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Document ID: 239269

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Page 1

Final Report

Summary of RemovalActions at MilwaukeeSolvay Coke and GasCo. Site

Volume 2

Appendices F thru I

Prepared for

Water Street Holdings, LLC311 E. Greenfield AvenueMilwaukee, Wl 53207

Prepared by:

Earth Tech, Inc.1020 N. Broadway, Suite 400Milwaukee, Wl 53202

March 2005

Milwaukee Solvay Coke and Gas Co. Project - Removal ActionsMilwaukee, Wisconsin Final Report

APPENDIX F

Other Waste Disposal Documentation

• F-1: Onyx Environmental Services

• F-2: Tires and Belts

• F-3: Advanced Waste Services

EarthTechA Tyco International Ltd. Company

L:\work\72534\Admin\Reports\Rpttext.doc


APPENDIX F-1

Waste Stream Information fromOnyx Environmental Services



Environmental Services

Fax CoversheetTO:

COMPANY:

FAX NUMBER:

FROM:

DATE:

Bill Kralj

Earth Tech - 1020 North Broadway Suite 400, Milwaukee, Wl 53202

1.414.225.5111

Allan Kountz

02/14/05

THIS MESSAGE IS INTENDED ONLY FOR THE USE OF THE INDIVIDUAL OR ENTITY TO WHICH IT ISADDRESSED. AND MAY CONTAIN INFORMATION THAT IS PRIVILEGED OR CONFIDENTIAL.

If the reader of this message is not the intended recipient, or the employee or agent responsible for delivering the message to the intendedrecipient, you are notified that any dissemination or distribution of this communication is strictly prohibited. If you have received thiscommunication in error, please notify us immediately by telephone, and return the original message to us by mail. Thank You.

Number of Total Pages Including Cover: 45

Special Comments / Instructions:

Bill,

Attached is the paperwork for Solvay Coke that

Onyx Environmental ServicesW1?.4 NS451 Bound-iry RoadMonomonee r.ai's Wl KOfi'Tel. 262-255-0:W3 • \ 'J< 2?;2-,':;5 57'.v.v,v "-nvxei.oofn

\ linvironnement

WASTE AND HAZARDOUS MATERIALS DIVISIONMICHIGAN DEPARTMENT OFENVIRONMENTAL QUALITY DO NOT WRITE IN THIS SPACE

ATT. D DIS. D REJ. D PR.D

Required under authority of Part 111and Part 121 of Act 451. 19»4, asamended.

Failure to file may lubject you to crimi-nal and/or civil penalties under Section.324.11151 or 324.12118 MCL.

Please print or type Form Approved. OMB Mb. 2050-0039

UNIFORM HAZARDOUSWASTE MANIFEST

I. Generator's US EPA ID No.Wl M 0 0 0 5 0 8 3 1 5

Manifest 2. Page 1

of 1

Information in the shaded areasis not required bv Federallaw.

inzo

zo

Generator s Name and Mailing AddressSOLVAY COKE AND GAS COMPANY31 1 EAST GREENFIELD AVENUEMILWAUKEE./* 5320?

A. State Manifest Document Number

Ml ; 93766738, State Generator'* »D

Generator's Phone ( 414— ™ - • •

645-0635Transporter 1 Company Name

ONYX ENVIRONMENTAL SVCS L.L.C.

SAME"If US EPA ID Number

| N J D O B Q 6 3 1 3 6 9State Transporters ID 1B13Q

D. Transporter'* Phone;, (873) 347-7111Transporter 2 Company Name 8.

I

US EPA ID Number State Transporter's ID

F. Transporter's PhoneDesignated Facility Name and Site Address 10. US EPA ID Number Q, State Facility's ID

M/A :MTP OOO7Z H X 51 H, faculty's Phon* ,

(383)355-6855 / A •

UST)OT Description \incluaing Proper Shipping Name, Hazard Class, andHM ID NUMBER).

12.Containers

No. I Type

13.Total

Quantity

14.Unit

MAfol

(.Waste*No. •

u.o

o

I

RQ. WASTE POLYCHLORINATED BPHENYLS, SOLID,(BALLASTS). 9. UN2915. II

0 0 O N 0 0 9 5 1 K

d.

J, Addition^ Descrtpttons for Materials Listed Above ,, „'in

ino

I

KlHandBnoCodwfoiWaste* Listed AbovB

> i a:

15. Special Handling Instructions and Additional InformationPACKING SUPS ATTACHED FOR CLARIFICATION - EMERGENCY NUMBER-INFOTRAC: 1-800-535-5053PC165 W TECH SERVICES

o

hUJIt-Oj»

s|Ir-iiu,OD <

ll

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and arclassified, packed, marked, and labeled, and are In all respects In proper condition for transport by highway according to applicable International and national government regulationsIf I am a large quantity generator, I certify that I have a program In place to reduce the volume and toxlcity of waste generated to the degree I have determineto be economically practicable and that 1 have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes thpresent and future threat to human health and the environment; OH; H I am a small quantity generator, I have made a good faith effort to minimize my wastgeneration and select the best waste management method that Is available to me and lhatj can ar" ~ Date

17. Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed Name

rspo

Signature

18. Transporter 2 Acknowledgement of Receipt of Materials

Month Day Yea*

J7iO|</Date

Printed/Typed Name Signature Month Day Yea

19. Discrepancy Indication Space

20. Facility Owner or Operator. Certification of receipt of hazardous materials covered by this manifest except as noted inItem 19

DanPrinted/Typed Name Signature Month Day Yea

E i Form 8700-22 (**. 9/88)^ •• ; •••^&£&&. EQP5110

u £ £ o 4 u i i

ONYX ENVIRONMENTAL SERVICES

Pll

aENenATOR

•pe or print In block letters. (Form designed for use on elite (12-prtch) typewriter.)

SPECIAL WASTE 1 - Generator's US EPA ID No. nnJSSBSftioMANIFEST TICKET kw ,'LLIn In , « « - , !< * TTTT

SOLVAY COKE AND GAS COMPANY . '311 EAST GREENRELD AVENUE SAMEM(LWAUKEE?VVl S32tW

4. Generator's Phone A\A ft/itrwW5. Transporter 1 Company Name 8. US EPA ID Number

I I I I- IONYX ENVIRON MP^1"*1 RVf^R i ir l i ^ l l r j l n t j l n f t ' a ^ g l n g7. Transporter 2 Company Name . 8. US EPA ID Number

• . ' ' - I I I9. Designated Facility Name and Site Address 10. US EPA ID Number

ONYX SPECIAL SERMCESmc' 1 75 MINERAL SPFJNGS DRIVE

11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 1 2. Conn

. HM . ' • ' ' No.a, •'•

b.

c.

: NOW-PCB TRANSFORMER. DOT NON-REGULATED. NONE.NONE

NON-REGULATED MATERIAL, NOM-RCRA, NON-DOT..(DRAINED TRANSFORMER), NONE. NONE

*. * •

. - ' ' . - I

' - IJ. Additional .DBSCripdona for Materials Listed Above / .. fu.

• Srkf ^t«ai/H^rs ^-^^^J b*4 /*n^V4- '•**

KOfMfV c?. - ""?^ 5> Arlt* £l\fj****3 ^ttJS~7b? fOo£\j£. (3k

Or-Jeii* "if^f/'7 / ^- /H/ii Ck»\inj-£ "QM </'5J>7t(» /t&i£.v&- I3te.

2. Page 1.of

•4

A. Manflesl Document Number

Y . 0043604B. Stats Generator's- ID

C. stale Trans. ID iaonnD. Transporter's Phone /n

E. Slate Trans. ID '

F. Transporter's Phone

G. Slate Faculty's 10

ft' H. Facility's Phone

/OlIners

C|M

C M

_L

13, 14Total Unit

Quantity WlA/o

6i /1 160 P

Ol l ^qC Pf

I I

I I

I A

L t-~- 'Waste No.

N O N E

N O N E

I

< â/idjingaode foryVastEic Listed Abova

oW &*&•*$)

15. Special HShdllng Instructions and Additional Information • . '

PACKJNG SUPS ATTACHED FOR CLARIFICATION - EMERGENCY NUMBERS NFOTRAD t-BOD-S35-5DS31 F 'IB5 , f-)i 1_ / • • i-

16. GENERATOR'S CERTIFICATION: I hereby declare mat the contents ol the consignment are Fully and accurately described above byproper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highwayaccording To applicable international and national government regulations.

,,: ' • . — • r-^

5N

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ACI

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Prii*M^Typed Name .• . Signafipfr ^^^ \, . — \ fi

' 1 J. \f* — sU«~ / / ^^\\ l\

17. Transported AeKrtovdedgemenVol Receipt of Matertals — J\ i f 'if}Prlrited^yped Name / ^^^ ^ Jigrjamis— — J/// t {Jr/*

rM^MJKj'.nlszK ' Âi**&l6JJyt~•* *^

^0^

Month Day Year

't

Month Day Year

18. TranspdnerÂcl<no ledd>mem .of Receipt o* Materials . ^ /^\Printed/Typed Name ^ ' ' Signature ( / Month Day Year

t M 1 119. Discrepancy Indlcallon Space

20. Facility Owner or Operator Certification of receipt of materials covered by Ihis manifest except as noted In Item 19.PrlnleO/Typed Name • ->. / ^ / •" Signature /~\ . , ^— \ /I Month Day Year

2-TRANSPOBTER 1 COPYSIGNATURE AND INFORMATION MWST BE LEGIBLE ON ALL COPIES

(MX mJMNW&L &R/EES L.L.C

BFtEttE

1 1 RTFrfi1 1

fi( rA ICT\

(MX location NEMKNEE WIE EPOLTIYAiteEB OFFICE

^MIECTIY ST

|EE2 | 475 |

.£<> S Tfcfrnlagy rapESted j\C Yc L HA END. WMXTBOB2151.

311 GST OTHSFMD PM&LE

(Mb 9999 99939SbabeM SirtiylB ZIP 53204'

a-inrRGL6 Qdgin^ RimVOCS

2. VfestelEneKB3.

4.

lab or Vfeebe Acsa

, SUPLN2315IGII HQait l]b VfeBte: Y HH: N ffl: N OW. N P: N_

IQEte: l.rCDOKRIlSKIEDHIMKKLS1.BHIJSB 2.

5.rtnVfistBctar X Obagpry Mix: N SO.: N

6. H^sical ard dHrirnl prp=rtjes:

a < 2_2 - 5

A 5 - 9d 9 - 12.5e >12.5

sect

cl < .o

b~.8 - 1.0c X 1.0d 1.0- 1.2e > 1.2

aect

Eladi EtrirtCF)a <80b 80- 100c ICO. - 140d 141 -200e >200f X roQaeti

.q-ilirfa0 - 0 % guqpsrki

100 - 100% FffflegMe0 - 0%diffoKed

0 - 0 % adi0 - 0 %\EBft?rFri1ii-ri'|-i1-y

0 - OHIU/lb

FTPP T.iqrid Firg^ 0 tn 0 %eect

StEte H-r>vinl iî GQ3TS Xm1 11qridpf

awcf "eoP

air reactivev^ter iEa±i\e

reactiveiEO±i\e

_ radicactive or NC reguOctad£itrktaip

oddizirg acidpanada ftmar

anonebmLMcstcong

irtelatica tezardic pLE^Liti2Ed.d ~ diris par 40 CFR 268.45h

BrCLFI

%Borine%(Mcrins% Hirrins% Iodine

_X single fiBBB

ty

Top laêr

rrediun(Qil)lcw(vd

X aiid

hiîfeynp)trediun(ail)

solid

mactiimfcil)]cwâsolid

mirrax

Lted oil y/h HOC < 1033 fpn KT > IflOO jpn WIPID. 493575

QHrical QjpKitiai IJ^terine Rdlitart, S=Sfeete Nferire RiMart, OCtae Cepletirg:IHirferlymg FtoKtus CtnstitiHt, Mercere tsE9£P, T=ORI Chemical, C=CEH\ Garcirocen]

CtnstituHts F&gss Utits

S,T,U,OIL, ILBSCKTttGEOMHCRBsFOHD HKHEMiIS OHH^MT Bf HKWW)mifsis

1.001.00

SB. 00

5.002.00

S9.00

%,%%

QtBC.

8. Is ttevfisbESbEanbeirginpited irto9. Edes t±E\«8sbEstiesncD±ainFCfe

PCS C£nH±isticn 500.0040OR?

10. Is the vastestcsn subject to the Nfenre RiMart11. Is the vasbstrean atjject to EenzETE KE9M3?

If i€s, is the vastestrean subject to NT1 fi rnt-lnVOrtual! GmErtraUm .00

12. Is the v\asbEStreana±rject to Rm aJbpart CT co±idls?

Lytical Nfettod?Qêistcr

B. Is YesNDXNDX

14. Gtrtaoiner

Irijpirg : UrLtsHM

.00 EferYear CteTineEESTOHKN:

15. Jnfr.itifi .icn

I hereby certify that all infomBticn aimittad. in this ard. all attachal ctnnsts contains trie ard accurate cfescdpticns cf thisvaste. Ay sanple sJmtted is reptBsartatixe as ctfirFrt in 40 OR 261 - pardix I or by usirg an agjnalert nethoi ALL relaa±infcznBticn recportirg krvn or aêcted haaicfe in the pcsasasicn cf the cpneratcr has bean disdc^d. I aiiirrias sanplirg cf

JSarpjrpcss cf TFrprt~ifirHt'irn.

SLgrature

If aapra-od fer narEgaret, Q^KX hss all the iby this prcfile.

r/psmits and ILCHBS for the vaste that has been ch3za±erizHi ard

WIP^D.

UF lÛfr O.

STATE OF WISCONSINChapter 291, Wis. Stats.Form4400-66P Rev. 1-99

ALL COPIES MUST BE LEGIBLE,PLEASE TYPE

State of WisconsinDepartment of Natural ResourcesBureau of Waste Management •Box 8094Madison, WI 53708

FOR DNR USE ONLY

Fon gned for use on elite (12-pitch) typewriter. Form Approved. OMB No. 2050-0039.Manifest

Document No.II I fl

Generator's US EPA ID No.UNIFORM HAZARDOUSWASTE MANIFEST

Information in the shaded areasis not required by Federal law.

3. Generator's Name and Mailing AddressSOLVAY COKE AMD GAS COMPANYJ11 I-AS F <3fveENFIBJp AVENUEMILWAUKEE, WI 53204

Site Location If Different

4. Generator's Phone6. US EPA ID Number

NJD080fl311flO5. Transporter 1 Company Name

ONYX F.NMRONfrlEN r,AI_ SVCS I I 08. US EPA ID Number7. Transporter 2 Company Name

9. Designated Facility Name and Site AddressONYX ENMRONMEN TAL SERVICESWt?4 NW451 BOUNDARY RO.

10. US EPA ID Number

W 00039871*18

TotalNo. Type Quantity11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number)

WAS TE AERO60UB. FLAMMABLE.(EACH NOT EXCEEDING 1L CAPACITY), 2 1ON1050

WAS re PROPANE. 2.1. UN 1978

c- RO. WASTE FLAMMABLE UQUIOS. n.o.s . (GA8OUNE). 3. UN1993, II. (0001)

WASTE FI.AMMAW.E LJQWDS. n.o.s.. 3. UN19fl3.lli o n Q a

15. Special Handling Instructions and Additional Information

PACWNG SUPS ATTACHED FOR CLAHFICATION - EMERGENCY NUMBER-)NFOTRAC: 1 QOO-5;»-5053PC10S W TECH SERMCES

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by propershipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to ap-plicable international and national governmental regulations and according to the requirements of the Wisconsin Department of Natural Re-sources. If I am a large quantity generator, I also certify that I have a program in place to reduce the volume and toxicity of waste generated to thedegree I have determined to be economically practicable and I have selected the practicable method of treatment, storage, or disposal currentlyavailable to me which minimizes the present and future threat to human health and the environment;

OR, if I am a small quantity generator, I have made a good faith effort to minimise my waste generation andselect the best waste management method that is available to me and that I can afford.

DatePrinte^Typed Name & Position Title Month Diy Year

17. TRANSPORTER 1 Acknowledgement of Receipt of Materials DatePrin yped & Position Title

18. TRANSPORTER 2 Acknowledgement of Receipt of Materials

Month Day Year

7 DatePrinteoVTyped Name & Position Title Signature Month Day Year

I I I I I I I19. Discrepancy Indication Space

[ 20. FACILITY OWNER OR OPERATOR: Certification of receipt of hazardous materials covered by this manifest except asnoted in Item 19.

i .intedyTyped Name & Position Title SignatureDate

Month Day Year

1 1 I I I

'iPA Form 8700-22 (Rev. 9-88) Previous editions are obsolete. Copy Distribution: 1 - Generator send to Wis. DNR_ „ . „ . . 2 — Generator retainEmergency 24 Hour Assistance 3 _ Facility gend to wig DNR

and Spill Reporting COPY 3 - Copies 1 & 3 mail to Wis. DNR at above address.Telephone Number (800)943-0003 iV\GUTY SEND TO WI DNR

4 — Facility retain5 — Facility send to Generator6 — Transporter retain

i VtfA;-.! l>: iViAfUF-'tiST1 :>''-.'i:ciiil!:'iit<>ri Shut:;

':.;.'!>;>r,>'i>; C ' 'S '"'.I'.11 >'.' ;'i'-'

WIM000508215

SOLVAY COKE AND GAS COMPANY311 EAST GREENFIELD AVENUEMILWAUKEE.WI 53204

(414)845-0835

I'M. i ri:,i•,.'•,(•„ n!er I Company Name

Pti. fYi.i''SpM'l'';r 2 Horiipriny Narno

L

| 04001 i 2 of* 3 ; .,-..

W1K363294

;.';'• UK-riP.u ii> NiiinijHi > N. Slate Tianu ID

| O. Ti'ans. Phono

";'>7'Ti6>7'A ]D~Nufnbor | "p~"State"frans:nD

SAME

"S. "DV-"DOT Dt'scriplion (Including Proper Shipping Afeirm?, H,i,',ir>J Cijt-b. nti<i ID A/;..

(5. Trans. Phone

30 :"i1 il.lot.jl j iliiit : VI:, }•,(-.

.

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X

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X

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WASTE FLAMMABLE LIQUIDS, n.o.s.. 3, UN1993.II•

L^FLAMMABLE LIQUIDS, n.o.s., (PETROLEUM

DISTILLATES). 3. UN1993. II

WASTE TOXIC SOLIDS. ORGANIC, n.o.s.. (LEAD.CHROMI UM), 8.1 , UN281 1 . Ill

RQ, WASTE SULFUR! C ACID. 8, UN2796. II . (D002)

WASTE CORROSIVE LIQUID. ACIDIC, INORGANIC,n.o.s.,8, UN3284.II

RQ. WASTE MERCURY. 8, UN2809. Ill , (D009)

OIL, n.o.s.. NONE. NONE

NON-REGULATED MATERIAL. NON-RCRA. NON-DOT.,(WATER), NONE, NONE

NON-REGULATED MATERIAL, NON-RCRA. NON-DOT.,NONE. NONE

I

0 0 2J D M

I

0 0 1

0 0 1

0 0 4

0 0 1

0 0 1

D O S

0 0 1

0 0 2

A;jd lioral Descriptions for Materials Listed AboveA) SA 493575 CWDDPK3 B) Ul 888487 CWDFUELS C) S/E 493575 CWDDPK8 D007D008 D)L/C822578STB001912 E) S/C 493575 CWDOPKB A F) S/E 493575CWDSUPHG G) LA 822579 CWDFUELS H) LA 885849 CWDOZLNHL I )SA 493575CWDDPI-WR

D V

D M

D F

D F

D F

D M

D F

C V\

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0 0 1 1 (j G

" ^ ' I

D001'

i

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1 1

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0 0 0 0 f

0 0 0 3 (

0 0 4 9 i

0 0 0 5 J

0 2 0 0 C

D008

LG l •.1. ...i. ..

G

G

G

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P

D002

D002

0000

NONE

NONE

INONE

;f. Handling Codas for Wastes l.i.-jlnd At> >•• • • • ;

T)2. Spt'i.Tal "l-ldiitlling Instructions and Additional InformationPACKING SUPS ATTACHED FOR CLARIFICATION - EMERGENCY NUMBEFMNFQTRAC: 1-800-535-5053

i. Tiv iViAiL TO - THD"3 >n'.;\:H-

WIM000508215 04001 3 of- 3 ! ' • • • •

SOLVAY COKE AND GAS COMPANY311 EAST GREENFIELD AVENUEMILWAUKEE.Wt 53204

WIK363294lo i i«ildi : .Uoi '. 'i ;

|414)845-0.835j .'4. ' ! " > •tii-'-iKiniii 1 iJofi'iptinv 'x'<

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UNIVERSAL WASTE-BATTERIES, (LEADACID BATTERIES),NONE, NONE

EMPTY DRUMS. NONE. NONE

NON-REGULATED MATERIAL, NON-RCRA. NON-DOT.,(RAGS. OIL). NONE. NONE

NON-REGULATED MATERIAL. NON-RCRA. NON-DOT..(TAR), NONE. NONE

;:0 (.^nlaino.s M^ ^^

j0 0 3| C W

0 0 7

0 0 2

0 0 1

3. Additional Descriptions for Materials Listed Above

A) SA 493678 CWDLEADAQD B) SA 885850 CWDORCEMPTY C) SA 885651CWDWTENHS D) SL>- 888488 SRRBO7828

D M

D M

D M

0 3 0 0 Gj p

0 0 3 8 5J c

. . J ....

0 0 1 1 0 J G

0 0 0 5 SJ G

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1

IT. Handling Codes K.I Was

NONE

NONE

NONE

NONE

32. Spe<;ial Handling Inatructions di'id Acifjilional Informntion

PACMNG SUPS ATTACHED FOR CLARIRCATION - EMERGENCY NUMBE^NFOTRAC. 1-800-535-5053

Land Disposal Restriction Notification Form

Gowrator Name SOLVAY COKE AND GAS COMPANY Man Doc No 04001

EPA ID Number \MM000508215 Manifest WIK363294

This notice is being provided in accordance with 40 CFR 268.7 to inform you that this shipment contains wasterestricted from land disposal by the USEPA under the land disposal restriction program. Identified below foreach container is the designaticn of the waste as a wastewater or non-wastewater, the Clean Water Act (CWA)permit flatus associated with the treatment/disposal facility, applicable waste codes and any correspondingsubcategories, list of any FOOT -F005 solvent constituents that are present in the waste, and any underlyinghazardous constituents (UHC) that are present

Container Number WO-0487045000-003

WIP / Approval Code:Form Designation / CWA Status:Waste Codes (Subcategcries):

Constituents CF001 - F005):UHCs Present:Treatment Requirements:Additional Notices:

Container NumberWO-0487045000-004WIP / Approval Code:Form Designation / CWA Status:Waste Codes (Subcategories):

Constituents (F001 -FOGS):UHCs Present:Treatment Requirements:Additional Notices:

Container Number WO-0487045000-005WIP/Approval Code:Form Designation / CWA Status:Waste Codes (Subcategories):Constituents (F001 - FOOS):UHCs Present:Treatment Requirements:Additional Notices:

Container NumberWO-0487045000-007WIP / Approval Code:Form Designation / CWA Status:Waste Codes (Subcategohes):Constituent* (F001 - FOOS):UHCs Present:Treatment Requirements;Additional Notices:

493578/CWDAEROSOLNon-Wastewater/ Non-CWAD001 (IGNITABLE CHARACTERISTIC WASTE, LIQUIDS >=10% TOG PER 261.2 1(a)(1))NoneNot ApplicableRestricted waste requires treatment to applicable standards.

493576 / CWDSUPHGNon-Wastewater/ Non-CWAD009 (INORGANIC MERCURY >=260MG/KG TOTAL HG THATINCLUDES INCINERA TOR & RMERC RESIDUES)NoneNoneRestricted waste requires treatment to applicable standards.

493576 /CWDDPK8IANon-Wastewater/ Non-CWAD002NoneNoneRestricted waste requires treatment to applicable standards.

493576 / CWDDPK6Non-Wastewater/ Non-CWAD006 (NONE), D007, D008 (NONE)NoneNoneRestricted waste requires treatment to applicable standards.

Page __!_ of 3

Container Number WO-0487045000-008WIP / Approval Code: 493576 / CWDDPK3Fcrrn Designation / CWA Status: Non-Wastewater / Non-CWA

Waste Codes (Subcategcries);

Constituents (F001 - F005):UHCs Present:Treatment Requirements:Additional Notices;

Container Number WO-0487045000-009

WIP/ Approval Code:Form Designation / CWA Status:Waste Codes (Subcategories);

Constituents (F001 - F005):UHCs Present:Treatment Requirements:Additional Notices:

Container Number WO-0487045000-010WIP/Approval Code:Form Designation / CWA Status:Waste Codes (Subcategories);


Container NumberWO-0487045000-011

WIP / Approval Code:Form Designation / CWA Status:Waste Codes (Subcategories):Constituents (F001 - F005):UHCs Present:Treatment Requirements:Additional Notices:

Container Number WO-0487045000-016WIP / Approval Code:Form Designation / CWA Status:Waste Codes (Subeategories):

Constituents (FOOT - F005);UHCs Present:Treatment Requirements:Additional Notices:

D001 (IGNITABLE CHARACTERISTIC WASTE, LIQUIDS >-10%TOCPER261.21(a)(1))NoneNot ApplicableRestricted waste requires treatment to applicable standards.

493576 / CWOOPK3Non-Wastewater/ Non-CWA0001 (IGNITABLE CHARACTERISTIC WASTE, LIQUIDS >=10% TOC PER 261.2 1(a}(1))NoneNot ApplicableRestricted waste requires treatment to applicable standards.

493576 / CWDDPK3Non-Wastewater/ Non-CWAD001 (IGNITABLE CHARACTERISTIC WASTE, LIQUIDS >=10% TOC PER 261.21 (a)(1 J)NoneNot ApplicableRestricted waste requires treatment to applicable standards.

622578/STB001912Non-Wastewater/ Non-CWAD002NoneNoneRestricted waste requires treatment to applicable standards.

888487 / CWDFUELSNon-Wastewater/ Non-CWAD001 (IGNITABLE CHARACTERISTIC WASTE, LIQUIDS >=10% TOC PER 261.2 1 (a)(1))NoneNot ApplicableRestricted waste requires treatment to applicable standards.

Page _2_ of _3._

container H urn dtsr WO-0487045000^13

WIP / Approval Code:Forrn Designation / CWA Status:Waste Codes (Subcategories);

Constituents (F001 - F005):UHCs Present;Treatment Requirements:Additional Notices:

Container NumberWO-0487045000-019WIP / Approval Code:Form Designation / CWA Status:Waste Codes (Subcategories):


493576 / CWDPROPANENon-Wastewater/ Non-CWAD001 (IGNITABLE CHARACTERISTIC WASTE, LIQUIDS >=10% TOC PER 261.2 1(a)(1))NoneNot ApplicableRestricted waste requires treatment to applicable standards.

888670/CWDFUELSNon-Wastewater/ Non-CWA0001 (IGNITABLE CHARACTERISTIC WASTE, LIQUIDS >=10% TOC PER 261.2 1(a)(1))NoneNot ApplicableRestricted waste requires treatment to applicable standards.

I hearby certify that all information in this and associated land disposal restriction documents is complete andaccurate to the beat of my knowledge and information.

Signature

Title Date ro^L

Page _3_ of _3_

ONYX ENVIRONMENTAL

RecertificfrtionONYX LOCATIONInvoice Address

WASTESTREAM INFORMATION

Disposal Cods

Manifest from - blank if direct

Generator EPA ID WIM0005Q8215

1. Generator Name SOLVAY COKE AND GAS COMPANY

Addrsn 311 EAST GREENFIELD AVENUE

CHy MILWAUKEE

SIC Cod* 9999

State Wattestream*

State Wl Country US Zip 53204

Source G11

IstNAICSCodt

Origin

2nd NAICS Code

Form W219

3rd NAICS Code

System Type

2. Waste Name UQ1JID WAX WITH PETROLEUM DISTILLATES Lab or Warts Area

3. Process Generating Waste UNUSED MATERIAL

4. Shipping Name FLAMMABLE LIQUIDS, n.o.s

Hazard Clan 3

RQ Desc 1.

UN/NA Number UN1993 Pack Group

2.

RQ Amount (Ib*.) 0

DOT Dae: 1. PETROLEUM DISTILLATES 2.

Waete Codec D001-IL

WastewatsrfY/N) N Sub-Category IL- IGNITABLE CHARACTERISTIC WASTE. LIQUIDS >= 10% TOC PER 261

6. Physical and chemical properties:

pH Lo 5 Specific Gravity Lo 0

pH HI 9 Spa

Solids:

Suspended Lo 0

Suspended Hi 0

Physical Stats:

Physical State 1

efflc Gravity Hi 0

Flash Point (F) Lo 100 Water Solubility

Flash Point (F) HI 140 Water Solubility

SetUeable {%) Lo 0 Dissolved (%) Lo 0 X Ash Lo

SetUeable (%) Hi 0 Dissolved (*) HI 0 % Ash HI

L - liquid

Physical State 2

Physical State 3

Halogen*:

Bromine (%) Lo

Bromine (*) Hi

'or Intensity

U ascription

Hazardous Characteristics:

Haz. Char. 1

Haz.Char.2

Haz. Char. 3

Chlorine (%) Lo Fluorine (%)Lo Iodine (*) Lo

Chlorine (% ) H 1 Fluorine (%) H 1 Iodine (%) H 1

Lo 0 BTU/lbLo 0

HI 0 BTU/lbHI 0

0 Free Liquid (H) Lo 95

0 Free Liquid (%) HI 100

Layers: B - Si-layered

Top C - low (water)

Middle

Bottom

Color 1 PNK

Color 2

Intensity

Contains Used Olr? No HOC < 1000 ppm HOC > 1000 ppm

1 Qf WIP NO. 888487

7. Chemical Composition;

Component

LIQUID WAXESPETROLEUM DISTILLATESWATER

.flier:

8. Is the vosteitream being imported into the U SA?

Low252510

Yas/No

No

High

757525

%/PPM/PPB

I

9. D oes the wattestream contain PCBs regulated by 40 CPR?

10. Is the wartestream subject to the Marine Pollutant Regulations?

11. Is the wattettream subject to Benzene NE5HAP?

If Yet, Is the WMtestream subject to Notification and Control Regs?

12. Is the waUettream subject to RCRA sutapart CC controls?

CC approved analytical method? General Knowledge?

13. Is the wattastream from a CERCLA or state mandated cleanup?

No PCB concentration:NoNo Benzene concentration:

No

No

Vol. Org. Cone., If known:

0.00 PPM

0.00 PPM

0.00 PPMW

U. Container Information (Identify UN container marking if known)

Packaging: Bulk Solid Type/Size: Bulk Liquid:

Other

Type/Size: Drum: Typa/Size:

Shipping Frequency: Units Per Month Quarter Year One Time Other

16. Additional Information:

'•* analytical or an MSDS available that describes the waste? Yes No If Yes. please attach.

AERATOR CERTIFICATION

I hereby certify that all information submitted in this and all attached documents contains true and accurate descriptions ofthis waste. Any sample submitted is representative as defined in 40 CFR 261 -Appendix I or by using an equivalent method.All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. Iauthorize sampling of any waste shipment for purposes of recertification.

NAME (Print or Type) PHONE DATE

—SIGNATURE TITLE

FACILITY NOTIFICATION

If approved for management, ONYX has all the necessary permits and licenses for the waste that has been characterizedand identified by this profile.

TSDF PROCESSING USE ONLY: PPE REQUIRED? DESCRIBE.

Page 1 of 2 WIP NO. 883487

ONYX ENVIRONMENTAL

WASTESTREAM INFORMATION} RecertificationONYX LOCATION D

{_} Invoice Address ADDRESS CITY ST

Q Manifest from - blank if direct

sposal Coda

IONYX TSDF requested Technology requested Generator No. 518683

1. Generator Name 5QLVAY COKE AND GAS COMPANY

Generator EPA ID W1MOOQ5Q8215

Generator State*

Address 311 EAST GREENFIELD AVENUE

CHy MILWAUKEE

State Wattattream*


SIC Code 9999

Source G11

lit NAICS Codt

Origin

2nd NAICS Cod*

Form W203

3rd NAICS Cod*

Syitem Type _

2. Watte Name GASOLINE Lab or Watte Area

Unused gasoline3. Process Generating Wasts

4. Shipping Name FLAMMABLE LIQUIDS, n.o.s.

Hazard Clan 3 UN/NA Number UN1993 Pack Group II RQ Amount (Ibs.) 100

RQDesc

DOTDssc:

1.

1. GASOLINE

2.

2.

Warts Codes D001-IL

WastMvaterfWN) N Sub-Category IL- IGNITABLE CHARACTERISTIC WASTE. LIQUIDS >= 10% TOC PER 261.21(a)fl)


pH Lo 5 Specific Gravity Lo 1

pH HI 9 Spa

Solids:

Suspended Lo 0

Suspended Hi 25

Physical State:

Physical State 1

title Gravity HI 1

Flash Point (B Lo 100 Water Solubility

Flash Point (F) HI 140 Water Solubility

SetUeable (%) Lo 0 Dissolved (%) Lo 0 X Ash Lo

SetHeable(%) HI 25 Dissolved (%) HI 25 % Ash HI

L - liquid

Physical State 2

Physical State 3

Halogens:

aromlnft(%) Lo

Bromine {%) HI


Haz. Char. 1

Haz.Char.2

Haz. Char. 3

Chlorine (%) Lo Fluorine (%) Lo Iodine (%) Lo

Chlorine (%) HI Fluorine (*) HI Iodine (%) HI

dor Intensity C strong

Description GASOLINE

Lo 0 BTU/IbLo 10001

HI 10 BTU/lbHI 99999

0 Free Liquid (%) Lo, 75


Layers: C - Single- Phase

Top C - low (water)

Middle

Bottom

Color 1 VAR

Color 2

Itttftiwny

Contains Used Oil? No HOC < 1000 ppm HOC > 1000 ppm _

1 .if 2 WIP NO. 388670

1. Chemic.il Composition;

Component

GASOLINEGASOLINE

ter:

o. Is thewntntreatn being Imported Into th* USA?

Low100100

Yw/No

No

High

100100

%/PPM/PPB

%%

9. D oes the wartestream contain PCBi regulated by 40 CPR?

10. Is the wntettream subject to the Marine Pollutant Regulations?11. Is tha wastestream subject to Benzene NESHAP?

If Yes, Is the wsntestream subject to Notification and Control Reqs?

12. Is the wBtestream subject to RCRA subpart CC controls?


13. Is (he wattestream from a CERCLA or state mandated cleanup?

No PCB concentration: 0 DO PPM

NoNo Benzene concentration: 0.00 PPM

No Vol. Org. Cone., if known: 000 PPMW

No

14. Container Information pdentify UN container marking if known)

Packaging: Bulk Solid Type/Size: Bulk Liquid: Typa/Siza:

Other.

Drum: Type/Size:

Shipping Frequency. Units Per Month Quarter Year One Time Other


Is analytical or an MSDS available that describes the waste? Yes _ No _ If Yes. please attach.

AERATOR CERTIFICATION

êreby certify that all information submitted in this and all attached documents contains true and accurate descriptions ofthis waste. Any sample submitted is representative as defined in 40 CFR 261 -Appendix I or by using an equivalent method.All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. Iauthorize sampling of any waste shipment for purposes of recertification.


TITLE



TSDF PROCESSING USE ONLY: PPE REQUIRED? HO DESCRIBE:

Pago 2 uf 7. WIP NO. 888670

ONYX ENVIRONMENTAL^ ONYX

WASTESTREAM INFORMATION") Recartification

ONYX LOCATION Disposal Cod8Q Invoice Address " ADDRESS CITY ST

r~j Manifest from - blank if direct IONYX TSDF requested Technology requested Generator No. 518663

1. Generator Nana SQLVAY COKE AND GAS COMPANY

Generator EPA ID WIMQQQ5QB21S

Generator State*


City MILWAUKEE

State Wastestream*

State W Country US Zip 53204

SIC Cod* 9999

Source G11

IstNAICBCod*

Origin

2nd NAICS Code

Form W403

3rd NAICS Cod*

System Type

2. Wart* Nam* TAR Lab or Wart* Area

3. Proceu Generating Wart* Unused product.

4. Shipping Nam* NON-REGULATED MATERIAL. NON-RCRA.NON-DOT.

Hazard Clan NONE UN/NA Number NONE Pack Group RO Amount (Ib*.) Q_

RQOMC

DOT Dae

1.

1. TAR

2.

2.

Wart* Coda* NONE

Wwt*wat*r(Y/N) N Sub-Category


pH Lo 5 Sp»

pH Ht 9 Spa

Solids:

Suspended Lo 0

Suspended Hi 0

Physical State:

Physical State 1

dflc Gravity Lo 1

cfflc GrawnV Hi 1

Flash Point (F) Lo 0 Water Solubility Lo 0

Flash Point (F) Hi 0 Water Solubility HI 0

BTU/lb Lo 0

BTU/lb HI 0

S«ttl*at>l* ft,) Lo 100 Dissolved (It) Lo 0 % Ash Lo 0 Fr«* Liquid {%) Lo 0

Settteable (X) HI 100 Dissolved {%) HI 0 % Ash HI 0 Fre* Liquid {%) HI 0

M - semi-solid

Physical State 2

Physical State 3

Halogens:

Bromine (%) Lo

Bromine (*) HI

*>dor Intensity

Description

Hazardous Characteristics: Layers: C - Single-Phase

Haz. Char. 1 Top A - high (syrup)

Haz. Char. 2 Middle

Haz. Char. 3 Bottom

Chlorine (X)Lo Fluorine (%)Lo Iodine (%)Lo

Chlorin*(%)HI Fluorin* (%) HI Iodine (%) HI

Color 1 BLK

Color 2

Intensity

Contains Used Oil? No HOC < 1000 ppm HOC > 1000 ppm

1 nf WtP NO. 388486

7. Chemical Composition:

Component

TAR

Low High %/PPM/PPB100 100 %

>er:

I* the wnteitrewn being Imported Into the USA?

9. 0 oat the wartsttream contain PCBs regulated by 40 CPR?

10. Is the wsBttftream subject to the Marine Pollutant Regulations?

11. Is the waitestream subject to Benzene NESHAP?

If Yn, hi the wartestream subject to Notification and Control Reqs?

12. Is me wasteBtream subject to RCRA subpart CC controls?


13. Is the wattettream front a CERCLA or state mandated cleanup?

Yes/No

No

No PCB concentration:

No

No Benzene concentration:

No Vol. Org. Cone., if known:

No

0.00 PPM

0.00 PPM

0 00 PPMW

14. Container Information (Identify UN container marking if known)

Packaging: Bulk Solid Typa/Siza: Bulk Liquid:

Other

Typa/Siza: Drum: Typa/Slza:

Shipping Frequency: Units Par Month Quarter Year One Time Other


Is analytical or an MSDS available that describes the waste? Yes No If Yes. please attach.

"•FNERATOR CERTIFICATION

ereby certify that all information submitted in this and all attached documents contains true and accurate descriptions ofthis waste. Any sample submitted is representative as defined in 40 CFR 261 -Appendix I or by using an equivalent method.All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. Iauthorize sampling of any waste shipment for purposes of recertification.


""SIGNATURE" TITLE



TSDF PROCESSING USE ONLY: PPE REQUIRED? _NO DESCRIBE:

Pagu 2 of 2 WIP NO. 888486

") RecertificationONYX LOCATION

Q Invoice Address

[~] Manifest from . blank if direct

ONYX ENVIRONMENTAL*r ONYX


ADDRESSDisposal Code

Generator EPA ID WIMOOOS06215ONYX TSDF requested Technology requested

1. Generator Mama 50LVAY COKE AND GAS COMPANY


CHy MILWAUKEE

SIC Code 9999

Source G32

lit NAICS Code

Origin

State Wl

2nd NAICS Code

Form W310

3rd NAICS Code

System Type

2. Warts Name OILY RAGS Lab or Watte Area

3. Process Generating Watte Clean up of oil spills.

4. Shipping Name NON-REGULATED MATERIAL. NON-RCRA.NON-DOT

Hazard Clan NONE UN/NA Number NONE Pack Group RQ Amount (Ibs.) 0_

RQ Dssc:

DOT Owe

1.

1. RAGS

2.

2. OIL

Waste Code* NONE

Wastswater (V/N) N Sub-Category


pH Lo 5 Sp»

pH HI 9 Sp*

Solids:

Suspended Lo 0

Suspended HI 0

Physical State:

Physical Stale 1

cflfc Gravity Lo 1

chic Gravity HI 1



BTU/lb Lo 5000

BTU/lb HI 10000

S*W«able ft) Lo 95 Dissolved ft) Lo 0 % Ash Lo 0 Fr»* Liquid (*) Lo 0

SeWeableW) Hi 100 Dissolved (%) Hi 0 % Ash Hi 0 Free Liquid (%) HI S

S - solid

Physical State 2

Physical State 3

Halogens:

Bromine ft) Lo

Bromine ft) HI

Odor Intensity B - mild

Jescrlptlon OILY

Hazardous Characteristics: Layers: C - Singja-Phase

Haz. Char. 1 Top D - solid

Haz. Char. 2 Middle

Haz. Char. 3 Bottom

Chlorine ft J Lo Fluorine (%) Lo Iodine ft) Lo

Chlorine ft) Hi Fluorine ft) HI Iodine ft) Hi

Color 1 VAR

Color 2

Intensity


1 >'f WIP NO. 885651


Component

OIL, LUBRICATINGOIL SOAKED RAGS

Low

095

High

5100

%/PPM/PPB

%%

or:

-. hi the waiteitream being Imported Into the USA?

9. Does the wartettream contain PCBs regulated by 40 CPR?

10. d the waiteitream lubject to the Marine Pollutant Regulation!?

11. Is the warteetream subject to Benzene NESHAP?

If Yet, hi the waiteitream subject to Notification and Control Reqs?

12. It the wattattream subject to RCRA subpart CC controls?


13. Is the wacteitream from a CERCLA or state mandated cleanup?

Yw/No

NoNo PCB concentration: 0 00 PPM

No

No Benzene concentration: 0.00 PPM

No Vol. Org. Cone., If known: 0.00 PPMW

No

U. Container Information (Identity UN container marking if known)

Packaging: Bulk Solid Typa/Size: Bulk Liquid:

Other.

Type/Size: Drum: Typa/Size:

Shipping Frequency. Units Per Month Quarter Year Ona Time Other


Is analytical or an MSDS available thai describes the waste? Yes No If Yes. please attach.

-NERATOR CERTIFICATION

,ereby certify that all information submitted in this and all attached documents contains true and accurate descriptions ofthis waste. Any sample submitted is representative as defined in 40 CFR 261 -Appendix I or by using an equivalent method.All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. Iauthorize sampling of any waste shipment for purposes of recertification.


v-SrGNATURE TITLE


If approved for management ONYX has all the necessary permits and licenses for the waste that has been characterizedand identified by this profile.

TSDF PROCESSING USE ONLY: PPE REQUIRED? _NO DESCRIBE:

P.3Q9 1 Of 2 WIP NO. 885651

1 RecertifiralionONYX LOCATION

|_J Invoice Address

Q Manifest from - blank if direct

ONYX TSDF

ONYX ENVIRONMENTAL*r ONYX


Disposal Code

Generator EPA ID WIMOOQ5Q8215



City MILWAUKEE

StateWattestream*


2.

SIC Code 9999 1st NAICS Code

Source 649 Origin

Watt* Nam* WATER

2nd NAICS Code 3rd NAICS Code

Form W113 System Type

Lab or Waste Area

3. Process Generating Warte RAIN WATER

4. Shipping Nam* NON-REGULATED MATERIAL. NON-RCRA.NON-DOT.

Hazard (

RQDesc:

DOT Owe:

:iass NONE UN/NA Number NONE Pack Group

1.

1. WATER

RQ Amount (Ibs.) 0

2.

2.

Waste Codes NONE

Wastewat*r(Y7N) N Sub-Category

8. Physical and ehsmlca

pH Lo 5 Sp»

pH HI 9 Spa

Solid*:

Suspended Lo 0

Suspended HI 0

Physical State:

Physical State 1

i properties:

dtlc GrawnV Lo 1

dflc Gravity Hi 1

Flash Point (F) Lo 0 Water Solubility

Flash Point (F) Hi 0 Water Solubility

SeWeabls (%) Lo 0 Dissolved (%) Lo 0 % Ash Lo

StttUeablsft) HI 0 Dissolved {*) HI 0 % Ash HI

L- liquid

Physical State 2

Physical State 3

Halogens:

Bromine (%)L«

Bromine (%) HI

•lor Intensity

-Description


Haz. Char. 1

Hn.Char.2

Hw. Char. 3

Chlorine (%) Lo Fluorine (X) Lo Iodine (%) Lo

Chlorine (%) HI Fluorine (%) HI Iodine {%) HI

Lo 0 BTU/lbLo 0

HI 0 BTU/lbHI 0

0 Free Liquid (%> Lo 75


Layer*: C - Sinalo-Phasa

Top C - low (water)

Middle

Bottom

Color 1 CLR

Color 2

Intensity

Contains Used Oil? No HOC < 1000 ppm HOC > 1000 oom

1 Uf WIP NO. 88564Q


Component

WATER

Low

100High

100

%/PPM/PPB

%

liar

.. Is the wartettream being Imported into the USA?

9. D oas the wattestream contain PCBs regulated by 40 CPR?

10. to the wajtettream subject to the Marine Pollutant Regulations?

11. to thewasteBtream subject to Benzene NESHAP?

W Yei, Is the wvtestream subject to Notification and Control Reqs?

12. Is the waitartream subject to RCRA subpart CC controls?


13. Is tha waitettraam from a CERCLA or state mandated doanup?

Yw/No

No

No PCB concentration*.NoNo Benzene concentration:

No

No


0.00 PPM

0.00 PPM

0.00 PPMW

14. Container Information (Identify UN container marking if known)

Packaging: Bulk Solid Type/Size. Bulk Liquid: Type/Size:

Other

Drum: Typo/Size:

Shipping Frequency: Units Per Month Quarter Year One Time Other


Is analytical or an MSDS available that describes the waste? Yes No If Yes. please attach.

GENERATOR CERTIFICATION

jereby certify that all information submitted in this and aH attached documents contains true and accurate descriptions ofthis waste. Any sample submitted is representative as defined in 40 CFR 291 -Appendix I or by using an equivalent method.All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. Iauthorize sampling of any waste shipment for purposes of recertification.

NAME (Print or Type) PHONE ATE

TITLE



TSDF PROCESSING USE ONLY: PPE REQUIRED? _N° DESCRIBE:

2 ot 2 WIP NO. 885649

* RecsrtificationONYX LOCATIONInvoice Address

ONYX ENVIRONMENTAL*T ONYX


ADDRESSDisposal Coda

(~1 Manifest from - blank if direct

Generator EPA ID WIMOQQ5Q821SONYX TSDF requested Technology requested


Addren 311 EAST GREENFIELD AVENUE

CHy MILWAUKEE

SIC Code 9999

Source G09

1st NAICS Code

Origin

Stale Wl

2nd NAICS Code

Form W307

3rd NAICS Code

System Type

2. Watte Name EMPTY DRUMS

3. Proem Generating Waste EMPTY DRUMS

4. Shipping Name EMPTY DRUMS

Hazard Clan NONE

RQDssc: 1.

Lab or Waste Area

UN/MA Number NONE Pack Group

2.

RQ Amount (Ibs.) 0

DOT Owe: 1.

Waste Codes NONE

Wastewatsr(WN) N Sub-Category


pH Lo 0 Sp*

pH HI 0 Sp*

Solids:

Suspended Lo 0

Suspended Hi 0

Physical State:

Physical State t

Physical State 2

cffie Gravity Lo 0

dffc Gravity HI 0



BTU/lb Lo 0

BTU/lb HI 0

Sefflaable ft) Lo 0 Dissolved ft) Lo 0 % Ash Lo 0 Free LInuld ft) Lo 0

Settteable ft) Hi 0 Dissolved ft) HI 0 X Ash HI 0 Free Liquid ft) HI 0

S - solid

Physical State 3

Halogens:

Bromine ft) Lo

Bromine ft) HI

~*<or Intensity

Ascription

Hazardous Characteristics: Layers: C - Single-Phase

Haz. Char, t Top

Haz. Char. 2 Middle

Haz. Char. 3 Bottom

Chlorine ft) Lo Fluorine ft) Lo Iodine ft) Lo

Chlorine ft ) HI Fluorine ft) HI Iodine ft) HI

Color 1 BLK

Color 2

Intensity


Paao 1 of WIP NO. 885650

7. Chemical Competition;

Component

EMPTY METAL DRUM

Low

100

High

100%/PPM/PPB

%

. to the wartestreant being Imported Into the USA?

9. Oo« the wastestream contain PCB* regulated by 40 CPR?

10. r* the wwrtntrewn subject to the Marine Pollutant Regulations?

11. Is the waBtatream subject to Benzene NESHAP?

If Yn, ts the wwtestream subject to Notification and Control Reqs?

12. hi the wattattream subject to RCRA subpart CC controls?


13. Is the wastettraam from a CERCLA or state mandated cleanup?

Yw/No

No

No PCB concentration:

No

No Benzene concentration:

No

No


0.00 PPM

0.00 PPM

0.00 PPMW

14. Container Information (Identity UN container marking if known)

Packaging: Bulk Solid Type/Size: Bulk Liquid:

Other

Type/Siza: Drum: Typa/Size:

Shipping Frequency: Units Par Month Quarter Year One Time Other


Is analytical or an MSDS available that describes the waste? Yes No If Yes. please attach.GENERATOR CERTIFICATION

nereby certify that all information submitted in this and all attached documents contains true and accurate descriptions ofthis waste. Any sample submitted is representative as defined in 40 CFR 261 -Appendix I or by using an equivalent method.All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. Iauthorize sampling of any waste shipment for purposes of recertification.

NAME (Print or Type) PHONE DAT

SIGNATURE TITLE


If approved for management ONYX has all the necessary permits and licenses for the waste that has been characterizedand identified by this profile.

TSDF PROCESSING USE ONLY: PPE REQUIRED? .NO DESCRIBE:

P.M|8 2 Of WIP NO. 885650

CNBC HWHOMEHffiL SERVICES L.L.C.

WtiLhtitKfcPM

CbcteReoerH fi raHm

OKX Location| | laacdae AJdreEB

NENJQJEE EMUS EPCTTiTIY

OFFICE

NEN3QJEE FKLLS WEGUY sr

552 476

WXX. TSCP ZBOpssbed

1. QEXExatnr Nane 9CLWMT CCKE flSD CTgJfecbrcQcgy zBtjjested _Gsnecabor NX 518663 Cfenerator H& ID NX

(Aerator State NXWM000508215

311 EflST (3SENFIELD AVENUECity MTLWdKEE

NKDCSCSIQ Gbde 9999

State va

Snuroe G09 Ctigfinj:

State tfestestrean ND.CbLrtay US ZIP 53204

Ram W119

2. Haste Efene SULKIilC KJD lab or Waste Area3. Process Qeoeiatdrg Vbste

rraferrial. _4. Stripping ffenre SULKKCC

8 UH/N\ NX LN2796 EG II_ HQ ant 100 3b Waste: Y Pffl: N IH: N OW: N P: NHQ Dffi: 1.D002

DC

5

6

rabcde

sm1Pfgardh

3TDss: 1.. Haste Cedes D002

H=tf=*i™=itT=r- W-n ttv4-nntip

. tttysioal and dbentLcal £»'£»-" H*^

< 2 a <.82-5 b .85-9 c 1.09 - 12.5 d 1.0> 12.5 e > 1

exact

T-^TSfnOF^l St^tfTP

solid asemi-solid w

X lie; rid cputpable semi-sol id ffloâble powder egas o_aerosol ppressurized licpiddebris per 40 CER 268.45sharps

r X Sub Cabego

B:

ic Qavity

- 1.0

- 1.2.2

exact

Ifezaair reactiveviater reactivecyanide reactivesulf ids reactiveexplosiveoxidizing ^yidperoxide f ormer

2.

wy Mix: N Sol: N

Kl eSi Rjint{F} .qrilirfaa < 80 0 - 0 % suspended 0 - 0 % ashb 80 - 100 0 - 0 % settleable 0 - 0 % âter solubilityc 101 - 140 0 - 0 % dissolved 0 - 0 BlU/lbd 141 - 200e X > 200 Free Tiiq.rid Range 75 to 100 %f no flash - exact

n*!*? n».^H^,:^;.^ r*r-r radioactive or NRC regulated a nones shock sensitive b mOdt tenp sensitive c strongm polyn^rizatico/TrDraTHir describen CfflA. carcinogen.i infectious ffilogensh inhalation hazard Br % Bromine

Zone: _ CL - % ChlorineF - % FluorineI - % Iodine

Layers: | a nuLtUayered: X single phase

lop LayerYLsooBi±y| high(syrup)

by | trediumfoil)layer: | X low(vater)

solid

Second Layerhigh (syrup)[tedium (oil)lew (water)solid

Bottom Layerhigh (syrup)irBdiiiTt(oil)low(vvater)solid

J^Cblcr| OR

11

1

Uaed oil yAi ffiC < 1000 jpn HOC > 1000 ppn page 1 WIPND. 622578

Chemical Obnpositicn [M=f>ferine Pollutant, S=Severe Nferine Pollutant, CtQzcre Deleting Substance,Uîdarlyirg Hazardous Ctnstituent, B=Benzere NESHAP, T=TRI Chemical, C=C6HA Carcinogen]

Qtnstituerts lunges ants

J ISULflKIC K3D I 50.001 90.00|J IWKIER | io.oo| so.ool

Otter:8. Is the vastestream being imported into the USA? Yes Nb9. Eces the vastestream rrntain PCBs regulated by 40CFR? Yes tb

PCB Concentration .00 ppm10. Is the vastestream subject to the Nferine Pollutant Regulations? Yes Nb11. Is the vastestream subject to Baizene NE35VP? Yes Nb

If yes, is the vastestream subject to ^bti±icatdorv'a3ntrol Regjiremants? Yes NoBenzene Ctncentraticn .00 ppm

12. Is the vastestream subject to RCRA. subpart CC ccntrols? Yes ttoÂilatile Organic Concentration .00 ppnw

CC proved Analytical Ntethod? Yes MD_Geoerator Micwledge? Yes No

13. Is the vastestream from a CERCtA or state mandated clean-p? Yes Kb

14. ttTtrri

ft^kaging: Type/Size:

EtetjMry: thits .00 Per Day _ Per Week _ Per Nfcnth _ Per Qtr _ Per Year _ Cne Tiire _CEM EESCRIPITCN:

15.

I hereby certify that all infontBticn siinrLtted in this and all attached dfcamants contains true and accurate descripticns of thisveste. Any sanple submitted is rqccesaftative as defined in 40 CFR 261 - ^pendix I car by using an eqjivalent method. All relevantinfomaticn regarding kncvn or suêcted hazards in the poesessicn of the gensrator has been disclosed. I authorize sanplirg ofany vaste shipnant for purposes of recertificaticn.

^ns (Print or Type) Hrae E&te

Sicpature on EHe/_Title

:f approvBd for managanaTt, CNYX has all the necessary permits and licenses for the waste that has been characterized andidentified by this profile.

page 2 WIP ID. 622578

SHWICES L.L.C.

Obde

! fi ryrtHrn

OJBC locaticn MEMM3JEE ERILS

Invoice Sddress CEFICK CTTY

wrST

1552 476

_TbdhnciLagy recpestedrecjjestei1. QaEtatoor Kne SCOffiY CCKE flSD CflS OMBOTf

It). 518663 EBV ID M>. WMD00508215- State No.

ftMress 311 BEST CTEENFIELD AVENUECity MTTMM"KFK

MOeS(Sie) Obde 9999

State WISource G09 Origin JL

State Wastestream R>.

GbLKtry OS ZIP 53204Rrm W209 System "type

2. Waste Rue OIL Lab cr Waste ftrea

3. Process Gmetatdng Waste

used and unusad matendal

4. Shaping l&ie OIL, n.o.s.Ifezard COass NCME tH/*«V ND. IQE

HQDES: 1.DOTEes: 1.

0 lb Waste: N EH: N IH: N_ 2.

2.

: N P: N

5. Waste Cbdes 1SCNESLfa Category Mix: N Sol: N

6

£a

bcd

e

sm1

Pf

gardh

. ft^sical and chaiical properties:

, 2 a <.82-5 b .8 -

X 5 - 9 c 1.09 - 12.5 d 1.0 -> 12.5 e > 1.2

exact

EîyfTiral FJ-nh=>

solid asemi-solid w

X 1 jry in ri C

punpable semi-solid fflowable povder e

gas oaerosol ppressurized ligjiddebris per 40 CFR 268.45sharps

: Qzwity

1.0

• 1.2I

exact

Ifeza

air reactivewater reactivecyanida reactivesulf ide reactiveexplosiveoxidizing acid

peroxide fortier

Flash Rint(F) Shi ifa < 80 0 -b 80 - 100 0 -c 101 - 140 0 -d 141 - 200e X > 200 Fref no flash - exact

ITtaK CTwrT^pri.^^

r radioactive or ISKC regu]

s shock sensitivet tairp sensitivem pDlytTErizatiaViTCratErn CfflA carcinogeni infecticush inhalaticn hazard

Zone: _

fe

0% susperrisd 0 •0% settleable 0 •0% dissolved 0 -

ae Tiirin'd Range 75 to

-ated a none

b mildc strcrg

describe

H:Br - !

a - '•F - '•I - '•

- 0 % ash- 0 % water solubility

0 BlU/lb

100 %

Cdor

alcgens

's Brarrirek Chlorinek Fluorine's Iodine

layers: | a phase

Viscceity

tyI ier:

Ttp Layer

high (syrup)

X rrBdium(oil)low(vater)

solid

Second Layer

high (syrup)

msdium(oil)

low (water)

j solid

I HDttrm Layer

I high (syrup)

| madiun(oil)| lav (water)

| solid

| CfcQcr

| BLK

1 _11

Usad oil y/n HT < 1000 jpn IEC > 1000 jpn page 1 WIP fO. 622579

Chemical CtupasiHrn [M=Marine Pollutant, S=Severe N&rine Pollutant, OOzcne Depleting Substance,IHhderlying Hazardous Cfcnstitusnt, B=Benzens NESftP, T=TRI Chemical, OCfflA. Carcinogen]

Ctnstituents Ranges UxLts

IOIL | 100.oo | 100.00

Otter:8 . Is the vestestream being inported into the LEA? Yes _ Mb9 . Eces the wastestrean cmtain PCBs regulated by 40CTR? Yes _ tb

KB CriXHiLratim _ .00 ppm10. Is the wBStestrean subject to the Iterine Pollutant Regulations? Yes _ tfc>11. Is the vestestrean subject to Benzene NE3ffiP? Yes _ Ifo

If yes, is the vestestrâm subject to Not" if i ratlrn/Cbntrol IteqjirertBrts? Yes _ tfc>BerEene Ctnoentraticn _ .00

12 . Is the wastestrean subject to RCRA subpart CE cmtcols? Yes _ Na _VTlafile Organic Ctnoaitraticn _ .00 pptw

CC proved Analytical Nfethod? Yes _ ND _Generator Kxwlecê? Yes _ ND _

13 . Is the wastestresm frcm a CEROA or state itHndated cleanup? Yes _ Kb

14. <">«d .-filler Ti iFt rnnt-i<-n ;

Efedcaging: _ Typa/Size: _ __ Type/Size: _ _

Ftetjjancy: thits .00 Iter Eey _ Bar Vfeek _ Ffer Mnth _ Efer Qtr _ R=or Year _ CneUCM EESCRIPnCN:

GEtERMCR CHZHFICKHKN

I hereby certify that all information submitted in this and all attached docuvaits contains true and accurate descripticns of thiswaste. Pry sarrple sutrtitted is representative as defined in 40 O?R 261 - .Pppaxiix I or by using an eqjivalent method. All relevantinformation regarding knew or suspected hazards in the possession of the generator has been disclosed. I mftT-nriTF- sampling ofany v«ste shipnnant for purposes of recertificaticn.

& E(Pri t or Type) Fhcne Date

Sicpature en File jTitle

approved for rranagerrent, CNYX has all the necessary permits and licenses for the waste that has been characterized and. df=ntified by this profile.

2 WIP N3. 622579

CKKX L.L.C

I I

(NXIttstioij I SicdceftHtESS

WSEEIREPM INKWKTEN ERDFHE

MENMEEE MIS BOUIYCEFEE OIY

WEST

(Trfc

|552 | 416

GteEtrr IDKx WMXXB03215

MJ3233 311 EPST (JEHtflHD

9SS99State WEQl Qdgin 1

Stabe VfeebesbEanlt).CbrtrylB 23P532M'

RjmVDQL

2. VfeBbe UBre IJffiQS (DCN)3. EtncES GfcmcLuij Waste

4.N3E IG W3Bte:

2.2.

5.Mix: N Sti: N

6. H^skal aii domical prqpertifiS:

a < 22 -55 - 9

d 9 -12.5e >12.5

aect

a <80b 80- 100c 101-140d 141 -200e >200f X noOaEh

0 - 0 - 0%aEh0 -0 - di^nlved

_P_j^_0 % veter solubility0 - OBRJ/Ob

FiBS T .1q riri 0 to 0esct

States X snlldm1 X Liqjidp pirpdole 9stl-3i1 idf fLodde podsrg ^sa X aetcsd.r preaajrisBd liqjidd d^yi.qpr 40 OR 268.45h

Qtrair

" vfiber reactiveQaiicfe readdvesulfide r6ac±±i«aplcsiveotidizirg add

r radicBcti\es drrk sensitivet tanp 33Kil±em prilyrpri TFJ-inn/mcr

n C9A cardirgsa

h i r tB la t im hazard

arrrebniii '_c strcng

BrQFI

% Chip-ing% Hirrins% Iodine

siigLe tittH

Ttplayer

ty nedirm(ail) nediijn(ail)

fMrr-

HE< 1000 gpn HE>lDOOipn P3CP1 W[P^D. 4S8515

drpcsttim Nârire Riitrt, &S3«e NBrme Riitart, OCtae Deleting:IKftterlyirg tearcb-E CtnstitiHt, B=BenzHTe KES¥f>, T=TRI Chemical, C=C9ft Cararcgan]

OnstitLHls tecps Unls

100.001" loo.ool

Qhar.Is t±eveste3b£ern being impacted irto tie IS?EtES the vastesttBsn cn±ainECfe iBgjMsd ty 40OR?RB Ctrrattatim .

8.9.

1Q11.

_12. Is t±B vasbestrEsm a±r|ect: to Ftm sdp^rt GC ca±icils?

\£ilduls Ct iic QjrHtrstiaiGC /£pOv6d Asl ticaL NfettacJ?Gtoerator Itewla^?

D . Is t±E vastesteem frcm a CEKIA or state narkted deaop?

TH t-h-* \Aflcj-ppJ-rmm .qhrp-f In thp Nfrrinp RSllitTTt-.Is the vastesdsan abject tn BSEHE ISE3*P?If >es, is ths \Aastestean atrject

CtrEHtriicn .00

YesYes

YesYes~lSbC

Yes

Ys _ ND_XYes IStTxYes ~~ ND~X

14 .

Ebagpary: LtiitsUCM

.00 EerNbfh EferCtr EerYear CteTine

15.

GHsEFFQER LfcKllt-lUUJU'lI hecety cgt-ify ttd; all irfatnaticn siimtted in this and all attadisd ctELments certains true and accurate cfescriptiaB cf thisv^te. Ay saqie aimtted is rgie3a±ati\e as cfeEined in 40 OR 261 - ^pardix I cr ty usirg an agji\alflt nethod. All tElaant•irrfrrrmMrn receding kr>n or suspected hazaids in ths pm-mim cf ths cpneratrrr has beai ctisdcffld. I authcriê ssnplirg cfany \A8Ete shipiet ftarpurpcBes of reaa±±Ei£3ticn.

or T^pe) Hxne Efete

Title

BOLHYIf ajpccxed farnHB^tet, OSKCltSdll UTS recEârypetnits ard LLCHBES for t±ev£6te that hasiifHiciHracterisdardxfatified iy this ptcfile.

;2 WIPID. 4SS576

OKX HMKNOIIZL SERflCE KL.C.

MQMSOCNBEETLE

I I

I I fiioceMiEffiCKKXIazticn E DCNEE EPOUIY

OEFKENEMMMEEPHK WE

CTIY ST|552 476

QttX T3F invested QEna7trT-Mx5LS6S3

3XL EPST OTENFTHD A\£KLE

toaster EBV ID tt>.: State It>.

WMXXE03215

CJiyMELWUEE StateWCtlfe9999 999S9

State VtetesttEHTiNb.QurfaylB ZIP 53204'

Qdgjnl^ RnnWB20

2. VfeBbsN&reHIBB3. EtaGEEBGtaaatirgVeste

4. Ehmirgl)BielMVERffiLWPSIE-MyESIfiratdClasMlElK^ND. 1SCNE RJ RQait 0 Tb Vtete: N Pffl: N Hi N DW: N P: N

IQD3S: I. 2.DQTE6S: 1.HIES 2.5. VteteCfttetQE

Vtebafiba: NH Wastoeter X StbCSEtpy Mix: N StiL: N

6 ft^fiifTll rff\ <}MIliml |TI JI-Tl IRRr

fH Specific Gkaoty Elaî Rart(F) Sa < 2 a < . 8 a < 8 0 0'-, 2 - 5 b .8 - 1.0 b 80 - 100 100j X 5 - 9 c X 1.0 c 101 - 140 0d 9-02.5 d 1.0-1.2 d 141-200e >12.5 e > 1.2 e > 200

aect - aect f X rofladi - sect

BiskaLStEte Kv<qrrtlp! aTn-ytTyicj-irc,s X gnliri a air rea±i\e r ladkBctive cr ISFC rm FRTJ-Fnlid w vefcer reacti\e s dxck ^nsLti\e1 ligrid c Qaroda iEacti\e t tsrp satiitiêp pjipable aari-siid f ajlfida reecti e m pclyrenstioyhiranf flrwiTlp prvdgr e eplcsi\e n OftcarciirEpiq c^ o oddizing acdd i infecticLBa geirfol p paocids ftrrrer h irfralatiaa hazardr prppRTrlTPd lirjrid 7mp:d cMris per 40 OR 268.45h ^^

laies: | a miit-i-feym* b hL-] eHi

j_ TfpLa.er SfecndlârviFrrrrity hiîfeynp) Mî(synp)

by nHiLim(aLl) rTB±un(cal)

| X sdaa | nrilid

- 100% pptl-.lffHp 0 - 0% v^pr.enhhility0% di.ei=ril\»=r\ 0 - 0 HEU/lb

Eras liqjid Ftop 0 to 0 %

QtraguQcbai amns

hmildc sbrig

er cteriba

HfflO^TBBr - %BrnTins

I ~ - ~ % locbre

c X sirgle 'jtBHB |

B±tomlâr (TSlrrhiîtsynp) VHTnedium(ail)lcw(vetar)

| goLid |

Ltedcily/h KE< 1000 gam HE>1000ipn W[P^D. 493577

OHricaL Ctnpcsitiai [KMinre Rilutant, &S3/ere Itons Et01i±a±, OCEcre E^pLeting atstarre,tHirtedyirrj FtearrtLS GtnstitLHt, Bteme KE3£P, T=1RI Chemical, COft. (

tinges lints

IBLLBS I ioo.oo| ioo.oo| %

8. Is t±E vastesttsan being inpcrtsd irto the LB£> Yes _ M3_X9. Etes thevastestreamcatamPCfe iegu]abai iy 40OR? Yes _ M}_X

KB GtnH±Etiai .0010. Is the vastestiEa^ atrject to the Iterine Rili±a± Ffegul£ticns? Yes _ t£>X1L. Is the vastestcBan subijed: toteEHEbEHM3? Yes_N3j(

If >es, is the vestEStisan atrject to N±ificaJ±Ti/Qi]bri tegjoiensts? Yes _ ND_XCtrrntiatJai .00

12. Is the vasbsstream sdbgect toFOA.aijH± CCortidls? Yes _ ISbJCQ^nic Qirgnhî-.lrn .OOgnw

(Snsratnr Itewls i? Yes _ tfe)C13. Is ttevastesbBariframailKIAcrstctenaifetHiclea^p? Yes _ lfc_X

14 . CtrtaiiBr Inftnraticn :

.qTinpiTg EiH}Erry: Hilts .00 EferE&^_ EferVfeek_ EerMrth._ Ier(3r_ EferYeaor__ CteTineLEM

1R

I herety oertify tiEt all inforiBticn submitted in this and all attacbai ctnnets crrtains true and accurate cfegcrjpticns cf ttrisvaste. Pn/ sanpOs ainitted is rep: BtHti\e as dsfirei in 40 CTR 261 - ^perriix I or by ising an eqjimlert nethoi. All relaa±infctndiiai le irdiig kr>n or sj sdad hazards in the pc^FFHirn cf the genR-alrr has beai dJaJcmd. I a±hal2e sanpling cfaryveste shipint fiarpaipcss cf iBG6a±ificaticn.

J^ne(Rrirt c^Tê^^ Ehzne ESte

IJU* rn iT t i Ju . < )^litle

EPOLDY MMEKHEKNIf a^m^d for nutyaiul, QSKX has all the raueaaay permits and lioa'BES for the vaste that has beai charBCteriaad and

I by thisptrfile.VHP tO. 4SS577

INCOMING PACKING SUMMARY

Generator Number 518663

SOLVAY COKE AND GAS COMPANY

311 EAST GREENFIELD AVENUE

MILWAUKEE, Wl 53204

Attn: TOMJACOBSON

EPA ID: WIM000508215

Manifest Number WIK363294Field System ID: WO

Work Order Number 0487045000

Date Shipped: 08/27/2004

Document Number 04001

PHY State: S

Container* WO-0487045000-002 Waste Area:

WIP: 493576 DisposalCodr. CWDLEADACID

Date Accumulated: 08/13/2004 Special Handling: Gen Drum ID:

Shipping Name: UNIVERSAL WASTE-BATTERIES, (LEADACID BATTERIES), NONE, NONE

Manifest Page/Line: 03 / A

No. of Commons: 03

Primary Waste Codes:

Total CmnsWt 3000

Outer Container PALLET-CW Inner Container

Unto1

Container Size

PALLET

SIC: 9999

Net Weight

Source G11 Form: W001 System: H141 Cubic Ft: 27M

Chemical Name

LEADACID BATTERIES

Container*: WO-0487045000-003 Waste Area: Manifest Page/Line 01 / A

WIP: 493576 DlspocalCode: CWDAEROSOL PHY State: S


Shipping Name: WASTE AEROSOLS, FLAMMABLE,(EACH NOT EXCEEDING 1L CAPACITY), 2.1, UN1950

No. of Commons: 01 Outer Container 141G-DF Inner Container

Primary Waste Codes: D001

Total CmnsWt 14 SIC: 9999 Source: G11 Form: W001 System: H141 Cubic Ft: 1.89

Units Container Size Net Weight Chemical Name1 14 G

AEROSOLS

Container*: WO-0487045000-004 Waste Area: Manifest Page/Line 02 / F

WIP: 493576 DlsposalCode: CWDSUPHG PHY State: S


Shipping Name: RQ, WASTE MERCURY, 8, UN2809, III, (D009)

No. of Commons: 01 Outer Container 301G-DF Inner Container


Total CmnsWt 30 SIC: 9999 Source: G11 Form: W001 System: H010 Cubic Ft: 4,09

Units Container Size Net Weight Chemical Name

2 5 GALMERCURY

Manifest Number: WIK383294 Work Order Number: 0487045000 Page 1 of 6

Container*: WO-0487045000-005 Waste Area: Manifest Page/Line: 02 / E

WIP: 493576 DisposalCode: CWDDPK8IA PHY State: S


Shipping Name: WASTE CORROSIVE LIQUID, ACIDIC, INORGANIC, n.o.s., 8, UN3264, II

No. of Commons: 01 Outer Container 051H2-DF Inner Container


Total Cmns Wt 5 SIC: 9999 Source: G11 Form: W001 System: H141 Cubic Ft: 0.68

Untti Container Size Net Weight Chemical Name

1 1GALCLEANER WITH SULFURIC ACID

Container*: WO-0487045000-006 Waste Area: Manifest Page/Line: 02 / I

WIP: 493576 DlsposalCode: CWDDPKNR PHY State: S


Shipping Name: NON-REGULATED MATERIAL, NON-RCRA, NON-DOT., NONE, NONE

No. of Commons: 02 Outer Container PALLET-CW inner Container:


Total Cmns Wt 2000 SIC: 9999

Units1

Container Size Net WeightPALLET

Source: G11 Form: W001 System: H141 Cubic Ft: 27.00

Chemical Name

NOW REGULATED MATERIALS SUCH AS MORTAR AND CHAULKS

Container*: WO-0487045000-007 Waste Area: Manifest Page/Line 02 / C

WIP: 493576 DisposalCode: CWDDPK6 PHY State: S


Shipping Name WASTE TOXIC SOLIDS, ORGANIC, n.o.i., (LEAD, CHROMIUM), 6.1, UN2811, III

No. of Commons: 01 Outer Container 551A2-DM Inner Container

Primary Waste Codes: D006, D007, DOOS


Units Container Size Net Weight Chemical Name3 5 GAL

DIRT AND DEBRIS WITH HEAVY METALS

Container*: WO-0487045000-008 Waste Area: Manifest Page/Line 02 / A

WIP: 493576 DlsposalCode: CWDDPK3 PHY State: S

Date Accumulated: 08/13(2004 Special Handling: Gen Drum ID:

Shipping Name: WASTE FLAMMABLE LIQUIDS, n.o.J., 3, UN1993, II

No. of Commons: 01 Outer Container 551A2-DM Inner Container


Total Cmns Wt 55 SIC: 9999 Source: G11 Form: W001 system: H141 Cubic Ft: 7,50

Units Container Size Met Weight Chemical Name4 5 GAL

PAINT RELATED MATERIAL

Manifest Number: WIK363294 Work Order Number 0487045000 Page 2 of 6

1GALPAINT RELATED MATERIAL

Container*: WO-048704500040fi Waste Area:


Date Accumulated: 08/1312004 Special Handling:

Shipping Name: WASTE FLAMMABLE LIQUIDS, n.o.s., 3, UN1SS3, II

No. of Commons: 01


Outer Container 551A2-DM

Manifest Page/Line: 02 / A

Gen Drum ID:

Inner Container

Total Cmna Wt 55 SIC: 9999

Units Container Size Net Weight4 5 GAL

3 1GAL

2 1pt

Source G11 Form: W001 System: H141 Cubic Ft: 7.50

Chemical Name



STAIN WITH MINERAL SPIRITS

Container*: WO-0487045000-010 Waste Area: Manifest Page/Line: 01 / D


Date Accumulated: 08/13/2004 Special Handling:

Shipping Name: WASTE FLAMMABLE LIQUIDS, n.o.s., 3, UN1993, II

No. of Commons: 01


Outer Container 141G-DF

Gen Drum ID:

Inner Container

Total CmnsWt 14 SIC: 9999

Units1

3

2

Container Size Net Weight5 GAL

1GAL

1pt


Chemical Name



STAIN WITH MINERAL SPIRITS

Container!: WO-0487045000-011 Waste Area: Manifest Page/Line 02 / D

WIP: 622578 DisposalCode: STB001912 PHY State: L

Date Accumulated: 08/13/2004 Special Handling:

Shipping Name: RQ, WASTE SULFURIC ACID, 8, UN2796, II, (D002)

No. of Commons: 04



Units Container Size1 30 GAL

Net Weight

Outer Container 301H1-DF

Source: GOB Form: W119

Chemical Name

SULFURIC ACID [50-90%]WATER [10 0%]

Gen Drum ID:

Inner Container

System: H111 Cubic Ft: 4109


Container*: WO-0487045000-012 Waste Area: Manifest Page/Line: 02 / G

WIP: 622579 DlsposalCode: CWDFUELS PHY State: L

Date Accumulated: 08/13/2004 Special Handling: Gen Drum ID;

Shipping Name: OIL, n.o.s., NONE, NONE

No. of Commons: 09 Outer Container 551A2-DM inner Container.



Units Container Size Net Weight Chemical Name1 55 GAL

OIL [100%]

Contained: WO-0487045000-013 Waste Area: Manifest Page/Line: 03 / D

WIP: 688486 DlsposaiCode: SRRBO7828 PHY State: M


Shipping Name: NON-REGULATED MATERIAL, NON-RCRA, NON-DOT., (TAR), NONE, NONE

No. of Commons: 01 Outer Container 551A2-DM Inner Container.



Units1


Source G11 Form: W403 System: H061 Cubic Ft: 7.50

Chemical Name

TAR [100%]

Container*: WO-0487045000-014 Waste Area: Manifest Page/Line: 03 / C

WIP: 885651 DlsposaiCode: CWDWTENHS PHY State: S


Shipping Name: NON-REGULATED MATERIAL, NON-RCRA, NON-DOT., (RAGS, OIL), NONE, NONE

No. of Commons: 02 Outer Container. 551A2-DM Inner Container



Units1



Chemical Name

OIL, LUBRICATING |0-6%]OIL SOAKED RAGS [95-100%]

Container*: WO-048704SOOO-015 Waste Area: Manifest Page/Line: 02 / H

WIP: 885649 DisposalCode: CWDOZLNHL PHY State: L


Shipping Name: NON-REGULATED MATERIAL, NON-RCRA, NON-DOT., (WATER), NONE, NONE

No. of Commons: 01 Outer Container 551H1-DF inner Container


Total Cmns Wt 55 SIC: 9999 Source: G49 Form: W113 System: H082 Cubic Ft: 750


1 55 GAL

Manifest Number WIK363294 Work Order Number 0487045000 Page 4 of a

WATER [100%]

Container*: WO-0487045000-016 Waste Area: Manifest Page/Lin* 02 / 0



Shipping Name: FLAMMABLE LIQUIDS, n.O.s., (PETROLEUM DISTILLATES), 3, UN1993, II

No. of Commons: 01



Unite

1

Container Size

55 GAL

Net Weight

outer Container: 851A2-DM

Source: G11 Form: W219

Chemical Name

LIQUID WAXES (25-75%)PETROLEUM DISTILLATES {25-75%]WATER [10-25%]

Inner Container 551H2-DF

System: H141 cubic Ft: 11.40

Container*: WO-0487045000-017 Waste Area: Manifest Page/Line 03 / B

WIP: 885650 DlsposalCode: CWDORCEMPTY PHY State: S

DateAccumulated: 08/13/2004 Special Handling: Gen Drum ID:

Shipping Name: EMPTY DRUMS, NONE, NONE

No, of Commons: 07


Outer Container. 551A2-DM Inner Container


Units

1Container Size Net Weight

55 GAL

Source: G09 Form: W307 System: H082 Cubic Ft: 750

Chemical Name

EMPTY METAL DRUM [100%]

Container*: WO-0487045000.018 WarteArea: Manifest Page/Line: 01 / B

WIP: 493576 DlsposalCode: CWDPROPANE PHY State: S

DateAccumulated: 08/13/2004 Special Handling: Gen Drum ID:

Shipping Name: WASTE PROPANE, 2.1, UN1978

No. of Commons: 02 Outer Container SMCYL-CY Inner Container


Total CmnsWt 4 SIC: 9999 Source G11 Form: W001 System: H141 Cubic Ft: 1.00

Units container Size Net Weight Chemical Name

1 CYLINPROPANE


Container*; WO-0487045000-019 Waste Area: Manifest Page/Line: 01 / C



Shipping Nam* RQ, WASTE FLAMMABLE LIQUIDS, n.O.S., (GASOLINE), 3, UN1993, II, (D001)

No. of Commons: 01 Outer Container 851A2-DM Inner Container 551A1 -DM


Total Cmns WC 85 SIC: 9999 Source: G11 Form: W203 System: H141 Cubic Ft: 11.40


1 55 GALGASOLINE [100%]GASOLINE [100%]

Itenlfest Number WIK363294 Work Order Number. 0487045000 Page 8 of 6

ONYX ENVIRONMENTAL SERVICES

Pie- 'pe or print In block letters. (Form designed for use on elite (12-pltch) typewriter.)

SPECIAL WASTEMANIFESTTICKET

1. Generator's US EPA ID No. Manifest,i ,1 A ,i .u ;U u i yuren: 2. Page 1of

3. Generator's Name and Mailing Address

bU.VAY COKE AND GAS COMHANY311 EAS r OÊNFTELD AVENUEMILWAUKEE. V* S&tM

' A. Manifest Document Number

0041595B. State Generator's ID

4. Generator's Phone 414 345-06355. Transporter 1 Company Name US EPA ID Number

J it * * * 4 H J» J>C. State Trans. ID 16139

|D. Transporter's Phone (Q73) 347-71117. Transporter 2 Company Name 8. US EPA ID Number

1

E. State Trans. ID

F. Transporter's Phone

9. Designated Facility Name and Site AddressONYX SPECIAL SERWCES,INC1275 MINERAL SPRINGS DRIVE

PORT WASHINGTON. VW 33074

10. US EPA ID Number G. State Facilty's ID

N/A

j v j r M * * * * * * * *

H: Facility's Phone

(282) 284-686511. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number)

HM

12. Containers

NO; Tyrw

13.Total

Quantity

14Unit

WWolWaste No.

UNIVERSAL WASTE-LAMPS. (BULBS), NONE. NONEN O N E

P

i i

J. Additional Descriptions for Materials Listed AboveA) SA 493577 SUP8ULB 40 X 8 FOOT;245X4 FOOT; 432XINCAND

K. Handling Codes for Wastes Listed Above


PACKING SUPS ATTACHED FOR CLARIFICATION - F.MERGENCY NUMBER-) NFOTRAC: 1-800-535-5053PC 1 H5 V* TECH SERM CES

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of the consignment are fully and accurately described above byproper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highwayaccording to applicable international and national government regulations.

Printed/Typed Name Month Day Year

/^l Y17. Transporter 1 Acknowledgement of Receipt of Materials

Printed/Typed Name Signature Month Day Year

18. Transporter 2 Acknowledgement of Receipt of Materials

PrinteoTTyped Name Signature Month Day Year


20. Facility Owner or Operator. Certification of receipt of materials covered by this manifest except as noted in item 19.

PrinteoTTyped Name Signature Month Day Year

1 LSIGNATURE AND INFORMATION MUST BE LEGIBLE ON ALL COPIES

9-TRANSPORTFR 1 COPY

SEE INSTRUCTIONS ON REVERSE SIDE OF COPY 6.STATE OF WISCONSINChapter 291, Wis. Stats.Form 4400-66P Rev. 1-99

ALL COPIES MUST BE LEGIBLE,PLEASE TYPE

igned for use on elite (12-pitch) typewriter.

State of WisconsinDepartment of Natural ResourcesBureau of Waste Management •Box 8094Madison, WI 53708

FOR DNR USE ONLY

Form Approved. OMB No. 2050^^0039.

ManifestDocument No.

I .1 I I

Generator's US EPA ID No.UNIFORM HAZARDOUSWASTE MANIFEST

Information in the shaded areasis not required by Federal law.

3. Generator's Name and Mailing AddressSOC. AY COKE ,'\HD '.!AS ":f'F.|!''A,'

Site Location If Different

4. Generator's Phone (6. US EPA ID Number

w5. Transporter 1 Company Name

8. US EPA ID Number7. Transporter 2 Company Name

10. US EPA ID Number9. Designated Facility Name and Site Address

GtvY/C

13.Total

Quantity wt/Voi12. Containers

No. Type11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number)

FLAMMABLE SOLIDS ORGANIC n (•.; . (AC HVATEO CARBON. F'lU'EFt .1.UN132S II

- iMTOHIPSi 9. NA3U77. ill.PQ HAZARDOUS WAS'fn SOUC/ N.J


PACKING SLIPS ATTACHED FOP CLARIFICATION - EMERGENCY NUMBER-INFOTRAC: 1-800-535.5053 PC »65 >..M FIELD SERV

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by propershipping name and are classified, packed, marked, and labeled, and are in aU respects in proper condition for transport by highway according to ap-plicable international and national governmental regulations and according to the requirements of the Wisconsin Department of Natural Re-sources. If I am a large quantity generator, I also certify that I have a program in place to reduce the volume and toxicity of waste generated to thedegree I have determined to be economically practicable and I have selected the practicable method of treatment, storage, or disposal currentlyavailable to me which minimizes the present and future threat to human health and the environment;

OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation andselect the best waste management method that is available to me and that I can afford.

DatePrinted/Typed Name & Position Title

- •Signature / T'

a^f JJuMonth Day Year

17. TRANSPORTER 1 Acknowledgement of Receipt 6f Materials 'LJ Datented/Typed Name & Position Signature

. —^' jfMonth Day Year

18. TRANSPORTER 2 Acknowledgement of Receipt of Materials & DatePrinted/Typed Name & Position Title Signature Month Day Year

I I I I I I I

19. Discrepancy Indication SpaceFAc£ I 90. FACILITY OWNER OR OPERATOR: Certification of receipt of hazardous materials covered by this manifest except asI noted in Item 19. DateY r tinted/Typed Name & Position Title

EPA Form 8700-22 (Rev. 9-88) Previous editions are obsolete.

Emergency 24 Hour Assistanceand Spill ReportingTelephone Number: (800)943-0003 r*\GL

Signature Month Day

I I I

Year

' ' 'Copy Distribution: 1 — Generator send to Wis. DNR2 — Generator retain3 - Facility send to Wis. DNR

'™OivY 3 - Copies 1 & 3 mail to Wis. DNR at above address.

SSNO TO Wl DNR

4 — Facility retain5 — Facility send to Generatoi6 — Transporter retain

Lau4 Disposal Restriction NQiifloaliot* Form

SOLVAY COXfc^ND GAS CZ-M-VîV

:3 /Tu :v;.;r \V1MC005G821-5 ; I^.ifiiL 'A/K359250

i'.otice "..', be:n5 provided -:". 5ccordsi;^5 ''"ith 40 3F3-- 25?.'" tc irifcir:: ycu that Lri:- sh:p;rw;:t crmîriS y;iit.c'a^d 1} cs7i ând !±3posii by rJ"<e USE3A linear che )i:d c^pcs^J rtjâ-ictjcsi p/o^'arij. laaitJil&d bs.'o'p fcr

n of ihev-afie as awaEtsvi'ater •crnan-v.raH.e'wat-^r t';5C.";9Hn'?'':?t=r Act 'C>*'?X'ir. siaiiLiE, iiscdated with tha^rea'jr.e'.L'tispczal fdcl:;"/, ipîicib'^î^Li cxisj, a^d av.' :on--;:v:cr..±::

s, iist of 3ny?00}-?OCo iOii'Sji cc^siiiusuj mat ore v-estra :;; Lae w.sst^, î<i s\ :jncsrlv:r-

rs: r i r f ••! •- :-'-'- e r V\A' -C'32^959939 -00 1822580 / CWDSHMHAZ

"rssts 33d9s(5ubc3tegca-ies} D003 (NOME)Caisncuaits -;F'XO - FOC'5): None

UKCs?rsser:t: NoneTrsatriisntS-squirananti: Restricted w3-st9 requires treatment to applicable ^tiAdditional i-fotices:

CcrînerfJurnDsrVW -0329959993-002\"? / Approval Cods. S22533 / 3RRCAR8ON-HAZFcrtti De^gnstion .••'' CWA Status- Non-Wsstewater / Non-CWA

v'aste Cede ;Subc.ategcn&s): D001 i'iGNITAELE CHARACTERISTIC WASTE, OTHER THANL'.QUIDS >=1C% TOC (INCLUDES ALL IGN. GASES.FLAMMABLE SOLIDS 3, OK(D(ZERS))

CariStituents (FC01 - F005) : NoneUHCs Present'. NoneTreatment RequirEir.aits: Restricted waste requires treatment to applicable standards.Additional Notices:

I haarfcy certify that all infcrnialiari in this and 5sscciat8d l-î dissoiai r5nriaion dccumaits is -csn-iplsfe ande to the best of my knowledge and

, ,

V I 2/0 4-

CNBC EWOBCWtNffiL SHWICK L.L.C.

HCFILE

OKX Location MHOOQEE F&LLS

| | Inucioe .Address CtVlCE

MEKKKEE FflLLS

CHY

552 476ST

CNDCTSCF1. General

_Tbc±rnlcgyr recjjesbad Generator No. . IDND. WIMD00508215

Rrne SXVKf <XKE 2ND CftS OMEENY QrTFTrltTr STrltTP

Address 311 EftST rCTFNFTTTD AVENCE

City MH>BO<EE

I«ICS(SK3 9999

State WISource G09 Origin I.

State Mastestream Nb.CbuntryLB_ ZIP 53204

Ram VM09 System T^pe

2. Haste Itma LESD EMNT CHIPS .AND CEERIS3. Process Qaoeratirg Waste

rarpval of nlH paint

lab cir VfestE Area

4. Sharping Ifene HAZSRDCCE tmSIE, 93LJD, n.o.3.Ifezard nans B UH/fR Nb. NA3077 EG III HQ ant 10 Ib

H3Des: l.DOOaEOT Ees:

Haste: N Pffl: N IHt N O«: N P: N2.2. HUNT CHIES

5. Waste ObdesDOOSNcn VbsteMater X Sib Categpry m. Mix: N SaL: N

6. Hiysical

E«a 2D 2 - 5; X 5-9i 9 - 12.5^ > 12.5

exact

abcde

Eic Qcavity<.8.8 - 1.01.01.0 - 1.2> 1.2

exact

Flash ftrirtCF)a < 80b 80 - 100c 101 - 140d 141 - 200e X > 200f no flash

.osi-irfa

0 - 0 % suspended 0 - 0 % ash0 - 0 % settleable 0 - 0 % veter solubility0 - 0 % dissolved 0 - 0 BlU/lb

Free Trifj,n'd Range 0 to 5 %exact

HiysLcal State

3 X solidn semi-solidL 1.1q.iid

D purrpable semi-solid: flcveble powiar1 gasj aerosol7 pressurized liqjid1 debris per 40 O^R 268.45i sharps

a air reactivew water reactivec cyanide reactivef sulf ide reactivee explosiveo oxudizxncf ^yî'Hp peroxide forrnsar

f^HrîTJ^»f IfJ-lfTCg

r radioactive or MiC regulateds shock sansitivet tenp sensitivem pcxLvmsrizaticn CEHA carcinogaii infecticush inhalation hazardZcne:

Ofcr

a none

b mildc strong

describe

BrO.F

I

% Bronine% Chlorine% Fluorine% Iodine

layers: bi-layered:

Tfcp layer Second Layer Frtton Layer CfcOor

VisccBity

tylayer:

high (syrup)medium (oil)lcw(vater)

X solid

high (syrup)msdium(oil)low (water)

| solid

| high (syrup)| rredium(oil)| lew (water)| solid

VAR

bad oil y/n HDC < 1000 jpn HE > 1000 jpn pags 1 WIPBD. 622580

GtnpCBLticn [JytMarine Ebllutant, S=Severe Marine Ebllutant, OOzcne Depleting Substance,tMttterlying Jfezardous Onstitusnt, B=Benzene NESÂP, T=TRI Chemical, C=C6HA Carcincgai]

Gbnstituents R*y=s tfaits

\I£PD .001 l .OOlIEMNT CHIES AMJ 99.0Q| 100.00

12

Other:8. Is the wastestream being irrported into the IBV?9. Does the wastestream contain ECEs regulated by 40CFR?

ECB Ccncentraticn .00 ppn10. Is the wastestream subject to the lYarine Ebllutant Regulaticns?11. Is the wastestream subject to Benzene NE3KP?

If yes, is the wastestream subject to tfatificati m/Qntrol Regjirenents?Benzene Qcncentraticn .00 gm

ccntxols?Is the wastestream subject to RCEA. subpart'\folatile Cttganic Ctncentraticn

CC ^proved Aalytical Nfethcd?C3enerator Kicwledgs?

13. Is the wastestream frcm a CEFOA or state irancfeted cleanLp?

YesYes

YesYesYes

Yes

. Nb

_Nb

Nb

.00

YesYesYes MD

14 . O i *-nf IMT' TfifiifilMl irn

E^daging:

Vrrrjm-y- Units

UCM

Type/Size:Type/Size:

.00 Per Eay_EESCRIPnCN:

Eer Meek Eer Fer Qtr Eer Year Cte

I hereby certify that all infarrraticn submitted in this and all attached docutEnts contains true and accurate descriptions of thisveste. ffy sanple submitted is representative as defined in 40 CFR 261 - Appendix I or by using an eqjivalent method. All relevat:infarnaticn regarding knovxi or suspected hazards in the possession of the generator has teen disclosed. I îiH-r-iH•*? sanpling ofany waste shipment forurposes of recertificaticn.

n 414 1M72I7.bfene (Print on Type)

Sicyature en File

Ehone / Eate

Signature

£-71 V

rarrr.TTVpproved for rranagerrent, CNYX has all the necessary permits and licenses for the waste that has been characterized and

by this profile.

2 VCP ND. 622580

OCX ENVHOMNffiL SERVICES L.L.C.

Wt>UKiLb*?M HtFUE

| | tteoerH fi ratn'm

Onuoiae AHtEBS

OKX location MEIOtME FRLLS FSCLUIY

CTFTCE

NBOOSEE FKLLS WI

CTIY ST476

CNBC TED* iBCfjestBd1. Generator Name 3XV7W CCKE

^technology WIMD00508215(XMEENY O-l IMTÎ I It).

Address 311 ERST Q3EENFIELD AVEMJE

CLty MILtMJKEE

NftKBtSKJ Gbtte 9999

State WESburoe G09 Cfcdgin I

State *fastestrean ffc>.

US ZIP 53204Rxm

2. tfesbe tfene FIUtR WTIH A^TIVSJHJ CBRBCN3. Process Gtaeraticg Hbste

used filter wit± activated rarhm

l£b or Vbste Area

4. admirer Itene FU*Mffl[£ SCtJDS, CR3*HC, n.o.s.Kazzard Class 4.1 W/fR. tb. USI1325 EG II HQ ant 0 3b

BQOes: 1.EOT DEB: 1.

Waste: Y Pffl: N2.2.

3H: N EJW: N P: N

5. Vfeste Gbdes D001Vfe Men tfastaefaer X Stto Gabegay IS Mix: N 9d: N

e. aIHabc Xde

s Xm1

Pf

gardh

y*=qra1 mA rH=nriral j»

2 a2 -5 b5-9 c9 - 12.5 d> 12.5 e

exact

Hiysical State

solidsemi-solid

purpable semi-solidflowable powder

gasaerosol]TjT=f3,ea iH 7fr\ Tirpi iH

debris per 40 OFR 268

sharps

1 • l-U |— IfiR-

yv1^ 'j^fHr* cias/ity

<.8.8 - 1.01.0

1.0 - 1.2> 1.2

exact

Haza

a air- reactivew water reactivec cyanide! reactivef sulfide reactivee explosiveo oxidizing acidp peroxide formsr

.45

Flash RaictCF) fl-il-irtaa < 8 0 0 - 0 %b 80 - 100 0 - 0 %c X 101 - 140 0 - 0 %

suspended 0settlaable 0dissolved 0

- 0 % ash- 0 % water solubility

OBIU/lbd 141 - 200e > 200 Free T.irfriri Ranee 0 to 5 %f no flash - exact

j^ Qmtft^;^ :r radioactive or NRC regulateds shock sensitivet temp sensitivem pnlym°'i-i'7aHm/ii[-n irt-vr

n CQft carcinogen

i infectioush inhalatkn hazard

Ztne: _

a noneb mildc strong

describe

IBra -FI

Cdbr

falrryng

% BrcmLne% Chlorins% Fluorine% Iodine

Li-layered: X Kirglp phase

Ttp Layer Seccnd ilayer Bjtton Layer Oder

viMTTRitYl high(syrup)by medium (oil)

Layer: | lcw(^^Bter)

X solid

high (syrup)

rredium(oil)

low (water)

solid

| high (syrup) |

| medium(oil)

| low(vater) j

| solid

VAR

ttedoily/n HX < 1000 ppn HOC > 1000 ppn page 1 WLP bD. 622583

CtenLcal Obnpositiai [M=Nbr±re Pollutant, S=Severe Nferine Pollutant, O=Ozane Deleting Substance,tMixterlying Hazardous Constituent, B=Benzene NE3RP, T=TRI Chemical, OQSfA Carcinogen]

Obnstituents fcngps Urits

J 1/CnVKIED CARECN LEED AS A FELTER | 100.00 | 100.001

Other:8. Is the vestestream being inported into the U3V? Yes Its9. Doss the vastestream contain ECBs regulated by 40CTR? Yes No

PCS Ctncentratim .00 ppn10. Is the vestestrean subject to the Iferine Pollutant Regulations? Yes No11. Is the wastestream subject to Benzene NEEHAP? Yes No

If yes, is the wastestream subject to Notificatim/CtntDol ReqjiretTEnts? Yes NoBenzene Ctnosntratkn .00 ppn

12. Is the ^^BStestrBatn subject to RCRA subpart CC ccnttnls? Yes No'WDlatile Organic Ctncentraticn .QQ

CC ^pproued Analytical ^fethod? Yes NoGenerator Hxwlectjs? Yes No

13. Is the VBStestteam fron a CEKdA or state unrelated cleanup? Yes No

14 . ri i J firrrTf*r Ti ifi wiiRt~inn :

E&ckaging: lyps/Size:Type/Size:

Etegpetxy: Lhits _ .00 Par Cay _ Per Week _ Per Mnth _ Par Qtr _ Par Year _ Che TineUCM ~

15. Z^Hil-irral ItltoUlblLdCQ

I hereby certify that all inforrraticn submitted in this and all attached documents contains true and accurate descriptions of thiswaste. Pny sample submitted is r^resenfcative as defined in 40 CTR 261 - .Appendix I or by using an equivalent method. All relevantinforttBticn regarding known or suspected hazards in the possession of the generator has been disclosed. I authorize satpling ofany i*aste shipnsnt for purposes of reoertificaticn.

Signature

approved for rranagemait, OtfOC has all the necessary permits and licenses for the v«ste that has beai characterized and

identified by this profile.page 2 mPVD. 622583

INCOMING PACKING SUMMARY

'jenarjitcr Number: *513SS3SOLVAY COKE AND GAS COMPANY

311 EASTG.R£ENRELOAVEN!..E

MILWAUKEE. -A?! 53204

Attn: TOM JA COBoONEPA ID: WMBOQ503215

Marlfe;t N'j.mUr. WlK2j3250

Held Systap; !D: VTf

Work Order Nuroc-5" 0?2SS5iS9y3

Date Shipped: 03/02SC04

Docurvi ent NUR oe'"' 5S2fO

:ir.er3: WY3323959999-002 Wasted

WiP: 622533 DispesaiCcde: 3RRCAReON-HAZ PHY State: S

Date Accumulated: GS/02-20Q4 Special Handling:

Manifest Pane;L;ne:

^" Drum !D:

Shipping Name: WASTE FLA?tf<iA8LE SOLiOS, ORGANIC, n.c.s., (ACTWATEQ CARSOM, FILTERS).. 4.1. UN1125.!!

Na. cf Comrisons: G3

Primar/Waste Codes: D001

Total CmnsWt: 165 SIC: 39')3

Container Size Net Weight£j5 GAL

Outer Container: 551A2-DM

ource: G09 Form: W4G9

tnisgi Name

!rtn;r Contsiner:

ystem: H061 Cubic Ft : 7.50

ACTIVATED CARBON USED AS A FILTER [!GO%]

Manifest Psge/Lir.e: 01 / BContainer*: WY-Q32S95a939-S01 Waste Area:

WIP: S225SO DispcsglCods: CWDSHMHAZ PHY State: S

DateAccum-jJated: 09/'02/2004 Special Handling: Gen Drum ID:

Shipping Name: RQ. HAZARDOUS WASTE. SOLID, n.o.s.. (LEAD. PAINT CHIPS). 3. NA3077. 111. (D008)

Mo. of Commons: 20 Outer Container: 551A2-DM Inner Container:


Total CmnsWt 1100 3!C: 9999 Source: G09 Form: W409 Sv stem : H 111 Cubic Ft: 7.50

Units Container Size Net Weight Chemicai1 55 GAL

LEAD [p-1%]PAiMT CHIPS AND DEBRIS [59-100%]

A.E.T.S.

Generator :

WIP Report By Generator # - Summary

518663 EPA ID : WIM000508215

WIP # Waste Name

493575 PCB BALLASTS493575 PCB BALLASTS493576 LABPACKS (DCN)493576 LABPACKS (DCN)493576 LABPACKS (DCN)493576 LABPACKS (DCN)493576 LABPACKS (DCN)493576 LABPACKS (DCN)493576 LABPACKS (DCN)493576 LABPACKS (DCN)493577 BULBS560353 NAPHTHALENE SOLIDS622578 SULFURIC ACID622579 OIL622580 LEAD PAINT CHIPS AND DEBRIS622581 NON-PCB OIL FILLED TRANSFORMER622582 EMPTY NON-PCB TRANSFORMER622583 FILTER WITH ACTIVATED CARBON885649 WATER885650 EMPTY DRUMS885651 OILY RAGS888486 TAR888487 LIQUID WAX WITH PETROLEUM DISTILLATES888670 GASOLINE

SOLVAY COKE AND GAS COMPANY311 EAST GREENFIELD AVENUEMILWAUKEE

Recert Due Status Approval Code

8/10/09 G SUPBALLAST8/10/09 A MIC4935756/08/08 G CWDAEROSOL6/08/08 G CWDSUPHG6/08/08 G CWDLEADACID6/08/08 G CWDDPK36/08/08 G CWDDPK8IA6/08/08 G CWDDPK66/08/08 G CWDDPKNR6/08/08 G CWDPROPANE8/10/09 G SUPBULB

I8/26/09 G STB0019128/26/09 G CWDFUELS8/26/09 G CWDSHMHAZ8/26/09 G SUPBALLAST8/26/09 G SUPBALLAST8/26/09 G SRRCARBON-HAZ8/27/09 G CWDOZLNHL8/27/09 G CWDORCEMPTY8/27/09 G CWDWTENHS8/28/09 G SRRB078288/27/09 G CWDFUELS8/27/09 G CWDFUELS

2/14/05 14:44:36 Page

WI 53204-

Facility App Exp Date

SSSMICCWDSSSCWDCWDCWDCWDCWDCWDSSS

STBCWDCWDSSSSSSSRRCWDCWDOMISRRCWDCWD

2/01/108/27/094/16/103/31/0912/31/2010/02/2010/02/2010/02/2010/02/209/30/204/05/20

5/29/2010/27/2011/27/202/01/102/01/101/17/101/31/077/24/2010/01/0410/26/0410/27/2010/27/20


APPENDIX F-2

Records Pertaining toManagement of Tires and Belts



ZIP CODE28021

3a. B/L or AWB NUMBER

08/03/2004 07:42 704-445-2373 SEAMATES INTERNATION PAGE 02/02

DOCK RECEIPT P A C E I1. EXPORTERScflLtnes Internationalfor Jjxz Amad3f» E. Main Street

yville, N.C.

5. DOCUMENT NUMBERchs045032

0. EXPORT REFERENCES

SE ALINES REF #9111

2. CONSIGNED TO

MSCC/OCSXRR

BEDFORD PARK TERMINAL

7000 71RST ST

CHICAGO, IL

3. NOTIFY PARTY/INTERMEDIATE CONSIGNEE

7. FORWARDING AGENT

S. POINT (STATE) OF ORIGIN OR FTZ NUMBERMILWAUKEE WI

9. DOMESTIC ROUTING/EXPORT INSTRUCTIONSCHEETAH TO HANDLE US INLANDMSCTO HANDLE OCEAN

Loading 8/3

I2,PRE-CARRIAG6BYCHEETAH14. EXPORTING CARRIERMSC CHINA VJ20R

13. PLACE OF RECEIPTMILWAUKEE WI1 S. PORT OF LOADINGNEW YORK

10. LOADING JTER /TERMINALMSC MAKER TERMINAL/NY

16. FOREIGN PORT OF UNLOADINGPORT QASIM PAKISTAN

17. CLACEOFDELIVERV 11. TYPEOFIrfOVEOCEAN

1 li. CONTAINERIZED

YESX NO

MARKS AND NUMBERS NUMBER

OFPACKAGES(19)

DESCRIPTION OF COMMODITIES

(20)

GROSS WEIGHT MEASUREMENT

(21) (22)CONTAINER*:. 1 X 20 OT USED BELTING

PCS: /

.TOTAL VALUE:

ACCORDING TO APFL1CABU INTERNATIONA], AND NATIONAL GOVERNMENTAL K£GULAT>ON$.

THESE COMMODmeS LICENSED BY THE U.S. COR ULTIMATE DESTINATION PAXISTAN.

DELIVERED BY:LIGHTERTRUCKARETVED-DATE __CHECKED BY

TIME

PLACED IN SHIP LOCATIONON DOCK FOR THE MASTER

BY DATE

RECEIVED THE ABOVE DESCRIBED GOODS OR PACKAGES SUBJECTTO AH, THE TERMS OF THE UNDERSIGNED'S REGUI,AR FOR OF

TRUCK RECEIPT AND BILL, OF LADING WHICH SHALL CONSTITUTETHE CONTRACT UNDER waSttl THE GOODS ARE RECEIVED. COPIES UNLOADED-OT WHICH ARE AVAILABU! FROM THE CARRIER ON REQUEST ANDMAY B£ INSPECTED.A/^NY OF ITS OFFICES

SIdNEDi

SH; MUST SIGN HERE

Auburndaie Recycling Center, Inc.10453 S. George AveAutmrntiaie, VI 54412Telepnone : 715.652.3622

uateTicket

07/07/04 11:041

mGrossTareNet

69680320603^620

IbIbIb

41Olnta.

ff(0<ocJin(O

Vehicle :

, Inc. t :

Customer:

Business Hours8:C 0 AM - 4:00 PM

Oil 2Auburndale Recycling Center

a)A

xre

AUBURNDALE RECYCLING CENTER, INC.P.O. Box 137

AUBURNDALE, Wl 54412(715) 652-3622

Stone* & ProccMtoig Uc. #03376Collection & Transportation Uc. #12567

UJCt9«]ttS Ifld ^'28877

oaa:

ra•ok.

l<

ss !'od

iSi

Nrt JO *y*. flM*e* eMrn •( Ih . ,, MM U. OMI 10 tey« tils pM ****>

UNFTP


APPENDIX F-3

Advanced Waste Services



UCML ay. MUVHNUCU W«{JltJ 0 414 475 4496; Mar-17-05 3:28PM; Page 5/15

1. Generator1! US EPA ID Nox NON-HAZARDOUSW

ManlfeirDocument No.

311 East Gn«nfi«lcL Wl 53204«. Generate Phan*( 4J4 ) 788-7447 Tt>W

US CPA ID NumbwS. Tramporter 1 Company Nameimporter 1 Company NameA<hr«ac«d W*st* Corners, Inc

7. Tromporter 2 Company Nam*

' ^ - . • : - - . . V ' • . ' . , •.:-..US EPA ID Number

9. De«anoted Podlity Main* and $r»e Addrni US EPA ID NumberDe«anoted Podlity Main*ChanWoriu, fac3801K Wist McEudey Ave

aa. WI 51708

11. Watt* Shipping Name and Description

Non Regulttad Matwiat

E. Handling Codet for Wane. Lilted AboveJ. Addlllonol Duaiptionf for Mgtarlali'Urtvd Above

a. ChemWwks Profile,

13. Special Handling Iruiruciloru and Additional Information

COO call for amountLtudtdia Tinker*

16. G04EHATOR'S CERTIFICATION: I e*Hify Ike metorieli ducrlbitf above on ihii manH*M an not wbj« la Ud.ral ngwlattam ler repvriine prapc dltfoial o(

17. Traniporrer 1 Acknowledgement of Keceipt of Mate

IB. Traniporler 2 Acknowledoemenl of Receipt of AAorteriali

Printed/Typed Name

19. Obtrepancy Indication Space

70. facility Owner or Operator, CvrtHkaHon o< receipt o< wail* mattriali covered by thli manifest e»cept at noted In Item 19,

Printed/Typed Name

T/S/D/F COPY

sen i ay: AUVANUtu Mar-1 / -0b 3:28PM;• ci

Page 3/15

NON-HAZARDOUSWASTE MANIFEST

1. Ganaroior'i US EPA ID No.

311 East Gtetnfieid, WI53304Generotor-,phon*( 414) 788-7447 TOM Ja«tA*imrantporter 1 Company Nam*

Advanced W»tte Canieft. Inc.A. Trantpoilcri P

1-900-34297427. Tranipertor 2 Company Nam* B. Tranipertir'f Phon*

9.. 0«tignat*d Facilily Nam* and Sit* Addrew C. Facilit/i Phan*gnat* Faciily Nam*CfaamWotks, Inc.3S01K W.st McKmley Av«.

11. Wa»t« Shipping Nam* and D*K(iption

W»sts, Non-Haa»rdaiM liquid; Noa Regulated Matanal

E. Handling Cedu far WoitM IJJled Abov*}. Additional Daicriplioni for Materials liiled Above

Ch*m Works Profile, G* Gallons

. Special Handling Instruction! and Additional Information

COD tall lor amount Pomp Liquid OnlyLoaded bt Tsakw* ^ / ?^

16. OCNEIATOrS CBTIHCATION: I «rtl(y ih. n.i. .k dwulbW .k-v. .« *k «..;i.ii M .M »>|MI M f«J~<J rôloHwu prap.r diipoul of Nazardoui Wo

Print*d/Typ*d Nam* MenlH Day Y

* ' '•r 1 Adtnawl«dg*m*nt of K*c*ip« of MoUflali

Mon/J. Day 1

.<',' I'lA.

PriM»d/Typ»a Nam*

18. TraniporMr 2 Acknewl«dg*m*nt of R*c*ipl of Mot*rlalt

Month Oaf

19. PlKrapancy Indication Spac*

20. Facility Owner or Operator: CaiMlcolion of r*e*ip1 e< wait* moMrlali eo«*r*d by tali manitut eicapt 01 noted in Item 19

Sent By: ADVANCED WASTE; 0 414 475 4496; Mar-1/-05 3:29PM;

NON-HAZARDOUSWASTE MANIFEST

I. Qenerator'i US EPA ID No. MamfeitDocument No.

311 East Gteaflfiold, WI532044. Generator's phone ( 414) 788-744? Totti J«cobsaa5. Tr,

s, Joe.US EPA ID Number A.

1-97427. Ttaniporur 2 Company Norn* US EPA ID Number B. Trantportei'i Phone

9. Deilcinaiedilgnatad Facility Norn* and Sit* AddrutChtmWuiiu, Inc.3801K Weit McEinlty Ave.MUw«uk»«, WI 53208

10. US EPA 10 Number C. Paeility'i Phone

414342-1852) 1. Wa»t« Shipping Nam* and Ducriptlon 12. Container*

No. Tvp.

13.Total

Quantity

14.Unit

W>/Vo

W»sta, Non-HazaidoOi Liquid; Non £tgulatcd Material 0 0 1 T. T

d. •

Ii). Additional DaKripfioni for Materiak Lilted Above

a. Chem Works Profile,

E. Handling Codei for V/art»i LJcrad Abov*

G * Gallons

IS. Spaeiol Handling Inilrucrioni and Additional Information

Loaded in Tarikfr* C CODNall for amount Pmap Liquid Only %

16. OiNERATOR'S CEKTIRCATION: I c.rti(y m> mol.riati Jmcribvd abor* on ihi> monifm ar» not «ubj«tl ro (»d«ral MQulalioM far r»poning proper diipotal <A Harardoxi WoKc.

. . Manlh Daf Vcor

. /., ./ ,..'-"'. .; l / . -V' l ) -? Ir

• Printed/Typed Norn*

[^ I I -• ,'i p,i:.'1T-

Signature.

17. Tron«(«)rt«r 1 A<kncwkdg,»m«n> of <«»ipt of Mot»riol>

Prini«d/Typed Nam* Oar Y*ar

18. Tranipprtvr 2 Acknewl*dg*m*nl of H»c«ip1 of Materials

Prinf*d/Typ*d Nam* Slgnalur* Mootfi Da/ r«<jf

19. Dl«ti»pun«y Indluillon S|»c«

20. Facility Owner or Operator Certification of receipt of wart* materiali covered by thU manifefl except as noted in rrem 19.

Printed/Typed Nam* > -\, Signature/

Month Oar

T/eWD/F GOPY

0 414 475 4496; Mar-17-05 3:29PM; Page 9/15ay: AuvANUtu

f

1. Generator^ US EPA ID Na ManifoifDocument No.

3- 1- 7- 0. 7N0IO-HAZARDOUS

J. eWn.ronr'l Name and /Mailing AddreuLaht States ImJuorial SnVk*

AttTonJjcctwonSr

7 8 6 - 7 4 4 76, US EPA ID Number

I W I O 0 0 B 8- 1- » 3- 8- 1A. Transporter i Phono5. Trompertar 1 Company Nam*

Advanoad Wastfl Cgtrlefs. IncUS EPA ID Numboi7. Transporter 2 Company Nairn B. Traniportor'i Phono

9. DnignaUd Facility Nam» and Silo Addrow

ChvnrnAbrto Tr»2tmsnt Fadliry

C. FociliTy'* Phono

12. Containon

No. Type11. WaHo Shipping Nome and Denription

Wut* Ncn-Haiardoua Liquid. Man Rtgulaud Material

J. Additional DoKriplioni lor Maroriak Lictod Abovo E. Handling Cadoi lor Wattoi Liitod Abovo

' a.

b.

15. Special Handling Initruciioru and Additional Information

Quids Otvbcwc)

16. GENEIAIOrS CBmnCATION: I cHirty Iht mowrMl 4*Krlb*d abov* an IhU monrt.it art not lubj.a to tederal ragulmiont I.r r«fwliii||

Manm Do/ r*or

17. Transporter 1 Ad<nowl«dg»m«n1 of Receipt of Mareriali

IB. Traniporter 2 Acknowledgement of RoeeigMf AAaferlall

Printed/Typed Name

19. DiKrepancy Indication Space

20. facility Owner or Operator: Certification of receipt of watt* material! covered by thii manHerl aacept ai noted in Itegi 19

Printed/Typed Name

T/S/D/F COPY

oeiii. ay: AUVANUtu 0 414 475 4496; Mar-17-05 3:30PM; Page 10/15

7 GeneroW« OS EPA ID N«.

311E.GrHnfitUAvt.63204 „ ,

4. Genewior'. Phone {?1 4)

US EPA ID NumberS.' Tromparwr 1 Company Nome

A«v»n«*d WM*» C»n1trt. InoA. Traniporwr's Phen*

I w i. Q Q Q a a. i. a. 3. s. 17. Tron«p«i«'2 Company Nom« US EPA 10 Numb«r B. TMniporwr'i PVon»

9. D«ilfli\atad facility Nam* and_Stgr/yiiiuH> ----- --•

3aQ1KW.UcKinitvAv».

Vtf 93206414 342-1892

11. Wait* Shipping Nam. and Dncriplion

a. WwM NorvHBJrdous Liquid, Non R«B ja«d MaarU

E. Handling Cndai for WaitM LilT*d Abov>

3. ' 6.

b. d.

D. Additional OeKriptiom for Material! liiiod Above

a- (L) 048801 WutoOilafWtew

24 Hour Efr»TB«ncy

Contact 800-842-B782

IS. Cp«bal Handling Inilruch'oni and Additional Information

Ouid« Orvboard

16. OCNiKATOfS CEITIRCATION: I t«olty ihi monriaB duaitwd obara MI ihi» maniUn ar»/nai mbj»a IB l«d.ml r»»ul;n|i»n> lo. mxrilng pmptr diipmol a< Horardooi

17. Tro-'njpoft«r 1 Aeknawl>dQim«nt at R«e>ipt of Malarial!

18. Tranipnrt«f 3 Acknowl+a'fltment at Receipt «< Motariolt

A4a»ln

I ' I ' I

Printed/Trped Nam*

19. Hicrepancy Indkotlen Space

20. Padlhy Owner or Operator: CerHfltatlon ef receipt of wait* maMrialt covered by fhli manl

TVWD/FOOPY

OCIIL Ljy. «UVMIMOCL/ HMO 1C, U Hit t/J H*taU iviar- i / -ua o.ourivi, raye 1 1 / 1 3

NON-HAZARDOUSIA/AST6 MANIFEST

1. Generated US EPA ID No.

311 East GrMnfidd, WI53204. Generator-, Phon. ( 414 ) 788-7447 Tom Jacabxan

J. Transporter 1 Company Narge .Advanctd Wtsta Camtn, lac.

A. Trantportar'i Phon*1-800-842-9742

7. Tramporter 2 Company Nam* t. Traniparteri Phone

C. Facility'* Phone9, DMianated Facility Nam* and Sit* Addreu

3801K Wist McKiaUy Av».WT 53208 414-342.1855

11. Watt* Shipping Norn* and Daicriplion

, Non-Hazardous liqui.d:

E. Handling Codei for Watte* Lilted Above0. Additional Daicnplioni (or Material* Lilted Above

a ChemWorks Ptofiie,

Special Handling Imtruclioni and Additional Information

COD call forLoaded to Tudur*

16. OENBIATOK'S Cj>TlFICATION<. I <«nirr tU moltiialt d.lgib i .bo»« on .hii manifaa ar. BQI iubf>it I. HJ«r«l .«»»l«ll«nl <»

17. Trantportar 1 Acknawlcdgemenhof Receipt of Materials

Printed/Typed Name

18. Traniportcr 2 Acknowladgonwnt of Receipt of Mai»rial«

Mv»Uf Oo.

I ' I ' I

Primed/Tvp«d Nam*

19. Discrepancy Indication Spec*

20. docility Owner or Operator; CerKftcotlon of receipt o< woiU naieriali covered by ihli manlfeit except at

'I ""**"^fcrt^^<

Sent By. ADVANCED WASTE; 0 414 4/b 4496J rage ia/ib

T/SiD/PCOPY

a e n u u 414ay; MUVANLLU WAG it;

*fc*.fc... ^TA^J OF WISCONSINChapter 291, Wis. Sum.Porm4400-66P ..... .'i Rev. 1-98

ALL COPIES MUST BE LEGIBLE,PLEASETYPE

IM on elite (12-pltch) typewritar.

44yb; w a r - w - O b 3:31PM;

State or Wisconsin'Department of Natural ResourcesBureau of Waste ManagementBox 8094Madison, WI 53708

UNIFORM HAZARDOUS•:'••'-• WASTE MANIFEST

1. Generator's US EPA ID No

Form Approved. OMB No. 205OO089. Expire* 9-3

Information in the ahaded areis not raqulrod by Federal la*

Si'

3:_ti%tt*rmtor's Name and Mailing AddressMarina Cr.a.-<eway

r'» Phone (

Six Location II

6^ TraniporUr 1 Compuiy NameAdvancccf. Wosta

7. T

Facility Name and Sita Ad.draMControl Tn<fusts:\es.

4343 '(Cennt'fly *v«.East Chicago. ItJ 46312

«. US BPA ID Nwabw

WI0000815381S EPA ID Numbar

10. US BPA ID Number

1NDOOG646943

11. US DOT Description (Including Pnpir Shipping Nom« Hazard OM« and ID ttumbtr)

waste.133

? W*s*#&> -'ft

16. Special Handling Inatructioaa Information

24 iiovu' ptierêncy C6;-;u.^cV. i^-00-342-9792 Eraergency Espouse C-r* lioardIS. GENERATOR'S CERTIFICATION: I hereby declare that the conttnu of thia consignment an ft

•hipp<"g nmm^maA •«n-U«atfU^, fia.-lj.ri, marfcaJ. mnA.lmhflmA, maA M»hiMHramaetainpropar enndiplicabla intarnaUonal and national governmental regulattau tod according to the requvemeatc <

1 fully and accurately described above bf properr condition for transport by highwrny tccar&aLfto'mp-

r_ ^ ^ m ntnt* of the Wlaconaln Department of Natural Ra>sourcea. If I am a large quantity generator. 1 also cer3ry that I have • program in place to reduce thavohme and tozicity of waste generated to thedegraa I have determined to be acoaomicalry practicable and I bav« aelected the practicable method of treatment, storage, or diepoaal currentlyavailable to me which minimises the preeent and fntura throat to human health and the environment;

OB, if I am a amail qumnUty generator. I have made a good faith effort to minimise my waate generation andselect the beat wute management method that ia available to me and that I can afford.

Dated Name & Position Title

17. TRANSPORTER 1 Acknowledgement of

tyV £jM.r,

Date

5at»18. TRANSPORTER 9 Acknowledgement of Receint of MaterialiPrmUoVTypod Name & PoaiUoaJltUtt#/?& &b kfOBCk Y<


20. FACILITY OWNER OR OPERATOR: Certification of receipt of hasardcnoted is Item 19.

i materiaJe cevend by thia a it except aa

Printed/Typed Name Signature

EPA Form 8700-32 (Rev. 948) Previoua editiana are obaolata. OBDJ Diitribuckni

Emargaacy 44 Hour AtaiaUnce Telephone NumberInWiaconain («06) 269-3239OutafcU Wtoconain (600) 4244802

FACIUTY SEND TO WIS. DNR

) - QeBeretac Mod to Wfa. DNBt — aaoetator ntafna - raoillty Mnd to Wla. DNR

Cophe 1 A j mall to Wl«. DNS at above addraia,

4 ~F»cOi<7 retain5 - r«dntr eentf to QeDeralA — Iruupottar ritaia


APPENDIX G

Analytical Data

• G-1: Analytical Data Tank Content Testing

• G-2: Analytical Test Data Relating to Liquid Dischargesto Milwaukee Metropolitan Sewerage District

• G-3: Asbestos Test Results Clearance Testing

• G-4: Asbestos Test Results Prior to Clearance

• G-5: Concealed Asbestos Response Action




APPENDIX G-1

Analytical DataTank Content Testing



i.2/01/2003 ..M: 3^ 0$lMTl«461 Great Lakes iS laT5 ^^ 8M1/W

LAKES 140 East Ryan Road Email: [email protected] Oak Creek. Wisconsin 53154 (414)570-0460 FAX (414) 570-9481

FAX TRANSMISSION COVER SHEET

ATTENTION

COMPANY:

FAX #:

: I Qv^T 6yf.obsfr\ Jo£t P > M K<

THIS IS PAGE ONE OF jQ_PAGES

DATE:

FAXED

TELEPHONE NUMBER: (414)570-9460 FAX: (414)570-9461

NOTES REMARKS

The p^ges accompanying this facsimile.transmission contain information from trie firm of GreatUkes Analytical. The pages are confidential or privileged. Th» information Is Intended for the use ofthe Individual or entity name on mis covar sheet. If you are not the Intended recipient, be aware thatany disclosure, copying, distribution or us* of the contents of this information is prohibited. If youhave received the facsimile In error, please notify us by telephone immediately so that we canarrange for the retrieval of me original documents at Bôost toj

A COPY OF THIS FACSIMILE WILLV WILLNOTv BE MAILED.

i2,iil/200;: 14:37 14146450645 LAKE STATES INDUSTRI PAGE 02

12/01/2003 m 0:39 FA1 4145709481 Great Lakes Analytical ®002/016

GREAT140 East Ryan Road Email: [email protected]

ANALYTICAL Oak Creek. Wisconsin 53154 (414) 570-«4eO FAX (414) 570-9461

01 December 2003

Tom JacobsonLake States industrial Service311 E. Greenfield Ave.Milwaukee, Wl 53204RE: Milwaukee Solvay Coke Site

Enclosed are the results of analyses for samples received by the laboratory on 11/14/03. Ifyou have any questions concerning this report, please feel free to contact me.

Sincerely,

Great Lakes Analytical

Andrea StathasProject Manager

19/01/2003 14:37 14146450645 LAKE STATES INDUSTRI

12/01/2003 ION 0:40 FAI 4145709461 Great Lakes AnalyticalPAGE 03

GREATLAKESANALYTICAL

140 Eaet Ryan RoadOaK Creek, Wisconsin 53154

Email: [email protected](414) 570-9480 FAX (414) 370-9461

Lake Stubs IndUMriil Swvtw311E.GnxnfleMA\w.Milwaukee WI, 53204

Prpjcec Milwaukee SofrBy Coke SitePiojoci Number [none]Frojoct Manager: TomJacobsoo 12/01/03 12:33

ANALYTICAL REPORT FOR SAMPLES

SaoplcID Mltrix

TOO3

T012

TOI4

TOI6

T023

TX122

T024

T023

T029

T033

W3H156-02

W311156-03

W3I1156-04

W3111SW5

W31115646

W3II156-07

W3U156-08

W«o(S)

Waste (S)

Wane (9)

W«te(S)

Wute(S)

Wnflte(S)

W31 1156-11

Waste (S)

Wutc(S)

11/13/0313:45

11/12/03 13:45

11/13/0314:00

11/12/03 13 0

11/13/03 10:00

11/13/03 10:25

11/12/03 10:15

11/12/0310:00

11/13/03 14:30

11/12/03 11:45

11/14/03 15:36

11/14/03 15:36

11/14/0315:36

11/14/0315:36

11/14/0315:36

11/14/0315:36

11/14/03 15:36

11/14/0315:36

11/14/03 15:36

Great Lakes Anoly&ml-Oak Creek The nulti In OOt rtport afffy to Hit tampia aufyrti in accordance *iik «*r tkdn ofcattoiy Jeeumtxt TUiattUytleolnfortnaathenpnitttcaSln la entinty.

Andrea Stathic, Project Manager Page 1 of12

12/01.0303 14:37 14146450645 LAKE STATES INDUSTRI PAGE 04

12/01/2003 MON 0:40 FAI 4U5709461 Great Lakes Analytical


140 East Ryan RoadOak Creek, Wljconsln 63154

Email: [email protected](414)570-9460 FAX (414) 570-9481

Like St»la Industrial Service311 E. Greenfield Ave.Milwaukee WI, 53204

Project; Milwaukee Sohmy Coke Sh*Project Number [none]

Project Manager TomJ«cob*onAcpeittf:

12/01/03 12:33

BTEX by £PA Method B260BGreat Lakcj Analytical-Buffalo Grove

AMiyw RMMlMReporting

Unit IMu Dilution JSctcb rrcjured AnWyzrt Method Nairn

TOO3 (W3111S<.Q1) WMM (S) SwopM: 11/13/03 13:45 Rooted: 11/14/03 I5:tt

BeozeneTolueneCcbylbeiuRieTotal XytraeaSurrogate: DlbromcfluortmurlhencSurrogate: 1 .2-Clchlor9*tham*l4Surrogate: ToluenexlgSurrOffrte: 4-Bromafluon>If«nsut»

11900001710000112009

2590000

23100231002310046300125%

9S./9SJ079t103 K

Vffa 5000 31 Hm H

*• •

m w

66.4-1*559.3-17164.S-139«.*-?«

)330 11/2CV03 1 1/2

ll

IV

1*

M

1/03 EPA I(260B

-jj

T012 (W3U15frQ2) Watte (S) Sampled: 1MWH 13:4S R«crfv«d: U/14/03 1S.3«

BomneTolueneCthylbUKBcTotal Xylene«

Surrogate: DibninqfluonmHhaneSurrogate.- 1 ,2-DiMonei)uine*!4Su/roguit: ToIuene-dSSurrogate: 4-Bromo/Juaroljentena

1320084303*1

6900

248248248495

t 'OXJ17X9S.SX93.396

ugte SO 311C« IR

" «

66.4-I4S59.S-17J64.5-13945.8-145

1330 11/20/03 11/3•

•

it

WO EPA!12SOB

TOl4(Wmi56-03)WMte(S) Sampled: 1J/13'«3 14:00 Received: 11/14/03 15J6

BourneTolueneEthylbenzeneTotnl Xylena

Surrogate; DibmmoflittrometHaieSurrogate; L2-Dlehlonnduai^d4Surrogate: Teluene^SSurrogate: *-Breatofluonbvame

24MO15«W

ND64100

3330«W33306670

HIM78.1 K102%

93.7 M,

u0fec 500 31Kw *

n P

H •

ff&4-/«59.3-17164.5.13945.8-145

330 TI/2VW I1ASA3 EPA*t260B

Gnat Lakes AnalyticaJ-Oak Creefc

Andrea Stathas, Project Mouge

J*f nenite m drii rtfcrl ifpfy ie Ae tampltt ma{yitd In accordant nltk tic etui* qfeustoify Joaomt. TMt amfytical report mat be rtpndvad in In merefi.

Page 2 of 12

14146450545 LAKE STATES INDUSTRI PAGE 05

12/01/2003 ION 0:40 FAI 4145709461 Great Lakes Analytical


140 East Ryan RoadOak Creek, Wtaconaln 53154

Email: lnfoQgMlabs.com(414)570-9460 FAX (414) 570-9481

Lake Suites Industrial Service311 E_ Greenfield Ava

Milwaukee WI. 53204

Projeo: Mihwukaa Sol vay Coke SiteProject Number [none]Project Manager TomJ«oobttn

Xcwted:12/01/03 L2-.35

BTKX by EPA Method 8260B

Great Lakes Analytical-Buffalo Grove

An«Iyi»ttqwRtog

Umft Unto DflnUon Batd. Aotlywd Metficd

T016 (WH115«%»4) Wait* (S) Sampled] 11/12/0313:20 borfve* 11/14703 15:36

BeameTolMneEthyUMozeneT<rt»lXylen«

Surrogate: DibromofluoromxthaneSurrogeu: 1 ,2-DicrJen«lhane44Surrngeto: Toluene-d8Surrogate: 4-Brontoflitotvbfnxai*

15300002580000191000

40200W

202002(32002020040300

104%68.8 X101%105%

o0*| SOW 31 K» i»* •• p

66.4-145$9.5-17164J-1S945.8-145

330 H/2(

P•

^»»t

1/03 11/21f

•

*

^

1/03 EPA!I

•

V

b

V

t

I260B

V

»

«

T013(W3ni56-OS)\V*«.(S) Swapted: 11A3/W 10:00 Revived: 15d«

BourneTolueneEthylbcnzcneTotal Xylcnei

Surrogat: DtiromtfhiororMtbaiuSurrogate: l.2-DleMoroefriar»44Surrvgatt: Teluene-dSSurrogate.' 4-BromDJluorobwaene

22000037000056200

1300000

19400194001940038*00

120%88.1%104%108%

uefcg 5000 31K• - •* « •

* • «

66.4-14559.5-17164.5-1394SM45

1330 11/2W3 11/2- • ii n •

' n *

r ^ j

r V i

f m I

• i* i

M)3 EPA*r <

i i

» j

• i

• i

* i

I260B1

1

*

*

r

T022JW?ni5MK) WMM (5) S«mptod: 11/13/03 10;M Rctclved.- 11/14AO 1S3<

BenzeneTolueneEthylbnueaeTotal Xylenw

Surrogate: DibromojluoromtthaneSurrogate: 1 ,2-DtfMort>€t)iane-d4Surrogate: Toluent-dSSurrogate: 4-Bromojlvorohfrotm

U70M37100044300

1050000

155001550015500310001J79679.4%103%97.9 M

ug/kt 4000 311 f• i p« • *• " i

$&*-;«J9.5-/77«.j-;jj>4S.t-HS

1330 11/21i I

i t

1 *

• i

it i

* i

r •

Vm 1105/03 EPA(1 H I

1 p* f

1 » •

' f 1

» » 1

f -r i

• v J

I2GOBi

1

I

r

V

it

Circst Lakes Analytioal-Oak Creekcuitotp denmmt. 7k(r analytical npert aMt be reproduced In la emtrty.

Andicii Suthas, Project Manager

12/01/2303 14:37 14146450645 LAKE STATES INDUSTRI

12/01/2003 m 0:41 FAI 4145709461 Great Lakes Analytical

PAGE 06

HGREATLAKESANALYTICAL

140 East Ryan RoadOak Creek, Wtocorwtn 53154

Email: Infw3glalabs.com(414)570-9460 FAX (414) 570-6461

Ukc States Industrial Service31 IE. Greenfield Ave,MII wmikoeWI, 53204

Project Milwaukee Solvty Coke SiteProject Nnmlier: (none]

Project Manager TomJecobsooR(p«lfCd!

12/01/0312:35

BTEX by EPA Method 8260BCrgat Lakes Analytical-Buffalo Grove

Anifyle RouhRepotting

Limit U«te niudoa BtRb PrarHired Analyzed MflJIOd NONaf

T024(W1115«-07)W«HtB(S) SwnpW: 11/12/8310;li Received: 11/14/03 1338

BenzeneTolaeneEthylbvazvneTotal Xyta«Surrogate: Dibfono/luorometfiancStirrogeUe: lJ-£Hckloroel)umt-d4Surrogate; ToluciK-JBSurrogate.' 4-BttunoflwTobtmsno

49M094WOOO41200

MMOO

2250225022504500

98.7%10/9678.7 %97.8%

tig/kg 900 3U(» • i* • i• V T

66.4-14559.5-17164.5-1394S.S-J45

U30 n/a< i< .i *« i• i• i* i

MB ll/l1 •

» 1

» 1

* P

f «

'1 M

t 1

MU EPA!> 1

1 •

' *

• J

1 t

• t

• i

2MB1

i

1

p

w

r

p

TOZ5(W31US6-0«)W««M(S) Sampled: 11/12/03 lOiOO tUcdved; 11/14/03

BOUCMTolueiMfitbylbeazaneTotal Xylcnc*

5uiT02itM: DibmmtrfhtonirutkantSurrogate l,2-Oicfilor#ahaiK-J4Surmgatt: Toluene-dSSurrogate: 4-BmaeJluorabeiae»e

sMooe51SOOO19«0

773000

1820018200moo36500109%72.5 K99 J%98.996

uf/kg 9000 31K•• M

• ft •

- • f

«./-/«

S9.)-17I64.S-J3945.1-HS

1330 11/2IV03 1 1/2•

» ii

* »

• i>

r K

• If

w

1/03 EPA!

*

•

w

1

L260B

T029(W3ni5W)9)W»rt,(S) SimpUd: 11/13/0314:30

BaoaoeTolueneEtnylbeoMnnTotal X^lenci

Surrogate: DlbromojluoroumkaneSurrogate: 1 ,2-DlcMerettkano-d4Surregon: Tohtena-dSSurrogate: 4-Brnmofluorobenxne

9630091290000

Ofl4AnTVfVW

2050000

30100 i301003010060200104 K

69.19699.0%99.3 %

loVfe* 5000 3111• r» i

• •) 1

ft * 1

69.4-14559.5-17164.5-13945.S-145

1330 11/21' I

1 1

1 i

t I

• (

1 i

> i

V03 1IAr i

i i

i i

V 1

f i

r <

i j

1/03 EPA1I *

I /

* 1

• I

• (

* i

» i

I260B1

1

w

«

Great Lakes Analytical-Oak Creek

Andrea Stathas, Project Manager

Ha nmta m tkii rejurt tpffy toautody doornail nit analytical repcn mat be npntuctd 'at fa vutrey.

12/31/2003 14:37 1414&450645LAKE STATES INDUSTRI PAGE 07



140 EMt Ryan RoadOak Creek, Wtocondn 53154

Email: [email protected]

(414)570-9460 FAX (414) 570-9461

Lake Sutei Industrial Service

311 E. Greenfield AvaMilwaukee Wl, 53204

Prqjtcc MUwankM Solv«y Cote Site

Project Number [DOM!Project Manager Tom Jtoohson U/01/03 12:35

BTEX by EPA Method 8260BGreat L*ks* Analytical-Buffalo Grove

Anolyio Rmft(Uporing

Unit (Jala Dihitim Bttth Prep«nd XWyroJ Melted Notts

1I/1VM 11:4$

BenzeneTolueneEthylbeiuieneTotal Xykna

Surrogate: DtbrornafluoromettiantSurrogate: l.2-DleUorptUiane^d4Surrogate: TeOient-dSSurrogate; 4-BromoJluerobemene

26800037400031800

•mow

19600 ntfhf 4000 3MO19600196003*100

118 X 66.4-14S94.9 K S9.S-I7)102 K tf*.J./jy92.7M 4SiS-I45

1330 11/31I *

1 1

> 1

* J

• 1

• 1

» t

V03 11/2'> i

P P

I 1

• i

p i

V 1

I i

W>3 BTAI1 R

1 P

• 1

V 1

• I

E260Brr

•

•

•

Grett Lakes Anftlydcal-Cak CreekcwlMOi tfMUHrnr. Ttir tnt^tieai rvfartmalbe repnJucet in lit mltrrty.

Andrea Stathaa, Project Mumger PageS of 12

12/31/2003 14:37 14146450645 LAKE STATES INDUSTRI PAGE 08

12/01/2003 ION 0:41 FAX 4145709461 Great Lakes Analytical


140 Eact Ryan RoadOak Creek, Wisconsin 50164

Email: lnfo®fl)alaD3.oom(414J57CW4SO FAX (414) 570-9461

Lake SOUR Industrial Service3I1 a Gracnfidd Avc.Milwaukee WI, 53204

Pitg'oeb Milwaukee SolvsyCofca SiteProject Number [none]

Project Manager Tom Jccabaoa 12/01/03 12:35

Polychloiinated Bfphenyls by EPA Method 8082Great Lakes Analytical-Buffalo Grove

Aaalyio Rcjnlt UflW Unite Dihidon Bitch Pitpml Analysed Mahal Note.

TOO3(W3111564>I)Wute(S) Sampled: 11/13/03 U:45 Rcniv«l: 1M4/03 15i3« G23

PCB-1016 ND 1500 uefe)PCB-I221 NP 1JOOPCB-1232 ' NP 1500PCB-1242 NO 1500PCB-1248 ND 1500PC3-1154 ND 1500PCB-1260 NO 1500

t«« 10 31K

Sumgait: Tetracklorv-maa-xyiaie 474 9* 10-125Surrogate Dteaeblomtlphturl 22.S96 10-14}

Ug 11/21V03 11/2.U03 EPA 8012

H

TOI2 (W3tnSfi-02) Wut>(S) S«mpltdr 11/12/03 13 3 Rttelvtdt 11/14/0315:M G23

PCB-1016PCB-1221PCB-1132PCB-1242PCB-1248PCB-1254PC8-1260

Surrogate: Tetrac)iioro-m<aa~tylrneSurrogate: DecacMomblphenyl

NDNONONDNDNDND

1510 ngfltfwd 10 J1I0441 U/2(M)3 1U25/03 6PAHOB2151015101510151015101510

J069t 10.J2S

A

H

»

ri

H

•

6.57 X 10~t43 " L

T014(TO1115M13)WM»(S) Sunpltd: 11/13/W 14:00 Rcc«J«d: 11/14/03 15:36 C23

PCB-1016 ND 1520 ue*(PCB-1221 ' ND 1520PCB-1232 ND 1520PCB-1242 NO 1520PCB-1248 ND 1520PCB-1254 ND . 1520PCB-1260 ND 1520

;woi 1D 31 1C

Surrogate: TeiroaUoro^mgia-3ylen» 9.S5 9t 10-12$Surrogate: DteaeMerobipkenyl 1.04 H 10-143

H48 11/2 M03 U/2,5/0} BPA van

LL

Orsat Lakes Analytical-Oik Greek

Andrea Stathoa, Prqjcct Manager

ntrctvla in tMr report apply to At lanptt* exatysallr tcardmct •otA tluchetii efauttafy document, nil analytical rtpon mot be repnOuetJ I

Page 6 of 12

,01/2003 14:37 14146450645 LAKE STATES INDUSTRI

12M/2003 m 0:42 FAI 4145709461 Great Lakes Analytical

PAGE 09


140 East Ryan RoadOak Creak, Wbcontfn 53154


Lake Stnias Industrial Sarviec

31IE. Orwnfidd Ave.Milwaukee WI, 53204

Project Milwaukee Solviy Coke SiaProject Number, [none]

Prujert Mumper TomJaooiMm 12/01/03 12:35

Polychlorinated Bipbcnyb by EPA Method 8082Great Lakes Analytical-Buffalo Grove

Anulyto RewhReporting

Lima Unto Dilution Bald) Pnj•red Analyzed Melted Not*

T016(W311)SW>4)'WMM(S) Stapled: 11/12/03 13:20 Ibctfrad: Jl/U/03 15-J« G23

PCB-1016 ND 1510 09^-0 1PCB-1221 ND 15>0PCB-1232 NO 1310PCB-1242 ND 1510PCB-1243 ND 1510PCB-1234 NO 1510PCB-T260 ND 1510

0 3L1C

Surrogatt: Tftrachhro-Mtta-jylme 112 9t 10-125Surrogate: DeeoeMorobipkoyl 26. J 9t 10-143

M4* 11/2 W)3 1L<2 !/tt EPA I0t2

T0» (\V31115»flS) Wuto (S) Sunpled: 11/13/0310:00 Rccrivtd: 11/14 03 15J< G23

PCB-1016 ND 1540 utfePCB-122I ND 1540PCB-1232 ND 1540PCB-1242 ND 1540PCB-1248 ND 1540PCB-I2S4 ND 1540PCB-1260. ND 1540

|W« I 0 3HC

Surrogate; TetraeUoro^nelf-jytfnt 28.4 9( (0-125Surrogate: DecaeMorvbiphenyl 17.3 9t 10-143

M4« (1/2 MM 11/2 S/03 BPA 8082

1022 (W311136-0fi) WMfa CS) StmpW: 11/13/03 1<h25 R«ceiv»d; U/14AO 15O6 023

PCB-1016 ND 1520 115%PCB-1221 ND 15JOPCB-1232 ND 1520PCB-1242 ND 1520PCB-1248 ND 1520PCB-12S4 NO 1520PCB-1260 ND 1520

fwet 10 3I1C

Surrogate.' TartuMon-mtia-xyttnt *0.3 9t 10-125Sunvgae; Dacachlorotilpfiwyl I5.1X 10.143

H4f 11/21V03 11/1

r

MK SPA KW2

Great Lakes Ajo«lyttal-Oak Creek

Andrea Statha*. Project Manager

Tilt rtsula lit Aii'npan tppfy to the tOOfltt analyse* In aeeor4ana *U» tfit chain ofaaatfioeumtal. Tkii auifytoi rlpon mat be nproJvctJ to ta cnti^ly.

Page 7 of 12

1-01/2003 14:37 14146450645 LAKE STATES INDUSTRI

12/01/2003 flUN 0:42 FAI4145709461 Great Lakes AnalyticalPAGE 10


140 East Ryan RoadOtt Creak. Wisconsin 53154

Emalli(414)570-0460 FAX (414) 57 -9461

Uke Sana InduatruU Service

3 HE. Greenfield Ave.Milwaukee WI, 53204

Project Milwaukee Sotay Coke SitePro/act Number [none]Project Mmgo: TomJicotoon

fepwto*12/01/03 12:35

PotydilQrmated BIpheayls by EPA Metfrod 8082Great Lake* Analytical-Buffalo Grove

AnolytelUpoctinJ

RooM Umh Unit* Dilution Bwcfc Planted Analyzed Mnbod Noioi

T024(W3111Sfr*7)W«it»(S) Sampled: 11/12/V3 10:15 Received: 11/14/03 15:3< C29

PCB-1D16PCB-1221PCB-1232PC8-1242PCB-1248PCB-1254PCB-1260

Surrogate! Trirackloro-mcta-xylatieSurrogate: Dceodiloroblphcnyl

NDNDNDNONDNDND

1520 ug/kg«d 10 31IM4» 1I/2W03 1)/25A»3 EPA«M2152015201520i52015201520

»

•

V

•

n

42.4% 10-12S411% 10-143 • H

TOZ5(W31115t48)Wute<S) Stmpltd: 11/12/03 10:00 Racdvtd: 11/I4/Q3 1S;M C23

PCB-IOI6 ND 1500 ng/k|PCB-1221 ND 1500PCB-1232 ND 1500PC1S-1242 ND 1500PCS- 1248 ND 1500PCB-1254 NO 1500PCB-1260 ND ISOt)

jwa 10 3110

Surrogate: TetmcHloro-matarsyleHf 63Stt 10-125Surrogate; DecacUenblpbtnyl 155 % 10-143

*U 11/21V03 11/2 S/03 EPA 8082

*J

U

T0290V31115«.»9)Wa«M(S} Sampled: 11A3/D3 14JO Received: 11/14*3 15J« G23

PCB-1016 ND 1470 ug/k|PCB-1221 ND 1470PCB-1232 ND 1470PCB-1242 ND 1470PCH-1248 ND WTOPCB-1254 ND 1470PCB-1260 ND 1470

twrt !D 3UC

Sumgait: Taradiloro^ftia-^ytaie 1060 96 JO-I2SSurrogate: DecacMomblplwyl 289 9t 10-143

4« liftMM l\f2iva EPA 8082

Hf t


Andrea Siathaa, Prqjcct Manager

7S« mH/iB in aUf upon offfy to At aafla amfyssi In maxrdaKt wM OH dim efautoety daemon jt^t an«lj>iicml rrport mat tt rwpndiicet lit lit tMtnfy.

Page 8 of 12

12/01/21303 14:37 1414G450&45 LAKE STATES INDUSTRI


PAGE 11


140 East Ryan RoadOak Creak, Wisconsin 53154


Lake States Industrial Service311 R Greenfield A vc.Milwaukee WI. 53204

Project Mflwmkcc Solvay Coka SiteProject Number [none]Project Manager Tom Jacotoon

Reported]12/01/03

Polychlorinated Biphenyls by EPA Method 8082

Great Lakes Analytical-Buffalo G

AnalyteReporting

RauJt Uimt Unto Ottawa Bach Prepare! Analysed Method Now

T03J (W3111S6.J 1) WMK (S) Swnpled: H/12/B311:45 Received: 11/14/09 15:36 G23

PCB-lQIft ND 1380 MtAiPCB-1Z21 ND 1380PCB-1232 ND 13*0PCB-1242 NO Z3SOPCB-1248 ND 1380PCB-1254 ND 1380PCB-1260 ND 1380

r** »0 31 1C

Surnogoit: Telnchlaro-*i*ta-wlcne 934 % 1 0-1 25Surrogate; Decochlotvbiptusnyl 93.S % 10-143

H4S It/Zvoj uaSA)3 EPA SOS2

H

Great Lakes Analytical-Oik Creek Tht nent/cr In Alt nperl apffy H itt lamfltx tMfyttt In aeeonlanet wifA Ik* duiii ofOOttiy document UU> tamfyHfal repan MUM b» npntaeei lit to tnlinlr.

Andrea Staihai, Project Manager Page 9 of 12

:?/01/2083 14:37 14145450645 LAKE STATES INDUSTRI PAGE 12



140 EMt Ryan RoadOak CreeK, Wisconsin 53154

Email: lnfDQglalabs.com(414)5700460 FAX (414) 570-8461

Lake States Induwritl Service

Milwaukee WI. 53204

Projecc Milwaukee Selvgy Cake SiteProject Number [DOM] Rcpntod:

Project Manage: Tom Jneoteoa 1 2/01 /03 1 i35

BTEX by EPA Method 8260B - Quality ControlGreat Lakes Analytical-Buffalo Grove

AtMlytc MtullJKCpQCQUf Bpntt 3Q1BDB

Umit Unto Lcvd Renlt%REC RPD

Batek 3110330 - EJPA SWOB (P/T)

Black (31 10330.BLK1)BenzeneTolunwBdiylhonMna

Sumgait; DlbnmefiuorefunkoneSitrngait: 1 ,l-Q\cHortx>Ouuu*USumgait; Jbhienf-tli

LCSO110330-B51)BenzeneTolueneCtDylbcnecacToml Xylonos

Sumgait: DihnmtfluommethantSufogau: I,l-Dlcklerotiliart»tlfSafngele: Tohacnr-JiSurrogate: 4-Brt>mqflia>roheaitxt

LCS Dup (3110330-BSD1)amzeneToluoiDEtiiyOwnzeoeTumi Xyfcaa

Surrogate: DlbromoflitonmeAanfSurrogate; l,2-Dtdthro»AaiM^4Surrogate folwme^SSurrogate: 4-SramqflttonlKiiam

KDNDNDND

SO.)

51.851.0

37.4186

58.646.3J3J63J

4«.S51.457J

179

14.0

50.4eo. e

Prewnoi 11/14^3s.oo ue*e2JO

2SOaso «

* JAOJftO.«.«M.O

Prepared: 1 I/I MBS.OO tiftt* 50.0250 ' 50.0250 " $0,0250 ISO

50.050.0SO.O

» SO.O

Prepared: 11/14/03s.oo vgrag so.o

2SO " 50.0250 ' ISO

SO.Osa.oSO.Oso.o

AnalyMd: U/2.0/03

JOS 66.4-14576.4 S9J.I11101 64.5-1)99S.S 45.8-Hi

Analyzed: 11/20/03104 63.5-145102 65.S.143115 M.7-140124 J9.7-147

117 66.4-14)92.6 S»J-I7!106 64.5-11912» 45.1-145

Analyst* 1 1720/0397.0 63.5-145 b,St 34.6103 65.5-143 07«i 31,5115 64.7.140 0.174 J6.4119 59.7-147 3.84 4]^

109 66.4-145X3J 59.3-ltl101 64J.I39111 43J-14S

Great Lakes Anfllytical-O«k Creek ninatliMt* Ait m*n apply* riutompta amtfyirt l«aceer<danee wM At ota/i t>fneledf torment, 'ftiii tnofyOeal report mtul be rtfrvjtteal in it*

Andrei Stitbas, Project Manager P««elOofl2

•01/2003 14:37 14146450645 LAKE STATES INDUSTRI

12/01/2003 M 0:43 FAI 4145709461 Great Lakes Analytical

PAGE 13


140 Efltt Ry«n ftoaflOak Crw*. Wlscomln 52154

Email: lnlbQglal8tw.com(414) 570-3460 FAX (414) 570-9461

Lake Stales rn<fciatrial Soviet311 E. Greenfield Ave.Milwaukee WT. 53204

Project; Milwaukee SoIvmyCokc SteProjaBtNwnbcr. [none]

Project Msnugw; Tamlaeobmi 12/01/03 12:35

Folychlorinated Blphenyb by EPA Method 8082 - Quality ControlGreat Lakes Analytical-Buffalo Grove

Aiulyte RauH Umii UntoSpwv SoutDOLevel Rault %REC

KRBC RTOumto RrD Llfflit Notcv

Batch 3110448 . £PA 3550B

Blank (3I1044S-BLK1)PCB-1016

PCB-1221

PCB-1J32PCB-I2«

PCB-1248

PCB.12S*

PCB-1260

Sttff&fOtC,* TiftfOCnforo tttfttf^jnffitSurragalt: Deeeeklerobtpkeiyl

LC5 0110448-851)PCB-1016

PC&-1260i* -. , . , .

SumgOK DfcatAtembifjhtayi

bCS Pup (31 tO*««-BSPl)PCB-1016

PCB-1I60

Surrogate: TtifacUorv-melo^yl*ncSiirrofutt; DccacrthrvbipttcHyl

ND

ND

NO

ND

ND

NO

ND

10.1

134

»

122

96.6

/Arf17.2

23.0 ugOtgwd

25,0

25JO

25.0

25.0

23.0 •

2S.O

-

2S.O Mftfcg we

25.0

1*

2S.O ug&gwti

2S.O

p

Prepared: 11/20/03

32.9

Prepared: 11/20/03

167

Prepared: 1 1/20/031 1(7

167

3J.43S.4

Analynk

SS.S61.1

Analyzed:

!2.0

JJ./ ""

Analyzed-.7J.1S7.S

40.7SIJ

11/21/03

IQ-t23JO-/43

\ 1/21/0310-13314-1J4

10-W10.143

11/21/0310.U3 ?JI 200l4-)3* 10.7 200

;OL/«

Great Lakes Analytkal-Oak Credc Thf rftula m (Mr n»^wT efptylelhe ttnptu unalyttA fc accordant* vidi die eluax <tf

Aadica Staihaa, Project Manager PflgelloflS

i-'0l/20B3 14:37 1414S450645 LAKE STATES INDUSTRI PAGE 14

12/01/2003 ION 0:43 FAX 4145709461 Great Lakes Analytical iOH/016

GREATLAKES 140 E«t Ryan Rort EmaH: lnfeOglaUilx.comANALYTICAL OaKCreek. WUconsIn 53154 (414)570-9460 FAX(414) 670-9461

Lake SUMS Industrial Service Project: Milwaukee Solvay Coke She3\ \ E. CieenfieW Avfc Project Number* [none}Milwaukee WI, 53204 • Placet Minager Tom Jacobstm 12/0^3)2:35

Notes and DcflnWons

G23 ThammplewM diluted due to tha pmeAOB oTMgh eonoenMtioru vf non-taifet miilyto*.

DET Anslyte DETECTED

ND AiulytelitOT DETECTED >t or abotethitqiathigUinit

NR •MatHepnrted

dry Sample RsiJtanûrwl on > dry wdgbt b«slj

RPD RaladveFcreMtDifleteaML

H

Great Lake* Analytieal-Bnflalo OTOVB Wisconsin DNR Conifiestiott Lab ID: 99991 7160

Great Late Anatytlcftl-Buffiilo Grove NELAPPlinuiyAeereditttian:lIltnoi« #100261

Great Lakes An4ytical-Bu£WoQroveNELAP Secondary Accreditation: New Jeoey ML001

Great Lakes Analytical-Oak CrecX WI Winconnn DNR Cwtificatioa Lab ED: 341000330

Grart liKe* Analytiul-Oak Creek, WI NELAP Primary Accreditulon: niinoi* #1 00307

Note: For analyses that require NELAP •corcdjtation, all aiulyteg, by matrix and method, are accredited following current NELAPstandards wnl*s» specifically noted by M«y of a qualifier lined above.

Great Lakes Analytical-Oak Creekoandy donoiou. niionafytttal report mat At mpnJaetfi* IB tHfrey.

Andre* Stathan, Project Manager Page 12 of 12


CHAIN OF CUSTODY REPORT

1380 Buacti Partway 140 E. Ryan RoadBuffalo Grow. IL 600694505 Oak Creek, Wl 53154

(847)806-7786 (414)570-9460 :

FAX (847) 808-7772 FAX (414) 57O9461

Hapon to: T<*» ->flLA acitoil a Shtenad G Ccurf.rO

HofBottbePmservatim Used

Protect it/POt:

LABORATORYID NUMBER

PIO;

PICK

HOf 'It- -ol

cs

k—• [.-.,•••-= CS

« °JS LO

£?CB

fts

r

mtn

01



1380 Busch Partway 140 E. Rya/» RoadBufiaJo Grove. !L 6M69-45C5 Oak Cree k, Wl 53154

(847) 808-7766 (414) 570-9460FAX (847) 806-7772 FAX (414) 570-S4S1

NJ

(S

i—' rot -; cs

CHanC BUI To:

Address:

StatoS,Program:

77fltone*:^xEO

a DM atuft IDAY

D NO-

igitUrtDlraOrrtlarow

oof MCLtn WEMP;

» of BottlesPmswvatt/a Used

M<-b

~r&i4*j<+

fij

WDf

Wft

P)D:

rtD:

W

^

v?

//4T^^

^«T

r-?

Mf/V

WWfflfi

K

OiAwabto ftctafltt I DeAwy iWsWrod.D STO DOU.I> IGLA M qi«rt_g SHOP* Q i

cnaui

m

men

en

12/16/2003 TUE 22:19 FAI 4145709461 Great Lakes Analytical iOOl/006

GREAT " > : i uLAKES 140 East Ryan Road Email: [email protected] oak creek. Wisconsin 53154 (414)570-9460 FAX (414)570-9451

17 December 2003

Tom JacobsonLake States Industrial Service311 E. Greenfield Ave.Milwaukee, Wl 53204RE: MSCG Pre Treatment List


Sincerely,Great Lakes .Analytical


12/16/2003 TUE 22:19 FAX 4145709461 Great Lakes Analytical

140 East Ryan RoadOak Creek, Wisconsin 53154


Lake Stem Industrial Service311 E. Greenfield Ave.Milwaukee, WI53204

Project: MSCO Prc Treatment ListProject Number: [none]

r Tom JacobsoaR*port*4:

12/17/OJ 09.51


SanptelD Laboratory ID Matrix Dxt* San^dod Date Received

T032

T038

W312132-01

W312132-02

Waste (L)

Waste (L)

12/10/03 16:30

12/10/03 16:30

12/10/03 17:00

12/10/03 17:00

Great Lakes Analytical-Oak Creek Thf naulu in thti report apply to tilt samples arufyud in accordance wick tke chain ofcustody document. This analytical report mat bt npnductd in ia intirtty.

Andrea Stathas, Project Manager Page 1 of 4

12/16/2003 THE 22:19 FAX 4145709461 Great Lakes Analytical




Late States Industrial Service31 IE. Greenfield AV«LMilwaukee, WI53204

Project: MSCC Pro Treatment ListProject Number, [none]

Project Manager TomJacobson 12/17/0309:51

Polychlorinated Biphcnyb by EPA Method 8082

Great Lake* Analytical-Buffalo Grove

Analytt RemitReporting

Limit Units Dilution Batch Prepared Amtyzcd Method Nowa

T032 (W312132-01) Wute (L) Sampled} 12/10/03 16:30 Received: 12/10/OT17:00"

PCB-1016 ND 7500 u«/PCB-1221 ND 7500PCB-1232 ND 7500PCB-1242 ND 7500PCB-1248 ND 7500PCB-1254 ND 7500PCB-1260 ND 7500

ks i 3120

SurrogaU:Tetrachloro-mtta-xylene 146% J 0-1 25Surrogate Dccachlorobipfienyi 58.3 % 10-143

377 12/1.S/03 12/1.SA)3 EPA 8082

H

T03«(W312132-02) Wait* (L) Sampled: 12/10/03 16:30 Received: 12/10/03 17:00

PCB-I016 ND 7500 ugiPCB-1221 ND 7500PCB-1232 ND 7500PCB-1242 ND 7500PCB-1248 ND 7500PCBM254 ND 7500PCB-1260 ND . 7500

fcg 1 J12C

Surrogate: TetracUoro-meta-xylene 69.0 % 10-125Surrogate; Dccacfthroblpheitjl 60.5 % 10-143

3T7 12/1.F/03 12/1 !A)3 EPA 80(t2

Great Lakes Analytical-Oak Creek The nsula in this report apply to At samplti anatjnid in accordance with the chain ofcustody documtnt. This analytical report mint b* reproduced la la entirety.

Andrea Stadias, Project Manager Page 2 of4


!S| GREATLAKESANALYTICAL



Lake State* Industrial Service311 E. Greenfield Ave.Milwaukee, WI53204

Project: MSCO Pro Treatment ListProject Number, [none]

Project Manager TomJacobsonReported:

12/17/0309:51

Potychlorlnated BIphenyls by EPA Method 8082 - Quality Control

Great Lakes Analytical—Buffalo Grove

An»JytcReporting

Result Limit UnitsSpikeLevel

Somce %REC RPDResult %REC Limita RPD Limit Note

Batch 3120377 - EPA 3S80A (Dilution)

Bbuk(3120377-BLKl)PCB-1016

PCB-1221

PCB-1232

PCB-1242

PCB-124S

PCB-1254

PCB-1260

Sumgait: Ttlradiloro-meto-jylmtSurrvfdtt: Decactilorobiptunyl

LCS(3120377-BS1)PCB-1016PCB-1260

Surrogate: Trtrackloro-mtta-iylfivSurrogaa: DtcacUarobipkenyl

Duplicate (3120377-DUP1)PCB-1016

PCB-1221

PCB-1232

PCB-1242

PCB-124*

PCB-I2S4

PCB-1260

Surrogate: Tclruchloro-mtta-zyleneSurrogate: Decachlonbiphayl

Prepared & Analyzed:ND

ND

ND

ND

ND

ND

ND

589726

7500 ugftg

7500 "

7500

7500

7500

7500

7500

m

m

10001000

Prepared & Analy/ed:3560

3290

636H9

Source:NDNDNDND

ND

NDND

1010671

750 ug/k*750

»"

W312132-017650 ugdcj

7650

7650

7650 "

7650

7650

7650

m

"

5000

5000

1000

1000

Prepared & Analyxed:

10201010

NDNDNDNDNDNDNO

12/15/03

5S-9 10-12572.6 10-143

12/15/0371.2 10-1M65.S 14-134

63.6 10-12581.9 10-143

12/15/03

99.0 10-12565.3 10-14}

20202020202020


Andrea Statha*, Project Manager

T)it TON/tt In Ih'a report apply to At naaiplu anafyied In accordance with the chain cfcustody document. This analytical report mat bt rtproductd in iti entirety,

Page 3 of4

12/1(5/2003 THE 22:20 FAX 4145709481 Great Lakes Analytical P05/006

jgSBGREATSil| LAKESKBM ANALYTICAL

Lake States Industrial Service311 E. Greenfield Avc.Milwaukee, WI 53204


Project: MSCOPre Treatment ListProject Number [none]

Project Manager. Tom Jocotraon


RtporrwJ:12/17/03 0931

Notes and Definitions

DET Aiwlytc DETECTED

NO Aiwfytc NOT DETECTED at or nfxrve the reporting limit

NR Not Repotted

dry Simple remit* reported on » dry weight basi*

RPD Rctata Percent DifferenceL Thifquah'tyCMIrolnKMuienienti} below tholabonUltyetlabluhed limit,

H This quality control m*Muremenl in above the liboratmy cnxbliihcd limit.

Great Lakes Analytical-Buf&lo Grove Wisconsin DNR Certification Lab ID: 999917160

Great Lakes Anatytical-Buf&lo Grove NELAP Primary Accreditation; Illinois # 100261

Gnat Lakes Analytical-Buffiilo Grave NELAP Secondary Accreditation: New Jersey #ILQO I

Great Lakes Analytical-Oak Creek, WI Wisconsin DNR Certification Lab ID: 341000330

Great Lakes Analytical-Oak Creek, WI NELAP Primary Accreditation: Illinois #100307

Note: For analyse* that require NELAP accreditation, all analytes, by matrix and method, are accredited following current NELAPstandards unless specifically noted by way of a qualifier listed above.

Great Lakes Analytical-Oak Creek The results In this report appfy to the sampla anafyxtd in accordant with tke chain ofcustody document, TMs analytical report must ht reproduced In Us entirely.


| GREATj| LAKES(•ANALYTICAL


1380 Busch Parkway 140 E. Ryan RoadBuffalo Grove. IL 60089-4505 Oak Creek, Wl 53154

(847) 808-7766 (414) 670-9460FAX (847) 808-7772 FAX (414) 570-9461

LABORATORYID NUMBER

iPH3:

WD: J/3J

PfD:

rtO:

PJD:

U

PID:

§J_

ITPtfJ:

10]

P/D:

RELINQUISHED OAft:

TIME

RECEIVED

RELINQUISHED

COMM&fTS:

DATE RELINQUISHED

77M£

DATE

TIME

flBQEMED

PAGE

DATE

TIME

OF i


APPENDIX G-2

Analytical Test DataRelating to Liquid Discharges to

Milwaukee Metropolitan Sewerage District

EarthTechA Tyco International Ltd Company

L:\work\72534\Adrnin\Reports\Rpttext.doc

Preserving The Environment <Improving Water Quality

December 4, 2003

Mr. Tom JacobsonLake States Industrial Services311 East Greenfield AvenueMilwaukee, WI 53204

Subject: Notice of Intent 2003.037

Dear Mr. Jacobson:

The Milwaukee Metropolitan Sewerage District (MMSD or District) has received a Notice ofIntent submitted by Environmental Associates, Inc., for the discharge of water from the formerSolvay Coke and Gas site, located at 311 East Greenfield Avenue, Milwaukee. The District isapproving the discharge of water from this site subject to the following conditions:

1. The former Solvay Coke and Gas site must be in compliance with the general and specificlimits set forth in Chapter 11, MMSD Rules. The pH discharge must be greater than 5.0standard units.

2. In the water discharged to the sewer system, the following pollutant levels may not beexceeded.

Cadmium 1.5 mg/1Chromium, Total 8.0 mg/1Copper 6.0 mg/1Cyanide, Total 5.0 mg/1Lead 2.0 mg/1Mercury, Total 0.0026 mg/1Nickel 4.0 mg/1Oil and Grease 300 mg/1Zinc 8.0 mg/1Total Suspended Solids 100 mg/1Total VOC Scan <5 mg/1

3. At least one sample must be taken and analyzed for the above pollutants during discharge.

4. No discharge may occur during periods of at least 0.5 inches of rain. If it does rain, alldischarge from the former Solvay Coke and Gas site must cease to the sewer system.Commencement of the discharge cannot occur until 12 hours after the rain has stopped.

miiwaukee metropolitan sewerage District260 W. Seeboth Street, Milwaukee. Wl 53204-1446

414-272-5100 • www.mmsd.com Q£>

Mr. Tom JacobsonLake States Industrial ServicesDecember 4, 2003Page 2

5. The total volume of water discharged should be reported to Mr. Harvey Matyas, DistrictSenior Industrial Waste Engineer, when the pumping is completed. At that time, the theformer Solvay Coke and Gas site will be billed by the District at the rate of $1.05 per 1.000gallons discharged.

The policies and procedures for these types of discharges to the sewer system are currently beingstudied by the District. You should be aware that this approval may be rescinded at any time orchanges to your conditions may occur.

If the former Solvay Coke and Gas site is in violation of this letter of approval at any time, theDistrict may take enforcement actions which may include, but are not limited to, issuing a Noticeof Noncompliance, a Notice of Violation or seeking injunctive or civil penalties up to $10,000 perday per violation.

If you have any questions concerning this matter, please contact Mr. Harvey Matyas, SeniorIndustrial Waste Engineer, at 225-2164.

Sincerely,

Peter R. TopczewskiWater Quality Protection Manager

Cc: Mr. Joe Michaelchuck, P.E.Environmental Associates, Inc.

PRT:HJM:jds

NOI 2003.037 Solvay Coke and Gas Site

.MNMENTAL ASSOCIATE, INC.

P.O. Box 136 • Thiensville. Wisconsin 53092OFFICE: 262 242.1088 • TOLL FREE: 800.494.4645 • FAX: 262.242.6554 • www.eolwl.com

December 4, 2003

Milwaukee Metropolitan Sewerage DistrictAttn: Harvey MatyasPO Box 3049Milwaukee, Wisconsin 53201-3049

Re: Notice of Intent to Discharge Non-Domestic Wastewater, Former Solvay Coke and GasSite, 311 E. Greenfield Avenue, Milwaukee, Wisconsin

Dear Mr. Matyas:

The purpose of this correspondence is to provide a letter of understanding regarding the proposedwastewater discharge at the Former Solvay Coke and Gas Site. This letter will describe theprocess, operations, activities, and circumstances that will produce wastewater at this site as wellas plans for discharge. The Notice of Intent to discharge non-domestic wastewater, as requiredby Section 11.401 of the MMSD rules, is provided in Attachment A.

Site Background

The Former Solvay Coke and Gas Site is being deconstructed in phases by Lake States IndustrialServices. Various sized aboveground storage tanks (ASTs) associated with the Former SolvayCoke and Gas Production Facility are located throughout the site. The ASTs have deterioratedover time and currently contain residual coal tar and storm water. As a part of Phase I ofdeconstruction these ASTs will be emptied, cut open, cleaned, and removed from the site.

Proposed Discharges

Non-domestic wastewater is generated in one of two ways:

(1) Contaminated Water that has Accumulated in each AST as a Result of Rain Infiltration

As part of the deconstruction of the site, the ASTs will be emptied, cleaned and cut up for scrap.The first step in the AST removal process is to drain the water that has accumulated in the tanksas a result of rain water infiltration. It is proposed that the water that has accumulated in thetanks as a result of rain infiltration be drained from each AST and disposed of through thesanitary sewer. Because this water has been held in these tanks for a number of years, in directcontact with residuals within the tanks, and because cyanide has been detected in this water, thisdischarge would not be considered "unpolluted water" that could otherwise be routed directly tothe waters of the state under a WDNR permit.

ENVIRONMENTAL ASSOCIATES, INC.

The total volume of water that will be discharged from the draining of contaminated water thathas accumulated in each AST is expected to be approximately 25,000. Water will be dischargedin five batch discharges of 5,000 gallons each over a four week period of time. It is anticipatedthat all five discharges will be completed within four weeks of receiving discharge approval fromMMSD. The proposed discharge location is a toilet (4-inch line) located in Building #11 (Figure1, Attachment D).

A representative sample of water that has accumulated in the tanks as a result of rain infiltrationwas collected on November 19, 2003 and submitted to Great Lakes Analytical in Oak Creek,Wisconsin. The sample was analyzed for the compounds listed in MMSD section 11.202 and11.203(l)(a). No compounds were detected, above laboratory method of detection limits, withthe exception of cyanide (0.0736 mg/L), which was detected below the MMSD limit of 5.0mg/L. Wastewater analytical results are summarized in Table 1, Attachment B, and presented inAttachment C of this submittal.

(2) AST Wash Water

After the contaminated water in each tank is emptied, coal tar residuals will be removed andproperly disposed. The empty tank will then be thoroughly cleaned using high pressure washingequipment. It is proposed that this AST wash water also be discharged into the sanitary sewer.

It should be noted that AST wash water has not yet been generated and, therefore, has not yetbeen tested at the site for the pre-treatment parameters listed in MMSD Chapter 11.203. It isanticipated that this wash water will require pre-treatment prior to being discharge into theMMSD sanitary sewer to meet Chapter 11.203 limits. Treatment of this water will consist of aclarifier cell (frac tank) and liquid carbon canisters.

In order to gain approval for discharge, it is proposed that prior to each batch discharge a sampleof the treated water be collected for Chapter 11.203 parameters, pH and TSS. These results willbe compared to Chapter 11.203 limits prior to discharge and, if they fall below these limits,discharge will proceed. If any of the Chapter 11.203 limits are exceeded, additional treatmentwill be conducted and the effluent will be retested prior to discharge. All testing results will bemade available to MMSD at their request.

The total volume of AST wash water that will be discharged to the sanitary sewer is expected tobe approximately 25,000. AST wash water will be discharged in batches. It is anticipated thatthe discharging of AST wash water will be completed within four weeks of receiving approvalfrom MMSD. The proposed discharge location is a toilet (4-inch line) located in Building #11(Figure 1, Attachment D).

2S:\Organization\Projects\855Solvay\004MMSD\855mmsd_noi_12-03.doc

ENVIRONMENTAL ASSOCIATES, INC,

Summary and Conclusion

Lake States Industrial Services is requesting written permission to discharge the above describednon-domestic wastewater at the Former Solvay Coke and Gas Site. As Lake States IndustrialServices would like to commence discharge before freezing occurs, your prompt review wouldbe greatly appreciated. If you have any questions or concerns, please feel free to contact us.

Sincerely,

Environmental Associates, Inc. Lake States Industrial Services

Joe Michaelchuck, P.E. Bert SneadSenior Engineer President

cc: File

Encl: $250.00 check payable to MMSD

3S:\Organization\Projects\855SolvayV004MMSD\855mmsd_noi_12-03.doc

ATTACHMENT A

Notice of IntentTo Discharge Non-domestic Wastewater,As Required by sec. 11.401, MMSD Rules

L Facility Information

(a) Facility name Former Solvay Coke & Gas Site

(b) Facility address311 E. Greenfield Ave.

Milwaukee, WI 53204

(c) Mailing address311 E. Greenfield Ave,

Milwaukee, WI 53204

(d) Contact person Tom JacobsonNameV.P. (Lake States Industrial Services)

Tide

414-645-0635 (office)Telephone

(e) Business description

The Former Solvay Coke and Gas Site is being deconstructed

by Lake States Industrial Services. Various above ground

storage tanks (ASTs) associated with the Former Solvay Coke

and Gas Production Facility are located throughout the site.

The ASTs have deteriorated over time and currently containresidual coal tar and water. As part of Phase I of deconstruction

these ASTs will be cut open, cleaned and removed from the site.

(f) Five digit NAICS code or four digit SIC code N/A

IL Discharge information

(a) Reason for submitting this notice of intent:

Constructing a new facility that will discharge process wastewater to the sewerage system

Taking possession or control of an existing facility that discharges process wastewater

Changing the physical size or operations at an existing facility to the extent that wastewatervolume or content will be substantially changed, including, but not limited to, a change inthe annual average daily discharge flow rate of 20% or more

Proposing to discharge contaminated groundwater

Commencing or modifying a discharge of hazardous waste that requires reporting accordingto sec. 11.411, MMSD Rules

Proposing to discharge non-domestic_JL_ Other. Explain on an attached page wastewater not previously reported

to the District.(b) Proposed date for the commencement of discharge as soon as possible (12 / 0 5 / 0 3)

(c) Describe the processes, operations, activities, and circumstances that will produce the non-domestic wastewater covered by this Notice of Intent

see cover letter

(d) Wastewater discharge rates for the facility as a whole. Complete this section if the dischargeis not a one-time discharge

Flow rates (gallons per day)Existing Proposed

Domestic

Non-domesticProcess

Non-contactcooling approximately 1,785 gallons per day

(see cover letter)Other

(e) Discharge type (fill in the spaces that apply)

1. Continuous discharge: hours per day days per week

2. Batch discharge: 1 0 , OOOgallons discharged per batch par ( 5 hai-nbas total)Frequency Time

3. One time discharge: gallons discharged over days

4. Other (explain the timing and type of discharge)

(f) List the pollutants potentially present in the wastewater covered by this Notice of Intent

See attached analytics.

(g) Sample results. If you are able to sample the wastewater covered by this Notice of Intent, thenattach sample results according to the instructions.

(h) Would the wastewater covered by this Notice of Intent be regulated as hazardous wasteaccording to sec 40 CFR 261 if it was not discharged to the sewerage system?

Yes x NO

If yes, contact the District for additional reporting requirements.

(i) Describe any proposed treatment procedures or equipment

None.

(j) Enclose a drawing of the site where the discharge will occur, This drawing must identify allconnections to the sewerage system; the processes, operations, or activities generatingwastewater; treatment facilities, and potential sampling locations.See Figure 1 .

DJL Certification and signature

/ certify under penalty of law that this document and all attachments wereprepared under my direction or supervision in accordance with a systemdesigned to assure that qualified personnel properly gather and evaluate theinformation submitted. Based on my inquiry of the person or persons whomanage the system or those persons directly responsible for gathering theinformation, the information submitted is to the best of my knowledge and belieftrue, accurate, and complete. I am aware that there are significant penalties forsubmitting false information, intruding the possibility of fine and imprisonment

violations^

Signature ' £ Date

Primed name and title

Notice of Intent

ATTACHMENT B

Table 1: Non-domestic Wastewater Evaluation, November 19,2003,Solvay Coke and Gas Site, Lake States Industrial Services, 311 E. Greenfield Ave., Milwaukee, Wisconsin

'arameter

Oil and Grease

Cyaniderss ' " " -3CXX:>sxt-*:a!a&"f>

PH • • •~'"""'"'"M'taJB1*-" •• -• — •••~irTiT«»BitiMPirn~nrin — "

Oreonic Compounds:Benzo(a)andiraceneMethyl bromide (Bromomethmne)Methyl chloride (CMoromethane)Phenanthrene

II ••.••-!',• ' \yjTf fft's3tSt$Styffi££;l&&EF-'3*'4f''.

[Lv/isc CompoundsllAcroleinAldrinalpha - BHCbeta - BHCdelta - BHCgamma - BHCAlkylated LeadBenzo(a)pvreneChlordane4,4-DDD4,4-DDE4,4-DDT3,3-DkhIorobenzidineDieldrinEndrosulfan IEndrosulfan IIEndosulfan SutfateEndrinEndrin AldehydeFluorantheneHeptachlorHeptachlor EpoxideHexachJorobenzeneMirex7entachlorobenzenePCB - 1016PCB - 1221PCB - 1232PCB - 1242PCB - 1248PCB - 1254PCB - 1260Toxaphene2,4,6-Trichlorophenol1 ,2,4,5-Tetrachlorobenzene

Selected MetalsCadmiumCopperLeadMercuryNickelSilverZinc

Units

mg/L

mg/L

mg/L

mg/L.V — * .- J*£"

mg/Lmg/Lmg/Lmg/L

v :?-. '..":.

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lrag/L

MMSDLimits'

300

5.0 " '' "

"£$'~^'• '", "" ^V. JT' ' •'•'•

0.0620.1830.3690.051

- ,-.'''^.V j

390-----131301.3--1.32600.65

See Footnote2

See Footnote2

See Footnote2

1.3-

1300.65-

130130130

See Footnote3

See Footnote3

See Footnote3

See Footnote3

See Footnote3

See Footnote3

See Footnote3

26130-

1.56.02.0

0.00264.05.88.0

Tank 13 Spill

<5

0.0736

<5

6.87 '""""' ... . '. M~*iSi"2

<0.010<0.010<0.010<0.010

J " . " . '"*

<50<0.03<0.02<0.03<0.03<0.03

NT<10

<0.26<0.04<0.03

<0.160<20

<0.03<0.03<0.05<0.1<0.1

<0.15<10

<0.04<0.02<10NT<20<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<10<20

<0.0005<0.05

<0.005<0.0002

<0.05<0.05<0.5

Foooiocea:1 MMSD discharge liinti bated on MMSD Chapler 11.202 and 11.203(IX«) local limits1 TTie MMSD disdurge limit fat Endomlfrn is 1.3 ug/L1 The MMSD discharge limit for Polychlorinated Biphenyl's is 1.3 ug/L. This applies to each specie

polychlorinMed biphenyl.

NT-Not Tested

- = No discharge standard

of

Environmental Associate*, Inc.855mnwill-03

ATTACHMENT C

12/U2/2U03 1UK 5:07 FAI 4145709461 Great Lakes Analytical IP 1)3/032

i GREATLAKES

(ANALYTICAL140 East Ryan Road

Oak Creek. Wisconsin 53154Email: [email protected]

(414) 570-9460 FAX (414) 570-9461

Lake States Industrial Service311 E. Greenfield Ave.Milwaukee WI, 53204

Project: MSCC3 Pre Treatment ListProject Number [none]

Project Manager: Tom JscobsonReported:

12/02/03 17:03

ANALYTICAL, REPORT FOR SAMPLES

Sample ID Laboratory ID Matrix Dale Sampled Date Received

Tank 13 Spill W3II185-01 Water 11/19/0313:30 11/19/0314:40


indrea Stathas, Project Manager

Tht raula in this report apply la the lamples analyzed In accon/uncr with the chzincustody dncunieni. This analytical rtpnrt must be reproduced in ill tntirety.

Page 1 of l -

12/02/2003 TUE 17:04 [TX/RX NO 5084]

12/02/2003 TIE 5:08 4145709461 Great Lakes Analytical

GREATLArvEo

ANALYTICAL140 East Ryan Road

Oak Creek, Wisconsin S31S4Email: [email protected]

(414)570-9460 FAX (414) 570-9461

Uikc States Industrial Service311 E. Greenfield Ave.Milwaukee Wl, 53204

Project: MSCG Pre Treatment ListProject Number: [none]

Project Manager: Tom JacobsonR«p«rt*d:

12/02/0317:03

General ChemistryGreat Lakes Analytical—Buffalo Grove

Analyte

Tank 13 Spill (W31118S-01) Water

Cyanide (total)Oil & Grease

Remit

S*mpl«d: 11/19/03

0.0736ND

Reporting1 Imil Units Dilution Batch

13:30 Received: 11/19/03

o.oi Co5.00

mg/l 1• II

14:40

3110J343110495

Prcpmvd Analyzed Method

11/25/03 H/2S/03 EPA9012A11/21/03 11/24/03 EPA 4 13.1

Notes

QC

Great Lakes Analytical—Oak Creek Tht nsulu In this report apply la the samples analyxd in accordance witli 111:: chaincustody document, Uiis analytical report must be reprvtiuced in la entirety.

jidrea Suthas, Project Manager Page 2 of

12/02/2003 TUE 17:04 [TX/RX NO 5084] ©on I

1Z/02/ZU03 TUK 4iU/iWbi ureai Lanes




Lake States Industrial Service

311 E, Greenfield Ave.Milwaukee Wl, 53204

Project; MSCG Pre Treatment ListProject Number [none]

Project Munagcn Tom JaeobjonReported:

12/02/03 17:03

Total Metals by EPA 200 Series MethodsGreat Lakes Analytical— Buffalo Grove

Anutyre

T»nk 13 Spill (W31118S-OI) Water

SilverCadmiumCopperMercuryNickelLeadZinc

ReportingResult Limit Units Dilution Batch Prepared

S.mpled: 11/19/03 13:30 Received: 11/19/03 14:40

NO 0.0500 mt/1 1 3110441 11/20/03ND 0.000500 " " 3120031 12/01/03ND 0.0500 " " 3I1044J 11/20/03ND 0.000200 " " 3H044S 11/20/03ND 0.0500 " " 3110441 11/20/03N D 0.00500 . . . »ND 0.500 -

Analyzed

12/01/0312/02/031 1/26/0311/20/031 1/26/U311/21/0311/26/03

Method

EPA 200.7EPA 2 13.2EPA 200.7EPA24S.1

--EPA "*00 7EPA 23Y.2EPA 200.7

Notes

QC

Great Lakes Analytical-Oak Creek 77i* mulu In this report apply In the samples analyzed in accnrdance with Ihv r:ha:ncustody document. This analytical report must bv rrprvduetct in its enllrvly.

uidrca Stathas, Project Manager Page 3 of 2?

12 /02 /2003 TUE 17:04 [TX/RX NO 5084] 12)005

run D;u5 I*AA Lanes iy uuu/


140 East Ryan RoadOak Creek. Wisconsin 53154


Lake States Industrial Service3 HE. Greenfield Avc.Milwaukee Wl. 53204

Project: MSCG Pic Treatment Li.itProject Number: [none]

Project Manager: TomJacobsonReported:

12/02/03 17:03

Volatile Organic Compounds by EPA Method 624Great Lakes Analytical—Buffalo Grove

AnMyte ResultReporting

Limit Units Dilution Baluh Prepared Analyzed Method Notes

Tank 13 Spill (\V311185-01) Water Snmpled: 11/19/03 13 JO Received: 11/19/03 U:40 QC

AcrolclnBromomelhan*ChloromcthancSurrogate: DlbromofluommttkuneSurrogate: l,2-Divhloroethanc-<i4Surrogate: Toluanc-d8Surrogate: 4-Bramt)fluorobenzene

NDNDND

50.010.010.0

3110438 11/20/03 11/20/03 EPA 624/8260B A-U1

108%75.6%104%99.8 %

75.8-12762.5-14576.6-1306S.9-123

Great Lakes Analytical—Oak Creek The results in this rtporl apply to th<t samples analyzed in accordance with the '.-hnin nfcustody document. This analytical report miat h* reproduced In Its tHIirvly.

jidrea Stathas, Project Manager Page ^ of 2?

12/02/2003 TUB 17:04 [TX/RX NO 5084] [g]00i;

;} THIS a:ua PM uu/uuwi breai Lanes Analytical

™ j~- —f "jfi ^^B GREATLAKESANALYTICAL


Email: [email protected])570-9460 FAX (414) 570-9461

Lake State* Industrial Service311 E. Greenfield Ave.Milwaukee WI, S3204

Project: MSCO Pre Treatment ListProject Number [nono]

Project Manager Tom JacobsonReported:

12/02/03 17:03

Organochlorinc Pesticides and PCBs by EPA Method 608Great Lakes Analytical—Buffalo Grove

Anulyte Raul IReporting

Limit Units Dilution Butch Prepare: Analyzed Method Nolc,

Tank 13 Spill (W31118S-01) Water SHmpIed: 11/19/03 13:30 Received: 11/19/03 14:40 QC

Aldrin

bcta-BHCdelta-BHCgumma-BHC (Lindanc)Chlordanc (tech)4,4'-DDD4. 4 '-DDE4,4'-DDTDieldrinEndosulfan IEndosult'on IIEndosulfan sulfetcEndrinEndrin aldehydeHepLaehlorT' -taclilor epoxide

phene» -j-1016TCB-1221PCB-.1Z12PCS- 1242PCB-1248PCB-1254PCS- 1260 ____

Surrogate: Tetrachlo ro-mcla-xytcnvSurrogate: Decachtnrobiphenyl

ND

NDNDNDNDNDND

-NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

0.0300 ug/l

0.02000.03000.03000.0300 "0.2600.04000.03000.160 • "0.03000.03000.0500

0.100o.ioo0.150

0.04000.0200

0.500O.SOO0.5000.500O.SOO0.5000.5000.500 ^_

82.4%32. K %

1 3110462 11/30/03 EHA608/8081/82

10-UO10-140


.idica. Stathas, Project Manager

Hit rtxultt in this report apply to thr xampltt analysed In accordance with the di~-custody document. This analytical i*ifi:r: mat be reproduced in ill entirety.

Page 5 of 2?

12/02/2003 TUE 17:34 [TX/RX NO 5084]

1 2 / U 2 / 2 U U 3 ILK PAA L3K6S

..SB GREAT'451 LAKESSmm ANALYTICAL




Project: MSCG Pre Treatment ListProject Number [none]

Project Manager. Tom JacobsonReported:

12/02/03 17:03

Base/Neutrals and Acids by EPA Method 625Great Lakes Analytical—Buffalo Grove

AnnlytcReportinc

Result Limit Units Dilution Batch Prepared Anulynxl Method Mole;

Tank 13 Spill (W311IS5-01) Water Sampled: 11/19/03 13:30 Received: 11/19/03 14:40 QC

Bcnz (a) anthraceneBenzo (a) pyrcne3,3 '-DichlorobcnzidineFluorantheneHexachlorobenzcncPhcnanthrcnc2,4,6-Trichlorophenol

Siirmgate: 2-FluorophenolSurrogate; Phenol-d6Surrogate: Nltrobtnztn<c-<tSSurruyattt: 2-FluorobiphenylSurrogate: 2, 4, 6-TrlbromophenulSurrogate: p-Tarphenyl-dl 4

ND 10,0ND 10.0ND 20.0ND 10.0ND 10.0ND 10.0ND 10.0

4.84 %4.19%18.5%Ht.5%17.7%17.4%

ug/1 1 3110

It •<

ti 1

M n

n II

10-11010-110

31.4-11010-11010-11010-147

424 11/19/03 11/21/03 EPA «i2S/8270CH M •II n it

M n *•

H II M

H n II

• H n

L" " " L

LH M m

It H tl

" H **

Great Lakes Analytical-Oak Creek 77i« results in this report apply to tit* samples analysed In atlconlanet with thecu.itn<fy document. This analytical rtport must be rtproducitJ in Its tntirtcy.

\ndrea Stathas, Project Manager Pngc 6 of H1?

12/02/2003 TT.TE 17:0-1 [T.X/RX NO 5084] © O o s





Lake States Industrial Service311 E. Greenfield Avc.Milwaukee Wl, 53204

Project: -MSCC Pre Treatment ListProject Number, [none]Project Manager: TomJacobson

Reported:12/02/03 17:03

Tentatively Identified Compounds by GC/MS EPA Method 8270Great Lakes Analytical—Buffalo Grove

Analytc ResultReporting

Limit Units Dilution Batch Prepared Anuljr*ud Method Note,

Tank 13 Spill (VV311185-01) Water Sampled: 11/19/03 13:30 Received: 11/19/03 14:40

1 ,2,4,3-Telrachlorobeny.ene3 ,3'-DiehlOTObcnzidincPentachlorobenzene

Surrogate: p-Tcrphcnyl-dl4Surragalt: 2. 4, 6-TrlbrvmophviolSurrogate; 2-FlvorobiphcnylSurrogate: tfitrobcuzcnc-dlSurrogate: Ph*nol-d6Surrogate: 2-Fhioropheaol

NDNDND

20.020.020.0

17.4%17.7 KIS.5%Jti.S%4.19%4.84%

us/1 1 3110424 11/1<

M M II

23-98to-isy31-8629-89IO-S3

10-124

)/Q3 1 1/2 A>3 EPA 8270C

«

II

m

H

L

LLLL

Great Lakes Analytical—Oak Creek The results In this report apply la tht samples analyzed in accordance with Ihv chsir.custody document. This analytical rtpn>t rnusl be reproduced In Us entirely.

Andrea Suihas, Project Manager Page 7 ol : -

1 2 / 0 2 / 2 0 0 3 TLÊ 17:04 [TX/RX NO 5084] © 0 0 9

12/02/2003 TUE 5:09 FAX 4145709461 Great Lakes Analytical 1^010/032



Email: [email protected] FAX (414) 570-9461

Luke States Industrial Service311 E. Greenfield Ave.Milwaukee Wl, 53204

Project: MSCG Prc Treatment ListProject Number, [none]Project Manager. Tom Jxcobson

Reported:12/02/03 17:03

General Chemistry - Quality ControlGreat Lakes Analytical—Buffalo Grove

AnulyteReporting


Source "JlECResult %R£C limili RPD

RPDLimit Notes

Batch 311049S - EPA 351 OC

Blmuk (3110495-BLK1)Oil SiCraac

LCS (311049S-BS1)Oil & Grease

LCS Pup (311049S-BSP1)Oil & Grease

Batch 3110S34 - General Prep WC

_frepared; 11/21/03 Analyzec:: 1/24/03

27.5

25.8

5.00 infi/1

___ Prepared: 11/21/03 Analyv-ed: .1/24/035.00 mg/l 30.0 91.7 C.6-123

Prepared: 11/21/03 Analyzed: ' :/24/03nuj/1 30.0 86.0 <LS-I23 6.385.00 52.4

Blank (3110534-BLK1)Cyunidc (tnul)

LCS (3110S34-BS1)

ND 0.0 100 nig/1Prepared &. Analyzed: 11/25^0:-

Prgnared & Analyzed:Cyanide (total)

* *r1v Spike (3110534-MS1)

0.504 0.0100 mu/1

Source: W3H185-01

0.480 105 iC

idc (total)

Matrix Spike Pup (3110534-MSD1)Cyanide (total)

O.S88 0.0250 mg/\Prepared & Analygcd: H/25;1^

120 0,0736 67.9 V

Source: VV31118S-U1 Prepm-ed & Analyzed: 1 \I25^;1.32 0.0250 me/\ 1.20 0.0736 104 Ii.2-174 39.1 11.2

Great Lakes Analytical—Oak Creek Tlit results In this report apply to the latrjiis analyzed in accordance with ll«.- chaincustody document. Hiii analytical rtpo"! mai be rtpmductd In Its enlirtly.

.idrca Stadias, Project Monager Page X of 2^

12/02/2003 TIT 17 : r , [TX/RX NO 5084] @]OH>

12/uz/zuu,} TUB a;ub FAA weai Lanes Analytical I f l U l i / U J Z


140 East Ryan RoadOak Cre«k, Wisconsin 53154


Lake Scales Industrm! Service311 E. Greenfield Ave.Milwaukee Wl, 53204


Project Manager. Tom JaeobsonReported;

12/02/03 17:03

Total Metals by EPA 200 Scries Methods - Quality ControlGreat Lakes Analytical—Buffalo Grove

Reportinc Spike Source %RHC RPDResult Limit Units Level Rsull %R£C Limits RfD Limit Notes

Batch 3110441 - EPA 3010A

Blank (3110441-BLK1)CopperLendNickelSilverZinc

LCS (3110441-BS1)CupperLeadNickelSilverZinc

Matrix Spike (3110441-MS1)Copper

1...ckclSilverZinc

Matrix Spike Dup (3110441-MSD1)CopperLead

NickelSilverZu:c

ND

ND

ND

ND

ND

3.970.0263

4.143.924.23

0,0500 rou/1

0.00500

O.OSOO

O.OSOO

0.500

o.osoo me/io.oosoo

O.OSOO

0.0500

0.500 "

Source: B31 1326-014,08

0.02933.96

ND

4.14

O.OSOO mg/1

0.00500

0.0500 "

O.U500

0.500

Source: B31 1326-0 14,09

0.02S5

4.01

ND

4.30

0.0500 mg/1

0.00500

0.05UO

O.OSQO

0.500

Prepared:

Prepared:4.00

0.02404.004,004.00

Prepared:4.00

0.02404.004.004.00

Prepared:4.00

0.02404.004.004,00

1 1/20/03

1 1/20/03

1 1/20/030.02280.00306

ND

ND

0.0260

11/20/030.0228

0.00306ND

ND

0.0260

Analyzed:

Analyzed:99 J2110

10493.0106

Analyzed:101109

99.0

103

11/26/03

1 1/26/0389.8-11571.7-14190-114

61.6-13688.8-117

1 1/26/0376.3-13617.2-176S2.2-I23

10-154 L76-135

Analyzai 11/26/03102

106

100

107

76.3-136 0.245 16.117.2-176 2.77 33.782.2-123 1.25 1<)10-154 60.h76-135 3.70 28.4

Great Lakes Analytical-Oak Creek The remit* In this report apply to the tamplts anatymd III accunlanc* wit/1 the cl'-i.r. : •'custody dncumtlril. 77//J analytical report must he reproduced in Its entirety.

.ndrea Scathas, Project Manager Page 9 of:9

12/02/2003 TUE 17:04 [TX/RX NO 5084] 0J 011

1 2 / u z / z u u j rut o ; u a MA tanes Analytical

UUOCHH GREATLAKESANALYTICAL



Lake States Industrial Service311 E. Greenfield Avc.Milwaukee WI, 53204

Project: MSCG PTC Treatment ListProject Number [none]Project Manager Tom Jacobson

Reported:12/02/0317:03

Total Metals by EPA 200 Series Methods - Quality ControlGreat Lakes Analytical—Buffalo Grove

AiialyteReporting


SourceResult %REC

V.RECLimits RPD

RPDLimit Nul»

Batch 3 11 0445 - EPA 7470 A

Blank (3II044S-BLK1)Mercury

LCS (3110445-BS1)Mercury

Matrix Spike (311044S-MS1)Mercury

Matrix Spike Pup (3110445-MSD1)Mercury

Batch 3120031 - EPA 3010A

ND 0.000200Prepared St. Analyzed: 1 1/20/03

mj/1

0.00159 0.000200Prepared & Analyzed: 1 1/20/03

mg/1 0.00150 106 76.6-124

0.00156Source: W311185-01

0.000200Prepared &. Amilyzcd: 11/20/03 _

mg/1 0.00150 ND 104 45.1-149

Source: W311185-010.00151 0.000200

Prepurcd & Analyzed: 11/20/03mg/l 0.00150 ND 101 45.1-149 3.26 22.8

Blank (3120031-BLXV)Cadmium

LCS (3120031-DS1)lium

Matrix Spike (3120031-MS1)Cadmium

Matrix Spike Pup (3120031-MSD1)Cadmium

NDPrepared: 12/01/03 Analyzed: 12/02/03

0.000500 nig/1

0.00207 0.000500 mg/1Prepared; 12/01/03 Analyzed: 12/02/03

0.00200 104 85-115

Source: B311462-01 Prepared: 12/01/03 Analysed: 12702/03mg/i 0.00200 O.OOOSS4 109 75-1250.00274 0.000500

Source: B311462-Q1 Prepared: 12/01/03 .Analyzed: 12/02/030.00275 0.000500 0.00200 0.000554 110 75-125 0.364 20

Great Lakes Analytical— Oak Creek The rfsutts In this report apply la the samples analyzed in accnrdanee with //';•_• chain •eiutody document. Th'u analyticalrrport must be rupruduftd in its entirely.

idrea Stathas, Project Manager Page 10 of 2?

1 2 / 0 2 / 2 0 0 3 TUE 17:04 [TX-'RX NO 5084] © O l J

HIE iwes




LaVc Suites Industrial Scrvtuc

311 E. Greenfield Avc.Milwaukee Wl, 53204

Project MSCCPre Treatment ListProject Number: [none]

Project Manager. Tom JacobsonReport ed:

12/02/03 17:03

Volatile Organic Compounds by EPA Method 624 - Quality ControlGreat Lakes Analytical—Buffalo Grove

Analyw

Batch 3110438 - EPA 5030B

BI«nkgllM38£LK12_Acrolem

Acrylonitrilc

Benzene

Bramndichlurame thane

BromoformBromomctbane

Corhott t«r»chioridc

CbJorobenzenc

Chlorudibroinaiiieth«n«

Chloruethanea-CllIorocthylvinyl etherChloroform

Chlovoinethftne

I "'-Dichlon'bcnzcncich lorobenzene

i ,t -Dichlorobenz«i«1 , l-Dichlorocthane

1 ,2-Diehloroethane

1 ,J -Dichloroelhcne

ci.s-1 ,2-DichlorocthencLran.i-1 j2-Dielilorc>cthene

1 ,2-DichIoropropanc

ci >- 1 ,3-DichloroprxipcneCT.iiis-1 ,3-Dichloropropenc

Ethylbenrcin:Mcttiylcne cllluridc

StyTCTlc

1 , 1 ,2.2-Tctiuchlorocttiaiie

Tctnchloroeihcnc

Toluene

1,1 .1 -Trichlorocthanc

1 , 1 ,2-Trichlorocth«iie

Tnchloroclhcne

Trich!orofluororncth«neV j n y l chloiide

Reauh

(P/T)

ND~~

ND

ND

NDND

ND

. NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Reporting Spike Source %REC RPDLimit Unit* Level Result %REC Limits RPD • Limit Notes

Prepared & Analyzed: 11/20/0350.0 u^l

50.0 «

5.00

5.005.00

10.0

5.00 "

5.00 "

5.00S.OO

100 "

5.00 "

10.0 "

5.00-

5.00

5.00 "

S.OO

5.00

S.OO

5.00

5.00

5,OO

5.00

5.00

S.OO

5.00 "

5.00

5. U(J

5.00

5.00

S.OO

5.00

5.00

5.00

5.01)

Great Lakes Ajvalytical—Oak Creek 77ir results in this report apply lt> the lamplis analyzed In accordance with Hie chaincustody document. Thin analytical report must be rrprvduetd In Its enllrvty.

rea Stathas, Projecc Manager Page 11 of 29

12/02/2003 TUB 17:04 [TX/RX NO 50841

12/02/2003 TUE 5:10 FAI 4145709461 Great Lakes Analytical 0014/032




Luke States Industrial Service311 E. Greenfield Ave.Milwaukee WI. 53204

Project; MSCG Pro Treatment ListProject Number, [none]

Project Manager Tom JacobsonRtported:

12/02/03 17:03


An.ilyieRqx>rting

Result Limit UnitsSpike Source V.REC RPDLevel Result V.REC Limits RPD Limit Notes

Bntch 3110438 - EPA 5030B (P/T)

Blank (311 (M38-BLK1)

Surrogatt: Dib'oinofluoromtthan*Surrogate; 1. 2-Dichtora*than*-d4

Surrogate: Tolutrtt-dSSurrogau: 4-SroinqftuorotHlntcnt

LCStm0438-BSl)Benzene

Broiruxlichlorumcthiinc

Bromoform

Brcmoru ethane

Curbon tetmchloridc

Chlorobcnzcne

Chloraclibtumomcthume

Clilorocthaue

lorocthylvinyl elher

jrofnrm

Chloromclhiine

1 ,2-DicUorobouCTie

1 ,3-Dichlorebenzene

1 ,4-Dichlornbcn7.cnc

1 . 1 -Dichlorocthmic

1 ,2-DicMoroclhane

1 , 1 -Dichlorocthcnc

c i> - l .2-Dichloroclhenc

trani-1 !-Dich]oro«licnc

1 .2-Dichloropropano

cis-U-Dkhlompropcnc

trans- 1 .3-DichIorppropcnc

Etliylbeaier.r

Mctliylciie chloride

Sryrcnc

1 . 1 ,2 ,2-Torachloroctbaiie

Telrjchlnmclhcnc

Toluene

1,1,1 -Trii:hloroeihflnc

1 . 1 ,2-Trichloroclhjne

34.943.8

51. V

SI. 7

41.0

40.0

44.8

41.0

42,4

45.4

47.1

S4.6

ND

41.9

37.7

48.h

50.3

43.9

41.3

38.6

40.1

42. A

43. S

40.4

38.0

30.5

47.2

43.7

45.7

43.3

50.5

41.7

42.1

3S.8

UK/IH

"

"

5.00 ug/l

5.00

5.00

10.0

5.00

5.00

5.00

5.00

100

5.00

10.0

5.00

5.00

5.00 "

5.00

5.00

5.00

S.OO

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

Prepared & Analyzed:

30.0

.10.0

50.030.0

Prepared & Analyzed;50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

SO.O

50.0

50.0

SO.O

SO.O

50.0

SO.O

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

11/20/03

1IU 75.8-127

87.6 K2.S-I4SHJA 76.6-130103 68.9-123

H/20/0382,0 61.3-142SO.O G5.9-I6289.6 30.2-170

82.0 33.X-1C1

84.8 40J-I64

90.8 79.9-132

94.2 54-159

109 37.1-163

80-120 L

83.S 78.6-132

75.4 34.3-158

97.2 78.6-139

101 79.1-136

87.8 7S.2-129

82.G 58.2-134

77.2 73-136

S0.2 58-136

85.2 76,3-135

87.6 53. 3-137

80.8 65.9-147

76.0 61-165

73.0 59.4-166

94.4 78.4-130

87.4 52.2-142

91.4 69.2-144

S6.6 40.3-164

101 44.9-165

83.4 77.4-131

K4.2 66.6-143

77.6 74.8-147

Great Lakes Analytical—Oak Creek Tlie rrsulti in tHlt report apply In the samples onatyztd in accordance *iilh th* ehacustody document. This analytical report must Ixt reproduced in Its entirely.

ndrea Stathas, Project Manager Page 12

12/02/2003 TCE 1 7 : 0 4 [TX/Ri NO 5084]

12/02/2003 TUE 5:10 FAX 4145709461 Great Lakes Analytical 10015/032




Lake Stutc* Industrial Service

311 E. Greenfield Ave.Milwaukee WI, S3204


Project Manager: Tom JacobsonReported:

12/02/03 17:03


AnnlytcReporting

Result Limit UnitsSpike SourceLevel Result V.REC

•/.REC RPDLuuils RPD Limit Notes

Batch 3110438 - EPA 5030B (P/T)LCS (3110438-BS1)TrichloroetheneTrichlorofluoromelhune

Vinyl chloride

Surrogate: DlbromofluoromethantSurrogate: l,2-Dichloroethane*d4Surrogate: Tolutnt-dSSurrogate: l-Iironiofluorobtinztnt

Matrix Spike (3110438-MSI)Benzene

BromoJichlaromctrianc

Bramoform6 romometrume

Ciirbon tctrachloridebenzene

( .fodibromomethonc

Chloractlune2-CMoro«hylvinyl elherChloroformClUoromelhanc

1 .2-Dichlonibcnzcne

1 , 3 -Dichlofobenzcnc

1 ,4-Dichlorob«:n£cnc

1,1 -Dichloroctliane1 ,2-Dichlomcthanc1 . 1 -Dic:hlorocthcnc

cii- 1 ,2-D'^hlim)cthcnc

MTHis- 1 ,2-Dichlorocthcnc1 ,2-Dichloropropoiic

i:ii- 1 ,3-Dichloropropene

irnn*- 1 ,3-DichlorepropcueEihyftcnicnc

Mclhylcne uhloricfc

Scyrvutr

1 ,1,2,2-TctracKloroellianc

Tclrjchlorocthcnc

47.347.741.9

49.934.84»,448.7

Source:96.9

47.0

52.2

41.S

51.1

52.4

52.4

54.1

ND

48.5

40.0

51. S

50.9

45.0

49.6

46,6

47.6

49.8

50.7

40.9

44.9

4S.O

5S.G

56.7

56.0

51.0

5S.4

5.00 ufi/1

5.00

5.00

"••

"H

W311185-OT

S.OO lie/'

5.00

5.00

10.0

S.OO

S.OO

5.00

S.OO

100

S.OO

10.0

5.00

5.UO

S.OO

S.OO

5.00

5.00

5.00

5.00

5.00

5.00

S.OO

5.00

5.00

5.00

S.OO

S.OO

Prepared & Analyzed:50.050.050.0

50.050.0so.a50.0

Prepared & Analysed:50.0

50.0

50.0

50.0 ND

50.0

50.0

50.0

50.0

SO.O

SO.O

50.0 ND

50.0

SO.U

SO.O

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

SO.O

SO.O

11/20/0394.695.483.8

99. 869.6V6.S97.4

46.7-16936-164

51.5-146

D.IS-12762.5-14576.6-1M68.9-12}

1 1/20/03194

94.0

104

83.0

102

105

105

108

97.0

80.0

103

102

VO.O

99.2

93.2

95.2

99.6

101

19.S

89.8

90.0

117

113

112

101

I I I

39.3-16S H

39.8-18&28.1-16')

33.2-164

10-181

56.1-15049-157

36.1-16S

80-120 1.

67.5-142

23.5-167

68.3-135

62.8-13062.1-130

46.7-142

60.6-151

38.7-l«249.2-15548-137

44.6-171

28.6-195

40.6-1 7656.1-144

41.9-15431.1-169

43.9-156

29.1-160

Great Lakes Analytical—Ook Creek TItt: ri'sula In this report apply ta the samples unotystd in accordane* with the chain icustody document, Thli analytical report must be reproduced In Its entirety.

.drea Statbas, Project Manager Page 13 ol'2S

12/02/2003 TUE 17:04 [TX/RX NO 5084]

12/02/2003 TUE 5:11 FAX 4145709461 Great Lakes Analytical P16/032




Lake States Industrial Service3 1 1 E. Greenfield Ave.Milwaukee Wl, 53204

Project: MSCG Pre Treatment ListProject Number (none]


12/02/03 17:03

Volatile Organic Compounds by EPA Method 624 - Quality ControlGreat Lakes Analytical— Buffalo Grove

ReportingAnalyse Result Limit

SpikeUniu Level

SourceResult %REC

%RECLimits RPD

RPDUmit Notes

Batch 3110438 - EPA S030B (P/T>

Matrix Spike (3110438-MS1)Toluene

I . I . I -Trichloroetkme

1 , 1 ,2-Trichlorocthane

Trichlorocthcnc

Trichlorofluoromcthlnc

Vjnyl chloride

Surrogate,' DlbromoJJuoroni*than«

Surrogate: I.2-Dichloro«thanc-d4Surrogate: Toluene-daSurrogate: 4-Bromafluarob«n2e>i*

Matrix Spike Dup (31I0438-MSD1)Benzene

Bromodieh!orom«h»nc

•jform

jomelhanc

Carbon tctrcchloride

Ch.lcirobcn7.cnc

Chlurudibrornomctlianc

Cliloroethanc

2-ChlorewlhyIvinyl ether

Chloroform

Chloromcthaiie

1 ,2-Dichlnrobcnzcne

1 ,3-Dichlorobcti7.cnc

1 ,4 -DichJopabcnicnc

1 . 1 -DichJoraelhunc

1 ,2-Dichloroelhanc

1 , 1 -Dichloroslliene

ci»-l ,2-Dichlorocthcne

(ranj- 1 ,2-Dich!orocthcnc

1 ,2-DichJoropropane

cis-1 ,3-DichJoropropene

tran<-l ,3-Dicllloroptopene

Elhylhcnrcnc

Mcthylcne chloride

Great Lakts Analytical— Oak Creek

Source:90. S

49.5

46.0

55.346.7

43.1

SO. I38.4

SO.O

S2.2

Source:91.0

46. 5

52.8

41.2

48.8

50.3

52.4

4'J.S

ND

47.5

38.0

51.7

4<J.7

44.3

48.9

47.3

47.1

49.2

49.S

47.5

44.6

44.4

57.0

55.4

W31118S-01 Prepared5.00

5.00

5.00

S.W5.00

5.00

ug/1 SO.O

50.0

SO.O

SO.O

50.0

50.0

" SD.O

SO.O

SO.O

" 511.0

W31118S-OI Prepared5.00

5. TO

5.00

10.0

5.00

5.00

5.00

5.00

100

5.00

10.0

5.00

s.oy5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

UE/1 50.0

SO.O

SO.O

50.0

" 50.0

50.0

50.0

SO.O

50.0

50.011 50.0

50.0

50.0

50.0

50.0

50.0

" 50.0

50.0

50.0

50.0

50.0

50.0

50.0

- 50.0

& Analyzed: 1 1/20/03

182

99.092.0

111

93.4

86.2

100

76.8100IIH

J6.2-1S2

42.2-152

69.5-15S

13.5-180

12-173

21.5-165

7S.&-127

62.5- Its76.6-1 3063.9-123

H

A Analyzed: 1 1 /20/031S2

93.0106

ND 82.4

97.6

101105

99.0

95.0

ND 76.0

11)3

99.4

S8.6

97.8

94.6

91.2

98.4

99.6

95.0

89.2

8S.8

114

111

39.3-16S

39.8-136

28.1-169

33.2-164

10-181

56.1-150

49-157

36.1-168

80-120

67.5-142

23.5-1S7

6S. 3-135

62.S-136

62.1-130

4(5.7-142

60.6-151

38.7-142

49.2-1SS

43-137

44.6-171

23.6-195

40.6-176

56.1-144

41.9-154

6.281.071.14

0.726

4.604.09

0.00

8.88

2.08

5.13

0.3SS

2.39

1.57

1.421.49

1.061.21

1.79

4.930.670

1.34

2.77

2.32

38.2 H

34.2

35,5 •

33.8

37.5

17.5

294«

20 L

17.5

33.8

14.8

15.7

15.219.9

16.V

23.5

18.6

20.1

32.4

43.6

39

24

23.8

Hie ffjults In thii report apply to the samples analyzed in accordance with the cha:>'. r

.idrea Stathas, Project Manager Page 14 of 29

12 /02 /2003 TUE 17 :04 [TX-'RX NO 5084]

12/02/2003 TUB 5:11 FAX 4145709461 Great Lakes Analytical IP17/032





31 1 E. Greenfield Avo.

Milwaukee Wl, 53204

Project; MSCC Pre Treatment List

Project Number: [none]

Project Manager: Tom JacobsoaReported:

12/02/03 17:03


Anslyte ResultReporting

Limit UnilsSpiVcLevel

SourceResult %REC

V.RECLimits RPD

RPDLimit Note*

Batch 3110438 - EPA S030B (P/T)

Matrix Spike Pup (3110438-MSD1)Slyrcne

1.1,2,2-Trtnchlorocthune

Tctrachtoroethene

Toluene

1.1.1 -TricKloroctlianc

1.1 .2-Trichlorocthanc

Trichloroelhen*

Trichlorofluoro methane

Vinyl chloride

54.3

51.4

53.2

84.1

4X.7

46.7

S3 2

46.3

41.4

Source: W311185-01ug/15.00

5.00

5.00

5.00

5.00

3.00

5.00

S.OO

5,00

Prepared & Analyzed: 11/20/03

50.0 " 109 31.1-llW 3.08

50.0 103 43.9-186 0.781

50.0 106 29.1-160 4.05

50.0 168 50.2-152 7.66

50.0 97.4 42.2-152 1.63

SO.O 93.4 69.5-155 1.51

50.0 106 13.5-1 SO 3.87

50.0 92.6 12-173 0.860

50.0 82.K 21.5-165 4.02

Surrogate: Dihrnma/IuoromclhancSurrogate: l,2-Dichlarurlhant-d^Surrogate: Tolutne-dSSurrufate: 4-Bromofluorobiinzeni:

4V.O42.S51.4

52.2

SO.O

so.nSO.O

SO.O

98.0

83.6103104

7 S.S-1 37

62.S-14S

46.4

33.3

32.3

28.6

20.1

29.2

34.1

39.754.1

H

68.V-123

Great Lakes Analytical—Oak Creek

fiThe resullj In thLi report apply la the xampltj analyzed In accordane* with the chaincustody document. Tl\lx analytical rtpnri must be reproduced in iLi tntircty.

4^TZfc&^=

drea Stathas, Project Manager Page 15 of

12/02/2003 TUE 17:04 [TX/RX NO 5084] ©01"

12/02/2003 TUE 5:11 FAI 4145709461 Great Lakes Analytical 1^)018/032




Lake Stntcj Industrial Service311 E. Greenfield AvtMilwaukee Wl, 53704

Project: MSCO Pre Treatment ListProject Number: [none]

Project Manager Tom JacobsoaR«por(c<l:

12/02/03 17:03

Organochlorinc Pesticides and FCBs by EPA Method 608 - Quality ControlGreat Lakes Analytical—Buffalo Grove

Annlytc ResultRcyxming Spike Source */.R£C RTD

Limit Unis Level Result %REC Limits RPD Limit Noics

Batch 3110462 - EPA 3510C

Blank (3110462-BLK1)Aldrinolpha-BHC

bctu-BHCdelUl-BHC

gamiua-BHC (LJndsrvc)Chloixlane (tech)

4,4'-DDD4,4'-DDE

4.4 '-DDT

Diel<lrin

Endosulfan 1

Endosulfon IICndojulfxu sulfale

'i

.1 aldehydeHcptichlorHeptachlor epoxidc

Toxijphcnc

PCB-I01«

PCB-1121

PCB-1232PCB-1242

PCB-124S

PCB-1254

PCB-1260

Surrogate: Terracttloro-mcto-xylenfSurrogate: nfc.nchlorobiphtnyl

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

NO

ND

ND

ND

ND

NDND

1.23O.J64

PreporeJ; 11/20/03 Analyzed: 12/01/030.0300 ug/10.0200

0.0300 "

0.0300 "0.0300

0.2<l()

0.0400

0.0300 "

0.160

0.0300 "0.0300

O.OSOO

0.100

0,100

0.1 SO

0.0400

0.0200

0.500O.SOO

0.5000.500

O.SOO

O.SOO

O.SOO

0.500

1.00 121 1U-1IO H1.00 3f>.1 10-140


,drea Stathas, Project Manager

The rvsults in this report apply to the samples analyzed In avcorjance with the chain "/custody tlccunierit. This analytical rcporl must he reproduced in I'M entirety.

Page 16 of 25

12/02/2003 TUE 17:04 [TX/RX NO 5084]

12/02/2003 TUE 5:11 FAI 4145709461 Great Lakes Analytical



Email: [email protected];414) 570-9460 FAX (414) 570-9461


3 1 1 E. Greenfield Ave.Milwaukee WT, 53204

Organochlorine

An^,e

Project: MSCG Pre Treatment List

Project Number: [none]Project Manager: Tom Jicobfion

RtporUd:12/02/03 17:03

Pesticides and PCBs by EPA Method 608 - Quality ControlGreat

Result

Lakes Analytical— Buffalo Grove

ReportingLimit

Spike SourceUnits Level Result %R5C

V.REC RPDLimits RPD Limit Notes

Batch 31 1 0462 - EPA 3S10C

LCS (3110462-BS1)Aldrin

iilpha-BHC

bcta-BHC

dclca-BHC

gumms-BHC (Llndane)

4,4'-DDD

4,4'-DDE

4.4'-DDT

Dicldrin

Enclosulfan 1

Endosulfun 11

Eadosul£in aulfatc

EndrinJu nldchyde

.chlor

Heptuchlor cpoxidc

Surrogate: Tetrachlnra-nitta-xylcncSurrogate: De.caehtoroblphenyl

LCS (3110462-BS2)PCD-1016

PCB-I260

Surrogate: Teirachloro-meta-xylcnt!.

Surrogate: Uecachloroblphiinyl

LCS Dup (3110462-BSD1)Aldrin

jlpha-BHC

b«ta-BHC

dclu-BHC

gammn-BHC (Lindane)

4.4--DDD

4.4'-DDE

4,4 -DDT

Dieldrin

Endosulfrn I

Great Lakes Analytical— Oak Creek

0.292

0.185

0.243

0.515

0.141

0.296

0.208

0.260

0.296

0.238

0.228

OJ277

0.230

0.250

0.190

0.287

0.7370.454

U.0300

0.0200

0.0300

0.0300

0.0300

0.0400

0.0300

0.160

0.0300

U.0300

0.0500

0.100

0.100

0.150

0.0400

0.0200

Prepared: 1 1 /20/03 Analyze!:ug/1 0.300 97.5

0.300 61.7

0.300 81.0

" 0.300 172

" 0.300 47.0

" 0.300 9S.7

0,300 69.3

0.300 86.7

0.300 58. 7

" 0.300 7?j

0.300 7&.S

0.300 92.3

0.300 76.7

0.300 83.3

0 JOO 63 j0.300 95.7

1. 00 73.71.00 *}.*

11/25/0324.4-121

25.7-118

28.2-124

26.6-117 H

26.4-120

29.9-154

22-129

10-168

44.4-12S

27.7-126

44-126

45-125

34.3-156

37-12S

32,1-122

25.7-134

10-11010-140

Prepared: 11/20/03 Analyze:: 12/01/034.443.77

0.I5JV0. 1 7.5

0.320

0.206

0.279

0.646

0.192

0.381

0.255

0.327

0.364

0.283

=CD

0.500

0.500

0,0300

0.0200

0.0300

0.0300

0.0300

0.0400

0.0300

0.160

0.0300

0.0300

ug/\ 5.00 8S.S

5.00 75.4

1.00 61.*

1.00 /-..'

Prepared: 1 1/20/03 Analy«=UB/I 0.300 i:~

0.300 t5.~

" ' 0.300 93 ^

0.300 :15

0.300 6-i.O

D.300 i;~0.300 sf.:OJOO 1C«

0.300 121

0.300 9<ij:-

77io n'julu In r/iii report apply lu tat .tjcustody document. This analytical /-rr»r>-

21.8-110

22-113

Ill-Ill)

10-140

: 1 1/25/0324.4-121 9.15 67.6

25.7-118 10.7 66.4

28.2-124 13.8 57.1

2(>.6-117 22.6 54.5 H

26.4-120 30.6 61.5

29.9-154 25.1 84.4

22-129 20.3 81.3

10-168 22. R 83.5

44,4-128 20.6 63.8

27.7-120 17.3 76.1

mplei analyz&t in accordance with the c/i"in <*-. must be reproduced in la entirety.

ndrea Stathas, Project Manager Page 17 of 29

12/02/2003 TIT I" •:-} [TX/RX NO 5084]

12 /U2 /2UU3 THE b:iz Ml 4145709461 Great Lakes Analytical 14)020/032




Lake States Industrial Service311 E. Greenfield Ave.Milwaukee Wl, 53204



12/02/03 17:03

Organochlorine Pesticides and PCBs by EPA Method 608 - Quality ControlGreat Lftkes Analytical—Buffalo Grove

AnMyte

Batch 3110462 - EPA 3510C

LCS Dup (3110462-BSD1)Endutiulfan IIEiidosuifon lulfaic

EndrinEndrin aldehydeHcpUchlorHeptnchtor cpoxide

Surrugatf.: Tetfachloro-m«ta-xyltntSurrogate: Dvcaehlorobiphtnyl

LCS Dup (3110462-BSD2)PCB-1016PCB-1260

Surrogate: Tatrachluro-meta-xyli:ntSurrogate; DtieucJilorablphtnyl

Result

0.297OJS40.3050.315

0.2300.337

0.7400.672

4.32

3.14

0.5400.149

ReportingLimit Units

0.0500 ug/10.100

0.100

0.150 "

0.0400 "0.0200 "

H

It

0.500 us/I0.500

it»

SpikeLevel

Prepared:0.300OJOO0.3000.3000.3000.300

1.001.00

Prepared:5.005.00

1.001.00

SourceResult V.REC

11/20/03 Analyxed:99.011810210576.7112

74.067.2

11/20/03 Analyzed:86.4

(S2.S

S4.014.9

%RECLimits

J 1/25/0344-12645-125

34.3-IS637-128

32,1-12225.7-134

ln-no10-140

12/OJ/0321.8-11022-113

10-11010-140

RPD

26.3

24.4

28.0

23.0

19.0

16.0

2.74

18.2

RPDLimit

63.9

56.6

53.3

77.8

50.3

63.5

71

86.3

Notes |

Great Lakes Analytical-Oak Creek Tlit results In Ihis report apply to the samples analyzed in accordant* viitli Ihv ehair. ofcustody document. This analytical tvport must be reproduced in Its entirety.

drea Stadias, Project Manager Page 18 of 29

1 2 / 0 2 / 2 0 0 3 Tt'E 17 :04 [TX-'RX NO 5084] ® 0 2 ' i


••:,---.'-.n--i ••

3»*S3M^Jil




Uike States Industrial Service

311 E. Greenfield Ave.Milwaukee Wl, S3204

Project: MSCG Pre Treatment ListProject Number, [none]

Project Manager. Tom JucobsonReported:

12/02/03 17:03

Base/Neutrals and Acids by EPA Method 625 - Quality ControlGreat Lakes Analytical—Buffalo Grove

AnalyteReporting Splice Source V.REC RPD

Rault Uinit Unit* Level Result VoREC Limits RPD Limit Notts

Batch 3110424 - EPA 3510C

Blank (31 10424-BLK1)Acenuphthcne

Accnnphthylenc

Anthracene

Bcn7.idinc

Bcnz (u) anthracene

Dcnzo (a) pyrcnc

Beozo (b) fluuranthcne

Bcnzo (glii) peiylene

Ben 70 (k) ttuorauthaie

Bi.s(2-chlorocthoxy)m«thaixe

Eis(2-chlorocthyl)etha-

Bi3(2-chloroisopropyl)«hcr

Bi5(2-cthylhcxyl)phlhalatc

T phcnyl phcnyl ether

L Benzyl phth*latc

4-Chloru-3-methyrphenol

?.-Chloro naphthalene

2-Chlorophcnol

4-Chlorophcnyl pheuyl ellier

Chrysenc

Diboxt (u.h) unthmccnc

1 .1-Dichloroboiztaic

1 ,.^-Dichlorobenzeue

l ,4-Dichlorobcnzeiie

j,3 '-Dichlorobcnzidine

2.4-Dichlarophcnol

Di fUiy l phlhubte

2,4-DiinediyIphenol

Dimctliyl phthalate

Di-n-buryl phihalate

•»,ft-DiniTn-2-mcthylphenol

2,4-Dinicrr)phenol

2s4-Duutrolo!ucnc

2,&-Dinitrololuene

Di-n-octyl phthalate

ND

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Prepared: 11/19/03 Analysed: 11/21/0310.0 up/1

10.0 "

10.0

50.0

10.0

10.0

10.0

•w l

10.0

10.0

10.0

10.0

10.0

iy.o10.0

10.0

10.0

10.0 "

10.0

1U.O

10.0

10.0

10.0

10.0 "

20.010.0

10.0

10.0

10.0

10.0 "

50.050.0

10.0

10.0

10.0

Great Lakes Analytical—Oak Creek The i-e.tults In this rrpari apply to the samples analyzed In accordance wllfi the cli'iindocument. Thii analytical report must bv reproduced in its entirely.

.;a Stathns. Project Manager Page

12-'02' '2003 17:04 [TX/RX NO 5084]

12/02/2003 TUE 5:12 FAX 4145709461 Great Lakes Analytical @ 0 2 2 / 0 3 2




Lake States Industrial Service311 E. Greenfield AvO.MilwaukeeWT. 53204



12/02/03 17:03


AnalyleReporting Spike Source V.REC RPD

Result Limit Units Level Result %REC Limits RPD Limit Koira

Batch 3110424 - EPA 3510C

Blunk (31tO*2.i-BLKl)Flucnmthenc

Fluormc

HtxacUorobouen e

Hcxachlorobutadiene

Hcxttchlnracyelopcntftdiene

Hcxuchlorocthine

ludeno (1 ,2,3-cJ) pyrcne

Isaphorone '

Naphthalene

Nitrobenzene

2-Nitruphoiol

4-Nitrophenol

N-Nitrosodimethylaraine

Ttisadi-n-propylaiiune

-roiodiphcnyl»mlnc

FenUchloraptunol

Phcoanthicue

Phenol

Pyrcne

1 ,2,4-Trichlnrobcn3;cnc

2,4,6-TrichloTophenol

Sitrrcjgutt:: 2-Fluornphe.nol

Surrogate: Ph^.nol'<i6Surrogate; NttrobemrnT~tlSSurrogate: 2-FluorobiphenylSurrogate: 2,4.fl-'rrlhrotnophcnolSurrogate: p-Tcrphcnyl-J 14

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

ND

ND

ND

9.16

5.4X

17.4

IC.S32.3

17.4

Prepared: 11/19/03 Analyzed; 11/21/0310.0 ug/l

10.0

10.0

10.0

20.0

10.0 "

10.0

10.0

10.1)

10.0

10.0 "

50.0 "

10.0

10.0

10.0

50.0

10.0

10.0

10.0

10.0

10.0

ns 7.33 10-110 LUS 4.3S 10-110 L62.S 27.8 31.4-1K) L62.5 26.4 10-111}

" !25 lfi.0 10-11062.5 27. S 10-147

Great Lakes Analytical—Oak Creek TTir rcxulu in ihii report apply to III* samples analyzed in accordance with the chicustody document This analytical rtfnrl must t>f reproduced in its entirety.

jdrca Stathas, Project Manager Page 20 of2;

12/02/2003 TUE 17:04 [TX/RX NO 5084] ®022

12/02/201)3 TUK 5:13 FAX 4145709461 Great Lakes Analytical 10023/032





311 E. Greenfield Awe., 53204

Project: MSCG Pre Treatment ListProject Number (none]

Project Manager: Tom JucobjonReported:

12/02/0317:03


AnulytcReporting

Result Limil UnicsSpike SourceLevel RejulL %REC

%REC RPDLimits RPD Limit Notes

Batch 3110424 - EPA 3510C

LCS(3tl0424-BSl)AccnnphthcneAcenaphthylene

AnthraceneBcnzidiiwBcn7 (a) anthracene

Bcnzo (») pyrcnc

Bcnzo (b) flunranthcnc

Benzo (fihi) perylcncBcnzo 00 fluonmUieoe

Bi.i(2-chloroctho*y)melnaneBis(2-ch loro ethyl Jcthcr

Bis(2-ch lonjisopropyl)ethCT

B is(2-elliylliexy\)phlhiiliitEimopkenyl plienyl eiher

bciiTyl plithal.Me

4-Chloro-3-mcthylphcnol

2 -Chloronaphthalcne

2-Chlorophenol

•4-Chlorophenyl phenyl etherChryscnc

Dibcnz (a,h) onthnccnc

1 J-Dichlorobcnzene

1 ,3-Diclilorobeoiene

1 ,4-Diclilorob*nêne

3,?'-DichIorobeniidine"Z ,4-Dichloroplicnol

Diclhyl phthiiloxc

2.4-Dimclhylphcnol

Dimetliyl phlhilatc

Di-n-butyl phlhulutc

-4 ,r,-Dinitro-2-uielhylphi3iol

2,4-Dintrrophcnol

2,4-Dinitrowlucne

2.6-Dinilrotolucne

Di-l)-oc[jl phlbalate

Prepared; 11/19/03 Analyzed: 11/21/0316.817.120.6

8.71 .24.ft

27.9

24.220.128.28.40

1.370.770

24.219.424.f,

15.5

13.4

ND

17.6

23.3

21.4

ND

ND

ND

25.60.07

2J.O

8.07

20.6

24.3

22.0

11.320.8

19.8

22.S

tO.O ug/1

10.0

10.0S.CXJ

10.0

10.0

10.0 "

10.0

10.01.00

1.00 "

0.100

10.0

10,010.0 "

10.0

10.0

10.0

10.010.0

10.0

10.0 "

10.0

10.0

20.0

1 .00

10.0

1.00

10.0

10.0

5.00

5.00

10.0

10.0

10.0

2S.O

25.0

2S.O

2S.O

2J,0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25. 0

25.0

25.0

25-025.0

25.0

25.0

25.0

25.0

2*£

25.0

25.0

25.025.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

67JZ

63.4

S2.4

34.8

98.4

112

96.8

80.4

113

33.6

5.4X

3.08

96.8

77.6

98.4

62.0

53.6

70.4

93.2

85.6

102

36.3!J2.0

32.382.4

97.2

88.0

45.2

83.2W2.

91.2

10-11413.6-114

14.7-11570-130

20.5-124

17.2-121

13.6-13610-164

13.2-128

14.4-11211.5-110

10-11310-159

14.6-1 IK '

10-164

10.8-11310-110

U.4-110

12.6-11710-110

10-148IU-11U

10-110

10-110lo-no

10.2-112

16.2-121

10-110

1X-122

1(1-120

10-129

10-123

12.5-126

14.3-127

lft-122

L

L

L

L

LL

Great Lakes Analytical—Oak Creek 'flit rttulu In this report apply to the samples analyzed In accordance wjV/i the ch'i'.r.custody document. This analytical report must be rvprvductd In lu entirety.

idrca StatKos, Project Manager Page 2 I of" :9

12/02/2003 TL'E 17:04 [TX/RX NO 5084] 12) 0 J.i

HIE a: la FAA 4 i 4 b Y U S 4 b i Great Lakes Analytical ,4024/032


140 East Ryan Road -Oak Creek, Wisconsin 53154



3U E. Greenfield Avc.

Milwaukee WI, 53204

Project MSCO Pre Treatment ListProject Number, [none}

Project Manager Tom Jacob-sortRcporttd:

12/02/03 17:03


Analyte ResultReporting

Limit UnitsSpiku SourcaLevel Result J4REC

V.RECLimit! RPD

RPDLimit Notes

Botch 3110424 - EPA 3510C

LCS (3110424-BS1)Fluorantheiie

Fluorcnc

Hexuch1arohcn7enc

HMJuhlorubutadienc

Hexachlorooyulopcntadicnc

Hexacliloroelhanc

Inclcno (1 ,2,3-cd) pyrene

LsJiphoronc

Nuphthulcnc

Nitrobenzene

2-Nitrpphcnol

4-NicrDphcnol

N-Nitn>Kodimcthylaminc

Niuosodi-n-propyl»minc

iLrosodiphcnylummc

Pcntachlorophenol

Phcnnnthrcnc

Phenol

Pyrene

1 ,2 ,4-Trichlorubcnzaie

2,4,f>-Tric>>laroph<niol

Surrogate: 2-f'luomphenol

Surrogate: rhrnul-d6Surrasate: Nitrohenzcnc-dS

Surrogate: 2'FluorobiphcnylSurrogate: 2, 4, 6-Tribromophcn0tSurrosaCf: p-Terphenyl-d J 4

19.7

19.2

20.0

0.810

3.79

ND

21.5

13.4

4JS

3.84

5.27

«.A1

ND

9.75

21.5

20.2

21.4

O.fiOO

22.4

2.76

K..O

fl.UO0.790

3.43

13.23S.122.1

1 0.0 ug/1

10.0 "

10.0

0.100 "

2.00

10.0

10.0

10.0 "

1 .00 "

1.00

1.00

5.00

10.0 "

1.00 "

10.0

5.00

10.0

0.100

10.0 "

1.00

i o.o""It

fl

"

"

Prepared: 11/19/0325.025.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.025.0

25.0

25.0

25.0

25.0

25.025.0

25.0

25.0

125

12562.1

63.3125fi 2. 3

Analyzed:7K.K

76.880.03.24

15.2

8<i.O

53.6

17.4

15.4

21.1

26.4

39.0

86.0

80.8

85.6

2.40

89.6

11.0

64.0

0.6325.49

21.1

28.135.4

1 1/21/031G.1-118

13.4-115

12.6-1 1&

10-110

10-110

10-110

10-155

11.5-110

10-110

11.1-112

10-114

10-110

70-130

11J-113

15.4-110

10-123

16.9-116

10-110

1IM73

10-UU

10-130

10-11010-110

31.4. I/O10-11010-1 in10-147

L

L

L

L

LLL


(j/M?ii#?jndrea Stathas, Project Manager

The results in this rrport apply to the samples analyzed in accartianc* with tlm chain c'custody document. This analytical report must frt- nprotluctd in Its entire!?.

Page 22 of 29

12/02/2003 TUE 17:04 [TX/RX NO 5084] CS 0 2 -t

12/02/2003 TDK 5:13 FAX 4145709461 Great Lakes Analytical 10025/032

WJt C23»J ^^H

^1LAKESANALYTICAL



LaVc States Industrial Service311 E. Greenfield Avc.Milwaukee Wl, 53204

Project MSCO Prc Treatment ListProject Number [none]


12/02/03 17:03

Base/Neutrals and Acids by EPA Method 625 - Quality ControlGreat Lakes Analytical— Buffalo Grove

Ajialyte ResultReportinc

LimitSpike Source

Unitx Level Result «/.RECV.REC RPDLimits RPD Limit Notes

Batch 3110424 - EPA 3510C

Matrix Spike (31I0424-MS1)Avauiphthene

Acenaphthytene

Anthracene

Bcnzidinc

Bcii7. (») anthracene

Bcnzo (a) pyrcnc

Beiua (b) fluonknthcno

Bcnzo (glii) pmylene

Bciizo (k) ttuoranthene

Bi.i(2-ch1orocthoxy)mcthanc

B is(2-chloroethyl)etncr

Bii(2-chloToi*upropyl)cthcr

Bis(2-ethylhe.\yl)phlhahilc

oinopheuyl phenyl eiher

benzyl phthalalc

4-ChIoro-3-methylphcnol

2 -Chloronaphlhalene

2-Chloropheuol

4-CMorophcn.y] phenyl ether

Chryscnc

Dibenz (u.h) unthracenc

L,2-Diehlotobenzene

1 ,3 •Dichlorobenzene

1 .4-Diclilorob<aizra«:

3 ,3 '-Diclilarobciizidine

2,4-Dichlnrophcnpl

Diclhyl phthulute

2.4-Dimethy Iphcnul

Dimethyl phihQlaie

Di-ii-butyl phLhalatc

4,6-Dinitrri-2-rncthylphaiol

2.4-DinitTTjphcnoI

1.4-Dinitn.lolucnc

2.6-D\nilrotulucnc

Di-ii-octyl phlhalutc


1 \ ^ C^ -J-UMsÛ^? ^ytifiH**.

Source: B3 11229-04 Prepared: 11/19/03 Analy2ed-.il/22/0310.320.1

22.1

4.14

21.8

23.8

21.9

12.3

25.S

19.1

IK.O

21. n

22.4

20.4

25.6

17.6

17.9

12.S

18.8

20.9

16.3

15.1

14.1

14.S

18.3

15,1

23.9

11.6

20.9

24.4

22.6

19.2

21 .S

20.7

21.4

10.0

10.0

10.0

0.500

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.010.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

2.00

10.U

10.0

10.0

10.0

10.0

5.00

5.00

10.0

10.0

10.0

us/1 25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

" 25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

2S.O

25.0

25.0

2S.O

25.011 25.0

ND

ND

NDNDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

77.2

K0.4

gS.4

16.6

87.2

95.2

87.6

49.2

102

76.4

72.0

86.4

89.6

SI. 6

102

70.4

71.6

50.0

75.2

83.6

65.2

60.4.

56.4

5S.2

73.2

60.4

95.6

46.4

83. G

97.fi

90.4

76. S

86.0

82.8

N5.6

70-130

70-130

70-130

70-130 L

70-130

70-130

70-130

70-130 L

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130 ' L

70-130

70-130

70-130 L

70-130 L

70-130 L

70-130 L

70-130

70-130 L

70-130

70-130 L

70-130

70-130

70-130

70-130

70-130

70-130

70-130

The results in thii report apply to tha samples analyzed in actvnJancc with the clia:n r-fcuxtndv t/fteument. This analytical report must be reproduced in its entirety.

<Z5

jidrca Stathas. Project Manager Page 23 of 2*

1 2 / 0 2 / 2 0 0 3 TL'E 1 7 : 0 4 [TX/RX NO 5084]

12/02/2003 TUB 5:13 FAI 4145709461 Great Lakes Analytical 1^)026/032




Luke States Industrial Service

3 1 1 E. Greenfield Avc.Milwaukee Wl, S3204

Project: MSCG Pro Treatment ListProject Number, [none]

Project Manager: Tom JncobsonReported:

12/02/03 17:03


ReportingAnalytc Result Limit Unite

SpikeLevel

SourceResult %REC

V.RECLimits WD

UPDLimit Note

Batch 3110424 - EPA 3510CMatrix Spike (3110424-MS1)Fluoraiithene

Fluorcnc

H exuchlorobcnzcnc

HcxachlornhuUdicncI lexachlorovyulopenuuiicnc

Hexachloroethane

Indcno (1 ,2,3-cd) pyieue

Isophtironfc

Naphthalene

Nitrobenzene2-Nitrophcnol

4-Nicrophcnol

N-Nitros<*iimcthy1«mlnc

rosotli-n-propylaminc•rosodiphenybimine

Pcntachlorophcnol

Phenunthrene

Phenol

Fyrcue1 ,2,4-Trieliloroben2ene

2,4,6-Trichlorophcnol

Surrogate: 2-FluorophcnolSurrogate: Phtnol-J6Surrogate: Niirobtnunt-dJSuirnfatc: 2-t-'luoroblphtinylSurrogate: 2,4,6-TribromophtnolSurrogate: p-Ttrphenyt-dl*

Source:21.3

21.4

19.6

13.19.7715.316.0

18.917.6

20,0I6.V6.606.80

22.123.521.222.6

2.7421.114.716.4

9.24S.UV1S.S17.737,210.7

B31 1229-0410.0 up/I

10.0

10.0

10.0

0.00

10.0

10.0 "

10.0

10.0

10.0

10.0

5.00

1.00 "

10.0

10.0

5.00

10.0 "

1.00

10.0

10.0

10.0

"»""""

Prepared:25.025.025.0

25.025.0

25.025.025.025.0

25.025.025.025.025.025.025.025.025.025.025.025.0

ns12562.562. 5ns62.}

11/19/03NDNDNDNDND

ND

ND

ND

ND

ND

ND

ND

NDNDND

ND

ND

ND

ND

ND

ND

Analyzed:R5.285.678.452.439.161.2

64.0

75.6

70.4

KO.O

67.6

26.4

27.2

88.4

94.0

84.X

90.4

11.0

84.4

53. 8

65.fi

7J94.7130.128.32V.S26.7

11/22/0370-130

70-13070-130

70-130

70-130

70-13070-13070-130

70-130

70-130

70-130

70-130

70-13070-130

70-130

70-130

70-13070-130

70-130

70-13070-130

10-11010-110

3I.4-1HIIO.r/0lo-no10-147

LLUL

L

L

L

L

^

L

L

LL

Great Lakes Analytical-Oak Creek Tlie results in this report apply (a th* lamftlr.i analyzed In accortlancr with the chair ofcustody dncumrnt. This analytical report mu.fi he rcproa'uccJ In lit entirtty.

idrca Stathas, Project Manager Page 24

12/02--2003 Tl'E 17:04 [TX/RX NO 5084]

12/02/2003 THE 5:14 FA1 4145709461 Great Lakes Analytical




Lake Slates Industrial Service3 1 1 E. Greenfield Avc.Milwaukee WI, 53204

Project MSCGPre Treatment ListProject Number; [none]

Project Manager; Tom Jacobson

Base/Neutrals and

Anulytc

Great

Rault

Reported:12/02/03 17:03

Acids by EPA Method 625 - Quality ControlLakes Analytical— Buffalo Grove

ReportingLimit

SpikeUnits Lcvd

SourceResult %R£C LrniiLi RPD

RPDLimit Notes

Batch 3110424- EPA 3510C

Matrix Spike Pup (3I10424-MSD1)Accu.tphtheneAccnaphlhylcnc

Anlhnu:ene

Beniidintf

Bcnz (a) anthracene

Bcn7.o (a) pyrcnc

Bcnzo (h) flunranthcne

Beruo (^hi) perylene

Benzo (k) fluuranlhcne

Bis(2-cliloroethoxy)me(hanc

B is( 2-chlomethyl)cthcr

Bis(2-chloroisopropy1)cther

Bis(2-elhylhexyl)phthiilate

•'Uiophenyl phenyl ether

. benzyl phlhalale

4 -CMoro-3-mcthylphcnol

2-Chlorunuphthulene

2-Chlorophcnol

4-Chlorophenyl phenyl ether

Chryscnc

Dihcn7 (a,h) anthracene

1 ,2-Dichlon)hCTl7.cne

1 ,3-DichloTobenzcne

1 ,4-DichluroboLtcne

3 .3 '-Dichlorobejiiidinc

2 .4 -Diehlorophcnol

D-.cthyl phthalutc

2.4-Dimcthylphcnol

Dimelhyl phlhalale

Di-n-bulyl phlhvilulc

4,r>-Dinmo-2-rae(hylphenol

2,4-Dinirrophcnol

2,4-Dinitrocolucnc

2.6-Dinitrutolucnc

Di-n-octyl phlhalutc


Source: B3 1 1 229-04 Prepared: 1 1/1 9/0317.1

17.6

18.14.14

U.2

18.7

16.3

12.3

NDIK.O

10.4

20.2

19.1

16.920.9

16.4

16.1

12.2

16.4

17.C.

15.5

14.3

13.7

11.4

15.2

14.5

20.3

13.4

18.4

18.9

19.5

14.0

18.2

17.6

18.3

10.0

10.0

10,0

0.500

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10,0

10.0

10.0

10.0

10.0

10,0

10.0

2.oo

10.0

10.0

10.0

10.0

10.0

5.00

s.oo10.0

10.0

10.0

ug/1 25.0

" 23.0

25.0

25,0

25.0

" 25.0

25.0

25.0

25.0

25.0

" 25.0

25.0

25.0

25.0

25.0

" 25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0'

25.0

25.0

25.0

25.0

25.0

25.0

25.0

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Analyzed:6S.470.4

72.4

16.672.8

74.8

66.0

49.2

72.0

41.6

80.8

76.4

67.6

H3.6

65.6

64.4

48.8

65,6

70.4

62.0

57.2

54.S

45.6

f.0.8

5S.O

81_2

53.6

73.6

75.6

78.0

56. 0

72.8

70.4

73.2

11/22/0370-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

12.1

13.3

19.9

0.00

18.0

24,0

28.1

0.00

S.93

53.5

6.70

15.9

18.8

20.2

7.06

10,6

2,43

13.6

17.1

5.03

5.44

2.8S

26.0

18.5

4.05

16.3

14.4

12.7

25.4

14.7

31.3

16.6

lfi.2

15.6

20 L

20

20

20 L

20

20 H

20 LH

20 L

20 L

20

20 LH

20

20

20 L

20 11

20 L

20 L

20 L

20 L

20

20 L

20 L

20 L

20 LH

20 L

20 L

20 L

20

20 H

20

20 LH

20

20

20

The mula in this report apply 10 the lamplti analyzed in accordance with Ihi' chain n(custody document. This analytical rtport muit h* reproduced in IU infinity.

<^>

jidrca Stathas, Project Manager Page 25 of 29

12/02/2003 TUE 17:04 [TX/RX NO 5084]


X2£3js:«

"HIGREATLAKESANALYTICAL



Lake States Industrial Service311 E. Greenfield Avc.Milwaukee Wl. 53204

Project MSCO Prc Treatment ListProject Number, [none]Project Manager Tom Jacobson

Rtported:12/02/03 17:03


AnalyteReporting

Result Limn UnitsSpite SourceLevel Remit %R£C

V.RECLimits RPD

RTDLimit Notes

Batch 3110424 - EPA 3S10C

Matrix Spike Dup (3110424-MSD1)FluoruithcneFluorcncHexachloppbengcncHexauhlorobutndieneHexachlorocyulopentudieneHcx.ichloro«(haneIndcno (1.2,3-cd) pyreneIsiTphoroncNuphlhulcncN ilrobtinzoiG2-Nitrophenol4-NitrophoiolN-Nicrosodinicthyiamuie

'roxodi-n-prnpylaniinc

.rasaUipHenylumine

PcntachloropUsnoI

Phcnunthrcnc

Phenol

Pyrcnc

1 ,2,4-TrichIorobaizcne

2 .4 ,6 -Trichlorophenol

Surrogate; 2-Flnorophtnot

Surrugute: Phtnol-dA

Surrogate: Nitrohenzene-dS

Surrogate: 2 -FluorobiphcnylSurrogate: 2,4. 6-Tribromophenal

Surrogate: p-Terphenyl-dl4

Source: BM 1229-0416.3

18.5

16.2

13.1

8.80

15.5

13.0

17.6

16.3

18.3

15.7

6,24

5.49

20.4

19.4

18.6

1H.S

2.85

16.S

13.6

15,3

V.43

6, OS17.2

If i .J

32.114.8

10.0 ug/I

10.0

10.0 "

10.0 "

2.00

10.0

10.0

10.0

10.0

10.0

10.05.00

1 .00

10.0

10,0

5.00

10.0

1.00

10.0 "

10.0 "

10.0

"""""

Prepared; 11/19/0325.025.025.0

2S.O

25.0

25,0 - •

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25,0

25.0

25.0

25.0

2S.O

125125

(i2.5

62.512J

62.5

ND

ND

ND

ND

ND

•ND •

ND

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

ND

Analyzcc65.274.064.R52.435.2

. 62.060.070.465.2

73.262.825.022.081.677.674.474.0

U.4

66.055.261.2

7.SS

4.84

27.5

25.S25.7

23.7

: 11/22/0370-13070-13070-130

70-130

70-130

• 70-130 •

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-1 30

70-130

10-110

1(1-110

31.4-11010-110IO-/IO

10-147

26.IS

14.5

19.0

0.00

10.4

• -1.-30-

6.45

7.12

7.67

8.88

7.3ft

5.M

21.3

8.00

19.1

13.1

20.0

3.94

24.5

6.32

0.94

20

20

2020

20

• 20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

LLL

LH

L

L

L

L

L

L

L

L

LH

L

LHI,

L

Great Lakes Analytical-Oak Creek Ttia results in this rtpon apply to l/iesamplui analyzed In accordance with the ch-i'.rcustody document. '/Ait analytical report must be rtprnductd in its entirety.

.idrea Statbas, Project Manager Page 26 of:"

12/02/2003 TUE 17:0-1 [TX/RX NO 5084] © 0 li •

12/02/2003 TUE 5:14 FAX 4145709461 Great Lakes Analytical 1^1029/032

•?rmr. J_?f |J

"SiGREATLAKESANALYTICAL




Project: MSCG Pro Treatment ListProject Number; [none]Project Manager Tom Jacobson

Reported:12/02/03 17:03

Tentatively Identified Compounds by GC/MS EPA Method 8270 - Quality ControlGreat Lakes Analytical—Buffalo Grove

AnalylsReporting

Result Limit UnitsSpike SourceLevel Result

%REC RPD%REC LimiU RPD Limit Noics

Batch 31 10424 - EPA 3S10C

Blank (31 10424-BLK1)1 ,2.4 ,5 -Tctrachlombcnrcn c

3.3'-DiehLor<obcnzitline

Fciu.ichlorobeuzaieNone

Surragate:p-Terplianyl-d]4Surrogate: 2.4,6-TribromophtnnlSurra/fact: 2-riuoroblphenylSurrogate; Nltroberaena-d5Surrogate: Phtnul-tltSSurrvyaie: 2-Fluoraphenol

LCS(3I10424-BS1)3,3'-Dichlorober»:idinc

Sitrrugutc: p-TfrphenyI-d/4%ate: 2.4.fr-7>l(iromoplii!Hol

agate: 2 -FluorobiphcnylSurrogate: h'itrvbtnztnt-dSSurrogate: Phcnnl-d6Surrogate: 2-Fluorophenal

Matrix Spike (3110424-MS1)

Surrogate: p-Ter(ihvnyl-<114Surrogate: 2. 4. 6-TrihramaphenolSurrogate: 2-FluoroblphenylSvrrogatt:; t^ltrobinzcnu-JSSurrogate: Fhenol-d6Surrogate: 2-Flunrophp.nol

ND 20.0 us/I

ND 20.0

ND 20.0

ND 20.0

17.432.5JC.S17.4 "S.4S9.16

27.1 20.0 ufi/1

22.13S.I "13.23.43

0. 790 "0.00

Source: B3 1 1229-04

16,7 ug/l37.217.7Ifi.aS.S99.24

Prepared: 11/19/03

rt7.J12562.562.312S

J2S

Prepared: 11/19/03

62.512S

62.562.5125

125

Prepared: 11/19/03

62.5121(,2.562.512.1125

Analyzed 11/21/03

27.8 23-ya26.0 JO-J592f.4 31-96 L27. 8 29-W U4.38 10-33 L7.33 10-124 L

Analyzed: 11/21/03

3S.4 23-9S28.1 10-15'J21.1 31-36 L5.49 29-89 LD.K32 1Q-H3 L

10-124 L

Anolyvced: 1 1/22/03

26. 7 23-9829.8 10-15')28.3 31-86 L30. ' 29-S94. 71 10-83 L7.10 10-124 L

Great Lakes Analytical—Oak Creek The raulcs In this report apply to thr lampla analyzed In accordance with the chain nfcustody document. This analytical rtpnn must be reproduced In Its tntirtry.

ndrca Stathas, Project Manager Page 27 of 2-

12/02/2003 TL'E 17:01 [TX/RX NO 5084]

iz/uz/zuua TUhi 5:15 4i457i)94bi ureat Lakes Analytical IP31/U3Z




Luke Suites Industrial Service311 E. Greenfield Avc.Milwaukee Wl, 53204

Projcxt: MSCO Pre Treatment ListProject Number: [none]Project Manager. TomJacobson

Reported:12/02/03 17:03

Notes and Definitions.

A-01 this tmulytc WHS quantified using an open scan.

QC The result lor one or more quality control measurements associated with this sample did not meet the laboratory and/or sourcemethod acceptance criteria.

DET Anulytc DETECTED

ND AnalyLe NQT DETECTED «t or above the reporting limit

NR Not Reported

dry Sample remits reported on a dry weight basis

RPD Relative Percent Difference

L This quality control measurement is below the laboratory established limit

H This quality Conlrtl measurement is nbove the laboratory established limit,

Great Lakes Analytical—Buffalo Grove Wisconsin DNR Certification Lab ID: 999917160

Great Lakes Analytical—Buffalo Grove NELAP Primary Accreditation: Illinois #100261

Great Lakes Analytical-Buffalo Grove NELAP Secondary Accreditation: New Jersey #IL001

Great Lakes Analytical—Oak Creek, WI Wisconsin DNR Certification Lab ID: 341000330

it Lakes Analytical-Oak Creek, WI NELAP Primary Accreditation: Illinois #100307

Note: For analyses that require NELAP accreditation, all analytes, by matrix and method, are accredited following current NELAPstandards unless specifically noted by way of a qualifier listed above.


f]

\

The results in Ihh rtpart apply to th< lamplix analyzed in accordanct with tlie chain \custuJy document. 7'Ai.t analytical report must be reproduced In Its entlrvly.

.drea Stathas, Project Manager Page 2 9 of 2-

12/02/2003 TUE 17:04 [TX/RX NO 50S4] ©031

COCJ

>s—Ica

-C

COCD

CO

t-JCOOJ

I GREATLAKES

(ANALYTICAL

LKJ.II..I i I .il 1

CHAIN OF CUSTODKEPORT Butlalo Grove, IL C0089-4S05 Oak Creek, Wl S31 r>4

(847) 608-7766 (414) 570-946FAX (847) 608-7772 FAX (414) 570-94o.

jy^ Mr faJ tcLj*r In /f/fl '

COOin

ULJH

oOOn

, //o'f/W.v,

ii'M PM 4i4!>YU94bi ireat Lakes Analytical P03/007





Project; MSCG Pro Treatment ListProject Number: [none]

Project Manned-. Tom JacobsoiiReported:

12/04/03 10:07


| Sample ID

Tank 1 3 Spill

Lnboratory ID Matrix

W3 12023-01 Water

DaCc Sampled Date Received

1 1/19/03 13:30 12/03/03 09:47

Great Lakes Analytical'-Oak Creek '111* result? in tkLi rtpvrt apply <O tile samples analyzed in accordance willi the chain nfcustody document, nit analytical report must be reproduced In lu entirety.


12/04/2003 THU 09:58 [TX/RX NO 5097] 121003

urn; u \ u i 4 i i avu»4Di breai LaKes Analytical IP04/007

SES1GREAT"*fS| LAKESJmm ANALYTICAL



Lake States Industrial Service311 E. Greenfield A«e,Milwaukee Wl, 53204

Piujcct: MSCG Pre Treatment LiltProject Number, [none]

Project Manager. Tom JavobsonReported:

12/04/03 10:07


Arnlytc

Tank 13 Spill (\V312023-01) Water

PHTotal Suspended Solids

ResultReporting

Limit Units Dilution

Sampled: 11/19/03 13:30 Received: 12/03/03 09

6.87ND S.OO

pH Unitsmg/l

1

Batch

:47

3120106312010S

Prepared

12/03/0312/03/03

Analysed

12/03/0312/04/03

Method

EPA 9040BEPA160J2

Molts

C5

Great Lakes Analytical-Oak Creek The result's in this report apply to the samples analyzed In accordance with the chain ofcustody document. This analytical nport must be reproduced In Its entirety.

.ndrea Statha-s, Project Manager Page 2 of4

12/04/2003 THU 09:58 [TX/RX NO 5097] @100-1

nuu i i io /ua io i weai Lanes UUI

"SH GREAT"fiBJL'BMB

ilLAKESANALYTICAL



Lake Slates Industrial Service311E. Greenfield Avc.Milwaukee WI, 53204

Project M SCO Pre Treatment ListProject Number: [none]

Project Malinger: Tom JacobsonReported:

12/04/03 10:07

General Chemistry - Quality ControlGreat Lakes Analytical— Buffalo Grove

AnalyteReporting Spike Source %REC

Result Limit Units Level Result %R£C LimitsRPD

RPD Limit Notes

Butch 3120106 - General Prep WC

LCS (3120106-BSl) Prepared & Analyzed: 12/03/03

P"

LCS Pup (3120106-BSD1)pH

Duplicate (3120106-DUP1)

6.99 pH Units 7.00 90.0 08.6-101.4

Prepared & Analyzed: 12/03/036.90 pH Units 7.00 99.9 98.6-101.4 0.00

Sources W312Q13-01 Prepared & Analyzed: 12/03/036.SS pH Units 6.87 0.292

Batch 3120108 - General Prep WCBlank (3120108-BLK1) Prepared: 12/03/03 Analyzed: 12/04/03Total Suspended Solids

Duplicate (3120108-DUP1)Total Suspended Solids

ND S.OO me/1

'Source: W312023-01 Prepared: 12/03/03 Armlyzcd: 12/04/03ND 5.00 mg/1 4.00 11.8 41.9

Great Lakes Analytical—Oak Creek The nisulu In tills report apply to the samples analyzed In accordance with thecustody document. This analytical report must be reproduced in Its entirely.


12/04/2003 THU 09:58 [TX/RX NO 5097]

nnu MA 4 i 4 & Y U S 4 b i i^reai Lanes Analytical 10006/007

^7l^r\T-^-7H IHfl I

!».«•• I

"Si

^B GREATLAKESANALYTICAL



Lake Stales Industrial Service311 E. Greenfield Avc.Milwaukee WI, 53204

Project MSCG Pic Treatment ListProject Number, [none]Project Manager. Toro Jacobson

Reported:

12/04/03 10:07


GS This sample was received past the method specified holdtime.

DET Analyte DETECTED

ND Analyte NOT DETECTED at or above the reporting limit

NR Not Reported

dry Sample reaulbi reported on i> dry weight busi-H

RPD Relative Percent DifferenceL Thin quality control measurement u hclnw the laboratory established limit.

H This quality control measurement is above the laboratory established limit.

Great Lakes Analytical-Buffalo Grove Wisconsin DNR Certification Lab ID: 999917160

Great Lakes Analytical—Buffalo Grove NELAP Primary Accreditation: Illinois #100261

Great Lakes Analytical-Buflalo Grove NELAP Secondary Accreditation: New Jersey ML001



:>te: For analyses that require NELAP accreditation, all analytes, by matrix and method, are accredited following current NTELAPandards unless specifically noted by way of a qualifier listed above.


LjLK0ll#?

The results In this report apply to Ihv Samples analyzed in acuorJanct with ihv t-ltuin ufcustody document. Thh analytical rtpart must bf nproduetd in its tntirtly.

\ndrea Stathas, Project Manager Page 4 of 4

12/04/2003 THU 09:58 [TX/RX NO 5097] Ig]006

nv MA <ii<to/imoi weai Lanes I f f lUUf/UU/

12/03/2003 WED 08:29 FAX 12822426554 ENV ASSOC.


Environmental Associates, Inc.P.O. Box 136

ThiensviUe, Wisconsin .$$092(262) 242-1088 faxQ262) 242-655 )

toll free (800) 494-4645. eahvL com

To: Andrea

Company: Great Lakes Analytical

Fax:

Re;

414-570-9461

Solvay

Sample Tank 13 Spill

W311185-01

From: Joe Midiaelchuck

Pages:

Date; 12/3/03

cc-.

D For Review D Pt«9$e Comment D Ph*d^> Reply Q Recycle

Andrea;

As we discussed, please analyze the above sample for TSS and pH as we originally requestedverbally with Dave Krueger. —— •"•

Please Fax results immediately upon completion.

Thanks.

Joe

C:VWINDOWSM>cskB>p\F«xcw4-01 -diic

12/04/2003 THU 09:58 [TX/RX NO 5097] @]007

ATTACHMENT D

0 Outfall#012

36* Orchard Street sewer to river -

City Sanitary Se

O

D06#008

'-19

.Sanitary Sawer

'emporary F«nonq

Concrete Block |Sediment Trap "

« i GCoal Tar Consolidation and Holding Tank <

O City Sanitary S«w*r

> „x\ Pês

Proposed Decontamination Pad ' ,(See FIGURE 5 for details) .

0

.Sa l

\ #004Ctty Sanitary Sev,er Railroad Tracks

LEGEND

Existing Permanent Fence Line

Temporary Fence Line

Site Rubble Pile

Site Building and Designation

Manhole/Sewer Grate

Storm Water Flow Direction

Drainage Area Delineation Boundary

Drainage Area Designation

Outfall Location and Designation

Shaded Area = Phase I of Demolition

Location of Non-DomesticWastewater Discharge

Subsurface Conveyances :

- - Kinnickinnick River (South)

- — Kinnickinnick river (North)

City Sanitary Sewer

Environmental Associates, Inc.

^ /vnBy:

RRG

8/1 3/03

Drawing :

File:

03-03855-003

stormwatermap.cvS

J\ser

\

Approximate Scale in Feet

0 100 200

FIGURE 1Former Solvay

Coke-& Gas SiteStorm Water Runoff Map

01/07/2004 ID 3:49 FAX 4145709461 Great Lakes Analytical $001/017

GREAT140 ewt Ryan Road Email: [email protected]

ANALYTICAL Oak Creek. Wisconsin 53154 (414)570-9460 FAX (4 14) 570-9461

06 January 2004

Tom JacobsonLake States Industrial Service311 E. Greenfield Ave.Milwaukee, Wl 53204RE: MSCG Pre Treatment List


Sincerely,

Great Lakes Analytical


01/07/2004 ID 3:49 PAI 4145709461 Great Lakes Analytical

SSI GREATLAKESANALYTICAL

140 East Ryan RoadOak Creek, Wfeconsin 53154

Email: [email protected](414)570-9460 FAX (414) 5704461

Lake States Industrial Service311 E. Greenfield A ve.Milwaukee, Wl 53204

Project; MSCG Pre Treatment List

Project Number [none]Project Manager. Tomlacobton

Rep*rted:01/06/04 17:18


Sample ID

Fractonlc-pojl Tr«tm«ot

Labontorjr ID M»tri*

W3I2248-01 Water

Date Smpled Dmtc Rnrmd

nmim 14:40 1Z^3/03 14:38

Gnat Lakes Analytical-Oak Creek The rtmla In All report appfy to the lompla antlyzttl in accordma with tkt chain ofcustody document. Tliis analytical np«ri anat bi rtprvductd In la entirety.

Andrea Stattaa*, Project Manager Page 1 of 15

01/07/2004 m 3:50 FAI 4145709461 Great Lakes Analytical



Email: lnf6Qgtalaba.com

(414)570-9460 FAX (414) 570-8461


31 IE Greenfield Ave.

Mitortnkee, Wl 53204

Project: MSCGPre Treatment List

Project Number [none]Project Manager. TomJacobson

Rcp«rt«d:01 WO* 17:38

General ChemistryGreat Lakes Analytical-Buffalo Grove

AnatytB ResultRepotting

Limit Units Dilation Bttcb PiefaaA AoHlyied Method Notw

Frw*«k-p<>»t Treatment (W3m4Ml)VV«ter Sampled] 12/22/9} 14:40 Received: 12/23/03 14:38

Cyanide (total)Oil&QiwueTotal Sasptndcd Solid*

0.150ND12.8

0.01005.005.00

mg/1 31206693120740312M95

12/29/W12/30/9312/2V/03

01/D6/04

I2/30AJ3

EPA9012AEPA 413.1EPA I60i

Great Lakes Analytical-Oak Creek 7S« route la this report apply to Ifi* sampla anafynd in accordance viidi fa chain ofau&ty document, nit analytical report ">"" *« rtproduced in la entirely.

Andrea Stathas, Project Manager Pago 2 of 15

01/07/2004 ID 3:50 FAX 4145709461 Great Lakes Analytical




Lake State* IixUwtrl*! Service31 IE Greenfield Avc.Milwaukee, Wl 53204

Project MSCGPrc Treatment ListProject Number [none]Project Manager Tom Jacobton 01/06/04 17:38

Total Metals by EPA 200 Series MethodsGreat Lakes Analytical—Buffalo Grove

Analyta RemitReporting

Limit Unto Dilution Batch Prepared Analyzed Method Notes

FraetOBk-poit Treatment (W31224S41) Water Sampled: 1172/03 14:40 Received: 12/23/03 1438

SilverCadmlvmChromiumCopperMercuryNickelLeadZinc

NO0.000727

NDND

0.000252ND

0.0123ND

0.0500 m<0.000500

0.01000.0500

0.0002000.0500

0.00500OJOO

tn 312067031207323120670

•401003?312W7040100293120670

12/29/0312/30/03I2<79A)3

«

01/0*0412/29/0301/05/0412/29/03

12/30/0312/30/0312/30/0312/30/0301/06/0412/30/0301/05/0412/30/03

EPA 200.7EPA 21316PA 200.7

H

EPA24S.1EPA 200.7

EPA 239.2EPA 200.7

QCQC

QCA-01

Great Lakes Analytical-Oak Creek Tlis rtmta tn Alt raport apply u At sanplts anatyul In accordant* viitli the chain cfcustody document. Tnls analytical report must te reproduced In la entirety.


ui/()7/2Ul)4 m 3:50 FA14145709461 Great Lakes Analytical



Email: infcK&jlalaba.com{414)570-9460 FAX (414) 570-3461

Lake States Industrial Service31 IE Greenfield Avc

. Milwaukee, Wl 33204

Attalyie

Project: MSCG Pre Treatment LiltProject Number [none] R*p»rt*d:Project Manager: Tom Jacobson 01 /06/04 17:38

Volatile Organic Compounds by EPA Method 624Great Lakes Analytical-Buffalo Grove

ReportingRemit Limit Unib Dilution Batch Prepared Anulyml Method Nota

Fraetonk-post Treatment (W312248-01) Water Sampled: 12/22/03 14:40 Received: 12/23/03 14:38 QC

AcroleinAcrjHoahrileBenzeneBmmodichloromethaneBromofbrtnn nUFvUIOlllVUUuiO

Carbon tctrachlorideChlorobenzeneChlorodibiinnomoaiaiicChloroethane2-Chkroethylvinyl c4herOriorofonnChlpromethane1 ,2-D!chlorobaizcne1 ,3-Dicfalorobenzene1,4-DlchtorobenMsie1,1 -Dich iCTocuiane1,2-Dichlorocthnnc1,1-Dichloroethenetis- 1 ,2-DichlonK4hcnetnnt-l,2-Dichloroethene1 ,2-DIchloropropanecia- 1 ,3-Dicfaloropropcnctrans- 1 ,3-DlchloropropeneEtfaylbenxeneMethylene chlorideStyrcne1,1,2,2-TetrachloroediancTctrachlorocthcncToluene1,1,1 -Trichloroctfaane1 , 1 ,2-TrichloroethanoTrichloroeiheneTrichlorofluaromcthaneVinyl chloride

Surrogate; DlbromofluorumtthantSurrogatr: l,2-Dichloroethane-J4Surrogate: Toluene-48Surrogate: 4-Bmmafluorobtraenc

ND 50.0 UB/1 1 4010034 01/05/04 01/05/04 EPA&4/S260BND 50.017$ 5.00ND 5.00ND 5.00ND 10.0ND 5.00ND 5.00ND 5.00ND 5.00ND 100ND 5.00ND 10.0ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND 5.00ND S.OOND 5.00ND 5.00

38.2 5.00ND 5.00ND 5.00ND 5.00ND 5.00

m m

« II

H •

M II

» It

M H

• R

H •

W N

« l>

n •

N «

"« *

N •

H n

•"

II M

. H

N fl

II II

n «

w m

H N

H It

• H

H m

m m

R H

H H

II H

H n

ND 5.00

97.2 % 75.8-12792.6% 62.5-14595.4% 76.6-130

N

"

m

m

*•*

M

m

m

m

m

w

M

H

"

H

«

II

B

M

H

"

•if

N

"

W

It

•

'

"

H

*

H

93.2% 68.9-123


Andrea Siathaa, Project Manager

Tilt rtsulti In Ait rtport apply to the iampla onafymd la accordance viA die chain ofcustody document. Thii matytital rtport mat be rtprotucti in it* mtirtty.

Page 4 of 15

01/07/2004 ID 3:50 FAI 4145709461 Great Lakes Analytical


140 East Ryan RoodOak Creek, Wtaconsln 53154

Em0B: [email protected](414)570-9460 FAX (414) 570-9461

Lake States Industrial Service31 IE Greenfield Avc.Milwrokcc,WI 33204

Project MSCGPre Treatment LwtProject Number, [none]

Project Manager Tom JacobsonR«fwr(*d:

01/06/04 17:38

General Chemistry - Quality ControlGreat Lakes Analytical-Buffalo Grove

AnriytoRepotting

limit UntoSpike Source %WEC RPDLcvd Result SREC LtaiU RPD Limit Note

Bitch 3120669 - General Prep WC

Blank (3I2Q669-BLK1)Cyanide (total)

LCS012Q&S9-BS1)

Prepared A Analysed: 12/29/03NO 0.0100 mg/1

Prepared & Analyzed: 12/29/03Cyanide (total)

Matrix Spike (3120669-MS1)Cyanide (total)

Matrix Spflce Pup (312M69-MSD1)

0.513 0.0100 mg/1 0.400 107 60.6-148

Cyanide (total)

Batch 3120695 - General Prep \VC

Scarce; 8311348-01 Prepared & Analyzed: 12/29/031.03 0.0250 mg/1 1-20 0.005*9 85.4 212.174

Sourer B312348-01 Prepared & Analyzed: 1M9/031.20 0.00549 92.0 24.2-17+ 7.4«1.11 0.0250 mg/I 11.2

Blank (312069&-BLK1)Total Suspended Solldi

Duplicate (3H069S-DUP1)Total Sitfpended Soliib

Batch 31Z0740 - EPA 3510C

Prepared: 12/29/03 Analyzed: 12/30/03ND 5.00 mg/1

Sow*; W3I224S-01 Prepared: 12/29/03 Andygal; 12^0/0313.6 5.00 me/I I2.S 6.06 41.9

Blink (312074Q.BLKI)OilAQrease

OU&GRUC

ND $.00

Prepared: 12/30/03 Anqlyxed: 01/06/04

Prepared: 12/30/03 Analyzed: 01/06/0426.R 5.00 nig/1 30.0 89.3 4X6-123


Andrea Stadias, Project Manager

The result} in Oils nport apply to tk* «mpt*i anatyiett la accordance with the chain ofcustody document, nti analytical report must be reproduced In Its entirety.

Page 5 of 15


3SSBGREAT\ LAKESIANALYTICAL



Luke State* Industrial Service31 IE. Greenfield Av».Milwaukee, Wl 33204

Project: MSCQPre Treatment Li«Project Nuinbw: [none]

Project Manager TomJacobtonReported!

01/06704 17:38

General Chemistry - Quality ControlGreat Lakes Analytical-Buffalo Grove

Analytt

Batch 3120740 -EPA3510C

ReportingRemit Limit Unit*

SpikeLcvd

SourceRwult %REC

HRECUmib RPD

RPDUmit Notes

LCS Dnp (3I20740-BSP1)Oil&Grawe 29.8 5.00 mg/1

Prepared; 12/30/03 Analysed: 01/06/0430.0 99.3 42.6-123 10.6 52.4

Great Lajces Analytical-Oak Creek TfW results In Ala nport apply ti> At samples aaefyud In aecordmc* wftA ike chain ofcustody docvmtnl. This analytical nport must be reproJuetd in its tatircty.

Andrea Stathas, Project Manager Pa$e6oflS





Lake Stales Industrial Service31 IE. Greenfield Avc.Milwaukee; WI53204

Project; MSCG Pro Treatment ListProject Number [none]Project Manager TomJaeobson

Rqxrtedt01/06/04 17:38

Total Metals by EPA 200 Series Methods - Quality Control


An*ly«e Result Limit UnitiSpike Source %REC RPDLevd Remit %REC Limit* RPD Umft Notes

Batch 3120670 - EPA 3010A

Blank (31M670-BLK1)LJIOflllUITl

Copper

NWcd

Sflver

Zino

LCS(3120670-BS1)Chromhun

Copper

Nickel

Silver

Zinc

Matrix Spflu (3120670-MS1)Chnnnium

Copper

Ntekd

Stiver

Zhio

Matrfa Spike Pap (3J2W70-MSP1) _Cbfoouuin

Copper

Nickel

Silver

Zinc

ND

ND

ND

NDND

3.M3.73

3.87

3.23

3.92

0.0100 rag/I

0.0500

0.0500

0.0500

0^00

0.0100 mgfl

0.0500 "

0,0500

0.0500

0.500

Sourw: B312457-013.80

65.0

4.07

0.0209

J5.1

0,0100 me/1

0.550

0.0500

0.0500

5.50

Sonrcei P312457-013.90

07.4

4.21

0.0212

35.4

0.0100 mg/1

0.550

0.0500

0.0500

5.50

Prepared: 12/29/03 Analyzed: 12/30/03

Prepared: 12/29/03 Analyzed: 12730/034.00 91.0 86.9-113

4.00 93 J 89.8-115

4.00 96.8 90-114

4,00 80.8 61.6-136

4.00 98.0 ((,8-117

Prepared: 12/29/03 Analyzed: 12/30/034.00 NO 95.0 79.9-120

4.00 69.3 NR 76.3-136 L

4.00 0.0549 100 82.2-123

4.00 ND 0.522 10-154 U

4.00 32.0 77J 76-135

Prepared: 12/29/03 Analyzed: 12/30/034.00 ND 97.5 79.9-120 2.40 17.7

4.00 69J NR 76.3-136 3.63 l».l L

4.00 0.0549 104 82.2-123 3.38 19

4.00 ND 0.530 10-154 1.43 60.6 L

4.00 32.0 85.0 76-135 0.851 28.4



7%e results In Oilt report apply to tht lomptes analyied in accontanct witA iht chain ofcustody document Tkb analytical ntpyrt mat bt reprrxhictJ In its entlnty.

Page 7 of 15



140 Eaat Ryan RoadOak CreeK. Wisconsin 53154


Lake Sates Ituhucriil Service311 B. Greenfield Ave.Milwaukee, WI53204

Project MSCOPre Treatment U«Project Number [none]

Project Manager: TomJaooteonRtporttd:

01/06/04 17:38

Total Metals by EPA 200 Series Methods - Quality ControlGreat Lakes Analytical-Buffalo Grove

AulyteImporting Spike Source HREC RPD

Result Umk Unlit Lowl Remit SREC Limit! RPD Limit Nota

Batch 3120732 - EPA 3010A

BUnk(312073a-BLKl)Cadmtom

LCS (3110732-BSt)Caddtium

M«bte Spike (3120732-MSl)

NO 0.000500 mg/tPrepared & Analyzed: 12/30/03

Prepared & Analysed; 12/30/030.00174 0.000500 mg/1 0.00200 S7.0 85-115

M«tri« Spike Dup (3120732-MSDl)

Batch 4010029 - EPA 3010A

Source: W312248-01 . Prepared & Analyzed-12/30/030.00215 0.000500 mg/1 0.00200 0.000727 712 79-129

Sourc*: W312248-01 Prepared & Analyzed: J2/30/03_0.00221 O.OOOSOO Mg/I 0.00200 0.000727 74.2 75-125 2.75 20

Blank (40IOC29-BLK1)Lead NO 0.00500

LCS (4Q10Q29-BS1)

Prepared & Analyzed: 01/05/04

Prepared & AmJyzod: Q1/Q5/04

Matrte Spite (4010079-MS»

0.0244 0.00500 mg/1 0.0240 102 71.7-141

Sourcct B312549-01 Prepared & Analyzed: 01/05/04

MabrU SpOaPup (401002».MSD1)

0.0233 0.00500 mg/1 0.02*0 0.0009l 93.3 17.2-176

Soqrct: B31254»-01 Pfepared Jt Analyzed: 01/05/04™0.0231 0.00500 mg/l 0.0240 0.000919 92.4 17:2-176 O.H62 33.7

Batch 4010037 - EPA 7470A

Blank (40IOQ37-BLK1)Mereury

Prepared: 01/05/04 Analysed: 01/06/04NO 0.000200 me/1


Andrea Statha*, Project Manager

n* rtntta In Alt npoft apply to At lamples anafyted In accordance with tht chain ofcustody document. This analytical rrport mutt 6* rsfrvdwxd In ill tntirely.

Page 8 of 15

U1/U7/2004 m 3:52 FAI 4145709461 Great Lakes Analytical




Lake States Industrial Service3 ME. Greenfield AvaMilwaukee, Wl 53204

Project: MSCG Pre Treatment Li«Project Number [none]

Project Manager Tom JacobronReported:

01/06/04 17:38

Total Metals by EPA 200 Series Methods - Quality ControlGreat Lakes Analytical-Buffalo Grove

AaalyteReporting Spike Source %REC RPD

Rcwih Limit Unit* Level Result HKBC Lhnfo RPD Lbnh Note*

Batch 4010037 - EPA 7470A

US(401<X»7-BS1)Mtrouy

Mitrta SpDce (4010037-MS1)

Prepared: 01 /OS/04 Analyzed: 01/06/040.00165 0.000200 mg/t 0.001 50 110 76.6-124

Source: W312248-01 Prepared: 01/05/04 Analyzed: 01 /06/04Meroory

M»tri» Spik. Dap (4010037-MSD1)_Mworoy

Sonrce: W312248-010.00199 0.000200 mg/t

Prepared: 01/05/04 Analyzed: 01/06/040.00150 o".ol»2S2 116 43.1-149 1.00 22.S

Great Lakes Analytical-Oak Creek n* muits in this report apply to Oa somplts anafyad in accordance wi'tA ttu chain ofcustody document. Thli analytical report must be reproduced In la entirety.

Andrea Stathas, Project Manasw Page9ofl5



140 East Ryan RoadOak Creek, Wlaconsln 53154


(414)570-9460 FAX (414) 570-9461


311E.GrcenfleWAve.

Milwaukee, Wl 53204

Project: MSCG Pus Treatment List

Project Number [none] RqwrfediProject Manager: TomJacobson 01/06/04 17:38

Volatile Organic Compounds by EPA Method 624 - Quality ControlGreat Lakes Analytical-Buffalo Grove

Analyle RttultReporting Sptk» SOUIOT HRBC RPD

Umit Unta Level Roull %REC Limio RPD Limit NOM

Batch 4010034 - EPA 5030B (P/T)

BUBk(40100J4-BLKl)AofOHsn

Acryfanitrile

BottOM

Bronxxflchloromettaio

Bronofbrm

Bromoraahnic

Curfxn tetraohtorido

Chlonbaizaw

ChlorodibroinomellHoe

Chlo(octli*nc

Z-Chlonxdiylvinyl ctficr

Chlnpform

ChkmjiuLihiiiie

1.2-DichlttOterane

1,3-DlohionbcaEcaro

1,4-Dkshlorobcnimo

l.t-DichlaneUwne

li-Dbhlotoettune

1.1-DtthlMoeOMM

oL-U-DtchlorocthcflC

tnn»-l,2-Dlehlcn>et1iono

IJ-Diuhloropnipane

cit-1 J-DichJoroptopcno

tno*-l J-Diehloropropoio

BOiynxnaJK

Methylcneehkiridc

Stynsw

l.UJ-Tetnchlancdunc

T«trachlo(o«thete

TOlUCD*

I.Ul-TricUatoeaiane

1,1,2-Ttlotiloroctbiiic

Triohloroethenc

TricMotofluoTOmetiume

VTnylehlofidt

ND

ND

NDND

ND

ND

ND

NDND

ND

NDNDNDNDND

ND

ND

NDND

ND

ND

NDND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

ND

ND

Prepared & Analyzed: 01/05/0450.0 BgA50.05.005.005.00

10.0

5.005.00

5.00

S.OO

100

5.0010.0

5.00

5.00 "

5.00

5.W

5.005.00

5.00

5.00

5.005.00

5.00

5.00

5.00

5,005.00

5.00

5.00

S.OO

5,00

5.00

5.00

5.00

Great Ukes Analytical-Oak Creek

/) p

U>4^2âÔ

The remits la Iliia report apply u ike samples analyzed in occordmct with tht chain ofcustody document. This analytical report muff 6* nproductd til Id entirety.


1)1/07/2004 ID 3:52 FAI4145709461 Great Lakes Analytical


140 East Ryan Road

Oak Creak, Wisconsin 53154


(414)570-9460 FAX (414) 570-9461

Lake State* Induttrial Service

31 IE. Greenfield Ave.Milwaukee, WI53204

Project: MSCG Pro Treatment Ust

Project Number [none]Project Manager Tom Jacobson

Reported:01/06/04 )7:38

Volatile Organic Compounds by EPA Method 624 - Quality Control


ArialytgReporting

RoiuJt Umh UnitsSpikeLevd

Source HREC RPDRamlt HREC Unit* KFD Unit Note*

Batch 4010034 - EPA 5030B (P/T)

Blank (4010034-BLM)

Su/rogait: DibnmafluanmtAaa

Surrogaa: 1.2-EXd>lon*tlvuw-d4

Surrogate: Toiutiu-dtSvmgvi*; 4-Bnanofbiorebtniui*

LCS(4010034-BS1)

Bonzea*

BrpmodicMoionMhaiM

Biomufbcfl)

Biumomethinc

Caifaon tctnchlnido

CMorobetuaae

CMorodibfomometiane

ChliJlljMllUlQ

2-Chtoroethylvtnyt ether

Cttkworonn

QdofonMffitM

1,2-DlghVrobmMM

U-Otchtambaizcno

1,4-Dichloiobenzene

I,l-Dichl0f0«thme

U-Dichtoro«h3M

1,1-Dichlorothcm

ci*-l ,2-Otehloroethenc

ttaaf- 1 ,2-DiebIonxthene

U-DicbloropTOpane

clvl ,3-Dlchloroproptut

tnn»-l 3-DicblofoprofKoe

Efliylbcnzcnc

Molbylawohlorklc

Styrene

1,1^2-TeMchloroethmie

TorachloKMOMM

Toluene

1,l,l-Trichloroc(h«nc

l,IJ2-Trichkjrocth»i«!

47.9

49.041.5

4SJ

ug/tM

m

'

30.0

)0.030.050.0

Analyzed: 01/05/04

95.6 7S.8-I27

99.0 tJ.S-1439S.O 76.6-23092.6 6S.9-I2J

Prepared A Analyzed: 01/05/044«.l

48.356.631.939.549,553.1

43.1

48.8

45.4

44.8

50.2

50.7

48.0

45.8

46.849.6

49.3

464

48.450.5

50.4

50.4

34.3

50.5

59.04V.O

43.3

43.2S3.5

5.00 uc/15.005.00

10.0

3.005.00

5.00

5.00

100

5.0010.0

5.00

5.00

5.004.00

$.00

5.00

5.00

5.005.00

5.00

5.00

5.00

5.00

5.005.00

5.00 "

5.00

5.00

5.00

50.0

50.0

50.0

50.0

50.0

50,0

50.0

50.0

50.0

50.0

5<J.O

50.0

50.0

50.0

50.0

50.050.0

50.0

50.0

50.050.0

50.0

50.0

SO.D

50.0

50.050.0

50.0

50.0

50.0

921 6U-142

96.6 65.9-162

U3 30.2-176

63.8 33.8-161

79.0 40.3-164

99.0 79.9-132

106 54-159

862 37.1-163

97.6 80-120

90.8 78.6-132

89.6 343-158

100 78.6-139

101 79.1-136

%.0 78.2-129

91.6 58.2-134

93.6 73-136

99.2 58-136

99.0 763-135

92.8 58.3-137

96.8 65.9-147

101 61-165

101 59.4-166

101 78.4-130

68.6 52.2-142

101 69.2-144

US 40.3-164

98.0 44.9-165

90.6 77.4-131

86.4 66.6-143

107 74.8-147

Great Lakes Analytical-Oak Creek Vie results in this report appfy 1C Iht stmpla analyiid in accordant* wiM ttu chain ofcustody document Ttiti analytical ntport mot bt nprotbictd In la snJlnty.

Andrea Stathas, Project Manager Page 11 of!5

01/07/2004 ID 3:52 FAI 4145709461 Great Lakes Analytical 1013/017




Lake State* Industrial Service31 IE Greenfield Avc.Milwaukee, WI53204


Project Manager: Tom JaoutaonRtportcdi

01/06704 17:38



Aoulylfi RaultRepotting

limit UnitsSpikeLevti

SourceResult KREC

ttREC RPDLimill RPD Limit Notes

Batch 4010034 - EPA 5030B (P/T)

LCS(4010034-BS1)TrW,ioroedicn.

Vinyl chloride

Surrogate: DthroaiafluoromahaneSurrogate; I,2-Dlchloroethant-d4Sumgait: Tohmc-dSSurrogat*: 4-Branafluarobeiuene

Mttrta Spike (4010034-MS1)BenzeneBtDmooScUonnnitlutmBroroofbnnBRHnomcOuuicCaibun tetnchlpride

ChloiodibfDitionKtliiuH)Chlorocthin*2-ChloiDcthylvinyl &hcr

Chloroform

CnloiDBtedMaeI ,2-Dichloiobenzene1 ,3-DichlofotenMBe1 ,4-Diehlon>benxenc1,1-Dichloroethane1,2-DichloroeUiane1.1-Dlchlofoethenecif-l,2-Di<:hloroetJbaietimra-1 ,2-DichtofDethene1,2-DlchloropTup.necit-U-Cfehloropropcwtiam-l,3-Dichlon>prnpeneEthylbazentMethytaM chlorideStyraie

1,1,2^-TetnchlgrocthjincTetnchlMOetbene

Prepared & Analyzed: 01/05/0448.748.1

46.8

SO.O48.647.045.5

5.00 ug/l5.005.00 "

m

m

tt

Sounxi B312479-0153.052.954,142.845.450.751.355.5

ND

48.541.047.749.2

43.8

51.4

53259.751.351.0

56.4

53.753.55Z240.651.561.648.9

5.00 ug/15.005.0010.0 "5,005.005.005.00100

5.00

10.05.005.005.005.005.005.005.00S.OO "5.005.005.005.005.005.00 "5.005.00

50.050.050.0

50.0SO.O30.050.0

Prepared: 01/05/0450.050.050.050.050.050.050.050.050.050.0

50.050.050.050.050.0

50.050.050.050.0

50.0

SO.O

50.0

50.0

50.0

50.0

SO.O

50.0

NDNDNDNDNDNDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

97.496.293.6

10097.294.091.0

Analyzed;10610610885.690.8101103111

97.082.095.498.487.6103106119103102113107107104

»U10312397.8

46,7-16936-164

51.5-146

75.S-12762.S-I4376.6-1306S.9-H3

01/06/0439-3-16539.5-18621.1-16933.2-164

10-18156.1-15049-157

36.1-16880-120 L

67.5-14223.5-16768.3-13562.8-13662.1-13046.7-14260.6-15138.7-14249.2-15548-137

44.6-17128.6-19540.6-17656.1-14441.9-15431.1-16943.9-18629.1-160

Great Lakes Analytical-Oak Creek n* raultt in this report apply to Iht sampla anafyitd In accordance with the chain ofcustody ttociantiu. This analytical rrport must h* reproduced In Its tnllrtlf.

Andrea Statfaa*, Project Manager Page 12 of 15





Lake States Industrial Service31 IE Greenfield Ave.Milwaukee, W153204

Project MSCGPrc Treatment UstProject Number [none]Project Manager: Tom Jacobdon

Reported:

01/06/0417:38

Volatile Organic Compounds by EPA Method 624 - Quality ControlGreat Lakes Analytical-Buffalo Grove

AnalyteReportiag

Remit Limit UnitjSpikeLevel

SourceReniK WEC

%RECLhnitf RPD

RPDLimit Not*

Batch 4Q10034 - E?A 5030B (P/T)Matrix SpflM (4010034-MS1)Toluene1,1.1-Trichlqrgcthjne

1,1,2-TrlchIoroetfune

TrichlMDeiheneTricblofofluoromcthjuievinyl chloride

Surrogate: fWuvmofluorcmelhajuSurrogate: l,2-Didilorotthant-J4Surronatt: Tolutnt-JSSurrogate 4-Bromofhiorobcnicnc

Matrix Spikt Dvp (4010034JMSD1)Benzene

BraaodkUoramethaiie

BnmkoCbnttBnpnomeuvuieCaiton tctDchloridc

dUOIDDCDZCClC

ChlOfOdibrtrawmelhaiu:

Qdofoethane2-ChkMoedtylvinyl etherChlonjfbnn

ChloiDmethane

1 ,2-DieUotubeazeDe

1,3-Dicbtaobenzene1.4-DichJorobenzene1.1-DleUoroetluuM1,2-DichloiQcthanc

1,1-Dichloroethene

Cis-l ,2-DivhlonKthene

tiattf-1 .2-Dichloiudhcno

U-Dichloropioparwcif-lJ-DwbkMoptopaMtnaa-U-Dlch1oTOpn»P<»«EUrylbarraie

Methylenechlofide

So«rce: B312479-0150.0

46.0

5<)J2

53.2

53.0

47.0

43,633.250.2

48.3

Source:54.9

57.7

37.4

44.6

48.4

54.A

55.7

56.2

ND

52.3

48.7

50.8

34.0

482

53.0

56,5

59.7

55.8

55.0

60.8

37.3

57.1

56.8

53.8

5.00 ug/l

5.00

3.00

5.00

5.00

5.00

•m

n

it

B312479-015.00 agft

5.00

5.00

10.0

3.00

3.00

5.00

5.00

1005.00

10.0

5.00

5.00

5.00

5.00

5.00

5.00 "

5.00

5.00

5.00

5.00

5.00

5.00

5.00

Prepared: 01/05/0430.030.050.050.0

50.0

50.0

50.0

}0.030.030.0

ND

NDND

ND

ND

ND

Prepared; 01/05/0450.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

30.0

50.0

50.0

50,0

50.0

50.0

50.0

NDND

ND

ND

ND

NDND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

ND

Analyzed: 01/06/0410092.0MS110106

94.0

97.2106too96.6

36.2-13242.2-15269.5-155

13.5-180

12-173

21.5-163

75.8-12762.3-14}

76.6-13068.9-123

Analyzed: 01/06/04110

115

11589^

96.8

109

111112

105

97.4

102

\0«96.4

110

113

119

112

110122

115

114

114

108

39.3-165

39.8-186

28.1-16933.2-164

10-181

56.1-150

49-157

36.1-168

80-120

67.5-142

23.5-167

68.3-135

62.8-136

62.1-130

46.7-142

60.6-151

38.7-142

49.2-155

48-137

44.6-171

28.6-195

40.6-176

56.1-144

41.9-154

3.52

8.68

552

4.12

6.40

7.41

8.22

1.25

7.54

17.2

6.29

9JO

9.57

6.77

6.02

0.00

8.40

7.55

7.51

6.49

6.51

8.44

28.0

38.2

34.2

35.5

33.8

37.5

17.5

29

46

20 L

17.5

33.8

14.8

15.7

13.2

19.9

16.9

23.5

18.6

20.1

32.4

43.6

3924

23.8 H

Great Lakes Analytical-Oak Creek The ruuta in till} report apply to Ih* iamplts anafyad in accordant* vith tkt chain ofcmtcxty docunwU. Thtt analytical rtpvrt omit b* reproduced in in uitirety.

Andrea Stathas, Project Manager Pagel3ofl5

01/07/2004 ID 3:53 FAI 4145709461 Great Lakes Analytical 8015/017





311 E. GreenfieW Ave.Mflwwjkee,WI 53204

Project* MSCGPrt Treatment List

Project Number [none]Project Manager TomJacobfon

Reported:01/06/04 17:38



Analyle RemitReporting

Limit Unit,SpikeUvrd

SourceResult %KEC

SMCLimit* RPD

RPDUmlt Nona

Batch 4010034 - EPA 5030B (P/T)

Mrtrh Spike Pup (4010034-MSDl)Stymie

1 ,1 ,2,2-TcnacfaloroctliiJic

Tetnchlonethoie

Tohrtfle

1,1.1-TMchkKoethane

Sourc*: B312479-01 Prepared: 01/05/04 Analyzed: 01/06/04

Triohloroobcno

Triff fmHijTHII m HI Hfl llMllfl

Vinyl uhkode

64.7

52.6

53.6

49.3

62.6

57.9

J7.7

J5.2

3.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

ug/l 50.0

50.0

50.0

30.0

50.0

50.0

50.0

SO.O

50.0

ND

ND

ND

ND

ND

NDND

ND

ND

: Dibnmqfluoromahm*Surrogatt: l.2-DtctiIoroethane-J4Surrogate: Totucne-43Surrosial*: 4-Bnanqfluorobemmt

4S.652.S49.947.1

SO.O30.050.0SO.O

1061291051079S.6125116115110

97.2103

9V.S94.2

31.1-169

43.9-186

29.1-160

56.2-132

422-152

69J-153

13,5-180

12-173

21.3-165

3.25

4.91

7.29

6.95

6.93

3.5S

4.77

S.49

62.5-14376.6-13068.9-123

46.4

33J

32.3

2J.6

20.1

29^

34.1

39.7

54.1

Great Lake* Analytical-Oak Creek The results in this report apply la ttu samples anafyud In accordance with the chain ofcustody documtnL This analytical report mat be reproduced la its entirety.

Andrea Stxthu, Project Manager Page 14 of 15

01/07/2004 ffED 3:54 FAX 4145709461 Great Lakes Analytical

| GREATLAKESANALYTICAL

140 East Ryan RoadOak Creek, Wlscontin 53154

Email: lnfcxgglalabs.com(414)570-9460 FAX (414) 570-9461

Lake States Industrial Service3H E, Greenfield Avc.Milwaukee, WI53204


Project Manager TomJacobwnRcportadi

01/06/04 17:38


A-01 Initial calibration verification recovery is 90%.

QC . TTic resuh for one or more quality control measurement! associated with this sample did not meet ihe laboratory and/or sourcemethod acceptance cntana.

OET Analytt DETECTED

ND AnaJyteNOT DETECTED at or abovt therepotting limit

NR Not Reported

dry Simple rejultjrqxjrtw) on* dry weight bau»

RPD Kdatrv* Percent DifleraeeL Th» qujdhy control mct»nmcnt if bdowU»Iaboratoty<at»bJiihcd limit.

H This quality control meuuraaenl ia above the bbontory crtaUisbed limit

Great Lakes Analytical-Buffalo Grove Wisconsin DNR. Certification Lab ID: 999917160

Great Lake* Analytical-Buf&lo Grove NELAP Primary Accreditation: Illinois #100261

Great Lakes Analytical-Buffido Grove NELAP Secondary Accreditation: New Jersey #IL001



Note: For analyses that require NELAP accreditation, all analytes, by matrix and method, are accredited following current NELAPstandards unless specifically noted fay way of a qualifier listed above.

Great Lakes Analytical-Oak Creek TTtt rault? In this report apply to tht aampla anafyted In accordant* with Ihe chain ofciatody document. This analytical report mutt be reproduced In ill trairwty.


BSSBGREAT{LAKES(ANALYTICAL

CHAIN OF CUSTODY REPORT1380 Busch Parkway

Buffalo Grove, IL 60089-4505(847) 808-7766

FAX (847) 808-7772

140 E. Ryan RoadOak Creek, Wl 53154

(414) 570-9460FAX (414) 570-9461

Mothod:Ctom D Shrpmd D Courier D

XofBoWosPreservative Used

/O NUMBER

If

PfD:

PtD:

PBX

W

F

«0r

PfDr

a.-?


APPENDIX G-3

Asbestos Test ResultsClearance Testing



LAKE STATES INDUSTRI PAGE 02

*-3"MICRO ANALYTICAL, INC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Fax: (414)771-6570

'-\ <

Lake States Industrial311 E Greenfield Ave.Milwaukee WI 53212

PCM FIBER COUNT REPORT

Tob ID: Building 3

Sampled By: Shawn Christen

Vnalyat: Aaron Engelman

Sample ID

B3-01A

B3-01B

Report # 63763

Date Received: 03/29/04

Date Analyzed: 03/29/04

Fibers/CC F/IQO Fids Comments

2.0<0.00214:00 16:30

<0.002 5.014:00 16:30

Lpm 12.00 Ltrs 1800.0

Lpm 12.00 Ltrs 1800.0

LOB jUmic o£ Detection) policy of MicroAnslytlcnl, Inc. la fl.9JF/nmS or 7fbrij/100fIdedesignated with a "«" sign.

AIHA 101057

12-.J.J 1414B450645LAKE STATES INDUSTRI

PAGE 03

Micro Analytical, IDC.11521 West North Avenue

Mi lwaukee,WI 53226414-771-0855 * Fax 414-77]-6570

Client: ^

Job ID: 3

Date Sampled:

Dale/Time Due:

Sajnple ID LocationyNamc Start Stop LPM Vol

feTteanqu.isb.ed by Date/Time Rece by DatoTime

Relinquished by Date/Time Received by Date/Time

Relinquished by Date/Time

Notes: Call Results #

Received By Date/Time

Fax#

Name/Pager #_ Other

FROM : Micro analytical FflX NO. : 4147716570 Jun. 09 2004 08=44flM P3

Micro Analytical, Inc.11521 West North Avenue

Milwaukee, Wl 53226414-771-0855 * Fax 414^771-6570

Client:

Job fc: ./tsj&/J4

Date Sampled.

Date/Time Due:

Sample ID Location/Name Start Stop LPM Vol

•{"»

n n

w

4*Recei'by Date/Time ved by Date/T'ime



Notes: Call Results #_

Name/Pager #_


Fax#

Other

.FROM : Micro Analytical FOX NO. : 4147716570 Jun. 09 2004 08:44RM P2

MICRO ANALYTICAL, INC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Fax: (414)771-6570



Job ID: Building 9 Clearance/


Analyst: Aaron Engelman

Sample ID

B9A-01

B9P-01

B9T-01

0.003 8.013:15 15:45

0 .002 9 .013:15 15:45

0.004 9 .013:15 15:45

Report ft 65300



Fibers/CC F/100 Fids Comments

Lpm 8.00 Ltrs 1200.0

Lpm 12.00 Ltrs 1800.0

Lpm 8.00 Ltrs 1200,0

LCD (Limit of Detection) policy of MicroAnalycical, Inc. is H.92F/«m2 of 7fbra/10Cfld«designated with a "<" Jign

AIHA 101057

FROM : Micro finalytical FflX NO. : 4147716570 May. 18 2004 09:44flM P4

MICRO ANALYTICAL, INC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Pax: (414)771-6570

O



Job ID: Building 9)Water / 7•»-«= . ^



Sample ID Fibere/CC F/1QQ Fids Comments

41704-01

Report ft 64885



41704-02

0.003 8.014:00 16:30

0.003 8.014:05 16:35

Lpm 8.00 Ltrs 1200.0

Lpm 8.00 Ltrs 1200.0

LOD (Limit of Detection) policy of Micrc&nalyClcal, Inc. is 8.SJP/mmJ or 7£br«/100fla»dcsignacad wich a "<" sign.

AIHA 101057

FROM : Micro final ytical FflX NO. : 4147716570 May. 18 2004 09:43flM P2

o,s P


c\



Job ID: Building 9 water

Sampled By: Shawn Christon


Report # 64887



Sample ID

040604-01

Fibers/CC

0.00308:00 11:00

F/100 Fids

12.0

Comment a

Lpm 10.00 Ltrg 1800.0

I£>D (Limit of Detection) policy of MicroAnalytical, Inc. is 8.92F/mm2 or 7£brg/loo£ldsdesignated with a "•=" 3ign.

AIHA 101057

FROM : Micro finalytical FfiX NO. : 4147716570 May. 18 2004 09:44flM P3

Micro Analytical, Inc.1)521 Wesl North Avenue

Milwaukee, WI53226414-771-0855 * Fax 414-771-6570

Client: M^ ^Tyt-T&J Dale Sampled: $ //0/0S

Job ID: &U''6/J,i/sf tf ^sfar /7 Date/Time Due:

Sample ID

•^j^jy-^/tfn&ti~0t*irtW.o^

Location/Name

C£t.JlrA*6s ^ &0e 7/

) * 11

Start

^2Zû

* % \Q&Pfa

2 -AJVu/*v

Stop

//'flO*.

tyffK

fytear^

///

LPM

/0*04? /*$Q /LX

to

Vol

.elinquished by Date/Time ived by Dais/Time




Name/Pager #^

Received By Dale/Time

Other

FROM : Micro finalytical

LAKb blATES INDUSTRI PAGE 02

FOX NO- : 4147716570 Feb. 23 2004 12:06R1 PI

MICRO ANALYTICAL, INC.11521 W. NORTH AVE.

AUKEkWj 53226(414)771-0855

FAX (414) 771-6570

Fax Transmittal

Date: L

To:

Company:

From:

Subject

FAX #-.

Comments:

Pages:

If you have any questions regarding this fax teansaction, please call (414) 771-0855.

TTiank-you.

ConTidoiuiilUy NoUcs; Unl«s Qlhsnvisc Ind^t^. UK iflfooMtkffl eeutined tn Ihls ftulmilt conmttniciiiMn ii eonridenGttliafomaUm intended fcr ut« of «b« taflvjflml noned above. If UK recipiam «f drin ftotimlle hw received II in error, you an berfcynotified ibii «y dineailnation or oopyinjof Oib ttOduiniaiieD is prohibited. If you hwe twolvod this ftasimlle In error, pleasedestroy it imnnaliaiejj. «ml notify the sender it the fhtrf number ibovo.

analytical

LAKE STATES INDUSTRI PAGE 83

FfW NO. : 4147716573 Feb. 23 2004 12:0SPM P2




Job ID: Building 12



Sample ID

B12-01

B12-02

212-03

0 ,003 8.013:15 15:20

<0.002 6.013:15 15:20

0.003 10.013:20 15:20

Report # 62962



Fibers/cc F/100 Flda commente

Lpm 12.00 Ltre 1500.0

Lpm 12.00 Ltrs 1500.0

Lpra 15.00 Ltra 1800.0

AIHA 101057

of Ine-

2U04 aa:bb 14146450645 LAKE STATES INDUSTRI PAGE 04

FOX KO • 4147716570 Feb. 23 2004 12:07Pfl P3: -Micro Analytical "W NU. • *i«rrn»r.o

Micro Analyticiljnc.11521 West North Avenue

Mil waukee,W) 53226414-771-0855 * Paa 414-771-6570

IcfolD; yfr,j'£0/'f4* /I— Date/Time Duet 2f1Cf0Y

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FROM : Micro ftnalyticalFflX NO. : 4147715570

Feb. 26 2004 04:52PM Pl_


MILWAUKEE, WI 53226(414)771-0855

FAX (414) 771-6570

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If.you have any questions regarding this fax transaction, please call (414) 771-0855.

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Confidentiality Notice: Unleu otherwiie indicated, the mfomittkm contained in this facsimile communication is confidentialInformation mtcoded for use of Die Individual named above. If the recipient of thi* facsimile ha received u in error, you are herbynodfiex) ftu my dissemination or copying of (his communication ii prohibited. If you have received tills facsimile in error, pleasedestroy it immediately and notify the sender at die phone number above.

FROM : 'Micro finalytical FflX NO. : 414771S570 Feb. 26 2004 04:53PM P3

Client:

Job ID: /9


Milwaukee, WI53226414-771-0855 * Fax 414-771-6570

. Date Sampled:

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FROM : Micro finalytical FPX NO. : 4147716570 Feb. 26 2004 04:52PM P2

MIClto ANALYTICAL, INC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Fax: (414)771-6570



Job ID: Bldg. 19


Analyst: Kevin

L2

Ul

Report # 63088



F/100 Flda

7.50.00315:00 17:00

<0.002 6.015:00 17:00

<0.002 3.515:00 17:00

Comments

Lpm 12.00 Ltrs 1440.0

Lpm 12.00 Ltrs 1440.0

Lpm 15.00 Ltrs 1800.0

LOD (Limit of Detection) policy of MiOroAnalytical, Inc. la a.SJP/imJ ot 7fbrB/100fIdsdeslgwted «ith » •«« sigrT

AIHA 101057

rprit-l ; I-1' r.ri.; final y t i ..;a ' FrV HO.


Lake States Industrial311 B Greenfield Ave.Milwaukee WI 53212


Job ID: Coke Oven Francis



Sample ID Fibers/CC F/1QO Fldg Comments

01

Report # 65872



02

<0.002 1.011:00 14:00

<0.002 1.011:00 14:00

Lpm 8.00 Ltrs 1440.0

Lpm 8.00 Ltrs 1440.0

LCD (Limit at Detection) policy o£ MicroAnalytical, inc. is 8.92r/ma or 7£bru/loo£ldadeaignacod with a "«• sign.

AIHA 101057

Client:

Job *


Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570

_ Date Sampled:

Date/Time Due: -J 0 -

Sample E) Location/Name Start Stop LPM Vol

J/As*

7, ff.^9

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Other


APPENDIX G-4

Asbestos Test ResultsPrior to Clearance



3- ^-o

.10 ANALYTICAL, INC.11521 West North AvenueMilwaukee, WI 53226 ''(800)771-9820 (414)771-0855Fax: (414)771-6570

Page 1 of 1

NVLAP 101247-0

BULK ASBESTOS ANALYTICAL REPORTUtilizing PLM and Dispersion Stain Technique


Report # 63439Name Building 3Received: 03/10/04Analyzed: 03/15/04Analyst Arthur_ -nekexIII

Sample ID: %Asbestos Description & Composition

MF1-01None Detected

Tan Compressed95% Ce 5% Pt MLM Tar

MFI-02None Detected


MFI-03None Detected


SP2-01

SP2-02

None Detected

None Detected

Off-White CompactTrace H 100% Gyp Pt MLM Qu Cal

Off-White CompactTrace H 100% Pt MLM Qu Cal

SP2-03None Detected

End of Report

Off-White CompactTrace H 100% Gyp Pt MLM Qu Cal

ry: Chrysotileos: Amositeoc-. Crbcidolite

-emoliteithophyllite

Fg: Fibrous GlassCe.- CelluloseSyn: Synthetic FiberH: HairSc: Silicate

Ver; Vermiculiteper: PerliteGyp: GypsumGs: Glass ShotPt: Participate

PL-M: Paint Like MaterialMLM: Mixed Limestone MaterialQu: QuartzCal: CalciteRs: Resinous MaterialDe.- Diatomaceous Earth

Test method: EPA/600/R-93/116. Quantitation is done by Calibrated Visual Estimation which has an acceptedRelative Percent Difference of 35. This report may not be used to claim product endorsement by NVLAP orany agency of the U.S. Government. This test report relates only to the items tested and shall not bereproduced except in full, without the written approval of Micro Analytical, Inc.

Client: /

Job ID:

# Samples:

Micro Analytical, Inc.

31521 West North AvenueMilwaukee, WI 53226

414-771-0855 * Fax 414-771-6570

Type: PCM PLM Lead TEM (circle one)

Sample ID Date Collected Location/Remarks

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,.eceived by Date/Time ' ' /Relinquished by Date/Time





Fax#

"Name/Pager #_ Other

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//

MICRO ANALYTICAL, INC.11521 VJest North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Fax: (414)771-6570



Job ID: Building 3



Sample ID

B3-01A

B3-01B

Report # 63763




2.0<0.00214:00 16:30

<0.002 5.014:00 16:30

Lpm 12.00 Ltrs 1800.0

Lpm 12.00 Ltrs 1800.0

LCD (Limit of Detection) policy of MicroAnalytical, Inc. is 8.92F/mra2 or 7fbrs/100fIdsdesignated with a "<" sign.

AIHA 101057


Milwaukee, WI 53226414-771-0855 * Fax 414-771-6570

Client:

Job ID: 3

Date Sampled:

Date/Time Due:





Notes: Call Results # Fax#


Name/Pager #_ Other

LAKE STATES INDUSTRI

NU. : 4147716570 Mar. 29 5904 04: 20PM P2

PAGE 02

•fffjMICRO ANALYTICAL, '/,INC.11521 West North AVenueMilwaukee, WI 53226(800)771-9920 (414)771-0855Pax: (414)771-6570

Page 1 of 1

NVLAP 101247-0


Lake States Industrial311 £ Greenfield Ave.Milwaukee WI 53212

Report # 63687Name Bldg 11 2nd floorReceived: 03/22/04Analyzed: 03/29/04Analyst Jon Yakiah

Description syCompoaitionSample ID:

Bll-1-01

Bll-2-01

None DetectedMulti Colored Woven60% Ce 40% Pt PL-M MLM Qu Cal

Black CompressedNone Detected 45% Ce 50% Pt MLM Qu Tar

5% H

End of Report

Affloil Amolicef-rao-Pitt;Tra*>.

AnchophylliteT««e ipuchodR»l« -

SC:

Plborcat*

v«xiPeri Mrlie*wn 915«B «hotPCi Partieuitte

nut:Outc«l i•«:De>

t*tee

M«con> K«e<iri*l

machad: fiS*/«9J/R-M/U<S. Quwieiwtioa 13 COB* by Culiteaeed Vllual Bttlnation «*ieh hu m lecepbod»™, jiX!U£'£?eK i *!°*35S2JL5- ~f' r°P?'t 'a^ »*«,»• "•« ea cl«i» product anacrsMwnt by RVI*| or^X,52S5S "L'*1* Vl3i 5P*»»5''i«t- JM* "»t «®att rtitten only to th« S»m» t«»tea WK» itail Soeb*reftroaoeeB «>W«BL «n full, wtctout che vrite«n «p?rov«l of Kioto Analytical, lea.

jo/ as:LAKE STATES INDUSTRI

Mar. 29 2004

PftGE 03

P3

Micro Analytical, Inc.1152! West North Avenue

Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570

Client: _

Job ID: //

Samples: ^ L* Type-. PCM Lead TEM (circle one)


* /

£foRelidquiahed by Dtte/Timt Received by Date/Time

Relinquished by Date/Time Racoived by Date/Time

Relinquished by Due/Time

Notes: • Call Results #_

Name/Pager #_


Fax#

OAer

FROM : Micro finalytical FflX NO. : 414771G570


ftpr. 14 2004 08:28m P2

- 1 £-0

LD / /



Job ID: Building 11 1st & 2nd Fir

Sampled By; Shawn Christen

Analyst-. Aaron Engelman

Sample ID

Bll-01

Bll-02

B11D-01

B11D-02

0 .002 8 .006:45 10:00

<0.002 6.006:50 10:00

0 .002 10.010:00 14:15

0 .002 8 .010:15 14:15

Report ft 64136




Lpm 12.00 Ltrs 2340.0

Lpm 10,00 Ltrs 1900.0

Lpm 12.00 Ltrs 3060.0

Lpm 10, nn. LtT£ 2400.0

WJD (Limit of Detection) policy of MicroAnalytlcal, Inc. i» S.SUF/inmi or 7fbr9/ioofldsd««ign«tcd wleft * •<• sign,

AIHA 101057

FRO!*! : Micro finalyticalFOX NO. : 4147716570 fipr. 14 2004 08:28ftM P3

Client:

Job ED: .


Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570

//

Date Sampled:L

Due:


h -

MO-ff I /u.

n - i >

Relinquished by Date/Time ived by Date/Time

Relinquished by Date/Time Received by Datc/Thne

Relinquished by DaiaTune


Name/Pager #_


Fax#_

Other

FROM : Micro Analytical FflX NO. 4147716570 ftpr. 19 2004 07:i9flM P2

MICRO ANALYTICAL, 'INC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Pax: (414)771-6570

Page 1 of 1

NVLAP 101247-0



Report # 64177Name Bldg 11 2nd FloorReceived: 04/12/04Analyzed: 04/18/04Analyst Jon Yakish

Sample ID; %A3beatos Description &/£omposition

01 Brown AssociatedNone Detected 70% Fg 30% Os Pt MLM Qu

Trace Ce

02 Brown AssociatedNone Detected 70% Fg 30% Gs Pt MLM Qu

Trace Ce


Trace Ce


Trace Ce


Trace Ce

End of Report

Chry: Chryaotila fg,Amog: Amosita Ca:Croci Crocidolite Syn;Act: JVC t lnoli te H:Tram i Tramalicp Sc:Antti: AnsJiophylliGe

Fibrous GlassCeUuJosuSynthetic FiberHair

Ver:

PC:

Vermtculte«PcrlitaGypaumQia»« Shoeparciculata

PL-M: Paint Like MaterialMLKi Mixed Linentone MaterialQu: QuartzGil

KoainouaDiatomaceoua Earth

Tcit methodRelative Percent' Difference o£ SsT" "This report may __ ___ _ _any agency of the U.S. Government. This teat roport"relace« only to the Item«~tested~and~sivi5:I riot bereproduces except in full, without the written approval of Micro Analytical. Inc.

Quantltation ii done Cy Calibrated visual Estimation vlUcti hag an acceptednot fle uaed to cl«i* product endorseoient by MVLAP or

FROM : Micro analytical FflX NO. : 4147716570 flpr. 19 2004 07:20flM P3

Client: .

Job ID: <$£

# Samples:


Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570

Type: PCM/fLM^ Lead TEM (circle one)


) >

"






Name/Pager #_ Other

ByANALYTICAL, INC.

11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-08557ax: (414)771-6570

Page 1 of 1

NVLAP 101247-0



Sample ID: %Asbestos

Report # 62267Name LSI.04.001Received: 01/14/04Analyzed: 01/16/04Analyst Arthur^ L Itarneke- III

^ t -Description & Composition

MFT-01None Detected

Multi Colored Linoleum5% Fg 75% Pt MLM Qu Cal Rs

20% Ce

MFT-02None Detected

Multi Colored Linoleum55% Ce 40% Pt MLM Qu Cal Rs5% H

End of Report

ChrysotileAmositeCrocidoliteActinolite

.:h: lophyllite

Fg: Fibrous GlassCe: CelluloseSyn: Synthetic FiberH: HairSc-. Silicate

Ver: VermiculicePer: PerliteGyp: GypsumGs: Glass ShoePt: Particulate

PL-M: Paint Like MaterialMLM: Mixed Limestone MaterialQu: Quartz

CalciteResinoug MaterialDiatomaceous Earth

Cal:

De :

Teat method: EPA/600/R-93/116. Quantitation is done by Calibrated Visual Estimation which has an acceptedRelative Percent Difference of 35. This report may not be used to claim product endorsement by NVLAP orany agency of the U.S. Government. This test report relates, only to the items tested and shall not bereproduced except in full, without the written approval of Mi-ero Analytical, Inc.

FROM : Micro finalytical FflX NO. '' : 4147716570 Jun. 02 2004 12:01PM P2


Page 1 of 1

NVLAP 101247-0



Sample ID: %Asbestp3

Report 4t 65198Name <^Bldg 12 Boiler Room;Received: 06;Analyzed-. 06/02/04Analyst Jon Yaki^h

Description a_ Composition

WPOl White LooseNone Detected .100% Pt MLM Qu

WPOl II Brown Compact7% Chry 93% Pt MLM Qu Cal

End of Report

hry;TOS:roc:

ChrysotileAroosiceCrocidoliteActlnpUteTreaoliteMithophyllite

TestRi 'Ji ny

Fg; Pibroue (JlasaCe: CulluloaeSyn; Synthetic FiberIT HairSc: 3ill.oace

Ver:Per:

VeruiicuiitePerlite

Claaa Shot

PL-H:MLM;

Si:Ra:De:

Paint; Like MaterialMixed HmestonB MaterialQuart!CalciteReainouB MaterialDiatotnaceoua Earth

except xifi full, without the written approval of Micro Analytical, Iflc,

FROM : Micro finalytioal FflX NO.. : 4147716570 Jun. 02 2004 12:01PM P3

Client: _

Job ID:

Sample ED


Milwaukee, WI 53266414-771-0855 * Fax 414-771-6570

/

# Samples: / Type: PCM /PU$/ Lead TEM (circle one)

Date CoUected Location/Remarks







Name/Pager #_


.Fax#_

Other

Micro finalytical FOX NG. : 4147716570 May. 24 2004 10:09PiM P2


Page 1 of 1

NVLAP 101247-0



Sample ID; %A3bestogL

Report #NameReceived:Analyzed:Analyst

Description y'/Compositjon

65024Building 12 Demo Debris05/24/0405/24/04Jon YaJcish

BD-D-01 Brown Compressed3% Chry 60% Fg 37% Gs Pt MLM Qu

Trace Amos Trace Ce

End of Report

Amos:Croc:ACt:

Trftm:With:

ChrysotileAmo»itecrocldoliteTreraonceAntnopnyllite

STSc:

Fibrous GlassCellules*Synthetic FiberHairSilicate

Ver; Vermiculite PL-M: Paint Like MaterialPer: Perlite MLM: Mixed Limestone MaterialGyp; Gypaum QU: QuarttCs; aiaoa Shoe Calj CalciteFt; participate RB: Resinous Material

De: Diatomaceous Earth

Teat method: EPA/600/R-93/116. QuantitdCion is done by Calibrated Visual Estimation which has an acceptedRelative Percent Difference of 35- This report may not be used co claim product en<lorH«n>ftnt by NVLAP orany agency of the U.S. Government. This teat report relates only to the items tested and shall not bereproduced except in full, without the written approval of Micro Analytical, Inc.

_£_ROM : Micro analytical FflX NO. : 4147716570 May. 24 2004 10:l0flM P3

Client:


Milwaukee, Wl 53266414-771-0855 * Fax 414-771-6570

Job ID:

# Samples: /_ Type: PCJ 1 Lead TEM (circle one)

Sample ID

#0-0-0'

Date Collected

s--2,c/^^

Location/Remarks

flu.' '&>' 'f^ />• O& fa 'j

l\ll





Name/Pager #_


Fax#

Other

FROM : Micro analyt ical FflX N O . - : 4147716570 Jun. 03 2004 0B:56ftM P2

MICRO ANALYTICAL, INC.11521 West North Avenue P&9e 1 of 1Milwaukee, WI 53226( 8 0 0 ) 7 7 1 - 9 8 2 0 (414)771-0855 NVLAP 101247-0

Fax: (414)771-6570


Lake States Industrial Report ft 65178311 E Greenfield Ave. Name Solvay CokeMilwaukee WI 53212 Received: 06/01/04

Analyzed: 06/03/04Analyst Arthur^L War:

,J S%Sample ID: %Asbestos Description & Composition

105 Tan Compressed50% Chry Trace Fg 50% Pt MLM Qu

Trace Ce

106 Multi Colored ResinousNone Detected 100% Pt MLM Qu Rs

End of Report

y. chrysoclle !*g: Fibrous Olasa Ver: vernioulitc PL-MI Paint Like Materiali: Amosite C«: cellulose Per: Perlite MLM: Mixed Limestone Material

Ctoc: Crocidolice Syn; Synthetic Fiber Gyp: Gypsum Qu; QuartzAce: Aciinolite H: Hiir GsT alasr. shot cal: Caicite

Treroolite Sc: Silicate Pt: Particulate S3; Resinous MaterialDe; Distonaceous Earth

Test method: EPA/600/R 93/116. OuantitaLion iu done by Calibrated Visual Eatlnution whicft Das an acceptedR«l*t;ve Percent Difference o£ 35. This report may not be used Co claim product endorsement by NVLAP or,_.. "y °t tie V-S. Governmant. This cest report relates only co the Item* tested and ahall not be

id except in full, without cho written approval of Micro Analytical, Inc.

FROM : Micro Analytical FflX NO... : 4147716570 Jun. 03 2004 08:56flM P3


Milwaukee, WI 53266414-771-0855 * Fax 414-771-6570

Client:

Job ID: SOL-JO**-*

# Samples: Type: Lead TEM (circle one)


o

tO w

Relinquished 6y Date/Time





Fax # 6

Name/Pager # Other

'FROM : Micro analyt ical FflX MC'. : 4147716570 Jan. 01 2004 01:53PM P2

MICRO ANALYTICAL, INC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Pax: (414)771-6570

Page 1 of 1

NVLAP 101247-0



Sample ID: %Asbeeto8

Report # 65169Name Bldg 12 DebrisReceived: 06/01/04Analyzed: 06/01/04Analyst Jon Yakish

Description WIComposition

BD-12-D01w

Brown Compressed65% Chry 35% Pt MLM Qu

End of Report

:r\ry: chrysotileunoi; Amosita"iocs Croeifloliteict; Actinolit*?rcm; Tremoliteinths Anthophyllite

Fg: Fibrous GlasaCo: CelluloseSyni Synthetic Fiberin Hairsc: silicate

ver: VermigulicePer: PerliteGyp: Gypsumsi- Olaaa ShotPt; Particulaue

PL-M: paint Like MaterialMLMi Mixed Limestone MaterialQu: QuartsCol; CalciceS.B: Resinous MaterialDe: Diatomacoous Earth

Teat meuhod: EPA/SOO/n-93/116. Quantitation is done by Calibrated Visual Estimation which has an acceptedRelative Percent Ditterenc* ot 3S. This report may not be unetf to claim product endorsement by NVLAP orany aaeney of the U.S. government- This teat report reiatca only to the itema tested and shall not bereproduced except in full, without the written approval of Micro Analytical, Inc.

'FROM : Micro analytical FAX NO'. : 4147716570 Jun. 01 2004 01:53PM P3

Client:

Job ID:

# Samples:

Micro Analytical, Inc.11521 West. North Avenue

Milwaukee, W! 53266414-771-0855 * Fax 414-771-6570

L

Type: PC; Lead TEM (circle one)


£>//

URelinquished by Date/Time received by Date/Time



Notes: Call Results # 4*/f/


Fax#

Name/Pager # Other

FROM : Micro analytical FflX NO. : 4147716570 flpr. 01 2004 04:36PM P2

1ICRO ANALYTICAL, Il&C..1521 West North Avenuelilwaukee, WI 53226;80Q)771-9820 (414) 771-085S'ax: (414)771-6570

Page 1 of 1

NVLAP 101247-0

BULK ASBESTOS ANALYTICAL REPORTUtilizing PT,M and Dispersion Stain Technique


Sample ID; %AabestO3

Report # 63901 Ack/09Name Bldg 12 arklng ftbove BoilerReceived: 04/01/04Analyzed: 04/01/04Analyst Kevin Hachey

Description & Composition

B12-01 Gray Compressed7% Chry 40% Ce 53% Gs Pt MLM Qu

End of Report

•hry:mot:Toe-ctiTom i

ChrysotU*Anodtecrocidolit«AceinoUUTrtmolit*

8T

Pibroua GlassCellulose

ntn: Anchophyllite

Teat methodi

Hairslllc*e»

V«r: varraisulitePer: Perlite

Pt!Glaae ShotPnrttculaeo

Pi-Hi Paine Like Materialm»-. Mima Umeetone Material

C»ii C*fciteKBi Reainoua MaterialM: Piatoinaceoua Sarch

ti BPVSOO/t-Sl/niS. guantitation is don* by Cnlibratod Vi«u»l Bitiiwtion which ha* an acceptedRelative Percent Ditierenee of 35. Tha« report way not be used to claim product endorsement by MVtAPorAny agtncy of th« U.S. Qovernment. This test report relate* oniy to the Ite«a tinted and ahali not Der«proauc«a eneept in full, without the written approval of Micro Analytical, Inc.

FROM : Micro finalytical FflX NO. : 4147716570 flpr. 01 2004 04:36PM P3

Client: _

Job ID:

# Samples:


Milwaukee, WI 53226414-771-0855 * Fax 414-771-6570

Type: PCM Lead TEM (circle one)







Name/Pager #_ Other

FROM : Micro finalytical FHX HO. : 4147716570 May. 13 2004 02:-"47PI'I P2•)=t' A

S//7"1 ' I


Page 1 of 1

NVLAP 101247-0



Sample ID;

B12-01A

Report # 64801Name Bldg. 12Received: 05/13/04Analyzed: 05/13/04Analyst ilon Yakisl

-Description &/Composition

None DetectedBlack Resinous35% Ce 60% Pt MLM Qu Cal Tar5% H

B12-01B Black Resinous3% Chry 27% Ce 67% Pt MLM Qu Cal Tar

3% H

End of Report

Chry:AmoiiCTOC-.Act iTram:iiith;

ChrysocileAraositecrocidoliteAcunoliteTroraolit*Anchoyihynice

?g: FibrousSyn: Synthatic FiberH: Hair

Ver;Par.Gyp:GilPC:

ParliceCypsumGlaoa ShoePurciculat*

PL-M; Paint Like MaterialMUV. nixed Liwtsnotie Material

Si "RS;

Calcit*Resinous MaterialDiatoiMccoua Earth

Teat methodi EPA/SOO/R-33/ll*. Quancitaeion is dore by Calibrated Visual Estimation which has an acceptfielacive Percent Difference of 35. This report may not be uaerd to olaim product endorsement by SVUip nany agency of the U.S, Government. Tnla csat reporc relates <>nly to che items beacad and ahall nor bersfroducea sxcept in full, uisnout the written approval of Mic:ro Analycisal. inc.

FROM : Micro finalytical FOX 110. : 4147716570 I'lay. 13 2004 32:47PH P:

Micro Analytical, lac.11521 West North Avenue

Milwaukee, WJ 53226414-771-0855 * Fax 414-771-6570

Client:

Job ID:


Sample ID

jf/j &>/•**+

&/ t

Date Collected

.r jJ-0'/

1 J

Location/Remarks

# £,*n/ srWl.^'*.,.

<l

/ 1) A^^c 7 /^^ j-~ >}-*>/ //LJ^LJL <*•>Relinquished by Date/Time Received by Date/Time




Name/Pager #_


Other

FROM : Micro analytical FflX NO. : 4147716570 flpr. 30 2004 07:47fiM P2

MICRO ANALYTICAL, TNC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 {414)771-0855Fax: (414)771-6570

"* 1-

Page 1 of 1

NVLAP 101247-0



Sample ID; %Asbestos

Report # 64540Name B12 - Building 12 WindowReceived: 04/26/04Analyzed; 04/30/04Analyst Kevin Hach«


OlA

01B

01C

01D

01E

02A

Trace Chry

Trace Chry

Trace Chry

Trace Chry

Trace Chry

3% Chry

Off-White Compact100% Pt PL-M MLM Qu Gal

Off-white Compact100% Pt PL-M MLM QU Gal

Off-White Compact100% Pt PL-M MLM Qu Cal

Off-White Compact100% Pt PL-M MLM QU Cal

Off-white Compact100% Pt PL-M MLM Qu Cal

Tan Compact97% Pt PL-M MLM Qu Cal

End of Report

Chry: ChrysotileAmos: AmositcCroc: CrocidoliteAct: ActinollteTrera: TrsaoliteAnth: Anthophyllite

Kg: Fibrous GlassCei CelluloseSyn: Synthetic FiberH' HiirSC: Silicate

Ver: VermicuUtePer; ParllCeGyp; GypsumGiT glSas ShotPt; Particulars

PL-M: Paint UX« MaterialMLHi Mixed Limestone MaterialOut QuartzCal: CaletteRs: Resinous MaterialDe: Diatomaceoug Earth

Test method: 8PA/<00/R-S3/11S. guantitation is done by Calibrated visual Estimation which has an acceptedRelative Percent Difference of 35. This report may not be used to claim product endorsement by tfVLM> orany agency or the U.S. Goverament. This teat report relates only to the items tested and shall not bereproduced except in Cull, without the written approval of Micro Analytical, Inc.

FROM : Micro flnalytical FfiX NO. : 4147716570 fipr. 30 2004 07:48fiM P3

Client:

Job ID:

# Samples:

Mi I'iu Analytical, Inc.11521 Wcsl North Avenue

Milwaukee, WI 53226414-771-0855 * Fax 414-771-6570



A-

C,

Relinquished by Date/Time Received by Date/tinidT





Fax#

Name/Pager #_ Other

FROM : Nicro Analytical FflX NO. : 4147716570 May. 19 2004 01:48PM P2

ICRO ANALYTICAL, INC.1521 West North Avenueilwciukee, WI 53226800)771-9820 (414)771-0855

'ax: (414)771-6570

Page 1 of 1

NVLAf 10J.217-0



Sample ID; %Asbe3tos

Report # 64923Name Bid, 12 - DebrisReceived: OS/19/04Analyzed: 05/19/04Analyst Jon Yakish.

Description tt/Composition

B12-BB-01 Tan CompactNone Detected 100% Pt MLM Qu Cal

B12-BB-02 Gray Compressed25% Chry 75% Pt MLM Qu Cal

End of Report

chry: Chrysotils po:Ann,;,.. ftmosiee CO:Croc; crooidolitiB Syn,ACt: Ju.-tlno.lit* H:Tr»ra: Tremolite 3c.Ancni Anthophylliee

fibrous classCslluloicSynthetic FiberHiirSilicate

vanPer:

Pt;

VenoiculicaPerliteOypsumGlass ShoeParticuiace

PL-H-, Paine Llk* MaterialMixed Limestone MaterialQuart*calciteResinous MaterialPiatojnaceoua Barch

QU;CaiHa,Da:

Teflt nethoO: EPA/600/R-93/H6. CmanCitstion is done by Calibrated Visual EatiirAtion which has an acceptRelative Perccrtt Dlffarancc of 35. This report may not be uflecl to claim pcoduct andorscmcnt by XVLXP oany agency of rbs U.S. Oovernment. This test report relates only to the Icema tested and shall r.ot bereproduces excepc in full, wiCJWut cho written approval of Micro Analytical, Inc.

FROM : Micro finalytical FfiX NO. : 4147716570 May. 19 2004 01:49PM P3

Micro Analytical, Tnc.11521 Wesl North Avenue

Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570

Client:.

Job ID:

# Samples: z.-

Type: Lead TEM (circle one)

Sample ID

/?/jL-^-^

// // -& Z

Date Collected

S- /f, o //

) /

Location/Remarks

<?/• <PafT fj*/7~

/s> s> ij

ITeliitfjuidTed by' Dale/Time

Relinquished by Date/Tinie Received by Date/Time



Name/Pager #


Fax#_

Other

FROM : Micro flnalytical FRX NO. : 4147716570 May. 18 2004 01:21PM P2


Page 1 of 1

NVLAP 101247-0


Lake States Industrial311 E Greenfield Ave,Milwaukee WI 53212

Sample ID: %Asbestos

Report # 64872Name MSCGReceived: 05/17/04Analysed: 05/18/04Analyst Jon Yakish

Description ^/Composition

BLD-12-01DNone Detected

Multi Colored Loose100% Gyp Pt MLM Qu

End of Report

cnry»otil«Aniosite

Croc: CrociooliccActinolie*Yrtroolit*Anttwphylllto

. •Trem;\nth;

Syn:H:Sc;

Fibrous Glasscellulose

Fiber

versPer-.

Silicate

VermioulitePerliteGypauinOlaas shoe

PL-Mi paint LiX« MaterialKLK: Mixed Limestone Material

Sa: Raainous MaterialDe: Diacomaceous

reproaucea except in full, without the written approval of Micro Analytical, Inc.

FROM : Micro finalytical FflX NO. : 4147716570 May. 18 2004 01:21PM P3

Client:

Job ID:


Milwaukee, Wl 53226414-771-0855 * Fax 4 14-77 1-6570

<

SI

# Samples: /_ Type: PCM Lead TEM (circle one)


Date/Time Received by Dateyiime




Name/Pager #_


Fax#

Other

FROM : Micro analyt ical FflX NO. : 4147716570 flay. 13 2004 01:29PM P2

1ICRO ANALYTICAL, INC..1521 West North Avenue Page 1 of 1lilwaukee, WI 53226(800)771-9820 (414)771-0855 NVLAP 101247-07ax: (414)771-6570


Lake States Industrial Report # 64805311 E Greenfield Ave. Name Building 12Milwaukee WI 53212 Received: 05/13/04

Analyzed: 05/13/04Analyst Jon Yakish

Sample ID; %A3bestoa Description

PB-01 Off-White CompactNone Detected 3% Ce 97% Gyp Pt MLM Qu Cal

End of Report

C!«yi chrysotile Fo,: fibrous Olasa Vcrs Vermiculite PL-M: Paint LiJte MaterialAmos. Amosite Ce: Cellulose Per-, Perlite HTM-. Mired Limestone MaterialCroci Crocidolite Syn.- Synthetic fiber Gyp: Oypauin Qu; Quart*Act; Actinome HF J»ir CS: GlSas Shoe Cai: calcite•ircm: Ttc.molite Sc: Silicata Pt: Particulate as: Resinous Materialtoch: Anthophyllic* De: Diatonaceous Sarth

T»»t msthod! EPA/eog/R-SJ/ilfi. Quantitation is done by Calibrated visual Estimation which has an jr,,,,,,™Relative Percent Difference of 35. This report may not be used to claim product endorsement; by NVLAP'oranvr 3*nei( thJ V'si 9?vcrrtitrf!Ht. This teat report relates only to tho items tested and shall not bereproduced «xc«pt in. full, »xtheut the writcnn .-ipproval o£ Micro Analytical, inc.

FROM : Micro analytical FflX NO. : 4147716570 May. 13 2004 01:30PM P3

Client:

Job ID:

# Samples:


Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570






Notes; Call Results #


Fax#

Name/Pager #_ Other

FROM : Micro fralytlcal FflX NO. 4147716570 Nay. 13 2004 02M7PH P2


Page 1 of 1

NVLAP 101247-0



Sample ID: feAsbestos

Report # 64801Name Bldg. 12Received: 05/13/04Analyzed: 05/13/04Analyst


B12-01ANone Detected

Black Resinous35% Ce 60% Pt MLM Qu Cal Tar5% H

B12-01B Black Resinous3% Chry 27% Ce 67% Pt MLM Qu Cal Tar

3% H

End of Report

Chry: ciirysocileAmoai hmositeCroc; CrocidoliteAct: AccinoliteTre«: Tromolic*• - - h i Anthophyllice

Fg: Fibrous siaua Vcr; vermiculiteCei Cellulose Pen PorliteSyn: Synch«cic Fiber Gyp: GypsumH-. Hair 33 •, Glaa? ShoeSc: Silicace Pt: Particulate

PL-N:MLHiQu:Cal:RB;De.-

Point LikeMixed Limestone Matsrlal

Re-iirtoui MaterialDiitoirucGoua Earth

any agencyreproduces except

titition is done by Calibrated Visual Estimation which fta* an acceptedt may not be us«d to claim product endorsement by NVLAP or

, . report relates <>nly to che items tested and shall not ben £ull, witnout the written approval o£ Mivro Analytical, Inc.

method; EPA/600/R- 93/116. Ouantitition is done by Calibrated Visual Estimation which fta* aKelative percent Difference of 35, This report may not be us«d to claim product endorsement by

of the TJ.S, Government. ThiB test report relates <>nly to che items tested and shallin

FROM : Micro finalytical FflX NO. : 4147716570 May. 13 2004 02:47PM P3


Milwaukee, WJ 53226414-771-0855 * Fax 414-771-6570

Client: ZA*^ STAffA "2-y!/

Job ID: /fo/?<5 /2.i_ /•

# Samples: 2^-

Sample ID

JT/V- - &/'-*+

Date Collected

j jj-jt/

i J

Type: PCM PLM Lead TEM (circle oae)

Location/Remarks

&##?/• /'WfK'j.t

'I

/

*>2^ 7 /^-t^, J~~ - / /^^fl i

(/ j J.O


0Relinquished by Date/Time Received by Date/Time

Relinquished by Date/Time Received By Date/Time

Notes: Call Results # Fax #

Name/Pager # Other

FROM : Micro analyt ical FfiX NO. 4147716570 May. 20 2004 02:36PM P2

vlICRO ANALYTICAL, INC.11521 West North AvenueMilwaukee, WI 53226(800)771-9820 (414)771-0855Fax: (414)771-6570

Page 1 of 1

NVLAP 101247-0



Report # 64958Name Building 12 PackingReceived: 05/20/04Analyzed: 05/20/04Analyst Jon Yakish

Sample ID: %Asbesto3 Description & Composition

B12-PK-01 Gray Compressed7% Chry 63% Fg 30% Gs Pt MLM Qu

Trace Ce

End of Report

Chry.AmoS:Croc:Act:Trem:Anth-

CHrysotU*AmositeCrocidolitcActinglitaTremolitcAnthOpnyllite

Fg; Fibrous Glass Var:C<: Cellulose Per:Syn: Synthetic Fiber Gyp:Tf, Hiir GITSc: Silicate Pt;

VermiculitePerliteGypGuitlGlaaa ShotParticular

PL-M: Paine LIKe MaterialK3M-. Mixed Limestone MaterialOUT QuartzCal: CmlciteS.B; Reeinou?) MaterialDC: DiacomaceouB Earth

Teat method: EPA/SOO/R-93/116. QuantitadoD la done by Calibroted Visual Estimation whicft haa an acceptedRelative Percent DiCterencs of 35. This report may not be usEid to claim product endorsement by NVLAP orany agency ot the U.S. Government. This test report related only to the itemi tested and shall not beproducedrepr

..except in full, without the written approval of Micro Analytical, loo.

FROM : Micro Rnalytical FflX NO. : 4147716570 May. 20 2004 02:37PM P3

Client:


Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570

Job ID:

# Samples: / Type: PCM /PLM/ Lead TEM (circle one)

Sample ID

*/*-/%-<?/

c-^2X/^>

Date Collected

6T" 2*0 -fity

- r-**~ov

v—-Location/Remarks

/3fx->^ *„**** Si-x

/)

/I// / /

IW «Wralinquidiedby DatftTime Received by Date/Time




Name/Pager #_


Fax#

Other

12/29/2003 MON 08:20 FAI 12622428554 Em ASSOC.

toon [ZiTS OK XS/Xil "'ST aflL COOZ/CZ/ZT

El 002

/yENVIRONMENTAL HAZARDS 8ERVICESLL.L-C.

7499 WHITE PINE ROAD - KICHMONP, VA804-275>4788 PAX 804-273-4907

BULK ASBESTOS SAMPLE ANALYSIS SUMMARY

DATE OF RECEIPT: 22 DEC 2003P.O. Box 136TbierwviH«,WI 53092

DATE OF ANALYSIS: 23 DEC 2003DATE OP REPORT: 23 DEC 2003

CLIENT NUMBER: 51-1899 DEHS PROJECT ft 12-03-2412PROJECT: 03-06855

EHSSAMPLE*

01

02

03

04 .

05

06

07

08

09

10

11

12

13

CLIENT SAMPLE 1ULABORATORY GROSS DESCRIPTION

87/Black GramUar-Uke

38/Black Granular-Lake

39/

407Black Granular-lake

417Black Granular-Like

42/Black Granular-take

437Black Granular-Like

44/

45/Black Granular-Like

Black Granular-lake

47/Black Graaular-Lika

48/Black Granular.Like

49/

* ASBESTOS

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

Trace, <1% Chrysotile

OTHER MATERIALS

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibroua

100% Non-FibrousBlack Granular-tike <1% Total Asbestos

~ PAGE 01 Of 03-

SH3:QI

12/29/2003 MON 08:21 FAI 12622426554 ENV ASSOC.

J0o® tziia ON ra/ixl t^si am COOZ/CZ/ZT

ENVIRONMENTAL HAZARDS SERVICES, L.L.C,CLIENT NUMBER: fil-1899 D£M3 PROJECT ft 18-03-2412PROJECT: 03-06865

EHS CUENT SAMPLE* % ASBESTOS

@1003

Black GranuJar-Ltke; Silver Paint-Like

OTHER MATERIALSawiri-sff

14

15

16

17

IB

19

20

21

28

23

24

25

26

27

28

29

SO/Black Granular-Uke

51/Black GranuUr-Like

Bkck Granular-Like



Black/Btowti Powder; Silver Foil-Like

Black Granular-Like

*

Black Grauiulflr-Like

sLkGranulatê


60/Black Graoular-Like


62/Black Powder-like

661Black Gtantilat'Like

64/Black Granulat-Like

65/

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

100% Non-Fibroua

100% Non-Fibtoua

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Nro-Fibroua

100% Non-Fibrous

100% Non-Fibroua

100% Non-Fibroua

100% Non- Fibrous

100% Noa-Fibroua

100% Non-Fibroua

100% Noa-FibroUB

100% Non-Fibrous

100% Non-Fibrous

100% Nott-Fibrous

~ PAGE 02 of 03-

SH3:QI £0,

12/29/2003 MON 08:21 FAI 12622428554 ENV ASSOC.

COO® IZiTS ON IH/tLJ V^9t 301

ENVIRONMENTAL HAZARDS SERVICES, L.L.C.CUENT NUMBER: 51-1899 DEH3 PROJECT fc 12-03-2412PROJECT: 08-06855

QC SAMPLE: M2-1996-2

QC BLANK: SRM 1866

REPORTING LIMIT: 194 Asbestos

METHOD: Polarized Light Microscopy, EPA Method 600/R-93/116'

ANALYST: Laura Holder

Reviewed By Authorized Signatory;Soward Vartter, laboratory DtnetorIrmo. fwtwtki, Quality AwtiMwu* CoordinatorDavid Xv. US, Senior GamutFeng Jiang, MS, Stniof GtologittMichael A MtcUer, Quality Attunttux Manager

Results, represent the analysis of samples submitted by the client Sample location, description, area, volume, etc., was provided bythe client This report cannot be used by the client to data product endorsement by NVLAP or arty agency of tha U.S. GovernmentThfe report shan,not be reproduced except In fud. without the written consent of Environmental Hazards Services, LJ-.C. CaMbmiaCertification #2319 NY ELAP #11714. All Infbrrhatton concerning sampling location, date, and time can be found on Chain*)*-Custody. Environmental Hazards Services, L.LC. does not perform any sample coHecDon.

Environmental Hazards Services, LLC. recommends reanatysls by point count (for more accurate quanUflcatton) or TransmissionElectron Microscopy (TEM), tor enhanced detection eapablMe«) for materials regulated try the SPA NESHAP (National EmissionStandards for Hazardous Air PoKutanb) and found to contain less than ten percent (<10%) asbestos by polarized light microscopy(PLM). Both services are available for an additional fee.

* All CalHbmla samples analyzed by Polarized Ught Microscopy, EPA Method 600/MM2-02Q. Dec. 1982.

LEGEND NAD a no asbestos defected " ~

phn1-doU07JAN2002f kh- PAGE 03 at 03 - END OP REPORT -

$0, 8S/3T9 /£ ""

tooo

-4ro

oo

DK

EHS 12-03-2412 ENVIRONMENTAL HAZARDS SERVICES. LLC.7469 Whilapirw Road Richmond, Vbybda.23237 Phono (804) 27W 789 Fax (B04) 276-4807

CHAIN OF CUSTODY FORM f * f >

Si

toO

ao

OO01

ENVIRONMENTAL HAZARDS SERVICES, L.LC.l,Vi

CHAIN OF... ->

3- °T ->

Company Nun*Contact N*a>Sampler Name:Anttfacf*

OttnrMetalsl Indoor

SampleDale 4Time

ORWipe AIM (R2)

ORSampleNumber Comnwus

Oowpoaagnptes aubmiBeo meet AS7W E1792Raieasedfay:Received by: V

Received by:// .. VIMSA A / *

^ o

V

eou

3

ENVIRONMENTAL . >*ZARDS SERVICES, L.L.C. ,7469 Whllapins Hoed Richmond Virginia 23237 Wwne (004) 27&4H6 Fax (604) 27S4907 ^ <s1 T

CHAIN OF CUSTODY FORM l

Cfly, Stole, Zfe:

EWSCtftniAccewt/flt.

Pfwmtf

P.ttft

SampleNumber

SampleOata&Tbite

Asbestos Lead

r Do wipe samples sufafpffiad meet ASTM £1792 faquiranients? YinI I

Other ftfetirtfi IndoorAirQuallfa

8

PuBodate Total WnutWOfHllSoq) QQ

Air Volume (L)OR

OR .fierce x

Comments

TI ^

m i>

Ols

OIsIs

ocS

FIL£ No.774 12/24 '03 10:20 ID: FflX:141002

PfiGE I/ 3

CLIENT:

ENVtRONMENTAL HAZARDS SERVICES, L.L.C.wnrr i ROAD - R n D ,

804-270-4788 FAX 804475-4907


Environmental AssociatesP.O. Box 136Xhiensvffle, WI 53092

DATE OF RECEIPT: 23 DEC 2003DATE OP ANALYSIS: 24 DEC 2003DATE OF REPORT: 24 DEC 200$

CLIENT NUMBER;EH3 PROJECT*PROJECT:

61-1899 D12-03-261603-06855

EHS CLIENT SAMPLE*/SAMPLE * LABORATORY GROSS DESCRIPTION

% ASBESTOS OTHER MATERIALS

01

02

03

04

06

lfc-22-VYellow Fib.; Black Tar-Uke

12-22-2/Black Tar-Like

12-22-2/White B!b.

12-22-4/Black Brittle

12-23-5/B)aok Fib.

12-22-6/Green Brittle Fib,

10%Total Asbestos

Cbtyeotile10% Total Asbestos

20%Amosite20% Total Asbestos

NAD

15% Total Asbestos

NAD

50% Fibrous Glass40%

90% Non-Fibrous

85% Nou-Fibrous

45% Fibrous Glass59% Non-Fibrous

QC SAMPLE:

QC BLANK:

REPORTING LIMIT:

METHOD:

ANALYST:

M2-1998-2

SRM

1% Asbestos

Polarized Light Microscopy, EPA Method 60Q/R-93/116

Katby Bisemore

Rervlewad By Authorized Signatory:Howard Vdmer, Laboratory DtnctorIrna RuaewM. QuatHy 4wwr<wic« CoordinatorDaaidXU, 413, Senior ChemistAw Jiang, US. Senior GeologistJMduulA. MuelUr,

- PAGE 01 of 02-

12/24/ZOO.1) WED 09:31 [TX/RI NO 5173] H001

fflUlN 10:43 *Ai 12622426554 ENV ASSOC. @003FILE No.774 12/24 '03 10:21 ID: FAX: RflGE 2/ 3

ENVIRONMENTAL HAZARDS SERVICES, L.L.C.CLIENT NUMBER: 61-1899 DIH3 PROJECT*: 12-08-2616

PROJECT: OS-06855

ReeuRB represent the analysis of samples submitted by ttw ottwit Sample location, description, area, valuriw, ate., was prevMed bythe dtant This report cannot be used by <ht client to cWm product nndorsement by NVUAP or any «g«ncy of tha U.S. GovernmentThiB report <hafl not ba reproduced except in fuH. without the written consent of Environmental Hazards Servicea, L.LC. CafifamiaCerWcatton #2319 NY ELAP f1l714. AU informaUon concerning «ampHn0 location, data, and fime can be found onCustody. Environmental Hazardi Service*, LL.C. does not perform any sample collection.

Hazards Setvices, U_c. recommends naanalysh by point count (fcr more accurate quanWkatfon) or TransmissionElection Microscopy (TEM), for enhanced detection capablflOes) for materials regulafed by the EPA NESHAP (Nafiooal EmissionStandard* for Hazanioue Air Pollutants) and found tt contain ten than ten percent (<10%) asbestos by polarized light microscopy(PLM). SocnseMcee are available for an additional foe.

• All CaSfomfa samples analyzed by Polarized light Microscopy, EPA Method 600/M4-82-020, Dec. 1982.

SCF » suspected ceramic fibersplm1.doM}7JAN2002/ MR

- PAGE 02 of 02 - END OF REPORT -

12/24/2003 WED 00:31 [TI/RX NO 6173] @OQ2

ENVIRONMENTAL HAZARDS SERVICES, L.LC.Id Richmond, Wfibfe 23237 Ph*» (SW) 2754788 Pw (604)276-4807

EHS 12-03*616 CHAM OF CUSTODY FORMK

i «

toOo

o

«J

§enH-aCJ

submitted meat ASTM E17S2 requJremants? Yes

HL£ No.130 12/31 '03 15=56 ID:PfiGE I/ 6

ENVIRONMENTAL HAZARDS SERVICES, L.L.C.7469 WHITE PINE ROAD • RICHMOND, VA 23237 ,

804-275-4788 FAX 804-275-4907 -=ff .

ASBESTOS SOIL ANALYSIS SUMMARY ^^ .r* ^ '. f *

CLIENT: Environmental AssociatesP.O. Box 136ThiensvUle, WI 53092

CLIENT NUMBER: 51-1899 DEHS PROJECT #: 12-03-3236PROJECT: 03-03855

EHS SAMPLE * CLIENT SAMPLE *

01 67

02 69

03 70

04 71

05 72

06 73

07 74

08 75

09 76

10 77

11 78

12 79

13 80

14 81

15 82

\ ' \

DATE OP RECEIPT: 31 DEC 2003DATE OF ANALYSIS: 31 DEC 2003DATE OF REPORT: 31 DEC 2003

G (iQ»£> U N' D £/*-> ''i Lii. A~ '-< N t—r> )70 w £(*•*> .

ASBESTOS DETECTED

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

•/ fit

-PAGE 01 of 02-

MLb No. 1 '03

ENVIRONMENTAL HAZARDS SERVICES, L.L.C.CLIENT NUMBER: 51-1899 DEHS PROJECT*: 12-03-3236PROJECT: 03-03855

METHOD:

ANALYST:

Polarized Light Microscopy

Melissa Boggs Steituger

Reviewed By Authorized Signatory:.award Varntr, Laboratory Director

Irma Faszewski, Quality Assurance CoordinatorDavid Xu, MS, Senior ChemistPeng Jiang, US, Senior GeologistMichael A. Mueller. Quality Afsuranot Manager

Result* represent the analysis of samples submitted by the client Sample location, description, area, volume, etc., was provided bythe client This report cannot be used by the client to dalm product endorsement by NVLAP or any agency of the U.S. GovernmentThis report shall not be reproduced except in futt without the written consent of Environmental Hazards Services, LL.C. CaliforniaCertification #2319 NYJELAP#11714

LEGEND NAD = no asbestos detectedAD = asbestos detected

asbwipe1.dot/07JAN2002/kh- PAGE 02 of 02 - END OP REPORT -

^\.

?UVV

b>_- *RDS SERVICES, L.LC.74 - f, VligWa23237 Phone (804)275^788 Fax <a04) 275-4907

EHS 12-03-3236 J OF CUSTODY FORM

-n

Company Name;. Hate: )2.-3c>'3

Crty.S*****Zfc.

Contact Name: _

m$ampterNamK.

EHS Cilvtt Account*

Pfr«w#:

P.O. ft:

SampleNumber Oate&

Time

Asbestos

m

o

Lead

n

.i§

Other MetalslaMtJMmM bdo

indoorAir Quality

M S m

Parikadata: Total Nubanoe (NIOSH 0600) fl

Air Volume (L)OR

Wipe Area (ft2)OR

ScrapeAreefcm2)

Comments

nooo

8

LS~

IS"

77 A/

rrJ.

" Do wipe meat ASTM E;792requfnemenls? Yes No ?Released fay: Signature: Oatamme:Received by: Signature: Date/Time:Released Signature: Date/Time:Received Signature:

ENVIRONMENTAL Hfu^RDS SERVICES. L.LC.7469 Whttapina Road Richmond, Virginia 23237 Phone (804) 275-4766 Fax (604) 275-4907

CHAIN OF CUSTODY FORM

Company that*:

Adftrvsr:

EMS Client Account Ik (

Phooe*:

P.O. #:

Fax*

-8

01

SampleNumber

SampleDate&Time

Asbestos

a

Lead

J1

Other Metala

rjWo^

CO

<£C

indoorAirQuaHty

Partcuteto: Total NuUuca (HtOSH 0600} Q

D

mJOT o> £

Air Volume (L)OR

W|pe Area (ft2)OR

Scrape

Comments

S.

«•

* Do wipe samples submitted meet ASTM £1792 requirements? Yes No

Released by: Signature: Date/Time: sReceived by: Signature: Date/Time:Released by: Signature: Date/Time:Received by: Sionalure: Date/Time: V*

FILE No. 130 12/31 '03 15:57 ID1-FAX: PAGE 5/ 6

CLIENT;

ENVIRONMENTAL HAZARDS SERVICES, L.L.C.ROAD- RICHMOND, VA23Z37

804-275-4788 FAX 804-275-4807


Environmental AssociatesP.O. Box 186Thiensville, WI53092

DATE OF RECEIPT: 31 DEC 2003DATE OF ANALYSIS: 31 DEC 2003DATE OF REPORT: 31 DEC 2003

CLIENT NUMBER:EHS PROJECT*:PROJECT:

EHS

01

02

51-1899 D12-03-326203-03855

CLIENT SAMPLE #/

66/Tan Gran.

68/Tan Gran.

ASBESTOSDON

OTHER MATERIALS

NAD

NAD

100% Non-Fibrous

100% Non-Fibrous

QC SAMPLE:

QC BLANK:

REPORTING LIMFT:

METHOD:

ANALYST:

Ml-1999-1

SKM 1866 Fiberglass

1% Asbestos

Polarised Light Microscopy, EPA Method 600/R-93/116

Melissa Boggs Steiniger

Reviewed By Authorized Signatory;.Howard Varna-, Laboratory DirectorIrma Posznotki, Quality Assurance CoordinatorDavid Xu. MS, Senior ChemiftFeng Jiang, MS. Senior GeologistAtichatl A. Mutlter, Quality Assurance Manager

Results represent th» analysis of samples submitted by the client Sample location, description, area, volume, etc., was provided bythe client This report cannot be used by the client to claim product endorsement by NVLAP or any agency of the U.S. Government.This report shaH not be reproduced except In full, without the written consent of Environmental Hazards Services, L.L.C. CaliforniaCertification #2319 NY ELAP #1 1714. All Information concerning sampling location, date, and time can be found on Chain-of-Custody. Environmental Hazards Services, LLC. does not perform any sample collection.

Environmental Hazards Services, LUC. recommends reanarysis by point count (tor more accurate quantification) or TransmissionElectron Microscopy fTEM). for enhanced defection capabilities) for materials regulated by the EPA NESHAP (National EmissionStandards for Hazardous Air Pollutants) and found to contain less than ten percent (<10%) asbestos by polarized light microscopy(PLM). Both services are available for an additional fee.

* AH California samples analyzed by Polarized Light Microscopy, EPA Method 600/M442-020, Dec. 1982.

LEGEND NAD -no asbestos detected ~" ~~ "~ "" '_ _ SCF" susoected ceramic fibersAl.dot/D7JAN2002/kh


Coatpaty Nativ _\ 0.

SERVICES. U..C.74 I. VkgWa 23237 Phone (804) Z7W788 Fax (804) 275-4907

EHS 12-03,3262 j QF CUSTODY FORM L

SampleNumber

SampleOale&Time

\-Do wipe

Asbestos

meetASTME;

eleased by:ecawadby:

ReleasedReceived

Lead OttterMetats

792 requirements? YesL. No

IndoorAir Quality

!m

PMUcubte: Total NubanoapNOSHasOl*

RMfdraUctWOSHOeOO)

Air Volume (L)OR

WêAreafft2)OR

Scrape ••Area(cm2

A/.

Comments

A sw.fcifl

JtiT

Signature: / -X-Signature:Signature:Signature-,- -

Date ime: / Z,-Date/Time-.Dateffime:Date ime: l?i

ro

8tn

e^*i

r

12/03/2003 WED 10:41 FAI 12622426554FILE No.109 12/03 '03 10:31 ID:

Em ASSOC.FAX:

i)002

PAGE I/ 4

ENVIRONMENTAL HAZARDS SERVICES, L.L.C.745STWHTTE HHE ROAD-RICHMOND, VAZ3237

804-275-478$ FAX 004-2754307


CLIENT:

CLIENT NUMBER: 51*1899 DEHS PROJECT r. 12-03-0136PROJECT: OB-03-855

Environmental AssociatesP.O. Boat 136

DATE OF RECEIPT: 02 DEC 2003DATE OF ANALYSIS; 02 DEC 2003DATE OF REPORT: 02 DEC 2008

GAL-U^X 3u>Gjf T^ I 7

EH3SAMPLE*

01

02

03

04

05

06

07

08

09

10

11

12

CLIENT SAMPLE*/LABORATORY GROSS DESCRIPTION

I/Silver Metal; Black Tar-Like

2/Black Powder

3/Black Brittle; Powder

47Black Powder

51Black Powder

Silver Metal; Black Tar-Like

IfBlack Powder

&1Black Powder

9/Black Powder

Id/Metal; Brown Fib.

ll/Black Powder

12/

% ASBESTOS

NAD

NAD

NAD

Trace. <1% Amosite *<1% Total Asbestos* Only one bundle found.

NAD

NAD

NAD

NAD

NAD

20% ChrysofcUe20% Total Asbestos

NAD

15% Cbrysotila

OTHER MATERIALS

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-Fibrous

100% Non-F&rcru*

100% Non-Fibrous

10% Cellulose70% Non-Fibrous

100% Non-Fibrous

80% Non-FibrousWhite Powder; Fib. 5% Amosite

20% Total Asbestos

~ PAGE 01 of 02-

12/03/2003 WED 09:41 [TX/RX NO 5089] lg]001

12/03/2003 WED 10:41 FAX 12622426554 ENV ASSOC

™.PAGE

MLE No. 109 12/03 '03 10:32 ID: ™.FAX-

ENVIRONMENTAL HAZARDS SERVICES, L.LC.CLIENT NUMBER: 51-1899 DENS PROJECT ft 12-03-0156PROJECT: OB-03-855

QC SAMPLE: M2-1999-3M2499B-1

OC BLANK: SRM 1866 Fiberglass

REPORTING LIMFT: 1% Asbestos

METHOD: Polarised Light Microscopy, EPA Method 800/R-93/116 *

ANALYST: Feng Jiang, MS.TaMtha. Jamison

Reviewed By Authorized Signatory^Howard Vamer, Laboratory DirectorJrma Jfodseuwfci, Quality 4*$uronce CoordinatorDtvtd Xu, US, Senior Chtmiftfbng Jiang, MS, Senior Gfokffift

Afueller, Qiiolity Assurance Manager

Results represent the analysis of samples submitted by the dlent Sample tocatfon, description, area, volume, etc.. was provided bythe client Thte report cannot ba used by the dlent to data product endorsement by NVLAP or any agency ar the U.S. GovernmentTtt* report sfiaW not to reproduced except in fuH, without the written consent of Envtrenmental Hazarda Servicee. LLC. CaRfemiaCe/tffieation 42319 NY ELAP #11714. AN intbrmaten concerning sampling location, date, and time can be found on Chain-of-Custody. Environmental Hazards Services, UL.C. does not perform any sampte cofledfon.

Environmental Hazards Servicas. U.L.C. recommends regnalysis by point count (for more accurate quantification) or TransmissionElectron Mfcnwcopy (TEM). for enhanced detection capabilities) fbr msrteoals regulated by the EPA NESHAP (National Emission'Standards for Hazardous Air PoDutaws) and found to contain less than ten percent (<10%) asbestos by polarized light microscopy(FtM), Both services are avaBable for an additional fee.

* All California samples analyzed by Polarized Ught MIcrascopy, EPA Method 600/M4-82-020, Dec. 1962.

LEGEND NAD = no asbestos detected " "SCF ° suaoactad


12/03/2003 WED 09:41 [TX/RI NO 5058] g]oo2

ItPLMFWiSONMENTAL HAZARDS SERVICES, L.LC. ,

Cftcnond, Virginia 23237 Phone (804) 2754700 Fax {304} 275-4907 (EHS12-03-0156 HAIM QF CUSTODY FORM

Company Nona: . faf f^*R*<~j* 0210:

&tSCibnt Account*Pfcow*

Contact Name:Sampler Name: M<

SampleNumber

SampleDate 4Time

Astjestos

* Do wipe samples submitted meat ASTM E1792 requirement? YeftLJ

Lead

I

Other Metata

i

indoorAir Quality

2

O

Air Volume (4OR

Wipe Area (R2)OR

ScrapeAreafcm1)

Comments

C:T)

r .~~r

Received by:Released by:Received by:

Signature: VSfgrrature: 7Signature:SianaJure:

Datemme:Date/Time:Date/Time:

oo

asCOoIQ

i

tooo

? :

00o

oo<M^v«•}O

CM

05INS

OBOlen

oO

oo

OTH

3

OJ

ENVIRONMENTAL HAZARDS SERVICES, LLC.T469 WMepineRofld RJdimcKd, Wflinte 23237 Pbcne (804) 275-4788 Fax (804)275^907

CHAIN QF CUSTODY FORM

tempanyttonm . ( ^

Contact Nafm:\Sampler Narrso:

BIS Client AccountHtan»£:

ftO.*

.SI

SampleNumber

jtL

Sampta

Time

Dowlpe 8atnp)es aubmlt|fld meet ASTWReleased

Asbestos

ecejvediM&d by:

aceived by:

Lead

i

Other Metatof

792 requirements?SIgnattfrer

IndoorAir Quality

S IB

FWfubtK T^NulMM»WIOSHti(BU})

flir Volume (L)OR

ORScrape

Arwtera*)

Q

O

Comments

oo

rni «•»O

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CM•H

ooen01

enoo

Sfgnatere:Signature: / vSionature:

Oate^ffmerDale/Time:Date/Time:

oo01

Rl£ No.130 12/31 '03 15:56 ID: FAX: PAGE I/ 6

ENVIRONMENTAL HAZARDS SERVICES, L.LC.7468 Wl4ITEl HwE ROAb » RICHMOND, VA 23237 ,

804475-4788 FAX 804475-4907 -=ff ,

ASBESTOS SOIL ANALYSIS SUMMARY ^ _r' ^ - f /

CLIENT:

CLIENT NUMBER:EH3 PROJECT*:PROJECT:

EHS SAMPLE *

01

02

03

04

05

06

07

08

09

10

11

12

13

14

15

Environmental AssociatesP.O. Box 136Thiensville, WI 53092

51-1899 D12-03-323603-03855

CLIENT SAMPLE #

67

69

70

71

72

73

74

75

76

77

78

79

80

81

82

/ J A/ / f^- /?_ ' LJ /^~- f-

\ *»

DATE OF RECEIPT: 31 DEC 2003DATE OF ANALYSIS: 31 DEC 2003DATE OF REPORT: 31 DEC 2003

(_J IN.-^'- - (^ ^ )_>, £_ /"C^ '* ^/ l_ ^_ y^ '^( ^ $ f-

~~fy ^\j fc. (L *•-,

(Î^Zfn

ASBESTOS DETECTED

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

NAD

-PAGE 01 of 02 -




Job ID: Coal Hopper Blast



Report # 63144



Sample ID

PE-01

PN-01

PS-01

PW-01


<0.012 1.512:10 14:05

<0.011 1.012:05 14:10

<0.011 4.012:10 14:15

<0.011 2.012:00 14:00

Lpm 2.50 Ltrs 287.5

Lpm 2.50 Ltrs 312.5

Lpm 2.50 Ltrs 312.5

Lpm 2.50 Ltrs 300.0

LOD (Limit of Detection) policy of MicroAnalytical, Inc. is 8.92F/mm2 or 7fbrs/100fIdsdesignated with a "<" sign.

AIHA 101057

Micro Analytical, luc.11521 West North Avenue

Milwaukee, WI 53226414-771-0855 * Fax 414-771-6570

Client:

Job ID:

Date Sampled: 3/7./ ;

Date/Time Due: 3 /I- / (? /


PE-OJ

/" -2-jr

7Relinquished by Date/Time Received by Date/Time





Fax#

Name/Pager #_ Other

FROM : Micro finalytical FflX NO. : 4147716570 Mar. 02 2004 02:15PM P2




Job ID: Coal Hopper Blast



Sample ID

PE-01

PN-Ol

PS-01

PW-01

<0.012 1.512:10 14:05

<0.011 1.012:05 14:10

<0.011 4.012:10 14:15

<0.011 2.012:00 14:00

Report # 63144



Fibers/CC F/lOO Fids Comments

Lpm 2.50 Ltrs 287.5

Lpm 2.50 Ltrs 312.5

Lpm 2 .50 Ltrs 312.5

Lpin 2 .50 Ltrs 300 .0

LOD (Limit of Detection) policy of MicroAnalytical, inc. ia B.«F/mm2 or 7fbra/100fldadesignated with a "<"

AIHA 101057

FROM : Micro analytical FflX NO. : 4147716570 Mar. 02 2004 02=15PM P3

Client:

Job ID:

Micro Analytical, Inc.1152! West North Avenue

Milwaukee, WI 53226414-771-0855 * Fax 4 14-77 1-65 70

&4-J 7"

Date Sampled: .f s

Date/Time Due: 3


/V.Y2T

* -Z..-T

it

I rff,ley





Name/Pager #_


. Fax#_

Other


APPENDIX G-5

Concealed Asbestos Response Action



May 27, 2004

Golden Marina Causeway LLC311 East Greenfield AvenueMilwaukee, Wisconsin 53202

Milwaukee SolvayCoke and Gas Site311 East Greenfield AvenueMilwaukee, Wisconsin 53204

Concealed Asbestos Response Action,Regulatory Authority Site Visit ActivitiesIncluding Polarized Light Microscopy Sample AnalysisAnd Internal Site Compliance Issues

Submitted To

SajiVilloth and Mark DavisDepartment of Natural ResourcesTonyCity of Milwaukee Dept. of Neighborhood Services

Submitted By:Kevin O'ConnellWisconsin Asbestos Inspector

Background

On May 27, 2004 I was invited to the Former Solvay Coke and Gas Site as analternate asbestos inspector, substituting for Shaun Criston the regular asbestosconsultant, who is on vacation. As the original pre-construction inspector (2002),I have complete understanding of the site and the covenants with the regulators.I have kept a limited role during abatement and demolition because I expect tohave an involvement in the excavation of surface soils in the later phases of theremediation. I am also an alternate for Shaun on the Historic Tewles SeedCompany project (1/2 mile north) where I was inspecting and observing thecomponent removal of Metal Window Panels with non friable asbestos in theglazing as well as suspected lead (very heavy weights for small strips).

Findings

Attached you will find the communications about the suspect and concealedasbestos materials identified on the tops of three boilers, the only remainingstructures left standing on Building 12 (the stack is also still standing).

The letter from Tom Jacobson to Mark Davis dated May 24th (Attached),describes the events of Saji's visit, the initial conclusions, and the responses ofall parties. Additional confirmation samples were also collected and rushanalyzed and submitted with this letter report. The following additionalinformation is not recorded in the original correspondence and is added for yourfurther consideration in the disposition of this matter.

Omitted in the letter was the conditions that led up to Saji's visit on the 26th. Notonly was the project stopped for the discovery of concealed asbestos (boilerbreeching collar), it was delayed for 7 days and 7 inches of rain. During theweather delay, the crew shifted to indoor work on Building 9. The two menreassigned to building 12 after a early morning bagout in Building 9 arrived at theboiler site (Bldg.12) about the precise time that Saji arrived. They arrived on footat the boilers before the other crew members moving the hoses from theprevious site. The two men reassigned to the boilers also had to move the reach(Lull) truck to the west side of the center boiler. While positioning the lift, theypicked up a few pieces of suspect mater (maybe two handfuls) Most of what thecollected was actually negative roofing insulation board (Sample FSC 104) andwhite "pyrobar" brick that was also negative (FSC 102). They did collect a fewstrands of rope gasket that Shaun had identified as positive ( and confirmed FSC103).

Conclusions

On May 27th at the site it became obvious that Tony was not kept up on thefindings, or response actions. This responsibility was previously the routine ofShaun, and I apologize for not realizing my role to continue this as Shaun'salternate for the week.

The circumference of each concealed breeching collar was <10 linear feet, andwere cleaned and set aside earlier (Tuesday) along with an unkown amount ofrope gasket. Upon reinspection on the 27th we found one small piece of yellowgasket less than 6", and it was sent for analysis.

In my opinion, after reviewing all of these activities, communications, andreactions this whole series of events is more a demonstration of a project underattentive management than anything else. And now two fine employees are outof a job because of the smallest lapse in judgment. Especially considering that allthe right things were going on (the water hosing was within 50 feet ofcompletion). Not to mention the whole activity was performed to search for anyscraps of material that were overlooked from the original abatement. One look atthe photos of the top of the boilers shows that it was important to stay on the lift,carefully inspect and pick up targeted suspect material without walking on theroof, or risking a spray of water that may dislodge the material down into the ribsof the boilers where it could not be retrieved.

I think the two workers should be reinstated following a verbal warning on theproper sequence of engineering controls. They each already lost hundreds ofdollars in pay for their infraction of a few handfuls of materials that were mostlynon-asbestos.

I repeat my apology to Tony for not knowing the constant communication he hadwith Shaun.

RespectfuUy,/Oz^-Kevin CfConnellWisconsin Asbestos Inspector 929

Attached:Lake States letter to Mark DavisPolarized Light Microscopy Analysis ReportsPhotos of the debris on top of boiler #3

FROM : Micro analytical FflX MO. : 4147716570 Hay. 28 2004 07:<57»l PI


MILWAUKEE, Wl 53226(414)771-0^55

FAX (414)771-6570

Fax Transmittal

*/**/<Date: ***<?

/fey/*/To:

Company: _

From: 4" —

Subject: _

FAX #: _

Comments:

Pages:

If you have any questions regarding this fax transaction, please call (414) 771-0855.

Thank-you.

Confitertutity Notice: Unlen otherwae indicated, *« infonnmian caooined in Dili fidimje communtartion it confidents)tofonrutkai mlendcd fbr use of ihc individiu) named above. If die rcciptant of this facsimile hw received it in error, you ire herfaynotified thai any taionination or copying ofthit coiranmiettion ia prohibit^, if you have received thii bcsirraie in error, pleasedestroy itimmaJwtdy and notify the sender «t (hs phone number tbovt

F'ROM : Micro finalytical FflX HO. : 4147716570 May. 2Q 2004 07:57PM P2


Page 1 of 1

NVLAP 101247-0


Kevin O'Connell141 N. Jackson St.Suite #414Milwaukee WI 53202

Sample ID;

FSC-101

%Asbestos

Report # 65146Name Former Solvay CokeReceived: 05/27/04Analyzed: 05/28/04Analyst Kevin Hactw


Tan CompactNone Detected 100% Pt MLM Qu Cal

FSC-102

FSC-103

FSC-104

Tan CompactNone Detected 5% Ce 95% Gyp Pt MLM Qu

Tan Plied80% Chry 20% Pt MLM Qu

Tan CompressedNone Detected 90% Ce 10% Pt MLM

End of Report

Chry i oiryaoeU*Amosi AnoiiC*ftroc: OrocidolitaAeti JLctinolit«Trftni TronwliCfAntni AnthoBhyl1icn

a;srBe.

Fibrou* QlaaiCilluloaaSynthetic Fiber•Aix

VanP«ri

Ot<Pt:

VeimiculiteP«rliC«aypaumOlki* 3hot?«rcicul»ct

PL-Hi Paine Lilt* (utcrialMJJ4: Mixad Limt»ron« M»t«rialu: Quarci^li 0»lait

Do; DiatOTK)C«"JU

Teac method: EPA/«OQ/n-93/ilS. Quantitacion iz done by Call&raced Visual Estimation which his an acceptedMlativ* p«rc«n( Diffarance of is. This report nay not be ufa-i to claim produce endorsement by NVLAP orany agency of the U.S. Oovammcnt. Thi» test report relates only to the Items tasted and shall nor, be

4««5 «X«»pt in fuU, without eft* yriccan approval of Micro Analytical. Inc.

FROM : Micro finalytical FflX MO. : 4147716570 May. 28 2004 07:57fiM P2


Page 1 of 1

NVLAP 101247-0


Kevin O'Conriell141 N. Jackson St.Suite #414Milwaukee WI 53202

Report # 65146Name Former Solvay CokeReceived: 05/27/04Analyzed: 05/28/04Analyst Kevin Hachey

Sample ID:

FSC-101

FSC-102

FSC-103

FSC-104

%Asbeatos

None Detected

None Detected

80% Chry

If ,U-*T* v

Description & Composition \

Tan Compact100% Pt MLM Qu Cal

Tan Compact5% Ce 95% Gyp Pt MLM Qu

Tan Plied20% Pt MLM Qu

Tan CompressedNone Detected 90% Ce 10% Pt MLM

End of Report

Che vi Chry sot U«imoii AaoliteC*OC' CrocidollteActi Aceinalic*Tr«rai TrcwoHtf

rlbroui OlaiaCellulose3ynttat.ic FiberMirac. silicic*

C«:3yriiHi

Var? VermiculitePer. PsrliteGyp: gyetuaOki Olkif ShotPt: Particulat*

PL-Mt Paine Uk* MaterialMLM: Mijud Linuiitan* M«c«ri«lQu: OuaxciCal i Calcic*

Do >

T«6C MCiiodi KM/<00/£-9l/ii6. Guantitjcion ii don* by Calibrated visual Estimation which h48 an acceptedS«l4tiv» p«rc*nt D{fr»r«nc« of is. Thii report may not be uaed to claim prooict andoraenjent by KVLAF orany agency of the U.S. Oovernmcnt. Thi» te»c reoort relateu only CO the. Items tested ano shall not bereproduced except in full, without tti* wriccan ifiprovtl or Micro Analytical. Inc.

FROM : Micro Analytical FflX NO. : 4147716570 May. 28 2004 07:58flM P3


Milwaukee, Wl 53226414-771-0855 * Fax 414-771-6570

Client: _

Job ID:

# Samples: Type: PCM(PLM) Lead TEM (circle one)v—"-


02, cgltA C^- QJl W ÔO&

Date/Time ' Received by Date/Time





Fax #

Name/Pager # Other

LAKESTATESNDUSmiAL 9EFMC88

Date: March & 2004

Mark DavisDepartment of Natural ResourcesDirector of Air ManagementMadison, Wisconsin

Re: Solvay Coke Site Visit to Building #12

Dear Mr. Davis:

1 am writing to address the clean up of ACM which was found during demolition operations onBuilding #12. The building had been previously abated and cleared for demolition activities, whichbegan on May 2004.

During the removal of the exhaust breaching from the northern most boiler on Wednesday May 19th,2004 it was discovered that there was a 1" layer of insulation in the seat of the duct which extendeddown into the boiler. Once the material was identified work was stopped, area was secured, a 10 manasbestos crew was dispatched to clean up the ACM using wet methods. Our project Manager BillCook contacted WDNR and notified what we found and discussed a procedure to be implemented toaddress the found ACM. A letter was written the same day and sent detailing the discussion. The letteris attached. After the clean up we investigated the remaining 3 boilers and found the next boiler in lineto the south contained what looked like a rope gasket but did not have the same type of insulation thatwas found on the third boiler. Shaun Criston to a sample for testing. The third boiler running southwas investigated and found to have a different type of insulation, which was sampled. The fourth andlast boiler was investigated which was found to again contain a different type of material. This wasalso sampled. When the results were received later in the day we found that boiler # 2 & # 3 had ACMand boiler # 4 was negative.

Upon assessment of how best to manage this small amount of ACM it was determined we wouldseparate the breaching from the collar that extended into the boilers which had the acm on it andremove this breaching in order to make it safe for our technicians to work on top of the boilers. Thiswork was done on Monday and the breaching was removed on Tuesday May 26, 2004. OnWednesday May 26, 2004 we directed a 2 man crew to investigate the top of the boiler and removethe ACM as specified in the letter dated May 19th, 2004. This crew began this work at approximately9:30. The Project manager had to leave the site for supplies and left the direction of the crews to ademolition foreman who is also a certified supervisor. The foreman told the 2 men where to work andwhat to do. There were directed as always to use water. At approx 10.30 am Saji Villoth observed our2 man crew in the boom lift with a single bag of ACM which was less than .5 cu' of material whichwas dry. Mr. Villoth then donned a harness and went up to the top of the boilers with one of theworkers. According to a discussion with Mr. Villoth when he came down he stated there was friableACM on top of Boiler # 2 which we were already aware. He asked why they were picking up looseACM with out water. And our 2 man crew being Hispanic and speaking very poor English stated thatdid not have a hose yet. In our discussion we determined that the 2 man crew went to the top of theboiler to survey the situation and began picking up the loose materials before the water line was setup. The 2 men were interviewed by you and found to hold valid license from the state to performabatement activities. In addition the site supervisor present during the incident also held a validlicense. After you and Saji left the site we interviewed the workers with our interpreter andreconstructed the event to determine how this happened. The results of our inquiry determined thefollowing;311 East Greenfield AvenueMilwaukee. Wisconsin 53204Office: 414-645-0635Fax:414-645-0645

LAKESTATESrjOUSTRIAL 9EFMCC9

1. The workers knew they should have been using water,

2. Water was available but the hose was not put in place yet.

3. They knew that a laborer was on his way to install a hose.

4. They mounted the boom lift to go to the top of the ovens to survey the situation.

5. Once on top of the ovens, they made an independent decision to pick up some loose ACMwhich was sitting precariously on the boiler. They explained they had planned to ad water tothe bag once they went down for the hose, but in there judgment the thought the ACM wouldbe safer in a bag than laying out.

6. The water was connected and the bag of ACM was wetted. \

7. The licensed supervisor was not in the immediate vicinity and was unaware they were notusing water.

In conclusion we had done the following,

1. Discharged the 2 employees for not using proper procedure.

2. Reviewed the incident with the supervisors and foreman of all our projects to be sure thisdoes not happen again.

3. We will hold an in service tomorrow morning with all employees to review procedures.

4. We will keep closer supervision of abatement activities.

Mr. Davis, I want to apologize for this incident and as the overall project manager I take fullresponsibility for the site operations. I do feel that there is always room for improvement and that thissite is constantly full of surprises for which we always try to be prepared for. Please contact me atyour earliest convenience to discuss this letter.

Regards,

Thomas P. Jacobson Sr.

Project Manager MSCGLake States Industrial Services, Inc.

311 East Greenfield AvenueMilwaukee. Wisconsin 53204Office: 414-645-0635Fax:414-645-0645

Photographs


APPENDIX H

MMSD Documentation

• H-1: Notice of Intent to Discharge to MMSD System

• H-2: Letter to MMSD Allowing the Discharge to TheirSystem




APPENDIX H-1

Notice of Intent toDischarge to MMSD System

€> EarthTechA Tyco International Ltd. Company


mONMENTAL ASSOCIATE, INC.,

P.O. Box 136 • Thiensville. Wisconsin 53092OFFICE: 262.242.1088 • TOLL FREE: 800.494.4645 • FAX: 262.242.6554 • www.eedvri.com

December 4, 2003

Milwaukee Metropolitan Sewerage DistrictAttn: Harvey MatyasPO Box 3049Milwaukee, Wisconsin 53201-3049

Re: Notice of Intent to Discharge Non-Domestic Wastewater, Former Solvay Coke and GasSite, 311 E. Greenfield Avenue, Milwaukee, Wisconsin

Dear Mr. Matyas:

The purpose of this correspondence is to provide a letter of understanding regarding the proposedwastewater discharge at the Former Solvay Coke and Gas Site. This letter will describe theprocess, operations, activities, and circumstances that will produce wastewater at this site as wellas plans for discharge. The Notice of Intent to discharge non-domestic wastewater, as requiredby Section 11.401 of the MMSD rules, is provided in Attachment A.

Site Background

The Former Solvay Coke and Gas Site is being deconstructed in phases by Lake States IndustrialServices. Various sized aboveground storage tanks (ASTs) associated with the Former SolvayCoke and Gas Production Facility are located throughout the site. The ASTs have deterioratedover time and currently contain residual coal tar and storm water. As a part of Phase I ofdeconstruction these ASTs will be emptied, cut open, cleaned, and removed from the site.

Proposed Discharges

Non-domestic wastewater is generated in one of two ways:

(1) Contaminated Water that has Accumulated in each AST as a Result of Rain Infiltration

As part of the deconstruction of the site, the ASTs will be emptied, cleaned and cut up for scrap.The first step in the AST removal process is to drain the water that has accumulated in the tanksas a result of rain water infiltration. It is proposed that the water that has accumulated in thetanks as a result of rain infiltration be drained from each AST and disposed of through thesanitary sewer. Because this water has been held in these tanks for a number of years, in directcontact with residuals within the tanks, and because cyanide has been detected in this water, thisdischarge would not be considered "unpolluted water" that could otherwise be routed directly tothe waters of the state under a WDNR permit.

ENVIRONMENTAL ASSOCIATES, INC,

The total volume of water that will be discharged from the draining of contaminated water thathas accumulated in each AST is expected to be approximately 25,000. Water will be dischargedin five batch discharges of 5,000 gallons each over a four week period of time. It is anticipatedthat all five discharges will be completed within four weeks of receiving discharge approval fromMMSD. The proposed discharge location is a toilet (4-inch line) located in Building #11 (Figure1, Attachment D).

A representative sample of water that has accumulated in the tanks as a result of rain infiltrationwas collected on November 19, 2003 and submitted to Great Lakes Analytical in Oak Creek,Wisconsin. The sample was analyzed for the compounds listed in MMSD section 11.202 and11.203(1 )(a). No compounds were detected, above laboratory method of detection limits, withthe exception of cyanide (0.0736 mg/L), which was detected below the MMSD limit of 5.0mg/L. Wastewater analytical results are summarized in Table 1, Attachment B, and presented inAttachment C of this submittal.

(2) AST Wash Water

After the contaminated water in each tank is emptied, coal tar residuals will be removed andproperly disposed. The empty tank will then be thoroughly cleaned using high pressure washingequipment. It is proposed that this AST wash -water also be discharged into the sanitary sewer.

It should be noted that AST wash water has not yet been generated and, therefore, has not yetbeen tested at the site for the pre-treatment parameters listed in MMSD Chapter 11.203. It isanticipated that this wash water will require pre-treatment prior to being discharge into theMMSD sanitary sewer to meet Chapter 11.203 limits. Treatment of this water will consist of aclarifier cell (frac tank) and liquid carbon canisters.

In order to gain approval for discharge, it is proposed that prior to each batch discharge a sampleof the treated water be collected for Chapter 11.203 parameters, pH and TSS. These results willbe compared to Chapter 11.203 limits prior to discharge and, if they fall below these limits,discharge will proceed. If any of the Chapter 11.203 limits are exceeded, additional treatmentwill be conducted and the effluent will be retested prior to discharge. All testing results will bemade available to MMSD at their request.

The total volume of AST wash water that will be discharged to the sanitary sewer is expected tobe approximately 25,000. AST wash water will be discharged in batches. It is anticipated thatthe discharging of AST wash water will be completed within four weeks of receiving approvalfrom MMSD. The proposed discharge location is a toilet (4-inch line) located in Building #11(Figure 1, Attachment D).



Summary and Conclusion

Lake States Industrial Services is requesting written permission to discharge the above describednon-domestic wastewater at the Former Solvay Coke and Gas Site: As Lake States IndustrialServices would like to commence discharge before freezing occurs, your prompt review wouldbe greatly appreciated. If you have any questions or concerns, please feel free to contact us.

Sincerely,

Environmental Associates, Inc. Lake States Industrial Services

Joe Michaelchuck, P.E. Bert SneadSenior Engineer President

cc: File

Encl: $250.00 check payable to MMSD


ATTACHMENT A

Notice of IntentTo Discharge Non-domestic Wastewater,As Required by sec. 11.401, MMSD Rules

L Facility Information

(a) Facility name Former Solvay Coke & Gas Site

(b) Facility address311 E. Greenfield Ave.

Milwaukee, WI 53^04

(c) Mailing address311 E. Greenfield Ave.

Milwaukee, WI 53204

(d) Contact person Tom JacobsonNameV.P. (Lake States Industrial Services)

Tide

414-645-0635 (office)Telephone

(e) Business description

The Former Solvay Coke and Gas Site is being deconstructed

by Lake States Industrial Services. Various above ground

storage tanks (ASTs) associated with the Former Solvay Coke

and Gas Production Facility are located throughout the site.

The ASTs have deteriorated over time and currently contain

residual coal tar and water. As part of Phase I of deconstruction

these ASTs will be cut open, cleaned and removed from the site.

(f) Five digit NAICS code or four digit SIC code

IL Discharge information

(a) Reason for submitting this notice of intent:

Constructing a new facility that will discharge process wastewater to the sewerage system

Taking possession or control of an existing facility that discharges process wastewater

Changing the physical size or operations at an existing facility to the extent that wastewatervolume or content will be substantially changed, including, but not limited to, a change inthe annual average daily discharge flow rate of 20% or more

Proposing to discharge contaminated groundwater

Commencing or modifying a discharge of hazardous waste that requires reporting accordingto sec. 11.411, MMSD Rules

Proposing to discharge non-domestic_JL__ Other. Explain on an attached page wastewater not previously reported

to the District.(b) Proposed date for the commencement of discharge as soon as possible (12 / 0 5 / 0 3)

(c) Describe the processes, operations, activities, and circumstances that will produce the non-domestic wastewater covered by this Notice of Intent

see cover letter

(d) Wastewater discharge rates for the facility as a whole. Complete this section if the dischargeis not a one-time discharge

Flow rates (gallons per day)Existing Proposed

Domestic

Non-domesticProcess

Non-contactcooling approximately 1,785 gallons per day

(see cover letter)Other

(e) Discharge type (fill in the spaces that apply)

1. Continuous discharge: hours per day days per week

2. Batch discharge: 1 0, OQOgallons discharged per batch pet ( 5 batches total)Frequency Time

3. One time discharge: gallons discharged over days

4. Other (explain the timing and type of discharge)

(f) List the pollutants potentially present in the wastewater covered by this Notice of Intent

See attached analytics.

(g) Sample results. If you are able to sample the wastewater covered by this Notice of Intent, thenattach sample results according to the instructions.

(h) Would the wastewater covered by this Notice of Intent be regulated as hazardous wasteaccording to sec 40 CFR 261 if it was not discharged to the sewerage system?

Yes x NO

If yes, contact the District for additional reporting requirements.

(i) Describe any proposed treatment procedures or equipment

None.

(j) Enclose a drawing of the site where the discharge will occur, This drawing must identify allconnections to the sewerage system; the processes, operations, or activities generatingwastewater; treatment facilities, and potential sampling locations.See Figure 1 .

HL Certification and signature

/ certify under penalty of law that this document and all attachments wereprepared under my direction or supervision in accordance with a systemdesigned to assure that qualified personnel properly gather and evaluate theinformation submitted. Based on my inquiry of the person or persons whomanage the system or those persons directly responsible for gathering theinformation, the information submitted is to the best of my knowledge and belieftrue, accurate, and complete. I am aware that there are significant penalties forsubmitting false information, iypfuding the possibility of fine and imprisonment

violtions

Signature ' Date

Printed name and title

Notice of Intent

ATTACHMENT B

Table 1: Non-domestic Wastewater Evaluation, November 19,2003,

Solvay Coke and Gas Site, Lake States Industrial Services, 311 E. Greenfield Ave., Milwaukee, Wisconsin

'arameter

Oil and Crease

Cyanide^^ . .-vunasmsamaBii, ...

pH -•---•— —LJ»««SB»*-™»-'-- -

', .T^ i/^SaCSHBBESHHBBBniBfS^CCrfn1 " " •'reonfc Compounds:lenzo(a)andiracene

Methyl bromide (Bromomethane)Methyl chloride (CMoromethane)'henanthrene

fac. CompoundsAcroleinAldrinalpha - BHCbeta - BHCdelta - BHCgamma - BHCAlkylated Leadlenzo(a)pyrene

Chlordane4,4-DDD4,4-DDE4,4-DDT1,3-Dichlorobenzkline

Dieldrinindrosulfan Iindrosulfan IIEndosidfan SulfateindrinEndrin AldehydeFhiorantheneHeptachlorHeptachlor EpoxideHexachlorobenzeneMirexPentachlorobenzenePCB -1016PCB - 1221PCB - 1232PCB - 1242PCB - 1248PCB - 1254PCB -1260Toxaphene2,4,6-Trichlorophenol1 ,2,4,5-TetrachIorobenzene

Selected Metals' "'""""CadmiumCopperLeadMercuryNickelSilverZinc

Units

mg/L

mg/L

mg/L

mg/Lvvv t y.jS i'

mg/Lmg/Lmg/Lmg/L

.'._!•_•.,

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

MMSDLimits'

300

5.0 '"'""

>{'"""*"'~ ' ' '". ' ViX:iJI^3 ': "'-' i"

0.0620.1830.3690.051

.. -,•!?',,•.,

390-----131301.3--1.32600.65

See Footnote2

See Footnote2

See Footnote2

1.3-

1300.65-

130130130

See Footnote3

See Footnote3

See Footnote3

See Footnote3

See Footnote3

See Footnote3

See Footnote3

26130-

1.56.02.0

0.00264.05.88.0

Tank 13 Spill

<5

0.0736

<5

6.87'VT.i'K"!.

<0.010<0.010<0.010<0.010

,

<50<0.03<0.02<0.03<0.03<0.03

NT<10

<0.26<0.04<0.03<0.160

<20<0.03<0.03<0.05<0.1<0.1<0.15<10

<0.04<0.02<10NT<20<0.5<0.5<0.5<0.5<0.5<0.5<0.5<0.5<10<20

<0.0005<0.05

<0.005<0.0002

<0.05<0.05<0.5

Footnote1 MMSD discharge Iimts baled on MMSD Chapter 11.202 md II .203( 1 Xa) local limits2 The MMSD discharge lunt for &)do«ulfiin i3 1.3 ug/L

1 The MMSD discharge limit for Porychlorinated Biphcnyi's is 1.3 ug/L. This applies to each species ofpolychlorinated btpheoyl.

NT = Not Tested

- = No discharge standardEnvironmental Associates, Inc.

8S5nmsdll-03

ATTACHMENT C

a;u / t.reai L

'-•• •"••••1

ll







12/02/03 17:03


Sample ID

Tank 1 3 Spill

Laboratory ID Matrix

W3 11 185-01 Water

Date Sampled Date Received

11/19/0313:30 11/19/0314:40

Great Lakes Analytical-Oak Creek Tht raula in this report apply to the lamplcs analyzed In accordance viih ihf chain ofcustody dacunient. 27ilf analytical rtpnrt must be reproduced In ill entirety.

Andrea Stathas, Project Manager Page 1 o f 2 ~

12/02/2003 TUE 17:04 [TX/R-X NO 5084] 12] 003

12/02/21)1)3 TIE 5:1)8 tAA 414i7U94bl lireai L3K6S Analytical

!KC££2£BH

"SI££• GREAT

LAKESANALYTICAL



LuXc States Industrial Service311 E. Greenfield Ave.Milwaukee Wl, 53204


Project Manager: Tom JacobsonRcpartcd:

12/02/03 17:03


Aaalyte

Tank 13 Spill (W31118S-01) Water

Cynolde (total)Oil Sc. Grease

Result

SampUd:

0.

11/19/03

0736ND

Reportinglimit Units

13:30 Received:

o.oioo5.00

mg/lM

DilutioQ Batch

11/19/03

1II

14:40

3H0534311049S

Prcpunri Analyzed Method

11/25/03 11/23/03 EPA9012A11/21/03 11/24/03 EPA 413.1

Notes

QC

Great Lakes Analytical-Oak Creek The resulu in this report apply to the samples nnalyzvJ in accordance wfrt the chain cfcustody dncumcnt. This analytical report must bn rilprvJuced in itt entirety.

uidrea Stathas, Project Manager Page 2 of 2^

12/02/2003 TVE 17:04 [TX/RX NO 5084]

1 2 / U 2 / 2 U U 3 TDK i > : u & I<M 414&7 ua«i ureai Lanes U.K




Lake States Industrial Service311 E. Greenfield Avc,Milwaukee WI, 53204

Project MSCG Pre Treatment ListProject Number: [none]Project Munugcr. Torn Jacobson

Reported:12/02/03 17:03

Total Metals by EPA 200 Series MethodsGreat Lakes Analytical—Buffalo Grove

Anulyie

Tuck 13 Spill (W31118S-01) Water

SilverCadmiumCopperMercuryNickelLc»dZinc

ResultReporting

Limit Units

Sampled: 11/19/03 13:30 Received:

NDNDNDNDNDNDND

O.OSOO0.000500

0.05000.000200

0.05000.00500

0.500

mt/ln

N

n

Dilul

11/19/03

1•

*

ion Batch

14:40

31104413120031311044131104453110441

It

Prepared

llttO/0312/01/0311/20/031 1/20/031 1/20/03

It

Analyzed

12/01/0312/02/0311/26/0311/20/0311/26/0311/21/0311/26/0.1

Method

EPA 200.7EPA 213.2EPA 200.7F-PA24S.1EPA ''OO 7EPAS3V.2EPA 200.7

Noics

QC

Great Lakes Analytical--Oak Creek Tht rtsults in this report apply In the samples analyzed in accordance with the chain u;custody document. Thin analytical report must be reproduced in Its entirely.

Andrea Stathas, Project Manager Page 3 of 2?

12/02/2003 TUB 17:04 [TX/RX NO 5084] ©00:,

a ;uo r/u iito/uaioi weai Lanes

E^ E IM

filGREATLAKESANALYTICAL




Project: MSCG Pro Treatment ListProject Number: [none]


12/02/03 17:03

Volatile Organic Compounds by EPA Method 624Great Lakes Analytical—Buffalo Grove

AnMyte ResultReporting

Limit Units Dilution Baluh Prepared Analyzed Mrfhod Notes

Tank 13 Spill (W311185-01) Water Snmpled: 11/19/03 13:30 Received: 11/19/03 U:40 QC

AcrolclnBramomelhaneChlaromcihancSurrogate: DibromnfluarnmtlhaneSurrogate: 1,2-DiMoroethane-d4Surrogate: Tolncnc~<l8Surrogate: 4-BrnmoJluorobemene

NONDND

50.010.010.0

3110438 H/20/03 11/20/OJ EPA624/8260B A-01

JQ8%75.6%104%99.S %

7S.8-I2762.5-14S76.6-1306S.9-J23

Great Lakes Analytical—Oak Creek The results in this report apply to the tamplts analyzed in accordance with the chair, nfcustody document. This analytical repart mat he reproduced In Its entirely.


12/02/2003 TUB 17:04 [TX/RX NO 5084]

12 /U2 /2UIM D'.ua weai t{tj UU I / UUi.



Email: [email protected])570-9460 FAX (414) 570-9461




12/02/03 17:03

Organochlorinc Pesticides and PCBs by EPA Method 608Great Lakes Analytical—Buffalo Grove

Anulyrc ResultReporting

Limit Units Dilution Butch Prep-eci Analyzed Method Nolcs

Tank 13 Spill (W31118S-01) Water Sampled: 11/19/03 13:30 Received: 11/19/03 14:40

Aldrin

ulphu-BHCbcta-BHCdelta-BHCjjwmmu-BHC (Lindanc)Chlordanc (tech)4,4'-DDD4.4'-DDE4.4'-DDTDieldrinEndosulfan IEndosult'aii IIEndosulfan sulfatcEndrinEndrin aldehydeHeplachlor

or epoxide

rCB-1016PCB-1221PCB-.1232PCB-1242PCB-1248PCB-1254PCS- 1260

ND

NDNDNDNDNDND

—NBNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

Surrogate: Tctrachloro-mcta-xylcneSurrogate: Decachlarobiphenyl

0.0300 ug/l 3110462 11/20/Cr 11/30/03 EPA608/8081/82

0.02000.03000.03000.0300

0.2600.04000.0300

0.160 •0.03000.03000.0500

0.1000.1000.150

0.04000,0200

0.500O.SOO0.5000.500O.SOO0.5000.5000.500

82.4 %32.8%

H 11

"

..

II It

II H

11 "

II -

" "

II ft

I.

II »

II It

• 1

II

II

n

II

„

II II

II I,

..

II

.1

It H

10-11010-140

Gre^t Lakes Analytical-Oak Creek


77i« rexulu in this report apply to me samples analysed In accordance with thecustody document. This analytical rrpr^r mat be reproduced in it* entirety.

Page 5 of 2?

12/02/2003 TUE i~:04 [TX/RX NO 5084]

12/U2/2UU,} TDK i)',ua fAA weai Lanes

U2UaH

"SiSB GREAT

LAKESANALYTICAL




Project; MSCG Pre Treatment ListProject Number [none]


12/02/0317:03

Base/Neutrals and Acids by EPA Method 625Great Lakes Analytical—Buffalo Grove

AnnlytcReporting

Result Limit Unite Dilurion Batch Prepared Anulyrcd Method Noi=,

Tsnk. 13 Spill (\V3inSS-01) Water Sampled: 11/19/03 13:30 Received: 11/19/03 14:40 QC

Bcnz (a) anthraceneBenzo (a) pyrene3,3 '-DichlorobcnzidineFluorantheneHexachlorobert^tncPhcnHQthrcnc2,4,6-TrichlorophenolSurrogate: 2-FluoraplienolSurrogate; Plicnol-d6Surrogate: Nilrobeiuenz-dSSii/Tuyatit: 2-FluorobiphenylSurrogate; 2.4, 6-TrlbromophcntitSurrogate: p-Terphenyl-dl 4

ND 10,0ND 10.0ND 20.0ND 10.0ND 10.0ND 10.0ND 10.0

4.84%4.19%l&.5%1X.S%17.7%17.4%

ug/1 1 3110

H n

11 t

II It

10-11010-110

31.4-11010-11010-11010-147

424 11/19/03 11/21/03 EPA 623/8270CI* II H

II n II

M II H

« n II

L" " L

LH H *

H It U

•f H H


Ui &lLgfi

Tlie resula in this report appfy lo the.tampltj analyzes! In acuonlanct with slit chaicu.iiady document. Hit's analytical report must bf reproduced in its tntirery.

Andrea Stathas, Project Manager Page 6 of I1?

12/02/2003 TUE 17:04 [TX/RX NO 5084]

12/02/2003 TUE 5:09 FA1 4145709461 Great LaKes Analytical

SSSSB GREAT\ LAKESI ANALYTICAL



Lake Stales Industrial Service311 E. Greenfield Avc.Milwaukee Wl, 53204

Project -MSCG Prc Treatment ListProject Number, [none]Project Manager. TomJscobson

Reported:12/02/03 17:03

Tentatively Identifled Compounds by GC/MS EPA Method 8270Great Lakes Analytical—Buffalo Grove

Anslytc ResultReporting

Umit Units Dilution Batch Prepand Anulyrod Method Notes

Tank 13 Spill (W31118S-01) Water Sampled: 11/19/03 13:30 Received: 11/19/03 14:40

1 ,2,4,5-Tetrachlorobeny.ene3,3'-Dii;hlorobcn2Jc3incPentachlorobenzene

Surrogate: p-Terphcnyl-a'14Surrogate: 2, 4, 6~TribrvmopHtnolSurrogate: 2-FltiorobiphenylSurrogate: Nltrobcnsene-dSSurrogate: Phenol-d6Surrogate: 2-Fhtorophenol

NDNDND

20.020.020.0

17.4%17.7%18.5%18.5%4.19%4.84%

us/I i 311011 • II

» H 11

23-9810-15V31-8629-89W-V3

10-124

1424 ll/lii n

1 r

1 i

f t

t 1

>l i

>* .

J/03 H/211 l<

1 «

* •

f f

V <

>l <

n i

L/03 EPA «> n

r »

* i

r i

• <

• i

H i

270C

Lr

LLLL

Great Lakes Analytical-Oak Creek The results In this report apply la the samples analyzed in accordance with thecustody document. This analytical repnit must be reproduced III its entirety.

Andrea Stathas, Project Manager Page 7 oil-

12/02/2003 TUE 17:04 [TX/RX NO 5084] @009

12/02/2003 TUE 5:09 FAX 4145709461 Great Lakes Analytical ISU1U/UJ2

£?££• GREAT\ LAKESI ANALYTICAL


Email: [email protected]•;<:••*) 570-9460 FAX (414) 570-9461

Lake States Industrial Service3 11 E. Greenfield Ave.Milwaukee W I, 53204

Project: MSCG Prc Treatment ListProject Number, (none] Reported:

Project Manager. Tom Jwcobson 12/02/03 17:03

General Chemistry - Quality ControlGreat Lakes Analytical— Buffalo Grove

AnulytuReporting Spike Source %R£C RPD

Result Limit Units Level Result %REC limits RPD Limit Note,

Batch 311049S - EPA 3510C

Blank (311049S-BLK1)Oil &GrcMc

LCS(3110495-BS1)Oil & Grease

LCS Dup (3110495-BSD1)Oil St Grcuc

Batch 3110534 - General Prep WC

Blank (31 10534-BLK1)Cyunidc (coul)

LCS (3110S34-BS1)Cyanide (total)

\triJt Spike (3110534-MS1)jmiJc (tnbil)

Matrix Spike t>up (3 H0534-MSD1)

Trepared: 11/21/03 Analyzed: : 1/24/03ND . 5.00 ing/l

Prepared: 11/21/03 Analyv<d: .724/0327 -S 5.00 me/1 30.0 91.7 C.S-123

Prepared: 11/21/03 Analyzed: " :/24/0325.8 5.00 mg/I 30.0 S6.0 T.S-123 6.38 S2.4

Prepared &. Anulyzcd: 11/25/D3ND 0.0100 nigt

Pnq>urc<3 & Analyzed: 1 1 /25-T:-?0.504 0.0100 mii/1 0.480 105 -K-S-HS

Source: W311185-01 Prepared &. Analyzed 1 1/2<;T~0.8S8 0.0250 tug/1 1.20 0.0736 67.9 >J2-J7J

Source: W311185-01 PrepHrcd & Analyzed: 1 1/ZS/c:-Cyanide (total) 11.2


Andrea Statha.s. Project Manager

The results In this report apply to the sarnies analyzed in accordance wllh the ch:nr. ~;custody document. Hits analytical npo*t mat bf reproduced In Its entirely.

Page 8 of 2?

12/02/2003 TUE 17::, [TX/RX NO 5084] So:

Tut, &:ua PAA 4i4aruMbi weai Lanes l^J Uli/ UJi

S^B GREATI LAKES(ANALYTICAL

4C2.ZZIM |

"Si140 East Ryan Road

Oak Creek, Wisconsin 53154Email: [email protected]

(414) 570-9460 FAX (414) 570-9461

Lake Stole; Industrial Service311 E. Greenfield Ave.Milwaukee Wl, 53204

Project: MSCGPre Treatment ListProject Number: [none]

Project Manager. Tom JncobaonReported;

12/02/03 17:03

Total Metals by EPA 200 Scries Methods - Quality ControlGreat Lakes Analytical—Buffalo Grove

Analytc ResultReporting

Limit UnitsSpikeLevel

SourceResult %K£C

V.REC RPDLimiLv RFD Limit Notes

Batch 3110441 - EPA 3010A

Blank (3110441-BLK1)CopperLeadNickelSilverZinc

LCS C3110441-BS1)CupperLeadNickelSilverZinc

Matrix Spike (3110441-MSD•riper

1NickelSilverZinc

Matrix Spike Dup (3110441-MSD1)CopperLeadNickelSilverZLiic

ND

ND

ND

ND

ND

3.970.0263

4.143.924.23

O.OSOO ma/10.00500

O.OSOOO.OSOO0.500

O.OSOO mg/10.00500

O.OSOO

O.OSOO

0.500

Source: B3 11 326-014.08

0.02933.96

ND

4.14

0.0500 mg/1

0.00500

0.0500

0.0500

0.500

Source: B311326-0 14.09

0.02854.01

ND

4.30

0.0500 mg/\

0.00500 "

o.osyo0.0500

0.500

Prepared:

Prepared:4.00

0.02404.004.004.00

Prepared:4.00

0.02404.004.00

4.00

Prepared:4.00

0.02404.00

4.00

4.00

1 1/20/03

1 1/20/03

U/20/030.02280.00306

ND

ND

0.0260

11/20/030.0228

0.00306ND

ND0.0260

Analyzed:

Analysed;99.2

110

104

98.0

106

Analyzed:101

1O9

99.0

103

Anaryzed.102106

100

107

11/26/03

1 1/26/0389.8-1 IS71.7-14190-114

61.6-13688.S-117

1 1/26/0376.3-13617.2-176S2.2-12310-154 L76-135

11/26/0376.3-136 0.245 16.117.2-176 2.77 33.782.2-123 1.25 ]<310-154 60.fi76-135 3.70 28.4

Great Lakes Analytical—Oak Creek The rtiutu in this rcpart apply to the samples analyzed In acvunlance with the rl-j'r •'custody dacumant. TJiij analytical report muxt he reproduced in la entirety

\rxdrea Stathas, Project Manager Page 9 of 25

1 2 / 0 2 / 2 0 0 3 TUE 17:04 [TX/RX NO 5084]

iim o ;ua TAA ti ta/imoi 4/ -JUJ .L/





311 E. Greenfield Avc.

Milwaukee Wl, 53204

Project: MSCG PTC Treatment List

Project Number [none]


12/02/03 17:03

Total Metals by EPA 200 Series Methods - Quality ControlGreat Lakes Analytical—Buffalo Grove

AiialyteReporting


SourceResult

V.REC%REC Limits RPD

RPDLimit Nulra

Batch 3110445 - EFA7470A

Blank (3110445-BLK1)Mercury

LCS (3110445-BS1)Mercury

Matrix Spike (311044S-MSI)Mercury

Matrix Spike Pup (3110445-MSD1)Mercury

Batch 3120031 - EPA 3010A

Prepared &. Analyzed: 11/20/03ND 0.000200 mg/\

0.00159 0.000200Prepared & Analyzed: 1 1/20/03

mg/l 0.00150 106 76.6-124

Source: W31118S-010.00156 0.000200

Prepared &. Analyzed: 11/20/03 _mg/l 0,00150 ND 104 45.1-149

Source: W311185-010.00151 0.000200

Prepared & Analyzed: 1 1/20/03me/I 0.00150 ND 101 4S.1-I49 3.26 22.8

Blank (3120031-BLK1)Cudmium

' CS (3120031-BS1)Imium

Matrix Spike (3120031-MS1)Cadmium

Matrix Spike Pup (3120031-MSD1)Cadmium

ND 0.000500 me/1Prepared: 12/01/03 Analyzed: 12/02/03

0.00207 O.OOOJOO mg/lPrepared: 12/01/03 Analyzed: 12/02/03

0.00200 104 85-115

Source: B311462-01 PrepareJ: 12/01/03 Angly/rd: 12/02/03mg/l 0.00200 0.000554 109 75-1250.00274 0.000500

Sou ret: B311462-Q1 Prepared: 12/01/03 .Analyzed: 12/02/030.00275 0.000500 0.00200 0.000554 110 75-125 0.364 20

Great Lakes Aoalytioal-Oak Creek Ihe results In this report apply la the samples analyzed in accnrdance wll/i //;•-• chain icustody document. This analytical rrport mutt be reproduced in its entirety.

\ndrea Stadias, Project Manager Page 10 of 2?

12 /0^ /2003 TIT 17:04 [TX/R.X NO 5084] @] 01 ^

HE a : iu FAA ureai Lanes V O i

S33H GREATI LAKES[ANALYTICAL



Lake Suites Industrial Service

3 It E. Greenfield AVC.Milwaukee WI, 53204

Project. MSCC Pre Treatment ListProject Number [none]

Project Manager. Tom JacobeanReported:

12/02/03 17:03


Analyre

Batch 3110438 - EPA 5030B (P/T)

Dlank_J3110438-BLKl)_Aerolcrn

AciylonimlcBenzene

Bromndichloromelhane

BromofonnBromomcthane

Carbon tccnchluridc

ChJoroberLcenc

Chlorudibromo[ueth«u<!Cllloru ethane

2-CliIorecthyIvinyl ether

Chlorofarm

Chlnromethanc ,

Dicblonibcnzencîuhlorobcnzane

1 .4-DichIorobaizcne1 , l-Dichloracthanc

1 ,2-Dichloroethane

1,1-Dichloroelhcne

ci.s- 1 ,2-Dichlorocthencimn?- 1 2-Dichloroclhcnc

1 ,2-Dichloropropiinc

c i »- 1 .3-Dichloroprupcn«

cr.iiii-1 ,3-Dii:hloropropenc

Echylbcn7aieM cthylfnc chluridc

Slyraic1 , 1 ,2,2-Tctrachloroeitia(ie

Tc^rachlproelhcncToluene

1 , 1 . 1 -Trichlorocthanc

l.l ,2-Trichloro«h«ue

TnchloroclheneTn ch loronuoroinethane

Viny l thlondc

Result

ND~

ND

ND

NDND

ND

ND

ND

NDND

ND

ND

ND

NDND

ND

ND

NDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Reporting Spike Source %REC RPDLimit UniU Level Result %R£C Limits RPD Limit Notes

Prepared & Analyzed: 11/20/0350.0 ug/150.0 "

5.00

s.oo5.00

10.0 "

5.00 "

S.OO

5.00

S.OO

100

5.00 "

10,0 "

5.00-

5.00

5.00 "

S.OO

S.OO

5.00

5.00

5.00 "

5.00

5.00

5.00

5.00

5.00

5,00

5.UO

S.OO

S.OO

5.00

5.00 "

5.00

5.00

5.00

Great Lakes Analytical— Oak Creek Tlie resulu in this repurl apply to the lampla analyzed In accordance, with tit? chain ofcustody document. Thit analytical report must be rrproductd In la fHtlmly.

irea Stathas, Projecc Manager Page 11 of 29

12/02/2003 TUB 17:0-1 ITX/RX NO 5084]





Luke States Industrial Service31 I E. Greenfield Ave.Milwaukee WI. 53204

Project: MSCG Pro Treatment ListProject Number [none]

Project Manager Tom Jacobson 12702/03 J 7:03

Volatile Organic Compounds by EPA Method 624 * Quality ControlGreat Lakes Analytical—Buffalo Grove

AnalyteReporting

Result Limit UnitsSpike Source V.REC R?DLevel Result V.REC Limits RPD Limit Notes

Batch 3110438 - EPA 5030B (P/T)

Blank (3110438-BLK1)

Surrogate: DibroinofluoromcthantSurrogate: 1. 2-Dichloro*than*-d4Surrogate: Tulutn*-d.SSurrogate: l-Broinofluonlxlnifne

LCS (3110438-BS1)BenzeneBroinodichloromcthunc

Bromoform

BmmonicthaneCurbon tctrnchloridc

Chlorobenzcnc

Chloiadibromomettumc

•"Moroethaue

:hlorocthylvinyl etherChloroform

Chloromclhmie

1 .2-Diclilorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlornbciw.cnc1 , 1 -DichlorocthnTie

1,2 -Die hloroc thane

1 , 1 -Dichloruelhcne

c is- 1 ,2-Dii:h[oroclhenc

:rani-l ,2-Dichloroetlicne

1 .2-Dichlnrnpropnno

cis-1 >3-Dic:hlorripropcncirans-1 .3-Dichlorcipropcnc

EtliylbenzeneMcthylcne chlorivleStyrcnc

1 , 1 ,2 ,2-Trtraehloroctbaiie

Telrichlumdhcnc

Toluene

1,1.1 -Trichlurocthanc

1 , 1 ,2-Trithloroelhunc

34.943.8Sl.VSI.7

41.040.0

44.8

41.0

42.4

45.4

47.1

S4.6

ND

41.9

37.74R.fi

50.3

43.941.3

38.6

40.1

42.6

43.8

40.4

38.0

36.547.2

43.7

45.7

43.3

50.5

41.7

42.1

3S.8

VK/Ia

""

5.00 ug/1

5.00

5.00

10.0

5.00

5.00

5.00

5.00

100

5.00

10.0

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.UO

5.00

S.OO

5.00

5.00

5.00

5.00

5.00

5.00

Prepared & Analyzed:

SO.O

JO.O

50.0

30.0

Prepared & Analyzed;50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

SO.O

50.0

SO.O

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

50.0

SO.O

SO.O

SO.O

11/20/03

110 75.S-12737.6 62.S-I45IOA 76.6-130103 68.9-123

11/20/0382.0 61.3-142SO.O 65.9-16289.6 30.2-176

82.0 33.R-16184.8 40J-I64

90.S 79.9-132

94.2 54-159

109 37.1-163

80-120 L

83.8 78.6-132

75.4 34.3-158

97.2 78.6-139

101 79.1-13687.8 7S.2-12982.G 58.2-134

77.2 73-136

S0.2 58-136

85.2 76.3-135

87.6 53.3-13780.8 6S.9-147

76.0 61-16573.0 59.4-166

94.4 78.4-130

87.4 52.2-142

91.4 60.2-14486.6 40.3-164

101 44.9-165

83.4 77.4-131

84.2 66.6-14377.6 74.8-147

Great Lakes Analytical—Oak Creek Tlit result! in Ihtt report apply tn the samples analyzed in accordance with thr chaicustody document. ThLs analytical report must br reproduced in Its entirely.

Andrea Statfaas, Project Manager Page 12 of 2S

12 /02 /2003 TUE 1 7 : 0 4 [TX/RX NO 5084]






31 I E. Greenfield Ave.Milwaukee Wl, S3204

Project: MSCG Pro Treatment ListProject Number; [none]


12/02/03 17:03


AnnlytcKcponing

Result Limit UnitsSpike SourceLevel Result %REC

%REC RPDLimits RPD Limit Notes

Batch 3110438 - EPA 5030B (P/T)

LCS (311U438-BS1)TrichloroetheneTrichlorofluoromelhime

Vinyl chlorida

Surrogate: DLbromofluarvmttlianeSurrogate: l,3-Dichhrvetliane-<{4Surrogate: Toluent-dRSurrogate: 4-Dromofluorobanzene

Matrix Spike (3110438-MS1)Benzene

BromodiuhloromethancBromoform

BroiTiomcthaiie

(~.<rbon tctraehloriderobcnzcnc

v-iiiorodibromomcthanc

Chloro ethane

2-Chlorocthylvinyl etherChloroformCliloromclhanc

1 ,2-Dichlorofacnzcnc1 ,3-Dichlorobemcnc

1 .4-Dichlorobeiiiene

1,1-Dichtoracthane1,2-DicMorocrtianc1 . 1-Dichlorocthcne

cii-1 ,2-Dii:hlon>ethcnc

tniixs-1 ,2-Dii;hlorocthcnc

1 .2-Dichlofoprtrpanccii-1 ,3-DichIoropropene

UTins-l ,3-Dichloropropcue

Eihylbcnicnc

Melhylcnc chloride

Sryp-'iie

1 , 1 ,2,2-Tctrachloroelhimc

Tcimchlorocthcnc

47.347.7

41.9

49.934.64».448.7

Source:96.9

47.0

52.2

4\.S

51.1

52.4

52.4

54. 1

ND

48.5

40.0

51.S

50.945.0

49.6

46.6

47.6

49.8

50,7

4l>.9

44.9

45.0

5S.6

56.7

56.0

51.0

55.4

5.00 uu/l

5.00

5.00

"ii

"

n

W311185-OT

5.00 ug/l

5.00

5.00

10.0

5.00

5.00

5.00

5.00

100

S.OO

10.0

5.00

S.UU

S.OO

5.00

5.00

5.00

5.00

5,00

5.0(1

5.00

5.00

5.00

5.00

5.00

S.OO

5.00

Prepared & Analyzed:50.050.0SO.O

50.0

50.0

so.aSO.O

Prepared & Analysed:SO.O

50.0

50.0

SO.O ND

50.0

SO.O

SO.O

50.0

SO.O

50.0

50.0 ND

50.0

so.ySO.O

50.0

50.0

50.0

50,0

50.0

50.0

50.0

50,0

50.0

50.0

50.0

SO.O

50.0

11/20/0394.6

95.483.SJ

99. 869.6V6.S97.4

46.7-16936-164

SI.S-146

75.0-13762.S-14S76.6-110fig.9-123

1 1/20/03194

94.0104

83.0

102

105

105

1US

97.080.0

103

102

MO.O

99.2

93.2

9SJ2

99,6

101

•59. S

89.8

90.0

117

113

112

102

111

39.3-165 H39.R-lg£>28.1-169

33.2-164

10-181

50.1-150

49-15736.1-I6S

80-120 1.

67.5-142

23.5-167

6S.3-13562.8-13062.1-130

46.7-142

6U.6-15133.7-U249.2-15548-137

44.6-171

28.6-195

40.6-17656.1-144

41.9-15431.1-169

43.9-1S6

29.1-160

Grea: Lakes Analytical-Oak Creek

flTin n-sula in Ms report apply to the samples analyzed in accordant.* with the chain i,fcustody document. This analytical report must be reproduced tn Its entirety.

-ndrea Stathas, Project Manager Page 13 of 29

12/02/2003 TUE 17 :04 [TX/RX NO 5084]


a.EâmmBcj.isa^B

"fil




Lake States Industrial Service3 1 1 E. Greenfield Ave.Milwaukee Wl. 53204

Project: MSCC Pro Treatment ListProject Number, (none]

Project Manager. Tom JucobsonReported:

12/02/03 17:03

Volatile Organic Compounds by EPA Method 624 - Quality ControlGreat Lakes Analytical— Buffalo Grove

Reporlini!Analyse Result Limit Uniu

Spike SourceLevel Result %REC

%RECLimits RPD

RPDUmit Notes

Batch 3110438 - EPA 5030B (T/T)

Matrix Spike (3110438-MS1)Toluene1.1,1 -TrichloroeUune

1 , 1 ,2-TriclUorocthaiie

Triehloroethcnc

TrichluruCluoromethancVjnyl chlorido

Surrogate: DlbromojluorometlianeSurrogate: 1 .2-Diclilnrotlhanc-J4Surrogate: Toluene-daSurrogate: 4-Bromafluorobfnztiie

Matrix Spike Dup (3H0438-MSD1)Qen7.cnc

Brumodichloromcthanc.ofurm

, ,uiomelhane

Carbon tctrachlorideChlnrebcnT.cne

ChlurodibromomethancChloroetliane

2-Chloro«thylvinyl ether

ChlorotbmiChloromahane

1 ,2-Dichlnrobcnzcne1 ,3 -Dichloro benzene1 ,4-DichIorobcnzcnc

1 , 1 -DicliJorocthuric

1 ,2-DichIoroelhane

l,l-Dlchloro«tbeue

cii-l ,2-Dichlorocthcneinrj- 1 ,2-Dichlorocthcnc1 ,2-DichJoropropane

cis- 1 ,3-Dichloropropcne

trans- 1,3-Dichloroprop cue

Hthylbcn^cnc

Mcthylcne chloride


OL^J^^*^

Source:90.849.546.055.346.7

43.1

SO.l3S.150.052,2

Source:91.046,552.8

41.2

4S.8

50.352.4

4'J.5

ND

47.5

38.0

51.7

49.744.3

48.0

47.3

47.1

49.2

40.il

47.5

44.6

44.4

57.0

55.4

W3 11 185-015.00 ug/15.00

5.00

5.00

S.OO

5.00

H

II

»

»

W3 11 185-01S.OO ug/1

5.W

5.00

10.0

5.00 "

5.00

5,005.00

100

5.00

10.0

5.00

5.00S.OO

5.noS.OO "

5.00

5.00

S.OO

5.00

5.00

5.00

5.00

5,00

Prepared & Analyzed:50.0

50.050.0

SO.O

50.0

50.0

ID. 1)

50.0

SO.O

SO.O

Prepared & Analyzed:50.0

SO.O

SO.O

50.0 ND

50.0

SO.O

SO.O

SO.O

50.0

50.0

SO.O ND

50.0

50.0

50.0

50.0

50.0

5(1.0

50.0

50.0

SO.O

50.0

50.0

50.0

- 50.0

11/20/03182

99.0<>2.0

111

93.4

86.2

IUU

76.8100104

S6.2-1S242.2-152

69.5-15513.5-180

12-173

21.5-165

7S.S-J2762.S-I457A.6-J306S.9-123

H

11/20/03182

93.0106

82.497.6

101

105

99.0

95.0

76.0

1(13

99.4

S8.6

97.8

94.6

94.2

08.4

99.6

95.0

89.2

S8.8

114

in

39.3-165

39.8-186

2«, \-169

33.2-16410-181

56.1-150

49-15736.1-168

80-12U67.5-14223.5-167

6S.3-135

62.S-13662.1-130

46.7-14260.6-1S1

38.7-142

49.2-155

4S-137

44.6-17123.6-10540.6-176

56.1-144

41.9-154

6.281.07

1.14

0.726

4.604.00

0.00

8.88

2.08

5,13

0.3S8

2.39

1.57

1.421,49

1,06

1.211.79

4.93

0.6701.34

2.77

2.32

38.2 H

34.2

35.5

33,8

37.5

17.S

29

4«

20 L

17.5

33.8

14.8

15.715.2

io.y16.V

23.5

18,6

20.132.4

43.6

39

24

23.8

The ivjults In thin repart apply to the samples analyzed in accordance with the clia-.i: r

-Oi

.ndrea Stathos, Project Manager Page 14 of:s>

12/02/2003 TUE 17:04 [TX/RX NO 5084] ©016

12/02/2003 IDE 5:11 FAl 4145709461 Great Lakes Analytical




Lake Stales Industrial Service3 11 E. Greenfield Avo.Milwaukee Wl, 53204

Project. MSCQ Pre Treatment ListProject Number: [none]


12/02/03 17:03


Aaislyte ResultReporting


SourceResult %B£C Limits RPD

RPDLimit Notes

Batch 3110438 - EPA S030B (PAT)

Matrix Spike Pup (3110438-MSD1)Slyrcnc

1.1,2.2-Temchloroethune

TcrnichloroetheneToluene

1.1.1 -Trichlorocthanc1.1,2-Trichloroethanc

Trichloroelhea*

TricMorofluoromethane

Vinyl chloride

Surrogate: Dihramo/luoromclhancSurrogate: l.J-Dichloruetnane-dlSurrogate: Toluene-dSSurrvgate: 4-

Source; W311185-0154.3 5.00 ug/1

31.4 . 5.00

53 2. 5.00 "

84.1 5,004X.7 5.00

46.7 5.00

53.2 5.00

46.3 5.00 "

41.4 5.00 "

Prepared & Analyzed: 11/20/0350.0

50.050.0

50.0

50.0

50.0

50.0

50.U50.0

42.SS1.432.2

50.0so.n50.050.0

109103

10616897.493.410692.682.K

98.0~8S.6103104

31.t-lfi9

43.9-18629.1-160

50.2-152

42.2-152

69.5-15513.5-180

12-173

21.5-165

JS.tS-12762.S-14576.fi-1306S.V-123

3.08

0.781

4.05

7.66

1.63

1.51

3.87

0.8604.02

46.4

33.3

32.32R.6

20.1

29.2

34.1

39.754.1

H

Great Lakes Analytical—Oak Creek The rcsulls In thLt report apply to the samples analyzed In accardanct with the chaincustody document Tills analytical report must be reproduced in lt.i entirety.

ndrea Stathas, Project Manager Page 15

12/02/2003 TUE 17:04 [TX/RX NO 5084]

12/02/2003 THE 5:11 FA1 4145709461 Great Lakes Analytical


140 East Ryan RoadOak Craek. Wisconsin 53154


Lake States Industrial Service311 E. Greenfield Ave.Milwaukee WI. 53204

Project: MSCO Pre Treatment ListProject Number: [none]

Project Manager Tom JacobionReported:

12/02/03 17:03

Organochlorinc Pesticides and PCBs by EPA Method 608 - Quality ControlGreat Lakes Analytical—Buffalo Grove

Armlytc ResultReporting Spike Source %R£C RPD

Limit Units Level Result %R£C Limits RPD Limit Nolm

Batch 3110462 - EPA 3510C

Blank (3U0462-BLK1)Aldrinnlphi-BHCbctu-BHCdellii-BHCgamiua-BHC (Lindanc)Chloixlanc (tech)

4,4'-DDD4,4'-DDE4. 4 '-DDTDieldrinEndosulfan 1Endosultvn IIGndosuli'aa sulfal^-

trinrin uldehydc

HcptachlorHepuchlor epoxideToxaphcncPCB-1016PCB-L221PCB-1232PCB-1242PCB-124SPCB-1254PCB-1260

Surrogute: Tetrachloro-mcta-iylcneSurrogate.: Oreachlorobiphcnyl

NDNDNDNDNDNDND

NDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1.210.364

Prepared; 11/20/03 Analyzed: 12/01/030.0300 ug/1

0.0200

0,0300 "

0.0300 "

0.0300

0.2*0

0.0400

0.0300 "

0.160

0.0300 "

0.0300

0.0500

0.100

0.100

0.150 "

0.0400

0.0200

O.SOO

0.500

0.500

0.500

0,500

0.500

0.500

0.500

I.OU 123 10-110 H

1.00 Jf,.4 10-140

Greut Lakes Analytical-Oak Creek

Siatbas, Project Manager

Tlic rvsulls in this report apply to the samples analyztd In aavordanr.r. with the choir. <-,fcustody document. TTii's analytical report must he reproduced in iu entirety.

Page 16 of 29

12/02/2003 TUE 17:04 [TI/RX NO 5084]


.' '-.-.ifinwm |

"ll:££• GREAT

LAKESANALYTICAL


Email: [email protected];414) 570-9460 FAX (414) 570-9461

Lake States Industrial Service3 11 E. Greenfield Ave,Milwaukee WT. 53204

Organochlorine

Analyte

Project: MSCG Pre Treatment ListProject Number: [none] Reported:

Project Manager TomJacobson 12/1)2/0317:03

Pesticides and PCBs by EPA Method 608 - Quality ControlGreat

Result

Lakes Analytical— Buffalo Grove

Reporting Spike Source V.REC RPDLimit Units Level Result %R3C Limits RFD Limit Notes

Batch 31 10462 - EPA 3510C

LCS (3110462-BS1)Aldrin

nlphn-BHC

b«a-BHC

dclta-BHC

Kumma-BHC (Luidane)

4,4--DDD

4.4--DDE

4.4 --DDT

Dicldrin

Endosulfan 1

EnJosulfun 11

Endosul£in sulfute

Endrin

'« aldehyde

jchlor

Hcptuchlor cpoiidc

Surrogate: Tetrachlnrn-nieta-jylene

Surrogate: Decochtoroblphenyl

LCS (3110462-BS2)PCB-1016

PCB-1260

Surrogate; Tctrachloro-tn4ta~3ylt.nl'.

Surrogate: Dccachlorablphiinyl

LCS Dup (3110462-BSDl)Aldrin

ilpha-BHC

beia-BHC

dclta-BHC

gamma-SHC (Lindanc)

4.4'-DDD

4.4'-DDE

4,4'-DDT

Dieldrm

Endosulfbn I


0.292

0.185

0.243

0.515

0.141

0,296

0.20S

0.260

0.296

0.238

0.22H

0.277

0.230

0.250

0.190

0.287

0.737

0.454

4.44

3.77

O.rtJ-/0. 1 7.5

0.320

0.206

0.27V

0.646

0.192

0.381

0.255

0.327

0.364

0.283

Ci

Prepared: 1 1/20/03 Analyzed 1 1/25/03U.0300 ug/1 0.300 97^ 24.4-121

0.0200 " 0.300 6!.T 25.7-118

0.0300 " 0.300 81.0 28.2-124

0.0300 " OJOO 172 26.6-117 H

0.0300 " 0.300 47.0 26.4-120

0.0400 " 0.300 9S.7 29.9-154

0.0300 " 0,300 69-5 22-129

0.160 " 0.300 86.7 10-168

0,0300 " 0.300 S8.7 44.4-128

0.0300 " 0.300 7-J^ 27.7-126

O.OS(X) " 0.300 76.0 44-126

0.100 " 0.300 92-3 45-125

0.100 " 0.300 76.7 34.3-1 56

0.150 " 0.300 83J« 37-12S

0.0400 " OJUO 63.3 32.1-122

0.020Q " 0.300 95.7 25.7-134

1.00 73.7 10-110

1.00 O.< 10-140

Prepared: 1 1/20/03 Analyze: 12/01/030.500 ug/l 5.00 8S.5 21.8-110

0.500 " 5.00 75.4 22-113

1.00 6}.* 1(1-110l.oo ;-.; 10-140

Prepared: 1 1/20/03 Aniilyrrc: 1 1/25/030.0300 u£/l 0.300 1" 24.4-121 9.15 67.6

0.0200 " 0.300 S5.- 25.7-118 10.7 66.4

0.0300 " 0.300 93.?. 28.2-124 13.8 57.1

0.0300 " 0.300 :i5 2fi.G-117 22.6 54.5 H

0.0300 " 0.300 6J..C 26.4-120 30,6 61.5

0.0400 " 0.300 i:- 29.9-154 25.1 84.4

0.0300 " 0.300 <.'.: 22-129 20.3 81.3

0.160 " OJOO 1C? 10-168 22.8 83.5

0.0300 " 0.300 121 44.4-128 20.6 63.8

0.0300 " 0.300 9-iJ- 27.7-120 17.3 76.1

77>o result! in thLi report apply lu tat x^nples analyzed in accordance with the cliiin acustody document. This analytical r^trf. must be reproduced in ia entirety.

jidrea Stathas, Project Manager Page 17 of 29

12/02/2003 TVE I [TX/RX NO 5084]

12/02/2003 TUE 5:12 FAA 41457094B1 wear Lakes Anaiyucai




Lake States Industrial Scrvlctf

3)1 E. Greenfield Ave.Milwaukee WI, 53204

Project: VISCG Pre Treatment List

Project Number [none]


12/02/03 17:03

Organochlorine Pesticides and PCBs by EPA Method 608 - Quality ControlGreat Lakes Analytical—Buffalo Grove

Annlyte ResultReporting

Limit UnitsSpike SourceLevel Result

%REC%REC Limit. RPD

RPDLlnilt Notes

Batch 31 10462 - EPA 3S10C

LCS Dup (3110462-BSD1)Endoiiulfan 11

Endosulfiin aulfaic

Endrin

Entirin Aldehyde

Hepuichlor

Heptachlor epoxidc

Surrogatr.; Tctrachhra-meta-Xyltnt

Surrogate: Dtcachlorobiphtnyl

LCS Pup (3110462-BSD2)PCB-1016

PCB-I2SO

Surrogate: Tetrachluro-meta-xylvnc<?'€rrof;att; Dccuchlornblphtnyl

0.297

OJS4

0.305

0.3 IS

0.230

0,337

0.740

0.672

4.32

3.14

0.5400.149

0.0500 ufc/1

0.100

0.100

0,150

0.0400 "

0.0200 "

"H

0.500 ufi/l

0.500

na

Prepurcd: 1 1/20/030.300

OJOO

0.300

0.300

0.300

0.300

/.OO

7.00

Prepared: 1 1/20/035.005.00

1. 001.00

Analyzed: 1 1/25/0399.0 44-126

118 45-125

102 34.3-1 56

105 37-128

76.7 32.1-122

112 2J.7-134

74.0 10-11067.2 IO-J40

Analyzed; 12/01/0386.4 21.8-110

ft2.8 22-113

S4.0 10-11014.9 10-140

26.3

24.4

28.0

23.0

19.0

16.0

2.74

18J2

63.9

56.6

53.3

77.8

50.3

63.5

71

86.3

Great LaJtes Analytical-Oak Creek The results In tin's report apply to the samples analyzed in accordance willi the chair, ofi-imtady document. Tills analytical rvpurt must be reprnduccd in its entirely.

.adrea Statbas, Project Manager Page 18 of 29

1 2 / 0 2 / 2 0 0 3 TLTE 17:04 [TX-'RX NO 5084)

12/02/2003 TUE 5:12 FAX 4145709461 Great Lakes Analytical IP21/U3Z

&Kiim

l





3 11 E. Greenfield Ave.Milwaukee Wl, 53204



12/02/03 17:03


AnalyteReporting SpiVe Source V.REC RPD

Roult Limit Units Level Result %REC Limits RPD Limit Note;

Batch 3110424 - EPA 3510C

Blank (3110424-BLK1)Acenuphthcne

Acun.iplithylene

Anthracene

Benzidinc

Bcnz (u) anthracene

Denzo (a) pyrcne

Benzo (b) fluuranthcneBciizo (glii) paylene

Bcnzo (K) fluorauthene

Bi.s(2-ch!orocthoxy)tnethaiie

Bis(2-chlorocthyl)ethcr

Bis(2-chloroisopropyl)cther

Bis(2-cthylhcxyl)phthalalc

•jmophcnyl phcnyl ether

j\ benzyl phthalatc4-Chloro-3-melhylphenol

2 -Cliloronnphlhaleue

2-Chlorophcnol

4-Chlorophcnyl phetiyl etherChrysencDiben^ (u.h) unthmccnc

1 .1-Dichlorobenzenc

1 ,3-Dichlorabcn2eae

1 ,4-DichIorobcnzeue3,3 '-CJichlorobcnzidine

2,4-DichlorophcnolDieUiy! phlhabtc

2,4-Dimetliylphenol

Dirnahyl phthalate

Di-n-butyl phthalale

4.6-Dinitm-2-mcthylphenol

2.4-Duiicrophcnol

2.4-Dmitrololutnc

2,6-Duiitrotoluene

Di-n-oetyl phthalate

NDNDNDNDNDND

NDNDNDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Prepared: 11/19/03 Analysed: 11/21/0310.0 ug/1

10.0 "

10.0

50.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0 "

10.0

10,0

10.0

10.0

10.0

10.0

10.0

20.0

10.0

1 0.0

10.0

10.0

10.0 "

sn.oso.o10.0

10.0 "

10.0 "

Great Lakes Analytical—Oak Creek The i-e.tulls In this report appfy to the samples analyzed In accordance with the chain ujtoeumunt. Thii analytical report must be reproduced in its entirety.

Statha.s, Project Manager Page 19 of 29

12/02/2003 TUE 17:04 [Ti/RX NO 5084]


££• GREAT{LAKESI ANALYTICAL



Lake States Industrial Service311 E. Greenfield Ave.Milwaukee WT, 53204


Project Manager Tom JacohiOnReported:

12/02/0317:03


AnalylcRcporling Spike Source %R£C RPD

Rcaiult Limit Unili Level Result %REC Limits RfD Limit Nni«


Blank (31 TO«.i-BLKl)Fluonmthenc

Fluorenc

Hetachlorotwru.cn e

HcxnchlorobutadieneHcxnch1nrocyclopcn(adleii«Hcxuchlorocthane

Iiideno (1,2,3-cd) pyrcnc

Isophorone

Naphthnlaic

Nitrobenzene2-Niliuphenol

4-NilrophaiolN-N itrosodim«lhy1ajnine

' itrosod i-n-propylauiine

.<Iitroii<xljphenylamincPentachlorcptiaiot

Phcnamhrcue

Phenol

Pyrcne1 ,2,4-Trichlorr>ben7,cnc2,4,6-Trichlorophcnol

Surrugul*: 2-FluornphenolSurrogate: Phc.nol-46Surrogate: Nltrobtnztnr-J5Surrogate: 2-FluorobiphenylSurrogate: 2,4,f,-Trlhroir\opheno\Surrogate: p-Tcrphcn)>I-<114

ND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

ND

9.16S.4X

17.416.532.S17.4

Prepared: 11/19/03 Analyzed: 11/21/0310.0 ug/l

10.0

10.0

to.o20.0

10.0

10.0

10.0

lo.o10.0

10.0 "

50.0

10.0

10.0

10.0

so.o10.0

10.010.0

10.0

10.0

125 7.3 J 10-110 LI2S 4,3$ 10-110 L

62.S 27.S 11.4-110 L62.5 26.4 H>-nO125 2fi.O 10-11062. S 27.3 10-147

Great Lakes Analytical-Oak Creek Tfif resula in this report apply lo ll'f sample* analyzed in accordance with the chair, .ifcustody document. Tills analytical report must bf reproduced in Its entirety.

Andrea Stathas, Project Manager Page 20 of 2?

12- / 02 /2003 TUE 17:04 [TX/RX NO 5084] Iffl 0 '12

12/02/2003 TIE 5:13 FAl 4145709461 Great Lakes Analytical




Lake States Industrial Service311 E. Greenfield Awe.MilwauVeeWI. 53204

Project: MSCG Pre Treatment ListProject Number [none] Rcporud:

Project Manager: Tom Jacobson 1 2/02/03 1 7:03


AnulytoReporting

Result LimilSpike Source %REC RPD

Units Level Result %REC Limits RPD Limit Notes

Batch 3110424 - EPA 3510C

LCS (31KM24-BS1)Accnaphthcnc

Acenaphlhylene

Anthracene

Bcnzidiiie

Bcn7 (s) anthracene

Boi7.o (») pyrcnc

Bcnio (b) flunnmhcne

Benzo (ijhi) pcrylcne

Bcnzo QO fluoranlhene

Bi.i(2-cnlnrocthoxy)me<hane

B is(2-chtoTOcthyl)cthcr

B is(2-ch kmjisopropyl)cthcr

B is(2-elhyUlexyl)phlhiilutc

romopkenyl plienyl dher

>y\ bcnTyl plithal.Me

4 -Chloro-3-methylphcnoI

2-Chloronaphtluilcne

2-Chlorophcnol

4-Chlorophenyl phenyl ether

Chryscnc

Dibcoz (n,h) anthracene

I .2-Dichlorobenzenc

1 ,3-DicUlorobeiitene

l,4.DicMorob*rc«ne:

3,3'-Di't;hlorobeniid£ne

2.4-Dichlorgphcnol

Diclhvl phthalalc

2.4-Dimcthylphcnnl

Dimethyl phlhaljte

Di-n-b(jlyl phlhulutc

4 /,- D i r i tro-2-uielliylphenOl

2,4-Dmirroph.cilol

2 T4-Dinitn7tti!ucnc

2.6-Dinilrotolucnc

Di-n-oclyl phlhalatc


/ i ^ 1\ 1 -rt-lUlr^&lLgfi &77ft»2rÂ

Prepared: 11/19/03 Analyzed: 11/21/0316.6

17.1

20.6

8.71 -24.A

27.9

24.2

20.1

28.2

8.40

1.37

0.770

24.2

19.4

24.f.

15.5

13.4

ND17.6

23.3

21.4

ND

ND

ND

25.G

9.07

23.0

8.07

20.6

24.3

22.0

11.3

20.X

19.8

22.8

10.0

10.0

10.0

5.00

10.0

10.0

10.0

10.0

10.0

1.00

1.00

0,100

10.0

10,0

10.U

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

20.0

1.00

10.0

1.00

10.0

1 0.0

5.00

5.00

10.0

10,0

10.0

ug/1 25.0

25.0

25.0

25.0

25.0

25.0

" 25.0

25.0

25.0

25.0

" 25.0

25.0

25.0

25.0

25.0

25-0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

67.2 10-114

68.4 13.6-114

82.4 14.7-115

34.8 70-130 L

98,4 20.5-124

1U 17.2-121

96.8 13.6-136

80.4 10-104

113 13.2-128

33.6 14.4-112

5.4.S H.5-110 L

3.04 10-113 L

96.8 10-159

77.6 14.6-11 K'

98.4 10-164

62,0 10.8-113

53.6 10-110

U.4-110 L

70.4 12.6-117

93.2 10-110

85.6 10-148

1U-11U E

10-110 L

10-110 L

102 10-110

36.3 10.2-112

92.0 16.2-121

32.3 10-110

S2.4 1X-122

97.2 20-120

88.0 10-129

4S.2 10-123

83.2 12.5-126

79.2 U.3-127

91.2 16-122

The results In this report apply to the samples analyzed In accordance vitll llic chair. <custody document. This analytical report mull bt reproduced in lit entirety.

<£=>


1 2 / 0 2 / 2 0 0 3 TVE 1 7 : 0 4 [TX/RX NO 5084]

1 2 / U 2 / 2 U U 3 TDK u: i3 I'M 4i4b7084tii wear Lakes Analytical

KKJKE3H

"HIGREATLAKESANALYTICAL

140 East Ryan Road —Oak Creek, Wisconsin 53154




Milwaukee WI, 53204

Project MSCG Prc Treatment List


Project Manage^ TomJacobson

Report »d:

12>02/03 17:03



Limit UnitsSpike SourceLevel Result %REC

•/.RECLimits RPD

RPDLimit Notes


LCS (3110424-BS1)Fluoraiitheiie

Fluorcnc

Hcxuchlcirpbcnzenc

Hexjuhlurubutadienc

Hexachlorocyclopcntadicnc

Hexacliloroelhanc

Indcno (1 ,2,3-ed) pyrene

LsnphoTOnc

Nuphthulcnc

Nilroboiiene

2-Nitrophcnol

4-Nicnophcnol

N-Nitrowidimcthylavninc

''Irosodi-n-propylaminc

ilrosodiphaiyluminc

Pcntaehloropheaol

Phcnanthrcnc

Phenol

Pyrcnc

1 ,2,4-Trichlorobenzene

2,4/>-Trichlorophenal

Surrogate: 2-FluorophtnolSurrogate: fhrnal-clfiSurrogate: Nitrnhen2enc-45Surrogate: 2-FluorobiphcnytSurrogate: 2,4, 6-Tribromophtnnl

Surrogate: p-'l'erphenyl*d 1 4

19.7

19.2

20.0

0.810

3.79

ND

21.5

13.4

4JS

3.84

5.27

A.Al

ND

9.75

21.5

20.2

21.4

0.600

22.4

2.76

10.0

fl.UO0.790

3.4313.2

3S.1

22.1

10.0 ug/1

10.0

10.0 "

0,100 "

2.00

10.0

10.0

10.0

1 .00 "

1. 00

1. 00

5.00

10.0 »

1. 00 "

10.0

5.00

1 0.0

0.100

10.0 "

1 ,00

10.0

••"

"*«

"

Prepared: 11/19/03

25.0

25.0

25.0

25.0

25.0

2S.O

25.025.0

25.0

25.0

25.0

25.025.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

12512562.S

fil.S125

62.5

Analyzed:7X.8

7fi.S

80.0

3.24

15.2

86,0

53.6

17.4

15.4

21.1

26.4

39.0

86.0

80.8

85.0

2.40

89.6

11.0

64.0

0.6325.4921.1

2&.135.4

11/21/0316.1-118

13.4-115

12.6-116

10-110

10-110

10-110

10-155

ll.S-110

10-111)

11.1-112

10-114

10-110

70-130

11-3-113

15.4-110

10-123

16,9-116

10-110

10-173

10-110

10-130

10-11010-110

31.4-1IQ10-11010-110

lfl-147

L

L

L

L

L

LL

Great Lakes Analytical—Oak Creek The results in this report appfy to the samples analyzed In accordance with ilia chain c:custody document. This analytical report must bv rrprutluctd in its entirtn.


12/02/2003 TUE 17 :04 [TX/RX NO 5084] E 0 2 -1

12/U2/UUU3 TUK b:i3 I'M 4i4b70U4Bi wear Lanes Analytical





3 11 E. Greenfield Avc.Milwaukee WI, 53204

Project MSCG Pre Treatment ListProject Number [none]

Project Manager. Tom Jacobson

Base/Neutrals and

Reported:

12/02/03 17:03

Acids by EPA Method 625 - Quality ControlGreat Lakes Analytical— Buffalo Grove

AJialyte ResultReporting

LimitSpike

Units LevelSourceResult %REC

%R£C RJPDLimits RPD Limit Notes

Batch 31 10424 - EPA 3510C

Matrix Spike (3110424-MS1)Acenuphthene

AcenaphlhyleneAnthracene

BcnzidineBc»7. (») anthracene

Bcnzn (n) pyrcne

Beiua (b) fluonmthoie

Benzo (glii) perylene

Bciuo (X) iluorantheneBij(2-chlgrocthoxy)mctlw>cDii(2-chloroethyl)cihcr

Bis(2-ch loroii;upropyl)cthcr

B is(2-elhylhexyl)]»hlhalate

rornophenyl pheuyl elher.yl benzyl phthalatc

4-Chloro-3-meihyTphcnol

2-ChIoronapblhaIene

2 •Cklorophoiol

4-Clilorophcuyl pheuyl etherChryscnc

Dibcm: (u.h) unthracene

1 .2-Dichloroben2ene

1 ,3 -Dichlorobenzene

1 .4-DichJorobejizene

3 ,3 '-Dichlorobciizidine

2,4-DichlornphcnolDiclhyl phthulmc

2 .4-Dimelhylphenol

Diiuelhyl phlhalaleDi-ii-butyl phlhalale

4,r>-Dimtro-2-mctljylph«uol

2,4-Dinitmphcnol

2,4-Dinitrulolucnc

2.6-Dinilrotulucnc

Di-u-oclyl phlhabtc


f I *l *\S1 -4-,UMsPU^? tZTtZTW-fa*

Source: B311229-04 Prepared:19.320.122.14.1421.823.821.9

12.325.S19.1IK.O

21.6

22.4

20.4

25.6

17.C.

17.9

12.5

18.8

20.9

lft.3

15.1

14.1

14.8

18.3

15.1

23,9

11.6

20.9

24.4

22.6

19.2

21,5

20.7

21.4

10.010,010.0

0.50010.010.010.010.0

10.010.0

10.0

10.0

10.0

10.010.010.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10,0

2.0010.U

10.0

10.0

10.0

10.0

5.005.00

10.0

10.0

10.0

ug/1 25.025.025.025.0

25.0

25.0

25.0

25,0

" 25.025.0

25.0

25.0

25.0

25.025.0

25.0

25.0

25.0

25,0

25.0

25.0

25.0

25.0

25.0

25.025.0

25.0

25.0

25.0

25.0

25.025.0

25.0

25.0

25.0

11/19/03NDNDNDNDNDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Analyzed:77.2

K0.4

88.4

16.6

87.2

95.2

87,649.210276.472.086.4

89.6

S1.6

102

70.4

71.6

50.0

75J2

83.6

65.2

60.4

56.4

59.2

73.2

60.4

95.6

46.4

S3 G

97. Ci

90.4

76. S

86.0

82.8

N5.6

11/22/0370-130

70-13070-130

70-130 L70-130

70-130

70-130

70-130 L70-130

70-130

70-130

70-130

70-130

70-13070-130

70-130

70-130

70-130 ' L

70-13070-130

70-130 L

70-130 L

70-130 L

70-130 L70-13070-130 L

70-130

70-130 L70-130

70-130

70-130

70-130

70-130

70-130

70-130

'file results in thii report apply to tfl<: sampUs analyzed in ucvurdance with the clia:n rcu.itady document. TTi/j analytical report must bv reproduced in ia entirely.

•O


1 2 / 0 2 / 2 0 0 3 Tl'E 1 7 : 0 4 [TX/RX NO 5084]


Ss^M GREAT[LAKESI ANALYTICAL



Lulto Stutcs Industrial Service

3II E. Greenfield Avc.Milwaukee WI, 53204

Project: MSCQ PnsTreatment ListProject Number, [none]

Project Manager: Tom JncobsonReported:

12/02/03 17:03


AnMytcReporting

Result Limit Unit*SpikeLevel

SourceResult V.REC

%RECLimits RPD

RPDLimit Note;

Batch 3110424 - EPA 3510C

Matrix Splice (3110424-MS1)FtuomitheneFluorcncHexuchlorobcnzcnc

HcxuuhlorohutadicncIlexacliloiocyclopcntadiene

Hexachloroclhanc

Indcno (1 ,2,3-cd) pyieneIsophoront

Naphthalene

Nitrobenzene

2-Nitrophcnol

4-NicrophcnolN -Ni tnwodimcthylnminc

litrusodi-n-prnpylamincNilrosodiphenyluininc

PcnCachlorophenol

Phcnunthrcne

Thenol

Pyrcuc

1 ,2,4-TricUlorobenzene

2,4,6-Trichlorophcnol

Surrogate: 2-FluorvphcnolSurrogate: Phenol-<ISSurrogate: Nitrohenz*ne-d5Sufragata: 2*f'°tuoroblph<i/ist

Surrogate: 2,4,6-TribnmophenalSurrogate: p-Terplicnyl-d 1 4

Source:21.3

21.4

19.6

13.1

9.77

15.316.0

18.9

17.6

20.0

16.V

6.60

6.80

22. L

23.5

21.2

22.6

2.74

21.114.7

16.4

9.24S.SVJS.S17.737.216.7

B3 11 229-0410.0 ug/1

10.0

10.0 "

10.0

0.00

10.0

10.0 "

10.0

10.0

10.0

10.0

5.00 "

1.00 "

10.0

10.0

s.oo10.0

1.00

10.010.0

10.0

"'•»""'•

Prepared:25.0

25.0

25.0

25.0

25.0

25.025.0

25.0

25.0

25.025.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

115

11562.5

f>2.5

12562. 5

11/19/03ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Analyzed:S5.285.6

78.4

52.4

39.1

61.2

64.0

75.6

70.4

KO.O

67.6

26.4

212

88.4

94.0

84.X

90.4

11.0

84.4

58. 865.6

7.394.7130.128.32V.816.7

11/22/0370-130

70-13070-13070-130

70-130

70-130

7y-13070-130

70-130

70-130

70-130

70-130

70-13070-130

70-13070-130

70-13070-130

70-13070-130

70-130

10-1 It)10-110

31. 4-1/1110-110

10-11010-147

LLL

L

L

L

L

L

L

L

L

LL


/] rtltJ>AL0?

Tilt results in this report apply to the lamri/t.i analyzed In accordanct with the chair, ofcustody dneumf.nl. This analytical report miat br. reproduced In Its enlirtly.

Andnra Stathas, Project Manager Page 24 of 2:

12/02-'2003 TUE 17:04 [TX/RX NO 5084]


££• GREATLAKES

I ANALYTICAL140 East Ryan Road

Oak Creek. Wisconsin 53154Email: [email protected]

(414)570-9460 FAX (414) 570-946T

Lake Slates Industrial Service3 1 1 E. Greenfield Ave.Milwaukee WI, 53204


Project Manager Tom Jacobson

Base/Neutrals and

Anulytc

Great

Remit

Reported:12/62/03 17:03

Acids by EPA Method 625 - Quality ControlLakes Analytical— Buffalo Grove

ReportingLimit

SpikeUnits Level

SourceResult %REC

%R£CLimiLl RPD

RPDLimit Notes

Batch 3110424 - EPA 3510C

Matrix Spike Dtip (3110424-MSD1)Accn.iphtheneAecnapMhylcnc

Anthracene

Betuddine

Bcnz (»} anthracene

Bcn^.o (a) pyrcnc

Dcnzo (b) flunranthcnc

Beiuo (jîi) perylene

Benzo (k) fluoranthenc

Bis(2-chloroethoxy)mcthanc

Bi.s(2-chlorncthyl)cthcr

Dis(2-chloroi»opropy1)cthcT

Bis^-elhylhexyOjrtithalate

rouiophenyl phenyl ether

.yl benzyl phlhalate

4-Chlorr>-3-mcthylplicnol

2-Chloruiuphthulenc

2-Chlorophcnol

4-Chlofophenyl phenyl ether

Cliryscnc

Dibcnz (n,h) » nth race ac

1 ,2-Dich!on)bcn7:ene

1 ,3-Dichlorubcrttene

i ,4-DichlorobcnzcTic

3 .3'-DichlorobenzicJine

2 .4 - D i ch 1 oroph enol

Diclhyl phthahitc

2.4-DimcLhylphcnnl

Dimethyl phlhalale

Di-n-butyl phthuhitc

4,G-Diniuo-2-rae(hylpb.enol

2,4-Dinirrophciiol

2.4-Dinitrscolucns:

2.6-DmilTotoluenc

Di-n-octyl phlhulutc


Source: B311229-04 Prepared: 1 1/19/0317.117.618.14,14

18.2

18.7

16.5

12.3

ND1K.O

10.4

20.2

19.1

16.9

20.9

16.4

16.1

12.2

16.4

17.6

15.5

14.3

13.7

11.4

15.2

14.5

20.3

13.4

18.4

18.9

19.5

14.0

I8J2

17.6

18.3

10.0

10.0

10,0

O.SOO

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10,0

10.0

10.0

10.0

10.0

10.0

10.0

2.00

10.0

10.0

10.0

10.0

10 05.00

5.00

10.0

10.0

10.0

ug/1 25.011 25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

" 25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

2S.O

25.0

25.0

25.0'

25.0

25.0

25.0

25.0

25.0

25.0

25.0

ND

ND

ND

ND

ND

ND

NDNO

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Analyzed:68.470.472.4

16.0

72.8

74.8

66.0

49.2

72.0

41.6

SO.S

76.4

G7.6

83.6

65.6

64.4

48.8

65.6

70.4

62.0

57.2

54.8

45.6

f.0.8

58.0

81.2

53.6

73.6

75.6

78.0

56.0

72.8

70.4

73.2

11/22/0370-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

12.1

13.3

19.9

0.00

18.0

24.0

28.1

0.00

S.93

53.5

6.70

15.9

18.8

202

7.06

10.6

2.43

13.6

17.1

5.03

5.44

2.8S

26.0

18.5

4.05

16.3

14.4

12.7

25.4

14.7

31.3

16.6

lfi.2

15.6

20 L202020 J,

20

20 H

20 LH

20 L

20 L

20

20 LH

20

20

20 L

20 11

20 L

20 L

20 L

20 L

20

20 L

20 L

20 L

20 LH

20 L

20 L•JO

20 L

20

20 H

2U

20 LI1

20

20

20

Thu rvsulu in this report apply to Ihi: samples anafyitd in accordance with lh>! chain -jfcustody document. This analytical report must he reproduced In Its enllnly.

• 3


12/02/2003 TUE 17:04 [TX/RX NO 5084]





Lake S tut CM Industrial Service


Milwaukee Wl. 53204

Project; MSCG Prc Treatment List


Project Manager Tom Jacobson 12/02/03 17:03


Analyte Resultfcportias

Limit UnitsSpike SourceLevel Remit %R£C

•/.RECLimits RPD

RPDLimit Notes


Matrix Spike Dup (3110424-MSD1)Fluoranlhenc

Fluorcnc

HcxachloKibcn£cnc

HcxachlorDbutadienc

Hexachlarticyulopcntaidiene

Hcxachloroelhaae

Indcno (1.2.3-cd) pyrene

Isiiphoronc

Nviphlhulcnc

Nitrobenzene

2-Nitroplienol

4-NUrophcuol

N -N i irosod i mcthylamine

!i(roxodi-n-ptY>py1aniinc

Nilrosodiphenylutnine

Pcniachlorophenol

Phcnunthrcnc

Phenol

Pyroic

1 ,2,4-Trichlorobenzcne

2.4,6-Trichloropheaol

Surrogate: 2-Flnorophtnol

Surrcigute: Phenol~d6

Surrogate: Nitroh€nzer\c-d5Surrogate: 2-FluorobifjlicnylSurrogate: 2.4. 6-TrjbromophcnolSurrogate: p-Terphenyl-dl 4

Source: BM 1229-0416.31H.516.2

13.18.80

\S.S15.017.616.318.315.76,245.4920.419,418.6IS.52.K516.513.815.3

9.4S6.0517.2If]. I32.114.8

10,0 ug/1

10.0

10.0 "

10.0 "

2.00

10,0

10.0

10.0

10.0

1 0.0

iti.o

5.00

1 .00

10.0 "

10,0

5.00

10.0

1.00

10.0 "

10.0

10.0

-"It

"""

Prepared: 11/19/0325.025.025.025.025.0

25.0 -

25.0

25.0

25.0

25.0

25.0

25.0

25,0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

125125f>2.562. 5

12162.5

ND

ND

ND

NDND

•ND •

NDNDNDNDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Analyzed: 11/22/03

65.274.064.R

S2.435.2

• 62.060,070.465.273.262.825.022.081.677.674.474.011,466.055.261.2

7.554.8427.525.825.723.7

70-130

70-130

70-130

70-130

70-130

•70-130 •

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

10-11010-110

31.4-11010-11010-/IO

1(1-147

26.6

14.5

19.0

0.00

10.4

•1.-30-

6.45

7.12

7,67

S.«8

7.3ft

5.61

21.3

8.00

19.1

13.1

20.0

3.94

24.5

6.32

6.94

20

20

20

20

20

- 20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

LL

L

LH

L

L

L

L •

L

L

L

L

LH

LLHI,L

Great Lakes Analytical—Oak Creek 77ic results in this report apply to the samples analyzed in accordance with the chulrcustody document. '1'hLi analytical report tnusl be reproduced in lu entirety.

Andrea Stathas, Project Manager Page 26 of :r

12/02/2003 Tl'E 17:04 [TX/RX NO 50S4] ®0-

12/02/2003 TDK 5:14 FAl 4145709461 Great Lakes Analytical

z33ia2;«H

"HiGREATLAKESANALYTICAL

140 East Ryan RoadOak CreeX. Wisconsin 53154



311 E. Greenfield Ave.Milwaukee Wl, 53204

Project: MSCG Pro Treatment ListProject Number, [none]Project Manager: Tom Jacobscm

Reported:12/02/03 17:03

Tentatively Identified Compounds by GC/MS EPA Method 8270 - Quality ControlGreat Lakes Analytical—Buffalo Grove

AnnlylsReporting

Result Limit UnitsSpike SourceLevel Result %R£C

%REC RPDLimit* RPD Limit Notts

Batch 3110424 - EPA3510C

Blank (31KM24-BLK1)l,2,4,S-Tctnicrilomt>en7cnc

3 J'-Dich lorobcnxidine

FcmnchlorobeuzaieNone

Surrngate: p-Terphcnyl-fll4Surrogate: 2.4.6-TribromoplitnalSurrogate: 2-riuoroblpHt.nylSurrogate; Nltfobcmcne-d5Surrogate: fhcnal-tlSSurrogate: 2-/rluaraphtnol

LCS(3I10424-BS1)3.3'-Diehloruben7.idine

S"rrugate: p-Terp1:enyt-dl4âtt: 2,-t.f>-TrU>ronv>phanol

• •agate: 2 -FtuorobiphenylSurrOgulK: Pt'itrubenzenf-d5Surrogate: Phenol-d6Surrogate; 2-Fluorophenot

MatrL\ Spike (3110424-MS1)

Surrogate: p-Tertihvnyl-dHSurrvgulv: 2. 4, fi-TrihramnphcnolSurrogate: 2-FluoroblphcnytSurrogate: f,'ltrobt!nzcnc-J5Snrrv%cjte: Phcnol-d6Surrcfate: 2-ftunrophp.nol

ND 20.0 us/1ND 20.0ND 20.0

ND 20.0

17.4 "32.5J6.SIT.4S.4S9.16

27.1 20.0 ue/1

22.135.1 "13.23.43

0.790 "(J.VO

Source: B3 11 229-04

76.7 ug/l37.217.7lfi.ltf.899.24

Prepared: 11/19/03

62. }12562J

62.312S

125

Prepared: 11/19/03

62.5125

62.562.5125

125

Prcpmcd: 11/19/03

62.5125rtJ.562.512512S

Analyzed:

^7.826.026.427.84.387.33

Analyzed:

35. 428.12 J.I5.490.632

AnnJyvced:

26.729.S28.3JO.'4.717.39

11/21/03

23-yH10-15931-36 L19-89 L10-83 L10-124 L

11/21/03

23-98IO-15'J31-86 L29-KO LIO-S3 L

10-124 L

1 1/22/03

23-98ia-IS')JI-SO L29-5910-33 L10-124 L

Great Lakes Analytical—Oak Creek The mulu in this report apply la the samples analyzed In eccorclanmt with tlm cliai<custody document. This analytical rtjinn must be reproduced In its entirety.

Stathas, Project Manager Page 27 of

12/02.'2003 TIT 17:01 [TX/Ri NO 5084]

12/02/2003 M 5:l& KAJL 414570H4G1 Great LaKes Analytical IffllW/UM

ff^Ty*-fr j^ HB

llGREATLAKESANALYTICAL



Luke States Industrial Service311 E. Greenfield A.VC.Milwaukee \V1.53204

Project: M SCO Pre Treatment ListProjccc Number: [none]Project Manager. Tom Jacobson

Reported:12/1)2/03 17:03

Notes and Definitions.

A-01 this tmulytc was quantised using an open scan.

QC The result for one or more quality control measurements associated with this sample did not rneet the laboratory and/or sourcemethod acceptance criteria.

DET Analylc DETECTED

ND Analylc NOT DETECTED ac or (ibovc tlie reporting limit

NR Not Reported

dry Sample results reported on a dry weight basis

RPD Relative Percent Difference

L This quality control measurement Is below the laboratory established limit

H This quality control measurement is above the Uhonuoiy cjt»blijhcd Unlit,

Great Lakes Analytical-Buffalo Grove Wisconsin DNR Certification Lab ID: 999917160

Great Lakes Analytical-Buffalo Grove NELAP Primary Accreditation: Illinois #100261


•"••real Lakes Analyiical-Oak deck, Wl Wisconsin DNR Certification Lab ID: 341000330

cat Lakes Analytical-Oak Creek, WI NELAP Primary Accreditation: Illinois #100307

Note: For analyses that require NELAP accreditation, all analytes, by matrix and method, ore accredited following current NELAPstandards unless specifically noted by way of a qualifier listed above.


UU !A#?The results in Ihti report apply to th*sample* analyzed in accordance wir/i tiia chain <cuslaJy document. This analytical report must be reproduced In Hi cntlrvly.

.Andrea SUthas, Project Manager Page 29 of 2-

12 /02 /2003 TUE 17:04 [TX/R.X NO 5084] ©031

1 LKJiU.t II .Hit

ANALYTICAL

3J

C//ent:

/Address. 3//

roject Name:

ZJ

OMMENTS:

<

P/)oneFax »:

PID:

P/D:

HO:

PiD:

PtD:

P;D:

P/D:

PtD:

(&47) 608-7766FAX (B47) B08-7772

(414) 570-9460FAX (414) 570-9461

/Address;

StefefiProgram:

Phone it: (

tfofSofflesPreservative Used

w

WT: STD. 4 DA/ 3 D/^Y 2 DAY t OAV V24 HflS,/

Q YES-TATiscrilical

D NO-TATisnolcirScal

Received:O ambient

Deliverable Package:

D STO d Other

rafrigafatoi

C^VgjtiftS.,OATEHKULrSNESKD:

Temp. Upon Receipt:

DefivyyMel/iod:

GLA^KLCliert 0 Shipped D Courier D

TIME

If

RELINQUISHED

RELINQUISHED

DATE

DATE

7

LABORATORY

ID NUMBER

RECEIVED DATE

JJJWE

RECEIVED

j r faJJfcL^ OF

oin

U

noo

o

CM

TTfilJ L L . U L f/U l iÛIU310i Vil tab LdhtS rtUai,y HLdi U U I

thMJuSSS I H

llGREATLAKESANALYTICAL




Project MSCGPrc Treatment ListProject Number: [none]

Project Manner. Tom JacobsoiiReported:

12/04/03 10:07


Sample ID

Tajik 1 3 Spill

Lnboratory ID Matrix

W3 12023-01 Water

Date Sampled Date Received

11/19/0313:30 12/03/0309:47


fl nlLJ?>£lL#?

'I'll* raulu in ihlf rtport appfy to Uie samples analyzed in accordance wiili the chain nfcustody document. This analytical report must be reproduced In Its entirety.

Andrea Stathas, Project Manager Page 1 of4

12/04/2003 THU 09:58 [Ti/RX NO 5097] 1)003

u / u o / ^ u u o nnu rt\\ t i i o /ua io i UUI



Email; [email protected](414)570-9460 FAX (414) 570-9461


Project: MSCGPre Treatment ListProject Number, [none]


12/04/03 10:07


Antlytc

Tank 13 Spill (W312023-01) Water

pHTotal Suspended Solids

Result.

Sampled: 11/19/03

6.87ND

ReportingLimit Units Dilution

13:30 Received: 12/03/03 09:

5.00pH Units

mg/11M

Butch

47

3120106312010ft

Prepared

12/03/0312/03/03

Analysed

12/03/0312/04/03

Method

EPA 9040BEPA 160.2

Notes

G5

Great Lakes Analytical-Oak Creek The results in IhLf report apply to the samples analyzed In accordance with the chain afcustody document. This analytical report must be reproduced In Its entirely.

Andrea Stathas, Project Manager Page 2 of4

12/04/2003 THU 09:58 [TX/RX NO 5097] 12] 004

n&u TAA ureai Lanes Aiiai,y utai

^SB GREAT'LAKES[ANALYTICAL




Project M SCO Pre Treatment ListProject Number, [none]

Project Muntiger: Tom JacobsonReported:

12/04/03 10:07

General Chemistry - Quality ControlGreat Lakes Analytical—Buffalo Grove



SourceResult %R£C

%RECLimits RPD

RPDLimit Notes

Batch 3120106 - General Prep \VC

LCS(31Z0106-BSt)" Prepared & Analyzed; 12/03/036.99

LCS Pup (3120106-BSD1)pl-l

Duplicate (3120106-PUP1)

pH Units 7.00 99.9 9S.6-101.4

Prepared &. Analyzed: 12/03/03pH Units 7.00 99.9 98.6-101.4 0.00

Source; W312023-01 Prepared & Analyzed: 12/03/03PH

Batch 3120108 - General Prep WC

6.85 pH Units 6.87 0.292

Blank (3120108-BLKl) Prepared: 12/03/03 Analyzed: 12/04/03Total Suspended Solids

Duplicate (3120108-DUP1)Total Suspended Solids

ND S.OO ms/1

' Source: W312023-01 PTepared: 12/03/03 Anulyzctl: 12/04/03ND 5.00 mg/1 4.00 11.8 41.9



The raiulu In this report apply to tHa samples onatyttid In accordance with the cham ofcustody document. This analytical report must be reproduced in Its entirely.

Page 3 of4

12/04 /2003 THU 09:58 [TX/RX NO 5097] (21005

ncu r/iA tita/uaioi breai Lanes




Late Suits Industrial Service311 E. Greenfield Avc.Milwaukee WI, 53204

Project: MSCG Pic Treatment ListProject Number: [none]Project Manager. Tom Jacobson.

Reported:12/04/03 10:07


GS This sajtiple was received past the method specified holdtime.

DET Analyte DETECTED

ND Analyte NOT DETECTED at or above the reporting limit

NR Not Reported

dry Sample rcsulta reported on a dry weight buxi.H

RPD Relative Percent DifferenceL This quality control measurement Li helnw the laboratory established limit.

H This quality control measurement a above the laboratory established limit.

Great Lakes Analytical—Buffalo Grove Wisconsin DNR Certification Lab ID: 999917160

Great Lakes Analytical-Buffalo Grove NELAP Primary Accreditation: Illinois #100261


Great Lakes Analytical—Oak Creek, WI Wisconsin DNR Certification Lab ID: 341000330

Great Lakes Analytical-Oak Creek, WI NELAP Primary Accreditation: Illinois #100307Tote: For analyses that require NELAP accreditation, all analytes, by matrix and method, are accredited following current NELAP.candards unless specifically noted by way of a qualifier listed above.

Great Lakes Analytical—Oak Creek The results lit this report apply If Inv Samples analyzed in accordance with ihv clmin ufcustody dacumtnl. This anafytfcal rtport must b* reproduced in la entirely.


12/04/2003 THU 09:58 [TX/RX NO 5097] @]006

u/uo/ûuo rrci; r/u iiio/uaioi weai Lanes

12/03/2003 WED 08:29 FAX 12622426554 ENV ASSOC.


Environmental Associates, Inc.P.O. Box 136

Thiensville, Wisconsin^3Q92(262) 242-1088 faxQ262) 242-6554^

toll free (800) 494-4645•www.eaiwi.cotn

To: Andrea

Company: Great Lakes Analytical

Fax!

Re:

414*570-9461

Soh/ay

Sample Tank 13 Spill

W311185-01

From: Joe Michaelchuck

Pages;

Date: 12A3/03

CC:

G Urgent D For Review D Pl«99e Comment O Pfoa*» Reply D Pfa

Andrea:As we discussed, please analyze the above sample for TSS and pH as we originally requestedverbally with Dave Krueger. - ~

Please Fax results immediately upon completion.

Thanks.

Joe

C:\WTNDOWS\DeslaDp\f«xcw4-01 .doc

12/04/200.3 THU 09:58 [TX/RX NO 5097] lg]007

ATTACHMENT D

0 Outfall#012

Concrete SlockSedimen\Trapx

36" Orchard Street sewer to river -

City Sanitary Se

#005.

306 #0.07

.Area

#008Coal Tar Consolidation and Holding Tank i

Q

:EL

Permanent Fencin

uvs«wer_

P O Crty Sanitary Sewer [_•>

Pipes

Proposed Decontamination Pad •'. .(See FIGURE S for details)

>-' 0

#004City Sanilary Sewer Railroad Tracks

I FftFND

A#001

Existing Permanent Fence Line

Temporary Fence Line

Site Rubble Pile

Site Building and Designation

Manhole/Sewer Grate

Storm Water Flow Direction

Drainage Area Delineation Boundary

Drainage Area Designation

Outfall Location and Designation

Shaded Area = Phase I of Demolition

Location of Non-DomesticWastewater Discharge

Subsurface Conveyances :

- - Kinnickinnick River (South)

- — Kinnickinnick river (North)

City Sanitary Sewer

Environmental Associates, Inc.

awn

I a/.-RRG

8/13/03

Drawing :

File :

03-03855-003

stormwatermap.cvS

\

\

Approximate Scale In Feet

FIGURE 1Former Solvay

Coke & Gas SiteStorm Water Runoff Map


APPENDIX H-2

Letter to MMSD Allowing theDischarge to Their System

€) EarthTechA Tyco International Ltd. Company


Preserving The EnvironmentImproving Water Quality

December 4, 2003

Mr. Tom JacobsonLake States Industrial Services311 East Greenfield AvenueMilwaukee, WI 53204

Subject: Notice of Intent 2003.037

Dear Mr. Jacobson:

The Milwaukee Metropolitan Sewerage District (MMSD or District) has received a Notice ofIntent submitted by Environmental Associates, Inc., for the discharge of water from the formerSolvay Coke and Gas site, located at 311 East Greenfield Avenue, Milwaukee. The District isapproving the discharge of water from this site subject to the following conditions:

1. The former Solvay Coke and Gas site must be in compliance with the general and specificlimits set forth in Chapter 11, MMSD Rules. The pH discharge must be greater than 5.0standard units.

2. In the water discharged to the sewer system, the following pollutant levels may not beexceeded.

Cadmium 1.5 mg/1Chromium, Total 8.0 mg/1Copper 6.0 mg/1Cyanide, Total 5.0 mg/1Lead 2.0 mg/1Mercury, Total 0.0026 mg/1Nickel 4.0 mg/1Oil and Grease 300 mg/1Zinc 8.0 mg/1Total Suspended Solids 100 mg/1Total VOC Scan <5 mg/1

3. At least one sample must be taken and analyzed for the above pollutants during discharge.

4. No discharge may occur during periods of at least 0.5 inches of rain. If it does rain, alldischarge from the former Solvay Coke and Gas site must cease to the sewer system.Commencement of the discharge cannot occur until 12 hours after the rain has stopped.

wifmwfeee metropolitan sewerage district260 W. Seeboth Street, Milwaukee, WI 53204-1446

414-272-5100 • www.mmsd.com v®

Mr. Tom JacobsonLake States Industrial ServicesDecember 4, 2003Page 2

5. The total volume of water discharged should be reported to Mr. Harvey Maty as, DistrictSenior Industrial Waste Engineer, when the pumping is completed. At that time, the theformer Solvay Coke and Gas site will be billed by the District at the rate of $1.05 per 1.000gallons discharged.

The policies and procedures for these types of discharges to the sewer system are currently beingstudied by the District. You should be aware that this approval may be rescinded at any time orchanges to your conditions may occur.

If the former Solvay Coke and Gas site is in violation of this letter of approval at any time, theDistrict may take enforcement actions which may include, but are not limited to, issuing a Noticeof Noncompliance, a Notice of Violation or seeking injunctive or civil penalties up to $10,000 perday per violation.

If you have any questions concerning this matter, please contact Mr. Harvey Matyas, SeniorIndustrial Waste Engineer, at 225-2164.

Sincerely,

Peter R. TopczewskiWater Quality Protection Manager

Cc: Mr. Joe Michaelchuck, P.E.Environmental Associates, Inc.

PRT:HJM:jds

NOI 2003.037 Solvay Coke and Gas Site


APPENDIX I

Waste Manifests from Waste Management, Inc.

• 1-1: Asbestos Waste Manifests - Waste Management,Inc.

• I-2: Coal Tar Manifests - Waste Management, Inc.

• I-3: Other Non-Hazardous Waste Manifests - WasteManagement, Inc.




APPENDIX 1-1

Asbestos Waste ManifestsWaste Management, Inc.



W£STE SHIPMENT RECORD/ASBESTOS MANIFEST*TSeeReverse (or Instructions)

1-A.Special Waste Profile Number NESHAP Notified

YES NO

WSR Number

773251

For Disposal Site Use Only

Elevation

North East

1-B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code) 1-C. Generator's Phone Number

1-0. Work Site Address 1-E. 24 Hour Emergency ResponseTelephone Number

Name and Complete Mailing Address Operator's Phone Number

3. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal Facility10712 South 124th Street; Franklin, Wl 53132

WDS Phone Number

414/529-6180

4. Name and Address of Responsible AgencyD Southeast District, Wisconsin Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212D South Central, Department ot Natural Resources

3911 Fish Hatchery Road, Fitchburg, Wl 53711

5. Description of Materials 6. ContainersNo. Type

7. Total Quantityyd3

Asbestos, 9, NA2212, III, RQ

non-friable asbestos Cat I Cat II.

8. Special Handling Instructions and Additional Information24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.

Printed/Typed Name and Title Date

1 0. Transporter 1 Company Name

Complete Mailing Address

Telephone Number (including area code)

-7 Cl

Driver Signature

Printed Name and Title

tJU? f LViDate

11. Transporter 2 Company Name



Driver Signature


Date


13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.

5 Printed/Typed Name and Title Signature Date

WHITE - Disposal Site

DCE-230-97-METRO 7 99

CANARY Generator(To be mailed by Disposal Site)

PINK - Transporter GOLD - Generator(To be taken prior to disposal}

/ WASTE SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse for Instructions)

-A.Speciat Waste Profile Number NESHAP Notified i

YES _NO

WSR Number

7732521-By .Generator Name, Contact N>me, and Complete Mailing Address (including Zip Code)

'


Elevation

North East

1-C. Generator's Phone Number

1-P. Work Site Address

':<j\\ r - C. V' C\ i v \ i \ c i1 - E. 24 Hour Emergency Response

Telephone Number

2. Operator's .Name and Complete Mailing Address

"•' >\V V\

Operator's Phone Number

u \ - L i A v3. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metrp RecycHng and Disposal Facility10712 South 124th Street; Franklin, Wl 53132

WDS Phone Number414/529-6180

4. Name and Address of Responsible Agency

P Southeast District) Wisconsin Department of Natural Resource?2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212

D South Central, Department of Natural Resources3911 Fish Hatchery Road, Fitchburg. Wl 53711

SvDescription of Materials 6. ContainersNo. Type


friable asbestoa. Asbestos, 9, NA2212, III. RQ

non-friable asbestpa Cat I Cat II

8. Special Handling. Instructions and Additional Information24 HOUR NOT|Ct GIVEN PRtOR TO DBPOSAL, MUST BE BURIED,

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and, are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland government regulations, t hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.

Printed/Typed Name and Title

"'\ ,\ vv -V VASignature; Date




Driver SigriSIure


<",*' f

Date^/ -

11. Transporter 2 Company Name v N



Driver Signature


VVDate1*'


13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by signature in trie case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest excepVas noted in Item 12.

Printed/Typed Name and Title Signature Date


DCE-230-97-METRO 7/99

CANARY - Generator(To be mailed by Disposal Site)

PINK - Transporter GOLD - Generator(To be taken prior to disposal)

SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse lor Instructions)

1-A.Speclal Waste Profile Number NESHAP Notified

X YES NO

WSR Number

77GG98


Elevation

North East

1-B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code)

Golden Marina Cauaaway311 last Graanfiald Av«nua» Milwaukoa, WI 53204


U4-64S-0635

1-D. Worksite Address

311 Eaat Graaofiald AvanucMilvaukaa, WI 33204

1-E. 24 Hour Emergency ResponseTelephone Number

414-645-0635

2. Operator's Name and Complete Mailing AddressLak« State* Industrial Services311 Eaat Graaafiald Avanu«; Mlltfaukae, tfl 53204


414-645-0635


Metro Recycling and Disposal Facility10712 South 124th Street; Franklin, WI 53132


4. Name and Address of Responsible AgencyS Southeast District, Wisconsin Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, WI 53212D South Central, Department of Natural Resources

3911 Fish Hatchery Road, Fitchburg, WI 53711

5. Description of Materialsplacei

6. ContainersNo. Type

7. Total Quantityyd3 '

friable asbestos

non-friable asbestos ~~>

Asbestos, 9, NA2212, llf, RQ

Call. Cat II or8. Special Handling Instructions and Additional Information

24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated with hpza"rdous, PCB, and/or any special waste.

Printed/TypjdjMame and Title

Ax..../'iignature i" Date


Qt'j-p^jqj *][*|-n/»^JT<


PO Boa: 4JLOi>Jf>tj H»yl-tn 'JT


,^ i ,

Driver Signature


/DriverDate




Driver Signature


Date




/Gat •'.Signature Data

DCE-230-97-METRO 7.'99

WHITE - Disposal Site CANARY - GeneratoriTo be mailed by Disposal Site)


WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See Reverse (or InstruoKuiuJ ""

-A.Special Waste Profile Number

10OVL-

NESHAP Notified

YES . NO

WSR Number

773667


Elevation

North East '

-B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code) 1-C. Generator's Phone Number

1-D. Work Site Address 1-E. 24 Hour Emergency ResponseTelephone Number

2. Operator's Name and Complete Mail ess Operator's Phone Number





2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212D South Central, Department of Natdral Resources



7. Total Quantityyd3.

asbestos Asbestos, 9, NA2212, III, RQ

non-friable asbestos Call Cat II.


9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper sfping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internation,and government regulations. I hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.



Complete Mailing Address '/£>(, j, r j~ 2 ? v

^ /J f~~

'SO

Driver Signature


Printed Name and TWe

X p Cr /• /

Date



Telephone Number (including area codej

Driver Signature


Date


v> 13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is Issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.


WHITE • Disposal Site

DCE-230-97-METRO 7/99



x/WASTE SHIPMENT RECORD/ASBESTOS MANIFEST(See nnrnnnjjr InnlnirHnml

1- A.Speclal Waste Profile Number

- *NESHAP Notified

V YES . NO

WSR Number

773223


Elevation

North_ . East_

1 - B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code)- - , \ \


1-D. Work Site Address 1 - E. 24 Hour Emergency ResponseTelephone Number

V, I2. Operator's Name and Complete Mailing Address Operator's Phone Number




4. Name and Address of Responsible AgencyO Southeast District, Wisconsin Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212D South Central, Department of Natural Resources

. 3911 Fish Hatchery Road, Fitchburg, Wl 53711



friable asbestos , Asbestos, 9, NA2212, III, RQ

non-friable asbestos Cat I. Cat II

8. Special Handling Instructions and Additional Information24 HOUR NOTICE 6IVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland governmentregulations. I hereby certify that theasbestos is not contaminated with hazardbuyPCB, arid/or any special waste. • • • .


-h r-Signature / / Date

l_







Driver Signature


Date

Driver Signature


Date


13, Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted In Item 12.



DCE-230-97-METRO 7/99



"tiii- :>' * ( L /I ^ -\-\ -• - /WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See/ieverse for Instructions)

.Special Waste Profile Number NESHAP Notified

y YES NO

WSR Number

773227


Elevation

North East

-B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code)

\>


1-D. Work Site Address

'- - '.


y. ; \\' . v^2. Operator's Name and Complete Mailing Address

"V\\


V- v... A\'.\3. Waste Disposal Site (WDS) Name and Complete Mailing Address



4. Name and Address of Responsible AgencyD Southeast District, Wisconsin Department of Natural Resources ,

2300 N. Or. Martin Luther King Jr. Drive; Milwaukee, Wl 53212D South Central, Department of Natural Resources




friable asbestos Asbestos, 9, NA2212, III, RQ

i non-friable asbestos Cat! Cat II

8. Special Handling Instructions and Additional Information' • 24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationalantfgbvemment regulations, thereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.

' / •Printed/Typed Name and Title

V \ i , V \Slgnatu Date


fa'tj /( ///* --Complete Mailing Address

/£.-(. J 7 ., S -Printeji Name and Title'

Telephone Number (including area code

rinte_ji Name a

* t f r ' tDate 7




Driver Signature


Date





DCE-230-97-METRO 7/99



SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse for Instructions)

1-A.Special Waste Profile Number

[00\

NESHAP Notified

YES NO

WSR Number

773230[Name. Contact Name, and Complete Majling Address (including Zip Code)

5320]1-E. 24 Hour Emergency Response

Telephone Number

2. OoMaiprjjyvlame and Complete Mailing Address









5. Description of Materials 6. ContainersNo.


friable asbestos Asbestos, 9, NA2212, III, RCl

non-friable asbestos Cat! Cat II.

B. Special Handling Instructions and Additional Information24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated with hazajAfus, PCB, and/or any special waste.

Printed/Typed Name and Title Sigi Date


U/Ajfa- /n>whComplete Mailing Address /

i


Driver Signature^— ^


Date




Driver Signature


Date





DCE-230-97-METRO 7/99


PINK - Transporter GOLD • Generator(To be taken prior to disposal)

- A . ' > - ' - '' 'WASTE SHIPMENT RECORD ASBESTOS MANIFEST'See f\e.«r»« tor *vmM*ar»i

•-A Spec* Waste ProMeNurrbar '.-.-tier

773229

Fcf Dsoosal Site Use Only

Norm East

•f1-B Generator *arr» and CCK-O*S «a«r« Aaor^ss ncuxxc Z°c : roe'

1-D

i-C. Generator's Phone Number

\\'il3 W«a» Ooodot 9to &fOS) Nanw *Jd Corrx»«9 Ma*rg Adores

MMD RKydhg and Oaposal Factty10712 So* I24*i Slreac Frvttn. Wl 53132

WOS Phone Nuitar

414629^180

O Soufmat Outlet. Wisconsin Departmanf o» Kaftjra* Resources2300 N Dr. Marln Lutwr King > Drv«: U«w%Aae Wl 53212

South Central. Department of Natural Resources3911 Rsn Hatchery Road Rlchburg, Wl 53711

No.

-faf


Asoescs. 9. S*22'2.

Ca! '

a Sp«3» Kbnolng moructart* ird Ado«an«24 HOUR NOT1CC GIVEN PRIOR TO DISPOSAL MUST 3C 8UR*D

9 GBCRATOROPERATORS C£RT1F1CAT)ON ~wtr, <j*oan fat tw oyiterts o- 1~'.s onsgnn-eni am My and aoxvaMy descitoed above by proper ship-ping nam* and are dteMtadL iMLtad. martad. arc ir«i«d. and » r al raspects r JTOCW co<x>tioo lor iransport by ftghvay acco»Jnq to anpicahtB international

h«r«by oroty s net cortarnra'sc!»-~ -va&roous PCS andor any special i

PnnMd>T|g*d Name and T««

V\;'-iL\Data

ID T i ConpartyName

Da-e

11 T

.'ndudng araa code)

"tie

Da:e

•2 DacnaMrcy mdcatcr Soac*

1 3 Wasa* Diwos* So* Oww ar OperauySpeoai Aasse Approval s ;• a 3*"-c"; i

s -i- •€•«• « • : >: is - ;-«-r

^xc vtane and "at

\ V.Vv. t I..- OftH"; r

•IPMENT RECORD/ASBESTOS MANIFEST" (See Reverse for Instructions)


RASB10642

NESHAP Notified

X YES _NO

WSR Number

774063


Elevation

North East


Milwaukee Solvay Coke & Gas311 East Greenfield Avenue; Milwaukee, Wl 53204


Hans Geyer414-645-0635


311 East Greenfield AvenueMilwaukee, UI 53204


414-645-06352. Operator's Name and Complete Mailing Address

Complete Decon, Inc.4690 East Second Street, Unit 3; Benicia, CA 94510


707-747-48003. Waste Disposal Site (WDS) Name and Complete Mailing Address



4. Name and Address of Responsible Agency3 Southeast District, Wisconsin Department of Natural Resources



5. Description of Materialspipe laggling/bpile* lagging



friable asbestos Asbestos, 9, NA2212, III, RQ

norvfriabld>asbestos Cat I. Cat!XXXX3XXXXXJXXXXXXXXXXXX


9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that (he contents of this consfgnrnerrt are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.

Printed/Typed Name and True Date

10. Transporter 1 Company Name Driver Signature.,


/DriverDate

1 1 . Transporter 2 Company Name Driver Signature

, Inc.

21107 Omega CircleFranksville, Wl 53126



Date

12. Discrepancy li Space



/Gate Attendant

Signature Date

WHITE • Disposal Sit*

OCE-230-97-METRO 7/99


PINK • Transporter GOLD - Generator(To be taken prior to disposal)

SHIPMENT RECORD / ASBESTOS MANIFEST<SM nevtne tor raruohm)

1-AS Nurtter

RASB10642

NESHAP

X

S-moef

774062


East

1-B Generator Name. Cortact Mini*, and Comcxaw Ua«ng Adores naming Zip Ccoe'

Milwaukee Solvay Coke & Gas311 East Greenfield Avenue; Milwaukee, VI 53204

1 -C. Generator's Phone Number


1-0 Work S* Addree*

311 East Greenfield AvenueMilwaukee, VI 53204

1-E 24 Hour Emergency ResponseTelephone Nviiwr

414-645-06352 Operator* Name and Complete Uaftng Address

Couple te Decon, Inc.4690 East Second Street, Dnit 3; Benicla, CA 94510

Operators Phone Number

707-747-4800Dwpoeal Sle nM>Sl Harm and OirnpM UaJrg Address

UMTO riauycfinq and Oopocal Faotry10712 Sou* 124* Street Frankfn. Wl 53132

414529-6180

4

s

M0no end AddYMB o> RMponsttto AQ<ncy

2300 N Or Martin LUher Khg Jr.

DMC paton of MftattrtMBpip«

Dnv« Miiwaukae. Wl 53212 391 1 Rsh Hatchery Road, F

laggling/boiler lagging

!

nort haote aabetfoe ! Call can _

6 ConNa

/

tanersType

&*

ii Natural Resources"rtchburg. Wl 53711

7. Total Quantity

0* &~

24 HOUR NOTICC carve* PRIOR TO OSPOSAL MUST BE BUREO

9 GENERATOHOERAKXTS C€RTF)CAT)ON *«njOy deotar* tnal tr* conarts * !hts coosl9nmert are My andpmg name and are cftaevAedi pectvrx merged, jnd ôevo. and w ^ aa nsspects IT proôr cooofton for transport by ta

ery descntwd above by proper ship-

and jo»am»iiai« ngUiatnrn. I haraby camfy nal 9x avi«n»n» a not cortarmated <r*- -azardous °C3. anoVor any special waste.ng to 3ppfec3tote

Eagle Disposal, Inc.

21107 Onega CircleFranksville, Wl 53216

i code)

262-895-4800 Daie

12 DaoepaiiLv tufcjaan Space

j

13 WafM OspoHl S» O*oar or OperatorSpeoal Wane Approval a 33000 oy S -JS^B .- r« ^s« o* a 3«ne-<c *soest:s ^co^va.Certfcaton o> necavi d asbestos -jae'as s>vec ^ r^s -a i'es: eicew as ->:•«! f iterr '2

Pmeo/Typad Name and T«e

/Gate Attendant

Sgr-S^B Date

30LO-Ts a* aun oror B dnpmali

» ,*»» !

ASTE SHIPMENT RECORD/ASBESTOS MANIFEST

1-A.Spedal Waste Profile Number' NESHA1* Notttod

* YES .

WSR Number

T73902

For Disposal Site UM Only

Elevation-'

a«lC^

^ji*!^';vr4" '

nut «r,«ucnu AW*! MUwii-.. in1-

1-0, Work Stte Addrfta*

MM* M «Wt J

1-E. 24 Hour EmtfQenty ResponM

v- ' ,

2. Operator Name vrfCoji1c**MttnaAddrM«" Operator's Phone Number

.C& M310

a Waste DiaposatSW (WOS) Nttnt M> Cdmpto» Mallno Addres*

UptfoflQdycDnflanttDlsftosalFadlliye,. 'i0712 SoJlh 124th Street; FranW i \Wf53t 32 ,

WDS Phono Nutnbv414/529-6180

4. Nairn and AUdrOMOtRespohsfete Agency _, ^S&irtNastDfefrfet vsfttoonslo Department of Mifturaf230&N? Or. Martn Lu«wr Klnfl Jr. Drive; MiW ukei.Wl 53212

Sbuth Centralk Department of Natural Resources3911 Fish Hatchery Road, Frtchburg.Wl 53711

2* HOUR NOTtCE'Qrv * PRIOR TO

9. GENEflAtORADPeBATOFTS CeRTIFteATION'. I hertfay dectareteat the corrterte of thh O«»Qnment are fully and accuracy described above by proper ship-ping name and ar* dassWed, packed, marked, and labeled, and am Kt at rea(!Bt* In prapaT«anJHIon<or transport by highway ao^8^ gWr«wr*regulatio«iU hereby carttytrwtto ' •

ir>. Transporter t Company Name

tat xuv.ta.fe*CompletoMaJlhgAddn

WX24F«1U» Wl 33031

code)

11. Transporter 2. Company Name

. - ' - ' . . . ' - 1! t .. • . . ... , .- .

Complete MaUftSg Address '

DrtwStgnatum

NameiindTWe

.' ^'-:' i,, ^f'^y^,-. ?&-..>:'?*•••..12. Discrepancy Indication Space

13. , ; ^ - . .Special Vâste;Apprci teJ88ued by sia iafuiw In tCertHicafion of receipt ofasbdsfce materials covered ttythtomaniteateweptaB notedln Hem 12.

Printed/Typed Name and TitleAtt**4*nt

Date

WHITE- CANARY-QanBrator PINK GOLD - Gwtwatorrr« h. igk

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST .pai H« •!•• *• *"*i rUhinal " ' "*

lASBUOttl

WESHAPI

* YES NO

WSRNurtJW

773901

For Dtoptlal Sa» UM Orty

1-B. laana. and CorapM* Oalng Addran OnAdng Zip Coda)

tolvay Co4» ft CM3U iMt OrMBfi*U ATMMI )fctlm»k*«» Wl 33204

1-C.

414-445-0435

i-a 1-E.MHovEa

414-445-0435

44M Str*«C, Vmlt 3| , CA 14510

414^29-618010712 Sou*) 124ti SVMC FrwMn. Wl 53132

4. HMW •no AddraM d 1rf TH«MM< mmrtrt Yflrrmin nipartmanl nf f IrtraT nnmnirrm

2300 ft Or. Uarth Lu*w Kino > CMw fcB*"Uu>«. Wl 53212Sauh.C«n(nlOapartniantaiNaluiralRe90urc8(3911 Rrfi Ha*c*w«y Rotf, Ffettug, Wl 53711

Track

7.TaMCkMrtky

CM)

2« HOUR MOTlXGWa*PWOR TO DCSPO6AL MUST B€BU«S>

9. GB<EBAI OHO rngnmert ara My »id

tff tfMf ifw•«! •« in al rwptea in prapar oontMon tar tampan by higt

it not corcvTWtvd v4h f jvdnji. PCB, snifu 3ftf i

10. TcMpaVr I Company MM*

Pnmed Name and T«« j:1 1 . T 2 Cotnpviy Drv«r

PrntBd Nara and Title

Tatanhi •*duarqi I . . ^ \ \ ( :^

12. Oaoapaney Mfcafti

to Approval it iajuad by aignalu* h Micaw o< * flarwnc AjbaakM Appnwal.of twaipl at lahxfa mi»nnai cowvrad by »w manfast «rcap» a notod n hem 12.

and

ODLD

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(SM Reverse for Instructions)

I 1-A.Special Waste Profile Number

USB10C42NESHAP Notified

YES _NO

WSR Number


MllvaufcM 3olT*T Coka k G*»311 bat Grt«nfl«ld Av«nu«j Mlluauk*a, VI 53204


Bait* Gayar414-645-0635


aaxa aa abova


414-645-06352. Operator's Name and Complete Mailing Address

Covplfta Dacca laie,4(90 Ua* Sacond Straat, Unit 3| Banloi«, CA 94310


707-747-48003. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal Facility10712 South 124th Street: Franklin, Wl 53132


4. Name and Address of Responsible AgencyB Southeast District, Wisconsin Department of Natural Resources


3911 Fish Hatchery Road, Rtchburg, Wl 53711

5. Description of Materials UMint/K>ll« W|!:.vi :-;^-->;i^.;6. ContainersNo. Type

7. Totat Quantityyd3

friable asbestos Asbestos, 9, NA221Z, III, RQTruck

non-friable asbestos Cat! Cat II.


9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are In all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated wRh hazardous, PCB, and/or any special waste.

Printed/Typed Name and Title Signature 77? Date

1Q. Transporter 1 Company Name

UM MUvmvkA*Complete Mailing Address

W124 MS945 Boundary loadXanopooa* F«ll«. Wl 53031

Telephone Number (Including area code)

262-251-4000

Driver Signature f tf f^/t. I T

Printed Name

/DriverDate




Driver Signature


Date


13. Waste Disposal Site Owner or Operator :

Special Waste Approval is issued by signature In the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.


/Cat* AttendantSignature Date

WHITE - Disposal Slta

DCE-230-97-METRO 7/99

CANARY - Qensrator(To be mailed by Disposal Site)


ASTE D/ASBESTOS MANIFEST

NO

i-a.

7T3904

ttil»»«fc»« S*lw Q&* *,SM3U BM* 9f***tt»lf Ar«»«f 33204

For ObpasH Sto UM Orty

VC. GMMf oC* Ptan* Nurber

1-0t t-E. 24Ha« EcwgMcy RMponMT*qtar»*ntm

4U-445-0435 •

«•*4H*li««

I CtnpMi aMhQ Addrvat

707-747-4JOO0*n*t SNKWOS) Nnw «nj) O

414/529^18010712 ^0*124ft S»Mt;l anMtV.W1 53132

2300 N. Or. NMta Uttwr King Jr. Drive W! 532123out» Ctrtat, Dcpartmeieot Nrtural Rasourcea3911 Rati HMctwy Road. FacNw» Wl 53711

« HOUR Nonce oivei PR«« TO oei oeAt. MUST BE BUWED

a. oe I fwBby dadipi tat Bv ccimvi& tf this c&nsjgrvrwtf ana katy MdKCtfliBly dncrtMi( )0¥A by propflr &(•{>-and aoateo, and w n al rnpvcB ^ ^vry^ contfbofi to/ Imnaport oy t40hMay ajooofOnQ to SBfaicBDia i

twnoa a not oartavninaMd «Ti T*zardau«. PCS. ancMor any

i^

M445fell*, n 53091

11. Ti

T«ta|ta«NMti«(hcta*rgapa.ood.)

. r V .

ama md TM*

12.

13.by S^Hfen • h* CM* Of • QwrlC AatMMM AOfTOMLi matariok COMKTWI bf Hi irmirtail ocopt as rated in Nam 12.

and TV*

ict•MTC QOLD-

(Tob*

I L-Z774051

1-B. Generator Name, Contact Name, and Complete Mailing,

G l i " i-1^ •->Q.l-..\«LK • I* ! • : .< . f ~ | j i . '..,_ - (.' ,i ..

;yu '•' • " •• -.- • : • - ll '*••'•-

le)


Elevation

North East


1-0. WorKSHe Address

-?"«'- .A-


.'J2. Operator's Name and Complete Mailing Address

L'iJr-1- ^.-MI (?•: .

I'.., :L ' - . 0 - JVOperator's Phone Number

I3. Waste Disposal SHe (WDS) Name and Complete Mailing Address


WDS Phone Number

414/529-6180

4. Name and Address of Responsible Agency& Southeast District, Wisconsin Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212O South Central, Department of Natural Resources

3911 Fish Hatchery Road, Fltchburg, Wl 53711

5. Description of Materials ' ' j ' > • '• ' ' • • . - - • i 6. ContainersNo.: Type


frlabl* asbe*o»\

^ ^/, 9. NA221X ID, RQ

non-friable asbestos: Cat.l. Cat It

8, Special Handling Instructions and Addttfonal Information24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated'with hazardous, PCB, and/or any special waste.




'" '• ' ' ' ': i i . '


Driver Signature


Date




Driver Signature


Date


T*513. Waste Disposal Site Owner or Operator

Special Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.



DCE-230-97-METRO 7/99



1

*

WASTE SHIPMENT RECORD ASBESSee Reverse tar mtuucaons)

' ^ — ' ' , ' '1-8 GeneranrNane Contact Name, and Cono»e» Uakng AoeTB

/ : • '

^" ; • 'V, „ /,"•• vi-O Work SM AdOrm iff

2 Operator* Name and CompMt Uaflng Address

3 / f ~'r> '• i 1 r- ' '1 Waal* Otapota) S»» (WOS) Name and Compww Mafcig Adorn

Metro Recycftng and Otapoaal Fabtty10712 Souti 124«h Street Frarttn. Wl 53132

Souvteesl Onirtct. wtxonsan DupjiUiMxil oi Natural2300 N. Dr. Itartn Luther King Jr Or>v« kMwaufcaa.

S.O^crôlM^^ , /Tl^^.

(*AM..M^

ft Vrk«M-Hari 1 • •••• if to a^ mjul A hBM 1 WA ahi

24 HOUR NOTICE Give* PRIOR TO DISPOSAL ULC

9 r ian*Trifij praA'TTiQ*^ fypnyif*_4Ty^^ > h«r w riM^H

Cciri0l»<i itoing Adctrwa

.r:. - .

TOS MANIFEST For 0«oosal &te Use Only I

I . c r: •> —roar Ewwaoon 1

_„ ; 774052 ... «45 sxaxjn; Sc C roe i - C Generator's Phone Number

:.' .'. ,. ..,:: • " '^ " î - E 24 Hour Emergency Response

Telephone Number

^ '4 st f /<? < /Operator's Ptione Number

s WOS f ions NtfntMf

414/529^180

Resources _ South Central. Oepartmeni of Natural ResourcesWl 53212 3911 Fish Hatchery Road, Rlctt)urg,WI 53711

.-, • ~ 6.Cortainers 7. Total Quantityf f ' f-*&Z** — , No. Type yd3

AjbMtos. 3 HA22'2. il' RG / y- *»*- •>

Cal I Cat M

5TB£ BURIED

«K*k M4lfe«* -J M<t AT« fc& < -*l 11 oAutuM I^J h' S

-.-". -'"•2'-s'

Pii-:*c Nane anc Titie

cotterDaw

Ccrrpn

2 Compary Nam*

^ AddrBO

'!-:«: l.a~e i'c

aree. cod*)Case

55 '3 *as«e Dspos* S«e Oner ar OperatorJ Sc*oa« *a«» Aocrcva a .ssêc :'. = ;.-i j-« - ri :aie :• a 3c"^'C -itrs'cs 4«-'2.a:

date

Cisco.**

,>v"#"'V

WASTE SHIPMENT RECORD/ASBESTOS MANIFEST(Sou Ravwrtt tor Inunxflon*)

NtSIAPNOtrRad

_YES .

1-B.

WSH Nianbw

. mid CompWt Mailing AddrtM (Wcludlnfl Tip Onto)

Wl <S2*3C4-

Metro Rocycllnfl and DitpuHMl i-»oiDty10/12 Smith I24th SVOOt, FrBnKDn, Wl 53132

4.NBTM «n Agwcy

El»v«lcn

Nonh _l

1-0. OoiUKuturti Rmw Numtw

1 E. 24 Hour Emaro*rtty RttMrtMluiuplioniiNuinbtr

Op*r»Wn Phono Numbor

414/529-6180

X SOU*I«HI Dtsoka, Wiaoorwin Department ol Natural Reaourcai' N. Or Martin LutfW Wiig Jr. Dftva; MlMMukM. Wl 53212

11 South Cflrtral, rv»partmom of Nahiml HHMUFOM3911 Fbh Halctiwv Hoid, DtchburQ, Wl 53711

B. DMoripdan n« Maloriolt

Ajb»itoi. 9. NA??1i> HI. HQ

Coil Cltll.

HNu


0. SCMCial Handing Irnliudtanf ind AdriMontf Irtformotton24 HOUR NOTICE QIVf-N HHIOR TO DBPOKAJ U»L<5T HE BURIED.

9. CCNrRATORAOPERAI UKtt CERT1RCAT1AN- I hereby dod*i« tn«i UM contann ol thin flmM>mivnl ora hdy and accuntary dMerflMd abOMi hy [X0|«« oliipping MfM tnd sm rtCKXuhud. pmiwd, mwfcud, «nd IA«l*d. ano aro in ufl rinpwat In pmp«r condition for nntpwl by lilghwmy •ocordno tn .Tp lcotfu imuiiulloortand flttMrrmMnt n ukdom. I hmby nuwy <h* ttn acbctlw it ml containlratMi with hrtrOnfcin POH antVor any iptcal wart*.

10. Tntntpvttor 1 Company Namn

frjA-ftz.Comoktt Uaing ArMrcco

(Including area o«V»)

11 Transport* 2 UuufNuiy Mama

u ft&yiDnvur 8ign«%rJ

Data

r>iMiud Num* an) I KM

Data

Driver signature

PtintaO NBJTW inn TMa

Dulo

12. OlMtrnpancy Indrawn Spact

13. Wacta OdpoMl Rrw Uwimr or OptratorSpecial Wieti Apprayal I* IttiMd hy niflnilluru in Uw cata

rUllcutlon of rectjftântxwoc malmiuiy oovar«d by th

666T-9T-Nbr

/

'K

ftASTE SHIPMENT RECORD / ASBESTOS MANIFESTSa* n*v«r»* tor mamjetomi

I r .- ^ « 774\ -.j j1-8 Ganaralor Kama. Cortaet Nam*, and Comcie'.a UaAng Adoress rx*j<sr>c Zo C ae

6-.^-:-. ' " .:;. -p ^' j,,— s~ * J i ~

"~>l \ ^ /-"5" • \ ' '1-D. Work SM Addreai - , / - , - . ,r\ \ j Ca- *• — . •

•51 » '.. - ''<-* • t-| r [>!^ ^-' •

2. QparalDr-t Mama and ComplaM Hafcig Address , r-

•^ * ^- niT'i''V1 6» f o !:• • - J3 WaM Olapoaal Sa* OMDQ Naav and CompMe Matng Address

Majftjo RvcycaViQ and Oltpoof FteMy10712 Souti 124«i S»M|; Fnrtfn, Wl 53132

*. MM and Adfraai of RaaponaM* Agane,

2300 M. Dr. Martin LUher ttng Jr. Drive; UaâAae. Wl 53212

5 Deacnpton of UaMriaM . * .- - •_^_______ '".Vj ^r ~' '•''•".-' f- ^ " • 'i r- - Z ' ' • - • : . •

/'Hat** aabaMM/ Astenor 9 NA2?i2 in. RO

non-Hatat aitiaM Call Cat n

24 HOUR NOTICE GIVEN PfUOfl TO DSPOSAL. UUST BE BURCO

For Osposat Ste Use Onty

054 M ^:-C Generator's Phone Number

i-E 24 Hour Emergency ResponseTelephone Number


WDS Pnona Number

414/529-6180

boun t QHim. uspdiiiieiN in rtuuâj rwsources•MI i Ft* HMt**v FVwl Rfcl iim Wl 1171 1

6- Container* 7. Total Quantityr' '•'.-;?.. NO. Typa. yd3

i ^3'- V — »V 0^- ./j J

PvWtv< ypwl MaW tntf TIM GayijftfB « '

njMMpf.il **j t W 1 ' "^H *" TVT^^^*0 intomatinnaland 'of any mocn^ wssate.

Data

-. ' z -,, -.-xyLt iv / -J '- ' ^

"^x // f^T aK.C *\ f ' • > > .^^ Prated Name a^ Tifle

T>m>torn y**rt»r dndbdng arx codt)/ y y * <" • '* / / Daae - i<~±>T- .^ r 1 s 1 , .}( j, |

:>'''~tec ^4aTê arc Ttie

Twaphon* Nurpber induing araa cod*)

i? Dsorvpancy fdcaton Spaca

I•3 A«s» 0«potat Se» O«nar or OperatorSoaoai Waste Approval «

a» -ocecf jf isbesrcs•< iasa o< a 3**-e-': ifCesSDS *co'3.aa

Prm«3 Tf^^d Hame and Dale

Ooccui Si*": ae 3««" 3-0- c

WASTE SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse for Instructions)

1-A.Speclal Waste Profile Number

/O 5*6NESHAP Notified

YES NO

WSR Number

774055


Elevation

North East


(Ero3/1

nV* t nt a_ C£L_ & e /../y<rv y^r^C-n^f lct [fit fji


1-D. Work Site Address , 1-E. 24 Hour Emergency ResponseTelephone Number

/< 7 :;

2. Operator's Name and Complete Mailing Address Operator's Phone Number

Address3. Waste Disposal She (WDS) Name and Complete Mailing

Metro Recycling and Disposal Facility10712 South 124th Street; Franklin. Wl 53132


4. Name and Address of Responsbl* AgencyID Southeast District, Wisconsin Department of Natural Resource!

2300 K- Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212South Central, Department of Natural Resources3911 Fish Hatchery Road, Fitchburg, Wl 53711

5. Description of Materials

Asbestos, '9, NA2212, HI. RQ

6. ContainersNo, Jype

f4


noD-Wabte asbestot Cat II.


9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are In .all respects In proper condition for transport by highway according to applicable Internationaland government regulations. I hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.


I rK.>

Date

10. Transporter 1 Company


' ji. ^-5 I ^ 4"v> l Akl , {UL, / - ; !


Driver Signature


Date




Driver Signature


Date





DCE-230-97-METRO 7/99



WASTE SHIPMENT RECORD ASBESTOS MANIFEST

1-A.S iNurrber '.-'«« .VSC '!.,-!

For disposal Site Use Only

Belabor

Norm East

IB Gerjmor Name. Contact Name and Cor-cwte

/VViri.VcAddress JXluanf Zto C 306

. \ M A i A K ft U/

t-C. Generaofs Ptwne Number

•-E 24 Hour Emergency ResponseTetopnaw Number

• •„ • i f Operator's Phone Nunber

Oapont Sto (VW36) Name and Compete VJ*n

U«ro nacyOng and Disposal FadMy10712 Sou* 124* S»Mt FranMn. Wl 53132

414^29-6180

VWnonsbi Dapanmant of Nakxal Resources2300 M. Or. Marfn Lulher (Qng Jr. Dnv« »«ra*ae. Wl 53212

South Central. Department of Natural Resources3911 Fish Hatchery Road. Frtchburg, Wl 53711

&ContainarsNo.

7. To«^ Ouantrtyy<0

AstwctDS. i NA22-2 Jl. RO

Cat It

8 Sp. iQlng InrtucSo I Add24 HOUR NOTKC GIVB4 PfOOR TO DISPOSAL. MUST BE BURIED

. tereby declare Ihat ffte contorts 34 this consujrynent are My and ipn0 name and arec

id above by proper ship-Mi packed, marked, and jceted and arc n al impacts m proper condoon tor uarmaon by hQTway jixm>^ to appfcrjbte international

and ju»«inmer« rerjeatitu I nareby carMy tt\a! r* jirwan« a not corttmir ieo <rr< .itartJous PCB. anoVor any special i

Prrf.*dTyfMd Hm and TV* C j' j Date

1 0 Traroponir 1 Company Name ' _)

ana Tfle

cods}

11 Traropoder 2 Company Name ~T.fr- îgr.aruie

Ca:e

• 2 Dtscr<cAnc> fdcaaey Soac*

I

I

*W» Ctsoosal Sk* Owrer or Coeratars

Date

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See Reverse for Instructions)

1 - A.Special Waste Profile Number NESHAP Notified

YES NO

WSR Number

7740411 - B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code)

ft] -• 1 /"<- ( / /L •—/ <"


Elevation __

North:


<M ; i . -.1rD. Work Site Address 1-E. 24 Hour Emergency Response

Telephone Number

i ! ' • ' • • • i ' t2. Operator's Name and Complete Mailing Address

•Operator's Phone Number



WDS Phone Number

414/529-6180

4. Nam* and Address of Responsible Agency• & Southeast District* Wisconsin Department oi Natural Resources-

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212'D South Central, Department of Natural Resources

391 1 Fish Hatchery Road, Frtchburg, Wl 5371 1

5. Description of Materials T;o' •->•• -;.,'. VV. 6. ContainersNo. , Type

7. Total Quantityyd3 ,

friable asbestos Asbestos, 9, NA221Z, III, RQ

non-friable asbestos Cat 1 CatH

w8. Special Handling Instructions and Additional Information

24 HOUR NOf ICE GIVEN PRiOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: 1 hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicable internationaland government regulations, t hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.

* fi.Printedflyped Name and Title Signatuf*'/- :; Date

10. Transporter 1 Company Name .



Driver Signature


Date

1 1 . Transporter 2 Company Name



Driver Signature


Date


1 3. Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 1 2.



DCE-230-97-METRO 7/99

CANARY - Generator PINK - Transporter(To be mailed by Disposal Site)

GOLD - Generator(To be taken prior to disposal)

TOCSTE SHIPMENT RECORD ASBESTOS MANIFEST(See r>e»er«e tor tietucteni)

1-A.Sp te Picfte Number NESr-*3 '•ct-'ec ASP '>*-!

For Ospcsa Ste Use Only

Eevaton

East r1-8 G*ww«or NOT* Corttd Myrw Aodress *» i-C. Generator's Phone Number

i-D . 24<Hy Emergency Response

Telephone Nwnber

2 Operators Name and Complete Uaftna Add Operator's Phone Number

3 Waste r>epo*« SM rWOS) Nam and Corroew Uari Address

U-oR. .-lfcpos-Fac.y10712 SoUh 124ti SkMt FranMn. W1 531 32

WDS Phone Number

414/52<H>180

4. MjHne ind Addmi of nMponctte AQcncy

fc Soutumi Ortict Whconein Department 01 Natoal Resouroes2300 N. Or. Uartn Lutfwr King Jr Orve: U»wa*ae Wl 53212

Souti Central. Departmart of Natural Resources3911 Ftsfi Hafchery Road. Fitchburg, Wl 53711

i OMCrtpton of 6. ContainersNo. Type

7. Total Quantityyo3

RC

30C* I Cat n

S Spea* HanrJng kvBucaor* and Additonal Wtor-jcon24 noun NOTICE GIVEN PRIOR TO OSPOSAL MUST BE BLBHED

9 GeeUTOROPBUTOfTS C€RTF)CATK>ipng nttne and 4re dbtcAvdl pflcted. ntarkad. arcand gpvmrmtr* leg Mont. 1 h«nby o*r*fy ttat r«

-wvby Otoan lhal the ccrteots o' rus consiyvnent are h^y and dascrtMd above by proper ship-and art o al rvapects proper condition for b^niA t ty t ^Miay aooonftng to appicable intemationaJ

• not ancantnaiecl ws- hazardous. °CB. anoVor any special «as*8-

PnrM»T]!>ed Ham* and Tte Sgnabxn Date

10 T i Corroany Name 3-vf Signature

nt^d ^4ame ana Title

T*)ieQitfioifie t jpftttr .'.vkdudvip •veil code)D3ts

11 Târaponer 2 Conpany Kan**

P-'-:*G Narv arc "tie

Telapfona fc fflQer ûnckjdkno area code)

12 DiVDToarcv J-dcaoor Scan

-3 ftass* disoc** S*» Owar or OperatorSc*o* Waste Aoorjsa/ s ss *: ~. s jy T« :ise c< a G*->*x

e'r'3 ^> ~s -ar 'es1 i.-*c- as

5 FrrMioT,5eeNai-« arc '"fie i 5.^-ar_ê

i

Date rDnccaj

" '3*

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(Sea Reverse for Instructions)


U3(AfNESHAP Notified

YES NO

WSR Number

7740*8


Elevation

North East


in v •/4/. Vl.kv wi

1-C. Generator's Phone Number.


-i" t. C ]] K , i i (


,'Vf - ///' ~I/,L 1

. Operator's Name and Complete Mailing Address . i

' .2.11 £ O r ^ i i f u M A/


i v i3. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal Facility1071 2 South 124th Street; Franklin, Wl 531 32 . .

WDS Phone Number

414/529-6180

4. Nam* and Address of Responsible Agency». Southeast District, VVIsconstn Departrnent of Natural Resources

/ 2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212D South Central, Department of Natural Resources

391 1 Fish Hatchery Road, Fitchburg, Wl 5371 1



non-triable asbestos

Asbestos, 9, 1 2, lit, 3dCatl Cat II


9. GENERATOR/OPERATOR'S CERTIFICATION: 1 hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicable internationaland government regulations. 1 hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.



IsJi. • j -( ( /*•' - ''•/ -- •<:Complete Mailing Address

'' • u- -- -•• ' . ' "

/ ,- .; ,.* •' , ..- t .-'•' .


Driver Signature





Driver Signature


Date


Sis

13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 1 2.



DCE-230-97-METRO 7 99




A Sp*c* WM»

IC5U* 774050


North East

IB Gpnerator Nam*. Cortact Nam. Ua*ng Vuress rcludmg Zip Ccoe< i C Generator's Phone Number

ID Work Sto MrJnm l-E-24 Hour Emergency ResponseTelephone Number

2 Opentgr-f Nam* and CompM* Ua*ng Address

3n A/


iv/3 Was** OivoMl Sto (WDS) Nm and CornrjMe Ua*ng AdO>«ss

IMro Ftocycfing ant Oispool Fac«y10712 SouBi124ti Street Frartdln. W1 53132

414^29^180

Souflwast Dttfct Wboonat Department of Nafcral Resources2300 N. Dr. Martn Luttv King jr. Drive. Mfc»autoo, Wl 53212

Sou* Central, Department of Natural Resources3911 Fish Hafchery Road, Rfchburg, Wl 53711

6-CortaitnrsNo. Typ*

7. Total Quantityy<*3

NA22-2. HI, BG

Cat! Cat II.

8 Special Handfc kwucftc atx24 HOUR NCmCC GrVEM PttOA TO C«SPOSM_ MUST B€ BURIED

9 GOCRATOROPERATORS CERTF1CAT1ON r«nby decbr* !hal ihe corttnts cv trxs corisjgnmeni are My and n.i.ui.aely desotod above by proper snip-prg name and am dawked. packad. markad. and 'aceied. and an *\ al respects <n proper condition tor Tampon by righmy axuctng to appfcrarte internationaland tfmmvi.mn prjuH iini I hereby certfy fat ft asbestos a not oonumratad «r- hazardous ^C8. anoVor any special waste.

T^Z/^/iAr *»*.

ID Trwportar l Conpony Ham*

anc Titt»

TOaprone Numtw )«<dUJng are* code)Dae

Tranaponcr 2 Company Hame

code)Dale

• 2 r> Soac«

i 1 3 Wasa* Oroposal Sat OMTW or OperatorSpacnat Waste Aoprosal s ssu*o :>

or -«ce<xr ~« is« o- a 3*-«r

-.erec e> -vs Ta- '«• e.:ec: is

^sec Mane and Jate

~: "x aur a-cr r a socaa

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See Reverse (or Instructions)


y YES NO

WSR Number

774027


Elevation

North East

1-B. Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code) 1-C. Generator's Phone Number


J

1 - E. 24 Hour Emergency ResponseTelephone Number

2. Operator's Phone Number

g. f \< tn \ t \ t \A Av Mi 111/ wt(WDS/I3. Waste Disposal SKe Name and Complete Mailing Address

Metro Recycling and Disposal Facility10712 South 124th Street; Franklin,; Wl 53132


4. Name and Address of Responsible AgencyJ^S6utr»as*tte1ric^WHW»nsto Department of Natural Resource*

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212South Central, Department of Natural Resources3911 Rsh Hatchery Road, Fitchburg, Wl 53711


9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in aH respects In proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated with hazardous, PCS, arid/or any special waste.

Printed/Typed Name and Title cWt<\

Date




Driver Signature -J


Date




Driver Signature


Date





DCE-230-97-METRO 7/99

CANARY - Generator PINK - Transporter GOLD - Generator(To be mailed by Disposal Site) (To be taken prior to disposal)

WASTE SHIPMENT RECORD / ASBESTOS MANIFEST *» o**** **« u*> <**»tSee rteneree tor ka*u4ons)

/I I (" > (r LfMESHAr SCON*

774028IB Generator Name. Corsscl N*me and Complete Ua*ng Aodress «JuoingZc Cc<J9

^ 11 f^ /• ->" r c/r*v/2. /Jr £_ ,H/TP^*• I 1 V— J i t - " - '

'7.1 p ^ t f t

^.(,, ,,, /U( i i iv7-^^

'\ ( IA S i &, iiv \i\i\ 5^.J;~ i3. WaM Dtopo** Sto (WdS) Mw and Como-en Waring Address

Metro Recyrtng and Dvposat FacOtyX 10712 Sou* 124fi Street FrarMn. Wl 531 32

North East

r1-C Generator's Pnone Number

, ,

1-E 24 Hoi* Emergency ResponseTelephone Number

1 • . r • '


WDS Ptions NtfvAnr414^29^180

Wh ki Department ol Natural Resources2300 M. Or. Uartn Lutier Kjr^ Jr. Drive: Mtoortae. Wl 53212

South Central, Department of Natural Resources3911 Fan Hatchery Road, Rfchburg. Wl 53711

6. CorttnersNo. Typ«

7. Total Quantityy<*3

n. 30

C*l CatM

8 SpeoM Handtag bwuctanc and MdMorM Womafcn24 HOUR NOTICC GIVEN PfOOfl TO CXSPOSAL MUST BE BURSD

9 GBC3UTOROPBUTORS CERHRCATK** I hereby dKttr* tnat t» color** o> this consgnment are Uy and acg»j*u*» dasotwd above by proper snp-pmg njHie and a»e otHeAed. pulnd marked, and laoeted. and are n al respects f proper condrtKxi tor transport by NgrMay dtxmfcig to appfcab4e international

. l hereby cerofy 9-M ft asbeetoi a not oontamraied **• lazarocus PCS. anotor any«

Name «nd TJfc

/ ) /«" / ^ In/;/ h /< C(_L10 Transporter l Company Name D—.•e' S<o.riatjre

Pn-rec Name anc Ttte

Cate

11 TransporMr 2 Company Name

Cornplele ItaftriQ Address

Teiepnone Number 'H^KfcHj y area cuds)

Stgnatjre

p'-ec Sane

Dae

12 Cw

' ^3 Wts» Disposal Se» Owner or OperatorSpeoai Waste Approval a r T-S âve ^ 3

| *>*WCMon a« tce«c a» JSMMSCJ - i-s'.as : -'*3 t> . -s a- »«: -.:ea as -c:«: - re-

5 P-irttMTtipeoHameaodTtse ' 5^%ax-e Oa:e

5.M



< YES _NO

WSR Number

77402G1-8. G Name, Contact Name, and Complete Mailing Address (Including Zip Code)

E. A*.


Elevation

North East



A1-E. 24 Hour Emergency Response

Telephone Number

2. Operator's Name and Complete Mailing Address

Ynil \ \


3. Waste Disposal Site (WDS) Name and Complete Mailing Address•



4. Name and Address of Responsible Agency8. Southeast District, Wisconsin Department of Natural Resources



5. Description of Materials 6. ContainersNo, Type


Asbestos, 9, NA2212, III, RQ :

non-friable asbestos Call. Cat II

8. Special Handling Instructions and Additional Information24 HOUR" NOTICE'GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are In all respects In proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos Is not contaminated with hazardous, PCB, and/or any special waste.

Printed/Typed Name and Title Sign

/ /Date




Driver Signature J


Date




Driver Signature


Date





DCE-230-97-METHO 7/99



SHIPMENT RECORD/ASBESTOS MANIFEST

NESHAPNcaBad

NO

WSP

773871

For Disposal Sto Use Only

North Edst_

a G««nK)r NHIW. OortKt Nvn«. and Co' Zip Cooe;

t-l.

i-C. Generator's Phone Number

1-0. 1-E. 24 HM Emagency Response

2. Operator* Main* and CompMa Uaflng Addn Op8ntof*s Phovw Nun wr

v .'• /' -S WMM OtopoMl Sto (WD6) Mm and Co

UMro tecycftng and Oiopocal FacaVy10712 Souti 124ft SVMl; FnnUn. Wl 53132

WDSPtan414^29^180

O Soutufret Dafrtet Wbcomin Depertnent 01 Nan** I2300 N. Or. Itartn lufter King Jr. Drive: Mwa*M. Wl 53212

G South Central, Department of Nawrat Resources3911 Rsft Hafcftery Road, Rfchburg. Wl 53711

-: 7 :. -, i •.- ''*-.." •--?*:i». .-.«?C->- r-f: •**.**•".; '•r

&ContainaraNo.

7. Total Quantity

9. NA2212. IU. BO

1C :Call. Cat 11

M HOUR Nonce orvdi P«OR TO DISPOSAL MUST BE

9. GaaBMTOfVOPBUTOfTS CEKmCATlON I -wreby dactars ihel t» oomarts of this consjgnmert am My and •n.maMif ttoajtied above by proper ship- vctv v*. t o^dH condôn for tampoit by IvQtwBjy aooordbvj to appficabte ntamabonala^wrh hazardous. PCS. anoVor any special was**.

PfWldrT ypvd Mw «WJ Tito SiQfVMLaTV ij ' U8t*t

' V^> /* ' *J t^^£f ^ ''/ • ' > ^* * + * / f

\

t&tftvtiQ M*nftflf (incfcjjiiij WB onto)

~~- . l,Pnrted Namf ana Tae

''-" X ' -^

Date - /y /

l>T\*f Signature

Prr-TBd Nam» ant) TBe

Datt

12 0>v»^vpwy ivoCarton SpMO9

{• HWaMiOMposalStoOMMr orOpmtor

r*

Sp*oal Wad* Affvoval is «au*d by kgnatura n v* cas« of a G«nanc Asbestos Approval.CcnitcaMn of r«o«t» of astestos 'lateruti cow«d oy ** manias; etoecx as ootad m nam 12.

w3 Pmad/Typad Name and T«e Senator.

MHTTE - Qapaa) Sit CMiWtv • Ovwaar = NK - ' ico-wr 3CU) - GOTraxOC£ ;30-»74«rnWTSB Tj * "*•«! s» :«po»» Sr»' Toteaunpnarladapan

Date

1

itWASTE SHIPMENT RECORD/ASBESTOS MANIFEST(4« Reverse for Instructions)

-A.Special Waste Profile Number NESHAP Notified

: YES .

WSR Number

7738721- B. Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code)


perator's Name and Complete

gc'-'-vî #Complete Mailing Address

3. Waste Disposal. Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal Facility • • •. • • •10712 South 124th Street; Frankllp. Wl 53132


Elevation. ' • •"'. '

North :

1-C. Generator's Phorte Number

1-6. 24 Hour Emergency Response.Telephone Number


WDS Phone Number

414/529-6180

4. Name and Address of Responsibly AgencyO Soutbcfast District. W»c6nslrv Department of Natural Resources

2300 N. Dr. Martin Luthar King Jr. Drive; Milwaukee, Wl 53212D South Central, Department of Natural Resources

3911 Rsh Hatchery Road, Fttchburg, Wl 53711

5. Description of Materials .; .•

friable asbestos ,

.ripn-friableesbwtoa

Asbestos, 9, NA22

<0 A>/4>

NA2212, Ilk RC>

Cat II


7. Total Quantity.yd3 . •

Wrtduf(N0ffibE'GrvENpmoRto:DispoSAL, MUST B| ÛRIEP,"

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, am) labeled, and are in all respect* In proper 'condition for transport by highway according to applicable Internationalanil gpverhmentVegulatibns. I hereby certify that the asbestos b not contaminated wimriazardoijs, PCS, atxltor any special waste.

PrlnteoVTyped Name and title


UComplete Mailing Address

Printed Nane .and Title







13. Waste Dlsposar Site Owner or Operator ~ ... >.. .. ' ' -Special Waste Approval Is issued by signature in the case, of a Generic AsbestOJi Approval.

'• Certification of receipt of asbestos materials covered by this rrtanffetf except as noted in Item 12.


\


DCE-230-97-METRO 7/99

CANARY • Generator PINK - Transporter(To be mailed by Disposal Site) ..


WASTE SHI<S*aHtvtntfe*

RECORD/ASBESTOS MANIFEST

i-ASptt

_YES NO 773873pMaUa Zip Code)

For Disposal Sia» Use Only

NortV EaJ-

1-C. Generator's Phomr Nwrt»r

i-E. 24 Haw Emageouy

Opantofs Phon* Numbsr

X Waaa Oaaoaal Sae (WPS) Mama and Oompua Uat

UMoRacyctngandOiapo«iFaca%10712 South 124* S»Mk RwMtfi. Wl 53132

- •» 11 . • » :..

414^29^180

Mctmai Oepanmeri ot Wfcm Rescues*2300 M. Or. Uartn UJih«r Wng Jr. Driv«; kAMAae, WI 53212

Soum Centra^ Department of Natural Resources3911 Rsh Hatchery Road Frtchburg. WI 53711

2« HOUR HOTCS GKO« WttOB TO DISPOSAL MUST Bt

9 GaaBMTOaOPBtATOfTS C€BTIF1CATX)N rwrvby deoar* mat ffw caments of the consqnraan are Uy and i«m*»l| deacnDed above by proper snip-OV^Q napia and an cflaavttad. packad% fnarkad, and abataHL and are *i al raapects in proper condition tor tuiupufl by rHQtaay aooonflng to yi^'rff*if iilOfnaflonal.

"". f hereby oat*y rv( r« aabadcB « •« contarrwi«ed »r* lazardojs. !>ca andtor any spacM«wl»: ""

S-gnaixj-7

10 Tranaponw 1 Company Nan*

v/rConpHi \

and Tfle

Dale _ -. iI- 3 - 2

i v Trawponar 2 Company Nama Orv»r

oods)

PTTIBO Name and TiBe

Dale

13. Waala Oiaposal Sta Ower or Operator• Approval « «so«o by sgnaLn r Jie case of a Generic Asbestos Approval.

i of racaipl of asbestcs -vaamafr cowed gy tfvs rraiVes1 eicapl as noted n item 12_

Data

MMTE CANAPV GOLDpnor 0 tfaponl)

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(Se« Reverse for Instructions)

1-A.Spectal WMte Profile Number NESHAP Notified

YES . NO

WSR Number

7-73614


Elevation. ' - . • - ' : - _-

North-


1-D.:WorkSK* Address 1-E. 24 Hour Emergency ResponseTelephone Number

2. Operator's Name and CompleteMalllnc; Address Operator's Phone Number

3. Waste Disposal Site (WDS) Name find Complete Mailing Address

• Metro Recycling and Disposal Facility . • :1Q712 South 124th Street; Franklin, yvt 53132

WDS Phone Number

414/529.-6180

4. Name and Adq>ess ol Hesponslble Agency• -Q Southeast Dfatrtot, Wteconsfti Department of Natural Resources.

• 2300 N. Dr. Martin Luther Kina Jr. Drive; Milwaukee, Vyi 53212O Soum Central, Department of Natural Resources

391 i Fish Hatchery Road, Rtchburg. Wl 5371 i

5. Description of Mdterlale 6. ContainersNo. . . Type

T. Total Quantityyd3

Asbestos, 9, NA2212, lit, RO iCat I. Cat II.

8, Special Handilna Instructions arid AddfttenaJ IntprmaBon' •'•'•'" 24fHbyRNOTie'E GivEft'PWOSTO DISPOSAL; Must B$ SuPiieb';:' ..

9, dENERATOFVOPERATOR-S CERTIFICATION: thereby declare that the contents of this consignment are fully and accurately described above fey proper ship-pine) name and are classified, psctied, marked,, and labeled, and are In ajl âspects In proper condition (or transport by highway, according to applicable internationaland government regulatfons. \ hereby certify'that ihe asbestos is not (xuiiarWr ed **i hazardoi.iB,PCB, and/or any special waste. • ' ' :

Printed/Typed Name and THle' DatT

10. Transporter 1 Company' w-Cbmplete Mailing Address

Driver Signature

Telephone Number (IncludingDate




Driver Signature


Date


11 Waste Disposal StteOWnar w Operator ; • •Special Wasta Approval is issued by signature in the case of a Generic Asbestos Approval.Certification'of receipt of asbestos rtiatertate covered by this manifest except as noted in Item 12.



OCE-230-97-METRO 7/99

CANARY - Generator PINK • Transporter(To be mailed by Disposal Site)


WASTE SHIPMENT RECORD/ASBESTOS MANIFEST

- A^peoeJ WM» Pwfc Ntntoer NESHAPNaefied

YES NO

WSP Number

773676

For Disposal Sto Use Only

Name. Uafing Address (indudnc Zip Code) 1-C. Generator's Phone Number

l-tXVtakSM» 1-E 24 How EiTMtqency Response

31 mx-

->C

and on*« UMhg Addrw*

: UMro tacydno ««• Ohport Fac*y10712 So* 1Z4» SttMC FnnUn. W1 53132

4147529^180

2300 N. Or. U**i Luffw King Jr. OnV*. . W1 53212Sooth Conlrat Departnflrt of Natural Raseurbes3911 Rah Hafcrfwy Road, RfcNjuy.Wl 53711


S. NA2212. Ul.no

I Addftwl kntvmelo» HOUR NOTICE OWEN PBIOfl TO D«SPOSAi-MUST BE BUHaK>;

guMone. I t*n certry tm tie atom** « not cortatnfnred ***• ^szattout. PCB. trtfdr any

if aionrnett ere fca> and >n.ualel» daacrfjerl above by proper shp-iKMoo tor tcaraport by rej fpey eopORftno to mifc rfiia kibMiNitfonal

10 Tranaponarl

X

Nunfcer fnoutng are* code)

' Primed Name atd TIMI

.f'' <• "'~

IV Ti

11 waatt Mooed 9» Oww or QprntotSpecial *m* *pprn i al H taauea by »QRMLM B tn one o< « Qanertc Aabettoi Approve.

-nata^Msowid9y Wair*nr*eet«x»pt at

PrtrtHtTyped N*ne and TVa

WWTE OOLODCC zrnr-»«rnio 7

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(Se» Reverse for InstQjfiVbns)


YES NO

WSR Number

773873


Elevation . •

1-a Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code) 1-C. Generator's Phone Number

1-D. Work Site Address 1-E. 24 Hour Emergency Respon'seTelephone Number

2. Operator's"

Complete MaHlia Address Operator's Phone Number


• Metro Recycling and Disposal Facility. .10712 South 124th Street; FranKIJn, Wl 53132 . . ,

WDS Phone Number

414/529-6180

4. Name and Address of Responsible Agency. O Southeast District, Wisconsin Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212 .. D South Central, Department of Natural Resources

3911 Fish Hatchery. Road. Fitchburg, Wl 5371J

S. Description of Materials . - - , 6. ContainersNo. Type

7. Total Quantity• ' . yd3 .

friabte asbestos Asbestos, 9, .NA2212, III, RC1

f*.fetl U, •_', , , . ;non-friab|easbestos Call. Cat|l.

8. Special Handling Instructions and Additional Information• : /: 24 HbUfi NQTIClfe Grv€NrPRiOR tb DISPOSAL, MUSTBE BORIEft

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are In aH respects In proper cordition for transport by highway according to applicable internationaland govemrnentVegulations. I hereby certify that the asbestos is not contaminated with Hazardous, PCB, and/or any spedar waste.

Pri Name and Slgi

MT:

Date





Date




Driver Signature


Dat»


1 3 . Waste Disposal SitaOwrfar o f Operator . . . • ' ' r ' _ .Special Waste Approval la issued by signature in the case o< a Generic Asbestos Approval..Certification of receipt of asbestos materials covered by this manifest except as noted in Kern 12.



DCE-230-97-METRO 7/99



WASTE SHIPMENT RECORD / ASBESTOS MANIFEST(S«* AMO* far Mtuclm)

NESHAPSoCM

/ YES NO

WSfl

7736771-a. Gmraor NMMI CortKl MM*. wd CompMa ktaAng AdffM* jndudng Zip Cod*)

£> .•'•-- ^- -'

*» «*P— sn. u» o*

Nnti Ea«f

1-C. Gmaior-* Phone Numter

1-E. 2* Hotf Eiinrgniuy ReaponMTalipharw Mntwr

Operator's F^vw Nun Mr£','. •-*

(MpoMl S»» (WOSJ Nww wd Compwo Urfng Ao>

Itafeo Rtcycino wd Otaport FwWy10712 So* 12«h Stwt Franttn, Wl 53132

WDS Phan* Nui«v4147529^180

m ^^^^^^ ^—^ A^L^^^^ jrf I*- ^HPIV n HQ^^VBV V •

C •jmMmgl rnnh I. Vflrnmtn PnparHTMini ntttfint ninmrrii2300 H. Or. Mv*i LutMr Khig Jr. OTVK U»m*M. W1 53212

Sou* Ccrtnl. Depadnwnl of Natural Resources3911 Fah Hathery Road, Rtchburg, Wl 53711

24 HOUR NOTCE QIVBl PflKM TO 0«POSM-MUST BE BUREO.

v>d iflbctad* vd w in rf rwpvcti m pnjpv ooNiftion tor twport by N tw r •ocofdhig 101I fNrabr c*rtfy •« r« IUJMIM • -xx ccnttnin«M ** huwtxxj*. PCS. wvVix «iy ^wdM i

10 Trmport* 1 Cenpcny NHM

; J ,;' /' / 3 J

Kt»>

D'v*r Sigmtur*

Prtm*d N«m* and TIM

///1 1 - T

ooov)

11 orQpmor

^-^-_ ""Ovwcrton of fvo^pt ofnffwiv««d Sy t«i .•nttVMt «)tc«p( u nowl m tarn 12.

MMTE OOLD


1-A.Spedal Waste Profile Number NESHAP Notified

A YES NO

WSR Number

77387*


Elevation. .

North

1-a Generator Name, Contact Name, and Complete Mailing Address (including Zip Code) 1-C. Generator's Phone Number

1-D. Worksite Address

"> .\



/?; '<j'!

3. Waste Disposal Site (WDS) Name and Mailing Address

' Metro Recycling' and Disposal facility10712 South 124th Street; Franklin, Wl 53132

WDS Phone Number

414/529-6180

4. Name and Address.of Responsible Agencyd Southeast Distrtcf, Wlsconiirt Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212 •D South Central, Department of Natural Resources


5. Deecriptlon of Materials f - - iêTO 6. Containers'No. , Type

7. Total Quantity

frtatte asbestos , 9, NA2212, III. RO • inon-friable asbestos,! Cat) Cat II

8, Special Handling Instructions and Additional Information ,•;'.'" ' ' 24 HOUR NOTICE GIVENi PRIOR TO DISPOSAL,- MUST BE BURIED:.- ' '. . •;; . ';,--- >i v ' ,

a. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship,ping name and ar» classified, packed, marked,, and, labeled, and are in all respects irVppper.condition for transport by highway according; to applicable internationaland government regulations. I hereby certify ftiat the asbestos Is not contamkateclt hazardoiis, PCB, and/or any special wast», ' • -

PrinteoVTed Name ar Title

1 Company Name


7 '. >' .


Telephone Number (ncluding area code)

Driver Signature11. Transporter 2 Company Name



Telephone Number (fncfuding area code)


It3. Waste Disposal Stte Owner or Operator '. ,-Special Waste Approval Is Issued by signature In the case of a Generic Asbestos /approval.Certification of receipt of asbestos materiats covered by this manifest except as noted in Item 12.

Printeo/Typed Name and Title Signature Date


DCE-230-97-METRO 7/99

CANARY • Generator PINK - Transporter(To be mailed by Disposal Site)

GOLD • Generator(To be taken prior to disposal)

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST

NESKAPMOI««J

V YES NO

WSRNumbw

772435

ta "»°-1 »• "» °*

f»^^ 1-C. GmnlVs Phone Number

^ /

1-E- 24 How EfTMfQtncy Rosponas

414 071 0070

2. OparaJort Nan* and OoeapMt Ma*ng Addraa** Mid Oom Optntaft Ptnn* Numtxr

41< 871 0070

3. Waaat Papoaal Sea (WPS) Mama and Compute i luang AddraaaOretvrt Hug* RDF • W124 N9965 Boundary Roaxt Manomorwa Fals. Wl 53O51

orUtfro ROf • 10712 Sou* 124*t Sdwl FfwMn. Wl 53132

262-253-8620414-526180

DMtal2300 N. Or. Mv«n LuffMr Wng Jr Oiw: Wl 53212

B. SpaoM rtandtag34 HOUR Monceowe* pf

9 GENeRATORO>BMTORS CERTFCAT1ON: 1 >»«

. I hantoy s»l*i t«( tfw

dada/v ffnt tfia cociiercs erf ttw oonsiQnniart aj*a Utjr and aocuataly daaxrtbad abova by ptopar 9Np-and ara in at raepects n proper condfton tor tiananorl t»y NgN*» aixun*ig to appfcabta imeinallunal

hazardous. PCS. and/or any special MBta.

IttTi 1 Company Nama

TtVaflp^W Ntf baW pnCJUaJaTIQ 9fH OOdlV)

414-671-6070

Signature

PrimadName and TIB*

Dale

11WM

ompany NMIM Dryer

W124 Nttes Boundary Roadi Fate. Wl 53061 Printed Name arxl Tffla

pnduwiy n«i cixto)

202-2S1-4000

C. • -.:.i I

Date

12

i iaauad by »gnaB«a n tw caaa of a Qanarc Asbestos Approval.I MitenPi m»«red by tv man4e5t excapt as notod in ham 12.

Mm art TT»» Date

1709

CMWtt~c S«

O0l£;To be OMn pnor

. WASTE SHIPMENT RECORD/ASBESTOS MANIFEST/ (See Reverse for Instructions) " •.

-A.Spedal Waste Profile Number NESHAP Notified

_^ YES . _NO

WSR Number

772453


Elevation,;

North Eart

-B. Generator Name, Contact Name, and_Complete Mailing Address (Including Zip Code) 1-C. Generator's Phone Number


414 071-00704'<# ± 7/y- 7-*

2. Operator's Name and Complete Mailing Address' ' '

1001 Meiih Olat Stroeti MHwnukse( Wl 63308 A/


414-071-9070

3. waste Disposal Site (WDS) Name and Complete Mailing AddressOrchard Ridge RDF • W1?4 N9aS5 Boundary Road; Menomonee Falls, Wl 53051.,"'•'• ' • ' • • - ' • • > > • • . • • • • • • . ' , o r - " • ' • •Metro RQF • 10712 SoirtJY 124th Street* franklijv, Wl 53132

WDS Phone Number

262-259-8620414-529-6180

4. Name and Address of Responsible AgencySoutheast District, Wisconsin Department of Natural Resources2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212

noivWaJ)(e asbestos,,, rj

8. Special Handling Instruction* and Ackfittonal Information'' QlWNP IOR TO blSPOSAL,MUsTBk BURIED,:,: P /,

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are dassHled, packed, marked, and labeled, and are In all respects-in proper condition for transport by highway according to applicable Internationaland go'ierhrnerrf regulations. I hereby certify trial the asbestos Is hcrt contaminated with hazardous, PCS, and/or any special waste.

Printed/typed Nam* ah&TftJB':' ^_" • j.; ~ | Slgnature__il' !^J ~J ~~T'~1 ~^ r~^ | Date


Complete Mailing Address /ft. i /MHwaukee. W| SOBO»" . /.':- 'N ' -

• -.. '.• •'• - •'. '•->-•• .. - i) :':" * . - . . : •

Telephone Number (including area code)• 414071 0070- i f , . - , I JIO(J

Driver Signature.


Date

11. Transporter 2 Company NameWM Milwaukee • : ' ;

Complete Mailing Address :S'~

W124 N8925 Boundary RoadMenomonee Falls, Wl 53051

Telephone Number (including; area code)

Driver Signature



I13. WwteDlsposalSteCJwjriardrClperaJW » : , ; , - . <

Special Waste Approval Issued by signature In the case qf a Generic As&estos.Approval.Certification of receipt of asbestos materials covered by this manifest except as noted In Item 12.


WHITE - Dfepoul SiteDCE-230-97-OR Team 7/03

CANARY-Generator(To b« mailed by Olspoul Site)

PINK-Transporter GOLD - Generator(To be taken prior to disposal)

Ig

I

'

|

•

1

OCX

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(Sfra n»«nM tor matrudfanal

U/=J,i/- V- - 773215\ '^ J L I/ V_ fi-a. GenKaiar Ham. Gonna Name, and Comptaai Miing Address j*x3uoing Zip Code) 1

- . - \. ' \ { \ J < \\ ''K\ .X • '••. Vl\-> 'v_ Lv_V-V -'' '" '-^- :v-^-1

i-D WortSaeMdraea

O\ v t. \v P -f O \ . ' 'A * VN*t . ^\\ . yV^ \

, v v.\ XV ^. k. -r. ~ x . - ''\ ' ; . NJX u ( ' L - ''• r^ C4. S. ' ; ^ - . • ' v x .r 'r iW^ \ v AvV «y^nv\3.WaaaiOH(KM«Sto(W06)Nan«andC<vTvMaMaB^/W>drw3 1

IMro Recydng and Dtapn* Fac«y10712 Sout» 124li S*Mt FrantdaT, Wl S3 132

4- MtfB0 md Advw OB nHpootfoiv AQsncy

5. OMcnpton of UaMiVvAi "• jpf'v^t'' " v " -- " fi:-^. % ~ f * * ~ * * < ' • •i^^-iSf^1'- ^

,- ftMb.* Hl.iH.taB ' MJWfft. 9. HA22T2, III. RQ

jup(.fc'"^f*t i ^^^ Ctf 1 Cat II

•1 f^^^^gj llaMMpfcan 1 BBifl I_U1_L JJUl i hH kliBBl LX l aVkn

24 HOUR NOntX aVBI PRIOR TO OCSP06AL MUST BE BUfVEO

9. GOCRATOftOPeWTOirS CtHIIHCATOX I n«nM>y dactare t4 fw acmarts ^ the co-is-gnmert are Uy end ai

Pr.artTnwlNM.nd Tte S^. /^ - ,

^f1 s 7^ • (-V- ^r Pnrao pame and Tio»

V^fl'-' '\ f^ '•

Dale -^Ti (I

1 1 Tiaraponw 2 Company Mania D^v^ Sgnatjre

Prreo Name ana "HBe

Dais

12 naaepanor mrfcafco Space

11 Waafc (kapoaal Sh»Oanar or Operator

Cartecjeon ot r»ca<« o< ytfxram Taseraa cav«r«d by 9w Tan'%s! eicapi as noted r item 12.

Pnraad.Typed Name and T*» Strati**

MMTE - Ovoool St» ZMtMn Zmrmx - •vf. ~ -vsxtvr GOLD -130-77 -tarntOTW ': M -wt*e > âpou S« Tot»t


North EastW

-C. Generator's Phone Number

-E. 24 Hour Emergency ResponseTelephone Number

Operators Phone Number

vuS Rion0 NtfVebflr

rf^f9lUt^^f^9^f

mcnory rtoao, rvcnourg, wi bo/n

L Cortann 7. Tolari Quantityto. Type yd3

'•• '^- ^- •/ v' .

Data

Date

G«fl»l*B

'x \./if t f t f ^ 'WASTE SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse for Instructions)


YES .

WSR Number

773213


Elevation .

Norttv-

1-B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code)1 • .V-\ \ > \'0- v \. ', ! '' • • ' . , ' i \ ._ <V.


"-\>Vi. \, '.. \' )' ( -^

1-p. Worksite Address

.) > r . \\ \ C' \

1 • E. 24 Hour Emergency ResponseTelephone Number

\ ,\

2. Operator's Name end Complete Maillno Address

f r'\ ^ f ' .- \


3. Waste Disposal Site (WDS) Name %nd Complete Mailing Address

, Metro Recycling and Disposal Facility10712 South 124th Street; Franklin, Wl 53132

WDS Phone Number


2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212O South Central, Department of Natural Resources


5. Description of Materials 6. ContainersNo.

7. Total Quantity

asbestos; Asbestos, 9, NA2212, III, RQ

non-friable asbestos Call. Cat II

8. Special Handling Instructions and Additional Information: ' 24 HOUR NOTICE GIVEN1 PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed., marked, and labeled, and are In all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby' certify"trial the asbestos is not contaminated with hazar/fous, PCB, and/or any special waste. '

Printed/Typed Name and Title '

o A^ HrDate• „- -s


Complete Mailing AddreuC /

,..:. •) i .- ., •+ '•"/ x-'-7


Driver Signature

Printed Name and Title*Date



' Telephone Number (Including area code)

Driver Signature



13. Waste Disposal Site Owner or Operator i •'Special Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted'in Item 12.



DCE-230-97-METHO 7/99


PINK • Transporter QOtO - Generator(To

/ I

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See ne»eue far tnrtruotons)

NO

WSM Number

773216


North East

1-B-GerwaBvMarne. Contact Name, and CompM Uaeng Address «<x3ucirfl Zio Codei 1-C. Generator's Phone Number

D.Wo*S«eAddree» 1-E. 24 Houf Emergency ResponseTelephone Number

-d.Z Operatr* M*m and Complete Uaflng Address Operator's Ptione Number

Otapoc* Sto (¥«9 Mw» and Compww hb*ng Address

Uako flacycii ant Disposal FatiMy10712 SoUh 124ft Strwt Frartdn. Wl 53132

WDS Phons Ntfnter

414^529^180

I? SouftMtt Prtrtct. Wsconsn Department at Nafarat ResoureasZ300 N. Or. Uvto Lmher King Jr. Drive hHwaiAae, Wl 53212

D South Centrat. Oepartmert of Natural Resources3911 Rsft Hachery Road. Rtcttxjrg, Wl 53711

&0eecnp*onolND- Type

7. Total QuwTbtyy«B

9. MA2212 IB.

Catl. Cat II

bvlrudkn andZ« HOtF NOTCC QfVBt PWOfl TO CXSPOSAL MUST BE BURCO.

pvv nane and aw c• CERTIFICATION- inacfced. marked, and

f hereby certify tat r«

declare mat 0w contents 3! thts consignment are Uy and accurately itnutmi above by proper shp-wid are fat respects r proper conctabn lor transport by Mglaray aumfcig to appicabte jntemational

a not cxxitarrjnafee *ff âzarbcus. PCB. ancVor any special vaste.

PrtniedrTyped Name and Tile

r: . .; - - J . r tDale

Traneponei \ Company Nvne

17

Tetephi dkxlng are* code)

oo

Name and Tiae

3 - 3 -11 Traneponar 2 Company Name

Cunqleli Ualng Address

Telephone NiMtoer rjndbrAnQ area code)

Pnrted Name arw Tn)e

Date

12 DiBfiepancy Indcaaon

11 Waat Oopocal Set Owner or OperatorSped* Watte Approval« ssuea o> s nabs* r ?w case o< a Geneve AsbestosCertfcaMn of rec*pt ol asoestta -a»naa a flfec By uvs nar. est etceo; as ictec in rwn 12.

Sgna&re Date

MMTTE

: a* -*«: ;> >«pc» 3«30LD.To IN

JON-10-1999 03370TO:96^50645

WASTE SHIPMENT RECORD /ASBESTOS MANIFESTpoo FtaMTN tor MUructfMM)

1- A.DPMUI Wwrtu Preflti Nwiter NESHAP NWHM WSKNuffllMr Q«viillon__

t-B QMttTttor NariM, Contna Nwrw, und CnnpMa Milling AtidrMi (Including Zip Co*)mpMB Milling Addn* l-t! Qcwntar't PhoiM Nundnr

1-D.WwKftlMMdnao 1 -E. 24 Hour PnwrgMKy Riyipomw

OMCrDlWI Phatt NumtMT

y. W«M ObixNuil Sit (Wixt) Nam* unri campta

Metro Hooycung and OlnpoM* Taofbiy1071? Soutti 124|n StHXK. Fn«)Wln, Wl 83132

W08 Wxir» Numbw414/529 6180

4. Nwiu nnd MHRNO of RM|MnalM« AovwyG SaulhoMt OMncL Wisconsin ntqartment m Natural Hmourcm

2300 N. Ui. Martm Lulhor King Jr. DrivM. Mlwauluw, Wl 53212D South Contra), Doponmwi ul Natural HMOUHUM

3911 F-feh HuWwy Road, Fttchbuvj, Wl 5371 1

A ContaiiWiNO lyiw

/ Tod/QuoriUvyd3

frUM ubcalM Ill, HO

non-frfcWu DdMtol

6 fl|iKii< H«vf Ing (rwttjctktfu uiU AddMeml lufncmHtenM 1 UUP NOTCta QlvrN PHIUR TO DBHOSAL. MU81 HF BUHIbD

U. GCNtBATOfVOI'tRATOR'S UGRTinCAI HtH: I hinby (ktolart tilt On corttm ol Ihli cwt*igniiMnl vti IgDy anri •eourWflly dMcribu) abovw by P»up<w <Np-pkig ndd» and M ctacOM, pwdnd. rMrtwii. onri labtltd. ixxlan In U ronrndi rn piupw condition tar trmnapott by hlghwuy nooorthg to appfcaw Numntfoniland UUY»TWI>O*« ngtMUon* I horuby c«ct>y thul |tw aibflkM « not conuniinflMd wilh homrdouw. PCR. «noVoi any ipaclll nuOM.

DCE-2SOIW METRO 7-»9rWABV-U»nwwor WNK - Tr*Spir*r(To hr ni.iikKJ by vMWOMI OM1

UOkO-OMWMgr(TO M Hktn F»Kx to <h«fiiv.il)

/ * IWASTE SHIPMENT RECORD/ASBESTOS MANIFEST(See RMTW tor InMuctonB)

- Sbeoal Waae Pro** Number NESfAP Motaed

YES NO

WSR

773237

For Disposal Site Use Onry

East

1-B Gararalor Name. Oirtacl Nanw. and Com0eti UaAng Address .nouctng Zo Code: l-C. Generator's Phone Number

10 Work S«» Address 1-E- 24 Hour Emergency ResponseTelephone Number

2 Operators Name and CpmplHi UaaYig Man Operators Phone Number

tisto 0«>S) N»n» and Comjawt Uaing Address

Uatjo RecydnQ vtd OBpoait r acfty10712 Souti 124ti SkMt; FrvMn, W» 53132

WDS Phone Number

414/529-6180

G SoutiBMl Planet Wiaconain Departnert o> Nafcjrai Resources2300 N. Dr. Uartn LuOwr King Jr Orv«: UtomAM. Wl 53212

Sou» Central, Department at Natural Resource!3911 fish Hatchery Road, Htdtourg, Wl 53711

No. Type7. Total Quantity

y<*3

Asbestos, 9 NA2212. ill,

Cat I Cat II

nttoekucft)M HOUR NOT1C( QWBIPMOB TD 0*SPOS*U MUST 3E BUWED-

PriflAVdTTyPMf MeaMe) VVl Tito f*Qf\&kf9f.

'• ,. '•* \ \ • •- ( \6'/>

. ,i.,W..1 T***on» Ntfrt* CndUftng .VM cod»)

1 11 Trwwpomr 2 Company Mtro

Ttf hon* Hunter fvckatftng am cod»)

"• / /' Dal*

Â- ,-.^"ted ftene and Tato

Caie ___, : i

OTI-*' Signatu'B

(*-1ed Name and Ta»

Oam

tf

• 13 Was»DopoMl S»a Oaner or Operator

Oai*faalui of recee^ of x#*wn ~fjer*a coverec

PnvaovTyped Name and T«e

» case of a 3en»rK Asbesuw Aporoval• by tms -anês! *xcep( as --wed m tem 12.

S^natua Date

GCXD-Jo t» u**r pnor 10 dopoor)

' 7

/ft/(S*

TF

ASTE SHIPMENT RECORD /ASBESTOS MANIFESTSee Revere* for Instructions) j

-A.Speclal Waste Proflte Number NESHAP Notified

Jd-YES . NO

WSR Number

7T32381-B> Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code)


Elevation . . • .

North


1-D..Work Site Address

V .1-E. 24 Hour Emergency Response

Telephone Number

131CA1iling Address

" AOperator's Phone Number


Metp» Reeydinfl-and PtepoMii10712 South 124th Street; ffinfc|}

WDS Phone Number

4. Name and Address of Responsible Agency••pi SoutheastOetrict, WlsCoosiRDepartment o( Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee. Wl 53212Q South Qeritralj Department .Qf Natural Resources :

3911 Fish Hatchery Road. Fltchburg, yyi KI7J1

8. Containers

•11,7. Total Quantity

;Ca^ r.. '.,..,,: .. ( Cat» .__,......

8. Special Handling Instructions ap<J Additional Information^>?^M:-24>fouR:Nicl(3JVI^p|^

9. GENERATOR/OPERATOR'S CERTIFICATION: t hereby declare that the contents of thli consijjnmerif are fully and accurately described above by proper ship-name and are classified, packed, marKed, and labeled, and are In all rftbects |n proper condition for transport oy highway according to applicable international30-vBmrflenir-eûlafens/l hereby certify thai the a^stoi is not '! • ' '

Printed/ryped-r4arfiearldThle" •,-•-• V: ::.??;>». V(fejft<,;;,}-;;rv; / > . • ' •


l*sfs\ :Complete Mailing Address-*

Driver Signature/

Printed Name and Title,


,11. Transporter 2 Company Name



Driver Signature


Date .

12. Discrepancy Indication Space\1

13. Waste Dlspoeal Sjte Owner er Operator . . > : . • ; :Special Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials'covered by mis manifest except as rioted in Item 12.

Printed/Typed Name and Title Signature Dafe

WHITE - Disposal Sto

DCE-230-97-METRO 7/99

CANARY • Generator . PINK - Transporter(To be mailed by Disposal Site)

.^"7.^ K


-

i1i

iK

9

I

PISTE SHIPMENT RECORD /ASBESTOS MANIFEST

/ £> 5 Q G» ^s "0t-tt. Generator Men*. Cwttct Nam, and CcmoM* Mating Address ,«*j*»; Bo Coda!

1 O.Wa*Sa*Adj*MK . vA

„ -x ' . .:. V\ t r s i • • v

^\\V?"<rr--. • • • * ' , 1 / w'v.3 Waale Oapoeal Sat (WfOS) Name and Comptew «a*ng MOrtsa

Matro Rwycino and Otopool FarJMy10712 Soult 124ti S»Mt;Fnr*fin, Wl 53132

4 NMW and AMwa of Reaporet* Agency

2300 M- Or Marto Lutfw Kr>g Jr Otv«' fuaTuntiJunt Wl 5321 2

5. Oetcnpton of MMenab V •

' kbJH* aatMetoa . Aabastoa. 9. NA2212. ill. R(

nort-fctatte aataekw Cat) Cat II

24 HOUR NOTKX GIVEN PROR TO OBPOSAU laUST BE BURtECX

PrinMTTyped Name and TWe Signature '

'. <* f ' v- \ v ' ,^- 1 - V / /'

/ / T "7 ^ -i -7 X .„ -'' /— | /: PTTad Name <

T-. .H r ,«*««,«« j J-'ff

\ Ut f] L '• 1 /^/j Date ^/

r t Traceporte' 2 Company N*r«e ' C-.-e' Stgr u--

CornpMe Uaftng Adrjra«

P--tse »4ame ,

Date

12 DexiepanQf Indcafton Space

13 Waala Oapocal Sa« Owier or OperatorSped* Want Approval a asuec D> s rtam n 3-« case of a Genenc Asoestos

•^TaâWi ^ttO NaTO «vv] iflc &OT^XLÔ

For Disposal Site Use Onry

773242 M M- 1

t-C. Generator-* Prone Number

1-E- M Hour Emergency ResponseTelephone Number

- . . i •.I "

Operator's f iom Nmnbor

-\\^\-(j ;>-i-'. -C Or ">SWDS Phone Number

414/529-6180

aouui \jtntu, UojxaiBiwiB ui Natural riesources

V S.Cantainen 7. Total Quantity• '. -' r? ' i*-. "- l*x T*l* y**3

1

sjgnn.fft «B My wu jmtfianli onciiMKl atxive by proper ship-

us f*ctJ. andiV any spaod •astt.

Oato

,y M-/V^'/"/

ind Tide /

- / 'J ' J W8

I"X3 TrBe

Approval

Dafc

r^ '

•u

CAMARY - Gerwacr acxo «TO bt 5*«n pnor la dapoal)



YES . _NO

WSR Number


1-Q. Work Site Address

31


444-aiLaozaA\\Â~Fzrp"}--^ ),.2. Operator's Name and Complete Mailing

Î ' l î- (

a \ \ v O


3. Waste Disposal Site (WDS) Nam* and Complete Mailing AddressOrchard Ridge RDF • W124 N?355 Boundary Road; Menomonee Falls, Wl 53051

' .--V1 ' • ' ' • ' • • " ' ; ' . ' • • - ' o r : ' • •Metro RDF »10712 Souttvt24th Street, Franklin, Wl 53132

WDS Phone Number

4. Name and Addres* of Responsible Agency- Sdiitfaasf DtBtrk* Wiscqrwjrt pepartrnpBj of Natural Respureesi2300 N- Or. Martirt Luther King Jr. Drive; Milwaukee, WJ 53212

8. Special Handling Instructions and Additional Information'

9. GENERATOR/OPERATOR'S CERTIFtCATtON: I hereby declare thai the contents of this coniilgnment are fully aiid accurately described above by proper ship-name and are classified, packed; marked, and labeled, and are in all respects In proper condition for transport by highway according to applicable International> • " -"-'-^'^" • - •

PrlntedfTyped Name end TWe

0. Transporter 1 Company NameTeam, Inc.

4901 North 3KI StreetMilwaukee. Wl

Telephofw Number p'rctudbig area <414-871-907d


BiliK

Date-'"

11. Transporter 2. Company Name' WM Milwaukee

Complete Malting Address'

W124 N8925 Boundary RoadMenomonee Falls, Wl 53051

Telephone Number (including area code)262-251-4000 V

Driver Signature

Printed Name and Tito

x £i< ,,

Dalerf:< \,


I13. Waste Disposal Site Owner of OperatorSpecial Waste Approval Is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted In ftem 12.



DCE-230-97-OR Team 7i



WASTE SHIPMENT RECORD ASBES(See

MANIF

i - A. Spec* Warti ProBe Number NESHAP Scaned

YES 773243Name, and Cerate* Uaing Address ndudng Zip Code!

For disposal Site Use Only

Beaton

East


1-0. \Mork See

•?!)l-E-24 Hour Emergency Response

Telephone Number

and CompMi Ua*ng Address Operator's Phone Number

I Set (WOS) Name and CompHw Uaflng Addresa

ino am inpniflt racany10712 Sou* 124* SkJMt Frarttn, W S3132

WOS Phono NmtMf

414^29^180

D Sou*MM OWLVfiKonin Department o< HaMa* Resources2300 H Or. Mar*f LJtm Kng J». Dnv«; MwaukM. Wl 53212

D SoutiCflrttaLOepartmanloi Natural Resources3911 fish Hatchery Road. Rtehburg. Wl 53711

li;-&No.

7. Total Quantityy<B

AsfaeEK*. 9. NAZJ12 ID. RQ

Call Cat il

•. SpecMl HandVig horucCam and Adcttonri mfcrrvaton24 HOUR NOTCC QWW PWOH TO DISPOSM- MUST BE BUHED.

I hereby dedare t<at t»e ccrteofc of irt* consignment are **V and aocuraWf described above by proper sNp-and '-abeftad, and are f al respects -r proper cudJoun lor kamport by h May acoofdng to appicable international

I lB»by certfy 9w tw aabaooi * not oontarari,- cad M * hazardous/PCs andtor any special «asai.

Paired Name anc Tiie

i T( . code^Daw

12

i11 Wa«e Oepocat S*> Owier or OperatorSpeoaJ Wast* Approval a ssi c c>Ortecakon or -voecx of asbestos -

r r« ^se c< a Generic Asoestos3> r* "•jrfes; e«ceci as ii'ec m tern 12.

5 PrmeaTêo Nam and T*e ! S^-ar^-e

ii

Date

VtHTTH -DiocxuSta7: a* aur grcr E cldpcsai

// WASTE SHIPMENT RECORD /ASBESTOS MANIFES

(See Reverse for Instructions)


Jh ^generator Nam

NESHAP Notified

YES NO

WSR Number

773250


Elevation. •__

North East__ _Name, Contact Name, and Complete Mailing Address (including Zip Code)

?-? \Yi\tAA


1-D. Wori> Site Address 1 - E. 24 Hour Emergency ResponseTelephone Number

2. Operator's Name and Complete Mailing Address' Operator's Phone Number

V..U i v u \ \ A j l3. Waste Disposal Site (WDS) Name and Complete Mailing Address

; Metro Recycling and. Disposal Faculty • . .107121 South 124th Street; Franklin, Wl 53132

. . ' . <,'S* :> : v :.:>.r •-' '• . ' i '

WOS Phone Number414/529-6180

4, Name and Addres* qlRe_spons(ble Agency

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 5321?Q South Centra*, Department of Natural Resources

3911 Fish Hatchery Road. Frtchburg, Wl 53711

6. Containers 7. Total Quantity. yd3 .

Asbestos, a, NA2212, ,|J| • RO

Caitv:_ :_ .; ... Cat 11^

8. Special Handling mstrucflona and Additional Information. I i-r •": \ # WCUH Nortel Q&ter* PBiotf.td DJSPOSA

' , .'K'.., .!.!.....-.-. . -,,;.., ...I - .1 .

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that tha contents of this consignment are Mty an? accurately described above by prepef shlp-' name and are' classifjedjpqcked, marked, and labeled, and are in ajj respects in proper condltjon for transport by. highway according to applicable International

: * ' • ' • i ' " '

10. Transporter 1 Company NaTJ^

Complete M^Hng Address

Telephone Number (including area codeumber (including

- Y A

• / //A r>Printed Name and Titte

V'W, 7Date


Complete Mailing Xddress


Driver Signature


Date .


13. Waste Disposal SHeOwnef or Operator •Special Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except aa noted in Item 12.


WHITf- Disposal Site

DCE-230-97-METRO 7/99



WASTE SMPMENT RECORD/ASBESTOS MANIFEST(SMl

_Yt8 NO 773246l-i. Ga

tiJ J

10712 Soutfl 12«ti SMM: FrwMn. Wl SS132

Far OtpOHt 3* UM Only

1C Q

1-E_ M Hotf EJM^Bncy nKponcA

414^29-6180

SouftMi OtaMet. Whoonto O^vtnvt of Nanl RMOUCM2300 It Or. MMi Lutar Hng > CW*r. MM*M. Wt 53212

Sou» C***. O^MiHrt o< Nttnl RMOUOM3911 Fbh Hatfiary HcMt FftcMwg. Wl 53711

M MOUM Noncz onei PMW TO OSPOSN. yusr K BURCO

xwfcor tor lAfupofl by taQ^wvif •coovdMO to NM/

(2.305*2.WASTE SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse for Instructions)

1-A.Speda! Waste Profile Number NESHAP Notified

YES _NO

WSR Number

741689B. Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code)

t t \\ A\/.


Elevation .

North



-'II f.



''11. t tt 71/73. Waste Disposal Site (WDS) Name and Complete Mailing Address

Orchard Ridge Recycling and Disposal FacilityW124 N9355 Boundary Road; Menornonee Falls, Wl 53051

WDS Phone Number

414/253-8620

4. Name and Address ol Responsible Agency:

j" Southeast Dfefrict, Wisconsin department of Natural Resources230Q N. Or. Martin Luther King Jr. Drive; Milwaukee. Wl 53212



Asbestos, 9. NA2212, III, RQ

rioofriable asbestos Cat I. Cat II

8. Special Hanaing Instructions and Additional Information24 HOUR NOTICE GIVEN PRIOR1 TO DISPOSAL, MUST BE BURIED

9. GENERATOR/OPERATOR'SI CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name arid are classified, packed, marked, and labeled, and are In all respects In proper condition for transport by highway according to applicable international'and government regulatiorft. I hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste. '


10. Transporter 1 Company Name Driver Sign


/Ot.27Printed Name and Title

Telephone Number (including area code)Date

7/J /></1.1. Transporter 2 Company Name



Driver Signature


Date


13. Waste Disposal Site Owner or OperatorSpecial Waste Approval Is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.


DCE-230-97-OR

WHITE - Disposal Site CANARY • Generator PINK • Transporter(To be mailed by Disposal Site)

GOLD - Generator(To be taken prior lo disposal)

/WASTE REtoRD / WsfeESTOS MANIFEST

1-A.SpWM

4iYES NO

WSHNc-nbw

773249ConHd Nam*, and Complete Uaicg AddteM (reUftng Zjp Code) K*w Numb*

1-0. 1 - E 24 Hour EmaryineyT efophon^ Nutrcwr

9.WOS Phom Nunbar414/529-6180

53132

O;; 3ot*M« DHMX. mtoamm Qppertr** at HaMtf Hwourcas2300 hLoTSlrtn tutw King *. D**; MhraiABa Wl S32«?

" • - • ' • • • • ' ' • •3911

S. Otacf /ton ol Ua»Mi ti!', 35': 7. ToM Ouvrty

Cass

•I 24 PWOA TO dlSPOS*. HUST B6 BURIED

9 Ot@4BWTORCfRArC)(rS C&mFICAtlCISI: ' fw*r dBdara <hj| DM ccr-jrrj o( Dis consiff mart are fcJr and acxuaMy desoiwd above by pnpw sl%)-«jlp«c*»<l. fTBrV«J and jD*»d, and i-e m al lespacs - yope> condfcon'or u»»<)ort by higfrnay acuxtfnq to appfcatte intematiooal

Hrtby cert+yHâ«r» aafcestn 3 rxa ajswrinrêc '-*1 "ajajd^LE-. PCB. andtr any speoaf wasin. ' . ; ! • - • •

10

V

P'rteo Name and "HOa,

,. -M .,«- >Ci-,

11. Ti

ConftMtUafingA

iriad Name and TTfc

Dala

iagrutx* n r« c«s* o» a Gane-c Asbestos

a*rw*ip»of a*t*s-o< -njairafc ccvjradtif Jhs -jrr'eir *tce« as ->o»)inl«jm li. . .2 P*«rtT>p«J M«T» and T*§ S^naa>-6 Da»

QCLO-To te anr prer to dapea»)

1-ASp»o<«t Waste Proflf* Number,,^.,.TT3?47' • i

' ^ ' ' ' - ' / ; : J j - : ' 1 ' 1 ' : : - ' ' - i '

£*m&w^v>& P:. .:...i:-,.^-;.. .-..,;-i. . . " • . » • - ..-.,» '- - • ' *:

?.Operato*'»NamtandC<)rt)pteteMailinaAddres<•-^^•^tS'^f-Vi't'f^'^^ *•<- ":> ••-î.tj •>« ,|4: ,:T*V f:X''^t/;i -"'> :S':i" v-,^''.v x'?;-:. «'

a Waste Olsppsal Sft^ (WD3) Name an<i Complete MallA* Addrew'"' " ' ' '' ' ' ' '

^(Mft^fe^%'-t. >$. '< '4>.<-»v 4 '^:^-i--i^% 5ii-.^?llt,K^î!ffg^H^^-^%>.^>îv^r>î^ff^

WDS Phone NumBer

414/ 9-6180;. /;w't:^ t -i v

' "

described ab6veby: proper sh)

10. Transporter 1 Coitipan)t Nanw"

12. Discrepancy Indicatkjn Spaca

iy,,a Qeneric

flte

ited/Typed Name and Title Qa»

WHITfe-DIspqwilSitB CANARY - Qenarator- • PINK - Transporter(To be malted by Disposal Stt»> -


/ 37WASTE SHIPMENT RECORD ' ASBESTOS MANIFEST,See P*.«r»« to mwiucftom)

i-*.; tNwnber NESH4.= sarfwj

'ES

//SO NumDer

NO 773248

«* ***** ate use onty

East

vB Generator Name. Contact Name. Uairg i-C GenaracTs Ptxxw Number

10 Woik SB* AddfM*

V •" -

i-E. 24 Hou- Emergency ResponseTelephone Number

2 Operators Nam and CompteM kfarfng Adoress Operator's Phone Number

1 WaM Dttpocal Sl» OM^ Nviw and CorncM Ua

Memo Rtcycfng and Otapos^ Fat«y10712 Souti 124ti SltMt; FranMn, Wt S3i 32

WDS Phone Nun*er

414/529-6180

O Soulw«t DMrtct Wisconsin Department of Natural Resources2300 N. Or. Uartn LUher King Jr. Dovr |y»»autoo, W1 53212

South Central, Department of Natural Resources3911 Fish Hatcnary Road, Ftehburg, Wl 53711

/ /

AJK12. ' I I . RC

No.

/

7. Total Quantity

Cat I

Add atMomwKZ4 HOUR NOT1CC GIVB4 PRIOR TO DISPOSAL UUST B£ BUR€D

and Bomjinmen legdafcna. l hereby ar»y rm T»

:CATX>4 i lereoy deoare ?al me contents o< ihs consignmenl arefcjy and accur Jtul| desofced above by proper ship-ifcad. andtaoeted and are n al respects m proper condnon tor uanapon by highway auxmtm to appicafile international

a not contarntaiecJ «rtt hazardous. PCS. andVor any special

Prr«KtTyp«j Nvna and Tto Date

10 Transporter 1 Company Name

\AJt\--ff fCompMe lia«ng Addma

r- ,.,Tanptiune Number (induing aree code)

anc3 TiOe

CV> • )Da-e

11 Transponer 2 Cornpany Name

Har-.e anc Title

code)

' 2 Dacnoarcy fx*ca*on Space

1« 13 WuMDoposat SrMOwier or Operator"1J.5 Prime

Speoal Wane Approval a &so«<: 5. s-.jr.arj-e .- r« :ase o4 a Ge'- '>c -sc-e-sros ^cc'?vadC*nAcaccr» of 'ocwot 3< aswar j, ' i>- is .-. •M i~, -.--s -'jr 'ei'. -•:«.• it •'i.' 1 ir ".wi ' 2

<5'f5e«3 Hame ard Tee ' i4-*\a: e

i

Dare

3CXC Ger«acrTc at awr

» -J -t



.YES . _NO

WSR Number

7416901-B. Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code)

3l/ £. fytmfald Av , iV/ 33204-


Elevation

North_


1-D. WorKSite Address 1-E. 24 Hour Emergency ResponseTelephone Number

Av. , wi 44-708-. Operator's Name and Complete Mailing Address Operator's Phone Number

3. Waste Disposal Srte (WDS) Nams and Complete Mailing Address ™ £_

ion 1WDS Phone Number

414/283-8636-

Un4. Name and Address of Responsible Agency

Southeast District, Wisconsin Department of Natural Resources2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212




non-friable asbestos Call Cat II.

8. Special Handling Instructions and Additional Information24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.


TomSignature Date


(J3MComplete Mailing Address

Driver Signal



/Date




Driver Signature


Date




1 I l>:imiu

Signature

^.nrrvvn rDat

DCE-230-97-OR

WHITE • Disposal Snte CANARY - Generator PINK - Transporter(To be mailed by Disposal Site)

GOLD - Generator(To be taken pnor to disposal)

r

WASTE SHIPMENT RECORD/ASBESTOS MANIFESTtar toevucaom)

1 • A Spaa* Waiai P"(** Number NESHAP '.cefied

T4169t


No*

l-B Generator Hunt Contact Nan*. and Compwe Uaang Address ZJQ Cede)

in A/ M.lwuktt wi


1-D IMorfc SM MdrM*

3// »v;i-E. 24 Hour Emergency Response

Telephone Number

u/WDS Phons NMTAMT

414/253^630

I DMd. Wtaxntfn Oapwtmam of Naftnt FtoxxrcesZ300 M. Dr. UMttn Lutwr King Jr. DnVe: M«waiAM. W1 53212

Na Typ.7. Total Quantity

y<0

non ftttbto

9. KA2212. III. RQ

50CM I Cat II

Ca Spaoal HandBng toeMtaana end Ac tf

24 HOUR Nonce Give* pmon TO DISPOSAL MUST BE BUWED

«M In* contents cy -Ns consignment am My and I id above by preper ship- ""v. /

. I hereby oanry net r* •and ar* *\ al rnnmrti r proper condition tor tiargport by hig>ti«By jucmJaig to appicabto intematkxiaJM « not contamnred wr ruzardous PCS. and/or any special waste

PfM«yTtpad Nam* and TIM

ShortSigrabin) Date

10 Ti i Company Name

Caaftmi llafcig Koanm

s. 1„ a//. P-irtod Name a'VJ Tfle

cod*) y/ -

Date

1 1 Tianaponv 2 Company Nam*

Comptakt UaAng

T*daption* NuvntMr i

P*i"ied Nana anc

Dal*

12 Diacrapancy l vAcaaon Spar<

ir * 13 Watte OapoM S*» Oww or Operator"5 Soeaa) Wan* Approval a saueo r-. r ?w casa o( a G«re-c 'i&estos

rês: e>;ec-t as 12

P-ir aOTjpad Nam* and Tg*

x..nnr-r»;iDate

^€ • DWOMI &«



•* YES NO

WSR Number


. \A/I


Elevation

North East


1-D. Work Site Address 1 - E. 24 Hour Emergency ResponseTelephone Number

744 12. Operator's Name a Operator's Phone Number




4. Name and Address of Responsible AgencyS/Southeast district, Wisconsin Department of Natural Resources

N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212D South Central, Department of Natural Resources

3911 Fish Hatchery Road, Fitchbtirg, Wl 53711



MabTtasbesto* Asbestos, 9, NA2212, IH, RO

non-friable asbestos Cat I >L CatH.


V 9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are In all respects in proper condition for transport by highway according to applicable internationaland government regulations, t hereby certify that the asbestos Is not contaminated with hazardous, PCS, and/or any special waste.



Oj^STt *V»'*Complete Mailing Address



ft o t\ u) £•Date 8

<< f c




Driver Signature


Date





DCE-230-97-METRO 7/99

CANARY - Generator(To be mailed by Disposal Sits)

PINK - Trarraporter GOLD - Generator(To be taken prior to disposal)

WASTE SHIPMENT RECORD ' ASBESTOS MANIFESTSee Weverse *x •narucsons

i - A. Seecia' Want Prom« Ffcs-oer

fr' 774058• B Generate* Mame Contact Name, and Corx'ece Uawng *ocr»ss Zc ~coe

For DsocsA Site Use Only

North East

-C Generator's Phone Number

wc«» sae »aare«iir d..

•-E 24 Hou- Emergency ResponseTelephone Nurfter

Z Operators Name and CompteM Uakng Address

r•. \


3 WMM Oapcaal Sa» 0»JDS) NOT» and ComptoM Uairg AooYass

Itako RKycang and Oispoeai FaaNy10712 Soud 124tt SVWt; Ffwftfe. Wl 53132

WDS Ptions NurntMr

4147529^180

G Soutnart Dana. Wiaconaln Department of Hafcrt Resources2300 N. Dr. Uarto Luttwr Nng Jr. Dm*: Mtaaukee. WI!

South Central. Department of Natural Resourcesish Hatchery Road. Rtcnburg. WI!

6-ContamertNo.

7. Total Quantity

9 \A22-:. II.

Cat I Cat i

24 HOUR Nonce GIVEN pmoR TO DISPOSAL. MUST BE BURIED

9 GENERATOROPEnATORS CERPRCATtON . hereby declare thai tie corteots crt tf»s consignment are My and JCtujeJy descnbed above by proper ship-ping name and are danAed. perted. narked, and latieted, and are in at reepects IT. groper oondtor tor transput by Ngtnoy amoidng ID appicaKe irtemaSonaland tfcoerimien reoUMonc. I hereby certry Vat ihe jmetrn a -o( contanrtatetf wt~ "azardous 9CB. anoVor any special i

PnrteoVTyped Name and TMe

10 T 1 Company Name

oodv)

Pntted Name anc T«e

Dae

11 Traraponer 2 Company Mane

CompM* Uafcng Addres*

Sime

> nctudog area code)

• 2 Dscmepanc* Jnbcasor Soace

i • 3 A isa» Dsposal Su» Owêr y CperaaorSpecial Aaste Aocf^-a) s 4i-*c :-. i yi-^-i - -^ âM :• 3 ;*"&•: isoes:c.s i.wr.aS«r?ScaDcn ^ -»ceot 3f asc*s:c< -i'-K-is rc.êc r. ~ s -i- 'es: ei :ec' 55 -:•»: - •»- '2

'.•sec »**-« arc Tc*

CJ'' o .. >>>

•NT RECORD/ASBESTOS MANIFESTr Instructions)

Profile Number NESHAP Notified

YES

WSR Number

773688


Elevation :

North


1-D. Work Site Address* 1-E. 24 Hour Emergency ResponseTelephone Dumber


3. Waste Disposal Site (WDS) Name agd Complete Mailing Address

Metro Recycling and Disposal Facility10712South 124th Street; Franklin. Wl 53132


4. Name and Address pf Responsible AgencyD Southeast district. Wisconsin Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212 ,D South Central, Department of Natural Resources

3911 Fish Hatchery Road, Rtchburg, Wl 63711

*-*—"~ :• 6. ContainersNo. Type

7. Total Quantity, yd3

friable asbestos Aab&stos, 9, NA2212. Ifl, RQ

non-friable

B. Special Handling Instructions and Additional Information' 24'HOUR NOTICE QIVEN PRIOR TO DISPOSAL, MUST BiE 0URIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, arid are in all respects In proper condition for transport by highway according to applicable Internationaland government regulations. I herebycertify that the asbestosIs'.hot wrttamlnated *ith hazardous, PCB, and/or any special waste.

Printed/Typed Nam6 and Title Signature Date


Complete Mailing ArJdress

Telephone Number (including area coda)

Driver Signatui


Date I (




Driver Signature


Pate


I13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by signature In the .case pf a Generic Asbestos. Approval.Certification of receipt Of asbestos materials covered by this manifest except as noted In Kern 12.


DCE-230-97-METRO 7/99

WHITE - Disposal Site CANARY • Generator PINK • Transporter(To be mailed by Disposal Site)


\. '\> Ar^• • • ' " - - , •CORD /ASBESTOS MANIFEST

1-A, NESHAP hotted

YES NO

WSR Mumber

773669wiMor Name. Coral Name, and Compew Uaftng Aden** indjOng Zip Code!

For Di jort Site UwOrty

1-C Generator Phone Number

1-tX 1 F 71 \tru fn»cgent> noopomo '

Operator's Ptaw Number

WMto OwMri Sto (IVDS) NKN «rri CompM* Uaing A<ttw*

UNO RKycfng and Ohpooi FteNy10712 SouH 124* S»Mt; FranMn, Wl 53132

WDS Phnw Nunbw

414^52^6180.

rtnent of Nafcrt Resources2300 N. Or. Mart* LU*MT King Jr. Om»: kBwauka*. Wl 53212

SoOlh Cartra*. Oepartmani of Natural Resources3911 Fish Hatchery Road, fifchburg. Wl 537t1

No. Type7. TaW Quanttr

, 9. NAZ?1?, m. RO

CalH

M HOUR NOnCC QIV9IPFHOA TO DISPOSAL MUST BE BURKD

9 GENBMTCMOPEflATOAS CatmCATION; I henby

I h0Fvby owffy ffvc Vv

Hat »• oont>ntt o< Ttm consignment an July and mcu rttfy Ueautml above by proper ship-witiori tor transport t p h^w f flccovcftrtQ ID dppftcsbta vrfjwiwJi^wksJ >, ^^

f*CB,

Dvtj ^ t/TtM^Mi A^BaÂ -njf T lWrTWBw IfDVD WPV ••! IW Sigrakrt

10 Tmportv i Company "»"> * D-vix

10 (. vM^^—

Prvnec Man and Tffl*

codv)Data

Tr<r«pa*r 2 Conpanr M«m*

CompMiMMng

Ttfe^tfiofv iOr w pndbdnQ «VM ood>)

Drver Sqnatur*

PT!ied N«m» ana Tine

i11SpwW Wta» Aspw* h inu*d try agn*u* n »» CM ol» Generic AsbectosQrtfcetoi o* r»cejp> c* Mbeam r-awUb ccwerad by ttM mantosi excan as ncted m torn 12.

rYv««^«4lypvo Signalur* Date

DMTE- CAHARY SOLD

'

WASTE SHIPMENT. RECORD/ASBESTOS MANIFEST•(See Reverse for Instruction*)

T-A.Special Waste Profile Number NESHAP Notified

YES NO

WSR Number

7738701-8. Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code)


Elevation ' .

North_


1-D. Worksite Address 1-E. 24 Hour Emergency ResponseTelephone Number


3. Waste Disposal Srt» (WDS) Name and Complete Mailing Address

• Metro Recycling and Disposal Facility • • • - •10712 South 124th Street; Franklin, Wl 53132


4. Name and Address of Responsible Agency[ Southeast District, Wisconsin Department of Natural Resources





friable asbestos Asbestos, 9, NA2212, III, RO

X'non-friabje asbesffiS^ST Cat I..

cff8. Special Handling Instructions and Additional Information

24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL. MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are hi all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is hot'contaminated with hazardous, PCB, and/or any special waste.

Printed/Typed Name and Title Signature . Date

«/1 0. Transporter 1 Company Name

W A Si £ <wA jv^ C-Complete Mailing Address

< o u i -» w z -rTelephone Number (including area code)

4 14 u -

Driver Signature


Date




Driver Signature


Data


13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by. signature in the case of a Generic Asbestos, Approval.Certification of receipt of asbestos materials covered by this manifestexcept as noted in Item 12.

/ame and Title Signaturs Date

llhDCE-230-97-METRO 7/9fl

WHITE - Disposal Site CANARY - Generator(To be mailed by Disposal Site)


/ff IWASTE SHIPMENT RECORD /ASBI

• l8ae nuarai fcr ustueaom)

,

/&£~^"7 / YES

l-B- Generator Name. Coraaa Name, and CompMe Uaang A

- V - '- \ .X-A\ •-• ' . . _ • .• r : -\ i i \ V \ ,"

1 D Mo* Se» Add*w

' ' . ( *\ < f\ \~ \£Opa^« Hare and CompliailaaangAdo>es« _

:STOS MANIFEST

WSR Nur-b«f

773217ddress nodudrif Zip Code)

1 ..'— w.V v- • 1 ^V- V— '

\ )

.: iKy^ ^ \\0 J\

' . v v \v ' \ "' r M

3. Wane Otapoea) Sat (»»8» Name and Compute Uaang Address

MakoRacycfeg and DiRiosal ftdBy10712 Sou* 124ft Street (FranWn. Wl 53 1 32

4 Name art Ad*aaiot RMponaU. Agency

2300 N. Or. Uarfn Luffwr King Jr. Orfw; UftvaUi

S-OeeovaoMolUatoriato *5k ' f i •" ; ' ~ >: V1;?* W *> *• . 1 . *&?*"

feWbtcaebealw

T^^^rr?^//^^ 5

EBA Wl 53212 3911 R

k*4*tf .-• ^^^^*-Âsbectos, 9 KA2212. III. RO

Call Cat II


Nor* East

1-C. Generators Phone Number

- .- w'.-, -LL.MC

1-E. 24 Hen* Emergency ResponseTelephone Number


414/529-6180

.entraJ, Oepartnwnl of Natural Resources<A H-**MMW [bewl RrMv vn Wl 1371 1

6-ContNo.

/

•ners 7. Total QuantityType yd3

% -cXT24 HOUR NQfndtf dfVBI PfVOIt TO DCSPOSAi. UU6T BE BURIEO.

9 GBgRATQROPerUTORS CEITDFlCtATTOH: • hereby dxJare tfm t*> oomprs ot ma coraignmerf are Ujy ardm-umuJi deacrteJ above by proper ship- \_,/pjap riaae and am cta»»«>d. pectadl mertod. and tttHid, and are «i a* r»tpaca m proper oond*en tot tr»ôi1 by K^« i) «jujii*ig to appicatite intefnalionaland pownnani faojj oro. I hereby cwttfy thM the asbeslDS s not cortvtwdod

PtMeaYlyped Nan* and T«e

10 T< Company Name

A. /. /^-^ *>v

(•ndbdbiQ «VM oodi)

V/2. and Tale

Data

r/''11 Tranepmr 2 Company Name

ConpMi Ua*ng Mdnee

Nunber (indbdrig area code)

Over

Prr-ed Name and Title

Oat»

Oiaoepancy kxicaton Space

i Owter or OperatorSpeoal WaM Approval « asuta by s nanre n 9* case o< a Gerenc Asbestos Ajjprovat.Certfcakon of receipt of asbestos -Jtenafc cowed Cy 9*s Tan>»s! e.capt as noted in torn 12.

5 PnresaVTyped Name and T«e&9na'U6

Data

• CMpool Ski CAKAKY -INK - ""»nsx««pr QOLD-(iTo M B**n prar s> dopoaq



X YES NO

WSR Number

773224


Elevation

North


- C? -. / '1-C. Generator's Phone Number

I; v

1 - D: Work Site Addres> 1-E. 24 Hour Emergency ResponseTelephone Number

's Name and Complete Mailing Address Operator's Phone Number

*- ' I - ' L V i > > > ! '3. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal FacilityJ07t2 &>uth 124th Street; Franklin, Wl 53132

WDS Phone Number414r529-et80

4. Name and Address of Responsible Agencyd, Southeast Di trfct, Wisconsin Department of Natural Resources

2300 N. Or. Martin Luther King Jr. Drive; Milwaukee. Wl 53212 'D South Central, Department of Natural Resources

3911 Fish Hatchery Road, Frtchburg, Wl 53711

5. Description of Materials'',>r?yji'îl'.^-.''f^ '^,tf, -ft ' : •.%pf«^!fr i\^-?y^jtiAy»».''''' y'P'.'^ -t'. • - - ' - . •* ' , ' ' t *'


7. Total Quantityyd3 .

jiV.'W frjabje asbestos Asbestos, 9, NA2212, til, RQ

Cat! X Oat II.

0. Special Handling Instructions and Additional Information• • : 34 HOUR NOTICE GiVBJPRlOPr JO DISPOSAL, MUST BE BURIED.

9, GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by 'proper ship-ping name and are classified, packed , marked, and labeled, and are in, all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby" certify that the asbestos isnmcontamfnmed with azardousjPCB, and/or any special waste. • ' ' -

Priritod/Tybedt Name-arid Title -

MSignature.1 Date




Driver Signature!'


Date




Driver Signature



'Tf13. Waste Disposal Site Owner or Operator : .> .

Special Waste Approval is issued by signature in the case of $ Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.



DCE-230-97-METRO 7/99

CANARY - Generator(To be mailed by Disposal Stte)

PINK - Transporter GOLD • Generator(To be taken prior to disposal)

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See Revne

1-A.S Number NESHAP So«*ed

* YES 773226.noudrvg Z* Cooe.

For Deposaf Site Use Only

East

l-C. Generator's Phone Nvnber

i-D Work S»» Addrees

3"

1-E 24 Hou Emergency ResponseTetoptarw Nuntwr

2 Opennrs Nvna jnd Compua Uaing Address Opentofs Phone Number

1 WM» OMpOMl Sto (VKOS) Mvn* «nd Comprtw U ng Adorass

UMO Racycing and Oaport Fac«y10712 Sou* I24ti S«*; FranMn. Wl S3132

WDS Phone Ntfnbef

414/529-6180

4 NameandAddraaiaiD SoutMeat DMrid. Wi

Agmyin Departn at Nafc*aJ Resources

2300 M Dr. Uartn Lutw King Jr Drive Mwaukae. Wl 53212~ South Central. Department of Natural Resources

3911 Rsh Hatchery Road. Rchburg. Wl 53711

6 CortanersNa Type

7. Total Quantityyds

. 3. VA221J III. RQ

-5a7r£7C* I

8. Spec* Handing Mructo24 HOUR NOTICE GIV»I PRIOR TO DISPOSAL MUST BE BURIED

a GENERATOROPEHATORS CERTIFICATION i hereby dedere that ffw comens at ttw consqnmer* are luly and auuaalBly doscrtoed above by proper snip- ^png neme and are otoaetted. pedod. markad. and tabeied. and are m al r«specs «- proper condition tor aansport by liighauy accantm to JTr â^ rtemat)Ofiar*[

. I nentty oenfy irtai »w iiit«i>» a not contarvxad «ttn i-.azaroous PCB. and>ior any special •ast*.

PrvwATyped Name and TMe

ffl.rt10 Ti

Compt

1 Company Name SignaturB

P-rac Name arxl Tfle

code)Date

11

Cont**» IWhng Addrws

!> *f Sigr.atjre

- -lea Nar>e a-xJ Tffle

Number fmdUJng area cod*)Date

12

ISpeoel Wacki Appnjvai a ssuee ^ s raare r r« case aCe>lfcJ*on of rec»(X o< asbesas -

Asoes-ose«:«cl as -oted r tern 12

5 Pnr«eaT>ped Name and T«e ,

ii

Sgraxre Date

3CXD - G«n«raDrDCE :

SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse for Instructions)


YES NO

WSR Number

773240


Elevation , . •

North

-B. r Nameôntact Name, and Complete Mailing Address (including Zip Code)

jl1-C. Generator's Phone Number


f. bvutrvWi^1-E. 24 Hour Emergency Response''

Telephone Number

2. Operator's NarneAnrf&inJpfiteMailing Address/ . MrOriL>

,/./. - . , ; = • • / / - /Operator's Phone Number


Metro Recycling and Disposal Facility10712 South 124th Street; ,f rapk|n. Wl 53132


4. Name and Address of RwpprwiR^ Agency: PI Southeast DJsJrj&A|Visi?on$ii Department of Natural Resources

2300 N. Or. Martjn Luther King Jr. Drive; Milwaukee, Wl 53212D South Central, Department of Natural Resources


5. Description of Materials 6. ContainersNo. , Type

7. Total Quantityyd3 "

. IriaWe'asbeptos. ASbestos. 9, NA2212, III, RQ

pat I - Cat II

8. Special Handling Instruction* and Additional Information'' ••'•' • 24 HO«|R'N«>T)CI GIVEN PfllOHTd DISPOSAL. MUST BE. BURIED:

9. GENERATOfVOPERATOR'S CERTIFICATION: I hereby declare that the contents oTthls ransignment are fully and accurately described above by proper ship-ping name and aw classified, packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicable Internationalarid govemmert regulator hereby ,^>, ^ • . ' • . :

Printed/Typed Name arid Title

T '6ate

10. T Company Name, ' Driver Signature


/el * "7' Printed Name and Title, ,





Driver Signature


Date


13. Waste Disposal Site.Owner or Operator •Special Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.



DCE-230-97-METRO 7/99

CANARY • Generator PINK - Transporter(To be mailed by Disposal Site)


/-—-WASTE SHIPMENT RECORD/ASBESTOS MANIFEST

(See n»iem tar tortruaom)

- A.SpwM WWW P>o«( Nurtw N6SKAPSoe6ed

YES NO

WSR Numb*

773241i-B.Gw««)rNMKartWNv«.»KlComow«kMÂd(trMs:(xiu(»oCZ«Codei

^ '


Bevafion .

1-c. Generator's Phone Number

t D Work Sto AdfrMt 1-E- 24 Hot* Emergency ResponseTelephone Nuntter

Lli

< Opentofs Phon» Nwnber

Otapam SH» (WOS) ftartw and CompMto Uring Add

UNO RKycfng and Otapool Fac*ty10712 Sou» 124ti SBMt; Frantdin. W1 S31 32

414^29^180

D riP I at Natural I2300 M. Or. Uarfci Lurhnr Wng Jr. Drive; M»tm*ee, Wl 53212

U Souft Contra!, Department of Natural Resources3911 Rsh Hafchery Road, FacMurg, Wl 53711

5 Ower*fcr <* 6-Cort»« 7. Tort CXiantty

9. NA2212. HI RO

CalU

8. S|Mcitf t ntfny fcvtncflonii3« HOUR «rnOeor*B(PftO«TC DISPOSAL MUST BE BUFBED

ft OBCRATOaOPERATORS CaTT]FX>TK>* Ionn HTMM and arv claHMirjdL pBdcedL marked* and

I Hflreojf cervy vvi ffie

!>er«br dedere tfva tie contents o« t»s consignmen are Uy and iand are in al rwpects n proper condftor lor trarapori by Ngfway

PCB. anevorarift

crind above by proper ship- •ing ID appfcafafe rtemafcnal

Mm and T«»

"*5?0. Ti iCompanrName

7 /' <

Tll riJI HV^ lttrJl*j4 lW /*ni-a r<jnri fg lk Mvtet

Pnrr»a Name ano Trte

f fDae

11 Transporter 2 Corapery Name Signature

Pn~ed stame ano Tide

code)Daw

12.1

13 W«M DopoMt Se» Owner or OperatorSpeae) Wane Approval a cssued s> sgnabxe /i He case ol a Generic XsOestos fporoval.Cenacjrjon o( receipt ol asbestcs -jftâts cc%«r«d Or ttw r-ar-<esi et:w as nared in item 12

PrrttevTypad Nam* and Tic* Sgnafore Dale

DCS-iJCHT-METRO *

QOLOTo M attn poor n daBcsa1-

'Ifur

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See Reverse lor Instructions}


YES . NO

WSR Number

773239


Elevation .

Norths

1-B. Generator Namej ontact Name, and Complete Mailing Address (including Zip Code)

f. '&<?rrM ^ .Ul\\\J t—V

1-C. Generator's Phorte Number


2. Open and Complete Mailing Address

9Operator's Phone Number

J - •

UVU- ta3. Waste Disposal Site (WDS) Name and Complete Mailing Address

: êtro Recycling and Disposal Facility10712 South 124th Street; Franklin, Wl 53132


4. Narrw and Address of ReppgnsMeAgBncyD SoQtl*^d(str(ct/Wi$( ii»DiBp*rtmantrt Resource?

23QON, Dr, Martin Luther King Jr. Driva; Milwaukee, Wl 53212D South Central, Department of Natural Resources

3911 Fish Hatchery Road, Fttchburg, Wl 53711

beecripflp»i pi Materials- 6. Containers/ 7. Total Quantity

!C-i,»i.'-' ; friable,.asbestos.; : •'

Asbestos, 9, NA221J; III, RQ

Cat!

8. Special Handling Instructfon* and AddWonaj Information'? : : ::-'24r^ftNOTICl<ÊNP&^^

9. GENERATOR^JPERATOR'S CERTIFICATION: I hereby declare that tne coriferrts of this conislgnmenrarii fuiry and accurately (fescrloed above by proper shlp-plng name and are classified, packed, marked, and labeled, and are in all respects In proper coruJHion for transbbrt by highway according to applicable (frtemationalandg&VeiWefrtrûlaWns.trfer&vcer^ ' ; - ? / < :

Printed/Typed Name and Trtte

7Date

fit-10. Transporter 1 Company Name

lM^Complete Mailing Address

Telephone Number (Ihdudfng 3rPa code)

Printed Name andT__., -

>:*J«^' PfUifc-



Telephone. Number (including area code)

Driver Signature


Date


13. Waste Disposal Site Owner or Operator :" \ ,Special Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted hi Item 12.'



DCE-230-97-METRO 7/99

CANARY - Generator PINK - Transporter(To be mailed fay Disposal Site)


JfcASTE SHIPMENT RECORD/ASBESTOS MANIFEST

NESHAP Nc*Md

YES NO

»Sn Numoar

772460

For Uapoaal Site Lisa Orty

Nati Eaal

t-a MMk Ad**M OndkJdng 3p Cod*) 1-C. Ganafatort Phona Hunter

TatapftonaNuratMr

Ofwmkx^ Phon» Nunter

414 B71 QQ7O

OK*IM| RU0B ROF • W1» M9J66 Boundary Ro«t htonomonM Fafc, Wl 53051• .: j .v • " '.; ' •;• . i orU*M ROF • 10712 Ffw*tv Wl 53132

WOS ftvrm Nunnter

262-253^620414 2 6180

fcji.rkad.rx) an in af (aspects IT prefer cooa ton lor tranapeiB Bj li||i»«|it fid conOirt* -&i BC *'ftr " uin^CHJt. ^"Co, I

•IMW* by prop*f at >-Q to appfcabb Waniaflooal

. Slitr-f-ia Trarwportw i Corapwy Mmt D-vw

/,/'Pnrrtad >

CXver Signature

CoepMt Utfng

and !»•

MjrtHr (Incfludhf aMtt oodb)

itv sgrtctm in ** COM rt a QarMnc Ajboitoa Approval.

cowwvdby MmanlMI ai pt as noted in Ham 12.

Nan* and Tito Signatrs Dale

DC€-230-»7-CR »•» 7093OU)(Tot)»

PMENI|»ECORD/ASBESTOS MANIFESTfor Instructions)

A.SpeciajVgBte Profile ..Number NESHAP Notified, . ' • • . v . . - f

* YES

WSR Number


Hilwaukaa Solvay Coka * Caa311 laat GraatiflaU Avamia} Milvaukaa, HI 53204


Bana fiayar414-645*0*35

1* D. Work Site Address ;

MMtt a* abova


414-645-0*352. Operator's Name and Complete Mailing Address

CoKplata Dacon* Inc.4*90 laat lactma1 fttraat, Dale 3j Banicla, CA 94310


707-747-4M03. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal Facility10712 South 124th Street; Franklin, WI 53132


4. Name and Address of Responsible Agency( Southeast District, Wisconsin Department of Natural Resources

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, WI 53212D South Central/Department of Natural Resources

391 1 Fish Hatchery Road, Fitchburg, WI 5371 1



friable asbestos Asbestos, 9, NA2212, III, HQ

non-friable asbestos Cat I Cat II

Truck $08. Special Handling Instructions and Additional Information

24HOIJR'NOtieE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

w 9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping naw and are classified, packed, marked, and labeled, and are In all respects in proper condition for transport by highway according to applicable Internationaland government regulations. I hereby certify that the asbestos Is not contaminated with hazardous, PCS, and/or any special waste. •

Printed/typed Name and Title Signature

77Date

*10. Transporter 1 Company Name

DM Kllwauk««Complete Mailing Address

V124 1*945 Boundary *o*4ttenowm** fall,, WI 53051

Telephone Number (including area code)262*251-4000

Driver Signature

/Driva*



telephone Number (including area code)

Driver Signature


Date

i'2. Discrepancy Indication Space

13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is Issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except? as nota^ in Item 12.

Printed/Typed Name and Title/0«t« Att*nd*n

Signature Date

WHITE - Diapoial Site

DCE-230-97-METRO 7/99

CANARY • Generator(To be mailed by Disced Site)

PINK • Transporter GOLD • Generator(To be taken prior to disposal)

^cfe SHIPMENT RECORD/ASBESTOS MANIFEST

1-AJ

1AJH0133

NESHAP T"1YES

WSP Number

NO 7738521-1 Generator Nam*. Comet Nam*, ml Complete Ua*ng Adores* ndudhg Zip Code)

HUfnuHr S«l**7 Cok« 4 CM311 IMC Cr««nfi«14 Av*ww| Hllw«uk««, VI 33204

For Disposal Sfto Use Orty

East


414-445-0435

1-0 i-E. 24 Hour Emergency Response

414-445-0435

2 OparfloTs Najne Mf C

!»•4494 IMC StrMt. felt 3| Wmixla, CA 94310

OperMort Phone Number

707-747-4100UaAnQ Addrwa

Utko Rccydng and Oepool FadMy10712 Souti I24«t SkBM; FranUn. Wl 53132

WDS Pfion* Nwnb6f

414/529^180

sin Oepanmem ol Mafcrt Ftesourcw2300 N. Or. Uartn Lutfw K«g >. Onw: MKraufcoa. Wl 53212

South Central. Department of Natural Resources3911 fish Hatchery Road, RtettwrB. Wl 53711

S DeeofetanciNO. Type.

7. ToW Quantityyd3

Can

Tnck

24 HOUR NOTICE OWEN PRIOR TO WSPO6W-, MUST BE BOWED

• GENERATOHiOPERATORS CCRTFKATION

and oo^ rnrne'V reQâtone^ I hereby oertly tfiat Vv

by declare M 9ie cements o» ifw consignment are Uy and aonid are ri al n»pea» m proper condition tar transport by Nqh>

laMy deserted above by proper ship- /•yaooordngtoappfcable ^"^

Pitted/Typed Name and Tete Sgnature

10 TfmpQrtBf i ConpvWy Nvnv

m Milt

«U4 Btf4S

Signature

2*2-251-4000

r«ll«, VI 53031

•ecod^

nd/*«

/DriverDaM '-

11 Tranapomr 2 Company Name

CompteM) Uaam Addreee

S^nature

P-i-lec Name a-x) Title

oodv)

12 Indcatori Space

13 Oajpocal SM Ooner or OperatorSpeoal Watte Approval * oeued oy sgnaue n tie aa» ol a Genera Asbestos Approval.

Ol recall of nKmrt Tattrak conerea by 9ns manias; eicapt as -vxsO m Ram 12

PmaoyTyped Name and r«e Sgnatire Oak)

KKMTTE GOLDo« Doooui SMI

SHIPMENT RECORD/ASBESTOS MANIFEST(See Reverse,for Instructions) '• ' • < • .

1 - A. Prlfc Number NESHAP Notified

YES NO

WSR Number


311 liiit Gr«*nfl«U AY*IW«| lUlvaufca*. ttt 53204


H*n» G*j«r • •''414-445-0635

1-D. Work Site Addres*

«

1-E.24 Hour Emergency ResponseTelephone Number ,. ' -

414-443-0435

Z. Operator's Name and Complete Mailing Address

CoapUU DtttO* Int.4490 &MC I««oad Strut, U*iC B«ai«i«, CA 94510


707*747-4*003. Waste Disposal Site (WDS) Name and Complete Mailing Address

>

Metro Recycling and Disposal Facility10712 South 124th Street; FranWin, Wt 53132


4. Name and Address of Responsible AgencyO*Southeast District, Wisconsin Department of Natural Resources'

2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee. Wl 53212

5. Description of Materials

O South Central, Department'of Natural Resources3911 Rsh Hatchery Road. Fitchburs(, \$ 53711


Asbestos. 9. NA2212, III, FK1

non-friable asbestos Cat). Cat II.Tnwk

8. Special Handling Instructions and Additional Information' 24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

:>iwi li'-i".*'.;,'9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately descrifttf above by proper ship-ping name, and are .classified, packed, marked, and labeled, and are In att respects In proper condition for.transport by highway according to apptifable Internationaland government regufafiorts. I hereby certify thai the asbestos is not contamirwted with hazardajs, PCB, and/or any special waste. '" •' =' ''\ ~

Printedn-yped Name and Title


WM KttiNrak**Complete Mailing Address

V124 M945 Boundary loud. VI 53051

Telephone Number (Including area code)242-351-4000

Driver Signature

Printed NaWe and Title,/Driver

DateV

1.1. Transporter 2 Company Name



Driver Signature

Printed Name sind Title

Pate


t3. Waste Disposal Site Owner or Operator ' :Special Waste Approval is Issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.

Printed/Typed Name and Title/Cat* Att«nd«xt

Signature Date'

WHITE - Disposal Sit*

DCE-230-97-METRO 7/99

CANARY - Generator(To to mailed by Disposal Site)

PINK • Transporter GOLD • Generator(To be taken prior to disposal)

rr j *? -<-- ' 7iÔ>i '>/-• (_WASTE SHIPMENT RECORD /ASBESTOS MANIFEST

f (See Renarse tor Inekuciona)

1 YES NO 772454

For Ospoeal S«s Use Only

North East

i- B Generator Name. Contact Name, and Complete Ua*ng Address fndurjng Zio Code) 1-C-Generatar's Phone Number

.-.:'. ... ^ • _ .-,< -x*c <v v^

'~DT'~^^r:>-1-E. 24 Hour Emergency Response

Telephone Number

414^871-90JO x-jr—

i Operator's Name and Cumplati llalnj Address y

Team, tec. '

3 waste Oepoael Ssa (WOS) Name andrt«. *.«.•< o>>««a one . utiioj ijcnc

* or| Metro ROF« 10712 SoUh 124* Street Frar**n.W1 531 32i I MIM uul • hhâ rf f^^^Ml 1 1 A

2300 N- Or. Martm Lu*wr King Jr

5. OeMcnpton of MtteVVtt »?;i£ '

trwteaatMetoe

,nr *"?-o' /;;a SMcari Handana kMrucSora and Add

Drive Mihvautee. Wl 5321

&*' •• -V .H'V f

Asb

Cat

"*."••/ 4TWTt-907e^

* " * - ' . <^ "™r " N "* . »

xiee Faite Wl 53051 262-253-8620414-529-6180

as2

% . * l i • , s • .. - . . • ' 6. Cominers^^tt ' ' " V ••• v v::» '. ""•Ji.'fHJ Mo. Type

sstos. 9. SA2212. III. RQ

I Cat H "»'

7. Total Quantity

.. —

24 HOUR NOTICE GrVB4 PRIOR TO DISPOSAL. MUST BE BURIED

9 GENERATORiOPERATORS CERTIFICATION ' »w«t>y oeokn ttw «M camwts of 9v oxttjymam m Uy and »u.uam» deecifced above by proper ship- \png name and are ae*e*ad. peekad, marked, and tatMtaa and •/» n «• mpecit r proper condoon tor traraport by Njfrnay auxmiiig to appfcaMe international

l hereby certty i • nol oortamnalecJ vrfr hazardous PCS. anoVor any

PnmadrTyped Name and TMeBel K Cook. President

Signature Data

10 TT i Company Name

4901 Norn 31« Street

) Mtrttwr fnAKflno «WM cods)4.14-871403)

Name and TiBeBill K Cook, PreeirJer*

Date

11 TiWM

2 Company Name >-v»r

W124 N8925 Boundary RoadUenomonee Fate. Wl 53061 and Tree

(toidbdfeig avee code)

262-251-4000 Dale

12 Oaoreparcy

1

i

13 WastsOepoeal Set Owier or Operator

Cenacaiui d fece^H ot atneara -naMnat» cov«rc<:

PnreaaTjped Name and Tla*

i case o» a Senate Asbestos Approval.1 Oy !Ni rianf!er except is ->olea r Mem 1 i v

Signature Date

DCH ;so-»r<» T.GOU) •(To 0* n**i prior o dapoaO

WASTE SHIPMENT RECORD/ASBESTOS MANIFEST(Sea nenaraa tor tnatrudtona)

1-A.SpacW WMto Pro* Number

RASB10643

WSA Number

774064

For DbpoeaJ See U»e Only

Elevation

Eaat

1-fl. Generator Name, Contact Name, and OompM* UMng Address (Indudng Zip Coda)

Milwaukee Solvay Coke & Gas311 East Greenfield Avenue; Milwaukee, WI 53204

1-C. Generator1* Phone Number


1-D.WorttS*aAddreas

311 East Greenfield AvenueMilwaukee, WI 53204

1-E. 24 Hour Emergency ReaponaaTelephone Number

414-645-0635£Opei«tor*hlaflie art Cample* MatogAddrMe

Complete Decon, Inc.4690 East Second Street, Unit 3; Benicia, CA 94510

Operator's Phono Numbflf

707-747-48003. Waste Dtapoaa) Sto (WOS) Nam wd Compta

Metre FtecycOng and Dtepoaal FadBty10712 South 124ft Street; FranMn, WI 53132

414/529^180

4. Naitw and Addraw of Rnponrtito AQtncy

2300 N. Or. Martin Luther King Jr. Or)nt of Natural Resources; MHwaufcM, WI 53212

D South Central, Department of Natural Resources3911 Fteh Hatchery Road. Rtchburg, WI 53711

5. Dwcripton of Materialsgasket?* floor covering

B.ConWnemNo. Type

7. Tool Quantityyd3

Aebeetoe. 8, NA2212. III. IKI

non frisble CMI Cat III.

8. Spedel Handeng kwkucttom end Addeo24 HOUR NOTICE GIVEN PWOR TO DISPOSAL, MUST BE BURIED.

9.OBtfRATOaOPERATOR-SCEHTMCATION: ItanbydedanlMlheconlmliof*t*iplno nainaflrid ve deHMed« padced, merited! end labeled, and are In al lejpacbi bifand uoxermneU rBgiaiaua). r heraoy carMy tat Via la not contan*«*ed with hazntloua, PCS, andtor any apodal waste.

nt are My and accurately described above by proper «hip-for imiopuil by raonvMy socoraViQ to sppfcflbte iniBnwtlonfll

Telephone Number (Indudhig ana code)

CHacrapancy Indteatton Space

13. Waste Diapoaal Saa Owner or OperatorSpedaJ Watte AppravaJ ia iawed by slgnatum In the caw of a Generic Aabegtoe ApprovalCertification of receipt of asbestos matanato covered by thfa inanMeat except as noted to Itam1&

Printed/Typed Name and Tttla

/Gate Attendant

WHITE - DtapOMl SH* CANARY- P1WC GOLD-rTM h* Mran n«4Mr <<

SMPMENT RECORD/ASBESTOS MANIFEST

IASB10643 YES MO 774065(Mulflng ap Cote)

Milwaukee Solvay Coke ft Gaa311 East Greenfield Avenue; Milwaukee, VI 53204

For

1-C. Ommort Pfcciw NumtMr


i-o.311 East Greenfield AvenueMilwaukee, VI 53204 414-645-O635

Complete Decon, Inc.4690 Ea«C Second Street, Unit 3; Benlcia, CA 94510

Qôaork Ptam NuitMr

707-747-4800

414 29-618010712 Sou* 124ft SvMC FrarMn. VM 53132

2300 N. Or. I S3M2O Souti Cental. Department ot Natural Heaources

3»11 FWi HeWwy Roed. RfcMwB. Wl 53711

roofing, gaakets, floor covering9. NA221Z •, RQ

M HOUR NOnCE <9VB4 PWOfl TO OOPOSM. MUST BE BUHB)

PrW«) Nvm «tf Tito

/Gate Attendant

*»>-•»

ÂSTE SHIPMENT-RECORD/ASBESTOS MANIFEST(See Reverse for Instruction*)

1-A.Speclal Waste Profile Number

UI110I43NESHAP Notified

• * YES . NO

WSR Number

7739521 - B. Generator Name, Contact Name, and Complete Mailing Address (Including Zip Code)

Ktlw«uk«« folTa/ Cok» 4 C4«311 i*«t OrMttficU A»«a«M| Milv»ttk««, tft 33204

1-C. Generator's phone Number

Han* (*•?•*414-643-0633

0. Work She Address :

CM M abov*


414-643-0433


Covytita OtcfHt IM» ' ' '4m *Mt S«e<m4 ltr««t. Bait 3| HolcU, CA 94310


707-747-4$003. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal Facility . ,10712 South 124th Street; Franklin, Wl 53132 . *

WDS Phone Number

414/529-6180

4. Name and Address of Responsible Agency$ Southeast District, Wisconsin Department of Natural Resources





• friable asbestos . ' , . . Asbestos, 9, NA2212, III, RQ

npcHriabfe asbestos , Call. Cat II.

T8, Special Handling Instructions and Additional Information

24 HOUR NOTICE GIVEN PRIOR T0 DISPOSAL, MUST BE BURIED,

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping; narrje and are classified, packed, marked, and labeled, and are In all respect? In proper condition for transport by highway according to applicable international

" government regulations. \ hereby certify that the asbestos Is not contaminated with hazaidous, PCB, and/of any special waste. •and



VM Milim«lM«Complete Mailing Address

¥12433031

Telephone Number (including area code)262-231-4000

Driver Signature

and Titlei

Dafe"




Driver Signature


Date


13. Waste Disposal Site Owner or Operator' ' •Special Waste Approval I; Issued by signature in the case of a Generic Asbestos Approval.

• Certification of receipt of asbestos materials covered by this manifest except as noted In Kern 12.

Printed/Typed Name and Title/Cat*

Signature Date


DCE-230-97-METHO 7/99

CANARY - Generator(To oe mailed by Disposal Site)


RECORD 'ASBESTOS^MANIFEST

1AJ110443NCSHAP

»-

11 YES NO 773953i-aG«MntorNMn*.C«MKtNMn*. and CompM*U4«ng Address nducfc^ Zip Code)

MUvrakM f«iT»y Celu ft C«»311 I«tft GTMafl«14 AT«no*» MUMuk««( VX 53204

l-C. GtrwnWs Phooa Nurrber

Baa* 6*y«r

1-0 WokSfct i-E- 24 How Emvgancy Response

414-445-OUSI and ConpMi Uaeng Addrao*

eoa IM.4490 iMt fi«o«4 ftrat. Obit 3| tonlcU. CA 94310

Oparalar's Ptuna Nurtwr

707-747-4100(WOS) Nw» and GtynpMi Ua*ng Add

Men "r f'T) ml10712 Soufi 124* Street Fnrtfln, Wl 531 32

WDS Pforv Ntfnbar

414529^180

atOMfctWi enOepi tof Nefexaj Resources

2300 N. Dr. Men* Lulher Mr? Jr. Dnve; Ma\»auke>. Wl 53212So* Central, Department of Natural Resource!3911 RshHathery Road, Ftetiourg. Wl 53711

6.1Mo. Typ«

7. Total Quantity

1.9. N^22'2. 111. RQ

Cai Can

24 HOUR MCmCt GIVEN PRIOR TO DISPOSAL. MUST BE BURIED

9 GB*BUTOaOPERATORS CERTFICAT1ON !pinQ naw and am cttaeBatf. pedvd^ martad. andand 1f**mmit najaaJoni. I hanby carHy »al f

•wtby dactm ihat ma co-torts cX ttus consgranant ant Uy and a<latialad. and am r al raapaos ^ proox condton tor tianapuit by highiM> .

•tydaacrtndi by proper ship- >^y

» not oortaminrad w<tD tazardous °CB anoVor any apaciatrdng to appfcatato intemational

Sqnann

Conpvny Nvne

VU4 M945* Fall*. VI 33051

Totantan* ikvi Mf 6nchjdra212-251-4000

cod>)

ll.Ti 2 Cor. rNama Signarura

and TJB«

Date

Own*

Sa» Oanar or OparatorSpaoal Want Approval • -ssuea Dy sgnatm n 0>a casa ol a Gar*nc Asbestos *op-ov».CarMkaaon ol racafpl of MMntrn -ftrja ao*«r«d by tr*s mani vst eicept as ->o;ec in .tarn '2-

/Gat* ACC«a4«acS naiur. Date

NMTTE'o b* Tatae 3, >•»•• Sw

GOLD(To t» Uttr poor to rtBUMifl



* YES NO

WSR Number

795823


Elevation

North East

1-B. Generator Name, Contact Name, and Complete Mailing Address (including Zip Code)Golden MAIin* C*u»«vay311 U»t Greenfield Av«nu«t Milwaukee, WI 53204


414-645-0633

1 -p. Wo* Site Address

311 Ia»t Greenfield Av«nu«Milwaukee, VI 53204


414-645-0635

2. Operator's Name and Complete Mailing AddressLake State* Industrial Services311 But Gronfltld Avenue| Milwaukee, WI 53204


414-645-0635


• Metro Recycling and Disposal Facility10712 South 124th Street; franklin, WI 53132

WDS Phone Number

414/529-6180

4. Name and Address ot Responsible AgencyO^Southeast District, Wisconsin Department of Natural Resources'

2300N.pr. Martin Luthtr King Jr. Drive; Milwaukee, WI 63212D South Central, Department of Natural Resources

3911 Fish Hatchery Road, Rtchburg, WI 537,11

9. Description of Materials 6. ContainersNo. :Type

WabW asbestos Asbestos, 9, NA2212, III, RQ


Call. Cat II

. Special Handling Instructions and Additional Information' 24 HOUR NOTICE GIVEN PRIOR TO DISPOSAL, MUST BE BURIED.

9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are. classified, packed, marked, and labeled, and are In all respects In proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos Is not contaminated with hazardous, PCB, and/or any special waste.

Printed/Typed Name and Title f I ±,

mpl t/t/l/f

Signature.

d

Date


Starline TruckingComplete Mailing Address

PO Box 410M«w Berlin. WI 53151


262-786-8280

Driver Si

Prinjed Name and Title

Date •r /•-•//11. Transporter 2 Company Name



Driver Signature

Printed Name arid Title

Date


I13. Waste Disposal Site Owner or OperatorSpecial Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.


Attend tatSignature Date


DCE-230-97-METRO 7/99




1-A.SC

I c CfclNESHA? vocftae

Y=S NO 774047


Bevabon

Norn East

i-B ft«~^. Nairn. Contact Nam*, and Conptew Unrc Aaomss :«xxx»ng Sc Cooe

C f/F ./', f, )<


ID

u1 -E. 24 Hour Emergency Response

Telephone Nutter,2. Operator* N«m* v^ Ua*ig

- , - ' / , . . i , , 'Operator's Phone Number

i Wa«e Otapoeri S»i (WDS) Name and Comptew Uaring Address

Me«n> Recyctng and Oopool Fao«y10712 Sou* 124ti Strwt Frarttn. Wl 53132

WOS Phone Number

414V529-6180

l OMiet WlKflraia Deparlmert at Mat** Resources2300 M Or. U**i Lutw King Jr Drive: Mfeaufce*. Wl 53212

Somh Central. Departmert of Natural Resources3911 Rsh Hathery Road. Fitctturg. Wl 53711

lOeeolptonoli

f\&Na


f NA22'2. ill RO

CJII Cat II

I '; 'Zc24 HOUR NOT1C€ GIVEN PflJOfl TO DtSPOSM- hAJST BE BURIED

• ' ' f

r ' i /, , 1 / / / ' . .

% , TfM0hon§ fittMr nindbiftng JPM codt)

fJ 1 1 Ttanaportar 2 Company Name

TMpncne NUTT** tiruutra VM code)

•2 Dacrfloancr Tcfcaoor Space

Signature Date

p. -.

~-

Pnrite<3 Name and T«e

Date

. .«: «ar-« a-c .«

Date

ihr Aaae Dsposa Sat Ow* or Operatoraste Aoprcval a :AS« 5- 3 j -*'.: iiC*5!;s *w:.

> -.5 -a- '&r ei :ec: as ->:•€•.•; >-

Date

- '.rf " ^-?c»:-"c--



YES NO

WSR Number

774043


Elevation

North East

1-B. Generator Name, Contact Name, and Complete Mailing Address includinq Zip Code)me, and Complete Mailing Address includinq Zip Code)

! &*?* ' ^- 1' i « /* ' ~


1-D. Work Site Address r 1-E. 24 Hour Emergency ResponseTelephone Number


,•",.'.*'•,- •••>' I'




4. Name and Address of Responsible AgencyD Southeast District, Wisconsin Department of. Natural Resources


3911 Fish Hatchery Road, Fitcnburg, Wl 53711



friable'asbestos

-


non-friable apbesto* Cat I Cat II


9. GENERATOR/OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland government regulations. I hereby certify that the asbestos is not contaminated with hazardous, PCB, and/or any special waste.

Printed/Typed Name and Titleinted/Typed Signature Date


U^"-,!r>/Complete Mailing Address

><• '?'"„• .5 ";•')*.*

I. '- i- •>' 'Telephone Number (Including area code)

/;///} ?/: / .

Driver Signature

Printed Title1

Datef..




Driver Signature


Date




WHITE - Disposal SiteDCE-230-97-METHO 7-99



WASTE SHIPMENT RECORD ASBESTOS MANIFESTSee nenne tor rstruOars

i- I Nwntoer '•SS° '..-t

774044


Bevafton

v B Generator Nam. Contact Nam* andCorrcfete Uadng Aodress >nau*ng. Zc C coe<

C,tult.i A ' - * . - . . * '.->.-,,;<..' / , . ,H t . Cy ' ;''' ' "• ' - - '

i-C Generator's Phone Number

, / . ^v , ,_' • - « ' . . - ,

i-D

\1-E 24 Hour Dmrqency Response

Telephone Number

2 Opener* Name and Co

/AM : /OperaKVs Phone Number

1 Wa*» Oapoul S»» |W06) Nvn* and CompM* Ualng Mama

ItakoftocycingandOiipcM^Factty10712 SoUh 12401 S*wt FranMn, Wl 53132

WOS Phone Number414/529-6180

^Sa**&C*^WItcort&tpaTrnei*al *****&**&*^2300 N. Or. Marfn Lutfiar King Jr Drive: Mhmutoo, Wl 53212

Sou*) Central, Department of Natural Resources3911 Fan Hatcnery Road, Fitchburg, Wl 53711

5. Oeecr*»an of; v. ,

6. Containers 7 TotaiQuantty

. 9. MA?2'J. n.

Cat 1 Cat l'' I' s '•• •> ' '

8. Sp ffjng ctont and AdMo c2« noun Nonce orvo4 PRIOR TO OSPCS*L MUST BE BURIED

9 QEHEHATOROPeRATOR-S CCRTFICATXDN I -weby oectare that !he conaenis of ttxs cons nmert are My and jLuiatart daacifceU above by proper ship-pno name and are dMeAed. packad. marked, and aoeted. and are r al respects r proper coodrtor tor Banspon by highway aooonfng to appfcabte internationaland gun nmenl regUMonc. I hereby oertfy tvt f* *»* T* a not oor*arrana~ed *r*~ hazardous PCS. anoVor any*

Mm *id Tito

"'l' J / l l , . . .

9ana«ure, Date

10 Transporter'. Company Name Sionat j-e

Pimeo Nama and T»e

TcieiJtione Ntfvber (OdudnQ mM code)Case

1 1 TranscorMr 2 Company Name

CompM* Uaftng Acttns

Tuapfarn NUitter fndulng area ax>»i

P-r-ac Nane aio ~ne

Date

•2 Dacrvparcf VtSc

I1 3 Was** Disposal Sat Owner ar OperatorSoeoM Was* Aoprovai s ssc«o :•, r* case * a

5 fîraeoTjped Name aro T«« ' >flratjfe date r~: r* •»•*- 3-0-1:

WASTE SHIPMENT RECORD /ASBESTOS MANIFEST(See Reverse lor Instructions)


, VES „WSR Number

774045


Elevation ..

North East


> i n


-' ! 4 I. Ji r. / /. '

1-0. Work Site Address 1-E. 24 Hour Emergency ResponseTelephone Number


/ n K'e c-j\f\\r ^ V i >Ht i -. ' ' ><-/;,Operator's Phone Number

t M3. Waste Disposal Site (WDS) Name and Complete Mailing Address

Metro Recycling and Disposal Facility . .1 071 2 South 1 24th Street; Franklin, Wl 531 32

WDS Phone Number

414/529-6180

4. Name and Address of Responsible AgencyXf Southeast District, Wisconsin Pepartment ot Natural Resources

' 2300 N. Dr. Martin Luther King Jr. Drive; Milwaukee, Wl 53212D South Centra), Department of Natural Resources

391 1 Fish Hatchery Road, Fitchburg, Wl 5371 1


7. Total Quantityyd3.

friable asbestos; Asbestos, 9, NA221 2, III, RO

/ non-friable asbeetos. Cat I X • CatIL

W'


9. GENERATOR/OPERATOR'S CERTIFICATION: 1 hereby declare that the contents of this consignment are fully and accurately described above by proper ship-ping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable internationaland government regulations. 1 hereby certify that the asbestos is not contaminated with hazardous, PCS, and/or any special waste.

Name and Title / Signa

v u •Date

"l<10. Transporter 1 Company Name

L>', /> , - . , , - . /• :Complete Mailing Address

' -


/ ^ ' " t>

Driver Signature^


Date




Driver Signature


Date


I

Ti13. Waste Disposal Site Owner or Operator

Special Waste Approval is issued by signature in the case of a Generic Asbestos Approval.Certification of receipt of asbestos materials covered by this manifest except as noted in Item 12.



DCE-230-97-METRO 7'99


PINK - Transporter GOLD - Generator(To be taKen prior to disposal)


APPENDIX 1-2

Coal Tar ManifestsWaste Management, Inc.

EarthTechA Tyco International Ltd. Con puny

L.\work\72534\Admin\Reports\Rpttext.doc

METROSPECIAL WASTE MANIFEST DISPOSAL TICKET

BILL TO:WM Milwaukee

GENERATORS SIGNATURE:

WASTE DESCRIPTION:

PROFILE # .

ACCEPTED BY:

DRIVERS SIGNATURE.

300416

A Waste Management Company

mt/~' TRANSPORTER:

GENERATOR:

WM Milwaukee

6olden Marina Causewflf LLC/ / /

Date

DateTRUCK NO.

WHITE t YEU.OW • GENERATOR COPY / PINK - CMSPOSAL SUE COPY / OOLO - TRANSPORTER COPY*Htn cow

TONS/YARDS

DCE-OW-WM

METRO SPECIAL WASTE MANIFEST DISPOSAL TICKET 8nn414

WM MIIWUIIK.-K IMfiVil A WMIe M«n,g,m«nt Company

vvM MilwaukeeTHANSI'OHIt-H

C-*>M»'n Mrinrtn 'CciiiiPway 1.1.COENthAiuH

OENfnATOHS SlGNATUHfc

Cool Tor

WASTF OFSCHIPTION

PROf II F #

ACCUMLOHY0*1*

DRIVERS SIGNATURE ^^.-f ,~-~ '" ' _/ Z TRUCK NO ^ JL/-- ' _____—, TONS/YARDSDilt

WMT1 » VIUOW MNMArOM CO^V ' MNK • (NtPOtAL UTI COf V / OOCO TNAMtMMTIII COf V OCI40*«M

METRO SPECIAL WKSl'E INVIINIF'ES \ tJfSf*l>SAt TICKt I

BSU.1t>:

TRANSPORTER:

GENERATOR:Golden Marina Causeway ILC

QEMERATORS SrSN'AruRE:

WASTE DESCRIPTION.

PROFILE # •

Co/Tar

ACCEPTED BY:

DRIVERS SIGNATURE:

Oat*

797881

A WMtt Mantgwiwnt Company

TONSÂRDSDate

WHITE 4 YELLOW - OCNIfcktO* COPY I PIN*. DISPOSAL SITE COP Y / GOLD • THANSPOHTEM COPY

SPECIAL WASTE MANIFEST DISPOSAL TICKET 769253


aLLTO

RANSPORTER

iENERATOR

JAjrv\Ukt

iENERATORS SIGNATURE:

/ASTE DESCRIPTION

ROFILE*

CCEPTEDBY

AVERS SIGNATURE: .TONS/YARDS

OC£-00»«4 FtoviMd M»

it: 706551 Driver: JBABCOCK«d by: AJONES.amor: 477-106O1B LAKE STATES INDUSTRIAL

311 GREENFIELD AVE EMILWAUKEE. CITY OF WI 53204

.: BERT SNEADtested by. ASAP

10627 Sotrih 27th SIFranMn. WI 53132(414) 761-2100(414) 761-3899 Fax

Date Requested: 08/05/2004Date Dispatched: 08/06/2004

414-645-0635

id Type:9 Site:

SWITCH OUTTONNAGE (METRO)

Map Code: Map Grid: OBR

Quantity P YardafARD SPECIAL WASTE OPEN TOP LOO T 30OSAL PER TON LOO T

Weight Job Special DescriptionCOAL TARMW483719

5-30S AFTER 7AM SEE CREW FOR SPOTTING INSTRUCTIONS-FRIABLE ASB10566-FRIABLE RASB 10567 FRIABLE COAL DUST RASE 10012 12-9-04X) NOT PUT ANY ORDERS IN FOR CUSTOMER WITHOUT CHECKING WITH ANTHONY

ature: Date:

Waste Management of Wisconsin, Inc.10627 S. 27th StreetFranklin, V1-800-640-5571

| DIVISION

-7257 Fax

ACCOUNT

91805.

METRO SPECIAL WASTE MANIFEST DISPOSAL TICKET

BILL TO:Milwoukce A Waste Managwnant Company

TRANSPORTER:.WM Milwaukee

GENERATOR:.

GENERATORS SIGNATURE: _k.

> WASTE DESCRIPTION:

,ofn^ A1-

Cool TorDate

PROFILE #

\CCEPTEO BY.

\VERS SIGNATURE:

Date

TRUCK I TONS/YARDSDate

WHITE 4 YELLOW - GENERATOR COPY / PINK - DISPOSAL •ITEÔPY / GOLD - TRANSPORTER COPYÔPY / OCE-00»-*»S

00

43

METRO

BILL TO

TRANSPORTER

GENERATOR

SPECIAL WASTE MANIFEST DISPOSAL TICKET

WM Milwaukee

WM Milwaukee

Golden Marina Causeway LLC

GENERATORS SIGNATURE.

WASTE DESCRIPTIONCool Tar

MW483719

ACCEPTED BY

I DRIVERS SIGNATURE

I 'TRUCK NO

797859

A Wan* Management Company

TONS^TAROS

WMTTI 4 VIUOW • OIMMTO* CO»Y / MM • (NMOtAk «TC CWT f QQLO THANWQHT1II CO»Y

Tr?

cnCMCMo

uu

oct

/METRO SPECIAL WASTE MANSFEST D5SPO3AL TICKET

/ -

"BILL TO.WM Milwaukee

-THANSPOhTER..WM Milwaukee

/"GENERATORS SIGNATURE:

WASTE DESCRIPTION:

PROFILE »

ACCEPTED BY:

-DRIVERS SIGNATURE:

CoalTtt*Z>

MW483719

77

Date

./ <_Date

TRUCK

797858


.TONSÂRDS

WHTT1 1 YELLOW - QENEIIATOn COPY / PIMK • DtSPOSAL SfTE COPY / OOLO - TRANSPOHTEM COPY

METRO

BILL TO


WM Milwaukee

TRANSPORTER

Golden Marina Causeway LLCGENERATOR

GENERATORS SIONATURfc lV-\ >

WASTE DESCRIPTION

PROFILE •

ACCEPTED BV

Coal Tar

MW4837J9

DRIVERS SIGNATURE

5 >

TRUCK NO

797857

A Wail* M«n«g«m«nt Company

WMTI • rtuow. MNHuron COM i MNN • on>OMi wn corr / O<KO TNANMONTIII co»»

TONSATAROS

OC(

I METRO SPECIAL WASTE MANIFEST DISPOSAL TICKET

BIU TO: WM Milwaukee

WM Milwaukee. . .

Golden McrirxirCausewayLLC

GENERATORS SIGNATURE:!

$ASTE DESCRIPTION: .

PROFILE #

ACCEPTED BY:

DRIVERS SIGNATURE

£oaft<

MW483719

TRUCK NO..

797853

A Waato Manag«m«nt Company

^JTONS/YARDS

WWTE • VCU.OW • OCNCMATOH COPY / MNK • DISPOSAL SITE COPY / OOID - TMANSPOItTtfl COPY OCE-OW

5=

cv/COCMOJ

uio

N

0

METPO

BILL TO

TRANSPORTER

QENEflATOR


WM Milwaukee

WM Milwaukee

6olden Morfoa Causeway LLC

OENFWATOflB SlQNATURE

WASTF

PTOFllE •

ACCEPTED 8t

£odl Tor

MW483719

DRIVERS &IONATURE

797855

D»l»

0«wTRUCK ^4O ,._. , TONS/YARDS

vtuow MNIMTO* co»» / MNK • MWOML wn co»r / o<xo

. s

OOCOCMo

oct

ft


BILL TO:WM MilWaukee

Golden LLC

GENERATORS SIGNATURE:Data

PROFILE #MW483719

'ACCEPTED BY:

DRIVERS 8l<5HATURE NO

7Q-7oc:>ir y f 0 0 4

A Watt> Management Company

TONS/YARD?: Date

. .'.: * - -. • ''••-' •WHTO • YELLOW - OENtMtTON COFT / MNR - DttPOSM. 8TTB COPY / OOLO - THANSOOHTEH COPY


BILL TOWM Milwaukee

TRANSPORTER:

GENERATOR.

WM Milwaukee


> SIGNATURE

WASTE DESCRIPTION . ....

PROFILE •

SACoal Tar

:, si jzj*D*tt

MW4Q3719

ACCEPTED BY

DRIVERS SIGNATURE

797856

A WlCte M«n«g«m«nl Company

&OSI

TONSÂROS

WHITl 4 Vf U.OW . OVMMTOII CO^T / MM • WMOMl WTI COPY / OOCO OCI

cv

/METRO

BILL TO:

-TRANSPORTER:

V*

GENERATOR >•<-

SPECIAL

WM Milwaukee

WM Milwaukee

6olden Marina Gjptneway

WASTE MANIFEST D

' Vi

'LLC j$lavl*5

GFNPHATOflS SIGNATUfle'lP-Ak|jQrM^faA/ ^ O' ' *• ; C/

H

WASTE DESCRIPTION

«*,? •

PROFILE #

Coal Tar

MW483719

Date

; ^ v /^Date

_

DateTRUCK NO

797852

A Wast* Management Company

.TCiNS/YAROS

WHITE • VEUOW • aCNEMTOfl COPY / PINK - DISPOSAL SITE COPY IOOLD • TBANSPORTEB COPY

METRO

BILL TO

TRANSPORTER:


WM Milwaukee

WM Milwaukee

GENERATOR

GENERATORS SIGNATURE

WASTE DESCRIPTION

PROFILE •

CCEPTED BY

SIGNATURE


Coal Tar

MW483719

> ST.

0«it

, ///. TRUCK NO

797851

A Watt* M>n>gwn«n( Company

. TONS/YARDS

WNfTI 4 VfUOW • OtmiUTO* COPY / MM . (MMOtAl tin C0»» / OOiO r«*N«»ONTIN CO»r

r-0

^0

V

CDCOCXIC\JCD

OC1



TRANSPORTER:WM Milwaukee

GENERATOR:.Golden Marina Causeway LLC

GENERATORa lGNATURl:"".

WASTE DESCRIPTION:

PROftLE« ;

Cool Tor

MW483719

ACCEPTED BY:

RIVERS SIGNATURE: TRUCK NO.Date

797850


3)1

WHITE » VEU.OW - OENeBATO" COPY / PINK - DISPOSAL SfTE COPY / GOLD - TRANSPORTER COPY

.TONS/YARDS

DCE-009-WM

\ •» I

3 §

•

MFTRO

BILL TO

TRANSPORTER


GENERATOR

GENERATORS SIGNATURE _

WASTE DESCRIPTION:

WM Milwaukee

WM Milwaukee

6olden Marina Causeway LLC

A W««t« M«n»g»m«nl Company

Coal Tar

MW4837I9

ACCEPTED BY

SIGNATURE „ TONS/VARDS

WMTI » VIU.OW • «MMN*TO« CO*V ' MM • *TI CO»» ' OA.O


WM Milwaukee

GENERATOR:

GENERATORS

WASTE

6dden Marina

ACCEPTED-6Y.

DRIVERS SIGNATURE:

MW483719

Daw

" Oat*TRUCK NO.

797848

A Watto M«rag«fn«nt Company

TONS/YARDS

WHITE • YELLOW - OENtRATOM COPY / *MK • DISPOSAL SITE COPY / OOLO - THANSPOHTEM COPY

SS

IiocE-oot-ams

CMCMCD

HIOu.u.o

METRO

BILL TO

TRANSPORTER

GENERATOR _


WM Milwaukee

WM Milwaukee



WASTE DESCRIPTION

PROFll f- •

ACCEPTED BY

ytOool Tor

MW483719

\DRIVERS SIGNATURE

797847

A Waal* Management Company

Dai*

.._.</ i...O/^TRUCK NODaw

WMITt 4 VILLOW OaMHATOD CO»T / MMK OM»Ot«l IfTt CO^T f OOlD TKANCVOHTIM COP»

. TONS/YARDS

OCI


WM MilwaukeeA Wtttt Management Company

WM Milwaukee

6oldenMarf


WASTE DESCRIPTION

PROFILE*

KMTE • VHJ.OW • <Mm0MTOft CO^V / MM - (NSPOMt VTt tOi»V / OOtO

J

*.

\ETRO

BILL TO

TRANSPORTER


WM Milwaukee A Witt* M«n«g»m«nt Company

WM Milwaukee

6olden MoriGENERATOR


WASTE DESCRIPTION

PHOf HE »'

uuc

Coal Tar

MW483719

o.t.

ACCtPTEO BY

SIGNATURE

WMTI i VtllOW CMNWMTOM CO»f / MM . OWOMl WTt CO»V / OOiO mANMOMTM CO»V OCI


BILL TO. WM Milwaukee

TRANSPORTER:,WM Milwaukee

GENERATOR:Golden Marina Causeway LLC

GENERATORS SIGNATURE:.

WASTE DESCRIPTION:

PROFILE #

Coal Tor

MW483719

ACCEPTED BY:

DRIVERS SIGNATURE

1 ,

TRUCK NO.Date

797844


. TONS/YARDS

WHTTC A YELLOW - GENERATOR COPY / HNK - DISPOSAL SITE COPY / GOLD • TRANSPORTER COPY OCC-OW V9S


BILL TO:

TRANSPORTER

GENERATOR

GENERATORS SIGNATURfc

WASTE DESCRIPTION

PROFILE »

ACCEPTED BY

DRIVCMi; SIGNATUHL

/ /

A Wait* Managamcnl Company

C ^VSa*S

wnm • YILLOW • MMiuTOR corr / MM • MPOML MTI COPY / OOLO • TMUMPOKTIR corr OCE 00* 04 RwlMd MM


,BILL TO:WM Milwaukee


GENERATOR-.Golden Marina Causeway ILC

.GENERATORS SIGNATURE:

WASTE DESCRIPTION.

PROFILE « '"'

ACCEPTED BY:

DRIVERS SIGNATURE:

Coal Tar

MW483719

7

797843

A Wast* M«nag«mem Company

TRUCK NO.. .TONS/YARDSDate

WHITE t YEULOW • OCNEmTOn COPY / PINK - DISPOSAL SITE COPY / GOLD • TRANSPORTER COPY OCE-OW-WM

o ,*HCD

I!

METRO

BILL ra _.

TRANSPORTER

GENERATOR


WM Milwaukee

WM Milwaukee



WASTE DESCRIPTION

PROflLE •

Coal Tar

MW483719

ACCtPTCO BY

DRIVERS SIGNATURE

797842

A Will* Management Company

On*

o«w

TWUCKNO

• rtuow . mnn* corr / MM • m»m»L vrt co*r /ooio TH«MMOHTIH COPY

TONS/YARDS

oci

ii

CDCDO

CD

£8O£EO




GENERATOR:Golden Marina Causeway LLC\

GENERATORS SIGNATURED

WASTE DESCRIPTION:

PROFILE #

ACCEPTED BY:.

DRIVERS SIGNATURE:

Coal TOP

MW483719

797841


400150Date

TRUCK NO..

Date

Dale

WHOC • YELLOW • OENEMTOK COPV / PINK . DISPOSAL 8>TE COPV / GOLD • TRANSPORTER COPY

. TONS/YARDS

00COo

o

i

»V

r METRO

BILL TO

TRANSPORTER

GENERATOR:

GENERATORS SIGW

WASTE DESCRIPTION

PROFILE •

ACCEPTED BY __

DRIVERS SIGNATURE

METRO SPECIAL WASTE MANIFEST DISPOSAL TICKET 797840

BILL TOWM Milwaukee A Wtft* M«n«g»m«nt Company

TRANSPORTERWM Milwaukee

GENERATORGolden Marino Causeway LLC


WASTE DESCRIPTION

PROFILE • _.

ACCEPTED BY

DRIVERS SIGNATURE

s, 7 .of-Cool Tar

DM. **+MW483719

D.I.

/ . . /„„ TRUCK NOOil.

TONSA-ARDS

WNIT1 4 Vt UOW . MMMTOM CO»V / MM • CO»r / OO«.0 TNANtKMTIII CO»V PCI

\ETRO SPECIAL WASTE MANIFEST DISPOSAL TICKET

WM Milwaukee

WM Milwaukee


'-PROFILE #".MW483719

ACCEPTED BY:

DRIVERS SIGNATURE:

Xi>^-Date

.1 /.Date

DateTRUCK NO

797839


WHTTE t reu-ow . oeNeRATcm COPY / MNK - onrbsAi sm COPY / GOLD • TMtopORTEfl COPY OCC-OOM/M

CDCDO

LUgto


BILL TO:

TRANSPORTER:

GENERATOR:


WASTE DESCRIPTION: ._

PROFILE «

ACCEPTED BY: __

DRIVERS SIGNATURE:

hk gtyz

783377

A Wfl.ilp Mnnngnmnnt Compnny

^

™«'«WNTT1 • VILIOW • OflNIIUTON COn / MM • OMfOtAL WTI COTV / OOCO • tlUNMOmill CO^V

TONS/YARDS

incoCD

CD

801OCu.o

ix:r

o

c


BILL TO: \VM Milwaukee


~i Golden Marina Causeway LLC *•'-GENERATOR. -~ :

7 ^

GENERATdRS SIGNATURE.

WASTE DESCRIPTION:

PROFILE #

ACCEPTED BY:

DRIVERS SIGNATURE:

Tflr

MW483719

797863

A Wwt« Management Company

Date

Oa»e .,

->, TRUCK NO.. .TONS/YARDSDate

WHTTC • YCU.OW - aeMrMATON COPY / emu • WSPOSAL srrt COPY / GOLD - TRANSPORTER COPY DCE-OM-WW

CDCD•rHO

Ul

~i.

I

• r


BILL TO

TRANSPORTER

GENERATOR


WM Milwaukee

WM Mitwoukee

Marina Causeway LLC

WASTE DESCRIPTION

PROFILE •

ACCEPTED BY

DRIVERS SIGNATURE

/ /0»lt

' - ~^ '___„ TRUCK NO

797864

A W«il« M«n«g«m«n| Company

TONS/YARDS

WMfTt 4 VIUOW • OIMNATOI* CO^V / PMH . (NMOtAl WTI CO»Y / 0<XO

00

CDoT-f

CD

oct

SPECIAL WASTE MANIFEST DISPOSAL TICKETc: :.7

'BILL TO:

WMMH*aukee

-GENERATOR:.Golden Marina Causeway LLC

• 7

| ;;$VAlSTE DESCRIPTIONCool T

- ACCEPTED BY:

bRJVPRS SIGNATURE:

MW483719

Date

DateTRUCK NO. .

797867


WHITE * YELLOW - aeNCMTOft COPY / PINK - DISPOSAL SITE COPY / GOLD • TRANSPORTER COPY

.TONS/YARDS

DCE409 MS

CDCD

01

) iT


A Waste Mfirmgomnnt Compnny

BILL TO: _

TRANSPORTER / J^T.^_

GENERATOR.


WASTE DESCRIPTION

PROFILE • [flW

ACCEPTED BY:

DRIVERS SIGNATURE:MM

TRUCK NO. *&m*(ir TONS/YARDS

WMITi • YtUOW - (MMMTON COTf / WNK - CNMOML WTl COTY / OOLO • TMANWONTIII COTt Dec

5


BILL TO:WM Milwaukee A Watt* Management Company


Xl Golden Marina Causeway LLCGENERATOR: __« V: '

O' :WASTE-DESCRIPTION:

PROFILE #

ACCEPTED BY:

DRIVERS SIGNATURE

Ôkie

TRUCK NO

WMTTB a VCU.OW - OCNeHATOH COPY / PMK • DISPOSAL tttE COPY /OOLO - TRANSPORTER COPY

TON30YAF

OCE-OOV-VN

\J

CDCDCDrH :O i

.

8. *

II

METRO

BILL TO


WM Milwaukee

GENERATOR

GENERATORS 8IONATURE

WASTE DESCRIPTION

PROFILE •

ACCEPTED BY

DRIVERS SIGNATURE


A Wait* M»n«g«m«nl Company

wwn • viuow. otw«n»To« co»v / MM • OMPOUI itrt co»t i ooco

t !

(

! (

O

; • i

IMETRO SPECIAL WASTE MANIFEST DISPOSAL TICKET

, BILL TO: ^_ MitauRee

WAStg DESCRIPTION.

PROFIE6 #

ACCEPf ED BY

DRIVERS "

/

,,Coat Tar

MW483719

Date

Date

797870

A WMt« Management Company

TRUCK NO.

MSPO&L SITE COPY / GOLD • TRANSPORTER COPY

TONS/YARDS

DCE-00»-M5

tf;

CDCvJ

o

IU

g

•f.


BtULTO

TRANSPORTER:

WM Milwaukee

WM Milwaukee

GENERATORGolden Marina Causeway LLC

OENf RATORS SIGNATURE

WASTE DESCRIPTION

PROFILE •

ACCEPTED BY

Coal TarDIM

MW4837I9

DRIVERS SIGNATURE TRUCK NO

WMfTt 4 VtUOW • OCMfKATOM CO*T / MM • MtPMAl tTTf C0»t («XXO

797869

A WMto Management Company

. TONS/YARDS

oct

SPECtAL WASTE MANIFEST DISPOSAL TICKET


TRANSPORTED:.

GENERATOR:

WM Milwaukee


W«STE

PROFILE f

CoolTar

MW483719

ACeEPTED BY:

DRIVERS SIGNATUR

Date

797833


tRUCK NO

WHITE • YELLOW • OENEfUTOII COPT / PMK - DISPOSAL SITE COPY / GOLD • TRANSPORTER COPY

TONS/YARD^

DCE-tiOtWK


* ;

BIU T0

TRANSPORTER

GENERATOR


WASTE DESCRIPTION

PROFILE •

ACCEPTED BY

DRIVERS SIGNATURE\

WM Milwaukee

WM Milwaukee

Cool Tor

MW483719

9>+t..*y-0«l*

I IOil*

A Watt* M«r»«7»m«nt Company

A?.

TONSA'ARDS0«M

WMR1 » tiUOW • 0**NMTO« CO*V I MM • 0»«>01»L MT1 CO»» ' OOlO TNM«t*0«Tt« CO»V

/*j

OCI

BILL TO:

TRANSPORTER:.

GENERATOR: _


WASTE DESCRIPTION:

PROFILE #

ACCEPTED BY:.

DRIVERS SIGNATURE:


sjL/^yDate '

TPUCKMO

768486


Date

WHITE 4 YELLOW - GENERATOR COPY I PINK - DISPOSAL 8ITC COPY / GOLD - TRANSPORTER COPY

ONSfYARC

DCE-009-94 Revised 6/00

METRO

BILL TO


WM Milwaukee

TRANSPORTER

GENERATOR


WASTE DESCRIPTION

WM Milwaukee

Golden Marino C LLC

Coal Tar

MW483719

ACCEPTED BY

DRIVERS SIGNATURE

797838

A Witt* M«n«g»m«n<

/ .. /OiH

TRUCK NO

wwn • viuow . • OH»O>*L wn co»» / oo«.o

TONS/VAROS

oct


: <*,' ' BILL TO: WM Milwaukee

WMTRANSPORTER:

GENERATOR1:y

.-f*

GENERATORS SIGNATURED

.WASTE DESCRIPTION:

'PROFILE #

Golden Morrrw

MW483719

ACCEPTED BY:

"DRIVERS SIGNATURE:Date

./ --LDate .

TRUCK NO.

797837


. TONSÂRDS

WMfTt a VELLOW - QeNCMTOff COPY / PINK - DISPOSAL SITl COPY / GOLD - TRANSPORTER COPY DCE-OOMt*

V

VETRO SPECIAL WASTE MANIFEST DISPOSAL TICKET

OIL TO WM Milwaukee

TRANSPORTERWM Milwaukee



WASTE DESCRIPTION

PROFILE •MW483719

ACCEPTED BY

bRIVERS SIGNATURE

797836

A Will* Management Company

i / ___ TRUCK NOData

. TONS/VARDS

WMOl t YtUOW • tin CO»T / OOiO TK«Nt»(MT|M oct

METRO SPECIAL WASTE MANIFEST DISPOSAL TICKET 797835i


IRATOR: _.«

m : • Sf,T -

j GENERATORS Si&NATURE:.

, WASTE DESCRIPTION:

"*::••} PROFILE*

DRIVERS SIGNATURE:Datt,

TRUCK NO

A Wast* MilrtagwTtcnt Company

.tONS/YARDS

•mure • v«u.o* . oewen*Tt« COPY / nm • OMMMAL wre cwv ' OOLO . TWAWPOHTM COPY oce-oo* i/i»

J)

BILL TO:

TRANSPORTER

GENERATOR: .__/r_*;


WASTE DESCRIPTION: . . ._

PROFILE*

ACCEPTED BY:

DRIVERS SIGNATURE:


,«M1 *> LlOil*

TRUCK NO.

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Date

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TWANSPORTtR

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Eagle Disposal

6old*n Marina Causeway ILC


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DCE-QOO-94 RMndtm, '.• -


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WM Milwaukee

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Cool Tor

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3*' TRUCK NO.

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rDate

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of£

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•m COW / OOLO • TIMMMUnM COW

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METRO/*/

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WM Milwaukee

Golden Marina CausewtlfLLC. //


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DRIVERS SIGNATURE: J ,Daw

773506

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TRUCK

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*

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WM Milwaukee

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Tor

MW4637I9

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Date

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Codfrar

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Date

DataTRUCK NO.


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MlEtftO SPECIAL WASTfe MANIFEST DISPOSAL TICKET 773499

A Wadto Mtttegwncnt Company

WWTC CTIUOW • OtHCTATO*...

OMI«OSAL »n% COET / O&P - T

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WASTE DESCRIPTION:

PROFILE #

• h

Coal TarDate

MW483719

ACCEPTED BY.

DRIVERS SIGNATURE:

Date

Date

WHITE * YELLOW - GENERATOR COPY / PINK • DISPOSAL. SITE COPY / GOLD - TRANSPORTER COPY

Customer Signature

:AI TICKFT 7"?'Â f\cif / 0430

nrtrin

MMrjV7\ A Waste Management Company

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Not Responsible F«ir Damage to Asphalt, Concrete or Landscaping

IAKE STATES INDUSTRIAL SERVICES3H1 East Greenfield Avenue • Milwaukee, Wl 53204' 414^645-0640 • F.ax: 414-645-0645

WMILOAD TICKET

IENT FOR MATERIAL ON THIS TICKET TO BE BY:LS.I.S. Q RECEIVER Q NO CHARGE Q

SCRAP TYPE.

CIRCLE THE SIZEBOX AND WRITEHOW MANY

15 20 25

OR:

35 40

FOREMAN'SSIGNATURE

/ \OFFICE COfTV 00074

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LAKE STATES MDUSTRIAL SERVICES311 EMtOrwrttokJ Avenue • MfcraukBe.WI 53204

/ 414-645-0640 • Fax 414-645-06451

LOAD TICKETRAYUBir FOR MATERML ON THS TICKET TO BE

LSJ.S.Q RECEMERO NOOMRGEQ

JOB NO:

o

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£ S o rn

, ' A T E R I A L

15 20 25 ( 30 ) 35 40

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WM Milwaukee



WASTE DESCRIPTION:.

PROFILE «

ACCEPTED BY:

DRIVERS SIGNATURE:

MW48371

TRUCK NO.

773491

A Wuto Management Company

.TONSA'AROS

WHITE ft YELLOW - OMMTM COW / PMK - DISPOSAL SHE COPT IOOLO • TMNSPOOTtP. COPY oce

> METRO SPECIAL WASTE 'nNIFEST DISPOSAL TICKET 773488'^

WM Milwaukee A WM» Man«g«n*nt Company

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5olden Marina CaiMcway LL£, -t f 1 I «

QENERATORfi SlflNATUHE: / ^« Wk /*-/ ' ^7

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PROFILE*

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1 " ' ' DMCoal Tar

MW463719

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Golden Marina Causzwoy LLC

ERATORS SIGNATURE:

TE DESCRIPTION: oaLTp

ERS SIGNATUI

WHITE a YELLOW - OENEftATOfl COPY / PINK • DISPOSAL SITE COPY / OOLO - TflANSPOtmW COT

'••!• Management Company

/_22_/_a3. TRUCK \.Jjfja1LS_Date

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WMMilwwfcee


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Lake States Industria Service. Inc. A Wuto Maiwg«iTMnt Company

Eagle Disposal

Golden Marina Causzway LLo,

QENCRATOM COPY / PINK • DISPOSAL SnCCOPV / OOLD • THANSPOMTEM CO

TONS/YARDS

OCE-OOMM

lin, Wl 53132640-5571

251-4000(414) 761-3899 Fax

Tickcti 660426 , Driven ROBERT OBRIEN Date Requested: 04/2L/20O4Opened byi KAMMERMA ~ Date Dispatched: 04/27/2004Customeri 477-10601B LAKE STATES INDUSTRIAL-PREPAY

311 GREENFIELD AVE EMILWAUKEE, CITY OF^-WI 33204 414--64S--0&3S

Attn.i BERT 8NEADRequested byi TOM 3 KLA R£0613WM

1 ' •'•' ' * ' . - " ' .

Load Typei SWITCH OUT ¥|Mj| 4 _ M«P Codei M«p Gridi QBRDump Sitei TONNA0E (METmfj ; ,_..'

-:-*^, -;;-; ' TService T)u_antjt'y P YfrdjL Weight Job Special Da»cript.xon __30 YARD SPECIAL WASTE OPEN TOP LOO T 30 ALL TONS DTN COAL TAR riW48-'.7l9DISPOSAL PER TON LOO 7 *,/<-, to -3O..

DEL 5-30S AFTER 7AM SEE CREW FOR SPOTTING INSTRUCTKJNS-FRlABl FNON- FRIABLE RASB 10567 FRIABLE COAL DUST RASB 10'.»12 12--9-04***DU NOT PUT ANY ORDERS IN FOR CUSTOMKK WJ1 HOUT CHF.CKJNP, WTlH ANT HUN

Signature! ( \JV 7 A x Datt-r ..'/ ^ '* '

Wl

Ticket: 66O434 Driven MIKE JOpened by: KAMMERMACustomer: 477-10601B LAKE STATES INDUSTRIAL-PREPAY

311 GREENFIELD AVE E

Waste Management10627 South 27th St.Franklin, Wl 53132(800) 640-5571(262) 251-4000(414) 761-3899 Fax

Date Requested: O4/21/2OO4Date Dispatched: 04/22/2OO4

MILWAUKEE, CITY OF WI 53204Attn.: BERT SNEADRequested by: TOM J KLA CWD

414-645-0635

Load Type:Dump Site:

SWITCH OUT - -*»"TONNAGE (METfH&

Map Code: Map Grid: OBR

• MM!Service """""Quantity ""P Yards Weight Job30 YARD SPECIAL WASTE OPEN TOP 1.00 T 3O ALL TONS DTNDISPOSAL PER TON 1.OO T

Special DescriptionCOAL TAR MW483719s/o 1O-30S

• tt

i DEL 5-30S AFTER 7AM SEEJ NON-FRIABLE RASB 10567! ***DO NOT PU

Signature:

CREJi 'OR SPOTTING INSTRUCTIONS-FRIABLE ASB10566COAL DUST RASB 10012 12-9--O4CUSTOMER WITHOUT CHECKING WITH ANTHONY

6&L Date:

o WM203-FrankHnWI

r

• H*M

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c• UMN

• •Mr

Ticketi 660421 Driven JBABCDCKOpened byi KAMMERMACustomer: 477-10601B LAKE STATES INDUSTRIAL-PREPAY

311 GREENFIELD AVE EMILWAUKEE, CITY OF WI 33204

Attn.i BERT SNEADRequested byi TOM JACOBSQN KLA flpre««

Date Requested!Date Di«p*t<-hed«

414-64 * O6"N«»

Load TypeiDump Sitei

SWITCH OUTTONNAGE

M«P Codei Map Gridi

10627 South 27th St.RunWIn.WI 53132(800) 640-6671(262) 261-4000(414) 761 -3899 Fax

04/22/2004

OBR

30 YARD SPECIAL WASTE OPEN TOPDISPOSAL PER TON

LOO TLOO T

30 ALL TONS DTN_De*cr vptiun

COAL TAR MW483719»/o 10-30«

'EL 3-308 AFTER 7AM SEE CREW FOR SPOTTING INSTRUCTIONS-FRIABLE ASB10S66NON-FRIABLE RASB 10367 FRIABLE COAL DUST RASB 10012 12-9-04***DO NOT PUT ANY ORDERS IN FOR CUSTOMER WITHOUT CHECKING WITH ANTHONYMW483719

• •Ml

:*0Signature! D*tei M M

Waste Management of Wisconsin, Inc.10627 S. 27th StreetFranklin, W153132

WASTE MANAGEMENT 1-800-640-5571 • (262) 25J-4000 • (262) 251-7257 FaxSERVICE TICKET AGREEMENT/NON-HAZARDOUS WASTES

I , -)

DIVISIONNUMBER •&

CUSTOMER

ADDRESS

CITY

ACTION ORD CITY

'ACCOUNTNUMBER

SERVICETYPE

ORDER NUMBER

TIME IN

ROUTE ID DISPOSAL ID DISPOSAL TICKET

SIGNATURE

SERVICE DESCRIPTION WASTE TYPE BILL CODE MEASUREA^.

SERVICE DATF

TIME OUT

COD AMOUNT

BILL QUANTITY"1

AMOUNT

COMMENTS

SERVICES ACCbP I hD SUBJECT TO THE TERMS AND CONDITIONS ON THE REVERSE 3!DE AND PAYMENT AGREED TO BE MADE !N ACCORDANCE WITH THE CONTRACTOR'SCURRENT RATE SCHEDULE

CUSTOMERSIGNATURE .

WM 213CIMS

CONTRACTORSIGNATURE

CUSTOMER COPY

••«*•«"[

NMMftUNflfl

Tickvti 660423 Drivvrt JWILTZIUSOp«n«d by i KAMMERMACumtom«n 477-106018 LAKE STATES INDUSTRIAL-PREPAY

311 GREENFIELD AVE EMILWAUKEE, CITY OF MI 93204

Attn.i BERT 8NEADR«qu«mt»d byi TOM J KLA

10827 South 27th St.FrtnkHn.WI63132(800) 840-5571(282)251-4000(414) 781-38M Fta

D*t» R«qu««t*di 04/21/2004Date Di»p«tch«di 04/22/2004

414-64S-0633

Load TypviDump Sitvi

.SWITCH OUTTONNAGE (ME

Map Gridi OBR

Service30 YARD SPECIAL WASTE OPEN TOP LOO TDISPOSAL PER TON LOO T-

36b _30 ALL TONS DTN

Soacial DamcrlptionCOAL TAR MW4837199/0 10-3O*

NttM* ; DEL S-30S AFTER 7AM SEE CREW FOR SPOTTING INSTRUCTIONS-FRIABLE ASB1O56&NON-FRIABLE RASB 10567 FRIABLE COAL DUST RA6B KXU2 12-9-04***DO NOT PUT ANY ORDERS IN FOR CUSTOMER WITHOUT CHECKING WITH ANTHONY

Signature Dat«i

•n^«


APPENDIX 11-3

Other Non-Hazardous Waste ManifestsWaste Management, Inc.

® EarthTech

L .wo,rk\725:-4\Ad'Tiin\Reports\Rpr text doc

A Waste Man«g rtent Cofnpa

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r:.; }"/',,K ' r * ' " • ' - ' • • • ' . - . " I - V ' " V: - ; - ' - f^ -v^V^ - ! • : • ; ! . ; , ' .•"

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. .

METRO

BILL TO:


Lake States Industrial Service, Inc.

7636S4

A Waste Managwnwit Company

TRANSPORTER:

GENERATOR:.Golden Marino Causzway LLC

r


WASTE DESCRIPTION:

PROFILE #

ACCEPTED BY:

DRIVERS SIGNATUR

Construction <Jt Demolition Debris

.TONS/YARDSOat*

WHITf a VCLLOW - ODWIUTOM COPY / PMK • OWTOML aiTf COTV / OOLO • THANSMMTEII COPV DCC-OOt-WM

•x

METRO

BILL TO

o o o

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763691

A WMto MMMQMM* Company

TRANSPORTER:

QENERATOR.6olden Marina Caunwoy LLC

SIGNATURE

WASTE DESCRIPTION.

PROFILE fl

ACCEPTED BY:

DIVERS 8»QR8 SIGNATURE

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Eagle Date:Disposal, Inc. O Qf cT

^

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2Q£

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B.UTO- Lake

SPECIAL WASTE MANIFEST Dl

States Industrial Service. Inc.

t Disposal

Golden Marina Causzway LLCGENERATOR: . » '


WASTE DESCRIPTION

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tGEPTED BY:

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f\ |\ jt-H\/\ \ 1 i\[ \J \ j[^/il ill n * \^\• \ v \ |S3^ uy* v/ \ i

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l(T~i I \S* \CM*

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A Watte MmaoMiwnt Company

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239269.pdf - Records Collections

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