Thermal Desorption System TD-30 series - … Brochure_e.pdf · The TD-30 series has been designed to enable Trap tube and O-ring, rotor of valve replacement and other maintenance

Thermal Desorption System

TD-30 series

1. Outstanding throughputTD-30R(120 tubes) and TD-30 (60 tubes) make it possible to use night time and weekend with high throughput with overlap function.

2. Restoring the sampleThe Tube quick cooling mechanism on the TD-30R made it possible to restore and reanalyze the sample.

3. TraceabilityNot only result of leak test, recorded temperature and flowrate helps to trace the reason of fault.Optional bar code reader allows samples to controlled using bar codes.Internal standard addition function on TD-30R helps to confirm the result of analysis.

4. Robustness and easy maintenanceNew designed tube protector prevents the tube related trouble.The seal trap and other consumables can easily be replaced from the top of instrument.

5. Ease of useAn easy-to-learn user interface and flexible setting help to prevent operating errors.

TD-30 Thermal Desorption SystemA Revolutionary TD with outstanding high throughput and reliability

The TD-30 series is developed for best solution of gas and material analysis. Its out standing high throughput and user-friendly design support all types of analysis, from research to quality control.

Outstanding throughput

Sample capacity

Tube conditioning mode

The capacity of 120 samples of TD - 30R and 60 samples of TD - 30 enables efficient use at night and on weekends.The analysis schedule can be set up to 1000 lines with the batch editor.The sample tray at the low position on the front of the instrument is accessible even during analysis and prevents misplacement of the tube.

Tube conditioning function allows you to condition a large number of tubes for sampling.

TD-30R TD-30

Comply to every tube

Various sample tubes sold for Shimadzu TD can also be used.The sample tube of ¼ 'x 3.5' corresponds to many sampling equipment and peripheral equipment.

Over-lap analysis

The time of analysis cycle is decreased by Over-lap function. If GC is not Ready, wait for injection to avoid analysis failure.

Restoring the sample

Quick cooling

Tube Desorb

Quick cool

•Simultaneous analysis from low to high boiling point compound

TD-30R Restoring analysis

Boiling pointLow High

Immediately after the tube desorb are completed, the tube heating block moves away from the tube and the tube is cooled at high speed by air blowing by the fan.As a result, sample tubes are held without breakthrough of low boiling point components.Since there is no need to replace the tube, there is no need to worry about air mixing due to tube replacing.

Flow path without cold point

Since there are no cold point on flow path recovery rete of High-boiling point components is high.A sharp peak shape can be obtained with a short transfer line with a small dead volume.

1st analysis

2nd analysis

Analysis of High boiling point hydro carbons

Traceability

When an optional bar code reader is installed, the bar code printed on the tube is automatically read and recorded. The barcode can be used for sample management and usage history management of sample tubes.

In addition to the leak test results, the function to record the temperature of the tube, trap and flow rate will support tracing of the cause of the abnormal result.

The internal standard sample addition function of TD-30R adds a gaseous standard substance to the sample tube to improve the reliability of the measurement result.It has a fixed addition mode using a heated sample loop and an addition amount variable mode using a mass flow controller.

2 types of Internal Standard Addition

Bar code reader

Pre treatment result browser

D8-Toluene 1ppmadd. 20mL/min×0.2minRSD%<2

Robustness and Easy maintenance

TD of cap attaching / detaching type is easy to handle but there was a risk of glass tube breakege. TD-30 prevents tube troubles by newly designed tube protection mechanism.

The TD-30 series has been designed to enable Trap tube and O-ring, rotor of valve replacement and other maintenance work to be performed easily from the top of the instrument.The joint of the capillary column places in the column oven of the GC and it is easy to install.Consumable Usage Counter records the number of uses for each part and reports when it reaches a set number, so it is possible to prevent troubles due to the lifetime of parts. This superior design minimizes downtime during maintenance and improves laboratory productivity.

Tube protection

Easy maintenance

By releasing the pressure before the tube release, it prevents the adsorbent and holding material from moving.

Pressure release

Trap

Column joint

O-ring

Consumable usage counter

Rotor

Usability

The control software of TD-30 is very easy to learn the operation method by the same user interface as GC, GC-MS method, batch file setting screen and look and feel.It is also possible to add or interrupt samples during batch processing.

Flexibility

If the operator forgets to place a tube in the sample tray or a leak error occurs due to an improperly sealed tube, the system allows the operator to select whether to stop the continuous analysis or skip the applicable tubes. That helps prevent wasting valuable time because of simple mistakes.It also allows the operator to select the actions to take in the event the barcode reader fails to read a tube.

Ease of Use

Convenient tools

An independent leak check function can be used for checking after maintenance and checking the state of the sample tube. By using the trap conditioning function you can lower the background immediately after replacing the trap.

The TD-GC-FID system with wide dynamic range can measure many components at the same time with low running cost.

VOC in Ambient air

11 3-chloro-1-propene12 Dichloromethane13 Acrylonitrile14 1,1-Dichloroethane15 cis-1,1-Dichloroethene16 Chloroform17 1,1,1-Trichloroethane18 CarbonTetrachloride19 Benzene20 1,2-Dichloroethane

31 m+p-xylene32 o-xylene33 Styrene34 1,1,2,2-Tetrachloroethane35 1,3,5-Trimethylbenzene36 1,2,4-Trimethylbenzene37 m-Dichlorobenzene38 p-Dichlorobenzene39 Benzylchloride40 o-Dichlorobenzene41 1,2,4-TrichlorobenzeneIS d8-Toluene

Work space air

2.0 3.0 4.0 5.0 6.0 min

GC-2030AF ＋ TD-30

It takes high cost to re-measure if atmospheric measurement fails in analysis. It is possible to lower the risk of failure of analysis by using the TD-30R restore and internal marking function.

1 Freon122 Freon1143 Chloroethene4 Chloromethane5 1,3-Butadiene6 Bromoethane7 Chloroethane8 Freon119 1,1-Dichloroethene10 Freon113

21 Trichloroethene22 1,2-Dichloropropane23 cis-1,3-Dichloropropane24 Toluene25 trans-1,3-Dichloropropane26 1,1,2-Trichloroethane27 Tetrachloroethane28 1,2-Dibromoethane29 Chlorobenzene30 Ethylbenzene

1st analysis

2nd analysis

Standard 100ng

Indoor Air

Tolu

ene

Hexane

Aceto

nitrile

Eth

ylb

enzene

Xyle

nes

Chemical release

Thermal Extraction

TD-30 with no cold point and short transfer line is ideal for SVOC measurement.Because it has low background, it can be used for trace analysis such as measurement of chemical release gas using chamber and measurement of atmospheric atmosphere in clean room.

VDA 278 of the method of measuring the emission gas of automobile parts, filling the tube with a sample piece, heating it to 100 ° C, measuring the VOC. After removing the sample, heating the tube to 280 ° C and measuring the SVOC on tube.The easy to access designed sample tray of TD-30 is suitable for the application.

Analysis of released gas from rubber

Simultaneous analysis of SVOC standard

VOC(100℃)

SVOC(280℃)

Flavor from foods

Odor from consumables

GCMS-TQ8040 ＋ TD-30R

Sample tray lays the tube horizontally TD-30 is not only solid but also viscous specimen can be set so it is suitable for analysis of aroma components in food.

The TD-30 series supports constant linear velocity carrier gas control by electronic flow controller. Therefore, semi-quantitative / qualitative using the retention index database can be used.

Analysis of cardboard

Retention index alkane

1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 7.0

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オーブン温度

保温バイアル数 最大12本オーバーラップ保温可能

TD-30seriesThermal Desorption System

Tube Dimension O.D.1/4‘ (6.35mm) L 3.5’（89mm)

Tube Desorb Temperature Setting: 0 to 430℃(in 1℃ unit) Control:Room temperature＋15 to 430℃(accuracy of ±1℃）

Tube Desorb Flow Setting: 20 to 200mL/min(in 1mL/min unit, accuracy of ±2mL/min）

Tube Desorb Time Setting: 0 to 240min(in 0.01min unit)

Trap Dimension O.D.1/8’(3.2mm)I.D.2mm L 102mm Silconert2000 Deactivated SUS tube

Trap Adsorbent TenaxTA 60-80mesh(60mg) StandardCarbopack(50mg)＋Carbosieve(10mg) OptionalCarboxene1000(70mg) Optional

Trap Desorb Temperature Setting: 0 to 350℃(in 1℃ unit)Control:0～350℃(accuracy of ±1℃）

Trap Cooling Temperature Setting: -40 to 80℃(in 1℃ unit) Control:Room temperature-50℃ to 80℃（Valve Temp.＜250℃), Room temperature-45℃ to 80℃(Valve Temp.＞250℃)accuracy of ±1℃

Split Ratio 1:5 to 1:200

Sample Path Silconert2000

Switching Valve 6 port 2 position high temperature Valve with Electric Actuator

Joint Temperature Setting: 0 to 300℃(in 1℃ unit) Control:Room temperature＋15℃ to 300℃(accuracy of ±1℃）

Valve Temperature Setting: 0 to 300℃(in 1℃ unit) Control:Room temperature＋15℃ to 300℃(accuracy of ±1℃）

Transfer Line Temperature Setting: 0 to 350℃(in 1℃ unit) Control:Room temperature＋15℃ to 350℃(accuracy of ±1℃）

Internal Standard Addition(TD-30R) Fixed Volume:0.5mL,Variable Volume:4mL to 2000mL

Dry Purge（TD-30R) Temperature Setting: -40 to 140℃(in 1℃ unit) Control:Room temperature-50℃ to 140℃(Valve Temp.＜250℃),Control:Room temperature-45℃ to 140℃(Valve Temp.＞250℃) accuracy of ±1℃、Flow：20 to 200mL/min(in 1mL/min unit),Time：0 to 30min(in 0.01min unit)

Carrier gas High-purity helium, nitrogen, Electronic control via Advanced flow controller (AFC) built into GC

Purge gas High-purity helium, nitrogen, Electronic control via mass flow controller (MFC) built into TD-30 series

PC Interface USB

Control Software TD Control Software

Software Operating Environment Microsoft Windows 7/10 (64/32Bit)

Guaranteed Operating Environment 13 to 33 °C, humidity 20 to 70 % RH (performance guaranteed at 18 to 28 °C)

Power Supply MAX1200VA

Dimensions TD-30R:720(W)470(H)690(D)mm, TD-30:580(W)470(H)550(D)mm

Weight 49kg(TD-30R), 48kg（TD-30)

Model Capacity Restore Dry Purge

ISTD addition

TD-30R 120 tubes 〇 〇 〇

TD-30 60 tubes

Dimensions (TD-30R GCMS-QP2020)

Specification and installation condition

TD-30R TD-30

1580

470

590

SilcoNert is a trademark of Silcotek.Tenax is a trademark of Buchem B.V.Carbopack Carbosieve Carboxen are trademark of MERCK.Windows is a trademark of Microsoft Corporation.