10/24/05 Technical Report for S M Stoller Star Center-WWNA Monthly; Largo, FL 7030-226 Accutest Job Number: F33038 Sampling Date: 07/06/05 Report to: S M Stoller [email protected]ATTN: Cathy Kelleher Total number of pages in report: Certifications: FL (DOH E83510), NC (573), NJ (FL002), MA (FL946), IA (366), LA (03051), KS (E-10327), SC, AK This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories. Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Conference and/or state specific certification programs as applicable. Harry Behzadi, Ph.D. Laboratory Director e-Hardcopy 2.0 Automated Report 18 1 of 18 F33038
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Technical Report for S M Stoller - Energy · Technical Report for S M Stoller ... all method specified calibrations and quality control performance criteria were met ... Metals By
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Section 4: Misc. Forms ............................................................................................................ 104.1: Chain of Custody ........................................................................................................... 11
Section 5: Metals Analysis - QC Data Summaries ................................................................ 135.1: Prep QC MP8284: As .................................................................................................... 14
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F33038
Accutest LabLink@41812 12:38 24-Oct-2005
Sample Summary
S M StollerJob No: F33038
Star Center-WWNA Monthly; Largo, FLProject No: 7030-226
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
F33038-1 07/06/05 09:37 JPC 07/06/05 AQ Ground Water PIN18-RW02-N001
F33038-2 07/06/05 09:38 JPC 07/06/05 AQ Ground Water PIN18-RW03-N001
F33038-3 07/06/05 09:39 JPC 07/06/05 AQ Ground Water PIN18-RW0501-N001
F33038-4 07/06/05 09:43 JPC 07/06/05 AQ Ground Water PIN18-EFF1-N001
F33038-5 07/06/05 09:45 JPC 07/06/05 AQ Water PIN18-EFF2-N001
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F33038
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: S M Stoller Job No: F33038
Site: Star Center-WWNA Monthly; Largo, FL Report Date 7/20/2005
5 Samples were collected on 07/06/2005 and were received at Accutest on 07/06/2005properly preserved, at 1.8 Deg. C and intact. These Samples received an Accutest job number of F33038.A listing of the LaboratorySample ID, Client Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For moreinformation, please refer to QC summary pages.
Metals By Method SW846 6010BMatrix: AQ Batch ID: MP8284
Samples F33010-2MS, F33010-2MSD, F33010-2SDL, F33010-2DUP were used as the QC samples for metals.All method blanks for this batch meet method specific criteria.RPD for Serial Dilution for Arsenic is outside control limits for sample MP8284-SD1. Percent difference acceptable due tolow initial sample concentration (< 50 times IDL).RPD for Duplicate for Arsenic is outside control limits for sample MP8284-D1. RPD acceptable due to low duplicate andsample concentrations.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for thesamples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data QualityObjectives for precision,accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: July 25, 2005Sue O. Bell, Project Manager (signature on file)
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Accutest LabLink@41812 12:39 24-Oct-2005
Report of Analysis Page 1 of 1
Client Sample ID: PIN18-RW02-N001 Lab Sample ID: F33038-1 Date Sampled: 07/06/05 Matrix: AQ - Ground Water Date Received: 07/06/05
Percent Solids: n/a Project: Star Center-WWNA Monthly; Largo, FL
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) RPD acceptable due to low duplicate and sample concentrations.
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Section 4: Misc. Forms ............................................................................................................ 104.1: Chain of Custody ........................................................................................................... 11
Section 5: Metals Analysis - QC Data Summaries ................................................................ 135.1: Prep QC MP8404: As .................................................................................................... 145.2: Prep QC MP8416: As .................................................................................................... 19
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F33829
Accutest LabLink@41812 12:39 24-Oct-2005
Sample Summary
S M StollerJob No: F33829
Star Center-WWNA Monthly; Largo, FLProject No: 7030-226
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
F33829-1 08/04/05 09:45 JPC 08/04/05 AQ Ground Water PIN18-RW02-N001
F33829-2 08/04/05 09:44 JPC 08/04/05 AQ Ground Water PIN18-RW03-N001
F33829-3 08/04/05 09:47 JPC 08/04/05 AQ Ground Water PIN18-RW0501-N001
F33829-4 08/04/05 09:51 JPC 08/04/05 AQ Ground Water PIN18-EFF1-N001
F33829-5 08/04/05 09:54 JPC 08/04/05 AQ Ground Water PIN18-EFF2-N001
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F33829
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: S M Stoller Job No: F33829
Site: Star Center-WWNA Monthly; Largo, FL Report Date 8/16/2005
5 Samples were collected on 08/04/2005 and were received at Accutest on 08/04/2005properly preserved, at 3 Deg. C and intact. These Samples received an Accutest job number of F33829.A listing of the LaboratorySample ID, Client Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For moreinformation, please refer to QC summary pages.
Metals By Method SW846 6010BMatrix: AQ Batch ID: MP8404
Samples F33780-1DUP, F33780-1MS, F33780-1MSD, F33780-1SDL were used as the QC samples for metals.All method blanks for this batch meet method specific criteria.
Matrix: AQ Batch ID: MP8416Samples F33767-1MS, F33767-1MSD, F33767-1SDL, F33767-1DUP were used as the QC samples for metals.All method blanks for this batch meet method specific criteria.RPD for Serial Dilution for Arsenic is outside control limits for sample MP8416-SD1. Percent difference acceptable due tolow initial sample concentration (< 50 times IDL).RPD for Duplicate for Arsenic is outside control limits for sample MP8416-D1. RPD acceptable due to low duplicate andsample concentrations.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for thesamples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data QualityObjectives for precision,accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: August 17, 2005Sue O. Bell, Project Manager (signature on file)
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Accutest LabLink@41812 12:39 24-Oct-2005
Report of Analysis Page 1 of 1
Client Sample ID: PIN18-RW02-N001 Lab Sample ID: F33829-1 Date Sampled: 08/04/05 Matrix: AQ - Ground Water Date Received: 08/04/05
Percent Solids: n/a Project: Star Center-WWNA Monthly; Largo, FL
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) RPD acceptable due to low duplicate and sample concentrations.
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Section 4: Misc. Forms ............................................................................................................ 104.1: Chain of Custody ........................................................................................................... 11
Section 5: Metals Analysis - QC Data Summaries ................................................................ 135.1: Prep QC MP8600: As .................................................................................................... 145.2: Prep QC MP8615: As .................................................................................................... 19
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F34617
Accutest LabLink@41812 12:39 24-Oct-2005
Sample Summary
S M StollerJob No: F34617
Star Center-WWNA Monthly; Largo, FLProject No: 7030-226
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
F34617-1 09/07/05 09:55 JPC 09/07/05 AQ Ground Water PIN18-RW02-N001
F34617-2 09/07/05 09:53 JPC 09/07/05 AQ Ground Water PIN18-RW03-N001
F34617-3 09/07/05 09:57 JPC 09/07/05 AQ Ground Water PIN18-RW0501-N001
F34617-4 09/07/05 10:01 JPC 09/07/05 AQ Ground Water PIN18-EFF1-N001
F34617-5 09/07/05 10:05 JPC 09/07/05 AQ Water PIN18-EFF2-N001
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F34617
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: S M Stoller Job No: F34617
Site: Star Center-WWNA Monthly; Largo, FL Report Date 9/26/2005 5:52:25 PM
5 Samples were collected on 09/07/2005 and were received at Accutest on 09/07/2005properly preserved, at 2.6 Deg. C and intact. These Samples received an Accutest job number of F34617.A listing of the LaboratorySample ID, Client Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For moreinformation, please refer to QC summary pages.
Metals By Method SW846 6010BMatrix: AQ Batch ID: MP8600
Samples F34535-4MS, F34535-4MSD, F34535-4SDL, F34535-4DUP were used as the QC samples for metals.All method blanks for this batch meet method specific criteria.RPD for Serial Dilution for Arsenic is outside control limits for sample MP8600-SD1. Percent difference acceptable due tolow initial sample concentration (< 50 times IDL).RPD for Duplicate for Arsenic is outside control limits for sample MP8600-D1. RPD acceptable due to low duplicate andsample concentrations.
Matrix: AQ Batch ID: MP8615Samples F34830-1DUP, F34830-1MS, F34830-1MSD, F34830-1SDL were used as the QC samples for metals.All method blanks for this batch meet method specific criteria.RPD for Serial Dilution for Arsenic is outside control limits for sample MP8615-SD1. Percent difference acceptable due tolow initial sample concentration (< 50 times IDL).
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for thesamples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data QualityObjectives for precision,accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.ALSE is not responsible for any assumptions of data quality if partial data packages are used.Narrative prepared by:
_______________________________________ Date: September 26,, 2005Sue O. Bell, Project Manager (signature on file)
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Accutest LabLink@41812 12:39 24-Oct-2005
Report of Analysis Page 1 of 1
Client Sample ID: PIN18-RW02-N001 Lab Sample ID: F34617-1 Date Sampled: 09/07/05 Matrix: AQ - Ground Water Date Received: 09/07/05
Percent Solids: n/a Project: Star Center-WWNA Monthly; Largo, FL
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) RPD acceptable due to low duplicate and sample concentrations.
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).