Clean Air Engineering - United States Environmental ... · R. Apa - Vertac Chemical Corporation P. Schwindt - US EPA M. McCorkle - State of Arkansas Department of Pollution Control

Clean Air Engineering

REPORT ONTRIAL BURN TESTING

Performed for:VERTAC SITE CONTRACTORS

Conducted at:VERTAC CHEMICAL CORPORATION

SUPERFUND SITEJACKSONVILLE, ARKANSAS

CAE Project No: 5815-1December 5,1991

VOLUME I

VERTAC SITE CONTRACTORSCAE Project No: 5815-1

CONTENTS

VOLUME I

1. SUMMARYINTRODUCTIONSUMMARY OF TEST RESULTS

2. DESCRIPTION OF INSTALLATION

3. SUMMARY OF PROCEDURESSAMPLING PROCEDURESANALYTICAL PROCEDURESQUALITY CONTROL PROCEDURES

4. COMMENTS

5. APPENDIXNOMENCLATURESAMPLE CALCULATIONSPARAMETERSCALIBRATION DATAWEIGHT SHEETSFIELD DATAFIELD DATA PRINTOUTSSTATISTICAL ANALYSISCHAIN OF CUSTODYQUALITY ASSURANCE REVIEW


CONTENTS (Continued)

VOLUME II • PROCESS DATA

VOLUME III - LABORATORY DATA

VOLUME IV - DIOXIN/FURAN DATA

VOLUME V - METHOD VALIDATION - SEPTEMBER 18 AND 19.1991

VOLUME VI - METHOD VALIDATION - SEPTEMBER 25 AND 26,1991


SUMMARY

INTRODUCTION

Clean Air Engineering was contracted by Venae Site Contractors to determinethe levels of particulate, dioxins/furans, hydrogen chloride andhexachlorobenzene emissions at the Vertac Chemical Corporation Superfundsite located in Jacksonville, Arkansas in support of their trial burn. Waste feedand process samples were taken and analyzed in accordance with the TrialBurn sampling and analytical plan.

The testing took place at the Stack on October 9 through 1 1 , 1 9 9 1 .Coordinating the field testing were:

R. Apa - Vertac Chemical CorporationP. Schwindt - US EPAM. McCorkle - State of Arkansas Department of Pollution

Control and EnergyC. Young - Independent Quality Assurance AdvisorJ. Chapman - Clean Air Engineering

SUMMARY OF TEST RESULTS

The test conditions and results of analysis are presented in Tables 1 through 3on pages 1-2 through 1-4.

To the best of our knowledge, the data presented in this report are accurateand complete.

Respectfully submitted,

CLEAN AIR ENGINEERING

John ChapmanVice PresidentResearch and Development

Kimberiy KemptManager, Technical Communications


EPA Method 5 and SW-846 MetParticulate/ChlorideStack

Run No.

Date (1991)Start Time (approx.)Stop Time (approx.)

Process DataHexachlocobenzene (Ib/hr)Cl" (Ib/hr from Hexachlorobenzene)Cl' (Ib/hr in waste feed)a-(Ib/hr total input)

Gas ConditionsTemperature (°F)Moisture (volume %)02 (dry volume %)COz (dry volume %)

Volumetric Row Rateacfmdscfm

Particulatagr/dscfgr/dscf @12% COzgr/dscf @7% OgIb/hr

ChlorideIb/hrppmv

ci" Removal Efficiencypercent (based on Ib/hr)

hod 0050

TBP-1

October 93:38 PM5:15 PM

100.074.7539614

20342.110.97.8

26,52012.280

0.00300.00460.00420.320

0.7911.6

99.87

TBP-2

Ocfeber 1012:13 PM

1:35 PM

100.074.7518592

20242.710.77.5

26,68012,220

0.00310.00500.00420.323

0.7711.5

99.87

TBP.3

October 111:01 PM2:07 PM

100.074.7425500

20341.510.97.9

24.63011,390

0.00270.00410.00380.260

1.0917.3

99.78

AVERAGE

100.074.7494589

20342.110.87.7

25,84011,960

0.00290.00460.0041

0.301

0.8813.5

99.84


TABLE 2 - Summary of Test

553559E5EIHStackRun No.Date (1991)Start Time (approx.)Stop Time (approx.)

Process DataInput Feed Rate

Hexachlorobenzene (Ib/hr)

Heat InputWaste Feed

MMBTU/hrHexachlorobenzene

MMBTU/hrTotal

MMBTU/hr

Carbon Monoxideaverage ppmv @ 7% Og

<3as ConditionsTemperature (°F)Moisture (volume %)Og (dry volume %)COg (dry volume %)

Volumetric Flow Rateacfmdscfm

Hexachlorobenzenelug/dscm

Ib/hr

Destruction Removal Efficiencypercent (based on Ib/hr)

1 See Comments, page 4-1.

Results

TB.1October 9

226 PM6:35 PM

100

18.43

0.32

18.75

5.8

20142.510.87.4

25,73011.860

0.95

0.0000421

99.999958

TB.2October 10

10:44 AM3:03 PM

100

20.13

0.32

20.44

1.5

20143.01 1 . 17.9

26,10011,940

0.93

0.0000416

99.999958

TB-3October 11

3:42 PM8:1 OPM

100

16.23

0.32

16.56

3.6

20242.211.07.5

26,07011,920

1.10(1.14)

0.0000490(0.0000499)

99.999951(99.999950)

Average

100

18.28

0.32

18.58

3.8

20142.811.07.8

25.97011.910

0.99

0.0000442

" •\•9.9999S8

1-3

C\Jr~-•^—00

"


TABLE 3 - Summary of Test Results

Waste Sample Determinations

SAMPLE HEXACHLOROBENZENE

COMBINED INCINERATOR SALTTB-1TB-2TB-3

CAUSTIC SOLUTIONTB-1TB-2TB-3

LIME SOLUTIONTB-1TB-2TB-3

PROCESS WATERTB-1TB-2TB-3

<16.67pg/kg ND<16.76 pg/kg ND<15.24ug/kg ND

<65.346 pg/L ND<62,515 pg/L ND<60,542 pg/L ND

<31.07pg/kg ND<23.69pg/kg ND<23.70 pg/kg ND

<0.735 pg/L NO<0.764ug/L ND<0.805 pg/L ND

HEAT CONTENT(Btu/lb)

N/AN/AN/A

N/AN/AN/A

N/AN/AN/A

N/AN/AN/A

CHLORIDE(percent)

N/AN/AN/A

N/AN/AN/A

N/AN/AN/A

0.000480.000490.00061

SOLID WASTE1TB-1TB-2TB-3

HIGH BTU LIQUID •Organic Waste-TB-1TB-2TB-3

INCINERATOR ASHTB-1TB-2TB-3

RECYCLE LIQUIDS -Scnibhar WaterTB-1TB-2TB-3

<1.37|Jg/g ND<1.18pg/g ND<1.12pg/g ND

<48,246 pg/L ND<49.483pgy1. ND<46,814 pg/L ND

<15.50 (ig^g ND<16.91 pg/kg ND<18.55 pg/kg ND

<0.725 pg . ND<0.770 ygfl. ND<0.857yg/L ND

7,1607,8877.245

9,0258.5209,149

N/AN/AN/A

N/AN/AN/A

28.026.027.0

26.027.026.0

N/AN/AN/A

N/AN/AN/A

1As measured prior to accounting for plastic.ND • Not Detected



QA/QC ResultsData Quality ObjectivesIsoklnetlclty

M5/26Partteulate and

Hydrogen Chloride%lsokinette

Data QualityObjectives

Run TBP-1Run TBP-2Run TBP-3

93.596.596.5

90-110%lsoklnette

SW-846 M0010Hexachlorobenzene

% Isoklnette

Data QualityObjectives

Run TB-1Run TB-2Run TB-3

101.8101.1102.4(99.2)*

90-110%lsokinetic

•Including correction for leakage.



QA/QC ResultsProcess SamplesHexachlorobenzeneMethod 8270Surrogate Recoveries

Run TB-1Recovered

Run TB-2% Recovered

Run TB-3% Recovered

Combined Incinerator Sa(t1,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

Caustic Solution1,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

Lime Solution1,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

Process Water1,4-Dibromobenzene-d41,3,5-Tricnlorobenzene-d3

StackGasTerphenyl-d141,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

SaMâssa.1,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

Hiqh Btu Liquid (Oroanic)1,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

Incinerator Ash1,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

Reevcle Liouids (Recycle)1,4-Dibromobenzene-d41,3,5-Trichlorobenzene-d3

58.248.1

105.974.6

58.447.1

68.048.1

66.2102.484.0

22.918.5

105.174.2

80.067.5

54.441.0

46.644.4

109.783.2

67.353.7

79.059.4

64.899.190.0

40.924.6

1 1 1 . 080.9

85.067.1

55.739.2

29.229.4

104.679.6

67.049.6

49.834.9

68.5103.9109.1

42.625.8

96.870.9

79.256.9

66.644.5


DESCRIPTION OF INSTALLATION

Vertac Site Contractors operates a transportable rotary kiln thermaldestruction unit (TDU) which is used to destroy hazardous wastes. The TDUis custom built specifically to process and destroy 2,4-Dichlorophenoxyaceticacid (2,4-D) still bottom and pesticide waste material located at the VertacChemical Corporation superfund site. The primary components include arotary kiln (primary combustion chamber), a hot cyclone, an after burner(secondary combustion chamber), a spray dryer/quench tower, fourbaghouses, a venturi/baffle plate absorber, an induced draft fan and a stack.

The testing reported in this document was performed at the Stack.

A schematic of the process is shown below.


SUMMARY OF PROCEDURES

SAMPLING PROCEDURES

The sampling followed procedures as detailed in U.S. Environmental ProtectionAgency (EPA) Methods 1,2,3,4,5 and 23. These methods are titled:

• Method 1 -- "Sample and Velocity Traverses for Stationary Sources;"• Method 2 — "Determination of Stack Gas Velocity and Volumetric Flow Rate

(Type S Pilot Tube);"• Method 3 — "Gas Analysis for the Determination of Dry Molecular Weight;"• Method 4 — -Determination of Moisture Content in Stack Gases;"• Method 5 — "Determination of Particulate Emissions from Stationary

Sources;"• Method 23 - "Determination of Polychlorinated Dibenzo-p-Dioxins and Poly-

chlorinated Dibenzofurans Emissions from StationarySources."

These methods appear in detail in Title 40 of the Code of Federal Regulations(CFR), Part 60, Appendix A.

Referenced with the above methods were EPA SW-846 Method 0010 andMethod 0050. These methods are titled:

•SW-846 0010

•Method 0050-

"Determination of Destruction and Removal Efficiency ofSemi-volatile Principal Organic Hazardous Constituents(POHC) from Incineration Systems;"

"Isokinetic HCI/Clz Emission Sampling Train."

Method 0050 is presented in the "Methods Manual for Compliance with the BIFRegulations". EPA/530-SW-91-010, December 1990.

The sampling apparatus are shown in Figs 1 through 3 on pages 3-3 through3-5. The sampling equipment was designed and manufactured by the NutechCorp. and Clean Air Engineering to meet U.S. EPA standards. All equipmentwas calibrated at the Clean Air Engineering laboratory prior to shipment to thejob site.


SUMMARY OF PROCEDURES (Continued)

Sampling Locations

The Stack has two ports. For paniculate and hydrogen chloride testing, 12points were sampled per port. The sampling time per point was 2.5 minutes fora total sampling time of 60 minutes. For hexachlorobenzene testing, 12 pointswere sampled per port. The sampling time per point was 10 minutes for a totalsampling time of 4 hours. The sampling locations are shown in Fig 3 onpage 3-5.

The solid and liquid waste and waste samples were collected at the locationsspecified in the Trial Burn sampling and analysis plan.


Figure 1

The EPA Method 5 and SW-846 Method 0050 sampling apparatus is shown.

NOZZLE FILTER TEAPERATURE

Impinqer Contents1) 100ml0.1NH2S042) 100ml0.1NH2S043) empty4) 300 g silica gel


Figure 2

The SW-846 Method 0010 sampling apparatus Is shown.

Impinger Contents1) 100 ml HPLC water2) 100 ml HPLC water3) Empty4) 300 g silica gel


Figures

The cross section of the Stack shows sampling point locations.

42 I NPORT 1

GAS FLOWOUT OF PAGE

PORT 2

TRAVERSE POINT123456789

101112

PORT TO POINT DISTANCE (\W41.039.237.034.631.527.015.010.57.45.02.81.0



ANALYTICAL PROCEDURES

Paniculate

The paniculate emissions were determined following procedures detailed inEPA Method 5. Paniculate samples collected on Pallflex 2500 QAT-UP Quartzfiber filters were analyzed gravimetrically. The probe and nozzles werewashed with acetone. The wash was transferred to tared beakers andevaporated to dryness. These weight differentials were combined to determinetotal paniculate matter.

Hydrogen Chloride

The hydrogen chloride emission rate was determined using proceduresdetailed in Method 0050. The stack gas from the paniculate run was passedthrough dilute sulfuric add. In the dilute add, the HCI gas was dissolved andformed chloride (Cl") ions.

An aliquot of the first three impingers of the paniculate train was analyzed forchlorides. The Cl" was analyzed by ion chromatography.

POHC Emissions

Sampling was performed to determine the emission rate and DRE of theselected POHC's by utilizing the procedures detailed in EPA SW-846Method 0010. SW846 Method 8270 was used for the analysis ofhexachlorobenzene.

The MM5 XAD traps used for sampling were pre-spiked with 100 micrograms(ug) of terphenyl-di4. The samples were spiked with 100 g of 1,3,5-trichlorobenzene-da and 1,4-dibromobenzene-d4 prior to extraction. The XAD,filter, and methanol/methylene chloride portions of the MM5 samples wereSoxhiett extracted for 16 hours with methylene chloride. The impinger andcondensate ponions were extracted with methylene chloride using a separatoryfunnel. The extracts were combined and concentrated to a final volume of 1.0milliliter prior to analysis. The hexachlorobenzene analysis is based on theguidelines of Method 8270.



ANALYTICAL PROCEDURES (Continued)

Dioxins/Furans

The emissions were determined according to the procedures detailed in EPAMethod 23 titled "Determination of Polychlorinated Dibenzo-p-Dloxins (PCDD)and Polychlorinated Dibenzofurans (PCDF) Emissions From StationarySources."

The analytical method entailed the addition of isotropically labelled internalstandards to all samples in known quantities, matrix-specific extraction of thesample with appropriate organic solvents, preliminary fractionalization andcleanup of extracts using a sequence of liquid chromatography columns andanalysis of the processed extract for PCDD and PCDF using high-resolutioncapillary column gas chromatography coupled with high resolution massspectrometry.

QUALITY CONTROL PROCEDURES

Quality control procedures for all aspects of field sampling; samplepreservation and holding time; reagent quality; analytical method; analysttraining and safety; and instrument cleaning, calibration and safety werefollowed. These procedures are generally consistent with EPA guidelinesdocumented in "Quality Assurance Manuals for Air Pollution MeasurementSystems," Vol 3, "Stationary Source Specific Methods" (EPA-600/4-77-027b).

An independent quality assurance review was conducted by Dr. Craig Young.Dr. Young is a private consultant organizationally independent of the trial bum'stechnical staff and is not directly responsible for any environmentalmeasurements nor accountable to those directly responsible. A copy of hisreport is included in the Appendix.


COMMENTS

At the half-way point of Run 3 of the MM5 sampling, the train failed to pass aleak check. The leak rate was 0.08 CFM. The cause of the leak wasdetermined to be a small chip In the connection between the probe and filterholder. The connection was replaced and sampling allowed to continue. Thechipped piece was rinsed and included In the recovery of the rest of thesample. The chipped connection was under a slight positive pressure due tothe pressure of the stack. Any leakage should have been out of the train, asopposed to into the train, and contamination of the sample is highly unlikely.However, calculations have also been performed using the technique ofMethod 5, Section 6.3 to correct the sample volume. These results areshown in parentheses ().

Prior to the testing in this document, two baseline runs were performed.These results are presented in a separate report.

During Runs 2 and 3. the liquid organic flow meter was not operatingproperly. The flow rate was obtained by measuring the level in the tank atspecific time intervals. See Volume II of the Appendix for details.

Sampling and analysis for dioxins/furans was conducted concurrently withMM5 Run TB-3. The results are presented in Volume IV of the Appendix perinstructions given by Arkansas DPC&E.

VOST sampling and analysis was performed during the trial burn. Theresults are presented in a separate report per instructions by ArkansasDPC&E. The results of the Method Validation Tests performed on September18 & 19 and September 25 & 26 are attached in Volumes V and VI assupplemental information.

No other deviations from standard U.S. EPA testing procedures were noted.


APPENDIX

NOMENCLATURESAMPLE CALCULATIONSPARAMETERSCALIBRATION DATAWEIGHT SHEETSFIELD DATAFIELD DATA PRINTOUTSSTATISTICAL ANALYSISCHAIN OF CUSTODY

VERTAC SITE CONTRACTORSCAE Project No; 5615-1

NOMENCLATURE

Nomenclature

absorbancecross sectional area of nozzle (ft2)cross sectional area o1 stack (ft2)proportion of water vapor In the gas stream by volume (%)proportion of water vapor In the gas stream by volume (%)at saturated conditionspitot tube coefficient (dimensionless)dilution factorratio of dry gas generated to gross calories (dscl/MBtu)ratio of gas generatedgross calorific value of fuel (Btu/lb)average pressure drop across meter box orifice (in. HzO)average square roots of velocity heads of stack gas ( /In. H20)meter orifice calibration coefficient (In. HgO)percent of isoklnetic sampling (acceptable: 90 %1 110%)pilot tube constant: 85.49 (ft/sec) mole)(ln. Hgf

V(0 R)(in. H20)spectrophotometer calibration factordry molecular weight of stack gas (IMb-mole)molecular weight of stack gas, wet basis (Ib/lb-mole)total amount of paniculate matter collected (gm)normality of tilrant (meq/ml)barometric pressure (in. Hg)initial barometric pressure (in. Hg)final barometric pressure (in. Hg)final pressure of flask (relative In. Hg)Initial pressure of flask (relative In. Hg)absolute stack gas pressure (In. Hg)volumetric flow rate, actual conditionsvolumetric flow rate, standard conditions, dry bastestandard conditions, 29.92 in. Hg, 68°Ffinal temperature of flask (°F)initial temperature of flask (°F)

average dry gas meter temperature (°F)average slack temperature (°F)absolute temperature, standard conditions (528°R)total sampling time (min)volume of aliquot (ml)volume of flask (ml)total volume of liquid collected in Implngers and silica gel (ml)volume of gas sample through the dry gas meter at meterconditions (ft3)volume of gas sample through the dry gas meter, standardconditions (ft3)volume of flask sample, standard conditions (ml)total volume of solution (ml)volume of titrant used to titrate aliquot (ml)volume of titrant used to titrate blank (ml)volume of water collected, standard conditions (ft3)stack gas velocity (ft/sec)gas meter correction factor (dimenslonless)


SAMPLE CALCULATIONS


SAMPLE CALCULATIONS • RUNTBP-1. STACK. PARTICULATE(Note: results are taken from computer analysis)

1. Volume of water collectedV^ »(0.04707)(^)

" (0.04707) (502)• 23.63 wscf

2. Volume of gas metered, standard conditions(17.64) (Vn.)[R. L,

vm- ' (460+TJ w

_ (17.64) (33.14) [30.04^1(460+77)

= 32.43 dscf

3. Moisture contentBwo

V.wdd

Vmrtd + V«<d23.63

32.43+23.63•0.4215=42.2%

4. Molecular weight of dry gas streamM, » 0.44(ycCOa) + 0.32(%0») + 0.28(%CO + %N»)

» 0.44(7.8) + 0.32(10.9) + 0.28(81.3)=29.68

5. Molecular weight of stack gasM. -M<(1-B^,)+18(B^)

• 29.68(1 -0.4215) +18(0.4215)• 24.76

6. Stack pressure (in. Hg)

"• M™). 30.04 JM)

V13.6J• 30.08

VERTAC SITE CONTRACTORSCAEProjectNo: 5815-1

SAMPLE CALCULATIONS (Continued)

7. Velocity of stack gas

V. ,K,C,(DP)iOLL4^KM.) (P.)]*

• 85.49 (0.84) (0.679) [203+460)[(24.76) (30.08)]*

B 46.03 ft/SCC

8. Total flow of slack gas

Q. »(60)(A.)(V.)»(60) (9.6) (46.03)•26,520acfm

Q ^Q.P.(17.64)(1-B^)*" ~ TT+460

_ (26.520) (30.08) (17.64) (1 - 0.4215)203+460

=12,280dscfm

9. Percent Isokineticy| n (0.09450) 0: + 460) Vn«d

P.V.A,9(1-B^)(0.09450) (203 + 460) (32.43)

(30.08) (46.03) (0.000452) (60) (1-0.4215)=93.5%

10. Paniculate

gr/dsd -(15^(15.43r(0.0064)

32.43• 0.0030

^ (gr/gscf)(l2)3 (20.9 - yoCOz)_ (0.0030)(12)~ (20.9-7.8)=0.0046

^ VERTAC SITE CONTRACTORSCAE Project No: 5815-1


10. Partlculate (Continued)

gr/dscfÔ,.^^20-9-7)u (20.9-%0,)^ (0.0030)03.7)° (20.9-10.9)» 0.0042

Ib/nr -(gr/ctecf)(Q^(60)7000

_ (0.0030) (12.280) (60)7000

=0.320



11. Chloride concentration

Ib/dscf(453.590'gt)(Vn^)

. (15-7)(453,590) (32.43)

"0.00000107

ppm ib/dSCf)-^85^10!-(molecular weight)

.OOOOOW385-3^(35.45)

=11.6

Ib/hr = (Ib/dscf) (dscfm) (60)=(0.00000107) (12,280) (60)=0.788

12. Hexachlorobenzene, Run TB-1

Ib/dscf -____^S____'(Vn...d)(1.000)(453,590)______(3.66)

(136.51)(1.000)(453,590)i5.91x10-"

pg/dscm ^Ja-f^ l(V^,)l m3 J

(136.51)•0.95

(35.31)

Ib/hr = (Ib/dscf) (dscfm) (60)=(5.91x10r")(11,860)(60)=4.21x10-6


PARAMETERS

VERTAG SITE CONTRACTORSCAE Project No: 5815-1

Run No. 3

SoikLWaslflOrganic Halides (mg/kg sample)Feed Rate (b sample/hr)

Cl-(Ib/hr)

Organic WasteOrganic Halides (mg/kg sample)Feed Rate (Ib sample/hi)

Cl- (Ib/hr)

Chloride Input/Waste Only)Ib/hr

Hexachlorobenzene% ChlorideFeed Rate (Ib/hr)

Cl- (Ib/hr)

Total Chloride InputIb/hr

252.0001.172.8

296

260,000937.85

244

539

74.7100

74.7

614

228,0001,670.6

381

270,000506.52

137

518

74.7100

74.7

592

234.0001.615.0

378

260.000182.6

47

425

74.7100

74.7

500

VERTAC SITE CONTRACTORSCAE Project No: 5815

PARAMETERS

STACK. PARTICULATE/CHLORIDES

Run No.

An

As

Bye%COi

^

DH

DH@

'(DPPs

%I

Md

Mn

MS

%0,

Pb

PS

e

Tm

TSVie

Vm

Ymstd

VB

Vwstd

Yd

TBP-1

.000452

9.6

.4215

7.8

.840

1.09

1.678

.679

93.5

29.68

.0064

24.76

10.9

30.04

30.08

60.0

77

203

502

33.14

32.43

46.03

23.63

.9898

TBP-2

.000456

9.6

.4273

7.5

.840

1.18

1.678

.682

96.5

29.63

.0067

24.66

10.7

30.00

30.03

60.0

84

202

532

34.73

33.56

46.31

25.04

.9898

TBP-3

.000456

9.6

.4152

7.9

.840

1.01 ^C^

1.678 « -

.628 Q

96.5 0

29.70

.0054

24.84

10.9

29.66

29.70

60.0

81

203

472

32.63

31.29

42.76

22.22

.9898

VERTACSITECON1CAE Project No: 581STACKCHLORIDE PARAME

RUN NO.DATE (1991)START TIMESTOP TIME

Vmstddsdm

ChloridemgCI-Ib/dscfppmto/hr

•RACTORS5-1

JERS

TBP-1Octobers338 PM5:15 PM

32.4312.280

15.70.00000107

11.60.788

TBP.2October 10

12:13 PMia5PM

33.5612.220

16.10.00000106

11.50.774

TBP-3October 11

1:01 PM2:07 PM

31.2911.390

22.60.00000159

17.31.069

VERTAC SITE CONTRACTORSCAE Project No: 5815-1Heat Input Determination

Run No. TB-1 TB-2 TB-3

SfllismasiaHeat of Combustion (BTU/lb)Feed Rate (b/hr)

MMBTU/hr

Orpanic WasteHeat of Combustion (BTU/lb)Feed Rate (b/hr)

MMBTU/hr

Total Heat Input Waste Only)MMBTU/hr

HaxaphlorobenffinaHeat of Combustion (BTU/lb)Feed Rate (Ib/hr)

8.4981,172.8

10.0

9.025937.85

8.5

18.4

3.222100

9.4571.670.6

153

8.520506.52

4.3

20.1

3.222100

9.0171,615.0

14.6

9.149182.6

1.7

16.2

3.222100

MMBTU/hr 0.32220.3222 0.3222

VERTAC SITE CONTRACTORSCAE Project No: 5815

PARAMETERS

STACK - HEXACHLOROBENZENE

Run No.

An

AsBô

%CO,

c?DH

DHB

"(DpTis

%I

Md

MS

%0,

Pb

PS

eTm

Ts

Vie

Vm

Vmstd

Vs

Vwstd

Yd

TB-1

.000452

9.6

.4254

7.4

.840

1 . 1 5

1.878

.659

101.8

29.62

24.67

10.8

30.04

30.08

240.0

80

201

2,147

137.47

136.51

44.67

101.08

1.0095

TB-2

.000452

9.6

.4300

7.9

.840

1 . 1 8

1.878

.668

101.1

29.71

24.67

11 .1

30.00

30.04

240.0

86

201

2,186

138.99

136.40

45.32

102.92

1.0095

TB-3

.000452

9.6

.4225

7.5

•840 01.16 ON

" I-1.878 -

S102.4

29.64

24.72

11.0

29.66

29.72

240.0

78

202

2,145

140*29

138.05

45.26

100.98

1.0095

VERTAC SITE CONTRACTORSCAE Project No: 5815-1INCINERATOR STACK

RUN NO. TB-3Date (1991) October 11Start Time (approx.l 3:42 PMStop Time (approx.) 8:10 PM

Leak Rate 0.08Max. Allowed Leak Rate 0.02Time Elapsed (min) 120

%C02 7.5%02 11.0Pb 29.66STATIC P 0.8CP 0.84As 9.6Vie 2,145Vm 133.09DH 1.16Yd 1.0095Tm 78

CALCULATED RESULTS

Vwstd 100.97Vmstd 131.03Bwo 0.4352AVGVELROOT 0.664AVQTEMP 202Md 29.64M8 24.57PS 29.72V8 45.40% Isokinetic 99.2Qa(acfm) 26,150Qstd(dscftn) 11,700

_ VERTAC SITE CONTRACTORSCAE Project No: 5815-1

Run No. TB-1 TB-2 TB-3 TB-3*

Vmstd 136.51 136.40 138.05 133.09dscfm 11,860 11.940 11.920 11,700

Hexachlorobenzene|i0 3.66 3.59 4.29 4.29bftlsd 5.91E-11 5.80E-11 6.85E-11 7.11E-11M/dscm 0.95 0.93 1.10 1.14b/hr 4.21 E-05 4.16E-05 4.90E-05 4.99E-05

*See Comments, page 4-1.

'r-0inyo0

TRIAL BURN FEED RATES

Test Period 1:Port 1

Solids Feed Rate, Ib/hr 1,175.0per WIT-135MOrganics Feed Rate, Ib/hr 855*6per LIT-402 _____

TOTAL 2,030.6Hexachlorobenzene, Ib/hr 100.0

Test period 2 ;Solids Feed Rate, Ib/hr 1,700.6per WIT-135MOrganics Feed Rate, Ib/hr 768.45per LIT-402 ______

TOTAL 2 , 4 6 9 . 0Hexachlorobenzene, Ib/hr 100.0

Test Period 3 ;Solids Feed Rate, Ib/hr 1,846.9per WIT-135MOrganics Feed Rate, Ib/hr 204.28per FT-127 _____

TOTAL 2,051.2Hexachlorobenzene, Ib/hr 100.0

Port 11,175.0

855.6

2,030.6

100.0

1,700.6

768.45

2,469.0

100.0

1,846.9

204.28

2,051.2

100.0

Port 2

1,170.6

1,021.1

2,191.7

100.0

1,640.6

244.58

1,885.2

100.0

1,383.12

160.94

1,544.1

100.0

Average1,172.8

937.85

2,110.65

100.0CM0in

1,670.6 •r"00

506.52

2,177.12

100.0

1,615.0

182.6

1,797.6

100.0

Test Series Average Feed Rates: Waste Feed, Ib/hr 2,028.4Hexachlorobenzene, Ib/hr 100.0

October t, 1991

\ (2 * ^ v \ c 0 ê

^(O^

DETERMINATION OF SOLIDS

Btu/lb and »C1-

ADJUSTED FOR PLASTIC DRUMS

KCTO

1/2

DATE: 1° V\______ INITIALS

Weight in Hopper

Weight in Hopper ' .0 > ^ 0 0 (i) ^(WIT-135M) 0

inDetermination of Btu/lb Value for Solids Processed into Hopper

00

Weight TotalDrums Number per Drum Weight(Size) (w/lid)

Number of 110's ______ x 62 Ib/drun = ______

Number of 85's '2- ^f x 43 Ib/drum » i > \ \^

Number of 55's 2. x 37 Ib/drun » ^C*!

Total Weight of Plastic 2.^0^0 (2)

Weight in Hopper T-QxtOO Ibs^ <1) ^Total Plastic - ^.0^0 Ibs^l2).,..

Total Solids I j toÔ Ibs (3)

Reported Btu/lb of Solids x Total Solids = Btu's of Solids

l.lC?0 Btu/lb x XLf/ll^ Ibs » 1^33 • t 0 Btu (4)( l a b ) ( 3 ) ————————

October 1. 1991 Ke<0

2/2

Total Plastic x 20,480 Btu/lb » Btu of Plastic

2.^0") 0 Lba x 20,480 Btu/lb » ^Z.) $^ ^00 Btu (5»(2) ^

Btu of Solids ^-33'S - (0(4)

+Btu of Plastic -t-^Z.^^ . l-U-0' ' ( i ) \ ^

Total Btu ^^^ '•\° (6)

Total Btu - Weight in Hopper s3 Composite Btu/lb ^

\-^-^ Btu. .-? Q Q Ib » Jl. 1...... BtU/lb S(6) ( t ) _ _

00

Determination of %C1- in Solida

Total Solids x Reported %C1- + 100 - Lbs Cl-

\^ ,[p^0 Ibs x 3*0-° %C1- + 100 - ^3-^ Iba Cl- (7)— — ( 3 ) ( l a b ) —————

Lbs Cl- -i- Weight in Hopper x 100 » » Cl-

^\^ ^ Ibs Cl- + Z-OnQQ Ibs x 100 . .? :JL-. »C1-(7) (1)

Oc<obCT». 19*1

I »r?-T V^^t <^ (-

^ 1 \^ f (\\IffO

1/2DETERMINATION OF SOLIDS

Btu/lb and »C1-ADJUSTED FOR PLASTIC DRUMS

DATE: ___________ INITIALS _________

Weight in Hopper

Weight in Hopper ^ i (c 0 0 (l) Ln

(WIT-135M) 0in

Determination of Btu/lb Value for Solids Processed into Hopper

Weight TotalDrums Number per Drua Weight(Size) (w/lid)

Number of 110 's _____ x 62 Ib/drum » ________

00

Number of 85's "0 x 43 Ib/drum - \ ,<i4^

Number of 55's 4 b x 37 Ib/drun = \ . ^ \

Total Weight of Plastic 2>) 4 4 0 (2)

Weight in Hopper ^ , (f00 Ibs-Y (1.).^- Total Plastic - .?>4HO Iba

-(2)Total Solids '3-H ) ll>C> Ibs (3)

Reported Btu/lb of Solids x Total Solids = Btu's of Solids

^t^"7 Btu/lb x ^ .vAi \bO Ibs - \.1\0^•[0 Btu (4)( l a b ) — — f t } ' ————————

October I, 1991 RevO

2/2

Total Plastic x 20,480 Btu/lb " Btu of Plastic

^4^0 Lbs x 20,480 Btu/lb - ^ O.^SÎOQ Btu (5)(2) ^

Btu of Solids l ^ °C>- \0(4)

+Btu of Plastic -0 Q > '4 2. 0 0!5) ^

Total Btu <y•w I P ' 1 0 (6)

Total Btu - Weight in Hopper = Composite Btu/lb ^

y^\o~\^ Btu.^.ô ib «..flLil.2.._ Btu/ib S(6) (1) -

00

Determination of %C1- in Solids

Total Solids x Reported %C1- + 100 - Lbs Cl-

*>JA . \ IP 0 IDS x 9-^-° %C1- + 100 - 6^-^ Iba Cl- (7)(3) (lab) —————

Lbs Cl- •'• Weight in Hopper x 100 = % Cl-

(^\ -^ ibs ci- + 2-IÔQ ibs x 100 - .-?-?.:?,.„ %ci-(7) (1)

Octoba I. 1991 KwO

172DETERMINATION OF SOLIDSBtu/lb and »C1-

ADJUSTED FOR PLASTIC DRUMS

DATE: __________ INITIALS

Weight in Hopper

Weight in Hopper 1^ .600 (1) r^(WIT-135M) —————— ^) ^ ^v——————— ^ Q

ir\

Determination of Btu/lb Value for Solids Processed into Hopper Q0

Weight TotalDrums Number per Drum Weight(Size) (w/lid)

Number of 110's _____ x 62 Ib/drua - ________

Number of 85'a U \ x 43 Ib/druni • | -^ L -\

Number of 55's ^l x 37 Ib/drun » \ 5 H

Total Weight of Plastic 2> . <^ (2)

Weight in Hopper ^S^500 Ibs

- Total Plastic - 2) .LÔ Ibs(2)

Total Solids 2^ P.ZD Ibs (3)

Reported Btu/lb of Solids x Total Solids s Btu's of Solids^^ Btu/lb x Z.\ 0 Ibs « f.^3'7 • f0^ Btu (4)

(lab) (3) ————————

Ocloba I. 1991 RevO

2/2

Total Plastic x 20,480 Btu/lb " Btu of Plastic

VL^Q Lbs X 20,480 Btu/lb - (/?71 i1^)HOQ Btu (5)(2) ^

I - ^ t VBtu of Solids ' ' ^ • > ^ - I C ?

(4)

+Btu of Plastic •»• ^'L^MiHOP_li_lUJL—i5) ^

Total Btu 9^^°^ • (0 (6)

CDTotal Btu - Weight in Hopper = Composite Btu/lb o

^cf\ • <o\tu ,. 1^.6oo ib = -9.?-j-Z—„. Btu/ib in(6) (I) o

oDetermination of %C1- in Solids

Total Solids x Reported »C1- + 100 » Lbs Cl-

^\ ^ 2^LO Ibs x ^-° »C1- + 100 » ^7^^.4 lb« Cl- (7)——W ——(libT —————'

Lbs Cl- -r Weight in Hopper x 100 = » Cl-

^^^'^ Ibs Cl- + SL^,600 Ibs x 100 = ,.?.S»'— »C1-(7) (1)


CALIBRATION DATA

Ivic fEh c.OX . LL . -ST ^. .Lit \Tr -

Operator: JQ Û\Qd V^tc| Meter Box No.: (^ \ - Meter Box AH@: \ " [ Meter Box Yd: . <U

Q

. 0.*/0

^2»L>~7

^2^1

All

,5•c)

L^\>^

3,o^0

AF

-^-2.'

-7,~)-•?."?

-^-"

Yds

LOOOC

iOQQQ

/(?(?(><?I.OOOC,

ZooooUiQQQ.

Standard Meter GasVolume fr

Initial

0^

—<a—-^-

^———JK————/r

Final

Socx/.-^00^

//»0f2.f/^lK

/QO/0

/nô

VdsNet

<<»</Â35-

H.OIZ./^/Sf

IO,QIQ/D^Q

Meter Box Gas Volumef?

Initial

Wwmw7?y,??a9Y9.7W

}?97y^9 ia?

Final

W^f^^w.

IWÔ

W.W

9osf2.v>W.73J-

VdsNet

</-)^^Q^

UH^.)L^

/o.<i^m<f<

Std. MeterTemperature

In

"?3>-?-S

-2^-Jl

-7Z7Z

Out

7^'?3

^^-7^

-)Z72

Td.sAvg

7573

7^7^

7Z72-

Meter BoxTemperature

In

-155 -

^LfOi

101bi

Out

^^0

^2.

^

^^0

Barometric Pressure: {^ ^ Q

TdsAve

^

93

^^

^^

Time0

l -S,

}^^^95-

/O./L1 0 . 1 7

Yd

.^^7

.^<?/y

,9^99,Wff

, 5-y.7?S3

All®

/.^^

1.^

/.7^y/.?^^79

/^7i

Nomenclature Calculations Vacuum Guuge Culibrallon Thermometer CallbnilloniPb

I AHlAPIVdI VdsJYdI Yds

Barometric PressureFlow Rate (cfm)Orifice Pressure Differential ('HiO)Inlet Pressure Differential ('rhd)Volume Dry Gas Meter (ff)Volume Dry Standard (ft")Meter Correction Factor (unitlcss)Standard Meter Correction Factor (unitless)

; AH@ Orifice Pressure Differential that cave 0.75 cfn1 ofairat7(TFand29.92"H8(*H20)

Ydrvds1 (Td 4- 460"1|pb •«• AP/13.6

[Vd J [I'ds + '160J |pb + Al 1/13.6

AH® -

Vd J ri-ds + 160J IPb

0.0317 AH Icrds-t-'XSOX)2"]

Pb(Td + 460) [(Vds)(Yds) J

17.64 (Vds)(Pb)

(Tds •<- 460)0

StandardWa)^9^mi^nT^.H

VacuumGauccs,o/ao/^.o•^0z^miv

0 0 1 5 1 0

Standard

^/GO/2o^0

Inlet

^101)t0HI

Outlet

^0/o/w/V/

D.nc: a-ô.'n operator: rn O.V-V-Lo-vc; Mcicr llox No.: ( o ( - (p Mclcr BoxAll@: 1.^1.^,. ........

Q

l.1/1

M,

^1.^l

Al-I

;".---t '..—

'3

.^

1.^1.$'

3.03.0

Al^J»s-=-:-:r—

-'-I."/

^\n

-'-t^

-^,1

-5.1-5 .1

Yds

1.00^1.<^XJO

(.00^0f.foCOO

l.<xoc>t.oa.-o

Standard Meter GasVolume fl-

lniliiil

6.coo0.000

0»C06

O.uOO

O.OCO

o.ooo

————

Final•-S-.SS-l'SUSCT- &.

'5.00^

.giQ'o

IJ^.063IQ.fJC^

10,OC>><

>0.<-0!^

VilsNet

J2.0^L>

.3.0 L ...

JA.e '7io.(X>^

\0-<^^^ -J>A. -

Meier Uox Gas Voluine. ri"

Iniliul

I^Ll^W. l-}3.

. .rf^cb.y^

^lO.^

ô.^.

l-'iiuil

^5,1 IX

11PA.3I?

^0,9JM1^

^.un^^50

Meter llox Ytl: 1.00^

Vil.s, Ncl

& ff.SLS'-ok-?-

^.OJ^3.J^JAk-

\c».\'<a-\mM

Stil. Mclcr'I'clnpcralurc

In

]^LJ^L.

.^.iL

l»S^

——•

Oui-•3±USnS5Z

-< L(?•-/

. ^L(.^

(nS(^

•l\l.s^1Sfc^Js'i-

. Lrn^

^^l(o'-f

Meter UoxTemperature

In

-i'-l?•-(

VS?

-•E

â

Â

—-.

Out

^l•S-1

9X

72-

"S'3

73

.-——

Barometric Pressure: - .q, 3 /

TdsAvg

?A,>'•Sr^.5

S^"S-.5-

S-?^-r7.r

Tiinc0

IS.îa.»?

/^^^/5':3 '

/Ci.SS'

/o.^

Yd

!.0/o5').6»0'7

./.O/-?6-/0(^

l.C^L.1

\^5t1

Aild?

l.-?^-?^^ts

1^2-2.

/.î

l.^W1.<7(7

Nomenclature VacDiii" (.'uiiyc Ciilibnitlon Tlicnuointlcr Calibration;rb!0IAHlAl'

naromctric PressureFlow R!|(C (criii)Orincc I'rcssiirtt DiffcrcnUal ("IliO)i di i Unlicc I'rcssiirc Uillcrciiliai ( l ijl

i Al' Inlet I'rcMiirc l)»Hcrci»li;il ("IhO)I V.l Volumu Dry Gas Mclcr (((')1 Vd.s Volume 13ry Sliuidaril (ft1)( Yd Mclcr Correction Factor (unillcs.s)I Yils .Standard Mclcr Corrccdon P.iclor (iinillcss): ^11(?9 Orincc Pressure Differential (liat mwc 0.75 cfn! ttf air »( 7(rF aiitl 29.92 "1 Ig ("I liO)

Yil -•(Yds•1\1 4- 'lc»(» I'l) + A P/1^.6

Td.s I- 'Kit) I'll l AII/1.V>

U.O.I 17 Al l (Tils •I- -ICtO^

l'l»(Ttl 4 ')(>()) (V<ls)(Yils)

17.6-t (Vtls)(l'l>)

(•r>l.s I- 'I<»0)0

Slaiulnrd(UK)

5:Z1 6 , (

1 U ^

•z^M^y\OL't.

Vacuum

f.O(0. 0

»5.o^0.0

... .5-. o^

Slandard

TO

/60(^0/<-/0

Inlet

^0

/ 6 //^/^C

Outlet

^ f

1 0 .1 ^ 1l*-/^

0 0 1 5 1 1

Critical Orifice Calibration Data Sheet

Meter 4t 61 - ^ 1

Meter Yd i °IQ 8 I

Meter DH@ 1,6>~^^

ElapsedVolume Time Tn»i

^5,06 «««»««« 1^

^^ZS ^ 00

ô.S\ /^ <So^<oS.^8 ^ 1^

Full Test

Critical i

iOrifice U

A-lA-2A-3

Tmo

•78-181-11-1

Cal. Dati

Drfice Ca

Pbar ^y9,

sed (circ

0.61570.62820.6063

Tamb

»«»»3k««

^5ISns

B7- / ^ - 1

1 . Date /'

^L

Ie)

C-lC^2

<^L

DH

«»«*«««

.n•'n•^

^0-//-?/

0.4244—0<4l65

0.429^

Vacuum

«X««»«t

2ZZZ

^Z

(M^~-ins—00

Calibrated by


Meter f 6]

Meter Yd

Meter DH@

Run f

***

1

2

3

. - 2

0.9898

1.678

Volume

955.00

957.75

960.51

963.28

Run f

1

2

3

avg

C]

0:

ElapsedTime

*****

5.0

10.0

15.0

Vn std

2.68

2.69

2.70

Full Tes

ritical 0]

rifice Us'

Tmi

78

80

80

79

Vcr std

2.75

2.75

2.75

st Cal. C

rfice Cal

Pbar

ed ?

Tmo

78

78

77

77

Y

1.0255

1.0223

1.0177

1.0218

late - - 0

. Date 1

29.66

C-3

Tamb

***

75

75

75

Yd

0.9898

0.9898

0.9898

0.9898

7/18/91

0/11/91

0.4284

DH

*****

0.97

0.97

0.97

Diff

3.49%

3.18*

2.74»

3.14%

mT~

LOVacuum

***** 00

22.0

22.0

22.0


Meter ft 6

Meter Yd

Meter DH@

Volume

/n,^(13.-1-) 5-

1 1 ^ .1 1 ^ . 3 0 ^

1-JL/.<30?J-

/'&7&

ElapsedTime

^ »»!(;»»»«

s^ ^

Full Tes

Critical

Orifice

A-lA-2A-3

Tfni Tmo

-l^ ^

~\^ ^

^1 -^^

1-1 ^

t Cal. Date

Orfice Cal.

Pbar ^-6C»

Used (circle)

0.61570.62820.6063

Tamb

)KiK«»t*» U

1^ 11$IS

•?-r?-Date

C-lC-2

CC--3

DH

;«««»«

f<0

^0(.0

ll/o ->1-V

0.4244 < -0.4165 ,-0.4284J>

s—00

Vacuum

»«»»««»

^

2-^2^

Calibrated by


Meter t 6]

Meter Yd

Meter DH@

Run f

***

1

2

3

. - 6

1.0095

1.878

Volume

111.00

113.77

116.53

119.30

Run f

1

2

3

avg

Q

0]

ElapsedTime

*****

5.0

10.0

15.0

VB std

2.72

2.70

2.71

Full Tei

ritical 0;

rifice Usi

Tmi

74

76

77

77

Vcr std

2.75

2.75

2.75

st Cal. O

rfice Cal

Pbar

ed ?

TBO

74

74

74

74

Y

1.0105

1.0156

1.0124

1.0128

•ate - - 0'

. Date li

29.66

C-3

Tafflb

***>.

75

75

75

Yd

1.0095

1.0095

1.0095

1.0095

7/17/91

3/11/91

0.4284

DH

*****

1.00

1.00

1.00

Diff

0.10%

0.601

.0.291

0.33%

vacuua

***** (

22.0

22.0

22.0

70699133S5 CLEMt-1 AIR Et-lG. F-20Q T-0b5 P-002 OCT 09 •9l l?:08

DATE /.g////?^ _ PITOT NUMBER ^'/V-^-/

TYPE S PITOT TUBE INSPECTION DATA

Pitot tube assembly level? \^/~ yes ____ no

PitOt tuce openings damacec? ___ yes (explain below) f^^^no

a , = ^"a KIO0), <r, = ^/ " «10°)/ pi - ^ " «5°)

Y = / /. 9 = 3 A - ^7<?0 en (in.)

2 " A sin X • .o^ cm (in.); < 0.32 era « 1/8 in.),

W = A sin 0 » W1 cm (in.); < 0.08 cm « 1/32 in.)

p ,3^>^_______ era (in.) P^ f'3>^ /______ en (in.)

P » t'a - Pb ) . .2

Dt « 4o?*==>0 cm (in.)

JL. = /.4/ 0 1 .05 &nd < 1.50)

COMKEHTS; r'TQT W) •= , &<^

Calibration required? _____ yes

Calibrated by: -^f^C^ •_____

Dace: _ 5^-5/Q?_____ Pitoc Number.: (?5^3.»

»TYPE S PITOT TUBE'INSPECTION DATA

Picoc cube asceobly levelt ^_ye« ____no

Pitoc tube openings daaaged? __ yes (explain below) ^r no

ai - 2 ° (<10-). a, - JL* «10*), 81 - 3 * «5')

) P» - JL* ^5')

Y-^'. 9'-^..A-,7^M (lo.).' * * '

Z •• A sin Y -,^2^c» (in.); <,&a52-»-«l/8 in.),

W - A tto Q - > 02^ c» (in.); < 0.08 en «1/32 In.)

? -. 0 — (In.) Pv .305 c« (in.)A ~—" D "————'

• /^D. - -Jl O ft» (in.) -f - .^——=W . <^1.05 »nd&1.50)' • -t 'vSp^" ,.

i •

COMMENTS: ^ •?/»bg-^__________________

Calibration required? ___ yes lo^no

CalilMted T»y: . ^^/îf^

Nozzle Calibration Data Sheet

Date: \0-^-^\

plant: JA>C-^SO^JLH>

Înit Number A/A-

Calibrated By

• -re-R/-i> Tg^y /'/k^Buns.

NozzleIdentification

.w

.~L^

^1

.1^

D1(inches)

.2?'?

.Z-

.W

.2^

D2(inches)

,2^

.W

.1^-1

.^^

D3(inches)

,m

.^

.ZfS

.W

D4(inches)

.Z^

•Z^

.2^1

,Z^^

AD(inches)

,000

,00 t

.00 1

, 000

ADavg(inches)

W

.2^

^^

^^

Where:

01 ,D2,D3,D4 = tour nozzle diameter measurements

AD maximum difference between anytwo diameters AD < 0.004 inches

average of D1 ,D2,D3,D4ADavg

<—D3


WEIGHT SHEETS

~OC Project # 58151

VaBIOH SHEET # 1 AS ENTERED

^ R R W F

O U T B WASH

5 N t IDENTIFIER T ML CCBR. GROGS TAPE NET*****************************************************************************

1 BLUK B 100 0.0000 100.0108 100.0108 0.0000

06 TOP-1 2 Kl B 125 0.0000 105.0124 105.0100 0.0024

07 TEP-2 3 G28 B 125 0.0000 107.8943 107.8926 0.0017

08 TOP-3 4 T14 B 150 0.0000 105.4653 105.4640 0.0013

06 TOP-l 5 90062 F —— ——— 0.3806 0.3766 0.0040

07 TOP-2 6 90063 F —— ———— 0.3799 0.3749 0.0050

08 TOP-3 7 90064 F —— ———— 0.3785 0.3744 0.0041*****************************************************************************

CBE Project • 58151

^T.T. WEIGHTS SORTED BY RDS

R R S W F

D U H T B TOSH

5 N t * JEBmSTS. T ML OCBR. GROGS TftBE tCT' *****************************************************************************

1 1 BLANK B 100 0.0000 100.0108 100.0108 0.0000

06 TBP- 1 2 Kl B 125 0.0000 105.0124 105.0100 0.0024

06 THP- 1 5 90062 P —— ——— 0.3806 0.3766 0.0040

DOS TOTOL 0.0064

07 TOP- 1 3 G28 B 125 0.0000 107.8943 107.8926 0.0017

' 07 TOP- I 6 90063 F —— ——— 0.3799 0.3-749 0.0050

FOS TOaL 0.0067

08 TOP-1 4 T14 B 150 0.0000 105.4653 105.4640 0.001308 •IEP- 1 7 90064 F —— ——— 0.3785 0.3744 0.0041

RDS TOOM. 0.0054

1 8 BO - —— ——— 0.0000 0.0000 0.0000. *****************************************************************************

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FIELD DATA

Orsat Readings Page. of

Client cPlant ^^co^vi /(e- A f^.Date /0 -^-?<Orsat ID

Project NumberUnit -Fuel TypeLeak Check? \^

20.9-%02Fo = ——————%C02

Fo= 1.083 to 1.230(for bituminous coal)

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Project Number T^cT- (UnitFuel Type w^s-ri.Leak Check? o (<i

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/<A/. 0 :10

Ctond,Temp.

A

^y^/at/^^6>^^^sa^3^^

.^^5^6 1

Ambient Temp. (°F) Bar. PreiL (in. Hg)A»umedMoi<ture(%)

Heater BoKSeltinc


IGS Bag ID Number%02H20(ml)Total V|c

StartTimc AM/PMJ StopTimc ). 7 AM/PMJ

raterTemp.

(%o?6^

ss^5^7^6(&

Ar6as" <'aâ^-?^6A^-l-2 .

ftobcTe^(

.?JJ

y^

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S^Q

ot^d</9

w<a<^7^<\w

Probe Heater Settiflf

Acetone Number

%C02Silica Gel (zm)

Noro»H>——iS———————————————————————

^L\—————^-z-5b$A^^Z^^6^

^^(.(6.S-

cr. 1-0ata-1 0 0 1 5 4 7


FIELD DATA PRINTOUTS

RAW DA-rA SET # 3

1 ) 12 ) 1

3 ) <

4 ) 1

5 ) 1

6 )

7 ) 1

8 ) 1

9 )10 )

11 )12 )

13 )

14 )

15 )

16 )

Pt. I*****

0 - C

A-1

A-1A-2

A-2

A-3

A-3

A-4

A-4

A-5

A-5A-6A-6

A-7

A-7

A-8

A-8

A-9

PlantLocatio

^perato

tote

RunNb.

Sanple

Meter E

Meter

KFactc

Pitot

leak?

Lsakf

Static

ftnbier

Barott

Assixne

t 0;******!

>

5

5

5

5

5

5

5

5

5

5

55

5

5

5

5

5

n

r

BoxN

OK N3

H@

ir

FactctateE

tate;

; Pres

it Ten

Aric

sdfrbj

Vac,»****<

4

4

5

5

5

5

5

5

5

5

55

5

57

7

7

b.

1.

ir

tefore

LCter

>., InH

peratur

Pressur

Lsture,

, TSk*******

203

202

202

200

202

203

203

203

201

200

200203

203

204

202

201

201

•raaUMT

A. I

10/!

ro-

61-<

1.8-

2.e0.8

0.0'

0.020 0.6

e 75

e 30.

% 40

DP3:*******

0.30

0.30

0.28

0.26

0.25

0.32

0.32

0.34

0.32

0.32

0.320.34

0.44

0.45

0.55

0.63

0.59

ocuvmr i saacXDGA

9/91

1

6

780

0

4

02018

03615

0

04

DH*******i

0.78

0.78

0.730.67

0.65

0.83

0.83

0.88

0.83

0.83

0.830.88

1.10

1.20

1.40

1.60

1.50

E, AR. 17

X 18 )

19 )

20 )

21 )

22)

23)

2 4 )

25 )

26)27 )

28 )

29)

30)

31 )

32 )

\ta»*********

665.65

668.00

670.40

672.74

675.02

677.25

679.73

682.20

684.77

687.25

689.73

692.19694.77

697.50

700.35

703.50

706.80

710.13

) Heat

Probe

N&zzle

Probe

t02

%002

Ml. H2

GM. SJ

Total

Start

Finid

Yd.

StackSanpU

mitiiFund

ItalJr******]

79

80

81

81

81

81

81

81

81

81

8181

82

82

82

83

84

.er Box

Length'

\ Diamet

Heater

SO

LLLcaGE

Tinei Time

Area

Ing Time

ilVblui

\& BEU

l 'SnoutMHHHHHkl

78

79

78

78

78

78

78

78

78

77

7777

77

77

78

77

78

Sett

,' F

W,

Sett

tl

> (MI

ne

CEKI

'tt;Infc'JrifrA

50

50

50

5147

45

5147

43

43

4650

46

45

46

49

48

tog

t.

'm.Ing

N/PT)

•S

Ttor*****i

250

247

268

262

255

251

245

255

251

249

252253

250

256

256

252

249

0.288

10.8

7.4

2109.0

38.5

2147.5

2:26 PM

6:35 EM

1.0095

9.60

5

665.65

tl*********

A. NOGA

100.1

102.0

102.9

103.9

103.8

102.1

101.7

102.7

102.0

102.0

101.2103.2

96.0

99.2

98.9

96.8

100.7

78 49 252 99.878 47 254 101.278 46 252 99.578 48 249 97.778 51 256 99.378 53 252 100.478 57 250 99.6

78 53 253 98.879 53 254 99.678 46 253 99.478 48 251 98.878 51 251 97.978 52 251 100.578 54 252 101.478 56 252 97.678 60 252 97.678 64 254 99.279 60 251 95.578 58 251 102.378 53 250 106.978 50 250 106.178 50 250 108.178 51 250 108.579 53 250 98.079 55 252 103.678 54 251 103.978 53 256 99.678 53 250 107.778 49 249 105.278 49 250 104.578 49 249 107.3

A-9A-10A-10A-llA-ll

A-12A-12

IEAKCKB-12B-12

B-ll&-11B-10B-10B-9B-9

B-8B-8B-7B-7B-6

B-6B-5B-5B-4

&-4

&-3&-3B-2B-2B-lB-l

5555

5

55

555555555

555

55555

5555555

77

877

77

7777777

7

8888776

66

6666666

201202200201202

203203

200200203203202201200199200201201202

200201201201202

202

201200200200201200

0.580.600.660.630.60

0.600.58

0.500.500.510.510.540.540.52

0.550.580.580.550.58

0.450.420.370.370.38

0.350.310.34

0.310.310.310.31

1.501.601.701.601.60

1.601.50

1.301.30

1.301.301.401.401.401.401.501.501.401.501.201.100.960.960.99

0.910.810.880.810.810.810.81

713.40716.77

720.25723.59726.90730.24

733.50

733.75736.75739.78

742.83745.86748.95752.13755.28758.40761.60

764.85767.90771.25774.34777.30780.13782.97785.57

788.21

790.70793.20795.78798.30800.80803.37

84848485858484

8081

8383838484848484

8484

8483838383

83828281818181

********************************************************************************

240 201 .659 1.15 137.47 80Total ftvg. Root Avg. Vbtune Avg.

RAW DA3CA SET # 4

1 ) 12 ) ]3 ) (4 ) 15 ) I6 ) i7 ) 1

8 ) 19 ) 11 0 )

11 )12 )

13 )14 )15 )1 6 )

Pt. 1*****

0 - C

A-1A-1A-2A-2A-3A-3A-4A-4A-5

A-5A-6

A-6A-7

A-7

A-8A-8

PlantLocatioDperato3ate

amito.Sanple»teterB

(feter

KFactcPitot

LaakF

LeakFStaticftrbier

BarcrreASSUtIlE

0'it'ltli'lv'ltiti

i

555555555

55

55

555

nr

BcocNOX MS

H!irFactc

late Eate f

; Presit Ten

•trierittoj

Vac,

445555555

55

57777

(0.

i.

>r

teforeLfter

>., Int

peratuiPressmLstura,

. T8

201200201201199199201201200

199198199202202

200200

JB3QWTS

A. N:

10/K

TB-2

61-61.67)

2.600.84

0.00!0.00

120 0.60

» 75» 30.0% 42

DPS 1

0.300.300.350.34

0.310.320.350.400.42

0.380.400.430.55

0.580.64

0.66

wmi1 SSfC

X3A

)/91

30

5817

2815

0

DH

0.780.780.910.880.810.830.911.001.10

0.991.001.101.40

1.501.701.70

E, AR. 17

X 18 )

19 )20 )

2 1 )22 )

23 )24 )25 )26 )

27 )

28 )29 )

30)31 )32 )

Vte

803.81

806.20808.58811.15813.73816.21818.69821.13824.00826.76

829.51832.26835.00838.18841.36844.80848.21

) HaatPrcbeNozzlePrcbe»02% 002

Ml. H2

CM. SlTotalStart

Finish

Yd.

StadcSarrpU

Initi<FH3EE

'Bnii

818182838486858687

878787

8888

8990

er Boxlength'iDlamet

Heater

0•lica Ge

Tims

i Tine

Area

[ng Tire

>lV3lin< & BEAT

1 'StOUt

808080808181818282

82828282

82

83

83

Sett

»' Fer«,Sett

il

) (MIB

ER*

'Ita

57

5353534444455253

4747

4851

5355

58

ingb.•m.ing

N/PT)

'S

•Ib

263256257258258254253254253

255254255255254254257

0.288

11.17.92149.037.52186.510:44 AM

3:03 EM1.00959.60

5803.81

%!

A. NOGA

101.6101.1101.1102.9103.2101.495.6105.198.5

103.0100.396.599.396.7

99.396.8

A-9A-9

A-10

A-10

A-ll

A-ll

A-12

ft-12

IEAK

B-12

B-12

&-11

B-ll

B-10

B-10

B-9

B-9

B-8

B-8

B-7

B-7

B-6

&-6

&-5

B-5

B-4

&-4

B-3

B-3B-2

&-2

B-l

B-l

55

5

5

5

5

5

5

CK

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

7

8

7

7

7

7

7

7

6

6

6

6

6

6

7

7

7

7

7

7

6

6

6

6

6

6

6

6

6

6

5

5

201202

202

202

199

199

200

200

201

202

202

200

199

201

202

202

201

200

199

202

202

202

199

199

201

202

202

200

200

200

201

201

0.660.68

0.64

0.64

0.66

0.66

0.66

0.59

0.48

0.48

0.50

0.50

0.50

0.48

0.52

0.52

0.54

0.50

0.40

0.40

0.40

0.40

0.38

0.40

0.38

0.35

0.34

0.35

0.31

0.31

0.25

0.25

1.70

1.80

1.70

1.70

1.70

1.70

1.70

1.50

1.25

1.25

1.30

1.30

1.30

1.25

1.35

1.35

1.40

1.30

1.00

1.00

1.00

1.00

0.99

1.00

0.99

0.91

0.88

0.91

0.81

0.81

0.65

0.65

851.66855.20

858.75862.27

865.80

869.39

872.90

876.28

876.61

879.45

882.32

885.20

888.15

891.14

894.10

897.15

900.24

903.43

906.47

909.28

912.05

914.80

917.55

920.30

923.05

925.77

928.40

930.96

933.61

936.10

938.57

940.88

943.13

9090

9191

91

91

91

92

83

87

88

89

89

90

90

90

90

91

91

90

90

90

90

90

89

89

89

89

89

89

88

87

8484

84

84

84

84

85

85

84

84

84

84

84

85

84

84

85

85

85

85

86

86

86

86

85

85

86

85

85

85

85

84

6058

60

60

60

58

55

55

62

46

49

53

57

46

45

46

52

56

59

4952

53

55

55

57

58

58

50

49

53

54

56

259

263

257

256

254

255

255

256

245

258

254

256

255

257

255

252

256

254

258

250

249

251

255

254

253

253

253

256

254

255

252

253

97.999.1

102.3

101.5

100.0

101.7

99.4

101.1

95.0

95.8

94.1

96.1

97.4

98.3

97.5

98.8

100.0

98.8

102.0

100.8

100.0

100.0

102.4

99.8

101.6

102.4

101.0

103.0

102.8

102.0

106.4

103.8

********************************************************************************

240 201 .668 1.18 138.99 86

Total Avg. Root Aug. Volixre Asg.

RAW DA3A SET # 5

1 ) E2 ) I

3 ) C

4 ) I

5 ) F

6 ) ;

7 ) t

8 ) ^

9 ) i10 )

11 )

12 )

13 )

14 )

15 )

16 )

Pt. #*****

0 - 0

A-12

A-12

A-11

A-11

A-10

A-10

A-9

A-9A-8

A-8

A-7A-7

A-6

A-6

A-5A-5

ft-4

•lant

Jocatio

ferato

late

tun No.

Sanple

tetexE

teter

(Factc

Pitot

Leakf

Leakf

Static

fttbier

Barone

Assure

0*******

5

5

5

5

5

5

5

55

5

5

5

5

5

5

55

n

r

BoxM

OOtMC

H9>r

Eactc

ate I

<atel

-.Pres

it Ta

»tric

)dM3:

Vacir****;

6

6

6

7

7

7

7

77

7

7

7

7

7

7

77

to.

).

>r

tetore

tfter

i.. In l

rperafcul

Pressm

Lsture,

. Tsk******i

204

204

202

201

202

203

203

203202

200

203

203

203

202

201

202202

JB3

UNT]

B. I

10/:

•1B-;

61-1

1.8-

2.61

0.8.

0.0:

0.0'

120 0.8

» 80

•s 29.

« 43

?3k*******

0.54

0.54

0.56

0.56

0.60

0.54

0.550.520.54

0.65

0.52

0.50

0.36

0.36

0.34

0.34

0.36

saivmr i sacTmczana11/91

?

5

7803

4

12815

03613

0

66

DH*******!

1.40

1.40

1.40

1.40

1.56

1.40

1.40

1.351.40

1.70

1.35

1.30

0.94

0.94

0.88

0.880.94

E, AR. 17

K 18 )

3 19 )

20 )

21 )

22 »

23 )24 )

25 )

26 )

27 )

28 )

29)

30 )

31 )

32 )

\tak*********

968.67

971.80

974.77

977.87

981.00

984.16

987.48

990.55

993.70996.86

1000.25

1003.18

1006.55

1009.37

1012.00

1014.60

1017.141019.77

) Heat

Prdbe

Nozzle

Prcbe

» 02

» 002

Ml. fC

04. SJ

Total

Start

Ftnisi

Yd.

Stack

Sanpl;

miti.FTT.'ni'l

ItalJ******

74

77

79

81

82

82

82

8282

82

83

83

82

82

82

81

80

.er Box

Length'

» Dianet

Heater

!0mr^ Ge

Tine

i Time

Area

Ing Tlni

il VOllXl

9.& •BEN

(i ibout*******!

74

74

74

75

75

75

75

7676

76

76

76

76

76

77

77

76

Sett

,' P

er',

Sett

il

1 (MI

ne!ER j

TCii***«

65

55

59

61

62

64

65

5960

60

62

60

59

58

58

60

62

Ing

t.

'Bl.

ing

N/PT)

.'s

Ibr*****4

B. E

253

267

268

268

270

272

271

273272

270

272

272

272

273

273

271

271

0.288

11.0

7.5

2109.4

36.02145.4

3:42 PM

8:10 EM

1.0095

9.60

5

968.67

%!i********

SYCZUBKI

99.1

93.7

95.8

96.4

94.0

104.1

95.4

100.699.0

96.7

93.5

109.6

108.1

100.7

102.3

100.1

100.9

A-4

A-3

A-3

A-2

A-2

A-l

A-l

LEKKCK

B-l

B-l

B-2B-2

B-3

B-3B-4

B-4

&-5

B-5

B-6

B-6

B-7

B-7

B-8

B-8&-9

B-9

B-10

B-10

B-ll

B-ll

B-12

B-12

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

7

7

7

7

7

7

7

6

6

6

6

6

6

7

7

7

7

9

9

9

9

9

9

9

9

9

9

9

9

9

9

203

203

201

200

201

203

202

203

202

200

200

202

203

203

202

201

200

202

203

203

202

201

201

201

203

202

200

200

202

203

202

0.36

0.33

0.30

0.30

0.30

0.28

0.30

0.30

0.30

0.30

0.30

0.30

0.30

0.34

0.37

0.37

0.37

0.59

0.59

0.59

0.59

0.57

0.53

0.55

0.55

0.53

0.53

0.53

0.53

0.53

0.53

0.94

0.86

0.78

0.78

0.78

0.73

0.78

0.78

0.78

0.78

0.78

0.78

0.78

0.88

0.96

0.96

0.96

1.50

1.50

1.50

1.50

1.50

1.40

1.40

1.40

1.40

1.40

1.40

1.40

1.40

1.40

1022.39

1024.90

1027.34

1029.76

1032.16

1034.52

1036.98

1038.10

1040.80

1043.27

1045.75

1048.20

1050.62

1053.04

1055.71

1058.43

1061.24

1064.02

1067.31

1070.68

1074.03

1077.44

1080.79

1084.12

1087.39

1090.68

1094.00

1097.22

1100.42

1103.61

1106.75

1110.08

81

81

81

80

80

80

80

7577

78

78

79

79

79

79

80

80

80

81

82

82

82

82

83

83

83

83

83

83

83

82

77

77

77

77

76

77

77

76

76

75

75

75

75

75

75

75

75

75

75

75

76

76

76

76

76

76

77

77

77

77

77

63

62

65

63

60

61

65

60

58

54

54

57

61

66

66

63

56

51

50

52

53

51

51

52

50

49

51

55

59

64

65

272

273

260

260

254

255

257

264

263

251257

249

257

264

259

258

255

262

259

20.

258

256

255

255

254

256

255

254

255

256

253

100.4

100.5

102.3

101.5

100.8

102.6

103.3

114.1 *

104.1

104.4

103.1

101.9

102.0

105.7

103.2

106.4

105.2

98.9

101.2

100.6

102.2

102.1

105.2

101.3

102.1

104.8

101.4

100.8

100.6

99.1

105.2

240 202 .664 1.16 140.29 78

Total Avg. Boob Aug. Volucre Aug.

EMR UR fRE«

RSiW DMTA SET # 6

1 ) Plant

2 ) Location

3 ) Operator

4 ) Date

5 ) Bun No.

6 ) Sanple Box No.

7 ) Meter Box No.

8 ) Meter H@

9 ) K Factor

10 ) Pitot Factor

11 ) Leak. Bate Before

12 ) Leak Bate After

13 ) Static Pres., in H20

14 ) Arbient Temperature

15 ) Barometric Pressure

16 ) Assumed Moisture, %

JaCKSCNVILUB,

UNIT 1 SOCK.

J. WEES.

10/9/91

TBP-1

61-2

1.6780

2.30

0.84

0.007816

0.00487

0.60

85

30.04

40

AR. 17 ) Heater Box Setting

18 ) Probe Length',' Ft.

19 ) Itozzle Dianeter'.'m.

20 ) Probe Heater Setting

21 ) % 02

22 ) % 002

23 ) Ml. H20

24 ) 01. Silica Gel

25 ) Total

26 ) Start Time

27 ) Finish Time

28 ) Yd.

29 ) Stack Area

30 ) Sanpling Tine (MIN/PT)

31 ) Initial Volune

32 ) FTT.TTO & BEAKER #'S

90062P

0.288

10.9

7.8

484

18

502

3:38 PM

5:15 PM

0.9898

9.60

2.5

711.94

KLB

Pt. * 0 Vac. TS DPs DH Vtn 'Dn in 'Dnout TC 1b %I********************************************************************************

0 - 0 711.94 J. WEBER

B-l

B-2

B-3

B-4

B-5

&-6

B-7

B-8

Br9

&-10

B-ll

B-12

IEAK

A-l

A-2

A-3

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.5

OK

2.5

2.5

2.5

2

2

2

3

4

3

4

4

44

4

3

3

3

3

203

202

202

202

203

205

205

204

204203

202

202

204

204

204

0.32

0.33

0.35

0.37

0.42

0.45

0.530.57

0.55

0.55

0.50

0.46

0.33

0.30

0.36

0.736

0.759

0.803

0.851

0.966

1.035

1.219

1.311

1.265

1.265

1.150

1.058

0.825

0.750

0.900

713.21

714.47

715.49

716.73

718.05

719.40

720.87

722.38

723.90725.42

726.80

728.15

728.23

729.50

730.64

731.95

73

73

75

76

77

78

79

80

80

81

82

81

77

77

78

72

72

73

73

73

73

74

74

75

75

75

75

76

76

77

56

56

52

50

54

60

63

65

65

65

65

64

65

52

52

259

253

251

250

250

251

252

258

261

252

253

252

256

258

257

102.8

100.4

78.7 *

93.0

92.9

91.9

92.0

91.0

93.2

93.0

88.4 *

90.2

100.6

94.7

99.2

A-4 2.5 3 205 0.32 0.800 733.16 79 76 50 255 97.2A-5 2.5 3 205 0.76 0.900 734.47 81 77 50 259 68.1 *A-6 2.5 3 204 0.35 0.875 735.74 81 77 51 256 97.2A-7 2.5 3 202 0.42 1.050 737.09 81 77 52 258 94.3A-8 2.5 4 203 0.57 1.425 738.62 82 77 52 258 91.8A-9 2.5 5 202 0.65 1.625 740.31 83 77 52 258 94.8A-10 2.5 5 202 0.67 1.675 741.98 84 78 53 257 92.1A-11 2.5 5 202 0.55 1.375 743.58 84 78 54 255 97.3A-12 2.5 5 201 0.60 1.500 745.16 84 78 57 258 92.0

********************************************************************************

60 203 .679 1.09 33.14 77Total Avg. Root Avg. Volute Avg.

RAW D2VTA. SET #

1 ) I

2 ) ]

3 ) <

4 ) 1

5 ) 1

6 ) l

7 » 18 ) 1

9 ) 1

10 )

11 )

12 )

13)

14 )

15 )

16 )

Pt. 4

0 - 0

B-1

B-2

&-3

B-4

&-5

B-6

B-7

B-8B-9

B-10B-11&-12

I£RK

A-l

A-2

A-3

A-4

Plant

Locatior

^pexabol

Sate

Run No.

Sanple I

Meter BeMeter I

KFactoi

Pitot I

LeakR

IsakR

Static

Atbieri

Barcnel

Assure

0

>

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.52.5

2.52.52.5

CK

2.5

2.5

2.5

2.5

l

30X1

«N

iS

r

i'acto

»te

ate,

Pre

: Te

:ric

1MO

Vac

22

2

2

2

2

2

22

222

2

2

2

2

N0.

0.

or

Before

After

s., in I

nrperatu]

pzessw

isture,

i. TS

203203

203

203

202

201

202

201202

202202203

202

203

203

204

sawr.B. I

10/:

TBP'

61-1.6

2.5

0.8

0.0

0.0

CO 0.4

re 70

re 30.

% 43

DPs

0.350.38

0.40

0.42

0.45

0.50

0.60

0.650.60

0.550.550.60

0.27

0.32

0.32

0.32

OCNVIU

r l SIK.aaczaiaLO/91

-2

2

780

0

4

10617

00810

0

00

DH

0.87

0.95

1.00

1.05

1.12

1.25

1.501.621.50

1.37

1.371.50

0.68

0.80

0.80

0.80

E, AR. 17

X 18 )

CT 19 )

20 )

21 )

22 )

23 )24 )

25 )

2 6 )

27 )

28 )

29 )

30 )

31 )32 )

Vta

748.58

749.85751.15

752.54

753.89

755.33

756.79

758.37

760.10761.73

763.27

764.82766.40

766.51

767.65

768.83

770.05771.27

) Heat

ProbeNozzlfPrcbe

« 02

% 002

ML. ffiQA. Si

Total

Start

Finisi

Yd.

Stack

Sarrpl-

mitiiFTT.TTJ

900631

•Itati

7879

80

81

83

84

85

8688

88

8889

85

85

86

86

sx. Box

Length'»Diarret

Heater

0LLLca Ge

TJire

\ Tine

Area

Ing Tint

il VOlUl

9. 6 BENp

a 'Dtiout

78

78

78

78

78

79

79

8080

80

8081

83

82

82

83

Sett

,' F

•er',

Salt

a

i (MI

•e

CT.1

Tc

6865

62

59

56

54

535456

5657

58

66

65

62

63

Ing

t.

'm.ing

N/PT)

t'S

Tb

B. !

249253

252

254

252

258

252

254258

258

255254

257

261

258257

0.289

10.7

7.5

520.5

11.5

532.0

12:13 BM

1:35 PM

0.9898

9.60

2.5

748.58

G28B

%!

SKZWSKI.

97.095.2

99.1

93.9

96.5

92.6

91.5

96.194.1

92.8

93.491.1

97.9

93.2

96.3

96.3

A-5 2.5 3 204 0.34 0.85 772.56 87 83 63 257 98.7A-6 2.5 3 203 0.36 0.90 773.84 87 83 65 254 95.1A-7 2.5 3 202 0.50 1.25 775.33 89 83 65 256 93.8A-8 2.5 4 201 0.60 1.50 776.95 89 83 63 257 93.1A-9 2.5 4 201 0.60 1.50 778.59 90 84 63 256 94.1A-10 2.5 4 201 0.60 1.50 780.24 90 84 64 258 94.6A-11 2.5 4 202 0.53 1.30 781.85 91 84 66 255 98.2A-12 2.5 4 203 0.53 1.30 783.42 91 85 67 256 95.7

********************************************************************************

60 202 .682 1.18 34.73 84Total Aug. Boot Aug. Volume Avg.

RW7 EUÊA. SET * S

1 ) I2 ) 1

3 ) (

4 ) I

5 ) 1

6 ) i

7 ) 1

8 ) 1

9 ) 1

10 )

1 1 )12 )

13 )

1 4 )

15 )16 )

Pt. ******

0 - 0

A-1A-2

A-3

A-4

A-5

A-6

A-7

A-8A-9A-10

A-11

A-12

I£ftK

B-1

B-2

B-3

B-4

?lant

location

;peratox

Data

ûnNo.

Saiple E

teterBc•teter t

KE-actoi

Pitot E

leak Re

Leak Re

Static

fttbient

BaronetAS81XIBC

0*******;

2.5

2.5

2.5

2.5

2.5

2.5

2.5

2.52.52.5

2.5

2.5

CK

2.5

2.5

2.5

2.5

>

loxlocit

18

âcti

>te I

He;

Pee

; Ta

;rlc

I Wo

vac•i***

22

2

2

2

2

2

222

2

2

2

2

2

2

to.

3.

or

Before

ftfter

s., inH

.iperatui

Pressm

isture,

i. Ts*******i

200

200

200

201

203

203

204

204204203

203

202

202

202

203

203

3ICK

wnB. E

10/1:

•IBP-:

61-2

1.67)

2.50

0.84

0.011

0.011

20 0.60

B 70

e 29.64 42

DP3 1;********

0.30

0.30

0.25

0.30

0.34

0.34

0.56

0.620.560.52

0.52

0.50

0.30

0.30

0.32

0.35

30NVIU

1 SOC

a3ac»L/91

?

30

3818

0@l5

6

DH******i

0.75

0.75

0.62

0.75

0.85

0.85

1.401.55

1.401.30

1.30

1.25

0.75

0.75

0.80

0.89

E, AR. 17

K 18 )

I 19 )

20 )

21 )22 )

23 »

24)

25 )

26)27 )

28 )

29)

30 )

31 )32 )

Vtalf********4

784.19

785.48

786.63

787.53

788.93

790.18

791.48

792.90

794.56796.21797.70

799.23

800.70

801.30

802.49

803.70

804.95

806.22

) teat

Prdbe

Nozzle

Prdbe

% 02

t 002

Ml. ffi

W. SJ

Total

Start

Finisi

Yd.

Stack

SanpL

miti-ETLrH

900641

TinlJr******

79

7879

81

83

83

84

868787

87

87

81

82

82

83

.er Box

Length'» Diarret

Heater

20

LlicaGe

Tine

i Tine

Area

ing TinealVblua

K & BEAf

?

a Incut.*******!

7878

78

78

79

79

79808081

81

81

82

82

81

81

Sett

,' B1

er\

Sett

0.

» (MI

fi

SR9

TCk***«

6870

61

58

55

55

55

555557

57

57

70

64

S3

60

ing

b.

'm.Ing

N/PT)

•S

ib:*****

B. ;

260262

257

257

256

257

259257

254256

255

254

256

255

259

260

0.289

10.9

7.9464

8

472

1:01 m.2:07 EM

0.9898

9.60

2.5

784.19T14B

»!*********

BKZ2NSKI

103.492.2

79.0 *

112.0 *

93.9

97.6

83.2 *

92.2

96.390.1

92.5

90.5

95.0

96.5

96.7

93.8

B-5 2.5 2 204 0.40 1.00 807.60 63 80 55 263 95.68-6 2.5 3 204 0.44 1.10 809.01 83 80 54 259 93.1B-7 2.5 3 205 0.45 1.20 810.47 83 80 52 257 95.4B-8 2.5 3 204 0.45 1.20 811.99 84 80 53 258 99.2B-9 2.5 3 203 0.45 1.20 813.49 83 79 53 259 98.0B-10 2.5 3 203 0.44 1.10 814.97 84 79 54 257 97.7B-11 2.5 3 202 0.32 0.80 816.20 84 79 56 256 95.0B-12 2.5 3 201 0.30 0.75 817.42 83 79 57 255 97.4

********************************************************************************

60 203 .628 1.01 32.63 81Total Avg. Boot kvg. Volute Avg.

RAW DAZCA. SET ^ 9

1 ) 12 ) :3 ) (

4 ) 1

5 > 16 ) ,7 ) 18 ) i

9 ) :10 )

11 »12 )13 )14 )15 )16 )

Pt. I*****

0 - C

B-1B-1B-2B-2

B-3

B-3D-4B-4

B-5

B-5B-6B-6

B-7

B-7B-8B-8B-9

Plant

Locatio^perato

DateRun No.SarpleMater EMeter

KEactc

PitotLaakF

LeakFStaticAlbierBaroneASSUIE

^ 0r*******

»

555

555555

5555

5

555

n

C

BoxNOXNC

HQ

»r

EactclateEtateJ!: Prosit Ten»trlcidMDJ

Vac,frtfrAifrAi

333444555

555

5

6666

to.

i.

irleforeifteri., InHperaturPressur

Lsture,

, Ts^*******

201201204205

205204202204205

205204

205202

203205205204

JVCKUNITA. Nt

10/13

TB-4

61-21.671

2.50

0.840.011

0.00-20 0.806 75e 29.6« 42

?3 :rlHHHHHH ifr

0.300.300.280.31

0.350.350.390.380.37

0.390.44

0.430.53

0,550.590.550.53

owmi sac.

X3A

L/91

30

3817

1615

6

DH"(HHHk<H i

0.750.750.730.780.870.870.960.950.93

0.981.101.10

1.30

1.40

1.501.401.30

E, AR. 17

X 18 )19 )

20 )

21 )22 )23 )24 )

25)

26 )27 )

28 )29 )30)31 )32 )

Vta**********

818.00

820.40822.83825.15827.60830.13832.73835.45838.10840.75

843.50846.24

849.00

852.10

855.15

858.43861.74864.97

) HeatPrctaNozzle

Probet 02t 002ML. H204. SJ

Total

StartFinidYd.StackSairpU

InttiiFILIEI

Toil•******i

747578808181828283

838484

8384

858585

er Box

Length'iDlan-Bt

Heater

0Ufa. Qa

Tinei Tima

AreaIng TimeilWhxii6 BEAfl

l 'Snout»******4

747374

757576767677

7777

78

78

78787879

Sett

»• E1er«,

Setfc

1

i (HIB

XR <

TCt****

626064

555455575858

595254

57

57

596060

ing

t.•Hi.

ing

N/PT)

•s

•tt)•*****i

259253259252260

256254253261

261262

261

249

253

261259264

0.287

11.07.1

20993621353:27 PM8:10 PM0.98989.605818.00

IIItititlt^t^t^t^dt

A. NOGA

101.2102.5101.1

101.398.4

100.999.898.699.9

100.994.6

96.397.4

94.1

97.7102.1101.3

D-9 5 6 203 0.53 1.30 868.17 87

&-10 5 5 203 0.40 1.00 871.10 85

B-10 5 5 204 0.40 1.00 873.92 85

B-11 5 5 205 0.38 0.95 876.72 85

B-11 5 5 205 0.38 0.95 879.50 85

B-12 5 5 203 0.40 1.00 881.74 85

&-12 5 5 202 0.40 1.00 885.11 85

I£AK CK 885.30

A-12 5 6 204 0.45 1.10 888.22 78

A-12 5 6 203 0.48 1.20 891.23 80

A-11 5 6 202 0.50 1.30 894.29 82

Aril 5 6 202 0.54 1.40 897.48 82

A-10 5 6 203 0.52 1.30 900.65 84

A-10 5 6 204 0.55 1.40 903.80 85

A-9 5 6 205 0.56 1.40 906.95 85

A-9 5 6 205 0.56 1.40 910.10 85

A-8 5 6 202 0.64 1.60 913.40 85

A-8 5 6 203 0.60 1.50 916.77 85

A-7 5 6 204 0.45 1.10 919.77 86

A-7 5 6 205 0.44 1.10 922.73 86

A-6 5 5 205 0.40 1.00 925.58 85

A-6 5 5 205 0.40 1.00 928.44 85

A-5 5 5 202 0.35 0.87 931.07 84

A-5 5 5 202 0.35 0.87 933.65 83

A-4 5 5 202 0.38 0.95 936.36 84

A-4 5 5 204 0.38 0.95 939.06 84

A-3 5 5 204 0.34 0.85 941.58 84

A-3 5 4 202 0.30 0.75 943.88 83

A-2 5 4 201 0.30 0.75 946.28 83

A-2 5 5 203 0.34 0.85 948.85 83

A-1 5 5 204 0.34 0.85 951.47 84

A-1 5 5 204 0.34 0.85 953.90 84

79 58 264 100.1

79 55 261 105.7

80 56 262 101.7

79 55 264 103.7

79 55 259 103.0

79 54 263 80.8 •»

80 57 262 121.3 *

77 54 262 100.277 53 258 99.877 54 258 99.177 55 257 99.5

78 55 258 100.5

78 55 257 97.1

78 56 261 96.3

78 57 257 96.3

78 57 258 94.2

78 55 256 99.4

78 55 259 102.1

78 53 260 101.979 54 262 102.9

79 48 259 103.3

78 46 257 101.5

78 46 256 99.6

79 46 256 100.3

78 48 256 100.1

78 52 256 98.8

78 53 256 95.9

78 54 257 100.0

80 57 256 100.6

79 59 257 102.6

79 61 256 95.2

********************************************************************************

240 204 .649 1.07 135.71 80Total Aug. Boot Avg. Voliro AVJ.


68

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QUALITY ASSURANCE REVIEW

REPORT ON QUALITY ASSURANCE MEASURES FORTHE TRIAL BURN AT VERTAC SITE CONTRACTORS

JACKSONVILLE ARKANSAS

The quality assurance effort conducted by Dr. Craig M. Young forthis project was divided into three main audits. The first was afield audit conducted during the trial burn at the Vertac SiteContractors Facility. The second audit was an audit of thelaboratory. Triangle Laboratories in Raleigh, North Carolina. Thefinal part of the audit was an audit of the trial burn reporteddata.

FIELD AUDIT

The trial burn began with a meeting of all the interested partiesin the conference room of Vertac Site Contractors on Oct. 7, 1991.The meeting was attended by representatives of the State ofArkansas, the USEPA, Clean Air Engineering, subcontractors to State Lnand Federal agencies, and Vertac Site Contractors and their v-subcontractors. The proposed testing was discussed and all present Qagreed that the proposed testing would meet the data requirements Qfor the establishment of permit operating conditions.

00

Test Run #1.Test Run #1 was conducted on Oct. 9 , 1 9 9 1 . Testing began at 2:33p . m . Leak checks of the M5 and MM5 sampling trains at thebeginning of the testing were within the limits of 0.02 cfm. Thesampling trains were switched from one port to the other after halfof the sample had been collected. The leak checks were againsuccessful. Sampling was restated without incident. Compositesamples of the dry combustion gas were collected over the entiresampling period from both the M5 and the MM5 sampling trains.These integrated gas samples were returned to the laboratorytrailer where they were analyzed using an Orsat analyzer. Finalleak checks were successful and the sample trains were returned tothe ground without incident. Process feed samples were collectedon a 15 minute time schedule. Grab samples of the other processsamples were collected during the last hour of the test. Thesampling trains were recovered without problems at the laboratorytrailer. The samples were labeled and stored in coolers containingice. The samples of the waste feeds were held in the trailer nearthe stack. Samples with trace level concentrations (ash, salt,water, and combustion gas samples) were held in the laboratorytrailer to prevent cross contamination.

Test Run #2.Test Run #2 was conducted on Oct. 10, 1991 with sampling beginningat 10:51 am. The M5 and MM5 trains were leak checked and samplingwas started. All leak checks of the sampling trains met the 0.02

cfm limit. The sample trains were lowered and recovered withoutincident. The process samples were collected on a 15 minuteschedule and no problems were encountered with their collection.After the M5 sample had been collected, the VOST samples werecollected in the port opposite the MM5 sample train. One pair ofVOST cartridges were broken while connecting to the train. Thebroken pair was set aside and a new pair of cartridges were used.The other cartridges were collected without incident. Four pairsof VOST cartridges were successfully collected. Each pair ofcartridges were leak checked before and after sampling. Aftercompletion of the sampling, the recovery of the sampling trains wasobserved and no problems were noted. The collection of samples ofthe VOST audit cylinders were then observed. The sample collectionsystem was assembled per the instructions included with theequipment. Ten liter samples of the audit gases was collected asdirected by the instructions included with the audit cylinders.The cartridges were capped, placed in a sealed tube and placed ina cooler with ice. C

COTest Run *3. \r\

The final set of samples was collected on Oct. 11, 1991. The M5 T-train was the first sample collected. The leak checks and recovery Qof the sample proceeded without problem. The MM5 and the M23 Qtrains were leak checked and started at 3:34 and 3 : 4 6 respectively.At the midpoint of the test, the M23 train leak checked fine. TheMM5 train was found to be leaking at a rate of 0.08 cfm. A chippedconnector was found between the probe and the filter housing. Thefitting was replaced and the system leak checked within limits.Preliminary calculation of the percent isokinetic sampling rate wasconducted and found to be within the 100 ± 10 percent specificationeven with the leak rate adjustment. Sampling was then restartedand finished without further incident. The final leak checks wereacceptable. Leak checks of the pitot tubes were fine. The chippedfitting was recovered with the MM5 train at the completion of thesampling. After completion of the sampling, the gas calibration ofthe dry gas meters were checked using a critical orifice. The datarecorded was accurate and the sheets appear in the trial burnreport. The Orsat analysis of the dry gas samples was observed andno problems were noted. The recovery of the sample trains wasobserved and no problems were noted.

LABORATORY AUDIT

The second part of the audits conducted was an onsite audit ofTriangle Laboratories, who were analyzing the MM5 samples forhexachlorobenzene. The audit took place on Oct. 18, 1991, with Dr.Hani Karan. The audit began with the GC/MS analysis of theprepared MM5 samples. The mass calibration was observed and thePFTBA sample was within the USEPA guidelines. The samples werebeing analyzed as the observations were made. After initialobservations of the analyses in progress, the rest of the audit wasconducted.

The sample receiving area was observed and the sample custody formsfor the samples from this project were produced showing theactivities that had taken place to date. Labeling andidentification of incoming samples was reviewed with the samplecustodian. Samples from this project were observed in the samplestorage cooler which was maintained at 4°C. The sample preparationarea was observed and the preparation of the samples from thisproject were discussed with the personnel. No problems were notedwith the samples as they went through the sample preparation steps.The dioxin samples were just beginning to undergo samplepreparation and observations on this process were made. Theanalysis of these samples was to begin in the next week.The VOST cartridges had been analyzed prior to the audit. One ofthe pairs of cartridges was lost due to a power failure during theanalysis which resulted in all the data being lost. The othercartridge pairs had been analyzed including the audit samples. Thedata from this analysis was in QA review during the visit. NÂt this point, the analysis of the MM5 samples for hexachloro- 00benzene were completed. The hexachlorobenzene samples were LOanalyzed using a seven point calibration curve. The anticipatedconcentrations in the samples was below the normal lowest ~calibration standard, so two additional standards were used at the ^lower end of the calibration curve. This technique effectively 0extended the calibration curve to near the concentrations of thesamples. The integration of the standards and development of thecalibration curve were observed. The calibration curve was linearover the area of concern. The samples were integrated andcalibrated using an extracted ion chromatogram. As a check on theidentity of the compounds, the peak at the retention time of theextracted ion peak was searched and identified by the data systemas hexachlorobenzene. A manual check of the identification agreedwith the identity of the peak. The analysis of the surrogatecompounds and internal standards were all within acceptable ranges.

REPORT AUDIT

The final part of the audit was an audit of the Trial Burn Reportcalculations. The calculations of the results from Test Run #1were calculated by hand as a check on the integrity of thecalculations. Field data sheets in the report was identical tocopies supplied as the data was collected. The audit resultsmatched the data supplied with the report. Additional spot checksof the calculations were conducted with no problems detected. Theresults of the hand calculations are attached.

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VERTAC SITE CONTRACTORS, A Joint VentureMRK Incineration, Inc. / MK-Environmental Services, Inc.

P.O. Box 547,1302 Marshall Road, Jacksonville. AR 72976 .,^F.C^j\/pn,'- <, f" r-. ' ^* w- • • %'1\' yr

TRANSMITTAL LETTER llct31 DEC i 7 .., „' 1 Ôuc,'"

•--•'-,;• ;';,,• •' ,'•'?( i" -•>L/<3810Contract No.TO: n--^- F-P&

Client: AR Dept. of Pollution Control & EcologyFountain Place 6 HEA, 1445 Ross AvenueDallas, TX 75202-2733 Location: Jacksonville, AR 72076_________

Transmittal Number: T-VSC/EPA-0149_________Ann: Richard EhrhartDate: December 10, 199]______________

References:

Item:Equipment/Item No.:Specification No.: —Purchase Order No.;Vendor

Client:

Vendor Order No.:Transmitted [3 Herewith Q Under separate cover are:

QUANT. TITLE/DESCRIPTION ITEM-tfY-

each Revised pages for the Trial Burn Report 00

Please remove the corresponding pages in Volumes I and IVand insert these attached pages in their place.

Q Approved D Approved as Noted D Disapproved D Released for Manufacture/FabricationFor: D Review and Comment D Approval D Record K3 InformationD Mark one copy with your Approval and/or Comment and return to this officeD Correct as indicated and:D Resubmit (___ Copies) For Final Approval D Send (___ Copies) I D "Certified for Construction"

(__ Repros) (___ Repros) I D "For Distribution"

REMARKS:

Very trutv yours,VERTAG SffEÔNTRACTORS. A Joint VentureRy ^^^X^ . \ ^

Title: Robert P. Apa onager

VERTAC SITE CONTRACTORS, A Joint VentureMRK Incineration, Inc. / MK-Environmental Services, Inc.

P.O. Box 547,1302 Marshall Road, Jacksonville, AR 72076

TRANSMITTAL LETTER

TO: U.S. EPA Contract No. 3810Fountain Place 6 HEA, 1445 Ross AvenueDallas, TX 75202-2733___________Richard EhrhartAttn:

Client: AR Dept. of Pollution Control R, Fr-nlngyLocation: Jacksonville. flR 7207fi________Transmittal Number: T-VfiC/EPft-OI . 1Date: December 12. 1991

References:

Item:Equipment/Item No.:Specification No.: —Purchase Order No.:Vendor

Client:

Vendor Order No.:Transmitted ©Herewith D Under separate cover are:

QUANT. TITLE/DESCRIPTION ITEM -IA-

each VOST Report from Clean Air Engineering, Volumes I, IIA, and IIB 00

D Approved D Approved as Noted D Disapproved D Released for Manufacture/FabricationFor: D Review and Comment D Approval 1Q Record B InformationD Mark one copy with your Approval and/or Comment and return to this officeQ Correct as indicated and:D Resubmit (___ Copies) For Final Approval D Send (——— Copies) 1 D "Certified for Construction"

(—— Repros) (__ Repros) ( D "For Distribution"

REMARKS

Very truly yours,VERTABy:^

Title: _

CONTRACTORS. A Joint Venture'^fr—2

Site Manager


SUMMARY

INTRODUCTION

Clean Air Engineering was contracted by Vertac Site Contractors to determinethe levels of paniculate, dioxins/furans, hydrogen chloride andhexachlorobenzene emissions at the Vertac Chemical Corporation Superfundsite located in Jacksonville, Arkansas in support of their trial bum. Waste feedand process samples were taken and analyzed in accordance with the TrialBum sampling and analytical plan.

The testing took place at the Stack on October 9 through 1 1 , 1 9 9 1 .Coordinating the field testing were:

R. Apa - Vertac Site ContractorsP. Schwindt - US EPAM. McCorkle - State of Arkansas Department of Pollution

Control and EcologyC. Young • Independent Quality Assurance AdvisorJ. Chapman - Clean Air Engineering

SUMMARY OF TEST RESULTS

The test conditions and results of analysis are presented in Tables 1 through 3on pages 1-2 through 1-4.

To the best of our knowledge, the data presented in this report are accurateand complete.

Respectfully submitted,

CLEAN AIR ENGINEERING

Q\J (\>Tfvv- U^-^y^î/ J

John ChapmanVice PresidentResearch and Development

Kimberiy KemptManager, Technical Communications


Run No.

Vmstddscfm

Dioxins and FuransngIb/dscfng/dscmIb/hrg/sec

TB-4

130.3811.420

4060.00000000000687

1 1 00.00000471

0.000000593

Clean Air Engineering - United States Environmental ... · R. Apa - Vertac Chemical Corporation P. Schwindt - US EPA M. McCorkle - State of Arkansas Department of Pollution Control

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