ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Pensacola 3355 McLemore Drive Pensacola, FL 32514 Tel: (850)474-1001 TestAmerica Job ID: 400-61296-1 Client Project/Site: 0147519/ Terminal Revision: 2 For: ERM Panama Via Ricardo J. Alfaro, Century Tower Piso 17, Oficina 1705 Panama City, Panama Attn: Nicolas Gwyther Authorized for release by: 3/26/2012 12:58:49 PM Marty Edwards Customer Service Manager [email protected]Designee for Mark Swafford Project Manager I [email protected]The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 9 10 11 12 13 14
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The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Definitions/GlossaryTestAmerica Job ID: 400-61296-1Client: ERM Panama
Project/Site: 0147519/ Terminal Balboa
Qualifiers
GC/MS VOA
Qualifier Description
F MS o MSD excede los límites de control
Qualifier
* LCS o LCSD excede los límites de control
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Case NarrativeClient: ERM Panama TestAmerica Job ID: 400-61296-1
Project/Site: 0147519/ Terminal Balboa
Job ID: 400-61296-1
Laboratory: TestAmerica Pensacola
Job Narrative
400-61189-1
C
CommentsNo additional comments. Receipt All samples were received in good condition within temperature requirements. GC/MS VOA Method 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for batch 400-144994 over recovered for the following analyte: Ethanol. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data have been reported. No other analytical or quality issues were noted. GC VOA No analytical or quality issues were noted. GC Semi VOA No analytical or quality issues were noted. Metals No analytical or quality issues were noted. Organic Prep No analytical or quality issues were noted.
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Detection SummaryTestAmerica Job ID: 400-61296-1Client: ERM Panama
TestAmerica Pensacola 136State ProgramWest Virginia DEP 3
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory's
current list of certified methods and analytes.
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Method SummaryTestAmerica Job ID: 400-61296-1Client: ERM Panama
Project/Site: 0147519/ Terminal Balboa
Method Method Description LaboratoryProtocol
SW8468260B VOC TAL PEN
SW8468015M 8015M GRO TAL PEN
EPA8015M DIesel Range Organics (DRO) TAL PEN
SW8466010B Lead TAL PEN
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001
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SERIAL NUMBER:
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD TestAmerica Pensacola Phone: 850-474-10013355 McLemore Drive Fax: 850-478-2671Pensacola, FL 32514 Website: www.testamericainc.com
QUOTE NO. BOTTLE ORDER NO. JOB NO.
LAB
USE
ONLY
- SA
MPLE
NUM
BER
CLIENT ADDRESSREQUESTED ANALYSIS
PAGE OF
PROJECT NAME PROJECT NO. CLIENT PROJECT MANAGER PROJECT LOC. (STATE) POSSIBLE HAZARDIDENTIFICATION
SAMPLED BY CONTRACT / P.O. NO. PRESERVATIVE MATRIX ∆ NON-HAZARD
No P
rese
rvativ
eHC
L - H
ydro
chlor
ic Ac
idHN
O3 -
Nitric
Acid
H2SO
4 - S
ulfur
ic Ac
id or
H3P
O4NA
OH -
Sodiu
m Hy
drox
ideCH
3OH
- Meth
anol
NAHS
O4 -
Sodiu
m Bi
sulfa
teNA
2S2O
3 - S
odium
Thio
sulfa
teOt
her:
Drink
ing W
ater
Aque
ous G
W, S
W, W
WSo
lid, S
emiso
lid, S
edim
ent
Air
NonA
queo
us (O
il,Solv
ent, e
tc.)
∆ FLAMMABLECLIENT PHONE CLIENT E-MAIL OR FAX ∆ RADIOACTIVE
∆ POISON BTAT REQUESTED: RUSH NEEDS LAB PREAPPROVAL □ NORMAL - 10 BUSINESS DAYS ∆ UNKNOWN□ 1 DAY □ 2 DAYS □ 3 DAYS □ 5 DAYS □ 20 DAYS (Package) □ OTHER: ∆ OTHER:SAMPLE DISPOSAL: □ RETURN TO CLIENT □ DISPOSAL BY LAB NO. OF COOLERS PER □ SEE CONTRACT □ OTHER: SHIPMENT:
SAMPLESAMPLE IDENTIFICATION NUMBER OF CONTAINERS SUBMITTED
SPECIAL INSTRUCTIONS/DATE TIME CONDITIONS OF RECEIPT
RELINQUISHED BY: (SIGNATURE) DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME
RECEIVED BY: (SIGNATURE) DATE TIME RECEIVED BY: (SIGNATURE) DATE TIME RECEIVED BY: (SIGNATURE) DATE TIME
LABORATORY USE ONLYRECEIVED FOR LABORATORY BY: DATE TIME CUSTODY INTACT? CUSTODY SEAL NO. TEMPERATURE OF COOLERS & REMARKS:
∆ YES ∆ NO
Login Sample Receipt Checklist
Client: ERM Panama Job Number: 400-61296-1
Login Number: 61296
Question Answer Comment
Creator: Hor, Koma
List Source: TestAmerica Pensacola
List Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
N/AThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded. 1.8°C
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.