Verticalrepmeanstatistics Copia

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

Calib Blank 1 612 1

g 5/16/2014 9:04:46AM

[0.00] %46.82mg/L13.45-28.7As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std1 613 2

g 5/16/2014 9:07:19AM

[0.05] %8.41mg/L3.7444.5As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std2 614 3

g 5/16/2014 9:09:51AM

[0.1] %15.23mg/L11.6176.2As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std3 615 4

g 5/16/2014 9:12:25AM

[1] %1.99mg/L13.79694.7As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std3 616 4

g 5/16/2014 9:15:00AM5/16/2014 9:15:01AM All analyte(s) passed QC.

1.0095 %1.881.0095mg/L0.01902701.6As 188.9795/16/2014 9:15:00AM QC value within limits for As 188.979 Recovery = 100.95%

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M5 E QU SHAN HAI 617 9

mg 5/16/2014 9:18:34AM

0.1011 %31.55mg/L0.031890.1011mg/L0.0318975.3As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M5 DP E QU SHAN HAI 618 10

mg 5/16/2014 9:22:08AM

0.0970 %3.27mg/L0.003180.0970mg/L0.0031872.5As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M6 E QU SHAN HAI 619 11

mg 5/16/2014 9:25:42AM

0.1081 %30.51mg/L0.032970.1081mg/L0.0329780.1As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M6 DP E QU SHAN HAI 620 12

mg 5/16/2014 9:29:17AM

0.1040 %14.72mg/L0.015300.1040mg/L0.0153077.3As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M7 E QU SHAN HAI 621 13

mg 5/16/2014 9:32:51AM

0.1166 %7.68mg/L0.008960.1166mg/L0.0089686.0As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M7 DP E QU SHAN HAI 622 14

mg 5/16/2014 9:36:26AM

0.1076 %13.14mg/L0.014140.1076mg/L0.0141479.8As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M8 E QU SHAN HAI 623 15

mg 5/16/2014 9:39:58AM

0.0856 %27.02mg/L0.023120.0856mg/L0.0231264.6As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M8 DP E QU SHAN HAI 624 16

mg 5/16/2014 9:43:30AM

0.0839 %18.60mg/L0.015600.0839mg/L0.0156063.5As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M9 E QU SHAN HAI 625 17

mg 5/16/2014 9:47:03AM

0.0874 %31.61mg/L0.027630.0874mg/L0.0276365.9As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std3 626 4

g 5/16/2014 9:50:36AM5/16/2014 9:50:37AM All analyte(s) passed QC.

1.0384 %1.281.0384mg/L0.01329721.5As 188.9795/16/2014 9:50:36AM QC value within limits for As 188.979 Recovery = 103.84%

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M9 DP E QU SHAN HAI 627 18

mg 5/16/2014 9:54:10AM

0.0895 %39.71mg/L0.035530.0895mg/L0.0355367.3As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M10 E QU SHAN HAI 628 19

mg 5/16/2014 9:57:44AM

0.0820 %12.33mg/L0.010110.0820mg/L0.0101162.2As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M10 DP E QU SHAN HAI 629 20

mg 5/16/2014 10:01:17AM

0.0647 %65.58mg/L0.042410.0647mg/L0.0424150.2As 188.979

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std3 630 4

g 5/16/2014 10:04:52AM5/16/2014 10:04:53AM All analyte(s) passed QC.

0.9846 %1.930.9846mg/L0.01903684.4As 188.9795/16/2014 10:04:52AM QC value within limits for As 188.979 Recovery = 98.46%

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

Calib Blank 1 631 1

g 5/16/2014 10:17:14AM

[0.00] %7.34mg/L5.8579.8Cd 228.802[0.00] %15.75mg/L33.30-211.4Cd 226.502[0.00] %10.58mg/L13.39-126.6Ni 231.604[0.00] %11.03mg/L25.21-228.6Ni 221.648[0.00] %6.16mg/L26.39-428.1Ni 232.003[0.00] %25.92mg/L19.1573.9Ni 341.476[0.00] %24.57mg/L13.3554.3Ni 227.022[0.00] %33.29mg/L12.96-38.9Pb 220.353[0.00] %389.67mg/L6.751.7Pb 261.418[0.00] %136.42mg/L23.33-17.1Pb 283.306[0.00] %64.39mg/L98.70153.3Pb 405.781[0.00] %59.93mg/L18.55-31.0Cr 205.560[0.00] %0.53mg/L35.656,732.6Cr 283.563[0.00] %0.90mg/L38.584,306.6Cr 284.325[0.00] %44.18mg/L34.9979.2Cr 357.869[0.00] %2.64mg/L8.44319.6Mn 257.610[0.00] %2.26mg/L860.0738,009.0Mn 259.372[0.00] %68.65mg/L23.8134.7Mn 260.568[0.00] %16.66mg/L10.80-64.8Mn 294.920[0.00] %77.22mg/L47.4161.4Mn 293.305[0.00] %5.44mg/L43.39-797.9Mn 279.482[0.00] %35.09mg/L17.19-49.0Mn 403.075[0.00] %1.42mg/L2.97209.3Zn 206.200[0.00] %1.08mg/L11.751,087.7Zn 213.857[0.00] %6.93mg/L21.00303.2Zn 202.548[0.00] %15.82mg/L13.30-84.1Zn 334.501[0.00] %34.59mg/L10.47-30.3Co 228.616[0.00] %23.91mg/L16.22-67.8Co 238.892[0.00] %178.51mg/L18.1010.1Co 230.786[0.00] %5.83mg/L20.38349.4Co 236.380[0.00] %681.80mg/L18.61-2.7Co 231.160[0.00] %12.44mg/L785.636,314.0Sr 421.552[0.00] %7.87mg/L106.791,357.1Sr 460.733[0.00] %20.65mg/L21.63104.7Sr 232.235[0.00] %9.36mg/L48.02513.2K 404.721[0.00] %70.86mg/L81,579.51115,120.9Al 396.153[0.00] %7.59mg/L1,543.0820,336.9Al 308.215

5/16/2014 10:17:15AM Saturated within auto integration window (code 4)[0.00] %78.11mg/L83,339.29106,697.5Al 394.401[0.00] %20.02mg/L1,034.295,165.3Al 237.313

[0.00] %4.07mg/L25.56628.3B 249.677[0.00] %1.67mg/L14.88891.8B 249.772[0.00] %48.25mg/L18.0037.3B 208.957[0.00] %275.63mg/L32.34-11.7B 182.578[0.00] %10.78mg/L15.54144.2Fe 238.204[0.00] %63.51mg/L22.8836.0Fe 239.562[0.00] %2.47mg/L14.91604.5Fe 259.939[0.00] %22.09mg/L13.9863.3Fe 234.349[0.00] %17.54mg/L11.07-63.1Fe 273.955[0.00] %13.54mg/L5.7542.4Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std1 multielemental 10% 632 2

g 5/16/2014 10:20:05AM

[0.01] %3.83mg/L7.12186.1Cd 228.802[0.01] %4.44mg/L19.13430.8Cd 226.502[0.01] %4.16mg/L42.261,015.8Ni 231.604[0.01] %52.48mg/L258.27492.2Ni 221.648[0.01] %7.12mg/L60.69852.2Ni 232.003[0.01] %4.10mg/L79.851,948.1Ni 341.476[0.01] %12.49mg/L57.71462.2Ni 227.022[0.1] %1.57mg/L3.10197.6Pb 220.353[0.1] %7.46mg/L19.32258.9Pb 261.418[0.1] %6.54mg/L37.98581.1Pb 283.306[0.1] %1.20mg/L18.761,559.9Pb 405.781

[0.01] %20.30mg/L26.03128.2Cr 205.560[0.01] %29.24mg/L270.34924.7Cr 283.563[0.01] %34.00mg/L181.12532.7Cr 284.325[0.01] %7.07mg/L62.55885.3Cr 357.869[0.1] %4.57mg/L929.2620,355.7Mn 257.610[0.1] %11.40mg/L2,728.9323,947.1Mn 259.372[0.1] %4.18mg/L433.4310,367.6Mn 260.568[0.1] %4.52mg/L314.026,944.1Mn 294.920[0.1] %4.06mg/L174.254,290.2Mn 293.305[0.1] %5.02mg/L208.434,155.1Mn 279.482[0.1] %3.74mg/L280.037,495.8Mn 403.075[0.1] %8.77mg/L94.131,073.5Zn 206.200[0.1] %6.50mg/L362.795,583.0Zn 213.857[0.1] %8.40mg/L146.791,746.5Zn 202.548[0.1] %6.73mg/L26.73397.4Zn 334.501[0.1] %4.94mg/L37.73764.4Co 228.616[0.1] %3.67mg/L99.112,699.3Co 238.892[0.1] %3.50mg/L22.13632.6Co 230.786[0.1] %5.03mg/L85.061,690.2Co 236.380[0.1] %5.17mg/L38.94753.6Co 231.160[1] %1.27mg/L60,793.264,776,134.8Sr 421.552[1] %6.50mg/L66,723.391,026,550.0Sr 460.733[1] %4.28mg/L29.65692.3Sr 232.235

[30] %7.27mg/L1,140.1915,680.1K 404.721[0.1] %134.43mg/L27,087.5520,150.3Al 396.153[0.1] %40.10mg/L7,465.9918,618.5Al 308.215[0.1] %145.17mg/L26,831.1118,482.7Al 394.401[0.1] %34.37mg/L1,535.384,466.9Al 237.313[0.2] %4.20mg/L256.716,106.2B 249.677[0.2] %4.65mg/L536.3411,543.5B 249.772[0.2] %4.74mg/L21.28449.0B 208.957[0.2] %2.59mg/L5.62217.2B 182.578

[0.04] %5.14mg/L730.9414,233.7Fe 238.204[0.04] %5.15mg/L953.3818,502.9Fe 239.562

[0.04] %4.80mg/L900.2118,766.8Fe 259.939[0.04] %4.68mg/L285.086,096.6Fe 234.349[0.04] %5.65mg/L123.992,195.3Fe 273.955[0.01] %25.04mg/L6.8827.5Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std2 multielemental 10% 633 3

g 5/16/2014 10:22:58AM

[0.02] %3.31mg/L12.21369.3Cd 228.802[0.02] %0.79mg/L6.30799.2Cd 226.502[0.02] %1.50mg/L30.542,041.9Ni 231.604[0.02] %2.64mg/L39.721,501.9Ni 221.648[0.02] %0.69mg/L11.371,651.6Ni 232.003[0.02] %1.96mg/L74.683,812.5Ni 341.476[0.02] %1.89mg/L17.79939.9Ni 227.022[0.2] %1.90mg/L7.28383.1Pb 220.353[0.2] %3.99mg/L20.21507.0Pb 261.418[0.2] %1.64mg/L18.231,109.9Pb 283.306[0.2] %3.30mg/L94.032,848.4Pb 405.781

[0.02] %5.14mg/L12.78248.7Cr 205.560[0.02] %82.06mg/L541.09659.4Cr 283.563

5/16/2014 10:22:58AM Standard intensity and concentration values are not in the same order.[0.02] %81.36mg/L419.89516.1Cr 284.325

5/16/2014 10:22:58AM Standard intensity and concentration values are not in the same order.[0.02] %3.09mg/L51.831,675.0Cr 357.869[0.2] %1.43mg/L584.0840,987.4Mn 257.610[0.2] %2.40mg/L1,029.8142,894.7Mn 259.372[0.2] %1.42mg/L293.4620,691.0Mn 260.568[0.2] %1.46mg/L201.2913,795.6Mn 294.920[0.2] %1.31mg/L112.738,575.2Mn 293.305[0.2] %0.70mg/L55.107,842.2Mn 279.482[0.2] %2.34mg/L337.0314,433.5Mn 403.075[0.2] %2.40mg/L53.272,223.9Zn 206.200[0.2] %1.33mg/L149.6411,221.1Zn 213.857[0.2] %2.61mg/L94.333,614.2Zn 202.548[0.2] %7.73mg/L59.84774.2Zn 334.501[0.2] %1.12mg/L17.081,526.9Co 228.616[0.2] %1.41mg/L81.125,763.7Co 238.892[0.2] %0.71mg/L8.941,252.7Co 230.786[0.2] %1.44mg/L48.303,346.6Co 236.380[0.2] %1.52mg/L23.131,517.7Co 231.160[2] %1.22mg/L110,581.809,052,940.9Sr 421.552[2] %6.05mg/L122,020.832,016,078.0Sr 460.733[2] %3.33mg/L46.761,404.5Sr 232.235

[50] %8.24mg/L1,847.1722,421.7K 404.721[0.2] %392.24mg/L51,615.5013,159.1Al 396.153

5/16/2014 10:22:58AM Standard intensity and concentration values are not in the same order.[0.2] %64.44mg/L8,840.6713,719.6Al 308.215

5/16/2014 10:22:58AM Standard intensity and concentration values are not in the same order.[0.2] %1,191.89mg/L44,605.843,742.4Al 394.401

5/16/2014 10:22:58AM Standard intensity and concentration values are not in the same order.[0.2] %74.68mg/L2,797.113,745.3Al 237.313

5/16/2014 10:22:58AM Standard intensity and concentration values are not in the same order.[0.6] %4.44mg/L791.3317,812.5B 249.677[0.6] %4.43mg/L1,486.8933,552.2B 249.772[0.6] %3.92mg/L51.401,311.1B 208.957[0.6] %7.13mg/L47.55666.5B 182.578

[0.06] %1.71mg/L369.1621,531.6Fe 238.204[0.06] %1.66mg/L464.2228,032.3Fe 239.562

[0.06] %1.52mg/L428.9228,278.5Fe 259.939[0.06] %1.74mg/L159.999,189.8Fe 234.349[0.06] %2.43mg/L79.873,288.5Fe 273.955[0.02] %3.58mg/L1.3036.3Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std3 multielemental 10% 634 4

g 5/16/2014 10:25:53AM

[0.03] %2.07mg/L9.66466.3Cd 228.802[0.03] %3.81mg/L38.291,004.1Cd 226.502[0.03] %2.36mg/L61.522,601.3Ni 231.604[0.03] %5.13mg/L90.401,763.4Ni 221.648[0.03] %2.87mg/L61.662,148.4Ni 232.003[0.03] %2.32mg/L118.015,077.5Ni 341.476[0.03] %2.70mg/L32.271,196.8Ni 227.022[0.3] %4.15mg/L20.46493.4Pb 220.353[0.3] %4.63mg/L30.86665.8Pb 261.418[0.3] %3.86mg/L57.051,477.7Pb 283.306[0.3] %7.16mg/L270.163,774.5Pb 405.781

[0.03] %5.19mg/L17.47336.3Cr 205.560[0.03] %7.41mg/L185.072,497.5Cr 283.563

5/16/2014 10:25:53AM Standard intensity and concentration values are not in the same order.[0.03] %5.48mg/L115.512,108.9Cr 284.325

5/16/2014 10:25:53AM Standard intensity and concentration values are not in the same order.[0.03] %2.71mg/L65.692,427.6Cr 357.869[0.3] %3.93mg/L1,941.3349,419.5Mn 257.610[0.3] %7.51mg/L3,987.4253,089.5Mn 259.372[0.3] %2.11mg/L568.2026,898.3Mn 260.568[0.3] %2.38mg/L423.7317,823.4Mn 294.920[0.3] %1.74mg/L192.7611,091.4Mn 293.305[0.3] %5.88mg/L613.3210,434.1Mn 279.482[0.3] %1.90mg/L381.2120,063.0Mn 403.075[0.3] %2.98mg/L84.242,822.7Zn 206.200[0.3] %4.37mg/L653.5114,970.5Zn 213.857[0.3] %3.26mg/L150.064,600.9Zn 202.548[0.3] %6.95mg/L73.531,057.3Zn 334.501[0.3] %2.16mg/L42.131,953.2Co 228.616[0.3] %2.13mg/L162.037,604.5Co 238.892[0.3] %2.32mg/L36.721,580.1Co 230.786[0.3] %2.46mg/L105.774,295.0Co 236.380[0.3] %2.67mg/L51.731,933.9Co 231.160[3] %4.27mg/L498,675.3511,686,828.3Sr 421.552[3] %5.50mg/L132,851.432,413,403.3Sr 460.733[3] %2.05mg/L34.951,705.1Sr 232.235

[100] %11.65mg/L3,431.7929,456.0K 404.721[0.3] %59.38mg/L127,928.00215,443.2Al 396.153

5/16/2014 10:25:53AM Standard intensity and concentration values are not in the same order.[0.3] %59.20mg/L30,869.0352,139.3Al 308.215

5/16/2014 10:25:53AM Standard intensity and concentration values are not in the same order.[0.3] %73.48mg/L126,508.52172,156.0Al 394.401

5/16/2014 10:25:53AM Standard intensity and concentration values are not in the same order.[0.3] %61.49mg/L4,859.597,903.5Al 237.313

5/16/2014 10:25:53AM Standard intensity and concentration values are not in the same order.[1] %1.67mg/L446.8226,834.8B 249.677[1] %1.98mg/L988.3949,865.3B 249.772[1] %3.12mg/L63.992,051.0B 208.957[1] %4.07mg/L42.851,053.3B 182.578

[0.08] %2.08mg/L515.4824,782.3Fe 238.204[0.08] %4.12mg/L1,243.0130,187.2Fe 239.562

[0.08] %1.99mg/L652.6332,780.6Fe 259.939[0.08] %2.11mg/L224.0210,626.4Fe 234.349[0.08] %1.06mg/L40.003,780.6Fe 273.955[0.03] %7.88mg/L2.8736.4Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std4 multielemental 10% 635 5

g 5/16/2014 10:28:48AM

[0.05] %3.30mg/L16.26493.1Cd 228.802[0.05] %2.80mg/L33.811,206.7Cd 226.502[0.05] %1.09mg/L34.693,196.6Ni 231.604[0.05] %28.42mg/L571.192,010.0Ni 221.648[0.05] %4.73mg/L91.201,928.1Ni 232.003

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.05] %4.99mg/L233.224,677.6Ni 341.476

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.05] %2.41mg/L35.701,478.8Ni 227.022[0.5] %4.13mg/L25.80624.4Pb 220.353[0.5] %3.30mg/L23.12701.5Pb 261.418[0.5] %1.49mg/L20.911,403.4Pb 283.306

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.5] %10.43mg/L390.663,744.5Pb 405.781

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.05] %5.82mg/L31.79546.3Cr 205.560[0.05] %3.27mg/L155.614,755.5Cr 283.563

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.05] %4.17mg/L123.742,966.5Cr 284.325

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.05] %13.63mg/L409.843,007.1Cr 357.869[0.5] %6.45mg/L3,936.1461,013.6Mn 257.610[0.5] %12.49mg/L6,278.1750,272.9Mn 259.372

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.5] %1.48mg/L492.1233,180.1Mn 260.568[0.5] %1.33mg/L297.4222,307.5Mn 294.920[0.5] %1.78mg/L243.6413,718.3Mn 293.305[0.5] %8.20mg/L749.879,145.3Mn 279.482

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.5] %1.97mg/L378.0219,161.7Mn 403.075

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.5] %3.45mg/L100.682,919.9Zn 206.200[0.5] %8.50mg/L1,009.8811,880.0Zn 213.857

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.5] %3.33mg/L157.774,736.2Zn 202.548[0.5] %6.27mg/L55.32882.2Zn 334.501

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.5] %1.38mg/L33.942,454.7Co 228.616[0.5] %1.25mg/L121.849,753.9Co 238.892[0.5] %1.40mg/L27.741,980.0Co 230.786[0.5] %0.62mg/L33.435,386.2Co 236.380[0.5] %0.89mg/L21.542,422.7Co 231.160[5] %5.65mg/L783,141.7513,856,443.2Sr 421.552[5] %4.73mg/L104,454.542,206,398.6Sr 460.733

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[5] %3.08mg/L69.922,273.5Sr 232.235

[150] %15.78mg/L3,854.8324,423.6K 404.7215/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.

[0.5] %306.43mg/L59,857.4619,533.5Al 396.1535/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.

[0.5] %37.17mg/L12,505.7233,646.3Al 308.2155/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.5/16/2014 10:28:48AM Saturated within auto integration window (code 4)

[0.5] %367.61mg/L50,373.0913,702.8Al 394.4015/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.

[0.5] %115.19mg/L28,564.6824,798.6Al 237.3135/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.5/16/2014 10:28:48AM Saturated within auto integration window (code 4)

[2] %1.79mg/L869.9248,684.6B 249.677[2] %1.65mg/L1,481.8689,810.8B 249.772[2] %1.39mg/L51.593,701.1B 208.957[2] %1.80mg/L33.671,865.8B 182.578

[0.1] %3.51mg/L833.2323,736.4Fe 238.2045/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.

[0.1] %3.60mg/L1,111.7430,918.8Fe 239.562[0.1] %3.56mg/L1,104.2331,037.9Fe 259.939

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.1] %3.94mg/L399.9710,157.8Fe 234.349

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.1] %3.73mg/L136.273,649.5Fe 273.955

5/16/2014 10:28:48AM Standard intensity and concentration values are not in the same order.[0.05] %12.11mg/L7.5462.3Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M5 E QU SHAN HAI 636 9

mg 5/16/2014 10:31:41AM

-0.001 %76.73mg/L0.0008-0.001mg/L0.000876.1Cd 228.802-0.009 %5.30mg/L0.0005-0.009mg/L0.0005-48.1Cd 226.502-0.008 %0.46mg/L0.0000-0.008mg/L0.0000-115.7Ni 231.604-0.013 %21.77mg/L0.0028-0.013mg/L0.0028-292.5Ni 221.648-0.019 %0.33mg/L0.0001-0.019mg/L0.0001-289.9Ni 232.003-0.011 %2.59mg/L0.0003-0.011mg/L0.0003-26.3Ni 341.476-0.006 %10.51mg/L0.0006-0.006mg/L0.00061.6Ni 227.022-0.019 %79.56mg/L0.0152-0.019mg/L0.015244.2Pb 220.353-0.024 %89.21mg/L0.0217-0.024mg/L0.021782.5Pb 261.418-0.128 %0.70mg/L0.0009-0.128mg/L0.0009-70.2Pb 283.306-0.073 %22.42mg/L0.0163-0.073mg/L0.0163196.9Pb 405.7810.001 %68.34mg/L0.00070.001mg/L0.000726.4Cr 205.5600.033 %16.38mg/L0.00550.033mg/L0.00552,856.6Cr 283.5630.045 %13.35mg/L0.00600.045mg/L0.00602,660.1Cr 284.3250.000 %463.12mg/L0.00060.000mg/L0.0006273.9Cr 357.869-0.061 %1.43mg/L0.0009-0.061mg/L0.0009650.7Mn 257.610-0.428 %0.73mg/L0.0031-0.428mg/L0.0031-29,823.0Mn 259.372-0.051 %2.19mg/L0.0011-0.051mg/L0.0011280.8Mn 260.568-0.050 %2.12mg/L0.0011-0.050mg/L0.0011223.2Mn 294.920-0.051 %2.86mg/L0.0015-0.051mg/L0.0015130.9Mn 293.305-0.690 %3.63mg/L0.0251-0.690mg/L0.0251-10,527.0Mn 279.482-0.085 %1.94mg/L0.0017-0.085mg/L0.0017305.0Mn 403.075-0.071 %25.68mg/L0.0183-0.071mg/L0.018395.4Zn 206.200-0.130 %11.66mg/L0.0152-0.130mg/L0.0152146.8Zn 213.857-0.072 %21.05mg/L0.0151-0.072mg/L0.0151156.7Zn 202.548-0.207 %9.17mg/L0.0190-0.207mg/L0.0190-152.4Zn 334.501-0.053 %0.98mg/L0.0005-0.053mg/L0.00059.1Co 228.616-0.043 %2.42mg/L0.0010-0.043mg/L0.001011.7Co 238.892-0.059 %6.84mg/L0.0040-0.059mg/L0.0040-2.4Co 230.786-0.034 %2.71mg/L0.0009-0.034mg/L0.0009229.2Co 236.380-0.060 %7.59mg/L0.0046-0.060mg/L0.0046-21.9Co 231.160-0.383 %1.77mg/L0.0068-0.383mg/L0.0068788,800.1Sr 421.552

-1.042 %1.75mg/L0.0182-1.042mg/L0.0182114,308.4Sr 460.733-0.086 %35.08mg/L0.0302-0.086mg/L0.0302192.8Sr 232.235-49.95 %1.52mg/L0.758-49.95mg/L0.758907.0K 404.7213.466 %55.86mg/L1.93603.466mg/L1.9360492,816.9Al 396.1531.942 %64.96mg/L1.26141.942mg/L1.2614152,565.1Al 308.2154.097 %72.96mg/L2.98924.097mg/L2.9892442,863.6Al 394.401

5/16/2014 10:31:41AM Saturated within auto integration window (code 4)1.103 %58.52mg/L0.64571.103mg/L0.645749,751.3Al 237.3130.860 %3.06mg/L0.02630.860mg/L0.026322,287.8B 249.6770.849 %3.17mg/L0.02690.849mg/L0.026940,889.9B 249.7720.851 %3.71mg/L0.03160.851mg/L0.03161,669.6B 208.957-26.83 %4.44mg/L1.192-26.83mg/L1.192-24,921.3B 182.578-0.008 %16.45mg/L0.0013-0.008mg/L0.0013752.7Fe 238.204-0.008 %13.93mg/L0.0012-0.008mg/L0.0012818.2Fe 239.562-0.009 %14.50mg/L0.0013-0.009mg/L0.0013703.7Fe 259.939-0.006 %19.89mg/L0.0013-0.006mg/L0.0013464.1Fe 234.349-0.008 %23.94mg/L0.0019-0.008mg/L0.0019100.4Fe 273.9550.029 %22.10mg/L0.00650.029mg/L0.006540.5Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M5 DP E QU SHAN HAI 637 10

mg 5/16/2014 10:35:29AM

-0.004 %28.39mg/L0.0010-0.004mg/L0.001051.7Cd 228.802-0.012 %3.45mg/L0.0004-0.012mg/L0.0004-108.6Cd 226.502-0.008 %4.02mg/L0.0003-0.008mg/L0.0003-106.7Ni 231.604-0.017 %24.45mg/L0.0041-0.017mg/L0.0041-464.1Ni 221.648-0.019 %2.17mg/L0.0004-0.019mg/L0.0004-299.0Ni 232.003-0.011 %3.54mg/L0.0004-0.011mg/L0.00044.4Ni 341.476-0.006 %3.62mg/L0.0002-0.006mg/L0.0002-2.0Ni 227.022-0.024 %22.83mg/L0.0054-0.024mg/L0.005438.7Pb 220.353-0.000 %10,155.48mg/L0.0156-0.000mg/L0.0156116.5Pb 261.418-0.101 %14.89mg/L0.0150-0.101mg/L0.01505.0Pb 283.306-0.099 %11.79mg/L0.0117-0.099mg/L0.01170.6Pb 405.7810.002 %55.27mg/L0.00130.002mg/L0.001340.3Cr 205.560-0.004 %237.98mg/L0.0102-0.004mg/L0.0102-731.7Cr 283.5630.005 %256.61mg/L0.01380.005mg/L0.0138184.7Cr 284.3250.000 %139.59mg/L0.00040.000mg/L0.0004283.6Cr 357.869-0.062 %2.23mg/L0.0014-0.062mg/L0.0014520.0Mn 257.610-0.486 %0.86mg/L0.0042-0.486mg/L0.0042-35,551.2Mn 259.372-0.053 %3.38mg/L0.0018-0.053mg/L0.0018211.4Mn 260.568-0.050 %1.65mg/L0.0008-0.050mg/L0.0008209.0Mn 294.920-0.051 %7.31mg/L0.0037-0.051mg/L0.0037137.6Mn 293.305-0.351 %22.40mg/L0.0786-0.351mg/L0.0786-4,253.4Mn 279.482-0.085 %3.70mg/L0.0031-0.085mg/L0.0031319.2Mn 403.075-0.056 %54.12mg/L0.0302-0.056mg/L0.0302187.0Zn 206.200-0.126 %15.40mg/L0.0194-0.126mg/L0.0194245.0Zn 213.857-0.057 %53.45mg/L0.0306-0.057mg/L0.0306294.5Zn 202.548-0.084 %31.55mg/L0.0265-0.084mg/L0.026570.7Zn 334.501-0.053 %7.06mg/L0.0037-0.053mg/L0.003711.7Co 228.616-0.047 %7.46mg/L0.0035-0.047mg/L0.0035-63.2Co 238.892-0.059 %4.17mg/L0.0024-0.059mg/L0.0024-2.6Co 230.786-0.030 %2.86mg/L0.0009-0.030mg/L0.0009271.1Co 236.380-0.059 %9.07mg/L0.0053-0.059mg/L0.0053-15.6Co 231.160-0.584 %2.25mg/L0.0132-0.584mg/L0.0132235,015.8Sr 421.552-1.254 %0.58mg/L0.0073-1.254mg/L0.007321,636.2Sr 460.733-0.319 %21.26mg/L0.0679-0.319mg/L0.067988.5Sr 232.235-56.46 %0.21mg/L0.120-56.46mg/L0.120-75.5K 404.7212.370 %3.69mg/L0.08752.370mg/L0.0875344,598.1Al 396.153

5/16/2014 10:35:29AM Saturated within auto integration window (code 4)

3.890 %16.57mg/L0.64483.890mg/L0.6448298,467.8Al 308.2158.370 %32.25mg/L2.69908.370mg/L2.6990885,040.9Al 394.4012.164 %17.58mg/L0.38032.164mg/L0.380399,647.8Al 237.3130.416 %6.14mg/L0.02550.416mg/L0.025511,604.5B 249.6770.405 %5.48mg/L0.02220.405mg/L0.022221,188.5B 249.7720.514 %9.33mg/L0.04800.514mg/L0.04801,050.6B 208.957-3.424 %27.40mg/L0.9383-3.424mg/L0.9383-3,134.1B 182.578-0.002 %240.79mg/L0.0042-0.002mg/L0.00422,246.5Fe 238.204-0.002 %189.24mg/L0.0044-0.002mg/L0.00442,791.8Fe 239.562-0.003 %146.16mg/L0.0043-0.003mg/L0.00432,597.3Fe 259.939-0.001 %416.14mg/L0.0045-0.001mg/L0.00451,032.4Fe 234.349-0.001 %382.98mg/L0.0041-0.001mg/L0.0041372.0Fe 273.9550.036 %26.09mg/L0.00950.036mg/L0.009548.2Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M6 E QU SHAN HAI 638 11

mg 5/16/2014 10:39:14AM

-0.012 %14.71mg/L0.0018-0.012mg/L0.0018-34.9Cd 228.802-0.005 %9.55mg/L0.0005-0.005mg/L0.000548.2Cd 226.502-0.005 %2.99mg/L0.0002-0.005mg/L0.000243.7Ni 231.604-0.005 %21.99mg/L0.0011-0.005mg/L0.001138.4Ni 221.648-0.010 %3.63mg/L0.0004-0.010mg/L0.000450.2Ni 232.003-0.010 %2.08mg/L0.0002-0.010mg/L0.000237.3Ni 341.476-0.007 %9.86mg/L0.0007-0.007mg/L0.0007-27.2Ni 227.022-0.024 %13.87mg/L0.0033-0.024mg/L0.003338.3Pb 220.353-0.039 %88.04mg/L0.0346-0.039mg/L0.034661.4Pb 261.418-0.089 %26.09mg/L0.0231-0.089mg/L0.023140.2Pb 283.306-0.102 %23.26mg/L0.0237-0.102mg/L0.0237-20.2Pb 405.7810.006 %121.22mg/L0.00710.006mg/L0.007178.2Cr 205.560-0.056 %10.72mg/L0.0060-0.056mg/L0.0060-5,623.9Cr 283.563-0.056 %6.83mg/L0.0038-0.056mg/L0.0038-3,647.8Cr 284.3250.008 %188.62mg/L0.01600.008mg/L0.0160781.2Cr 357.869-0.068 %0.67mg/L0.0005-0.068mg/L0.0005-188.4Mn 257.610-0.511 %0.02mg/L0.0001-0.511mg/L0.0001-38,041.5Mn 259.372-0.056 %0.30mg/L0.0002-0.056mg/L0.0002-39.2Mn 260.568-0.052 %1.05mg/L0.0005-0.052mg/L0.0005125.9Mn 294.920-0.055 %1.74mg/L0.0010-0.055mg/L0.001011.5Mn 293.305-0.077 %0.85mg/L0.0007-0.077mg/L0.0007819.1Mn 279.482-0.090 %3.81mg/L0.0034-0.090mg/L0.0034121.7Mn 403.075-0.120 %4.04mg/L0.0049-0.120mg/L0.0049-192.1Zn 206.200-0.176 %0.86mg/L0.0015-0.176mg/L0.0015-990.4Zn 213.857-0.117 %1.03mg/L0.0012-0.117mg/L0.0012-272.8Zn 202.548-0.072 %121.76mg/L0.0871-0.072mg/L0.087193.5Zn 334.501-0.056 %3.36mg/L0.0019-0.056mg/L0.0019-6.6Co 228.616-0.043 %2.75mg/L0.0012-0.043mg/L0.001212.4Co 238.892-0.058 %9.04mg/L0.0052-0.058mg/L0.00520.8Co 230.786-0.066 %4.05mg/L0.0027-0.066mg/L0.0027-113.3Co 236.380-0.061 %5.09mg/L0.0031-0.061mg/L0.0031-27.6Co 231.160-0.672 %0.01mg/L0.0000-0.672mg/L0.0000-5,775.6Sr 421.552-1.306 %0.05mg/L0.0006-1.306mg/L0.0006-1,093.2Sr 460.733-0.682 %6.95mg/L0.0474-0.682mg/L0.0474-73.5Sr 232.235-57.24 %1.21mg/L0.690-57.24mg/L0.690-192.8K 404.721-1.027 %0.20mg/L0.0021-1.027mg/L0.0021-115,103.2Al 396.153-0.359 %0.16mg/L0.0006-0.359mg/L0.0006-19,751.4Al 308.215-1.212 %0.16mg/L0.0020-1.212mg/L0.0020-106,549.6Al 394.401-0.064 %1.18mg/L0.0008-0.064mg/L0.0008-5,178.0Al 237.313-0.018 %460.63mg/L0.0809-0.018mg/L0.08091,148.0B 249.677-0.024 %337.41mg/L0.0804-0.024mg/L0.08042,162.9B 249.772-0.012 %713.09mg/L0.0834-0.012mg/L0.083483.0B 208.957

-0.032 %273.82mg/L0.0889-0.032mg/L0.088922.9B 182.578-0.010 %0.85mg/L0.0001-0.010mg/L0.000138.2Fe 238.204-0.012 %0.67mg/L0.0001-0.012mg/L0.0001-158.5Fe 239.562-0.013 %0.79mg/L0.0001-0.013mg/L0.0001-612.0Fe 259.939-0.011 %1.58mg/L0.0002-0.011mg/L0.0002-77.7Fe 234.349-0.010 %7.72mg/L0.0008-0.010mg/L0.00089.5Fe 273.955-0.028 %40.35mg/L0.0113-0.028mg/L0.0113-22.6Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M6 DP E QU SHAN HAI 639 12

mg 5/16/2014 10:43:03AM

-0.014 %7.36mg/L0.0010-0.014mg/L0.0010-48.7Cd 228.802-0.005 %14.17mg/L0.0007-0.005mg/L0.000743.0Cd 226.502-0.005 %5.50mg/L0.0003-0.005mg/L0.000350.8Ni 231.604-0.005 %6.75mg/L0.0003-0.005mg/L0.000338.8Ni 221.648-0.008 %9.15mg/L0.0007-0.008mg/L0.0007144.9Ni 232.003-0.011 %4.22mg/L0.0004-0.011mg/L0.000412.7Ni 341.476-0.005 %3.55mg/L0.0002-0.005mg/L0.00028.1Ni 227.022-0.007 %290.87mg/L0.0197-0.007mg/L0.019759.4Pb 220.353-0.023 %43.15mg/L0.0098-0.023mg/L0.009884.7Pb 261.418-0.039 %12.64mg/L0.0049-0.039mg/L0.0049181.9Pb 283.306-0.032 %97.95mg/L0.0317-0.032mg/L0.0317499.3Pb 405.7810.023 %2.11mg/L0.00050.023mg/L0.0005261.1Cr 205.560-0.043 %1.84mg/L0.0008-0.043mg/L0.0008-4,456.7Cr 283.563-0.048 %0.21mg/L0.0001-0.048mg/L0.0001-3,126.8Cr 284.3250.147 %4.19mg/L0.00620.147mg/L0.00629,172.2Cr 357.869-0.068 %0.25mg/L0.0002-0.068mg/L0.0002-227.5Mn 257.610-0.511 %0.03mg/L0.0001-0.511mg/L0.0001-38,013.5Mn 259.372-0.057 %0.22mg/L0.0001-0.057mg/L0.0001-62.4Mn 260.568-0.052 %0.95mg/L0.0005-0.052mg/L0.0005118.9Mn 294.920-0.055 %3.84mg/L0.0021-0.055mg/L0.002113.0Mn 293.305-0.078 %3.24mg/L0.0025-0.078mg/L0.0025804.4Mn 279.482-0.088 %8.77mg/L0.0077-0.088mg/L0.0077192.2Mn 403.075-0.012 %12.07mg/L0.0014-0.012mg/L0.0014446.3Zn 206.200-0.028 %5.98mg/L0.0017-0.028mg/L0.00172,647.1Zn 213.857-0.005 %29.67mg/L0.0015-0.005mg/L0.0015793.2Zn 202.5480.093 %8.05mg/L0.00750.093mg/L0.0075392.1Zn 334.501-0.052 %1.47mg/L0.0008-0.052mg/L0.000812.4Co 228.616-0.043 %2.61mg/L0.0011-0.043mg/L0.001113.0Co 238.892-0.056 %3.45mg/L0.0019-0.056mg/L0.00196.6Co 230.786-0.065 %3.22mg/L0.0021-0.065mg/L0.0021-105.8Co 236.380-0.059 %6.96mg/L0.0041-0.059mg/L0.0041-14.9Co 231.160-0.672 %0.01mg/L0.0001-0.672mg/L0.0001-5,696.6Sr 421.552-1.306 %0.02mg/L0.0003-1.306mg/L0.0003-890.2Sr 460.733-0.643 %3.51mg/L0.0226-0.643mg/L0.0226-56.3Sr 232.235-57.04 %0.92mg/L0.527-57.04mg/L0.527-163.0K 404.721-1.026 %0.04mg/L0.0004-1.026mg/L0.0004-114,927.3Al 396.153-0.360 %0.06mg/L0.0002-0.360mg/L0.0002-19,804.5Al 308.215-1.212 %0.14mg/L0.0017-1.212mg/L0.0017-106,621.8Al 394.401-0.065 %0.14mg/L0.0001-0.065mg/L0.0001-5,212.7Al 237.313-0.036 %4.71mg/L0.0017-0.036mg/L0.0017697.2B 249.677-0.042 %2.52mg/L0.0011-0.042mg/L0.00111,373.9B 249.772-0.035 %7.85mg/L0.0028-0.035mg/L0.002839.4B 208.957-1.011 %4.33mg/L0.0438-1.011mg/L0.0438-887.5B 182.578-0.010 %0.73mg/L0.0001-0.010mg/L0.0001186.1Fe 238.204-0.011 %0.77mg/L0.0001-0.011mg/L0.0001107.2Fe 239.562-0.012 %0.44mg/L0.0001-0.012mg/L0.0001-362.7Fe 259.939-0.010 %1.55mg/L0.0002-0.010mg/L0.000221.2Fe 234.349-0.010 %8.71mg/L0.0009-0.010mg/L0.000919.7Fe 273.955

-0.033 %38.21mg/L0.0127-0.033mg/L0.0127-28.3Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M7 E QU SHAN HAI 640 13

mg 5/16/2014 10:46:51AM

-0.012 %14.68mg/L0.0018-0.012mg/L0.0018-33.9Cd 228.802-0.004 %23.93mg/L0.0009-0.004mg/L0.000979.1Cd 226.502-0.005 %7.62mg/L0.0004-0.005mg/L0.000467.8Ni 231.604-0.005 %5.69mg/L0.0003-0.005mg/L0.000343.5Ni 221.648-0.008 %2.65mg/L0.0002-0.008mg/L0.0002130.7Ni 232.003-0.011 %3.65mg/L0.0004-0.011mg/L0.0004-14.5Ni 341.476-0.006 %13.35mg/L0.0009-0.006mg/L0.0009-21.6Ni 227.022-0.017 %66.88mg/L0.0113-0.017mg/L0.011346.9Pb 220.353-0.039 %23.22mg/L0.0091-0.039mg/L0.009161.6Pb 261.418-0.094 %11.88mg/L0.0112-0.094mg/L0.011224.3Pb 283.306-0.087 %14.50mg/L0.0127-0.087mg/L0.012788.7Pb 405.7810.007 %10.38mg/L0.00080.007mg/L0.000893.3Cr 205.560-0.054 %0.61mg/L0.0003-0.054mg/L0.0003-5,441.5Cr 283.563-0.055 %1.01mg/L0.0006-0.055mg/L0.0006-3,585.4Cr 284.3250.052 %1.33mg/L0.00070.052mg/L0.00073,426.6Cr 357.869-0.068 %0.33mg/L0.0002-0.068mg/L0.0002-209.8Mn 257.610-0.511 %0.03mg/L0.0002-0.511mg/L0.0002-37,983.8Mn 259.372-0.056 %0.44mg/L0.0002-0.056mg/L0.0002-31.4Mn 260.568-0.053 %0.62mg/L0.0003-0.053mg/L0.000384.7Mn 294.920-0.057 %3.08mg/L0.0018-0.057mg/L0.0018-36.4Mn 293.305-0.076 %2.62mg/L0.0020-0.076mg/L0.0020829.4Mn 279.482-0.085 %4.46mg/L0.0038-0.085mg/L0.0038315.5Mn 403.075-0.000 %433.29mg/L0.0019-0.000mg/L0.0019512.1Zn 206.200-0.015 %8.54mg/L0.0012-0.015mg/L0.00122,977.7Zn 213.8570.005 %11.42mg/L0.00060.005mg/L0.0006889.8Zn 202.5480.100 %25.61mg/L0.02570.100mg/L0.0257405.5Zn 334.501-0.054 %1.96mg/L0.0011-0.054mg/L0.00116.3Co 228.616-0.043 %1.54mg/L0.0007-0.043mg/L0.000717.4Co 238.892-0.054 %6.12mg/L0.0033-0.054mg/L0.003316.8Co 230.786-0.065 %8.74mg/L0.0057-0.065mg/L0.0057-102.3Co 236.380-0.058 %14.62mg/L0.0085-0.058mg/L0.0085-12.8Co 231.160-0.672 %0.01mg/L0.0001-0.672mg/L0.0001-5,817.6Sr 421.552-1.306 %0.01mg/L0.0001-1.306mg/L0.0001-1,029.5Sr 460.733-0.642 %0.64mg/L0.0041-0.642mg/L0.0041-56.0Sr 232.235-56.72 %2.11mg/L1.198-56.72mg/L1.198-115.5K 404.721-1.027 %0.07mg/L0.0007-1.027mg/L0.0007-115,111.5Al 396.153-0.359 %0.17mg/L0.0006-0.359mg/L0.0006-19,768.6Al 308.215-1.214 %0.13mg/L0.0016-1.214mg/L0.0016-106,801.4Al 394.401-0.065 %0.72mg/L0.0005-0.065mg/L0.0005-5,222.0Al 237.313-0.065 %3.17mg/L0.0020-0.065mg/L0.002016.0B 249.677-0.069 %0.81mg/L0.0006-0.069mg/L0.0006144.8B 249.772-0.070 %3.12mg/L0.0022-0.070mg/L0.0022-23.6B 208.957-0.525 %2.73mg/L0.0143-0.525mg/L0.0143-435.2B 182.578-0.010 %1.00mg/L0.0001-0.010mg/L0.0001208.4Fe 238.204-0.011 %1.38mg/L0.0001-0.011mg/L0.0001135.8Fe 239.562-0.012 %0.37mg/L0.0000-0.012mg/L0.0000-350.2Fe 259.939-0.011 %3.31mg/L0.0003-0.011mg/L0.00034.0Fe 234.349-0.009 %6.91mg/L0.0007-0.009mg/L0.000748.0Fe 273.955-0.035 %47.06mg/L0.0163-0.035mg/L0.0163-30.1Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M7 DP E QU SHAN HAI 641 14

mg 5/16/2014 10:50:38AM

-0.012 %6.37mg/L0.0008-0.012mg/L0.0008-33.5Cd 228.802-0.005 %36.07mg/L0.0016-0.005mg/L0.001660.4Cd 226.502-0.005 %1.42mg/L0.0001-0.005mg/L0.000166.8Ni 231.604-0.006 %7.22mg/L0.0004-0.006mg/L0.00044.4Ni 221.648-0.009 %7.99mg/L0.0007-0.009mg/L0.0007126.0Ni 232.003-0.011 %4.22mg/L0.0005-0.011mg/L0.0005-6.3Ni 341.476-0.006 %8.47mg/L0.0005-0.006mg/L0.0005-18.2Ni 227.022-0.025 %33.94mg/L0.0085-0.025mg/L0.008537.0Pb 220.353-0.040 %40.77mg/L0.0165-0.040mg/L0.016559.8Pb 261.418-0.080 %10.87mg/L0.0086-0.080mg/L0.008665.9Pb 283.306-0.096 %18.60mg/L0.0179-0.096mg/L0.017922.7Pb 405.7810.005 %36.74mg/L0.00180.005mg/L0.001866.4Cr 205.560-0.058 %0.38mg/L0.0002-0.058mg/L0.0002-5,819.7Cr 283.563-0.058 %1.10mg/L0.0006-0.058mg/L0.0006-3,778.2Cr 284.3250.025 %4.21mg/L0.00110.025mg/L0.00111,777.9Cr 357.869-0.068 %0.11mg/L0.0001-0.068mg/L0.0001-201.6Mn 257.610-0.511 %0.08mg/L0.0004-0.511mg/L0.0004-38,011.6Mn 259.372-0.057 %0.56mg/L0.0003-0.057mg/L0.0003-56.0Mn 260.568-0.053 %0.94mg/L0.0005-0.053mg/L0.000573.0Mn 294.920-0.055 %5.30mg/L0.0029-0.055mg/L0.002916.3Mn 293.305-0.077 %0.73mg/L0.0006-0.077mg/L0.0006808.6Mn 279.482-0.087 %3.08mg/L0.0027-0.087mg/L0.0027255.9Mn 403.075-0.011 %30.73mg/L0.0035-0.011mg/L0.0035447.9Zn 206.200-0.026 %2.87mg/L0.0007-0.026mg/L0.00072,701.3Zn 213.857-0.006 %11.80mg/L0.0007-0.006mg/L0.0007785.6Zn 202.5480.076 %44.70mg/L0.03390.076mg/L0.0339360.8Zn 334.501-0.053 %1.73mg/L0.0009-0.053mg/L0.00097.9Co 228.616-0.043 %1.85mg/L0.0008-0.043mg/L0.000811.2Co 238.892-0.057 %5.39mg/L0.0031-0.057mg/L0.00312.0Co 230.786-0.065 %1.34mg/L0.0009-0.065mg/L0.0009-103.1Co 236.380-0.059 %7.50mg/L0.0044-0.059mg/L0.0044-16.8Co 231.160-0.672 %0.00mg/L0.0000-0.672mg/L0.0000-5,765.4Sr 421.552-1.305 %0.08mg/L0.0010-1.305mg/L0.0010-747.8Sr 460.733-0.633 %2.49mg/L0.0158-0.633mg/L0.0158-52.0Sr 232.235-56.48 %1.53mg/L0.865-56.48mg/L0.865-79.3K 404.721-1.027 %0.04mg/L0.0004-1.027mg/L0.0004-115,106.1Al 396.153-0.360 %0.03mg/L0.0001-0.360mg/L0.0001-19,816.1Al 308.215-1.215 %0.12mg/L0.0014-1.215mg/L0.0014-106,930.8Al 394.401-0.064 %0.75mg/L0.0005-0.064mg/L0.0005-5,198.7Al 237.313-0.072 %0.57mg/L0.0004-0.072mg/L0.0004-166.6B 249.677-0.079 %0.71mg/L0.0006-0.079mg/L0.0006-269.3B 249.772-0.076 %2.25mg/L0.0017-0.076mg/L0.0017-34.5B 208.957-0.547 %1.72mg/L0.0094-0.547mg/L0.0094-455.5B 182.578-0.010 %0.82mg/L0.0001-0.010mg/L0.0001228.3Fe 238.204-0.011 %0.41mg/L0.0000-0.011mg/L0.0000124.2Fe 239.562-0.012 %0.42mg/L0.0001-0.012mg/L0.0001-382.7Fe 259.939-0.010 %0.90mg/L0.0001-0.010mg/L0.000125.7Fe 234.349-0.010 %0.84mg/L0.0001-0.010mg/L0.000137.1Fe 273.955-0.024 %40.17mg/L0.0097-0.024mg/L0.0097-18.4Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M8 E QU SHAN HAI 642 15

mg 5/16/2014 10:54:25AM

-0.013 %2.91mg/L0.0004-0.013mg/L0.0004-46.0Cd 228.802-0.005 %17.28mg/L0.0009-0.005mg/L0.000943.1Cd 226.502-0.005 %6.79mg/L0.0003-0.005mg/L0.000379.2Ni 231.604-0.006 %6.32mg/L0.0004-0.006mg/L0.0004-6.0Ni 221.648-0.009 %5.66mg/L0.0005-0.009mg/L0.000597.5Ni 232.003-0.011 %2.33mg/L0.0003-0.011mg/L0.0003-7.7Ni 341.476-0.006 %11.08mg/L0.0007-0.006mg/L0.0007-13.7Ni 227.022-0.022 %35.71mg/L0.0079-0.022mg/L0.007940.3Pb 220.353-0.035 %35.19mg/L0.0122-0.035mg/L0.012268.1Pb 261.418-0.091 %13.34mg/L0.0121-0.091mg/L0.012133.7Pb 283.306-0.099 %12.78mg/L0.0126-0.099mg/L0.01264.1Pb 405.7810.002 %36.14mg/L0.00080.002mg/L0.000838.9Cr 205.560-0.060 %0.67mg/L0.0004-0.060mg/L0.0004-6,001.8Cr 283.563-0.058 %0.82mg/L0.0005-0.058mg/L0.0005-3,806.5Cr 284.3250.013 %7.20mg/L0.00100.013mg/L0.00101,076.2Cr 357.869-0.068 %0.33mg/L0.0002-0.068mg/L0.0002-195.6Mn 257.610-0.511 %0.04mg/L0.0002-0.511mg/L0.0002-38,028.3Mn 259.372-0.056 %0.74mg/L0.0004-0.056mg/L0.0004-41.0Mn 260.568-0.053 %0.73mg/L0.0004-0.053mg/L0.000463.5Mn 294.920-0.055 %0.71mg/L0.0004-0.055mg/L0.000421.6Mn 293.305-0.077 %2.91mg/L0.0022-0.077mg/L0.0022819.3Mn 279.482-0.082 %3.26mg/L0.0027-0.082mg/L0.0027419.4Mn 403.075-0.025 %4.82mg/L0.0012-0.025mg/L0.0012365.6Zn 206.200-0.044 %2.43mg/L0.0011-0.044mg/L0.00112,260.4Zn 213.857-0.020 %10.70mg/L0.0021-0.020mg/L0.0021653.6Zn 202.5480.084 %58.71mg/L0.04900.084mg/L0.0490374.7Zn 334.501-0.053 %4.73mg/L0.0025-0.053mg/L0.00258.7Co 228.616-0.043 %0.43mg/L0.0002-0.043mg/L0.00028.6Co 238.892-0.059 %6.14mg/L0.0036-0.059mg/L0.0036-4.1Co 230.786-0.062 %3.99mg/L0.0025-0.062mg/L0.0025-75.9Co 236.380-0.057 %9.60mg/L0.0055-0.057mg/L0.0055-7.1Co 231.160-0.672 %0.00mg/L0.0000-0.672mg/L0.0000-5,732.7Sr 421.552-1.306 %0.00mg/L0.0000-1.306mg/L0.0000-969.9Sr 460.733-0.643 %5.05mg/L0.0325-0.643mg/L0.0325-56.4Sr 232.235-56.93 %0.88mg/L0.501-56.93mg/L0.501-146.3K 404.721-1.026 %0.04mg/L0.0004-1.026mg/L0.0004-114,968.2Al 396.153-0.361 %0.06mg/L0.0002-0.361mg/L0.0002-19,858.5Al 308.215-1.215 %0.07mg/L0.0008-1.215mg/L0.0008-106,851.4Al 394.401-0.065 %0.71mg/L0.0005-0.065mg/L0.0005-5,208.2Al 237.313-0.077 %0.10mg/L0.0001-0.077mg/L0.0001-290.6B 249.677-0.083 %0.74mg/L0.0006-0.083mg/L0.0006-457.3B 249.772-0.082 %2.37mg/L0.0019-0.082mg/L0.0019-45.4B 208.957-0.603 %1.78mg/L0.0107-0.603mg/L0.0107-508.4B 182.578-0.010 %0.76mg/L0.0001-0.010mg/L0.0001213.1Fe 238.204-0.011 %0.11mg/L0.0000-0.011mg/L0.0000128.2Fe 239.562-0.012 %0.94mg/L0.0001-0.012mg/L0.0001-378.7Fe 259.939-0.010 %0.95mg/L0.0001-0.010mg/L0.000133.8Fe 234.349-0.010 %7.52mg/L0.0007-0.010mg/L0.000742.8Fe 273.955-0.037 %69.74mg/L0.0257-0.037mg/L0.0257-32.5Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

Calib Blank 1 643 1

g 5/16/2014 11:34:52AM

[0.00] %11.52mg/L8.6675.2Cd 228.802[0.00] %5.99mg/L12.51-208.9Cd 226.502[0.00] %14.19mg/L16.01-112.8Ni 231.604[0.00] %10.67mg/L33.70-315.7Ni 221.648[0.00] %0.77mg/L3.04-394.4Ni 232.003[0.00] %26.99mg/L25.5994.8Ni 341.476

[0.00] %18.27mg/L10.2656.2Ni 227.022[0.00] %59.93mg/L12.69-21.2Pb 220.353[0.00] %14.40mg/L2.1915.2Pb 261.418[0.00] %164.48mg/L32.14-19.5Pb 283.306[0.00] %50.71mg/L134.53265.3Pb 405.781[0.00] %46.85mg/L16.56-35.4Cr 205.560[0.00] %1.02mg/L65.236,394.8Cr 283.563[0.00] %0.40mg/L16.454,079.8Cr 284.325[0.00] %21.39mg/L42.65199.4Cr 357.869[0.00] %1.85mg/L6.06328.4Mn 257.610[0.00] %0.69mg/L302.5743,670.5Mn 259.372[0.00] %63.00mg/L19.5331.0Mn 260.568[0.00] %20.79mg/L20.84-100.2Mn 294.920[0.00] %117.66mg/L24.2520.6Mn 293.305[0.00] %16.86mg/L97.02-575.6Mn 279.482[0.00] %151.90mg/L107.2670.6Mn 403.075[0.00] %1.89mg/L3.27173.1Zn 206.200[0.00] %1.73mg/L19.971,156.4Zn 213.857[0.00] %5.51mg/L14.41261.4Zn 202.548[0.00] %17.08mg/L11.73-68.7Zn 334.501[0.00] %22.22mg/L8.91-40.1Co 228.616[0.00] %21.54mg/L15.72-73.0Co 238.892[0.00] %98.47mg/L14.5914.8Co 230.786[0.00] %10.68mg/L40.89382.7Co 236.380[0.00] %206.19mg/L17.838.6Co 231.160[0.00] %1.97mg/L107.585,469.3Sr 421.552[0.00] %7.68mg/L110.031,431.9Sr 460.733[0.00] %4.63mg/L4.97107.4Sr 232.235[0.00] %15.76mg/L80.78512.6K 404.721[0.00] %16.14mg/L3,538.1821,916.6Al 396.153[0.00] %5.11mg/L458.368,974.3Al 308.215[0.00] %14.43mg/L2,622.9118,172.0Al 394.401[0.00] %16.12mg/L165.251,025.0Al 237.313[0.00] %4.12mg/L18.66453.0B 249.677[0.00] %4.95mg/L32.35653.5B 249.772[0.00] %19.26mg/L5.6129.1B 208.957[0.00] %27.96mg/L6.00-21.4B 182.578[0.00] %11.41mg/L12.08105.9Fe 238.204[0.00] %36.50mg/L18.34-50.3Fe 239.562[0.00] %4.69mg/L28.40605.1Fe 259.939[0.00] %36.71mg/L39.92108.7Fe 234.349[0.00] %21.56mg/L14.54-67.4Fe 273.955[0.00] %37.22mg/L16.4044.1Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std1 multielemental 10% 644 2

g 5/16/2014 11:37:43AM

[0.01] %3.03mg/L5.15169.8Cd 228.802[0.01] %2.42mg/L7.38304.9Cd 226.502[0.01] %1.40mg/L10.69765.7Ni 231.604[0.01] %43.75mg/L155.62355.7Ni 221.648[0.01] %0.38mg/L3.17840.1Ni 232.003[0.01] %0.46mg/L9.031,965.7Ni 341.476[0.01] %5.51mg/L20.07364.0Ni 227.022[0.1] %7.64mg/L10.27134.5Pb 220.353[0.1] %9.44mg/L25.42269.4Pb 261.418[0.1] %6.78mg/L40.68599.9Pb 283.306[0.1] %2.63mg/L40.161,529.9Pb 405.781

[0.01] %20.49mg/L21.93107.0Cr 205.560

[0.01] %3.41mg/L13.94408.9Cr 283.563[0.01] %18.10mg/L27.53152.1Cr 284.325[0.01] %4.69mg/L39.81848.0Cr 357.869[0.1] %0.64mg/L108.6917,043.5Mn 257.610[0.1] %1.94mg/L338.1717,401.6Mn 259.372[0.1] %0.65mg/L56.248,689.3Mn 260.568[0.1] %0.90mg/L51.665,769.1Mn 294.920[0.1] %1.10mg/L39.753,603.6Mn 293.305[0.1] %2.05mg/L88.894,329.1Mn 279.482[0.1] %0.34mg/L26.957,825.4Mn 403.075[0.1] %1.71mg/L11.89695.9Zn 206.200[0.1] %0.40mg/L18.844,760.6Zn 213.857[0.1] %3.81mg/L42.781,123.2Zn 202.548[0.1] %11.17mg/L33.77302.3Zn 334.501[0.1] %1.59mg/L9.82615.9Co 228.616[0.1] %0.79mg/L17.862,247.8Co 238.892[0.1] %4.07mg/L20.63506.7Co 230.786[0.1] %4.19mg/L56.261,343.9Co 236.380[0.1] %4.88mg/L29.17597.9Co 231.160[1] %0.24mg/L10,711.114,538,966.2Sr 421.552[1] %2.00mg/L21,426.961,072,805.7Sr 460.733[1] %2.03mg/L10.49517.3Sr 232.235

[30] %2.88mg/L478.5116,632.6K 404.721[0.1] %91.53mg/L19,105.2120,872.1Al 396.153[0.1] %22.11mg/L531.552,404.0Al 308.215[0.1] %88.51mg/L16,224.4018,331.4Al 394.401[0.1] %21.21mg/L158.49747.3Al 237.313[0.2] %0.58mg/L38.886,686.6B 249.677[0.2] %0.37mg/L46.0412,440.5B 249.772[0.2] %2.92mg/L14.10483.6B 208.957[0.2] %7.80mg/L21.79279.4B 182.578

[0.04] %0.57mg/L65.2611,459.2Fe 238.204[0.04] %0.30mg/L45.6314,999.1Fe 239.562[0.04] %0.41mg/L63.1815,558.8Fe 259.939[0.04] %0.40mg/L19.824,969.2Fe 234.349[0.04] %0.49mg/L8.711,778.9Fe 273.955[0.01] %48.65mg/L14.4429.7Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std2 multielemental 10% 645 3

g 5/16/2014 11:40:35AM

[0.02] %3.99mg/L14.20355.5Cd 228.802[0.02] %1.88mg/L11.64620.7Cd 226.502[0.02] %1.15mg/L17.981,564.3Ni 231.604[0.02] %4.02mg/L44.161,097.4Ni 221.648[0.02] %1.19mg/L20.941,756.0Ni 232.003[0.02] %1.15mg/L47.284,109.7Ni 341.476[0.02] %0.55mg/L3.80697.9Ni 227.022[0.2] %0.96mg/L2.70281.5Pb 220.353[0.2] %2.06mg/L10.32500.7Pb 261.418[0.2] %2.72mg/L33.001,215.0Pb 283.306[0.2] %0.80mg/L25.603,203.9Pb 405.781

[0.02] %4.30mg/L9.66224.8Cr 205.560[0.02] %5.09mg/L49.97980.9Cr 283.563[0.02] %2.34mg/L9.50405.5Cr 284.325[0.02] %0.47mg/L8.431,778.3Cr 357.869[0.2] %0.39mg/L134.1934,812.8Mn 257.610[0.2] %1.64mg/L611.6337,293.1Mn 259.372[0.2] %0.36mg/L62.7617,590.1Mn 260.568

[0.2] %0.24mg/L27.3111,618.5Mn 294.920[0.2] %0.21mg/L15.097,263.4Mn 293.305[0.2] %2.71mg/L235.788,708.2Mn 279.482[0.2] %1.13mg/L182.8516,239.5Mn 403.075[0.2] %0.96mg/L14.001,453.5Zn 206.200[0.2] %0.86mg/L88.1010,236.9Zn 213.857[0.2] %0.26mg/L6.062,322.7Zn 202.548[0.2] %4.94mg/L30.62619.5Zn 334.501[0.2] %0.64mg/L7.751,211.8Co 228.616[0.2] %0.28mg/L13.284,760.7Co 238.892[0.2] %1.27mg/L12.38972.3Co 230.786[0.2] %0.61mg/L16.362,665.5Co 236.380[0.2] %0.80mg/L9.511,194.9Co 231.160[2] %1.07mg/L96,107.668,997,199.1Sr 421.552[2] %3.22mg/L70,245.842,182,324.8Sr 460.733[2] %0.98mg/L10.131,034.8Sr 232.235

[50] %4.02mg/L1,147.0228,508.5K 404.721[0.2] %38.21mg/L10,321.0927,008.9Al 396.153[0.2] %40.62mg/L3,096.397,622.1Al 308.215[0.2] %39.54mg/L9,693.6124,518.0Al 394.401[0.2] %43.86mg/L1,017.602,320.2Al 237.313[0.6] %1.01mg/L207.2820,442.3B 249.677[0.6] %0.95mg/L365.4138,300.5B 249.772[0.6] %0.87mg/L12.551,446.5B 208.957[0.6] %1.64mg/L13.10800.1B 182.578

[0.06] %0.51mg/L88.9717,336.9Fe 238.204[0.06] %0.43mg/L98.9622,749.6Fe 239.562[0.06] %0.57mg/L136.0123,677.1Fe 259.939[0.06] %0.49mg/L36.757,509.0Fe 234.349[0.06] %0.57mg/L15.302,662.2Fe 273.955[0.02] %30.94mg/L7.9025.5Cu 221.459

5/16/2014 11:40:35AM Standard intensity and concentration values are not in the same order.

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std3 multielemental 10% 646 4

g 5/16/2014 11:43:30AM

[0.03] %1.51mg/L7.99530.4Cd 228.802[0.03] %2.15mg/L20.36948.7Cd 226.502[0.03] %0.84mg/L20.172,388.0Ni 231.604[0.03] %5.45mg/L81.281,490.2Ni 221.648[0.03] %0.47mg/L11.902,552.4Ni 232.003[0.03] %0.57mg/L34.556,066.7Ni 341.476[0.03] %1.97mg/L21.461,089.8Ni 227.022[0.3] %2.57mg/L11.03428.9Pb 220.353[0.3] %1.19mg/L9.10766.7Pb 261.418[0.3] %2.38mg/L42.641,790.2Pb 283.306[0.3] %2.04mg/L96.324,732.9Pb 405.781

[0.03] %5.97mg/L19.29323.1Cr 205.560[0.03] %2.22mg/L36.521,644.9Cr 283.563[0.03] %0.49mg/L3.37690.8Cr 284.325[0.03] %1.24mg/L32.752,635.4Cr 357.869[0.3] %0.34mg/L170.4849,643.0Mn 257.610[0.3] %0.95mg/L530.1255,559.5Mn 259.372[0.3] %0.10mg/L25.9226,775.3Mn 260.568[0.3] %0.18mg/L32.3917,596.2Mn 294.920[0.3] %0.36mg/L39.8710,978.6Mn 293.305[0.3] %0.52mg/L66.2612,806.4Mn 279.482[0.3] %0.24mg/L57.9123,944.8Mn 403.075[0.3] %0.76mg/L17.562,316.1Zn 206.200

[0.3] %0.20mg/L32.1315,858.7Zn 213.857[0.3] %0.57mg/L21.153,709.9Zn 202.548[0.3] %0.73mg/L7.381,009.7Zn 334.501[0.3] %0.64mg/L11.861,838.6Co 228.616[0.3] %0.04mg/L2.587,298.2Co 238.892[0.3] %0.08mg/L1.141,463.5Co 230.786[0.3] %0.88mg/L35.284,006.0Co 236.380[0.3] %0.33mg/L5.971,804.1Co 231.160[3] %0.37mg/L48,679.8513,328,428.0Sr 421.552[3] %2.39mg/L75,824.293,166,697.2Sr 460.733[3] %1.11mg/L17.521,581.4Sr 232.235

[100] %1.03mg/L582.1856,409.6K 404.721[0.3] %13.13mg/L4,681.0235,661.0Al 396.153[0.3] %2.29mg/L156.966,859.9Al 308.215

5/16/2014 11:43:30AM Standard intensity and concentration values are not in the same order.[0.3] %13.65mg/L4,336.0431,773.1Al 394.401[0.3] %2.47mg/L47.211,914.7Al 237.313

5/16/2014 11:43:30AM Standard intensity and concentration values are not in the same order.[1] %0.44mg/L144.0432,561.2B 249.677[1] %0.52mg/L310.1260,157.7B 249.772[1] %0.85mg/L20.642,435.6B 208.957[1] %0.84mg/L11.141,326.5B 182.578

[0.08] %0.19mg/L44.2523,625.6Fe 238.204[0.08] %0.09mg/L26.4531,079.7Fe 239.562[0.08] %0.14mg/L46.1532,194.6Fe 259.939[0.08] %0.28mg/L28.2010,154.7Fe 234.349[0.08] %0.63mg/L22.493,595.4Fe 273.955[0.03] %31.62mg/L8.4426.7Cu 221.459

5/16/2014 11:43:30AM Standard intensity and concentration values are not in the same order.

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

std4 multielemental 10% 647 5

g 5/16/2014 11:46:27AM

[0.05] %1.71mg/L14.19827.3Cd 228.802[0.05] %0.78mg/L11.771,517.6Cd 226.502[0.05] %0.48mg/L18.843,892.6Ni 231.604[0.05] %3.33mg/L92.672,783.5Ni 221.648[0.05] %2.14mg/L85.263,987.5Ni 232.003[0.05] %1.28mg/L123.049,585.6Ni 341.476[0.05] %0.53mg/L9.241,755.1Ni 227.022[0.5] %1.46mg/L10.17695.9Pb 220.353[0.5] %1.79mg/L21.931,222.4Pb 261.418[0.5] %1.53mg/L42.332,774.4Pb 283.306[0.5] %1.13mg/L83.097,349.1Pb 405.781

[0.05] %4.28mg/L21.81509.3Cr 205.560[0.05] %0.91mg/L28.123,099.4Cr 283.563[0.05] %2.52mg/L34.341,364.4Cr 284.325[0.05] %2.77mg/L113.004,073.4Cr 357.869[0.5] %0.46mg/L372.9481,763.8Mn 257.610[0.5] %0.86mg/L777.5590,148.1Mn 259.372[0.5] %0.75mg/L315.5041,899.7Mn 260.568[0.5] %0.22mg/L62.7628,722.4Mn 294.920[0.5] %0.37mg/L66.2017,904.3Mn 293.305[0.5] %1.99mg/L397.7820,004.4Mn 279.482[0.5] %1.93mg/L673.4734,881.2Mn 403.075[0.5] %1.01mg/L34.313,397.9Zn 206.200[0.5] %1.04mg/L235.7422,702.2Zn 213.857[0.5] %0.84mg/L45.925,451.5Zn 202.548[0.5] %0.51mg/L7.361,449.9Zn 334.501

[0.5] %1.40mg/L41.572,977.5Co 228.616[0.5] %0.53mg/L65.3712,379.0Co 238.892[0.5] %0.76mg/L18.462,416.8Co 230.786[0.5] %0.34mg/L22.356,523.0Co 236.380[0.5] %0.34mg/L10.162,955.3Co 231.160[5] %0.17mg/L37,108.7321,268,248.3Sr 421.552[5] %2.16mg/L105,679.414,886,460.9Sr 460.733[5] %1.42mg/L35.922,526.6Sr 232.235

[150] %3.60mg/L2,817.1178,305.7K 404.721[0.5] %2.82mg/L1,502.1353,332.8Al 396.153[0.5] %5.82mg/L596.6810,253.1Al 308.215

5/16/2014 11:46:27AM Standard intensity and concentration values are not in the same order.[0.5] %2.96mg/L1,416.1847,784.6Al 394.401[0.5] %5.65mg/L159.382,822.2Al 237.313

5/16/2014 11:46:27AM Standard intensity and concentration values are not in the same order.[2] %1.28mg/L805.4263,156.1B 249.677[2] %1.15mg/L1,334.25116,331.4B 249.772[2] %0.18mg/L8.424,655.8B 208.957[2] %0.97mg/L24.542,533.5B 182.578

[0.1] %0.35mg/L99.5828,661.1Fe 238.204[0.1] %0.76mg/L272.0435,925.3Fe 239.562[0.1] %0.70mg/L263.6837,443.7Fe 259.939[0.1] %0.42mg/L51.1012,313.8Fe 234.349[0.1] %0.38mg/L16.544,337.9Fe 273.955

[0.05] %4.47mg/L2.8162.8Cu 221.4595/16/2014 11:46:27AM Standard intensity and concentration values are not in the same order.

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M5 E QU SHAN HAI 648 9

mg 5/16/2014 11:49:20AM

0.007 %14.52mg/L0.00100.007mg/L0.0010125.3Cd 228.8020.004 %4.15mg/L0.00020.004mg/L0.0002120.0Cd 226.502-0.001 %15.48mg/L0.0002-0.001mg/L0.0002-85.9Ni 231.604-0.010 %1.49mg/L0.0001-0.010mg/L0.0001-637.6Ni 221.648-0.001 %2.75mg/L0.0000-0.001mg/L0.0000-29.6Ni 232.003-0.001 %28.57mg/L0.0002-0.001mg/L0.0002-17.5Ni 341.4760.000 %430.54mg/L0.00040.000mg/L0.000410.1Ni 227.0220.005 %276.31mg/L0.01490.005mg/L0.01497.4Pb 220.3530.003 %130.75mg/L0.00330.003mg/L0.003321.0Pb 261.418-0.047 %6.79mg/L0.0032-0.047mg/L0.0032-208.0Pb 283.3060.002 %267.39mg/L0.00670.002mg/L0.0067146.4Pb 405.781-0.002 %25.30mg/L0.0005-0.002mg/L0.0005-13.6Cr 205.560-0.000 %166.63mg/L0.0008-0.000mg/L0.0008-187.8Cr 283.5630.001 %107.34mg/L0.00100.001mg/L0.0010-62.4Cr 284.325-0.002 %5.35mg/L0.0001-0.002mg/L0.0001-106.9Cr 357.8690.000 %35.39mg/L0.00010.000mg/L0.0001834.3Mn 257.610-0.022 %3.05mg/L0.0007-0.022mg/L0.0007-3,841.7Mn 259.3720.000 %208.18mg/L0.00030.000mg/L0.0003452.1Mn 260.5680.003 %7.77mg/L0.00030.003mg/L0.0003269.4Mn 294.9200.003 %17.54mg/L0.00050.003mg/L0.0005162.8Mn 293.305-0.542 %2.28mg/L0.0124-0.542mg/L0.0124-21,371.3Mn 279.482-0.011 %4.26mg/L0.0005-0.011mg/L0.0005302.1Mn 403.075-0.012 %20.63mg/L0.0025-0.012mg/L0.0025-34.8Zn 206.200-0.018 %0.13mg/L0.0000-0.018mg/L0.0000-312.3Zn 213.857-0.019 %3.57mg/L0.0007-0.019mg/L0.0007-134.9Zn 202.548-0.160 %3.80mg/L0.0061-0.160mg/L0.0061-449.5Zn 334.501-0.001 %36.31mg/L0.0005-0.001mg/L0.00058.4Co 228.6160.007 %14.62mg/L0.00100.007mg/L0.001024.4Co 238.8920.001 %245.55mg/L0.00300.001mg/L0.003017.0Co 230.786

0.000 %520.78mg/L0.00190.000mg/L0.001940.0Co 236.380-0.007 %8.83mg/L0.0006-0.007mg/L0.0006-32.0Co 231.1600.451 %2.11mg/L0.00950.451mg/L0.00952,183,277.5Sr 421.5520.372 %4.04mg/L0.01500.372mg/L0.0150471,887.1Sr 460.7330.541 %9.60mg/L0.05200.541mg/L0.0520290.0Sr 232.23511.70 %2.89mg/L0.33811.70mg/L0.3387,357.4K 404.721-0.072 %1.66mg/L0.0012-0.072mg/L0.0012-1,687.8Al 396.153-0.062 %40.50mg/L0.0250-0.062mg/L0.0250-242.2Al 308.215-0.075 %2.85mg/L0.0021-0.075mg/L0.0021-1,886.3Al 394.401-0.072 %42.74mg/L0.0308-0.072mg/L0.0308-32.0Al 237.3130.551 %1.09mg/L0.00600.551mg/L0.006018,001.3B 249.6770.551 %1.01mg/L0.00550.551mg/L0.005533,319.3B 249.7720.541 %0.72mg/L0.00390.541mg/L0.00391,293.7B 208.957-54.62 %0.72mg/L0.394-54.62mg/L0.394-69,019.3B 182.5780.001 %3.08mg/L0.00000.001mg/L0.0000416.0Fe 238.2040.000 %14.58mg/L0.00010.000mg/L0.0001520.3Fe 239.5620.000 %9.75mg/L0.00000.000mg/L0.0000527.5Fe 259.9390.004 %4.10mg/L0.00020.004mg/L0.0002530.1Fe 234.3490.001 %25.57mg/L0.00030.001mg/L0.000368.9Fe 273.9550.001 %1,516.21mg/L0.01970.001mg/L0.01977.0Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M5 DP E QU SHAN HAI 649 10

mg 5/16/2014 11:53:12AM

0.007 %17.33mg/L0.00120.007mg/L0.0012125.4Cd 228.8020.005 %6.15mg/L0.00030.005mg/L0.0003155.4Cd 226.502-0.001 %11.54mg/L0.0001-0.001mg/L0.0001-80.9Ni 231.604-0.016 %19.80mg/L0.0031-0.016mg/L0.0031-970.8Ni 221.648-0.001 %3.97mg/L0.0001-0.001mg/L0.0001-51.5Ni 232.003-0.001 %10.76mg/L0.0001-0.001mg/L0.0001-43.3Ni 341.476-0.000 %1,492.01mg/L0.0006-0.000mg/L0.00065.5Ni 227.0220.009 %78.53mg/L0.00730.009mg/L0.007312.9Pb 220.3530.000 %2,126.61mg/L0.00730.000mg/L0.007315.6Pb 261.418-0.047 %11.80mg/L0.0055-0.047mg/L0.0055-209.0Pb 283.306-0.003 %175.90mg/L0.0047-0.003mg/L0.004770.0Pb 405.781-0.002 %85.59mg/L0.0014-0.002mg/L0.0014-8.8Cr 205.5600.000 %100.56mg/L0.00030.000mg/L0.0003-138.5Cr 283.5630.003 %51.10mg/L0.00160.003mg/L0.0016-1.2Cr 284.325-0.002 %26.72mg/L0.0006-0.002mg/L0.0006-118.4Cr 357.869-0.000 %31.24mg/L0.0001-0.000mg/L0.0001756.4Mn 257.610-0.020 %9.65mg/L0.0020-0.020mg/L0.0020-3,537.5Mn 259.372-0.000 %52.43mg/L0.0002-0.000mg/L0.0002402.8Mn 260.5680.003 %5.94mg/L0.00020.003mg/L0.0002250.6Mn 294.9200.002 %21.98mg/L0.00050.002mg/L0.0005134.2Mn 293.305-0.553 %1.17mg/L0.0065-0.553mg/L0.0065-21,796.4Mn 279.482-0.012 %6.35mg/L0.0007-0.012mg/L0.0007264.4Mn 403.075-0.016 %5.91mg/L0.0009-0.016mg/L0.0009-58.1Zn 206.200-0.022 %2.75mg/L0.0006-0.022mg/L0.0006-488.2Zn 213.857-0.024 %4.15mg/L0.0010-0.024mg/L0.0010-182.2Zn 202.548-0.184 %3.09mg/L0.0057-0.184mg/L0.0057-518.8Zn 334.501-0.001 %97.09mg/L0.0011-0.001mg/L0.001110.3Co 228.6160.006 %4.10mg/L0.00030.006mg/L0.000318.2Co 238.8920.000 %983.71mg/L0.00370.000mg/L0.003713.0Co 230.786-0.000 %943.30mg/L0.0014-0.000mg/L0.001433.3Co 236.380-0.006 %36.09mg/L0.0023-0.006mg/L0.0023-29.2Co 231.1600.459 %0.44mg/L0.00200.459mg/L0.00202,220,627.5Sr 421.5520.387 %2.02mg/L0.00780.387mg/L0.0078486,545.7Sr 460.7330.542 %2.30mg/L0.01250.542mg/L0.0125290.4Sr 232.23512.04 %1.70mg/L0.20512.04mg/L0.2057,537.5K 404.721

-0.062 %6.39mg/L0.0040-0.062mg/L0.0040-734.4Al 396.153-0.054 %36.00mg/L0.0195-0.054mg/L0.0195-87.6Al 308.215-0.062 %9.67mg/L0.0060-0.062mg/L0.0060-699.2Al 394.401-0.069 %31.76mg/L0.0218-0.069mg/L0.0218-13.7Al 237.3130.542 %1.39mg/L0.00750.542mg/L0.007517,712.8B 249.6770.541 %1.37mg/L0.00740.541mg/L0.007432,741.1B 249.7720.530 %1.62mg/L0.00860.530mg/L0.00861,269.2B 208.957-34.95 %0.62mg/L0.215-34.95mg/L0.215-44,152.0B 182.5780.001 %23.32mg/L0.00020.001mg/L0.0002310.4Fe 238.2040.000 %114.98mg/L0.00020.000mg/L0.0002410.1Fe 239.5620.000 %129.79mg/L0.00020.000mg/L0.0002391.7Fe 259.9390.004 %7.06mg/L0.00030.004mg/L0.0003492.5Fe 234.3490.000 %158.22mg/L0.00070.000mg/L0.000741.7Fe 273.9550.007 %166.36mg/L0.01220.007mg/L0.012213.4Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M6 E QU SHAN HAI 650 11

mg 5/16/2014 11:57:04AM

0.006 %5.51mg/L0.00030.006mg/L0.0003108.4Cd 228.8020.003 %24.52mg/L0.00080.003mg/L0.0008107.2Cd 226.502-0.001 %38.80mg/L0.0003-0.001mg/L0.0003-59.2Ni 231.604-0.007 %15.36mg/L0.0011-0.007mg/L0.0011-508.5Ni 221.648-0.002 %9.45mg/L0.0002-0.002mg/L0.0002-65.4Ni 232.003-0.001 %16.99mg/L0.0001-0.001mg/L0.0001-60.9Ni 341.476-0.000 %356.01mg/L0.0002-0.000mg/L0.00025.1Ni 227.0220.013 %85.83mg/L0.01130.013mg/L0.011318.4Pb 220.353-0.005 %151.40mg/L0.0079-0.005mg/L0.00792.1Pb 261.418-0.036 %13.36mg/L0.0047-0.036mg/L0.0047-146.4Pb 283.3060.005 %74.41mg/L0.00350.005mg/L0.0035179.1Pb 405.7810.001 %269.79mg/L0.00180.001mg/L0.001815.1Cr 205.560-0.000 %3,251.00mg/L0.0006-0.000mg/L0.0006-157.9Cr 283.5630.003 %19.84mg/L0.00060.003mg/L0.00061.5Cr 284.325-0.002 %20.73mg/L0.0004-0.002mg/L0.0004-114.4Cr 357.869-0.001 %13.22mg/L0.0001-0.001mg/L0.0001702.5Mn 257.610-0.022 %21.49mg/L0.0047-0.022mg/L0.0047-3,803.3Mn 259.372-0.001 %25.00mg/L0.0002-0.001mg/L0.0002362.8Mn 260.5680.003 %19.06mg/L0.00050.003mg/L0.0005221.5Mn 294.9200.003 %36.78mg/L0.00100.003mg/L0.0010144.0Mn 293.305-0.483 %1.23mg/L0.0059-0.483mg/L0.0059-19,007.5Mn 279.482-0.012 %7.78mg/L0.0010-0.012mg/L0.0010220.0Mn 403.075-0.018 %19.41mg/L0.0036-0.018mg/L0.0036-77.2Zn 206.200-0.023 %1.48mg/L0.0003-0.023mg/L0.0003-530.9Zn 213.857-0.023 %1.11mg/L0.0003-0.023mg/L0.0003-179.9Zn 202.548-0.147 %8.37mg/L0.0123-0.147mg/L0.0123-408.9Zn 334.501-0.001 %145.18mg/L0.0019-0.001mg/L0.00198.8Co 228.6160.006 %2.42mg/L0.00010.006mg/L0.0001-3.5Co 238.892-0.002 %175.14mg/L0.0032-0.002mg/L0.00322.5Co 230.7860.003 %32.56mg/L0.00090.003mg/L0.000972.5Co 236.380-0.005 %24.03mg/L0.0013-0.005mg/L0.0013-22.9Co 231.1600.368 %1.82mg/L0.00670.368mg/L0.00671,832,088.8Sr 421.5520.315 %3.75mg/L0.01180.315mg/L0.0118415,661.8Sr 460.7330.415 %15.91mg/L0.06610.415mg/L0.0661226.2Sr 232.23510.83 %5.59mg/L0.60510.83mg/L0.6056,898.4K 404.721-0.073 %2.61mg/L0.0019-0.073mg/L0.0019-1,787.4Al 396.153-0.070 %7.05mg/L0.0050-0.070mg/L0.0050-418.3Al 308.215-0.074 %1.58mg/L0.0012-0.074mg/L0.0012-1,774.0Al 394.401-0.084 %8.46mg/L0.0071-0.084mg/L0.0071-95.4Al 237.3130.558 %1.02mg/L0.00570.558mg/L0.005718,195.6B 249.6770.557 %0.89mg/L0.00490.557mg/L0.004933,706.5B 249.772

0.544 %1.31mg/L0.00710.544mg/L0.00711,301.5B 208.957-45.16 %0.92mg/L0.414-45.16mg/L0.414-57,062.9B 182.5780.001 %12.00mg/L0.00010.001mg/L0.0001170.9Fe 238.204-0.000 %5.67mg/L0.0000-0.000mg/L0.0000207.0Fe 239.562-0.000 %14.69mg/L0.0001-0.000mg/L0.0001170.7Fe 259.9390.003 %1.33mg/L0.00000.003mg/L0.0000377.2Fe 234.3490.001 %39.71mg/L0.00020.001mg/L0.000244.9Fe 273.9550.018 %64.08mg/L0.01140.018mg/L0.011424.6Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M6 DP E QU SHAN HAI 651 12

mg 5/16/2014 12:00:56PM

0.005 %14.74mg/L0.00080.005mg/L0.000898.2Cd 228.8020.003 %12.71mg/L0.00040.003mg/L0.0004108.7Cd 226.502-0.001 %41.15mg/L0.0003-0.001mg/L0.0003-64.4Ni 231.604-0.005 %11.88mg/L0.0005-0.005mg/L0.0005-353.6Ni 221.648-0.001 %23.75mg/L0.0003-0.001mg/L0.0003-46.7Ni 232.003-0.001 %35.22mg/L0.0003-0.001mg/L0.0003-39.0Ni 341.4760.000 %677.66mg/L0.00040.000mg/L0.00049.2Ni 227.0220.008 %55.54mg/L0.00440.008mg/L0.004411.0Pb 220.3530.009 %63.24mg/L0.00590.009mg/L0.005937.7Pb 261.418-0.037 %4.21mg/L0.0016-0.037mg/L0.0016-156.7Pb 283.306-0.000 %3,735.99mg/L0.0125-0.000mg/L0.0125104.7Pb 405.7810.002 %92.40mg/L0.00150.002mg/L0.001524.4Cr 205.560-0.001 %62.02mg/L0.0004-0.001mg/L0.0004-193.7Cr 283.5630.001 %23.09mg/L0.00030.001mg/L0.0003-56.7Cr 284.325-0.002 %13.48mg/L0.0003-0.002mg/L0.0003-118.1Cr 357.869-0.000 %28.69mg/L0.0000-0.000mg/L0.0000775.3Mn 257.610-0.025 %15.18mg/L0.0038-0.025mg/L0.0038-4,382.9Mn 259.372-0.000 %52.98mg/L0.0003-0.000mg/L0.0003400.5Mn 260.5680.004 %8.88mg/L0.00030.004mg/L0.0003272.6Mn 294.9200.003 %20.96mg/L0.00060.003mg/L0.0006159.6Mn 293.305-0.487 %1.26mg/L0.0061-0.487mg/L0.0061-19,152.9Mn 279.482-0.012 %1.95mg/L0.0002-0.012mg/L0.0002248.4Mn 403.075-0.013 %8.12mg/L0.0010-0.013mg/L0.0010-38.9Zn 206.200-0.020 %1.86mg/L0.0004-0.020mg/L0.0004-381.5Zn 213.857-0.021 %9.70mg/L0.0020-0.021mg/L0.0020-149.9Zn 202.548-0.149 %1.88mg/L0.0028-0.149mg/L0.0028-417.0Zn 334.501-0.001 %122.87mg/L0.0017-0.001mg/L0.00178.6Co 228.6160.006 %14.58mg/L0.00090.006mg/L0.000918.1Co 238.892-0.004 %42.33mg/L0.0016-0.004mg/L0.0016-6.9Co 230.7860.000 %420.88mg/L0.00060.000mg/L0.000637.1Co 236.380-0.005 %24.67mg/L0.0012-0.005mg/L0.0012-20.9Co 231.1600.364 %1.59mg/L0.00580.364mg/L0.00581,814,951.5Sr 421.5520.304 %3.36mg/L0.01020.304mg/L0.0102404,717.1Sr 460.7330.436 %9.98mg/L0.04350.436mg/L0.0435236.8Sr 232.23510.07 %5.00mg/L0.50410.07mg/L0.5046,499.6K 404.721-0.060 %1.11mg/L0.0007-0.060mg/L0.0007-507.4Al 396.153-0.060 %3.91mg/L0.0023-0.060mg/L0.0023-208.2Al 308.215-0.059 %1.24mg/L0.0007-0.059mg/L0.0007-494.6Al 394.401-0.066 %5.96mg/L0.0039-0.066mg/L0.00392.8Al 237.3130.535 %0.98mg/L0.00530.535mg/L0.005317,487.0B 249.6770.536 %1.17mg/L0.00620.536mg/L0.006232,438.4B 249.7720.527 %0.23mg/L0.00120.527mg/L0.00121,260.3B 208.957-45.54 %1.69mg/L0.771-45.54mg/L0.771-57,537.5B 182.5780.001 %5.37mg/L0.00010.001mg/L0.0001339.3Fe 238.2040.000 %33.74mg/L0.00010.000mg/L0.0001436.7Fe 239.5620.000 %23.16mg/L0.00000.000mg/L0.0000399.3Fe 259.9390.003 %3.50mg/L0.00010.003mg/L0.0001439.7Fe 234.349

0.001 %15.62mg/L0.00020.001mg/L0.000271.8Fe 273.9550.006 %285.28mg/L0.01630.006mg/L0.016311.7Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M7 E QU SHAN HAI 652 13

mg 5/16/2014 12:04:49PM

0.009 %6.92mg/L0.00070.009mg/L0.0007167.5Cd 228.8020.005 %11.41mg/L0.00060.005mg/L0.0006174.1Cd 226.502-0.001 %0.49mg/L0.0000-0.001mg/L0.0000-57.5Ni 231.604-0.008 %3.38mg/L0.0003-0.008mg/L0.0003-536.8Ni 221.648-0.001 %7.52mg/L0.0001-0.001mg/L0.0001-30.9Ni 232.003-0.001 %11.44mg/L0.0001-0.001mg/L0.0001-67.9Ni 341.476-0.000 %319.84mg/L0.0002-0.000mg/L0.00024.3Ni 227.0220.015 %56.20mg/L0.00820.015mg/L0.008220.3Pb 220.3530.005 %94.32mg/L0.00460.005mg/L0.004626.7Pb 261.418-0.035 %13.88mg/L0.0048-0.035mg/L0.0048-142.8Pb 283.3060.003 %77.24mg/L0.00210.003mg/L0.0021149.2Pb 405.781-0.002 %32.15mg/L0.0005-0.002mg/L0.0005-7.3Cr 205.560-0.001 %130.59mg/L0.0008-0.001mg/L0.0008-193.4Cr 283.5630.002 %65.50mg/L0.00110.002mg/L0.0011-43.7Cr 284.325-0.003 %9.81mg/L0.0003-0.003mg/L0.0003-177.9Cr 357.8690.001 %23.56mg/L0.00010.001mg/L0.0001887.6Mn 257.610-0.024 %6.79mg/L0.0016-0.024mg/L0.0016-4,233.5Mn 259.3720.000 %162.43mg/L0.00030.000mg/L0.0003453.4Mn 260.5680.004 %11.52mg/L0.00050.004mg/L0.0005305.8Mn 294.9200.003 %5.19mg/L0.00020.003mg/L0.0002158.5Mn 293.305-0.529 %0.73mg/L0.0039-0.529mg/L0.0039-20,841.2Mn 279.482-0.011 %4.39mg/L0.0005-0.011mg/L0.0005330.7Mn 403.075-0.019 %9.17mg/L0.0017-0.019mg/L0.0017-78.5Zn 206.200-0.024 %0.54mg/L0.0001-0.024mg/L0.0001-559.2Zn 213.857-0.025 %5.78mg/L0.0015-0.025mg/L0.0015-199.8Zn 202.548-0.201 %1.95mg/L0.0039-0.201mg/L0.0039-570.0Zn 334.501-0.001 %205.54mg/L0.0010-0.001mg/L0.001013.7Co 228.6160.006 %14.81mg/L0.00080.006mg/L0.00081.2Co 238.892-0.003 %141.74mg/L0.0039-0.003mg/L0.0039-2.2Co 230.7860.002 %71.13mg/L0.00120.002mg/L0.001258.2Co 236.380-0.006 %12.03mg/L0.0007-0.006mg/L0.0007-25.6Co 231.1600.382 %0.88mg/L0.00340.382mg/L0.00341,892,611.5Sr 421.5520.307 %2.45mg/L0.00750.307mg/L0.0075407,737.4Sr 460.7330.469 %2.86mg/L0.01340.469mg/L0.0134253.5Sr 232.23511.77 %1.67mg/L0.19611.77mg/L0.1967,394.8K 404.721-0.078 %1.59mg/L0.0012-0.078mg/L0.0012-2,300.5Al 396.153-0.078 %3.97mg/L0.0031-0.078mg/L0.0031-578.3Al 308.215-0.080 %1.55mg/L0.0012-0.080mg/L0.0012-2,372.9Al 394.401-0.087 %4.65mg/L0.0040-0.087mg/L0.0040-113.0Al 237.3130.589 %0.60mg/L0.00350.589mg/L0.003519,176.9B 249.6770.588 %0.42mg/L0.00250.588mg/L0.002535,478.6B 249.7720.570 %0.79mg/L0.00450.570mg/L0.00451,360.3B 208.957-46.18 %0.44mg/L0.201-46.18mg/L0.201-58,350.7B 182.5780.003 %4.56mg/L0.00010.003mg/L0.0001726.5Fe 238.2040.002 %2.74mg/L0.00000.002mg/L0.0000912.7Fe 239.5620.001 %4.37mg/L0.00010.001mg/L0.0001912.0Fe 259.9390.006 %1.12mg/L0.00010.006mg/L0.0001712.4Fe 234.3490.003 %26.60mg/L0.00070.003mg/L0.0007135.6Fe 273.9550.006 %229.51mg/L0.01270.006mg/L0.012711.5Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M7 DP E QU SHAN HAI 653 14

mg 5/16/2014 12:08:40PM

0.009 %0.89mg/L0.00010.009mg/L0.0001153.0Cd 228.8020.006 %11.78mg/L0.00070.006mg/L0.0007196.5Cd 226.502-0.001 %19.54mg/L0.0002-0.001mg/L0.0002-71.7Ni 231.604-0.009 %20.46mg/L0.0019-0.009mg/L0.0019-617.1Ni 221.648-0.001 %19.02mg/L0.0003-0.001mg/L0.0003-44.8Ni 232.003-0.001 %4.40mg/L0.0000-0.001mg/L0.0000-71.9Ni 341.476-0.000 %105.71mg/L0.0005-0.000mg/L0.0005-9.5Ni 227.022-0.002 %880.07mg/L0.0154-0.002mg/L0.0154-2.6Pb 220.353-0.003 %363.40mg/L0.0093-0.003mg/L0.00938.6Pb 261.418-0.043 %4.67mg/L0.0020-0.043mg/L0.0020-187.7Pb 283.3060.007 %117.22mg/L0.00790.007mg/L0.0079209.7Pb 405.781-0.002 %160.63mg/L0.0030-0.002mg/L0.0030-10.8Cr 205.560-0.001 %83.30mg/L0.0009-0.001mg/L0.0009-223.5Cr 283.5630.002 %25.53mg/L0.00050.002mg/L0.0005-38.7Cr 284.325-0.003 %2.79mg/L0.0001-0.003mg/L0.0001-201.5Cr 357.8690.001 %13.09mg/L0.00010.001mg/L0.0001877.6Mn 257.610-0.019 %8.94mg/L0.0017-0.019mg/L0.0017-3,264.7Mn 259.3720.000 %111.06mg/L0.00020.000mg/L0.0002457.2Mn 260.5680.004 %4.48mg/L0.00020.004mg/L0.0002285.2Mn 294.9200.003 %4.99mg/L0.00020.003mg/L0.0002162.8Mn 293.305-0.531 %0.59mg/L0.0031-0.531mg/L0.0031-20,941.7Mn 279.482-0.011 %12.59mg/L0.0014-0.011mg/L0.0014313.1Mn 403.075-0.019 %3.47mg/L0.0006-0.019mg/L0.0006-79.0Zn 206.200-0.023 %1.08mg/L0.0002-0.023mg/L0.0002-534.3Zn 213.857-0.024 %3.82mg/L0.0009-0.024mg/L0.0009-190.9Zn 202.548-0.209 %4.00mg/L0.0084-0.209mg/L0.0084-594.8Zn 334.501-0.001 %100.79mg/L0.0011-0.001mg/L0.001110.0Co 228.6160.006 %6.63mg/L0.00040.006mg/L0.00043.9Co 238.892-0.000 %1,036.88mg/L0.0046-0.000mg/L0.00469.0Co 230.7860.001 %158.06mg/L0.00220.001mg/L0.002253.1Co 236.380-0.007 %27.28mg/L0.0018-0.007mg/L0.0018-31.9Co 231.1600.392 %0.11mg/L0.00040.392mg/L0.00041,934,870.2Sr 421.5520.323 %0.62mg/L0.00200.323mg/L0.0020423,383.7Sr 460.7330.506 %8.40mg/L0.04250.506mg/L0.0425272.3Sr 232.23512.20 %1.26mg/L0.15412.20mg/L0.1547,621.7K 404.721-0.060 %9.17mg/L0.0055-0.060mg/L0.0055-536.5Al 396.153-0.051 %58.33mg/L0.0295-0.051mg/L0.0295-17.4Al 308.215-0.065 %10.47mg/L0.0068-0.065mg/L0.0068-973.0Al 394.401-0.063 %49.32mg/L0.0310-0.063mg/L0.031018.0Al 237.3130.566 %1.65mg/L0.00930.566mg/L0.009318,473.0B 249.6770.565 %1.90mg/L0.01070.565mg/L0.010734,160.8B 249.7720.549 %1.77mg/L0.00970.549mg/L0.00971,313.3B 208.957-36.27 %1.44mg/L0.524-36.27mg/L0.524-45,820.6B 182.5780.003 %10.50mg/L0.00030.003mg/L0.0003784.5Fe 238.2040.002 %11.13mg/L0.00020.002mg/L0.00021,005.5Fe 239.5620.002 %14.99mg/L0.00030.002mg/L0.00031,026.5Fe 259.9390.006 %3.78mg/L0.00020.006mg/L0.0002767.6Fe 234.3490.003 %12.37mg/L0.00030.003mg/L0.0003134.0Fe 273.9550.003 %221.28mg/L0.00610.003mg/L0.00618.6Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M8 E QU SHAN HAI 654 15

mg 5/16/2014 12:12:30PM

0.012 %4.64mg/L0.00060.012mg/L0.0006216.1Cd 228.8020.009 %8.26mg/L0.00070.009mg/L0.0007269.2Cd 226.502-0.001 %45.03mg/L0.0004-0.001mg/L0.0004-63.1Ni 231.604-0.024 %1.52mg/L0.0004-0.024mg/L0.0004-1,437.1Ni 221.648-0.002 %10.59mg/L0.0002-0.002mg/L0.0002-61.1Ni 232.003-0.001 %22.44mg/L0.0002-0.001mg/L0.0002-53.2Ni 341.476-0.000 %272.10mg/L0.0003-0.000mg/L0.00033.2Ni 227.0220.002 %694.07mg/L0.01190.002mg/L0.01192.2Pb 220.353-0.008 %76.01mg/L0.0061-0.008mg/L0.0061-4.8Pb 261.418-0.034 %10.33mg/L0.0035-0.034mg/L0.0035-137.0Pb 283.306-0.003 %67.09mg/L0.0020-0.003mg/L0.002065.7Pb 405.781-0.001 %46.60mg/L0.0003-0.001mg/L0.00032.0Cr 205.560-0.001 %147.36mg/L0.0008-0.001mg/L0.0008-190.2Cr 283.5630.003 %26.21mg/L0.00070.003mg/L0.0007-16.1Cr 284.325-0.003 %14.09mg/L0.0004-0.003mg/L0.0004-165.0Cr 357.869-0.001 %22.56mg/L0.0002-0.001mg/L0.0002681.7Mn 257.610-0.024 %8.29mg/L0.0020-0.024mg/L0.0020-4,143.9Mn 259.372-0.001 %21.83mg/L0.0002-0.001mg/L0.0002368.5Mn 260.5680.003 %32.78mg/L0.00100.003mg/L0.0010236.4Mn 294.9200.003 %21.09mg/L0.00070.003mg/L0.0007162.5Mn 293.305-0.459 %1.76mg/L0.0081-0.459mg/L0.0081-18,056.7Mn 279.482-0.013 %5.12mg/L0.0006-0.013mg/L0.0006208.0Mn 403.075-0.020 %15.19mg/L0.0030-0.020mg/L0.0030-87.0Zn 206.200-0.025 %1.81mg/L0.0004-0.025mg/L0.0004-612.1Zn 213.857-0.025 %2.20mg/L0.0006-0.025mg/L0.0006-198.9Zn 202.548-0.193 %2.63mg/L0.0051-0.193mg/L0.0051-545.8Zn 334.5010.000 %1,018.60mg/L0.00070.000mg/L0.000717.2Co 228.6160.004 %20.81mg/L0.00090.004mg/L0.0009-31.5Co 238.892-0.002 %81.05mg/L0.0014-0.002mg/L0.00142.8Co 230.7860.003 %67.07mg/L0.00180.003mg/L0.001869.7Co 236.380-0.005 %48.58mg/L0.0025-0.005mg/L0.0025-23.0Co 231.1600.335 %1.25mg/L0.00420.335mg/L0.00421,693,166.3Sr 421.5520.279 %1.74mg/L0.00490.279mg/L0.0049380,272.7Sr 460.7330.431 %3.61mg/L0.01560.431mg/L0.0156234.3Sr 232.2358.519 %1.87mg/L0.15968.519mg/L0.15965,681.1K 404.7210.027 %237.72mg/L0.06530.027mg/L0.06538,200.3Al 396.153-0.002 %260.86mg/L0.0056-0.002mg/L0.0056957.0Al 308.2150.027 %238.96mg/L0.06470.027mg/L0.06477,233.1Al 394.401-0.014 %40.14mg/L0.0058-0.014mg/L0.0058282.6Al 237.3130.444 %0.78mg/L0.00350.444mg/L0.003514,618.3B 249.6770.441 %0.54mg/L0.00240.441mg/L0.002426,985.6B 249.7720.433 %0.81mg/L0.00350.433mg/L0.00351,041.9B 208.957-45.18 %0.64mg/L0.291-45.18mg/L0.291-57,083.7B 182.5780.004 %3.75mg/L0.00020.004mg/L0.00021,285.1Fe 238.2040.004 %5.13mg/L0.00020.004mg/L0.00021,684.9Fe 239.5620.004 %5.18mg/L0.00020.004mg/L0.00021,713.2Fe 259.9390.008 %0.42mg/L0.00000.008mg/L0.0000968.3Fe 234.3490.004 %3.38mg/L0.00010.004mg/L0.0001210.3Fe 273.9550.012 %39.01mg/L0.00480.012mg/L0.004818.7Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M8 DP E QU SHAN HAI 655 16

mg 5/16/2014 12:16:20PM

0.012 %0.88mg/L0.00010.012mg/L0.0001204.7Cd 228.8020.009 %3.81mg/L0.00030.009mg/L0.0003280.0Cd 226.502-0.001 %26.73mg/L0.0003-0.001mg/L0.0003-75.8Ni 231.604-0.012 %2.83mg/L0.0004-0.012mg/L0.0004-794.1Ni 221.648-0.001 %11.08mg/L0.0002-0.001mg/L0.0002-43.3Ni 232.003-0.001 %8.45mg/L0.0001-0.001mg/L0.0001-51.1Ni 341.476

-0.000 %34.01mg/L0.0002-0.000mg/L0.0002-8.6Ni 227.0220.020 %9.37mg/L0.00190.020mg/L0.001928.0Pb 220.3530.001 %528.25mg/L0.00550.001mg/L0.005517.4Pb 261.418-0.038 %12.14mg/L0.0047-0.038mg/L0.0047-162.0Pb 283.306-0.000 %1,640.58mg/L0.0078-0.000mg/L0.0078102.6Pb 405.781-0.001 %85.57mg/L0.0012-0.001mg/L0.0012-5.7Cr 205.560-0.001 %47.36mg/L0.0006-0.001mg/L0.0006-241.3Cr 283.5630.001 %85.62mg/L0.00060.001mg/L0.0006-67.6Cr 284.325-0.003 %13.17mg/L0.0004-0.003mg/L0.0004-171.8Cr 357.869-0.002 %3.01mg/L0.0001-0.002mg/L0.0001423.4Mn 257.610-0.025 %5.33mg/L0.0013-0.025mg/L0.0013-4,308.1Mn 259.372-0.003 %11.87mg/L0.0003-0.003mg/L0.0003216.4Mn 260.5680.001 %24.19mg/L0.00030.001mg/L0.0003134.1Mn 294.9200.001 %122.00mg/L0.00090.001mg/L0.000977.2Mn 293.305-0.439 %0.60mg/L0.0026-0.439mg/L0.0026-17,243.0Mn 279.482-0.014 %5.40mg/L0.0008-0.014mg/L0.000894.0Mn 403.075-0.020 %3.87mg/L0.0008-0.020mg/L0.0008-91.4Zn 206.200-0.024 %0.79mg/L0.0002-0.024mg/L0.0002-584.2Zn 213.857-0.025 %5.24mg/L0.0013-0.025mg/L0.0013-195.3Zn 202.548-0.186 %3.08mg/L0.0057-0.186mg/L0.0057-526.7Zn 334.501-0.001 %292.54mg/L0.0019-0.001mg/L0.001912.9Co 228.6160.006 %8.79mg/L0.00060.006mg/L0.000621.2Co 238.8920.002 %40.01mg/L0.00070.002mg/L0.000720.0Co 230.7860.003 %43.35mg/L0.00130.003mg/L0.001373.9Co 236.380-0.006 %58.61mg/L0.0037-0.006mg/L0.0037-29.1Co 231.1600.330 %0.32mg/L0.00110.330mg/L0.00111,671,203.4Sr 421.5520.274 %1.61mg/L0.00440.274mg/L0.0044375,825.5Sr 460.7330.410 %13.16mg/L0.05400.410mg/L0.0540223.6Sr 232.2358.405 %1.85mg/L0.15538.405mg/L0.15535,620.9K 404.721-0.065 %2.15mg/L0.0014-0.065mg/L0.0014-1,026.2Al 396.153-0.069 %5.40mg/L0.0037-0.069mg/L0.0037-379.7Al 308.215-0.066 %2.59mg/L0.0017-0.066mg/L0.0017-1,065.6Al 394.401-0.082 %4.30mg/L0.0035-0.082mg/L0.0035-86.7Al 237.3130.412 %0.94mg/L0.00390.412mg/L0.003913,607.0B 249.6770.409 %1.26mg/L0.00520.409mg/L0.005225,101.5B 249.7720.411 %1.02mg/L0.00420.411mg/L0.0042989.6B 208.957-49.67 %0.55mg/L0.271-49.67mg/L0.271-62,764.4B 182.5780.001 %1.88mg/L0.00000.001mg/L0.0000423.9Fe 238.2040.001 %5.24mg/L0.00000.001mg/L0.0000561.2Fe 239.5620.000 %3.39mg/L0.00000.000mg/L0.0000521.1Fe 259.9390.005 %2.01mg/L0.00010.005mg/L0.0001589.6Fe 234.3490.001 %37.53mg/L0.00040.001mg/L0.000462.6Fe 273.9550.012 %120.64mg/L0.01420.012mg/L0.014218.1Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M9 E QU SHAN HAI 656 17

mg 5/16/2014 12:20:11PM

0.009 %10.38mg/L0.00100.009mg/L0.0010164.5Cd 228.8020.007 %7.53mg/L0.00050.007mg/L0.0005226.1Cd 226.502-0.001 %32.54mg/L0.0003-0.001mg/L0.0003-72.7Ni 231.604-0.012 %7.48mg/L0.0009-0.012mg/L0.0009-788.8Ni 221.648-0.001 %5.61mg/L0.0001-0.001mg/L0.0001-43.0Ni 232.003-0.001 %7.73mg/L0.0001-0.001mg/L0.0001-67.7Ni 341.476-0.000 %2,558.35mg/L0.0005-0.000mg/L0.00056.3Ni 227.0220.010 %81.44mg/L0.00850.010mg/L0.008514.4Pb 220.353-0.006 %123.74mg/L0.0080-0.006mg/L0.0080-0.9Pb 261.418-0.043 %11.05mg/L0.0048-0.043mg/L0.0048-188.2Pb 283.3060.007 %86.26mg/L0.00590.007mg/L0.0059210.8Pb 405.781-0.001 %136.96mg/L0.0011-0.001mg/L0.00110.2Cr 205.560

-0.002 %17.40mg/L0.0004-0.002mg/L0.0004-284.7Cr 283.563-0.000 %182.81mg/L0.0006-0.000mg/L0.0006-97.3Cr 284.325-0.003 %10.24mg/L0.0003-0.003mg/L0.0003-195.2Cr 357.869-0.001 %11.92mg/L0.0002-0.001mg/L0.0002577.4Mn 257.610-0.027 %14.10mg/L0.0038-0.027mg/L0.0038-4,696.8Mn 259.372-0.002 %14.90mg/L0.0003-0.002mg/L0.0003298.1Mn 260.5680.002 %13.89mg/L0.00030.002mg/L0.0003196.5Mn 294.9200.003 %12.88mg/L0.00030.003mg/L0.0003141.6Mn 293.305-0.464 %0.32mg/L0.0015-0.464mg/L0.0015-18,229.4Mn 279.482-0.014 %3.66mg/L0.0005-0.014mg/L0.0005129.0Mn 403.075-0.021 %6.53mg/L0.0013-0.021mg/L0.0013-92.4Zn 206.200-0.025 %1.69mg/L0.0004-0.025mg/L0.0004-635.2Zn 213.857-0.027 %5.05mg/L0.0014-0.027mg/L0.0014-219.2Zn 202.548-0.181 %5.28mg/L0.0096-0.181mg/L0.0096-511.8Zn 334.501-0.002 %193.20mg/L0.0037-0.002mg/L0.00375.2Co 228.6160.005 %3.02mg/L0.00010.005mg/L0.0001-21.6Co 238.892-0.000 %656.56mg/L0.0030-0.000mg/L0.00309.0Co 230.7860.003 %25.80mg/L0.00070.003mg/L0.000768.5Co 236.380-0.006 %38.84mg/L0.0024-0.006mg/L0.0024-28.0Co 231.1600.380 %0.80mg/L0.00310.380mg/L0.00311,882,018.2Sr 421.5520.302 %1.72mg/L0.00520.302mg/L0.0052402,788.8Sr 460.7330.459 %8.91mg/L0.04090.459mg/L0.0409248.5Sr 232.2359.007 %4.84mg/L0.43579.007mg/L0.43575,938.2K 404.721-0.061 %1.79mg/L0.0011-0.061mg/L0.0011-634.2Al 396.153-0.052 %50.88mg/L0.0264-0.052mg/L0.0264-45.1Al 308.215-0.062 %4.20mg/L0.0026-0.062mg/L0.0026-770.3Al 394.401-0.058 %49.49mg/L0.0285-0.058mg/L0.028546.9Al 237.3130.437 %0.44mg/L0.00190.437mg/L0.001914,393.4B 249.6770.434 %0.25mg/L0.00110.434mg/L0.001126,566.3B 249.7720.432 %0.40mg/L0.00170.432mg/L0.00171,038.7B 208.957-48.76 %2.21mg/L1.080-48.76mg/L1.080-61,613.7B 182.5780.002 %1.33mg/L0.00000.002mg/L0.0000659.6Fe 238.2040.001 %7.38mg/L0.00010.001mg/L0.0001843.5Fe 239.5620.001 %8.63mg/L0.00010.001mg/L0.0001802.1Fe 259.9390.005 %1.95mg/L0.00010.005mg/L0.0001653.2Fe 234.3490.002 %11.63mg/L0.00020.002mg/L0.0002110.1Fe 273.9550.004 %140.30mg/L0.00500.004mg/L0.00509.5Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M9 DP E QU SHAN HAI 657 18

mg 5/16/2014 12:24:00PM

0.010 %5.09mg/L0.00050.010mg/L0.0005169.8Cd 228.8020.007 %9.23mg/L0.00070.007mg/L0.0007225.3Cd 226.502-0.001 %23.93mg/L0.0002-0.001mg/L0.0002-72.2Ni 231.604-0.009 %8.12mg/L0.0008-0.009mg/L0.0008-626.4Ni 221.648-0.001 %7.03mg/L0.0001-0.001mg/L0.0001-42.9Ni 232.003-0.001 %36.27mg/L0.0003-0.001mg/L0.0003-45.7Ni 341.4760.000 %21.80mg/L0.00010.000mg/L0.000118.5Ni 227.0220.011 %12.08mg/L0.00130.011mg/L0.001315.2Pb 220.353-0.004 %137.79mg/L0.0055-0.004mg/L0.00555.0Pb 261.418-0.039 %15.59mg/L0.0060-0.039mg/L0.0060-162.9Pb 283.3060.001 %213.52mg/L0.00240.001mg/L0.0024125.9Pb 405.781-0.001 %50.14mg/L0.0004-0.001mg/L0.0004-0.5Cr 205.560-0.001 %4.10mg/L0.0000-0.001mg/L0.0000-200.9Cr 283.5630.002 %8.25mg/L0.00020.002mg/L0.0002-28.6Cr 284.325-0.003 %15.08mg/L0.0004-0.003mg/L0.0004-171.4Cr 357.869-0.000 %51.71mg/L0.0002-0.000mg/L0.0002721.9Mn 257.610-0.022 %22.08mg/L0.0049-0.022mg/L0.0049-3,826.5Mn 259.372-0.001 %5.89mg/L0.0000-0.001mg/L0.0000388.8Mn 260.568

0.003 %8.34mg/L0.00030.003mg/L0.0003244.9Mn 294.9200.003 %27.37mg/L0.00080.003mg/L0.0008161.7Mn 293.305-0.466 %1.12mg/L0.0052-0.466mg/L0.0052-18,309.1Mn 279.482-0.012 %7.63mg/L0.0009-0.012mg/L0.0009227.6Mn 403.075-0.019 %19.18mg/L0.0037-0.019mg/L0.0037-83.1Zn 206.200-0.024 %2.16mg/L0.0005-0.024mg/L0.0005-587.0Zn 213.857-0.026 %4.87mg/L0.0013-0.026mg/L0.0013-206.1Zn 202.548-0.185 %6.05mg/L0.0112-0.185mg/L0.0112-523.1Zn 334.501-0.001 %166.42mg/L0.0014-0.001mg/L0.001411.6Co 228.6160.006 %3.79mg/L0.00020.006mg/L0.00027.8Co 238.8920.000 %733.10mg/L0.00340.000mg/L0.003413.4Co 230.7860.003 %56.77mg/L0.00200.003mg/L0.002080.9Co 236.380-0.008 %23.30mg/L0.0019-0.008mg/L0.0019-41.5Co 231.1600.405 %1.66mg/L0.00670.405mg/L0.00671,989,169.1Sr 421.5520.349 %4.63mg/L0.01610.349mg/L0.0161448,767.5Sr 460.7330.486 %13.98mg/L0.06800.486mg/L0.0680262.2Sr 232.2359.626 %6.70mg/L0.64499.626mg/L0.64496,264.5K 404.721-0.065 %1.67mg/L0.0011-0.065mg/L0.0011-1,041.7Al 396.153-0.062 %25.21mg/L0.0157-0.062mg/L0.0157-253.1Al 308.215-0.067 %3.65mg/L0.0025-0.067mg/L0.0025-1,220.2Al 394.401-0.073 %19.47mg/L0.0142-0.073mg/L0.0142-36.2Al 237.3130.450 %0.92mg/L0.00410.450mg/L0.004114,799.8B 249.6770.447 %0.83mg/L0.00370.447mg/L0.003727,295.2B 249.7720.442 %1.41mg/L0.00630.442mg/L0.00631,063.3B 208.957-49.57 %2.16mg/L1.070-49.57mg/L1.070-62,635.5B 182.5780.002 %2.27mg/L0.00010.002mg/L0.0001642.6Fe 238.2040.001 %7.99mg/L0.00010.001mg/L0.0001848.0Fe 239.5620.001 %2.97mg/L0.00000.001mg/L0.0000830.8Fe 259.9390.005 %4.62mg/L0.00020.005mg/L0.0002676.9Fe 234.3490.002 %8.56mg/L0.00020.002mg/L0.0002121.1Fe 273.9550.011 %52.47mg/L0.00600.011mg/L0.006017.7Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M10 E QU SHAN HAI 658 19

mg 5/16/2014 12:27:50PM

0.013 %4.49mg/L0.00060.013mg/L0.0006223.0Cd 228.8020.011 %7.98mg/L0.00090.011mg/L0.0009333.9Cd 226.502-0.001 %9.45mg/L0.0001-0.001mg/L0.0001-75.4Ni 231.604-0.017 %6.58mg/L0.0011-0.017mg/L0.0011-1,066.9Ni 221.648-0.001 %27.72mg/L0.0004-0.001mg/L0.0004-38.2Ni 232.003-0.001 %11.85mg/L0.0001-0.001mg/L0.0001-61.3Ni 341.4760.001 %58.16mg/L0.00030.001mg/L0.000326.1Ni 227.0220.001 %982.23mg/L0.01290.001mg/L0.01291.7Pb 220.353-0.015 %22.70mg/L0.0033-0.015mg/L0.0033-21.2Pb 261.418-0.032 %10.52mg/L0.0033-0.032mg/L0.0033-124.5Pb 283.306-0.004 %270.89mg/L0.0105-0.004mg/L0.010552.1Pb 405.781-0.002 %113.54mg/L0.0022-0.002mg/L0.0022-12.0Cr 205.560-0.001 %42.97mg/L0.0004-0.001mg/L0.0004-220.4Cr 283.5630.001 %126.31mg/L0.00160.001mg/L0.0016-53.8Cr 284.325-0.004 %7.21mg/L0.0003-0.004mg/L0.0003-244.6Cr 357.8690.000 %31.91mg/L0.00000.000mg/L0.0000808.7Mn 257.610-0.019 %17.73mg/L0.0033-0.019mg/L0.0033-3,229.2Mn 259.372-0.000 %69.88mg/L0.0001-0.000mg/L0.0001425.5Mn 260.5680.003 %13.21mg/L0.00040.003mg/L0.0004262.5Mn 294.9200.002 %23.83mg/L0.00060.002mg/L0.0006139.0Mn 293.305-0.472 %1.40mg/L0.0066-0.472mg/L0.0066-18,550.3Mn 279.482-0.012 %4.79mg/L0.0006-0.012mg/L0.0006241.7Mn 403.075-0.015 %6.66mg/L0.0010-0.015mg/L0.0010-52.1Zn 206.200-0.022 %3.84mg/L0.0008-0.022mg/L0.0008-489.3Zn 213.857

-0.026 %6.61mg/L0.0017-0.026mg/L0.0017-206.6Zn 202.548-0.266 %6.59mg/L0.0176-0.266mg/L0.0176-763.0Zn 334.501-0.000 %73.75mg/L0.0004-0.000mg/L0.000413.9Co 228.6160.005 %14.00mg/L0.00060.005mg/L0.0006-25.5Co 238.8920.003 %151.81mg/L0.00410.003mg/L0.004124.3Co 230.7860.004 %42.06mg/L0.00160.004mg/L0.001684.6Co 236.380-0.008 %35.92mg/L0.0029-0.008mg/L0.0029-40.6Co 231.1600.393 %1.60mg/L0.00630.393mg/L0.00631,939,769.6Sr 421.5520.319 %4.58mg/L0.01460.319mg/L0.0146420,115.8Sr 460.7330.534 %3.75mg/L0.02000.534mg/L0.0200286.3Sr 232.2359.211 %4.44mg/L0.40889.211mg/L0.40886,045.6K 404.7210.019 %12.26mg/L0.00230.019mg/L0.00237,323.2Al 396.1530.040 %13.19mg/L0.00530.040mg/L0.00531,808.9Al 308.2150.014 %21.65mg/L0.00310.014mg/L0.00316,076.4Al 394.4010.031 %20.99mg/L0.00660.031mg/L0.0066531.1Al 237.3130.405 %0.19mg/L0.00080.405mg/L0.000813,396.1B 249.6770.402 %0.26mg/L0.00110.402mg/L0.001124,705.4B 249.7720.398 %1.05mg/L0.00420.398mg/L0.0042959.4B 208.957-47.15 %1.46mg/L0.687-47.15mg/L0.687-59,575.3B 182.5780.007 %4.24mg/L0.00030.007mg/L0.00032,141.4Fe 238.2040.007 %5.45mg/L0.00040.007mg/L0.00042,780.2Fe 239.5620.007 %4.67mg/L0.00030.007mg/L0.00032,833.0Fe 259.9390.012 %3.79mg/L0.00040.012mg/L0.00041,497.5Fe 234.3490.007 %8.60mg/L0.00060.007mg/L0.0006320.4Fe 273.9550.005 %183.39mg/L0.00900.005mg/L0.009010.9Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M10 DP E QU SHAN HAI 659 20

mg 5/16/2014 12:31:41PM

0.013 %4.55mg/L0.00060.013mg/L0.0006221.6Cd 228.8020.010 %4.32mg/L0.00040.010mg/L0.0004319.7Cd 226.502-0.001 %18.52mg/L0.0002-0.001mg/L0.0002-80.9Ni 231.604-0.012 %4.29mg/L0.0005-0.012mg/L0.0005-763.2Ni 221.648-0.001 %17.38mg/L0.0002-0.001mg/L0.0002-35.0Ni 232.003-0.001 %18.81mg/L0.0002-0.001mg/L0.0002-53.5Ni 341.476-0.000 %141.12mg/L0.0006-0.000mg/L0.0006-7.4Ni 227.0220.024 %50.37mg/L0.01200.024mg/L0.012033.3Pb 220.353-0.007 %49.95mg/L0.0034-0.007mg/L0.0034-1.9Pb 261.418-0.038 %1.01mg/L0.0004-0.038mg/L0.0004-160.4Pb 283.306-0.007 %48.99mg/L0.0035-0.007mg/L0.00355.1Pb 405.781-0.002 %63.19mg/L0.0014-0.002mg/L0.0014-13.9Cr 205.560-0.002 %13.26mg/L0.0002-0.002mg/L0.0002-268.1Cr 283.5630.002 %44.81mg/L0.00090.002mg/L0.0009-35.3Cr 284.325-0.004 %12.16mg/L0.0004-0.004mg/L0.0004-229.7Cr 357.869-0.001 %6.16mg/L0.0001-0.001mg/L0.0001552.6Mn 257.610-0.025 %7.40mg/L0.0019-0.025mg/L0.0019-4,418.1Mn 259.372-0.002 %8.25mg/L0.0001-0.002mg/L0.0001288.5Mn 260.5680.003 %24.60mg/L0.00060.003mg/L0.0006217.6Mn 294.9200.002 %29.06mg/L0.00060.002mg/L0.0006125.4Mn 293.305-0.460 %0.23mg/L0.0011-0.460mg/L0.0011-18,070.5Mn 279.482-0.013 %3.24mg/L0.0004-0.013mg/L0.0004156.3Mn 403.075-0.015 %8.66mg/L0.0013-0.015mg/L0.0013-55.4Zn 206.200-0.021 %2.12mg/L0.0005-0.021mg/L0.0005-456.7Zn 213.857-0.024 %6.20mg/L0.0015-0.024mg/L0.0015-186.5Zn 202.548-0.277 %1.99mg/L0.0055-0.277mg/L0.0055-795.7Zn 334.5010.000 %1,805.17mg/L0.00170.000mg/L0.001717.3Co 228.6160.007 %10.42mg/L0.00070.007mg/L0.000724.8Co 238.892-0.002 %161.09mg/L0.0026-0.002mg/L0.00263.5Co 230.7860.001 %228.52mg/L0.00250.001mg/L0.002549.6Co 236.380

-0.008 %79.71mg/L0.0060-0.008mg/L0.0060-36.6Co 231.1600.400 %0.66mg/L0.00260.400mg/L0.00261,967,949.3Sr 421.5520.325 %1.32mg/L0.00430.325mg/L0.0043425,984.3Sr 460.7330.521 %9.24mg/L0.04810.521mg/L0.0481279.8Sr 232.2358.351 %1.82mg/L0.15238.351mg/L0.15235,592.2K 404.721-0.053 %2.01mg/L0.0011-0.053mg/L0.0011221.7Al 396.153-0.056 %1.04mg/L0.0006-0.056mg/L0.0006-135.8Al 308.215-0.054 %1.55mg/L0.0008-0.054mg/L0.000813.0Al 394.401-0.064 %3.86mg/L0.0025-0.064mg/L0.002511.3Al 237.3130.380 %0.94mg/L0.00360.380mg/L0.003612,604.8B 249.6770.376 %0.97mg/L0.00370.376mg/L0.003723,213.9B 249.7720.371 %1.05mg/L0.00390.371mg/L0.0039897.5B 208.957-91.03 %0.47mg/L0.431-91.03mg/L0.431-115,049.2B 182.5780.003 %3.91mg/L0.00010.003mg/L0.0001855.6Fe 238.2040.002 %4.05mg/L0.00010.002mg/L0.00011,083.4Fe 239.5620.002 %3.24mg/L0.00010.002mg/L0.00011,095.7Fe 259.9390.007 %2.70mg/L0.00020.007mg/L0.0002927.7Fe 234.3490.003 %10.12mg/L0.00030.003mg/L0.0003132.9Fe 273.9550.005 %110.62mg/L0.00530.005mg/L0.005310.7Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Sample)

M11 E QU SHAN HAI 660 21

mg 5/16/2014 12:35:32PM

0.008 %0.68mg/L0.00010.008mg/L0.0001145.1Cd 228.8020.007 %12.89mg/L0.00090.007mg/L0.0009225.3Cd 226.502-0.001 %12.45mg/L0.0001-0.001mg/L0.0001-72.1Ni 231.604-0.000 %965.26mg/L0.0019-0.000mg/L0.0019-105.6Ni 221.648-0.001 %10.82mg/L0.0001-0.001mg/L0.0001-10.5Ni 232.003-0.001 %46.94mg/L0.0003-0.001mg/L0.0003-25.3Ni 341.476-0.000 %63.64mg/L0.0002-0.000mg/L0.0002-3.0Ni 227.0220.007 %63.95mg/L0.00450.007mg/L0.00459.7Pb 220.353-0.007 %127.66mg/L0.0092-0.007mg/L0.0092-2.7Pb 261.418-0.043 %7.61mg/L0.0033-0.043mg/L0.0033-188.5Pb 283.306-0.009 %67.94mg/L0.0059-0.009mg/L0.0059-18.9Pb 405.781-0.001 %125.43mg/L0.0007-0.001mg/L0.00072.5Cr 205.560-0.002 %34.56mg/L0.0006-0.002mg/L0.0006-269.2Cr 283.5630.002 %47.16mg/L0.00110.002mg/L0.0011-23.6Cr 284.325-0.003 %16.33mg/L0.0005-0.003mg/L0.0005-170.2Cr 357.8690.001 %22.67mg/L0.00030.001mg/L0.0003975.1Mn 257.610-0.017 %15.90mg/L0.0027-0.017mg/L0.0027-2,913.3Mn 259.3720.001 %9.15mg/L0.00010.001mg/L0.0001503.6Mn 260.5680.004 %9.53mg/L0.00040.004mg/L0.0004311.9Mn 294.9200.004 %23.41mg/L0.00100.004mg/L0.0010205.8Mn 293.305-0.514 %0.36mg/L0.0019-0.514mg/L0.0019-20,233.3Mn 279.482-0.011 %5.95mg/L0.0006-0.011mg/L0.0006351.7Mn 403.0750.005 %38.49mg/L0.00180.005mg/L0.001883.4Zn 206.200-0.004 %34.43mg/L0.0012-0.004mg/L0.0012365.9Zn 213.857-0.005 %18.14mg/L0.0010-0.005mg/L0.001020.7Zn 202.548-0.163 %3.29mg/L0.0054-0.163mg/L0.0054-458.4Zn 334.5010.000 %180.87mg/L0.00090.000mg/L0.000919.7Co 228.6160.004 %29.19mg/L0.00120.004mg/L0.0012-34.6Co 238.892-0.002 %86.08mg/L0.0013-0.002mg/L0.00133.8Co 230.7860.003 %41.39mg/L0.00140.003mg/L0.001479.5Co 236.380-0.006 %67.97mg/L0.0043-0.006mg/L0.0043-29.5Co 231.1600.315 %0.44mg/L0.00140.315mg/L0.00141,607,051.1Sr 421.5520.262 %3.24mg/L0.00850.262mg/L0.0085363,880.2Sr 460.7330.408 %10.05mg/L0.04100.408mg/L0.0410222.6Sr 232.23510.93 %2.88mg/L0.31510.93mg/L0.3156,949.0K 404.721-0.051 %23.71mg/L0.0121-0.051mg/L0.0121374.5Al 396.153

-0.065 %20.70mg/L0.0134-0.065mg/L0.0134-300.5Al 308.215-0.052 %20.31mg/L0.0105-0.052mg/L0.0105203.8Al 394.401-0.073 %22.10mg/L0.0162-0.073mg/L0.0162-40.0Al 237.3130.337 %1.83mg/L0.00620.337mg/L0.006211,244.9B 249.6770.332 %1.38mg/L0.00460.332mg/L0.004620,615.5B 249.7720.323 %2.36mg/L0.00760.323mg/L0.0076786.4B 208.957-7.251 %1.76mg/L0.1274-7.251mg/L0.1274-9,138.7B 182.5780.004 %3.34mg/L0.00010.004mg/L0.00011,162.4Fe 238.2040.003 %6.62mg/L0.00020.003mg/L0.00021,515.4Fe 239.5620.003 %5.29mg/L0.00020.003mg/L0.00021,549.2Fe 259.9390.007 %3.96mg/L0.00030.007mg/L0.0003904.3Fe 234.3490.004 %15.64mg/L0.00060.004mg/L0.0006188.1Fe 273.9550.017 %49.11mg/L0.00840.017mg/L0.008423.8Cu 221.459

Mean Data

ID: Seq. No.: A/S Pos:

Sample Qty: Prep. Vol.: Dilution: : Date:Analyte Corr. Intensity Conc (Calib) Std. Dev. Calib Units Std. Dev. Sample Units RSDConc (Samp