Unguenta SalisilatUNGUENTA SALISILATPenimbangan bahan
formulaASAM SALISILATFormulaIIIIIIIVWadah
(g)14.50114.11214.55414.042Wadah + isi
(g)15.02114.61215.06514.542Isi
(g)0.520.50.5110.5VASELINFormulaIIIWadah (g)4645Wadah + isi
(g)145.3139Isi (g)99.593.9CERA FLAVAFormulaIIWadah (g)44Wadah + isi
(g)49.93Isi (g)5.6PEG 400FormulaIIIIVWadah (g)45.94960.721Wadah +
isi (g)90.17288.37Isi (g)44.22327.649PEG 4000FormulaIIIIVWadah
(g)94.68988.148Wadah + isi (g)149.998160.076Isi (g)55.30971.928UJI
HOMOGENITASFormulaIIIIIIIVReplikasi123123123123HomogenHalusUJI DAYA
SEBARFormula IFormula IIFormula IIIFormula
IV05010015005010015005010015005010015044.024.124.223.884.034.154.233.43.43.43.42.22.22.3152.315UJI
KEMAMPUAN PROTEKSIFormula IFormula IIFormula IIIFormula IV
15"v15"v15"v15"v30"v30"v30"v30"v45"v45"v45"v45"v60"v60"v60"v60"v180"v180"v180"v180"v300"v300"v300"v300"vUJI
DISOLUSIPenimbanganFormulaI (basis vaselin)III (basis PEG)Berat sel
disolusiBerat sel disolusi + unguentaBerat unguentaLarutan Stok (C
= 1mg/mL)Cara:25mg as. salisilat ad aquadest 250mL
Absorbansi blankoSeri larutan bakuABSORBANSISeriC
(mg/mL)Abs10.020.36920.030.5430.040.63840.050.76350.060.868a =
0.147b = 12.21r = 0.995y= 12.21x + 0.147PENGUJIAN DISOLUSI
UNGUENTAFORMULA I (basis vaselin)Menit ke-AbsC
(x/5mL)00.05-0.0079450.066-0.00663100.069-0.00639150.075-0.0059250.077-0.00573350.079-0.00557450.081-0.00541FORMULA
III (basis PEG)Menit ke-AbsC
(x/5mL)00.089-0.0047550.092-0.0045100.099-0.00393150.1-0.00385250.1-0.00385350.104-0.00352450.109-0.00311
Suspensi SulfadiazineSUSPENSI SULFADIAZINEMETODE PRESIPITASI
& METODE DISPERSIPenimbangan Metode PresipitasiSulfa (g)As.
sitrat (g)Met. paraben (g)NaOH (g)CMC-Na (g)Wadah (g)Wadah + zat
(g)Zat (g)00000Penimbangan Metode DispersiSulfa (g)As. sitrat
(g)Met. paraben (g)NaOH (g)CMC-Na (g)Wadah (g)Wadah + zat (g)Zat
(g)00000Penimbangan Sukrosa untuk Metode Presipitasi & Metode
DispersiSukrosa (g)Wadah (g)Wadah + zat (g)Zat (g)0UJI DIAMETER
PARTIKELKalibrasi =
Metode PresipitasiDiameterFrekuensiDiameter sesungguhnyaLog
DFrekuensi x log D
Jumlah000Rata-rata SD Antilog SD Metode
DispersiDiameterFrekuensiDiameter sesungguhnyaLog DFrekuensi x log
D
Jumlah000Rata-rata SD Antilog SD Metode
PresipitasiHari0136ReplikasiV0VtV0 - VtVtV0 - VtVtV0 -
VtI000II000III000Metode DispersiHari0136replikasiV0VtV0 - VtVtV0 -
VtVtV0 - VtI000II000III000SISTEM FLOKULASI & DEFLOKULASI
SUSPENSI // PENGAMATAN VOLUME SEDIMENTASIDerajat Flokulasi: B=
FORMULA AReplikasiWaktu (Menit)05101520253040I (cm)II (cm)III
(cm)Rata-rataBFORMULA BReplikasiWaktu (Menit)05101520253040I (cm)II
(cm)III (cm)Rata-rataBFORMULA CReplikasiWaktu
(Menit)05101520253040I (cm)II (cm)III (cm)Rata-rataBFORMULA
DReplikasiWaktu (Menit)05101520253040I (cm)II (cm)III
(cm)Rata-rataBFORMULA EReplikasiWaktu (Menit)05101520253040I (cm)II
(cm)III (cm)Rata-rataBPersentase
PemisahanFormulaAMenit05101520253040Vo(mL)V (mL)%Pemisahan
FormulaBMenit05101520253040Vo(mL)V (mL)%Pemisahan
FormulaCMenit05101520253040Vo(mL)V (mL)%Pemisahan
FormulaDMenit05101520253040Vo(mL)V (mL)%Pemisahan
FormulaEMenit05101520253040Vo(mL)V (mL)%Pemisahan
/(~)
EmulsiEMULSIUJI STABILITASEmulsi MixerEmulsi BlenderEmulsi
HomogenizerVol. Pengendapan (mL)Vol. Pengendapan (mL)Vol.
Pengendapan (mL)123123123H0H + 30'H + 60'H + 1H + 2H +
3SENTRIFUGASIReplikasiEmulsi MixerEmulsi BlenderEmulsi
HomogenizerIIIIIIPERSENTASE PEMISAHANDengan
SentrifugasiReplikasiEmulsi MixerEmulsi BlenderEmulsi
HomogenizerIIIIIIRata-rata Tanpa SentrifugasiEmulsi Mixer (%)Emulsi
Blender (%)Emulsi Homogenizer
(%)123Rata-rata123Rata-rata123Rata-rataH0 H + 30' H + 60' H + 1 H +
2 H + 3 PERHITUNGAN RESEPOleum arachidis80g x 3 = 240gTween -
SpanFormula 1Formula 2Formula 3Tween 80Span 80Tween 80 Span 80Tween
80Span 80
Aquadest500 - (80+20) = 400g400g x 3 = 1200gData Hubungan HLB
dengan Stabilitas EmulsiFormula 1Formula 2Formula 3Tween 80Span
80Oleum ArachidisTween 80Span 80Oleum ArachidisTween 80Span 80Oleum
ArachidisWadah (g)31.797.932.991.730148Wadah + zat
(g)37.95197.945.4191.748.75248Wadah + sisa
(g)31.797.932.991.730148Zat
(g)18.756.2510012.512.51006.2518.75100NILAI HLB CAMPURANFormulaHLB
TweenHLB SpanHLB
CampuranI11,251,07512,325II7,52,159,65III3,753,2256,97VISKOSITAS
EMULSIReplikasiWaktuForm. IForm. IIForm.
IIIAir106,374,764,697,41205,305,144,526,53305,285,204,895,43Perhitungan
Viskositas Emulsi air pada suhu 28oC = 0.8904KV air =0,92Koefisien
alat (KV) = V=
FormulaVKVI1,16810.401866496II1339.1911.92414776III1562.513.9125Rata-rata12.079504752VISKOSITAS
FORMULA 1 = KV x
FormulaVHI9811.2313460502II1179.241.024346592III1183.711.02047839011.0920570108VISKOSITAS
FORMULA 2 = KV x
FormulaVHI1313.020.9199787324II1215.950.9934211729III1201.921.00501736820.9728057578VISKOSITAS
FORMULA 3 = KV x
FormulaVHI1332.620.906447806II1382.740.8735919082III1291.320.93543852430.9051594128UJI
PEMISAHAN EMULSIPersen Pemisahan EmulsiTF I (cm)F II (cm)F III
(cm)R IR IIR IIIR IR IIR IIIR IR IIR III0000000000145Persen
PemisahanHari0145R IR IIR IIIR IR IIR IIIR IR IIR IIIR IR IIR IIIF
I100100100100100100100100100100100100F
II100100100100100100100100100100100100F
III100100100100100100100100100100100100Rata-rataHari0145F
I100100100100F II100100100100F III100100100100
75/100 20=1525/100 20=550/100 20=1050/100 20=1025/100 20=575/100
20=15