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TiAu based micro-calorimeters for the XEUS space mission by Bob Dirks on behalf of the Sensor Research and Development Division Depicts: artist's impression of the XEUS spacecraft Copyright: ESA
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TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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Page 1: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

TiAu based micro-calorimeters for the XEUS space mission

by Bob Dirks

on behalf of the Sensor Research and Development Division

Depicts: artist's impression of the XEUS spacecraftCopyright: ESA

Page 2: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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Outline:1. XEUS

-satellite and instruments-detector specifications

2. Transition Edge Sensors (TESs)- Detection principle- Pixel and array development

3. EURECA

4. Measurement results (highlights)- RT-measurements- X-ray resolution with Cu/Bi absorbers- Cross-talk

5. Conclusions

6. Perspective and future plans

Page 3: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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1. X-ray Evolving Universe Spectroscopy (XEUS)Satellite and instruments:

detector spacecraft

~35 m

• Formation flying mission• Detector spacecraft:

1. high spectral resolution imager 2. wide field imager3. hard X-ray imager4. non-imaging high time-resolution spectrometer5. imaging X-ray polarimeter

mirror spacecraft

Transition Edge Sensors in 32x32 array (SRON)

Page 4: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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1. X-ray Evolving Universe Spectroscopy (XEUS)

Characteristics:

energy range 0.1 – 20 keV

energy resolution 2 eV @ 2 keV5 eV @ 6 keV

pixel size (μm2) 240x240

filling factor > 92%

Detector specifications: high spectral resolution imager

Page 5: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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2. Transition Edge Sensors (TESs)Detection principle

Page 6: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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2. Transition Edge Sensors (TESs)

Testing:- different detector geometries - different absorber-TES couplings

SRON in-house capabilities: -detector production (clean room)-characterization (cryogenic facilities)

Pixel development

2.5 eV @ 6 keV

Page 7: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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2. Transition Edge Sensors (TESs)

“Paddo” (mushroom shaped absorber) 5x5 prototype produced and under test

top viewside view

Array development

Page 8: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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2. Transition Edge Sensors (TESs)

32x32 array produced, prototype for XEUSArray development

8 mm1.25 mm

Page 9: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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3. EURECA (EURopean-JapanEse Calorimeter Array) project

Vb

Rs TES

L

C

SQUID

t

I

3.66 eV@320 kHz

Frequency Domain Multiplexing read-out

Technological readiness of 5x5 pixel array with read-out

Page 10: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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4. Measurement results: RT measurements on arrays

-0.02

0

0.02

0.04

0.06

0.08

0.1

0.12

0.14

0.16

0.095 0.1 0.105 0.11 0.115 0.12 0.125

Res

ista

nce

(ohm

)

Themperature (K)

RT TT086-26-chip19

pix 21pix 13pix 1

pix 10pix 15pix 19pix 20pix 25pix 5pix 7

Critical temperature (112 mK) homogeneousin array!!

“Paddo” prototype array

Page 11: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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4. Measurement results: X-ray resolution Cu/Bi absorbers

2.5 eV @ 6 keV (FWHM)100 μs falltime

Cu: 1 μm, Bi: 2.64 μm

Bi

K-Alpha spectrum with Holzer fit

increase stopping power

Page 12: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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Max. amplitude (thermal) black/ red signal: @ 20 keV

nearest neighbor ~5x10-4 10 eV

diagonal neighbor ~7x10-6 0.14 eV

4. Measurement results: cross-talk

thermal

electronic

trigger threshold:

150 eV

Page 13: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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5. Conclusions

- Central absorber coupling most promising

- Homogeneous Tc in arrays

- Adding bismuth to absorber no influence on detector performance (energy resolution)

- Cross-talk: << 150 eV, no problem for astrophysics applications

- Promising results with Frequency Domain Multiplexing:3.7 eV (FWHM) @ 6 keV

Page 14: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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6. Perspective and future plans

CuBi

“Paddo”

2.5 eV @ 6 keV

Bi

Bi

Cu

Cu

Pixel development:

Page 15: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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6. Perspective and future plansArray development:Frequency Domain Multiplexing Read-out

Page 16: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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Thank you for your attention.

Questions?

Page 17: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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3. Experimental setup and measurement methods

Adiabatic Demagnetisation Refrigeration

ADR Kelvinox

dilution fridge

Completely automated!

Page 18: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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Complex Impedance:

Page 19: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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SQUID feedback circuit:

Bias circuit:

Page 20: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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TES-based Single Pixel Microcalorimeters; X-ray

• TES: superconducting thin film with Tc = 100 mK (TiAu)

• Silicon-Nitride micromachining

0 2000 4000 6000 8000Energy (eV)

0

20

40

60

Cou

nts

5870 5880 5890 5900 5910 5920Energy (eV)

0

20

40

60

Cou

nts

FWHM = 3.9 eV

ΔE = 2.5 eV at 6 keV; 100 μs(state of the art performance)

0.0

0.4

0.8

1.2

1.6

0.1057 0.1059 0.1061 0.1063Temperature (K)

Res

ista

nce

(Ohm

) ΔT= 200 μK

Supercon-ducting

Normal

Page 21: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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• Integrate 5 x 5 TES-array and FDM read-out in an ADR coolersynchrotron testing

• Development AC-bias electronics, MUX/de-MUX,acquisition and command and control electronics (ASICs)

• Flexible set-up: testing of different detectors and FDM concepts

• SRON-lead effort with EU and Japanese partners; a strong EU consortium develops

• Test-bed for XEUS TRL

EURECA Prototype X-ray Instrument

Page 22: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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EURECA test set-up at PTB-BESSY

• Measurement run at BESSYSXR700 beam line April 2007

• Energy range: 0.2 – 1.8 keV

Page 23: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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EURECA test set-up at PTB-BESSY

High count rate (250 eV) dE = 1.55 eV @ 50 cpsdE = 1.72 eV @ 500 cps

Page 24: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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• Arrays need multiplexed read-out (because of limited cooling power, electronics power budget, mass budget)

• Multiplexing is done in the frequency domain (FDM)

Multiplexed Read-out of TES-based Arrays

Vb

Rs TES

L

C

SQUID

t

I

Vb

Vbf1

f2

NBF

f

columnSQUID

columnSQUID

AC and DC performance similar; FDM concept validated

320 kHz3.66 eV

Page 25: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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SRON clean room

Large in-house clean room facility at Utrecht (upgraded in 2007)- Lithography: development and production 300 m2 class 100- Assembly and instrumentation test area 600 m2 class 10000

Profile of the activitiesLithography, thin film technology, silicon-micromachining

Development of novel (superconducting) sensors and components for future space instruments for which no commercial production route is available

The choice of materials (and their combination) is unique The dedicated in-house facilities allow for short turn around times in research, performance optimization and final production

Collaborations with MESA+, Philips, Delft University when needed

SRON facilities also available for external parties

Page 26: TiAu based micro-calorimeters for space applicationsndip.in2p3.fr/ndip08/Presentations/3Tuesday/A-Midi/212... · 2008-06-17 · 2. Outline: 1. XEUS-satellite and instruments-detector

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The SRON clean room