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Page 1: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

Figure H-1.75

Page 2: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

Figure H-1.76

Page 3: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

Figure H-1.77

Page 4: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

Figure H-1.78

Page 5: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

26-Aug-11Date:Advanced Technology Laboratories

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Lab Order: 119461CASE NARRATIVE

The sample for SM5210B (BOD) analysis was subcontracted to American Scientific Laboratories with ELAP Cert.# 2200.

Sample Receiving / General Comments

Sample received beyond holding time for SM4500-H+B (pH) and SM4500-Cl G (Residual Chlorine) analyses.

Results were J-Flag. "J" is used to flag those results that are between the PQL (Practical Quantitation Limit) and the calculated MDL (Method Detection Limit). Results that are "J" Flagged are estimated values since it becomes difficult to accurately quantitate the analyte near the MDL.

Analytical Comments for SM5540C

Sample 119461-001A-MSD, Matrix Spike Duplicate (MSD) is outside recovery criteria; however, the analytical batch was validated by the Laboratory Control Sample (LCS).

Page 1 of 12

2 of 13

Figure H-1.79

Page 6: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3

Client Sample ID: P-103 Aug 2011/UCLA Lot 36

Collection Date: 8/19/2011 8:00:00 AM

Matrix: GROUNDWATER

Analyses Result Qual Units Date Analyzed

CLIENT: AMEC E&I

Lab Order: 119461

Lab ID: 119461-001A

DF

Advanced Technology Laboratories Print Date: 26-Aug-11

PQLMDL

ANALYTICAL RESULTS

SURFACTANTSSM5540C

Analyst: AAGRunID: WETCHEM3_110819C 75067QC Batch: PrepDate: 8/19/2011

MBAS 0.050 mg/L 10.11 0.026 8/19/2011

PHSM4500-H+B

Analyst: FDRunID: PH4_110819A R135952QC Batch: PrepDate:

pH H0.10 pH Units 17.0 0.10 8/19/2011

TURBIDITYEPA 180.1

Analyst: MPRunID: TURB_110819A R136052QC Batch: PrepDate:

Turbidity 0.10 NTU 12.7 0.10 8/19/2011

TOTAL AND FREE CHLORINE DPD COLORIMETRICSM 4500-CL G

Analyst: MPRunID: SC_110819A R136053QC Batch: PrepDate:

Chlorine, Total H0.10 mg/L 1ND 0.054 8/19/2011

TOTAL NON-FILTERABLE RESIDUESM2540D

Analyst: PTRunID: WETCHEM_110822C 75052QC Batch: PrepDate: 8/22/2011

Suspended Solids (Residue, Non-Filterable)

10 mg/L 1ND 10 8/22/2011 08:00

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference

Results are wet unless otherwise specified DO Surrogate Diluted Out

3 of 13

Figure H-1.80

Page 7: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3

Client Sample ID: P-103 Aug 2011/UCLA Lot 36

Collection Date: 8/19/2011 8:00:00 AM

Matrix: GROUNDWATER

Analyses Result Qual Units Date Analyzed

CLIENT: AMEC E&I

Lab Order: 119461

Lab ID: 119461-001B

DF

Advanced Technology Laboratories Print Date: 26-Aug-11

PQLMDL

ANALYTICAL RESULTS

SETTLEABLE MATTERSM2540F

Analyst: PTRunID: WETCHEM_110819A 75024QC Batch: PrepDate: 8/19/2011

Settleable Matter 0.099 ml/L 1ND 0.099 8/19/2011

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference

Results are wet unless otherwise specified DO Surrogate Diluted Out

4 of 13

Figure H-1.81

Page 8: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3

Client Sample ID: P-103 Aug 2011/UCLA Lot 36

Collection Date: 8/19/2011 8:00:00 AM

Matrix: GROUNDWATER

Analyses Result Qual Units Date Analyzed

CLIENT: AMEC E&I

Lab Order: 119461

Lab ID: 119461-001C

DF

Advanced Technology Laboratories Print Date: 26-Aug-11

PQLMDL

ANALYTICAL RESULTS

ICPMS METALSEPA 200.8

Analyst: SRB

EPA 200.8

RunID: ICP7_110823A 75046QC Batch: PrepDate: 8/22/2011

Copper 1.0 µg/L 11.3 0.058 8/23/2011 12:33

Lead J1.0 µg/L 10.21 0.10 8/23/2011 12:33

Selenium 0.50 µg/L 16.9 0.26 8/23/2011 12:33

Zinc J10 µg/L 17.9 2.5 8/23/2011 12:33

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference

Results are wet unless otherwise specified DO Surrogate Diluted Out

5 of 13

Figure H-1.82

Page 9: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

26-Aug-11Date:Advanced Technology Laboratories

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 150.1_4500H+B_W

Sample ID: 119461-001ADUP

Batch ID: R135952 TestNo: SM4500-H+B Analysis Date: 8/19/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: pH Units

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 135952

SeqNo: 2227722

DUPSampType: TestCode: 150.1_4500H+

pH 10 H0.10 6.970 06.970

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

6 of 13

Figure H-1.83

Page 10: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 160.2_2540D_W

Sample ID: 119461-001A-DUP

Batch ID: 75052 TestNo: SM2540D Analysis Date: 8/22/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 135977

SeqNo: 2228189

DUPSampType: TestCode: 160.2_2540D_

Suspended Solids (Residue, Non-Filter 1010 0 0ND

Sample ID: LCS-75052

Batch ID: 75052 TestNo: SM2540D Analysis Date: 8/22/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW

RunNo: 135977

SeqNo: 2228190

LCSSampType: TestCode: 160.2_2540D_

Suspended Solids (Residue, Non-Filter 96.60 98.3 80 12010 095.000

Sample ID: MB-75052

Batch ID: 75052 TestNo: SM2540D Analysis Date: 8/22/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW

RunNo: 135977

SeqNo: 2228191

MBLKSampType: TestCode: 160.2_2540D_

Suspended Solids (Residue, Non-Filter 10ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

7 of 13

Figure H-1.84

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3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 160.5_2540F_W

Sample ID: MB-75024

Batch ID: 75024 TestNo: SM2540F Analysis Date: 8/19/2011

Prep Date: 8/19/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ml/L

PQL

Client ID: PBW

RunNo: 135938

SeqNo: 2227506

MBLKSampType: TestCode: 160.5_2540F_

Settleable Matter 0.10ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

8 of 13

Figure H-1.85

Page 12: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 180.1_W

Sample ID: MB-R136052

Batch ID: R136052 TestNo: EPA 180.1 Analysis Date: 8/19/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: NTU

PQL

Client ID: PBW

RunNo: 136052

SeqNo: 2229349

MBLKSampType: TestCode: 180.1_W

Turbidity 0.10ND

Sample ID: 119461-001ADUP

Batch ID: R136052 TestNo: EPA 180.1 Analysis Date: 8/19/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: NTU

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 136052

SeqNo: 2229353

DUPSampType: TestCode: 180.1_W

Turbidity 100.10 2.690 4.172.580

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

9 of 13

Figure H-1.86

Page 13: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 200.8_W

Sample ID: MB-75046

Batch ID: 75046 TestNo: EPA 200.8 Analysis Date: 8/23/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: PBW

RunNo: 136009

SeqNo: 2228660

MBLKSampType: TestCode: 200.8_W

EPA 200.8

Copper 1.0ND

Lead 1.0ND

Selenium 0.50ND

Zinc J102.760

Sample ID: LCS-75046

Batch ID: 75046 TestNo: EPA 200.8 Analysis Date: 8/23/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: LCSW

RunNo: 136009

SeqNo: 2228661

LCSSampType: TestCode: 200.8_W

EPA 200.8

Copper 10.00 99.4 85 1151.0 09.935

Lead 10.00 97.4 85 1151.0 09.735

Selenium 10.00 103 85 1150.50 010.259

Zinc 100.0 93.8 85 11510 2.76096.535

Sample ID: 119461-001C-MS

Batch ID: 75046 TestNo: EPA 200.8 Analysis Date: 8/23/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 136009

SeqNo: 2228663

MSSampType: TestCode: 200.8_W

EPA 200.8

Copper 10.00 80.4 70 1301.0 1.3419.379

Lead 10.00 89.6 70 1301.0 0.20759.166

Selenium 10.00 97.1 70 1300.50 6.92916.636

Zinc 100.0 83.7 70 13010 7.86491.604

Sample ID: 119461-001C-MSD

Batch ID: 75046 TestNo: EPA 200.8 Analysis Date: 8/23/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 136009

SeqNo: 2228664

MSDSampType: TestCode: 200.8_W

EPA 200.8

Copper 10.00 79.2 70 130 201.0 1.341 9.379 1.229.265

Lead 10.00 88.4 70 130 201.0 0.2075 9.166 1.369.043

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

10 of 13

Figure H-1.87

Page 14: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 200.8_W

Sample ID: 119461-001C-MSD

Batch ID: 75046 TestNo: EPA 200.8 Analysis Date: 8/23/2011

Prep Date: 8/22/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 136009

SeqNo: 2228664

MSDSampType: TestCode: 200.8_W

EPA 200.8

Selenium 10.00 96.0 70 130 200.50 6.929 16.64 0.66316.526

Zinc 100.0 85.5 70 130 2010 7.864 91.60 1.9393.385

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

11 of 13

Figure H-1.88

Page 15: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 425.1_5540C_W

Sample ID: 119461-001A-MS

Batch ID: 75067 TestNo: SM5540C Analysis Date: 8/19/2011

Prep Date: 8/19/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 135988

SeqNo: 2228442

MSSampType: TestCode: 425.1_5540C_

MBAS 0.5000 83.2 80 1200.050 0.11100.527

Sample ID: 119461-001A-MSD

Batch ID: 75067 TestNo: SM5540C Analysis Date: 8/19/2011

Prep Date: 8/19/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 135988

SeqNo: 2228443

MSDSampType: TestCode: 425.1_5540C_

MBAS 0.5000 79.8 80 120 20 S0.050 0.1110 0.5270 3.280.510

Sample ID: LCS-75067

Batch ID: 75067 TestNo: SM5540C Analysis Date: 8/19/2011

Prep Date: 8/19/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW

RunNo: 135988

SeqNo: 2228444

LCSSampType: TestCode: 425.1_5540C_

MBAS 0.5000 105 80 1200.050 00.523

Sample ID: MB-75067

Batch ID: 75067 TestNo: SM5540C Analysis Date: 8/19/2011

Prep Date: 8/19/2011

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW

RunNo: 135988

SeqNo: 2228445

MBLKSampType: TestCode: 425.1_5540C_

MBAS 0.050ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

12 of 13

Figure H-1.89

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3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: MTA Westside Extention, 4953101561/6.2.3.3.

CLIENT: AMEC E&I

Work Order: 119461ANALYTICAL QC SUMMARY REPORT

TestCode: 4500_CL_G

Sample ID: MB-R136053

Batch ID: R136053 TestNo: SM 4500-Cl G Analysis Date: 8/19/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW

RunNo: 136053

SeqNo: 2229354

MBLKSampType: TestCode: 4500_CL_G

Chlorine, Total 0.10ND

Sample ID: LCS-R136053

Batch ID: R136053 TestNo: SM 4500-Cl G Analysis Date: 8/19/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW

RunNo: 136053

SeqNo: 2229355

LCSSampType: TestCode: 4500_CL_G

Chlorine, Total 1.000 97.0 80 1200.10 00.970

Sample ID: 119461-001AMS

Batch ID: R136053 TestNo: SM 4500-Cl G Analysis Date: 8/19/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 136053

SeqNo: 2229357

MSSampType: TestCode: 4500_CL_G

Chlorine, Total 1.000 95.0 80 120 H0.10 00.950

Sample ID: 119461-001AMSD

Batch ID: R136053 TestNo: SM 4500-Cl G Analysis Date: 8/19/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: P-103 Aug 2011/UCL

RunNo: 136053

SeqNo: 2229358

MSDSampType: TestCode: 4500_CL_G

Chlorine, Total 1.000 95.0 80 120 20 H0.10 0 0.9500 00.950

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

13 of 13

Figure H-1.90

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Figure H-1.91

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Preliminary Geotechnical and Environmental Report

Appendix I – Environmental Site Assessment

W E S T S I D E S U B W A Y E X T E N S I O N P R O J E C T December 21, 2011

APPENDIX I ENVIRONMENTAL SITE ASSESSMENT

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Preliminary Geotechnical and Environmental Report

Appendix I – Environmental Site Assessment

W E S T S I D E S U B W A Y E X T E N S I O N P R O J E C T December 21, 2011

FIGURES I-1.1 THROUGH I-1.1071 ANALYTICAL TEST RESULTS OF SOIL AND GROUNDWATER

SAMPLES (PE PHASE)

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Figure I-1.1

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3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

06-Jul-11Date:Advanced Technology Laboratories

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Lab Order: 118577CASE NARRATIVE

All volatile analyses were performed using 5035 preservation requirements. Any high level dilutions were performed on a preserved methanol sample unless otherwise noted.

Page 1 of 17

2 of 18

Figure I-1.2

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3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-45

Collection Date: 6/21/2011 11:15:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-001A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: BDRunID: MS5_110624A T11VS109QC Batch: PrepDate: 6/22/2011

1,1,1,2-Tetrachloroethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,1,1-Trichloroethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,1,2,2-Tetrachloroethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,1,2-Trichloroethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,1-Dichloroethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,1-Dichloroethene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,1-Dichloropropene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2,3-Trichlorobenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2,3-Trichloropropane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2,4-Trichlorobenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2,4-Trimethylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2-Dibromo-3-chloropropane 6/24/2011 04:16 PM7.8 µg/Kg 1ND

1,2-Dibromoethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2-Dichlorobenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2-Dichloroethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,2-Dichloropropane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,3,5-Trimethylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,3-Dichlorobenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,3-Dichloropropane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

1,4-Dichlorobenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

2,2-Dichloropropane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

2-Chlorotoluene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

4-Chlorotoluene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

4-Isopropyltoluene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Benzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Bromobenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Bromodichloromethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Bromoform 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Bromomethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Carbon tetrachloride 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Chlorobenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Chloroethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Chloroform 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Chloromethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

cis-1,2-Dichloroethene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

3 of 18

Figure I-1.3

Page 23: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-45

Collection Date: 6/21/2011 11:15:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-001A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: BDRunID: MS5_110624A T11VS109QC Batch: PrepDate: 6/22/2011

cis-1,3-Dichloropropene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Di-isopropyl ether 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Dibromochloromethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Dibromomethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Dichlorodifluoromethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Ethyl Tert-butyl ether 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Ethylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Hexachlorobutadiene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Isopropylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

m,p-Xylene 6/24/2011 04:16 PM7.8 µg/Kg 1ND

Methylene chloride 6/24/2011 04:16 PM3.9 µg/Kg 1ND

MTBE 6/24/2011 04:16 PM3.9 µg/Kg 1ND

n-Butylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

n-Propylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Naphthalene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

o-Xylene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

sec-Butylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Styrene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Tert-amyl methyl ether 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Tert-Butanol 6/24/2011 04:16 PM78 µg/Kg 1ND

tert-Butylbenzene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Tetrachloroethene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Toluene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

trans-1,2-Dichloroethene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Trichloroethene 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Trichlorofluoromethane 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Vinyl chloride 6/24/2011 04:16 PM3.9 µg/Kg 1ND

Surr: 1,2-Dichloroethane-d4 6/24/2011 04:16 PM65-141 %REC 198.0

Surr: 4-Bromofluorobenzene 6/24/2011 04:16 PM57-134 %REC 189.5

Surr: Dibromofluoromethane 6/24/2011 04:16 PM70-128 %REC 189.3

Surr: Toluene-d8 6/24/2011 04:16 PM72-123 %REC 188.0

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

4 of 18

Figure I-1.4

Page 24: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-50

Collection Date: 6/21/2011 11:30:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-002A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: BDRunID: MS5_110624A T11VS109QC Batch: PrepDate: 6/22/2011

1,1,1,2-Tetrachloroethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,1,1-Trichloroethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,1,2,2-Tetrachloroethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,1,2-Trichloroethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,1-Dichloroethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,1-Dichloroethene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,1-Dichloropropene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2,3-Trichlorobenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2,3-Trichloropropane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2,4-Trichlorobenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2,4-Trimethylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2-Dibromo-3-chloropropane 6/24/2011 04:35 PM7.3 µg/Kg 1ND

1,2-Dibromoethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2-Dichlorobenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2-Dichloroethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,2-Dichloropropane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,3,5-Trimethylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,3-Dichlorobenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,3-Dichloropropane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

1,4-Dichlorobenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

2,2-Dichloropropane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

2-Chlorotoluene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

4-Chlorotoluene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

4-Isopropyltoluene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Benzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Bromobenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Bromodichloromethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Bromoform 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Bromomethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Carbon tetrachloride 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Chlorobenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Chloroethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Chloroform 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Chloromethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

cis-1,2-Dichloroethene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

5 of 18

Figure I-1.5

Page 25: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-50

Collection Date: 6/21/2011 11:30:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-002A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: BDRunID: MS5_110624A T11VS109QC Batch: PrepDate: 6/22/2011

cis-1,3-Dichloropropene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Di-isopropyl ether 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Dibromochloromethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Dibromomethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Dichlorodifluoromethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Ethyl Tert-butyl ether 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Ethylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Hexachlorobutadiene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Isopropylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

m,p-Xylene 6/24/2011 04:35 PM7.3 µg/Kg 1ND

Methylene chloride 6/24/2011 04:35 PM3.6 µg/Kg 1ND

MTBE 6/24/2011 04:35 PM3.6 µg/Kg 1ND

n-Butylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

n-Propylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Naphthalene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

o-Xylene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

sec-Butylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Styrene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Tert-amyl methyl ether 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Tert-Butanol 6/24/2011 04:35 PM73 µg/Kg 1ND

tert-Butylbenzene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Tetrachloroethene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Toluene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

trans-1,2-Dichloroethene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Trichloroethene 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Trichlorofluoromethane 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Vinyl chloride 6/24/2011 04:35 PM3.6 µg/Kg 1ND

Surr: 1,2-Dichloroethane-d4 6/24/2011 04:35 PM65-141 %REC 199.4

Surr: 4-Bromofluorobenzene 6/24/2011 04:35 PM57-134 %REC 187.8

Surr: Dibromofluoromethane 6/24/2011 04:35 PM70-128 %REC 1101

Surr: Toluene-d8 6/24/2011 04:35 PM72-123 %REC 189.1

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

6 of 18

Figure I-1.6

Page 26: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-55

Collection Date: 6/21/2011 11:50:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-003A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: BDRunID: MS5_110624A T11VS109QC Batch: PrepDate: 6/22/2011

1,1,1,2-Tetrachloroethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,1,1-Trichloroethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,1,2,2-Tetrachloroethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,1,2-Trichloroethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,1-Dichloroethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,1-Dichloroethene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,1-Dichloropropene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2,3-Trichlorobenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2,3-Trichloropropane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2,4-Trichlorobenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2,4-Trimethylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2-Dibromo-3-chloropropane 6/24/2011 04:53 PM7.2 µg/Kg 1ND

1,2-Dibromoethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2-Dichlorobenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2-Dichloroethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,2-Dichloropropane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,3,5-Trimethylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,3-Dichlorobenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,3-Dichloropropane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

1,4-Dichlorobenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

2,2-Dichloropropane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

2-Chlorotoluene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

4-Chlorotoluene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

4-Isopropyltoluene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Benzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Bromobenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Bromodichloromethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Bromoform 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Bromomethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Carbon tetrachloride 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Chlorobenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Chloroethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Chloroform 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Chloromethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

cis-1,2-Dichloroethene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

7 of 18

Figure I-1.7

Page 27: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-55

Collection Date: 6/21/2011 11:50:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-003A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: BDRunID: MS5_110624A T11VS109QC Batch: PrepDate: 6/22/2011

cis-1,3-Dichloropropene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Di-isopropyl ether 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Dibromochloromethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Dibromomethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Dichlorodifluoromethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Ethyl Tert-butyl ether 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Ethylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Hexachlorobutadiene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Isopropylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

m,p-Xylene 6/24/2011 04:53 PM7.2 µg/Kg 1ND

Methylene chloride 6/24/2011 04:53 PM3.6 µg/Kg 1ND

MTBE 6/24/2011 04:53 PM3.6 µg/Kg 1ND

n-Butylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

n-Propylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Naphthalene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

o-Xylene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

sec-Butylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Styrene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Tert-amyl methyl ether 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Tert-Butanol 6/24/2011 04:53 PM72 µg/Kg 189

tert-Butylbenzene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Tetrachloroethene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Toluene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

trans-1,2-Dichloroethene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Trichloroethene 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Trichlorofluoromethane 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Vinyl chloride 6/24/2011 04:53 PM3.6 µg/Kg 1ND

Surr: 1,2-Dichloroethane-d4 6/24/2011 04:53 PM65-141 %REC 199.2

Surr: 4-Bromofluorobenzene 6/24/2011 04:53 PM57-134 %REC 187.8

Surr: Dibromofluoromethane 6/24/2011 04:53 PM70-128 %REC 196.1

Surr: Toluene-d8 6/24/2011 04:53 PM72-123 %REC 187.0

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

8 of 18

Figure I-1.8

Page 28: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-40-45

Collection Date: 6/21/2011 12:50:00 PM

Matrix: GROUNDWATER

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-004A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: SLLRunID: MS2_110624A Q11VW116QC Batch: PrepDate:

1,1,1,2-Tetrachloroethane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,1,1-Trichloroethane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,1,2,2-Tetrachloroethane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,1,2-Trichloroethane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,1-Dichloroethane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,1-Dichloroethene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,1-Dichloropropene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2,3-Trichlorobenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2,3-Trichloropropane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2,4-Trichlorobenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2,4-Trimethylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2-Dibromo-3-chloropropane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2-Dibromoethane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2-Dichlorobenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2-Dichloroethane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,2-Dichloropropane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,3,5-Trimethylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,3-Dichlorobenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

1,3-Dichloropropane 6/24/2011 08:50 PM0.50 µg/L 1ND

1,4-Dichlorobenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

2,2-Dichloropropane 6/24/2011 08:50 PM0.50 µg/L 1ND

2-Chlorotoluene 6/24/2011 08:50 PM0.50 µg/L 1ND

4-Chlorotoluene 6/24/2011 08:50 PM0.50 µg/L 1ND

4-Isopropyltoluene 6/24/2011 08:50 PM0.50 µg/L 1ND

Benzene 6/24/2011 08:50 PM0.50 µg/L 1ND

Bromobenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

Bromodichloromethane 6/24/2011 08:50 PM0.50 µg/L 1ND

Bromoform 6/24/2011 08:50 PM0.50 µg/L 1ND

Bromomethane 6/24/2011 08:50 PM0.50 µg/L 1ND

Carbon tetrachloride 6/24/2011 08:50 PM0.50 µg/L 1ND

Chlorobenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

Chloroethane 6/24/2011 08:50 PM0.50 µg/L 1ND

Chloroform 6/24/2011 08:50 PM0.50 µg/L 1ND

Chloromethane 6/24/2011 08:50 PM0.50 µg/L 1ND

cis-1,2-Dichloroethene 6/24/2011 08:50 PM0.50 µg/L 1ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

9 of 18

Figure I-1.9

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3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10

Client Sample ID: E-101-40-45

Collection Date: 6/21/2011 12:50:00 PM

Matrix: GROUNDWATER

Analyses Result Qual Units Date Analyzed

CLIENT: Mactec

Lab Order: 118577

Lab ID: 118577-004A

DF

Advanced Technology Laboratories Print Date: 06-Jul-11

PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: SLLRunID: MS2_110624A Q11VW116QC Batch: PrepDate:

cis-1,3-Dichloropropene 6/24/2011 08:50 PM0.50 µg/L 1ND

Dibromochloromethane 6/24/2011 08:50 PM0.50 µg/L 1ND

Dibromomethane 6/24/2011 08:50 PM0.50 µg/L 1ND

Dichlorodifluoromethane 6/24/2011 08:50 PM0.50 µg/L 1ND

Ethylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

Hexachlorobutadiene 6/24/2011 08:50 PM0.50 µg/L 1ND

Isopropylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

m,p-Xylene 6/24/2011 08:50 PM1.0 µg/L 1ND

Methylene chloride 6/24/2011 08:50 PM1.0 µg/L 1ND

n-Butylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

n-Propylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

Naphthalene 6/24/2011 08:50 PM0.50 µg/L 1ND

o-Xylene 6/24/2011 08:50 PM0.50 µg/L 1ND

sec-Butylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

Styrene 6/24/2011 08:50 PM0.50 µg/L 1ND

tert-Butylbenzene 6/24/2011 08:50 PM0.50 µg/L 1ND

Tetrachloroethene 6/24/2011 08:50 PM0.50 µg/L 1ND

Toluene 6/24/2011 08:50 PM0.50 µg/L 1ND

trans-1,2-Dichloroethene 6/24/2011 08:50 PM0.50 µg/L 1ND

Trichloroethene 6/24/2011 08:50 PM0.50 µg/L 1ND

Trichlorofluoromethane 6/24/2011 08:50 PM0.50 µg/L 1ND

Vinyl chloride 6/24/2011 08:50 PM0.50 µg/L 1ND

Surr: 1,2-Dichloroethane-d4 6/24/2011 08:50 PM70-130 %REC 193.0

Surr: 4-Bromofluorobenzene 6/24/2011 08:50 PM70-130 %REC 190.2

Surr: Dibromofluoromethane 6/24/2011 08:50 PM70-130 %REC 194.2

Surr: Toluene-d8 6/24/2011 08:50 PM70-130 %REC 189.7

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit

S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

10 of 18

Figure I-1.10

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3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

06-Jul-11Date:Advanced Technology Laboratories

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_S_5035

Sample ID: T110624LCS1

Batch ID: T11VS109 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 134388

SeqNo: 2196672

LCSSampType: TestCode: 8260_S_5035

1,1-Dichloroethene 50.00 86.7 70 1305.0 043.350

Benzene 100.0 88.7 70 1305.0 088.700

Chlorobenzene 50.00 97.0 70 1305.0 048.510

MTBE 50.00 88.2 70 1305.0 044.080

Toluene 100.0 93.3 70 1305.0 093.300

Trichloroethene 50.00 97.2 70 1305.0 048.620

Surr: 1,2-Dichloroethane-d4 50.00 78.0 65 14139.000

Surr: 4-Bromofluorobenzene 50.00 82.6 57 13441.310

Surr: Dibromofluoromethane 50.00 88.0 70 12844.000

Surr: Toluene-d8 50.00 86.9 72 12343.430

Sample ID: T110624MB1MS

Batch ID: T11VS109 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134388

SeqNo: 2196673

MSSampType: TestCode: 8260_S_5035

1,1-Dichloroethene 50.00 85.3 70 1305.0 042.660

Benzene 100.0 91.4 70 1305.0 091.380

Chlorobenzene 50.00 100 70 1305.0 049.980

MTBE 50.00 91.6 70 1305.0 045.810

Toluene 100.0 94.5 70 1305.0 094.460

Trichloroethene 50.00 97.1 70 1305.0 048.550

Surr: 1,2-Dichloroethane-d4 50.00 81.5 65 14140.740

Surr: 4-Bromofluorobenzene 50.00 81.1 57 13440.570

Surr: Dibromofluoromethane 50.00 85.1 70 12842.560

Surr: Toluene-d8 50.00 85.8 72 12342.910

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

11 of 18

Figure I-1.11

Page 31: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_S_5035

Sample ID: T110624MB1MSD

Batch ID: T11VS109 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 134388

SeqNo: 2196674

MSDSampType: TestCode: 8260_S_5035

1,1-Dichloroethene 50.00 86.1 70 130 205.0 0 42.66 0.88743.040

Benzene 100.0 91.1 70 130 205.0 0 91.38 0.35191.060

Chlorobenzene 50.00 104 70 130 205.0 0 49.98 3.7551.890

MTBE 50.00 95.0 70 130 205.0 0 45.81 3.6247.500

Toluene 100.0 94.7 70 130 205.0 0 94.46 0.26494.710

Trichloroethene 50.00 97.3 70 130 205.0 0 48.55 0.20648.650

Surr: 1,2-Dichloroethane-d4 50.00 83.4 65 141 0041.680

Surr: 4-Bromofluorobenzene 50.00 92.7 57 134 0046.330

Surr: Dibromofluoromethane 50.00 87.2 70 128 0043.590

Surr: Toluene-d8 50.00 90.0 72 123 0044.980

Sample ID: T110624MB1

Batch ID: T11VS109 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/Kg

PQL

Client ID: PBS

RunNo: 134388

SeqNo: 2196675

MBLKSampType: TestCode: 8260_S_5035

1,1,1,2-Tetrachloroethane 5.0ND

1,1,1-Trichloroethane 5.0ND

1,1,2,2-Tetrachloroethane 5.0ND

1,1,2-Trichloroethane 5.0ND

1,1-Dichloroethane 5.0ND

1,1-Dichloroethene 5.0ND

1,1-Dichloropropene 5.0ND

1,2,3-Trichlorobenzene 5.0ND

1,2,3-Trichloropropane 5.0ND

1,2,4-Trichlorobenzene 5.0ND

1,2,4-Trimethylbenzene 5.0ND

1,2-Dibromo-3-chloropropane 10ND

1,2-Dibromoethane 5.0ND

1,2-Dichlorobenzene 5.0ND

1,2-Dichloroethane 5.0ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

12 of 18

Figure I-1.12

Page 32: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_S_5035

Sample ID: T110624MB1

Batch ID: T11VS109 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/Kg

PQL

Client ID: PBS

RunNo: 134388

SeqNo: 2196675

MBLKSampType: TestCode: 8260_S_5035

1,2-Dichloropropane 5.0ND

1,3,5-Trimethylbenzene 5.0ND

1,3-Dichlorobenzene 5.0ND

1,3-Dichloropropane 5.0ND

1,4-Dichlorobenzene 5.0ND

2,2-Dichloropropane 5.0ND

2-Chlorotoluene 5.0ND

4-Chlorotoluene 5.0ND

4-Isopropyltoluene 5.0ND

Benzene 5.0ND

Bromobenzene 5.0ND

Bromodichloromethane 5.0ND

Bromoform 5.0ND

Bromomethane 5.0ND

Carbon tetrachloride 5.0ND

Chlorobenzene 5.0ND

Chloroethane 5.0ND

Chloroform 5.0ND

Chloromethane 5.0ND

cis-1,2-Dichloroethene 5.0ND

cis-1,3-Dichloropropene 5.0ND

Di-isopropyl ether 5.0ND

Dibromochloromethane 5.0ND

Dibromomethane 5.0ND

Dichlorodifluoromethane 5.0ND

Ethyl Tert-butyl ether 5.0ND

Ethylbenzene 5.0ND

Hexachlorobutadiene 5.0ND

Isopropylbenzene 5.0ND

m,p-Xylene 10ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

13 of 18

Figure I-1.13

Page 33: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_S_5035

Sample ID: T110624MB1

Batch ID: T11VS109 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/Kg

PQL

Client ID: PBS

RunNo: 134388

SeqNo: 2196675

MBLKSampType: TestCode: 8260_S_5035

Methylene chloride 5.0ND

MTBE 5.0ND

n-Butylbenzene 5.0ND

n-Propylbenzene 5.0ND

Naphthalene 5.0ND

o-Xylene 5.0ND

sec-Butylbenzene 5.0ND

Styrene 5.0ND

Tert-amyl methyl ether 5.0ND

Tert-Butanol 100ND

tert-Butylbenzene 5.0ND

Tetrachloroethene 5.0ND

Toluene 5.0ND

trans-1,2-Dichloroethene 5.0ND

Trichloroethene 5.0ND

Trichlorofluoromethane 5.0ND

Vinyl chloride 5.0ND

Surr: 1,2-Dichloroethane-d4 50.00 85.5 65 14142.770

Surr: 4-Bromofluorobenzene 50.00 86.2 57 13443.090

Surr: Dibromofluoromethane 50.00 88.3 70 12844.160

Surr: Toluene-d8 50.00 90.8 72 12345.380

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

14 of 18

Figure I-1.14

Page 34: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_WP_LL

Sample ID: Q110624LCS1

Batch ID: Q11VW116 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: LCSW

RunNo: 134423

SeqNo: 2198138

LCSSampType: TestCode: 8260_WP_LL

1,1-Dichloroethene 20.00 89.8 70 1300.50 017.950

Benzene 40.00 93.3 70 1300.50 037.320

Chlorobenzene 20.00 98.6 70 1300.50 019.710

MTBE 20.00 92.4 70 1300.50 018.470

Toluene 40.00 99.3 70 1300.50 039.720

Trichloroethene 20.00 96.2 70 1300.50 019.250

Surr: 1,2-Dichloroethane-d4 25.00 79.4 70 13019.850

Surr: 4-Bromofluorobenzene 25.00 91.8 70 13022.960

Surr: Dibromofluoromethane 25.00 82.6 70 13020.660

Surr: Toluene-d8 25.00 91.9 70 13022.970

Sample ID: Q110624MB3MS

Batch ID: Q11VW116 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 134423

SeqNo: 2198139

MSSampType: TestCode: 8260_WP_LL

1,1-Dichloroethene 20.00 82.6 70 1300.50 016.510

Benzene 40.00 91.8 70 1300.50 036.700

Chlorobenzene 20.00 99.0 70 1300.50 019.810

MTBE 20.00 92.7 70 1300.50 018.540

Toluene 40.00 95.7 70 1300.50 038.260

Trichloroethene 20.00 92.4 70 1300.50 018.470

Surr: 1,2-Dichloroethane-d4 25.00 79.6 70 13019.890

Surr: 4-Bromofluorobenzene 25.00 90.8 70 13022.700

Surr: Dibromofluoromethane 25.00 82.7 70 13020.670

Surr: Toluene-d8 25.00 89.9 70 13022.470

Sample ID: Q110624MB3MSD

Batch ID: Q11VW116 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 134423

SeqNo: 2198140

MSDSampType: TestCode: 8260_WP_LL

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

15 of 18

Figure I-1.15

Page 35: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_WP_LL

Sample ID: Q110624MB3MSD

Batch ID: Q11VW116 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 134423

SeqNo: 2198140

MSDSampType: TestCode: 8260_WP_LL

1,1-Dichloroethene 20.00 79.8 70 130 200.50 0 16.51 3.4515.950

Benzene 40.00 93.1 70 130 200.50 0 36.70 1.4337.230

Chlorobenzene 20.00 102 70 130 200.50 0 19.81 2.8420.380

MTBE 20.00 88.3 70 130 200.50 0 18.54 4.8617.660

Toluene 40.00 98.2 70 130 200.50 0 38.26 2.6639.290

Trichloroethene 20.00 92.7 70 130 200.50 0 18.47 0.37818.540

Surr: 1,2-Dichloroethane-d4 25.00 78.4 70 130 0019.610

Surr: 4-Bromofluorobenzene 25.00 92.9 70 130 0023.220

Surr: Dibromofluoromethane 25.00 82.6 70 130 0020.660

Surr: Toluene-d8 25.00 92.6 70 130 0023.140

Sample ID: Q110624MB3

Batch ID: Q11VW116 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: PBW

RunNo: 134423

SeqNo: 2198141

MBLKSampType: TestCode: 8260_WP_LL

1,1,1,2-Tetrachloroethane 0.50ND

1,1,1-Trichloroethane 0.50ND

1,1,2,2-Tetrachloroethane 0.50ND

1,1,2-Trichloroethane 0.50ND

1,1-Dichloroethane 0.50ND

1,1-Dichloroethene 0.50ND

1,1-Dichloropropene 0.50ND

1,2,3-Trichlorobenzene 0.50ND

1,2,3-Trichloropropane 0.50ND

1,2,4-Trichlorobenzene 0.50ND

1,2,4-Trimethylbenzene 0.50ND

1,2-Dibromo-3-chloropropane 0.50ND

1,2-Dibromoethane 0.50ND

1,2-Dichlorobenzene 0.50ND

1,2-Dichloroethane 0.50ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

16 of 18

Figure I-1.16

Page 36: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_WP_LL

Sample ID: Q110624MB3

Batch ID: Q11VW116 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: PBW

RunNo: 134423

SeqNo: 2198141

MBLKSampType: TestCode: 8260_WP_LL

1,2-Dichloropropane 0.50ND

1,3,5-Trimethylbenzene 0.50ND

1,3-Dichlorobenzene 0.50ND

1,3-Dichloropropane 0.50ND

1,4-Dichlorobenzene 0.50ND

2,2-Dichloropropane 0.50ND

2-Chlorotoluene 0.50ND

4-Chlorotoluene 0.50ND

4-Isopropyltoluene 0.50ND

Benzene 0.50ND

Bromobenzene 0.50ND

Bromodichloromethane 0.50ND

Bromoform 0.50ND

Bromomethane 0.50ND

Carbon tetrachloride 0.50ND

Chlorobenzene 0.50ND

Chloroethane 0.50ND

Chloroform 0.50ND

Chloromethane 0.50ND

cis-1,2-Dichloroethene 0.50ND

cis-1,3-Dichloropropene 0.50ND

Di-isopropyl ether 0.50ND

Dibromochloromethane 0.50ND

Dibromomethane 0.50ND

Dichlorodifluoromethane 0.50ND

Ethyl tert-butyl ether 0.50ND

Ethylbenzene 0.50ND

Hexachlorobutadiene 0.50ND

Isopropylbenzene 0.50ND

m,p-Xylene 1.0ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

17 of 18

Figure I-1.17

Page 37: Westside Subway Extension - Final Environmental Impact ...media.metro.net/projects_studies/westside/images/final_eir-eis/22.Vol 3_Part20.pdfSelenium 0.50 µg/L6.9 0.26 8/23/2011 12:33

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

Project: METRO WESTSIDE EXTENSION, 4953-10-1

CLIENT: Mactec

Work Order: 118577ANALYTICAL QC SUMMARY REPORT

TestCode: 8260_WP_LL

Sample ID: Q110624MB3

Batch ID: Q11VW116 TestNo: EPA 8260B Analysis Date: 6/24/2011

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: µg/L

PQL

Client ID: PBW

RunNo: 134423

SeqNo: 2198141

MBLKSampType: TestCode: 8260_WP_LL

Methylene chloride 1.0ND

MTBE 0.50ND

n-Butylbenzene 0.50ND

n-Propylbenzene 0.50ND

Naphthalene 0.50ND

o-Xylene 0.50ND

sec-Butylbenzene 0.50ND

Styrene 0.50ND

Tert-amyl methyl ether 0.50ND

Tert-Butanol 10ND

tert-Butylbenzene 0.50ND

Tetrachloroethene 0.50ND

Toluene 0.50ND

trans-1,2-Dichloroethene 0.50ND

Trichloroethene 0.50ND

Trichlorofluoromethane 0.50ND

Vinyl chloride 0.50ND

Surr: 1,2-Dichloroethane-d4 25.00 93.9 70 13023.480

Surr: 4-Bromofluorobenzene 25.00 95.1 70 13023.770

Surr: Dibromofluoromethane 25.00 93.2 70 13023.300

Surr: Toluene-d8 25.00 92.3 70 13023.070

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out Calculations are based on raw values

18 of 18

Figure I-1.18