59 CHAPTER 4 MATERIALS AND EXPERIMENTAL PROCEDURE 4.1 GENERAL To accomplish the objective of this study, the experimental work was carried out on nine GFRP reinforced concrete deep beams with and without web reinforcement. The details of the materials used for casting the deep beam specimens, fabrication of GFRP reinforcements and testing procedures are given in the subsequent sections. 4.2 MATERIALS AND ITS PROPERTIES 4.2.1 Concrete The concrete used for casting was prepared in the testing laboratory using a portable concrete mixture machine. All the specimens which were tested were cast by using cement concrete and the cement used was confirming to the specification of IS 8112 (1989) code. The concrete was designed to achieve the 28 day compressive strength of 40 N/mm 2 (M40 Grade). The concrete mix proportion adopted was 1: 1.02: 1.93 with water /cement ratio of 0.38. The material proportions per cubic meter of concrete: 1) 1059 kgs of coarse aggregate (maximum size 20mm) 2) 560 kgs of natural river sand (sp.gr =2.53) 3) 548.5 kgs of ordinary port land cement(43 grade) 4) 208 litres of water
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59
CHAPTER 4
MATERIALS AND EXPERIMENTAL PROCEDURE
4.1 GENERAL
To accomplish the objective of this study, the experimental work
was carried out on nine GFRP reinforced concrete deep beams with and
without web reinforcement. The details of the materials used for casting the
deep beam specimens, fabrication of GFRP reinforcements and testing
procedures are given in the subsequent sections.
4.2 MATERIALS AND ITS PROPERTIES
4.2.1 Concrete
The concrete used for casting was prepared in the testing laboratory
using a portable concrete mixture machine. All the specimens which were
tested were cast by using cement concrete and the cement used was
confirming to the specification of IS 8112 (1989) code. The concrete was
designed to achieve the 28 day compressive strength of 40 N/mm2 (M40
Grade). The concrete mix proportion adopted was 1: 1.02: 1.93 with water
/cement ratio of 0.38. The material proportions per cubic meter of concrete:
1) 1059 kgs of coarse aggregate (maximum size 20mm)
2) 560 kgs of natural river sand (sp.gr =2.53)
3) 548.5 kgs of ordinary port land cement(43 grade)
4) 208 litres of water
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The coarse aggregate used was crushed granite stones of 20 mm
and less in size with specific gravity of 2.58 and fineness modulus of 6.9. The
locally available river sand which was sieved by passing through 2.36 mm
sieve and retained on 75 m sieve and which had a fineness modulus of 3.1
was used as the fine aggregate. The cement used for preparing the concrete
was tested in the laboratory conforming to IS 8112 (1989) standards with
respect to initial and final setting time, specific gravity, fineness and
compressive strength.
Along with each batch of the concrete prepared for casting the deep
beam specimens, concrete cubes were cast to determine the material
properties and to confirm its strength. Testing of these cubes was done after
7 days and then 28 days after casting. The cubes were de-moulded the next
day of casting and it was cured in water before it is tested. The details of cube
tests results are shown in Table 4.1.
Table 4.1 Concrete cube test results
BEAMS
Compressive
Strength N/mm2
(7Days )
Compressive
Strength
N/mm2 (28 Days )
GFRDB-1 28.7 41.9
GFRDB-2 30.9 43.3
GFRDB-3 28.8 40.8
GFRDB4 34.9 40.1
GFRDB-5 33.4 41.3
GFRDB-6 28.5 42.9
GFRDB-7 29.8 42.5
GFRDB-8 29.5 40.7
GFRDB-9 30.5 41.9
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4.2.2 About GFRP Constituent Materials
4.2.2.1 Glass Fiber
The glass fiber used for fabricating the GFRP reinforcements is of
E- Glass fiber type of Saint-Gobain Vetrotex with identification number as
RO 99 2400 P 566. The fiber which was available in roving of 2400 normal
liner density (tex) was specifically selected for the purpose of manufacturing
by ‘Manual Fiber-Trusion’. The proprietary sizing system of the selected P
566 type fiber was designed to give a high level of performance with greater
compatibility with Polyester, epoxy, vinyl and phenolic resins. The test
specifications supplied by the fiber manufacturer are as shown in Table 4.2.
Table 4.2 Specification of E-Glass Fiber
PROPERTY VALUE TEST METHOD
Glass content (%) 60-65 BS 3691
Tensile Strength (Mpa) 1700-1800 BS 3691
Tensile Modulus (Gpa) 65-75 BS 3691
Some of the other advantages of using this type of fiber include
fast and complete wet-out of fibers with most resins, good resin wettability by
fibers, excellent spreading on the mandrel which gives a smooth and regular
surface, high mechanical properties, good composite translucency. These
were found to be needed for this type of manufacturing process to be efficient
and hence this type of fiber was adopted.
4.2.2.2 Epoxy resin
Epoxy resin is the extensively used matrix material compared to
other category of resins particularly for reinforcement bars due to their high
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mechanical property to bond with fibers. Epoxy is a thermosetting polymer
formed from after mixing a peroxide resin with a hardener in a suitable
proportion.
Epoxy resins have high strength, good corrosion resistant and can
very well bond with fibers, high glass transition temperature, superior
electrical properties, high dimensional stability, and low shrinkage. Epoxy
resins which have a wide range of mechanical properties can be used in all
FRP manufacturing processes.
The slow curing epoxy resins used in this work takes a long gel
time to become solid, which is considered to be more advantageous for the
‘Manual Fiber-Trusion’ process as it requires more time for moulding the
uncured impregnated fibers pulled from the Fiber-Trusion die.
Epoxies used for this work was found to have an average tensile
strength of 95 MPa. Their density varied between 1.2 -1.4 Kg/m3. The
percentage of cure shrinking was observed to be 3.1%.
4.2.2.3 Proportion of mix for resin
To provide the correct calculated quantity of fiber in the GFRP bars
and stirrups the fibers were cut to a desired length using the technical
specification provided by the glass fiber manufacturer. From the specification
supplied by the fiber manufacturer, the weight of fiber required per unit
length was calculated and the required amount of fiber to achieve 75% of
fiber volume fraction in the GFRP composite reinforcement material was
calculated. The calculated amount of fiber was then counted and removed
from the rovings to the desired length of the reinforcement. The glass fiber
cut-out from the roving was suitably impregnated in a resin tub containing
25% of resin and hardener mix by volume.
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The amount of fibers used for fabricating the GFRP bars and
stirrups varied with respect to the required diameter. For a greater diameter of
the bar, the required amount of fiber was higher to maintain the 75% fiber
content in the finished product.
A number of trails were made and tested to finally arrive at a
particular combination of fiber and resin which was finally adopted to
produce bars of 8mm, 10mm and 22mm diameters. The details of calculation
showing the amount fiber -resin mix required for this manufacturing process
has been illustrated in Appendix 1.
4.2.2.4 Properties of GFRP used in the experiment
Tension tests on GFRP bars were conducted to know the ultimate
tensile strength and modulus of elasticity for the bars used for this
experiment. The bars were placed inside the specially made pipe fixtures
fitted at its ends and filled with a mixture of epoxy and sand to avoid slippage.
The results of which prove to be greater than values of the FRP bars
manufactured by conventional pultrusion method. The calculated values of
some of the physical properties from the test results are tabulated in Table 4.3
Table 4.3 Properties of Fabricated GFRP material
Material Average Tensile
Stress (f frp) Mpa
Ultimate tensile
Strain ( )
Modulus of Elasticity
(EGFRP) Mpa
GFRP 780 0.017515 44,530
To obtain good bond strength with concrete, the GFRP bars which
were coated with a layer of coarse and fine sand sieved particles on the rebar
surface one over the other. After providing this type of sand coat a very
effective bond between GFRP bars and concrete was obtained. Pull-out tests
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were carried out on sixteen rebar specimens and the results proved to be better
in terms of bond strength, when compared to other GFRP bars with different
surface finish.
4.3 MANUAL FIBER-TRUSION
4.3.1 ‘Manual Fiber-Trusion’- a new method of Manufacturing
GFRP Reinforcement
FRP Composites are being manufactured by various techniques and
with emerging new technologies, production is easy and fast. Among the
various methods of manufacturing FRP composites, pultrusion by machine is
one way of manufacturing. The Pultrusion method employs machines to
manufacture FRP composite which make the process expensive. Moreover
they require high initial investment and the process of manufacturing is slow.
In addition to all this, there exist some shortcomings with respect to
the strength criteria of FRP bars manufactured through mechanised
pultrusion. This is due to the use of low strength filler material during the
manufacture of pultruded FRP composites. These filler materials are used for
the smooth production of pultruded sections and also to reduce the gel time
during the pultrusion process. The presence of filler material in FRP
composites is an impediment to achieve higher tensile strength. The filler
material in these FRP bars reduces the volume of fiber and matrix materials
and this in turn reduces the strength of the FRP composite material.
In the present day mechanised pultrusion process, the presence of
filler material cannot be avoided for the reason that it is this filler material
which ensures the smooth running of pultrusion manufacturing process
without interruption. Moreover, the cost of pultrusion machine and its
maintenance is very high which in turn has a bearing on the production cost of
FRP composite materials.
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To overcome this problem, it was needed to develop a new way of
manufacturing FRP composites. The outcome was the conception of a simple
manufacturing method called “Manual Fiber-Trusion” developed during the
course of this research work. The “Manual Fiber-Trusion” method of
manufacturing FRP bars and stirrups was found to be cost effective with an
advantage of having greater tensile strength. By using this novel method, FRP
bars can be made to any size and shape which is not possible in the machine
pultrusion. The greatest advantage in this Manual Fiber-Trusion method is
that, FRP bars can be bent during and also after the process to any desired
shape, which cannot be achieved by machine pultrusion. A schematic diagram
showing the various stages of ‘Manual Fiber-Trusion’ process is shown in
Figure 4.1.
Figure 4.1 The ‘Manual Fiber-Trusion’ process
Although there are many FRP composite manufacturing companies
in India, most of them mainly manufacture GFRP bars for electrical
applications only. In such GFRP bars, the insulation property is considered
primarily important than the strength of the bar. When tested the strength of
these bars were found to be less as their fiber content was less than 65% and
RESINTUB
GLASS FIBRE CREELS
DIE
MANUAL
FIBER-TRUSION
RE BARROLLERS
DIRECTION OFMANUAL PULL
66
a substantial amount of filler materials was present in it. Such a combination
of low fiber and high matrix materials used for manufacturing these GFRP
bars leads to low strength and thereby reduces their load carrying capacity.
These GFRP bars which were manufactured for electrical applications were
tested earlier, before adopting this ‘Manual Fiber-Trusion’ method of
manufacturing. Thus the option of using the readily available GFRP bars from
the market was not preferred.
To overcome the entire above problem, it was decided to produce
the GFRP reinforcement bars having high strength. After experimenting by
various methods, many trails were carried out to manufacture high strength
bars economically. Some of the trail specimens are as shown in Figure 4.2.
Figure 4.2 Some trail GFRP reinforcement specimens fabricated
During the trail fabrication, the GFRP rebar specimens were
manufactured by altering the composition of individual constituent materials
and also by adopting different techniques of manufacturing.
67
Fabrication of GFRP rebars and stirrups with open moulds of
different sizes and shapes, fabricating stirrups using continuously looped fiber
impregnated in matrix, casting of rebars using ribbed flexible pipes as mould,
were some of the techniques that were tried during initial trails for fabricating
the GFRP rebars and stirrups.
Some of the other procedures adopted were; altering the percentage
volume of the resin and fiber combinations in the composites. Ultimately,
with a considerable effort, a new method suitable for fabricating the GFRP
reinforcement material was found. This new method of fabricating FRP rebars
through manual Fiber pulling resulted in the naming of this method as
“Manual Fiber-Trusion” method by the author.
4.3.2 Arrangement of Parallel Fibers for Fiber-Trusion
Based on the percentage of fiber to be adopted for making the
GFRP bars of required diameter and also based on the weight per unit length
of the fiber supplied by the fiber manufacturer, the required numbers of
strands were removed from the roving creels and looped. The fibers were
looped between two fixed points of required length and after looping they
were removed from the arrangement and kept ready for sinking in a tub of
resin. Looping is mainly done to facilitate proper gripping of fibers during
manual pulling. The arrangement made for looping the fibers is shown in
Figure 4.3. The arrangements of fibers were carefully maintained until the end
of the manufacturing process to ensure the parallel alignment of fibers.
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Figure 4.3 Looping of glass fibers
4.3.3 “Manual Fiber-Trusion” Process
The fibers which were looped were tied to a steel rod which has a
provision to hook the fiber loop at one end. This steel rod with hook at one
end and with a handle at the other end was used to pull the impregnated fiber
after the wet fibers pass through the die. The looped fibers are then pulled
through the preset die arrangement which is fixed over the table through
which it is passed. This was done to get the fibers molded to the required size
and shape of the die and also to remove the excess resin from the wet fiber
which is recycled into the resin bath. The “Manual Fiber-Trusion”
arrangement used for fabricating the GFRP main bars of 22mm diameter is
shown in Figure 4.4. Each batch of resin prepared has to be utilised before it
starts curing. It took about 30 minutes to complete one cycle of fabrication of
a GFRP element.
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Figure 4.4 ‘Manual Fiber-Trusion’ for fabricating GFRP main bars
These fibers pulled out from the die which was in a flexible state
were passed into suitable moulds to form bars of the required shape and size.
4.3.4 Moulding of Bent Bars and GFRP Stirrups
The method of fabricating the stirrups was slightly different from
that adopted for GFRP straight bars. The process was the same till the fibers
were pulled out of the die. Then the flexible wet fibers in the cylindrical form
were placed inside a flexible mould. The type of mould adopted for
fabricating the stirrups is shown in Figure 4.5.
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Figure 4.5 Fibers impregnated in resin and placed inside a
closed mould to make stirrups
The tension of the fibers was maintained till the resin had cured
considerably. The mould was placed exposed to direct sunlight for about 2 to
3 hours after it was molded. Then it was made to dry under shade for about
12 to 15 hours. Figures 4.6 and 4.7 shown below are photographs of trail
stirrup specimens fabricated during the initial stages before the final
fabrication of bars and stirrups for experimentation. Different types of moulds
such as open mold, glass tube mold and P.V.C. flexible mould were tried
during the trail phase of fabrication.
Figure 4.6 View of trail pieces GFRP stirrup specimens
71
Figure 4.7 GFRP stirrups specimens fabricated and used in this work
4.3.5 Post Curing Process
After allowing the moulded GFRP bars and stirrups to be naturally
cured under atmospheric temperature for about 12 -15 hours under dry
condition, the GFRP material is removed from the mould. To complete the
curing process the GFRP bars and stirrups are further post-cured by placing
these GFRP materials inside an electric oven which is maintained at
120o temperature for about 2 hours. This is done to cure some of the uncured
resins inside the core of the GFRP material. The post curing of GFRP bars
and stirrups in a large size electric oven is as shown in Figure 4.8.
After post-curing the specimens, they were given a finishing
treatment such as by cutting and removing the excess resin which had over-
flown the mould during the moulding process and also cutting and removing
72
the ends of the GFRP fiber material present beyond the mould. This finishing
work for the stirrups is shown in Figure 4.9.
Figure 4.8 Post-curing of GFRP bars and stirrups
Figure 4.9 GFRP stirrups finishing work
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In order to prevent the glass fibers from penetrating into the skin,
handling of the GFRP finished product was carried out using leather gloves.
The post cured bars and stirrups were found to be extremely hard.
4.4 PREPERATION OF BEAM SPECIMENS
4.4.1 Sand Coating
After the finishing work, the GFRP bars and stirrups were coated
with a layer of epoxy over which coarse sand was spread uniformly over the
entire surface. The coarse sand used for this first layer of sand coating was
obtained after sieving the sand through a 0.5 mm sieve. After curing for about
two days, a second layer of fine sand was applied over the existing layer of
coarse sand. The fine sand used for this purpose was obtained after passing
through a 100 micron sieve. The fine sand fills between the gaps of the coarse
sand in order to develop a complete rough surface over the entire GFRP
material. Figure 4.10 shows sand coated GFRP stirrups kept under the
sunlight for surface curing.
Figure 4.10 Curing of sand coated GFRP stirrups
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4.4.2 Fixing of Strain Gauges
To understand the internal behaviour of GFRP reinforcement in
deep beams, all the deep beam specimens were affixed with electric foil strain
gauges at critical points where the strains were expected to be more and need
to be measured. In case of non-isotropic materials like the GFRP
reinforcement, the material is very strong when the fibres are unidirectionally
oriented. But in the same material, when the fibers are bent, it becomes weak
leading to failure. To effectively understand the response of GFRP
reinforcements, the strain gauges were placed at vital places over the surface
of the GFRP bars and stirrups, where the cracks in the beam were expected to
cause a considerable amount of strain in the GFRP reinforcement. After fixing
the strain gauges over the GFRP reinforcements, the electrical resistances of
the strain gauges were checked to ensure that all the strain gauges have the
required resistance of 120 ohms. This also ensures the working condition of
the strain gauges before concealing them inside the water proofing latex
cover. Checking the resistance of the strain gauges which were fixed over the
GFRP reinforcements is shown in Figure 4.11.
Figure 4.11 Checking of strain gauges fixed over the GFRP bars
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4.4.3 Binding of GFRP Reinforcement
After fixing the strain gauges over the GFRP reinforcements at
selected locations, the bars and stirrups were tied according to the beams’
reinforcement configurations. Self-locking nylon ties were used to bind the
GFRP bars and stirrups. At every junction, two nylon ties were provided in a
criss-cross fashion to ensure that no slippage of reinforcement takes place. A
GFRP cage tied for beam GFRDB-8 by nylon ties is shown in Figure 4.12.
Figure 4.12 Binding of GFRP reinforcement for beam GFRDB-8
The main GFRP bars and horizontal bars were projected beyond the
point of support for effective anchorage. The anchorage length was calculated
as per the guidelines given in ISIS Design Manual 3(2001). To avoid any
rupture in the GFRP bars with the steel stirrups which were provided beyond
the test area, the ribs of the steel stirrups were removed by properly grinding
at the places of contact with GFRP bars. This also helped to prevent the
scraping of the sand coated over the GFRP bars during extreme forces in the
anchor zone usually during the peak loading condition. The cage
reinforcement for all beams is as shown in Figure 4.13.
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Figure 4.13 GFRP reinforcement cage for deep beams
77
4.4.4 Casting of Deep Beams Specimens
Three steel moulds of the same dimensions were fabricated for
casting the beam specimens to be tested in this study. The moulds were
properly cleaned and greased for easy de-moulding after casting. The concrete
required for casting was prepared using a concrete mixture machine.
Before pouring concrete, the reinforcement cages were placed
inside the mould with suitable small sized cover blocks. The beams were cast
with the concrete which had the required slump as per the IS code
specifications. The concrete was properly compacted using a needle vibrator.
All the beams were cast to the same dimensions of 160 mm depth, 530 mm
height and 1970 mm overall length. The mould used for casting is shown in
Figure 4.14.
Figure 4.14 Mould used for casting deep beams
The concrete beam specimens were de-moulded the day after they
were cast. Subsequently, they were cured in water for 28 days before being
subjected to testing. Along with each batch of concreting, concrete cubes
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were also cast to ascertain the 7 day and 28 day strength of concrete. The
beams cast is shown in Figure 4.15
Figure 4.15 Deep beams cast and cured in moisture by using gunny bags
and dried hay stalks
4.5 EXPERIMENTAL SETUP AND TESTING
4.5.1 Test Equipment and Instrumentation
To monitor the change in the strain of the internal GFRP web
reinforcement, the strain gauges were fixed at vital locations of the GFRP
reinforcement. The variation of strain during the experiment was observed
using a Multi-Channel digital strain meter. During testing of the deep beam
specimens, the concrete surface strain varies and this surface strain was
measured using a demountable mechanical gauge (De-Mech gauge) along the
line joining the point of loading and the point of support. The deflection of the
beam was measured using a mechanical dial gauge at the mid-span section.
One externally placed GFRP bar which does not form a part of the
beam’s reinforcement, was kept exposed to atmosphere and was connected to
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the strain meter for auto-correction of strain due to temperature variation. This
was done for temperature compensation of the strain gauge used inside the
concrete deep beam specimens. The size of the strain gauge foil used in this
testing varied from 20 to 50 mm gauge length. The layout of the strain gauges
fixed to the reinforcement of all the deep beam specimens is shown from
Figure 4.16 (a) to 4.16 (e)
Figure 4.16 (a) Location of strain gauge (SM) in main bar of beam
GFRDB-1
The strain gauges are abbreviated as:
1) SS - Strain Gauge at straight portion of stirrup.
2) SB - Strain Gauge at bent portion of stirrup
3) SM - Strain Gauge at Mid-Span of the Main Bar
4) SHB - Strain Gauge at horizontal web reinforcement (bottom)
5) SHT - Strain Gauge at horizontal web reinforcement (top)
The locations of the strain gauges fixed in Series-II beams were the
same as that of their counterpart beams in Series-I.
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Figure 4.16 (b) Locations of strain gauges in deep beams GFRDB-2 and GFRDB-3
81
Figure 4.16 (c) Locations of strain gauges in deep beams GFRDB-4 and GFRDB-5
82
Figure 4.16 (d) Locations of strain gauges in deep beams GFRDB-6 & 7
83
Figure 4.16 (e) Locations of strain gauges in deep beams GFRDB-8 and GFRDB-9
84
Figure 4.17 Mechanical strain gauge and crack width microscope
The mechanical strain gauge used for measuring the concrete
surface strains had a least count of 1/40 mm. This strain gauge was used for
measuring the diagonal surface elongation by which the surface strains can be
calculated. The surface elongation occurs due to formation of cracks in the
shear span region of the beam. The type of crack width microscope used
during the experimental work is shown in Figure 4.17
Figure 4.18 Multichannel strain meter
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The strains in GFRP reinforcement were measured using the above
strain meter as shown in Figure 4.18. This digital instrument was connected
simultaneously all strain gauges fixed to a specimen and the strains were
recorded.
4.5.2 Details of Beam Specimens Tested
The GFRP deep beams were tested under two categories, namely
under Series-I and Series-II. In Series-I nine GFRP deep beams were tested
with a ‘shear span to effective depth ratio’ of 0.72 under the four point
bending condition. In Series-II four deep beams with a ‘shear span to
effective depth’ ratio of 1.08 were tested under three point bending. In total
13 deep beams were tested to study their ultimate shear strengths.
Apart from the above mentioned tests conducted on GFRP deep
beams, some tests on GFRP slender beams were also conducted initially to
check and confirm the use of ‘Manual Fiber-Trusion’ bars in concrete beams
before commencing the testing of heavy deep beams. Twelve beams were cast
and tested in which nine beams were cast using only GFRP main bars as
reinforcement and three beams were cast using only steel main bars
reinforcement. The details of slender beam specimens tested are discussed in
section 4.5.5.
Details of the deep beam specimen regarding dimensions, amount
of reinforcement and grade of concrete are as shown in Table 4.4. The details
of the deep beams which were provided with different web reinforcement
configurations are shown in Figures 4.19 (a) to 4.19 (c).
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Table 4.4 Details of GFRP deep beam specimens in Series-I and Series-II