n I II I II II I III I I II I I II I I III · FROM: SSFL Analytical Chemistry,W WORT LA-105/t/90 REFERENCE: 1,B 90 p 97; NO 1251, pages 161 - 174 G it u ~7 SAMPLE 1Nr0RMAT10N FOR
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CERTIFIED - RETURN RECEIPT REQUESTED
12 October 1992 In reply refer to 92RC '
Califcrria EnvironmentalProtection Agenc yDepart ment of Toxic Substances Contro l1405 North San Femnando Roa dBurbank, Ca 9'501
Attention Maria Fabell a
Subject Soils analysis iron? area ' Thermal Treatment Fa flit 38 and 199 2
Rockwe ll international Corporation, Rocketdyne Division isIieieLY submiltiny information requestedduring teleph one conversation betNe- n Environmental Protection Stitt an Maria Fabella of Cal EPA
Department of Toxic Substances C>ntrol .
In the telephone conversation, Maria hula la asked for analytical iepons tram soil samples taken at theArea I Thermal Treatment faci lity in 1902 and 1990 . The analytical reports for soil samples taken i n1982 were included in the Revised C osure plan previously submitted . Analytical report . for soi lsamples taken in 1990 are attached .
ROCKVvLLL INTERNATIONAL CORPORATIONRocketdyne Divisio n
M F Jansen, ManagerWater and %%aste Programs
n I I II I II II I III I I II I I II I I IIIBNA03136397
HDMSe00042520
[-')Hr '30 1334 1+ L ;__-EP P . c
CHEMICAL ANALYSI SR1r POR'i'
('i'rtio 22) prior tD allltw5i-AL3R°-'.'1 ATTC .S t
.;L !z 'torrr drt( otcd.2Trace )
T
543-inn FHONE : 392-5319opr/o ouP :
ChemisterManagltocketdYnc SSFL Analytical Cnemistrv RocketdY1te SSFL Analyt cs1 Chemistr y
I III II II II I III I I II I I I IBNA0313639 8
af1' Flviroi: mental f)ockWcll Internatiana 9,t
vDiolJ VT:=kRecFROM: SSFL Analytical Chemistry,W WORT LA-105/t/90REFERENCE : 1,B 90 p 97 ; NO 1251, pages 161 - 17 4
ui tG
~ 7
SAMPLE 1Nr0RMAT10N FOR 940441 2
Southslt[A Pad 1, distance = 1 too tlSi oi ,on :Sa*tie DrteorptRegp . . Htrr : Beatrice Hephnr t
ta 1KeRe4ueated Analyain :Received : 04/23/90 at 10:15;CO
SO 01 le Time' 9 : ?8_ 00SemSampler: M . HajvereonSamplad : 04/23/90
Sampler 10 MH4 : D423 p
61Ak, LEVEL
ANALYTE RESULT LIT CONTAMINATE METHODISU.IC E---------------- -
-------- ---------- -----------
AtLYmony *** ND<0 .0I c ,g/kg DNA 6010, SW-b4 6SR-84 G
Arsowt scar 0 .16 mg/kg UNA 7060,
6**sriuB
55 sg/ug DNA 7060, SW-6 4ma
Bcryiliua 0 .064 mS/kB DNA 6010, 5G-84 6'
**sC d i 0 .69 mE/ktS DNA -84 46010, SF6uma m
Chromium *** 21 mi/kE UNA 6010, SG-8 4
C b lt $ * 1 .2 mg/kg DNA 6010, SF-64 6o a
*** 917 m~1/kx DNA 6010, sa-R4 aCopperLPAii **'A .22 mg/kg DNA 6010, N-84 6
W 9cur ***M ND<0.042 ®AJkA DNA -3 47470, S
-Cyernum *bdl ID<0 : :53 m8/tie nNA 84 6olo . ,; W
esio yNickel *** 3.2 mglks DNA b0l0, sV-3s 5
W- 6l l 4 .Z ND<0 .57 mg/kg DNA 3 4Colo, Sec u mti e
Silver xs# ND<0 .04 ag/kg DNA E010, Si-B46-
Tha'1ium >t4 ND(O .C4 mgtlg DNA 346folo, 9VW 846
adiua xt *V 0 .91 tglkg DNA -6010, San
Zinc sal 90 ms/kg DNA 6010, SW-846
------------- ---------- -------------------- -------- ----------- -------- -
SNYC'6I :ATICN : DNA ;Area I Burn Pad for 1CRA Fe_rt 9 Permit )
SPECIAL NOTES : B. Kephart F.nv . S :g . in charoo of DrnJecr . Der.rr. rain :uaoff cor.,tm, No
etated limits . WET extract i,riur t, anaiy .~a : .
C0!g*1ENTS:*** ForiAformatica oniy . 1amp' a Was ex tracted p .r the h,V Etrnctior vrocedur e
3) ( = Less thinL) ,R E ; y .5 . = Not StatedK1,p1 T4) > Greater than 5) DNA = sops not=7) 4ss - Non-certified result for indication purposes on ly
APPROVED : -
R
HDMSe0004252`1
riA F-5 'SD 13:3= I« LASER P. S
CHEMICAL ANAT .VSI SREPORT
y• 543-000 PHONE : 592-5314RUU .YG* Enviraun_utal Unit az-1 Ruckwcl1 Internttienal, 2/539-169, ext . 9R21
v .yue DRocke: dl Chemistry 1
fiEFERFUCE : LB 90 1, 97, FB125:, Paget 161-,SSpL nalytlea REPORT DATE: 05/25/90F170M :
=
SMYLL .FPJkMAT1C' FUR i60147 1
sample Descrptiont soil, Bestaide pexi 1, distance = 3 Fee t
Refluester :- Beatrice KephartMetaiei;equeeted Analyel s
Received: 04/23/90 at 10,16:004ff0 20S Sample Time : 9!37:00
Sampler : .M . Halverfaa nSampled : 04/23/90
19Sampler ILO : 04?
)W . LEVE L
AN ALIiTE RESULT UNIT CONTAMINATE M;:1MU6/SOURCL
--------------- ----------- - ------ -----------
Sw-846------NW 01 mg/kg D4A E010,
-Antimony -k DNA 04 67063, $W
t**i 0 .22 m$/ g w-846Argen ctC
38 mt/km DNA 7060, sW-846Dariue
** *yIiI 0.11 mg/kg DNA 6010, $SW-8 6umpwr
=*_dmi 0_37 mg/kg DNA 4bul0,-8 6umCa
s**iCh 0.82 mg/kg DNA 4G010, SWSW-846ruu um
lt :YxbCt_5 me/ka:t DNA 6010,
W-846aoc e *** 3 .6 a9,/kg DNA 6010, S
W 94 6opp rd :u 1. 4 11 g,/kg DNA -6ulu, S
46Lea
mercury ***
lybdenum 9**M
ND<0.043ND<0.63 nR /ka Dora
DNA1470, SW- 86010 , sw-64 6
W-84 6ol ** *Nick 0.73 ag /kg DPA 6010, S
W-8466eium s:*l
NDt0 .S5 agAg DNA 010, S
6W-ense*4' *e ND<O .U4 m8/kg DNA 0 4G010, B
6.3i1vm T=ll iTb NArn .04 mg/kx DNA b01C, SW-8 4
W-84 6uad *1* 0 .47 mg/l+g DNA 5010 , S
Vana ium
Z;nc ssr 37 mg/kg DNA suit), sW-846
-------------------- ------ -
SP)rt;ifll:ATIOIQ : DNA {Area I Burn Pall t . RCRA P art 6 Permit l
SPECIAL N0 723 : 9. Kephart Snv. Eng. Licl.cr'e of project, Deter. rni r
ml).4 ) = Oteator than 5 ) oNA _ Does nu
? sa* = Non-certified result Yor indication puryases only
-, . . . . . rr :c tam' N o
stated liaite , WET Nx1rAr r prior to xna ya's .
C01 :MENTS ; *** Por informatiob only. Sample ~aa e!tracted }per the 6E2 °_xtract Procedure
(Title 22) Prior to analYsisj A&SREVIA4I~t+9;
?} NO I) TH =Trace done dctcoted 3y c ❑ I .-- n thanNot Statod
.L
APPROVED : MSIGNED
Chemist-- flanvgarAocltctdyne SSFL Analytical Chamiatry Rt,,l .tdyue 92FL Analytical Cbemiatr y
I II II II II I III II IBNA03136399
U
HDMSe00042522
3S 1» ASER P 43+ • _1i MAY c- 9C
CHEMICAL ANALYSI SRE POEt•1'
Log Number900441 4
l --9nta Unit DR"/CROUP : 54S-000 PHONE : 992-5314t:' .rU :1
FEOM: SSFL Analytical Dhcmintry, RocketdYne Div . Roekveil lntcrnational , 0/539-169, ext 5527
25 05 / /REFERENCE; La 9u p 91 ; N8 1251, pages 161-174 REPORT DATE
: 0
SAMPLE INFORMATION FOR 900441 .4
SAmpie neerrption: Soil. Nurtbbidt find 1, disttnte a 1 Foot
Jequctter : Beatrioe Aaphart
Requested Analysis : krti,tl e
Received: 04/23/ 90 at 10 :15100le Tina : 9' 29700
Sampler : M- 9a1ver9nn
Samuled 04/23/40
Sampler IDA : 042300!1803 Samp
ANALYTE EESULf UN:TMAX. LEVELCONTIMINATh MtL1l00/SOU &CS
--------------
-------- ------------- -AntimonT lax ND<D 01 ask ;, DNA 6u1U 5w-a46
Aratnic *** 0 .30 mg/kg DNA 7000, Or 8-1 6
barium *x : 21 mx/kK DNA '7060, sK-84 6
I)eryllium *'~* 0.021 m¢/kg DNA 6010, 3W-84C•
Cadmium 0 .13 mR/ka DNA 6010, SW-84 6
Chromium tart 0.15 mg/kg DNA 6010, 9W-846
Cobalt **s 1.2 me/kg DNA 601 0 , SW-84 6
Copper set 0 .62 mg/kg DNA 6010, SW-84 G
,Lead x** 3-7 mg/kg DNA 6010, SW-84 6
Mercury 4*~ 9.1 mg/kg DNA "1 470, SW-84 C
Molybdenum *U Kt<0 .53 mg/kx DNA 6010, SW-84 6
Nickel •tt 0.46 m3/k6 DNA €010 , SW-84 0
Selenium t** ND<0 .4fi Wks DNA 6010, SW-84 6
Si1,tr •i++ NDt0 .04 mg/kg DNA 6010 , SW-64 6
Thxl! ium **x ND'rO_oa ms/kg DNA 6010, SW-84 6
canedium *** C .e& mg/kg DNA 6010, SW-84 C
Zinc *** 6 .3 mg/kg DNA 6010, sw-84 6
----- --------- --- -
SPECIFICATION! DNA (ar-a I Rnrn Paid for- $CRA Fmi-t 0 Permit )
SPECIAL NOTES : B. Kephart Env. Erg . in charge of project . Ceter . ra runoff Contain . No
stated Haas . WET extinct prior t o
COMMENTS : {** For information onl :' . Sample uax extracted ,n,-.r HET Fs :'a4taur~ Prottdurt
; T1t1e 22 ) prin^ Ln anhlykis .s sPis1 E~":F.i71bNS ►
[4) ) TR Trace ND = None detected 3) t Less ch,u ,
) > = Greater than 3 ; DNA x Unna not apply 0) N .S . Sot Statcd
ax4 = Non- . :rrtilied result fuc itndication parpoaee onl y
1 3ICNF,D : ~ iC1.~ rn :'APpBn
Manager Chemist3ocketa~ne '_-PL Anal ; ti es! Chemistry Rocketdyae S.4FT. A,wlyti- .1 Chemistry
I II I IIII II III II IIIII II 111 1BNA03136400
HDMSe00042523
,no,,, ?S 4n 17 :'an I* L=SERP . 5
CHEMICAL ANALYSI SREPOT 't'
Log Number0001416
r- ST f,' T : C L
Manager ' e5eniatRcct Q.tdyne 4SFL Analytical Chtm : .strti Ru<:4crtQfn4 SSFL Analytical t'hamietry
I I II I IIIII I III III I III iBNA0313640 1
To: Environmental Unit DEPT/GROUP :FROM; SSFL Analytic'.l chemistry , Rockctd-n* Div .REFERENCE : Lb 90 p 97 ; NB 1251, pages 161-174
543-000 PHONE : 392-531 4Roclac11 International, D/09-169' ext. 592 7
k& 't)NT DATE : 05/25/9 0
SAMP1E INFORMATION FOR ?004413
Sample 0 Sc: rpiion: Sc1l, Norms da Pad 2, d1 tante a I Foo t
Bcquester3 Beatrice KeDliarLReQUeaLed Anal' 21nt $.ta 1 4
Peocivod 04/23190 at 0 .15 :0 03amplcr : a, Halverson Sampicr ID4 : 0423901'4104Saeplea : 04/23/90
Sau1r Tiae: 9 :32tt O
!tAX LEVE L
ANALYTE RESULT UVIT CONTAMINATE METHOD/SOURC E------------------------ ---------
--
------ -
Antimony *** NDx0 .01 mglkg DNA 6010 , SW-846AreeCic a;* 0.46 mg/k ; DNA 7050 , SW-846
Darium *** 30 mg/kg DNA 7060, 3A-84C
Roryllium I T 0 .042 arA t; DNA 6010, SW-$36
Cadmium *** 0.40 mg/kg DNA 60X0, SW-846
ebroainm *** 2 .1 mg/l,g DNA 6010 , SW-346
Cobalt *1* 1 .1 m6'kg DNA "6010, 3W-$4G
Copper ss* 5 .2 a-/kg DNA 5010, sx-84 6
Lead *** 3-5 mg/Lg DNA 6010, SW-846
Morciiry xxz 45 mglkg DNA 747D , SW-84 6
Molybdenum **= NDtQ .53 me/kg DNA 6010, SW-84 6
Nickel ;** 3 .5 Mg/kg DNA 6010, yk-84 6
3elvaium *44 ROc0 .46 ng/kg DNA 6010 SW-846Silver ***Thal1lum **4
ND<0.01 0ND<O .04
mx/" qaS/'k6
DNADNA
6010 , 9W-84 66010, SW-$4b
t'anadina x** 1,0 aalkY DNA 6010 , SW-84 6Zzac * c4 42 m6/lg DNA 6010, 3W-D40
SPECIAL NOTES : B . Kephart Loy. Eng. in chncg.- ~f project . Deter . rain rur.off contain . No
atatnd 1initn WET estrAct prior to analynin .
CO D4ENIS: *=Y For Information Only. 3amyle was extracted per the WIT Procedure (Title 22)uriur to ana1y5t1s .
AnDREVIATION31) TV - Trace 2) ND T Nona detactett --- 3) t • Lesy than
4) ) = Grater than E : DNA ~ Dees notA001r 6) N .S . = Nr,r. SrAted
7) 44* = Non-certifled -exult rnr lndieat lon purpoaec onl y
--------------------------- - ---------DNA (Area I Burn Fad for RCRA Part k Permit )
Ak+NN()VED•t,
HDMSe00042524
Mfli 15 '90 13•36 It Li;SER P.
CHEMICAL ANALYST S
REPbRT
TO : Envirunmrnlnl [ r, t. DEPT/O,.DUF : 543 000 FHC~F' 3y''-5~14
. Rockwell Intert ,xi- -u' lCi vokoclet ml Chcmictry 0 2?G . exit& ~ ': io t 161-1
BEFEWC.T . TR 50 p 91 ; NE 12$i,, 15y9SBFL Analytica p 1 Uli!P20H 7 4
52,NPLE INFOFMATION FOA 900441 6
Sample Tlcscrpticn; Sc_1, Edcteice pad 1, diFtaacc - 1 Foot
gamester: Beatrice Ke~ifhar L
fle ueated Aaaly5is : Clctat s
to e4ved: 04/23/90 htIO•t5 :00
42290MH05 Sample Tier: 9 :34 :00
Sampler : N. 11alversonled' D4/23/9 0S
Saapier 1U ; : 0
auP
MAX LEVPL
ANALYTE RMULT UNIT CONT .414INATE xYTNOD/StK --- -__---_
i *t`* hD<0.01 ---
mglkg DNA 6010 ,
7060
SW-P., 6
94-84 6mon YAnt:ss C .45 mNe DNA .
60 SW-84 6Ar8en1 -
Barium *** 2506 30
mSlk 6mY/kX
DNADNA
70 ,6010 . SW-' 3
Beryllium**~
.C .46 Wks L)NA 6010 ,
06SWI-R4 6BW-64 6Cadmium
S=* 1,! mg/kg DNA ,01W-5i 6Chromiu m
Co`t,Ult *** 1 .4 mg/kg DM 6010 ,6010,
SSW-84 6
zsx 3 .0 mg,kg DNA06 3W-81 FCoppe r
Lead *** 3 . 1it
mg/ksm5/kg
DNADNA
,0 17410, Bc"-64 6
mercury VS 3NDEO g/ke' UNA 6010, SW-84 8
-KolyLt1euums : :
.2 .4 m$/k& DNA 6010 ,
060
84 6SWSW-84 6Nickel
*+* ND<0.46 mSl g DNA ,1W-84 6selenium
x=i 0 .46 mJ'kg DNA 6010 . $SW-846Silver
m ** *ll 0<0 .044 mg/kg DNA 5010 ,
60 0 SW-84 6i uThaxc sd 1 .1 mgY1~Y DNA 1 ,
00 SW-846iumVanaZinc t** 25 ng/k$ DNA ,6 1
(Title 22) prior to analysis, A9RAEVla?704 8
2) ND = Nonc detoat©d 3)1) TB - TraGc 6) V4) ) Greater r:han 5) DNA = Duns not MPDI Y
7) «** _ Non-ccrtif_ed result for indication purposes onl y
SPECIFICATION : DNA (Area I Burn Pad for &CSA fart B Permit);ain uneiP Contain . No
IAL W SPEC S! B . Koph*rt Y. Ens, in charge nr prnjr,a. Deter .
Stated limits. WET extract prior to analysis.
gxnpl c uns extracted j r leLice WET extraction ?roeedureCUDLKhN•fS : __* 5'Or !nlOrnation Only .
- - - -------------------- --------
APPROVED : +
Recketdyno SSFL Annlyt ic .=1 r.~,r,*1yt,•y
ST ON FD .* _
= 1X++y Libnu
3 . Not 9tatea
Chemis t8ockttdyne SSI"L Analytical Chcmirtry
I I II I II II 0I 0III I I I I 11 1BNA03136402
HDMSe00042525
r1AY 25 '90 13:37 I* LRSER P,;
CHEMICAL ANALYSXSL C)IR-
Log Number900441 T
TO' Environmental Unit DEt'T /GPOUP : 543-0G0 PHONE! 392-521 4
REFERENCE : LB 90 P UI; ND 1251, pcLgco 1G1 -174 RE:PO1L DATT- 05/25,'4 0
SAMPLE INFORMATION POR 900441 79Amyle D. •rption- Sail, Wectaido pud 2, diatanoc = 1 Foo t
Requester: Beatrice Kephar tRequested Aaalyzia: M.tala
Received: 04/20/90 at 10 :15 :00Sampler!. M . HalvvraonOemnled: 04/23/90
Samplcr ID8 : O423UOME06 Sample Time : 9 :36 :00
4NALYTE RESULT UNITMAT . LEVELCONTA.MII ATE NETHOD/SOURCE
------ ----- -----------------
Antimony 44* NO<8 .U1 mg/kg DNA 8010 . SW-846A. ocnie *** 0.44 mg/kg DNA 7060, SW-81 6Rarium *4* 29 mg/kg DNA 7060, SW-84 6Beryllium **1 0.062 mg/ke DN A 6010, SW- 9 '1 6Cadmium *** 0 .4 .4 as/kg DNA 6010, 3W-84 6Chromium *** 0 .68 mg/kg DNA c010, $N-d1 6Cobalt 4** 1 .6 mg/kg DNA 6010 . SW-84 0copper*** 2 .7 mg/kg DNA h710, SW-H .1 61yad $as
7
mglk : DNA 0010, SW-R 4Mtresry 4*4 Nn<0 .D4 mg/kg DNA '?17O, SW-14 iMClybdeaum 44* 440, 53 mg/kf DNA 6010, SW-bo aNickel *** 1 .9 mg/kg UNA 6010 , S';-61 3Selenium *44 ND<0 .6b mglkt DNA 60ti1, gW-A4 ASilver *** sn(0 .04 mg/kg DNA SUJU , SW-846Thallium s- ND<0 .04 mo/k>; DNA 8010, SW-84 6Vanadium **4 RD<0 .51 mg/k$ DNA 6010, SW-81 6Zinc i*s 21 mg/kg DNA 0010, SW-R4 8
------------------------ -------------------- -------- ----------- --------- -SPECIF$4'ATION : DNA CArea I Burn Pad for RCAA Part B Permit }SPECIAL NOTES . S . Kephart . Rnv. Fng. In charge of project . Deter . rain runoff canter .
stated limits . Wtl' extract prior to analysis .C0MMENT3 : ***For Information Orly. SAmpie eras extracted per the WET extracticn procodarc
(Title 22) prior to analy*ia .* ANRRF.VIATIONS *
11 T8 =Trace 2) ND Nona dctCeted 37 < = Leas than4) = Greater then S) DNA Does not apply 6) 5 .3 . = Not Stated7) 44* = Non-certified resulr for indication purposee only
APPROVED :- llaa1ager 'Chemist
aoeketdyae 3SFL Analytical Ct,.-eictry Rockotd'-e SSPL Analytical Chcmistry
I I II I II II I III I I I I II II 0 I RBNA0313640 3
PEON : OSPL Anzlyti' 11 Chemistry , Roct8tdyno Div . Rockwelllntc:motionci, D!530 1C1, ext. 582 7
fSIGN*D :
HDMSe00042526
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