-Other: Sol (__Sample /

Shipper Name: £VD }2-

Address: $4o4 fMh Ds Aje? fcg K4-Number Street . City State Zip'Code

Collector's Name: /^4xsL Telephone:

Signature V(H^) &tQ

Date Sampled BUzju- g/?*l ^ Time Sampled_hours

Type of Process Producing Waste So,7 'br.lLy /Wy;

Field Information^ ^ ^ /V W//

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OATE TIME REASON FOR CHANCE OF CUSTOOY

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DATE TIME REASON FOR CHANCE OF CUSTOOY

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DATE TIME REASON FOR CHANCE OF CUSTOOY

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OATE TIME 'reason for chance of custody

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APPENDIX F

DRAWINGS

SEE ATTACHED PLAN SET

APPENDIX G

MODELING RESULTS

Figure #1Appendix G

9 Wells Creating Initial Condition

2000

1500

1000

500

OolO

ooo

ooto

oooC\1

|Set-Up Creating Initial Groundwater Piezometric Surface Geohydrological Report Phase II

iRiamqnd Voqel Paint IMaunce. Iowa ____________

Terracon Consultants, Inc. .Cedar Falla Cedar Rapida Davenport Dee Moines, IA I

Kansas City Wichita, KS Oklahoma City Tulsa, OK

RRT |As showji Feb/ ‘8S| 884719

February 28, 1985Table #1 Appendix G Page 1 of 2 TCI Job #884719

Remedial Investigation, Phase II Diamond Vogel Paints

Maurice, IowaModeling Sink/Source Coordinate Listing

Well No. X-Coordinate Y-Coordinate

1 6002 6003 5004 4505 900Z 1850Z‘ 200Z" 1450Y 1900Y' 50Y" 1600X 1850X' 0X'* 1650P 900P' 800P" 5200 800O' 7500" 500N 750N* 650N" 550R 1000R' 175R" 975S 1100S 1 150

1000120014001600650

12500

23001400

022251550

1502075

900800

19501000975

18501100100017001500875

15501500

775

u

February 28, 1985 Table #1 Appendix G Page 2 of 2 TCI Job #884719

Well No. X-Coordinate Y-Coordinate

S“TT'T“UU'U“VV'V"WWW"AA'A"BB‘B“CC'C"DD'D“EE1E“

11751200

12511501300

10012251400

7513001500

5013801525200

12701400300

11201300

31010601200290

10101070270950

16001500675

16751500600

17401500500

18001500400

18501340325

20251260440

20001280520

19501350650

18251390

7801700

U

©©©

Pumping Well Injection Well

Pumping Image Well Recharqe Image Well

Wells creating initial condition

Figure #3Appendix G

2000

1000

1000

500

Ql©Y"

©X‘

Oom

ooo

oo

oooCM

Dption A Well Set-Up Seohydrological Report Phase II Diamond Vogel Paint Maurice, Iowa

Terracon Consultants, Inc.Cedar Falls Cedar Rapids Davenport Dea Moines, IA

Kansas City Wichita. KS Oklahoma City Tulsa, OK

RRT f\s showfi Feb/'851884719

FIGURE 'JA

APPEND 11 G

TCJ JOB *684719

EMUErr start PATE duration in dats OPTION A RECOVERY MODEL SCHEDULE6/. ns DIAMOND VOGEL PAINTS

NOTE : THE CONTAMINATION SOURCE IS ASSUMED TO CEASE

AT DAT 240 DUE TO COMPLETION OF TRENCH CLEAN UP OPERATIONS.

Figure #4

Appendix G

O Pumping WellInjection Well i

© Pumping Image Well © Recharge Image Well © Wells Creating Intial Condition

(Option B Well Set-Up (Geohydrological Report Phase II IDiamond Vogel Paint Maurice, Iowa

Terracon Consultants, Inc.C«darF*Jl* Cedar Rapids Davenport Oes Moines, IA


|As shotji Feb/'8j 884719

FIGURE *4A APPENDIX G

TCI JOB *484719

OPTION B RECOVERY MODEL SCHEDULE DIAMOND VOGEL PAINTS MAURICE. IOWA

6/1 660

: THE CONTAMINATION SOURCE IS ASSUMED TO CEASE AT DAT240 DUE T0 completion of trench clean up Orations

: INJECTION WELLS N.O & P ARE PUMPED WELLS X.T & Z ARE PUMPED AT 7 GPU. AT 5 GPU. AND

TERRACON CONSULTANTS. INC.

Figure #5Appendix G

C\J

Note: This contour map is based on an analytical groundwaterflow model and may not represent the actual groundwater flow condition at the time shown.

Note: This contour map represents the piezometric surface ofthe groundwater (Ft.) before any pumping was done.This represents the initial condition for both options A and B.

Groundwater Flow Contour Map Geohydrological Report Phase II Diamond Vogel Paint Maurice, Iowa

Terracon Consultants, Inc.CadarFalie Cedar Rapid* Davenport Dea Moines, IA

Kansas City Wichita, KS Oklahoma City Tuiaa, OK

RRT frs showji Feb/'85|884719

U

II

Figure #6Appendix 6

Active Injection Well

Active Pumping Well

• Y

Note

model and may not represent the actual groundwater contaminant condition at the time shown.

This contour map represents the position of the contaminant plume (inp.p.m. ) before any pumping has been performed for either Option A (wells A thru E,X,Y and Z) or Option B (wells tJ,0,P, and R thru W)

Contaminant Plume Contour Map Geohydrological Report Phase II Diamond Vogel Paint Maurice, Iowa

Terracon Consultants, Inc.Cadar Falla Cadar Baplda Davenport Dot Moines, IA

Kansaa City Wichita, KS Oklahoma City Tulaa, OK

As shovjn Feb/‘85| 8847~

Figure #7Appendix G

Note: This is a 3-D representation of the contaminant plume before anypumping has been performed. This figure represents the initial contaminant condition for both recovery Option A and B. This view is from the north east corner of the grid system shown in figure 6.

Note: This 3-dimensional map is based on an analytical mass transportmodel and may not represent the actual groundwater contaminant condition at the time shown.

3-Dimensional Contaminant Plume Geohydrological Report Phase II Diamond Vogel Paint Maurice, Iowa

Terracon Consultants, Inc.CadarFaiU Catfar Rapid# Davenport DoeMolnea.

Kanaaa City Wichita, KS Oklahoma City Tuiaa, OK

RRT |NTS |Feb/‘85 j 884719

IA

Figure #8Appendix 6

O Active Injection WellActive Pumping Well

Note:

Note:

This contour map is based on an analytical groundwater flow model and may not represent the actual groundwater flow condition at the time shown.

This contour map represents the peizometric surface of the groundwater (Ft.) after 90 days of pumping with well A at 35 G.P.M. and injectinq with wells X,Y, and 2 at 12, 13, and 12 G.P.M. , respectively.


Terracon Consultants, Inc.CetfarFall* Cedar Rapids Davenport Oes Moines, IA

Kiami City Wichita, KS Oklahoma City Tulaa. OK

own |Feb/‘85 884719

Figure #9Appendix 6

Note: This 3 - Dimensional map is based on an analytical groundwaterflow model and may not represent the actual groundwater flow condition at the time shown.

Note: This 3-D map represents the groundwater peizometric surface after 90 days of pumping under Option A conditions.

3-Dimensional Groundwater Flow Map Geohydrological Report Phase II Diamond Vogel Paint Maurice, Iowa

Terracon Consultants, Inc.Cadar Fall* Cadar Rapida Davanport Oaa Moirtos, tA

Kartaaa City Wichita, KS Oklahoma City Tulaa, OK

RRT |NTS |Feb/‘85 j884719

U

Figure #10Appendix G # Active Injection Well

© Active Pumping Well

the time shown.

Note: This contour map represents the piezometric surfaceof the groundwater (Ft.) after 700 days of pumping under Option A Conditions. Pumping well E has just pumped for 160 days at 35 G.P.M. and injection wells X, Y, and Z have been injecting continuously at 12, 13, and 12 G.P.M. respectively.


Terracon Consultants, Inc.Falls Cedar Rapids Davenport Dee Moines, IA


RRT /ts~Thowij Feb. 8S|884719 "

Figure #11Appendix G ti> Active Injection Well

® Active Pumping Well O Inactive Pumping Well

NOTE:

NOTE:

reDresSt0thpn^^M,ibaSed h" f analytical mass transport model and may not rep.esent the actual groundwater contaminant condition at the time shown.IfterC^n°liLrPfrepreSentS 5he P°sition of the contaminant plume (in p.p.m.)pulped fSr 60 daIsPatP3^rPM "h ?t-°n;A conc)itl'ons- P™P™q Well B has just ?„3“.or ho days at 35 GPM and injection wells X, Y, and Z have beeninjecting continuously at 12, 13, and 12 GPM, respectively.

CONTAMINANT PLUME CONTOUR MAP GEOHYDROLOGICAL REPORT PHASE II

DIAMOND VOGEL PAINT MAURICE, IOWA

Terracon Consultants, Inc.Ctidar Falls Cactar Bapld* Osvonpod Des Moines, lA

Kin*** City Wichita, KS Oklahoma City Tulsa, OK

RRT frsthnJ Feb 85 | 884719“

II

Figure #14Appendix G

NOTE: This 3-dimensional map is based on an analytical mass transport modeland may not represent the actual groundwater contaminant condition at the time shown.

NOTE: This is a 3-dimensional representation of the contaminant plume after700 days of pumping under Option-A conditions. This view is from the northeast corner of the grid system.


Terracon Consultants, Inc.Cadar Falla CadarRapida Davenport Dos Moines. IA

Kansas City Wichita, KS Oklahoma City Tulsa. OK

RRT | NTS |Feb. 85 | 884719


H Active Injection Well ® Active Pumping Well O Inactive Pumping Well

This contour map is based on an analytical mass transport model and may not represent the actual groundwater contaminant condition at the time shown.

NOTE: This contour map represents the position of the contaminant plume (in p.p.m. after 930 days of pumping under Option-A conditions. Pumping Well E has just pumped for 100 days at 35 GPM and Injection Wells X, Y, and Z have been injecting continuously at 12, 13, and 12 GPM, respectively.


Terracon Consultants, Inc.Cedar Falla Cedar Rapids Davenport Oos Moines, IA


[\s showji F*eb 8i> [ 884719

Figure #16Appendix 6

NOTE: This 3-dimensional map is based on an analytical mass transport model and maynot represent the actual groundwater contaminant condition at the time shown.

NOTE: This is a 3-dimensional representation of the contaminant plume after 930 days of pumping under Option-A conditions. This view is from the northeast corner of the grid system.


Terracon Consultants, Inc.Cedar Falla Cedar Rapids Davenport Des Moines, IA

Kansas Cily Wichita, KS Oklahoma City Tulsa, OK

RRt | NTS | Feb. 85|884719

u

® Active Injection Well

<b Active Pumping Well

Figure #17 Appendix G

NOTE: This contour map is based on an analytical groundwater flow modeland may not represent the actual groundwater flow condi.ton at the time shown.

NOTE: This contour map represents the piezometric surface of the groundwater(Ft.) after 300 days of pumping under Option-8 conditions.


Terracon Consultants, Inc.Cedar Fails Cedar Rapid* Davenport Das Moines, IA

Kansas City Wichita. KS Oklahoma City Tulsa, OK

RRT [As shovji Feb. 8$ 884719

' U


<0 Active Injection Well

® Active Pumping Well

NOTE: This contour map is based on an analytical groundwater flow model andmay not represent the actual groundwater flow condition at the time shown.

NOTE: This contour map represents the piezometric surface of the groundwater(Ft.) after 700 days of pumping under Option-B conditions.


Terracon Consultants, Inc.CadarFalia CacUf Rapid* Davanport Oes Moines, IA

Kanata City Wichita. KS Oklahoma City Tulaa, OK

RRT | As shoi|/n Feb 85j 884719

* u

Figure #20 i Appendix G

% Active Injection Well

© Active Pumping Well

• Y

NOTE:

NOTE:

This contour map is based on analytical mass transport model and may not represent the actual groundwater contaminant condtion at the time shown.

This contour map represents the position of the contaminant plume (in p.p.m.) after 330 days of pumping under Option-B conditions. Pumping wells R, S, T, U, V, AND W have been pumping continuously at 6 GPM. Injection Wells X, Y, and Z have been injecting continuously at 7 GPM and Injection Wells N, 0, and P have been injecting continuously at 5 GPM.


Terracon Consultants, Inc.Cedar Fails Cedar Rapids Davenport Des Moines, IA


RRT Showi| Feb. 85 884719

U


OPT. B 660DAYS

NOTE: This 3-dimensional map is based on an analytical mass transport modeland may not represent the actual groundwater contaminant condition at the time shown.

NOTE: This is a 3-dimensional representation of the contaminant plume after660 days of pumping under Option-B conditions. This view is from the northeast corner of the grid system.


Terracon Consultants, Inc.Cedar Falla Cedar Rapid* Davenport Dee Molnea, IA

Kaneae City Wichita, KS Oklahoma City Tulaa, OK

RRT | NTS |Feb. 85 1884719~

Figure #22Appendix G • Active Injection Well

® Active Pumping Well


NOTE:

NOTE:

This contour map is based on an analytical mass transport model and may not represent the actual groundwater contaminant condition at the time shown.

This contour map represents the position of the contaminant plume (in p.p.m.) after 660 days of pumping under Option-B conditions.


Terracon Consultants, Inc.CadarFalli Cadar Rapids Davenport Dos Moines, IA


RRT |As shovji Feb 851 884719

FIGURE 24 APPENDIX G REMEDIAL INVESTIGATION PHASE II

DIAMOND VOGEL PAINTS

MAURICE, IOWAESTIMATED RECOVERY OPERATION CONCENTRATION REMOVED VERSUS OPERATION TIME

Geohydrological Report, Phase II Uncontrolled Waste Site ...

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