n I II I II II I III I I II I I II I I III · FROM: SSFL Analytical Chemistry,W WORT LA-105/t/90 REFERENCE: 1,B 90 p 97; NO 1251, pages 161 - 174 G it u ~7 SAMPLE 1Nr0RMAT10N FOR

CERTIFIED - RETURN RECEIPT REQUESTED

12 October 1992 In reply refer to 92RC '

Califcrria EnvironmentalProtection Agenc yDepart ment of Toxic Substances Contro l1405 North San Femnando Roa dBurbank, Ca 9'501

Attention Maria Fabell a

Subject Soils analysis iron? area ' Thermal Treatment Fa flit 38 and 199 2

Rockwe ll international Corporation, Rocketdyne Division isIieieLY submiltiny information requestedduring teleph one conversation betNe- n Environmental Protection Stitt an Maria Fabella of Cal EPA

Department of Toxic Substances C>ntrol .

In the telephone conversation, Maria hula la asked for analytical iepons tram soil samples taken at theArea I Thermal Treatment faci lity in 1902 and 1990 . The analytical reports for soil samples taken i n1982 were included in the Revised C osure plan previously submitted . Analytical report . for soi lsamples taken in 1990 are attached .

ROCKVvLLL INTERNATIONAL CORPORATIONRocketdyne Divisio n

M F Jansen, ManagerWater and %%aste Programs

n I I II I II II I III I I II I I II I I IIIBNA03136397

HDMSe00042520

[-')Hr '30 1334 1+ L ;__-EP P . c

CHEMICAL ANALYSI SR1r POR'i'

('i'rtio 22) prior tD allltw5i-AL3R°-'.'1 ATTC .S t

.;L !z 'torrr drt( otcd.2Trace )

T

543-inn FHONE : 392-5319opr/o ouP :

ChemisterManagltocketdYnc SSFL Analytical Cnemistrv RocketdY1te SSFL Analyt cs1 Chemistr y

I III II II II I III I I II I I I IBNA0313639 8

af1' Flviroi: mental f)ockWcll Internatiana 9,t

vDiolJ VT:=kRecFROM: SSFL Analytical Chemistry,W WORT LA-105/t/90REFERENCE : 1,B 90 p 97 ; NO 1251, pages 161 - 17 4

ui tG

~ 7

SAMPLE 1Nr0RMAT10N FOR 940441 2

Southslt[A Pad 1, distance = 1 too tlSi oi ,on :Sa*tie DrteorptRegp . . Htrr : Beatrice Hephnr t

ta 1KeRe4ueated Analyain :Received : 04/23/90 at 10:15;CO

SO 01 le Time' 9 : ?8_ 00SemSampler: M . HajvereonSamplad : 04/23/90

Sampler 10 MH4 : D423 p

61Ak, LEVEL

ANALYTE RESULT LIT CONTAMINATE METHODISU.IC E---------------- -

-------- ---------- -----------

AtLYmony *** ND<0 .0I c ,g/kg DNA 6010, SW-b4 6SR-84 G

Arsowt scar 0 .16 mg/kg UNA 7060,

6**sriuB

55 sg/ug DNA 7060, SW-6 4ma

Bcryiliua 0 .064 mS/kB DNA 6010, 5G-84 6'

**sC d i 0 .69 mE/ktS DNA -84 46010, SF6uma m

Chromium *** 21 mi/kE UNA 6010, SG-8 4

C b lt $ * 1 .2 mg/kg DNA 6010, SF-64 6o a

*** 917 m~1/kx DNA 6010, sa-R4 aCopperLPAii **'A .22 mg/kg DNA 6010, N-84 6

W 9cur ***M ND<0.042 ®AJkA DNA -3 47470, S

-Cyernum *bdl ID<0 : :53 m8/tie nNA 84 6olo . ,; W

esio yNickel *** 3.2 mglks DNA b0l0, sV-3s 5

W- 6l l 4 .Z ND<0 .57 mg/kg DNA 3 4Colo, Sec u mti e

Silver xs# ND<0 .04 ag/kg DNA E010, Si-B46-

Tha'1ium >t4 ND(O .C4 mgtlg DNA 346folo, 9VW 846

adiua xt *V 0 .91 tglkg DNA -6010, San

Zinc sal 90 ms/kg DNA 6010, SW-846

------------- ---------- -------------------- -------- ----------- -------- -

SNYC'6I :ATICN : DNA ;Area I Burn Pad for 1CRA Fe_rt 9 Permit )

SPECIAL NOTES : B. Kephart F.nv . S :g . in charoo of DrnJecr . Der.rr. rain :uaoff cor.,tm, No

etated limits . WET extract i,riur t, anaiy .~a : .

C0!g*1ENTS:*** ForiAformatica oniy . 1amp' a Was ex tracted p .r the h,V Etrnctior vrocedur e

3) ( = Less thinL) ,R E ; y .5 . = Not StatedK1,p1 T4) > Greater than 5) DNA = sops not=7) 4ss - Non-certified result for indication purposes on ly

APPROVED : -

R

HDMSe0004252`1

riA F-5 'SD 13:3= I« LASER P. S

CHEMICAL ANAT .VSI SREPORT

y• 543-000 PHONE : 592-5314RUU .YG* Enviraun_utal Unit az-1 Ruckwcl1 Internttienal, 2/539-169, ext . 9R21

v .yue DRocke: dl Chemistry 1

fiEFERFUCE : LB 90 1, 97, FB125:, Paget 161-,SSpL nalytlea REPORT DATE: 05/25/90F170M :

=

SMYLL .FPJkMAT1C' FUR i60147 1

sample Descrptiont soil, Bestaide pexi 1, distance = 3 Fee t

Refluester :- Beatrice KephartMetaiei;equeeted Analyel s

Received: 04/23/90 at 10,16:004ff0 20S Sample Time : 9!37:00

Sampler : .M . Halverfaa nSampled : 04/23/90

19Sampler ILO : 04?

)W . LEVE L

AN ALIiTE RESULT UNIT CONTAMINATE M;:1MU6/SOURCL

--------------- ----------- - ------ -----------

Sw-846------NW 01 mg/kg D4A E010,

-Antimony -k DNA 04 67063, $W

t**i 0 .22 m$/ g w-846Argen ctC

38 mt/km DNA 7060, sW-846Dariue

** *yIiI 0.11 mg/kg DNA 6010, $SW-8 6umpwr

=*_dmi 0_37 mg/kg DNA 4bul0,-8 6umCa

s**iCh 0.82 mg/kg DNA 4G010, SWSW-846ruu um

lt :YxbCt_5 me/ka:t DNA 6010,

W-846aoc e *** 3 .6 a9,/kg DNA 6010, S

W 94 6opp rd :u 1. 4 11 g,/kg DNA -6ulu, S

46Lea

mercury ***

lybdenum 9**M

ND<0.043ND<0.63 nR /ka Dora

DNA1470, SW- 86010 , sw-64 6

W-84 6ol ** *Nick 0.73 ag /kg DPA 6010, S

W-8466eium s:*l

NDt0 .S5 agAg DNA 010, S

6W-ense*4' *e ND<O .U4 m8/kg DNA 0 4G010, B

6.3i1vm T=ll iTb NArn .04 mg/kx DNA b01C, SW-8 4

W-84 6uad *1* 0 .47 mg/l+g DNA 5010 , S

Vana ium

Z;nc ssr 37 mg/kg DNA suit), sW-846

-------------------- ------ -

SP)rt;ifll:ATIOIQ : DNA {Area I Burn Pall t . RCRA P art 6 Permit l

SPECIAL N0 723 : 9. Kephart Snv. Eng. Licl.cr'e of project, Deter. rni r

ml).4 ) = Oteator than 5 ) oNA _ Does nu

? sa* = Non-certified result Yor indication puryases only

-, . . . . . rr :c tam' N o

stated liaite , WET Nx1rAr r prior to xna ya's .

C01 :MENTS ; *** Por informatiob only. Sample ~aa e!tracted }per the 6E2 °_xtract Procedure

(Title 22) Prior to analYsisj A&SREVIA4I~t+9;

?} NO I) TH =Trace done dctcoted 3y c ❑ I .-- n thanNot Statod

.L

APPROVED : MSIGNED

Chemist-- flanvgarAocltctdyne SSFL Analytical Chamiatry Rt,,l .tdyue 92FL Analytical Cbemiatr y

I II II II II I III II IBNA03136399

U

HDMSe00042522

3S 1» ASER P 43+ • _1i MAY c- 9C

CHEMICAL ANALYSI SRE POEt•1'

Log Number900441 4

l --9nta Unit DR"/CROUP : 54S-000 PHONE : 992-5314t:' .rU :1

FEOM: SSFL Analytical Dhcmintry, RocketdYne Div . Roekveil lntcrnational , 0/539-169, ext 5527

25 05 / /REFERENCE; La 9u p 91 ; N8 1251, pages 161-174 REPORT DATE

: 0

SAMPLE INFORMATION FOR 900441 .4

SAmpie neerrption: Soil. Nurtbbidt find 1, disttnte a 1 Foot

Jequctter : Beatrioe Aaphart

Requested Analysis : krti,tl e

Received: 04/23/ 90 at 10 :15100le Tina : 9' 29700

Sampler : M- 9a1ver9nn

Samuled 04/23/40

Sampler IDA : 042300!1803 Samp

ANALYTE EESULf UN:TMAX. LEVELCONTIMINATh MtL1l00/SOU &CS

--------------

-------- ------------- -AntimonT lax ND<D 01 ask ;, DNA 6u1U 5w-a46

Aratnic *** 0 .30 mg/kg DNA 7000, Or 8-1 6

barium *x : 21 mx/kK DNA '7060, sK-84 6

I)eryllium *'~* 0.021 m¢/kg DNA 6010, 3W-84C•

Cadmium 0 .13 mR/ka DNA 6010, SW-84 6

Chromium tart 0.15 mg/kg DNA 6010, 9W-846

Cobalt **s 1.2 me/kg DNA 601 0 , SW-84 6

Copper set 0 .62 mg/kg DNA 6010, SW-84 G

,Lead x** 3-7 mg/kg DNA 6010, SW-84 6

Mercury 4*~ 9.1 mg/kg DNA "1 470, SW-84 C

Molybdenum *U Kt<0 .53 mg/kx DNA 6010, SW-84 6

Nickel •tt 0.46 m3/k6 DNA €010 , SW-84 0

Selenium t** ND<0 .4fi Wks DNA 6010, SW-84 6

Si1,tr •i++ NDt0 .04 mg/kg DNA 6010 , SW-64 6

Thxl! ium **x ND'rO_oa ms/kg DNA 6010, SW-84 6

canedium *** C .e& mg/kg DNA 6010, SW-84 C

Zinc *** 6 .3 mg/kg DNA 6010, sw-84 6

----- --------- --- -

SPECIFICATION! DNA (ar-a I Rnrn Paid for- $CRA Fmi-t 0 Permit )

SPECIAL NOTES : B. Kephart Env. Erg . in charge of project . Ceter . ra runoff Contain . No

stated Haas . WET extinct prior t o

COMMENTS : {** For information onl :' . Sample uax extracted ,n,-.r HET Fs :'a4taur~ Prottdurt

; T1t1e 22 ) prin^ Ln anhlykis .s sPis1 E~":F.i71bNS ►

[4) ) TR Trace ND = None detected 3) t Less ch,u ,

) > = Greater than 3 ; DNA x Unna not apply 0) N .S . Sot Statcd

ax4 = Non- . :rrtilied result fuc itndication parpoaee onl y

1 3ICNF,D : ~ iC1.~ rn :'APpBn

Manager Chemist3ocketa~ne '_-PL Anal ; ti es! Chemistry Rocketdyae S.4FT. A,wlyti- .1 Chemistry

I II I IIII II III II IIIII II 111 1BNA03136400

HDMSe00042523

,no,,, ?S 4n 17 :'an I* L=SERP . 5

CHEMICAL ANALYSI SREPOT 't'

Log Number0001416

r- ST f,' T : C L

Manager ' e5eniatRcct Q.tdyne 4SFL Analytical Chtm : .strti Ru<:4crtQfn4 SSFL Analytical t'hamietry

I I II I IIIII I III III I III iBNA0313640 1

To: Environmental Unit DEPT/GROUP :FROM; SSFL Analytic'.l chemistry , Rockctd-n* Div .REFERENCE : Lb 90 p 97 ; NB 1251, pages 161-174

543-000 PHONE : 392-531 4Roclac11 International, D/09-169' ext. 592 7

k& 't)NT DATE : 05/25/9 0

SAMP1E INFORMATION FOR ?004413

Sample 0 Sc: rpiion: Sc1l, Norms da Pad 2, d1 tante a I Foo t

Bcquester3 Beatrice KeDliarLReQUeaLed Anal' 21nt $.ta 1 4

Peocivod 04/23190 at 0 .15 :0 03amplcr : a, Halverson Sampicr ID4 : 0423901'4104Saeplea : 04/23/90

Sau1r Tiae: 9 :32tt O

!tAX LEVE L

ANALYTE RESULT UVIT CONTAMINATE METHOD/SOURC E------------------------ ---------

--

------ -

Antimony *** NDx0 .01 mglkg DNA 6010 , SW-846AreeCic a;* 0.46 mg/k ; DNA 7050 , SW-846

Darium *** 30 mg/kg DNA 7060, 3A-84C

Roryllium I T 0 .042 arA t; DNA 6010, SW-$36

Cadmium *** 0.40 mg/kg DNA 60X0, SW-846

ebroainm *** 2 .1 mg/l,g DNA 6010 , SW-346

Cobalt *1* 1 .1 m6'kg DNA "6010, 3W-$4G

Copper ss* 5 .2 a-/kg DNA 5010, sx-84 6

Lead *** 3-5 mg/Lg DNA 6010, SW-846

Morciiry xxz 45 mglkg DNA 747D , SW-84 6

Molybdenum **= NDtQ .53 me/kg DNA 6010, SW-84 6

Nickel ;** 3 .5 Mg/kg DNA 6010, yk-84 6

3elvaium *44 ROc0 .46 ng/kg DNA 6010 SW-846Silver ***Thal1lum **4

ND<0.01 0ND<O .04

mx/" qaS/'k6

DNADNA

6010 , 9W-84 66010, SW-$4b

t'anadina x** 1,0 aalkY DNA 6010 , SW-84 6Zzac * c4 42 m6/lg DNA 6010, 3W-D40

SPECIAL NOTES : B . Kephart Loy. Eng. in chncg.- ~f project . Deter . rain rur.off contain . No

atatnd 1initn WET estrAct prior to analynin .

CO D4ENIS: *=Y For Information Only. 3amyle was extracted per the WIT Procedure (Title 22)uriur to ana1y5t1s .

AnDREVIATION31) TV - Trace 2) ND T Nona detactett --- 3) t • Lesy than

4) ) = Grater than E : DNA ~ Dees notA001r 6) N .S . = Nr,r. SrAted

7) 44* = Non-certifled -exult rnr lndieat lon purpoaec onl y

--------------------------- - ---------DNA (Area I Burn Fad for RCRA Part k Permit )

Ak+NN()VED•t,

HDMSe00042524

Mfli 15 '90 13•36 It Li;SER P.

CHEMICAL ANALYST S

REPbRT

TO : Envirunmrnlnl [ r, t. DEPT/O,.DUF : 543 000 FHC~F' 3y''-5~14

. Rockwell Intert ,xi- -u' lCi vokoclet ml Chcmictry 0 2?G . exit& ~ ': io t 161-1

BEFEWC.T . TR 50 p 91 ; NE 12$i,, 15y9SBFL Analytica p 1 Uli!P20H 7 4

52,NPLE INFOFMATION FOA 900441 6

Sample Tlcscrpticn; Sc_1, Edcteice pad 1, diFtaacc - 1 Foot

gamester: Beatrice Ke~ifhar L

fle ueated Aaaly5is : Clctat s

to e4ved: 04/23/90 htIO•t5 :00

42290MH05 Sample Tier: 9 :34 :00

Sampler : N. 11alversonled' D4/23/9 0S

Saapier 1U ; : 0

auP

MAX LEVPL

ANALYTE RMULT UNIT CONT .414INATE xYTNOD/StK --- -__---_

i *t`* hD<0.01 ---

mglkg DNA 6010 ,

7060

SW-P., 6

94-84 6mon YAnt:ss C .45 mNe DNA .

60 SW-84 6Ar8en1 -

Barium *** 2506 30

mSlk 6mY/kX

DNADNA

70 ,6010 . SW-' 3

Beryllium**~

.C .46 Wks L)NA 6010 ,

06SWI-R4 6BW-64 6Cadmium

S=* 1,! mg/kg DNA ,01W-5i 6Chromiu m

Co`t,Ult *** 1 .4 mg/kg DM 6010 ,6010,

SSW-84 6

zsx 3 .0 mg,kg DNA06 3W-81 FCoppe r

Lead *** 3 . 1it

mg/ksm5/kg

DNADNA

,0 17410, Bc"-64 6

mercury VS 3NDEO g/ke' UNA 6010, SW-84 8

-KolyLt1euums : :

.2 .4 m$/k& DNA 6010 ,

060

84 6SWSW-84 6Nickel

*+* ND<0.46 mSl g DNA ,1W-84 6selenium

x=i 0 .46 mJ'kg DNA 6010 . $SW-846Silver

m ** *ll 0<0 .044 mg/kg DNA 5010 ,

60 0 SW-84 6i uThaxc sd 1 .1 mgY1~Y DNA 1 ,

00 SW-846iumVanaZinc t** 25 ng/k$ DNA ,6 1

(Title 22) prior to analysis, A9RAEVla?704 8

2) ND = Nonc detoat©d 3)1) TB - TraGc 6) V4) ) Greater r:han 5) DNA = Duns not MPDI Y

7) «** _ Non-ccrtif_ed result for indication purposes onl y

SPECIFICATION : DNA (Area I Burn Pad for &CSA fart B Permit);ain uneiP Contain . No

IAL W SPEC S! B . Koph*rt Y. Ens, in charge nr prnjr,a. Deter .

Stated limits. WET extract prior to analysis.

gxnpl c uns extracted j r leLice WET extraction ?roeedureCUDLKhN•fS : __* 5'Or !nlOrnation Only .

- - - -------------------- --------

APPROVED : +

Recketdyno SSFL Annlyt ic .=1 r.~,r,*1yt,•y

ST ON FD .* _

= 1X++y Libnu

3 . Not 9tatea

Chemis t8ockttdyne SSI"L Analytical Chcmirtry

I I II I II II 0I 0III I I I I 11 1BNA03136402

HDMSe00042525

r1AY 25 '90 13:37 I* LRSER P,;

CHEMICAL ANALYSXSL C)IR-

Log Number900441 T

TO' Environmental Unit DEt'T /GPOUP : 543-0G0 PHONE! 392-521 4

REFERENCE : LB 90 P UI; ND 1251, pcLgco 1G1 -174 RE:PO1L DATT- 05/25,'4 0

SAMPLE INFORMATION POR 900441 79Amyle D. •rption- Sail, Wectaido pud 2, diatanoc = 1 Foo t

Requester: Beatrice Kephar tRequested Aaalyzia: M.tala

Received: 04/20/90 at 10 :15 :00Sampler!. M . HalvvraonOemnled: 04/23/90

Samplcr ID8 : O423UOME06 Sample Time : 9 :36 :00

4NALYTE RESULT UNITMAT . LEVELCONTA.MII ATE NETHOD/SOURCE

------ ----- -----------------

Antimony 44* NO<8 .U1 mg/kg DNA 8010 . SW-846A. ocnie *** 0.44 mg/kg DNA 7060, SW-81 6Rarium *4* 29 mg/kg DNA 7060, SW-84 6Beryllium **1 0.062 mg/ke DN A 6010, SW- 9 '1 6Cadmium *** 0 .4 .4 as/kg DNA 6010, 3W-84 6Chromium *** 0 .68 mg/kg DNA c010, $N-d1 6Cobalt 4** 1 .6 mg/kg DNA 6010 . SW-84 0copper*** 2 .7 mg/kg DNA h710, SW-H .1 61yad $as

7

mglk : DNA 0010, SW-R 4Mtresry 4*4 Nn<0 .D4 mg/kg DNA '?17O, SW-14 iMClybdeaum 44* 440, 53 mg/kf DNA 6010, SW-bo aNickel *** 1 .9 mg/kg UNA 6010 , S';-61 3Selenium *44 ND<0 .6b mglkt DNA 60ti1, gW-A4 ASilver *** sn(0 .04 mg/kg DNA SUJU , SW-846Thallium s- ND<0 .04 mo/k>; DNA 8010, SW-84 6Vanadium **4 RD<0 .51 mg/k$ DNA 6010, SW-81 6Zinc i*s 21 mg/kg DNA 0010, SW-R4 8

------------------------ -------------------- -------- ----------- --------- -SPECIF$4'ATION : DNA CArea I Burn Pad for RCAA Part B Permit }SPECIAL NOTES . S . Kephart . Rnv. Fng. In charge of project . Deter . rain runoff canter .

stated limits . Wtl' extract prior to analysis .C0MMENT3 : ***For Information Orly. SAmpie eras extracted per the WET extracticn procodarc

(Title 22) prior to analy*ia .* ANRRF.VIATIONS *

11 T8 =Trace 2) ND Nona dctCeted 37 < = Leas than4) = Greater then S) DNA Does not apply 6) 5 .3 . = Not Stated7) 44* = Non-certified resulr for indication purposee only

APPROVED :- llaa1ager 'Chemist

aoeketdyae 3SFL Analytical Ct,.-eictry Rockotd'-e SSPL Analytical Chcmistry

I I II I II II I III I I I I II II 0 I RBNA0313640 3

PEON : OSPL Anzlyti' 11 Chemistry , Roct8tdyno Div . Rockwelllntc:motionci, D!530 1C1, ext. 582 7

fSIGN*D :

HDMSe00042526