ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Denver 4955 Yarrow Street Arvada, CO 80002 Tel: (303)736-0100 TestAmerica Job ID: 280-107262-1 TestAmerica Sample Delivery Group: DN0332 Client Project/Site: S18-003/X18-005/W18-003/W18-002/S18- 002 For: CH2M Hill Plateau Remediation Company PO BOX 1600, MS H8-41 Richland, Washington 99352 Attn: Mr. Scot Fitzgerald Authorized for release by: 4/9/2018 5:46:16 PM Darlene Bandy, Project Manager I (303)736-0100 [email protected]The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 9 10 11 04/09/2018 REV.0 .. ........ .... LINKS ... ........ . Review your project results through Total Ac cess Have a Question? ~ k The Ex ert Visit us at: www. testa merica inc.com Test America • THE LEADER IN ENVIRONMENTAL TESTING
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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Denver4955 Yarrow StreetArvada, CO 80002Tel: (303)736-0100
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Case NarrativeClient: CH2M Hill Plateau Remediation Company TestAmerica Job ID: 280-107262-1Project/Site: S18-003/X18-005/W18-003/W18-002/S18-002 SDG: DN0332
Job ID: 280-107262-1
Laboratory: TestAmerica Denver
Narrative
CASE NARRATIVE
Client: CH2M Hill Plateau Remediation Company
Project: S18-003/X18-005/W18-003/W18-002/S18-002
Report Number: 280-107262-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
The laboratory is not able to achieve project specified Highest Allowable Practical Quantitation Limits (HAPQL limits) for several analytes. These include: Boron 6010D, Phosphorus 6010D, Beryllium 6020B, Silver 6020B, Tin 6020B, Total Organic Halides 9020B. All analytes
met statistical limits, unless otherwise detailed in the individual sections below. As instructed by the client, the data is reported.
The Chain of Custody requests “6020_METALS_ICPMS: GW 01” analysis. Service List “6020_METALS_ICPMS: GW 01” includes Thorium, and while TestAmerica Denver holds Washington State (WDOE) accreditation for method 6020B, Thorium is not on the accreditation certificate at this time. Please note that Thorium is on TestAmerica Denver's primary ORELAP certification, and TestAmerica Denver is
pursuing full WDOE accreditation for this element. As instructed by the client, the laboratory proceeded with the requested Thorium analyses by method 6020B.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
RECEIPT
The samples were received on 3/9/2018 9:55 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 1.8º C.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples B3HFP1 (280-107262-2) and B3H047 (280-107262-6) were analyzed for volatile organic compounds (GC-MS) in accordance
with EPA SW-846 Method 8260B. The samples were analyzed on 03/14/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SEMIVOLATILE ORGANIC COMPOUND (GC/MS SIM)
Sample B3HL11 (280-107262-1) was analyzed for Semivolatile Organic Compound (GC/MS SIM) in accordance with SW-846 8270D. The samples were prepared on 03/14/2018 and analyzed on 03/18/2018.
Benzo[a]anthracene, Chrysene and Fluoranthene were detected in method blank MB 280-407819/1-A at levels that were above the method
detection limit but below half the reporting limit. The values should be considered estimates, and have been flagged. If the associated
sample reported a result above the MDL and/or RL, the result has been flagged.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL METALS (ICP)
Samples B3HFP1 (280-107262-2), B3HFP4 (280-107262-3), B3HFN4 (280-107262-4) and B3HFN7 (280-107262-5) were analyzed for
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Case NarrativeClient: CH2M Hill Plateau Remediation Company TestAmerica Job ID: 280-107262-1Project/Site: S18-003/X18-005/W18-003/W18-002/S18-002 SDG: DN0332
Job ID: 280-107262-1 (Continued)
Laboratory: TestAmerica Denver (Continued)
Total Metals (ICP) in accordance with EPA SW846 6010D. The samples were prepared on 03/15/2018 and analyzed on 03/17/2018,
03/21/2018 and 03/22/2018.
Calcium, Magnesium and Potassium were detected in method blank MB 280-407758/1-A at levels that were above the method detection
limit but below half the reporting limit. The values should be considered estimates, and have been flagged. If the associated sample reported a result above the MDL and/or RL and the method blank concentration was greater than 5% of the sample concentration, the
result has been flagged.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
(280-107262-12), B3H4B0 (280-107262-13), B3H490 (280-107262-14) and B3H4B1 (280-107262-15) were analyzed for Total Metals (ICP/MS) in accordance with SW846 6020B. The samples were prepared on 03/15/2018 and analyzed on 03/16/2018 and 03/19/2018.
The Chain of Custody requests “6020_METALS_ICPMS: GW 01” analysis. Service List “6020_METALS_ICPMS: GW 01” includes Thorium, and while TestAmerica Denver holds Washington State (WDOE) accreditation for method 6020B, Thorium is not on the accreditation certificate at this time. Please note that Thorium is on TestAmerica Denver's primary ORELAP certification, and TestAmerica Denver is pursuing full WDOE accreditation for this element. As instructed by the client, the laboratory proceeded with the requested Thorium
analyses by method 6020B.
Strontium, Thallium and Manganese were detected in method blank MB 280-407757/1-A at levels that were above the method detection limit but below half the reporting limit. The values should be considered estimates, and have been flagged. If the associated sample reported a result above the MDL and/or RL and the method blank concentration was greater than 5% of the sample concentration, the
result has been flagged.
The accuracy and precision of Strontium in the MS/MSD performed on sample B3HFP1 (280-107262-2) in prep batch 280-407757 could not be reliably calculated due to the sample concentration reading greater than four times the spike amount. Control limits are not applicable and the MS/MSD results have been flagged “X”.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ALKALINITY
Samples B3HFP1 (280-107262-2) and B3H3R4 (280-107262-11) were analyzed for Alkalinity in accordance with SM20 2320B. The samples were analyzed on 03/15/2018 and 03/16/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL ORGANIC HALIDES
Samples B3HJ95 (280-107262-7), B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8 (280-107262-10) were analyzed for
total organic halides in accordance with EPA SW846 Method 9020B. The samples were analyzed on 04/02/2018.
It can be noted that, due to analyst oversight, the MS/MSD for batch 280-409938 was re-analyzed on sample B3HJ95 (280-107262-7), , and all spike parameters were within control limits: MS = 107%; MSD = 110%; RPD = 3% (control limits: MS/MSD 75-125%; RPD 20).
The following samples in this SDG are associated with this MS/MSD: B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8
(280-107262-10). Please note that only the first analysis for sample B3HJ95 (280-107262-7) +MS/MSD in batch 280-409937 is reported.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL ORGANIC CARBON
Samples B3HJ95 (280-107262-7), B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8 (280-107262-10) were analyzed for total organic carbon in accordance with EPA SW-846 Method 9060A. The samples were analyzed on 03/28/2018 and 04/03/2018.
Due to analyst oversight, CHPRC project sample specific MS/MSD was not performed for analysis batch 280-409524. MS/MSD was
performed in the batch, but not on a CHPRC sample. All spike parameters were withing control limits: Sample 280-107418-3: MS =
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Case NarrativeClient: CH2M Hill Plateau Remediation Company TestAmerica Job ID: 280-107262-1Project/Site: S18-003/X18-005/W18-003/W18-002/S18-002 SDG: DN0332
The following samples in this SDG are impacted: B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8 (280-107262-10).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
We certify that this data package is in compliance with the SOW, both technically and for completeness, including a full description of,
explanation of, and corrective actions for, any and all deviations, from either the analyses requested or the case narrative requested. Release of the data contained in this hard copy data package has been authorized by the Laboratory Analytical Manager or designee and
the laboratory’s client services representative as verified by their signature on this report.
Reviewed and approved:
Darlene Bandy
Project Manager
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Login Sample Receipt Checklist
Client: CH2M Hill Plateau Remediation Company Job Number: 280-107262-1
SDG Number: DN0332
Login Number: 107262
Question Answer Comment
Creator: Pottruff, Reed W
List Source: TestAmerica Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.
60 CPM
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded. 1.8 C
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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CH2MHill Plateau C.O.C.#
Remediation Company CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST S18-003-437 l?age 1 of 1
Collector: Ed"- t)NO"';"'$-Z, ContacURequester: Karen Water s - Hu s t ed Telephone No.: 509-376 -4 650 JCtlPRC
Project Title: CERCLA, MARCH 2 018 Logbook No.: HNF -N-50 6 - Cf /-7 J Ice Chest No.: /2i u}S-- r llf 7 Shipped To (Lab) TestArne rica De nver I Method of Shipment Commercial Carrier Bill ofLadin"g/Air Bill No.: 1'7J'1 ~73'1 '-feids Protocol CERCLA Priority: 30 Days Offsite Property No.: C,f I ?S~ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ** **Contains Radioact i ve Mater ial a t concentrat ions · t hat are N/ A not r e gula t ed f o r t r anspor tat i on p er 49 CFR / IATA Dangerous Goods Regula tions but are not releas abl e pe r DOE Order 4 58. l
-
Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative •- A -
,.
B3HL11 N WI Al\ U O LUI: 'il)'=t 4xl - L a G 8270 SVOA GCMS SIM : COMMON 7 / 40 Days Cool <=6C - - -
n 111 n rn 11111111 280-107262 Chain of Custody
D~J\'6 ~6 , \ i2..? ~-°1-l~
Relinquished~ 2":,,__/ ~ \'65? Received By: MAR O 8 2018 13~ Matrix .. ICHPRC - MAR O 8 20fR - - - - ---- = ~~~1.A.1'4--,..1=-ou.-._.,___::..._:_ ---=- S = Soil DS;;; Drum Solids
Print First and Last Name Signature '/Jate/Time Datemme SE = Sediment DL ;;; Drum Liquid
Relinquished By· ,~_,,_.,.,_....r,.n , , ~ / \~ Received By: ... ____ ______ ____ SO= Solid T ;;; Tissue
1~· -~-------- SL = Sludge WI = Wipe _ _ ate/Time Print First and Last Name Signature Datemme W =·Water L = Liquid
Recei~e~ B¼ f.,1 ,__ ~ N,.. ~ I 1W- -~-, ~ C°':5"5 o = O_il V = Vegetation - --- 1 K,.Q.~~ ~ 'h ~ V~ 1? i . A = Air X = Other
Date/Time Print First and Last Name Signature Date/Time
Relinquished By: Fe.cl £x,, Signature Print First and Last Name
Relinquished By: Received By:
Print First and Last Name Signature Datemme Print First and Last Name Signature Datemme
FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process): Disposed By: Date/Time:
DISPOSITION Printed On 2/26/2018 FSR ID = FSR58268 A-6004-842 (REV 3)
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CB2MBi11 Plateau C.O.C.#
Remediation Company CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST S18-003-194 Pagel of l
SAFNo.: S18 - 003 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71
Project Title: CERCLA, MARCH 2018 Logbook No.: HNF-N-506 CJ8 /s-:} ! lceChestNo.: (-jjj)- 74' / Shipped To (Lab) TestArnerica Denver II Method of Shipment Commercial Carrier Bill of Lading/Air Bill No.: ry,7 i t-]~{]~9 ~o~R Protocol CERCLA Priority: 30 Days Offsite Property No.: 01?-.f~ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****contains Radioactive Material at concentrations that are N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1
Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative
B3HFP1 N w 3-S ... ,o JO.;to lxSOO -mL G/P 6020_METALS_ICPMS: GW 01; 6 Months HN03 to pH <2
6010 METALS ICP: GW 06
B3HFP1 N w r 1X250-mL G/P 2320 ALKALINITY : COMMON 14 Days Cool <=6C
B3HFP1 N w Sx40-mL aGs* 8260 VOA GCMS: COMMON 14 Days HCl or H2S04
,l/ ~---to pH <2 / Cool <=6C
B3HFP4 y w s-0-,0 Jd~ lXS O 0-mL G/P 6020_METALS_ ICPMS: GW 01; 6 Months HN03 to pH <2 6010 METALS ICP: GW 06
Relinquish~ 3, ~--~.,, MAR n~ Received By: Troy Sa=-r- l,,.. /!;u,c,-/i tOS~ Matrix"
,. ' .• , rl,J'l./1 CHPRC '_/,,d"'f.._ • MAR. D B j1§/T1me s =Soil DS = Drum Solids
Print First and Last Name l Signature Date/Time Print First and Last Nam~ Signature
MAR n B ?f118 ? 11 (lt Received By: !=EDEX SO= Solid T = Tissue CHPRC , ,
SL= Sludge WI =Wipe Print First and Last Name Signature Date/Time Print First and Last Name §ignature Datemme
~fbZ w =Water L = Liquid
Refinquished By: F~ctE~ Rec~d B~ pc{f.y- a= - 3-~-tt aq~ 0 =Oil V = Vegetation l Q. C W:::i, A =Air X = Other
Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time
Relinquished By: Received-By:
Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time
FINAL SAMPLE I Disposal Method (e.Q., Return to customer, per lab procedure, used in process): DISPOSITION
I Disposed By: I Datemme:
Printed On 1/15/2018 FSR ID= FSR57113 A-60D4-842 (REV 3)
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.0CH2MHill Plateau C.O.C.#
CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST S18-003-193 Remediation Company
Page 1 of l
Collector: 1-anyRosane ~RC !) No"?:, "'Z-- Contact/Requester: Kar en Waters-Husted Telephone No.: 509 - 3 76- 4 65 0
SAF No.: S18-00 3 Sampling Origin: Ha n for d S i t e Purchase Order/Charge Code: 300 0 72
Project Title: CERCLA, MARCH 2 018 Logbook No.: HNF-N-5 06 qfJ l~s Ice Chest No.: GLu~-1({ J Shipped To (Lab) TestAmer ica Denver I Method of Shipment Commercial Carr i er Bill of Lading/Air Bill No.: '7 '7f '7 5'7?l1 L/(X?t> Protocol CERCLA Priority: 30 Days Offsite Property No.: q1?,S POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concent r ations t hat a r e N/A not regul a ted for tran sportation per 49 CFR / I ATA Dangerous Goods Regulat ions but are not relea sable p er DOE Order 45 8 .1
Sample No. Filter * Date Time NofType Cont.11iner . Sample Analysis Holding Time Preservative
B3HFN4 N w '5 ,'j-Jfd Ot:tJv; lxS OO -mL G/ P 6 020_METALS_ICPMS, GW 01; 6 Months HN03 to pH <2 6 010 METALS ICP: GW 0 6
B3HFN7 y w 3--g - i<cl oq~ lxSOO-mL G/ P 6020_ METALS_ICPMS : GW 01 ; 6 Months HN03 to p H <2 6 01 0 METALS ICP: GW 06
Relinquish~~ '-{ r:_ - A u 'R O 8 , ,n1g loss Received By: Troy Ba~_n,f L-· ~ Uft.D !'I 8 zn1a/0$5 . Matrix.. . :th'"?fl.e ....J~ ' PH-i -~ 1 · CHPI>~ l'l fl _/J~_'.i~- S = Soil OS= Drum Solids
Print First andLast Name Signature Date/Time Print First and LastName Signature Datemme SE S d. t DL D L" .d :;;; e 1men = rum 1qw
Relinquished By: Troye~onv. L· ~ 71118 . ·t.JO Received By: FEDEY. SO= Solid T = Tissue ------ -ce-11P-R"H-6 - 'P"'/\ MAR n 8 --- !1-j - - ------ - -------- - ---- SL = Sludge WJ = Wipe
Print First and Last Name Signature Date/Time Print First and Last Name Signal/Ke Date/Time W W t L L" "d , , ; a er = 1qu1
Relinquished By: 6?,cl tx Re~~f ott--l,\,r..P-- ~ ~~°' -1.f a1SS- o : O_il v = Vegetation
Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time A - Atr X - 0th er
Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time
FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process}: I Disposed By: I Date/Time:
DISPOSITION
Printed On 2/26/2018 FSR ID = FSR58267 A-6004-842 (REV 3)
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CB2MBi11 P1ateau C.O.C.#
CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST XlS-005-143 Remediation Company
Pagel of 1
COiiector. l:anyRosane
J)ru0~7v Contact/Requester: WATERS-HUSTED, K Telephone No.: 376 - 4650 1':HPRC
SAF No.: X18 - 005 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71 . Project Title: Groundwater Background Study, Logbook No.: HNF - N- 506 91 /S3 Ice Chest No.: f,-)LiJ)-7lf7 Shipped To {Lab} TestAmerica Denver I Method of Shipment Commercial Carrier Bill of Lading/Air Bill No.: '701 fJ S()Y, 400B Protocol SURV Priority: 30 Days Offsite Property No.: q(?)$ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS *Contains Radioactive Material at concentrations that are not be Batch with A, I, S, and W SAFs. regulated for transportation per 49 CFR/IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1.
Sample No. Filter " Date Time No/Type Contatiner Sample Analysis Holding Time Preservative B3H047 N w 3-ff ... /~ IOJ3
5x40-rnL aGs* 8260_VOA_GCMS: COMMON 14 Days HCl or H2SO4 to pH <2 /
Cool <=6C
Relinquis-~ Ji f<~ MAR D 8 2019 ,o,s Received By: "f; s rr;. • t?-~ rp5J Matrix* · IC.ti!'BI; GlNl-:4 rcite:~on ~ £,' ~ 1 MAR D 8 Z018 Ji S = Soil DS = Drum Solids Print First and Last Name Signature Date/Time Print First and Last Name- Signature Date/Time
SE = Sediment DL = Drum Liquid Relinquished By: 'rg(.~Rn L,., ~ MAR n 8 ')fl1R I ~l) 0 Received By: FEDEX - SO= Solid T =Tissue
Print First and Last Name 4 Signature Datemme Print First and Last Name Signature Date/Time SL= Sludge WI =Wipe W =Water .. L = Liquid
Relinquished By: ~e..clG:. Rec:;':l~{d Ve H-V\v{f- ~k ··1-ei -I$ 69.,-:, 0 =Oil V = Vegetation A =Air X = Other Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time
Relinquished By: Received By:
Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time
FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process): DISPOSITION
I Disposed By: I Date/Time:
Printed On 11/21/2017 FSR ID= FSR54035 A-6004-842 (REV 3)
SAFNo.: WlS - 003 Sampling Origin: Hanford Site Purchase Order/Charge Co~e: 3 o o o 11
Project Title: RCRA, MARCH 2018 Logbook No.: HNF-N-506 - C/'1-70 Ice Chest No.: {~W~- '74- / Shipped To (Lab) TestArnerica Denver I Method of Shipment Commercial carrier Bill of Lading/Air Bill No.: 'lf/ I J{ '51709 40l,'3 Protocol RCRA Priority: 30 Days Offsite Property No.: 0,f ?n POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concentrations that are N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1
Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative
B3HJ95 N w lx250-mL aG 9060 TOC: COMMON 28 Days HCl or H2S04
M ,RO 7 2018 l'i07 to pH <2 / Cool <=6C
B3HJD6 N w lxl-L aGs* 9020 TOX: COMMON 28 Days H2S04 to p H <2 / cool <=6C
B3HJD6 N w lx250-mL aG 9060_TOC: COMMON 28 Days HCl or H2S04 to pH <2 / cool <=6C
B3HJD7 N w lxl-L aGs* 9020 TOX: COMMON 28 Days H2SO4 to pH <2 / Cool <=6C
B3HJD7 N w l x250-mL aG 9060 TOC: COMMON 28 Days HCl or H2SO4 to pH <2 /
Cool <=6C B3HJD8 N w \ / ~,. lxl-L aGs* 9020 TOX: COMMON 28 Days H2SO4 to pH <2
/ Cool <=6C
RelinqyishedBy: (A~~ ~AR .· [[;oo Received By: SSU-f- MARO 7 1fl18t.S-o . Matrix* _ ~ 0 2 ,mt=--- - -----~~~ ______ __::....:.:....c:..:....=.. ·- S = Soll DS = Drum Solids
Print Pliiiiiz,~ Signature Date/Time Print First and Last Namf},. Date/Time SE = Sediment DL = Drum Liquid
Relinquished By: SSU-1 MAR O 8 2018 ro':;> MAR O 8 2018 1035 so= Solid T = Ti~sue . =-..:..=-----<=c.__ SL = Sludge WI = Wipe
re Date/Time Print First and Last Signature Date/Time W W t L L" .d = a er = 1qu1 Relinquished By: .....s1RCc;:,,e MAR O 8 2018 \~ Received By: FEDEX O = O!I V = Vegetation
. ---- A = Air X = Other Datemme Print First and Last Name ~1gnature Date/Time
Relinquished By: J:ed~ Ren~&JYc~1= ~ 'j BLt-,g 09'P Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time
FINAL SAMPLE I Disposal Method (e.g., Return to customer, per tab procedure, used in process): Disposed By: Date/Time: DISPOSITION
Printed On 1/15/2018 FSR ID = FSR57207 A-6004--842 (R~ 3)
SAF No.: W18-003 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71
Project Title: RCRA, MARCH 2018 Logbook No.: HNF-N-506. t!f'1- 7 0 Ice Chest No.: (A(fh- 7ll J Shipped To (Lab) TestAmerica Denver I Method of Shipment Commercial Carrier Bill of Lading/Air Bill No.: rJ0 f '7 ~-;7?{:f lf rf 11~
Protocol RCRA Priority: 30 Days Offsite Property No.: q[~5 POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concentrations that a re N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1
Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative
B3HJD8 N w ~ARO 7 20'
lx250-mL aG 9060 TOC: COMMON 28 Days HCl or H2SO4
9)~ to pH <2 / i l Cool <=6C
B3HJ95 N w J, ..J, lxl - L aGs* 9020 TOX: COMMON 28 Days H2SO4 to pH <2 / Cool <=6C
Relinquished By: fl/l-t-Cl£ MAR D-7 7ft"1 [50C Received By: 1~00 Matrix*
§fflfn;1 MAR O 7 7019 Prin~ast Name Signature Date/Time
S = Soil DS = Drum Solids Print First and L --;;------;;;- Signature Date/Time
SE = Sediment DL = Drum Liquid Relinquished By: SSU-1 MARO 8 2018 I~ Received By: ~~ G \-i CQ MAR O 8 2018 ro3S SO = Solid T = Tissue
Print First and Last Name /\ Sig,qatlJl'e Date/Time Print First anrf L~e · Signature Date/Time SL = Sludge WI = Wipe
Relinquished By: ~ 1~ifb.V y MAR O 8 20JB j ~ D() W == Water L = Liquid
Received By: FEOEX 0 == Oil V = Vegetation
Print First and Last NameV -- Signature Datemme Print First and Last Name J,ignature Date/Time A =Air X = Other
SAF No.: W18-002 Sampling Origin: Hanford Site Purchase Order/Charge Code: 300 071
Project Title: RCRA, February 2 018 Logbook No.: HNF- N- 506 - Ci 'i/q
Shipped To (Lab)I TestAmer ica Denve r Method of Shipment Commercial Carrier 8 Protocol RCRA Priority: 30 Days O!fsite Property No.:
POSSIBLE SAMPLE HAZARDS/REMARK ****Contains Radioactive Mater ial at c oncentr at i ons tha t are not regulat~d for transportation per 4 9 CFR / IATA Dangerou s Goods Regulations but are not releasable per DOE Order 458. 1
Sample No. I Filter 1 * Date Time I No/Type Container Sample Analysis
B3H3R4 N .w 1-3-i· L ~ IQ · 1x125-rnL r.; j p I 2320 ALKALINITY: GW 01 ,
-Relinqu~-"' Ru·
--..--.. ' .) M4R O 8 2818 Received By: Trg~g~~ l:~ MAR O 8 2018 l:?47f'. 'I. Jt.-wPRC I 1:26 ':I ,
Print First and Last No Signature Date/Time Print First and Last Name ___/ Signature Date/Time
Relinquished BYi-roy Bac~Jlbj__ l.• ~ MAR n B 1018 b "160 Received By: FEDEX CHPli'C
Print First and Last Name Signature Datemme Print First and Last Name " Signature Date/Time
Relinquished By: Fe.cl Ex R~aB~H-rvZf ,Lil,~) ;-v.- 2-'i-ar (trs:s Print First and Last Name Signature Date/Time Print Fil'st and Last Name Signature Date/Time
Relinquished By: Received By:
Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time
FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process): DISPOSITION
I Disposed By:
Printed On 1/4/2018 FSR ID= FSR55848
Holding Time Preservative
14 - Da ys Cool <=6C
Matrix" s =Soil DS = Drum Solids SE = Sediment DL = Drum Liquid SO= Solid T =Tissue SL= Sludge WI =Wipe W =Water L = Liquid 0 =Oil V = Vegetation A =Air X = Other
I Datemme:
A-6004-842 (REV 3)
Page 14 of 44
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Remediation Company CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST SlS-002-020 Page 1 of 1
SAF No.: S18-002 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71.
Project Title: Sitewide Surv, February 2018 Logbook No.: HNF-N-'-506-',tj /11 Ice Chest No.: H t"S--'7 ll (-/ Shipped To (Lab) TestAmerica Denver I Method of Shipment commercial carrier Bill of L.adingfAir Bill No.: r](] f '7 '373 q £.IO[p i Protocol SURV Priority: 30 Days Offsite Property No.: 9{~5 POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concentrations that are N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1
Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative B3H489 N - W ~-%-J!? uori lx500 -mL G/P 6020_METALS_ICPMS: Chr-omium (1) 6 Months HNO3 to pH <=2
B3H4B0 y w 3-8--J ?" I \0Cj lxS00 - mL G/P 6020_METALS_ICPMS: Chromium {1) 6 Months HNO3 to pH <2
- ---~ - -Relinquisliea u:,. (:~"'- / J MAR O 8 1018 t ""2.-0~ Received By: Tt~~~ 6 ~ MAR U 8 2018 l ?It( Matrix*
PrintFirstandLastNJme/ Signature Dateflime Print First and Last Na---j(ff Signature Date/Time s =Soil DS = Drum Solids
~ SE = Sediment DL = Drum Liquid
Relinquished By: Troy Ba~ /::'j {_ ~ MAR O 8 ?01R llfoO Received BfEOE)C SO= Solid T =Tissue CHPRC ' , • SL= Sludge WI =Wipe
Print First and Last Name Signature Datemme Print First and Last Name - Signature Date/Time W =Water L = Liquid
SAF No.: S18 - 0 02 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71
Project Tit.le: Sitewi de s u rv, Feb ruary 2 018 Logbook No.: HNF- N- 5 06 - "f'7 / l) Ice Chest No.: GLO~~rJlf } Shipped To (Lab} Test Arnerica Denver I Method of Shipment commercial Carrier Bill of Lading/Air Bill No.: 'l '7 f '{ 511'1 t.l tfo5 Protocol SURV Priority: 30 Days Offsite Property No.: 0113~ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS **** Cont a i n s Radioactive Mat erial at concen trations that are N/ A not r egul ated for transportation per 49 CFR / IATA Dange rous Goods Regul ations but are not r e l easabl e per DOE Order 458.1
Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative B3H4 90 N . w 3-!?1 i i /oq· lx5 00 -mL G/P 6~2 0_METALS_ICPMS: Chromium (1 ) 6-Months HNO3 to pH <2 B3H4Bl y w ~-8-l i° 1104 l x S O O -mL G/P 602 0_METALS_ I CPMS: Chromium (1) 6 Months HN03 to p H <2
,.,--
Relinquished By. ~-e~---;---MAR J! 2018 J.;ur<f Received Bl/ir~~~~~ b~ MAR o 81018 l:Mf.{ - --- - - ----+--=.__-=e'--- S- ig_n_a_tu_re____ Date/Time Print First and Last Na:I Signature Dateffime SE S d. t DL D L" "d = e ,men = rum 1qU1 Relinquished By: r~:~~~ L· ~ MAR O B ?01R 111 p() Received BYfEDEX SO: Solid T : Tissue
Print First and Last Name Signature Date/Time Print First-and Last Name Signature Date/Time WSL - WSludt ge WL 1 - Wil_ IP~d _ = a er = 1qw Re~iv.Q,~ &tt--r,$ ~l 1¥--- s-'1-t.g c,q-s5 0 = O_il V = Vegetation .! · --- ~ ---~ - ~ ~ - ~~ A =Air X =Other Print First and Last Name Signature Date/Time
S =Soil
Relinquished By: FedEx Print First and Last Name Signature Date/Time
Matrix* DS = Drum Solids
Relinquished By: Recefved By:
Print First and Last Name Signature Date/Time I Print First and Last Name Signature Date/Time
FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process): DJS POSITION
I Disposed By: I Datemme:
Printed On 12/13/2017 FSR ID = FSR55331 A-6004-842 (REV 3)
Page 16 of 44 4/9/2018
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