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7A VOLATILE CONTINUING CALIBRATION CHECK
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case NoI
SAS No SDG No 2083
Instrument ID HP5970X3 Calibration Date 111596 Time 1006
Lab File ID G2636 Init Calib Date(s) 091096 091096
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
c
p p p p 0 CO cn en CO to O TJ CO O
o c c mdash C 10 TJ
3 c z ra mdash
lt bull o o mdash
mdash 3 o cn ra C C 0 = ra ra lt
01 O fO U( o (O ra z en O ogt z
o55| O bullbull cn
O co lt QO VI M O
i v O co CO ogt
cn en CT lta
-Bronochloroiiethane (13260) en u O)
-1 2-Dichloroethcine-d4 (14708)+
-11-Difluorobenzene (15979)
JoIucne-d8 (20116)
o o mdash O 73 3 mdash ra ogt C T f r e T 3 C
O 3 o ~j ra mdash bullbull 3
ra ra bcnzene-d5 (21292)+ Q
rt mdash 7J cn CO
cn u
-Bronof luorobenzene (2775-1)
lta ra
3044
C
Data File chemhp5970g1961115bg2636 d Page 1 Report Date 15-Nov-1996 1048
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2636d Lab Smp Id vstdOlO Client Smp ID vstdOlO In] Date 15-NOV-96 1006 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961115gbelNET Misc Info f 4 f 3 f J U t i t r t t
Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
30446
o ~a co o o o c c mdashc c
-BroHOchloroiiethane (13221)+
=trade=raquoshy
12-Dichloroethane-d1 (11662)+
-11-0ifluorobenzene (15951)
-Toluens-dS (20121)
Chlorobenzene-d5 (21318)
-Bronofluorobenzene (27801)
30447
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
c
p p p p 0 CO cn en CO to O TJ CO O
o c c mdash C 10 TJ
3 c z ra mdash
lt bull o o mdash
mdash 3 o cn ra C C 0 = ra ra lt
01 O fO U( o (O ra z en O ogt z
o55| O bullbull cn
O co lt QO VI M O
i v O co CO ogt
cn en CT lta
-Bronochloroiiethane (13260) en u O)
-1 2-Dichloroethcine-d4 (14708)+
-11-Difluorobenzene (15979)
JoIucne-d8 (20116)
o o mdash O 73 3 mdash ra ogt C T f r e T 3 C
O 3 o ~j ra mdash bullbull 3
ra ra bcnzene-d5 (21292)+ Q
rt mdash 7J cn CO
cn u
-Bronof luorobenzene (2775-1)
lta ra
3044
C
Data File chemhp5970g1961115bg2636 d Page 1 Report Date 15-Nov-1996 1048
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2636d Lab Smp Id vstdOlO Client Smp ID vstdOlO In] Date 15-NOV-96 1006 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961115gbelNET Misc Info f 4 f 3 f J U t i t r t t
Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
30446
o ~a co o o o c c mdashc c
-BroHOchloroiiethane (13221)+
=trade=raquoshy
12-Dichloroethane-d1 (11662)+
-11-0ifluorobenzene (15951)
-Toluens-dS (20121)
Chlorobenzene-d5 (21318)
-Bronofluorobenzene (27801)
30447
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970g1961115bg2636 d Page 1 Report Date 15-Nov-1996 1048
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2636d Lab Smp Id vstdOlO Client Smp ID vstdOlO In] Date 15-NOV-96 1006 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961115gbelNET Misc Info f 4 f 3 f J U t i t r t t
Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
30446
o ~a co o o o c c mdashc c
-BroHOchloroiiethane (13221)+
=trade=raquoshy
12-Dichloroethane-d1 (11662)+
-11-0ifluorobenzene (15951)
-Toluens-dS (20121)
Chlorobenzene-d5 (21318)
-Bronofluorobenzene (27801)
30447
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970g1961115bg2636 d Page 1 Report Date 15-Nov-1996 1048
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2636d Lab Smp Id vstdOlO Client Smp ID vstdOlO In] Date 15-NOV-96 1006 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961115gbelNET Misc Info f 4 f 3 f J U t i t r t t
Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
30446
o ~a co o o o c c mdashc c
-BroHOchloroiiethane (13221)+
=trade=raquoshy
12-Dichloroethane-d1 (11662)+
-11-0ifluorobenzene (15951)
-Toluens-dS (20121)
Chlorobenzene-d5 (21318)
-Bronofluorobenzene (27801)
30447
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
30446
o ~a co o o o c c mdashc c
-BroHOchloroiiethane (13221)+
=trade=raquoshy
12-Dichloroethane-d1 (11662)+
-11-0ifluorobenzene (15951)
-Toluens-dS (20121)
Chlorobenzene-d5 (21318)
-Bronofluorobenzene (27801)
30447
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
30446
o ~a co o o o c c mdashc c
-BroHOchloroiiethane (13221)+
=trade=raquoshy
12-Dichloroethane-d1 (11662)+
-11-0ifluorobenzene (15951)
-Toluens-dS (20121)
Chlorobenzene-d5 (21318)
-Bronofluorobenzene (27801)
30447
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
30446
o ~a co o o o c c mdashc c
-BroHOchloroiiethane (13221)+
=trade=raquoshy
12-Dichloroethane-d1 (11662)+
-11-0ifluorobenzene (15951)
-Toluens-dS (20121)
Chlorobenzene-d5 (21318)
-Bronofluorobenzene (27801)
30447
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970gi961116bg2652d Page 1 Report Date 16-Nov-1996 0851
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2652d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 16-NOV-96 0806 Operator dry Inst ID hp5970gi Smp Info vstd010vstd010961116gdryNET Misc Info 2310 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-Nov-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 3 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30451
Y (xlO~5)
O 13 to O O O C pound mdash P
c ID TJ ra ra r ra mdash 3
bullo o mdash mdash ro mdash 3^ mdash 3 O mdash ra c c -tgt ltA 3 o z ra ra bullbull lt o v bullbull bullbull (A lt O
lt laquo I 37 O Ngt (A Q CD ra agt tn bull-raquo o en 3
mdash co TJ O bullbull en bull mdash CO lt tn vi ltA o rt a
2 i O CO - at CO mdash en mdash
p CT
CT-Broi-iochloronethane (13291) ra
-12-Dichloroethane-dl (14748)+
-1 4-Dif luorobenzene (15990)
(20147)
o o O TJ 3 mdash ra (I c ~i 3 (3
c O 2
amp ^ ft - bullbull 3 S O- raquo ra ra rraquo mdash 3
robenzene-dS (21323)+ ra TO T en
(O
3 tn CO
-Bronofluorobenzene (27791)
P lta
Data File chemhp5970gi961121abg2712d Page 1 Report Date 21-Nov-1996 1357
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2712d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 21-NOV-96 1315 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010961121agbelNET Misc Info 2310 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 15 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
AMOUNTS
QUANT SIG (AL-AMT (DN-COL Compounds MASS RT EXI RT RE1 j RT RESPONSE ( ugL) 1 ugL)
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30456
p p p p amp en CD 00 (~gt ~U CO O O O
o c c mdash c c c Q O C ^ 3
bullo ro 3 no C (X
o v bullC o i
ltD 3- ra
O) 3
8 -3^ en O
CJbullbullPt
tJ Ul (O
CD 1 o
s 01 O
CO O)
ro ro
CTv^
01 01
3
-BronochIoronethane (10165) yi a
-12-Dichloroethane-cH (11619)
bull-14-Difluorobenzene (13674)
o o o -o mdash ra c I ^3 C
lt-raquo
ooT ra
-Toluenc-d8 (17926) Sra _ 01
3 TJ tn (D ^J
sect
Ji CI
raquolorobenzene-d5 (21 245)+
bull-Broiiof luorobenzene ( 2 3 7 1 1 )
30457
Data File chemhp5970hi961122hbh22l5d Report Date 25-Nov-1996 1528
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2215d Lab Snap Id vstdOSO Client Smp ID vstdOSO Inj Date 22-NOV-1996 1348 Operator jss Inst ID hp5970hi Smp Info vstdOSOvstdOSO96ll22hjss NET Misc Info 13 10als 1 Comment Method chemhp5970hi961122hbhvoam Meth Date 25-Nov-1996 1454 jims Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d
Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30461
Data File chemhp5970hi961123hbh2237d Report Date 23-Nov-1996 0906
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961123hbh2237d Lab Smp Id vstdOBO Client Smp ID vstdOSO Inj Date 23-NOV-96 0837 Operator dry Inst ID hp5970hi Smp Info vstdOBOvstdOSO961123hdry NET Misc Info 23 10als 1 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Quant Type ISTD Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 1 Continuing Calibration Sample Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VGA 390
30466
Data File chemhp5970hi961125hbh2259d Report Date 26-Nov-1996 1004
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file Chemhp5970hi961125hbh2259d Lab Smp Id vstdOSO Client Smp ID vstdOBO Inj Date 25-NOV-96 1116 Operator jss Inst ID hp5970hi Smp Info vstd050vstd050961125hjss NET Misc Info 23 1 0 i i i i i i i a l s 1 Comment Method chemhp5970hi961125hbhvoam Meth Date 26-Nov-1996 0921 jims Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 1 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data F i l e chei-ihp5970g i960910abg2096d Page 2 Date 10-SEP-1996 1033
C I lent ID BFB I nstrui-ient hp5970g i
Sanple Info BFBBFB960910gabe INET
Operator be I
Colurm phase CflP Coluhn diai-ieter 053 1 bfb
flvg Scans 222-221 (6 20 ) Background Scan 208 23
22 ~~
2 1 shy
20
19 17lt118
1 7
1 6
1 5 75
1 1
13
12
9 1 1 gtc ~ 1 0
09
08
07
06 SO N
05
01
03
02 A 1 1 y 13 101 i i ^ 0 1 |
100 ill I n Jll 1 1 1 II ll i i 10 50 60 70 80 90 100 110 120 130 110 150 160 170
MZ
X RELflTIVE he ION f lBUNDf lNCE CRITERIf l flBUNDflNCE
bullr mdash
r i i 95 I Base Peak 100x relative abundance 1COOOJ
i 50 I 800 - 10 00 of hass 95 2178
i 75 I 3000 - 6600X of hass 95 5885 i 96 I 500 - 900X of hass 95 -r~ jss ^ i 73 I Less than 200x of Mass 171 000 ( 000) i 71 I 5000 - 12000X of hass 95 7179 i 75 I 100 - 900X of MUSS 171 625 ( 835) i 76 I 9300 - 101 OOx of hass 171 7308 ( 9772) i 77 I 500 - 900X of hass 176 119 ( 6 11)
30472
Data F i l e chci-ihp5970g i 960910a bg2096 d
Date 10-SEP-1996 1033
Page 3
C l lent
Saiiple
Colui in
ID BFB
Info BFB BFB 960910ga be I NET
phase CflP
Instrui-ient hp5970g i
Operator be I
Colunn diaiieter 053
Data F i l e g2096d Spectrun flvg Scans 222-221 ( 620) Background Scan 208 Largest hz 9500 Nuriber of peaks 55
1 177 I 500 -- 900X of ciass 176 569 ( 627) bullbullshy
30475
Data F i l e cheiihp5970g i961 11 5 bg263S d Page
Date 15-NOV-96 0916
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFBBFB961115g be I NET
Operator be I
Colui-m phase CflP Colucin dianeter 053
Data F i l e g2635d Spectrum flvg Scans 223-225 ( 620) Background Scan 210 Largest i-iz 9500 Nunber of peaks 61
11Z MZ HZ nz ____ mdash -__ + _
bullf shybull-------mdash+shy
1 36 CO 571 I 5800 70 I 8000 251 I 116 00 73 1 1 37 CO 2070 I 6000 353 I 81 00 1333 I 1 1 7 00 91 1 1 38 CO 1561 I 6100 1713 I 8200 338 I 119 00 12 1 1 39 CO 166 I 6200 1679 1 8300 69 I 128 00 181 1 1 13 CO 81 I 6300 910 I 8700 1035 I 132 00 69 1
1 11 CO 181 I 6100 181 I 8800 1121 I 111 00 155 1 1 15 CO 352 I 6800 3191 I 9200 976 I 113 00 350 1 1 16 CO 91 1 6900 3117 I 9300 1112 I 159 00 75 1 1 17 CO 561 I 7000 328 1 9100 3968 I 172 00 90 1 1 19 CO 1712 I 7200 211 1 9500 27592 I 171 00 25096 f
1 50 CO 6810 I 7300 1719 1 9600 2102 I 175 00 1995 1 1 51 CO 2183 I 7100 1831 I 9700 70 1 176 00 25018- 1 1 52 CO 105 I 7500 15121 I 10300 163 I 177 00 1571 1 1 51 CO 83 1 7600 1399 I 10100 161 | 1 1 55 CO 277 I 7700 168 I 10500 93 I 1
1 56 CO 697 I 7800 202 I 11200 77 I 1 1 57 CO 980 1 7900 1398 I 11100 91 1 1
Data F i l e chenhp5970gi961115bg2635d
Date 15-NOV-96 0916
C l l e n t ID BFB
Sai ip le Info BFBBFB961115g be I M E T
Colunn phase CflP
Instrunent hp5970gi
Operator be I
Column diaiieter 053
1 6 shychenhp5970g196111Sbg2635d
Page 1
1 5 shy
1 1shy
1 3 shy
1 2shy
1 1 -
1 0shy
ui o
09shy
03shy
07shy
06shy
05shy
01shy
03shy
0 2 shy
0 1 shy
12 11 16 18 50 52 51 56tt i n
58 60
30477
Data F i l e chenhp5970gi961116bg2651d Page 2
Date 16-NOV-96 0737
C l lent IDr-SFlf I nstrunent hp597pg~gti
Sanple Info BFBBFB961116gdry NET
Operator dry
Colurm phase CflP Colunn dianeter 053 1 bfb
flvg Scan $26-228 ( 623) Background Sco(n 213 J
25 2 4
2 3 7^ 22
2 1
20
1 9
1 8
17
1 6
1 5 75
1 4
f 13
2 12 X
~ 1 1
bull 1 0
0 9 shy
0 8 shy
0 7 shy 50v
06
0 5 shy68
0 3 shy
02
0 1 9 H 2N
00- 1 I l l h l lJ 1 il 1 Jl II ll i nl i i l- 40 50 60 70 80 90 100 1 JO 120 130 140 150 160 170 180 190 200 210 220
MZ
v RELflTIVE i-ie ON flBUNDflNCE CRITERI f l f lBUNDflNCE
1 1 1 1 95 I Base Peak 100x re la t i ve abundance 100 00v 1 1 50 I 800 - 4000x of Mass 95 2431 I 1 75 1 3000 - 6600X of nass 95 5382 1 1 96 1 500 - 900X of i-iass 95 623 1 1 173 I Less than 200 of Mass 174 000 ( 000) 1 1 174 | 5000 - 12000X of MUSS 95 8867 bull I
1 175 I 400 - 900X of i-iass 174 666 ( 751) 1 1 176 1 9300 - 101 OOx of wass 174 3537 ( 9627) 1
1 177 I 500 - 900x of i-iass 176 5 44 ( 637) 1
30478
Data F i l e chei-ihp5970g i 961 I 1 6 bg265 I d Page 3
Oats 16-NOV-96 0737
C l l e n t ID BF8 Instruiient hp5970gi
Sanple Info BFB BFB 961 I 1 6g dry MET
Operator dry
Co lurm phase CflP Colunn dianeter 053
Data F i l e 9265 ld Spectrun flvg Scans 226-228 ( 623) Background Scan 213
I I 1 I 95 | Base Peak 100x relative abundance 1I 50 | 800 -- 1000X of i-iass 95 1I 75 I 3000 -- 6600 of Mass 95 II 96 | 500 -- 900X of i-tass 95 II 173 | Less than 200X of Mass 171 II 171 | 5000 - 12000X I- of nass 95I 175 | 100 -- 900X of nass 171 II 176 I 9300 -- 101 OOx of nass 171 II 177 | 500 -- 900X of nass 176 1
I I 95 1 Base Peak 100 relative abundance 1 10000 50 I 800 - 1000 of i-iass 95 I 1990 75 I 30 00 - 6600 of nass 95 1 1858 96 1 500 - 900 of nass 95 I 711 173 1 Less than 200 of nass 171 I 000 ( 000) 171 | 50 00 - 12000 of MOSS 95 1 9796 175 I 100 - 900 of nass 171 I 722 ( 737) 176 1 93 00 - 10100 of i-iass 171 I 9878ltIOO 35)
177 | 5 00 - 900 of nass 176 1 611 ( 652T
30487
Data FHe^ cheithpS970h 1961 1 22h bh221 4 d Page 3
Date 22-NOV-961321
C l l e n t ID bfb Instrui-iem hp5970h i
Scmple Info bfb bfb961122hjss NET
Operator jss
Column phase DB502 Colurm diai-ieter 053
Data F i l e h2211d Spectruri flvg Scans 189-191 ( 592) Background Scan 181 Largest HZ 9500 Number of peaks 12
HZ Y HZ Y HZ Y bulliZ Y
I 3600 81 I 5100 961 1 7100 bull 2118 96 00 1031 I I 3700 1008 1 5600 332 1 7500 6718 100 00 151 I I 3800 719 I 5700 519 1 7600 152 119 00 153 I I 3900 156 1 6000 78 1 7900 171 131 00 100 I I 11 00 69 1 6100 692 1 8100 176 171 00 1 13607 J
I 1300 180 I 6200 621 1 8700 592 175 00 1CO3 I
I 1100 16 1 6300 529 1 8800 182 176 00 1 3722 J I 1500 216 I 6800 1671 1 9200 133 177 00 ~51 I I 1700 258 I 6900 1298 1 9300 585 207 00 67 I I 1900 631 I 7000 161 1 9100 1612 I
00 I I I I ll Jll I II l l 1 1 r 10 50 60 70 8b 90 100 110 120 130 110 150 160 170_ 180 190 200
MZ ry RELflTIVE Me ION RBUNDflNCE CRITERIfl flBUNDflNCE
1 95 Base Peak 100 relative abundance 1 10000 50 800 - 1000 of MOSS 95 I 2112 75 3000 - 6600 of MOSS 95 I 1936
96 500 - 900 of MOSS 95 I 721 173 Less than 200 of Mass 171 I 000 ( 000) 171 5000 - 12000 of Mass 95 1 9172 j 175 100 - 900 of Mass 171 I 683 C 721) j 176 9300 - 101 OOX of MOSS 171 I 9068 C 9571)
177 500 - 900 Of Mass 176 1 618 ( 715)
30493
Data F i l e chei-ihp5970h i961125hbh2258d
Date 25-NOV-96 1054
Page 3
C l l e n t ID bfb Instrui-ient hp5970h i
Sanple Info bfb bfb96H25h jss NET
Colurin phase DB502
Operator jss
Coluiin diaiieter 053
Data Fi le h2258d Spectrui-i flvg Scans 200-202 ( 603)gt Background Scan 192 Largest nz 9500 Nunber of peaks 39
MZ Y MZ Y NZ Y MZ Y
11111
3600 3700 3800 3900 4100
272 908 867 103 50
55005600570060006100
78 324 523 69 789
73007400750076007900
bull 763 2553 7835 710 492
9400950096001190017400
1747 I 15872 1 1145 1 70 1 15034 I
11111
4500 4700 4900 5000 5100
209 298 658 3399 1060
62006300680069007000
654 489 1739 1577 84
81008700880092009300
467 606 643 444 722
17500176001770020700
1084 I 14393 1 1029 1 69 1
1
30494
Data F i l e chei-ihp5970h 19611 25h bh2258 d Page t
Date 25-NOV-96 1051
Clicnt ID bfb Instrument hp5970hi
Sanple Info bfb bfb961125hjss NET
Operator jss
Co I mm phase DB502 Colunn diai-ieter 053
85shy82-j 80-78shy75shy72shy70shy681 65 62-i
chenhp5970h 1961 125hbh225 Sd
bull-M
0CO ^ pound J3
mdash
r 60 58shy55shy52- r 50shy
~ 18shyr is o 12shyx 10-
r 38
35 32shy30- r 28^ 25 22shy20-18shy15shy12shy10shy08shy05shy
i y
r ~
l2 1^1 1^6 18 5io 5^2 Sl 5^6(1 1 n
5^8 6^ 3 6^2 6^1 6^6 6^8 7^0 7^2 j~
30495
3 D ( 2 ) BLANK DATA
30496
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride_ 10 U
50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 11- Dichloroe thene 10 U 75-34-3 11-Dichloroe thane 10 U
10 U 67-66-3 Chlorof orm_ 10 U 107-06-2 12-1 10 U 78-93-3 2- But anone 50 U 71-55-6 111 -Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-5 12 -Dichloropropane 10 U 10061-01-5 cis-13-Dichloropropene 10 U 79-01-6 Trichloroethene 10 U 124 -48-1 Dibromochloromethane 10 U 79-00-5 11 2-Trichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene 10 U 75-25-2 Bromof orm ~ 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2 -Hexanone 50 U 127-18-4 10 U 79-34-5 1 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Tr ichlorof luoromethane 10 U
FORM I VOA 390
30497
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1115G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1115G
Sample wtvol 2500 (gmL) ML Lab File ID G2637
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111596
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i DP nc A 10 u 1 1 0-7^ ftshy 10 u
10 u QC _ AH f 10 u CAIDf4X ni O i JL j ~jjicnjojOJjenzcnc 10 u T Cpound_LUO AC iD n plusmn ~jjicnjojrojjenzcnc 10 u qc en -i 10 u
FORM I VGA 390
30493
Y (xicrs)
o ^o co o o oo^ c c mdash s c Cz3
O D it) ra mdash 3 ra t
o pound
bullbull -n bulla31
Oat
o mdash mdash 3
c -h z o
mdash ^ bullbull
mdash mdash cn Q
i bullbull z
bullbull bullbull O lt O
ou
lt mdash I rs) CT TT _ cn mdash mdash ltD
3 ra 2
73 O shy shy S mdash cn TJ mdash 0 mdash cn cn mdash CO
lt 2 degO 0 CT
CO ogt
bull-BronochIoronethane (13279) cn IS)agt CO
CT
-1 2-Dichloroetliane-cH (14821)
1 jl-Difluorobenzene (15978)
Toluenc-d8 (20135) o o 0 bullo mdash ra c -i
1 S a
oT Q
3 c Z CT o ra
gtnc-cChlorobenzeric-dS (2^311) in (O
igtcn cn
CO
Broriof luorobenzcnc (27792)
bullo
30499
c
Data File chemhp5970gi961115bg2637d Page 1 Report Date 15-Nov-1996 1143
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961115bg2637d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 15-NOV-1996 1100 Operator bel Inst ID hp5970gi Smp Info vblklllSgvblklllSg961115gbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961115bgvoa25m Meth Date 15-Nov-1996 1045 Quant Type ISTD Cal Date 15-NOV-96 1006 Cal File g2636d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1116G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1116G
Sample wtvol 2500 (gmL) ML Lab File ID G2653
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 111696
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 U 74-83-9 Bromomethane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chi oroethane 10 U 75-09-2 Methylene Chloride 10 U 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 1 U 75-35-4 11 -Dichloroethene 1 U 75-34-3 11-Dichl oroethane 1 U 540-59-0 12-Dichloroethene (total) 1 U 67-66-3 Chloroform 1 U 107-06-2 12 -Dichloroethane 1 U 78-93-3 2-Butanone 50 U 71-55-6 111-Trichloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichloromethane 10 U 78-87-510061-01-5
12 -Dichloropropane cis-13-Dichloropropene
10 10
U U
79-01-6 Trichloroethene 10 U 124-48-1 Dibromochloromethane 10 U 79-00-5 112 -Tr ichloroethane 10 U 71-43-2 Benzene 10 U 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromof orm 10 U 108-10-1 4-Methyl-2-Pentanone 50 U 591-78-6 2- Hexanone 50 U 127-18-4 Tetrachloroethene 10 U 79-34-5 112 2-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 10 U 100-42-5 Styrene 10 U 75-69-4 Trichlorof luoromethane 10 U
FORM I VOA 390
30501
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
108-0 c^ A
C Q110-7
1541-7
95-50 T
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1116G Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1116G
Lab File ID G2653
Date Received
Date Analyzed 111696
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30502
Y (x lO~5)
CO Jk _c
00 o 00 o 73 co o lt3 o o c c mdash c c C 3 Q i C
3 ^ ra lt-f bullbull -n bullo o mdash mdash mdash mdash ~ mdash 3 cgt CD ra c c -^ bullbull i bullbull ct mdash o z ra ra bullbull lt o ~x bullbull bullbull CT lt o
lt mdash I 3 o is) CT bull mdash ra D cn mdash mdash co zbullD bull TT mdash lto xgt
O mdash mdash cn 3shymdash co -o mdash IQ O cn co co co
mdash O lt co gta
bull-Broiiochloroiiethone (13 165)
-12-Dichlorogthang-d^ (14710)
co co
ogt
Q
CO
CT
ro cn cn co
1 4 - 0 f luorobenzenc (15914)
-IS)plusmn0 3 Tcluene-d8 (20 111 ) co
o o
rs)poundraquo
Chlorobenzene-dS(24327) 19-5
O cn
3-bullo cn co
IS)00 Broi-iofluorobenzenc (27820)
CO rsgt~
TJ3
30503
Daca File chemhp5970gi961116bg2653d Page 1 Reoort Date 18-Nov-1996 1238
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961116bg2653d Lab Smp Id vblklllSg Client Smp ID vblklllSg Inj Date 16-NOV-1996 0919 Operator dry Inst ID hp5970gi Smp Info vblklllSgvblklllSg961116gdryNET Misc Info 3BLANK10 Comment Method chemhp5970gi961116bgvoa25m Meth Date 16-NOV-1996 0846 Quant Type ISTD Cal Date 16-NOV-96 0806 Cal File g2652d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1121AG Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1121AG
Sample wtvol 2500 (gmL) ML Lab File ID G2713
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112196
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
10 U 7A Q3 Q 10 u 7C m A 10 u 7^ nn i 10 u TC rQ O 10 u pound7 poundA 1 - 50 u 7C T C n 10 u 7cr _ ~i c A shy 10 u 7CT O j f tA 7 10 u D J
1 bull FN-i -raquoVgt 1 --v-lt-^ipoundit- l-i eir-d f f- ^l- -3 1 u10 pound7 poundrc o _ _ 10 u i-LU n7 U D nc -zo mdash 10 u 7Q QT 7 50 u 71 n cr c 10 u c r 07 c 10 u 7C 9 7 _ A _ 10 u 7Q 07 c 10 u
10 u 7 Q ~ m ^ 10 u 1 9A AQ 1 10 u 7 q _ n n R 10 u 71 A1 O 10 u i n n ^ i no f 10 u
10 u i np i n i 5 0 u C Q-1 -70 C 50 u 1 9 7 - l f l d 10 u 7Q ^A ^ 10 u i np pp-7 10 u i np on 7 10 u i n n AI A - 10 u i n n AO c 10 u
10 u
FORM I VOA 390
30505
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i no nt^ A i i n 7^ Q shy
QC A7 pound
C A T r75 1
1 Dpound Aamp 7 QC en 1D DU -L shy
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
VBLK1121AG Contract GEI
SAS No SDG No 2083
Lab Sample ID VBLK1121AG
Lab File ID G2713
Date Received
Date Analyzed 112196
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL Q
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30506
ooooooooo r o r o r o r o r o r o r o N ) r o r o c o c o c o c j c o c o c o c o u i c o _ c
O U CO O O O o c c mdash c c C ifi O O ( p z ra mdash 3 3 ra lt-raquo bull- -n
O o mdash mdash ro mdash 3- mdash 3 o mdash ra C c -n bullbull i bullbull w z o ~z ra ra bullbull lt o gt CT lt o
lt mdash i 3shyo ro CT JT mdash ra TD bull 7^ mdash ltpoundgt V
O mdash ro en 3~ ro c mdash en
O O
CT TT CO
OT
ro
p CO CT o
ia bull -Broiiochloroiiethane (13269) ro
-12-Dichloroethane-cH (H8H) CT ra
-oW luorobcnzcne (15987)
o o o -a 3 mdash ra (I C -5
i S 1 C
o O T
E mdash CT O Q
ra 7gt Chlorobenzend-d5 (21290) -gt Ol
O |Q
en CO
Brouof luorobenzene (27772)
8shy
TJ p
30507
Data File chemhp5970gi961121abg2713d Page 1 Report Date 21-Nov-1996 1449
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961121abg2713d Lab Smp Id vblkl21ag Client Smp ID vblkl21ag Inj Date 21-NOV-1996 1408 Operator bel Inst ID hp5970gi Smp Info vblkll21agvblkll21ag961121agbelNET Misc Info 3BLANK10 Comment Method chemhp5970gi961121abgvoa25m Meth Date 21-NOV-1996 1354 Quant Type ISTD Cal Date 21-NOV-96 1315 Cal File g2712d Als bottle 16 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) shy
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 11 -Dichloroethene 5 U 75-34-3 11 -Dichloroethane 5 U 540-59-0 1 2-Dichloroethene (total) 5 U 67-66-3 Chloroform 5 U 107 -06-2 12 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichloromethane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Tr ichloroethene 5 U 124-48-1 Dibromochloromethane 5 U 79-00-5 11 2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-13-Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 5 U
5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1122H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1122H
Sample wtvol 5000 (gmL) ML Lab File ID H2216
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112296
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HQJUO rd U D A i ~ v myj icet-aue 5 U 1 1 H_L_L U 7^ D QO diJOiOcLnyjv my Jshy eunex 5 U
QC7D AH plusmn ampD shy _~ ltanQ p Ayj-cne 5
5 U U
C A T T T 5 U i n^ AS 7 5 U QC en i 5 U
FORM I VGA 390
Y (x10~5)
O)
b O TJ (J) O C7 O O^ C C mdash C C
C ltQ ^ O f3 C s ra mdash 3 3 ra ~ gtgt -r|
73 o mdash mdash ro mdash 3 mdash 3 oo ra C C -iraquo bullbull Ugt 2 O o ra bullbull lt CT lt o
i 3shyo tn CT ^~ OD bull mdash mdash to ^ mdash ra-
ro 3- mdash 01 N) if^ to
(OO)
lto agt
3 ro ro
a) bull -Broiiochloroi-iethane (10199) CL
bull-12-Dichlorocthane-d-l (11 662)
bull-14-Dif luorobenzene (13718)
o a o 73 3 mdash ra (A C -T 2 pound 3 fgt
O a T
bull-Toluene-d8 (17979) ra ui lt-gt ut 3 f) bulla -j or
(Oxi O p
in
Chlorobenzene-dS (21288)
Broi-iof luorobenzene (23755)
30511
Data File chemhp5970hi961122hbh2216d Report Date 22-Nov-1996 1458
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961122hbh2216d Lab Smp Id vblkl22h Client Smp ID vblkl22h Inj Date 22-NOV-1996 1426 Operator jss Inst ID hp5970hi Smp Info vblkl22hvblkl22h961122hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961122hbhvoam Meth Date 22-Nov-1996 1412 Quant Type ISTD Cal Date 22-NOV-96 1348 Cal File h2215d Als bottle 2 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf
Data File chemhp5970hi961122hbh2216d Report Date 25-Nov-l996 1521
Data file Lab Stnp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Dil Factor Integrator
NET Cambridge
Unknown Compounds Quantitation Report chemhp5970hi961122hbh2216d vblkl22h Client Smp ID vblkl22h 22-NOV-1996 1426 JSS Inst ID hp5970hi vblkll22hvblkll22h961122hjss NET 3BLANK 10als 2
chemhp5970hi96H22hbhvoam 25-NOV-1996 1454 jims 22-NOV-96 1348 Cal File h2215d 2 QC Sample BLANK 1000 Target Version 312 HP RTE Compound Sublist allsub
Sample Matrix WATER Quantitative Mode Use RF of Nearest Std
- NO TENTATIVELY IDENTIFIED COMPOUNDS shy
3051
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
74-A7 7 shy 5 U 7 A -R Q 5 U c m A T f bull - ll- ~ -n-W-l Jy-t D UJ- ft v my j Lii_LOi iQe 5 U
5 U 7c nQ- o 5 U poundbullbull7 poundbull A 1 TV - A_ 1mdash - D O4 -L cc u one- 25 U bull7C -1C nD JD U 5 U bull7C 7 C A 5 U 7C T A 5 D Jplusmn J 5 U t^A n c Q n 5 U pound7 poundpound 7 - 5 U im npound o 5 U 70 Q-J O 25 U bull71 c C C-L DD D 5 U cr 97 c _ 5 U TC O7 A 5 U 70 0-7 c 5 U
5 U 7Q_ni fi shy 5 U
T^-I VN-V-gt-HraquoVlaquoy-N^^Vl T --f - yy 4- V i- y^ ^-^ 1 O A A Q 1_LZplusmn to J_- 5 U 7Q nn c 5 U 71 AT 9 shy 5 U i nn^i no ^ 5 U 7C oc 9 O J OiUOLO j-Ul 5 U i no in i A TUT -- gtj WT raquoT o T^^^-I mdashi ir-xraquo^ x^ -LUO JU J_ ft iiscnyx amp t sntlaquono ric 25 U CQ-] 70 c 25 U
rji v_ n mdash_raquoraquo i_ 1_ T-I -v 1 O7 I R A 5 U 7Q-7A R 5 U
rp _ ~| -bullbulllaquo^1 nR QR 7 io j-UGns 5 U 1 nft -QO 7- 5 U i nn AI A Tt-v n ^f- mdash -^-mdashmdash 5 U inn AO Rshy 5 U 7C poundTQ A 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1123H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1123H
Sample wtvol 5000 (gmL) ML Lab File ID H2238
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL Q
1 HQ rc A 5 U i i n i^ ft - shy-L _LU 13 O 5 U
5 U QC^ AT C - _ 5 U C11 Hl 1DftJ J L j jJicrij-Oj-TODenzcne 5 U -i rc AC 7 5 U QC en 1 5 U
FORM I VOA 390
mdash mdash mdash mdash mdash r s gt r s gt N r s gt N M C O M u c o j b b amp b b t n t n lt s i u i i n O T3 CO o o 0 C g c c C 10 7) z ra mdash c
-n 73 O mdash 3- mdash 3 C C -raquo 01 Z O ra ra bullbull
bullz o
o ui cr 0) bull mdash i O x-
mdashmdashro
CO Z CO x m 3shy
3^ O en CO CO
mdash Otn 3shyo-r
(OO)
10 3
CO 3
CT ^ 3-
CO a CO
bull-Broiiochloroiiethane (10266) -5
bull-12-Dichloroethane-dl (11720)
bull-14-Dif luorobenzene (13766)
0 0 o -a 3 mdash ra w C T - C 3 lt-raquo
aOT ra
bull-Toluene-d8 (18007) rra
Q -i
3 73 tn O3 VI g
J 01
Chlorobenzene-d5 (21306)
NJ Ji Bronofluorobenzene (23752)
ro oo
CO O
3051R
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
Data file Lab Smp Id Inj Date Operator Smp Info Misc Info Comment Method Meth Date Cal Date Als bottle Oil Factor Integrator
NET Cambridge
VOLATILE ISTD AND RATIO REPORT chemhp5970hi961123hbh2238d vblkl23h Client Smp ID vblkl23h 23-NOV-1996 0915 dry Inst ID hp5970hi vblkll23hvblk123h961123hdry NET 3BLANK 10als 2
chemhp5970hi961123hbhvoam 23-NOV-1996 0903 Quant Type ISTD 23-NOV-96 0837 Cal File h2237d 2 QC Sample BLANK 1000 HP RTE Compound Sublist allsub
Data File chemhp5970hi961123hbh2238d Report Date 25-Nov-1996 1424
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2238d Lab Smp Id vblkl23h Client Smp ID vblkl23h Inj Date 23-NOV-1996 0915 Operator dry Inst ID hp5970hi Smp Info vblkll23hvblkll23h961123hdry NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 2 QC Sample BLANK Dil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10256 1258461 50000
CONCENTRATIONS QUANT
RT AREA ON-COLI ugL) FINAL(ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS
2545 710700 28 28 20
Unknown CAS
3007 5093143 200 200 20
30513
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulf ide 5 U 75-35-4 11- Dichloroethene 5 U 75-34-3 11- Dichloroethane 5 U 540-59-0 12-Dichloroethene (total) 5 U 67-66-3 Chloroform _ 5 U 107-06-2 12-Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 111-Trichloroethane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1 2-Dichloropropane 5 U 10061-01-5 cis-13-Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124-48-1 Dibromochlorome thane 5 U 79-00-5 1 5 U 71-43-2 ^ 5 U 10061-02-6 trans-13-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentanone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 1122 -Tetrachloroethane 5 U 108-88-3 Toluene ~ 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluoromethane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1125H Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID VBLK1125H
Sample wtvol 5000 (gmL) ML Lab File ID H2260
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 112596
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
i no nc AJUO UD plusmn 5 U i i n 7R Q 5 U
5 U QC AH CiD ft D Ay-Lerie 5 U CAI HI i 5 U 1 Hpound AC H 5 U QC _ crn -i 5 U
FORM I VOA 390
i s gt r s gt c o c o c o c o ji cn cn en cn
c o c o O r s gt C i C o O O r _d co O T3 CO O C7 O_ C pound mdash C
C ~~ Q C ra mdash
3 o f o mdash mdash ro mdash mdash 3 o cn ra
C c -n bullbull i bullbull (I 3 O Z ra ra bullbull lt o v bullbull bullbull CT lt O
lt mdash I 3 o cn cr ^ mdashbull ra CD bull mdash mdash to mdash
I O 7T mdash U3 ~v mdash IS) CO 3
7 mdash cn -a X fs) 3 mdash cn
cn mdash (D
cn O lt CS) 3
CO CO
IS) cn
IS) en
to IT CO
IS) 3shycn IS)
IS) CO o
ot ltnbull -Broi-ioch I oronethane (10 468)
bull-12-Dichloroethane-d4 (11932) o 3 ra 2 s 3shybullo cn CO
bull-14-Dif luorobenzene (13977) s
(0 O)
0 0 mdash IS) O TJ 3 cn mdash ra w 3 C T ^
2 C -gt 3 rt C
O Z 3 Q T fraquo rs) - 3 IS) C
g ra uibull-Toluene-d8 (18239) laquo W 3 ra 7) -raquo cn bull bull CO
3 O 3shy
IS) O
Chlorobenzenc-d5 (21198)
Brohofluorobenzene (2392 )
IS)or
rsgt CO
30523
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-Nov-1996 1212 Quant Type ISTD Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Data File chemhp5970hi961125hbh2260d Report Date 25-Nov-1996 1223
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961125hbh2260d Lab Smp Id vblkl25h Client Smp ID vblkl25h Inj Date 25-NOV-1996 1152 Operator jss Inst ID hp5970hi Smp Info vblkl25hvblkl25h961125hjss NET Misc Info 3BLANK 10als 2 Comment Method chemhp5970hi961125hbhvoam Meth Date 25-NOV-1996 1212 Cal Date 25-NOV-96 1116 Cal File h2259d Als bottle 2 QC Sample BLANK Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist allsub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10478 1266376 50000
CONCENTRATIONS QUANT
AREA ON-COM ugL) FINAL ugL) QUAL LIBRARY LIB ENTRY CPND
Unknown CAS ft
3078 4796243 190 190 20(L)
QC Flag Legend
L - Operator selected an alternate library search match
30525
ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer ERROR Free() passed a NULL pointer
1A EPA SAMPLE XO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MS Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MS
Sample wtvol 5000 (gmL) ML Lab File ID H2244
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL) _
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 HPLUO CC UD A ft - vinyj Acecaue 5 U i i n id QJJU D O 5 u
5 U QCD AH i CO 5 u cnD4plusmnT OC
-7-5 O
AfC
Tplusmn n
5 2
u J
QC CA T 20
FORM I VOA 390
O O O O r o r o r o r o r o c o c o c o c o c n c n c n o j O T C T ) O bullD CO rgt o O o c ^ 3
C T ia ra
c 5_ ra
mdash
ra 3 ^
c r^ ra
C fraquo
c -n
tgt lt 0 ^ __ ro _
3shyP c
3 -traquo
Cgt
COi
ra CD z 0 -z rabull bull
o
ralaquobull
cn ^ cn
CO romdasht^
lt 1
CO
X
o 3 r
CO 1 ltX)X
O
XI
CO
8 3 CO
00 3 C
^ mdash
cn
CO
mdash
-T
X
3^ -a cn CO
CO mdash XI xl
O ro -
CO 01
3
00 CO x 3 CO C CD
z It
mdash ro mdash mdash
CO 3shy
CO bull
o cr 3 CO
x 3shy
laquo ro CO cn mdash
ro^ plusmn1
ro a CO
-1 2-D ich loroethane-d^ (11681) CO xl cn
bull -14-Difluorobenzene (13727)
o a mdash Omdash
~O ra
3 CD
C T -raquo z c -gt 3 rt C
ooT z ra
bull-Toluene-d8 (17978) - bullbullOz a ra T
3 i-raquo
rtra
gtlt 3 TJ
- cn co xl O
O 3
Jgt mdash cn
Chlorobenzene-dS (21277)+
Broriof luorobenzene (23721)
Pshy
8-f
30530
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
VOLATILE ISTD AJSfD RATIO REP ORT Dat a file chemhp5970h i961123hbh2 244 d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Ope rator dry Inst ID hp 5970hi Smp Info 157380MS 92113nalmlll96MS 96 1123hdry 3 754 Mis c Info 2 0 8 3 3 MS 10 15-NOV- 1996 als5 Com ment Met hod chemhp5970h i961123hbhv oa m Met h Date 23-Nov-1996 09 03 Quant Type ISTD Cal Date 23-NOV-96 08 37 Cal File h2237 d
~~ Als bottle 8 QC Sample MS Dil Factor 1 000 Int sgrator HP RTE -- s^r Compound Su blist 8240 sub Tar get Version 3 12 Con -entration Formula Uf i
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30532
Data File chemhp5970hi961123hbh2244d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2244d Lab Smp Id 157380MS Client Smp ID 92113nalmlll96MS Inj Date 23-NOV-96 1317 Operator dry Inst ID hp5970hi Smp Info 15738QMS92113nalmlll96MS961123hdry3754 Misc Info 20833MS1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 8 QC Sample MS Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
I STD RT AREA AMOUNT
20 Bromochloromethane 10228 1383591 50000
CONCENTRATIONS QUANT
RT AREA CN-COL jgD FINAL( ugD QUAL LIBRARY LIB ENTRY CPND tt
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
NA1M1MSD Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2083
Matrix (soilwater) WATER Lab Sample ID 157380MSD
Sample wtvol 5000 (gmL) ML Lab File ID H2245
Level (lowmed) LOW Date Received 111596
Moisture not dec Date Analyzed 112396
GC Column DB-VRX ID 045 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
HA P7 1 5 U 7A PI Qshy 5 U bull7C ni A 3 JJL plusmn v my j v^iiJ-Oi icic 67
-jc nn 7 5 U 7c nQ-9 5 U en CA 1 ~MLeL-one 25 U 7C -ic n 5 U bull7C o c A 51 IC ~ QD Jft O 19 CA n CTQ n 110 pound7 poundpound 7 5 U i n7 npound o 12 7Q Q^ _2 25 U 71 CR ^ J- OD -D 5 U CC O7 cr _ 5 U bull7C 07 A 5 U TQ Q7 R O O 3 z Jjicnj-Oiopiropciiic 5 U i nnci m cr 5 U 7Q m fi 82
J-4 bull V^-Vi-^V-l-lVin ri --L- yy - ^ lT - ^- -1 OA A fl 1LZ^t plusmnO - X mdash uiDiOuiocnxojroiiicLnane 5 U 7Q nn c uu D x z li icnxoiroeuiiaJie 4 J 71 A3 O 56 i nn^i nsgt-f i 5 U bull7C oc o 5 U
gt1 it fr T- _ _T ^S Tl^w^4- mdash iv^x^ i no i n i-LUo XU -L - plusmn -ivieunyx z fenua-nonG 25 U C Q T 70 poundT _ 25 U
rri-^L^ T^T V JTJIL JT1 O I P A leuiacnxoioeunene 10 Q 1A Q y Jfplusmn -D ~ x z z~ i6ujraCnplusmnojroeuroLnaJie 5 U 1 OP QP T shy iojiiene 55 1 Oft -QO 7 - 52 i nn AI A 2 J
O^- ^^ --bdquoi nn AO c ouyirene 5 U 7R poundQ A i IT ic nxo JTOt j_ uo IT orne L nane 5 U
FORM I VOA 390
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column DB-VRX
Soil Extract Volume
CAS NO
1 Oft DR-A
1 1 C 7c oJJU D O
QC AH a yo plusmn 1 O CA1 Tl 1Dft-L J -L i nc Apound iJLUD plusmnD qc qn 1- shyJZgt 3U -L mdash
5000 (gmL) ML
LOW
ID 045 (mm)
(uL)
COMPOUND
NA1M1MSD Contract GEI
SAS No SDG No 2083
Lab Sample ID 157380MSD
Lab File ID H2245
Date Received 111596
Date Analyzed 112396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
5 U 5 U 5 U 5 U 5 U 2 J
20
FORM I VOA 390
o o o o mdash r o r o r o r o c o c o c o c o c o ro jgt co co O 0 ~D co o o o
o^ c o mdash a c C poundJ ~O ra ra Ci z ra mdash 3 3 ra rt bullbull -ri D O mdash mdash ro mdash 3 mdash 3 O CO ra C c -n bullbull i bullbull 01 ^ o z ra itraquo bullbull co o x IS) lt O
mdash mdash i 3shyo en en mdashbull co ra CD bull vi co co ^ l_ O CO 3
3 C mdash mdash L T3
_ - cn CO mdash O CD O mdash O vl
- mdash OCO CO 3 ro co
mdashmdash CO3 mdash v CO O CO 3 CO c mdash ^ ro mdash CO mdash 3
CO CT CO v^ 3 3^ cn ro o ro
-Cgt co cn CO
ro CO
-12-Dichlorocthane-d4 (11529)
bull-14-Difluorobenzene (13584)
o o c n 3
a
bull-Tolucnc-dS (17816) O ra
3 ra bulla
cn (O
g3shyJi cn
Chlorbenzene-d5 (21175)+
Bronof luorobenzene (23fj41)
30538
Data File chemhp5970h i961123h_bh2245 d Report Date 26-Nov-1996 1518 shy
NET Cambridge
7OLATILE I 3TD AND RAT] 0 REPORT Data f i le chemhp5970h i961123h bh224~5d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD I n j Date 23 -NOV-96 14 ( )0 Operator dry Inst ][D hp5970h i Smp Info 157380MSD 9211 L3nalmlll9 5MSD 9611231-i dry 375 -shyMisc Info 2 0 8 3 3 MSD 1 0 15-NOV-1996 als5 Comment Method chemhp5970h -i-961123h bhvoa m Meth Date 23-Nov-1996 0 3 0 3 Quant Type ISTD Cal Date 23-NOV-96 081 57 Cal FD le h2237d Als bottle 9 QC San iple MSD Oil Factor 1000 Integrator HP RTE Compox ind Sublist 8240 sub Target Vers ion 3 12 Concentrate on Formula Uf 1
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
QC Flag Legend
a - Target corrpound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test R - SpikeSurrogate failed recovery limits M - Compound response manually integrated
30540
Data File chemhp5970hi961123hbh2245d Report Date 26-Nov-1996 1518
NET Cambridge
Unknown Compounds Quantitation Report Data file chemhp5970hi961123hbh2245d Lab Smp Id 157380MSD Client Smp ID 92113nalmlll96MSD Inj Date 23-NOV-96 1400 Operator dry Inst ID hp5970hi Smp Info 157380MSD92113nalmlll96MSD961123hdry375 Misc Info 20833MSD1015-NOV-1996 als5 Comment Method chemhp5970hi961123hbhvoam Meth Date 23-Nov-1996 0903 Cal Date 23-NOV-96 0837 Cal File h2237d Als bottle 9 QC Sample MSD Oil Factor 1000 Target Version 312 Integrator HP RTE Compound Sublist 8240sub Sample Matrix WATER Quantitative Mode Use RF of Nearest Std Concentration Formula Uf 1
Name Value Description
Uf 1000 ng unit correction factor
ISTD RT AREA AMOUNT
20 Bromochloromethane 10065 1430524 50000
CONCENTRATIONS QUANT
RT AREA ON-COL( ugL) FINAL( ugL) QUAL LIBRARY LIB ENTRY CPND
Ethane 12-dichloro-112-trifluoro- CAS 354-23-4
5 052 365097 13 S3 NBS75K1 10049 20
30541
FD CASE 2124
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Proj ect Tinkham Garage
FD Case 2124
Section One
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
H HAD23
Section 1
Section 2
Section 3
Section 4
Section 5
Section 6
Section 7
Section 8
Section 9
Section 10
Section 11
Section 12
TABLE OF CONTENTS
Report Front
1A Table of Contents
IB NarrativeCover Letter
1C Main PageSample Cross Reference
ID Chain of Custody Forms
IE Sample Receipt Logbook
IF Data QualifierFlag Descriptions
1G Document Inventory Sheets
1H Control Charts
Metals Analysis Data
Volatile Organics Analysis Data
Semi-Volatiles Analysis Data
PesticidesPCB Analysis Data
Herbicide Analysis Data
Organophosphorus Pesticides Data
Diesel Range Organics Analysis
Gasoline Range Organics Analysis
Cyanide Analysis Data
Page Number
DX VoccSs
1CCOU ) ccol AV cco$ 6ccfl AlAshy
No Analysis Requested
30000
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
No Analysis Requested
Total Petroluem Hydrocarbons DataNo Analysis Requested
General Chemistry Analysis Data No Analysis Requested
10001
Cambridge Division 12 Oak Park NATIONALlgtiy-VI IWINyiL Bedford MA 01730
ENVIRONMENTAL i trade 275-3535 NET TESTING INC
January 3 1997
Mr Bob Mullin GEI ConsultantsNHSuffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 2124 NET job number 9604043)
This narrative addresses all comments for all samples as listed below
92113-LGSW-1296 158551 12OS1996 1305 12071996 GROUND WATER
10002
Cambridge Division 12 Oak Park NATIONAL Bedford MA 01730
ENVIRONMENTAL Tel (617)275-3535 Fax (617)275-1151 NET TESTING INC Fax (617)275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals Analysis No Analysis Requested Volatile Organics Analysis TABLE 3 Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis Requested Organophosphorus Pesticides Analysis No Analysis Requested Diesel Range Organics Analysis No Analysis Requested Gasoline Range Organics Analysis No Analysis Requested Cyanide Analysis No Analysis Requested Total Petroleum Hydrocarbons Analysis No Analysis Requested General Chemistry Analysis No Analysis Requested
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1
SAMPLE RECEIPT amp LOGIN FD2124
GENERAL COMMENTS No comments necessary
1000
TABLES
VOLATILES ORGANICS NARRATIVE SUMMARY FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total i2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal -to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
10005
NET Cambridge Division
ANALYTICALREPORT
Report To Reported By
Mr Bob Mullin
GBI ConeultantsNH
Suffolk Building
S3 Regional Drive
Concord NH 03301
National Environmental Testing
NET Atlantic Incorporated
Cambridge Division
12 Oak Park
Bedford MA 01730
Report Date 01031997 NET Job Number 9604043
Project Tinkhara Garage NET Client No 14755
PO No 7889 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No 9110820471
This report has been approved and certified for release by the following staff Please feel free to call the NBT
Project Manager at 617-275-3535 with any questions or comments
Conr Report prepared byPetePeterr MM Conroy
NET Project Manager NET Reports Groiap
Analytical data for the following samples are included in this data report
SAMPLE NBT DATE TIME DATE
ID ID TAKEN TAKEN RBCD
92113-LGAW-1296 158550 12061996 1155 12071996 GROUND WATER
92113-LGSW-1296 158551 12061996 1305 12071996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
10006
^ -~ LU CO O LU LU gt
2Z ^
i_ Q l^ sectbull OC 3
liss
isgg I- CshyO -I ltO
SS Q QZ lt lt LU K X Z LL UJ OCO LU LU
spound3raquosect
Jv0
r
bull5
I V
CO cr UJ a lt LU cr
f LU
sid^ o5O
C
io
sg Bs lt LU P OC Z LU
55LU u
t 3 o yCO LU
lt CO LU O
it Q
sectO
0lt I- LU DCO LU LU Q CO
12 ^^ LU O
Se |iOT
z w 01 QC D O O I- LU LU EC OC _
lt COO a co Q cc LU Q Z
LU oc
a lt CO
Ishy
(0 u O O O
w r 1
S=vvt ^a^rn Mf
ORGANIC FLAGS AND SAMPLE SUFFIXES
The following qualifiers have been used for reporting results
B - The B flag indicates that the analyte was found in the associated blank as well as in the sample
E - The E flag indentifies compound concentrations that exceed the calibration range of the GCMS instrument For Benzo (b) and Benzo (k) Flouranthene the calibration range of each peak will be considered separately Ortho para and meta xylene are quantified as two peaks the calibration range of each peak will be considered separately
D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported the diluted analysis will have the DL suffix All concentration values reported for the diluted analysis will be flagged with a D
U - The U flag indicates that the compound was analyzed for but not detected The reported U value is the detection limit for the given compound The value is corrected for dilution and for percent moisture
J - The J flag indicates an estimated value The flag is used for tentatively identified compounds where a 11 response is assumed or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit
P - The P flag indicates that the quantitated value of a target pesticidePCB differs by more than 25 on the two GC columns that were reported
Y - Compound values that are flagged with a Y have been edited on our RTEMS data system
X - Compound values that are flagged with a X have been edited on our Foremaster data reporting system
The following sample suffixes have been used
XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD raquo matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution
10008
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 0000
3A 3B 3C
PC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
0001 0007 0026
3D 3D1 3D2 3D4 3D4
Raw PC Data BFB Tunes Blank Data -Form I Matrix Spike Raw Data Matrix Spike Duplicate
Ib Raw Data
Raw Data
0049 0056
NR NR
10009
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 2124
Section Three Volatiles Analysis
NET Job Number 9604043
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number
M MAO23
TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY
FD 2124
GENERAL COMMENTS The samples were analyzed using a modified low level method 624 with a 25 ml sample purge volume Data forms were produced using our CLP forms software
MANUAL INTEGRATIONS Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography This is confirmed by visual inspection by the analysts The M flag indicates that a manual integration has been performed
Compound Total 12-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers
SURROGATES All system monitoring compound recoveries were within the contract required QC limits
BLANKS A method blank was analyzed for each twelve hour time period on each GCMS system used for analysis No blank contained greater than five times the reporting limit of Methylene Chloride Acetone and 2-Butanone or greater than or equal to the reporting limit of any other volatile target compound
TUNE All instrument performance check criteria were met prior to the start of sample analysis
CALIBRATION All calibrations met the QC criteria
INTERNAL STANDARDS All internal standard areas and retention times were within the QC limits
HOLDING TIMES All samples were analyzed within required holding times
DILUTIONS No dilutions were necessary
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH
NET Job Numbers 9604043 Tinkham Garage
FD Number 2124 Tinkham
ITEM PAGE
3 GCMS VOLATILE ORGANIC ANALYSIS DATA 3 0000
3A3B3C
QC Summary -Forms II III IV V Sample Data -Forms I Ib Raw Data Standards Data -Forms VI VII VIII Raw Data
3 3
3
0001 0007 0026
3D3D13D23D43D4
Raw PC Data BFB Tunes Blank Data -Form I Ib Raw Data Matrix Spike Raw Data Matrix Spike Duplicate Raw Data
3 0049 3 0056
NR NR
3 VOLATILES DATA
Qr-EJshy
30000
3A QC SUMMARY
30001
2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO (TOL) (BFB) (DCE) OUT
50 80 - 400 of mass 95 218 75 300 - 660 of mass 95 588 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 65 173 Less than 20 of mass 174 00 00)1 174 500 - 1200 of mass 95 748 175 40 - 90 of mass 174 62 ( 84)1 176 930 - 1010 of mass 174 731 ( 977)1 177 50 - 90 of mass 176 45 ( 61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
50 80 shy 400 of mass 95 263 75 300 - 660 of mass 95 576 95 Base Peak 100 relative abundance 1000 96 50 - 90 of mass 95 81 173 Less than 20 of mass 174 00 ( 00)1 174 500 - 1200 of mass 95 587 175 40 - 90 of mass 174 47 ( 79)1 176 930 - 1010 of mass 174 561 ( 956)1 177 50 - 90 of mass 176 40 ( 72)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
AREA UPPER LIMIT = +100 of internal standard area AREA LOWER LIMIT = - 50 of internal standard area RT UPPER LIMIT = + 050 minutes of internal standard RT RT LOWER LIMIT = - 050 minutes of internal standard RT
Column used to flag values outside QC limits with an asterisk Values outside of QC limits
page 1 of 1 FORM VIII VGA 390
30006
3B SAMPLE DATA
30007
LA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGAW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG NO 2124
Matrix (soilwater) WATER Lab Sample ID 158550
Sample wtvol 2500 (gmL) ML Lab File ID G2871
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
1 75-27-4 Bromodichloromethane 1 78-87-5 12 -Dichloropropane 1 10061-01-5 cis-13-Dichloropropene 1 79-01-6 Trichloroethene 1 124-48-1 Dibromochlorome thane 1 79-CJO-5 11 2-Trichloroethane 1 0 71-43-2 Benzene 13 10061-02-6 trans-13-Dichloropropene_ 10 U 75-25-2 Bromoform 10 U 108-10-1 4-Methyl-2-Pentanone 10 U 591-78-6 2-Hexanone 10 U 127-18-4 Tetrachloroethene 10 U 79-34-5 1122-Tetrachloroethane_ 10 U 108-88-3 Toluene 10 U 108-90-7 Chlorobenzene 10 U 100-41-4 Ethylbenzene 25 100-42-5 Styrene 10 75-69-4 Trichlorof luoromethane 10
FORM I VOA 390
30008
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i n o n^ A shy-i -i n-7^ ft
QQ A pound shy
CAI TI i 1 0pound Apound-7shyQC en 1yo ou Jmdash
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
LGAW Contract GEI
SAS No SDG No 2124
Lab Sample ID 158550
Lab File ID G2871
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 U 2 -^1^1 f^TY^^t Vll ^71 TTV1 ft~ H^T 10 U
10 U 10 U 10 U 10 U 8 4
FORM I VGA 390
30009
o o o o mdash - - mdash mdash o ~o cn o o o o c c mdash o c
z ra mdash 3
y mdash 3 ^ co rs C C -gt bullbull I bullbull laquo 3 O OQ ft mdash rn O O
mdash c o rsgt cnr D cn oo -o bull cn
O cn O
I o 3
mdash raus r to OT 3
-3 mdash Ul
bulla c mdash O
CO cn
rgt
co
COa)
O ra
-Broi-iochlororicthanc (13269) tsgt oo
-1 2-Dichloroethane-cH (11 8H)
-0ifluorobenzeJie (15 977)
Toluene-^8 (20124) o o
c 5 Q
C
a 3 a TJ
Chiorobenzene-db (24300) -5 cn (O
p
CO
Broi-tof I uorobenzene (27781)
COJl
CO 00
30010
Data File chemhp5970gi961213bg2871 d Page 1 Report Date 13-Dec-1996 1503
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2871d Lab Smp Id 158550 Client Smp ID Igaw Inj Date 13-DEC-1996 1414 Operator bel Inst ID hp5970gi Smp Info 158550Igaw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp597Ogi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 7 Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
Scan 3098 (32593 inn) of g2871d (x DIFFERENCE) ICO
SOshy60shy
10shy38 63 112X x113 20shy
il
pound -20 S -10
-60shy-80shy
-1COshy10 50 60 70 80 90 100 110 120 130 110 150
11 Z
30015
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID 158551
Sample wtvol 2500 (gmL) ML Lab File ID G2872
Level (lowmed) LOW Date Received 120796
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chlorome thane 10 74-83-9 Bromome thane 10 75-01-4 Vinyl Chloride 31 75-00-3 Chloroethane 10 75-09-2 Methylene Chloride 10 67-64-1 Acetone 10 75-15-0 Carbon Disulfide 10 75-35-4 11 -Dichloroethene 10 75-34-3 11 -Dichloroethane 2 6 540-59-0 12-Dichloroethene (total) 16 67-66-3 Chloroform 10 u 107-06-2 12-Dichloroethane 10 u 78-93-3 2 -Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-5 12 -Dichloropropane 10 u 10061-01-5 cis-l3-Dichloropropene 10 u 79-01-6 Trichloroethene 16 124-48 -1 Dibromochlorome thane 10 79-00-5 11 2-Trichloroethane 10 71-43-2 Benzene 6 0 10061-02-6 1r ans -13-D ichl oropropene_ 10 u 75-25-2 Bromof orm 10 u 108-10-1 4-Methyl-2-Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 1122-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 2 6 100-42-5 Styrene 10 75-69-4 Trichlorof luorome thane 10
FORM I VGA 390
30016
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
LGSW Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol 2500 (gmL) ML
Level (lowmed) LOW
Moisture not dec
GC Column CAP ID 053 (mm)
Soil Extract Volume (uL)
CAS NO COMPOUND
i nfl nc A 1 1n 1^1 flshy
QR-47 pound shyC A T F73 i
1 Dpound 4pound-r7 QC en 1
Contract GEI
SAS No SDG No 2124
Lab Sample ID 158551
Lab File ID G2872
Date Received 120796
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30017
Y (X1CT5)
O O O O f o r o N gt r v j r o c o c o t o c o c o u i a i u i Tgt CO O c cT r c (Q -O c ra mdash
ro
o mdash co ra
C cn _ _ ra ra bullbull mdash Q
mdash Ul o is) cn r 3gt cn agt
cn O cn
oi
mdashcocoo)
o 3-ra z shy^ 3-
cn cn o z co gto
CO CO
co N) cn
CO IS o
U) CT ra CT
-Bronochloroiiethane (13291)
-1 bull-Pirhlnrnrrhfinr- fH f 11 8271
rJb 1 4-D i f luorbenzene (16000)
[ Toluene-d8 (20127)
o o O TJ mdash a C T
i S o
a -i c Z CT
Chlorobenzene-dS (2-1303)
ran^^ mdash a
CT bullo cn co
cn co
IS) 03 Bronof luorobenzene (27775)
CO O
T3
30018
C
Data File chemhp5970gi961213bg2872d Page 1 Report Date 13-Dec-1996 1543
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2872d Lab Smp Id 158551 Client Smp ID Igsw Inj Date 13-DEC-1996 1458 Operator bel Inst ID hp5970gi Smp Info 158551Igsw961213gbelGEI Misc Info 01007-DEC-1996 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 8 Dil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf
Compounds with required minimum RRF and maximim RSD va] ues All other compounds must meet a minimim RRF of 0010
page 2 of 2 FORM VI VOA 390
30023
o o o o o o o o o mdash
c c - c c bulla ra ra c
lt mdash 5 deg 3 5 3 raquo C C -bullraquo bullbull I bullbull cn = o en ra ra bullbull lt m v 01 -a o
i o is) w co ra u ui laquo O) 3
O O r-o mdash 3shy0 vi TJ ro bullbull en - O co lt mdash vi 01 O laquo ifl
CO
co sectO) CO O co o
cO
C
o CO
-Broi-iochloroitethane (13256) +
I)2-Dichloroethonc-d4 (H675) +
bull -1 4-D if luorobenzene (15967)
-Toluene-d8 (20116) 0 0 mdash 0 - 0 3 mdash ra oi C T raquo 2 C T 3 ft C
O 2 Q T laquo mdash 3
i o- raquo ra (O laquo mdash 3shyra bullo T en
co -Chlorobenzene-dS (2 295)+
en CO
-Bronof luorobenzene (27769)
bullo
30029
c
Data File chemhp5970gi960910abg2103d Page 1 Repcrt Date ll-Sep-19961019
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2103d Lab Snp Id vstd002 Client Smp ID vstd002 In] Date 10-SEP-961701 Operator bel Inst ID hp5970gi Smp Info vstd002vstd002960910gabelNET Misc Info - - - - t 1- t V t r i f i i i
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als octtle 7 Calibration Sample Level 1 Dil Factor 1 000 Intearator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantisation(BLOQ)
Q - Qualifier signal failed the ratio test M - CcTpound response manually integrated
30031
o o o o o o o o o
IS)
-BronochloroMethone (13270)+
12-Dichloroethane-dlt1 (14708)+
-14-Difluorobenzene (15971)
-Toluenc-d8 (20120)
-Chlorobenzene-dS (21299)
8shy
-Brot-iofl uorobenzene (27773)
O U CO O O O o c c mdash c c _ -J 2 mdash rl -i c a o i9 Q cj 2 raquo mdash 3 3 lt raquo ~ - 2
bullo o mdash mdash mdash mdash ~~ mdash 3 O O fJ C C I 01 2 O cn ra ra bullbull
o rsgt w co ra D cn laquo co 3bullo bull ao O
bullo ui
co co 8
co sectCO O
c o lto c
IS)
o
D O mdash O TS 3 mdash ra laquo C T laquo 3 C -gt 3 f C
O 2Q T ra
C laquo2 cr mdash 3 ra TJ -gt cn
to
cn u
bullo
30032
C
Data F_le chemhp5970gi960910abg2104d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2104d Lab Snp Id vstd004 Client Smp ID vstd004 Irn Dare 10-SEP-96 1744 Operator bel Inst ID hp5970gi Smp Info vstd004 vstd004 960910ga bel NET Misc Info -- -L
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle Calibration Sample Level 2 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
Q - Qualifier signal failed the ratio test M - Compound response manually integrated
30034
-BroMochloroiiethane (13265)+
-12-Dichloroethanltz-d1 (1
-111-0ifluorobenzene (15976)
-Toluene-d8 (20135) 0 0O TJmdash ra
mdash 3 M
C T laquo 33
C t
T C
Q r oshy
Iorobenzene-d5 (21301) 03
-BroMOfluorobenzene (27768)
a-i
bulla
30035
c
Data File chemhp5970gi960910abq2102d Page 1 Report late ll-Sep-1996 0958
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data f i le chemhp5970gi960910a bg2102d Lab Smp Id vstdOlO Client Smp ID vstdOlO Inj Date 10-SEP-1996 1544 Operator bel Inst ID hp5970gi Smp Info vstd010vstd010 960910g bel NET Misc In fo 2 3 1 0 Comment Method chemhp5970g i960910a bgvoa25 m Meth Date ll-Sep-1996 09 58 brian Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 10 Calibration Sample Level 3 Oil Factor 1000 Integrator HP RTE Compound Sublist all sub Target Vers ion 312 Concentrati on Formula Uf 1
a - Target compound detected but quantitated amount Below Limit Of Quantitation(BLOQ)
M - Cc-ipound response manually integrated
30037
O TJ O) o o O C C mdash c mdash 1 2 C O T )2 ltraquo mdash 3 lt T) O mdash 3 mdash 3 oq c ft I ogt 3 o U)
m
o tsgt o aD en 8 e
cn =
bull O M O O O -^
CO TI bullbull tn N) CO
Ut ^ s ltf laquoQ
8 N O CO
co s s CO
(O o C
O tn
Broi-iochloroiiethanc (13269)
bull-12-Oichloroethane-dlt1 (H727)
--1H-Difluorobenzenc (15980)
-Toluene-d8 (20129) o o o -a mdash M C T 3 C 3 laquo C
O 3
tn co
ChIorobenzeng-d5 (24396) Obulla
cncj
-Broiiof luorobenzene (27772)
|Q a
30033
c
Data File chemhp5970gi960910abg2105d Page 1 Report Date ll-Sep-1996 1013
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2105d Lab Smp Id Inj Date
vstd02010-SEP-96 1827
Client Smp ID vstd020
Operator bel Inst ID hp5970gi Smp Info vstd020vstd020960910gabelNET Misc Info 1410 t t r f t I
Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bottle 9 Calibration Sample Level 4 Dil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
Name Value Description rjf 1 000 ng unit correction factor
mdash M U J k t n o o v i c o e o O mdash o TJ to 0 c e c crt ^
re re C z re mdash 3 3 lt bullo o mdash 3 mdash 3 O re C C -laquo i bullbull 01 3 O cgt re re bullbull
bullo o I 3
o fo oi a co re s in raquoraquo O 01
lt w-raquo sect
sect o (O
(O o C o
10 c cr ra
Bronochloronethane (13260)+
-12-Dichloroethane-d4 (11708)+
-1i^-Difluorobenzene (15971)
-Toluene-cIS (20130) o o mdash o -a 3 mdash re (A c -raquo bullgtraquo 2 C T 3 laquobullraquo C
O Z a i re mdash bullbull 3 sect a
^raquo re re f mdash 3 re -a -i 01
-ChlQi-obenzene-dS (21397) (0
U1 u
ro bull-BroMofluorobenzenc (27773) oo
cjO)
CJ O)
3004C
Data File chemhp5970gi960910abg2106d Page 1 Report Date ll-Sep-1996 1012
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi960910abg2106d Lab Smp Id vstd040 Client Smp ID vstd040 Inj Dane 10-SEP-96 1910 Operator bel Inst ID hp5970gi Smp Info vstd040vstd040960910gabelNET Misc Info 1510 Comment Method chemhp5970gi960910abgvoa25m Meth Date ll-Sep-1996 0959 Quant Type ISTD Cal Date 10-SEP-1996 1544 Cal File g2102d Als bo~tle 10 Calibration Sample Level 5 Oil Factor 1000 Integrator HP RTE Compound Sublist allsub Target Version 312 Concentration Formula Uf 1
All other compounds must meet a minimum RRF of 0010
page 2 of 2 FORM VII VOA 390
3004^
p p p oraquo agt to o -o O
o c c -c 10 z ra
lt 13 O mdash mdash mdash mdash
3C C -K bullbull I at = O O a ra bullbull lt m
ltA o ISJ Ut Q (D U) laquo O 01
b S 0shyp I lt ltJI O
bulla
O)
O) ro M Ul
o-
CT-BroMOChloroMethone (13289) ra CO
CO araquo raquo
a 12-Dichloroethonc-d4 (14726)+
bull-14-0ifluorobenzene (15998)
-Toluene-d8 (20125)
o o mdash o -o 3 mdash 19 M C T f r c bullgt 3 C
a OT ra shy
c ~ Z CT ra ra laquo mdash 3shy-Chlorobenzene-d5 (24310)+ ra ij T 01
ui to
-BroMofluorobenzene (27772)
w rj
3004
Data File chemhp5970gi961213bg2868d Page 1 Report Date 13-Dec-1996 1113
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2868d Lab Snap Id vstdOlO Client Smp ID vstdOlO Inj Date 13-DEC-96 1022 Operator bel Inst ID hp5970gi Smp Info vstdOlOvstdOlO961213gbel NET Misc Info -5 -L laquo f Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 2 Continuing Calibration Sample Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1
mdashmdash--i I 5700 1 1 1 4 I 7700 162 I 10400 178 I
30054
Data F i l e chenhp5970gi961213bg2867d Page
Data 13-DEC-96 1002
C l lent ID BFB Instrument hp5970g i
Sai-iple Info BFB BFB 961 21 3g be I HET
Operator be I
Co I linn phase D6502 Colunn dianeter 053
chenhp5970gi961213bg2867d
12shy
52 54 Urn
30055
3D(2) BLANK DATA
30056
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK1213G Lab Name NET CAMBRIDGE Contract GEI
Lab Code CAMBRG Case No SAS No SDG No 2124
Matrix (soilwater) WATER Lab Sample ID VBLK1213G
Sample wtvol 2500 (gmL) ML Lab File ID G2870
Level (lowmed) LOW Date Received
Moisture not dec Date Analyzed 121396
GC Column CAP ID 053 (mm) Dilution Factor 10
Soil Extract Volume (uL) Soil Aliquot Volume (uL)
CONCENTRATION UNITS CAS NO COMPOUND (ugL or ugKg) UGL
74-87-3 Chloromethane 10 u 74-83-9 Bromomethane 10 u 75-01-4 Vinyl Chloride 10 u 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride 10 u 67-64-1 Acetone 10 u 75-15-0 Carbon Disulfide 10 u 75-35-4 11 -Dichloroethene 10 u 75-34-3 11-Dichloroethane 10 u 540-59-0 12-Dichloroethene (total) 10 u 67-66-3 Chloroform 10 u 107-06-2 12 -Dichloroethane 10 u 78-93-3 2-Butanone 10 u 71-55-6 111-Trichloroethane 10 u 56-23-5 Carbon Tetrachloride 10 u 75-27-4 Bromodichloromethane 10 u 78-87-510061-01-5
12-Dichloropropane cis-l3-Dichloropropene
10 10
u u
79-01-6 Trichloroethene 10 u 124-48-1 Dibromochlorome thane 10 u 79-00-5 112 -Trichloroethane 10 u 71-43-2 Benzene 10 u 10061-02-6 trans-13-Dichloropropene_ 10 u 75-25-2 Bromoform 10 u 108-10-1 4 -Methyl -2 -Pentanone 10 u 591-78-6 2-Hexanone 10 u 127-18-4 Tetrachloroethene 10 u 79-34-5 ll22-Tetrachloroethane_ 10 u 108-88-3 Toluene 10 u 108-90-7 Chlorobenzene 10 u 100-41-4 Ethylbenzene 10 u 100-42-5 Styrene 10 u 75-69-4 Trichlorof luorome thane 10 u
FORM I VGA 390
30057
1A EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name NET CAMBRIDGE
Lab Code CAMBRG Case No
Matrix (soilwater) WATER
Sample wtvol
Level (lowmed)
Moisture not dec
GC Column CAP
Soil Extract Volume
CAS NO
i HQ n^ A 1 1n TQ-Q
QC^D-plusmnA7 do cn T _ i 1 Ofi dfi 7
i7DQC DU en X
2500 (gmL) ML
LOW
ID 053 (mm)
(uL)
COMPOUND
vmyjL Aceuace
Ay-Lcllc
VBLK1213G Contract GEI
SAS No SDG No 2124
Lab Sample ID VBLK1213G
Lab File ID G2870
Date Received
Date Analyzed 121396
Dilution Factor 10
Soil Aliquot Volume (uL)
CONCENTRATION UNITS (ugL or ugKg) UGL
10 u 10 u 10 u 10 u 10 u 10 u 10 u
FORM I VGA 390
30058
O O O O i s ) M r v j i s ) M c o c o c j c o c j i i - amp c i U T c i c n c n lt n o 13 to n O 0 C C mdash C
C tO 73 19 ~ 19 mdash 3 3 lt r a bdquo
73 O mdash mdash 3 mdash3 O O C - bullbull CD = O o
m O
mdash I 3O M pound7 mdashbull 19 D cn mdash mdash CO shy
IV) CO gt b = mdash agt 3shy
CO 73 bullo mdash cn
NJ CO -vj
mdash O
CO M cn CO
bull-BroMOChloroMethane (13289) O) tO -vj
poshyr-r a
1 i^-Di f luorobenzenc (16007)
lplusmno-
Si
IV) cn I
00 r CO o-
CO IV)
CO Ji
Toluene1s (20131)
Chlorobenzene-d5(21310)
Bronof luorobenzcne (27782)
o o o 73
19 c -I
3 Cr O
a
o-19
19 -I
3bulla cn co
cn co
Tgt
bulla C
CO 00
30059
Data File chemhp5970gi961213bg2870d Page 1 Report Date 13-Dec-1996 1340
NET Cambridge
VOLATILE ISTD AND RATIO REPORT Data file chemhp5970gi961213bg2870d Lab Smp Id vblk213g Client Smp ID vblk213g Inj Date 13-DEC-1996 1214 Operator bel Inst ID hp5970gi Smp Info vblk213gvblk213g961213gbel NET Misc Info 3BLANK10 Comment Method chemhp5970gi961213bgvoa25m Meth Date 13-Dec-1996 1110 Quant Type ISTD Cal Date 13-DEC-96 1022 Cal File g2868d Als bottle 4 QC Sample BLANK Oil Factor 1000 Integrator HP RTE Compound Sublist 8240sub Target Version 312 Concentration Formula Uf 1