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TASK 210: SUBSURFACE SITE INVESTIGATION New HavenRail Yard Temporary M-8Acceptance Facility New Haven, Gonnecticut Volume1 ConnDOT Assignment No.202-3464 ConnDOT Project No.301-88 Prepared for: @ State of Connecticut Department of Transportation Prepared by: ilt GfiOT'|P Maguire Group Inc. One Court Street Newington, Connecticut 06131 New Britain. Connecticut 06051 April24,2007
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Page 1: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TASK 210:SUBSURFACE SITE INVESTIGATION

New Haven Rail YardTemporary M-8 Acceptance Facility

New Haven, Gonnecticut

Volume 1

ConnDOT Assignment No. 202-3464ConnDOT Project No. 301-88

Prepared for:

@State of ConnecticutDepartment of Transportation

Prepared by:

iltGfiOT'|P

Maguire Group Inc.One Court Street

Newington, Connecticut 06131 New Britain. Connecticut 06051

April24,2007

Page 2: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

t . 0

2.0

3.0

TABLE OF CONTENTS

INTRODUCTION

SITE DESCRIPTION

LOCAL ENVIRONMENT & RECEPTORS

3. I Groundwater

3.2 Surlace Water

3.3 Geology

SUBSURFACE INVESTIGATION

4.1 Geoprobe€) Soil Borings & Soil Sample Analyses

4.2 Ballast Grab Sample Collection & Analyses

4.3 Railroad Tie Grab Sample Collection & Analyses

4.4 Groundwater Grab Sample Collection & Analyses

4.5 Project Quality Assurance/Quality Control Practices

DISCUSSION OF SAMPLE RESULTS

5. I Regulatory Critcria

5,2 Results of Geoprobe@ Boring Soil Sample Analyses

5.3 Results of Ballast Grab Sample Analyses

5.4 Results of Railroad Tie Grab Sample Analyses

5.5 Results of Groundwater Grab Sample Analyses

5.6 QualityAssurance/QualityControl Samples

DISCUSSION OF AFF'ECTED RESOURCES

6.1 Soil Areas of Bnvironmental Concem

6.2 Railroad Tie Area of Environmental Concem

6.3 Groundwater Area of Environmental Concem

RECOMMENDATIONS

LlMITATIONS

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Figure I - Site Location Plan

Page 3: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 0F CONTENTS (continued)

Figures (continued)

Figure 2a Task 2 10 Project Area & Sampling Locations

Figure 2b Task 210 Project Arca & Sampling Locations

Figure 2c Task 2 l0 Project Area & Sampling Locations

Figure 2d Task 210 Project Area & Sampling Locations

Figure 2e Task 2 l0 Project Area & Sampling Locations

Figure 2f- Task 210 Project Area & Sampling Locations

Tables

Table l(a) to l(n) Results ofGeoprobe@ Boring Soil Sample Analyses

Table 2(a) & 2(b) Results ofBallast Sample Analyses

Table 3 Results of Railroad Tie Grab Sample Analyses

Table 4(a) & 4(b) Results of Groundwater Grab Sample Analyses

Appendices

Appendix A Boring Logs (Volume 1)

Appcndix B Tables from MGI's 2005 hrterim Shop (Running Repair Shop)

Task 210 Investigation (Volume t)

Appendix C Soil Sample Laboratory Reports (Volume2)

Appendix D Ballast Sample Laboratory Reports (Volume 2)

Appendix E Railroad Tie Sample Laboratory Reports (Volume 3)

Appendix F Groundwater Sample Laboratory Reports (Volume 3)

Appendix G Q.drQC Sample Laboratory Reports (Volume 3)

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Page 4: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 210 - Subsurface Site Investigation ConnDOT Project No. 301-88

1.0 INTRODUCTION

on behalf of the connecticut Department of rransportation (connDor), Maguire Group Inc.

(MGI) has conducted a Task 210 - Subsurface Site Investigation in association with the New

Haven Rail Yard remporary M-8 Acceptance Facility project in New Havcn, connecticut. The

project will involve the construction of an acceptance area for the new M-8 rail cars and will be

locatcd to the east and southeast ofthe existing EMU Shop building. Figure I clepicts rhe project

area.

This Task 210 - Subsurface Site Investigation was conducted in areas of anticipated construction

activities for the New Haven Rail Yard remporary M-8 Acceptance Facility project. The

purpose of thc Task 210 - Subsurlace Site Investigation was to verify the absence or presence

and location of subsurlace contamination, and to assess the potential pollutant impacts to be

encountered during construction. It is anticipated that Task 310 Plans and Spccifications will

subsequently be prepared to assess construction related activities (i.e. proper storage,

classification, transport and disposal of contaminated materials), in relationship to the

envtronmental conditions prevalent within the project limits, as well as to specify remedial work

to be includcd in the Contract Bid Documents.

2.0 SITE DESCRJPTTON

This Task 210 - Subsurlace Site Investigation was conducted at the New Haven Rail Yard in the

area of the proposed Temporary M-8 Acceptance Facility. The proposed Temporary M-8

Acceptance area will be constructed to the east and southeast ofthe existing EMU Shop building

on land owned by the State of Connecticut Department of Transportation. The site area is

depicted in Figures 2a through 2f-Task 210 Project Area & Sampl.ing Locations.

ConnDOT Assisnmenl No. 202-14f,4 Page t

Page 5: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
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Page 12: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 2 l0 - Subsurfac. Sire Inveslisarion ConnDOT Prqect No. 301-88

Numerous environmental investigations completed at the New Haven Rail Yard property have

indicated the widespread presence oftotal petroleum hydrocarbons, volatile organic compounds,

polycyclic aromatic hydrocarbons (PAHs), and RCRA 8 metals contamination, as well as

isolated occurrences of polychlorinated biphenyls (PCBs) in on-site soils and groundwater. Thc

contaminated soil has been encountercd at depths ranging from the surface (0) to approximately

eight (8) feet below the ground surface. The soil and groundwater contamination detected

exceeded the applicable Connecticut Department of Environmental Protection Remediation

Standard Regulations. In addition, the concentrations of leachable lead previously detected in

on-site soils at the site have exceeded the RCRA hazardous waste concentration in isolated areas.

3.0 LOCAL ENVIRONMENT & R.ECEPTORS

3.1 Groundwater

The 2005 edition of "Environmental GIS Data for Connccticut" provided by the CTDEP, depicts

the groundwater classification for the area as "GB." A "GB" groundwater classification

indicates that the groundwater has been adversely impacted by waste discharges, spills or leaks

of chemicals, or land use impacts. The groundwatcr is not suitable for direct human

consumption without the need for treatment and a public water supply source is available.

Groundwater was encountcred at the site at depths ranging from approximately 4 to 6 feet below

the ground surface. The New Haven Rail Yard and its surrounding properties are all connected

to the South Central Regional Water Company's public water distribution system and the City of

New Haven sewer system. In addition, there are no public water supply sources within a one-

mile radius of the Site, according to the CTDEP Bulletin 4, "The Atlas of the Public Water

Supply Sources and Drainage Basins of Connecticut," June, 1982.

ConnDOT Assienment No. 202-3464 Page 9

Page 13: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 210 - Subsurface Site Investisation ConnDOT Project No, 301-88

3.2 Surface Water

There are no surface water bodies sinrated on the New Haven Rail Yard property- The project

area is located within the South Central Shoreline Regional Drainage Basin, within the South

Central Coast Major Drainage Basin. The general topogaphy of the site is relatively flat. Based

upon previous investigations conducted at the site, the infened direction of groundwater flow is

south,/southeast, towards Long Island Sound. Long Island Sound is located approximately %

mile southeast of the New Haven Rail Yard.

3.3 Geoloqy

The 2005 edition of "Environmental GIS Data for Connecticut" provided by the CTDEP, depicts

the surlicial materials at the site as Artificial Fill, which is described as earth materials and

manmade materials that have been artificially placed. Soil encountered during this investigation

consisted of brown to red-brown sand units, and fill comprised of black ash and cinders. The

Bedrock Geological Map of Connecticut, compiled by John Rodgers in 1985, indicates that the

bedrock unit underlying the site area is the New Haven Arkose, which is a red-brown arkosic

sandstone. Bedrock was not encountered during this investigation.

4.0 SUBSURFACEINVESTIGATION

Due to the contaminants previously detected in the soil and groundwater on the New Havcn Rail

Yard property, a comprehensive sampling program was conducted within the proposed

construction areas to be impacted by the Temporary M-8 Acceptance Facility project. The

following subsections detail the investigation.

ConnDOT Assignment No. 202-3464 Page l0

Page 14: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Truk 210 - Subsurface Site Investisation ConnllOT Projcct No. 30t-88

4.1 Geoprobe@ Soil Borines & Soil Sample Analyses

On March 15, 19,21, ail26,2007, tifty{kee (53) Geoprobe@ soil borings (M8F-l to M8F-53)

were advanced in areas of anticipated construction activities for the Temporary M-8 Acceptancc

Facility. The Geoprobe@ borings were advanced by Logical Environmental Solutions, under the

direction ofMGI. The locations ofthe Gcoprobe@ soil borings are depicted on Figurcs 2ato2f-

Task 2 l0 Project Area & Sampling Locations.

The Geoprobe@ soil borings were advanced to a depth of 8 feet below grade. Continuous soil

samples were collected utilizing a 4-foot long, 2-inch diameter Macro Core Sampler with

dedicated acetate liners. Thc soil samples were visually inspected in the field for staining, and

described as to physical characteristics and soil type. In addition, the soil samples were screened

in the field for total volatile organic compounds utilizing a Photovac photoionization detector

(PID). Soil boring logs were generated in the field by Maguire field personnel. The boring logs

denote the types of soil encountered, the depth to groundwater and./or bedrock, the total depth

reached in each boring, and the highest observed PID reading. Copies of the boring logs are

included at the end ofthis report in Appendix A.

Based upon freld screening results and visual observations, one soil sample from each boring

was placed in glassware supplied by Spectrum Analytical Laboratory, and stored in an ice-filled

cooler. The shallow soil sample (2' to 4' below grade) was selected for laboratory analyses if

field screening and visual observation did not indicate the presence of contaminants in the other

sample intervals- The analyses for each soil sample included volatile organic compounds

(VOCs) utilizing EPA Method 8260, semi-volatile organic compounds (SVOCs) utilizing EPA

Method 8270, petroleum hydrocarbnns utilizing the Connecticut ETPH method, pesticides

utilizing EPA Method 8081A, polychlorinated biphenyls (PCBs) utilizing EPA Method 8082,

and total and SPLP RCRA 8 metals.

All Geoprobe@ soil borings were back-filled upon completion utilizing clean sand and/or

hydrated bentonite. All down-hole sampling equipment was decontaminated in accordance with

MGI's February 2007 Task 210 - Subsurface Site Investigation Work Plan.

ComDOT Assiunment No. 202-3464 Page I 1

Page 15: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 210 - Subsurlbce Site Investisation ConnDOT Project No. 301-88

4.2 Ballast Grab Samnle Collection & Analvses

SLx (6) ballast grab samples were collected from selected locations where existing tracks will be

removed. The ballast grab samples were placed in glassware supplied by spectrum Analltical

Laboratory, and stored in an ice-filled cooler. The analyses for each ballast grab sample

included VOCs (EPA Method 8260), BNAs (EPA Method 8270), petroleum hyrlrocarbons

(Connecticut ETPH), pesticides (EPA Method 8081A), PCBs (EPA Method 8082), and total and

SPLP RCRA 8 metals. The locations of the ballast sample poinrs (M8FB-l rhrough M8FB-6)

are depicted on Figures 2d and2f Task 210 Prqect Area & Sampling Locations.

4.3 Railroad Tie Grab Samole Collection & Analyses

Two (2) composite railroad tie wood grab samples were collected at selected locations where

existing tracks will be removed so that specifications regarding handling and disposal of the

material can be provided. The railroad tie wood grab samples were placed in glassrvare supplied

by Spectrum Analltical Laboratory, and stored in an ice-filled coolcr. The analyses for each

wood sample included VOCs (EPA Method 8260), SVOCs (EPA Method 8270), petroleum

hydrocarbons (Connecticut ETPH), pesticides (EPA Method 8081A), PCBs (EPA Method 8082),

and total and TCLP RCRA 8 metals. The locations of the railroad tie sample points (M8FT-l

and M8FT-2) are depicted on Figures 2d and 2f Task 210 Project Area & Sampling Locations.

4.4 Groundwater Grab Samnle Collection & Analyses

Groundwater grab samples were collected from borings M8F-14, M8F-24, M8F-42, and MSF-

50. The groundwater grab samples were collected by inserting one-half inch diameter, schedule

40, l0-slot, PVC well screen and riser casing into the borehole. The 5-foot section ofwell screen

was temporarily installed approximately 4 feet into the observed water table depth. Dedicated

polyethylene tubing was placed into the temporary well and the groundwater sample was drawn

through the hrbing using a low-flow peristaltic pump.

ConnDOT Assignment No. 202-3464 Page 12

Page 16: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 2l0 - Subsurface Site Investisatio[ CourDOT Projcct No. i0l-81t

The groundwater samples were collected for laboratory analysis of VOCs (EPA Method 8260),

SVOCs (EPA Method 8270), petroleum hydrocarbons (Connecticut ETPH), pesticides (EPA

Method 8081A), PCBs (EPA Method 8082), and roral RCRA 8 metals. The groundwarer

samples were placed in laboratory-supplied glassware, and stored in an ice-filled cooler.

4.5 Proiect Quality Assurance/Oualitv Control Practices

To assess the collection of samples in the field in terms of the sampling techniques and

decontamination procedures followed, quality control and quality assurance samples werc

collected. Four (4) trip blank samples (TB-l through TB-4) were prepared by Spectrum

Analytical Laboratory and four (4) field blank samples (FB-l tkough FB-4) were collected in

the field one on each day of sampling.

The trip blank samples were stored with the daily samples in the sample cooler until subsequent

delivery to the laboratory for analysis of VOCs. The FB-l and FB-3 field blank water samples

were collected by pouring laboratory supplied de-ionized water tluough an acctate liner and

macro-corc cutting shoe, and collecting the rinsate in appropriate sample containers. The FB-2

and FB-4 field bla* samples were collected by directly pouring the laboratory supplied de-

ionized water into the appropriate sample containers to check the quality ofthe de-ionized water,

glassware, and laboratory sample handling and analyical procedures. The field blank samples

were stored with the daily samples in the cooler until delivery to the laboratory, and were

analyzed for the same parameters as the daily samples.

All samples collected in the field were stored in a manner that preserved the integrity of the

sample chemistry. Samples intended for organic analyses were stored in an ice-filled cooler until

delivery to the laboratory. Chain-of-Custody (COC) forms were filled out and accompanied all

samples collected as a legal record of possession of the sample. The COC was initiated in the

field and accompanied the containers during sample collection, transportation to the lab,

analysis, and final disposal of the sample. All sampling equipment was either dedicated to a

specific sample or was decontaminated prior to and between each use. Sampling equipment was

not placed near solvents, gasoline, or materials that may impact the integrity of the samples.

ConnDOT Assisnment No. 202-1464 Page 13

Page 17: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 210 - Subsurface Site tnvestigation ConnDOl' Prqcct No. 301-li8

5.1

5.0 DISCUSSION OF SAMPLE RESULTS

Regulatorv Criteria

The CTDEP adopted Remediation Standard Regulations (Regulations of Connecticut StateAgencies, Section 22a-133k-l to 3 and 22a-133q-l) as of January 31, 1996. The Remediation

Standard Regulations (RSRs) apply to any site undergoing voluntary remediation under Public

Acts 95-lf:13 or 95-190, a transfer ofan "establishment" under public Act 95-183, or any sire as

ordered by the crDEP commissioner. The Regulations also outline the processes for

establishing altemative site-specific numerical standards for certain sites, upon approval by the

CTDEP.

The RSRs criteria applicable to the soil and groundwater sampled during this investigation arc

summarized below. The application of these RSRs to the results of the laboratory analyses from

this investigation is discussed in subsections 5.2, 5.3,5.4, and 5.5 of this section.

Soils Criteria: The RSRs are organized into two sets of criteria: the Dircct Exposure Criteria

(DEC) and the Pollutant Mobility Criteria (PMC). The DEC and pMC arc briefly explained in

the following sub-sections, in relation to how they would be applicable to the t]?es of analyses

conducted on the soil samples collected for this investigation. Please refer to the RSRs for a

complete explanation of the Regulations.

Direct Exposure Criteria

The purpose ofthe DEC is to protect human health from risks associated with the direct contacr

with or ingestion of various common soil contaminants. The DEC are applicable to soil within

approximately 15 feet of the ground surface. Concentrations of contaminants are evaluated

based upon mass-based analyses and different criteria are established for residential and

commercial/industrial properties. The use of the less stringent commercial/industrial standards

requires the placement of a land use restriction on the property.

ConnDOT Assignment No. 202-3464 Page 14

Page 18: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 210 - Subsurface Site Investigation ConnDOT Project No. 301-88

Thc DEC are not applicable to inaccessible soils, including soil more than 4 feet below theground surface, 2 feet below pavement greater than 3 inches thick, or below an existing building,provided that an Environmental Land Use Restriction (ELUR) is placed in e ffect for thepropeny.

Pollutant Mobilitv Criteria

The purpose of the PMC is to evaluate the potential for contaminants to leach from the soil inconcentrations that may degrade groundwater quality. Dilferenl numerical criteria areestablished for GA and G.dA groundwater areas, versus GB groundwater areas. since theproject area is situated within a GB groundwater area, the least stringent criteria apply.

Groundwater Criteria: Contaminants in the groundwater are compared either to backgroundquality or the Groundwater Protection Criteria (GPC), the Volatilization Criteria, as well as theSurface water Protection criteria (SWPC). The Gpc, Volatilization criteria, and SWpc arc

briefly explained in the following sub-sections, in relation to how they would be applicable to thetypes ofanalyses conducted on the groundwater samples collected for this investigation.

Grou0dwaler Prorection Criteria

The purpose of the GPC is to protect the groundwater quality in areas thar have the potential to

use gjroundwater as a drinking water resource {GA & GAA groundwater classification areas).

Since the project area is situated in a GB groundwater area, the GPC do not apply to this Site.

Volatilization Criteria

The putpose of the Volatilization Criteria standard is to ensure that volatile organic compounds(VOCs) in groundwater do not pose an unacceptable risk to human health due to the inhalation of

Vocs that may enter into a structure on the property. The Volatilization criteria only apply

when impacted groundwater is located within 15 feet of the ground surface or any structure.

Different criteria exist fbr residential and commerciaVindustrial properties. The use of the less

stringent commerciavindustrial standards requires the placement of an ELUR on the property.

Since groundwater was within 15 feet of the ground surface, the Volatilization Criteria apply to

this Site.

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Surface Water Protection Criteria

The purpose ofthe SWPC standards is to ensure that groundwater discharging to a surlace water

body will not adversely affect surface water quality. Since groundwater likely discharges to

Long lsland Sound, the SWPC apply to contaminants detected in the groundwater.

5.2 Results of Geoprobe@ Borins Soil Sample Analvses

soil samples collected during the advancement ofthe Geoprobe@ borings were sent to Spectrum

Analytical Laboratory for laboratory analyses. Summaries of the laboratory results from the soilsamples are presented in Tables l(a) to 1(n), which are located at thc cnd of this report, and

copies of the soil sample analytical results are included in Appendix c- The fo owing

summarizes the results of the analyses conducted on the soil samples.

Petroleum hydrocarbons were detected in the soil samples at concentrations ranging from Below

Reporting Limits (BRL) ro fl,5 l0 parrs per million (ppm). The following fifteen ( I 5) soil

samples contained rPH at concentrations that exceed the crDEp Residential DEC of 500 ppm:

MgF-'7,2' to 4' (5,070 ppm); M8F-8, 2' to 4' (3,020 ppm); M8F-9, Z' to 4' (2,450 ppm); M8F-

1 0 , 2 ' t o 4 ' ( 2 , 6 6 0 p p m ) ; M 8 F - 1 3 , 2 ' t o 4 ' ( 8 9 9 p p m ) ; M 8 F - 1 7 , 4 ' t o 6 ' ( 8 , 5 l 0 p p m ) , M 8 F - 1 9 ,

2' to 4' (3,260 ppm); M8F-23, 2' to 4' (5s4 ppm); M8F-28, 2' to 4' (932 ppm); M8F-35, 2' to 4'

(2,480 ppm); M8F-40, 2'to 4' (797 ppm), M8F-41, 4' to 6' (128 ppm); M8F-42, 2, to 4, (776

ppm); M8F-46, 2' to 4'(1,150 ppm); and M8F-47,2, to 4, (t ,310 ppm). The petroleum

hydrocarbon concentration detected in the M8F-7, 2' to 4,, M8F-8, 2, to 4,, M8F-10, 2' to 4',

M8F-17, 4' to 6', and M8F-19,2'to 4' samples also exceed the CommerciaVlndustrial DEC of

2,500 ppm. No other sample contained petroleum hydrocarbons at concentrations that exceed

any applicable CTDEP RSR criteria.

The VOCs benzene, ethylbenzene, isopropylbenzene, naphthalene, n-propylbenzene, styrene,

tetrachloroethene, toluene, 1,2,4-trichloroethene, and total xylenes were detected at varying

concentrations in the soil samples collected from borings M8F-5, M8F-14, M8F-15, M8F-17,

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M8F-19, MBF-24, M8F-29, M8F-31, M8F-38, M8F-39, M8F-40, M8F-42, M8F-45, and M8F-

47. The 2 to 4 foot sample collected from boring M8F-14 contained the VOC benzcne (1.52

ppm) at a concentration that exceeds its GB PMC of 0.2 ppm. No other soil sample contained

VOCs at concentrations that exceed any applicable CTDEP RSR criteria.

Various concentrations of SVOCs were detected in the soil samples, and total SVOC

concentrations ranged from BRL to 289.93 ppm. Twelve (12) soil samples contained

concentrations of SVOCs that excecd applicable CTDEP RSR Criteria. The 2 to 4 foot sample

from boring M8F-l contained the compounds benzo(a)anthracene (1.12 ppm), benzo(a)pyrene

(1.09 ppm), benzo(b)fluoranthene (1.12 ppm), benzo(k)fluoranthene (1.16 ppm), and chrysene

(1.38 ppm) at concentrations that exceed their respective GB PMC. In addition, the compounds

benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene were detected at concentratlons

that exceed their respcctive Residentral DEC. The compound benzo(a)plrene was detected at a

concentration that also exseeds its Commercial/Industrial DEC.

The 2 to 4 foot sample from boring M8F-7 contained the compounds benzo(a)anthracene (3.85

ppm) and chrysene (4.9 ppm) at concentrations that exceed their respective GB PMC. In

addition, the compound benzo(a)antluacene was detected at a concentration that exceeds its

Residential DEC.

The 2 to 4 foot sample from boring M8F-8 contained the compounds benzo(a)anthracene (1.74

ppm) and chrysene (2.17 ppm) at concentrations that exceed their respective GB PMC. In

addition, thc compound benzo(a)anthracene was detected at a concentration that exceeds its

Residential DEC.

The 2 to 4 foot sample from boring M8F-9 contained the compounds benzo(a)anthracene (1.7

ppm) and chrysene (.2.21 ppm) at concentrations that exceed their respective GB PMC. In

addition, the compound benzo(a)anthracene was detected at a concentration that exceeds its

Residential DEC.

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Task 2 l0 - Subsurfacc Srte lnvestiea(ion ConnDOT Proyect No. 301-88

The 2 to 4 foot samplc from boring M8F-14 contained the compounds benzo(a)anthracene (1.51

ppm), benzo(a)pyene (l .89 ppm), benzo(b)fluoranthcne ( l.tl6 ppm), benzo(k)fluoranthene (2.03

ppm), and chrysene (1.84 ppm) at concentrations that exceed their respective GB PMC. In

addition, the compounds benzo(a)anthracene, benzo{a)pyrene, and benzo(b)fluoranthene were

detected at concentrations that exceed their respective Residential DEC. The compound

benzo(a)pyrene was detected at a concentration that also exceeds its CommerciaVlndustrial DEC-

The 2 to 4 foot sample from boring M8F-17 contained the compounds benzo(b)fluoranthenc

(l.la ppm) and chrysene (1.37 ppm) at concentrations that exceed their respective GB PMC. In

addition, the compound benzo(b)fluoranthene was detected at a concentration that exceeds its

Residential DEC.

The 2 to 4 foot sample from boring M8F-23 contained the compounds benzolb)fluoranthene

(1.37 ppm), benzo(k)fluoranthene (1.18 ppm), and chrysene (1.09 ppm) at concentrations that

exceed their respective CB PMC. In addition, the compound benzo(b)fluoranthene was detected

at a concentration that exceeds its Residential DEC.

The 2 to 4 foot sample from boring M8F-25 contained the compound chrysene (1.18 ppm) at a

concentration that excecds its GB PMC.

The 2 to 4 foot sample from boring M8F-31 contained the compounds benzo(a)pytene (1.2

ppm), benzo(b)fluoranthene (1.02 ppm), benzo(k)fluoranthene ( l.l6 ppm), and chrysene (1.39

ppm) at concentrations that exceed their respective GB PMC. In addition, the compounds

benzo(a)pyrene and benzo(b)fluoranthene were detected at concentrations that exceed th€ir

respective Residential DEC. The compound benzo(a)pyrene was detected at a concentration that

also exceeds its Commercial/Industrial DEC.

The 2 to 4 foot sample from boring M8F-35 contained the compounds benzo(a)anthracene (28.0

ppm), beuo(a)pyrene (28.2 ppm), benzo(b)fluoranthene (29.2 ppm), benzo(k)fluoranthene (36.3

ppm), chrysene (33.8 ppm), indeno( 1,2,3-cd)pyrene (12.7 ppm), and pyrene (58.5 ppm) at

concentrations that exceed their respective GB PMC. In addition, the compounds

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benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, and

indeno( | ,2,3-cd)pyrene were detected at concentrations that exceed their respective Residential

DEC. The compounds benzo(a)anthracene, benzo(a)plrene, benzo(b)fluoranthene, and

indeno( 1,2,3-cd)pyrene were detected at concentrations that also exceeds their respective

Commercial/Industrial DEC.

The2to 4 foot sample from boring M8F-37 contained the compounds benzo(a)anthrac ene (2.47

ppm), benzo(a)pyrene (2. I 5 ppm), benzo(b)fluoranthene (2.61 ppm), benzo(k)fluoranthene (2.47

ppm), and chrysene (3.37 ppm) at concentrations that exceed their respective GB PMC. In

addition, the compounds benzda)antkacene, benzo(a)pyrene, and benzo(b)fluoranthene were

detected at concentrations that exceed their respective Residential DEC. The compound

benzo(a)py,renc was detected at a concentration that also exceeds its Commercial/Industrial DEC.

The 4 to 6 foot sample from boring M8F-41 contained the compounds benzo(a)anthracene (1.41

ppm), benzo(a)pgene (1 .27 ppm), benzoib)fluoranthene (1.67 ppm), benzo(k)fluoranthene (1.84

ppm), and chrysene (2.18 ppm) at concentrations that exceed their respective GB PMC. In

addition, thc compounds benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene were

detected at concentmtions that cxceed their respective Residential DEC. The compound

benzo(a)pyrene was detected at a concentration that also exceeds its CommerciaVlndustrial DEC.

The pesticides 4,4-DDD, 4,4-DDE, 4,4-DDT, a-chlordane, g-chlordane, and dieldrin were

detected at varying concentrations in the M8F-4, M8F-21, and M8F-15 soil samples. The 2 to 4

foot sample from boring MBF-35 contained the pesticide dieldrin (0.0625 ppn) at a

concentration that exceeds its the GB PMC of 0.007 ppm and Residential DEC of 0.038 ppm.

No other pesticides were detected at concentrations that exceed any applicable CTDEP RSR

criteria.

PCBs (total) were detected at varying concentrations ranging from 0'0171 ppm to 3-5 ppm in the

soil samples collected from borings M8F-2, M8F-4, M8F-5, M8F-6, M8F-12, M8F-13, MSF-16,

M8F-17, M8F-18, M8F-19, M8F-20, M8F-21, M8F-22, M8F-23, M8F-25, M8F-26, M8F-31,

M8F-32, M8F-35, M8F-40, M8F-46, and M8F-47. The 2 to 4 foot samples from borings M8F-

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12 (2.12 ppm) and M8F-13 (3.5 ppm) contained total PCBs at concentrations that exceed the

Residential DEC of I ppm. No other sarnple contained PCBs at concentrations that excced any

applicable CTDEP RSR crircr ia.

Total concentrations of the metals arsenic, barium, cadmium, ckomium, lead, mercury,

selenium, and silver were detected at varying concentrations in the soil samples tkoughout the

site. The following seventeen (17) soil samples contained total arsenic at concentrations that

exceed the CTDEP Residential and CommerciaVlndustrial DEC of l0 ppm: M8F-5,2' to 4'

(14.4 ppm); M8F-6, 2' to 4'(13.6 ppm); M8F-7, 2' to 4' (10.4 ppm); M8F-t2, 2' ro 4' (12.2

ppm); M8F-l 3, 2' ro 4' ( l 3. I ppm); M8F-15, 4' ro 6' (29.3 ppm); M8F-20, 2' ro 4' (10.3 ppm);

M 8 F - 2 5 , 2 ' t o 4 ' ( r 0 . 1 p p m ) ; M 8 F - 3 5 , 2 , t o 4 ' ( 1 7 . j p p m ) ; M 8 F - 3 6 , 4 ' t o 6 , ( l 1 . l p p m ) ; M 8 F -

J7, 2' to 4' (28.8 ppm); M8F-38, 2' to 4' (20.5 ppm); M8F-39, 2' ro 4' ( l 1.8 ppm); M8F-40, 2'

to 4' (10.4 ppm); M8F-45, 4' to 6' (.2t.6ppm); M8F-46, 2' to 4' (19.j ppm); and M8f-4'/, Z'

to 4' (10.7 ppm). The following three (3) soil samples contained total lead at concentrations rhat

exceed the CTDEP Residential DEC of 500 ppm: M8F-13, 2' ro 4' (518 ppm); M8F-15, 4, ro 6'

(841 ppm); and M8F-21, 2' to 4'(694 ppm); No orher sample contained total metals at

concentrations that exceed any applicable CTDEP RSR criteria.

Leachab.le co centrations (via SPLP) of barium, chromium, and lead were detected at r.arying

concentrations in the soil samples. However, the concentrations of leachable metals detected in

the soil samples do not exceed any applicable CTDEP RSR criteria.

f,.J Results of Ballast Grab Samole Analvses

The six ballast grab samples (M8FB- I through MSFB-6) collected during rhis Task 2 l0

investigation were sent to Spectrum Analyical Laboratory for laboratory analyses. Summaries

of the laboratory results from the ballast grab samples are presented in Tables 2(a) and 2 (b),

which are located at the end of this report, and copies of the ballast grab sample analy.tical results

are included in Appendix D. The following summarizes the results of the analyses conducted on

the ballast grab samples. For the purpose of comparison, the results of the ballast grab sample

analyses were compared to the CTDEP RSR soil criteria.

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Petroleurn hydrocarbons, VOCs, SVOCs, pesticides, and PCBs were not detected in the ballast

grab samples. Total and leachable concentrations of the metals barium, cadmium, chromium,

and lead were detected at varying concentrations in the ballast grab samples. However, the

samples did not contain total or leachable metals at concentrations that exceed any CTDEP RSR

criteria.

5.4 Results of Railroad Tie Gtab Sample Analvses

The two railroad tie grab samples (M8FT- I and MSFT-2) collected during this Task 2 l0

investigation were sent to Spectrum Analytical Laboratory lor laboratory analyses. Summaries

of the laboratory results fiom the railroad tie grab samples are presented in Table 3, which is

located at the end of this report, and copies of the railroad tie grab sample analltical results are

included in Appendix E. The following summarizes the results of the analyses conducted on the

railroad tie grab samples. For the purpose of comparison, the results of the railroad tie grab

sample analyses were compared to the CTDEP RSR soil criteria.

Petroleum hydrocarbons were detected in the M8FT-l (l1,600 ppm) and M8FT-2 (33,600 ppm)

samples at concentrations that exceed the GB PMC and Residential DEC of 500 ppm, and thc

CommerciaUlndustrial DEC of 2,500 ppm. Both of the railroad tie samples contained the VOC

naphthalene at low concentrations of 6.02 ppm and 5.69 ppm, which do not exceed any CTDEP

RSR criteria.

The railroad tie samples contained several SVOCs at varying concentrations. The M8FT- I

sample contained the SVOCS benzo(a)anthrac ene (227 ppm), benzo(a)pyene (99.3 ppm),

benzo(b)fluoranthene (160 ppm), benzo(k)fluoranthene (lti7 ppm), carbazole (152 ppm),

chrysene (358 ppm), dibenz(a,h)anthracene (10.9 ppm), dibenzofuran (26.9 ppm), fluoranthene

(876 pprn), indeno( 1,2,3-cd)pyrene (40.4 ppm), phenanthrene (463 ppm), and pyrene (640 ppm)

at concentrations that exceed their respective GB PMC. The compounds benzo(a)anthracene,

benzo(a)pytene, benzo(b)fluoranthene, benzo(k)fluoranthene, carbazole, chrysene,

dibenz(a,h)anthracene, and indeno( 1,2,3-cd)p),rene were also detected at concentrations that

exceed their respective Residential DEC. In addition, the compounds benzo(a)anthracene,

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benzo(a)pyrenc, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)antkacene, and

indeno( 1,2,3-cd)pyrene were detected at concentrations that exceed their respective

Commercial/Industrial DEC.

The M8FT-2 sample contained the SVOCs benzo(a)anthracene (137 ppm), benzo(a)pyrene (54.3

ppm), benzo(b)fluoranthene (144 ppm), benzo(k)fluoranthene (143 ppm), carbazole (199 ppm),

chrysene (449 ppm), dibenz(a,h)antfuacene (6.38 ppm), dibenzofuran (19.3 ppm), fluoranthene

(369 ppm), indeno( 1,2,3-cd)pyrene (24.4 ppm), phenanthrene (l5l ppm), and plrene (301 ppm)

at concentratlons that exoeed their respective GB PMC. The compounds benzo(a)anthracene,

benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, carbazole, chrysene,

dibenz(a,h)anthracene, and indeno( 1,2,3-cd)pyrene were also detected at concentrations that

exceed their respective Residential DEC. In addition, the compounds benzo(a)anthracene,

benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthcne, dibenz(a,h)anthracene, and

indeno(1,2,3-cd)pyrene were detected at concentrations that exceed their respcctive

Commercial/Industrial DEC.

The railroad tie samples did not contain detectable concentrations of pesticides. Total PCBs

were detected in the MSFT-I (0.332 ppm) and M8FT-2 (1.255 ppm) samples. The PCB

concentration detected in the MIIFT-2 sample exceeds the Residential DEC of I ppm.

Total and leachable (via TCLP) concentrations of the metals barium, cadmium, chromium, lead,

and mercury were detected at varying concentrations in the railroad tie grab samples. However,

the samples did not contain total or leachable metals at concentrations that exceed any CTDEP

RSR criteria.

Results of Groundwater Grab Sample Analvses

The four (4) groundwater grab samples (M8F-14 GW, M8F-24 GW, M8F-42 GW, and M8F-50

GW) collected from the site during the advancement of the Geoprobe@ borings were sent to

Spectrum Analytical Laboratory for laboratory analyses. Summaries of the laboratory results

from the groundwater grab samples are presented in Tables 4(a) and 4(b), which are located at

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Task 210 - Subsurface Site lnvestisation ComDOT Project No. 301-88

the end of this report, and copies of the groundwater anal)tical results are included in Appendix

F. The following summarizes the results of the groundwater grab sample analyses.

The groundwater samples did not contain detectable concentrations of VOCs, pesticides, and

PCBs. The M8F-24 GW sample contained petroleum hydrocarbons at a concentration of 1.0

ppm, which does not exceed any applicable CTDEP criteria. No other groundwater sample

contained detectable concenfiations of oetroleum hvdrocarbons.

SVOCs were detected in varying concentrations in the M8F-14 GW and M8F-24 GW samples.

The M8F-14 GW sample contained the compounds benzo(a)anthracene (0.425 parts per billion

[ppb]), benzo(b)fluoranthene (0.762 ppb), bcnzo(k)fluoranthene (0.65 ppb), and phenanthrene

(0.35 ppb) at concentrations that exceed their respective SWPC. No other SVOCs were detected

at concentrations that exceed any applicable CTDEP RSR criteria.

The groundwater samples contained total arsenic, barium, cadmium, chromium, lead, and

mercury at varying concentrations. The MSF-14 GW sample contained total arsenic {0.007 ppm)

and total chromium (15.7 ppm) at concentrations that exceed their respective SWPC of 0.004

ppm and 0.11 ppm. The M8F-24 GW sample contained total mercury (0.00221 ppm) at a

concentration that exceeds its SWPC of 0.0004 ppm. The M8F-42 GW sample contained total

lead (0.0132 ppm) at a concentration that exceeds its SWPC of 0.013 ppm. The M8F-50 GW

sample contained total arsenic (0.0062 ppm) at a concentration that exceeds its SWPC of 0.004

ppm. No other metals were detected at concentrations that exceed any applicable CTDEP RSR

criteria.

5.6 Ouali tyAssurance/Quali tvControlSamples

The field blank samples (FB-l through FB-4) did not contain detectable concentrations of

contaminants. In addition, the trip blank samples (TB-l through TB-4) did not contain VOCs at

concentrations that exceed any laboratory detection limits. Copies of the anall'tical reports

associated with the quality assurance/quality control samples are included in Appendix G.

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Task 210 - Subsurface Site Investieation ConnDOT Project No. 301-88

6.0 DISCUSSION OF AFFf,CTED RESOURCES

6.1 Soil Areas of Environmental Concern

Based upon the results of laboratory analyses perfomed on the soil samples for this Task 210

investigation, as well as the analJtical results of soil samples collected from within the projcct

area during MGI's February 2005 Task 210 for the Interim Shop (Running Repair Shop), four

(4) soil areas of environmental concem (AOECs) have been identified where contaminants are

present at concentrations that exceed applicable CTDEP RSR criteria. In addition, the remainder

of the project site has been designated as a low-level area of environmental concern (LLAOEC)

for soil. In these areas contaminants were detected at concentrations below applicable CTDEP

RSR standards, but above laboratory detection limits. The locations of the AOECs within the

project area are discussed in the following sections. Tables summarizing the analy'tical results

from soil samples collected during MGI's February 2005 Task 2 l0 for the Interim Shop

(Running Repair Shop) are included in Appendix B of this report. In addition, the locations of

the 2005 borings (denoted as IS-#) are depicted on Figures 2a and 2b Task 210 Project Area &

Sampling Locations.

AOEC #l: Area Encomnassing Borings M8F-l & 15-6:

Analfical results from the soil samples collected from borings M8F-1 and 15-6 indicate the

presence ofSVOC contamination at slightly elevated concentrations in shallow soil ranging from

2 to 4 feet below grade. The contamination detected exceeds the GB PMC, Residential DEC,

and CommerciaVlndustrial DEC.

AOEC #2: Area Encompassing Borings M8F-5. M8F-6. M8F-12. M8F-13, M8F-14,

M8F-15. IS-8 . IS-10 . IS-11 . IS-12 . IS-13 . IS- ls . & IS-18 :

Analytical results from the soil samples collected from borings M8F-5, M8F-6, M8F-12, M8F-

i3, M8F-14, M8F-15, IS-8, IS-10, IS-11, IS-12, IS-13, IS-15, and IS-18 indicate the presence of

total arsenic, total lead, petroleum hydrocarbon, VOC (beruene), SVOC, and PCB contamination

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Task 210 - Subsurlace Sirc Investieation ConnDOT Project No. l0l-88

at elevated concentrations in shallow soil ranging from 2 to 8 feet below grade. The

contamination detected exceeds the GB PMC, Residential DEC, and Commercial/lndustriai

DEC.

AOEC #3: Area Encomoassine Borings M8F-7. M8F-8, M8F-9. M8F-10. & M8F-11:

Analytical results from the soil samples collected from borings M8F-7, M8F-8, M8F-9, and

M8F-10 indicate the presence ofpetroleum hydrocarbon, SVOC, and total arsenic contamination

at elevated concentrations in shallow soil ranging from 2 to 4 feet below grade. The

contamination detected exceeds the GB PMC and Residential DEC. This AOEC also

encompasses boring M8F- I l, although contaminants at this location were detected at

concentrations slightly below CTDEP RSR criteria.

AOEC #4: Area Encompassing Borines M8F-17. M8F-19. M8F-20. M8F-21. M8F-21,

M8F-25. M8F-26. M8F-28, M8F-31. M8F_32. M8F-35. M8F_36. M8F_37.

M8F-38. M8F-39. M8F-40. M8F-41. M8F_42. M8F_45. M8F-46 & M8F_47:

Analyical results from the soil samples collected from borings M8F-1?, M8F-19, M8F-20,

M8F-21, MnF-23, M8F-2s, M8F-28, M8F-31, M8F_35, M8F_36, M8F_37, M8F_38, M8F-39,

MBF-40, M8F-41, M8F-42, M8F-45, M8F-46, and M8F-47 indicate the presence of toral arsenic,

total lead, petroleum hydrocarbon, svoc, and pesticide (dieldrin) contamination at elevated

concentrations in shallow soil ranging from 2 to 6 feet below grade. The contamination detected

exceeds the GB PMC, Residential DEC, and CommerciaVlndustrial DEC. This AOEC also

cncompasses borings M8F-26 and M8F-32, although contaminants at these locations were

detected at concentrations slightly below CTDEP RSR criteria.

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6.2 Railroad Tie Area of Environmental Concern

Analytical results from the railroad tie grab samples indicate the presence of petroleum

hydrocarbons, SVOCs, and PCBs at elevated concentrations that exceed the GB PMC.

Residential DEC, and Commercial/lndustrial DEC. The concentrations however, do not exceed

the RCRA hazardous waste toxicity concentrations. All areas where railroad ties will be

removed from the project site have been designated as a Railroad Tie Area of Environmental

Concern (RTAOEC).

6.3 Groundwater Area of Environmental Concern

Analytical results from the groundwater samples collected from borings M8F-14, M8l.-24, M8F-

42, and M8F-50 indicate the presence of SVOCs, total arsenic, total chromium, total mercury,

and total lead at concentrations that exceed the SWPC. In addition, the M8F-24 groundwater

sample containcd petroleum hydrocarbons at a concentration that does not exceed any applicable

CTDEP criteria, but may impact allowable discharge permit limits. Therefore, the entire project

area has been designated as a Groundwater Area of Environmental Concem (GWAOEC).

ConnDOT Assisnment No. 202-1464 Page 26

Page 30: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 210 - Subsurface Site Investigation ConnDOT Pro.lect No. -10 t -88

7.0 RECOMMENDATIONS

The results of the Task 210 - Subsurface site Investigation for the New Haven Rail yard

Temporary M-ll Acceptance Facility project in New Haven, Connecticut indicate the presence of

petroleum hydrocarbon, VOC, SVOC, PCB, pesticide, total arsenic, and total lead contamination

in shallow soil samples collected from the project area, at concentrations that exceed the

applicable RSR criteria. Soil samples collected from within the project area in 2005 by MGI

during the lnterim Shop (Running Repair Shop) Task 210 indicated similar results. The

contamination was detected in soils ranging in depth from 2 to 8 feet below grade. Railroad tie

samples collected from areas where the railroad tracks will be removed indicate the presence of

petroleum hydrocarbons, SVOCs, and PCBs at concentrations that sxceed the CTDEP RSR

criteria, but not the RCRA hazardous waste toxicity concentrations. Groundwater collected frorn

the site is also contaminated with SVOCs and total metals at concentrations that exceed

applicable RSR criteria. In addition, concentrations of petroleum hydrocarbons were detected in

the groundwater collected from within the project area, which may impact discharge permit

requirements. Four (4) Areas of Environmental Concern (AOECs) for soil, a site-wide Railroad

Tie Area of Environmental Concem (RTAOEC), and a site-wide Groundwater Area of

Environmental Concem (GWAOEC) have been identified within the project area. In addition,

the remainder of the project site has been designated a Low Level Area of Environmental

Concem (LLAOEC) for soil. Special considerations for treatmenVdisposal, dewatering

activities, and worker health and safety must be given to these areas in order to ensure

compliance with all local, State and Federal laws. Task 310 Plans and Specifications are

therefore recommended for the areas of construction within the Areas of Environmental Concem

and Low-Level Areas of Environmental Concem addressins the soil. railroad ties and

groundwater described in Section 6.0.

ComDOT Assisnmenr No. 202-3464 Page 27

Page 31: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 2 t0 - Subsurface Site Investisation ComDOT Prqiect No. 301-88

8.0 LIMITATIONS

All work product and reporls provided by Maguire Group Inc. (MGI) in connection with the

performance of this Task 210 - Subsurface Site Investigation are subject to the following

limitations:

I . The observations described in this reporl were made under the conditions stated therein. The

conclusions presented in the report were based solely upon the services described therein,

and not on scientific tasks or procedures beyond the scope of dcscribed services provided to

ConnDOT.

2. In preparing this report, MGI has relied on certain information provided by State and local

offrcials and inlormation and representations made by other partics referenced therein, and

on information contained in the files of State and/or local agencies made available to MGI at

the time of this investigation. To the extent that such files are missing, incomplete or not

provided to MGI, MGI is not responsible. Although there may have been some degree of

ovcrlap in the information provided by these various sources, MGI did not attempt to

independently verity the accuracy or completeness of all information reviewed or received

during the course of this investigation.

3. The conclusions and recommendations contained in this report are based in part upon the

data from subsurface explorations. The nafure and extent of variations between these

explorations may not become evident until further explorations are completed. If variations

or other latent conditions become evident, it will be necessary to re-evaluate the conclusions

and recommendations of this reoort.

4. The water level readings made lor this investigation were made at the times and conditions

stated on the boring logs. However, it must be noted that fluctuations in the level of the

groundwater may occur due to variations in rainfall, passage of time and other factors.

Should additional data become available in the future, these data should be reviewed by

MGI, and the conclusions and recommendations presented herein modihed accordingly.

ComDOT Assignment No. 202-3464 Page 28

Page 32: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task 2 l0 - Subsurface Sile lnvesrisation ConnDOT Project No. 30 i -llll

5. Where quantitative laboratory analyses have been conducted by an outside certified

laboratory, MGI has relied upon the data provided, and has not conducted an independent

evaluation ofthe reliability ofthese tests.

6. If thc conclusions and recommendations contained in this report are based, in part, upon

various types of chemical data then the conclusions and recommendations are contingent

upon the validity ofsuch data. These data have been reviewed and interpretations made in

the reporl. It should be noted that variations in the types and concentrations of contaminants

and variations in thcir flow paths may occur due to seasonal water table fluctuations, past

disposal practices, the passage of time, and other factors. Should additional chemical data

become available in the future, these data should be reviewed by MGi and the conclusions

and recommendations presented herein modified accordingly.

7. Chemical analyses were performed for specific parameters during the course of this

investigation, as described in the text. However, it should be noted that testing for all known

chemical constituents was not performed. The conclusions and recommendations contained

in this reporl are based only upon the chemical constituents tbr which testing was

accomplished.

The following qualifications apply to the undersigned's opinton:

The activities described and opinions included herein are based on information gathered during

this subsurface site investigation, which was limited in scope in adherence to the terms of our

agreement. The professional opinion provided herein is based on the information described in

this report.

ConnDOT Assigrrment No. 202-J464 Page 29

Page 33: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Task ? l0 - Subsurface Sitc Investisation ConnD0T Project No. 301-88

The inlormation contained herein was prepared for the use of ConnDOT solely in conjunction

with the task descriptions for this assignment. The conclusions and recommendations set forth in

this report are based on site conditions at the time of the investigation. Future studies and

findings could change the contents of this repoft. The professional opinions presented in this

report have been developed by using that degree of care and skill ordinarily exercised, under

similar circumstances, by reputable environmental engineering consultants practicing in this or

similar localities. No other warranty, expressed or implied, is made as to the professional

opinions included in this report.

Prepared by: Approved by: Reviewed by:

Jane Witherell, P.E., L.E.P.Principal EngineerLogical Env. Solutions

David R. Stock, P.E.Program Manager

ConnD0T Assisnment No. 202-3464 Page 30

Page 34: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLES

Page 35: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(a) - Results ofceoprob€@ Boring Soil Sample AnalysesNew Haven Rail Yard M-8 Acceptance Facility

New Haven. Connecticut

Boring I.D-:

Sample Depth:

M8F. I M8F.2

2',-4'

M8F-3

z'4'

M8F-4

z',-4',

CTDEP PMC GBGroundwater

Area

CTDEP DEC ResidentiaUCommercial & Industrial

CT ETPH - (ppm) t 5 9 83.5 BRL 67 .4 2,500 ppm 500/2,500 ppm

VOCS - Method 8260 (ppm) BRL BRL BRL BRL

SVOCs - Method 8270 (ppm)

tsenzo(a)antkacene

Benzo(a)pyrene

Benzo(b)fluoranthene

B€nzo(k)fluoranthene

Chrysene

Fluoranthenc

Pyr€ne

Total SVOCs

1.12

r.09

1.12

l. t6

I.3E

2 . 1 5

2 . 1 3

t 0 . l 5

BRl-

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

I ppm

I ppm

I ppm

I Ppm

I ppm

56 ppm

40 ppm

l/7-ti ppm

Ul ppm

l/7.8 ppm

8.4/7ll ppm

84/780 ppm

1 ,00012,500 ppm

1,000/2,500 ppm

Pesticides - Method 8081 (ppm)

4,4-DDD

4,4.DDE

4,4.DDT

BRL

BRL

BRL

BRI

BRL

BRL

BRL

BRL

BRL

0.0082

0.00871

0.0142

None Established

None Established

None Established

2.6i24 ppm

1.8/17 ppm

1.8/ t7 ppm

PCBS Method 8082 (ppm) BRL 0.0588 BRL 0.0219 Not Applicable l /10 ppm

Total RCtu{ 8 Metals ppm

Arsenic

Barium

Cadmium

Chromium

Lead

Mercury

3.16

37.3

0.3 94

82.6

t t7

0.34

3.9'7

44.5

0.49

44.3

269

0.222

8.1

18.2

BRL

1 .93

3 5 . 8

BRL

9.9

52.4

l . t 9

26,2

t't 6

0 . 1 5 8

Not Applicable

10/10 ppm

4,700/140,000 ppm

34/l,000 ppm

100/100 ppm

500/1,000 ppm

20/610 ppm

SPLP RCR,{ 8 Metals - ppm

Barium

Cbromium

Lead

0.0198

0 . 0 1 3

0.0319

0 . 0 2 1 I

0.0148

0.0424

0.01 I

BRL

BRL

0.012

0.0t22

0.0217

10.0 ppm

0.5 ppm

0.15 ppm

Not Applicablc

BRL - Below Reporting Limits (see labofatory reports for compound specihc detection limits)

The compounds listed above ar€ those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.

Page 36: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

' I ABLE 1(b) - Results of ceoprobe@ Boring Soil Sample AnalysesNew Haven Rail Yard NI-8 Acceptance Facilit-v

New Haven, Connecticut

BRL - tsclow Reporting Limits (see laboratory reports for compound specihc detection lirnits)

The compounds listed abovc are those that were detected - please see laboratory reports for full lists ofcompounds and their specihc detection limits.

Boring I.D.:

Sample Depth:

M8F-5 M8F-6 M8F-7 M8F-8 CTDEP PMC GBGroundwater

Area

CTDEP DEC ResidentiaVCommercial & Industrial

CT ETPH - (ppm) 2 5 1 205 t,070 3,020 2.500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm)

Tetrachloroethene 0.00?5 BRL BRL BRL 1.0 ppm l2l I 10 ppm

SVOCs - Method 8270 (ppm.)

Benzo(a)anthracen€

Chlysene

Fluoranthene

P].rene

Totat SVOCS

BRL

BRL

BRI-

BRL

BRL

BRL

BRL

BRL

BRL

BRL

3.85

4.9

9 . 3 7

r 0.228.32

1.74

2.17

4 . 1 1

) .o)

t3.6'7

I ppm

I ppm

56 ppm

40 ppm

1/7.8 ppm

84/780 ppm

1,00012,500 ppm

1,00012,500 ppm

Pesticides - Method 8081 (ppm) BRL BRL BRL BRL

PCBs Method 8082 (ppm) 0.0399 0,0713 BRL BRL Not Applicable 1i 10 ppm

Total RCRA 8 Metals - ppm

Arsemc

Barium

Cadmium

Chromium

Lead

Mercury

14.4

53.6

1 . 6 8

25.0

268

0. t9

13.6

5 S . l

t .91

297

0.208

10.4

91.6

0 . 8 1 8

22.5

5'1.4

l . 7 t

4.86

47 .0

0.4t1

l0. t

28.3

0 . 9 1 2

Not Applicable

10/10 ppm

4,700/ t40,000 ppm

34/ 1,000 ppm

100/100 ppm

500/1,000 ppm

20/610 ppm

SPLP RCRA 8 Mctals - ppm

Barium

Chromium

Lead

0 . 0 1 7

0.0105

0.0507

0.0155

0.007

0.0454

0.0106

BRL

BRL

0.012

BRL

BRL

10.0 ppm

0.5 ppm

0.15 ppm

Not Applicable

Page 37: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(c) - Results of Geoprobe@ Boring Soil Sample AnalyscsNew Haven Rail Yard M-8 Acceptance F'acilify

New Havcn, Connecticut

Boring I,D.:

Sample Depth:

M8F-g M8F- 10 M8F- l I

2'4',

M8F-12

2'-4',

CTDEP PMC CBGroundwater

Area

CTDEP DEC Residcntial/Commercial & Industrial

CT ETPH - (ppm) 2,450 2,660 BRL 263 2,500 ppm 500/2,500 ppm

VOCS - Method 8260 (pFm) BRL BRL BRL BRL

SVOCs - Method 8270 (ppm)

Benzo(a)anthracene

Chrysene

Fluoranthene

P1rene

Total SVOCs

1 . 7

2.27

3.6r3.94

I 1 . 5 2

BRL

BRI-

2.68

2.94

5.62

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

I ppm

I ppm

56 ppm

40 ppm

l/7.8 ppm

84i780 ppm

1,0002,500 ppm

1,000/2,500 ppm

Pesticides - Method 8081 (ppm) BRL BRL BRL BRL

PCBS - Method 8082 (ppm)

PCB-1254

PCB-1260

Total PCBs

BRL

BRL

BRL

BRL

BRL

BRL

BRI-

BRL

BRL

1.15

0.91

2.12

Not Applicable

Not Applicable

Not Applicabte

l/10 pptn

l/ l0 ppm

Ulo ppm

Total RCRA 8 Merals - ppm

A-rsenlc

Barium

Cadmium

Cbromium

Lead

M€rcury

Silver

3.38

33.9

0.4t I

8.49

26.2

0.631

BRL

6.54

5 2 . 1

0.52

7 .28

87.5

0.3'7 5

l0. t

7.89

7 6.0

0 . 5 t 5

9.03

t52

0.342

BRL

12.2'72.3

1 . 3 5

t 6 . 0

3 3 9

0.908

BRL

Not Applicable

10/10 ppm

4,700i 140.000 ppm

34/1,000 ppm

100/100 ppm

500/1,000 ppm

20/610 ppm

340/10,000 ppm

SPLP RCRA 8 Metals - ppm

Barium

Chromium

Lead

0.0106

BRL

BRL

0.006

BRL

BRL

0.0335

BRL

BRL

0.0263

BRL

BRL

10.0 ppm

0.5 ppm

0.15 ppm

Not Applicable

BRL - Below Reporting Limits (see laboratory r€ports for compound specific detection limits)

Thc compounds listed above are those that were detected - please see laboratory repofts for fulI lists ofcomoounds and their soecific detection limits.

Page 38: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(d) - Results of Geoprobe@ Boring Soil Samplc AnalysesNew Haven Rail Yard M-8 Acceptance Facility

New Hay€n, Connecticut

Boring I.D-:

Sample Depth:

M8F- l3 M{rF- t4 M8F- t5

4'-6'

M8F- r6 CTDEP PMC GBGroundwater

Atea

CTDEP DEC Rcsidcntial/Comrnercial & lndustrial

CT ETPH - (ppm) 899 180 BRL 345 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm)

Benzcnc

Ethylbenzene

lsopropylbenzene

Naphthalene

n-Propylbenzene

Toluene

1,2,4-Trimethyltrenzene

Xylenes (total)

BRLBRLBRLBRLBRIBRLBRLBRL

1.520,3090.07530.4470.1433.O20.209t . 4 1 3

BRLBRLBRLBRLBRL0.008BRLBRL

BRLBRLBRLBRLBRLBRLBRLBRI

0.2 ppm10.1 ppm132 ppm

56 ppml4 ppm

67 ppm70 ppm19.5 ppm

2l1200 ppm

500/ I,000 ppm500i 1,000 ppm1,000/2,500 ppnr500/ 1,000 ppm500/ 1,000 ppm500/1,000 ppm500/ I,000 ppm

SVOCs - Method 8270 (ppm)Benzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChlyseneFluorantheneIndeno( 1,2,3-cd)pyrenePlreneTotal SVOCs

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

L 5 11.891.86

0.9s82.031.842.82

0.9682.45

t6.326

BRLBRLBRLBRI,BRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

1 pPm1 ppmI ppm42 ppm

I ppmI ppm56 ppmI ppm

40 ppm

l/7.8 ppm

Ul ppm1/7.8 pprn

1,000/2,500 ppmli.4/78 ppm84i780 ppm

1.000i2,500 ppnrI i7.tt ppm

1,000/2,500 ppm

Pesticides - Metlod 808 t (ppm) BRL BRL BRL BRLPCBs - Method 8082 (ppm)

PCB-1254PCB-1260Total PCBs

2.261.243.5

BRLBRLBRL

BRLBRLBRL

BRL0.02740.0274

Not ApplicabteNot ApplicableNot Applicable

li l0 pprnl i l0 ppml i l0 ppm

Total RCR{ 8 Metals - ppmArsenlcBariumCadmiumChromiumLeadMercury

13.166_4t . l 820.55 1 8

0.242

9.0r96.60.628.3?q?

0.2'l

29.3156

0.56134.',7841

0.0698

5.5928.8

0 . 6 1 530.449.'l

0.0707

Not Applicablc

10/10 ppm4,700/140,000 ppn

34/1,000 ppm100/ 100 ppm

500/1,000 ppm

?0/610 ppm

SPLP RCRA 8 Metals - ppmBariumChromiumLead

0.0216BRL

BRL

0.0142BRL0.031

0.04180.012BRL

0.05710.0 t930 . 0 1 6 1

10,0 ppm0.5 ppm0,l5 ppm

Not Applicable

BRL - Below Reporting Limits (see laboratory reports for compound specific d€t€ction limits)

The compounds listed above are those that were d€tected - please see laboratory reports for full lists ofcompounds and thet specihc detection limits.

Page 39: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(e) - Results of Geoprobe@ Boring Soil Sample AnalysesNew Haven Rail Yard M-8 Acceptaoce Facilit!

New Haven, Connecticut

Boring LD.:

Sample Depth:

M8F-17

4'-6'

M8F-18

2',-4',

M8F-19

?'4 '

M8F-20 CTDEP PMC GBGroundwater

Area

CTDEP DEC ResidentiaUCommercial & [ndustial

CT ETPH - (ppm) 8 , 5 1 0 287 3,260 136 2,500 ppm 500/2,500 ppm

VOCs - Method 8260 (ppm)

Naphthalene 0.268 BRL 0.0067 BRL 56 ppm 1,000/2,500 ppm

SVOCs - Method 8270 (ppm)

Anthracene

Benzo(a)anthracene

Benzo(a)p)'rene

Benzo(b)fluoranthene

Bcnzo(g,h,i)perylene

Benz-o(k)fluoranthene

Chrysene

Fluoranthene

Phenanthrene

Plrene

Total SVOCs

BRL

0.988

BRL

1.14

BRL

0.93

1.3 7

2.99

BR]-

l .o2

10.438

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

0.4'75

0.652

0.77 4

0 ; 1 7 8

I ' .J)J

0.674

0 . 8 1 2

t .68

0.848

t . '1

8.746

400 ppm

I ppm

I ppm

I pPm

42 ppm

I ppm

I ppm

56 ppm

40 ppm

40 ppm

1,0001?,500 ppm

lr.8 ppm

1/1 ppm

1/7.8 ppm

1,000/2,500 ppm

8.4/78 ppm

84/780 ppm

1,000/2,500 ppm

I,000/2,500 ppm

1,000i2,500 ppm

Pesticides - N{ethod 8081 (ppm) BRL BRL BRL BRL

PCBs - Method 8082 (ppm) 0.0216 0.0484 0.247 0.0286 Not Applicable l /10 ppm

Total RCRA 8 Metals ppm

Arsenic

Barium

Cadmium

Chromium

Lead

Mercury

6.41

46,1

0.569

38.4

79.8

0 . r 3 5

4.53

30.li

0.6'74

34.3

44.8

0.0605

5.6tt

42.7

0.735

56.9

124

0 . 1 9 5

t0.l

l 0 l

1 .9

12.3

283

0.641

Not Applicable

10/10 ppm

4,700i 140,000 ppm

34l1,000 ppm

100/100 ppm

500/1,000 ppm

20/6 l0 ppm

SPLP RCRA 8 Metals - ppm

Barium

Chromium

Lead

0.044

BRL

0.0298

0.085

0.0312

0.019

0.03

BRL

0.0161

0.0277

BRL

0.0182

10.0 ppm

0.5 ppm

0.15 ppm

Not Appticable

BRL - Below Reporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits-

Page 40: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(f) - Results of Geoprobe@ Boring Soil Sampl€ AnalysesNew Haven Rail Yard M-8 Acceptance Facility

New llaven, Connecticut

Boring [,D.:

Sample Depth:

M8F-21

2 ' 4 '

M8F-22

2'4',

M8F-23 M8F-24

2 ' 4 '

CTDEP PMC GBGroundwater

Area

CTDEP DEC Residential/Commercial & Indusrial

CT ETPH - (ppm) BRL t64 554 262 2,500 ppm 500i2,500 ppm

VOCs - Method 8260 (ppm)

Naphthalene BRL BRL BRL 0 . 1 9 8 56 ppm 1,000/2,500 ppm

SVOCs - Method 8270 (ppm)

Benzo(a)anthrac€ne

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Fluoranthenc

P1,re ne

Total SVOCs

BRL

BRL

Bzu-BRL

BRI-

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

0.888

1.37

t . I8

1.09

2.09

2 . 2 1

8.828

BRL

BRL

BRL

0.426

0.'77 L

0.705

t.902

I PPm

I PP.''

I PPm

I PP*

56 ppm

40 ppm

l/7 .8 ppm

li 7.ti ppm

8.4/78 ppm

It41780 ppm

1,000/2,500 ppm

1,000/2,500 pprn

Pesticides - Method 808 | (ppm)

a-Chlordane

g-Chlordane

0.0363

0.039

BRL

BRL

BRL

BRL

BRL

BRL

None Established

None Established

None Established

None Established

PCBs Method 8082 (ppm) 0. t04 0.0354 0.109 BRL Not Appticabte l /10 ppm

Total RCRA 8 Metals - ppm

Arsenlc

Barium

Cadmium

Chromiunr

Lead

Mercury

Selenium

9.91

60.8

0.61 I

7 . 3 1

694

0,0556

2.8

4.95

28.8

0.695

40.9

48.9

0.0614

BRL

6.41

39.2

0.599

29.4

99.7

0. t93

BRL

4 _ 1 1

34.9

0.70 t

44.9

22.0

0 . t t 5

BRL

Not Applicable

l0/10 ppm

4,700/140,000 ppm

34/l,000 ppm

100/100 ppm

500/ 1,000 ppm

20/610 ppm

340/10,000 ppm

SPLP RCRA 8 Metals - ppm

Barium

Chromium

Lead

0,0144

BRL

0.0088

0.0682

0.0214

BRL

0.0427

BRL

0.0336

0.03

BRL

BRL

10.0 ppm

0.5 ppm

0.15 ppm

Not Applicable

BRL - Below Reporting Limits (see laboratory reports for compound specifrc detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcomoounds and their sDecific detection limits.

Page 41: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABI E 1(g) - Results of Geoprob€@ Boring Soil Sampl€ AnalysesNew Haven Rail Yard M-8 Acceptance Facilit-v

New Haven, Connecticut

Boring I.D.:

Sample Depth:

M8F-25

z'-4'

M8F-26 MgF-27 M8F-28 CTDEP PMC CBGroundwater

Area

CTDEP DEC ResidentialCommercial & Industrial

CT ETPH - (ppm) 206 404 BRL 932 2,500 ppm 500/2,500 ppm

VOCs - Method 8260 (ppm) BRL BRL BRL BRL

SVOCs - Method 8?70 (ppm)

Anthracene

Benzo(a)anthrac€ne

Benzo(a)pyrene

Benzo(tr)fluoranthene

tsenzo(g,h,i)perylcne

Benzo(k)fluoranthene

Chrysene

Irluoranthenc

lndeno( 1,2,3 -cd)plrene

Phenantfuene

Pyrene

Total SVOCs

0.59?

0.946

0.982

0.98

0.483

0.88

1.18

2.3 5

0.433

0.942

2.36

1 2 . 1 3 3

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

0.876

0,876

BRL

BRL

tsRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

400 ppm

I ppm

I ppm

I ppm

42 ppm

I ppm

I ppm

56 ppm

I pp-

40 ppm

40 ppm

1,000i2,500 ppml / ? R n n m

l i I ppm

l/?.8 ppm

1,000/2,500 ppm

8.4/78 ppm

84/780 ppm

1,000/2,500 ppm

1,000/2,500 ppm

1,000/2,500 ppm

Pesticides - Mcthod 8olt I (ppm) BRL BRL BRL BRL

PCBs Method 8082 (ppm)

PCB-1254

PCB-1260

Total PCBs

0,0259B R L

0.0259

0.43 I

0.0592

0.4902

BRL

BRL

BRL

BRL

BRL

BRL

Not Applicable

Not Applicable

Not Applicable

I /10 ppm

li t0 ppm

l/10 ppm

Total RCRA li Metals -ppm

AISenlc

Barium

Cadmium

Chromium

Lead

Mercury

10.7

t44

3.4'l

1 2 . 4

287

0.7 4'7

8,56

58.7

BRL

7 . t I

123

0 . 1 4 1

BRL

| 1 . 5

BRL

3.97

l { .18

BRL

1.6

r 9.3

0.33 3

7.39

25.3

0.0388

Not Applicable

l0/10 ppm

4,700/140,000 ppm

34/l,000 ppm

100/100 ppm

500i 1,000 ppm

20/610 ppm

SPLP RCRA I Metals - ppm

Barium

Lead

0.0362

0.023

0.0148

0.0226

BRL

BRL

BRL

BRL

10.0 ppm

0.15 ppm

Not Applicable

BRL - Below Reporting Limits {see labomtory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and thcir spccific detection limils.

Page 42: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(h) - Results of ceoprobc@ Boring Soil Sample AnalysesNew Haven Rail Yard M-8 Acceptance Facility

New Haven, Connecticut

Boring I.D.:

Sample Depth:

M8F-29 M8F-30

2' -4 '

M8F-3 I

2',4'

M8F-32

2',4'

CTDEP PMC GBGroundwater

Aiea

CTDEP DEC ResidentiaUCommercial & lndustrial

CT ETPH - (ppm) 294 475 184 450 2,500 ppm 500/2,500 ppmVOCS - Mcthod 8260 (ppm)

Naphthal€ne

Stlrene

BRI-

0 . t 8 3

BRL

BRL

0.192

BRL

BRL

BRL

56 ppm

20 ppm

1,000/2,500 ppm500/1,000 ppm

SVOCs - Method 8270 (pprn)

Anthacene

Benzo(a)anthracene

B e nzo( a)pyene

Benzo(b)fluoranthene

Benzo(g,h,i)perylene

tscnzo(k)tluoranthene

Chrysenc

Fluoranthenc

Phenanthrene

Pyrene

Total SVOCS

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRI

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

0.q2q

0. rJ l4

1.2

1.02

0.53

1.16

1.39

3.09

1. t t9

2.97

14.993

BRL

BRL

BRL

BRL

t . 3 t

BRL

BRL

1.52

BRL

2.5',1

5.4

400 ppm

I ppm

I PpmI ppm

42 ppm

1 ppm

t Ppm56 ppm

40 ppm

40 ppm

1,000/2,500 ppml/7.8 ppml/ l ppm

U7.8 ppm

1,000/2,500 ppm

8.4/78 ppm

84/780 ppm

1,000/2,500 ppm

1,00012,500 ppm

1,000/2,500 ppm

Pesticides - Method 8081 (ppm) BRL BRL BRL BRL

PCBS - Method 8082 (ppm)

PCB-1254

PCB- 1260'fotal PCBs

BRL

BRL

BRL

BRL

BRL

BRL

BRL

0.017 |

0.017 t

0.039

0_0185

0.0575

Not Applicable

Not Applicable

Not Applicable

l i l0 ppm

ti l0 ppm

l/10 ppm

Total RCRA 8 Metals ppm

Arsenlc

Barium

Cadmium

Chromium

Lead

Mercury

Silver

BRL

t 5.2

BRL'7 .06

r 6 . l

BRL

BRL

BRL

t 2 . 2

0.284

5 . 1 I

1 4 . 5

BRL

BRL

9 ; 1 7

1 3 8

1 . 8 8

l2_0

266

0.753

BRI-

8.03

0.931

7.01

t7'7

0.098 5

| . 1 8

Not Applicable

l0 i l0 ppm

4,700/140,000 ppm

34/1,000 ppm

100/100 ppm

500/l,000 ppm

20/610 ppm

340/10,000 ppm

SPLP RCRA 8 Metals - ppm

Barium

Lead

BRL

BRL

BRL

BRL

0.0242

0.0254

0.0 t 26

0.0179

10.0 ppm

0.15 ppm

Not Applicable

BRL - tse lou' Reporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and thek soecific detection limits.

Page 43: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

' I 'ABl,E l{i) - Results of Geoprobe@ Boring Soil Sample AnalysesNew Hayen Rail Yard M-8 Acceptance Facility

New Ilaven, Connecticut

Boring I.D.:

Sample Depth:

M8F-33 M8F-34

4',-6',

M8F-35 M8F-36

4',-6',

CTDEP PMC GBGroundwater

Area

CTDEP DEC Residential/Commercial & [ndustdal

CT ETPH - (ppm) BRL BRT, 2,480 BRL 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm) BRL BRL BRL BRLSVOCs - Method ti270 (ppm)

Accnaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene

B enzo(b) fluoranthene

Benzo(g,h,i)perylene

Benzo(k)fluoranthene

Chrysene

Fluorantle ne

Indeno( 1,2,3-cd)pyrene

Phenanthrene

Pyrene

Total SVOCs

BRL

tsRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

7.'76

3 . t 2

28.0

28.2

29.2

9.95

36.3

33.839.5

12.7

2.9

58.5

289.93

BRL

BRL

BRL

BRL

BRL

BRL

BRI-

BRL

BRL

BRL

BRL

BRL

BRL

84 ppm

400 ppm

I ppm

I ppm

I ppm

42 ppm

I ppm

I pP-

56 ppm

I ppm

40 ppm

40 ppm

1,000/2,500 ppm

1,000/2,500 ppm

l/7.8 ppm

1/1 ppm

1/7.E ppm

1,000/2,500 ppm

8.4/78 ppm

84/780 ppm

1,000/2,500 ppm

U7.8 ppm

1,000/2,500 ppm

1,000i2,500 ppm

Pesticides - Method 8081 (ppm)

Dieldrin BRL BRL 0.0625 BRL 0.007 ppm 0.03E/0.36 ppm

PCBs Method 8082 (ppm) 8zu, BRL 0.194 BRL Not Applicable l/10 ppm

Total RCL{ 8 Metals - ppm

Arsenlc

Barium

Cadmium

Chromium

Lead

Mercury

Selenium

BRL

I l . - )

BRL

3.1t6

8 . l 6

BRL

BRL

BRI

10.4

BRL

4.41

3.65

BRI

BRI

1 7 . 7

72.4

0.957

7 .53

230

0 . 1 9 8

2.03

I 1.1

64.5

0.607

3.85

21.2

BRL

Not Applicable

10/10 ppm

4,700/140,000 ppm

34/l,000 ppm

100/100 ppm

500/1,000 ppm

20/610 ppm

340/l0,000 ppm

SPLP RCRA 8 Metals - ppm

Barium

LeadBRL

BRI

BRL

BRL

0.0126

0.03

0.0059

BRL

10.0 ppm0.15 ppm

Not Applicable

BRL Below Reporting Limits (see laboratory reports for compound specific d€tection limits)

The compounds listed above ar€ those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.

Page 44: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(i) - Resulls of Geoprobe@ Boring Soit Sample AnalysesN-ew Haven Rai[ Yard l\I-8 Acccptancc Facility

New Hay€n, Conoecaicut

Boring I.D.:

Sampte Depth:

M8F-37

2',4',

M8F-38

2'-4'

M8F-39 M8F-40 CTDEP PMC GBGroundwater

Area

CTDEP DEC ResidentiaYCommercial & [ndustrial

CT ETPH - (ppm) BRL BRL BRL 797 2,500 ppm 500/2,500 ppm

VOCs - Method 8260 (ppm)

Naphthalene

Toluene

Xylenes (total)

BRL

BRL

BRI,

BRL

0.106

BRL

0 . 1 7

BRL

BRL

0 . 1 8 1

0. t 5lt

0.2143

56 ppm

67 ppm

19.5 ppm

I,000/2,500 ppm

500/1,000 ppm

500/1,000 ppm

SVOCs - Method 8270 (ppm)

Bcnzo(a)anthracen€

Benzo(a)p5,rene

Benzo(b)fluoranthene

tscnzo(k)fluoranthene

Chrysene

Fluoranthene

Pyrene

Total SVOCs

2.15

2.61

3.37

3.94

4.26

21 .27

BRL

BRL

BRL

BRL

BRL

BRL

BRI

BRL

BRL

BRL

BRL

BRL

tsRL

BRL

BRL

BRL

BRL

BRL

BRI

BRL

BRL

2.03

2.09

4 . 1 2

I ppm

I ppm

I ppm

I pp-

I ppm

56 ppnr

40 ppm

l/7.8 ppm

Ul ppm

1/7.8 ppnr

8.4/78 pprn

84/780 ppm

1,000/2,500 ppm

I,000/2,500 ppm

Pcsticirles - Method 80xl (ppm) BRL BRL BRL BRL

PCBs Method 8082 (ppm) BRL BRL BRL 0.02_]4 Not Applicable l /10 ppm

Total RCRA 8 Metals - ppln

Afsenlc

Barium

Cadmium

Chromium

Lead

Me rcury

Selenium

Silver

28.8

64.5

0.937

1 4 . t

102

1 . 0 3

BRL

20.5

58.6

0.'795

7 .41

299

0.872

J , J J

BRL

I1.8

l 0 l

0.367

4.34

233

0.209

3 . 3 5

6.73

10.4

5 2 . 1

1 . 0

25.0

201

0 . r 3 6

BRL

L , 2 4

Not Applicable10/10 ppm

4,700i 140,000 ppm

34/1,000 ppn

100/100 ppm

500/1,000 ppm

20./610 ppm

340/10,000 ppm

340/10,000 ppm

SPLP RCRA 8 Metals - ppm

Barium

Lead

0.0126

0.0542

0.0121

0.0492

0.0098

BRL

0.0128

0.0263

10.0 ppm

0.15 ppm

Not Applicable

BRL - Below Reporting Limits (se€ laboratory reports for compound specific detection limits)

The compounds listed above are those that \acre detected - please see laboratory reports for full lists ofcompounds and their specihc detection limits.

Page 45: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 1(k) - Results of Geoprobe@ Boring Soil Sample AnalysesNel Haven Rail Yard NI-8 Acceptalce Facility

New Haveo, Conn€cticut

Boring I.D.:

Sample Depth:

M8F-4 |

4'-6',

M8F-42 M8F43

z',-4'

M8F44

1' , -4 '

CTDEP PMC GBGroundwat€r

Area

CTDEP DEC ResidentiaVCommercial & Industrial

CT ETPH - (pprn) 728 776 BRL 3 8 8 2,500 ppm 500/2.500 ppmvocs - Method 8260 (ppm)

EthylbenzeneNaphthalene

Toluene

1,2,4-Trimethylbeznene

Xylenes (total)

BRL

BRL

BRL

BRL

BRL

0.1230. r550 . 1 5 4

0.0696

0.342',7

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

tsRL

10. I ppm

56 ppm

67 ppm

70 ppm

19.5 ppm

500/l,000 ppm

t,000/2,500 ppm

500/1,000 ppm

500/1,000 ppm

500i | ,000 ppm

SVOCs - Method 8270 (ppm)

Bcnzo(a)anthracene

Benzo(a)pyrene

Benzo(tr)fluoranthene

Benzo(k)fluoranthene

C@sene

Fluoranthene

Pyrene

Total SVOCs

1.41

1.27

1.67

1.84

2.18

3 . t 4

3 . 1 I

14.62

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

tsRL

tsRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

1 pp-

I pp-

1 ppm

1 ppm

I ppm

56 ppm

40 ppm

l/7.8 ppm

1/l ppm

1i7.8 ppm

8,4/78 ppm

84/780 ppm

I,000/2,500 ppm

1,000/2,500 ppm

Pesticidcs - Method 80li | (ppm) BRL BRL BRL BRL

PCBs Method llOlt2 (ppm) BRL BRL BRL BRL Not Applicable l/ l0 ppm

Total RCRA 8 Metals ppm

Arsenlc

Barium

Cadmium

Chromium

Lead

Mercury

Selenium

9.64

40.4

0.516

9.8 rt52

0.307BRL

'7 .95t09

0.584It .73651.021.68

3.98

53.4

t t . lo2

4 . l l

5 l . l

0.0532.22

1.O

76.2

0.46r9.6

I t 9

0.586

BRL

Not Applicable

l0/10 ppm

4,700i 140,000 ppm

34i 1,000 ppm

t00i 100 ppm

500/1,000 ppm

20/6 10 ppm

340/ 10,000 ppm

SPLP RCRA 8 Metals - ppmBariumLead

0.009

0.0252

0.0962BRL

0.0064

BRL

0.0914

BRL

10.0 ppm

0.15 ppm

Not Appticable

BRL Below Reporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory repotts for full lists ofcomtounds and their soecific detection limits.

Page 46: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 1(l) - Results of Geoprobe@ Boring Soil Sampl€ AralysesNew Hayen Rail Yard M-8 Acceptanc€ Facility

New Haveo, Connecticut

Boring I.D.:

Sample Depth:

M8F-45

4' -6 '

M8F46

z'4'

M8F-47

2',-4'

M8F48

2'-4'

CTDEP PMC GBGroundwater

Area

CTDEP DEC Residential/Commercial & Industrial

CT ETPH - lppm) 203 I,I50 1,310 BRL 2,500 ppm 500/2,500 ppm

vocs - M€thod 8260 (ppm)

Benzene

Naphthalene

Toluene

Xylenes (totat)

0 . 1 8 8

0 . t 7 7

0.339

0.3237

BRL

BRL

BRI,

BRL

0.0725

0 . r33

0.202

0.24ss

BRL

BRL

BRL

BRL

0.2 ppm

56 ppm

67 ppm

19.5 ppm

2l1200 ppm

1,000/2,500 ppm

500/l,000 ppm

500/1,000 ppm

SVOCs - Method 8270 (ppm)

Fluoranthene

Plrene

Total SVOCs

BRL

BRL

BRL

t . 1 2

t .99

3 . 1 I

2.'77

3.26

6.03

BRL

BRL

BRL

56 ppm

40 ppm

1,000,'2,500 ppm

I,000/2,500 ppm

Pesticides - Method 8081 (ppm) BRL BRL BRL BRL

PCBs - Method 8082 (ppm) BRL 0.02t2 0.028 BRL Not Applicable l /10 ppm

Total RCRA li Metals ppm

Arsenrc

Barium

Cadmium

Chromium

Lead

Mercury

21.6

59.6

BRL

65.3

0.094rJ

19.7

69.0

0.457

7 .82

1 3 6

0.363

10.7

54.7

0.5 89

8.64

t 8 3

0 . 1 8 2

l .6 l

39.3

0.87 |

10.4

228

BRL

Not Applicable

l0/10 ppm

4,700/l40,000 ppm

34/1,000 ppm

100/100 ppm

500i 1,000 ppnr

20/610 ppm

SPLP RCRA 8 Metals - ppm

Barium

Lead

0.0216

BRL

0 . 0 1 3

0.0146

0 . 0 t 2

0.0261

0 . 0 1 5

0.021

10.0 ppm

0.15 ppm

Not Applicable

BRL - Below Reporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory r€ports tbr full lists ofcompounds and their specific detection limits.

Page 47: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(m) - Results of Geoprobe@ Boring Soil Sampte AnalysesNew Hayen Rail Yard M-8 Acc€ptance Facility

New Haven, Connecticut

Boring I.D.:

Sample Depth:

M8F-49 M8F-50

2'-4',

M8F-51

2',4',

M8F-52

2',4',

CTDEP PMC GBCroundwater

Area

CTDEP DEC ResidentiaVCommercial & Industrial

CT ETPH - (ppm) BRL BRL BRL BRL 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm) BRL BRL BRL BRL

SVOCS - Method 8270 (ppm)

Fluoranthe ne

Pyrene

Total SVOCS

o.447

0.486

0.933

BRl-

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

56 ppm

40 ppm

1,000i2,500 ppm

1,00012,500 ppm

Pesticides - Method 8081 (ppm) BRL BRL BRL BRL

PCBs - Method 8082 (ppm) BRL BRL BRL BRL Not Applicable l/ l0 ppm

Total RCRA 8 Metals - ppm

Arsenic

Barium

Cadmium

Clromium

Lead

Mercury

Selenium

Silver

l . &

2t.6

BRL

4.29

23.6

0.0683

BRL

BRL

1.98

23.5

BRL

5 . t 2

9.99

0.0344

BRI,

BRL

I .96

25.6

BRL

6.56

6_6

BRL

BRL

BRL

3.94

95.3

0.499

t0.2

320

2.87

1.82

t .62

Not Applicable

10i l0 ppm

4,700/140,000 ppm

34/l,000 ppm

100/ 100 ppm

500/1,000 ppm

20/610 ppm

340/10,000 ppm

340/10,000 ppm

SPLP RCRA 8 Metals - ppm

Bsrium

Lead

0.0186

0.0497

0.0r46

BRL

0_0064

BRL

0.01 t8

0.0138

10.0 ppm

0.15 ppm

Not Applicable

BRII- Below Reportng Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompound.s and their specific detection lirnits.

Page 48: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE l(n) - Results of G€oprob€@ Boring Soil Sampl€ AnalysesNew Haven Rail Yard M-8 Acceptance Facility

New Haveo, Connecticut

Boring I.D.:

Sample Depth:

M8F-53 CTDEP PMC GBGrourdwater

Area

CTDEP DEC Residential/Commercial & Industrial

CT ETPH - (ppm) BRL 2.500 ppm 500/2.500 ppm

VOCs - Method tt260 (ppm) BRL

SVOCS - Method 8270 (ppm) BRL

Pesticides - Merhod 801{ I (ppm) BRL

PCBS Method 8082 (ppm) BRL Not Applicable l/10 ppm

Total RCRA 8 Metals - ppm

Aisemc

Barium

Cadmium

Chromium

Lead

Mercury

Selenium

4.42

98.3

0 . 5 2 1

5.68

333

2 . 2 1

t . 8 t

Not Applicable

l0/ l0 ppm

4,700/140,000 ppm

34/ I ,000 ppm

100/100 ppm

500/ 1,000 ppm

20/610 ppm

340/10,000 ppm

SPLP RCRA 8 M€tals - ppm

Barium

Lead

0.0208

0 . 0 1 I I

10.0 ppm

0.15 ppm

Not Applicable

BRL - Below Rcporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that w€re detected - please see laboratory reports for full lists ofcompounds and their specific dctection limits.

Page 49: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 2(a) - Results of Ballast Samplc AnalysesNew Haven Rail Yard M-8 Acceptance Facility

New Hayen, Connecticut

Sample l.D.: MSFB-1 M8FB.2 M8FB-3 MI]F8.4CTDEP PMC GB

GroundwaterArea

CTDEP DEC ResidentiaVCommercial & Industrial

CT ETPH - (ppm) BRL BRL BRL BRL 2,500 ppm 500/2,500 ppm

vocs - Method 8260 (ppm) BRL BRL BRL BRL

SVOCs - Method 8270 (pprn) BRL BRL BRL BRL

Pesticides - Method 808 | (ppm) BRL BRL BRL BRL

PCBS Method 8082 (ppm) BRL BRL BRL BRL Not Applicable t/10 ppm

Total RCRA 8 Metals - ppm

Barium

Cadmium

Chromium

Lead

10.8

0.626

1.97

5.08

13.2

0.506

3.22

3.78

t3.4

0.731

2 . 1 2

4.'l

l 1 .4

0.775

) t )

5.95

Not Applicable

4,700/140,000 ppm

34/1,000 ppm

100i 100 ppm

500/ I,000 ppm

SPLP RCRA 8 Metals - ppm

Barium 0.0066 0.0082 0.009 4.0072 10.0 ppm

Not Applicable

BRL - Below Reporting Limits (s€e laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits-

Page 50: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 2(b) - Results of Ballast Sampte AnalysesNew Haven Rail Yard M-8 Acceptance Facility

New Haven, Connecticut

BRL - Below Rcporting Limits (see laboratory reports for compound specihc detestion limits)

The compounds listed above are thos€ that were d€tected - please se€ laboratory reporls for full lists ofcompounds and their specific detection limits.

Sample [.D.: M8FB.5 M8FB-6CTDEP PMC GB

GroundwaterArea

CTDEP DEC ResidentiaUCommercial & Industrial

CT ETPH - (ppm) BRI BRL 2,500 ppm 500/2,500 ppm

VOCs - Method 8260 (ppm) BRL BRL

SVOCs - Method 8270 (ppm) BRL BRL

Pesticides - Method 8081 (pprn) BRL BRL

PCBs - Method 8082 (ppm) BRL BRL Not Applicable l/10 ppmTotal RCRA 8 Metals ppm

Barium

Cadmium

Chromium

Lead

12.7

0.565

1 . I

3.89

t3.2

0.707

2.82

I 1 . 4

Not Applicable

4,700/140,000 ppm

34l1,000 ppn

100/ 100 pptn

500/l,000 ppm

SPLP RCRA 8 Metals - ppm

Barium 0.0073 0.005 10.0 ppm

Not Applicabte

Page 51: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 3 - Results of Railroad Tie Samplc AnalysesNew Haven Rall Yard M-8 Acceptance Facility

New Haven, Connecticut

BRL - Below Reporting Limits (see laboratory reports for compound specific detection timits)

The compounds listed above are those that were detected - please see laboratory repofts for full lists ofcompounds and their specific detection limits-

Sample I.D.: M8FT.1 M8FT.2CTDEP PMC GB

GroundwaterArea

CTDEP DEC ResidentiaUCommercial & Industrial

CT ETPH - (ppm) 11,600 3 3,600 2J00 ppn 500/2,500 ppmVOCS - Method 8260 (ppm)

Naphthalene 6.02 5.69 56 ppm 1,000/2,500 ppmSVOCs - Method 8270 (ppm)

AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneCarbazolcCluyseneDibenzo(a,h)anthraceneDitrenzofuranFluorantheneFluoreneIndeno( 1,2,3 -cd)pyrcnc

l -Methylnaphthalene

2-MethylnaphthalenePhenanthrenePlreneTotal SVOCs

29.0t6.9

282.0227.099.3r60.034.2187.0152.0358.010.926.9876.042.140.43.78BRL463.0640.0

3,649.08

| 5.310.4

250.0137.054.3

144.02 t . lI4J.O199.0449.06.JE19.3

369.026.624.45.0

4.461 5 L 0301.0

2,330.24

84 ppm84 ppm

400 ppmI ppmI ppmI ppm42 ppr\I ppmI ppmI ppmI ppm

5.6 ppm56 ppm56 ppmI ppm

None Established9.u ppm40 ppm40 ppm

1,000/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm

1/7.8 ppm1/1 ppm

li7.E ppmI,000/2,500 ppm

8.4/78 ppm311290 ppm84/780 ppm

lil ppm270/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm

U7.8 ppmNon€ Established474/2,500 ppm1,000/2,500 ppnI,000/2,500 ppm

Pesticides - Method 8081 (ppm) BRL BRLPCBs - Method 801i2 (ppm)

PCB-1254PCB-1260Total PCBS

0 . 1 6 80.1640.332

0.4020.8531 .255

Not ApplicableNot ApplicableNot Applicable

1/10 ppml/10 ppml/10 ppm

Total RCRA 8 Metals - ppmBariumCadmiumChromiumLcadMercury

13.90.7 t42.962 1 . 8

0.0425

5.0uBRLt.768.4

BRL

Not Applicable4,700/140,000 ppn

34l I,fi)o ppm100/100 ppm

500/1,000 ppm20/610 ppm

TCLP RCRA 8 Metals - ppmBariumCadmiumLead

0,07610.0050.0244

0.1050.0040.0135

10.0 ppm0.05 ppm0. 15 ppm

Not Applicable

Page 52: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 4(a) - Results of Groundwater Grab Sample AnalysesNew Haven Rail Yard M-8 Acceptance Facil ity

N€w Ifuyen, Connecticut

Sample I.D.: M8F-14GW

M8F-24GW

CTDEP SurfaceWater Protection

Criteria

CTDEP Volatilization Criteria

ResidentiaVCommercial & Industrial

CT ETPH (ppm) BRL 1 .0 None Established Not Applicable

VOCs - EPA Method 8260 (ppb) BRL BRL

SVOCs - EPA Method 8270 (ppb)

Benzo(a)anthracene

Benzo(b)fluoranthenc

Berzo(g,h,i)peryle ne

Benzo(k)fluoranthene

Chrysene

Fluoranthene

Indeno(1,2.3-cd)plrene

P he nanthrene

Pyrene

0.42 5

0.762

0.73 8

0.65

0.5

0 . 9 1 2

0.6

0.35

0_85

BRL

BRL

BRL

BRL

BRL

0.27 |

BRL

BRl-

0.4

0.3 ppb

0.3 ppb

None Established

03 ppb

None Established

3,700 ppb

None Established

0.3 ppb

I10,000 ppb

None Established

None Established

None Established

None Established

None Established

None Established

None Established

None Established

None Established

Pesticides - EPA Method 8081A (ppb) BRL BRL

PCBs - EPA Method 8080 (ppb) BRL BRL

Total RCRA I Metals ppm

ATSENIC

Barium

Cadmium

Cfuomium

Mercury

0.007

0.0096

0.0048

15.7

0.00026

BRL

0.276

BRL

0.0079

0.00221

0.004 ppm

None Established

0.006 ppm

0.11 ppm

0.0004 ppm

Not Applicable

BRL Below Reporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.

Page 53: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TABLE 4(b) - Results of Groundwater Grah Sample AnalysesNew Haven Rail Yard M-t Acceptance Facility

New Haven, Connecticut

Sampte I.D.: M8F-42GW

M8F-50

GWCTDEP SurfaceWater Protection

Criteria

CTDEP Volatilizntion CriteriaResidenrialCommercial & Industrial

CT ETPH (ppm) BRL BRL Nooe Established Not Applicable

VOCs - EPA Method 8260 (ppb) BRL BRl-

SVOCs - EPA Method 8270 (ppb) BRL BRL

Pesticides - EPA Method 8081A (ppb) BRL BRL

PCBs - EPA Method 8080 (ppb) BRL BRL

Total RCRA 8 Metals - ppm

Arsenic

Barium

Lead

tsRL

0.058

0.0132

0.0062

o.0122

0 . 0 1 2

0.004 ppm

None Established

0.013 ppm

Not Applicable

BRL llelow Reporting Limits (see laboratory repofts for compound speciiic detection limits)

The compounds listed above are those that werc det€cted - plcasc see laboratoqr reports fbr full lists ofcompounds and their specific dctcction limits.

Page 54: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

APPEI\DIX ABoring Logs

Page 55: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

EIgiggI Temporary M-8 Acceptance Facitity

Location: New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: MgF-l

Inspector: C. Criscuolo

Date:3-19-07

l 0t l l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Por'F, e A ATv/Backhoe-Moun6d Geoprcbes

E 6e a )o =

E

o

Description €.ao oo =

c ) o -o - 5

Sample Interval

Ground Surface 0.0

1 .0 -

2.0-

3.0-

4.0-

5.0-

6.0-

7.0-

Gray medium to coarse GRAVEL (BALLAST)

0.2 Macro Core 0'-2'

Dark-Brown fine to coarse SAND, trace Ash, Cinders, Concrete,Brick, & Wood (FILL)

Groundwater at 6'6.0

1 . 2

0.2

Macro Core 2'-4'

i . ! . . i l l t i -+ i: :q: ; : :q: l : : :q: i

::"::;.:r. i j;".:ii ! : . i ! j i - ! .

: :q: i : : { : i : . : :q: i

::r;:;_ :q.;i:j:".i

: :q:a :t:ij :i :q:l

:{:a:{:a:i:q:i

::q:ii:q:i:;:q:i

r,"-;r :qi; j :q:i

Macro Core 4L6'

8.0

0 .1 Macro Core 6'-8'

9.0-

10.0-

I t . u -

12 .0 -

End of Eoring at 8'

Soil Oescriotion: and = 35-50% some = 20.35% litlle = 10-20o/o trace = 1-10V"

Driller: W Lineberry

8k' Geoprone 540U

Depth to Water: 6'

Borinq Depth: 8'

Borinq Dia.: 2"

eAgg, 1 of 1

Page 56: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG l 0- r\ t I

Logical Environmental Solutions354 South River Road

Tolland, CT 06084f ru c k, Port a b I e & A TV/ B ac kh oe-M o u n tecl Ge oprobes

Proiect: Temporary M.8 Acceptance Facility

lgggE$, New Haven Rail Yard

g.Igq! Maguire croup lnc.

Borinq: l,l8F-2

lnsp€ctor: C. Criscuolo

g9!g 3-19-07

E 6{ r @

o

o

Descriptionc L oo o 6 a

F C L

Sample Interval

Ground Surface 0.0lv q\i,D-o1 Gray medium to coarse GRAVEL (BALLAST) 0.5

0 Macro Core 0'-2'{:i;:.qi

l:td j-!1

t:i i:{:

s,-.:.d.:

q:i!:/:

4 i : : :

{:i"':q:r

cris.: :.::". i

(:if :q:i

?ri.r :i:q. :i

{ : i : ; :q. i

?:i{ :,::ol:i

ft:;:q:i

,i.i'.tti

qi i -q: i

i i r : ; .c: i?'..d rt.!:{:i i.{:i

?i i :c: i

Dark-Brown fine to coarse SAND, trace Ash, Cinders, Concrete,Brick, & Wood (FILL)

Groundwater at 6'6 .0

0.8 Macro Core 2 -4'

0.3 Macro Core 4'-6'

8.0

0 .1 Macro Core 6'-8'

9.0-

10 ,0 -

| | .u -

1 2 . O -

End of Boring at 8'

Soil Description: and = 35-500/6 some = 20-35% little = 10-20% trace = 1.10%

Driller: W. Lineberry

!!9. Geoprone 540U

Deoth to Water: 6'

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: I of I

Page 57: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

rei$li Temporary M.8 Acceptance Facility

Location: New Haven Rail Yard

e.Igg! Maguire Group Inc.

Borinq: M8F-3

Inspector: C. Criscuolo

Date:3-19-07

ifLogical Environmental Solut ions

354 South River RoadTolland, CT 06084

Truck, Pottable & AfylBackhoe-Mountecl Geoprobes

; : io o

o

ct)

Description 5.a3,s

Fo a; i c r

Sample lnterval

Ground Surface 0.0

1 .0 -

3.0-

4.0-

c.u-

6.0-

7.0-

.v q rhv

p"CI.# Gray medium to coarse GRAVEL (BALLAST) 0.5

0.4 Macro Core 0 -2'Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete & Brick (FILL)

t . 3

t . . ll t

Red-Brown fine Sand, little Silt2.5

2.4 Macro Core 2'-4'ii;::t*1::i,i'ii .e ii.o.:i

'.d.::;.qi;::ni

t :d : l :a : iq : r'.?:; .z i .::z i

:qi :{ i : ;qi

-! :a:! .1: i . ! :

:q: i :{ : i : j :q: i

r:q:aY:i:;:q:i

;:o.:i ti, :;:'.:i

r:q:i;qri::;:q:i

Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

Groundwater at 6'6.0

2.O Macro Core 4'-6'

8.0

0.5 Macro Core 6 -8'

9.0-

10.0-

1 1 . 0 -

12 .0 -

End of Boring at 8'

Soil Descriotion: and = 3S50% somo = 20-35% little = 10-20% trace = l-10%

Driller: W. Lineberry

gg; Geoprone 540U

Depth to Water: 6'

Borinq Oepth: I'

gg!i!s-B.is- 2"

Paoe: 1 of I

Page 58: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG t - ^

i o| I '

Loqieal Environmental Solutions354 South River Road

Tolland. CT 06084Truck Porleue & ATv/gackhoe-llounted ceoo.obes

Plgigg!' Temporary M-8 Acceptance Facility

Location: New Hav€n Rail Yard

Client: Maguire Group Inc.

Borinq: M8F4

Inspector: C. Criscuolo

Date: 3-l S7

E 6o c to g

o

oDescription Fg6 a

d g

Sample Interval

Ground Surface 0 .0

' t .0-

2.O-

3 ,0 -

4.0-

5.0-

6.0-

.::q-i:qa::q:

iii:iEl: o - . o . . : <

j ; f l . . .9 . . , j l_+ :_or'.c_a :.10 . . o . ' . . : (lo "o :co.-:r.o-. .q..: j .{.o : .o. ,co :' : o . . o . . : {:O. ' o- :Co -

t3.=&tjt - E - . r ' ,

.': 'q^.+l

.F:-1;--#i. o lri :l. i

$,w"$l io ld 'i: i

F,u'$ir,lu a.t.f :-1l,"'.Ft, o.f" :?, t

.f "+"..f', o 9; .?, t'9;,;*i s;

ASH & CINDERS, little fine to coarse Gravel (FILL) 0.5

0.3 Macro Core 0'-2'

Dark-Brown fine to medium SAND, little Silt, Ash & Cinders,trace fine to coarse Gravel (FILL)

3.03.4 Macro Core 2'-4'

Red-Brown fine to coarse SAND, little Silt

Groundwater at 5.5'c . J

1 . 1 Macro Core 4'-6'

8.0

0.2 Macro Core 6 -8'

I 0-

1 0

1 1 . 0 -

12.0-

End of Boring at I'

Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-l0olo

Driller: W. Lineberry

Elgj Geoprone 54Ou

Depth to Watgr: 5.5'

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: I of 1

Page 59: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGProiect: Temporary M.8 Acceptance Facility Borino: MgF-s

!9991!iS, New Haven Rail Yard Inspector: C. Criscuoto

Client: Maguire Group Inc. Date: 3.15.07

l o\J I

Loqical Environmental Solut ions354 South River Road

Tolland. CT 06084fruck, Poftahle & Afv/Beckhoe-Mountd Ceoryobes

: i :o oo g

Eo

Description -aEo o o o -

Sample Interval

Ground Surface 0.0

1 .0-

2.O-

3.0-

4.O-

5.0-

6.0-

7 .O-

F:i,I:i,;:iiih-!:d:f:t:i-l:t6ii:'';;.:. -o . . o - : . ' - c: o i o : C o l

i : oj' l;; :. . o . . + . . . . n:O r ' 0 : dq l;i P-. .q...;;.1o : o , _ {o :. _ .o . . 4 . . ' _o: O r ' O : C O _r : 9 . q . r : a

t - 8 . . ) . .

oY.9;.ol-F.ii".Ft - F . . r - .

oY.9-.o!*f :i.;-.rf. o lft :?i iE : . - : : . . s :.r V.rl ,<1ft: i ; ts -.- S-.f.'.r".ff ,o io.?1i :

$,";$f, o lo :?1t:'e; ;i s-

ASH & CINDERS, little fine to coarse Gravet (F|LL)

o.2 Macro Core 0'-2'

Dark-Brown fine to medium SAND, lit e Silt, Ash & Cinders.trace fine to coarse Gravel & Concrete (FILL)

3.04.4 Macro Core 2'-4'

Red-Brown fine to coarse SAND, little Silt

Groundwater at 5.5'5 .5

0.9 Macro Core 4'-6'

8.0

0.3 Macro Core 6'-8'

9.0-

10.0-

11 ,0 -

't2.o-

End of Boring at 8'

Soil Descriotion: and = 35-50o/o some = 20-35% tittte = 10-20o/o trace = 1-10%

Driller: W. Lineberry

B!S, Geoprone 540U

Deoth to Water: 5.5'

Borino Depth: 8'

Borinq Dia.: 2"

Paoe: I of 1

Page 60: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG l 0( t l

Loqical Environmental Solut ions354 South River Road

Tolland, CT 06084fruck, Podable & ATv/Backhoe.lloune l Geop.obes

elgiggli Temporary M-8 Acceptance Facitity

Location: New Haven Rail Yard

Client: Magui16 Group Inc.

Borinq: M8F-G

lnsoector: C. Criscuolo

Date: 3-15-07

=aao oo =

E

oDescription -o.6

o { ) o Eo - 5

Sample Interval

Ground Surface 0.0

1 .0 -

2.0-

3.0-

4.0-

5.0-

6.0-

7.0-

:?:ij:'.:iii!:i

:".:; :D. ir :.: :o.:i

Gray medium to coarse GRAVEL, little Elack Ash & Cinders u.5

0.3 Macro Core 0'-2'

Red-Brown to Olive-Brown fine to coarse SAND. trace fine tocoarse Gravel & Ash (FILL)

3.01 . 6 Macro Core 2'-4'': e.9ft :{. i

. 9 : . - j s :

"f:1j".F' :91* '?: t. $ : . - ; i i l :

" rU.F'.,i'Y;);,:$ 9; .?, rS

- . : - S:

.F:-1r".F':5 9; .?; r

F,"sil, it 9; .1, t

.f -1).f1:6 9; .f, t

Red-Brown fine to coarse SAND, some Ash & Cinders {FILL)

Groundwater at 5'5.0

0.6 Macro Core 4'-6'

8 .0

0 Macro Core 6'-8'

9.0-

10 .0 -

11 .0 -

12.O-

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = 1-10%

Driller: W Lineberry

B!$. ceoprone 540U

9ed[!4@s'

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: 1 of 1

Page 61: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

ElgiCgl! Temporary M-8 Acceptance Facility

!99a!!9![ New Haven Rait yard

Client: Maguire Group lnc.

Borinq: M8F"7

Inspector: C. Criscuolo

9a!9, 3-26-07

I

i o\, I

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Portable & ATv/aackho*MounEd Geoprol,t.s

c L oO C '

o

U'

Oescription E.Eo oo 5

6 ao - =

Sample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

4.O-

5.0-

6.0-

7.0-

rv rl \r|,,'r\.a).ff;-RX;r:y--qb*v_o : .o:t .co :- : o . . o 1 . . <o - o : c o l: l d . : q . ; j Jo : o : . 4 0 :. : o . . o - 1 . : <o r 'o' :co .-: ' .o' . .q . j : Ja : 4 j . c 0 - j' : o - . - o . : : (

r . p-. .q' . . i , Jo : g ; . ( a :: o . . o . . : <

r, p-. .q.. .1i1.0 : 9 r ' . ca :- : o . . q - . - : (

Gray medium to coarse GMVEL (BALLAST)1 . 0

0 Macro Core 0'-2'

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick, trace Concrele & fine to coarse Gravel (FILL)

5 .0

0.8 Macro Core 2'4'

o.2 Macro Core 4'-6':i,;'::1,t':i;1:".:;-;:'.:ij.i:ol

Y.!:{.t:i.s:q:a:4:i:.::q

:"::;e.:i:::'l

:q:l:4:!;::q

:F.:;::'.:iri:el

Black ASH & CINDERS, little fine to coarse Sand & Gravel(FrLL)

Groundwater at 6'6.0

8.0

0 Macro Core 6'-8'

9.0-

10.0-

1 1 .0 -

12.0-

End of Boring at 8'

Soil Descriotion: and = 35-50% some = 20-35% liftle = l0-20o/o trace = 1-10%

Driller: W. Lineberry

B!$, Geoprone 540U

Depth to Water: 6'

Borino Depth: 8'

Eorinq Oia.: 2"

Paqe: I of I

Page 62: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility Borinq: MgF-g

!9ga!!9!j New Haven Rail Yard lnspector: C. Criscuolo

Client: Maguire Group Inc. Oate:3-26-07

t , ^

i oi t l

Loqical Environmental Solut ions354 South River Road

Tolland, CT 06084Truck, Portable & ATv/Backho*lllounted Caoprcbes

E a6 g

E

tt,

Descriptionc L o

3 g o 6 .Sample Interval

Ground Surface 0.0

1 .0 -

2.O-

3,0-

4.0-

5.0-

6.0-

7 .0-

$rHGray medium to coarse GRAVEL (BALLAST)1 . 0

0 Macro Core 0'-2'g_ :.ol '_4.o :. : o . - - + . : : cO r ' O : C o l1 ; { . 9 : . , ; {o : o . . a d :

9 .:1o.:.cq ri , q . 9 . i , . 1. d i P : - Jg :' : o . . o . : . 4o : o : c o lr,9: q..r;-1.o : Pr ' .4 t :. : 0 . . o . . : a

r;r,...9:.. i i t. o : _ o j . c _ a :. :o . . o . . : co ._ a .co- .

:q:a:q:i i:qi:".i'j:o. i,j j:'.:i

?.1:{.r:;.s-1:qi;q: i : :qi

:"jj:". ij-j :'. t

:r. i :/. i: ::q:i

:r.:;'::t,:iij:?.:i

:q:ii.{ri::.::q:i

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick, trace Concrete & fine to coarse Gravel (FILL)

5.0

0.2 Macro Core 2'4'

0 Macro Core 4'-6'Black ASH & CINDERS, little fine to coarse Sand & Gravel(FrLL)

Groundwater at 6'6.0

8.0

0 Macro Core 6'-8'

9.0-

10.0-

1 1 .0 -

12 .0 -

End of Boring at 8'

Soil Description: and = 35-50% some = ?0-35% little = 10-20% trace = 1.10%

Driller: W. Lineberry

Eigj Geoprone 5/t0U

Depth to Water: 6'

Borinq Deoth: 8'

Borinq Dia.: 2"

Paqe: I of 1

Page 63: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG I

i o( t l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truc R, Pottable & AMEactihcE-M ounEd Geoprobes

EIgiCgl! Temporary M-8 Acceptance Facitity

lggetig![ New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: M8F-g

InsDector: C. Criscuolo

Date: 3-26-07

E t oo o

o.(lcg,

Description E 5( r o o a Sample Interval

Ground Surface 0.0

1 .0 -

4.0-

c.u-

o_u-

7 .O-

l"r-%lGray medium to coarse GRAVEL (BALLAST)1 0

0 Macro Core 0'-2'.o-i.ii' : o . . - o . . :: O . + : c a,, .--. ..c..., :a : o : ' : . { a' : o . . - q . . . ::A r 'O : gq: j 9 . . .q . . ; ;

b : o r t . 4 { _.10 . . ' o . : . :

, j .9 . . . .9 . . , io : -4. .C_O

0 : _o. .c_o

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick. trace Concrete & fine to coarse Gravel (FILL)

5 .0

0.4 Macro Core 2 -4'

0.2 Macro Core 4 -6'

l: .. :!1 i:i +:

:{:i;{:i:i:{:

Black ASH & CINDERS, little fine to coarse sand & Gravel(FtLL)

Groundwater at 6'6 .0

8.0

0 Macro Core 6!8'

9.0-

10.0-

1 1 .0 -

12.0-

End of Boring at I'

Soil Description: and = 35-50% some = 20-35% little = 10-20o/o trace = l-10%

Orill€.: W. Lineberry

Elgj Geoprone 540U

Depth to Water: 6'

Borinq Deoth: 8'

Borino Dia.: 2"

gggei I of 'l

Page 64: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG I

A O| I l

Logical Environmental Solutions354 South River Road

Tolland. CT 06084Truck, Portable & ATvl8eckhoo+lount .l ceoprcbes

e!gi$j[ Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

Client Maguire Group Inc.

Borinq: M8F-10

lnsoector: C. Criscuolo

Date: 3-26-07

-o. 6

o d )o g

o

oDescription

o . oo o o a Sample Interval

Ground Surface 0.0

1 . 0 -

2.O-

3,0-

4.0-

5 .0 -

6.0-

7 .O-

av grhv's^o1t3no.€r:\./--qb+\4o : + r ' - c 4 :. : o . . - o - . : <' a _ . + : c o l; : p . . . o . . i r Ji l: or'io' :. .o . . o . : :<

, ; .8 . .q . . r ,J.o : .or'.c9 :. - . 4 . . o . . : <o . c . c + . ': , .o . q . . i j t.o : .ar-.c.0 :. - -o ._ o - : - : (

::.ol .o..-., lt.o' : .ar'.cf :. - -o . . o . : :<

Gray medium to coarse GMVEL (BALLAST)1 . 0

0 Macro Core 0'-2'

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little 8rick, trace Conc.ele & fine to coarse Gravel (FILL)

5.0

Macro Core 2'-4'

o.4 Macro Core 4'-6'-q:i :{:l l:q:'.o.ti

.qi;.i .21

s.';14 ;a:i a..{:i :r':.:i:q:

:c.:; :". i.i:'.:i-!1'. :! .! :i.!'.:qr i :{ i : ; :q: ii.{1ri:l:i:i.{::o.ri:'.:i!.:;:q:ii.i1.:l:.i:i.!:

:q:l::{:Ii'q:i

Black ASH & CINDERS,(FrLL)

Groundwater at 6'

little fine to coarse Sand & Gravel

6.0

8.0

0 . 1 Macro Core 6'-8'

9.0-

10 .0 -

1 1 . 0 -

' t2.o-

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = 1-10%

Driller; W. Lineberry

8!S, Geoprone $40U

Depth to Water: 6'

Borinq Depih: 8'

Borino Dia.: 2"

Paqe: I of I

Page 65: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

r a .

i o( t l

Loqical Environmental Soluiions354 South River Road

Tolland, CT 06084Truck. Podaue & A|U/B ackhoe-tttounted Geoprohes

Proiect: Temporary M-8 Acceptance Facility

Egql!!g![ New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: M8F-l I

Inspector: C. Criscuolo

Date:3.26-07

tL clo o .n

Description €.aI E o a

Sample Interval

Ground Surface 0.0

1 .0 -

2.0-

4.0-

5.0-

6.0-

7.0-

1v q rhv

/(\ /)/c;kvhiv-qts'-vd : o : - . c o -' _ o . ' o . : . : <

; : o ' ' . c ; ' :. : o . o . : : <

r ; .9 . . . .q . : ; r-o :.o j:.c.o :. - .o . . o -1 : (. : o . - o . . : <.a j 9: I .1.o-:. : 0 . . o 1 . - <' o r ' o : co l. : d - d . . : <

i : 0 , ' . i i ' ::o . . o . . .<

Gray medium to coarse GRAVEL (BALLAST)1 . 0

0 Macro Cor€ 0 -2'

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick, trace Concrete & fine to coarse Gravel (FILL)

5.0

0 Macro Core 2'4'

0 Macro Core 4'-6':q:a:qiii:;:q:i

:q:;:q:il:j:q::i

'x.'at4 .'it;v .':C:i.{:i.:r:{:i:o_D: :e. :iri i :"1:i

.q: i :q: i i :q: i

;q:i: :?. :ir: :j :qi

Black ASH & CINDERS,(FrLL)

Groundwater at 6'

liftle fine to coarse Sand & Gravel

6.0

8.0

0 Macro Core 6'-8'

9.0-

10.0-

1 1 .0 -

12 .O-

End of Boring at 8'

Soil Doscriotion: and = 3t50% some = 20-35% little = '10-20% trace = 1'10%

Driller: W. Lineberry

E!$, Geoprone 540U

Depth to Water: 6'

Borino Depth: 8'

Borinq Dia.: 2"

Pggg 1 of 1

Page 66: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG I

i.ot r l\ t l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Portaue & AruBackhoe.Mounted Geoprobes

&i99$ Temporary M.8 Acceptance Facility

!999!ig![ New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: MgF-12

Inspector: C. Criscuolo

Oate:3-15-07

: : :o oo 3

cU)

Description . c ^E 6o c to g

o aSample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

4.O-

5.0-

6.0-

7 .O- <i.F-+:-L-..fi r ' d . . r " ,: r J . f t . 1 : i

Black ASH & CINDERS with little to trace Red-Brown fine tocoarse SAND & fine to coarse Gravel (FILL)

Groundwater at 5.5'5.5

0 .1 Macro Core 0'-2'

0.4 Macro Core 2'-4'

0 .1 Macro Core 4 -6'

8.0

0 Macro Core 6'-8'

9.0-

10.0-

11.0-

12.0-

End of Boring at 8'

Soil Description: and = 35.50o/o some = 20.35% little = 10-20% traee = l-10%

Driller: W. Lineberry

!!g Geoprone 540U

Depth to Water: 5.5'

Borinq Depth: g'

Borinq Dia.: 2"

Pggg. 1 of 1

Page 67: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

iiLoqical Environmental Solutions

354 South River RoadTolland, CT 06084

Truck, PorTahle & AfvlBackhoe-Mounted Geoprohes

Proiect: Temporary M-8 Acceptance Facility

Locaiion: New Haven Rail Yard

Clienl: Maguire Group Inc.

Borinq: M8F-13

Insoeclor: C. Criscuolo

Date: 3-15.07

1 .

a

J .

A

5 .

6 .

Black ASH & CINDERS with little to trace Red-Brown fine tocoarse SAND & fine to coarse Gravel (FILL)

Macro Core 0'-2'

Macro Core 2'4'

Macro Core 4'-6'

Macro Core 6'-8'

5.5

0

o.2

0 .1

0

End of Boring at 8'

Soil Description: and = 3s50% some = 20-35% little = 10-20o/o trace ='l-10%

Driller: W. Lineberry

8!gj Geoprone 540U

Depth to Water: 5.5'

Borinq Depth: 8'

Sil$b-2"

Paqe: 1 of 1

Page 68: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG t ^

i of l l

Logical Environmental Solutions354 South River Road

Tolland, CT 06084f ruck, Pothble & AlylBackhoe.tlounte<I Geopfobes

&i$!: Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: MgF-14

Inspector: C. Criscuolo

Date: 3.19-07

a 6o { ,o 5

o

at,

Description E ^7 1o oo 9

o ad - 5

Sample Interval

Ground Surface 0.0

'1.0-

2.O-

3.0-

4.Q-

5.0-

6 .0 -

7 .O-

Gray medium to coarse GRAVEL (BALLAST) 0.5

0.3 Macro Core 0 -2'

Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete & Brick (FILL)

4 ,0

Macro Core 2'-4'

Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FlLL, wet)

6.0

4.0 Macro Core 4'-6'

Red-Brown fine to medium Sand, trace Silt

8.0

0.4 Macro Core 6 -8'

9.0-

10.0-

1 1 .0 -

12.O-

End of Boring at 8'

Groundwater Grab Sample Collected

Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = 1-'10%

Driller: W. Lineberry

Elgj Geoprone 54lU

Depih to Water: 4'

Borinq Depth: 8'

Borino Oia.: 2"

Paqe: 1 of 1

Page 69: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Elgigg! T6mporary M-8 Acceptance Facility

!999!!9q. New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: M8F-15

Inspector: C. Criscuolo

Date: 3-19.07

l ^

i o( t l

Loqical Environmental Solutions354 Souih River Road

Tolland, CT 06084f ru c k, Poda b I e & A TV/B ac k hoe- rll ou nte.l G e o probe s

E 6q r o

o

U'

Description 5.aq ' { 'o g

o ao - =

Sample Interval

Ground Surface 0.0

1 .0 -

2.0-

3.0-

4.0-

5.0-

o-u-

7 _0-

rv q.h\.,/(\ n,/(ilrPri8:q:-Y:i;::q::o::ij ,F. +j;::o. :

;q:a:q:a;:q:'.o.t:q :i;i'.o.:

:q:l':q:iJ:::q:' .2$:qi; . ; .7:

:qi:qd:::q:

: i : ; : i : i t i : :

i{,'i-i{-'ritF. :'.4,i.q.i .:.r.1

i-l:r:!:.:i):'./.:i:qi:.1:

'.F.i:q i .: .a.1

:q:l':q:i:;::q:

....:

Gray medium to coarse GRAVEL (BALLAST) 0.5

0. '1 Macro Core 0'-2'

Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete & Brick (FILL)

4,0

3.4 Macro Core 2 -4'

Black Ash & Cinders, lattle fine to coarse Sand, trace fine tocoarse Gravel {FILL, wet)

6.0

3.4 Macro Core 4 -6'

Red-Brown fine to medium Sand. trace Silt

8.0

0.6 Macro Core 6'-8'

9.0-

10.0-

11 .0 -

12.O-

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-10%

Driller: W. Lineberry

8!gj Geoprone 540U

Depth to Water: 4'

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: I of I

Page 70: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility Borinq: M8F-16

Location: New Haven Rail Yard Inspector: C. Criscuolo

9U9!l[ Maguire croup Inc. Date: 3-21-07

toa r .

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Portable & ATvlBackhoe-Mounbd Geoprcbes

€a6 E

o

o

Description - c ^X r i@ a Do g

o a- o .

Sample Interval

Ground Surface 0 .0

1 .0 -

2.O-

3.0-

4.0-

5.0-

6.0-

7 .O-

':i+: ii,i: i ii.

: { i : { i j i : { :'.d..j;:2i; .;.4:

:c:ii :q:i:i:q:i

+i:,i::4.:l

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

0 Macro Core 0'-2'

0 Macro Core 2'4'

_ d : . o : - . t t :. -o . . - a . . . .4' O r ' q : C O l

: ; .9.. ..q. .; ; .19 : .o:: . i9 :- : o . . o . . . : 4:O r 'O ;CO l9 ' : a : . c l :. : o - . o . : . : 4' O j O : d O . -

, ' .o , . .q . . . , , {

Red-Brown fine to medium SAND, little Silt, trace fine to coarseGravel

Groundwater at 4'4.0

5.00 Macro Core 4'-6'

ffiGray Clayey SILT

8.0

0 Macro Core 6'-8'

9.0-

10.0-

1 1 . 0 -

12.0-

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% littte = 10-20% trace = 1.10olo

Driller: W. Lineberry

BiS. Geoprone 540U

Deoth to Water: 4'

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: 'l of 1

Page 71: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

r a .

i o\!t I

Loqical Environmental Solut ions354 South River Road

Tolland. CT 06084Truck, Portable & AfV/Ba*hoe-M ounted Geopmbes

Proiect: Temporary M-B Acceptance Facility

Location: New Haven Rail Yard

Client: Maguire Group lnc.

Borinq: MgF-17

Inspector: C. Criscuolo

Date:3-21-07

E 63 e jt

Description cl oto q , 6 a

E E

Sample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

4.0-

c.u_

o . u -

7.0-

i3:'.:b.'.'i :i]:t:aj;.i.;:'.zti

r:q:i:{ii:q:i

r:o.:;j:9i..j .q:i

i'-i:iFj. : o - . c l . . c

, .O .q . . : IA :9 : . 4 -d :' : o . . - o . . : i

+ i i ' i ' c b i'1o. . - c . : (r , 9 . . q . r , . 1; . ; . . ; .

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

2 .5

0 .1 Macro Core 0'-2'

1 .9 Macro Core 2'-4'Red-Brown fine to medium SAND, little Silt, trace fine to coarseGravel

Groundwater at 4'4.Q

5.03.6 Macro Core 4'-6'

W4

+1Gray Clayey SILT

8.0

0 Macro Core 6'-8'

9.0-

10.0-

| | . u -

12.0-

End of Boring at 8'

Soil Descriotion: and = 35-50% some = 20-35% little = 10'20% trace = l-10%

Driller: W. Lineberry

Blgj Geoprone 540U

geslL@ls4'

&4!s-9s88'

Borino Dia.: 2"

Pgge:. I of 'l

Page 72: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

I

i ol r l

Loqical Environmental Solul ions354 South River Road

Tolland. CT 06084Truck, Portable & ATUlBackhoe-MounGd Geoprcl€s

elgigli Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

gliqli Maguire Group lnc.

Borino: MgF-18

USpCglgC, C. Criscuolo

Date: 3-21-07

=;ao ( ,o = o

Description t L oo o o a

o - - =

Sample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

4.0-

J . U -

6.0-

7 .O-

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

0 Macro Core 0'-2'

0 Macro Core 2'4'I : .O- .C.O. : o . . o . . . 'Q . o : c O

o : -o. ,+o. 1 4 . . q . . . :o . _ o : c oo :.o;i.!.o'' ' o - o . : . '

Red-Brown fine to medium SAND,Gravel

Groundwater at 4'

little Silt, trace fine to coarse

4.0

U Macro Core 4'-6'w)ffi+r4

Gray Clayey SILT

8.0

0 Macro Core 6'-8'

9.0-

10.0-

t z , v '

End of Boring at 8'

Soil Descriotion: and = 3$50% some = 20-35% little = 10-20% trace = l-l0o/"

Driller: W. Lineberry

B!$. Geoprone 5/()U

Depth to water: 4'

Borinq Oeoth: 8'

Borinq Dia.: 2"

Pgge: I of I

Page 73: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Proiect: Temporary M-8 Acceptance Facility

Egel!g![ New Hav6n Rail Yard

Client: Maguire Group Inc.

Borinq: M8F-i9

Insoeclor: C. Criscuolo

Date:3-21-07

I

i of l i

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084T ruck, Podable & ATv/Backhoe-Mounted Geoprobes

E 6o o

6

Description E 6o oo =

. r iSample Interval

Ground Surface 0 .0

4.0-

6.0-

':ii::ii"::i;

:F-ij .9ii :;:el:

:i:; :'. iJ j:"1:i.t:a:l:rt.l:

:q:i;q:i-j:q:

:{j.:q:ii:q:

:;.i::t:;r :;:i::'l:;'::q :i.r i:el:

:q:ij:o. iij:e.:

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt, mlxed with Gray to OliveBrown Clayey Silt (FILL)

Gtoundwater at 5'5.0

0 . 1 Macro Core 0'-2'

2.6 Macro Core 2'4'

Macro Core 4'-6'5.5

Black ASH & CINDERS {FILL)

8.0

0,3 Macro Core 6'-8'

9.0-

10.0-

I t . u -

12.0-

End of Boring at 8'

Soil Descriotion: and = 35-50o/o some = 20-35% little = 10-20% trace = t-10%

q!0!9! W. Lineberry

8!g: Geoprone gou

Deoth to Water: 5'

Borinq Depth: I'

Borinq Dia-: 2"

@ , 1 o f 1

Page 74: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Plgigll[ Temporary M-8 Acceptance Facility

kggll$ New Haven Rall Yard

gljgq! Maguire Group Inc.

Borino: M8F-20

Inspector: C. Criscuolo

@3-21-07

I

0Loqical Environmental Solut ions

354 South River RoadTolland, CT 06084

Truck, Podable & ATV,/B atkhoa-Mounted Geoprobes

E L Oo o

E

o

Description z ,rio oo g

o dSample Interval

Ground Surface 0.0

1 .

2 .

3 ,

4,0-

5.0-

6.0-

7.0-

:qi:qi i;qj

rir''?+ j:ii

i .11.:f :ait-: ;q:i :{:i j ;{:1 ...i .z i; j .zl

t.q:tr:i:.::/.:

: .ai:q i .; .2)

::q: i :{+:.r:q.

t:d.t;:z ii .i:o.l

;:q:i :{a:.::q:

i'.d.i:iii!:d.:

i'.l:i.(t ,i:o.t

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt, mixed with Gray to OliveErown Clayey Silt (FILL)

Groundwater at 5'5.0

0 .1 Macro Core 0 -2'

0.4 Macro Core 2'-4'

0 .1 Macro Core 4'-6'5.5

:q:ii:qi i:q:ir:cl:i ?:i.l :.:I:ii.!1t+:! :i-lt--.::q:iit:ii:;.q:i

::"-;j :e ir :;:qji

: :'.:i:'.i i:.:i: :'::;_: :D. :i.r j:ol:i

Black ASH & CINDERS (FILL)

8.0

0 Macro Core 6'-8'

9.n -

0-10 .

1 1 . 0 -

12.O-

End of Boring at I'

Soil Descriotion: and = 35-50% some = 20-35% little = 10-20% trace = l-10%

g[er: W. Lineberry

Big: Geoprone 54(lU

Deoth to Water: 5'

gpfjls-qellE8'

Borinq Dia.: ?"

Eegg, 1 of 1

Page 75: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORTNG LOG l 0f I r

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, PorAble & ATU/Backhae-t ounled Geoprobes

Proiect: Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

Client: Maguire Group Inc.

Borino: M8F-2'l

hslector: C. Criscuolo

Date:3-26-07

sg U'

Description 5 ac L o{ r o o o -

Sample Interval

Ground Surface 0.0

'1 .0-

2.0-

3.0-

Gray medium to coarse GMVEL (BALLAST) 0.5

0 Macro Core 0'-2'

Black ASH & CINDERS, little Brick & Gray Sitt (FtLL)

4.0

U Macro Core 2'-4'

Refusal on CONCRETE at 4'

Soil Descriotion: and = 35-50% some = 20-35% little = 10-20% trace = 1-10%

Driller: W. Lineberry

BiS, Geoprone 540u

Depth to Water: Dry

Borinq Depth: 4'

Borino Dia.: 2"

Paqe: I of 1

Page 76: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG | -il

i ot t l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Tructr, Portable & Afv/Backhoe-Mounte.l Geoprobes

e!gig!: Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

gliClg Maguire Group Inc.

Borinq: MgF-22

Uaso€ctor: C. Criscuolo

Date: 3-21.07

o o

o

oDescription

cL (lto (tt c I 0 -

d g

Sample Interval

Ground Surface 0.0

i-!1r,1:ali!'.:F. : ; j : ' . i : : ; : ' . :

i-qld,! i:i!:

Black ASH & CINDERS, liule fine to coarse Sand, trace fine tocoarse Gravel {FILL)

1 . 0

3.0

0 Macro Core 0'-2'i'-F:;l. : 0 . . - o . 1 . : <'o , . o :co . .

i :.o..i.ii '-:. 1O ._ - O : . : <' a

. . q : i . a lrr P: : .q.. : : Jo : 6 . ' ; b - :

Red-Brown fine to coarse SAND

0 Macro Core 2'-4'

:'jj :d. rii ::?.:

: .r'.i !:4 .; .t l

Dark-Gray to Black fine SAND & SILT, little Ash & Cinders{FILL)

Groundwater at 6'6.0

Macro Core 4'-6'

:i,;::c,.:i:q:i;".:i:'.i.j:"..ii ! : i i :5: i i i l l.q:! :{i:.r :q:

r:q:i::t:i :,::q: 8.0

Macro Core 6'-8'

9.0-

10 ,0 -

1 1 . 0 -

I z . u -

End of Boring at I'

Soil Description: and = 35-50o/o some = 20-35olo little = 10-20% trace = 1-10%

Driller: W. Lineberry

8jg, Geoprone 5,40U

Depth to Water: 6'

Borino Depth: 8'

Borinq Dia.: 2"

Paqe: I of 1

Page 77: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

elgiegE Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

Clieni: Maguire Group Inc.

Borinq: M8F.23

Inspector: C. Criscuolo

Date:3-21{7

l 0!7 1

Loqical Environmental Solut ions354 South River Road

Tolland. CT 06084Truck, Poitable & AMBackhoe-Mounte<t Geoprobes

€ ao oo g o

Description ; :o a bo g

o ao - =

Sample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

4.0-

5 .0 -

6.0-

7 .O-

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

1 . 00 Macro Core 0'-2'.1-Fi.6t' : o . . o . : : (

4 . q : c O . -_ : o . - o - , : (a', o.lsi'-,. ' _o . . o . : : (O r ' O : C O .. : 4 . O . : <

_o : .o: _c.o :

Red-Brown fine to coarse SAND

3.0

6.0

0.4 Macro Core 2'-4'

i.a.t:..'.t::{:i:{i

::eli::".':i.l

::q:a:{:i

i.+:.:+:!

li.4.:;.q:

:i::.:: t -1:

:.:.q:

t,:ti:

Dark-Gray to Black fine SAND & SILT, little Ash & Cinders (FILL,Detroleum odor)

Groundwater at 6'

0.3 Macro Core 4'-6'

8 .0

0 Macro Core 6'-8'

9.0-

10.0-

1 '1 .0 -

12 .0 -

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-10%

Driller: W. Lineberry

Blgj Geoprone 540U

Depth to Water: 6'

Borinq Depth: 8'

Borinq Oia.: 2"

Eggg, 1 of 1

Page 78: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Elgi$h Temporary M-8 Accepiance Facility

!999!!9!j New Haven Rail Yard

Client; Maguire Group lnc.

Borino: M8F-24

EgE!g!' C. Criscuolo

Date:3-21-07

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Ponable & ATv/gackhoe-Mounted Geoprcbes

E 6o q ,

o

Description c L oo oo = -

o ao - ' =

Sample Interval

Ground Surface 0.0

l1 .0 - l

2.0-

3 .0 -

4.0-

5.0-

6.0-

7 .0-

Black ASH & CINDERS, little fine lo coarse Sand, trace fine tocoarse Gravel (FILL)

1 . 00 Macro Core 0'-2'

o o . . t _ o : l. 4 . - " o l

: c o

o . c,oa'o r ' o , gq

; : ; , . ' ' ; ;

Red-Brown fine to coarse SAND

3.0

o . u

1 . 6 Macro Core 2'-4'

Dark-Gray to Black fine SAND & SILT, Iittle Ash & Cinders (FILL'petroleum odor)

Groundwater at 6'

u.o Macro Core 4'-6'

8.0

0 Macro Core 6'-8'

9.0-

10.0-

1 1 .0 -

12.O-

End of Boring at 8'

croundwater Grab Sample Collected

Soil Description: and = 35-5oo/o some = 20-35o/o little = l0-20o/o trace = 1-10%

Driller: W Lineberry

Eig= Geoprone 540U

Depth to Water: 6'

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: I of 1

Page 79: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGProiect: Temporary M"8 Acceptance Facility Borinq: M8F-2S

Location: New Haven Rail Yard Inspector: C. Criscuolo

Client: Maguire Group Inc. Oate: 3-21-07

t ^

i oq t l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Portabte & ATvlgackhoe'Mounte<l ceoprobes

se (t

Description 5 ac L oo o o a

o - =

Sample Interval

Ground Surface 0.0

1 0 -

2.0-

3.0-

4.0-

5.0-

o-u-

i-!1J:!12:i-!1

i-!1.:!11:i-U

:q:i-c:i:;;q:

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,littfe fine to coarse Gravel, trace Silt, mixed with Grav to OliveBrown Clayey Silt (FILL)

Groundwater at 5'5.0

0 .1 llacro Core 0'-2'

1 . 1 Macro Core 2 -4'

u.c Macro Core 4'-6'5 .5

;:q:i:q:ir:;.{:i

::".:;r: u.;r;;:'.:i

: :q, i :qi i :qi

: :" . :d:r. : i i :q.: i

:q+:{: i : :q: i

:o. i: :'. i:i:F. I

Black ASH & CINDERS (FILL)

8.0

0 Macro Core 6'-8'

9.0-

10 .0 -

1 1 .0 -

' t2.0-

End of Boring at 8'

Soil Descriotion: and = 35-50% some = 20-35% liftle = 10-20% trace = 1-10%

Ddller: W. Lineberry

Bj$. Geoprone 540U

Depth to Water: 5'

Bodnq Deoth: 8'

Borino Dia.: 2"

Paoe: 1 of 1

Page 80: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

r a .

O\ t l

Loqical Environmental Solut ions354 South River Road

Tolland, CT 06084fruck, Poraa e & ATvlBackho*Mounted Geoprobes

Proiect: Temporary M-g Acceptance Facility

tggali$. New Haven Rail Yard

glg!l!: Maguire Group Inc.

Borino: M8F-26

Inspector: C. Criscuolo

Daie:3-19-07

€ crL ol

3 E (t

Description o. o,o oo =

O C LSample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

4.O-

5.0-

o_u-

7 .O-

Dark-Brown to Black fine to coarse SAND, little Ash & Cinders,trace Concrete. Brick & fine to coarse Gravel (FILL)

2.0

0.3 Macro Core 0 -2'

:q:l,{:ir:.;:q:

:?l:i ?|i.j i3. :

:"j;-::''.:ii:::ol: Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL. wet)

Groundwater at 5.5'5.5

0.9 Macro Core 2 -4'

.f:i.:";{:.ij

Macro Core 4'-6'

8.0

0.2 Macro Core 6'-8'

9.0-

10.0-

'1 1 .0-

12 .0 -

End of Boring at 8'

Soil Descriotion: and = 35-50% some = 20-35% little = 10:20old trace = 1'10%

Driller: W. Lineberry

Elgj Geoprone 540U

Oepth to Water: 5.5'

Boiinq Depth: 8'

Borinq Dia.: 2"

Eggg! I of I

Page 81: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Slgigg[ Temporary M{ Acceptance Facility Borinq: MgF-27

!99el!!9![ New Haven Rail Yard Inspector: C. Criscuolo

g!!g!: Maguire Group Inc. Date: 3-21-07

I

i o\7 I

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Portable & ATvlBackhoe-Mounted Ceoprobes

E 6q r oo g

Eo

Description €.ao o6 =

o aE g

Sample Interval

Ground Surface 0.0

i.i.

i.t.

i.q.

,..t,

' :..:

o

9

o i c a'. :q . : ;.ar ,Jg

.a,l.ii,_ .o . : - :' o : c o' ' o . :i r r ' ; i

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

?.5

Macro Core 0'-2'

0 .1 Macro Core 2'-4'Red-Brown fine to medium SAND, little Silt, trace fine lo coarseGravel

Groundwater at 4'4.0

5.00 Macro Core 4'-6'+1

uGray Clayey SILT

8.0

0 Macro Core 6 -8'

9.0-

10.0-

1 1 . 0 -

12 ,0 -

End of Boring at 8'

Soil Descriotion: and = 35-50% some = 20-35% little = 10-20% trace = 1-10olo

Driller: W Lineberry

Bigj Geoprone 5,40U

Deoth to Water: 4

Borinq Oepth: 8'

Borino Dia.: 2"

Paqe: 1 of 1

Page 82: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG l 0r I '\ y l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Po.lable & Aw/Aackhoe-Mounted Geoqobes

Proiect: Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: M8F-28

Insoector: C. Criscuolo

Date:3-21-07

E 6r D o

o

IJ'

Description x ?o o o a

o - s

Sample lnterval

Ground Surface 0.0

1 .0 -

2.0-

3.0-

4.0-

5 .0 -

6.0-

7 .O-

:q: l ;{ : l r :ql

:{i;;q:ii:qi

:". :;:j :o. :;rj .;?:l

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

2.5

4.0

0 Macro Core 0'-2'

0,6 Macro Core 2'4'i":iJiF::o . . o . . . :<'o .. a :co.-

, { . ,9. . i r '1o a . c 9 ;' : o . . o - . . : (o . -o .co - 'o : o j i t o :' : o . . o - : . : (

,1 o.,. ,9..ir '1

T+)i l l+r)| l l

){)i l ll)- |

Red-Brown fine to mediumGravel

Groundwater at 4'

SAND, little Silt, trace fine to coarse

5.00 Macro Core 4'-6'

Gray Clayey SILT

8.0

Macro Core 6'-8'

9.0-

10.0-

1 1.0-

12.0-

End of Boring at 8'

aoil Description: and = 3$50% some = 20-35% fiftfe = 10-20% llace = 1-10o/o

Driller: W. Lineberry

&, Geoprone 540U

Depth to Water: 4'

Borino Depth: 8'

&dry-Pjsn2"

Paq€; I of 1

Page 83: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Plgigg Temporary M-8 Acceptance Facility

!99a!!9!j New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: M8F-29

Inspector: C. Criscuolo

Date:3-21-07

Logical Environmental Solut ions354 South River Road

Tolland, CT 06084fruck, Portahle & AfvlBackhoe-Mounte.l Geoprobes

* eo q t

E

o

Description E 6o o6 g

o a Sample Interval

Ground Surface 0.0

1 . 0 -

2.O-

3 0 -

4.0-

5.0-

o.u-

7 .O-

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

1 . 00 .1 Macro Core 0'-2'a-Fii

. - . o . . o . . :

j ; P . . - q . : ;

C: .or'J.o.-_o.. o.'. ..

- : 4 . O . . :

b : o , ' - 4 i' : o . . o - . :- : o ' . - o - . :

i : i : ' .ai. -_o . . o - ' . . .g- : o. .co. : o . _ o . 1 . -O r ' O i C O; ;9 . . 9 . . ; ;pi4-;# Aq : o . c g. : o . . - o . . -o - o : c o::.9. ..9...: lg_ : o : : . co' : o . . - o . . :q . -o : c .o; i .9 . .1 . . , ;9_ : -o r : .4O' 1 0 . . ' o . :

; , .o . . .q . . : ;O : _or1.cO' t o . _ o . . . :

:9

n:

1:

9I9o

:.

Red-Brown fine to medium SAND. little Silt. trace fine to coarseGravel

Groundwater at 4'4.0

1 . 1 Macro Core 2'-4'

0.5 Macro Core 4'-6'

Dark-Brown medium to coarse SAND. trace Silt

8.0

0 Macro Core 6.-8'

9.0-

10.0-

1 .1 .0-

12.O-

End of Boring at 8'

Soil Description: and = 35-50% €ome = 20-35% little = 10-20olo trace = 1'10%

gfi!!g' w. Lineberry

E!S, Geoprone 5401J

Depth to Water: 4'

Eel!!s-ge&8'

Borino Dia.: 2"

Pegg. 1 of I

Page 84: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG

elgigq!: Temporary M-8 Acceptance Facility Borinq: M8F-30

!Egl[g$, New Haven Rail Yard Inspector: C. Criscuolo

g!C!l!i Maguire Group Inc. Date: 3-21-07

I

l o( t l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Poraaue & ATv/Backhoe-Mounbd Geoprcbes

E 6o o

E

.n

Description : :o oo 9

o aSample Interval

Ground Surface 0.0

I

' o-l

2.O'

3.0-

4.0-

5.

6.

7.0-

;;;,:;;f J:il:'-:ij :t i: :i :"::

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

1 . 00 Macro Core 0'-2'i'-Tdil' - .o . o . .q

o r ' d : C a l;; P-. .q . : ; {o : o . 4 0 :- : a . . o - : . aO r ' O : { O jrr p- ..9 .i;.t-o : .o: .c.o :. ' .o . . 'o . : . :o

: , P . . q . . j ; . {b: + : ' -co ' :. : o . . o . . . : 0c : c : . q g ,. : o . . 0 . : . : a'o r'c .c.o --, ,n. . lq. . ; , . !4r i+ c:o : c . c a :: o . o - : . : o

' : a . o . : to : .0 : . c .o :' .o . . 'o . : . -4' o : o ' : c o r, 'O . . .q . ; i .1_d : .o r ' .4 .o :- :o . . o l . c: o - o : 4 q . .t : 9 : . . q . j : Ib ; o r ' . c b :. o . o : t (

Red-Brown fine toGravel

medlum SAND, little Silt, trace fine to coarse

Groundwater at 4'4.O

0.3 Macro Core 2 -4'

5.0

8.0

0.1 Macro Core 4'-6'

Dark-Brown medium to coarse SAND, trace Silt

0 Macro Core 6'-8'

9.0-

10.0-

1 1 . 0 -

12.0-

End of Boring at 8'

Soil Description: and = 35-5{rolo some = 20-35% little = 10-20% trace = 1'10%

Driller: W. Lineberry

Bigj Geoprone 540U

Deoth to Water: 4

Borinq Deoth: 8'

Borinq Oia.: 2"

Paqe: 1 of 1

Page 85: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Proiect: Temporary M-B Acceptance Facility

!994!!9!! New Haven Rait Yard

Client: Maguire Group Inc.

Borinq: M8F-31

Inspector: C. Criscuolo

Date:3-21-07

I

A O\!t I

Logical Environmental Solutions354 South River Road

Tolland. CT 06084f.uck, Pottable & ATvlBackhoe-Mounted Geoprohes

=aao oo g o

Description a 6o o6 g

o ao - =

Sample Interval

Ground Surface 0.0

'1.0-

2.O-

3.0-

4.O-

o.u-

i.qld:l:jit.l

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt {FILL)

1 . 00 Macro Core 0'-2'

$ : .o:. .4.d. : o . . - + 1 . .o : o : C o. : o . - o - , . :

_o : _o: ,c_d: o . . o . . . :

' : o ' - o . - :

_o :qi .c9'' : o . . q . . . :

i i -o:. .:C... i;o : .c ; . co. : o . o - : . 'o - o ; c ci;d. .9... i jo : 9 ; . 4 9. - o . . o . . . 1-^--:at it, , .w .w.v. ' _o . . + . :o r ' o : c o. : o . o , :9 :.o j:.{.o. : 0 . - o . 1 . -

:;o: ' :4..:;o : a : r . a q' :a - . + . . - - .a : o c o

0 : a r ' . c 4' 'o . o ._ . . :

Red-Brown fine to medium SAND. little Silt. trace fine to coarseGravel

'. Groundwater at 5'

1 . 7 Macro Core 2'-4'

0.5 Macro Core 4'-6'

8.0

Dark-Brown medium to coarse SAND. kace Silt0 Macro Core 6'-8'

9.0-

10.0-

12.0-

End of Boring at 8'

Soil Description: and = 35-50o/o some = 20-35% liftle = 10-20% irace = 1.10%

Driller: W. Lineberry

[!91 Geoprone 540U

Depth to Water: 5'

Borino Deoth: 8'

Borinq Dia.: 2"

Paqe: 1 of 1

Page 86: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

elgiglE Temporary M.8 Acceptance Facility

!9ga!!9!! New Haven Rail Yard

gljggE Maguire Group lnc.

Borinq: M8F-32

Inspector: C. Criscuolo

Date:3-19-07

l / l

l oC l r

Loqical Environmental Solut ions354 South River Road

Tolland, CT 06084Truck, Porlattle & AruEackhoe-Mounted Georyobes

E 6o o

o

E

at

DescriptioncL dto oo 9

o a Sample Interval

Ground Surface 0.0

1 .0 -

7 .O-

: :q:a;q: i i :q: i

: t i t i i , i i : i . : i

::q:ari-::q:i: :". :;: F. ir j:cl:i

;:t:it_-:i:::n

Dark-Brown to Black fine to coarse SAND. little Ash & Cinders,trace Concrele, Brick & fine to coarse Gravel (FILL)

2.0

o.2 Macro Core 0 -2'

Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FlLL, wet)

Groundwater at 5.5'5.5

1 . 1 Macro Core 2'4'

0.5 Macro Core 4'-6'

8.0

0 .1 Macro Core 6'-8'

9.0-

10 .0 -

1 1 . 0 -

't2.0-

End of Boring at 8'

Soil Descriotion: and = 35-50% some = 20.35% little - 10-20% trace = l-10%

pd!!e! w. Lineberry

!!g; Geoprone 540U

Oepth to Waler: 5.5'

Borino Deoth: 8'

Borinq Oia.: 2"

Begg, 1 of 1

Page 87: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGelgigg! Temporary M-8 Acceptance Facility

!99a!!9I[ New Haven Rail Ya.d

Client: Maguire Group Inc.

Borinq: M8F-33

InsDector: C. Criscuolo

Date:3-21-07

I

i ot t i

Logical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Po.table & Afv/Backhoe-Mounted Georobes

E 6C ' O

oll

o

Description : :o oo g

o ao - =

Sample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

4.Q-

5.0-

6.0-

7 .0-

:q,!:{:i:.::q,i

i,tii:F:' t o . . - o . . . : {, ,O. .q. . : i .1g : 9 . . . c o :. : o - . + . . . : 4o : - o d+ l,,O. :q .. i!.1o : o ; . c o :. : o . . + . . : 4'c ..-o : c? ..: , .o-. .:1 ...; .1-+ : 9r'.C-O :' o . - o : c a l;,.9.. .q...,; IO : o : r . 4 9 - :. : o . . - 4 . . . : i

: j .o-. .q .i:.10 : o r ' ' + o :: o . . o . . - : c' q . . - c g a l

:' o;. .1, :,1.o : 9; .c.4 :' ' o . _ o . : . : 4' O

r - O : C O . .rl.9- -y1..:r I

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)

5.5

0 Macro Core 0'-2'

Red-Brown fine to coarse SAND, trace Silt & fine to coarseGravel

Groundwater at 5.5'

0.1 Macro Core 2'-4'

0 Macro Core 4'-6'

6.5

0 Macro Core 6'-8'I+))+)Gray Clayey SILT

8.0

9.0-

10 .0 -

1 1 . 0 -

12 .O-

End of Boring at 8'

Soil Descriptlon: and = 35-50o/o some = 20-35% little = 10-20% trace = 1'10%

Driller: W. Lineberry

Sigj Geoprone flou

Depth to Water: 5.5'

Esrus-gs48'

Borinq Dia.: 2"

Paoe: I of 1

Page 88: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Plgiggltj Temporary M-8 Acceptance Facility

!99at!9!! New Haven Rail Yard

g!jg!l!: Maguire Group Inc.

Borinq: MgF-34

h9p9q!9! C. Criscuolo

Date:3-21-07

r / l

i of l l

Logical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Portabte & Afv/Beckho*Mounte.I Geoprcbos

o o! r oo g

oco

Description 6.6o oo g

o ao - g

Sample Interval

Ground Surface 0.0

1 .0-

2.0-

3.0-

5.0-

6 .0 -

7 .O-

:i,i':.'i,r'::i:

!riiF:- : o . . o . . : {j , .o - . .9 . . i , I0 :_or,.c.o :

; , .o - .9 . . . , , Io : 9 : . 4 9 ,- t o . c . . . : (

r r .9 . . .9 . . i ; Io : q : : . + o :' 1 0 . . c . . : (

r , .9 . . . .q . . : i .19 : 9 . . 4 9 :' ' o . . c . . : <' : o , o . , : <

9 : . o j . c 9 :

r r ' - o . q , : j lo : .or'.{4 :

r . . 4 . - . q - . ; ; J

Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL) 0.5

5.5

0 Macro Core 0'-2'

Red-Brown fine to coarse SAND, trace Silt & fine to coarseGravel

Groundwater at 5.5'

0 Macro Core 2'4'

0 Macro Core 4'-6'

6.5

0 Macro Core 6'-8'W)k)

Gray Clayey SILT

8.0

9.0-

10.0-

1 1 .0 -

12.0-

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% liftle =10-20% trace = l-10%

Driller: W. Lineberry

E!S, Geoprone 540U

Depth to Water: 5.5'

Borlno Deoth: 8'

Bodnq Dia.: 2"

Paoe: I of I

Page 89: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG ioC l l

Logical Environmental Solutions354 South River Road

Tolland. CT 06084Truck, Portable & ATvlBackhoa-Mounte.t Geoprobes

Proiect: Temporary M.8 Acceptance Facility

Location: New Haven Rail Yard

glblE Maguire croup Inc.

Borinq: M8F-35

Inspector: C. Criscuolo

Date:3-26-07

-*E6 s \o

Description E O

o ( , o 5 .Sample Interval

Ground Surface 0.0

5.0-

6.0-

7.0-

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

2.0

0 Macro Core 0'-2'

; :q : i .q+ : j :q : l

;:c.:;j:o. i,;:;:".ri

;:q:i-q:ir:i:q:i

i . l : . : l r i . i . t : :

i.5.'. i:+'.a it.i:

r .q l r :+1! . t l : r

i .q: . q l i ; i9 : :

:l:.:4.; ":qi

i . ! : . : l . i : i . ! : r

Black ASH & CINDERS

Groundwater at 4.5'4.5

Macro Core 2 -4'

0.4 Macro Core 4'-6'

8.0

0 Macro Core 6'-8'

9.0-

10.0-

12.0-

End of Boring at 8'

Soil Description: and = 35.50% some = 20.35% little = 10-20% trace ='l-10%

Driller: W. Lineberry

Bigj G€oprone 540U

Deoth to Water: 4.5'

Borino Depth: 8'

Borinq Dia.: 2"

Eggg. 1 of 1

Page 90: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility Borinq: MBF-36

Location: New Haven Rail Yard Inspector: C. Criscuolo

Client: Maguire Group Inc. Date:3-26-07

t l

i of l l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, P ottable E Afvlaackhoe-Mounted Geoprcbes

t ^E 6o o

o

Description E 6o o o A

- c rSample Interval

Ground Surface 0.0

'I .0-

2.0-

4.0-

5.0-

6.0-

7 .O-

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

2.0

0 Macro Core 0!2'

Black ASH & CINDERS

Groundwater at 4.5'4 .5

0 Macro Core 2'-4'

0 Macro Core 4'-6'

8.0

0 Macro Core 6'-8'

9.0-

10 .0 -

1 1 . 0 -

12.0-

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% tittle = 10-20% trace = l-10%

Drill€r: W. Lineberry

Ejgj Geoprone 54Ou

Depth to Water: 4.5'

Borinq Oepth: 8'

Borinq Dia.: 2"

Paqe: I of I

Page 91: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

llgigglE Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

gI!S!l[ Maguire Group Inc.

Borinq: MgF-37

InsDector: C, Criscuolo

Date: 3-26-07

I

A O( t l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Po,TaNe & ATv/Backhoe.Mounte.l Geoqobes

Macro Core 0 -2'

Macro Core 2L4'

Macro Core 4'-6'

Macro Core 6'-8'

Black ASH & CINDERS, Iittle fine to coarse Sand, trace fine tocoarse Gravel (FILL)

2.0

4.0

0

0.4

0.3

0

End of Boring at 8'

Driller: W. Lineberry

Elgj Geoprone 540U

Depth to Water: 4'

Borinq Depth: 8'

Eorinq Dia.: 2"

eg$,1 of 1

Page 92: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGelgigli Temporary M-8 Acceptance Facitity

!99a!i9E New Haven Rail Ya.d

Client: Maguire Group lnc.

Borino: M8F-38

Inspector: C. Criscuolo

Date:3-26.07

l 0a t l

Logical Environmental Solut ions354 South River Road

Tolland, CT 06084Truck, Portable & Afv/Backhoe-Mounted Ceoprobes

a 6q r oo g o

Description E E{ r oo g

Fo 6 .

Sample Interval

Ground Surface 0.0

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

2.0

0 .1 Macro Cole 0'-2'

:q:i:4i:i:q:i

:,::; :'. i. :i :'. :ii.!:r:!:rilr

,q;i :{rf I :q:ii3:-. 1:l :i!-.:q: : : t : ; i : i : " . : i

:q:i:q:ia:i:q:i

:ql:ir :o. i: :l :q:i

:q:i:qi j:q:i

:cl;::o. i'::i:P::i

:q: i :q: i i :q: ii-!1.:l1J:i-!i: " . : ; :F. : i : ;X: ii-t1.,:l:t :i-!ir:q:i:{ri:;:qri

;:". :i:'. :;i :;:9 :i

Black ASH & CINDERS

Groundwater at 4'4.0

o.2 Macro Core 2'-4'

8.0

0 Macro Core 4'-6'

0 Macro Core 6'-8'

9.0-

10.0-

1 1 . 0 -

12.O-

End of Boring at 8'

Soil Description: and = 35-50% some = 20-35% liftle = 10-20% trace = l-'10%

Driller: W. Lineberry

BlS Geoprone 540U

Depth to Water: 4'

Borinq Depth; 8'

Bodnq Oia.: 2'

@ , 1 o f 1

Page 93: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Elgiggl! T€mporary M-g Acceptance Facility

Ee!!S, New Haven Rail Yard

gljgllE Maguire Group Inc.

Borinq: M8F"39

InsD€ctor: C. Criscuolo

Date:3-26-07

I

i o\ J t

Logical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Porlable & Afv/Backhoe-lt ounted Geoprcbes

1 .

3 .

A

5.

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel {FILL}

Black ASH & CINDERS

2.0

4.O

0

0 .1

U

0

Macro Core 0'-2'

Macro Core 2'4'

Macro Core 4'-6'

Macro Core 6'-8'

End of Boring at I'

Driller: W. Lineb€rry

Eigj Geoprone 540U

Depth to Water: 4'

Borinq Oepth: 8'

Borinq Dia.: 2"

Paoe: 1 of I

Page 94: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Plqipd! Temporary M-8 Acceptance Facility

!9pq!!9!: New Haven Rail Yard

g!!q! Maguire Group lnc.

Borinq: MgF40

Inspector: C. Criscuolo

Date: 3-19-07

I

i.oLoqical Environmental Solutions

354 South River RoadTolland, CT 06084

Truck, Por'3ble & ATvlBackhoe-Mounb l Geoprobes

=aao oo g

co

Description E 6o o o a

Sample Interval

Ground Surface 0.0:i:i::i:i::::il:C:i- :t':i.r j :q:

:r-:; :r. :; r :r.:

rSirliir.{n

Dark-Brown to Black fine to coarse SAND, Iiftle Ash & Cinders,trace Concrete, Brick & fine to coarse Gravel (FILL)

2.0

0.9 Macro Core 0'-2'

:qi ! :q: i l :q: i

:"::i.r:".':i.::i:".:i

:c:i :q:ii :.: :q:i

:o::;r :o. i: :::'l:i

:q:i:q:i:i:q:ii - ! ' . . : l1i : i ! :

.{:i:qi i:qj

:". j;r :'. :;.j :;:'. :i

:qr i :q: i : ! : i;:q. :;.. :'. :iJ :;:q. :i

r:q:iJ:{ri,::::q:i

;:q. :;j ?:ij:;:q, :i

: :q: i :q: ir : . :q: i

::?:;r:a.:irij:q:i

Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

Groundwater at 5'5.0

J . O Macro Core 2'-4'

1 . 3 Macro Core 4'-6'

8.0

0.4 Macro Core 6'-8'

9.0-

10.0-

1 1 .0 -

12.O-

End of Boring at 8'

Soil Description: and = 35-50o/o some = 20-35% liftle = 10-20% trace = l'10%

Driller: W. Lineberry

B!g: Geoprone 540U

@!sg5'

Borinq Depth: I'

Borinq Dia.: 2"

gggCj 1 of I

Page 95: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facitity Borinq: MBF-41

Location: New Haven Rail Yard Insoector: C. Criscuolo

Client: Maguire croup Inc. Date: 3-.19-02

r i

i o( t l

Logical Environmental Solut ions354 South River Road

Tolland, CT 06084Truc& Porlable & ATvlBackhoe-Mounted Geoprobes

€a3 E

occ,

Description * ao o o a

; i c L

Sample Interval

Ground Surface 0.0

1 .0 -

2.0-

3.0-

4.O-

5.0-

6.0-

::ii'?:ii: : t;a.ql'dl:t r.!:i:e. ii :qir j:'. ii.q:d.1.:t:i9:

:r:i;q:ai:qi::p.:i tq t;i tzi

' :qi :{ : i : :q: i

::q+j:{i j:qi

::F.ij:c. iji:".:i

::qi:r*:.::q:i

::c.:i,-:r.:;j::.ci

:.i.i"4ii:'...tii -+:. ! : t t ! :

:q:i:{i j:q:i

Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete, Brick & fine to coarse Gravel (FILL)

2.O

0.6 Macro Core 0'-2'

Black Ash & Cinders, liftle fine to coarse Sand, trace fine tocoarse Gravel (FILL)

Groundwater at 5'5.0

1 . 8 Macro Core 2'-4'

Macro Core 4'-6'

8.0

o.2 Macro Core 6'-8'

9.0-

10.0-

1 1 .0 -

12.0-

End of Boring at 8'

Soil Oescription: and = 35-50% soms = 20-35% little = 10-20% trace = 1-10o/"

Driller: W. Lineberry

Elgj Geoprone 540U

Deoth to Water: 5'

Borinq Deoth: 8'

Borinq Dia.: 2"

Paqe: I of I

Page 96: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

BgiggE Temporary M-B Acceptance Facility Borinq: M8F-42

Location: New Haven Rail Yard Insoector: C. Criscuolo

g!ig! Maguire Group Inc. Date: 3-26-07

r l l

i oLoqical Environmental Solutions

354 South River RoadTolland, CT 06084

fruck, Potable & ATvlBackhoe-Mounted GeoprctEs

E t oo o

E

tt,

DescriptioncL olo d t O C L

o - =

Sample Interval

Ground Surface 0.0

1 .0 -

2.O-

3.0-

: ;q: i :qr j i :q:

::o. :;::". j; i:o. I

::(:l :{i :.::4:

"4:i:4i;.::d,'

ASPHALT U.J

0 .1 Macro Core 0'-2'Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

ii:d:l:a:i.i:

i.l: r :|:ii :i-! .

: :q: i : ' . : ; r i : ' . : i

::q:a;q:i:.::q:i

r:q:it:i;::q:i

::'. ij trir :i:o::i

r:q:i:q:i:i:q:i

;:'l:i:". :i :i:q:i

::q,i::q:i jr:i

r:c.:;i:o.:ii:;r:ii.qlii:.b:ii :i-!1

:q:i::{:ij :;:q:i

BIacK ASH & CINDERS

Groundwater at 5'c.u

8.0

3.5 Macro Core 2'-4'

2.2 Macro Core 4'-6'

0.2 Macro Core 6'-8'

9.0-

10.0-

1 1 . 0 -

12.0-

End of Boring at 8'

Groundwater Grab Sample Collected

Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-10%

Driller: W. Lineberry

B!g: Geoprone 54oU

Depth to Water: 5

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: { of I

Page 97: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOG I

O( t l

Logical Environmental Solutions354 South River Road

Tolland, CT 06084T I u c ?' P orlEb I e & ATU/Bac kh oe- M o u nted G eo p rc be s

Elgigg!: Temporary M-8 Acceptance Facility

!994t!9!! New Haven Rail Yard

Client: Maguire Group Inc.

Borino: M8F43

Inspector: C. Criscuolo

Date:3-26-07

E 6o o

o

Description E 6o o 6 a

Sample Interval

Ground Surface 0.0

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

2.0

0 Macro Core 0 -2'

Black ASH & CINDERS

Groundwater at 5'5.0

0 Macro Core 2'-4'

0 Macro Core 4'-6'

8.0

0 Macro Core 6'-8'

9.0-

10.0-

12,0-

End of Boring at 8'

Soil Description: and = 35-50% some = 20.35% little = 10-20% trace = l-'10%

Driller: W. Lineberry

B!$, ceoprone 540U

Deoth to Water: 5'

Borinq Depth: 8'

Borina Dia.: 2"

egE 1of 1

Page 98: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

glgi9g! Temporary M-g Acceptance Facility

!9ga!!9!: New Haven Rail Yard

Client: Maguire Group Inc.

Borinq: M8F.44

Inspector: C. Criscuolo

Date: 3-26-07

r ^ .

i o( J I

Logical Environmental Solutions354 South River Road

Tolland. CT 06084Truck, Porlable & ATv/Backhoe-Mounted Geoprcbes

E 6o oo g

oE

@

Description E aE g o A

Sample Interval

Ground Surface 0.0:q: i :{ i

:".:;:?:i

:q:;r:{:i

:":il:".:ii . l . . : l : i

:q:i:{:i

:q.:;j:?:i

:q:a:q:i

: " . : ; :o . : ;.q-{:q:i

:qi:q:i

i : i : { :

i:,::'::

::l:"::

::.::q:i:i.1.: i :?. ii:i.9.

:i:q::i

:--::q:ii:i.+.a-.:ql:i

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

4.0

0 Macro Core 0'-2'

0 Macro Core 2'-4'

Red-Brown fine SAND & SILT, trace fine Gravel (wet)

8.0

0 Macro Core 4'-6'

0 Macro Core 6 -8'

9.0

10.0

1 1 . 0

12 .0

End of Boring at 8'

Soil Description: and = 35-50% som6 = 20-35% little = 10-20% trace = 1-10%

Driller: W. Lineberry

Bj&, Geoprone 540U

Deoth to Water: 4'

Borino Deoth; 8'

Borino Dia.: 2"

Paqe: 1 of 1

Page 99: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

| -il

i of r t

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Podable & ATvlBackhoe-Mounted Geoprcbes

Proiect: Temporary M-8 Acceptance Facility

@3!9![ New Haven Rail Yard

Client Maguire Group Inc.

&!iE&. M8F-4s

Inspector: C. Criscuolo

@.3-19-07

€.ao oo g .A

Description 6.6It, oo g

o ao - 5

Sample Interval

Ground Surface 0.0

'1 .0-

2.O-

3.0-

4.0-

5.0-

o .u -

7 .0-

:ol; :D_ :;,r :i:ol:

'.n1.41i .: ..1

:'. :i t:i :; t:

:q:; .q:a:;:q:

:q: i :q: i : . : :q:

Dark-Brown to Black fine to coarse SAND, little Ash & Cinders,trace Concrete, Brick & fine to coarse Gravel (FILL)

2.O

1 .0 Macro Core 0'-2'

Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

Groundwater at 5'5.0

3 . 1 Macro Core 2'-4'

4 . 5 Macro Core 4'-6':".:;::o.:;- i;q.i

:q: i : { . j j ;q i

'9i .s :4 .: tz'.i

r:q:i:q:a:i:q:i;:q:;r :r. :i.: :l :r. :i

: :q : ; i :o . : i r : i :o . :

8.0

0.9 Macro Core 6'-8'

9.0-

10.0-

11.0-

12.O-

End of Boring at 8'

Soil Description: and = 35-50o/o some = 20-350/. little = 10-20% trace = 1-10%

gfi!!er: W. Lineberry

8!gj Geoprone 540u

Deoth to Water: 5'

Borinq Depth: 8'

Borinq Dia.: 2"

Paoe: I of I

Page 100: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Elgigq[ Temporary M-8 Acceptance Facility

!9!g!94j New Haven Rail Yard

q!!gq! Maguire croup Inc.

Borinq: M8F.46

Inspector: C. Criscuolo

Date: 3.19-07

GEOPROBE SOIL BORING LOG

Soil Description: and = 35-50% some = 20-35%

r ^ .

i o( t rLoqical Environmental Solutions

354 South River RoadTolland. CT 06084

fruck, Poftable & ATvlAeckhoe-Mounbd Geoqrobes

cL olo d ,

o

o

Description!t 9l o a

Sample Interval

Ground Surface 0.0

1 .0 -

2.0^

3.0-

4.0-

5.0-

6.0-

7 .Q-

Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete, Brick & fine to coarse Gravel (FILL)

2.0

0 .3 Macro Core 0'-2'

Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel {FILL}

Groundwater at 5'J .U

0.9 Macro Core 2'-4'

o.2 Macro Core 4'-6'

8.0

o.2 Macro Core 6'-8'

9.0-

10.0-

11.0-

End of Boring at 8'

little = 10-20% trace = 1-10%

Driller: W. Lineberry

8iS Geoprone 54DU

Depth to Water: 5'

Borlno Degth: I'

Borino Dia.: 2"

Paqo: 1 of 1

Page 101: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

&igq!: Temporary M-8 Acceptance Facillty Borinq: MgF47

!9e!!!9!j New Haven Rail Yard hsElq, C. Criscuolo

Client: Maguire Group Inc. Date:3-19-07

I

l o( t l

Loqical Environmental Solut ions354 South River Road

Tolland, CT 06084f ruck, Porta e & ATvl8ackhoe-ll ounted Geoptube$

=aarl, oo g

co

Description E to oo g

o 6 .o - =

Sample Interval

Ground Surface 0.0

, t n-

4.O-

5.0-

6.0-

Dark-Brown to Black fine to coarse SAND. little Ash & Cinders,trace Concrete, Brick & fine to coarse Gravel (FILL)

2.0

1 . 2 Macro Core 0'-2'

Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

Groundwater at 5'5.0

Macro Core 2'-4'

0.9 Macro Core 4'-6'

8.0

0.4 Macro Core 6'-8'

9,0-

10.0-

1 1 .0 -

12.0-

End of Boring at I'

Soil Description: and = 35-50o/o some = 20-35o/o little = 10-20% trace = l-10'/"

Driller: W. Lin€berry

&, Geoprone gou

Dsoth to Water: 5'

Borinq Depth: 8'

Borinq Dia.: 2"

Paoe: 1 of 1

Page 102: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGrei$! Temporary M-g Acceptance Facitity Borinq: M8F-48

lgggl.iglt New Haven Rail Yard hspgglg! C. Criscuoto

g!g!! Maguire Group Inc. Date:3-26-07

t l

i of l r

Logical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Ponable & Afv/Backhoe-Mounted Geoprcbes

Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)

Red-Brown fine SAND & SILT, trace fine Gravel (wet)

4.0

0

0

0

0

Macro Core 0 -2'

Macro Core 2'-4'

Macro Core 4'-6'

Macro Core 6'-8'

End of Boring at 8'

p!i!!q' w. Lineberry

!!91 Geoprone 540U

Depth to Water: 4'

EI!s-g€&8'

Borino Dia.: 2"

egge:. 'l of 1

Page 103: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility

Location; New Haven Rail Yard

Client Maguire Group Inc.

Borinq: MeF.49

Inspector: C. Criscuolo

Date: 3-15-07

r ^ .

i oq t l

Logical Environmental Solutions354 South River Road

Tolland. CT 06084fruck, P oftable & ATvlBeckhoe-tlou nted Geoqobes

E 6o oo g 6

Description E 6o oo g

o Eo - =

Sample Interval

Ground Surface 0 0

'1 .0-

3.0-

4.0-

5.0-

6.0-

7.0-

Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)

1 . 50 .1 Macro Core 0'-2'

ro'Ji.s .:'-:- .s.F:i).t':6 1; .?..t.sl .--ASl

.f '";"..f: v f t . 1 . t

E: . - - ; - . i l

,ts'i;-.f' u

f t t rs :; sls.ir--F', tr 9; .?, t.lt . -.;l -g

.n.".;-.E'r6'ft ?;t

..f .-1r-.F:el ; '?r t

F,.;i' ;1 9* .?: t

Red-Brown fine to coarse SAND. trace Silt

Groundwater at 4'4.Q

0.4 Macro Core 2'-4'

8.0

0.1 Macro Core 4 -6'

0 Macro Core 6'-8'

9.0-

10.0-

'1 1.0-

12.0-

End of Boring at 8'

Soil Description: and = 35-500/" some = 20-35% liftle = 10-200/" trace = l-10%

Driller: W. Lineberry

Big: Geoprone 540U

Depth to Water: 4'

Borinq Deoth: 8'

Borinq Dia.: 2"

gqg.l of 1

Page 104: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

!g9l9g[ Temporary M.8 Acceptance Facitity

Location; New Haven Rail yard

Client Maguire Group Inc.

Borinq: M8F-50

Insp€ctor: C. Criscuolo

@,3-1s-07

GEOPROBE SOIL BORING LOG

$eil Description: and = 35.500/" some = 20-35%

I

l of r i

Logical Environmental Solutions354 South River Road

Tolland, CT 06084fruck, Ponable & ATvlBackhoe-Mountoct ceoprcbes

r f 0 'o o

o

c

oDescription * a

o o o ao - . =

Sample Interval

Ground Surface 0.0

1 .0 -

2.0-

3.0-

J . U _

6.0-

7.O-

Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)

t . J

0 Macro Core 0 -2'

.:o l;- r,-.i

$,i.'*f .69ot ) t. s : . - : : - s :-F:"*r"..#f .6 9o . f , t, S : . - . ; : S :

.r.t'.r1,6 l ; .?, t

$,i"'}l, tr 9; .?, t

$',vo$'16 9n f: t

;";o'}f .6 9o .?, ta : . - : . $ :.f ::r**ff ,6 ?; 1?, ts : . : - : - s :

Red-Brown tine to coarse SAND, trace Silt & fine Gravel

Groundwater at 4'4.0

Macro Core 2 -4'

8.0

Macro Core 4 -6'

0 Macro Core 6'-8'

9.0-

10.0-

1 '1 .0 -

12 .0 -

End of Boring at 8'

Groundwater Grab Sample Collected

l i t t le = 10-20% trace =1-1070

Driller: W. Lineborry

8!gj Geoprone 540U

Deoth to Water: 4'

Borino Depth: I'

Borino Dia.: 2"

EAgg. 1 of 1

Page 105: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

elgiggl[ Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

glgllE Maguire Group Inc.

Borinq: M8F-51

lnsoector: C. Criscuolo

Date:3-15-07

t ^

i oU I

Loqical Environmental Solut ions354 South River Road

Tolland, CT 06084T I uc k, P o da b I e & A f VlB a c P,ho.- M ou n Ed G eo p rcbe s

c L oo o

o

E

.t>

Descriotion -oEo o o a

- o

Sample lnterval

Ground Surface 0 0r:ii''::i:ii:::i;i::q.:;:'. iji:o.:i

r:q:a:q:i:.::q:i

r:q:;:o.:i::.::q:;

Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)

1 . 50 Macro Core 0L2'

1;6 9; .l i

$,";.}' ,0 9; .2, t

F,";&:o-9e .?.!.i:j*lao.lu .'.!

e1J'51re lo 'l;t

,F,.;i1:6 9* .l: t

.e:1).ts1 '6?; l : t$,vo.}l . n9 f t : f : i. s : . : - l s

Red-Brown fine to coarse SAND. trace Silt & fine Gravel

Groundwater at 4'4,0

0 Macro Core 2L4'

8.0

0 Macro Core 4 -6'

0 Macro Core 6'-8'

9.0

10.0

1 1 .0

12.0

End of Boring at 8'

Soit Description: and = 35-50% some = 20-35o/o little = 10-20% trace = t'10%

Dri er: W. Llneberry

E!$. Geoprone 540U

Depth to water: 4'

Borinq Depth: 8'

Borina Dia.: 2"

eegg, 1 of I

Page 106: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Proiect: Temporary M-8 Acceptance Facility Borinq: M8F-52

Location: New Haven Rail Yard Inspector: C. Criscuolo

Client: Maguire Group Inc. Date:3-26-07

I

i oLoqical Environmental Solutions

354 South River RoadTolland, CT 06084

Truck. Podable & AfvEackho*Mounted Geoyobes

-o to 6 )a g

ocU>

Description = :o ( | lo g

a EA =

Sample lnterval

Ground Surface 0.0

t . u -

2.0-

3.0-

4.0-

c .u-

6.0-

7.0-

:q: i :qr i : ; :q:

:". ; :'. :;: i :q. :i!:t,!14:i !:

:cf :{: i i :4,: " : i : r : i " :q l :

Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)

1 . 50

0

Macro Core 0'-2'

', tr ?; .1, t:

$"J$..Y:.Q;'ols:1;-*f' 6 f t . 1 1 ts. ' -- .$.f :1-".f1:6 9o .?; r

*f :";-.fl, tl ?o .?, t

$,";o$1:e 9; ' l : is : , : - s..f -L-.rt . - q . . t , ,' t

f l . 1 : rs : . : r t s :.P.".''r--.ff, tr 9o .1, t. S ;

- . : S :

Red-Brown fine to coarse SAND, trace Silt & fine Gravel

Groundwater at 4'4.0

Macro Core 2'-4'

8.0

0

0

Macro Core 4L6'

Macro Core 6'-8'

9.0-

10.0-

11 .0 -

12.0-

End of Boring at 8'

Soil Description: and = 35-500/" some = 20-35% Iiftle = 10-20olo trace - l-10%

Driller: W. Lineberry

8!q: Geoprone 540U

Depth to Water: 4'

EgEls_EcElh:8'

Borinq Dia.: 2"

Paqe: 1 of I

Page 107: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

elgigg! Temporary M-8 Acceptance Facility

Location: New Haven Rail Yard

9lgl! Maguire croup Inc.

g!49. M8F-53

Inspector: C. Criscuolo

Oate: 3-26-07

| -/l

i o\ t l

Loqical Environmental Solutions354 South River Road

Tolland, CT 06084Truck, Portable 4 AfvlBackhoe-Mounted Georobes

E 6{ r o

o

oDescription E : i

o oo =

o a Sample lnterval

Ground Surface 0.0

:9.:;_:F.:i.::j:o.

:L:i':.c:i -:.{

Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)

1 . 50 Macro Core 0'-2'

t . : d : . t ;I u . t t . 1 1s . : r s :

.F j:j".F

i r n l f t : ? . i

$+.}lr o.lft :?r t

Fe;i , o . ) . .I u._ft .1: 1

S"ri' ' u - f l . - as l . : l $ ..f :'.r"..fi - a . ) ,' t v f t . 1 : ts : . - : : - s :.f :j".Fljo li :?: r' E t . . - ! . S l

.r",.}.Fi , o l ; ' ? , t.s: . ' . - -s:

Red-Brown fine to coarse SAND, trace Silt & fine Gravel

Groundwater al 4'4.0

0 Macro Core 2'-4'

8.0

0 Macro Core 4'-6'

0 Macro Core 6'-8'

9.0-

10.0-

I L U -

12.0-

End of Boring at 8'

Soil D$criotion: and = 35-50o/o some = 20-35% little = 10-20% trace = l-10%

Driller: W. Lineberry

Ei$ ceoprone 540U

gsP![!@4'

Borinq Depth: 8'

Borinq Dia.: 2"

Paqe: 1 of I

Page 108: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

APPENDIX BTables from MGI's2005 Interim Shop

(Running Repair Shop)Task 210 Investigation

Page 109: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

MGI's 2005 Task 210 InYestigationTABLE 1(a) - Results of Geoprobe Boring Soil Sample Analyses

New Haven Rail Yrrd Interim ShopNew Htven, Conn€cticut

Boring LD.:

Sample Depth:

GPIS.3 GPIS4 GPIS-5

2' ,4 '

GPIS.6 CTDEP PMC GBGroundwaier

Area

CTDEP DEC ResidentiaVCommercial & lndustrial

CT ETPH - (ppm) t75 168 BRL 68.8 2.500 ppm 500/2.500 ppmVOCs - Method 8260 (ppm) BRL BRL BRL BRLBNs - Method 8270 (ppm)

Acenaphthene

Acenaphthylene

Anthmcene

Benzo(a)anthracene

Benzo(a)pyrene

B enzo(b) fluoranthene

Benzo(k)fluorantbene

Benzo(g,h,i)perylene

Dibenz(a,h)anthracene

Dibenzofuran

Chrysene

Fluoranthene

Fluorene

Indeno( 1,2,3-cd)plrene

2-Methylnaphthalene

Naphthalene

Phenanthrene

Pyrene

Total BNs

BRL0 . 1 80.3460.6370.5 750 . 5 7 l0.5250.3650.672BRLBRLt.72BRL0.292o.212BRL0.952o.8't47.921

BRLBRLBRL0.4220.3970.5330_3610.2850.558BRLBRL0.786BRL0.2510.399BRL0.6770.6075.276

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRL0.3 260.53L051.071.2 7

0 . 7 t 20,695BRLBRL1.132.85BRL0.6'12BRLBRLt.251.97

l3_525

84 ppm84 ppm

400 ppml ppmI Ppo'I pprnI ppm

42 ppmI ppm

5-6 ppmI ppm56 ppm56 ppmI ppm

9.8 ppm56 ppm40 ppm40 ppm

I,000/2,500 ppm1,000/2,500 ppmI,000/2,500 ppm

1/7.8 ppm

Ul ppm1/7.8 ppm

8.4/78 ppm1,000/2,5ffi ppm

l/l ppm270/2,500 ppm

84/780 ppm1,000i2,500 ppn1,000/2,500 ppm

1/7.8 ppm474/2,500 ppm

I,000/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm

Pesticides - Method 8081 (ppm) BRL BRL BRL BRLPCBs - Method 8082 (ppm) BRL BRL BRL BRL 0.005 ppm li l0 ppmHerbicides - Method 8l5l {ppm) BRL BRL BRL BRLTotal RCRA 8 l{etals ppm

Arsenlc

Bariurn

Cadmium

Chromium

Lead

Mercury

BRL25.81.029;12200BRL

BRL62.62.78 . 7 4tt2

BRL

BRL18.6BRLt t - l

8.5{iBRL

BRL

BRL) _ J O

62.3BRI

l0/10 ppm4,?00/140,000 ppm

34/1,000 ppm100/100 ppm

500i 1,000 ppm201610 ppm

SPLP RCIRA 8 Metals - ppmBariumLead

0.0248BRL

BRL0.0224

BRLBRL

BRLBRL

10.0 ppm0.15 ppm

BRL Below Reporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.

Page 110: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

MGI's 2005 Task 210 Inv€stigationTABLE l(b) - R€sults ofGeoprobe Boring Soil Sample Analy$es

New Haven Rail Yard Interim SbopNew Hav€I|, Conncciicut

Boring I.D.:

Sample Depth:

GPIS.7

4',-8'

GPIS-8

2 '4 '

GPIS.9 GPIS.I O CTDEP PMC GBGroundwaier

Area

CTDEP DEC ResidentiaVCommercial & Industrial

CT ETPH - (ppm) BRL 1,460 1 0 8 t 8 8 2.500 ppm 500i2,500 ppmVOCs - Method 8260 (ppm)

AcetoneTetrachloroethylcne

BRLBRL

0. t440.033

BRLBRI

BRLBRL

140 ppmI ppm

500/1,000 ppmt 2/1 10 ppm

BNs - Method 8270 (ppm)

Acenaphthe neAcenaphthyleneAntfuaceneBenzo(a)anthraceneBerzo(a)pyrcneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(g,h,i)peryleneDibenz(a,h)anthraceneDibenzofuranChryseneFluorantheneFluorenelndeno( 1,2,3 -cd)pyrene

2-MethytnaphthaleneNaphthalenePhe nanthrenePlreneTotal BNs

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRL

0.6940.6632.88s.034.1I4.673.212.6?0.53 |0.7884.461 8 . 5

0.5382.261 . 2 7| .07t0.'19.72

73."t t4

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.22BRLBRLBRLBRLBRL0 . 1 6 70.387

BRLBRLBRL0.3660.3660.4440.33o.272BRLBRL0.4440.736BRL0.244BRLBRL0.2920.5444.038

84 ppm84 ppm

400 ppmI ppmI ppmI ppmI ppm42 ppmI ppm

5.6 ppmI ppm56 ppm56 ppmI pp-

9.8 ppm56 ppm40 ppm40 ppm

1,000/2,500 ppm1,000/2,500 ppm1,000i2,500 ppm

1/7.8 ppmUl ppm

l/7.8 ppm8.4/78 ppm

I,000/2,500 ppml/1 ppm

270/2,50O ppm84/780 ppm

I,000/?,500 ppm1,000/2,500 ppm

l/7.8 ppm414/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm1,000i2,500 ppm

Pesticides - Method 8081 (ppm) BRL BRT, BRL BRLPCBs - Method 8082 (ppm)

PCB-1260 BRL 0.0465 BRL 0.0566 0.005 ppm 1/10 ppmHerbicides - Method 8l5l (ppm) BRL BRL BRL BRLTotal RCRA 8 Metals - ppm

ArsenrcBariumCadmiumChromiumLeadMercury

BRL1 3 . 9BRL4.863.96BRI

7 . t lt022.623 1 . 0280l . 5 l

BRLl1.6BRL38.914.2BRL

BRLt9.'r0.5349.343. tiBRL

l0/10 ppm4,700/140,000 ppm

34/1,000 ppm100/100 ppm

500/1,000 ppm20/610 ppm

SPLP RCRA 8 Metals - ppmBariumChromiumLead

BRLBRLBRL

0.0726BRLBRL

BRL0.0 r06BRL

BRL0.0090.0078

10.0 ppm0.5 ppm0.15 ppm

BRL Below Reporting Limits (see laboratory reports for compound specific detectian limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.

Page 111: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

NIGI's 2005 Task 210 InvestigationTABLE 1(c) - Results of G€oprobe Boring Soil Sample Analyses

New Haven Rail Yard Interim ShopNew Haven, Connecticut

Boring I.D.:

Sample Depth:

GPIS-I 1

2 ' -4 '

GPIS.12

2'4',

GPIS. I3

4 ' -8 '

GPIS.15

7',4',

CTDEP PMC GBGroundwater

Area

CTDEP DEC ResidentiaVCommercial & Industrial

CT ETPH - (ppm) 1,120 r,670 1,070 330 2,500 ppm 500/2,500 ppmvocs - Method 8260 (ppm)

Acetone

Tetnchloroethylene0 .1260.0376

BRL0.0143

BRL

BRL

tsRLBRL

140 ppmI pPm

500/l,000 ppml2i I l0 ppm

BNs - Method 8270 (ppm)

Acenaphthylene

Anthmcen€

Benzo(a)anthracene

Ben2o{a)p}rene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(g,h,i)perylenc

Chryscne

Dibenz(a,h)antkacene

Fluoranthenc

2-Methylnaphthalene

Naphthalene

Phenanthrenc

Pl,rene

Total BNs

0.3 9BRL0_359BRT-0.394BRLBRL0.541BRL0.6431.05

0.8790 . 8 1 20.4645.532

BRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLtsRLBRLBRLBRLBRLBRLo.542BRL0.4910.97',7BRL0.8

0_4521.262

0.920.8572.2

t . / J

1.470 . 3 1 9

6.991.290.33) L 1

4.4829.866

84 ppm

400 ppmI ppmI ppm

I ppmI ppm

47 ppmI ppmI ppm

56 ppm9.8 ppm56 ppm40 ppm40 ppm

1,000/2,500 ppm1,000/2,500 ppm

l/7.8 ppml/l ppm

l / 7 R n n m

8.4i78 ppm1,000/2,500 ppm

84/780 ppm

l/l ppm1,000/2,500 ppm47412,500 ppm1,000/2,500 ppm1,000/2,500 ppmI,000/2,500 ppm

Pesticides - Method 8081 (ppm) BRL BRL BRL BRLPCBs - Method 808? (ppm)

PCB-1260 1.21 BRL BRL 0.005 ppm 1/10 ppmHerbicides - Method 8 t5l (pprn) BRL BRL BRL BRLTotal RCRA 8 Metals - ppm

Ars€nlcBariumCadmiumChromiumLeadMercury

BRL1722 . 3

21 .02581.03

BRL52.2

0.8029.0349.1BRL

8.8 880.10.75845.lJ3542.32

BRL64.3l . t 46.7 |t36

0.295

l0/10 ppm4,700/140,000 ppm

34/1,000 ppm100/100 ppm

500/l,000 ppm201610 ppm

SPLP RCRA 8 Metals - ppmBariumChromiumLead

0 . t l 9BRLBRL

0.0234BRI,BRL

0.0160.007t0.026

0.019BRLBRL

10.0 ppm0.5 ppm0.15 ppm

BRL - Below Reporting Limits (see laboratory reports for compound specific detection limits)

The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific dctection limits.

Page 112: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

MGI's 2005 Task 210 Investigation'IABLE l(d) - Rcsults ofGeoprobe Boring Soil Sample Analyses

Nerv Haven Rail Yard Interim ShopNew IIaven, Connectlcut

Boring LD.:

Sample Depth:

GPIS-18 CTDEP PMC GBGroundwater

Area

CTDEP DEC ResidentiaYCommercial & Industrial

CT ETPH - (ppm) 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm)

Tetrachloroethylene 0.0367 t ppm l2l I l0 ppmBNs - Method 8270 (ppm)

AcenaphthencAcenaphthyleneAnthraccncBenzo(a)anthraceneBenzo(a)pyreneBeuo(b)fluorantheneBenzo(k)fluorantheneBe nzo(g,h,i)peryleneDibenz(a,h)anthraceneDibenzofuranChryseneFluorantheneFluorenelndeno( 1,2.3-cd)pyrene2-MethylnaphthaleneNaphthalenePhenanthrcnePlreneTotal BNs

0.3 392.412.536.3 36.165.764.923.49

0.9820.8466.061 6 . 8| _021.140.737t.0'79.1 '7t 0 .6

82.164

84 ppm84 ppm

400 ppmI ppmI ppml ppmI ppm

4? ppmI PP-

5.6 ppmI ppm56 ppm56 ppmI ppm

9.8 ppm56 ppm40 ppm40 ppm

1,000/2,500 ppmI,000/2,500 ppm1,000/2,500 ppm

l/7.8 ppml/l ppm

1/7.ti ppmIt.4/7li ppm

I,000/2,500 ppml/l ppm

27012,5O0 ppm84/780 ppm

1,000/2,500 ppm1,000/2,500 ppm

l/7.1t ppm47412,500 ppm1,000/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm

Pesticides - Method 8081 (ppm) BRLPCBs Method 8082 (ppm) BRI 0.005 ppm l/10 ppmHerbicides - Method li l 5 ! (ppm) BRL

Toral RCR{ 8 Metals - ppmAIsenlcBariumCadmiumChromiumLeadMercury

10.61 7 8

34.41,3400.949

l0ll0 ppm4,700/140,000 ppm

34/1,000 ppm100/100 ppm

500/1,000 ppm201610 ppm

SPLP RCRA 8 Mctals - ppmBariumChromium[,ead

0.04160,01

0.0785

10.0 ppm0.5 ppm0.15 ppm

BRL Below Reporting Limits (see laboratory r€ports for compound specihc detection limits)

The compounds listed above are those that were detected - please s€e laboratory reports for full lists ofcomoounds and their soecihc detection limits.

Page 113: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TASK 210:SUBSURFACE SITE INVESTIGATION

New Haven Rail YardTemporary M-8 Acceptance Facility

New Haven, Connecticut

Volume 2

ConnDOT Assignment No. 202-3464ConnDOT Project No. 301-88

Prepared for:

@State of ConnecticutDepartment of TransportationNewington, Connecticut 06131

Prepared by:

IilRiliEGnouf

Maguire Group Inc.One Court StreetNew Britain. Connecticut 06051

April24,2OO7

Page 114: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

APPENDIX CSoil Sample

Laboratory Reports

Page 115: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Report Date:2'7 -Mar0'l t1 :35

Logical Environmental Solutions354 South River RoadTolland, CT 06084Attnr Cindy Knight

SPECIRUM ANALYTICAL, INC.f.atarihg

HANIBAL TECHNOLOGY

Laboratory Report

gtrE

Final ReportRe-Issued ReponRevised Report

Project: NHRY M8 Acceptance Facility - New Havel, CT

Project 301-88

Lrboratorv lDsAs9464-01sA59464-02sA59464-03sA59464-04sA594&-05sA594g-06sA594g-07sA5946t-08sA594A-09sA5944r0s45946+l ISA59,16.f-12SA59.164- I lSA59,l&l-14sA594fl- l5SA5946.1-16sA59,r64- t7SA59,164-18SA59,l6,l- I9

Client Sample IDM8F-4 2'-4,M8F-5 2'-4,M8F-6 2',-4'M8F-12 2,4'M8F-11 2,4'M8F-49 2'-1'M8f-50 2'4'M8f-5I 2'4'M8FB.1MSFB-2MTFB-3MSFB-1M8FB-5M8FB-6MSFT-IMSFT-2FB-ITB-IM8F-50CW

Matdx

SoilSoilSoi lSoi lSoilSoilSoilSoi l

BallastBallastBallastBallastBallastBallastWoodWood

Blank WaterBlank Water

Ground Water

Date Ssmpledl5-Mar-07 0D:00l5-Mar-07 00r00| 5-Mar-07 00r00l5-Mar-07 00:00l5-Mar-07 00:00l5-Mar-07 t)0:00l5-Mar-07 00r00l5-Mar-07 00r00l5-Mar-07 00:00l5-Mar-07 00r00l5-Mar-0r 00r0015-Mar-07 00r0015-Mar-07 00:00l5-Mar-07 00:00l5-Mar-07 00:0015-Mar{7 00r0015-Mar-07 00r00l5-Mar-07 00:0015-Mar-07 00:00

Drte R€celv€d

l9-Mar-07 l-5;33l9-Mar-07 15:3319-Mar-07 l5:3319-Mar-07 lJ;3319-Mar-07 l5:1319-Mar-07 l5:33l9-Mar-07 l5:33l9-Mar-07 l5:ll19-Mar-07 15:3319-Mar-07 l5:13l9-Mar-07 15:33l9-Mar-07 15:33l9-Mar-07 l5:33l9-Mar-07 15:3319 Mar-07 15:33l9-Mar-07 15:33l9-Mar-07 15:31l9-Mar-07 15:33l9-Mar-07 15:31

Headgud e^: 11 Almgen[)live & E10 Silv€r Str€€1. Aga\esm, MA 0100t . t-800-?89-91l5.4lt-789-90lE. FAX 4t3-.t9-40j6fl, Divnidz:8180 Wedland Cstq Bouldard. TatIpd, FL 33614. l-E8E49?,52?0. Elt EEt,9io7. FIX 800-4t0 643i

www-spectrum.analylical.com Pag€ I of 152

Page 116: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

I atest f|at the ilfo.rnatioD contaioed within the report bas been reviewed for accuracy and checked ogaitrst the quality conholrequirements for each merhod. Thes€ results rclale only to thc sample(s) as rcceivedAll applicable NELAC .equirements have beetr m€LPleas€ oote that this nepoft contalns 152 pages of analytical data plus ChaiD of Custody documen(s).This repon may not be reproduced, except in full, withour written approval from SpecFum Analytical, Inc-

Massachus€tts Certifi cition #Coorccticut # PH4777Flo'ida # E8'76(Jf,n87 936MriDe # MA138New Hampshire # 2538/2972New Jersey # MAol I A{A012New York # 11393/11840Rio& tsland # 98usDA # s-51435VerEotrt # VT-l l39l

M-MAt38MAt I l0 Authorized by:

nfrd-Hanibal C. Tayeh, Ph.D.President/l^aboratory Director

Technical Reviewels Initial:

Spectrnn Analyticdl, Inc. it o NELAC accredited laboralory or4anization and meets NELIC tellting sr.rndflrb. Use of the NELIICloSo howewr does not ittsure that Spe.lrum rs cunently accrcdiledfor the sryilc method or anal@ indicated. PteaEe refer lo our"QualiE web page at www.spectrnmaralytical.confor alu tisting ofour current ceftirtca ons andJields ofat:creditation. Statet inwhich Spechm Anolytical, Inc. holds NELAC cerlifrcation are New york, New Hampshire, New Jersqt and Floida. Alt anatytiea!worklol Yoldlile Orgdnic and Air analysis ue lrarsfefted lo and con&rcted at our 830 Silver Srreet tocation NH-2g72. Ny-l1840.FL-E879 3 6 and NJ - MA1 I 2).

ThB ,abonatry Epor, is aot polful ui aal ad azrtodzd stg.raatre o" thz coter psse.

. Reportiblc Dsr.ction Limit BRL = Below R€pniing Linit Ptg.2of 152

Page 117: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Report Date:28-Mar-07 09;55

Logical Environmertal Solutions354 South River RoadTolland, CT 06084Attn: Cindy Knight

SPECTRUM ANALYTICAT-, INC.Fedta,ing

HANIBAL TECHNOLOGY

Laboratory Report

gtrtr

Final ReportRe-Issued ReportRevised Repon

Project: NHRY M8 Acceptance Faciliry - New Haven, CT

Project 301-88

nfrd-Hatribal C. Tayeh, Ph.D.President'I-aboratory Director

Technical Revieweis ILritial:

Speclntm Analyti.al, Ihc. ts a NELAC accredited laboralory organizalion and meets NELAC testing standards- Use ofthe NELAClogo however does not itlsLtre that Spec!rum is currently accreditedfor lhe speclic metlnd or anab,te indicated. pleare rcfer lo our"Qualily" web page at www.spectrun-analytical.comfor afull tisting ofour curren! certifcalionr andfielde oJaccreditatioa. Sl.lres inwhich Spectrum Analyticul, Inc. holds NEL4C certificalion are New Yorh New Hampshire, New Jersey and Florida. All analyticalworklor folatile Otgarlic and Air analysis are trunslefied to ond conducted at our 830 Silvel Strcet location NH-2g72. Ny-l1E40.FL-887936 and NJ-M40 I 2).

Laboratorv ID Client Sample IDsA595t7-01 M8F_124 'sA595l7-02 M8F_2 24'sA595r7-01 M8F-3 24'sA595l7-04 M8F-14 2_4sA595l?-05 M8F-15 +6'sA595l?-06 M8F_26 2-4'sA595r?-07 M8F-12 2-4'sA595t?-08 M8F-40 2_4'sA595l7-09 M8F-41 4_6'sA595l7-t0 M8F-45 4_6'sA595t?-l I M8F46 2_4'sA595 | 7- t2 M8F47 24'sA595l7-ll M8F-14 cWsA595 t 7- l4 FB-2sA595 t?- l5 TB_2

Matrix

SoilSoilSoilSoilSoil

Soi lSoi lSoilSoi lSoi lSoi lSoil

Grouod WaterBlank WaterBlank Water

Date Sampledl9-Mar-07 00:00l9-Mar-07 00:00l9-Mar-07 00:00l9-Mar-07 00:00I9-Mar-0? 00:00l9-Mar-07 00-00t9-Mar-0? 00:00l9-Mar-07 00:00l9-Mar-07 00:00l9-Mar-07 00:00t9-Mar-07 00i00l9-Mar-07 00:00I 9-Mar-07 00:00l9-Mar-0? 00:0019-Mar-0? 00:00

Date Received

20-Mar-O'7 14:4820-M^r-0'l 14:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4;4E20-Mar-07 l4:4820-Mar-07 14:4820-Mar-07 l4:4820-Mar-07 14:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 14:48

I atlest that thc information contaiDcd within the repon has b€en rcviewed fo. accuracy and checked against the quality co rolrequirements for each method- These results relate only to the sampl€(s) as received.All applicable NELAC .equirements have be€n met.Please Dote that this reporr contains 124 pages ofanalytical data prus chain ofcustody document(s).This repon may not be reproduced, except in full, without witten approval from Sp€ctrum Anallrical, Ioc.

Massachusetts Certification # M-MAl3BA{Al I l0 Authoriz€d by:Comecticut # PH-0?77Florida # 8E7600/E8?936Maine # MA 13 8New t{ampshire # 2538/2972New Jersey # MA0l lMAol2New York # I l39l l 1t840Rhode Island # 98usDA # s-51435Vermont # VT-l1393

fltur'q@t4tst ll Alng.€t Drivc & 810 Silv€.Sr@r . Agaearq MA0t00t . l-S0O-789-91t5 .4lj-789-90It . FAX 4Lj ?89 40?brZ Ddridr: E lE0 Woodland Cent€r Boulward . Tamp4 FL 31614 . l-888-497-52t0. 813-888-9507 . FAli E00-4E0 6435

wv,w'3 pectaum-analytical-com Page I of 124

Page 118: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Report Date:29-Mar-07 16:45

Logical Envitonmental Solutions354 South River RoadTolland, CT 06084Attr: Cindy Knight

SPECTRUM ANALYTICAL, INC.F.at!.ing

HANIBAL TECHNOLOGY

Laboralory Report

gutr

Final ReportRe-Issuql ReportRevised R€port

Project: NHRY M8 Acceptance Facility - New Haven, CT

Project 301-88

Laboratorv lDsA5964l-0tsA5964l-02sA5964l-01sAs964l -04sA5964l-0ssA5964r-06sA5964l-07sA5964l-08sA5964l-09sA5964l-10sA5964l-11sA5964l- r2sA5964r-tlsA5964t-t4sA5964 t -15sA5964l- t6sA59d,!l-17sA5964l-18sA5964t-19

Cli€pt Semple (D

M8F-16 2,-4'M8F-17 4'-6,MEF-lE 2,-4,M8F-19 2,4'M8F-20 2'-4'M8F-22 2,4'M8F-23 2,4,MEF-24 2,4,M8F-25 2'4'M8F-27 2'-4,M8F-28 2,-4,M8F-29 2'4'M8F-10 2'-4'M8F-3 t 2'-4'M8F-31 2'-4'M8F-34 4-6'M8F-24 CWFB-:}TB-]

Mrtrix

SoilSoilSoilSoilSoilSoilSoi lSoilSoilSoilSoilSoilSoil

SoilSoi lSoil

Cround WaterBlank WatetBlank Water

Oate Sampled2l-Mar-07 00:002l-Mar-07 00:002l-Mar-07 00-002l-Mar-07 00:002l-Mar-07 00:0021-Mar-{7 00:0021-Mar-07 00:0021-Mar-07 00:002l-Mar-07 00:002l-Mar-07 00:0021-Mar-07 00:002l-Mar-o? 00:0021-Mar-0? 00-0021-Mar-07 00:002l-Mar-0? 00:002l-Mar-07 00:002l-Mar-07 00:002l-Mar{7 00:0021 Mar-07 00:00

DrJc ReceiY(d

22-Mar-07 l5:3 5

22-Mar-07 15i35

22-Mar-07 15r3522-Mar-07 I513522-Mar-07 15r3522-Mar-07 15r3522-Mar01 15135

22-Mar-07 l5:35

22-Mar-07 l5:3522-Mar-07 15r35

22-MaF07 l5:3 5

22-MaF07 l5:35

22-MaF07 15i35

22-MaF07 15i35

22-M^t-07 1513522-Mar-07 15r3522-Ma(07 l5:i522-Mar 07 15:3522-Mar-07 | 5135

Ha.kluutn: tr AlnB.enDrive & 8J0 Silver SrMt. Agawsfl. MA 01001 . I-8On ?E9,91l5 .4ll-789-90tE. FAX 413-789,,1076F, Drysio,:8180 WoodLand Center Borlevard . Tamm" FL136l4. L,EEE 497-5270 .613-888-9507 . FAx Eoo 480-6435

www.EF€ctrumnnalttletl.comPage I of 165

Page 119: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

I attest that the information contained within the report ha' beetr rcviewed for accumcy and checked against the quality colltrolrcquircmeots for each method These r€sults .elate only to the sampl{s) as received,Atl applicable NELAC rcquiremeDts hare been met.Please note tlMt this reporr contaios 165 pages ofana.lytical data plus Chain of Custody documen(s)-This .eport may oot be reproduced, except in full, witho r+Titteo app.oval from Spectrum Anal)4ical, Inc.

Massacbusetts Certificarion # M-MAI38MAI I l0 Aurhorized by:Connectiout # PH-0777Florida # E87600/E87936Maine # MAl38New Hampshire # 2518/2972New Jersey # MAol lMAol2New York # I 1393/ 1 1840Riode Islaod # 98usDA # s-51435Vermodt # VT-I1393

nfrd-HaDibal C. Tayeh, Ph-D.

Presideff/Ilboralory Dir€cior

Technical Revi€wels Initial: .eSIEctn/m Analtlical, Inc. is a NELAC arcrediled laboralory organizatiok and meett NELAIC testing staruh t. IJse of the NELAClogo however daas ̂ ot irLsure thal Epectrufi is canently accredited for the spectlrc method or aaalye indicated- Pleose rckr to our"Sualit!' web page al ww'w.specttlrm-qnallti4al.comlor afull listing ofour cutenl certifications andftelds of@credilarion. States inrihich Spectrum Analytical, Inc. holds NELAC certification are NeN, york New Eampshirc, New Jersey and Florida. Alt anolyticalworkfor Volatile Organic and Ail analysis are trarrilerred to and cohducled at our 830 Sifuer S|eet location (NH-2972, NY-t 1840,FL-E87 9 j6 and NJ- MA| I 2).

Thk loboftlory Eport b ,rot talU withotd aE aslhotigll sigaoure ot, the cove'. pag..

' R€pottabl€ f,)etectioo Limi. BRL = Below R€portine Limit Page 2 of 165

Page 120: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Report Date:04-Apr-07 13:06

Logical Environmenhl Solutions354 South River RoadTotland, CT 06084Attnr Cindy Knight

SPECTR(IM ANALYTICAL, INC.Fealu,ilg

HANIBAL TECHNOLOCY

Laboratory Report

gtrtr

Fin:rl ReporiRe-lssued ReportRevised Rcport

Project NHRY M8 Acceptance Facility - New Ilaven, QT

Project 301-88

Laboratorv lDsAs980l-01s459803-02sA59803-03sA59803-04sA59803-05sA59803-06sA59803-07sA59803-08sA5980l-09sA5980l-10sA5980l-l IsA59803-t2sA59803-tlsA59803-14sA59803- l5s459803- t6sA59803-17sA59803-t8s459803-t9sA59803-20

Client Srmple lDM8F-7 2,-4'M8F-8 2'4'M8F-9 2'-4'M8F-10 2'-4'M8F-l t 2'-4,M8F-21 2'-4'MEF-35 2,-4'MEF-36 4,-6,M8F-37 2,4,M8F-38 2,-4'|\f8F-J9 2-4,M8F42 2'4'M8F-43 2,-4'M8F-44 2,4,M8F48 2,-4,M8F-52 2,-4,M8F-53 2,-4,M8F-.{2 cwFB-4TB4

Metrix

SoilSoilSoilSoi lSoiLSoilSoiLSoiLSoilSoilSoilSoilSoiISoi lSoi lSoi lSoi l

Groutrd WaterBlank WaterBlank Water

Date Sampl€d26-Mar-07 00:0)?6-Mar-07 00:0t)26-Mar-07 00:0026-Mar-0? 00:l}l26-Mar-0? 00:0026-Mar-07 00:0026-h{ar-07 00:0026-Mar{7 00:0026-Mar-07 00:0026-Mar-07 00i0026-N4ar-0? 00:0026-Mar-07 00:0026-Ma.-07 00:002GMar-07 00:0026-Mar-07 00:0026-Mar-07 00:0026-Mar-0? 00:0026 Mar-07 00:0026 Mar-07 00:0026-Mar-0? 00:00

Date Received

27-Mar-07 l2:502'1 -M^r-O1 12-502'1 -M^t-O'7 12:5027 -Mar-O7 12:5027-M^t-07 12.502'1-Mar-07 12.5027 -M^t-07 12.502'l -M^t-07 12.502'l-Mar-l1 12:50

2'l-Mar-I1 12:502?-Mar-07 12:5027-Mar-07 1?:502'7-Mat17 l):502'7 -Mar-07 12:502?-Mar-07 l2:50

2?-Mar-07 l2:5027-Mar-07 l?:502?-Mar-07 l?:5027-Mar-07 l?:5027-Mar-07 I2:50

HaadquaFte.s: ll Alngrcn Dtirc & Elo silvdsf.€et. Agavam, MA 01001 , I,Eoo-7E9 9l 15,4ll-789-9018 . FA-Y 4t]-78940?6F, Divjsid': 8180 Wmdl t Ccnre. Boulevard . Tanpa, FL 316 t 4 . t -E8B-497,5?70 . E ll-E88-9jo? . FAX 800-480{415

www.spectaum-analytical.comPage I of 154

Page 121: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

I attest that tbe itrformation cortiined within the repoft has been reviewed for accuracy aDd checked against the quality controlrequirements for each method. Thes€ results relate only to tte sam!,le(s) as receivd.All applicable NELAC requiremenas have beetr met_Please Dote that this report cofltains 154 pages ofsDalyticnl data plus Chain ofcustody documeEt(s)-This repon may not be reFoduce4 except in full, witbout writtei approval from Speotrum Analytical, ltrc.

Massachusetts Certiftca.ion # M-MAllt/MAl I t0 Authorized by:Couecticut # PH4777Ilorida # E87600iE87936Maine # MAl38New Hampshire # 2538/29?2New J€rs€y # MAol l/MAol2New York # I t39l/t 1840Rhode lsland # 98usDA # s-51415V€rmont # VT-l1393 &

-ffi a^d-Hanibal C. Tay€h, Ph.D,PresideEt/Laboratory Direator

Technical Reviewedr ltritiali

speclrum Analytical, Inc- Lg a NELAC rrccredited laboratory organi rtion and meers NELAC tesling standards. IJse ofthe NELACIogo however daes not insurc lhat Spectrum is cuftehtly occrelited for lhe specific method or otallte indicdeA. Please eJer to our"Quality" web page at www.spechlm-atu ylical.con Jor alutl listing of otr cunent certilcatione atd felds oJ aecredianion. Sta/€s inwhich SPeartufi Analytical Inc. holds NELIC certijcation are New York, Nei' Hampshirc, New Jersqt and Florida. All analyticalu,orkfor Volatile Organic and Air dnalysis are translened lo and coflducted at our 830 Silver S\eet locarion (NH-2972, Ny-|1840,FI- 88 79 3 6 a nd NJ- MA0 l 2 ) -

Ihb lsbordaA ryort b not eaM l,|a6otd tn a4tlur.iael siptntre on ,hc caver pge.

' RQortable Detection Limit BRL = Belo* Reponing Limil Pag€ 2 of 154

Page 122: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdenrificationMtF-l 2-4'

sA59517 0 l

Client Proiect #301 -88

Collection Date/Timel9-Mar-07 00:00

MatrixSoil

Received20-Mar-07

CAS No. Anslyte(s) Flag Ania 'RDL Dilu.ion Method R4 PEparcd A aryzed Borch Analptvolalil€ Org.nic Colhpornds

VOC Exkaclion Field extracted

PS/kS dry 6 5

PS/kg dry 130

!s/kg dry 6-5

PStkSdry 6-5

!S/ko dry 6-5

Pg/kg dry 6 5

LIVkS dry 6.5

!s/ks dry 6.5

lSftS dry 13 0

Ugks dry 6{ 8

lrdkgdry 6.5

Ug/kg dry 6.5

Pg/kg dry 6.5

Pg/kg dry 32.4

ldkq dry 6.5

rc/tS dry 6_5

Ugkq dry 13.0u€/kS dry 6 5

ldkS dry 13.0

ug/kS dry 6.5

US/kg dry 6.5ps/rg dry 13.0

udkS dry 6.5p94q dry 6.5

IjSAS dry 6.5pdkS dry 6 5pdkg dry 6.5

!S/kS dry 6.5

!S/kS dry 13 0

!g/kg dry 6 5

LiS/kg dry 6.5

!S/kg dry 6-5

!g/kg dry 6.5

Pdkg dry 6.5

l./sfts dry 6.5

US/kg dry 6.5

Pgks dry 6.5pg/kg dry 6.5

!g/kg dry 6.5

t4fts dry 6.5

t'g/kq dry 6.5

t'dks dry 6 5

ttSilq dry 64.8

t S/kS dry 6.5

ldkS dry 65

lsl(gdry 6.5pgkS dry 64.8

UdkS d.y 64.6

Isfts dry 6.5

21'[r€r07 21-ft4ar 07 7031261 BDVolatile Ofoanic Compounds

P.epared by method SW846 5035A Soit (tow tevet)

76-13-1 1,1,2-Tdchtorohfluoroethane(FreoBRL67'64-1 '@tone BRL107,13-1 Acrylon(rile BRL714-2 Benzene BRL108{€-1 Bromobenzene BRL74-97-s Bromochlommethane BRL15-214 Bromodichtoromelhane BRLT5-2+2 Bromolorm BRL74-€39 Bromomethane BRL78-sg3 2-Butanone (MEK) BRL1o4-5J+ n-Eutylb€rEene 8RL135-98{ sec-Eutylbenz€ne SRL98{c6 ten-Butylbenzene BRL75-15-0 Carbon disllfide BRL56'23-5 Carbon teEachtoride BRL108-90-7 Chtorobenzene BRL75-00.3 Chtoroethane BRL6766-3 Chlototo'm BRLf4 a7-3 Chtoromethane BRL95-49-8 2.Chtorototuene gF.L

106-43-4 4-Chloroto{uene BRt96-12{ 1,2-Dibromo-3-chloropropane BRL124-48-1 Oabomochloromethane BRL10c434 1,2-Dibromoet ane (EDB) BRL74-9t3 Dibrornomethane ARL95,50,1 l,2-DichlorobeMen€ BRL5)41,73 r I,3-Dichtorobenzene BRL106-46-7 l,4-Dichtol.obenzene BRL7s'71-8 Dicilorodifluoromethan€(Freon12)BRL7s 3'l-3 1,l-Dichtoroethane 8RL107{6-2 l,2-Oichloroedune BRL75-3F4 l.l.Dichloroethene BRL15€-5€-2 cjs-1,2-Dichtoroethene BRL1ffi-s trans-1.2-Dichtoroethene BRL7Bi7-5 1.2-Dichloroprcpane BRL142-28-9 1,3-Dichtorcprop€ne gRL

594-20-7 z,2.Dichtomprcp€ne BRL4,6+s8{ 1,l-DichtorcprcPene BRL10061{1.5 cis-1,3-0icthlorcpropene BRL10061-02€tans-l,lDicthloropropene BRL100-a1-a Etht'lbenzene BRL87{0-3 ller€chloobutadiene BRL5s1-78{ 2-t-lexanone (MBK) BRL98424 lsopropylbenzene BRL9947,6 +lsopropyttoluene BRL1634-04-1 Methyl tsd-butyl ethe. BRL10e-r0-l 4-Mehyl-2-pentanone(M|BK) BRL75-09-2 Methylene chtoride BRL

SW84662604 2z-Marlt 22'Ma(47 7031335 RU1

1

1

1

1

I

1

1

1

1

1

1

1

1

1

1

1

l

I

I

I

1

1

1

1

1

1

1

1

1

1

1

1

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191'2G3 Naphthabne

Pa€e 2 of 124

Thh tabonlory rcpon k not wlid st hoa an aathod?rd signrrlre o.t the coser page.

t R€portable D€tection Limit BRL = Belo* Reporting Limir

Page 123: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SamDle ldenril_rcationM8F,l 2-4'sA595l7-01

Client Pmiecr #301 -88

Collection Date,'fimel9-Mar{? 00:00

MahixSoil

Received20-Mar-0?

CnS No- A,'aryte(s) FloS Unirl *RDL Dilutioa L{ethod ReI. Prcparcd Antryzcd Bakh Anebst

103-65-1 n_Propylbenzene10G:t2-5 Styrcne63S20$ |,.1,|,2-Tetachloroelhane7934'5 t, 1 ,2,2-Tetrachloroethane12718-1 TekachloDethene10844-3 Toluene87{1$ 1,2,}Trichlorobenaener20,e2-1 1,2,4-Tdchlorobenzene7155$ t,1 , t -Trichtoroethane

7940r I ,1 ,2-TrichtoroetMne79{1€ Trichloroelhene

lblstile Orgrnic Compounds

Volalile Oroanic Comoound!Pfepared by me{hod SW846 5035A Soit (tow tevet)

BRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRL

75494 Trichtorofluoromethane (Freon '11) BRLs6-18-4 i,2,3-lrichtoropropane BRL9543-6 1,2.+T methylbgnzene BRL10867i 1,3,5-Trimethytbenrene BRL7s{1-4 Vinylchtoride BRL1330-2+7 m,p-xylene BRL95-475 o_Xylene BRL10*9{r-9 Tetrahydrofuran BRL60-2*/ EthyrerfEr BRL99+05+ Tert-amyl methylether BRL637-92,r Ethy,t ted_butyl eher BRL1oe2o 3 Di_isoptopyt ether BRL7545,0 Tert_Butanot/ butyt atcohol BRL123-91J t,4-Dioxane BRL

Sumgate rccov€neE:460401 4-Bromofluorcbenzene

2@7-2eS Toluene4g

1 706407 o 1, z-Dichlorcethane 44

1A6A-53-7 Abrcmofluorcmelhane

Extmctrble Pearolesm Hydftrcrrhons

Extractable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

8006$1,9 Gasoline6847+3G2 FuetOit#26847G31-3 Fuet Oit #468s53{O-4 Fu€t Oit #6M09800r)00 Motof oilJ00100000 Aviation Fuel

Unidentified

Other Oil

Tolal Peboleum Hydrocarbons

Cg-C36 Aliphatic Hydrocarbons

Sutogate recovdies:3ieG$-2 1-Chlorooctadecane

S€mivohtile Orgalic Compoundr by CC

Orqanochlorine Pesticides SW846 8081A

Prepared by method SW846 35508

3090l)!2 Atddn

Lig/kg dry

udks drypdts dryLig/kg dry

!S/kS dry

ldks dry

!S/kS dry

!gl(g dry

usnlg dry

ldkS dry

|lg/ks dry

pg/kS dry

usftg drypstkg drypS/kg dry

lEkg dry

!s/ks dry

ug/kg drypdks dry

lgr(s dry

ldl€ dry

PdkS dry

!s&s dry

UdkS drypSllg dry

6.5

6_5

6.5

6.5

6-5

6_5

6.5

6.5

6.5

6.5

6 5

6-5

13.0

6.5

64.8

6-5

6_5

6.5

6.5

6 4 8

r30

SW 846 82608 22-Ma.47 224,AarO7 7031335 RU

+CTETPH 22-Mat47 234 a147 7031281 DS

99106107105

BRLBRLBRLBRLC€lqrlated asBRL159BRL153159

7G130%

7G130 %

70-130 %

70-130%

.t€/kg drytrE/kg drynq/kg drymg/kg drymdkg drymg/kg drynvkg dryrngkg drym9k9 drym€/kg dry

2632432 6 32A.328.324.328.328.328.328.3

40-140 %

!S/tg dty SW846 8081A 22.Mar{7 26.tlar{7 7031275 TG

Thir loboralo|! Epatt is not vaIU withotr.n au^oriud siga,,ture on tha dtrer pnge

' Reportable Detection Limit BRL = Below Reponing Limit Page 3 of 124

Page 124: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeotificationM8F-l 2-41sA595l7-01

Cli€nt P.oiect #301-88

MatrrxSoil

Received20-Mar-07

Cotlcction Date/TimeI +Mar-07 00:00

CAS No, Ahtlrt (s) FI"C 'RDL Dilutloa Method netr Prcparcd Adalwi Balrh Ad4bst

Semivoladle O.grtric Compouods by CCOmanochlodne Pesticides SW846 8081Aftepared by mehod SW846 355083i9{4{ a€HC319-85-7 b-Bt{c319€€.€ d€Hc58-8+9 g-BHC (Undane)57-7+9 Cl orden€72.54-s 4,4-DDD (p,C)72-s5.s a,+ODE G,p.)so-2e-3 4,4-DDT (p,p')60-57-r Di€ldrin95$9E{ Endoculfan I$21345-9 Endo$lfan llr03i{7-8 EidosulfanSullaten-2oi End.in7421-93-4 Endrin AJdehydeIG-44{ H,sptachlotf24Ts Melhoxychlor1024-57-3 H€placHor Epoxjd€ ..8001-3t2 Toxapfi€nesi03.71-9 a-Chlodane5s66.3+7 g.chlodene539470.5 Erukin Ketone

Su7Dgate rccoveies:1038& z l,QBndaiuorobiphenyl (Sr)ms1-2a7 Docechtotobiphenyt (Sr)Polvchlodnated Biohsnvb bv SW846 BOB2Prepared by mehod SW846 3S5OB12674-11-2 rc810t61110/-2&2 PCB 122111i41-16-5 PCB 12325346e2r-9 PCB 124212672-?95 PCB 124811097{Sn rcg l2s110€€{25 PC8 12603n2+n4 PCB 12621r10cr44 PCE 1268

Surrog€16 /ecovs/iesi1 03&4+2 4, 4 -D&OdaEuorobiplr€nyt (SrlN51-2+i Dacachlorobipltenyt (Sr)

Sendvohdl€ Org.dic Compounds by GCMS

BRLBRTBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRI-BRLBRLBRLBRLARLBRLBRLBRLBRL

43106

BRLBRLBRLBRLBRLBRLBRLBRLBRI-

BRLBRLBRLBRLBRLBRLBRL1,120

pSftS dryrqtg drytig[l(g dry

U€/kS d.y

tgts drypgkg dry

Fgl(s dry

ldlg dry

Idtsdry 6.01

!gl(g dry 6.01

lgl(S dry 6.01

ldks dry 6.01pdko dry 30.0

PSftSd.Y 6.01

ldkS dry 6 01

IgkS dry 6.01

lCftS dry 6.01

Ig/kg dry 6.01pClqdry 6.01

lS,/tgdry 6.01

Ltdkg dry 6.01pSikg dry 6.01

Ig/kg dry 6.01pgtSdry 6.01

udksdry 6.01pSi(S dry 30-0

ldks dry 6.01

ligftsdry 4.01

ldrS dry 6.01

30-15030-150 %

udksdry 12.o

!g&s drv 12.o

lrgkgd.y 12.0

FgkSdry 11.0

ldkgdry 12.0

Ugh€dry 12.O

rs^g dry 12.0pdks dry 12.OpEtg dry 12.o

N-150 %30-1fr %

'|t

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SW846 806fA 22-MaFO7 26-l,,ef47 7031275 TG

SW846 6082 22.|,,,a'47 24 lar47 7031271 MP

Semivolatil€ Omanic Compounds bv SW846 8Z?OCPrepared by metiod SW846 35508&13?-9 Ac€naphtEne20cs6-8 Ac€iaphhyl€n€@€+3 Aniine1412-7 Attl|?cdne1912.249 Afazineto3-3:r-3 AzobenzendDipfienytdiatne92{7-5 BerEjdine56-5+3 Benzo (6) anthracen€

70r I

701 |

701 I

701 1

701 I

701 '|

701 1

701 |

SW84G 8270C 2.-Mat47 24.lli'd47 781279 M.g

Thit lthotutoq Eport ls not vatU Hirtoet rn atthortaal 1igrutap on th. @e.r poge.

+ Reportable Detectioo Limit BRL = B€low Reporting Linir Page 1 ot 124

Page 125: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificarionMtF-l 24'sA595l7-01

Cliont Proiect #l 0 l - 88

Collection Date/Timel9-Mar-0? 00:00

MatrixSoil

Received

20-Mal-07

CAS No. Aaagte6) Fl"s Unia *RDL Diluiotr Prepdnd Analfzed Batch Anallst

Scmivol{tile Organlc Compounds by CCMS

Semivolatile Oroanic Comoounds bv SWO46 9270CPrepared by method SW846 35508

50-32{ BerEo (a) pyrene20199,2 Benzo(b)fluoranthene1s1-2a-? Benzo {g,h,i) perylene207{Sg Benzo (k) lluofanthen€65{50 Eenzoic acid100-s1€ Benzylalcohol1r1-91-t Bis(2rhloroethory)mehane111-.lt-a Bis(2-chloro€thyl)€ther39638.3"-9 8is(2.chloroisopropyt)ether117-81-7 Bis(2€gylheryt)phthatate101-55-3 4-Bromophenyjpbenyl€the/8s6a-7 Butyl benzyl phthatateE6'74-B Carbazole59'5G7 4-Chloro-3.methtiphenol106-47-8 4-Chloroaniline91-54-7 2_Chtoronaphthalene95 573 2-Chtoropt|enol7005-72 3 4-Chtorophenyl phenyl ether218{19 Chrysene53-70'3 Dibenzo(a,h)anthEcene13254-9 Dibenzofuran9s-so-1 1,2-Dichtorobenzener,r1-73-1 1,3-Dichlorobenzene106-46-7 l,4.Dichlorobenzene91-94'r 3,3lDichlorobenzadane120-83-2 2,4_Oichtorophenol84S6-2 Diethylphthatate131-11-3 Dim€thyl phthatate

105{7-9 2,4_Dimethfphenolu-74-2 Di-n-butylphthelates34-s2-1 4,6,Diniho-2_methytphenols1'28'5 2,4-Oinitroph€not121-14-2 2,4_Oinitrotoluene60+20-2 2,6-DanatrotOluene117+a{ Di-n-octytphthalate20Ha{ Fluoranlhene86-73-7 Fluorene11t-7rl'l Hexachlorobenzene87-6&3 Hexachlorobutadiene71474 Hexachlorocyclopentadiene61-72-1 Hexachbroethane193-39-5 Indeno (1,2,3-cd) pyrene9G12rl 1-Methylnaphthalene78-591 lsophorones1,5rc 2-Metlrylnaphthatene95-48,7 2-Methytphenol

108-39-4, 3,4-Methylphenol106-44-591-20-3 Nephthatene8A-74{ 2-Nilroanitine99{9'2 }Nitroanitin€

1,0901,120

1 ,160BRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLARLBRLBRL1,380BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RL2.150BRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRL

BRLgRL

SRL

ldkS dry 7O1

ldftS dry 7o1

!g/kg dry 7O1

!g/kg dry 7ol

ldks dry 701

UdkS dry 7O1

Ug/kg dry 701

Ug/kg dry 701

ldkS dry 101

PS/Kg dry 701pq|kgdry 7O1

!S/Kg dry 701

tlgkS dry 701

9Ekg dry 701

f.rs/Kg dry 1o1

Vgkgdry 7O1

ldKs dry 7o1

UdkS dry 701pgkS dry 701

ldkS dry 7O1

lSftS dry 701

Ig/KS dry 701

|lgkg dry 701

ugkg dry to1pdKs dry 7o1

UgkS dry 7O1

lig/kg dry 7O1

!g/kg dry 701

ldkg dry 7o1pgxgdry 7D1

ug/Kg dry 7O1

!g/kg dry 7O1

!g/kg dry 701

!gr(g dry 701

uqftg dry 701pS/kS dry 7O1

ldkg dry 701

ldkg dry 701

ldtS dry 701

S4{S dry 701psn(g dry 7O1pdkS dry 701pEkS dry 7O1

llgkgdry 7O1

rcAS dry 7O1

ldkS dry 7O1

ldkS dry m1

lgko dry 7O1

PgkS dry 7O1

t4/kS dry 7O1

I

1

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SW846 8270C 22-Mat47 24.ilaF17 7031279 M.a

Thh laboralory reporl it nal wlid roilhod on aartorized sigdzlure on ahe cover paEe .

' Reporiabte Oetection Limit BRI. = B€low Repoffng Limit Page 5 oa l24

Page 126: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationMtF-l 2-4'sA595 r7-01

Cli€nt Proiect #301-88

Matri{Soit

Received20-Mar-07

Coltectiod DatelTimel9-Mar-o7 00:00

CAS No, AnaIY.(s) Resdt Fl4g rRDL Dilu.iol L{ethod nel, Prepared ,lrralXzpd Batch Atelyst

S€mivoladle Orysnh Compoundr by GCMSSgmivolatile Oraanic Comoounds bv SWBit6 8?70Cft€pared by melhod SW846 35508100fi6 +Nilroaniline

9&9t3 Nifob€nzene€&755 2-Mtophenol10G02'7 +Nihoph€nol@-7!9 N-Nitrosodirhethy'amin€621q-7 N.Nitac6odi_n_pfopylamin€{16-10{ }SNitrosodipheflylarfilne

€7€F5 pentachloroptEnoi

85{l-6 Phenanhr€ne

i0&95-2 Phenol

r29{x}.0 n/rene1ro{6n Pyridine120{2n 1,2,+Trid{ombenzene95r.Ss4 2,4,tTridorophenol88{€F2 2,4,GTridoropnenol

&r?Dga*e /rougrbsr12t-6o.a 2-Fluorobhhentlfi7-124 2-Fluorophenol1t65404 Nitrobenzene4s4165"62 2 Phefiol45171&s14 Teryhenyt44lts-79-6 2,1,enib,!,t1ophofid

Totll Met li by f,PA 6000/7000 Series Mettods

743947{ I\rerc!ry

Tot{l M€{{b by EPA 20o S€rt€s Mcthodj

7444-?24 Silvet

7440{{12 ArgerilC.

7440n+3 Badsm

744{14}9 Cadmiun

71.1{}47-3 Chromium

7439-92.1 Leqd

rr82492 Selonium

SPLP Metals by EPA l3l2 & 6000/7000 Seri€r Method6

sr.LF Enrad|on

Z4&22-a Sllver

74,10-3&2 AF€nic

74r{},3$3 Barium

7440-449 Cadmfum

Zt4{}|7n Cho.hium

7439-9rc Merqlry

749-92-1 Lead

7782-4$2 S€'l€flium

Ge trerrl Ct€mbtry PerrDea€rr

% Sollds

1 SW846 8270C 22'&1atr47 24l"',a(47 7q|1279 M.B

t '

1 '

t '

1 '

1 '

I '

t '' l '

1 '

I SWA4i 74llA zGMar{7 27-N[ar-07 7m1322 Y?

I EPA 200.7 26.Mar-07 26+,lar47 7031321 HB

1 '

1 -

I '

1 '

1 '

1 sw8461312 ?2-MaFO7 22-MaA7 7m1344 BD

I SW8.f{l 1312/G0'108 2341Ff47 24-ttaF07 703l4og LR

1 '

I SW84813121/470A ' 26-lra.-07 7031409 YP

I SW84A 1312/60i08 ' 24.|i,.at.ol 70314S LR

BRLBRLBRL8RLBRLBRLBRLBRLBRLBRL2,130BRLBRLBRLBRL

806779529078

0.340

BRL

37.3

0.394

82.6

117

BRL

Co.npletsd

BRL

BRL

0.0198

BRL

0.0t 30

BRL

0.m19

BRL

87.4

lgl(sdry 2800pgr'kg dry 7O1

WJkSdry 701

UCrtS d.y 2m0

lgl(gdry 7o1

US/kS dry 7O1

Ekgdry 7O1

FgftSdry 7O1pgts dry 7o1

LrdkS dry 7O1

lryro dry 7Ol

frd?€dry 7O1pglsdry 7O1

ttgltgdtJ lO1

trg/kS dry 7O1

*130%,s110%30-r30 %1+11004*130%tg r l 0 %

mgftgdy 0-0340

fitgr'kg dry 1.14

mgn(g dry 1.71

rngrlg y 0.570

mgftg dry 0.285

m€r'kg dry 0.570

mg/€ d.y 0-856

mgikg d.y 1.7r

N/A

t',lSil 0.01m

mgd 0.0150

flEn 0.0050

rEif 0.0025

n€t 0.0O5O

mg/l 0,00040

trEl 0.m75

mSn 0.0150

% SM254OG Mod. 2}l',€t47 23-Met47 7031429 QP

Thit ldhonlorf .qod is ^ot tdful *tthaul aE authorizcd dgionte on ttE .av., pzge.

+ Reportlblc D€tectioo Limit BRI_ = Betoc, ReDorting Limit Paec 5 of I24

Page 127: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldertificationM8F-2 2-4'sA595l7-02

Client Proicct #301 -8E

MatrixSoil

Received20-Mar-Oj

Collection Date/Timel9-Mar-07 00:00

CAS No, Anolyte(s) FloS Units *RDL Dilutiorl Method Retr. Preryed Analrzed Eotch ,4ntlltst

Volalile Org.nlc Compounds

VOC Extraction 21-Mat47 21-l,Lar07 7031261 BDField exkacted

Volatile Orqanic Compouhds

Prepared by method SW846 50354 Soit (tow tevet)

76-13-1 1,1,2-Trichlorotrinuoro€thane (FreoERL67 64 1 Acetone BRL107 13 1 Acryionitrile BRL7113-2 Benzene BRL10&8F1 Bromobenzene BRL74-97-5 Brofilochloromethane BRL15-2f4 Bromodichloromethane BRL75-25-2 Bromoform BRL74{3-9 Bromomethane BRL78,s3-3 2-Butanone (MEK) ARL104-51-8 rFBuMbenzene BRL13.198-8 sec-Butylbenzene BRL98116-6 t€rt-Bulytbenzene BRL7s,15.0 Carbon disulfide BRL56,23 s Carbon telrachloride BRL108-90-7 Chlorob€nzene BRL75'00-3 Chtoroethane 8RL67€6-3 Chlofoform BRL74.a7-3 Chloromethane BRL95-49-8 2-Chlorotoluene BRL106-43-4 4-Chtorotoluene BRL96-12-8 1,?-Dibrorno-3-chbroproF,ene BRL124481 Dibromochloromehane BRL106-e3-1 1,2-Dibromoethane(EoB) 8RL74 9s-3 Dibromom€thane BRL95-5G1 1,2-Dichlorobenzene BRL541-73-1 l,3-Dichlorobenzene BRL1096-7 '1,4-Dichlorobenzene ARL

T5-7 l-a Dichlorodifluoromethane (Freon.l2)BRL75-34-3 1,1-Dichloroethanero74G2 i,2-Dichloroethan€7535-4 1,1-Dichloroethene154F59-? cis.1,2-Dichlorcethenet56-60-5 hans-'t,2-Dichloroethene7A-57-5 1,z-Dichloropropanet42-28'9 1,3-Dichlorcpropane

59420,7 2,z-Dichlofopropane583-58$ 1,1_Dichtorcpropene1m61{1-5 ds-1,3-Dichlorop.opene10061-02{ trens-1,3-Dichloropropene100-114 Ehylbenzene

87S&3 Hexachtorobutadiene

591-78$ 2-Hexanone(MBK)!t8€2t lsopropylbenzene9947-a +Eoptopt/ oluene1634.{M-4 Methyl ted-b{jlyl eflref

BRLARLBRLBRLARL8RL8RLBRLBRL8RLBRLBRL8RLBRLBRLBRLBRL

108n0-1 4.t\tethyt_2+enlanon€(M|BK) BRL7sn 2 M€thylene chloride BRL

pSftS dry 5.9pdks dry 118

!g/kg dry 5.9

!S/kS dry 5.9pdkq dry 5 9

ldkS dry 5 9

!g/kg dry 5.9pS/kS dry 5-9

!g/kg dry r'r.8

ldks dry 59.0pS/kS dry 5 S

FS/kS dry 5.9pdkg dry s.9pqkS dry 29 5pSftS dry 5.9pSikg dry 5.9pqkSdry 114

Fg/(g dry 5.9

!g/kg dry 11.8

!S/kS dry 5.9

ldks dry 5.spg/kg dry 11.8pg/kg dry 5.9pdkS dry 5.9

Ig/kg dry 5.9

rc/kg dry 5.9

UgkS dry 5I

US/kS dry 5 9

Ug/kg dry 11 I

UdkS dry 5 I

!g/kg dry 5-gpg/kg dry 5.9

!g/kg dry 5.9

l,g/kg dry 5.9pSftSdry 5,9ps/ks dry 5.9

ldkS dry 5.9pg/kg dry 5 IpqkS d.y 5.9pdkg dry 5 I

!g/kg dry 5,9pg/kg dry 5,9

t g/kg dry 59.0

ldkSdry 59pelkgdry 5.9pdksdry s.9

t'dkg dry s9.0

Fs/kg dry 59.0pdkSdry 5.9

SW846 82604 22-MarOI 22-Ma(4f 7031335 RLJ

91.2G3 Naphihalene

Pagel ol 124

Thb labonlory Rpod i| not valid Nihou aa &arhorl@l slgaa,urc on the cot)e, page .

* Reportable Detection Limir BRL = Below Reporring Limit

Page 128: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple IdetrtificationMtF-2 2-4'sA595 | 7-02

Client Proiect #301-88

MatrixSoil

Collection Date./Timel9-Mar-07 00:00

ReceivedzGMar-07

CAS Na, A','dE 4s) Resdt Flzg Afits *RDL Dllulian Method Retr. Pnparcd Analwd Bateh Anrtfst

Volatile Org.nic Compoun&

Volaf le Oroanic ComoouodsPrepd.ed by n€thod SW846 5035A Soit (tow teve{)

75'49-4 Tric*rlorofiuoromethane (Faeon l1) BRL

103-6$' GPrcpylb€nzeoe100-42'5 Slylen€€0-20{ 1,1.'1.2-T€b_acf oroethane?9,345 1,1,2,2.T€trdcHoroethane127-18-4 Tet€d omethene10&88-3 Toluene€7{1{ 1,2,}Trichlorob€nzene120{2-1 1,2,4-Taichltrobenzene71-5$6 l,l,l.Trichloro€tEne7e{P5 1,1,?-Tdchloro6thane79{1{ Trkt orcefien€

s6-18-4 1,2.+Trichlorop.opane95496 i,2,4Trimethylb€nzene10867{ l,3,tTrimethylbenzene7fr{1-4 Vinyl drtoride133G2G7 m,p-Xyteoe9147€ o-Xy'on€10+99-9 Tet(drydrofucan60-2$7 Ethyl elh€r994{5}a Teft.amylmethytether637-e23 Etry4 teft-buM 6d1€r10&20-3 Diisopropylether75{s{t Tcft-Butsnol/ h.rqy' abotlol123-91-1 1,4-Dioxane

Sutrogate tecovedes:46040.4 +Btufioauorcbenzene2037-26-s Tolueno4St 7o@-o/ -o 1, 2$ichbrcathane44fi 68-s 3,7 D itttdrlof, uo to n€th a n e

Enrrct ble Petrolcrm Hydroc.rtrons

Extractable To{al Pelroleum Hvdroc€rbonsPrepa.ed by method SW846 355088006i1-9 Gasoline6847630-2 FuelOil #26047F31.3 Fu€l Oit #4605s$0{r4 Fuet oil #6M0€8fim00 Motoi oil$0100000 Avislion Fuel

Unid€nlifiedOhe. c)ilTotal Pebol€um HydrccarbonsCS436 Aliphatic Hydrocarbons

Sa,nog|ab r€co!,,arbsr1u,6-33-2 1 -Chloroodealecano

Selr|irohttle Orgrnlc Compouldr by CCOroanochlorine Posticides SW846 8081APrepared by melhod SW846 35508309-00.2 Aldrin

SW 846 82808 22+tar47 22t4*47 7031335 RLJBRL

BRL

BRLBRLBRLBRL

BRLBRLBRLBRL

8RLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RL

99104

110

BRLBRLBRT8RLCalqilated asBRL

BRL83.583.5

115

pdts dry 5,9pdkg dry 5.spdkg dry 5.9pStkg dry 5.9pdkSdry 5_9pg/l(gdry 5-9

lglsdry 5.9

USI(S dry 5.9

ItSJkSdty 5.9

WI€ d.y 5.9pCAS dry 5.9

ugtgdry s.9

ldxS dry 5.9

ldkS dry 5.9

!g/kS dry 5.9

ttgJkgdry 5.9pErgdry 11.8pdl€dry 5.9pdkgdrt 59.O

VdkSdty 5.S

tl4/ks dry 5.9

Udks dry 59

Fgtg dry 5.9pdkgdry 59.0pS/XS dry r18

70'130 %70'1i0 %70-130%70-1fi %

mglkg dry 27.4ntdkS dry 27.4o€rkg dry 27.4mg/kgdry 27.4ndkS dry 27 -4n'dkS dry 27 .4mdkg dry 27.4mg/kg dry 27 .4rEikgdry 27.4nEfl(g dry 27.4

4)-140.A

1II

I

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7

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I

+CTEIPH 22',l',a'47 23-$9f-07 70312A1 DS

BRL ldkS dry 6.13 StrE46 80AlA ?2-MaIo7 8 tiat47 7G11275 TG

Thb lahotuory Epon is ,tot eolil Nlthott z, auahotlz.d sigdslare oE ,h2 coear ltoge.' Reportslrle Delaction Limit BRL = Below R€porting Limir Pag€ 8 of 124

Page 129: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationM8F-2 2-4'

sA59517-02

Client Proiect #301 -88

MatrixSoil

Received20-Mar 07

Collection Date,,Timel9-Mar-117 00:00

CAS No. Anabte(s) FloC Unatr *RDL Duutian PPparcd Autltzed Bath Analpt

S€mivolatile O€adc Compounds by cC

Orqanochlorine Pesticides SW846 808 tA

Prepared by melhod SW846 35508

319 84s a,8HC319-Br7 b_gHc319-863 d_BHC58{+e g-BHC (Lindene)5T-74I Chlodane72 54-a 4,4.DDD (p,p )72-5ss 4,4-DDE {p,p,)50-2+3 4,4{DT (p.p.)60'57 1 Dieldnn959-98{ Endosulfan I3321355-9 Enclosulfan ll1031-07,8 EnctirsulfanSullate72-2O-B Endrin7421-s3-4 EndrinAtdehyde76'44€ HeptachtorI24us l\,,lethoxychlor1024-57-3 Heptachtor Epoxideeo01-3t? Toxaphene510171,9 a_ChlordEne5,566,34,7 g-Chlordane

53494-70'5 Endrin Ketone

Sunogate rccoveries:103868+2 4,4-DB-Ochnuombiphenyt (Sr)

2051 2z j Docachlorobiphenyt (Sr)

Polvchlorinated Biohenvts bv SW846 8082Prepared by melhod SW846 35508

12674-11 2 PCB 101611104-28-2 PCB 722111141-16-5 PCB t23253463-21-9 PCB 124212672-294 Pc:B 12481to9t6s-1 PCB 12lA11096-82,5 PCg 126037324-23-5 rcB | 26211100-14-4 rc8 1268

Suftogale rcco@ies103868+2 4,4DgoclaflLtotobiphenyl (St)

m5t?+3 Decachtotobiphenyt (Sr)

Semlvolrtile Orgrnic Compouods by CCMS

BRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

89

BRLBRLBRLBRLBRLBRL58.8BRLBRL

7090

BRLBRLBRLBRLBRLARL

BRLBRL

pStkSdry 6.13

t SIq dry 6.13

!g/kg dry 6.13

!g/kg dry 6-13

IiS/kS dry 30.6

ldkS dry 6-13

ldkS dry 6.13pdkg dry 6.13

UdkS dry 6.13pdkS dry 6.13pS4g dry 6-13

t gks dry 6.13pSftS dry 6 13

ldkS dry 6.13

Pdks dry 6.13

FdkS dry 6,13

liS4q d.y 6.13

USftg dry 30.6pSlkS dry 6 13pdkS dry 6 13pS4(S dry 6.13

30-150 %30-150 %

psfts dry 12.3

Pg/kg dry '12-3

Ig/kS dry 12.3pdks dry 12.3

fidks dry 12.3

t S,/kS dry 12.3

lYkS dry 12.3

!g/kg dry 12-3

lgkS dry 12.3

30-150%io-150 0,4

ldkg dry 679

ldkS dry 679

!g/kg dry 679

UgkS dry 679

tig/kg dry 679

!g/kg dry 679

!S/kS dry 679

lgkS dry 679

swa46 80814 22-1,1ar47 26-Mat-07 7D31275 IG

SW846 8082 22-MaA7 24'Ma?O7 7031274 MP

Semivolatile Orqanic Cofioounds bv SW646 8270CPrepared by method SW846 35508

83-32-9 Acenaphthene208-s4 Acenaphthylene62-5!3 Anitin€120-12-7 Anlhracen€1912-24-9 Atrazin€10133-3 Azobsnzen€y'Diphenytdiazine92{7-5 Benzidine56-55.3 Benzo (a) anthracene

SW846 8270C 22-Mat47 214nat07 7031279 M-B

Thit lzborztory rcpon ir not valU x'ithoat aE o!rtofi.ed signeture on the @ter page .

+ Reportable Detection Limit BRL = Below Reponing Limit Page 9 of 124

Page 130: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole [deotihcationN{EF-2 2-4'sA595l7-02

Cliedt Proie€t #301-88

Collection Date/Timel9-Mar{7 fi}:00

MatrixSoil

Rec€ived20-MaF07

CAS No. Anaryb(s) Resalt Flag *RDL Diluittr Mdhod Rel. Prqued A,,alwn Bdch Antlysl

S€mivol.tlle Orgonic Compoundr by ffMS

Semivolatile Oroanic Comoosndg bv SW846 B2Z0CPrepared by mglhod SW846 355083)-324 Benzo (a) py.oneat99l Benzo (b) ffuoranfhener9r2,1-2 Elenzo (g,h,i) perytene207{&9 BerEO (k) fruo|antlenett545-0 Benzoic add10G51{ Benzylalcohol11r-91-1 Bis(2-chlomethory)methan€11141.4 Bis{2-cruoro€thyt)etE.3963s32,S Bis(2+hlorcisoprcpyl)e0Er117-81.7 Bis(A.ethy,lh€)qt)phthalate101.553 4_Bromopheny' phenyi elh€r8s.64-7 Bu!/benrylphthatate8G74{ Csrbazole59{Gz 4-Chtoro-3-fiethyiphenol10€-4?{ +Chtoroaniline91-5&7 2-Chloronaphthatens95'57-8 2.Chlorcphenol700$72.3 4-Chloroph€nyl phenyt ether2t8{1.9 Chrysenes3-7{t3 Oibeozo (a,h) anthrac€ns132444 Oibenzofuran95{Gr |.2-Dichlorob€nzen€54i-73n 1,3-Oichlorobefizene10€-{6-7'1,4-Oidhlorobenz€ne9l-94-1 3,3'-Didtlorobenzidine120-8!2 2,+Dbhloropheflola4{&2 Diethytphthatate13rnt-3 lImethylphthatale1ffi7-e 2,4loirnetiyldlenolu-r4-z D-n-bUVphthalate53+52-1 4,6-Dinilro-2-methylphenol51-20-5 2.+Dinitrophond12i{+2 2,4-Dinilrotoluene60G20-2 2,6oinitrototuene117-e4.o D-fl-octyl phhatale206..(+0 FluoranttEne8&7+7 Ffuorsne11&7+l Hoxachlo@benz€ne07{&3 Hex€ctorobutadieneT1474 Hexachtorocydopentadiede67-72-1 H€XaClOroethane1e'396 Indeno (l,2,3-cd) pyrenes0-12-0 t-i,trethylnaphthaleno7&s*l lsophoaono91.t$ 2-Methytnaphhateno

4$7 2-ldethylph€nol10&39-1, 3,4-Methylph€nol1ftr-4.r.591-2c3 Naphthatene&744 2.Njtroaniline99{$2 }Nitroanitine

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRIIERLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLERL

BRLBRLBRL

ldkS dry 679

ldlq dry 67S

|Jg/kS dry 679

Ugl*qdry 67S

ldtgdry 679

ugkSdry 679

trg./kg dry 679

lrSikS dry 679

lqkS dry 679

ldkSdry 679

!Sn(S dry [email protected] 670

FSftSd.y 679pdksd.y 679pdks dry 67S

UdkS dry 679

t Sl(rgdry 679pS^S d.y 679pg19 dry 679pdkS dry 679

t dkg dry 679pgikS dry 679

Igr(g d.y 679pdrqdry 679

UdlSdry 829

IdkS dry 679pSil€ dry 679

udks dry 679

Lidrgdry 679

ug/kg dry 679

t'dksdry 679pgfts dry 679

rsrks dry 679

rgls dry 679

Ugr'kg dry 679

rcrkS dry 679pg/kg dry 673ps,ts dry 679

ldtSdry 67s

lgkg dry 679

$gnKS dry 673

Fgrtg d.y 679ps/ks dry 67s

ldkS dry 67S

[dkS dry 679

lldko dry 679

t sikg d.y 679

pS,/kS dry 679

lgrsdry 679

IdkS dry 079

1

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SW846 8270C 2-Met47 24+,i,a147 7O3r279 M-B

Thh labodoq rqo.l it ^oa eqlAl lrtoet qtt aalhoriad dgnafune od tlt coter pag..

'Rcportable Detectim Limit BRL = Below R€porting Limit Page lO of 124

Page 131: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificarionM8F-2 2-,tl

sA595l?-02

Client Proiect #30r -88

CoLlection Date/Timel9-Mar-07 00:00

MatrixSoil

Received20-Mar-o7

CAS No. An4utc(s) Flog Unia *RDL Dilulinn Method Retr. Prepared Aru$'zed Rzt.h Andlrst

S€mivolrtil€ Orgrnic Compounds by CCMS

Semivolatle Orqanic Compounds bv SW846 8270C

PEpared by melhod SW846 35504

100-016 4-Nitroaniline

9O-9t3 Nikobenzene

00-7t5 z-Nitrophenol

100-02-7 4-Njtrophenol

62-7re N.Nitrosodimehytamine

62144-7 N-Nitrosodi-n-propylamine

€G3G6 N.Nitrosodiphenylamine

87€s5 Pentachlorophenol

8F1-8 Phenanthrene

108-95-2 Phenol12s0.o Pfene11c86-1 Pyridine12{)!821 1,2,4-Tddllorob€nzene

s5-efl 2,4,STichlorophenol

€3-0+2 2,4,6-Tricftlorophenol

Swrogale rccoveries:3214Ga z-Fluot&iphenyt

367-124 2-Fluorophenol

116,4a4 Nitrcbenzene45

1165-62-2 menol4s

1718 51 0 Terphenyl4l4

11a-794 Z4,ETibrcmophenot

Total Metals by EPA 6000n000 S€ries Methods

7,139 97-6 Merc!ry 0.222

Total Metds by EPA 200 S€ri€s Methorts

sw846 8270C 22-MarO7 24-Mat4/ 7031275 M.B

1 SW8467471A 26-Mar0l 2741at47 7031322 YP

BRLBRLBRLBRL

BRLBRLBRL8RLBRL

8RLBRL8RLBRLBRLBRL

786378528574

BRL

3.97

44.5

0_490

44.3

269

BRL

Comdeted

BRL

BRL

0 .0211

BRL

0.0148

BRL

o.0/24

BRL

90.0

pdkS dry 2120pg/kg dry 679pg/kg dry 679pdkgdry 2720

!g/kg dry 67S

ldkS dry 679pdkS dry 679

!q/kg dry 679pdkS dry 679

!g/kg dry 679pg/kg dry 679

!g/kg dry 679

ldkS dry 679

!Sn(S dry 679

!g/kg dry 679

30-tm o/,

1rf l00A30-130 %t 5-110 %30-130 0/o

15-110 %

nu/kg dry 0.0327

mdkS dry 1-07

mg(s dry 1.60

mg/kg dry 0.533

mg/kg dry 0 266

mg/kg dry 0.533

rirgftS dry 0.799

mg/kg dry r.60

mg/l 0.0100

mSl 0.0150

.'r,q[ 0.0050

mgn 0.0025

mgn 0.0050

mSI 0.00040

.r€l 0.0075

nE/l 0.0150

%

1

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7440-22-4 Silver

7440-38-2 AFenic

7440-39-3 Eadum

7440-43-9 Caclhium

744047-3 Chromium

743s92-1 Lead

778?4+2 Selenium

EPA200-7 26-Mat47 274,Aa( 07 7031321 HB

SPI,P Metsls by EPA ll12 & 600fl7000 Sert€s Methods

7440-224 Silver

7440-3&2 Arsenic

744{-39'3 B€riuft

744{143-9 Cadmjum

7440-47-3 Chromium

7439-976 Merotry

7a39-92-1 Lead

7782-49-2 Sel€nium

General Chemlstry Parrmetets

% Solids

1 SW8461312 22^nar.07 22-MaA7 7031344 8D

1 SW846131260108 z3-Mal.Ot 2{.Mar0l 703'1408 LR

1 "

1 "

1 ' ,

1 SW846131217470A " 2€{,lar{7 7031409 YP

1 SW846131260109 " 244nat47 7031408 LR

1 '

1 SM2540 G Mod. 23-t4ar-07 23-Mar-07 7031429 QP

Thb lahontlory fepora is not ttlld toithoul dn outhoriie.I sigAatare on the cover page

+ Reportable Detec.tior Li Di! BRL = Berow Reporrjng Limil Page 1l of 124

Page 132: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F.3 2-a,sA595l7-03

Client Proiect #301-88

Collection Date/TimeI 9-Mar{7 00:00

MatrixSoil

Received20-Mar-07

CAS No. Analrte(s) Flae aRDL Inaitn Method Rtl PEWed Aaalr'?.ed Bdch Analysl

Volrtile Orgmic Compounds

VOC ExtractionVolatile Orcanic ComooundsPrepared b!' method sw846 5035A Soil (tow tevet)7e.i3-l l,l:-Trkhlorofinuoroothane(FreoPRL67i+t Acetofi€ BRLio7nll Adylonibile BRL71!32 Benzen€ gRL

i08.6€-1 Bromobenzen€ BRLra-97-5 Bro.nodllorofiethane BRL

75-2+2 Brornofofln BRL74{}9 Bromo0elhane BRL70-9+3 2-Buhnone(MEK) BRL104'51{ rl-Bu9lbenzene BRL13t9&€ s€c€utylbonzene BRL9e{6-6 tsd€utylbenzen€ BRL7t154 Carbon disulfde BRL50.23-5 Carbon lebachloride 8RL10990-7 Chlorcb€n2ene BRL75{0-3 Chb.o€thane BRL67€&3 Chlorobrm BRL7447-3 Chlommothene BRL9s-49.a z-Chlorotolu€n€ BRL10fF43-1 +Chlorctolueno BRL96-12-8 1,2-Dbro.no-3-chloroprop€ne BRL12.r-4{-1 Dibromod oromethene BRL1c'6934 l,2-Dibromoethane(EDB) BRL74-9!3 DibomometrEne BRLg+s(l.l l,2-Dichtofobenzene BRL541-7311 l,3-oichlorobenzene ARL106-46-7 l,+Dichlorobenzsne BRL75-7 1-8 Dicfilorodifluoaomeihane (Faeonj2) BRI75-34-3 1,'1-Dichlofoethane ARL107-Oe2 1.2-Dict{oro€thane BRL75-35-,! .1.1-Oichtoroethene BRL1se592 cis-1,2-Dlchloroetheie BRL15Sq],s ten6-l,2.Didhloro€hetre SRL7€{7-5 1.2-Oid orcpropane BRL142-28-9 '1,3-Dichlofopropane BRL59{-2F7 2,2-Dichloropropene SRL561584 1,|-Dichtoroprcp€ne BRL1006i41'5 cis"1,3-Dichlorogrop€ne BRL1006142{ tan91,}Dichlo.ogrop€ne BRfl0G41-. Ehy'bsnzfie 8RL8z€+3 Hexachto.obuladhne BRL5Sr-70S 2-t{6xanone (MBK) BRL

lsotropylberEen€ 8RL€{7{ +tsffropy'btu€ne SRL1634{4-4 Methyl ted+oty'l €trer BRL10&rcl +Me&yl-2.pentaftne{M|BK} BRL754e-2 irethylene chtoride BRL

21-iiar-o7 21-l4ar{7 7031261 8D

22-ll,.at47 22+taFO7 761335 RLJ

BRL

Field e)daactod

UdtSdry 7.5

trslt(S dry 151

FSI€dry 7.5

U919dIy 7.5

ldkg dry 7.5

rd*S dry 7.5

rc/kg dry 7.5pdrs dry 7.5

ldls dry ts.ipdkgdry 7s.4

IdkS dry 7.5

Fgtkg dry 7.5

FSftSdry 7-5pdkS dry 37.7

tdkS dry 7.5

lgkS dry 7.5

l4k0 dry 15.1

Fgtgdry 7.5

!4k9 dry 15.1

rglxSdry 7.5pSn(S dry 7.5pglqdry 15.1

US&S dry 7 _5pgrSdry 7.5

Idkg dry 7.5

!gl!s dry 7.5pgftgdry 7.5

US/kgdry 7.5pdkgdry ls. l

udlgdry 7.5

ugtsdry 7.5

lrSlkg dry 7 5pS/kg dry 7.5

Ugl(gdry 7.5

udkSdry 7.5

t gkS dry 7.5

FS/kS dry 7.5

US^S dry 7-5

$g/kSdry ? s

tdkg dry 7.5

Ug/kS dry 7.5

Fg/t€ d.y 7.5

ISftS dry 75.4

fgkg dry 7.5

ldkS dry 7.5

rcn(S dry 7.5

F€ikgdr, 75.4

f.fSikgdry 75.1pC/kS dry 75

voc

sw 846 82608

9t-u}3 Naphthalane

PagE l2of 124

fhk laboratory Epotl h not vdtd wiahoa ae surtorited slgnatsre ol the cowr 1,q..' Reportable DEtection Limit BRL = Below Re!|orting Limir

Page 133: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentilicationM8F-3 2-4'

sA595l7-03

CLient Proiect #30r,88

Collection Date/Timel9-Mar-0? 00-00

MatrirSoil

Received20-Mar-o7

cAs No. Anfute(st Res,h F,aE Unia ARDL L[e,ltod ReI. Preta4d Analrzed Balch Ana|.st

Volrtile Orgrnlc CompouEds

Volatile O.qanic ComooundsPrepared by method SW846 50354 Soit (tow tevet)

75€94 Trichtorofluorcmethane (Freon .t 1) BRL

1o}gs-t n-PrcpylterEene10G12 5 Styrene630205 1,1,'l,2_Tetrachtoroethane79{4_s I,1,2,2-Tetrachlorcethane127n8-4 Tetrachbro€thenel0a€4,3 foluen€87.€16 1,2,lTrichtombenzene120€2-1 1,2,4-Trichtorobenzene71-s5{ l,1,t_TrirhtoroetfEne79{tr5 1,1.2_Trichtoro€thane79{l€ Trichloroelhene

96-18-4 t,2,STrichloropropane9s43{ 1,2,+Trimethytbenzene108€7-6 1,3,+Trimethytbenzene75414 Vinylchtoride1330-2G7 m,p-Xylen€95-47-6 +Xylene109-9s9 Te{rahydrofuran60-?s7 Ethytether994{5€ Terl-amyt methyl ethef637.92-3 Ethytled-butytetf€r108-20-3 Di_isoprDpytether75{5{ Ted-Butanot/ bntyt alcohol12391-1 1,4-DioxeDe

Surrogale ,€cover'es_160a04 +Brcnofluorcbenzene

m37-26-s Tduene4S

1 1066074 1,2-Oichloroethane-d4

1868-sAr Dibr'ofllolfufrrcmethane

ExtyNctable Petroleum Hydrocrrtons

Exlractable Total Petroleum Hvdrocafuons

Prepared by method SW846 35508

800€-61,9 Gasotine6847&30,2 Fuetoit#26847e31-3 FuelOil#468553{0-4 Fueloil#GirogSomaJo Motof OilJ00100000 Avjaijon Fuel

Unidentified

Olh€r Oil

Total Pekoleum Hydrcc€rbons

C9-C36 Aliphatic Hydrocarbons

Sunoga6 ,ecovedes'3386-3}2 l-Chlotoodadecane

S€mivobtile Oryrnic Comportrdr by GC

Oroanochlorine Pesticides SW846 8081A

Prepared by method SW846 35508

3OlO0-2 Aldrin

SW 846 82604 22-Ma47 22-MaF07 7031335 RLJBRLBRLBRLSRLBRL

SRLBRLBRLBRLBRLERL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRL

9410110998

WkS dty 7.5

UdkS dry 7.5

ldkS dry 1.5

pdkS dry 7.5

ldkS dry 7.5

!94(S dry f_5

pg/kg dry 7.5

pg/kg dry 7.5

pg/kg dry 7.5

f.ig/kg dry 7.5

lSftS dry 7 5

f.iS/r€dry 7_5

!g/kg dry 7 5

UdkS dry 7 5

Ug/kg dry 7.5

lrSlkS dry 7_5

udks dry 15.1pg/kg dry 7 5

US/Kg dry 75.4

IgkS dry 7 5

USftS dry 7 S

lgkS dry 7.5

ldkS dry 7.5

ldkS dry 75.4

,rgkS dry 151

7L130 0t

70-130 %70-130 %70-130 %

mdkS dry 44.1

mSI$ dry 44.1

mdks dry 44.1

mgLikg dry 44.1

.ng!4q dry 44.1

lrglxgdry 44.1

mg!4(g dry 44.1

mgL/Kg dry 44-1

mgr'kg dry 41.1

mg(g dry 44'.1

40-140 %

pdkq dry 7.11

1

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BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

120

+CTETPH 224JtaA7 2}Mafi7 7031281 DS

BRL sw8,r6 8081A 22-Mat47 27-Mar47 7031275 TG

Thir ltbororor! ftFod is not eoIU xlithoat an auhortted sigrroitw on the covr page .

+ Reportable Detection Limit BRL = Below Reporring Limit Page l l of 124

Page 134: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ld€otificationM8F-3 2-4'sA595l7-03

Client Proiect #l0l-88

MatrixSoil

Collection Dat€/Tirnel9-Mar47 00r00

Received20-M^r-07

CAS Na Aulru(s) Fhc *RDL Dilulo', Mdhod Rel. Pnpared Addlyzed DatEh Atulfsr

Semivolrtile OrggDic Compolrnds by CC

Orqanocfilorine Pesticides SW846 8081A

Prepared by rnethod SW846 35508

319{4-€ E-BHC319457 b"BHC319-86{ d-BHC

58{Bs +BHC (Lindan6)

tl-74-9 Chlordan€72€4{ 4,,1-ODD (p,C)

?2.s5.9 A,+DDE (p,C)

5o-2s-3 4,4-DOT (p.p')

60-57-1 Oehrin95$!Xl{ EndGulfan I332133$9 Enalo€ulfan lllq3t{7+ Endo6ulhn Sulfab72-204 Enddn742143-4 EndrinAldehyde76414 Heptad or72435 Methoxydtlorl02a€7-3 tl€ptachlof Epoxide8t1o1.3.t2 ToxapfEne511)0-71-9 aql|ordan€5s66-3+7 g-Chlordanes3494705 E ldrh Ketrn€

Srrzog6l€ '€ooyr/bs--1 uae&a2 1,1,&Ociaf, @@biptenyl (Sr)

m51-243 @cdchlorobiph4nyl (St)

Polvdrlodnaled Biohenvls bv SW846 8082

Prepared by rnethod SW846 35508

1267411-2 Pcg 10161110+28-2 PCB lzl11r41n65 PCg 1232534&+21-s PCB 1242

12672-?34 PCB 1248i1097€$1 PCB 12541109€-82-5 PCB 12603ru423{ PCB 12621n0sr1-4 PcB .t268

St'rogEfe rgcovenbsirc38e8+z 4,4Dg-Ocdluorobipheni (Sr)

tu51-21-3 Decachbrobbhqnyl (Sr)

SelIivd.liL Orgsnic Cornlorf,ds by CCMS

BRLBRLBRLBRLBRLBRLBRLgRL

BRLBRLBRLBRLARL8RLBRLBRLBRLBRLBRLBRL8RL

4180

BRLBRLBRLBRLBRLBRLBRLBRLsRt

4070

BRL

BRLBRLaRrBRLBRLBRLBRL

l,gr'ko dry

USikS dry

lrgrkS dry

FS/kg dry

usl(g dD/

rcfts dry

us& drypsftg dry

FgkSdry r.t1

ucrls dtv 7.11gdXS dry 7.1rpdlq dry f .11pgl€ dry 35.6

FS{(g dry 7 11pdkS dry 7 'l1

pdksdry t. tr

IrS/kS dry 7-0O

!€ €dry 711

leit(g dry 7.r1pg/rS d.y 7.11

lJdks dry 7.1r

udxS dry 7 -11pSftg dry 7.11pg/kg dry 7.11

rdrgdry 7.11

lglqd.y 3s.6

ldlS dry 7.11

UdkS dry 7-11

UdkS dfy 7.11

3It-150 %*150%

IS/kg dry 14-2

FgrSdry 14.2

lgllqdry r4.2

Ugr'kg dry 14.2pS/kS dry 14.2

lgl€dry 14_2pdksdry 142

ldlS dry 14.2

rdks dry 14.2

3G150%30.150 %

SW8{6 80€1A 22-lhr-O7 Z7+,,ar4f 7031275 TG

Sernivoladlo Oruanic Comoounds bv SW846 8270CPrepar€d by metlEd SW846 35508&3-32-9 Aconaphth€ne2n&scs Apen€phthybn€62{}3 Anfline14n12-7 Anthrecene19'12.2+9 Atsazine10$33-3 Azobenzens/Diphenyldiazine92{7-5 Bonzidln€5€.5$3 Bonzo (a) anthrscane

97 1

547 1

547 1g7 1

547 |g7 1

97 1

97 1

SWa,{6 8082 n.Maf{7 24-MatA7 7081274 MP

SW846 8270C 22^4,tr47 24-t'6t47 7031279 M.B

Thb bbrotiry rqod is ,tot tdd pidroo att ouhorid signJ,t tE on tIE co16 page.

r R-epo.table DetEctbtr Limit BRL = Below Reporting Limit Pagc 14 of 124

Page 135: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samolo IdentificationM6F-3 2-4'sA595l?,01

Client Proiect #l 0 l - 88

Collection Dare/Time1g-Mar 07 00r00

Mat.ixSoil

Received20-Mar-07

CAS No. Anzlrte(s) Resul! FlaE Unia *RDL Dil@ion Method ReJ Ptepared Analyed Ectch Analrsl

S€mlvolatlle Orgenic Compounds by CCMS

Semivolatile Orqanic Comoounds bv SWO46 8270CPrepared by method SW846 35508

50,32+ EerEo (a)pyrene

20+99-? Benzo (b) lluot?nJ1e,le191-24-2 Benzo (9,h,0 perylenem7-08 9 Eenzo (k) nuoranthene6545-0 EerEoic acid10(l-s15 Benzylalcohol11r!'1J Bis(2dlloroethory)methane111-44-4 Bis(2-chioroethyl)€drer39638-32-9 Bis(2_chloroisopropylFther117{l 7 8is(2-€Uiythexyt)phthatate101'553 4-Brcmophenyl phenyl ethera55a-7 EuVl benzyl phthaiatem-74-A carlrazoles9-m-7 4-Chtoro-3-methytphenol10eF47{ 4-Chlo{oaniline9i-sa-7 2-chloronaphdalene95-s7-a 24htrrophenol?005-72-3 4-Chtoropllenylphenylether

218{1-9 chrysene53-t0-3 Dibenzo (a,h) anthracene13?$43 Dibenzofuran95,5G1 1,2-Dichlorobenzene:t41-731 1,3_Dichlombenzene106-46-7 1,4-Dichtorobeflzene91-941 3,3'-Djchlorcbenzidjde120S3-2 2,4,Dichlorophenol&46G2 Dierhylphthalate131-11-3 Dirnehyl phthalatre

10s7-s 2,4-Dimethylphenolu-74-2 Di-n-butylphthatate53.1.52-1 4,6-oiniko-2-inethylphenol51-28-5 2,4_Dinitrophenol121r4-2 2,4-Dinih.otoftJene

606-20-2 2,6-Dinitrototuene117-84{ Di_n_octy'phfralate206-444 Ftuoranhene86-7!7 Fluorene11&741 Hexachlorubenzene474&3 Hexachkaobutadien€77174 H€xacfilorocyclopentadiene61-12-1 H€Xechloro€lhene1913S-5 InderE (t,2,3d) pyrcn€!10'12{ l,tlethy'naphthalene78.59.1 lsophoronee1.57-6 2-Methylnaphhalenee54a-7 2-tr,,tehylphenol

10H$4, 3,4-Methylphenol106-44-5e1-2G3 f{aphthalene8a-74-4 2-Nitroanitine99{92 3-Nitroaniline

sw846 8270C 22-Ma(O7 24-Ma(O7 1031279 M.BBRLBRLBRLBRLBRLARLBRLBRLBRL

BRLBRLBRLBRLARLBRLARL8RLBRLBRLBRLBRLBRLBRfBRLBRLBRLBRL

BRLBRLBRLSRLBRLBRLBRL

BRLBRLBRLBRLARLARLBRLBRLBRLBRLBRLBRL8RL

BRLBRLBRL

pg/Kg dry 547

ldksdry 517

!g/kg dry aA7

lrsiKg dry u7

lsixs dry 547

lrgxs dry 547

tr9/k9 dry 547

lSftS dry 547

!S/kS dry 547

PYko d.y 547

ldkS dry 547

ldkS dry 547

!S/kg dry 547

!S^S dry 547pS/kg dry *7gSJkgdry 547

trS/kS dry 547

UdkS dry 547

ldkS dry 547

lgkg dry 547

!S/r€ dry 547

ligKs dry 547

lgikg dry 517

!g/kg dry 541pSJtrS d'y 547

lrg/kq dry la1pS/kS dry 547gdks dry 517

rc/kg dry U7pg/kg dry U7

lS.ftg dry 547pdkg dry 547pg/kg dry 547pdkgdry aalpdKs dry 547

f.iS/kS dry aA1

!g/kg dry g7

!S/kg dry 547

ttgtKsdry aa7

!9I(S dry aA1

FSI(S dry Y7psfts dry 547

USftS dry 547

lSftS dry g7

!S/1S dry 547

ldtS dry 547pdks dry 547

!g/kg dry 547pdkS dry 547

lgikS dry 547

th& Iabonroo' Eport ir nat uzlid ,oirtod .n aartorivd signaitrre oh ahe co4, pagc -

' Report{ble D€rection Lirnit BRI- = Betow Repotting Limir Page l5 of 124

Page 136: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificationM8F-3 2-4'sA595l7{l

Clieot P.oiect #301-8r

Matri{Soil

Collection Date/Timel9-Mar-07 00:00

Received2O-Mat41

CAS No. Adab',e(s) Res t FIog |RDL Diluion Mefiod nctr. hepand Awlwd Batah Analysl

Semlvohtile Orglnic Compoundi by GCMS

Semivolatil€ Omanic Comoouods bv SW84ti 8270CPr@ar€d by m€thod SW846 35508

10G01€ 4-Nitoaniline98{+3 Nifob€nzene08-7SS 2-NitIoph€nol100{2-7 4-Nitlphenol€a-75-e l+.Nbosdimethyiamine6?r€a-7 N-Nitrosodi-n-propylamine0F305 t+Nitooodiph€nylamine87{6{ Pefitaahlorophenol85-01{ Ph€flenthene10&9+2 Phenol129{0{ Pyrcne110-8t1 F)tidiner2o82-l li,+Trid oobenzene

2,4,$Trichlor@h€nol8&062 2,4.$T.ichloroph€not

Surrogate r€cgveres:32160-8 2+tuotobiphenyt

7-124 2-Fluorophenol41 6!,6ILO Nitobenzene45416542-2 Phenol4strts-o|a Teffienyl4l4t1&7*6 L4,&Ttihtofllophenol

SW6,f6 827{rc n rat47 2+Mat47 7031279 M,B

1 SW8467471A 26.Mar$ 2l-irarfi 7031322 YP

1 EPA 200.7 26+td47 2741ar47 7031321 HB

I '

1 '

1 '

1 '

1 '

1 swe46 f312 22{d6147 ?']l[ar4T 7031344 BD'1 SW8461312160108 2 nat47 24-Mar47 7031408 LR

Z1|()-3+2 Arc€nic744on93 B€dum74{04$9 Cadmium

7,140-47-3 dlromium7€9.973 tbrcury74394+1 teadr/82492 S€tenium

Ce trerrl Chemlstry PrEmcteas

% Solids

Ugr'kg dry 21fi

udks dry s7

Udkgdry 547

ugkg d'y 2190p4kS dry 47gSlkS dry g7

ldrg dry 547pS4€ dry g7

US/kg dry 547pg,lgdry 547

udksdry s47

udks dry 547pdks d,y 547

UdkS dry 541pdks dry 547

tulm%16110 %30-130 %1+110%30-130 %trtt0 %

mglkgdry O.O3?3

nqtg dry 1 .'1 9

mdlgdry 1.78

hgr'kg dry 0.594

m€/kg dry 0-410

mdkS dry 0.594

rE/ks d.y 0.890

mgnqdry 1.7a

nEI 0.01m

rE/I O-015O

'ngn 0.0050

mgl 0.0025

mSn 0.0O5O

nrdl 0-m040

mgL/l 0.0075

mdl 0O15O

%

sw8461312|,4704

SWS46 13121160108

26-Mar-tY 781{0s YP

2{-l.i3r{7 7q}l.l0A LR

BRLBRLBRLBRL

BRLBRLBRfBRLBRLBRLBRL8RLBRLBRLBRL

8I)58

188977

Total Metrlr by EPA 6000/7000 S€ries Methods

743+975 Mefcun/ BRL

Totd M€rrb by EPA 20O Sed.s Mettods

7,{4G22r Silver

744G3&2 AFenic

744{}3$l Badum

7,1404+9 Cadmium

744047,3 (hromium

7€9€2-1 Lead

282-492 S€tenium

BRL

8.30

74.2

BRI-

7.93

BRL

SPLP M.Lh by EPA 1312 & 6001y70m Seri6 Methods

SPLP Exhadirn Compl€bd

7440-22-a Silv6r BRL

BRL

0 .0110

aRrBRL

BRL

BRL

BRL

80.3 SM2540GMod. 2UMar47 23+'tar47 7o3flm @

nhit lab$loA r@d b ,tat edu flirtout .n au{rotitd slg',ad . orr dt @er pag.,

'R€po.€ble h.ction Linit BRL = Below Reporring LiDir Pegc 16 of 124

Page 137: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdcotificationM8F-4 2'-4'sA59464-01

Client Proiect #301-88

Collection Date/Timel5-Maf-07 00:00

MatrixSoil

Receivq!l9-Mar-07

CAS No. Analye(s) Resuk Fl"g Units *RDL Dilution Method ReJ, Prcpared Analr,zzd Bdlch Antbst

Volatile Organic Compo nds

VOC Ext actionVolalile Orqanic Comgounds

UdkS dry 4-7

lS^gdry 94_3

lsixs dry 4_7

lgks dry 1.7

tigiko dry 4.7

!g/kg dry 4.7pg/kg dry 4.7pSlkS dry 4.7

!S/kS dry 9.4pS/kg dry 47.2pS/kS dry 4.7pS/tS dry 4-7pg/Kg dry 4.7

!g/kg dry 23.6

,Jdhs d.y 1.7

lgkg dry 4.7

!g/kg dry 9.4pg/kg dry 4.7pq/kg dry 9.4pdkS dry 4.7pS/kS dry 1.7pdkS dry 9.4

fgkg dry 47

tsksdry 4.7pSnqdry 4.7

us/ks dry 4.7

rc/kg dry 4.7

ldkS dry 4.7pS/kS dry 9,4

UdkS dry 4-7pS/fS dry 4 7

uSn(S dry 4 7

udkgdry L7pg/kg dry 4_7

ldkS dry 4.7

lqkS dry 4.7

lglkg dry 4.7pSAg dry 4.7

US/kg dry 4.7

lSikS dry 4.7

ldkg dry 4-7pgkg dry 4.7

ttdkS dry 47.2

udkS dry 4.7

l||dkS dry 4.7

ldkg dry 4.7

ldks dry 47-2pgftgdry 47.2

US/kS dry 4.7

2GMar47 m+1afi7 7031156 BD

Prepared by melhod SWM6 5035A Soit (tow tevet)

76-13'1 |,1,2-Trichlorotriffuoroethane(FreoERL

67€4'1 Acefone BRL107-13-1 Acrytonitrile BRL7143-2 Benzene BRL10&G1 Bromobeozene BRL7447-5 Bromochloromethane BRL7s-274 eronodichloromethane BRL7s2+2 eromofom BRL74€3-9 Bromomethane BRL78-e3-3 2_Bubnone (MEK) 8RL104-51€ GButyJbenzene 8R{_13tsa€ Sec.Butylbenzene 8RL98{6{ tert-Eutylbenzene ARL/5-1+0 Carbon disulfide BRL56-23-5 Carbon tetrachloride BRL10&9G7 Chlorcbenzene BRL7s4+3 Chtoro€tEne BRL675e3 Chbroform BRLt4.97-3 Chbromethane BRL954$a 2_Chlorotoluene BRL106-43-4 ,4-Chlorctoluene BRL96'12'8 1,2-Dibromo-3-chlo.opropane BRL124-4{l-l oibrcmochlorcmehane BRL106-sr3-4 |,z-Oibromoethane(EOA) BRL7+913 Dibromomethane BRL

95-6G1 l,2-Dichlorcbenzene BRLar41-73r l,3_Dichtorobenzene BRL106-.46,7 l,4_Dichtorobenzene BRL15-7 1 4 Oichtorodif uoromethane (Freon12)BRL75-14-3 |,1-Drchloroethane 8RL107-06,2 l,2-Dicldoroethan€ BRL75-35-4 1,.1-Dichloroethen6 BRL1se59-2 Cis-1,2-0ichtoroethene 8RL15€40-5 trans- l ,2 -Oichloro€th€ne BRL7447-5 1,2-Dicl{oropropane BRL142-28-9 1,3-Dachloropropane BRL591-?!.7 2,2-Dic6lotop6lane ARL56's€s I,I -Dichloropropene BRL1m61-01-sCis-1,3-Dichloropfopene BRL10061{2€tEns-.1.3-Didlloropropene BRL10(|414 Ethylbenzene BRL8r€8-3 Hexachlorobutadiene BRL

591-78{ 2-HexarDne (MBK) BRL

9€{2-8 lsopfopylbenzene BRL

s€{76 4-tsopropyltoluene BRL

163.r{44 Methyt tert_butyl etl|er BRL108.10-1 4-Methyt-2-pentanone(MIBK) BRL75{S2 Methyleno chloride BRL

SW 846 82608 21-l at-O1 22-+,ta(o7 7031233 TR

BRLs1-2G3 Naphthalene

Page 3 of 152

Thb btorrtaq rcpofl is nol taIU *irhout tn autho.irerl sigaaturc o^ tha cover lmge.+ Rcportable Det€ction Limit BRL = Belo{'Reporting Limit

Page 138: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentil-lcntionMEF{ 2'-4'sA59464-01

Clieot Project #301-r8

Collection Date/TimeI 5-Mar47 00:00

MatrixSoil

Rec€ivedl9-Mar-07

CAS No- Aaalfta(s) Flae 'RDL Dilation Mdhod ReJ Paparcd /lnatad Bslch Analfst

Vohlile org.tric Corpoundr

Volalile Oroanic CoinpqundsPrepared by mehod SW8,{6 50354 Sdt (tow levet}1014+1 n-Prcp!'lb€nzene BRLr0G42-5 styrene BRL63,G206 1,1,1,2-T6hectoroetfEne BRL79-3L5 1,1,2,2-T€t-actdoro€hane BRL127.18-.r fet€drlorcellrene BRL108-84-3 Toluene BRL67616 l,2.S.Tdchlorobenzene BRLi21>82.i l,2.4Trlchlorobenzene BRL71.55€ 1,1.1-Trichloroethane BRL7$0G5 1,1,2-Tddlloroethane BRL79.01€ Tridtloroethen€ BRL7559-4 TricfiloroflUorornethane (61gon 111 BRL96n8-.1 1,2,&Trichboprop6ne BRL9S16 | ,2,,{-Tdm€thylbenzene BRL10&67{ l.3,tTrimedty'benzene BRL75{11 Vinyl cfiloride BRf1330-20-7 m,p-Xyl€rE BRL9547$ o-Xyl€n€ BRL10+99-9 Tet?hydrofuran BRL6t)-297 Ethyl ethe.s94{5{ Teft-dry'm€thytehef

fi7-92n Edryi ted-butyl eherr08-2G3 Di-isopropt e €r75€5{ Te.t-Blthnol / butyl alcohol12+91-l l,4oioxane

Surogate rccolr'€des:4a04o'4 +Bawttofluorcbenzene

toiT-26-5 Totuene4S

1 706041 4 1, 2 -Dhhloroethane-d4

186A-5?7 Abrcnof,uo@nethane

E raoLblo P€foleum HydrocrrboN

ExtEdable Tolal Peboleum tMrocarbon!.

Prepared by method S1V846 35508

8006-61-9 cas€line

6€a7F3c2 Fuet Oil #268a7G31-3 FustOit #4€8s5il-(B4 Fuet Oil #6iro90o000o Motor oil.jOOToOOOO Aviatid F@l

Unidenlified

ohe. Ol

BRLBRLBRLBRLBRLBRL

1N1041 1 7103

ldrSdry 4.7

ldko dry 4.7ygikS d.Y 4.7

udlq d.y 4.7

udkg dry 4.7

ldkS dry 4.7

ldtgdry 4.7pS4qdry 41

USikg dry 4.7pgl(gdry 4.7

lgtSdry 4.7

!Sn(S dry 1.7

l|gnls drv 4.7

FgtS d.y 4.7pdks dry 4.7

rdkS dry 4.7

UgkSdry 9,1

tr/kgdry 47

XCftg dry 17.2pdkgdry 4.7

tdl<S dt't 4 7

ldkS dry 4.1

FdkS dry 4.7

lgksdry 11.2

Lrgl(gdry 94.3

70-130 %70-130 %7&130%70,1n %

sW 845 82608 214tiat47 22-Mar47 7031233 TR

BRLARLARLBRLBRLBRL67.4Calqrlated as

msASdry 21.9mg,kg dry 21.9mdks dry 21.snE/kg dry 21.9mgkSdry 21.9drgr(rg d.y 21.9mgikg dry 21.9'ngr'kg dry 21.9dtdks dry 21.9mg/kg dry 21.9

40-t$ %

+CT ETPiI 21-Msr-07 2t-I.lar47 7031187 DS

TotalP€ElleumHydrocarbons 67.4C9C36AliphaticHydrocs.bo.ts 67.4

St,|rogate €coyerl?ri338&33-2 l-Chlomodadecane

Sejlivolldle Orgrdic Compo[trdr by CC

O.oanoafilorine P€stcides SW846 8081APrepared by m€rt€d sw846 355083Os-O0-2 AJd.in t'dtg dry SWE f6 80alA m.+'li,ato7 25*let47 703t06a TG

nirit l4br@ry ,qort iE "at

eolitt fthou an aartorid sigt dat ot, the coter INg..i RlporEble DetedioD Limit BRL = B€lol,v R€porting Limit Page 4 of 152

Page 139: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMEF-4 2'-41sA59464-0r

Client Proiect #301 -88

MatrixSoil

Reccivedt9-Mar-07

Collection Date/Timel5-Mar{? 00:00

C,4S No. An ye(s) Flag Antus *RDL Dilution Method ReJ. Pnpared Aaallzed Botch Aru\st

Semivolrtile O.ganh Compounds by CC

Orcanodrlorine Pesticid€s SW846 8081A

Prepared by method SW846 3f508

319{4{ a_BHC31s5-7 b-BHC31+86-8 d-BHC58{s-e g_BHC {Lindane}s7-f4'9 Chlordanef2.s-6 a,4_DDD (p,p')72-ss-e 4,4_DDE (p,p.)so-2s-3 a,4_DDT (p,p.)60-57-1 Dietdrin95S-98{ Endosutfan I33213-65-S Endosutfan ll103147-8 Endosutfan Sulfatel2-2O-A Endrin742r,934 EndrinAldehyde1644 a Heptachtor7243-s Metlrcxychlor102a'57-3 Heptachtor Epoxide8001-3+2 Toxaphene5103-71-9 +Chlordane5566-34-7 g-Chlordane

534!14-10-5 €nddn Ketone

Sutogde rccoveries:103BFe+2 4,+DE-Octafluotobiphenyt (54

N51-2+X Decachlorohiphenri (Sr)

Polvchlodnated Eiohen!,ts by SW846 8082Prepared by method SWB46 3545A

12674 11,2 pCB 1016111o4-2v2 PCB 122111141-rE 6 PCB 12325346e-214 pc81242

12672-29€ PC8 1248110s7{9-1 pc81254

110ec€2-5 pcB 12603732+23-5 PCB 1262'r1100-11-4 PCB 1268

Sunogal€ /.cmv€nes:10386 842 4,4-DB-OctafluoroNphenyl (Sr)

2051-2+3 Oecachlotobipheny' (St)

S€mivolstile Organic Compounds by GCMS

BRL

BRLBRLBRLARL

8.208.7114.2BRLBRLBRLERLBRLBRLBRLBRLBRLBRLBRLBRLBRL

49103

SRLBRLBRLBRLBRLBRL21 .9BRL

BRL

4586

BRL8RL8RL8RLBRL

BRLBRLBRL

!g/Kg dry 5.93

Lidks dry 5.93

!g/l{9 dry 5-93

uglkg dry 5.93

us/ks dry 29.6

ldkS dry 5.93

!g/kg dry 5.S3

ldkg dry 5.93pdkS dry 5.93pSIq dry 5.S3pS/kS dry 5.S3pslks d'y 5.93pg/kg dry 5-S3

PgkS dry 5.93

l.rgks dry 5.93

lEkS dry 5.93

!S/kg dry 5.93

ldkS dry 29.6

!s/(s dry 5.93

t/gkS dry 5.93

ldkS dry 5-93

30-150 %30-150 %

UdkS dry 11.9

tig/ks d.y 11.9

t!91k9 d.y 11.9

ldkg dry 11.9

ldkS dry 11.9

!SI(S dry 1l.SpS/kS dry | 1.9pSlkS dry 11.9

FdkS dry 11.9

30150 %30-150 %

Ign(g dry 543

US/kS dry 543

ldkS dry 543pdkS dry 543psJkgdrt 543

!Sl(S dry g3

ps/ks dry 543

!94(S dry 54:]

1

1

1

1

1

1

1

1

1

1

1

I

I

I

l

I

1

1

1

1

sw846 8081A 20.Mar{7 25-L,lar47 7031068 TG

SW846 8082 21-M€F07 23-MaG07 7031181

SW8,r6 8270C 22-Mat47 244.t1et47 7031278 MB

Semivolatilo Oroanic Comoounds bv SW846 g27OC

Preparod by m€thod SW846 3SS0B8+32-9 Acenaphthene20e96{ Acenaphfiylene62-5+3 Aniline12012-7 AtltlxAcene1912-2+9 Al,raine10+33-3 Azobeozene/Diphenyldiatne92{7-5 Benzidine5C5+3 Benzo (a) antttaacene

This lahomtory reporl ir ttot voIU ttuuA dn 4rdtoried signsrure on the cove. Nge.i R+ortrble Detection Limit BRL = Below Reporting Linir Page 5 of 152

Page 140: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldetrtificationM8F4 2,-{',sAs9.164-01

Clieot Pmiect #301-88

MatrixSoil

Collectiod Date/TimeI 5-Mar-07 00:00

Receiv€d19-Ma!-07

CAS NtL An4lftc(s) Result Fl4E Unia |RDL Dilutiot Mahod Retr Prcpated Adsltzztl Botch 'lnalfs,

Semivolatile Organic Comlnlrds by CCMS

Semivdatle Orqanic Compounds bv SW846 8270CPrepared by melhod SV\t846 355085{L32{ Benzo (a)pyreaemS99-2 Benzo (b) ffuoranth€neisr-24-2 Benzo (g,h,i) p€rylene20748€ BeMo (k) fluo.anthene65€$0 Benzoic acid,0G51{ Benzyl alcohol111'91r Elis(2-cft loroethory)rn€tnanei1tr4-. Bis(2drtoroethyl)eh€t3963e32{ 8is(2-{trh.oisop.opyt)€lher1174t-7 Bis(2-etryihexyl)phtElate101.Sr5-3 +B@mophenylphenylether05€8.7 BuVbenzytphtElate8B-71-a Carbazole5e-50-7,t-chtom-3-methytphenol106474 4-Chlooanilin€91-s&7 2-Chloronaphthetene9+57€ 2-Chlorophenol7005-72'3 +Chlotrophenyl ph€nytethet2r${14 Chrys€ne5!7G3 Dib€nzo (s,h) anthracene132+l-9 Oibenzofuran95-5Gl 1,2-oichtorobenzen6541-73-1 1,3-DichlorobefEene106-1&7 l,+Dichlorobenzene91€+1 3,3'-Dichlorobenzidine1?0-ar-2 2,4-Didrlorophenol84SG2 Di€hytphthalate13r-11-3 Dinrethyl pfithalatei05F6?-9 ?,+Oime$rytphenol&4-74-2 fx-niutylphthatate$4-s2n 4,6-Dinit'o-2{n€Uryloenol51-2&s 2,4-Dinitrophsnol121-i4.2 214-t)inibototuene606-2().2 2,eDinitEtoluene117€4-0 DLn-OdMp,hthstatem6-{44 Ffuoranhen€&f+7 Fluoreoe11874-1 Hexadrlorcb€nzene87€&3 l-lexachlorobutsdien€n47-1 Hexachlorocfdopentadiene67-r?-t H€xaafitoaoetlEn€19!3+5 Indeno (1,?,3-cd) pyrene90.t2{ l-M€fiyloaphthatene786+1 lsophororE91-57{ 2-Methylnaphhalenee5-{+? 2-ltedryiPh€nolt0&39-{. 3,+Me0rytphenolr06-44-69t-2G3 Naphthalene08-144 2-Nihoanilin€99{+2 }Nitroanilane

SW8,f6 827(rc 2]lns47 U4ld47 7031278 M.BBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRLBRI-BRLBRLBRL

8RLBRfBRLBRLARLBRLBRLBRL

BRLBRL8RL

BRI.

BRTERL

t4il€ dry 5.lA

!g/kS dry Yg

lJgkg dry 543

lgkS dry 543

UdkS dry 543

t,g/ko dry 543

ldtg dry 543

Psrksdrv 543

UdlqS dry 54i)

ldkS dry 543pdko dry 543

US/kSdry 543

Fdkgdry 543

Fdkg dry 543

ldkg dry 543

WkS dry 543

rc/kS dry 543pgl(gdry 54:,

ldtsdry 54:l

UdkSdry 543

tdkS dry 543pgks dry 543

lrdlS dry 543

ldkS dry S43

rdkg dry 543

lgr'Xg dry 543

UdtSdry At3pgrsdry 543

Ug,l€ drt 543

lgkgdry 543pgks d.y 543

uSikg dry 543

Fgl*gdry 543

lidkS dry tl3

|,9n€ dry 543

t Sikg d.y 543

UdtS dry 543pdkg dry g3

ldkS dry 543

Idllg dry $43

rsrtgdry 543

rsaSdry 543

Fdkg dry 543

ldkSdry 543

Udkgdry 543

Fdkgdry 543

ldtSdry 543

FdkS dryugkg dry||gikg d.y

t4:]

5439t3

Thit lab.ohrf Epott b ,et wlid tellhost .tt auLorizcd sEn@trc on ahe coter poge.

+ RQorbble Delection Limir BRL = B€tow Repqting Limit Pegc 6 af t5?

Page 141: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentihcationM8F-4 2'-,1'sn.594&-01

Client Proicd #101_88

Matrl{Soi l

Receivedl9-Mar-07

Collection Date/Timel5-Mar-07 00:00

cAs No. Anautz(s) ftesull FIag Uaits *RDL Dil,/tion lwethod ReJ. PEprrcd AruIWd Balch Analpt

Semilolalile Organic ComFounds by CCMS

S6mivolatile Ofoanic Cornpounds bv SW846 B2ZOCPrepared by method SW846 35508

100{14 4-Nitrc6nitine3€-95-3 Natrobenzenem-75,5 2_NitrophenolloGoz 7 4-Nitro,phenol62-7+s N-Nitrosodimethylamine621-84-7 N_Nilrosodi-n_propylamanea63o-6 N-Nitrosodiphenylamine87{SS pentachlorophenol

85418 PhenEnthrene10s,95-2 Phenol129-m4 pyren€

11G86-1 pyridine

120-82-1 1,2,+Trichlorobonzene95-954 2,4,tTrichlorophenol8arl6-2 2,4,GTric+rtorophenol

SurrDgal€ r€coy€aes:321-@-a 2-Fluor&iphenyl

367-124 2-Fluorophenol

4165404 Mrcbenzene4s

416u62-2 Phenot4s

1718-St4 Terykenyl4l4

118-79-6 2,4,6-Tnbtumophenol

1

1

1

1

1

1

1

1

I

I'|'|

1

1

1

I SwE46 74714 23-MarO7 26-Mar47 7031306 YP

EPA200.7 23-MaF07 24-l\,4ar{7 7031305 HA

SPLP Extraction

74a{l?24 Sitvef

744034-2 Ans€nic

7440393 Barium

7410-4!9 Cadmium

744G47-3 Chromium

743F97€ Mercury

7439€2-1 Lead

7782-4+2 SelenaiJm

C€neral Cbemistry PNrumeters

% Solids

!g/kg dry 2170pg/kg dry 543

t/g/r(g dry 543

UdkS dry 2170

!g/kS d.y 543

rg/kg dry 543

t Sikg dry 543pgkS dry 543pg/Xg dry 543

!S/kg dry 543

PgKg dry 543

lgkS dry 543

ldkS dry 543pS/& dry 543pdkS dry t13

3Gt 30 %15,110 %30-130 %1Ut10 %3&t 30 %t5-110 %

nrg/to dry 0.0341

rYE/kS dry 1.O2

mgkS dry 1-52

msftg dry 0.508

frEikg dry 0.254

ndkS dry 0.508

rYE/t(S dry 1 02

lwkS dry 1.52

nEn 0.0100

nEn 0.0150

mgl 0.0050

mgn 0.0025

nE/l 0.0050

nEn 0 0{040

rngil 0.0075

mSn 0.0150

%

BRLBRLBRLARLBRL

8RL8RL8RLBRL8RLBRL

BRLBRLBRLBRL

7662

598375

'| otrl Metlls by fPA 6000/7000 Serier Methods

743$9rc l\rercury

Totrl ltetrb by EPA 200 Serirs Mrftortt

7440-22-4 Sitver

lr4o-382 Arsenic

74.10-39,3 Badum

7440.43-9 Cadmium

7.{{047-3 Chromium

7439-92r Lead

282-4$2 Selenium

SPLP Metals by EPA 1312 & 6000fl000 Sertes M.thods

0.158

BRL

9.90

52.4

1 . 1 9

26.2

176

BRL

Completed

BRL

BRL

0.0120

BRL

0.0122

BRL

0.0217

BRL

81.7

I SW8461312 211,ttar07 21-MEt47 7031229 BD

1 SW846131260108 22-MarO7 24-Mat-O7 7031323 LR

1 "

t "

1 "

1 SW84613127470A ' 23-lii€147 7031324 yp

'l SW846131260108 ' 24-[4ar{7 7031323 LR

1 '

1 SM2540 G Mod. 22-Mat47 22-Met47 7031307 YM

This taborqloqt ftpn ls ^olecla *ithaua an oatho.ateC sign,'lure onthe coltar page.

{ Reportable Det€ctior Limir BRL = Below Reforting Limit Page 7 of 152

Page 142: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentihcationM8F-s 2'-4'sA594#1-02

Client Proiect #301-88

MatrixSoil

Collectiop Data/Timel5-Mar-0? 00:00

Receiv€dl9-Mar-07

CAS No. Anrlyte(s) Resall Flag Aaia *RDL Dlhnion Melhod R.J PEpaled Arralfzld Aafth Anzltst

Volrtile Orgrnit Com!'oundr

VOC ExtractionVolatle Orqanic Comoounds

pdrg dry s.3

lgv€dry 105

Ug/tg dry 5.3

Udkg dry s.3

tr9/k0 dry 5.3

liS4qdry 5.3pSrkS dry 5.3

lgrgdry 5.3

!g/kg dry 10.5

ttglkgdty 52.6pdlq dry 5.3

tdkgdry 5.3

FS/tgd.y s3pCASdry 26.3pgxgdry 5.3

!SI(g dry 5.3

rcftg dry 10.5

la/kS dry 5.3

usAodry 10.5pdks dry 5.3

lgl(g dry 5.3

|lgI(S dry 10.5

Igkg dry 5.3

t S/kS dry 5-3

Idkg d.y 5.3

USftSdry 5.3

lgksdry 5.3

ldxS dry s.3

rcIqC dry 10.5

ug,l€ dry 5.3pg/ko dry 5.3

rdkg d,y 5.3pgtSdry 5.3

lg/lqg dry 5.3

FdkS dry 5.3p9/€ dry 5.3pdkS dry 5.3

lgkSdry s.3pSASdry 5.3pglqdry 5.3

US/kgdry 5.3

USI(S dry 5.3

rc4q d.y 52.6

lSilg dry 5.3

lSikgdry 5.3pgls dry 5.3

ldkSdry 52.6

ldkS dry 52.6

IdkS d.y 5.3

2o-[,lar47 2o-Marfi 7031156 BDField ext"acted

ftepared by mehod SW8,l6 5035A Soil (low levsl)76-1$1 1,1,2-lricfilorotriffuoroethene(FreoERl_67{+1 Acetona sRL107-13-1 Acrylonitib BRt_714}2 Benzen€ BRL108{G1 Btonobsnz€ne BRL7+97-5 BtoriochloronEthane BRL7r2f1 BrodEdictlloromethane BRLf5-zuz Bromobfm BRL71419 Brcmohelhane SRL7&913 2-Bubnone(MEK) BRL104-514 n-Butylbenzen€ BRLi35-96-€ sec-Butylbenz€ne BRL9a{6{ tert€Utylbenzen€ BRL7t15-0 C€rbon disutfde 8RL5G235 Carbon tefachlorid€ BRL'10&90.7 Chlofob€rEefle BRL75{0-3 Chlo@othane BRL67{+3 C o.ofonn BRL741?-3 Chlorornethane BRL95-49{ 2-Chlorototuene SRL106-434 +Chlorotolu€ne gRL

!a't2€ 1,2-Dibrorno-3dtloropaopan€ ARL124-44-1 Dibrornodllorom€thane BRLt0ce3-1 l,2-Ofrfomoehane (EDB) BRL7+95-3 Dibmmomelhane BRL95-SO-1 i.z-Dichlorobenzene BRL411.73-1 i,3-Dichlorob€nzene BRL10re-7 |,4-Diohlorob€nzefle BRL75-71€ Dicitorodinuoromethane (Freonj2)BRL75-3rl-3 'l,l-Dichloaoethane BRL107.06-2 1,2-Dichlo{oethane BRL7t35-4 1, t-Dichloroethene BRL15+5*2 d!-1,2-Dichloroetheoe BRL15€-60.5 lrans-'1,2-Dichloroethene BRL7&.47.s 1,2-Dichloropr@ane 8RLi42-2E'9 1,3-DicHo,opropane BRL.re4-207 2,2-Dichlo.oprop6ne BRL4|615&6 1,1-Dichloropropene BRL10{r€1{1{ ds-1,3-Dichloropopene BRLi006i{2€tlans-1,3-Dichloroprop€ne BRLt00-41-4 Ehy{b€nzene BRL876&3 Hexed*rrobutadiene BRL4,91-78{ 2-Ho6none(MBK) BRL98{2-a lsoproptb€nzene aRL99{7{ +lsopropyttoluene BRL1634{1--{ iledryl tert-bulyt edler BRIloelo.i +Metht't.2fentanone(Ml8K) BRr75{9-2 Methylene chtoride BRL

SW 846 82608 2l-Mar47 224a147 7031233 TR

91-?G3 Naphlhalene

P{ge 8 of 152

Thi! laborzto.f.qoi is not valAl wllhoet an a.tdrati@4 sigEate oa dr2 cowr IMge.. R€portable Dck{rion Limit BRL = Below R@orting Limir

Page 143: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [deotificationM8F-5 2'-4's459464-02

Client Proiect #301 -88

MatrixSoil

Receivedl9-Mar-07

Collection Date/Timel5-Mar-07 00:00

CAS No. Analrfu(s) Resull Floe a n s *RDL Dilation Method ReJ Prcparcd Analttzed Balch Anallst

Vohtlle Orgrnic Compounds

Volatile Oroanic ComooundsPrepared by method SW846 50354 Soil (tow lever)

BRLBRLBRLBRL

BRLBRLBRLBRLBRLBRL

7559-4 TrichlQrofluoromethane (Freon 1t) BRL

103{5-1 n-Propylbenzene10H25 Styrene630-20€ 1,1,1,2-Tetrachlor€thaneT9-34-5 1 , 1 ,2,2-Tetrachloroethane12H6-4 Tet€d{oro€thene1$.€a-3 TOlUene47s16 1,2,3-Trichtorobenzene120€21 'l,2,+Trichlorobenzen€

71 s5 6 1,1 ,l-Trichloroethen€79{0 5 1,1 ,2-fticttlo.oethene7s{1-6 Tdchloroethene

SW 846 82608 21-Ma.-O7 22-MaG07 7031233 TR

+CT ETPH 21-Ma(47 21'!lar07 7031'167 DS

{1618-4 1,2,}Trichtoaopropane

95{3{ 1,2,4-Trimethylbenzene

108{7+ 1,3,5-Trjmethy,benzene15414 Vinylchlorider33O-2G7 m,p_Xylene95474 o-Xylene

109993 Tekahydrofuran

60-23-7 Ethytether

991H15€ Tert-atnytm€thytether637-923 Ethylted_bstytether108-20-3 Di-isopropyleher75€s-0 Tert-Butanol/butylatcohol12991r '1,4-Diorane

Surragalg recovaties:46040-4 +Bromofluorcbenzene

2037 26-5 Toluen*d8

1 f o6Go t 4 1,2-Dichloroelhene<!4

1a68-5x7 Abromofluorcmethane

Extrrctrble Petroleum Hydroc.rbons

Extractable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

800641-9 Gasoline6847e30-2 Fuet OiJ #?6847S31-3 Fuet Oil#46855!09 Fuel Oil t[6M0980m00 Motor OilJ00100000 Avialion Fuel

unidentified

Otr|€r Oil

Total Petroleum Hydroc€rbons

C9-C36 Aliphatic Hydrocarbons

Suaogale recoyehies:

$e6-33-Z l-Chloroocledecene

S€mivolrtite Orgrnic Comporrds by cC

Oroanochlorine Pesticides Svry'846 8081A

Prepared by method SW846 35508

3OS-00-2 Aldrin

BRLBRLBRLBRLBRLBRLBRIBRLARLBRLBRLBRLBRL

88101102110

BRLBRLBRLBRLCElorlat€d as8RL251BRL251251

!g/ks drypgkg dry

lgts dry

ldks dry

tt4k9 dry

tidkg dry

Fgftg dry

tiSlq dry

FSnq drypgtks dry

lSftS dry

lSftS dry

US,kS dry

ldks dry

I!9*.S dry

lgftS dry

lgftS drypg/kg drypgKg dry

!s/ks dry

ldks d.y

lEkg dry

wks drypg/kg dry

trSlkS dry

5.35.3

5.35.3

5.35.35.35.310.55.352_65.3

5 352.6105

70-130 %70'130 %7G130 %70-130 %

mgLi kq drymgkg drymdks dryrYEAg drynEftg dryms/kg drynE^g drymdkg drymdkg drymgn(g dry

24.1

24_1

24.1

21_1

24-1

24_1

24.1

24.1

24.1

24.1

40-140 %

ldKs dry SW8{6 8081A 20'ti,lar47 25+lar{7 7031068 TG

This labo&bry rcpod k not Jelid ilithout en oalhorivd signatarc dE lhc aver page.

'Reptrhbl€ D€tection Limit BRI= Below Reporting Limit Page 9 of 152

Page 144: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdcntificationM8F-51'-4'sA5946442

Client Proi€ct #301-88

Collection Dare/Time1 5-Mar-07 00:00

MatrixSoil

R€ceivedl9-Mar{7

CAS No, Analye(s) Floc 'RDL Dilution Llahon Retr, Prcpee Aazlyat Batt Aa44s1

Semivohttle Orgatric Compodtrds by GC

O.oanocfilo.ine P€sticides SW846 8081APrepared by me6od SW846 35508

319++€ a-BHC3t9€5-7 b-BHC319-864 4BHC58499 gFBHC (Undane)57-7+9 Chlordanen-544 a,ADDo (p,p')72.s+s 4,+DDE (p,p.)5&i'+3 4,+DDT (p.p,)EilL57-1 Diohrin95+9€{ Endosulfan I3321165.9 Endosultan ll103147'8 Endbgullan Sultatle

742143-4 EndrinAtdehtdo7644-a Heptachlor7243-5 Metlorychlori0?4s7.3 H€9tacHor Epoxlde8001+tz Toxaph€ne5103-71-9 a4hbrdanefi566-34.7 g-Chtordan€s349rL?G5 Enddn Kelong

surDgata tecolldrrbsj103e64+2 44-Dg-Odan@robiphenyt ( Sr)20s1-213 Ddcachlotobiphenyl (Sr)

Potvchlodnaled B-rohenvls bv SW8,td 8082Preparcd by method SW8il6 3545A12674,1r-2 PC81016111O1?l-2 PCB 1221i1141-16-5 PCB t232536e21-9 PCE t24212672-2s{ PCg 124811097{e-1 PCB 12541i096+2-s PCB.t2603732+23.s rcB 126?1110G14-4 PCB 1268

Ssnqg€le a€coFrigs:1 03E04+2 4, 4ae-Octafl @robiphenyl (Sr)mstu-3 Docechlorcbipheny, (St)

Sesivolrtile Org.nic Compoutrds by mMSSemivolatile Omanic Comoounds bv SW846 827(rcPrepa.ed by method SW846 355088332{ Acenapht}Eno2O&S{ Acenaphthyteng6a-5}3 Anllne12Gi2-7 Allhrac€ne19r?-21L9 At?inei0!33+ Azobenz€ne/Dphenytdiatnes2€ru Bertzidin€s6-5$3 BerEo (a) anhrec€ne

sw846 80814 2{}i,lar-07 2s.fvlar{7 7fi1106a TG

SW846 8082 21][trat47 23 td47 703116/

sw846 6270C 2:$d47 2{-Mat47 7031278 M.A

BRLBRLSRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL8RLBRLBRLBRLBRL

44

BRLBRLBRLBRLBRLBRL39,9BRLBRL

45

BRLBRLBRLARLBRLBRLBR!BRL

Udl(g dry s.87

Ws dtv 5.87

ldks dry 5.Alpg[r(gdry 587

lgrs dry 29.3

$slksdry 53?

UdkS dry 5.87

rdkg dry 5.87

ldkg dry s.87pgl(g dry 5.87

ldkS dry s.87

UdkS dry 5 87

ldkS dry 5 87pdkg dry 5.87pdko dry 5.87pEtg dry 5 87

lrdkgdry 5.87pg/Ig dry 29-3

USI(S dry 5.87

UgkSdrY 5.67

lSfts dry 5.87

30-1fi %30-154 %

wrxg dry . . 11 .7

USAS dry 11.7

Ugr'*O dry 11.7

ldlS dry 11 7pgkC dry 11.7

uS/kg dry r1.7

t Sftg dry r1.7

ISrkg dry 11.7pg/tg dlt 11-7

30-150 %3G150 %

FdkS dry 597

usftgdry 597g/kodry 5s?

FS/kg d.y 597pdts dry 5€7pgkgdry 507

Ugn(g dry 597

tglkgdry 597

fhb bborubry npod b ,et ttdli.I tsidrold ott oa&ortzed sigdafur? on d,e @va poge.

* Reportable Detecriotr Limit BRL = Below R?orting Linir Page l0 of 152

Page 145: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-5 2'-4'

sA59464-02

Client Proiect #301-88

MatrixSoil

CoLlection Date/TimeI 5-Mar-{)7 00i00

Receivedl9-MaG07

C''lS No. Analr,e(s) Fldq 'RDL Dilatian Mdhod Rel. Pnparcd Analyed Ealch Anebst

Scmivolrtilc Orgrnic Compoundr by CCMS

Sernivolatile Oroanic Comoounds bv SW846 8270C

Prepared by method SW846 35508

Q-32-s BEtEo (a) pyrcne20+9s-2 Benzo {b) fluoranthene1s1-24-2 B€nzo (g,h,i) pefylene207-0€-9 Benzo {k) fluo.antfEne65-85-0 B€nzoic acid100-51€ B€nzylalcohol111-91-1 Bis(2_chloroethoxy)methane111<4-4 Bis(2_chloroethyl)eher3963&32-e Bis(2-chlofoisopopyl)ether117{1-7 Bis(2€ft,rytheryt)phthatate101-55-3 +Brornophenylphenylether

85-6+7 Butylbenzylphthalate86-748 Carbazole59-5G7 4_Chtoro_lmethylphenol106{{ +Chtoroanitines1-5&7 2-Chloronaphtrabne95-57{ 2_Chlorophenol7005-72-3 +Chlorophenylphenytether2r8-O1-9 Chrysene53-7G3 Dibenzo(a,h)anthrecen€1325{,9 Oibenzofuranssa5Gl 1,2_Dichlombenzene541-t3-1 1,3-Dichlorobenzene10646,7 1,4-Dichlorobenzenes1€4,1 3,3_Dichtorob€nzidine120+3,2 2,4-Dichtorophenol8446 2 Oiehyt phlhatate

131-11-3 Oimethylphthalate10+679 2,4-Dimethylphenplu-74-2 D_n_butylphthajales34-52r 4,6_Dinitro-2_methytphenol51-2€-5 2,4-Dinilrophenol121 14 2 2,4-Dinitrotoluene606-202 2,6-Dinitrotoluene111444 Dij:,4dyl phhatate

206-444 Fluoranlhene6-TVI Fluorener18-74r Hexachtorobenzene8740-3 Hexactorobutadiene17474 Hexachlorocyclopentadlene6T-12-1 Hexachloroethane1e3-3e-5 Indeno (1,2,3_cd) pyren€

s0-1?{ 1-Methylnaphthalene78{91 lsophorones1{rc 2.Melhy{naphthalene95-48-7 2-Methylphenol

100-39-4, 3,4-lt4ethylphenol106{4-591-20-3 Naphthatene0a-74-4 2-Njlroaniiine99{S-2 3-Nitroanitine

BRLBRLBRLBRLBRL

8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL8RLBRL8RLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

tdksdry 597

ldks dry 597ps/ks dry 5s7

IdkS dry 507

rdks dry 597

IS/kg dry 597

Ig/kg dry 597

rdks dry 87

[dkS dry 5S7

US/kS dry 597

uS/kg dry 597

IgkS dry 597

uS/kS dry 597

Udkg dry 597

tiS/kS dry 597

!94!g dry 597

Lrg/ks dry 597

ldkg dry 597

ldks dry 597

!S/kg dry 597

!Sn(S dry 5S7

ldkS dry 597

!g/kg dry 597

!g/kg dry 597

!g/kg dry 597

!S/kS dry 597

Fqkg dry 597pgks dry 597

!SI(S dry 5S7

lSftS dry 5S7

USftS dry 597

rc/kS dry 597

rc/tS dry 5S7

!S/kg dry 597pSlkSdry 557pS/rc dry 597

t S/kS dry 597

Udko dry 5S7

ugnlg dry 597

Vskgdtt 597

!S/tS dry 597

!Sn(g dry 5S7

FdkS dry 597

ldkS dry 5s7pgks dry 597

FqkS dry 597

lgks dry 597

uqkgdry 597

Wkgdry 597pS/kS dry 557

SW&46 827OC 22-Ma(07 24-Mar47 7031278 MA

Thb laborotory rcpod is nal wli.l toithout on arahorired signrtare on the corer page.

* Reporiable Deteation Limit BRI = Below ReoortiEs Limir Page I I of 152

Page 146: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ [dentihcatiodMrF-s 2'-4'sA59464-02

Client Proiect #l0l -88

MatrixSoil

Collection Date/Timel5-Mar47 00:00

Rec€ivedl9-Mar-0?

CAS No. Arralfuk) Rcsuk FI"t *R.DL Dilution Methad Rel, Prepand AnaflEed Balch Attzlrst

Semlvoletile Org.ni€ Cotrrpo{nd! by GCMS

Semivo{atil€ Oroanic Compounds bv SW846 8270C

Prepared by method SW846 35508ro(}or{ 4Niro6nilirE{l&95-3 Nitrobenzone8S75-5 2-Nboph€nol100{2-7 +NitEpheflol€A-7Ss N-Nitrcsodi.nethylamine621{4-7 l$Nih6odi-nfropylamine88i10$ N-NitEeodiphanytamirE87€45 Pentac+llorophonolE5{14 Phenanthrene10&9+2 Phefiol!29{04 Pyreneil{}s&1 FlrUino12G@-r 1,2,4Tdcl{o.obenzene95.954 2,4,STdchtorophonol86{$2 2,4,GTricfilorophenol

Sttnogale dcoveies:afio-g 2+luq6wenrdfir-121 2+fuoropltqol1lf,!,e4 |tilrohenzene45116552-2 Phend4s171&514 TerpheryI4l411$79.6 2,4,6-Trb.omophenol

1 sW846 8270C ?2-Mat47 244nat47 7031278 M.B

1 '

t '

l "

1 '

1 '

1 "

1 "

1 '

1 '

1 ' ,

l '

I SraJ846 7471A 23-0/ta(-07 26'trta(-07 70313ffi YP

1 EPA 200.7 z3-Met47 24-Mar47 7031305 HS

1 '

I '

1 "

1 '

1 SW8,{61312 21-Mar47 214a.47 703129 BD

1 SW846131260108 22-ltar47 2X tat47 70313?3 LR

1 ' ,

8RLBRLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRI-

BRI'BRL

8063

1588

t gkg dry 2390

t dko dry 597pgrtSdry 597

ldl(g dry 2390

ldkdry s97

ugkSdry s97

US/kSdry 5S?

ldkgd.y s97

Fqrcdry s97

ldkgdry 507

r€l/kS dry 597pdkg dry 597

t€ikg d.y 597pg/kg dry 597

ldtg dry |87

30-130 %15-110 %il-130 %t *110 %30-130 %lU I tO%

nryrg dry 0.0340

nE/kg dry 1.05

mgftg dry |.57

n'gkS dry 0.524

mdks dry 0.262

mglkg d.y O.5

m€L/kg dry 1.05

n|g/kS dry |.57

mg/] 0.0100

mgl 0.0150

nEn 0-&)50

mgr'I 0.0025

mSn 0.0050

mgLI 0.00040

mSI 0.0075

odl 0.0150

%

I '

1 '

1 SW8461312r|470A

1 SW84€ 1312/@'t0B

1 '

23+r€r-07 7031324 yp

23Mar{7 7031323 LR

74eU1 Sibel

7440-38-2 AE€nic

?{40'33.3 Earium

?,t4Gals Cadmium

1|{}47.3 Chromium

743€F92n Le€d

Ir82-492 S€bdum

Totrl M€trk by EPA 600u7000 serl€3 M€rhod!

74399rc Me&rry 0.190

To.rl Met{b by f,PA 200 Series Methodt

BRL

14.4

53_6

1.68

25.O

BRL

SPLP M€trl! by EPA l3l2 & 50{0n000 S€rtes Meahods

SPLP Extraction Compleled

71,40-?2-1' Situet BRL

744t!3&2 AFenic BRL

744039-3 B6dum 0.0170

r!s)-43-9 C€dmium BRL

7.rlo-47-3 Chrcmiurh 0.0i0S

7,138-97-6 Mercury BRL

7€9€2n Lead 0-0507

Zg2-4s2 S€l€nium BRL

Ccrctrl ChcDirtiJ Prrrmet€r!

SM254 G Mod. ?,{at47 2-Md47 703 1 307 YM% Solids

Page l2 of I J2

Thl| Iabonlory qn t is rrot vdid ei&ott.a aulhott1rtr signararc oa the oter page.

'R€porfibl€ DetectioE Limit BRI = Below Repo.tinS Limir

Page 147: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samp[€ IdentificationM8F{ 2'-{'sA59464-03

Client Project #301 -88

Collection Date/Timel5-Mar{7 00r00

MatrixSoil

Receivedl9-Mar-07

CAS No. ,4n4te(s) Fl"C *RDL Dilutio,, ,[ethod Rel. Prcpued Aadyei Bolch Adaljst

Volatile Oigrnic Comp,orndr

VOC Extraction

!g/kg dry 5_8

!sn(S dry 116

ugKg dry 5.8

lgKs dry 5.8

tg/Kg dry 5.8

!g/kg dry 5 8

uglkg dry 5 8

!g/kg dry 5.8yg/xg dry 1r.6

FyKg dry 57_9

Ug/kS dry 5.8ygkS dry 5.8

Ug/rcdry 5.8pgrc d.y 29 0pgkS dry 5.8pdkS dry 5.8

UdkS dry 11.6pSftS dry 5.8

lgkS dry 11.6

lgkS dry 5.8

HqkS dry 5.8

lqks dry 11.6

Fgfl(g dry 5.8

Ltglkgdry tE

ldkS dry 5.8pdks dry 5.Apg/kS dry 5-8pS/kg dry 5-8pdkedry 11.6

!S,&S dry 5-S

!94(g dry 5.8

fgkS dry 5.8

tS/kS dry 5.8

lglqdry 5.8

ldkS dry 5.8pdkS dry 5.8

ldkS dry 5.6psAS dry 5.8pdks dry 5.6

PgkS dry 5.8

PS&S dry 5.8pSn(g dry 5.8

Ug'l(gdry 57.9

USftS dry 5.8

UdkS dry 5.0

USAS dry 5.8

ugkg dry 57.9pS/kg dry 57.9

ISAS dry 5.8

20-1,/aF07 20-Mar-07 7031156 BDField erhectedVolatile Orqanic ComDounds

Prepared by method SW846 5035A Soii (torv tevet)

76-11-1 1,l,2,Tdchlorotrifluoro€thene(FreoBRL674-j Acetone BRL107'13-1 Acrylonitrile BRL714+2 Benzene ARL10s{6-1 gromobenzene BRL74'9r'5 Bromochloromethane BRLr5-2t4 Brornodichloromethane BRL15-212 Bromofofin BRLz4{3-9 Bromomethane BRL70-9!3 2-Butanone (MEK) BRL104-51{ n-Butytbenzene gRL

13+9€{ sec-Butylbenz€ne BRL9€{6s tert_Butylbenzene BRL75-154 Carbon disutfide BRL56'23'5 Carbon tetrachloride BRL104-90-7 Chtofobenzene BRL?5-00-3 chtoroetfEne BRL674$3 Chloroform BRL74i'-3 Chtoromehane BRL95-49-a 2-Chlorototuene BRL1oe-43-4 +Chlorctoluene BRLs6-12-a 1,2-Dibronro-3-chtoropropane ARL124{a-1 Dibrcmochlo.omeflane BRL10F93-4 t,2,Dibrornoethane(EDB) BRL74-9$3 Dibromomethane BRL95-50-1 l,2-Dichlorobenzene ARL5.1173-1 l,lDichtorobenzene BRL106-46-7 1,4_Dichlorobenzene BRL75-7 1 -g Dictrlirrodifluoromethan€ (Freonl 2IERL75-3zl-! 1 ,l-Dichtoroethane BRL107.06,2 1,2_Dichtoroethan€ ARL75-35-4 1.l-Oichloroethen€ BRL15F5+? cis-1,2-Dichloroethene ARL156{0.5 taans-1.2-Oichloroethene ARL78s7-5 1,2_Oichtoropropane BRL142 ?8-9 j,3-Dichtoroprop€ne BRLss4-20-7 2,2-Dichtoropropene SRLs63585 1,l-Dichloroprop€ne BRL1o061{1.s cjs- l,3.Dichloropropene BRL10061-02€ trans-l,lDichtoroprop€ne BRL100-41-4 Ehylbenz€ne BRLB76E-3 Hexachlorobutadien€ BRL141-78{ 2-Hexanone (MBK} BRL9€{2{ tsopropytbenzene BRL99{7+ zl-lsopropyftoluene BRL16349a'4 Methyt tert-butyt elher BRL108-10-1 4-l\,lethyl-2.pentanone{M|BK) BRL7s-o92 Methytene chtoride BRL

1

I

1

I

1

1

1

1

1

1

I

1

1

1

1'I

I

1

1

1

1

1

I

1

1'|I

I

1

1

1

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1

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SW8468m0B 21-Mat47 22 naFO7 7031233 TR

BRL91-2C3 Mphthalene

Page 13 of 152

Tht lohoratoe rcW is aot wlitl toithou ttn 4athori1ad sigtature on rhz cowr palc -

* Reportable Detection Limit BRL = Below Reporring Limir

Page 148: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeptificationMEFS 2'-{,sA59464{3

Clieot Projgct #l0l-88

MatrixSoil

Receivedl9-Mar-07

Collertio'$ Dat€/Timel5-Mar47 00:00

CAS No. Anatrte(s) Resuh Fhc *RDL lxlulloa Mdhott Rel. Prepsred Analfzed Borch Aialfst

Vohlite Orgonlc Com0o{trdi

Volat-.b Oroanic ComooundsPrepared by melhod SW846 5035A Soil (ton, levet)io3{tr n_ftopytbenzgne BRL100-42-5 Styrene 8RL63020{ i,1,|,2-Tehsd om€thffe BRL79-3+5 1, 1,2,2-Teb'6chloro€thane BRL127-1E{ Teha.hloroethene 8RLroSje{ Toluene BRLA?€15 l,2,3-Trid orobenz€ne aRLi2G82-l 1,2,+Trichlofobenz€ne BRL71-55-€ 1,1,1-Trid,toroethan€ BRL79oG5 1,1,2_Triatrtoroethan€ BRL79416 TdchloroettEne BRL7si9-4 Tidllorofiuoronethane (Freon fi) BRL{,6-16-4 l,2.S.Trict oropropane BRL95-€3-6 l,2,,fTdm€thytbenzene BRL108-67{ I,3,5-Trimeflrytbenzen€ BRl-?s{14 Vint ctllodde1330-Z+7 |TlFFXyle{1e95-47{ o-Xylene1099€-9 T€trahydrafuran60-2S7 E8ryl elhergs4-Otr Tert-dnytmethylether637-92J Etry t€Nt_butyt ether10&20-3 Diisopropyteti€r7tr5-o Tert€utanol / butyl alcohol123.91J 1,4obxane

St rmgaie tecowrnrs--461,404 +Btumofluorcbenzqnem37-26-s TdtGna4S| 7 060474 l,?Qichlot@thane44

BRLBRLBRL

BRLBRL8RLBRLBRLBRLBRL

1041@1G)

ta6a5.:lz

Ettrrctrble PetaoleuIr| HydrocrrborsEdi"actuble Total Pol.oleum HvdrccarbonsP.epared by rneltbd SW84{i 355088006{1{ Gasoline68476-30.2 FuolOlt #26847&313 Fqel Oll fi46455!0Ga FuelOilt 6trogtfrooo tbto. OilJoo1dxloo Avialion Fuel

UnidentifedOd|€r oillol,al Petroleum HydrocarbonsC9436 Aliphatic Hydrocarbons

SuTDgare recorr'gnss--33BB-3.}2 |-Chlotwcladecene

Semlvolrailc Ory{nh CoEpo[n& by CCO.oanochlodne Pesticidos SW8,16 808 1 APrepared by rnethod SWE46 35508309-OG2 Aldrin

pg/kS dry 5.8

lg,irsdry 5.8

lqkS dry 5,8

ldko dry 5.8

lrykg dry s.6pgl,l(gdry 5,8pCrlg dry 5.8

lgr'kg dry 5.8pdks dry 5.8

tdkg dry 5.8

uqlqdry 5.8

PdkSdry s.8

IdkSdry s.8

ldkg dry s.8

Igkgdry 58pCftgdry 5.8

LidfS dry 11.6

ldkg dty 5.8

ttgtkSdry 57.9

USikS dry 5-8

t'dksdry 5.8

t/dkS dry 5.8

!g/kg dry 5.8

t dkS dry 57.9

USftSdry 116

TG lm%7G1m%7G134%7G130 %

1

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SW846 82608 2l-Mar47 22{.',,at47 7m123:| TR

BRLBRfBRLBRLCdculabd asBRL205BRLrc5205

144

BRL

msftsdry 25.4mgikS dry 25.4nWkS dry 25.4rEftg dry 25.4figr'kg dry 25.4mdkgdry 25.4n'g/kS dry 25.4nE/kg dry 25.4mdrgdry 254nrdlq dry 25.4

40-l40 %

+CT ETPfI 21-Mar47 21]lngf'o7 7091167 DS

US/f,S d.y 6.27 SW846 8081A 20+lar-07 25-lrer47 7o3l06a TG

Thts labotutuq rypod is ,rot l'dtd uih4d .a authoriztd funzntre on &a @Er prg..' Rrportable Detection Umit BRL = Below RQortinC Linir Page 14 of 152

Page 149: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samgle IdentificatiooM8F-6 2'-1'sA59464-01

Client Proiect #301-88

MatrixSoit

Received19-Mar-0'l

Collec!ion Date/Timel5-Mar 07 00:00

CAS No, Analyte(s) Resull Fhs A n s *R.DL Dilution Method Ret Pteparcd Aaalrzed Bakh At'agrt

S€mivolrtile Orgrnic Compounds by CC

Orqanochlorine Pes0cides SW846 8081A

Prepared by melhod SW846 35508

3198a€ a-BHC31e{+7 b-8HC31e-86€ d_8HCs€-aee g-BHC (Lindane)

s7-74'9 Chlordane72'54.a 4,4-DDD (p,p,)

72 s+e 4.a-DOE (p,p,)

so,2e-3 4,4DDT (p,p')

60-57-1 Dielddn959'983 Endosulfan t33213S5-9 EndosLujtan,l1031{7{ Endosulfan Sutfate72-20-a Endrin7421-93-4 EndrinAtdehyde76.1+A Heptachtof124!5 Mefiorydtlor1024-57-3 Heptachlof EFoxade8{X,1-3tz Toxaphene5103-71-9 a-Chlodane5566-3.4-l g-Chtodane

5349+70!5 Enddn Keione

Suftogale rccoveies:103a6-8+? 4,+D&Octallwrcbiphenyl (Si

2051 -2+3 Decachbtobiphenyl (Si

Polvcf o.inated Eiohenvls bv SW846 8082

Prepared by method SW846 35454

12674.11-2 PC8 10t61110.4.n-2 PCB 122111141-16-5 PCB 1232

53469-21-9 PCB 1242

12672-294 PCB 1248

11097€91 PCB .1254

1109C€2,5 PCB 12601f u4-2r5 rc8.f621r10e14-4 PCB 1268

Suarogale r€@ligriesl1Na68+2 4, +DB-Oclelluorobiphenyl (Sr)

2051-2+3 Deeachlotobipheny4 (54

Sernivolrtile Organic Compounds by CCMS

BRLBRLBRLBRLBRLBRLBRLBRL

BRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

45108

BRLSRLBRLBRLBRL8RL

BRLBRL

4075

pgKS dry 6 27

US/KS dry 6-27pS/kS dry 627

ugkg dry 627

ldkg dry 314pdkg dry 6.21

udkS dry 6.27

f.ig/kg dry 6.21

!g/kg dry 6.27pg/kg dry 6.27

!g/kg dry 6.27

!g/kg dry 6 27p$ftg dry 6 27

lSn(g dry 6 27

sdkg dry 6.27pS/(g dry 6.2/

lSixq dry 6.27

ldkg dry 31.4

ldkg dry 6.27

lig/kg dry 6.27pdkS dry 6.27

30-150 %3Gl5O To

lSftS dry 12.5

ldkS dry 12.5pg/kg dry 12.5

udkg dry 12.5

lSikg dry 125pdkS dry 12 5pg/Kg dry 12 5

!g/kg dry 12.5

ldkS dry 12.5

3U150 %30-150 %

pS/kS dry 630

uS/kSdry 630

Ug/kg dry 630pg/(g dry 630

!S/kS dry d30

lgks dry 630pdks d.y 630

lSftS dry 630

1

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SW846 8081A 2O-Mat47 25-Mat47 7031064 TG

sw846 8082 21-Mat47 23+Jlar07 703116/'

Semivolatile Orqanic Comoounds bv SW846 8270CP,epared by method SW846 35508

83-32,9 Ac€naphthene208,964 Acsnaphthyiene62-5!3 Anilin€i2G12-7 Anthracene1912-24-9 At€zine103-331 Azobenzene/Diphenyldiazine9247-5 Benzidine56-5t3 B€nzo (a) anthracene

8RLBRLBRLBRLBRLBRLBRLBRL

SW846 8270C 22-Ma(07 24-Maro7 7031278 M.B

Thh labontory ftporr k not vald v'irhout or auahotiz.l slpatarc on tha cotu Fage .

a Reporlrblc D€tection Limit BRL = Below ReportinC Limit Pag€ l5 of 152

Page 150: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldcntificationMtF{ 2'-4's45946443

Client Proieca #301-88

MatrixSoil

Collection Dare/Timel5.Mar{7 00:00

Receivedl9-Mar{7

CAS No. Anolrte(s) Resalt Flag *RDL Dilation Melh4d Ret PrcWed AaaIWd Batch A,'/'lyt

Semlvolraile Org{trlc Cohportrd! by GCMS

Semivolalile Orqanic Co$pounds bv SW846 8270C

Prepared by method SW8,t6 3550850-32{ Benzo (a) pyrene20599-2 Benzo (b) fruoranthene191-24-2 Eenzo (g,h,i) perybne20748-9 Benzo (k) fuoraohene

Benzcic acilr0G51€ Benz!4 ekof|1cl11i-91-1 Bis(2rhlooettpxy)m€lhane1tt-,4-4-4 Bis{2-chh.etryt)€66r3963e32-9 Bis(2-chloEisoprop!'l)etheri17-81-7 Bis{2-€hylhexyl)phbetatetol-5t3 +Ekornophent pheny' ethers5{&? BuM benzyt phhatate86-74-8 C€rbazoles9.5o7 44lloro-!ft€tttytphenol10647r +chloroanilin€91{$7 2-Chloronaphthab{re9+s7-a 2€htofahenol7006-72-3 4-Chlclophefl yt ph€nyt ether218{1-9 Chrysene53-?G3 OiberEo (€,h) anthrac€nei32-64-9 Dibenzofuran96.:!Gt l.2.Oid{oobenzene541-73-1 l,3,DichlofoberEene1OM-7 t,4,Dichlorcbenzene9144-'1 3,3:Dichlordenzjdine12C43-? 2.+Dichlotrophenolu&z Diehyt phhatate13r-1r-3 Dimehyiph0rstatei05-67-9 2,+Dlnefftylphenola+74.2 Di-n-butylphrletat€534-s2-l 4,6-Dinito-2-mefiylphenol5t-2&5 2,4-Oinitrophenol121-t4-2 2,+Dinitotoluen€60e20.2 2,&Dinitotoluene1 rru4{ Di-fl-oc{yl phthaht€2t6-444 Fluoranthen€86-7$7 Fluorerig11+74-1 H€xa€l{orcbenzeno87{&3 }texEdbrcbutadisne71474 Hexadorccydopentadien€67-72-1 H€r€c*tlorcethane193-s9-5 Indeno (1,2,3{d) pyr€ne$t2{ t.tlodrynaphthalene7&1t91 lsoptubne91'57-6 2.Llofrytnaphthatene95-4&7 2-Mgthytphenol10s38a, 3,+M€thy{phenol106-44-5e1-2G3 Naphthalene8€-744 2-Niboaniline9s{+2 }Nltroanitine

BRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLSRLARLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLARLBRLBRLBRL

BRLARLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

pqkgdry 630 1

ldkS dry 600 1

ugksdry 630 1pS/kg dry 630 |

trSf€d.y 630 1

PsrkS dry 630 1

ldkgdry 630 |

ldlq dry 630 I

ldkg dry 630 |pSlkgdry 630 1ySAS dry 630 1pdkSdry 630 |pdkgdry d30 1

ldkS dry 630 1pdks dry 630 1

t4/ks dry 630 1pgrsdry &,0 t

tgr(g dry 630 1

ldkS dry 630 1

Ug@dry 630 1pS/kg d.y 630 1pcftS dry 630 I

lidl(gdry d30 |

ldkS dry 6il0 1

USrkS dry 630 1

lrSikS dry 630 1

FSAgdry 630 1

PS/kg dry 630 |

ldkgdiy 630 1

|lSn(S dry 6il0 1pdksdry 630 1

ISikSdry 630 1

FC^S dry 630 1pdksdry 630 |

IdkS dry 630 1pdkS dry 630 1pSftS dry 6:10 1

FSftS dry lI)0 1pdks dry 630 |

ldkgdry 600 1

rcfl(S d.y 6il0 I

Ug/kS dry 630 1

ISilqdry G30 1psilgdry 630 |

Fdkgdry 630 |

fldkSdry I

ldkg d.y 630 1

IdtSdry 630 1pCftS dry 630 I

Idrgdry 630 |

Thit lzbontery tqorl is r@t ialu wAhoa .n aalhodTd sigaate oa lhe colet pqe .

+ Reportrble Detection Limit 8RL = Betow RcForting Limir Page 16 of lJ2

Page 151: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldsotificationM8F-6 2'-4,

sA59464-03

Cli€nt Proi€ct #301 -88

MatrixSoil

Received

19-MaF07

Collection Date/Timel5-Mar-07 00:00

CAS No. Analrte(s) Resull FIag Uzis ,RDL Method ReJ PQpored Anabzrd Bokh Anarysl

Semivoletll€ Orgaric Conpounds by CCMS

Semivolatile Omanic Compounds bv SWg46 8270CPrepared by method SW846 35508

100-01{ 4-Nito6hiline98-95-3 Nikobenzene8a-75-5 2-Nitrophenol100{2-7 4-Nttrophenol

62-7+9 N-Nitrosodirnethylamine

621$4,7 N-NitrcGodi-n-propylamine86-30-6 N-Nitrosodiphenylamine87{6-5 penlachloropfEnol

8541.8 Phenanthfene10&95 2 Phenol129'004 Pyrene110-m-1 Pyridine120.82-1 1,2,{-Trichtofobenzeness-9t4 2,4,tTrichtorophenol86{G2 2,4,&Trichtorophenol

Suftogate reco|,En€'s:32140-a 2-Fluorobiphenyl

367-'2-4 z-Flu(nophenol

41654a4 Nitrobenzene4'

4165-62-2 Phenol4s SO1718-514 Teryhenyt4l4 8611e79-6 2,4,6-Thbronoph6nd 7l

Torrl Metats by EPA 6000f10o0 S€ris Methods

BRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

77

71

Compl€ted

BRL

BRL

0.0r55

BRL

0 0070

BRL

0.0454

BRL

86.0

ug/kg dry 2520

ug/ks dry 630

ldkS dry 630

!s/ks dry 2520pdk0 dry 630

lig/kS dry 630

lSikS dry 630

lis/ks dry 630

t s/kg dry 430

PSn(g dry 630

lgil(g dry 630

lqkg dry 630

!S/kS dry 630pdkS dry 630pdkS dry 630

m-130 %15-110 %30-130 %trl t0 0A

30-130 %15-110 %

mg/kg dry 0.0342

mg/kg dry 1 13

mgr'kg dry 1.7o

ng/kg dry 0-566

mg/kg dry 0.203

ogr'kg dry 0.566

mgftSdry 1.13

mg/kg dry 1.7O

mgfl 0.0r0o

mg/l 0.0150

mgl' 0.0050

mg/l 0.0025

mSI 0-0050

mg/l 0.0o(Xo

mSl 0.0075

mg/l 0.015t)

%

I

I

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SW8{6 8270C 22-MatsO7 24-Mat47 7031278 M.B

7439-97$ Mercury

Totrl Metds by EPA r00 Series Methods

74'lO 22t Salver

74.10-38-2 Arseoic

7440.393 Earium

7,r4or3-9 Cadmium

74-4047-3 Chromium

7a39-921 Lead

7782-492 Selenium

SPLP Extraction

7440,224 Sitver

7440 3A-2 Arsenic',440-39-3

Baium

7440-43-9 C€dmiuh

7440]7-3 Chromiqm

7439-97{ Meac1lry

7439-92-1 Le€d

7782-4$2 Selenium

C€deral Cft etni3ary Psrsmeasrs

% Solids

o.208

BRL

13 .6

59.1

1 .97

23.1

297

BRL

1 SWE467471A 23-Mar47 26-tvlar{7 7031306 YP

EPA200.7 23-Mat47 24+,4a(47 7031305 HB

SPLP Metalr by f,PA I I | 2 & 60001000 Sertes Methorts

1 SW8461312 21-Mat.o7 211\lat47 7031229 BD

1 SW846131260108 22-Mat-O7 23.tr\Aa(47 7031323 LR

1 ''1 "

t "

1 '

I SW84613127470A ' 23-Mat47 7031324 W

1 SW8{6131260108 ' 23-Mat47 7031323 LR

1 "

1 S[,f2540 G Mod 22-Mat47 22-Mat47 7031307 YM

Thls laborulory rcport is aal tclU wirto( an aulhoriaed signatarc on the @ve, page.

+ Reportable Dercction Limit BRL = Below Reporting Lidl Page l7 of l52

Page 152: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 153: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-7 2'-{'sA5980l-01

Client Proiect #30r-88

MatrixSoil

CoLlection Date/Time26-Mat-07 00:W

Received27 -Mar-07

CAS No. Ana\,te(s) Resall Flos A n s *RDL Dilution Method Rel. PEpored Awlrzfll Bach AnalJts!

Vol.til€ Organic Compornds

VoC Extracrion Field exLacted

Volalile organic Camoounds

Prepared by method SW846 50354 Soil (low levet)

76131 1,1,2'Tidrlootdnuoroehane{Fr€on 8RL6I+41 Acetcne BRLr07.1$r Acrylonitate 8RLJ14+2 Benzene 8RL

100{61 Bomobenzene 8RL

1447-5 Bromoc+ioromelharE BRL7}274 Bomodichlommelhane 8RL

15-25-2 &omofonn 8RLt4-83'9 Bornomehane 8HL784+3 2-Butanone (MEK) 8RL

10,1.51-3 n-BltylbB.rzene BRL135.98-8 sec-gL{ylbenzerE BRL

98464 lerl-Butylbenzene BRL75-15,0 Carbch disutfrde 6fl1

IUA

p4rs dy 21.0

PS4€ dry 421

$/kS dry 21.0pS4S dry 21.0

$*S dry 2l.0pglrg dy 21.0pdr(S dry 21.0

rcAS dry 21.0pdls dry 42.1

Pg/tS dry 210

llg/kS diy ?1.0

rrgls dry 21.0

ldkS dry 21.0

trS4S dry 105

pS4S dry 21.0

}4^S dry 21.0

l4AS dry 42.1

|Jg/rS dry 21.0

pdxs dry 42.1

lgtS dry 21.0

pVlS d,y 21.0

|EtS dry 42 |

$/ks dry 21.0

!S/fS dy 21-0

IAAS dy 21.0

lSftS dy 21.0

ptsdy 21-0

Msdry 21.0

pSAS d,y 42.1

pgr(! dy 21.0

!dk! dry 21!

Udlq dry 21.0

ldkq dry 2l.0

ldfS dry 21.0

|4,tS dry 21.0

iVtS dry 21.0

ldkS dry 21.0

!s/rs dry 21 0

tS,& dy 21.0

MSey 21.0

t]oAS dy 21.0

lgrq dV 21-0

llgAsdv 210

pSf.S dV 21.0

tj['t!0dy 2ln

l'dlq dry 21I

UdlS dry 210

pdlq dry 210

pdts dry 21.0

voc

sw 846 82608

28-Mar-07 28-Mar-07 7m176?

5Fr+5 C€rbchteiEchtodde10S.90-7 Otlorobenzene7s{l}3 Cfiloro€l}€n€6/{6 3 Chlorofom71-87.i Cilorofieharc96-49.0 z-Cruorotduene10641-4 4{Hoaololoene

9t!12-s 1,2-Dibrom+Sdtloropropane

124-!41 Dibromodoron€har€106sH l,2-Dbrcmo€thane{EDB)

749s3 DibronEmethanegtscr 1,2-Dsorobenzene

54r.73.r 1,3-Di$toob€nzene10e.{67 lj-Didtlorob€nzere75_71-8 oichloodilluoromethane(Fre!ni2)E*3 1,l-Dichloroelhane

10746-2 l,2-Drchloroelhane

75-35-4 l,l-Drchloro€lhene

156592 os-1,2-0ichloroethene

156@5 tans-l,2-Didooelhene73{7.s 1,2-Oc.iompropar€

1{2 26e 1,3{)id oroprcpar€

s942G7 2,2-Dichtoopmpane

s63.s8-6 1 I -oic+toroprcpene

10061{1.s cist,S.Didlo.opropene10061-t2€ trans-l,g0ictilooptopene10041-4 Eryb€nzene

875&3 Hexachtoobutadiene

5e1 73 6 2-H€xa1on€ (MgK)

98-6e-8 kopropytb€n:€ne

e9-8/j +lsopropy'lduefl€r&4-04-4 Msttyt t€n-blty' €th€r10€nGr 4-l,lethyf2-penbnone{M|BK)

7549-2 ft,telhylenechbrtje

91.20-3 Naphhalen€

BRL

8RL

8RL

BRL

8R!

8HL

BRL

BRL

BRL

8RL

8RL

8RL

BRL

BRT

BHL

BRL

BffL

BRL

BFL

BRL

BRL

BHL

BHL

BRL

BRL

BRL

8RL

8RL

8RL

BRL

B8L

BFL

BFL

881

BRL

Thb labo4to,J, rcpod b nol talu fiUhoU aa authortzed sigdtttu.e on lhe cot$ page.

+ R€podable Det€crion Limit BRI = Below Reporting Limit Page 3 of 154

Page 154: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samol€ IdentificationM8F-? 2'-4'sAs980l-01

Client Proiect #30t-t8

Collection Date/Time26-lvlar4? 00:00

Rectived27-MaF07

MatrixSoil

CAS No. Analrtz(s) Result Flog Uait **DL Dilatio.t Mdhod Rc[. hepated Anabzed Bath A^olW

Voldile Orgrnic Compounds

Volane Orcanic C!.ruounds

Prepared by method SW846 5035A Soil (low t€vet)

1@{5.1 $-PnflA€nreie BfrL

lllc'P.5 SlyrEne BRL

6s!20{ 1,1.11-Tetraohloodnane BnL

?83,t6 1,l2r-Telradlorodl3ne 8RL

1n-1s1 T€fad ooghene BRL

106-0&3 Tduefc BRL

'I{1-€ 12,}T J olob€n2ene BFL

120-82-1 I,2+T*t oobejlzen€ 8RL

7l-5s 1,1,1-TdJ oroetlane 8fi1

?Bs6 1 ,'12-Tfthloroe$a1e BFL

19{16 Td* otoet\ore BRL

Td$lonftrorofirehane (F€dl ll) 8ft-

$l8t tz$Td$lorQropane BRI

96-63.6 1,2,+Tft1€hylbenzene BRL1n06't0 1,3,$Tdmstrytbenzefle BRL

?v14 Vhy' chlod& 8RL

133+2ol n,pxtle0o BRL

9t17.6 exyi€fie BRL

1099s4 T€lrafi@uran 8RL

6G2e7 Eryeher BfrL

99{453 T€n-anyl meftyj s$er BFL

637{J-3 Ehyll€d+dy'ef€l 8FL106?l!3 Di+opmgyletitor 8RL7$5q) f€rl-gutanol/ buM alcord BRL12+s1.1 1,40i(*arc BRL

d6t @r +EflNitMobenane 95

M7-h-t fdudv$ 16170f,474 1,2-hfilotd11dE44 I$Etttnil Dkryr'fir{'onahme !)6

f, xlrlct{ble Petrolerm Hydrocirbons

Enradabl€ Totd P€trcle0n |Mrc.aftoos

Prepard by .nehod SW846 35508

BRL

BRL

8R-

BRI-

BHL

BfrL5,070Colc{lahd as5,0705.070

t'Vhgdr) 21-0

|Jg4SdY 21.0

lgkS dl 2r.o

tgrS dry 21.0

ldts dy 21.0

|'Er'lq dy 2!ll

tgrgd'y 21.0

lrylq (} 21.0pyto dry 21.0

lgrS d') 21.0yg&dy 21n

uc4q dy 2r.0

USIq df x.0

lglq d! 210

lg/kdy 21.0

lsl€ dy 21.0

ldEdry 210

|lyrSdy 210

lgkSdy 2t.0

lErS dy 21.0

lgtS dy 21.0

tryl€try 21.0

lSIq dy 210

lalrg st 421

7lllg 70

7F l f i%

701f i%

7tr1& %

rWkS dr, 1240rldh dry 1210msredry 1244mylSdry 1240mg/lq dy 1240nS.,kS !q' 12{0mq/rg dry l24onE/l€dry l21omgrqdry 1244mgtSdry 1240

1e140

s'vt 846 &604

|cI EIPH

I

I

l

I

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1

1

1

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29-ltrri{7 2$Uarfl ffi1?S0 ru

&661.9 GardinB6s4?G.!-2 F!elo{f26847e31'3 Fu€t 0d*46ss}00-4 Fuelol +61f91100000 l,lotorol

ro1w0 Alialih FLd

unil€nt'fiod

ohe. olTdd Potden tidocarboGC!.c36 Alirhatic Mrcaitons

Semivolrlil. Org.nic Compo!trds by CCorganodh{in€ Psdi.ites SV{8,46 8081APrepared by method SW846 3g5As]D2 Aktin

2g-llar{? $}l|3I{7 700177?

BRL ldlqdy 6t9 swB,{6 808rA zg-,lizrnT 02.Apr{7 7m1739 IG

Thb lahonlary rqoti it rrot ttdid w&hod an auihatizel ipatuE on aha coea page.

' Repotuble D€tection Gmn BRI: Belos, ReDorririg Limit Page 4 of t54

Page 155: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiooM8F-? 2',-4'

sA5980l-01

Client Proiect #30t -811

Collcction DatelTime26-Mar-07 00:00

MatrixSoil

Received

27-Mar-07

CAS No. AnalJte(s) FloC Units *RDL Dilutiot' lrlethod Ref. PrepaEd Ancbzed Bot..h Anavsl

Semivolatilc Orgrnic Connounds by CC

oeanochlorineFesricides SW8468081A

Prepared by method SWB46 3545A

319-84-6 &BHC31+8s-7 b-Bflc319-86.0 dBHC58.8e.e *BhC (Undane)tt-7+9 Chlordane?.s+8 4,4"O0D (p,p)

72.55-e 4,4!00E (p,p')

s02s3 4,4L0DI h,p,)60.tr Dieldlin

95+9{l-0 Endosulfan I

30213-619 Endosllfanrm147'8 EndosulfanSulfale72-20-6 Er in74214X-1 Enddfl Atddyde76-r,13 Heptachtor

2415 Mef|orylhlo(102+57 I H€llachlor Epoxide&Il13t2 Toxaphene5r@719 a{hlordde550e34.7 g{hlordate

53,194.705 EfidinKelone

1e?raa.2 a,a.D84cEnuotobbhenl(54

N1++3 Decehtonbipheny)(k)

Polvchlodnated Biohenvls bv SWe,46 8082

Prepared by method SW846 3545A

1267411.e PCB 1015111M2e2 PCB 1?2|l l14r 165 PCB 1232$16921-e PCB 124212672 As PC812481r0e7 6+r Pc8125411mfi25 PC81260373242+5 PCB 12621110s14-1 PCB 126g

1038644.2 1,4-D84clafluottu0lgnl64

2051.24.3 Decd otobiptEnyl(*)

S€mivolrtit€ Orgrnic Compounds by CCMS

S€mivolalil€ orcanic Comoounds bv SWB46 8270C

Prepared by m€thod SW846 35508

3$349 Acemphhene20s46 0 Acenaphthytene

62 t13 Anillne12n121 Anlhfacene1912-21-9 Alra2ine1q!$-3 Azobenaene,Diphef4ldiaane

9{7.5 8€nzidine566$3 B€{Eo(a)anthrac€ne

SFL

BNL

BFL

BNL

BffL

BFL

BFL

snLBRL

BHL

BFL

BFL

BHL

BRL

BRL

BRL

BRL

8RL

8HL

BNL

BRL

59

108

8RL

8RL

BRL

BRL

BRL

BRL

BFL

BFL

BRL

fl

fl

BRL

BRL

BRL

BffL

BHL

8Rt

BRL

3,e50

65.9

65.9

65.9

65.9

33{)

65.9

65.S

65.9

65.9

65.9

65.9

65.9

65.9

65.9

€ 5 9

65.9

65.9

sto659&59659

ps,'lq dy

ldks dry

!S/iq dry

fdks dry

!s4q dy

lsxq dyps q dry

lsnq dry

!g4q dry

uc4q dry

udkg dry

uqks dly

lqks dry

ldlq dry

ldlq dy

lE|q dry

|lg/ks dry

|.dks dry

|lg,lg dry

$4q dry

|ls^sdry

3A-154%

3Gt50 %

!SI(g dry

!g/lq dry

pglq dy

pyrq dy

usnq dy|lglq dry

pdkg dry

wts drypdkS dry

# t f l%

fr-150%

s',Y846 8081 A

sw846 E08?

sw846 8270C

I

I

I

I

I

I

I

I

I

1

1

I

l

l

1

1

1

2E4a"{7 02-Atr47 7031739 TG

132

r32

t32

132

132

132

132

132

1 U

z&l',lar{7 30-Mar.07 7031738 SM

usks dy

usiq dyp9rk9 dv

Fdkg dry

$/rs dry

lsl|(s auStS dry

ldks dly

768 r768 I

768 I

768 t

768 1

768 1

768 I

768 I

29+1arc7 0!Apr'07 703124 M.B

Thb laborulory rcpo4 is trot valid without an zaahoized sigaature on thc eovcr prge .

' Reportable D€tection Limit BRL = Belo,x Reponing Limit Page 5 of 154

Page 156: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dedtificationM8F-7 2,-{'s459803{l

Client Project #301-88

MatrixSoil

Collection Dat€y'Time26-Mar-o7 00i00

Received21-lia.-01

CAS Na Anotytc(s) Resa,A ntg Unis 'RDL Dilltio,t Lldh4d Retr, PrcWed Analfzed Boftk A,,4lfst

Semtvolrtile Orgrnic Compoobdi by GCMS

Semivolatls oroglic Comoounds bv SW846 eB70C

Prepared by m€thod SW846 35508

:G!a{ 8€rED {a) pyrene

a5{9.2 Benm(b)fluoranhone191.2,1.2 B€nzo (glli) peryl€ne

207{a9 8€nzo (k) ffuoranhe'les6ss{ &natc a.id1@516 Ssqlrtcotol111€rr As(2d|hroatloxy)n'€han€111-414 Bis(ldllordfit)efief

$s.!e-D 8js(2drlooi6oproptl)g$er1r7-0r.7 8i{2€ryhoxyt}phfidale101_563 4€dmph€ny' phenyt etEr85.6&? &rMbst4tpfifElale8F744 Csbazolesgsr}.',r {4hloo.3{rBlfuphend

10G47-8 44hlo.oddhe

s1-s&7 2€Hq,onafht|d€ne

s7{ 2{hlo.opha,ld

ruF72-3 {act orcdrsyl phg]yl€tref

210{1-9 ChryE€n€597G3 Dibonzo (e,h) anilEcae13e{49 ob€luotulan

S5Gl 12-Ddloob€nzene5417$1 l,3-Odltotot€fterc106.1&7 t,4{)icilo.ob€nz€fle

91€+1 3,3'-Dichbltrenzidne120-€+2 23{ktotophonolat&2 oiefM pafietaie

13rr1.3 Dicttyl pfthahb

106'6-r.9 2,4.Orn#rylpheflol&112 D-n-h4yl phfiatals

$4521 4,eDiniu.!.2meryphenot

51'28-5 2+fini[lphCtoll2r-l+2 e4.oiritobtusne6{6,2!-2 e€{hitoblt e{err7-€r{ o-n{dt pnhalab

a6444 Fluordrfi€ra{St$? Fluorrlo

11&7+1 H€xddoobgrz€n€

E7{8-3 }tsxddJo|ohJhd€n€

17171 Hexadtoroqcbpenladiene

6l-721 lleiad OO6U€IErs30-5 h&no (1,a3<4 pyEneqr12{ l{,tstttitnaFfial€ie781&1 lsophorfie9r5/-t 2{r€{tylneph{rahrcs{€.7 2.t{dtt}dphed

10G3!'-4, 3,4-l,tst$&h{rdtEn45S1.203 t{aFtDlffF&fu 2{nroaflfln€9rF2 }t{itwnilne

8fit-BRL

B8LBFLBFL8R-BRL

BFLBFL8RL8FlBRLBNLBNLBRL8RLBFLBFL4,9008RL8Ft

MLBfiLBFLBRLBRL8RL881BRI.8RLBRI8RL8nLBFL8RL9,370gRL

BNL

BFLBRI.Bft-BRLgfiL

B8L8FLBFLBH.

8FLBFLBRf

lc|qA$/tq d)

|]9r9 tryudkg dyab dvFS{q dy

r4rc dy|jgls d]

lgls dy

Ars *y!91€ dy

|lg/t€ dl

wts dvlglq dv

ugts dy

IJdE A

!S,lq dV

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tdlq dy

|dlq d'v

|,glq dry

ldrs dy

lgxS d)

ti4kS dy

Uglrg dy

|dE dv

abdvldks dy

|Jdis ey

ryrg dry

|dhdry0lg dv

ldh aldlq dy

wk! dv

E/lq dy

|lglqd]

|Jdlq dy

ldlq rt

vllt dy

t{/l€ dry

$,lqdy

|{lq dV

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Elq dy

|dh d-y

@ev

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lglq dv

766

m!

768

76E

766

768

7€8

768

766

766

768

768

766

768

ru7e76€768

76t

768

7€8

7t8

76€

7€f

7€E

768

768

768

768

ru768

768

768

768

768

768

768

7€8

7€8

768

766

768

76€

sw846 8270C 29.1'rer.07 o3-t{'47 7031774 lil.B

Thh leborultry report Lt aot rdU withnct on salhoizcd slgnals.e od thz cover psgd .

+ Repofbble Detection Limit BRL = Belo* Reponing Limit P.ge 6 of 154

Page 157: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samolc IdcntificationMEF-7 2'-4'sA5980l-0t

Client Proiect #30r-88

Collection Dare/Time26-Mar-07 00:00

MatrixSoil

Received

2'7 -Mnr-07

CAS No. Analrteq) Result Flos Uni6 *RDL Dllurbn Method Rel. Prcpated Analyzed Batch Anabst

Semivohiile Org{[ic Cohpornds by CCMS

Semivolafle orqanic Comoounds by SW846 8270C

Prepared by mothod SW846 35508

100{1{ 4-Nilrcaniline98-9s'3 Nilrob€nzene88-75-5 2,Nitrophenol!0042.7 +Niliodenol627t9 N-Nirosodimefrytanine621447 N-NiEosodi-n-propytamine8630{ llNihosodiph€nytanine678e5 P€nlachlooph€nol85{l-8 PlEnanlhr€ne10e95 2 Phenol

110+6.r Pyddn€120-8p-r 12,4-Tnchtomb€rEene

9G954 2,4,5-Trichtorcrphenot88-0G2 2,4,6-Trichlomphenol

3216o4 2-Flwohiphenyl

3n7-124 2-Fluotophgnol

{165JG! llitdenzene4'

4te6-62,2 PtEt1ol4,

1713 5r1) TeAhenylaC4

tt&Ni 2,1,&Tribnnophenol

2941at41 03-Apt41 lb1-t74 M.88RL

BHL

BHL

BflL

BHL

BflL

SRL

BRL

BFL

BHL

10,2n

BflL

BRL

BRL

BRL

u58

n60a4n

sw846 8270Cug^s (y 3o7o

|lg,{S ry 768

|4/ks &y 7€8

lS,rc dry 3070

WkS dry 768

!S/kS dry 768

WkS dry 766

udkS dry 7€E

pq/tg dry 7€€

llg^s dry 76E

rgtks $y 78

lC(g fy 76€

lqrs dry 768

UgftS ry 7€a

fgftS fy 768

34130 %

15110%

3+1@ %

t5-110%

30-130 %

t5-1tD%

mdks dry 0.0704

mo/kg dry 2.21

rndhdry 332

rgAgdry 1r1

nrg,lq diy 0 553

mdkg dry Ll1

nSftS ey 1.66

mCfto dry 3e

mgn 0.0100

mg/I 0.0150

ng.4 o oo5o

mgl 0.0025

mgl 00125

firg/r odlMl

mga 0.0075

rngl 00150

sw846 7471A

EPA200.7

sw8451312

sw846 t312/60108

sw64613t274704

sw8.461312]6010a

Sll2540 G Mod.

Toaal Metrt! by EPA 6m0/7m0 seri.s Merhods

Total M€trls by EPA 20{ Scrier Methods

714t.22-4 Sitver

7{,O.3S2 dsenrc

74|+393 Eaium

7110-43-9 Cadmium

I44o47l Chromium

743992'1 L€ad

[email protected]? Selenilm

A2-4.{n47 03-Apr-07 7031810 YP

BBL

10.4

91.6

o0 l8

n.5

574

8Rt

02-Apr{7 HB

SPLP M€t ls by EPA 1312 & 60007000 Sert$ Methods

SPLP Exlr&lion compl€l€d

4J-n4 Sitver BRL

714I3&l Ars4nic BRL

7.{rl! 3+3 Badum 0.0106

744G'|}g Cadnium BFL

7,110-4/-3 Ctrornium BRL

zlss 97-6 Merc!ry BRL

74!+Se,r Lead BRL

nv4s2 Sslenium SRL

Gen€ml Chemislry Prtrmeters

% Solids 41 5

2B-Mar07 2&mr-07 7031763 BD

30-ttar{7 02-AF{7 7031806 Ln

" @'Apr{7 7031806 YP

' C-Apl{7 7031E05 La

3&tuar{7 3&Mar.07 7011879 YM

This hnonhry Epo,l ir not vdu withod ar cuthottud sigatan on thc cover page .

* R€porlable Detection Limir BRL = B€low Repolting Limii Paee 7 of 154

Page 158: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample lde[tificationMtF-8 ?'-4's,A59803-02

Clieot Proiect #30t-88

MatrixSoil

Collectiop Date/Time26-Msr{7 00:00

Received27-Mafi7

CAS No. Anavta(s) ncstdl Flos Ani6 *RDL Dihttion Method Retr. Prcporcd Arebapd Bouh Anabst

Vohdle Orgsnic Compounds

VoC Eiffaditn

Volatile OKanb Comoqln&

Field e!(ad€d

lglq dv

rigkS fy

|4h dv

|8lqdv

|lgIq dY

|ldl€ d]

wl'gdt

!dk! dtl

B/tq dy

EIq dy

rrtbdtugh rvHAo dlwrgtlrt4l4dyudl(etvidlqdY

wks trv!S/fq dV

ldlq dry

Ah *v

r4h d'y

!91q dry

!9lq dt

Irgt0 fy

!g4q dv

H/lq dry

|dh d'v

rdk d'y

!04q d]

tlgts fv

Eq t r ylsrq fry

|!lq dry

I{i€ dry

!o/Iq dV

lgrS dry

lsnq dry

|dkg dry

rdbdvtdlq dry

|4rg 4v

|Js/ks d)'

us,/rs Y|ldb fy

l4lqdv

US,lq dy

$fig fv

t'gkS &y

voc

sw 846 82ffi

28+&r{7 28.lrar{7 781767

Prepared by method SW846 50354 Soil (low l€v€l)

76.111 1,1,2-Tricntootiffuooehane(F.eon BRLBFL

BFi.

BRL

B8I.

sRrsnlBFLBFLBRL88L8RL8nL8RLSFLBRLBFI.BRIERLBALBFLBRL8RL8RL8RLBRLBFLBFLBRL8tu8Rt-B8tB8L

8FL8RLBRLBRL8RLBFLBFLBRLBRL

BRLENL

BFLEFL8Rt-SHt.8FL

614+1 Aaeloie10r'1$1 k4ionlt'iten4E2 E€i2en€rc6.06n BrcnobgEsl€71171 0r([md orolr€hene.827.4 Srcrsdidrkd(rr\€t1al]e74.2t2 &onoloim7'r.839 Brundnetfte]€?&e-3 2-Buanoio (MEK)

10rr51-8 n Buybqrqn135.98-8 sec-Eulylben2ao€

l€n-0ulylbenz$€

75.1s Ce|bofl di$lfida

5e295 C€don lelEd{dide1084G7 ollod€rEgro7S0.3 chboohane6/,663 cttbotom71'X7 3 ctdo|lln€he/rq$.!$8 2{l{o|ottu€ns106<H a{tlorolduene

9@12_8 l2-Dbromo3diomprqane

124_,1&1 $bromod{O|unetlane1d ss4 l2oib.omoot'an€ (EDB)7445-3 Dhbnomehane9t5G1 1,2.0i$lorobenrene54r-7+r t,$oidllomb€nzene106-{&7 l,+ttdtlorob€nzene

?5714 t&torodiffuoromethane(Freonlz)

lS4 3 l.l{)ichloDe$Ene10/{6-2 l2oidttsogthane

75.39 1,1-0lctoro€tlEn€156-592 cigl,2oid{oroefpne15ffi taansn 2-Dct o.o€tlFn€7B.Er-5 lJ.Dcnlorcpropar€112-289 1,3oidlic@gmFane

t91207 22OirildoFop6ne5A+566 t,t.Oidllorqrope|re

10061{1-5 ciel,3{*liorcpropsn€1[(6]+2J talg-l,alDidr oropr,op€nelllo41{ E$tlbeEeno87{&3 Hoxddoobuhdiec591.78.6 2-Har4tone(MgK)ss&€ hoerlpylb€nzg]€s87{ +&ot oMolu€n€1034{t-r l{ehyitod{rfyleber

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65

tzg

6.5

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&.7

129

6.5

123

6J

55't29

6.5

6.5

6.5

6_5

6.5

5.5

129

6.5

6.5

6.5

6_5

6.5

6.5

6.5

6.5

E.5

6.5

u.7

6.5

84.7

64.7

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This lrfutzloq rqon it noa ed@ w hoa an dtttloizd signonlre oE the cover pgg..

+ Reporbble D€{ectioo Limir BRL: Below Reporting Limit Psge I of 154

Page 159: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-8 2'-4'sA59803-02

Cliert Proi€ct #l0 r-88

MatrixSoil

Rcceived2'l-Mar01

Collection Date/Iime26-Mar{7 00:00

CAS No. AnalJE(s) Resuk FIAS anils *RDL Dilution Method ReJ. Pnpared Anal].Zetr Eatch AMh,\t

Volraile OrgaIic CortrFo{rds

Volatle Orqanic Cornpounds

Prepar€d by m€lhod SW846 5035A Soit (low levet)

103-6t1 nfrcpylbenzene BRL

1m 42 5 Styreoe BRL

630-?0 6 1,1,1,2-T6lradlloroelhan€ BRL

1+t+5 1,1,2,2-Telrachtoroethane BBL

12t.144 Telrachloro€bEne BBL

103 3&3 Tduene BBL

e7{r-5 l,2,3Tn€nbmb€nrene 8FL

lm-6e-r l,a4-Tti{* oroberDene BFLrr 516 1,1.1_Tti*toroehane BRL

7s{0.5 l,l2.Ticitoroshene BRLrs{r$ Tri{:htorD€tn€ne BBL

BRL

BFL

B8L

SFL

BRL

BRL

BFL

BFL

BFL

BRL

8RL

BRL

8RL

8RL

97

103

1ffi

N

BFLBFL8RL8RLBRLBRL3,m0Caid.ilated as3,m03,m0

160

!4ts dy

Lrg^g dy

l4/ts dry

llg/rs dv

9SrrS 6y

$/xS dry

!S4S dryp4kS dry

ur4s dy

lgtg drypdk{ dfy

|ls^sdrypglsdrv

!g4q dry

!g4q drv

!g4q dry

!gt! dry

ISAS dry

us&sdry@xs ev

lSilS (ty

lglq dy

lsfrs dy

lqtS dry

wn$ dv

7V130 %7013/%7G130%70tg%

mdt(s dry 667

mSitS dry 667

mg*g dry 667

mdks dy 67

mElgdry $1

nSI(S dry 67

mgl(g dry 67

mgas dry 667

mdlq dry 667

rnglq dry 667

4+140 %

UglS dry 2

sw 8{6 8260A

+CTETPH

6.5 l

6 5 1

6 5 1

6.5 1

6 5 1

6 5 1

6 5 1

6 5 1

6.5 I

6.5 1

6.5 1

6 5 1

6 5 1

6 5 1

6 5 1

12.9 1

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a 5 r

6.5 |

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4.1 1

12S r

E 6sl Trirhlorolluoromethan€ (FGon 1 1 )s13-r 1,z,3-Tdchtorcprcpanee533'6 l,2,tt.Trinehytben2ene108-678 1,3,5-Trimellrylbenzene75.01-4 Viny' dtodde17tu 7 n,p-Xylene9547-6 Cxylene109999 TetaMofuran

60?9'/ EthylefBr

994{58 Ted€my mehyi efier63742 3 Ethyl lsrt-buM e$€rlG 2G3 D,hopropyl sther75654 Ten€{lanot / butyl alcohol123-911 l,4-Dioxane

4ta-N4 4-g@nofludobenzene

2tA7-26.5 Tdler,e.fr

t7o@4r4 l,28icl d@tlqtE44

I46JS|7 Dibrcnmiuonnethane

f,raractable Petroleum Hydrocarbons

&lraclable Tolal Petroleum ltdroaarbons

Prepared by method SW846 35508

m0G6!.9 Gasoline

684rC3G2 Fuelotl2

6847631 '3 FU! CljJ J4

6€6$aH Fu€lo( 16ms€mcoo otoroil

J001qFI Avialion Fu€l

Llnidentifed

orher ol

Total Petolsrn Hydrocarbos

C$C36 Alipf lalic l-lydr@rbon€

338F33? 14hwo6ldeca1e

Semivolrlile Orgrnk Compoundr by CC

oroamd oflilo Pestiides SW846 8081A

Prepared by method SW846 3545A

@4G2 Atd.in

29Mar-07 &.lt^t47 J0$n2

BRL sw846 8031A 28-1rfffl Oe-AprO7 m31?39 TG

This ltbonloA reporl is ttol vald withost aa aaahoiratt signzrurc on the cryu page

* Reporiabl€ Detection Lirnit BRL = Below Reporting Limit PagE 9 of l54

Page 160: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificationM8F-t 2'-{'sAJ9803-0?

Clielt Proiect #l0r-88

Collection Dale/Time26-Mar-0? m:oo

MatrixSoil

Received27-Mar{7

CAS No. A"zlrk(sJ Res l Fl{g Ania *RDL Dilation Method Rel Pnpated Anaiwd BtEh AnAttst

Semivolalile Orgrnic Compo|rnds by CC

Oruanodiodne Pe6licide6 SW846 8081A

Prepared by m€thod SW846 35454

319-8:16 D&lC319057 tsBHC3r$063 dSHC58{e s gBfC (tjndarc}

,.7+s cltodne12 5,13 a,4{00 (Ap )72 55-s 1,4,O0E(p,C)5c2s.3 4,4!DT1p,p16Gt.1 Uetdrins5998-€ Endo6ufian I321s65.9 Endcudan ll1031-07{ Endog/fansdhto72-@-8 Endin7t21.934 Endfln Abehyde?9{48 Hegtad{or724!s M€fioryd or102+57-3 H@d'torEponde3{,01i,S2 Tdaphd|e510c7r-9 achtordane556 r-7 g4hlodan€

E!4s.{-7r"t Eddn Kelms

te4-84a 4,4-Dg4cbftbtdidwl(54

Nr21.i Der,fJlht&ipw (St)

Pohahlorinald Bid€nvts bv SW846 808?

Prepared by method SW846 35t5A

1267+112 PC810161t1o+2E2 PC91E1rr14r.165 Pcg lzllsr.r6$21-9 PCE 12421A72.En PCg12481109t+e 1 PCB 1254fi(,€632.5 PC81260fie+2$ PCg 1Z&[email protected]{ PC8 t2f8

1N&.84 1,+08.&'eiwteMyt(Srl

N12.:3 De{a./,otc6ip]l€nl(54

Scmivolrtlle Orgroic Comporndr by GCMS

Semlvolatl€ Oqanic Comoour6 by SW846 e27OC

P.epa.€d by method SW846 35508

al@4 A.enapfibs|e1846.8 Aconaphtlylons82-s3.3 AnitirEl&\2-7 fuhracdE191?+4{ Afazin€10933-3 Alobon2€i€/Diph€ny'da2ine94.C/.5 8fiidin65G5F3 SduD(a)uihracerE

BNL

8RL

BHI

BHI.

BNL

BRL

BRI

BRt

8FI-

SHL

BRL

BRI

BRL

BF(

8nL8ALBFLBFI.8RLBFLBRL

58ttt6

BNL

B8L

BFL

BRL

BRI

8n_8RL

BNL

BFL

fi

BRI.BRL8RLBRL8fi18Ft-BRL1,f6

2t2262x2x2r31

26.2282x2x2a2626.2ffi2x2x26262t3 l262

2%2

!91€ dypdls dv

!c/rs d]

|ls,fts dlv

lgilq trvpdlq dvpc4q dry

usrq dv

|jdks rv

tilgdrlt4l4d.v|.€/lq dy

ugrq dY

lgrq trv

ldks dv

alq fv

l4lq dv

lgre dv

|,c4s dv

lgtg tv

tigAg dy

*150x*tg%

!s4q dY

llElS trv

lglq dY

$g{q dY

lyxs dY

!04q dry

lgkS drypS/tS fy

|rylqdy

*1flgrlfl %

|lBredY|Jdrs dv$/tg dY

$!Iq eY

rdEdvI'd& dry

Arg dv

lgrg dv

surE46 8081A

sw846 8082

sr!a46 @70c

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2$l,lar{7 @-4p|{)7 7@1739 rG

523

52.3

5L3

52.3

52.3

52X

52.3

5L3

827

u7

e7827nf827

u7

?€]l,Eto7 3{l.l{ar.07 7031738 SM

z$M3r{t O3dIV{7 ?lB1l/4 lr.B

This tzboraurry rqod b noa ealil wirhou an a4dr4ded stg'@tE on th. @eer page .

. Repo.table D€tectiotr Limia BRL = Beiow R€porting Limia Pag€ l0 of 154

Page 161: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ld€ntificationM8F-8 2,-4'sA59803-02

Client Prciect #l 0 l - 88

Collection Date/Time26-Mar-07 00:00

MatrixSoiL

Received27 M -0'7

CAS No, An lte(s) Resu Flag U^i6 aRDL Dilatioa twethod Ref Prepa.ed Ana!]qed Batch Analtst

Srmivolrtile Orgrnic Compoutrds by GCMS

Ssmivolal B oroanic Comoounds bv SW846 8270CPrepared by mehod SW846 35508

5qe.0 B€n:o lalpyrene205-9s.? Berl:oiblfluoranthenels124.2 B€nzo {g,h,i) perytenem?-00-e B€rEoik)fluoranth€n€6ts5.o B€nzoic acidrm51$ B€i4laltohdrrl411 Bis(2drlorc€lhory)rnetEne111.14.1 Bis(2dttoro€h/)ether3s8.4 e Bis(2dtlorois€protyl)eher117.81.7 Etisl2sttytheryl)phthatate101-55,3 +Brcmoph€iyt phenyt ehere6-68.7 Buttb€nzyphthatateuj.74-8 calbazole5$50-7 4{hlorc}m€thytphsdl{16-473, l ,ChlorDeni l inB

91-s&? 2-Chlorcnaphhalene9557-8 z.Chtolopnenol7D05-72 3 4-Chloro9henyl phenytehet

218{14 Chrysenes+r03 Dibenzo la,h) anlha.en€132-64,9 Dibenzofuran95.50.r l,2,Didtorob€nzene54173'1 l,3,Didtlorob€nz€n6116.1$7 l,4,Dichlorob€nz€n691-9,1-1 3,3'.Didombenzidne120.33, 2,4,Ochloroph€nol34{6-2 DielhylphtEtate13i-11-3 Dimefvhhdale10567-9 2,4omehytphend8r-74.2 D-n-bryphihakte

534-52.1 46-Dinitr62{ehylphsol51.2&5 a4-DmtoDh€ml12114.2 2,4-tlnjlrotoluenem6m2 2,GDinitrotdu€ne117_&.0 D{-fl_odyllhfiatatea6-440 Fluo€ntfisne

110'7+1 Herachloob€nzene

tr€!.3 HexacntorDbuladenen414 HexachloMycbpenhdiene

6r rzt Hexact{orDehanere+3e 5 Ind€no (1,2,3-€d) pyr€fl€90.12{ 1+r€thy'naphhal€ns78.59-r lsophorcnosr-t$ 2-frehytnaphhat€|lee&,r&? z_Meftylpheiol

10s39-4, 3,4-Mehylphenol106.14-591.2c3 Naphhelslos&7,r,4 2_Nitroa ines${9-2 +Nilroenitine

BffL

BFL

BFL

BFL

BfrL8RLBFL8RL8RL8FL8RL8RL8fr18RLBRLBRLEHLBHL2,170BHLBRL8RL8RLBRL8RL

BRLBBLBRLBRLBFLBRLBFLBRLBRL8RL4 , t108RLBRLBFLB8LBFLBRL8RL8RLBRLBFLBRf,

BRL

8RLSRL

!94€ dry

!c4q dry

ldks dry

t94q dry

udrq dry

|lg/rq dry

udkS dry

|lg4rS dry

lqfts dry

ugrq dry

ldlq ry

|{y|q dry

!E*4 dry

!S4(S dry

tdrs dry

liS,tS dryp91q dry

US,tS dry

lStS dry

l4,4(s dryydls my

lsas dryps,4(sdrypsiq dry

lgts dy

lgkS dry

rcn.S dv

ldkS d'y

lgks dypqrc d,y

|l9fr9 dry

tS4q dry

!4rs dypSlq dry

!Sn{ dry

US4(S dryps/ksdry

lio/kg dry

lgrs dy

IS,lq dyp4lq dypgrs dryps4q dy

lSeS drv

t4/rg dry

trylq dy

lSftS dry

lJg,4(s dry

lldks dry

l]dks dry

827

827

827

827

627

827

8?7

8?7

827

827

E27

E27

821

827

827

827p7

827

827

421

v1

e7

821

827

MI

827

827

827

827

8?7

w7

827

827

827

427

&1

427

@7

&7

827

427

82f

u7827

827

827

827

&7@1

e7

sw846 8270C

This labomlory repod is ,rol wIU teilhou an aathorized signsture on dte cot)er pagc .

* Repqiable Detectioo Limir BRL = B€low Reporting Limit P a g e l l o t l 5 4

Page 162: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F{ 2,-4,

sA59803-02

Clie Proiect #301-88

MatrixSoil

Colle€tion Dat€lTime26-Mar{7 00i00

Received27 -Ma.-07

CAS Nd Analrte(s) Resuh Fl8 Unia rRDL Dilutio| Merhod Rel, Prepared Anzb.d Bdch Antlyst

Semivolatile Org.nic Coopound! by CCMS

S6mivolalile oroaric Comodnds bv SW846 8270C

Pr€pared by m€thod SW846 35504

100{1{ 4Nitroan'lir}6ga.Osil l.ftobenzslE

8|175.5 2-Nitfopfi€nol

100-n2-7 {-i6lroph€nol

62-754 N-tlitrosadhdMamin€

@14+7 N-iSlrosdi-l}poptlanin€

EG30-6 N.NEosodpienylanin€

E/€G5 P€l achhrophenol85{1-8 PlEnadfi@ne

1(F952 Plt€nol

t2940{ PWerE110{s1 Pyidnetm-€ar 12,+fridorcbenrene

w5.4 a4,s.TrichtoroptEnol&l.0Ga a4,S.Tddrtorophenot

gta-a 2+Iwobiplldlyl

6t-12r 2-Fh.ptWlEM

29+&r-{f7 @A{47 7ff11n4 M.BBRLBRL8RL8RLB8L8FL8Rt-8RL8RL8RL5,65,0BHLBRLBF!BRt

IEIEty 3310

DSikg trt &7

lgkg dry p7

|jg4q dy 3310

14& d,y P7

ttgrQd] @7

p04(s try v7ldkg dy e7

lsrqo P7pdr€ d.y 827$1rqdy 827

I9ISdI U7

pgtS fy &7

lg4qdy P1

l44Sdy 821

9-19%

1+110%

*t30

l S l t o %

30-|fi

t11t0%

nghfrV 0o3i16

ngnq dry 109

'I€nq dry 1.s4

nvlEdry 0.515

mdks dy o.E7

ms.t{ dry 0515

rislq dfy 0.m

trr9lgd'y 1.s4

ruAmgl O01m

ng/l 0.0150

nSI 0.m50

'r'S4 0-m25

mgl 0l)125

rngt 0.m040

mg/l 0.m75

mdl 0.0150

s!\4.$ 8270c

s1lv346 74714

€PA 200.7

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,r165s.0 Nifuar,Eene4' 63

416sjl-2 Ptptptd5 48

t7t8-514 Tqptt yld4 66113-794 Zl,efibtdnoipnd 4i

Totrl M.tsls by EPA 6000t000 Series M€.bods

7{1s975 ti4€rwry 0.912

Toril Merrlr by EPA 200 series Merbodr

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l{0

02-&r{7 0+Asr{? ?431810

11,0?24 Site.

Z[l03&2 Ac€nic

741S993 Baium

7.|]rtl+0 Cadmium

11411-3 Chror Um

BHL

4.86

4?3

0.r17

1 0 1

7'F9€2n Lead 28.3

.r!a-4l!2 S€t€niwn gRL

SPLP Metsls by OPA l3l2 & 60{01000 Sertes Methodt

SPtP Extadlx CoflFlet€d

11,&24 Silver BRL

74{$a&2 AEenic BRL

7'uo3s3 Bai|jn 0.0120

740.4+9 C€drium BffL

7a4017-3 Ctmium BRt

?s-s75 MeEtry BRL

74:Fe-1 Lsad BRL

7t@+2 Sd€niurn BBL

Ge.enl Cteoiltry Prrrmetcr!

%50116 86.6

S{rJ8461312 84afi7 28.1r.r.07 7C}l7E 8a}

SW8,46 1312/60108 3llllar-o7 (I2.I9r.07 78181b tR

Svi€46131224704 ' @+p..07 781806 lP

sw816 r312/m1G ' (P.AI[{7 m1805 t-H

SM2'10G Mod. so{rsrfl Cl- dfl 7dl87r Y[l

Thb la'lorrtorf rcpsd ls .(tt ratd iihou aa atdtoiatn sigrru.e oi ,he @w, prEe-

' Reportrble tltection Limit BRL = Below Rcporting Limit Page 12 of 154

Page 163: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SampLe IdentificationM8F-9 2'-4'sA5980l-03

Client Proiect #301-88

Collection Date/Time26-Mar-0? 00:00

MatrixSoil

Received

27-Mar Q'7

CAS No, Anabtte(s) Result Fl4S Anits 'RDL Dilutinn Mcthod Eetr. P4pared Anabzed Batch AMIFI

Volatile Organic Compounds

VoC Efiraclion

Volatile Oroanic Compolnds

Field €nraded

Prepared by mettod SW846 5030 Soit (high tevet)mr': 1,1,2-Trid orotrifluo.oethane (Freon BRL67-6+r Acelone BFL107-13 r Acrytcjnitdte BFL71-492 Benzene BFL10316 | BomobHzene BFL14 915 Bbmochloomslhane BFLfin4 BromodichtoronefEne BFL14252 Srcmdom BFL7.1-&3I Emmom€tlan€ BFL7&93.c 2-8utanofls (i,tEK) BFL104.s1-8 n-Sutylbenzene BnL13+90.8 sec.Srybenzene BFL9846.6 led-futy,berz€ne BBL7'1s4 Carton disullid€ 8Bts623.s Celbon tdBchlodde BRL

VOC z})Jat4l 28tl,a47 7031761 BD

!C4q dry 61.7

pS4qdry 1230

lglqdy 61.7

pg4q dry 61.7

US*S d'y 61.7

PSIq dv 61.7

US4iS dy 6lJ

W^g dy 61.7

lgftg dy 123

|{Asfy 617pg/l(0 fry 617

tJg4(g dry 6lJ

I0ft9 dry Bt.l

|lg/l(S dry 308

!gA0 dry 617

tCIq dry 61.7

pCIq dry 123

|lvtS dry 617

Msdry tn

lMS dry 611

lrytgdry 51.7

lJgftS dry 1a

|1g^g dry 6l-7

lglq dry 61.7

tyls dry 6r.7

pglT(S dry 61.7

PSAS dr!' 61 7

p!4q dy 617

psAS dry 123

usilq fy 61.7

pS,?.S dy 61.7

!s/ks dy 61.7

pgrcdy 61-7

t'drq dy 61.7

ldlq dy 61.7

tgtlq6,J 61.7

lJdlq dry 61.7

fdksdy 61.1

lo4€ dy 61.7

9dhdry 61.7

l44q dy 61.7

yEre dy 6t.7

lSlq dry 617

!S4S dy 61.7

ru4q ey 61.7

Mq dry 61.7

tgts &y 617

tidh dy 617

tidhdry 617

sw 816 02608

108.9G7 Chlorobenzene75ill3 Chloro€lhane6756 3 Chlorolom/147.3 ChtoromettEne!r5.t9 3 2{hlorotduene10e'|3-4 ,l{hlorctctuene

9e12.0 [email protected] Dibomo4hloromefian€106.93-4 l,2,Obromoehane(ED8)7495.3 Dibornomelhane9+501 1,2-0ichlo(ObenZene54173r l,3.oichloaobenzen€106-45 7 I,4_Dic+ oj.obenzene75-71-8 Dichtorodnuoromelhane(Freon12)16.34-J l, t Oichtoro€than€107{S2 1,2{id1lorc€than€75-35-4 jl-Dchloo€lhsne

15sss.2 ciel,2.Dichtoosthene156rt0.5 tans,l2-Dchloroelh€nen874 l,2.Oc.l{oopropane142-28.9 l,?nidnooproo€rcs9+2G7 2,2.0ic1{oopropanes695€.6 l,1-Didomprcpone1061{1-5 cis-l,S.Didlloropropdl€1006l.02-6 rans-1,3-DidioropDpsne100-tl-4 Ehylbenzene6r{&3 f{exadttoobubdiene591784 2_He|anone (MB(|

S-!?-8 lsopropyftenz€ne99.€7-6 4lsop.opyltoluene1q',1{4.,r Mehyll6nbutyleflerr0&1cr 4+retiyl-2f€nlanooe([{BK)75{9-2 Mehytenechloride91-2!.3 Naphhat€ne

8FL

881

8Rt-

BRt

BBL

8BL

BRL

8RL

BRL

BRL

B8t

B8L

BRL

BFL

BFL

BFL

BFL

SFL

SRL

BAL

BET

BfrL

BRL

8nL

BRL

8RL

8Rr

BRT

BRt

8RL

8RL

BRL

BRL

BRL

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

fi

50

ffi

50

50

50

50

50

50

50

5{)

50

5{)

02-&47

This laboftlory rcpod h ,tol tald v had an althodztl signat!rc on tfu cowr psge

* Reportable Dete.tion Limit BRL = Belovr Repofling Limir Page l l of 154

Page 164: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ld€trtificationM8F-9 2'-4'sA5980t{3

Cli€nt Proiect #l0l-88

MatrixSoil

Received27-Mar-0'7

Collection DatdTime26-Mar-07 00:00

CAS No. Aaolrta(s) Resak FloS Unirs rRDL Dllaliaa trIethod Rctr Prcparcd Analyud Bzlch Argtyst

Vol.tile OrgE tc Co|Ipourds

Vdaile Organic Cofilo0nds

Prepared by method SW846 5030 Soil (high tevet)

1q]-6rr ftPrcpytodone 8RL1m{25 StyrcE 8RL630roi |,t,1,2-Telract{oro6lhan€ 8RL?9.3't5 t,t,2,2-T€trac orc€thene 8RL121.1n1 Tet|adrlooef|ene BRL1os.€r.3 Tolueoe BFL

!761'6 l2,$Trinbrob4nzene 8FLr2o-xar 1,2+Tri* orcbemeno 8RL

7r-s5+ 1,1,1-Tricldoro€tEne BRt

a+5 1,1,2-T J oEe$ane gR[

7941{ lri*brdn€ne BRL

T**{orofiuororcftele (Freon 111 BFL

Flo{ 1,2,}Trit oropmpane BnL

S.6+6 lz+Tf,mghylbenz€ne10s.6I{ 13,$Ttifl*tlylbeozeneTsor-4 Vinydthrids1@&7 m,Fxyleie9647{ DXytaE10!r"9$e Tetr*ydDtuan

@&7 Eqt{et€rg€,HE-8 Teil€myl medry' eltter

67q2-X E$yl brt-tdyt edler1@al3 O-rsoprwyl eh€f

7s3fl1 Tert-Sutenot / hiyt alcohol,'91n 1,+otorane

A,40.4 +ErffiofrN$en|ene

&7161 [email protected]

ttM474 |,2-Ac otoelhene44

l@-5J-/ Dibtonofi@rhalhane

Exlrsctrble Pelrolcum Hydrocsrbons

Eftaclabl€ Total Pgdeum tlydrccarbons

Pr€Oared by method SW846 35508

ffi31.9 Gesdne

6.76{02 Ft€toil*z

6t17+i|ln Firel Ol *4685t${+4 FUelOtt6li0806jo0 it otoroil

"m100mo Aviati)n fuel

t nt sttitd

odl€rOl

Tot l P€totEUm Hydrearbdls

CS{36 AiiDrlaUc Mmarborts

Ne&2 l4ttM&ca1e

Semivol..dl€ Orgretc Compoutrd! by GC

Ouenod odn€ P€sli.ii€s SWE46808'lA

Prepared by method sw846 3545A

3@{l}2 A|ddn

8Rt-

BRI.

8RL

BAL

8FL

BFL

8Rf

BRT

8R|

BNL

BNL

BFL

97

101

v109

8RLBRLBRI.BRLBFLBBL

2450Cdqihbd as2,4S02,450

14:J

pg4q dy 61.7

lqredy 61.7

UdkS d'y 61.7

$/rqdy 61.7

tlgrstt 61.7

r4/hfy 61.7

l4/ts dt 61.7

lryrS d.y 61.7

udhd] 517

l4/lqdy 61.7

tJgU dy 61.7

tlE}gay 6r.7

dts fy 61.1

llg/rs fy 61.7

|lg/tq dy 617

Blqdry 6r.7

lgLS *y tz3

tg4q fy 61 7

l4^Sdy 61/

p0/t€ay 611

ldhdry 5l7

Srqdry 61.7

lgtgdy 617

!C,rS fy 617

uqk0 dy 1ru

7Gl$ %

701f i%

701f l%

76130%

mqre drymgflq dry

tt4/rg dry

rnS,fS dy

oqkg dry

,r'4kS dry

odlq dry

mglq dry

ng[q dry

rng4g dry

1t 40 %

|lgrg dy 333

sw 8{6 82608

+CT ETPII

5050503)505050tu505{l5050fi5l)505050505050505n65050

02dtr-07 oe.tpr{7 7040017 rn€r

2gn ar.07 30lilar{7 7mln2m5 16{b 1

605 1

605 1

605 1ql5 I

m5 1

66 I

606 1

fls 1

sRt s1846 80814 ?€4a-07 {P.AorO7 7G17JB TO

This labonrorf Eqorl is 60l valid l'ithotd dl zurtodad dgEthtn oa the cawr page.

. Reporbble Delectior Umfi BRI- = Bdow Reporring Lirbil Page 14 of 154

Page 165: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple IdentiticationM8F-9 2'4'sA5980l-03

CIient Proiect #301-88

Collection Date/Time26-Mar-117 00;00

Mat.ixSoii

Received27-Mar07

CAS No. At'alyte(s) FoS Unir: 'RDL Dilarinn Method R4 P,elnnd Amlfzed ga!(h Anabtt

Scmivohtil€ Orgenic Compounds by cC

ooanocilodne Pesbcides SW846 0081 A

Prepared by method SWM6 3545A

319-84-6 a-BHC31s85.7 ts8HC319-aS0 d.BHC5&8e-e +BHC (Ljndane)

671+9 Chlordane7?-54-8 4,4'O0D (p,p')

?l.ss-s 4,4LD0E (p,p')

50-2$3 a,a'{oT (p,p i6S57-1 Diet&in959-93{ EnCjoSUIan I3213{5-9 Endo6ulla0 ll1031{7 0 Endostllan Sutlabn2!8 Endin71219X.4 EMin Aldehyde76-44-0 Heptachlor72-.13.5 Mefioxycitor1024 t-3 HeptadrJor Epoxide3mr.3r2 Toxaphsne51037r-9 a.chlodan€tt66.34-7 gthlordan€

5las4 7c5 Endrin Keldre

t0w41, 4,4oe4dafl|&tofulEnt4 l9l,051.2+3 DecehlooMhenyl(St

Polyoh/o[?aled Eiphends bv SW846 8082

Prepared by method SW846 35454

1267+1r.e PCB !016111042+2 PCB 122111r4r.r&5 PCB 123253469.219 rcB 12421267129-6 rcB 1 24€r !097 69.1 PCB 1254]1096{2-5 PCB 1260t:1321-21-5 PCB12621 1 r @ r 1 { P C 8 1 2 8 8

1t30644? 4,4-DSoclanuodiplEnyllsl

20s124-3 Deachl1tohohenyl(St)

Semivolrtile Organic Compounds by CCMS

Semivolalib Orcanic Comoounds bv SWg46 8270C

Prepared by method SW846 35508

83.32-9 Ac€naphh€n€208.96.8 Acenaphthylene61.53-3 Aniline1N.12-7 Anhracene19122+9 Afaane10133-3 Azobenzene/Dipheq4diarine9e-87-5 &nzidine56-5t3 Eenzo (a) adhracene

BRL

BEL

8RL

BRL

ERL

BRL

BBL

BBI-

BBL

BFL

BFL

BFL

BFL

BFL

BflL

8RL

8RL

BRL

BntBRL

BRL

N

104

8fr1

8RL

8RL

BRL

BRL

BRt

8RL

BRL

BBL

105

BRL

8FL

BFL

BFL

SRL

BRL

8RL

1,700

611

67.7

67.7

671

87.1

67.1

671

677

671

750

lSJ

750

750

750

750

750

75t)

tgr(g ory

tCL ! dry

rSfrS dry

|JErs drvysra dry

!SA0 dry

lcas ry!44S 4y

lj'rs 4v

lsnq dv

us,ls d,l

!S/kS dy

!94q dry

lqrs dry

!dl(g dry

$r'sdqUS4q dry

|ls/ks ey

lgts dry

|Js/l(s drv

tqtS dry

wl f l%

&1f l%

UdrS dry

ldkg dry

u91q dry

wrs dfY

vqks ey

lJvkg ory

lJ94(S dry

lgtS dy

us/](sq

3G1fl %

&tlq %

ugrsdry|JEI(gryus/l(s dry

!sr'{ dyps,'lg dry

ldks dry

ldred,ylsnq fy

sw846 8081A33.6 1

t3f I

33t 1

33€ 1

169 1

33.8 1

33€ 1

3S.8 1

!c.8 1

!0.8 1

!4.8 1

33.8 r

33.8 1

33.8 1

33.8 1

338 1

138 1

169 |

33E r

33.8 1

33.6 1

284lar-07 02-ApF07 7031739

sw846 808?

sw8{6 8270C

28-Mar-07 30Mar.07 7031738 SM

?9tt^t47 c&Apr 07 7031774 M.B

Thb laboruaory rcpod k ,toa tolid wAhoul ad a.llho.ized slpzlarc on the coter page.

' Reportable Delection Limit BRL = B€low Reporting Limit Page 15 of 154

Page 166: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ld€ntificatiooM8F4 2'4'sA59803-03

Client Proicct #30 t-88

MatrixSoit

Collection Drte/Time2GMar47 00:00

Received27-Mar-07

CAS N.L AmlrE(s) Fl"C Unlb *ADL Dilaion Method ReJ hepued A tlwi Bdch An^lyst

S€tr|ivolatile Otgrnic Compounds by CCMS

S€mivdatle Oruanic Cdnooun& bv SW846 6270C

Prepared by rnelhod SW846 35508

50n2{ 8€izo (alpyrcnem5.992 o€nzo(b)ffuoranfieoe191242 Bel\Io (g,hj) perji€ie

Ar.0s9 8€{zo(k}lhroanh€fe65'85{ &nzoic ejd1651{ B€nzyj ahoholtrr.!r1.1 Bis(2dfurethoxy)rnetEne11r-4r4 Bir(2d'loroot{)ater386!e32.9 9ie{A.dlbdscpropyl)€fier11t41.1 8b(Z€httrsxyi)phrhdatorn5s.3 +B{crnotaHyt pherryt efter0F4s 7 Bulyt beryl phhatete

s.?'t-8 Cadszolos$sc7 ,t4hlotoFlne{Vph€nol

10Ga7ll 4.chloro€nifin€sl,5+7 z.chlotdBstfulei\ee$r{ Z-ChtolEpl,€nolM5-12-3 44ldorcFheny dslyi etr€r21041.9 OlrySen€51ti!3 Ob€nzo (a,hl antracene132-64.9 oibduofurans5so1 t2-Dicfilorobsdsr€5.1-73-1 r,ltkhlorobenz€nerc€..{e7 l,4{idbrcbenz€n€s1{+1 33--Dbhloroben2ljfl€12!.03? 2,+D**ttrophenols[6e2 Deftylphhatale|31-1r.3 Otr'€fttpftflalat€105+7-S 2,4-Dm4ph€nolw7+2 D,n+ulyj phhatate

a+52-r 4,MinitD2-mdhylpnenolsr.2o-s 2,+Dinitoptend121.14-2 2,+Dinitohtlene@2FZ z,FDnitobfu€ne117€,t-o oi.tuody pfit slate206{,{i FUoGn l€rE6n7 fl-orene1rs7+l ltBxichkcbe$lene&/$83 Hoxad{oobuladenen..74 HgxadoDalrlopentadi$efl-12.1 Hgx# oo€dUne1cl3ss ld€no {j2r3{d) pyrdt€$r24 l.lretldrBphfutae7&5$ | lsdlorqjo9157-6 2+ldiylfiNph$at€nec5.{&7 2lre$rylph€nol

toeiF{, 3,4.lr@phendl{t6-,4+5sr-20-3 t&phfid$e!+74.1 z.Nir@rilinos{s" fi,lito€n ins

BRL

BAL

BFL

BRL

BRI.

8RL

BRL

BAL

8RL

BRL

8RL

8RL

BflL

BRL

BFL

8RL

8Fl

BRI.

470BFL

BRL

SRL

BRt

BFL

BRL

BFL

BRL

BRI-

8RL

8nLBALBFL8FI

8RL8R!3,610g8L

BqL

BFL8RL8RLBRLBRI.BFLBFLBRI.BFI.

BFLBf,LBFL

|ls,4(s dypsrq fiY

ugnq trY

$qd tvlcrq dY

lgrh dy

$/h dv

H/lq fiy

ldlq dv

lsrq dy

!s4q dY

|4rs ryt,474tl

ldls evpgn(sdv

wr!alqLg d-ypS/rg dy

ldrs d}

IS,10 dy

lgrq dYpgrg dv

lgikg try

td}4drl!{rl(s 6v

!9t9 dry

{c/rs dry

!s4(0 dy

|dh dv

$rq dty

|€4q fv

u9?€dtvlJc4sdYlgrg dI

!S,+rS dl

!g/rg dY

f94q dry

l,g/tgdylgkS *y

t04q dvpgls drv

rdkS dry

t94q dv

ru,lq dry

$4q dY

!S/rS d,

lgtS dry

psh d'Y

ucnq dry

|'g4s dy

750

750

75,0

750

750

750

750

7ta

7ai

7fi

7il

750

750

750

750

/50

750

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ffi

750

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79

750

751)

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750

750

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750

750

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7fi

750

750

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swe$ 8270c 2g-lraf{7 (B+F{? 7t6124 ti,!.B

Thh toborubrf rqtod &r not asld fit hotd M atrrhodrrd sBnaUre od lhe cova page-

' R€portable Der€dion Limit BRL = Bebw Repodng Limit Page 16 of I54

Page 167: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sanple IdedtificationM6F-9 2'-4'sAs980l-01

Client Proiect #l0 r-88

Collectiop Date/Ttme26-Mar-07 00:00

MatrixSoil

Reccived27 -Mar-0'l

CAS No. Anatrte(s) Result Flas Units *RDL Dilutinn Metholt Rel, Prcporcl Aaalyetl Batch Ana\'rt

S€mlvolrtil€ Orgrnic CoInpornds by CCMS

Semivolatjle orcanic Corflpounds bv SWg46 8270C

Prepared by method SW846 35508

100-01-6 +Nitroeniline90.95.3 Ntdenzenen475 5 2,Nitroph€nolrm{2 7 4-Nilrophenol62'759 N-Nitro€odimelh!4amine621.617 N-Nillosodi-n-Fopyhmhes6 o 6 ttNilrcsodiphenylamine8r-36.5 pentachtoophenol

85"018 Phenantkenel@9$2 Phenol14940_0 pyaene

110-66r Pyn:dine120{21 l,2,+Triclorobenzenese954 2,4,5-Trid{oopherml3S062 2,4,6-Ticnbfophenol

gt@-o 2-Htbtobipherryl

6/-12-4 2-Fluotjphenol

1165404 M1$qzene4s

4t6542.2 Phenol-ds

t7t&514 Teryh€'ry|-d4

tt31 2,4,6Ttib@noghend

zJNar|T @lvo? 7031774 M.BBFL

EBL

BFL

BFL

BNL

BFL

BFL

BRL

BRL

BRL

3,9.10

BRL

BRL

BFL

BFL

57

52

72

50

66

45

754

751)

7fl

7il

1il

751)

750

750

750

750

750

750

750

udks dry

WxCdtyps/ks dry

fS.ftS dry

Udlq dry

UdrS dry

pdrq dry

pS/kS dry

lgks dry

!s/lq dry

ldkS dry

lEkq dry

pdkg dry

l01q dry

ldkg dry

30-1U%

15-110%

30-130%

tr l t0%

30-130%

trt10%

sw846 8270C

S1iv846 7471A

EPA 2t]O 7

Totrl Metrls by IPA 50{0/7000 S'€ries Methods

743€.97-6 Mero!ry

Total M€tlts by EPA 200 Serics Method$

74!0!224 Silver

74,|0.39.3 Badum

7440-43.9 Cadmium

14!o.11.X Chromium

iB$P,1 Lead

BNL

3 3 8

339

0.411

8.€

26.2

ndrq dry 0.43?2

n'9fr9 drr/ 1.08

mdkS dry t62

mg/kg dry 0.541

mgAS dry 0271

mS,ftS dry 0.541

mglg dry 0 812

n0,4qdry 1.62

mg/l 0 0100

m94 0.015,0

mM 0.0050

mdl 0.0025

nM 0.0125

ngl' 0.m040

mM 0.007s

rng,r 0.0150

@-Aprfl 6SAtr07 7031810 YP

H8

ns2.1s-2 Sdenium BRL

SPLP }Idth by EPA 1.312 & 6000t000 Series Methods

SPLP Extraclion ftmdeted

7440.24 Silver BFL

7,t4G3S2 Ajs€rjc BBL

71!0.39-3 Badum 00106

7140<r.9 cqdmium 8RL

7411047-3 Chromium BRL

713$t-6 Lle{c!{y 8nL

7€S9ar Lead BRL

na24s.2 setenium 8RL

C€nerrl Ch€mistry ParNm€tcrs

% Soiids 90.6

Sw€461312 ze.lna4i 2&i,lar{7 7031763 BD

SW84613126010g 3&i,lar{7 @.Apr{7 7031805 LB

Svfi$1312t74794 ' 02-Arr{7 7031806 YP

SW8461312/€0108 ' 02-A9r{7 7031805 tR

SMzslocirod. 3041a47 n-Nal'07 7031879 YLl

This la.bofatoueport is not raIU x'ithout an aahottad sig&nne o" the uee. page .

. Reportable Derection Limit BRL = Below Reporring Limir Page l7 of 154

Page 168: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdcntificationMtF-r0 t'-4,sA59803-04

Client Prciect #301-88

Collection DatdTime26-Mar-07 00;00

MatrixSoil

Received27-MaF07

CAS No. Anolra(s) Resul! nag U,'i'l *RDL Dih tion Methad ReI, Prepann Adrlyzed Bdch Analfst

Volafl o OLlanic Cqrmunds

Pr€pared by method SW845 50354 Soit (lorr levet)

Tsiil-1 1,12-TrichlorotdfluoEefiano(Freon BFL@&1 Acelone BRLron$r Acryl6nfie BRI71<f2 Benzene BRL1@-0G1 BDmlbg'Eene BFL7447.5 Brcmodlloaomelhane SRL7s271 godDdichbomefEne BFtEE-2 Brcnotoin BHL7r-899 &Dmcrn€liEno BnL78lIr-3 2-Bulanone (MEK) BFL10rs1{ ltsBuiytdlz€ne EFL

trr€6{ s€c€{Vt€nzone ERLgs{fi tert-Eutylbenzone 8RLE1i4 Ca6on diejlfide BFL5&?+s Cartd\ tsirad{odde BRL10&s'7 Chbptjsnz€ne 8RL?5.0c3 Chtofoe0lane 8RLlt{6.3 Cfilorofonn SnL7a{7-3 Chloro.nehan€ BFLs49.6 2-Cl orotolueno BRl,1(F-43-4 4-Ch'ofotdu$o BFt9612-8 tj_Obromo3d o.opropane BHI12'14!1 oibronbdioomeham BFL106!B-1 l,z.Dbrornoefiane (Eog) BFL7{-es3 Dbofibn|9hane 8RLsG501 j2{icnbrob€filene BHt541-7x1 1,$tlihlorooenzer€ BflL116_{$7 l+Ocf oobenzsne BffL7t7r-€ Dchhrodifuofdnethans (Freon t2) BBLIn34 3 l,l-oidllorceftane BRL107.0+2 j.?.0ichlordtlan€ BRL?!54 .1,1-ganlofo€tEne €,qL15&59-2 chl,Z-Dk orDotlone Bntrs6.6os fians.1z.Dcnto|Ddhgne BRLn&'s 1 2old oopmp€ne 8RLrtr2-r8{ i&D.fttsopro0ane 8Rt*2J-7 2:.D0t oropropang BnL5e50.6 l,l Ochtorogogare BFL10{6t{'-5 cts-.t,gDidloroprc!€ne BRL10061{2{ hans-lSoiohtooFDp€ne BRLl0o4r.. E$ytbenz€rE SRL

2&4a/{7 28.lllar{7 7031787 80

?9.{l/'u47 2$irt07 7m1790 RU

Volatile Org40ic ComFounds

vOC E{rftibn

07&3 fleEdloobLiadene

501-70€ 2-Hodlore(MBtqs-€e{ kopf4}tbstz€.I€&E/t 4lsogopythbffe

16314,r"l omy' t€+butt sttlgr1@rG1 4-M€dty1.2{*rb]q1e{MIBK)r5'G-2 lr€trliho€diorid€Er'2O-3 tlaptihals€

ldlq dy 7.4

l44q dy 141

i4/lq dy 7.1

!C4q dy 7.1

lgrS dy 1.4

la4q dry 7.4

ld& drY 1.4

tg/|qdry 7.1

wb dy 14.7

IrEh try 73.5

K/tq dy 7 -4

udbdy 1a

lglqdy 1.1

rrSASdy 368

ldh ff, 7.4

@r0frt 7t

lslqdy 117

IEIS dy 7.4

lErStu 14.7

ystS dry 7.4

uc4€ ('t 7a

E lqdy 141

|Jg/lg dy 7.4

lg4qtry 1.4

ldlS try 7.4

uc4q dy 7A

dl€dry r.1

lElS dy 7.4

lgrlg dy 14.?

Fdlq dy 74

Irdbdry 74

H&a 1.4lgrq dV 74FSIEtrl' 7.1

144€ dy 7.4

Uqnqdry 7 A

lClqdry 7.4

lg/rqdy 7.4

l4rg Ay 7.4

ldlS dy 1-4

lj9k dry 7.4

lgtg dy 74

lElq fy 735

lglq try 7.4

Fglq dy 7.4

pdlqdy 7.4

!919 dy ?3.5

!S/fS dy ns

pdlq d)' t.4

Fidd sxt'd€d voc

S'/V 846 82mI

1

i

1

1

1

1

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l

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BNLBFL0Rt-

8R-8RL8nLBRLgFt_

Ihh llbo.atory ?qa|t is ,td yalid wiahod ad oartoitqd :tignafrare on the cowr We.i Repoftahle Detection Lirit BRI = B€low Repoaing Lirnit Page 18 of 154

Page 169: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationM8F-10 2,-4'sA59603-04

Client Proiect #301-88

MatrixSoil

Collection Date/Time26-Mar47 00:00

Receivsl2'7-M^t-0'7

CAS No. Analyte(s) Resuk FloS Unkt rRDI Dilu.ioa Itethod Rel. Prepoled Ann\rzed Barch Araltst

Vol.tlle OrBanlc Compounds

Volalile Ooanic Comoo{ndsPrepared by method SW846 50354 Soit (tow tevet)r03i!r n_propr,lb€azgn€100-42-s Styre$eff10 204 1, t,1,2.Ieta{htoroethene7s 3rr-5 1, j ,2,2_Tetlachtoroelhane12710.4 Tstrad onethene100 8€-3 Toluene0t.61-6 1,2,!Tri$torob€n:ene12{.8t,1 1,2,+Tdcilorob€flzene7r-55-6 1.1,1.Tridttorelhane7e.oo_s 1,1,2_Tri$torelhane7+01$ TricNoroeh€ng75 6e-4 Trlchlorolluoromehane (Fleon l 1 is1&4 1,2,3-Tdchloropropan€9543-6 1,2,+Tdmelhyibenzer€100t7-8 t,3,5.Trimeh!,jbenrene7Ir01{ Vinyldloride

1310.?G7 n,Fxylene95-47'6 oxylene109.9$9 Tetrahydoluran

60'29-7 Efrvlelher9e,L{s3 Tedamyl melhy ether637.9?-3 E$yttsrt-bl]tyi€lherr0s.20.3 Di,istprop/€lh€r7s{5{ Ted_Butend / bLrtyt almholrzJ.Sr-t 1j-Dioxar€

464CA1 4-Er1mon\O@beizene

to3/-26-5 Tdrcne$

17060474 1,2-IicllwoellBne-d4

186&53-7 Dihbfionwonahane

Exlrrctrbl€ P€troleum Hydrocarbons

ExlEclable Total Petrolefin Hvdrocarb$s

Prepared by method SW846 35508

m06-61.9 Gasolir€6617S1G2 Fuelol {?

6847631-3 Fu€lOl {4685s3{0-. FuelOl#6M)9€r)0c00 MolorollJ00]0OC0 Avjal'on FUel

unid€ndi€d

oher Ol

fotal Petole{rm l-lydrocarbons

C9{36 Aliphatic Hydrocadons

3J86-i3-2 lohlon$tadecane

Semlvol.tlle Orgsnlc Compoln& by GC

Orcanochlodne Pesliddes SW846 8{]81 A

Prepa,ed by method SWM6 3545A

$94G2 Al(trii

8RL

8RL

8FL

BRL

BFL

BFL

BRL

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BFL

BAL

BFL

BFL

BfrL

BRL

BNL

BFL

BFL

BFL

BRL

BRL

BHL

BFL

8RL

8RL

8RL

95

105

122

76

8RL

BBL

BFL

BFL

BFL

BFL

2,660

Calculaled as

2,660

2,660

151

Nrs$y 71

lgeg dry 7.1

lgkg dry 7.4

!S,lq d.y 7.4

lgrq dry 7 4

UdkS dry 7.1

pgkS dry 7.4

ldlq dry 7.4

|rg,,ltg d,] 7.4

!dk!@ 7.4

!S,1rS dry 7 4

ldlq dry 7.4

ligrq dry 't.4

fdlqdry 7.4

ldlq dry 7.4

pdks dry t.4

lEtS dry 14.1

ldksdry 1.4

ldrS dry 73-5

Uglgdry 7 4

ldlqdry 7.1

|Jdlq dry 7 4

pdkS dry 1.4

f4ts dry ?3.5

tdkS dry 147

7trt30 %

7c-t30 %

7G134 %

70tw%

ms/rs &ym94q dy

mYtg dry

mdkg dry

mg/k! dry

|ngnq dry

mgrq d'y

m94q dry

ndtg dry

n€/rg dry

4+110%

lSnqty 39.0

sw 6.16 82608

I

1

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1

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1

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n-M3t47 8-Ma4l 7431t90 RU

724

124

724

724

t24

724

724

721

724

721

29+lad7 3GMar07 7031772

BNL slli8{6 m81A 28.!larq ()q-Apr{7 m3173S TG

This lehorulory rcFnrt is aol wlu *ilhod an or.lhoti?eil signoine on lhe cover page .

t Reportable Deiection Limit BRI- = Below Reporting Linit Page 19 of | -54

Page 170: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole [dentificationM8F-r0 2'-4'sA5980l-{x

Client Proi€ct #301-88

MatrixSoil

Collectiolr Dat€/Time26-Mar-o7 00:00

Received27 -Nlato7

CAS No, .4nslyt (s) Flas ,RDL DiIUion LTdhod ReJ Prcpa?cn Aaalwd Bateh A^zW

Semivolctile Orgrnlc Coflpound! by CC

Oroanodlorin€ Pesticides SWE45 8081 A

P.€pa.ed by method SW846 3515A

319.84{ +8HC319.95.7 bBl.tc319.06S dBHCss{$e gtsBHC (Undans)

t.11.9 Chlodane?2-5,r+ 1,4,-D0O (p,p )7as-!r 4J,-D0E{p,C}

502s3 4400T{p,p)m'5/-1 fiddin

Erd@jlEn I102r3{t9 EdGuIan ll1@r{7{ Endo6u[d| Sdlab,2-2n{ Enddn

7rr21-s-4 Edrh Atd$yde76-448 H€pracl or72"(3-5 il€Eroxyd orrE+r3 HeFfudJor Eponde8EO13t2 Tof,aphs€51ll!71.9 a{ihadan€s66t47 gchloadane

5i!94705 Endnn Keloalo

1@8641-2 A,+DB4cbtu athptenyt (Sr)

Nt2+3 Decachlotofiolw (St)

Poh/d odnated Ephenvls hi/ SW846 80€2

Prepared by method SW846 3545A

126r&1r? PC810161110+?42 l\812111141-16.5 rcB1232s.6+21-9 PCB 124212612-293 PCB 124S11qr-6s1 PC8l25!l11096-€?-5 PC81260tt3e+4s Pcg1V621t1@1rt-1 PCB 1268

rM44z 1,4{8-odatufr6iptsg$l

M144 D*J/ctiht(t,ifrr.,1yt F4

SeElvolrdle Orgroic Comporn& by (rcMS

S€mivoladlo Olanic Conoounds bv SW846 8270C

Prepared by method SW846 35508

lo.aa{ AcemphtErE208.96-0 [email protected] Aniline1 .t2-7 Anfirdc€ng1912.2+9 Atazirc1B.1go Azobgnz$oDiphorryktazines4875 Bquidine56'55t BsEo (a)anhresne

39.039.0

38.01S539-031339.03S0$i39.039.039.03S0393!9.039.01{153€O33.039-0

BRL

BHI

BNL

BFL

BFI.

BRL

BR.

BBL

BflL

BRL

BRL

8RL

BRL

8tuSFL8RLBRL8RLBNLBFLORL

$Ig dYpgrg dY

wrg dI

lglq dv

|lgl€ ffv

|ldlqdvtAtg dY

lglq frY

$nrg dy

lgrq dY

udls dv

udlq dv

lglq fv

uSftS dry

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lgkdvrgh trY

lls/}s dv

$/tS fy

|a4q dv

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s1{6,16 8081A

sw846 8082

sw8l6 82Zr

2&llarfl l}2-Apr{7 7(Bi7Jg TG

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E ei47 &1947 1fi1n4 M.8

97

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BRLBRLBRLBFLBBL8RrBRLBRLBFL

898

898

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ESE

898

€98

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8RLBBLBf,LBRLBRI.BFI.BflLB8L

|dlqdv!o4q rt'

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t'c14&ysgqd)

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t4ks dlv

sgrgty

Ikh tobonbry rqod is rrd idid wirtou ar, tr/,thodqd tUnaare on the coyer page

t Reportable D€iestion Limit BRL = Below Rcporting Linil Page 20 of I t4

Page 171: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-10 2,-4'sA5980l-04

Client Proiect #301 -88

MatrixSoil

Rcceived21-Mat-0'1

Collection Date/Timc26-Mar-o7 00:00

CAS No. AttlJ,te(s) FIoC UEib *nDL DilutiDrt Prcpuel Amltz?t Bdth Andbst

Semivolatile Orgstric Compound! by GCMS

Semivolalils oroanic Cornoounds bv SW846 B2Z0C

Prepa.ed by melhod SW846 35508

50-32{ B€nro (a)pyrene205.e9.2 Eenro F) nuoranthene19124.2 Bs02o (g,h,i) perytene207-0s s 8€flzo {k)ffuol?rihene6t-85{ 8€nzoic acidl0csr 6 Benzyt ahohol1 r 1-s r ' r Bts(2{htoroethory)nelhate11 1 .14 4 Etis(2{hlomeh}4)ether39633 324 &s(2drtodsopropylielter1r73'7 8ts(2+fiyiheryt)piihalate101-55.3 +Brunophentlphenyle$eret-6€-7 tuMb€n4iphhalate96-74-8 Calbazole595.!7 +Ctioto_xlrldhytr'?f,l(r''10647.S 4{hloroanilin€91.5&? Z{hloomphthatene9&s7-8 Z-Chloophe{ol7005.72-3 4-Chloophen!4phenyleth€f218{1.9 Chrysene5?/0-3 oibenzo(a,hlanthracen€132'84.9 Dtbon2ofuan9+sG1 1,2-Didorobenzenes41731 l,3-Didrlonberuene10616.7 l,4_Dichtorcbenzene9r'g,{-r 3,3-Dcfitorobenzidne120.33.2 2+Dicnbrcphenolu{62 oiethyl phlhaiate

131-1r-3 oimehgphf\aiale105674 2,4.Dimelhyiphsldu.74.2 oi-n-butylptihatates34.52-1 4,6-0ioitrG2-melhylphatd51.20.5 2,+Dnivophenolt21.1+2 2,4{iniuotohrenem6.2G2 2,6{iniEololuene117.€4.0 Din-odt4phthatale2C5-14 0 Fluofafllh€ne

r18 74 1 Hexachlofobenzene37-€&3 flexehloobdadienen414 HexehloD€yd@eflladiene6J:/7-1 Hexachlorcethanere13s5 Indeno 11,a3{d) pYrcne

9G124 l-M€tiylnaphlhdene7!-59-1 lsophoronesr.575 2-MslhylnaphtEtene96.{&7 2_ €thylFh€nol

10t.3s-4, 3,+Mehylphsnol$G.4-5s1-2O3 lhphthaleneN.7+1 2-Niboan ins99{92 }Nitroariline

BRL

BFL

BHL

BFL

BFL

BFL

BFL

BFL

BFL

BFL

BFL

BFL

BFL

BEL

BRL

881

BFL

BFL

BFL

8RL

SRL

BFL

BRL

SRL

8RL

8RL

8RL

8RL

BRL

BRL

8RL

8RL

SRL

8RL

8RL

2,680

BRL

BBL

BFL

BFL

BFL

BFL

BFL

BRL

8RL

8RL

8RL

BRL

BF].

8RL

us^s dylgfu my!S^S dry

lls/}sdryps^sdry

us^sdrypglsdrytld](sdrypg}sdrvpsfts dry

rcAs dry

!S4S dry

lgks dry

lrat\S drl

|]s^s dry

lEkg dry

!Yt(q dry

us^s ryl'ls/ls dry

Nksd!'l!S.4q dry

llgts dry

uqts d.y

ldkS dry

lgra dy

lJs4to dy

ldle *v

lgts dypgtsd'ypyrs dy

!91tS dry

|Jgt€ drypcts dry

Utlq dry

udts dry

rclq ftv

ldlq dry

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t44q &y

la/rs dry

$ts dy

lqks dry

lStS dry

lgkg dry

!c/k dry

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ps4(sey

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838

898

898

898

898

8S8

898

83€

898

8S8

898

898

E98

E9'

EgE

898

898

m8

898

898

898

898

898

698

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6S8

898

898

898

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89S

8S8

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898

89E

898

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898

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896

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sw846 8270C

898

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89S

This lzborzaory rcpon k ,oa jvlU xtithoat tn asthoriud slgnalarc tA the rver psge-

* Reportabt€ Detection Limit BRL = Below Report'ng Lirnit Page 2l of 1J4

Page 172: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Identific6tiopM8F-10 r'-4'sA5980l-04

Client Proiect #l0 t-88

MahixSoil

Collection Date/Time26-Mar-07 fi):00

Received27-Mar-07

CAS No, Analyk(9 R.sdt FIAS Urrits *ADL Dthttioa Mahod ReI, PEpaRi Analfeed Botch An4lrsl

Semivslrtile Organic Comportr& by GCMS

Sentuolane Or-Eanic Comoounds bv SVlS4li 82mC

Preparcd by method SW846 35508

100.011 +NitofltiirF$115.3 l,llrob€iEgle8s755 2-ilitoph€nollsdat +NirophdDl@-754 NM.r6Odim€hyiam{l€@1417 MMtocodi-ngopyhnine&3ll-6 N+,litosodipneqdernine874$5 pg]bd oaophenol86-{114 PhemnlhGrei0&9+2 Pnenolla}{l-o pyYene

trH&1 foidneral82.r 12,+Tri*lorobenz6n€9€'o5.. a4,tTri$lorcphenols{e2 2,4,eTridttooph€nol

@1&3 2-Fket@

fi7-124 "Fhgqlwot116ai@4 'VfooDedle-ds

41654a-t Pt|€ro,ns

tn&514 lotdwrJl44

n&84 zl$nbrq@t€nd

8Rr-BAL

BFL

BRL

sRt-88L

8ArBfiLBFLBRL2,WBRL8ALBfuBFL

g

47n,E

66

o375

1 0 1

6.54

52.1

0.520

rdkg dv

ldkq r!/

t&ev|db dv

|ldlqdv

ldlg dty

!s4q dv

|Jdks f)'

Elkrvlgls dv[grs dYlgtg dy

lqlq t}'

Ah dv

lch dv

*130%

15.l10%

xt lN%

t r n 0 %

Ttn%

t6n0%

mdks dty 0'(B68

mdkg dry r.!l

mg,Iq dry 1.65

mgag dy 0.553

'ng/hdry 02n

rtlS/r,g dry 0553

mdlqdry 0 830

mtrsdry t 94

mgl 0.0100

ngl 0.0150

mS, 0.0050

ngr! 0-ll0?5

mS, 0.0125

ng4 0.(m1{]

|l'91 0.0075

mSI 0.0150

sw846 6270C

sr{E46 7171A

EPA?fi.7

3590

E98

898

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8S8

898

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838

€s89€

69E

Etts

E96

6S

ES

I

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I

I

I

1

I

1

1

1

1

1

2$Mar{7 0}Apr$ 7031114 MB

Totd Merrts by EPA 60o{V7000 Scrt€s M€rhods

7(19.s76 MeroJry

Tot{l Merrb bt EPA 200 S€ri6 MEthods

7a,044 SituEr

?{4}9&2 Als€oic

7|l$59n Baiun

7l{0-4}9 CadtiuT

,4{0{7-3 Olmmiom

7r3+4.r Lead

v82+2 s€lerfum BRL

SPLP Mel.b by EPA 13 12 & 60001000 S€ris M€thodt

SPtPExftrdon Comdd€d

14{044 Sih€r BFL

741(1.3&2 Alsenrc BRL

t4('-393 gaiun 0.q160

74,O{lro Ca&ium BRt-

74rC47.3 ch|qnium BflL

7(89|.6 tii6rury BFL

[email protected] Leed BRL

7,12.'192 S€l€ntum BR.

Cencrsl Ch€sistry Farsmt{crs

M-,{r47 034pr{7 70318t0

7.8

8 7 5

@.&r{7

80.1

S|,v6461312 bll,{47 2}t]l3J{7 7031763 BD

Sw845131260108 3!luar{7 m-Aprl)7 7081805 LH

SW8461312/14704 ' m-Apr{7 71181806 YP

SW8461312/6016 ' 024pr-07 m3i805 |.n

$12!t{l G ilod. 3} ar{7 30'liladT ru1879 Ytil% Solids

P4e22 ot 154

Thh |a.!toto.t fp*t X rrrtadU NAhoar an auhortzzd signeoe oE the coj6 pagc.

i Reptrrable Detecrion Limit BRL = Betow RepodinC Limit

Page 173: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiorM8F-l l2'-4,

sA5980l-05

Clielt Proiect #l 0 l - 88

MatrixSoil

Received

27-Mar-0'1Collection Datc/Time

26-Mar-07 00:00

CAS No- A"alrk(s) Resutt FIag Unia 'RDL Dilutil,rl Method ReJ Prcporcd Anallzed Betch Ahabal

Volatle orcanic Comoounds

Prepared by m€lhod SW846 5030 Soil (high levet)

7r.r3r 1,l2-Trichtorotdfluoro€hffB(Freon 8RL61.*1 Acetone 8RL107r3-r AcMonilnle BRL714!2 8€nzene 8RL103-3t1 8mfi\ot€nzene 8RL7'l s7 5 Bo|rlochloro'n€than€ BRLrr27-1 Eono(ichtoromethane 8RL

ErDndlom BRL74.03-s BrDmom€flane BRL78 e3 3 2-8ubno{€ (MEK) 8RL10,ts1-8 n-Buvtbenzene BRL135-9&3 sec-Eutylbenzene BRLs{6.6 terl-$rtyibenzene 8RL75154 Ca6on dtsdftde 8RL

56.2$s Ca6on telEchtoride BRL

108.9G7 Chlorotrejzme BRLi5{G3 Chtomefiane BRL

67{6-3 Chtorolonn BRL

14.8r-3 Chb,o'rledian€ BBLFe B 2-Chlorcbluene BBL10G.434 {-ftiorohluene BFLF12 3 1,2{ikome3drloropropane BBL124-181 DbomodrtorcnEthane SFL

106.93.l i,2,Dikonoelhane (EDB) BffL

?44s.3 Dibronhelhane BFL

9+50.1 1,2-oichtoobenzene BFL

541.711 l,3-DcHorcbenzene BffL

'06:45-7 l,4-Dtciloobenzene BFL

757rr Dichtorodifluoromethane (Freon12) BHL

7534,3 t,t-Dd oroethane BHL

1cr!$.2 l,2-Dichloroethane BRL

7s354 l,l nidbroethene BRL

28.{farfl 2l-Mar47 7031767 B0

O2-4W47 02-ApF07 70,{0017

volNtite Orgrnic Compourds

VoC Enraction

pSAS dry 67.3

ldks dry 1350

PdkS dry 67.3p94q dy 67.3

!g4g dry 673

ldkS dry 673

|lgr'tS dry 67-3

lgkg dry 67.3

p94q dry r35

Pdre dry 673

lSredry 673

ldq dry 67_3

!S4(S dry 67 3

gg&griry 336

ldkS dry 67-3

pdks dry 67.3

lyq dry 135

p9?€ dry 67.3

vdtodty 135

t€/rS dry 67.3

P$S dry 673

|]g4S dry r35

lgkS dry 67.3

|Jg,4(S dry 67J

lsrls dry 613

lS.ftS dry 67.3

!S^g dry 67.3

ISAS dry 67.3

lClq dy 135

!g4q dy 67.3

!SI,.S dy 67.3

|lg4S dy 67.3

pdks dry 67.3

lsnq dy 67.3

p91q dry 67-3

ldkS dry 67-3

lStS dfy 67.3

pglq dw 67.3

|44q dry 673

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!9+S dry 673

pg*s dry 67.3

lS.ftS dry 673

lgnq dry 67.3

!{it.cdy 67.3

!9rg dry 67 3

U0Iq dy 673

ldk€ dy 673

pplqdy 673

F eld exlraded voc

sw zu 8260a

BRLBRL8RLBRLBRLBBLBFLBRLBFLBflL8RLBRL8RtBRLSFLSRLBRL

50

50

50

50

50

50

50

50

50

50

50

50

50

50

5D

50

50

5t)

50

50

50

50

50

50

5l

5l

50

50

50

50

50

50

5{)

50

50

50

50

50

50q

50

5{l

50

r5e5s.2 cis-1,2,Drdoroetkne

1545 tlans-1,2-DidoD€lhene

4S7-5 l,2,Dichtorcpropane142.2s9 l,$Dichtoropopan€

w.2ot 2,2-Dichlorcpropane

563.rS4 l,1-Didoropop€ne10061{r'5 ci5-1,}Didiorcgropene10061{2-6 lran6,j,}Didlo€prop€ne100-111 Efrybenzen€0753 3 H€xaal Oobuladien€59r.73-6 2-Hsx one (MBK)

9A{2-3 lsopmpybsnzsn€998/{ +lsopropylofuene1641.0,r-4 [4etvltM-tulyleherl0&io'1 4-[telhyl.2?edanorc(MIBK)

7s2 Mehylene dioride91-2G3 llapittdqe

Thk laborutory repor, it not jslid wilhoua an euthoi.ed sigdatun on the cowr page

t Reporrable Derection Limit BRL = Below Reporting Limir Page 23 of 154

Page 174: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentifica6onM8F-u 2.4,sA5980l-05

Client Pmiect 4301-8E

Collection Date./Time26-Mar-07 fi):00

Received21-Mar07

MatrixSoil

CAS No. An!b@(s) Resuh FIag Uatb *RDL DUsliad Met'od R4. Pftpued Anzlyzed Bd.h Andlfsl

Yol.tlle Orgrnic Compourds

Vohtle Oroania Comoo|'l(lg

Prepared by method SW846 5030 Soit (high tevel)

lm.6'1 n+@pylbqzeno BRL

100-,125 slyreje sRt-

ac2ll$ t,1,1,2-Tetladtoroeflane BnL7+34-5 t,1,Zl.T€trad oroethane BffL1n-10.. Tetnd oo€fion€ BFL108-$-3 Tofuae BBL

87-€1{ 12,3-Tnchbaooenz€n€ 8RLt20€2r 't2,{-Trid oro0€{zeno BfiL7r_sE-G 1,1,1-Trid o.oghans Bf,L,9rxt5 1,i,2-Ti*bro€dlan€ 8FLII4I3 TftfiDrc€dl E BFL7s94 Tndlordluorfi|gbane {Frmn 1 t, 8Rf9618-4 lz,STridrloropl'opano gnl

s4$.6 1,2,+Tdm€fny'benzene BFL100.67{ l,3,FTnrnedrylbenzene BRL75-01{ \.hy' d orftle 8RL1SO.2G7 m,Pxt6ne 8RL95476 oxylene SRLlollllrse Tefahydofuran BFLdr2s7 Etryefw BRL

99{45-8 T€nsrrylmohylehd BRL697s2'3 Ehylhn-hlu eher 8FLr06a!3 oii$popytdt|or BFL75-65{ Ted-B{hrbt/ hrylatcoftrt BnL1&91-1 1,4{io{afi6 BRL

1@@1 4BonofrJoobenalE fiNr-4-5 ldtwc4S 101t706oa74 lz'ok:ltbrEfndne44

t8dn-tt7 Di&ottofiw@|€tlr€ne lM

Ertrctable Petroleum Hydrocrrbons

Edraciable Tod Peudqrn hdrocadons

Pr€pared by merhod SW84ti 35508

oe.Aprfl m.AF{7 7(Kxlt7 nalwh dy 67.3

|jg/k! dy 671

l4lq dy 57.3

$Iqdy 67.3

lglq dry 67.3

|lglS dV 673

|4/l€ dry 671

$lq dy 67.3

$/lq dV 67 3

lgrq dy 67.3

pg/kS fy 67.3

lglqfy 67J

|lglkg dy 623

ldlq dy 613

UdkS trt' 67.3

pghdrv 673

lg4qdry 135

|lg/|(! dy 673

|Jg/}S trI 673

ldlS dY 67.3

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$/t€ dy 673

lglq dV 67J

|gl(s rv 6nug*get 1s0

TVtn %

7r\1&%

7813t) %

70-ti4 %

n'S*Sfi 6s2

IIdh dy 652

ngilqdry 65.2

'nglq dry 652

rfldkgdv 652

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mdlqdry 452

mgnqdry 65.2

mytg d] 652

mg/kq dq 65?

4+110%

sw 846 82608

+CT ETPti

50

50

50

50

50

50

50

50

50

50

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50

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uilidsnifi€d

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CS{36 Alqffic Hydr@fto(B

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Semivolatile Orgrdc Compootrds by cC

oroanod odne Pesticil€s 5$/846 8081A

Prepar€d by method SW846 3tt5A

$s+2 Aldrin

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ta

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Thb ,obo.alory rcpod k not yoli4 tdrhoal a arlhodzad signafine on lhz cove.IRge.

i R€portrble D€tection Limit BRL = Below Rcpding Limit Pag€ 24 of | 54

Page 175: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-lt 2L4'sA59803-05

Client Proiect #301 -88

Collection Date/Time26-Mar-07 00:00

MatrixSoil

Rcccived27-Mat07

CAS No. Anatyeb) Rcsult FloC Ania *RDL Dilation Llzthod Rel. Prcpored Arc$zed Balch AruLtsl

Scmivolrtile Organic ComFornds by CC

orcanodibrine Pesticlies SW846 8081 A

Prepared by method SW846 3545A

319r4i a_BHC31s85 7 tsBHC31946-3 dBHC5ars s 9BHC (Lindane)

'/-71.9 Chloidanep.54.n

4a _oDD lp,p )72-56.s 44-DDE (p.p')

s0-el3 a,a -00r lp,p,)6G57.1 Dieldin951,.9€.8 Ericdlllan I332196+9 Erdosutan ll1061-07.8 Endosullanslllate72-20-n Endrin7,r?r,s4 Erdin AtdehyGfi44 a kdacntoru3.5 Metlorychtolroe4 573 Heplachtor Epoxrde0001 15, Toxaphenes103 71-9 a-Chlordan€5566-3,17 g-Chlordane

53494.7'5 Endin K€lcme

103t6-81-2 4,+D&(Nanuorcbi$entt (Si

fr51-24-t De.a orcbiphe / (Sr)

Potuchlorinated Eiphen!,ls bv SW846 8m2

Prepared by method SW846 3545A

!257+1r ! PC81016r 04.2s2 PCB 12211114r 165 rc8123i2$169.2r-9 rc81242p6n-2+6 PCB1248r1os76+1 PC81254110s6S2-5 PC8 126037u4-23-5 PC81m21r1m 11-4 PC8 1268

t03&-8+2 4,4-Dgl,aanuoronFtunt4(St)

m5t-21-3 UcachknobiofEnl$|

S€nivolrtile Organic Compounds by c,CMS

Semivolatil€ orqanic ComoounG bv SW846 8270C

Prepared by method SWB46 35508

33'32 9 Acsnaphh€ns203-963 Acenaphfiyieno62-53-3 Aniline1tu12.1 Anfr&€ne19122+9 Alrazine103333 A2ob€02€n6,Diph€nyldialine92-87-5 genzidine

Benao (al anhraccne

BRLBRLBRLBRLBRLBRLBRLBRL8RL

BRL8RL8RLORLBRLBRLBRLBRLBRLBRLBRLBRL

62107

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ffi

105

33.2

33.2

33.2

332

165

332

33.2

33.2

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13.2

33.2

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n233.233.28.2166

33.2

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332

lyks dy

!s4q dy

!s.4q dypg4q dry

lsnq dy

tig.4q dry

us.4q dypS/kS drypSikS dry

!s4q dry

!S/kS dry

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!gl$ dry

lllas dry

!s&s dry

ldk€ dry

!s/ks my

tr!/kQ dry

lgeg d]

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fi-150 %

3+150'n

!s4q dry

!g]|(S di]

pdxg dry

PqtS dty

lgkq dry

!s4q dry

tjs,ks dry

r{vlq dry

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wt50%

3+1f l%

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tCksdty

su,/846 €081A

sw€46 Er)82

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664

664

66.4

6 6 4

66.4

66.4

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66.4

28-Ma(07 02.Apr07 703173s

28tta(07 30-Mar-0i 7031738 Slvl

ZS+,laro7 03'Apl47 7031774 M.8808

80€

806

808

808

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Thit laboratory repod h nol ealA n'ilhou an auhoriud siqrutlure on lhe corcr page .

a Reporoble Detection Limit BRL = Below Reporting Limit Page 25 of 154

Page 176: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldendficationM8F-ll2'-,1'

sA59803-05

Client Proiect #301-88

MatrixSoil

Collection Dat€/Tifte2GMar-07 00:00

Received21-Mar47

CAS No. Anatflz(s) Fbg |RDL DiIuiM Method ReJ Paparcd Analwn Babh Anoltst

Semivol.tile Org{tric Compoltrds by GCMS

Serivdalil€ Orcanic Comlouds bv SW846 Pe70C

Prepared by method SW846 35508

$'32 s Eeruo (a) plmng

20ss2 Sgnzo (b)ffUo{v hene191-242 Bgnro {g,h,i) D€rftne207{&9 B€rEo(k)0uoranh€ne6C85 0 BdnrIJiC rcid10r!51{ BsEyta|conol11141-1 Bis{2dlloroehory)fiFt|€ne111-4,t4 Bis(2dorcery)dhe.s€48-32{ 8is{2dordsop&pi)dh€r!17+1-7 8E{2€hyh€xy)pt{hahtel0r-5s3 +Ercrnoph€rM pl€ryt slherBffi'7 &M bon4l phthdale

&f44 Calbazol€5s,5{r7 44oo+melhylpt€nol106-471 d4 oloatitino915&7 24tfuonaphtha/sne96t8 24Ho(ophetd7m6.72-3 {{llsoohe$ytph€ny'stlei210.01-9 Chrysenes0-?u3 Dibsruo i4h) arthfacon€l@6,14 Dben2ofurin9&5G1 1,2{)idlo|Db€.Eenes,rr-7iir 1,$Uanbrobeftene16.467 l,4ohlorobsnr€ne91€4r SSoidiorob€flridne120.83.2 2,+DdtorophsEl04{6-2 D€fly' drtuJalo13111-3 D{nrehylphhalate105{ttt 2,a.0inehMph$d&r+2 Di4-bdyi ptdEtate

531-52'1 4,eDinib+24$dtrylphexol5r2&s z,4.0rtffophsnol121112 2,4.0iduobtueisoG2O2 2,GJiriroblueneIri-o/}{ Dfl.ttphhahte?!6144 FuoraJ,|,tst€

!S7J7 FluOtEn€l1€.7+l tlenclorob€nzeie87€.3 Hemd*l@butad€n€tu74 Hexado@qdop€{ndiere

-n1 H€xaddoE€haae1s+3e5 Ind€m(1,2,3{d)pyrsle

s12{ 1{.|€dryjnphfial€ne7€.59r lsootlo|one91-rt 2+t€dvtrleshhalei€1646-7 2-lrofttiht'arol

1fi-39{ 3,1.fr€0ryhhstd10€-4i.59r.20.3 llaphfralene

0&7r-a 2.1{itmnit'fls00-0+2 3{tt(rdrttrn€

BFLBRLBR.8FT8RLB8LB8LBRLSRLBFIBnI

snlB8LBRL8RL8RL8RL8RLB8L8FLBRI8RLBFI.BHLBflLg8L

BFLBRI.BR.BFL

BRLBflLBFLBFLBRL0R-8RLBNLBALBFLBRL8RL8RL8RLBRLBRLBFL

8Rt-B8L8H-

ugrq dy

lgrq dv

!g/rg dly

tdrg dv

|rsnq dv

rsre dv$4q dv

!s4q dr)'

uc4q dy

|ldkS dty

|dhdv

uglq dYpyrsdv

$gks dv

wh evrjdh dv

lrylq frvpE/l€ dy

!gL0 dl'

lgls dv

lgk fiv

!g/1€ rYpgh dY

ldks d'Y

ugtq dv

lErs fy

!E]q fiv

lgts dY

E/lq frypdh dv

lldksd'YUS,lq dy

|jg}s dy

lErg fv

!S/rS dy

|ldts dy

rcnq dY

19& dY

|dkg dv

lgts fy

!919 dy

!g'tq dy

Ars dvudlq dv

|jglq dY

lgrq dy

wh dv

tryla&'JuEl€ dv

rab dv

808

8m€48

8{€

808

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€08

zum808m8

m8m88088d,80€808808elo808

808

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60€

svlBl€ 8270c n+1u41 E y-07 7$tn4 M.B

fhis lztontory rcpott is ,rd vaUd uahout an a&l*otlz.d signaure o,. the coecr page.

. Reportable Det€.rion Limit BRL = Betow Reooding LiEir Page26 of 154

Page 177: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificatiopMtF-lt 2'-4'

sA59803-05

Client Proiect #l0r-88

MatrixSoil

Rcccivcd2'7-Mar-01

Collection Date/Time26-Mar-07 00:00

CAS No. Analytc(s) Resull FIaS Uaits *RDL Dilu tn Prcparcd Andwn Bztch Analrsl

Semivolrtil€ Orgrnic Compounds by GCMS

Semivolalile oroanic Compounds bv SW846 8270C

Prepafed by method SW846 35508

100'01$ 4-Lljlroaniljru 8BL9€'9ss NiFob€nzene 8RLo&7ss 2-Natophenot BRL100-02-7 4-Nitophenol BRL62_75_9 N-Nitrosodmehylamin€ 8RL@1-6+7 l{.Niliosodi-n-propylemin€ BRL06-10-6 N.Nitrosodrpl^e.Mamine BRLflt6-5 Penlacilorophenot BRL05{1,8 pherEnhrene 8RL100-9t2 phenol BRL12940-0 pyrene BRL110.0F1 4rndine 8RL1n'a21 1,2,+Tichtoobenzene 8RL9ss-4 2,4,5-Trichbrophenol 8RL$116-2 2,4,6-Tridrlorophend BRL

@160-a 2-Fhnobiphenyl 5,fi/124 2-FluoroplBnol Sa4t65nM Nitrcbenrseds n1185n2-2 PheMUS 4t1/1e51-0 feryhent+da 75lt'ns 2,4iTtihornophend 49

Totrl Metals by EPA 6000,rru0 S€rie5 Method!

€-Mad7 03Apr{17 7031774 M.BlJg+tSdry 3230

!94q dry 808

ldkq dry al8

lgrq diy 3-?30

u94q dry zu

u94q dy 808

USrkS dry 8{l€

ti9kS dy EoE

lsas dy 80€

lsAs dy E0€

!9ks dy EoE

PSI(S ('y m8

lEkS dy 808

pslq dry m8

lSIq dy 808

3+130 %

15110 %

3U130 %

15-110%

3&130 %

15-110 %

r'q?{ dry 0.0338

mqkS dry 1.10

mS,?.S dry 1.64

rnS,1q dry 0.51|8

"dkg dry 0274

mdrq dry o.:l'E

m94q dry i-|n

tn9,k9 dry 1.€4

mgn 0.0100

mqn 0.0150

n91 0 0050

mql 0.0185

mg,l 0.0125

mg4 0.0@10

m!,,1 0 m75

'ngrl 00150

sw8,46 8270CI

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7139-97{ _ Metcury

Toaal llet ls by EPA 200 S€ries M€rhodr

74{o-u4 Silver

?,rlG3$a Badum

7,t4I1439 Ca*niun

71rra 47 3 Chrcnium

/aq.92r Lead

]?l!492 S€lenium BFL

SPLP Metrts by EPA l3l2 & 6000/7000 Sedes M€thods

SPIP ExtrJclion Compleied

7414-22-4 Silver BRL

71.4033 2 A6enic BFL

74{G39 3 Barium 0.0fi}5

7'llo-43I Cadmium BRL

t41a!7 x Chromium BHL

7it3e9?{ l,lerorry BRL

7+lser Lead BRL

r@-ae 2 S€leflium BRL

G€nerrl Chcmistry Prrametetr

% Solids 88 6

0 342

BRL

7.8S

760

o515

s08

152

st{846 7471A

EPA2M-7

SW8,161312

s-w&61312/60t08

sw8461312Ir470

sw846 t31 Z60t0B

SM2540 G Mod.

02-&r{7 03-Apr,07 70lr8l0 YP

H8

28-l'1a47 28.ilar-07 7031763 80

30-Mar{7 02'AF-07 7031805 LR

' @.Apr{7 7031806 YP

' 02-Apr47 7031805 LH

30.{'lar.{7 3$Mar-07 761879 Yl',!

This lsbomtory HNd h ^ot vald withrlt aE s$thorized slgnalurc on the cowr prye

I Reportable D€rection Limit BRL = Below Reporting Limit PaE 27 ot 154

Page 178: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple ldenti ficationM8F-t2 2'-{'sA59464-04

Clietrt Proi€ct #30t-88

Mat ixSoil

Receivedl9-Mar-07

Collection Datel[imel5-Ma.-07 m:0o

CAS No. Aqrlyt4s) Resak Flas Aab *RDL Dihtthn Llahod netr Prcpared AnaPzed Bdch Analfsl

Vol.til€ Org.nic Compounds

VOC Extraction

ISlkgdty 4.9

t,€ikgdty 9E.6

PSn(g dty rt.g

ldks dry 4.9

Fgts dry 4.9

ldks dry 4.9

ldks d.y 1.9pg/ls dry 4.9

!g/kg dry 9.9

ldkS dry 49-3

t dks dry 4_9

IdkSdry 4_9

ldkgdr, 4.9

ldkS dry 21.6

Ueftg dry 4.9pdkS dry 4.S

Ug/lqdry 9.9

Idtg dry 4.9

rcr(S dry 9-9

ldkS d.y 4.9

tidks d.y 4.9pg/r(g dry 9.9

lSfl(gdry 4.SgdkSdry 4.9

lSlkS dry 4-9pg/tg d,y 4.9

IdrSdry 4.Sygrsdry 4.s

[gtS dry 9.9

t grko dry 4.9

ldkgdry 4.9

|lgn(g dry 4.9

ldkgdry 4.9

!s/kg dry 4.9

t g@ dry 4.9

Ig/kgdry 4.9pdksdry 4.s

ldkS dry 4.9

fldlg dry 4.9

I'gkS dry 4.9

t4/*S dry 4.gydkgdry 4.9

ldrg dry 49.3

ldkSdry 4-9

lSit€dry 4-9pS/Xgdry 4.9

ldkgdry 49.3

ldkg dry 49_3

ldtsdry 4-9

20-ltat47 20''.,ar4? 7031156 8DField extracledVolalil€ O.oanic CompoundsP.epa.ed by rnetlnd SW846 5035A Soit (tow tevet)7F111 1,1,z-Tri€frlorcfinuoroelhane(FreoSRL6?€+1 Ac€lone 8RL107-1+1 Aq,ylonible BRL71-4+2 Eenzen€ BRL108{6-1 Bromobenzene BRL714r-5 BmmochhrometlEne BRL71274 Brcrnodiclloromethane BRL75-2+2 Baornoform BRL74{}9 Bromomethaoe BRf78-9+3 2€utanone (MEK) BRL10,!-51+ tuBulylbenzone BRL13+9€{ sec.Bulylbenzone 8RL98{66 te(€utylbenzene BRL75-l$o C€rbon disulfide 8RL56.23-5 C€rbon tetehtoride BRL1O8-Cr7 Chlorcbenz€oe BRL75.oGs Chloroethane BRL67€6.3 Chtoroform BRL74{7n Chbromethane BR!95-19{ 2-Chtorctotuene BRL10643-4 4chloobluene 8RL96-12{ l.2oibrono-ktloropropane BRL124.18-1 Dib@rnocf$oromethane 8RLioca34 l,2oibromoef|ane (EOB) BRL74-9rF3 Dibromome$€ne BRL95{01 l,2Srchlorobenz€ne BRL541-73r 'l,3tichlorpbenz€ne BRLl06a6-7 I .+Dichlorobenzen€ BRL75-714 DdJorcdifuoromehan€(Freon12)BRL75{4n t,lohNoroe$tane BRL107.06-2 1,2-Dichlorc,€thane BRL7+3s4 1, I Obhlofoeth€ne BRLl5€-5s2 cis-tJ-Dichloro€th€n€ BRL156{cs t€nel,z-Oidttotuethene BRL78{7€ |,2-Oichloropfopane BRL142-2€.9 l,3oichloropaopane BRL59a-2Gr 2,2-Dichloropropan€ BRL563-58€ l,l.Dichloropropene BRf10061415 cis-1,3-Dichloropropene BRLt0c6r{2$ bans.1.}Dichloropropen€ BRL100.41.1 Efiylbenz€ne BRL87{&3 Hexachlorobutadiene BRL591-784 2-He,€none (MBK) BRL9€{2{ lsopropyibenzene BRL99-€7{ +tsopropyltoluen€ BRL1634{4-4 tvl€thy' tert-buFy' eher BRL10s10r +Meury'l-2.pentanone(Ml8K) BRL7s+r.2 Methy'€ne chtoride BRI_

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SW 846 82608 21 -ttla.-o7 22Jt €r-07 7031 233 lR

9l-i+3 tlaphthEbne

Page lE of lJ2

Thb lzbortroq rqo.t is ro! ealid wifua ad dtdtori?td slgfi tke oz th2 coeer ?tagc.' R@rfable Dctecrio{ LiEir BRt = Bclow Reporting Limit

Page 179: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentiftcatiolMtF-I2 2'-4,

sA59464-04

Client Proiect #301-88

Collection Date/Timet5-Mar-07 00:00

Mat ixSoil

Rec€ivell9-Mar-07

CAS No. Anzbte(s) Resull Fhs Uni/5 'RDL Ditaaion Meahod Retr. PPpaHd Atubaed B eh AnalFt

Vohlile Org.nlc CompoInds

Volatile Oraanic ComooundsPrepared by method SW846 50354 Soit (torr,/ tevet)

7s59-4 Trichlorofluoromethan€ (Freon 11) BRL

10165r n-Propylbenzene10042-s Styrene630-206 1,1,1,2-Tetrachlorcethane79-34-5 1 . 1 ,2,2-Tetrachloroethane127-184 Tetrechloroelhene104{€-3 Toluen€87-614 l,2,STrichtofobenzene120-82,1 1,2,4,T.ichtorobenzene71'5s'6 I,I,l.Trichtoro€thene79-oG5 1,l,2.Trichtofo€thane7941-6 Trichloreth€ne

s6-18'4 l,2,3.Trichloroprop€nes5€35 1,2,4-Trimethylbenz€ne108-67-8 1,3,s-Trimethylb€nz€ne7s{1-4 Vnylchlorider33O,?C7 m.p_Xytene95-475 O-Xylene1(A-99-9 Tetrahydrofuran60-2+7 Efrylettlersg4{€.0 Tert-amy' methyl ether637-92-3 Ethyltert-butylether1D&2!-3 Di-isopropylethe.7s€t0 Tert-Butsnol / butyl alcohol123,91-1 j,4_Diolane

Sunogate rccowdes:1604t14 +Bromolluorobenzene

m3r.2€-5 Toluenedg

1 7 0604? 4 1, zDichlorcethane44

186&53-7 Dibromofluorcmethane

Extrsctrble Pelrole|rm Hydrocarbons

Exlractable Total Petroleum HvdaocarbonsPrepe.ed by melhod SW846 35504qxl641-9 Gasoline58174302 Fuetoit#26847&313 Fuetoit#46€55100-1 Fuet oil /{15l\.109800000 Motor OilJ001 00000 Avietion Fuel

unid€ntified

Otl,er Ol

Total Petloleuft Hydrocsrbons

C9-C36 Atiphetc Hydroc€dons

Su/rogate recoveaiesl

338+33-2 1-Clrlotoodedecane

Semirolatlle Orgrnlc Compourldr by GC

Oroanochlorine Pesticidos SW846 8081APrepared by mettEd SW846 35508

309{+2 Aldrin

SW84682608 21-Mat47 22-Ma(07 7031233 TRBRLBRLBRL

BRLBRLBRLBRLBRLBRLSRLBRL

BRL8RLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRL

103105101104

BRLBRLARLARLBRLBRL263Cal laled es263263

pgkS dry 4.9

ldks dry 4.9

lgikg dry 4.9

!g/kg dry 4.9

ldks dry 4.9pg/kg dry 4.9pSl(S dry 4-9

ldkS dry 4.S

lgftS dry 4.9

UgkS dry 4.9

ldkS dry 4.9

lig/kg dry 4.9

lCkg dry 4.9

!g/kg dry 4 9

!9kS dry 4_9pcks dry 4I

UgftS dry 9.9

lgkg dry 4.9

ldkg dry 4s.3pqkg dry 4.9pStkgdry 4.9pS/kS dry 4-S

ldkS dry 4.Spg/kS dry 49-3

ldkS dry 98,6

70-t m %70-130%70.tm %70-130%

mgfl(g dry 34. I

ndl(g dry 34.1mg/kg dry 34.Inglkg dry U.Img/kg dry 34. ImdkS dry 3. ImS/kS dry 34 1'rldxg dty 34.1m€/kg dry 34-1['SI(S dry Uj

40-140 %

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+CTETPH 21-Mar{7 2 '1+vlar{77031167 DS

ldkg dry sw846 8081A 2O.Mat47 25-Mat47 7m1068 TG

Thh lsbotuaary nFo.t is ttot ldU trithou an auhodzed sigaature on the coeer page* Reportabl€ Detection Limir BRL = Below Reporting Limit Page l9 of 152

Page 180: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificationM8F.12 2,-C'sA59464-04

Clint Proiect #l0l-88

MatrixSoil

Collectioo Dste/TimeI 5-Mar47 00:00

Receivedl9-Mar-07

CAS No- A,uiyz(s) ResJ|h Fleg aalts iRDL Dihriat Maho,l Rel Prcpa.ed ,lazalz"i Batch ,laalyst

S€mivol{tlle Orgetric Comporrdr by GC

Omanochhdne Pesticides SWA46 808 | A

Prepard by mehod SW846 35508

319€44 a€HC3r9.S5-7 b_BHC319-86-8 d-BHC58{99 gFBHC (L,ndane)s7-7+9 Chlordane72s+8 4,4-DDD (p,9')

72-55-s 4,4.DDE (p,p.)

5o-2e-3 4,4-DDr (p,p')dr.57-r Dieldaln95s-98$ Endosulfen I$2ra65.9 Endosulfan tlt03t474 Endosultensultatef2-2o4 Endain7421-93-4 ErdrinAldehyde76-14€ Heptad ori24+s Mehoxydtlor1024-57,3 flsplachlor EFoxide8OOl3t2 Toxapltene5103-714 a-Chlordane5,566-3,t-7 g_Chbrdane

s349+705 Endrin Kebne

SurrogaG €couEnies.1o38M+2 4, 4'&Oclan uorcbiphenyt (St)

2051 -zaa Decachhtobiphenyt (Si

Polychlo.inated Biohenvls bv SW846 8082PrepaEd by rnettbd SW846 3545A

1267411-2 PCB t0161110+28-2 PciB,12lI1tl,rr-16,5 rcB 12325346s21-9 PCB 124212672-84 PCB 12481toq74s1 PCB t2541t096{2-5 rcB 12603732+?3-5 PCB 1262ii10G14-4 PCB 1268

Sutqele Bcot/Elks:| 0386a+2 444goclaf u?,'ohiptlFJnyt (Sr)

2051-24,i Decachlotubiphenyt (Sr)

Serdiyolrfle Orgrtrtc Conpounds by GCMS

BRLBRL

BRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRL8RL8RL8RLBRLBRLBRLBRLBRL

47109

BRLBRI.BRLBRLBRL1.150970BRLBRI-

4045

sw8{6 8061A

sw846 8082

udkSdry 6.48

IrgkS dry 6.48pgftgdry 6.48

fdkS dry G.48

rdkSdry 324

WkS dry 6.48

US/IS dry 6.48

ldrg dry 6.48

usftsdry 6.4€pSikg dry 6.40ps^gdry 6-41)

Udrgdry 6.40

lgkS dry 6.48pdkSdry 6.48pdkgdry 648

FS/kS dry 6.48

ldksdry 6.4a

rgks d.y 32.4

Pg/kS dry 6-,18

lglS dry 6.48

ISrkg dry 6.4a

30-t 50 %3Gt 50 %

pgrsdry 13-0

TSrkS dnl 13.0

P+ftS dry 13.0

Ig/kg dry '13.0

lCAgdry 13.0

ldkS dry 13.0pdkgdry 13.0

rcftS dry 13.0

lgrsdry 13.0

3G150 %3f.150 %

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21-Mat47 23ttlar47 10311€/.

22-t\-tar{? 24-i&f47 ?0312?g M,B

Semlvolatile Oroanic Comoounds bv SWe46 B27OCftepar€d by method SW846 3550883t2.9 Acen@htlEne21ls968 Acenaphdly'ene€A-5t3 Aniline12Gt2-7 Anthracefle1912.2+9 At€dne10333-3 Azob€nzent/Dipheny'diazines{7-5 B€nzidine5d€+3 B€nzo (a) dnlhrEcofie

8Rr_BRLBRLARLBRLBRLBRLBRL

ldlg dry

ISftg dry

rcas dryt S/kg dry

t4lkS dry

FS/IS dry

|lgiks dry

ldks dry

846

E46

846

8,tos468468466,16

sw848 A270C

Thk lzbordory Eport ls nea yalid withadt on qstt oried slgrrdtue on thc cava page -+ R€porbblc Det€ction Limit BRL = Below Repofting Linit Psge 20 of 152

Page 181: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificalionMtF-r2 2'-4ts45946+A

Client Proiect #301-88

MatrixSoil

Collection Date/Timel5-Mar-07 00:00

Receivod19-Mar-07

CAS No- Aaolrtz(s) Resull FloS a n s IRDL Dilatioa Method Ref Prcpffed Anaqrrd Eatch Analrst

Semivolalile Organic Compounds by GCMS

Somivolatile Oroanic Compolnds bv SW846 O27OCPrepared by method SW846 35508

50 32-€ Benzo (a) pyrene

205-99,2 Eenzo (b) nuoranthene1e1-24-2 Benzo (g,h,i) perylene

207 08 9 Benzo (k) ffuoranthene65rto Benzoic acad100-514 Benzytalcohol111-91-1 Bis(2dilorcethory)methane11r-444 Bis(2-chloroehyl)eth€r3963&32-9 Bis(2-chloroisopropyl)eth€l1 1 t-81 -/ Bisl2-ehylhexyl)ph&ratate101-s5l 4-Bmmopheny phenyl €ther8564-7 Butyt benzyl phthalate86-743 CarbaZole595G7 4-Chloro-3-methylphenoi106173 +chtoroanijjne9158-7 2-Chtoronaphthalene9s,57-8 2-Chtorophenoi7005-72'3 4-Chtorophenytphenylether218 01-9 Chrysene53-70 3 Dibenzo (a,h) anthracene13?s-9 OibenZofuran9t5G1 1,2_Dichlorobenzene

4141,73-1 .t,3-Dichlo|obenzene

106-{67 1,4_Dichlorcbenzene91-941 3,3'-Dichtorobenzidine120-832 2,+Dichlofophenoln466-2 Oiethylphthatate131-11-3 Dmethylphthatate1r)5{7'9 2,4-DimeUrytphenolu-7+2 Dt-n-butytphthatete534-52-1 4,6-Dinitrc-2-methytphenol51-28-5 2,4-Dinitrophenol121-14-2 2,4-Dinitrotolu6ne606-4t-2 2,6-Dinilrotoluene117€4{ Di-n-octylphthalat€206444 Fluo@nthene6-7Tl Fluorene

11€-74-1 Hexachlorobenzene

87{s3 Hexachloaobuiadiene

77-4f4 Hexachlorocyclopentadi€ne

67-72-1 Hexachloroethane

193-39'5 Indeno ('l,2,3-cd) pyren€

90-124 f-i,lethylnaphthalene

78{9-1 lsophorone

91-57€ 2-Methy'naphthalene95-.{8-7 2-Mett\ylphenol

100-394, 3,4-Methytphenol106-4-t-591-20-3 Nephthaiene

E8-744 2-Nilroaniline

99-0+2 3-Nitoanitine

BRLBRLBRLBRLARLBRLBRLBRLBRL8RLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLARLBRLaRtBRLBRL8RLBRLBRLBRLBRL

BRLBRLBRL

lgkg dry 846

ldks dry 846

tidkS dry 8,16

USiftS dry 846

Ug/kg dry 846

ldks dry 046

IrS/kS dry 846pdkS dry €46pSn(S dry 846

ugKs dry a6

uS/r(g dry 846

Ugi@dry E46

lqKg dry 846

lsiKg dry 846

lrglkg dry 646

!q/kg dry 846

t SikS dry 846

!S/kS dry 846pSlkS dry 846

rcftS dry 846

ldkS dry 846

PSKS d.y 846

rs&s dry 846

rgkg dry 846

uSr(g dry 846

t4,'k9 dry 846

USftS dry 846

USftS dry 846

!g/kS dry 846pgftS dry 846

Ug,ttg dry U6pSftS dry 846

!g/kS dry 846

uSftg dry 846ydkg dry 846

tghSdrl 846

l,gkg dry 046y9ft0 dry 846

udkg dry 846

!s/kg dry 846

US/kg dry 846

US/kg dry 846pdrS dry 846

Ugikg dry 846

lslks dry 846pS/kS dry 846

t€ftS dry 846

pslqdry S46

r|dks dfy 846

!S/kg dry 845

1

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SW846 0270C 22-MarO7 24-Mat47 7O3127A M.B

Thit lzbontory npod it t ot vzlid withoat ad r horiAtt sigt ztuc on the covr Nge.* Rqortable Det€ction Lirnit BRL = Below Reporting Limir Pag€ 2l of 152

Page 182: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Idg ificationnfiF-r2 2'-{'sA59464-04

Clietrt Proiect #l0l-88

MatrixSoil

Receivedl9-Mar47

Colleqtiotr Date./TimeI 5-Mar47 00:00

CAS No. Analyte(s) Flq 'RDL Diluio Method Retr. Prcparul Analyzen Bdch Anabtsl

S€mivoltdle Olganic Comporrds by GCMS

Semivolatile Orqanic Comoounds bv SW846 8270CPrepared by method SW846 35508100{1€ +Nltnoanitine96€+3 Mtob€rEene8$7t5 2-Mtropftenol100-02-7 +NiaEphenolE?.75!9 N-Nitiosodimethylanxn€621{+7 lgl{trosodi-rFpaopytemine86-30{ t&NitrosddiFhenylarnine87{e5 PeotachlorophenolB54l€ Ph€mnthrene10&95t Ph€nolr2$oo{ pyrene

110-86-r Pyridine12(W-r 1,2,+Taicl{ombenzene95-954 2,4,tlrichlofophenol88{fF2 2.4,GTricftlorophenol

S{nrogate /€corrdries,'izlaas 2-Fluotobiphenyt67-t2a 2-Ffuorophenol1165$04 Nitobenzene4s1t65$2-z Phenol-ds1718.514 Tedlenyql4t1&794 2,1,€>Tribrcmophend

Totd Me{rk by EPA 60{M000 Serte3 Metbodi

I SW84A 8270C 22-l,llar9l 2+Met47 7031278 M.A

1 '

1 "

1 '

I '

1 '

1 '

1 '

1 '

1 "

1 '

1 "

8RLBRL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

766d67

u76

0.908

SRL

12.2

72.3

1 .35

16.0

339

BRL

Cornd€ted

BRL

BRL

0.0253

BRl-

BRL

BRL

BRL

BRL

82_8

Pgl(S dry 3380

UdkS dry 846pdkS dry 846pglkSdry 3380pdkSdry 8,16

ldkg dry 646

Igks dry M6

lgl€ d.y 8,16

ldksdry 846pgkS d.y 846

vgkgdty 846

ldkS dry 846

Fdkg dry 8,16pSAgd.y 846

ldkgdry 846

3L1fi%t r t t 0%30-130 %1s l10%30-130 %,81 r0%

mg/kgdry 0 0352

mS/ko dry 1.21

nrdkS dry 1.81

mS,kgdry 0.603

n4r'kg dry 0.301

mg/kg dry 0.603

nElkg dry 1.21

mgtkg dry 1.6r

r€I 0.0100

mgl o.015O

mg/l 0.0050

fign 0.0025

mgn 0.0050

mg/l O.00o{0

msil 0.m75

ftigl 0.0150

yo

743,9-976 Me.ojry

Toad M€lrb by EPA t00 Seri$ Metbods

7,14G22-4 Silv€r

74.40-3€,2 Arsenic

74{+3+3 Barium

7i!40-43-9 Cadmium

7,140{7-3 Chromium

7439.92-l Lead

7?8?-{s2 selenium

I SW846 7471A 23-tUar{7 2&Mar-07 70013ff} YP

1 EPA20O-7 2r+],€,t-Ol 24+tat47 7031305 HS

1 '

1 '

t '

t '

1 SWa46'f312 21-Vlar47 21+n€f47 7031229 BD

1 SW846 f31z6ol0E U+lat47 tuMet47 7U!1323 LR

1 '

1 "

1 ' ,

1 Sw846131217470A " 23+1.?r47 7031324 n'1 sw8461312i60108 ' 2$Mer{7 70313,i13 LR

1 '

1 SM25,l0 G Mod- 2-lht47 2+nef47 7031307 YM

SPLP Meldr by EPA lJ 12 & 60001000 S€ries Methods

SPI-P Exhadion71.10-22-4 Sllv€tr

7r40it&2 Arsanlc

Zr4{)393 Badum7.l,l04$9 Cad[ Um7140-47-3 Chro.nlum

7€e.97{ lfercury

743942-1 L€ad

n824S2 S€lsnium

Generrl CherDtlry Psl'metels

% Solids

Thft bfu@4ry .epF1 is naf wlid ulthout an ad@dzd signottre on tha @js '[ge.' Reporrabl€ Detecbn Limit BRL = Below Reporting LirDit PaAE2Z ot 152

Page 183: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-I3 2'-4'sA59464-05

Client Project #301-88

MarL{Soil

Receivedl9-Mar-07

Collection Date/Timel5-Mar-07 00i00

CAS No, AnalJte(s) Resuk Flos U.'its 'RDL Dilation Method ReL PEparcd ,4nal!.ed Bach AnalytVolatile Org.nic Compounds

VOC ExtractionVolatile Oroanic Comoounds

!g/r(g dry 3.3

UdkS dry 66 5

t S/kg dry 3 3

lrglq dry 3-3pgr$ dry 3.3pgl$ dry 3 3

tigkS dry 3.3pdks dry 3.3pSikS dry 6.7

Pg/kg dry 33-3

!g/kg dry 3.3

!g/kg dry 3-3

Ug/Kg dry 3.3

!g/kg dry 16.6

Uglkg dry 3 3

UdkS dry 3.3

!g/ks dry 6.7pdkS dry 3.3

lVftS dry 67ug/Kg dry 3.3

UEkg dry 3.3

lgkg dry 6.7gqkg dry 3.3

trgkS dry 3.3ggr'(S dry 3.3

UgkS dry 3.3

US/kS dry 3.3pdkS dry 3.3

WxS dry 6.7

PgkS dry 3-3

l4lKg dry 3.3

trg/kg dry 3.3

ljg(S dry 3.3pS/kS dry 3.3

W/kg dry 3.3pg/kg dry 3.3p.gKS dry 3.3pg/Kg dry 3.3

PdkS dry 3.3pgrs dry 3.3

lgkg dry 3.3

!Sn(S dry 3.3

tdkedry 33.3

!Sl(S dry 3.3

US/kS dry 3-3

!g/kS dry 3.3

!g/kS dry 33.3

!S/kS dry 33.3pdks dty 3.3

Field extracted VOC 20-Ma.-07 2clvar-o/ /031156 BD

Prepared by method SW846 S03SA Soit (tow tevet)76-'i3-1 l,l,2.Trichlorobifluoroethane(FreoSRL67{4-1 Acetone BRLr07-13-i Acry4onitrite BRLn1T2 Benzene BRL10e-86-1 Bromobenzene BRL74-97-5 Brcmochloromethane BRL7s-zr4 Bromodichtoromethane gRLT5-25-2 Bromoform BRL74{3-9 Eromomelhane BRL78-s3-3 2-Butanone (MEK) BRL104-51i n-Butylbenzene BRL135-98€ sec_Burylbenzene gRLga{ffi tert,Butylbenzene 8RL75-15{ Carbon disulfrde BRL5G23-5 C€rbon tetrachtoride BRL108-90,7 Chlorobenzene BRL7s-00-3 Chtoroethane BRL8746-3 Chtorcform BRL74€r-3 Chtorcmethane gRL95498 2-Chlorctotuene BRL10643-{ 4_Chlorotoluene BRL96-12+ 1,2-Dibromo_3_chtoropropane BRL124-4€-1 Dibromoc* oromethane BRL10G93-{ 1,2_oibromoethene(EDB) BRL74'95'3 Oibromom€thane BRL95 5o-1 I ,2. Oichlorobenzen€ BRL5.11-73-1 l,3-Dichlorobenzen€ BRL106-46 7 1,4_Dichlofobenzene BRL75-71-8 Dichlorcdifluoromethane(Freont2)BRL75-34-3 1,l-Dichtoroethane BRL10746-2 1_2_Dichtoroe$:'ane gRL7s-35-4 l,l.Dichtoroethene BRL15G5S? cis-1,2-Dichtorcehene BRt15ffio-5 trans-1,2_Dichtoroe{hene BRL78€7-5 l,2.Dichtoroprcpane BRL142-28,9 1,&Dichtoroprcpane BRL594-?0 r 2,2_Oichbrcpropane gRt563-58{ 1,l-Dichloropropene BRL10o61{1-s cis.l,3_Dichtorcpropene BRL10061{2{ t€ns-1,3_Dichtorcpropene BRL10@1a Ethylbenzene BRL€7€&3 Hexachloobutadiene BRL591-78+ 2-Flexanone (MBK) ARL98€2€ lsopropylbenzene BRL99{7{ 4_lsopropyltoluene BRL1634{a-4 Mehyt tert.butyl ether BRL108-10.1 4-Meffnyt-2-pentanone(M|BK) BRL7549-2 Methylene chloride BRL

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191-2(!3 Nsphthalene

Page 2l of 152

Thit ttboralorf rcporl is not wli.l withod aa aahorhad stgaafurc on the cowr page.

' Reportable Der€ction Limir BRL = B€low Reporting Limit

Page 184: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8F-13 ?'-4'SA59,16f05

ClieftProiect#30r-88

Coll€ctioq Date/Timel5-Mar-07 00:00

l,tatdxSoil

Received19-Ma.47

CAS No. naabac(s) Fl4e 'RDL Dllutiatr Itahod Retr. Prcporcd Aubzed Borch Analtst

Volalile OrgoDic Compoutrds

Volatih Orqanic CompoundsPrepared by rn€thod SW846 5035A Soit (tow tovet)103{5-1 n-Propylbenzene BRLr0o-42,5 sb,rene63420-6 1,1,1,2-Tstrachloroethane79-3?L5 |,l.a2-T€Fadorcethane12 6a Tebachloroethene

YdxS dry 3.3

ldkS dry 3.3

ldrS dry 3.3pglSdry 3.3

Fdl(g dry 3.3

udkS dry 3.3pglro ffy 3.3pgtsdry 3.3

lgr(s dry 3.3

Idl€ dry 3.3p9/k0 dry 3.3ygkS dry 3.3

ldkg dry 3.3

ttgfiodry 3.3

ldkgdry 3.3

usil€dry 3.3pdlgdry 6.7

ls/kgdry 3.3

tNkS dry 33.3

$dkgdry 3_3pdkgdry 3,3

ldkgdry 3.3

tg4(e dry 3.3

t'gl/kgdry 33.3

rgkgdry 6G s

7Gt 30 %70-130%70-130 %70-1m%

BRLBRLBRLBRLBRL

BRLSRLBRLARLBRL8Rr8RLBRLBRLBRL

1011U114105

8RLBRLgRL

BRI-

BRLBRL8SSCatculsbd as899899

sw 846 826081

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21-Ma(47 2trlet47 7031233 TR

i0B€83

87{1€

Toloene

75ir-4 vinytd{oride133G?G7 m,p.Xyt€nes647$ o-Xy,leflei0+9$g T€t€hydrofursn60-2s7 Ethylether99+@ Tert amyl m€thyl ether637-e2-3 Ediyl tert-but/ etheri08-20-r Di_isopmpylether75-65{t T€rt-Bubnol/butyjalcotlol12+91-1 1,4-Oioxane

Sa,,riDgate raco€abs--16040', +&omofluorcbenzene,w7-26-5 foluene4Slf 06047 4 l,2oichlo6ethane44t 868-5,+7 Abrunofr rfr lo m o th ane

f,xtrrcarbl€ lclrol€ m Hydrocarb{ns

EfJ9ctabl€ Total Peboleum Hydroca.bonsP.epared by method SW846 355088006414 Gasolin€68476-30-2 Fuel Oit #26847s31n Fu€l Oil f46855toc4 Fuet Oil #6M0e800000 lvlotof oitJ00100000 Aviadon Fuel

Uoidentifiedotta( oilTotal Petroleum Hydror4rbonsC$C36 Aliphalic Hydrocarbons

Surrogate /oooy€r,esi3J8el3'z 1-Chlotooctdde@ne

Semtvol.db Orgrdc Cohpo[I|rk by cCOroanochlo.in€ P€stic les SWE46 6Od1APrepared by mothod SW846 355083'o+ca Aldrin

1,2.$Tricftlorobenzene BRL12G€?r 1.2.+Trichloobeazeno BRL71.5rF6 l,t..l.Trichh.oethane BRL79{lr5 1,1,2-Tdchloroethane BRL79{t1{ Trichlorcei}Ene BRL7s{9-4 Trichlorof,uorofirethan€(Freonl.l)BRL96-18-4 l,2,$Trid oroproFne BRL95€3-6 .l,2,+Trimethylb€nzeno BRL1oS€7€ 1,3,5-Ttimehylb€nzene BRL

|ltsr(o dry 148mgrtg dry r4Emgffgdry 144mgikg dry 148nlg/kS dry 148oE/kg d.y 148nrgr'kg dry 148r'grkg dr/ 144mgilqdry 148dEl/kg dry l4a

4tr140

5

5

5

5

5

5

+cT ETPH 214a14't 2l-tttato7 f81167 DS

lryko dry 6.14 SW8,r6 808iA 2Gli.led7 2fliar{7 7l}31068 TG

This,abotuloq repod ls hot tatid tdthak! za rathorlaet sEnrturc on ahe coec, paE -' Reporhble Det€ctioo Limit BRI = B€low Repo.ting Linit PtgE 24 ot 152

Page 185: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8F-13 2'-41sA59464-05

Cliflt P.oiect #l 0 l - 88

Collection Date/Timel5-Mar-07 00:00

MatrixSoil

Receivedl9-Mar-07

CAS No. Analyt4s) Result Flae Units +frDL Dil,ltioh Method ReL Prepoted Anaryzed Belch AatlrstS€mtvolatiLe Orgroi. Cornpoutrds by cC

Oroanochlorine Pesticides SW846 808.1APreparod by method SW846 35508

319-84€ a-BHC319{5,7 b-BHC31$€6€ d-BHC58{9-9 g-BHC (Lindane)

5I-7+9 Chlordane72,54-€ 4,4-DDD (p,p')72-5rs 1,4-DOE (p,p.)

fi-2s3 4,4-DDr(p,p')@-57-1 Dietdrin959-98{ Endosulfan I33213-65-9 Endosulfun ll1031-07-8 Enctosulfan SulfateT2-2O-A Endrin7421 914 Endrin Atdehyde76-44{ Heptachtor724+5 Methoxydrtor1024-57-3 HeptechtorEpoxide4001-3+? Toxaphen€5103-71-9 a-Chlordane556614-7 gchlordane

53a9470's Endrin Ketone

Sunogate rscover'esr1038d8+2 1,4-D*Octafluorobiphenyl (Sr)

2051 -21-3 Decachlorobiphenyl (Sr)

Polvchlorinated Biohenvls bv SW846 8082Prepa.ed by method SW846 3545A

12674-11-2 PCB 101611101-24-2 PCB 122111141r6-s PCB , |232

5y6s-21,s PCB 124212612-294 PCB 12481r0s7{91 PCB 125411096-€2-5 PCB 12603732+2X PCB 12621110G14-1 PCB 1268

Surrogate recoysflesito38G8+z 4,4-D8-Octafluorobiphent4 (Sr)

2051 -2+3 Decachlorobiphonyt (St)

Semivolatile Orglnic Compoutrds by GCMS

BRLBRLBRLBRLBRLBRLBRLBRLBRLARLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRfBRL

4653

BRL

BRLBRLBRLBRL2,2601,240BRLBRL

4040

t4lkg dry 6.14

!S/kS dry 6.'14

!s/ks dry 6_14pdkS dry 6.14

lqkS dry 30.7

!g/kg dry 6.14

!g/kg dry 6.'t4

!g/kg dry 6.14

ldkS dry 6.14

Ug/kg dry 6 14pS/kS dry 6.14

ldkS dry 6.14

Ug/l(S dry 6-14pdkS dry 614pgks dry 6.14

!S/kS dry 6.14pS/kS dry 6.14

!g/kg dry 3O.7pg/kg dry 6.14

lgkS dry 6.14

UdkS dry 6.14

30-150 %30-150 %

lrs/'(g dry 12-3

lgkg dry 12.3pdkS dry 12.3

ligkg dry 12.3

lqkg dry 12.3

!g/kq dry 12.3

ldkg dry 12.3

us/ks dry 12.3pg/kg dry 12.3

30-150 %s0-150 %

t SIlg dry 736pg/kg dry 736

Lidksdry 736

ldkg dry 736

rdks dry 736

rcnS dry 76

US/IS dry 736

Ig/tS dry 736

sw846 8081A1

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m-Mar47 2541'ai-07 7031058 TG

sw846 8082 21-Mafi1 2rMafi7 703116/

Semivolatile Orqanic Comoounds by SW846 8270CPrepared by rn€lhod SW846 35508

a3'32-9 Acenaphthene208-964 Acenaphthyiene62.53'3 Aniline120-12,7 A,rthfacene1912-24-9 Atrazine103.333 Azobenzeneoiphenytdiaane92{7-5 Benzidines6-5+3 Benzo (a) anthracene

BRL

BRL

BRL

SRL

BRL

SRL

BRL

BRL

sw646 8270C 22'-MarO7 264llat47 7O3127A M.B

fhit lfionloq rcpoa k not vdid wirtoa aE azttoipn signaturc on rhe cot!4 page.

* Reportable Detecrion Limir BRL = Belov/ ReportinB Limit Page 25 of 152

Page 186: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiotrM8F-n 2,-4'sA59464-05

Clietrt Proiect #301-88

Collectiotr Date/Timel5-Mar-07 00:00

MahixSoil

Rec€ivedl9-Mar-07

C,lS No. AQzlrte(s) Resull Flag 'RDL Dilution Melh4dRetr, heparcd AnzlWA Both Anoust

Semivolrlil€ Organlc Comportr& by CCMS

Somivolatile O.qanic Comoounds by SW846 8270C

Prcpared by method SW846 3550850.324 Benzo (a) pyr€ne20199" Benzo 0) nuoEntlrener9r-2+2 Benzo (g,h.i) pery,tene20ru84 Benzo (k) firorantEne65{5{ Benzoic acjd1ql516 Be(uylalcohol1 i 1 -91 -1 Bis(2-d1lorcethory)nEthanet11-444 Bis(2-d{oroethyt)€0Er3963&32.9 Bis(2d&Kisogropytlethef117€r-7 Bis(2-etrtheryl)phthalatet01-513 +Bromoph€ny phenyt ethef€sa'7 Butyl berEyl plfihalatE86'7rr€ Carbazol€59's0.7 +Chloro-&methylph€nol106-47{ +Chtoroaniline91'5+7 2-Ch*c.onsph$alene95-57{ 2-Chlorophenol700172-3 4chloroph€nyt phenyl ether21841{ Chrysene53-703 Obenzo (a.h) enthracenej32-64.9 Dibenzofuran95-5Gl 1.2{)icilorcbenz6n€541-rcn 1,3-Dichlorcbenzen€l06..ez 1!-DichlorobefEene91-9+1 3,3'-Oic+orobenzidin€120-83-2 2,4-Did{q.ophenol8,ri&2 Oiethylphu.ratate131-11,3 Dime{lyl ph[iatate10s7-9 2,4-Dimedrylphenolu-r4'2 Di-n-butylphthalate534-52-1 4,SDinife2-methytphenol51-2&s 2,+Dinitroph€nol121-141 2,+Dinitniotuene60@2G2 2,6-Dinll.otohrene11741-0 Di-n-octylph$alat€206,44{l Fluoranhene86.7$? Fluorenet1&711-1 Hexadllorob€nzenea76a-3 Hgxschlo.lbut6diem7r4r4 llExec*tlorocyc.lopentiadieoe67-72-1 H€xachbroetlune193305 lrdeno (1,2,3-cd) pyrcne9G12{ l.Mohylnaphthalone78-59-1 lsophoroneel-57{ 2-i,l€thylnephthatenes6-4&7 ?-tiiethylphenolio&3s-1, 3.'l-Mcthylphenol106-,14-591-2G3 Naphthalene88-74-4 2-NitoanilinelE{x}2 }Nitroaniline

SW846 8270C 22+{iaf'o7 zstrtat47 7031278 M.BBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRI-8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBR|-BRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRL

BRLBRf8RL

ldkS dry 736pSilg d.y 736p{kS dry 736

ldrSdry 736

ISAS dry 736

UgkS dry 736

lgkS d.y 7SygkS rtry 736

$dtsdry 736psftSdry 736pdks d.y 736pdkgdry 736

FdkS dry 736pSn(S dry 736

t'dksdty 736

ldks dry 736pdks dry 7fipgft€ dry 736

!gl(9 dry rupdts dry 736

lgkgdty 736

lgftS dry 736

Wit€ d.y 736pS/kS dry 73{ipS/kS dry 736pdrsdry 736

ldtg dry 736

ldkS dry 7

!Sn(S dry 736pgltlg dry 734

Fdkg dry 736

lSftSdry 736

FglS dry 736perlq dry 736

ldkSdry 736

udkg dry 736

USftS dry 7

udkg dry 736p€ikS dry 736

ldksdry 736pdkS dry 736pgrS dry 736

ldl(gdry 736

ldks dry 736

ldkS dry 736

lgrkg dry 736

t4Jkgdry 736

rd*gd.y 736p4ksdry 736

|JdXo dry 736

T rtts labodorf rcpod b ,tot vdid vahoa an suthoid signrttn oA t a coter pege.

' Repodable D€recrion Limit BRL = Below Reporting Limit Page 26 of 152

Page 187: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificarionM8F',.r3 2'-4'sA59464-05

Clie Proiecr #30t -88

MatrixSoil

Received

l9-Mar-07Collection DatdTime

l5-Mar-07 00:00

CAS No. Analyte(s) Resah FloC Unib *RDL Dilulinn Metho.l ReJ Preparen Ana\zed Batch AnabslSemi!oletil€ Orgrnic C0mpounds by CCMS

Semivolatite Orqanic Comoounds bv SW846 8270CPrepa€d by method SW846 3S5OB

100{1€ 4_Nitroanitine9€-9+3 Nitrcbenzene88-/n5 2-Nitrophenol10r),02-7 4.Nitrophenol62-7tS N-Nilrosodimethytamine621.64,7 N-Nitrosodi-rFpropylemine8G306 N-Nitrosodiphenytamine87{e5 Pentac*tlorophenol85{1-8 Phenanlhrene

108 95-2 Phenol129-00 {t Pyrene110{6-r Fyridine120€2-1 1,2,4-Tdchlorobenzene95-954 2,4,s-Trichtorophenol8a-06-2 2,4,GTrichtorophenol

Sumgale rccovelies,32140-8 z-Fluorobiphenyl

36H24 z-Fluorophenol

41 654co Nitrobenzene-ds

416542-2 PhenoHS

1718-514 Teryhenyl4l4

118-79-6 2,4,6Tibtoflnphenot

Ug/kg dry 2950

uS/kS dry 736

!$'l(g dry 736

!S/kS d.y 2950

ldtS dry 736

!g/kg dry 736

!g/kg dry 736

UdkS dry n6

!g/kq dry 736

!S/kS dry 736

t/S/kS dry 736

!S/kg dry /36pSn(S dry 736pSftS dry 736

ldkS dry 736

30-130 %t5-110 %30.130%15-110 %3U130%15.110 %

mg/kg dry 0.03.44

mg/kg dry 0.990

mg/kg dry 1.48

mg/kg dry 0.495

mS/kS dry 0.247

fi'SAS dry 0.495

rE/kg dry 0 990

nlg/|.g dn/ 1.48

msil 0.0100

mg/| 0.0150

mgn 0.0050

m9 0.0025

m9 0.0050

m9 0.00040

mSI 0.0075

rhg/l 0.0150

yo

I SW846 8270C

1 '

1 '

1 "

1 '

1 '

1 '

1 '

1 "

1 "

1 "

1 "

I '

l '

1 SW846 7471A

22-MarO7 2s-+l,ar07 7031278 MBBRLBRLBRLBRLBRLBRLARLBRLBRLBRLSRLBRLBRLBRLBRL

77

661M79

0 242

BRL

13 .1

66.4' 1 .18

2 0 5

5 r8

8RL

Totrl Metrls by EPA 60{0/?000 Series Methods

7-43947{ Mercury

Torrl M€tNts by f,pA 20{ seri6 Merhods

7440 22-4 Sifuer

74'tG3&2 Arsenic

7440-393 Badum

7440-43 9 Cadmium

74,{)-47-3 Chromium

7439,92-1 Lead

778249-2 Selenium

23 Mar-07 26.tlar-07 2031306 YP

EPA 200.7 23-lvar.07 24-Mar-07 7031305 HB

BO

LR

LR

SPLP Metdr by EPA 1312 & 6000/?000 S€rics M€rhods

SPLP Exhaction

74-40-22-4 Silver

7440-3&2 Arsenic

7"40-3+3 Badum

7440-4+9 Cadmium

7440473 Chromium

7439-97{ Merstry

743+92-1 Lead

7782-49-2 S€l€nium

Cen€rd Chemistry Param€ters

% Solids

1 SW8461312 21-Mat47 2141,aA7 7031229

1 S'/v8461312/60108 22.1,iat47 23 ltarl7 7031323

1 '

1 '

1 '

1 '

1 SWM6'131217470A " 23+,nar47 7031324

1 SW84613126O108 . 23-Mat47 7031323

1

Completed

BRL

BRL

0.0216

BRL

BRL

BRL

BRL

BRL

86.9 1 SM25.f0 G Mod zz-Ma..oi 22.$ia'-Ol 703t307 Yl\4

This loborulory rcpod is not vdd ithoa 4n aalro zed sign tan on the cover page.

* Reporlrble Detection Limir BRL = Below Reporring Limit Paze 21 ot 152

Page 188: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 189: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdenfificationM8F-I4 2-{'sA595l7-04

Client Pro.iect #l 0 l - 88

Collectior Date/Timel9-Mar-07 00:00

MatrixSoil

Received

20-Mar-07

CAS No, Anob.e(s) Result Ftoe Unik *RDL Mahod Ref, Prepued Anolyttd Batth Atu\st

Volrtile Orginlc Compounds

VOC ExkactionVolalile Oroanic ComDounds

Ug/kg dry 67,8

Ug/r(g dry 1360

PgKS dry 67.8

lgKs dry 67.8

US/Kg dry 67.8

!g/kS dry 67.8

!S/kS dry 67.8

!g/kg dry 67Ipg/kg dry 136pSlkS dty 67Apg/kg dry 67.8pg/(g dry 67.8pg/kq dry 67.8pg/kg dry 339pg/kg dry 67.8

US/kS dry 67.8

!g/kg dry 136pg/kg dry 67.8

!g/kg dry 136

B9/K9 dry 67.8

rc/kg dry 67.6

!g/kS dry 136pS/xS dry 67.4

WBS dry 67.4pS/kS dry 67.8

Wkg dry 67.8pg/kS dry 67.8pg/kg dry 67.8pgikg dry 136pg/kg dry 67.8

!S/kg dry 67.8

!g/kg dry 67.8

!g/kg ory 67.8

lgkS dry 67.8pg/kg dry 67.8

IgKg dry 67.8

!g/kS dry 67.8

tgkgdry 67.4

ldkS dry 67.8

lgftS d.y 67.8

ldkS dry 67.8

!S/kS dry 67 I

liS/kS dry 678

!S,4(S dry 67.8

trS/tS dry 67.8pS/kS dry 57-8pdks dry 67e

ldks dry 678

Lrdkg dry 67_8

21-Ma.{7 21-Mar-07 7031261Field extracted

Prepared by method SW846 5030 Soit (high tevet)761t1 1,1,2-Tricfilorotnfluometftane(Freo€RL67-64-l Acetone107-13r Aoylonitile7143-? Benzene

SW 846 82608 2r-Ma.-O7 274taFO7 7031602 mar8RLBRL1,520

505050505050505050505050505050505050505050

50505050505050505050505050505050505050505050505050505050

108{6-1 Bronrobenzene BRLT4-97-5 Brormdtloromethane BRL75-274 Bromodichloomethan€ BRL75-212 Brormform gRL

7443-9 Bromomethane BRL78-93-3 2.Eutanone (MEK) BRL10.F51€ n-Buvlbenzene BRL13ts8€ sec€utylbenzene BRL9€ 1)6-6 tert_Buvlbenzene BRL75'1t0 Carbon disultide BRL56 23,5 Carbon tebachtorade BRL108-90-7 Chtorcbenzene BRL75{0-3 Chtorcethane BRL6766-3 chloroform BRL7447-3 Chloromethane sRL95-4S-8 2-Chlorototuene BRL10H34 4-Chlorotoluene BRL96-12{ t,2-Diblomo-3rhloropropan€ BRL12+46-1 OibromochloromefEne BRL106-e3-4 t,2_Dibromoefiane(ED8) BRL74,9S3 Dibromomethane BRL95-s0'1 t,2-Dichtorobenzene BRL541-731 t,3_DicJatorobenzene BRL10616'7 t,4-Dichtorobenzene BRL75'71-a Dichlorodifuoromehane(Freon12)gRL75-34-3 1,1 . Dichloroethane BRL107{6 2 l,2-Dichloroehane BRL75-3+4 .l,l-Dichloroethene BRL1s6-5s2 cjs- 1 ,2-Dichlorc€theyte BRL156+5 rans- 1,2-Dichloroethene BRLTA-47-5 l,2-Dichloropropan€ BRL142-28-s l,3-Dichloropropane BRL594-2G7 2,2-Dichloropopane 8RL56$58€ t,1-Djchlo{op{Dpene BRL1061{1-5ds_1,3_Dichloropropenc BRL10061{?5 tans-1.3-Dichloropropene 8RL10$41-4 Ethylbenzene 309875+3 Hexachlorobutadiene BRL591-76€ 2-Hexanofte (MBKI BRL9€42-8 lsopropylbenzene 75.399+74 +lsoPropyitoluene sRL1634{44 Methylte(-but\y' ethe. BRL108-10-1 4-Methyt-2-pentanone(Ml8K) BRL7s{92 Methylene chlodde BRL

44791.20.3 Naphthatene

Pa€e l7 of 124

This labontory report it not wliil htlthout on ashoizctt signorurc on the cowr pdge

r Reportable Detection Limit BRL = Below Reporting Limit

Page 190: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdcntifrcationMtF-l{ 2-l'sA595t7-04

Cli€ot Project #301-88

MatrixSoil

Colle€tion Date/TimellMar{7 00:00

Received2O-Mat-01

CAS No. Analyt2(s) Resal FI"S 'RDL DiIatL'n Merhol Retr, Pepaled AMIWd Batch Aizlt\.

Voladle Organlc Co|npounds

Volatile Oroanic ComooundsPrspared by mettbd SW84.6 5030 Soit (high levet)

7t69-4 Trichlorofluomm€tEne (Freon 1l) BRL

10s-65r n-P|opylb€n2erlel0o-42'5 Styrene63()'Al€ |,1,1,2-Tetrachtoroethans7s34-5 t,i.2,2-Tetrac+lloroethan€127-18-a Tet€chlometh€ne108{83 TOlUenO87{1{'1,2,}Tfidt lorobenzene12G€2n |,2,+Trichlo|obenzene7l{5{ 1,1,1-Tridofo€lhane79{G5 1,1,2-Trichloro€thane79{1{ Trichloroethene

9+18-4 l,2,3.Trichlompropane956+6 1,2,+Tdmethylb€nzene10&67€ 1,3,5-Trimethylbenzene7541'1 Vlnylcfitoride1 3ilo?G7 m,p-X!,t€ne95-47{ o-Xylene'109€99 TetEhydofuran@'29-7 Ethyl ofEr99as€ T€d-amylmeulytether637-9?3 Ed1yt terttutyl €d1e10&?0-3 Diisop.opylelh€r7565{ Tert-Butanol / but},t alcohol123-31,1 .l,4-Dioxane

sltrog|ab ,Bcoverbsj4&-@1 +Brcmolluotubenzene2037-2&5 Toluene4E1 lffi 047 -o 1, z-Dicl' o@ehane441 gJoIrS+l Abromofl uotonethane

f,ltract ble PctrolflI|l Hydrocfibons

Ettra.lable ToUl Petroleum HvdrocarbonsPr€pa.ed by m6hod SW846 355088006{1€ Gesoliat€€8,17G30-2 Fu€t Oit #26447G313 FuetOit #46€553.0il4 FuetOit#6u090000o0 tilobf oilJ00100il0O Avlatioo Fuel

Unlr€ndfiedOt|€ OilTotal Peboleum HydrocgrbonsC9436 Aliphatic Hydroa€.boos

sl/rDg|ale aecor,en€ar$tr633-2 l-Chlofiloctadecano

Semlvolrtile ()rgrdc Coltrpoutrd3 by cCOrlanocfilorine Peslicid€s SW846 8081APrepared by method SW846 3550930$llG2 Aldrin

$W 846 82608 27-Ma(07 274at-O7 7031602 marr43BRLBRL

BRLBRI-3,020BRL

BRLBRLBRLBRL

pg/kS dry

LrdkS dry

ugko dry

!s/*s dry

PgkS dry

lgks dty

ugvadrypgks dry

FdkS dry

ldks dry

!94!S dry

Itdkg dty

FgkS dry

lglqS dry

Idkg drypdks dry

US/rg dry

ldls dry

UgkS dry

ttSJkS dryyg/kS drypdks dry

rcftS dry

lgkS dry

UgkS d.y

67.8

67,8

67.8

67.6

67_8

67.8

67.a

67.8

67.8

67.6

67.8

67.8

67.E

67.8

67.8

136

67.8

674

67.8

67.8

67.4

678

1360

BRL2@BRLARL906507BRLBRLBRLBRL8RLBRLBRL

s91079295

505050505050

505050

5050505t)50505050

50

50

7t).1fr%7G130 %70-130 %7Gt30 %

BRI-BRL

BRLBRLCdoJliaiad asBRL380BRL3803m

drykg drynE/kg drynrgL/kg dayrrlgnlg dry.ns/ks dfymdks drynE (g drymgikg dry.ng/kg dryr|gkg dry

30_530,530.5

30.5

30.530.5

+CT ETPH ?2-Mat47 234Ja(47 7031281 DS

BRL

40.140 %

pS/rS dry 6.41 SWE ft SOatA 22+nt47 Z7ilar47 703t275 TG

This labotubry Eporl lt not tat t utthottt ott dhorirpd sFt ttttft on,hc cow. pate.

+ Reportrbl€ Dete.lion Limit BRI- = Below Reporting Limit P a g e l S o f l 2 4

Page 191: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8F-14 2-4'sA595l7-04

Client Proiqct #301-88

Matri(Soil

Collectioq Datc/Time19-Mar-07 0O:00

Received20-Mar07

CAS No. Anatrte(s) Flag U r s *RDL Dilution Merhod Ref, P,eparcd Ansbzed Batch Anat!:st

Semlvalrtile Orgrnic Compornds by cC

Orqanochlofine Pesticides SW846 SOBIAPrepared by .r€thod SW846 3SSOB

319-845 a-BHC319{5-7 b-BHC31e-8ffi d-BHC5,4{e-e g.BHC(Lindane)

s7-74-9 Chlordane7251{ 4,4-DDD (p,p.)72'5te 4,4-DDE {p,p')5{r2e3 a,4-DDT (p,p,)6O-s7,1 Dietdrin959-98{ Endosulfan I3213$5-9 Endosulfan tl1031i?-8 Endosutfan sutfuteT22GA Endrin7421-934 EndrjnAtdehyde76-44-A Heptachlor724?5 Methoxychtor1024-s7'3 Heptachlo{ Epoxide8001-35-2 Toxaphene5103-71-9 a-Chlordane5566-3,|'7 g-Chlordane

5349.-70-5 Endrin Ketone

Surogale rccowies:1we68+2 4,4og-Octafluotobiphenfl (542051-243 Decachlorobjphenyl (Sr)

Polvchlorinated Biphenvls bv SW846 8Og2Prepared by method SW846 35508

r2674 11-2 PCB l0 l611104-28-2 PCB 122111141-1es PCB.t232s34€+21-s PC8 124212672-2en PCB 124811097{9-1 PCB 12541109F€2-5 PC8 12603732+23-5 PCB 12621110C14{ PCB 1268

Suftogate .scoveias:

10386-84.2 4,4-O8-Octaf,uotobiphenyt (Sr)

2OSt-?4-i Decachlorobiphenyl (3r)

Semlvolrtlle Orgrnic ComponEds by cCMS

SW846 8081A 22-Mat47 27-Mat-07 7031275 TGBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLSRLBRLBRLBRL8RL8RLBRLBRLBRLBRL

3258

BRLBRLBRLBRLBRLBRLBRLBRLBRL

50

BRLBRLBRLBRLBRLBRLBRL1 ,510

pdkS dry 6 4tpdks dry 6 41

!g/kg dry 6.41

USI(S dry 6 41

ttStkgdry 32.O

US/kg dry 6.41pg/kg dry 6.4'l

Udkg dry 6.41ps/ks dry 6.41pS/tS dry 6.41

PqkS dry 6.41pdkSdry 641pg/kg dry 6.41

PdkS dry 6.41

ldkg dry 6 41

ldkg dry 6 41

UdkS dry 6.41

lSlkS dry 32.0

tig/kg dry 6.41

Pg/kg dry 6.41

l4/kg dry 6.41

30-150 0a

30-150 %

US4q dry 12.4

Ugks dry 12.8

UqkS dry 12.4

UgkS dry 12.4

Ug/kg dry 12_a

Udkg dry 12.Apgkgdty 12.8pg/kg dry 12.4

ldkS dry 12.a

30-150 %30-150 %

USn(g dry 757

lgl€ dry 757

lSftS dry 757

ttglqg dry 757

PeJkgdty 757

rglls dry 757pSn(S dry 757pSlqdry 757

1

r1

1

1

1

1

1

1

1

1

I

1

1

1

1

1

1

1

1

I

SW846 8082 22-Mat41 24-Mat41 1031274 MP

Semivolatile Oroanic Comoounds bv SW846 g27OC

Prepared by method SW846 35508a3i2-9 Acenaphthen€20&96-€ Acenaphhylene62,53-3 Aniline120-12-7 Anthacene1912-24-9 Atazjne10133,3 Azobenzene/Diph€nytdiazine92-s7-5 Beruidine56-5!3 Benzo (a) anthracene

SW846 8270C 22-Mar07 24-Mar-O7 7031279 M.B

Thb lqbotulory EForl as,rotvsltl 'ithout an raahod?ld sigrrddtrc on the coter page.

. Ret onable Detecrion Limir BpL = Below Rgporinl Limit Prge 19 of t24

Page 192: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Salnple IdefiificatiopM8F-l{ 2-4'sA595l?-04

Client Proiect #301-88

MaFixSoil

Collectioo Date./Time| 9-Mar{7 00:00

R€ceiv€d20-Mar-07

CAS No. Anslrta(s) Flos Unib *RDI Dilutioa Method Rctr. Prepated Adalyed Bdch An4lrst

Semlv0hltl€ Oryrnlc Compoun& by GCMSSemivolatile Orqanic Compouods bv SW846 82ZOCP.epared by method SW846 355085O32,a Benzo (a) pyren€205'9$2 Benzo O) ftioranthene1sl-24-a 8€nzo (g,h,i) perytene207{r!r.9 Benzo (k) f,uoranhene65{s-O B€nzoic acjd10{}.51.€ Berizy alcoholilt-91_l Bis(2€hloroethoxy)methaneIfi-{.44 8i6(2-ddotpehytFher3963&32€ Bis(2d{oroisopropyt)ether117-01-7 Bs(2-€thyltleryl)phfl€tater0l-5+3 4-Brofttophenylphenylefter85{&7 Bu!/benzytphfiataie8t?4{ Carbazole59,5G7 +Chtoro_g-methyiph€nol106-47{ 4chloroenitine91-5€.7 2_Chloonaphthalene!15-57{ 24hbrophenolnE5'72-3 +Chlo.oph€nyl phenyt €ther2i8-01.9 Chrysene5+7G3 Dibenzo (a,h) antrrrscen€i32{4€ Dib€izofuaan95-5Gt l.2-Diof orobenzen€541'73-t l,lDichtorobenzens10646-7 1,4-Dichlor.obenzene91€4,1 3.3'-DichlorobefEidinei2o{3-2 2,4-Oic orophenol04{c2 oiethyt phfElat€13i-1r-3 Dimethy{phthatale105-67-9 2,+Dim€drylph€noto+7+2 Di-n-buty'phfiatats53+,52-1 4,6-DiniblF2-[rehytphenol5l-?&5 z,+Dinifoptrend12r-14.2 2,4_Dioilr,otoluene60c20-2 2,6-Dinitrhiu€ne117{4{ D-n{d}tphhatat€m6-{4-O Fluo.€ndEne8€-73-7 Fluor€ne1l&7+l llexachloiobenzene874&3 HexadJombutsdiener|474 Hexet orocyclopentadi€ne6r-72-1 Hexadlloro€thane19&3$5 Indeno (1.2,4cd) pyr€ne9G12{ l.Methy'nryhthalen€78-5+1 lsophoavt€9157.6 2-irGhytnaphthatene9+4&7 2-M€byhhenol10&3s.a, 3,+M6thylphenol1oc44-s91+03 Naphtla|€.|€&7.1-4 2-Nitro€r{he994+2 $Nltroendine

1,8901,8609582,030

8RLSRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLr.840BRIBRLBRLARL8RLBRLBRLgRL

SRLBRI-BRI-BRLBRLBRLBRLBRL

2,820BRLBRL

BRLARLBRL968

BRI-

BRLBRL

BRI-

BRLBRLBRL

UdkSdry 757pdks dry 757

WkSdry 757pg,rs dry 157

ldkgdry 757

ldkg dry 757

tdkgdry 757

lSftgdry f57pCftSdry 757

ldks dry 757pdkgdry 757pSlgdry 757

FS/kS dry f57pglsdry 757

ldkS dry 757

lgl(g dry 757pCxS dry 757pqkg dry 757p4kgdry 757

Uglkgdry 757pSI(S dry 757

t4,lksdry r57ygts dry 757

ldrsdry 757

llg/kS dry 757

US/kSdcy 757

Igil€dry 757

rdkgdry 757

['dkg dry 757

rdksdry 7s7

ItSlkqdty 757

uqlSdry 757p91(9 dry 757

USeSdry 757

udkS dry 757pdkS dry f'f

Fdkgdry 757pdks dry 757

FdkS dry 757

!9rS dry 757

sgko dry f57gtlqdry 157

tytS dry 757

ldks dry 757pdkS dry 757pSJRgdry 757

us/kgdry 757

pgjkgdry 757

!dl(S dry 757

ldkg dry 757

t

1

1

1

1'|

I

1

1

I

1

1

I

I

1

I

1

1

I

I

1

1

1

I

t

1

1'|

I

1

I

1

I

I

1

1

1'|I

1

1

1

I

1

1'|

I

1

1

SW8,'{18270C 22 tar0l 24+lat47 7O3l27S M.6

Ihls ,4brobry Epott is ,',ot ttdld withod att aalho.iael twEdue oa the cow! page.

* Repo.table Der€ction Limir BRL = Below Reporting Limir P€e 20 ofl24

Page 193: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-14 2-4,sA595 t7-04

Client Proiect #301-88

MatrixSoil

Collection Date/Tirne| 9-Mar-0? 00:00

Received20-Mar-07

CAS No. Analrre$) Fl4S Ani6 *RDL Diluliot Method Retr Preparcd Analyzed Bakh AMUst

S€mivolattle Orgsnic Compoutds by GCMS

Semivolatile Oroanic Comoounds bv SW846 B27OCPrepared by melhod SW846 35508

100{14 4-Nitrcaniline98-9t3 Nitrobenzene€8-7$5 2-Njtrophenol10GO2-7 +Niroph€not62-7t9 N-Nitrosodimethytamine6216{-7 N-Nihosodi_n_propylamine86-3G6 N-Nibosodiphenytamine87{e5 PentacfilorcphenolB5{1 I Phenanlhrcne108-95-2 Phenol129{0{ Ptrone110-86-1 P,yridin€120{21 1,2,4_Trichtorobenzene95-9s4 2,4,5,Trichtorophenol08{6-? 2,4,GTrichlo.ophenol

Sufiogale rccoveies:321a0-8 2-Fluorobiphenyl

367-124 2+luoropheool

4165-60-0 Niuobenzene4s

116U62-2 Phenol4s

1718-s14 Tery,leny'4l4

1ra-79 6 2,4,6-Trbrcmophenol

Tord Merrts by EPA 6000/7000 series Methoos

743997$ Mercury

Totrl Metals by EPA 200 Seriti Methods

744G22-4 Salver

7.4401&2 ArsenaC

7440-3+3 Barium

7440-4+9 Cadmium

71{r)-47,3 Chromium

743+92-1 Lead

77€2-49-2 Selenium

SPLF Metrls by f,PA l3l2 & 6000/7000 Sert€r Merhods

SPLP Erdraction744C22-4 Silvef

744G3e2 A6enic

744C3*3 Barium

7.1,10-4!9 Cadmium

f 44(47-3 Ch.omium

743S97€ Mefcrrry

7439.92,1 Lead

7182-4+2 Selenium

Generol Chemistry Param€ters

% Solids

BRLBRLBRLBRL

BRLBRL8Rr_BRTBRLBRL2,450BRL

BRLBRLBRL

57725180

0.270

BRL

9_01

0 600

28.3

292

BRI

Comdeted

BRL

BRL

0.0r42

8Rt

BRL

BRL

0.0310

ARL

86.3

pdr(g dry 3030pS&S dry 757pqkSdry 757

!$ftS dry 3030

lgkS dry 757

PdkS dry 757

fdkg dry 757

lidKS dry 757

PsftSdry 757pg/kg dry 757

ldks dry 757

trErq dry 757pS/kS dry 757

!d(g dry 757

f./dkS dry 757

30-130 %1G|10 %a-130 %15-110 %34-130 %15110 %

mgr'kg dry 0.0342

rYtgfl(g dry 1_14

mg/kS dry 1.71

m$ftg dry 0 571

nEukg dry 0 206

msfts dry 0,571

mgks dry 0.857

mgikg dry 1 71

mgn 0.0ro0

mS,4 0.0150

mg/l 0.0050

mg/l 0.0025

nV, 0.0os0

mg/t 0 00(X0

mg/l 0.0075

mg/l 0.0150

%

1

I

1

1

1

1

1

1

1

1

1

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1

1

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SW846 8270C 22-Mat47 24.n|/,a(O7 7031279 M.B

1 SW846 7471A 26-Mafi7 27.Ma..oI 7031322 YP

EPA 200.7 26-Ma'-07 27-Mat-07 7031321 HB

1 SW8461312 22-Mat47 22-Ilar'O7 7031344 BD

1 SW846 1312/60108 23-Mar-07 24-Mar-07 7031408 LR

1 '

1 '

1 "

1 '

1 SW8461312/7470A ' 26-Mar-07 7031409 YP

1 SW84613't260108 ' 24-Mar{7 7031408 LR

1 '

1 SM2540 G irod. 23-Mat47 23-inal.O7 7031429 QP

Thb labrutoq fcpofl is not vdid withoa at ot/rtoized signatuE on the cover pge.

' Reporfrbl€ Detectbn Limi BRL = Below R€?or,tng Limir Page 2t of 124

Page 194: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ld€ntificationMtF-15.1-6'sA595t7-0J

Client Proiect #301-88

MatfixSoil

Collectioo DatdTimel9-Mar47 00:00

Re{eived20-|.tlat-07

CAS No. ,!nable(s) Flag rRDL D aaA'" iterhod Retr PrepoQl Attalfzd Bat h Ana$st

Volrtile Org lc Cmpoundi

VOC E.xtraclion Field o)draded

Volatile Orqanic CompoundsPrepared by m€thod SW846 5035A Soit (tow tewt)7&1!1 l,l,2.Trichtorotriffuoroothane(Freo€RL474+1 Acetone BRL10?.13-1 A.rtonitdl€ BRL71<.T2 B€nzene BRL108€e1 Brcmb€nzene BRIZt€75 Eromo<filoromethane BRLfr271 Brornodichloromethane BRL7+212 S.oanoform SRL7a{}9 Broflrdnethene BRL78.e!13 2€ubnode (MEK) BRL1(X-sl4 rFButylbenz€ne BRL13+S{ sec-Butt4benz€ne ERL98{6-6 t€rt€utylbenzen€ 8RL75-15.0 Cer0on disuhde BRL5G215 C€rbon teb&hlorftte BRL10&90-7 O o{obenz€ne BRL75{G3 Chloroethsno BRL67{6-3 Chtoloform BRLzr{7-3 chlolofir€Ersne BRL95{9{ 2-Chlorctolu€ne BRI1o6-4i14 4-Chlorctoluon€ BRL9€_12{ 1,2-Oibrorno.3.c}o@propan€ BRLl2a-48-1 Dbromochbromethane BRL10e9+. l,2-DibromoedEn€ (EOB) BRtz,t-9+3 Dibro.nomethane BRL9s5G1 l,2oidllorobenzene BRLs41.?:lr l,3oicHofob€nzene BRL106-{s7'1,4-Obhlo.ob€nzene

uglkgdry 7.3

t dkS dry 146

trSikg dry 7.3

Pgkg d.Y 7.3

ldkgdry 7.3

ustkgdry 7.3

vdkgdry 7,3

Fg/kgdry 7-3

lrsjkg dry 14.6

lgkg dry 73.1

IdkS dry 7.3ygkS dry 7.3

lg,tSdry 7.3pdkS dry 36.5

t/dkS dry 7.3

ldkg dry 7.3pg/tg dry 14-6

lCftS dry 7_3pOkS dry 14.6

UgkS dry 7.3

ItgkS dry 7.3

t dkS dry '14.6

UCAS dry 7-3pdkS dry 7.3

rdks dry 7.3pdkS dry 7.3pgkS dry 7.3pS^g d.y 7.3pg/kg dry 14.6

sdkS dry 7.3

FSftS dry 7.3

ldkS dry 7.3pgAS dry 7.3

FgkS dry 7.3

trS/kS dry 7.3

FdkS dry 7.3

USilg dry 7.3

lgrS dry 7.X

!gl(9 dry 7.3

IdkS dry 7.3

ldks dry 7.3

IBAS dry 7.3pdkgdry 73.r

tglqdry 7.3

|lgftS dry 7.3pSfl€dry 7,3yqkgd.y 73.1pdkS dry 73.1

UgXSdry 7.3

21-Mat47 21'l[ta'.07 7031261 BD

7s-7t+ Dchtorcdifrloromethan€(FGont2)BRL75-3+3 l,l-Dichlofoethsne BRI_107S-2 |,2oichloro€thane BRL7s-35-4 1,l -ttictdo.o€thsne BRLls&59-2 cis-i2-Dicfdorcethen€ BRLlsf!6o{ bans-l,2oichtoroethene BRL78{7.5 l,?-Dicl oroFopane BRI-t42-2&9 t,3-Did{o|tpropsne BRL59+41"7 2,2€icHorcprcpane BRL56450{ 1,l-Dichtoropropen€ BRL10061{1-5 cigl,3-oichloropaoD€ne BRL10(E1.02{hane.t,3oidrlorcpmpede BRL10041-4 EthytbqE€ne BRL874s3 Hexacfibrobutadbne BRLi91-78{ 2-H6xanm€ (MBK} BRLs{2{ tsop.@ytbeiEen€ BRLse{7{ 4-tsopropyltoluene BRI10:x{4{ M€hyt t€rtrbuM €sler BRLloslGl +Mefiy&2-p6nlanooe(MIBK) BRL75.{)!}2 Meth}4€n€ drloride BRL

SW 846 82608 22+nar07 2X4ar47 70313:15 RU

BRL

1

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I91-20"3 NspMalen€

Pagezz of 124

Thb bborolory tqod ie nd pallt wlthotd on zulho.iaed sigrrrt/re 06 ,he covu page.

'Reporbbl€ Detectim Limit BRL= BelowRrportiag Limit

Page 195: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-I5 44'

sA595l7-05

Client Pmject #301-88

Collection Date/Timel9-Mar-07 00:00

Received20-Mar-07

MatrixSoil

CAS No. Anoqta(s) Flog 'RDL Dilatioa Itethod Retr. Prcparcd Analfzed Batch Analjts/

volatile Organic CompoundsVolatile Oroanic CompoundsPrepared by method SW846 5035A Soit (tow bvet)

75$9-,{ Trichlorofluoromeltune (Freon 11) BRL

10!6tl n-Propytbenzene100-42 5 Styrene63C20$ 1,1,|,z-Tetrachloroethane793.1-5 1,1,2,2-Tetrachloroethane127'18-4 T€tEchloroeihene10&€&3 Toluehe87$1$ 1,2,3-Trichlorobenzene120-821 1,2,4-Trichlorobenzene71_55_o 1.1 , t_Trichloroethane79{0-5 1.1,2-Trichlorcethane79{1-6 Trichloroethene

96,18-4 1,2,3-Trichlorop.otEne95$36 1,2,4-Trim€thylbenzene108-67{ 1,3,gTdm€thytbenzene75414 Mn/chlodde13m-20-7 m,p.Xylene9s-47-6 o-Xylene10+994 Tetrahydrofuran60-29-7 Ethylether99€tr Tert-amyl meftyl ether6r7-e2-3 Ethylte(-butytether10&20-3 Di-isopropylethef756t0 Tert-Butanol/ but/i alcohol123-91-1 1,4-D:bxene

Suri.ogato recol€oesi

41040-4 +Bromofluorcbenzene

203/-2cs Tduene4S

| 7 @G074 1, 2-Dbhlotoe.Ihane44

1E6a-5?7 Dibrotnofluoromethane

Erhact ble P€koleum Hydroqrbons

Extractable Total Petroleum Hvdrocadons

Prepared by method SW846 3545A

8006{l-9 Gasoline6ea7+30-2 FuelOil#260476-31-3 Fuel Oil #46€55+00-{ FuelOil #6il09e{0000 Motor OilJo01 00000 Avialion Fuel

Unidentified

Ohe(Oit

Total Pe&oleum Hydrocabons

C9.C36 Atiphatic Hydrcc€rbons

Suftqde recovedes:fia63?2 l-Chlotooctdecaie

Semivolatil€ Otgrnlc Compounds by cC

Orqanochlorine Pesticides SW846 8081A

Prepared by method SW846 35508

309{0-2 Aldrin

SW 846 82608 22-Mat41 23'llr''a147 7031335 RLJ

+CTETPH 22-MaF07 26.M€47 7031284 DS

BRLBRLBRL

BRLBRL

8.0BRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARL

99107100101

BRLBRLBRLBRLBRL

BRLgRL

BRLBRLBRL

75

uSi kS drypdks dry

US/kg drypdks dry

ldko drypdkS dry

ldkS drypdks drypdks dry

ldks drypdks dry

lSftS dry

fg/kS dry

!g/kg dry

Pg/kg drypg/kg drypdks dry

US/kg dry

Ug/kg dry

IdkS dry

!S/kS d.y

udks dry

Ug/kg dry

ldks dry

Pdkg drl

7.37.37.37.37.37.3

7.37.37.37.37_37.37.37.37_3

14,6

7.373.17.37.37.37 373_1144

1

1

1

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/0-130%7G1m %/0130 %70-130"a

mdkS dry

mg/kg dry

mg/kg dry

mgL/kg dry

ftg/kg dry

mgL/kg dry

mg/kg dry

.tWkS dty

'rs!ftS dry

'YVks dry

20.620.620.620.620.620.6

2 0 6m.620.620-6

40-t44 %

lgikg dry 7.1O SW6.f68081A 22-MaFO7 27-Ma(O7 7031275 rG

This labo ttory ppod ls not,old *ilhoul an azthorhel si4nrture on the coeer FzEe.+ Reportabte Der€cdon Limir BRl- = Below Repordng Limit Pzse 23 ot 124

Page 196: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sahpl€ [dentificationM8F-15 4{'sA5951745

ClietrtProiect #30t-88

MatrixSoil

Collection DatdTimeI 9-Mar47 00:00

Rec€ived20-Mar{7

CAS No. Adalyte(s) Fhs Anht rRDL Dilution Method Rttr, hepoted Analytd Bozh Ansllrt

Se$rivohtile Orgrrlc Compound! by CC

Oroanochlorine Pesticid€s SW8,+6 808 1 APreparBd by melt|od SW846 3550831$e4s a-BHC319-e'7 b"BHC

31986{ d-BHC

50{se g€HC (Lindan€}

57-74-9 Cfilordane12-544 a,+DDD (p,C)

72-s5a 4.+DDE (p,p,)

5o-2s3 4,+DDT (p,p,)

60-57-1 Dield.in95$9F€ Endosulhn I332116'9 Endoeutfan ll103r{7{ Endoslltan sulfate72-204 Eoddn7421.93-4 Endain Ald€hyde764+A Heptacruor724Y5 MethorycNoi'1024-57-3

H€ptachlof Eporide0001,3$2 Toxapheoe

5ro3-71-9 a-Chlordane4,56fi+7 g-Chtordane

53a9+70{ Endrin Kelone

S/J/rogab reeovedes:1 038Gw-2 1j.D8-M uotpdphenyl (Si

m51-24-3 De@chbrobiphenyl (Sr)

Polvchlorinated Bbhenvls bv SW846 8082

ft@ared by mehod SW846 35508

i267+11-2 PCB 10161110+28-2 PCB 12211i14r-t6-s rcB 1232s316+21-9 PCB 124212872.n4 PCB 1248'110s7-€9-1 PcB 12541109e82-5 PCB 126031:t24'n.s PCB 126211t0+r4-4 rcB 1268

Sfimg /e rccovedes:| 0386.342 4, 4D*Octafl uotobipl6nyl (Sr)

mst-2+j Deca&torobiphenyl (Sr)

Seftivolrtile Org.dc CodrpouEdr by G,CMS

BRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRfBRLBRLBRLARL

36127

BRIBRLBRLBRLBRLBRLBRLBRL

BRL

50

SRLBRLBRLBRL

BRLBRL8Rr-BRL

US4(S d.y 7.1OpdXS dry 7.1O

lsASdry 7.10

ldxgdry 7.1O

UdkS dry 35.5

rgks dry 7.10

rgts d.y 7.10

ldkg dry 7.10

udkodry 7.m

UdkS dry 7.1O

lrgn€ d.y 7.1OpdkS dry 7.1o

ldkS dry 7.1O

Udks &y 7.1o

l|gikg dry 7.10

ldkS dry 7.1O

!s,nq dry 7.r0ydl€ dry 35.5

rdkg dry 7.10

f.fS/tg dry 7.1O

Fdkgdry 7.10

30.150 %w-lf i%

IrSlkS dry 14.2

US/tSd.y 14.2pgrkg dry 14.2

ldkS dry 14.2pS/kS dry 14.2

trgr*gdry 14.2

FSrlgdry 14.2pdksdry 14.2

!S/kS dry 14.2

30.150 %30-1fi%

1

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SW846 80014 n-Maro7 27l',,aFO7 7031275 TG

SW846 8082 2z-lhtof 24-Mat47 7031214 MP

S€rnivolatile Oroanic Comoounds bv SWg46 8220CPrcpar€d by method sw8,t6 35508a3{2-9 Ac€nephthene20&964 Acenaphtrylefle6?-533 Aniline12G12-7 AnthrEcene

1912-243 At€inel0$S3-3 Azob€nze{r€Oiphenyldiezine

9247'5 BerEidine5€513 B€nzo(a)anthrac€ne

SW846 E270C T2-Mat47 21,l'',a147 7frr279 M.BpdxSdry s10

WkS dr, 51O

IdkS dry 510

Igit€d.y 5t0pgutg dry 510

ldkg dry 510

t dkS dry 510

tgkg dJy 510

This l4brelorf repo.t it tut valld toilholt a asrtoriztl siguarc oa thc uvet ptge.

* Reptrtable kectiorr Limit BRL = Below Reporting Limir PaEe 24 of 124

Page 197: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-15 4i'sA595l7-05

Client Proiect #301-88

Collection Date/TimeI9-Mar-07 00:00

MalrixSoil

Received2O-Mar-07

CAS No. Azalj-k(s) Resall Fl"e *RDL DiIt/tiorl Method ReJ Prcparcd Anatrzed Balch Antlysl

Selnlvotalile Organic Compounds by (;CMS

Semivolatile Orqahic Comoounds by SW846 8270CPrepa.ed by method SW846 35508

s0-32{ Benzo (a) pyrene

20ts92 Benzo(b)fluo.anthen€1s1-24 2 Eenzo (g,h.i) perytene

207 08 I Eenzo (k) fluoranthene65{54 Benzoic acid10os15 Benzytalcohol111-91 1 8is(2drloroethoxy)rnethane111.44i Bis(2-chtorce$yt)et1er3963&32-9 Bis(2-chloroisopropyt)ether117-81-7 Bis(2-ehyth€xyt)phthatate101-5s-3 +Brcmophenyl phenyi ethefA54A-7 Butt| benzyt phthatate86-74{ Carbazoles9-5|}7 +chlord3-rn€lhylphenol106-473 +Chlo|oaniline9r.58-7 2-Chloronaphthalene

95-57{ 2-Chlorophenol7005-72-3 4,Chtorophenylphenylether21&01-9 Chrysene

53,70-3 Dibenzo (a,h) anthracen€132{4 9 Dib€nzofuran95-5Gl 1,2-Dichlorobenzene

541-73r 1,3-Dicl.{orobenz€.r€106-46-7 1,4-Dicj{orob€nz€ne91-94.1 3,3'-Dichk'roberErdine12033-2 2,4-Dichloropheool445+2 Diethy,jphthatate

131-11-3 Dirnethytphthalate109,67-9 2,4-Dimethylphenol

w-14-2 O-n+utytphthalate531-52'1 4,6-Dinilrc-2-mehylphenol

51-2&5 2,+Dinitroph6nolr21-14-2 2,+Dinitrctoluene

60e20-2 2,6-Dinit'otolu€n€

117{,{{ Di-n_octylphhatate

206-,4{ Fluoranth€n€

86-7$7 Fluoren€118-7t-1 Hexacfilo/ob€nzene87iA-3 Hexachlorobutadi€n€77471 Hexadllorocyclopentediene

67-72-1 Hexachloroethen€193-39-5 lndeno (1,2,3-cd) pyreneso.12-0 l-Methylnaphthat€n€78-5+1 lsophoronee1-57{ 2-Methylnaphthaleness-48-7 2-Methylphenol

l0&3s-a, 3,4-Methylphenol106-.{4-5gt-2o-x Naphthalene

8a-744 z-Nitroaniline99{$2 }Nitroaniline

SW846 8?70C 22-Mar07 24-Mat47 7031279 M.BBRLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLARLARLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRL

BRL

BRLBRL

ldkSdry s10

tls/ks dry 510gikg dry 510

ldkS dry 510

trSftS dry 510

trgftS dry 510

Udkg dry 510gdkg dry s10

USftS dry 510

US4$ dry 510

UdkS dry 510pgkSdry 51O

UdkS dry 510

UdkS dry 510

tr9'k9 dry 5to

UdkS dry 510

USn(g dry 510

UdkS dry 510

USftS dry 510

USftS dry 510

UgkS dry 510

ugks dry 5r0

USftS dry 510

UdkS dry 510pqkgdty 51o

US/l(q dry 510

US,4<S dry 510

ldkS dry 510

Wn(g dry 510pS/kS dry 510pS,to dry 510

Ug/kS dry 510pg/kg dry 510

UgkS dry 510

!S/kS dry 510

US/kg dry 510

ldkg dry 510

Uglkgdry 510

!S/kS dry 510pdkg dry 510

ldkS diy 510

llg/kg dty 510pg/kg dry 510

ldks dry s10

ldkS dry 510pdkS dry 510pS{(S dry 510

USftS dry 510

lSftS dry 510

!S/kS dry 510

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

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This labontory rcpod is aot valid wirhour za authoized sigtutarc on the cot)er ptge _

+ R€portable Detection Limjt BRL = B€tow Reporting Limit Page25 of 114

Page 198: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SaEple ldentificatiotrM8F-r5 4{'sA5951745

ClieDt Proiecl #301-88

Collection Date/Timet+Mar47 00r00

MatrixSoil

Rec€ived20-Ma.r-07

CAS No- Aialyta(s) Ratuk Flog 'RDL Dilut*trt Method Retr, Prcpred Anzlyed Batch Aazlyst

Semivolrtile Orgroic Compoutrdr by cCMSS€mivolalile Oroanic Comoounds bv SW846 8270CPrepa.ed by method SW846 35508

10rrc1{ 4Nitoaniline

9€-9+3 Nitrob€nzen€

08-75_s 2-Nitrophenol

10G02.7 4-Nitroph€nol

62:1us N-Nitrosodimethytamine

€41+a.7 N-Nitrosodi-n-propylamin€863ts N-Nitrosodiph€nylamine07.06-s Penlacibr@h€nd85-01i Phensnthrene100-9s-2 Ph€hol129{0r' P}rfierlG€Fl B/ddin€12O-e2-1 1,2!-Trichlorobeflrene95-954 2,4.STrichtoroph€nol884&2 2,4dTncfibrophenol

Sufiogale rffivedes:321-604 z+fuotobiphenyl

367.124 2-Ftuprophenol

4165-604 Ni'&enzene4s

416542-2 Phenol4s

1118-514 Telphenyl4l4

1 1&794 Z4,$Taibtomophenol

Toarl M€trb by EPA 6000t000 S€ri€3 M.ttods

'l SV'1848 E27DC 2:n1at47 24{ie E 7 001 279 M.A

t '

1 't '

1 '

1 -t 't '1 '1 "

I gwg46 7471A 26+16-07 27-Mar$ 7031322 YP

1 EPA2OO.l z&tir€r{7 27-lrat-07 7031321 HB

1 ' ,' t "

t "

1 '

1 "

t '

I SW8,r61312 22-iiar-O7 22-itar-07 7031344 8D

I SW8461312/60108 ?3-Mar-07 24+larry 7(B14m LR

1 '

t '

1 '

1 '

I SW8{6131274704 ' 26l,re-07 7031409 YP'l S1rV8.l6 1312180109 ' 24+vlar47 7031408 LR

1 '

I SM2540 G ttod. 23-ldar.07 23-$lerry 7031429 qP

BRLBRLBRLBRLBRLBRLBRI-BRLBRLBRLgRL

BRLBRLARLBR|-

f7

64a4

0.0698

BRL

29.3

t56

0.s61

34.7

841

BRL

Co.npleted

BRL

BRL

o.0418

BRL

0.0t20

BRL

BRL

BRL

9glk9 dry m40

ldks dry 510

t!r'kg dry 510

t gkg dry 2lX0

lrgrkg dry 510

t/dXSdry 5'10

YdkS dry 51o

ldko dry 5lopdfs dry 510p4lqdry 510

UgkS dry 510

ll84€ dry 510peig dry 510pgr(g dry 510

ldkS dry 510

30-t3lt %t5-110 %fi-1$%15-110 %30-130 %tutl0 %

org/kgdry 0-0382

rngftg dry 1.28

mgrkg dry l.9l

rflg/kg dry 0.638

mdko dry 0.319

'rEAg dry 0.638

mg,kSdry 0.357

mgLfl(g dry l-91

N1A

firvl 0.0100

mg/l 0.0150

mgLt 0.0050

rnSI 0.0025

msn 0.0050

msn 0.000,tt)

rrBn 0-0075

mgl 0.0150

%

7439-974 Merdry

Tohl Mctrb by EPA 200 S€rier Metlods

7440-224 glver

71,4G33-2 Als€stic

744n.393 g€dum

74aG4$g Cadmium

7440.47_3 Chrcmium

?43{l-92n Lead

za2-4$2 Selenium

SPLP Metrk by EPA l3l2 & 60001000 S€.ics Mcttods

SPLP Exhac{ion714{1224 Sifu€r

7440-3&2 Arsenic

7440nF BA um744043t9 C€dmiutn

74(X73 Chrornium

7€9.9rc i,l€rcury

7439€2-1 Lead

77&492 Selenium

Cen€rll Chehlslry Pr.rmctets

% SolkJs

Thb kbordary .epod ti ,tot vdid witho'd .a .lthothd sbndnrc on thc cawr pag.

. R@rtable Dcteclioa LirEi! BRL = Berore R€po.tinC Linir Page 26 of 124

Page 199: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentifications{8F-16 2'-4'sA5964l-01

Client Proiect #301 -88

Collection l)alelTime2l-Mar-07 00:00

Mari\Soil

Received22-Mat0l

CAS No. Ahabtz(6) Resu& Fhs *RDL Dilution Method Ref, Prcpared Analt'a,ed Batch Analrsl

Volalile Orgrnic ComtrN)undf

VOC Extraction Field extracled

BRL

!S/kg dry 5.4pg/kg dry 1O7pdkS dry 5.4pdkSdry s.4

r.ig/kg dry 5.4pg/kg dry 5.4

US/kS dry 5.4

lSlkg dry 54

IdkS dry '10 7pg/kg dry 53 6

|JS/kg dry 5.4

VqlkSdry 5.4

|,g/kg dry 5.4pg/kg dry 26I

Ug/kg dry 5.4gdkSdry 5.4pg/l€ dry 1O.7

tdkg dry 5_4

t S/kS dry 10.7

Vqkgdry 5.4

ug/kg dry 5.4pg/kg dry 10 7

Irdkg dry 5.4

llStkSdry 5.4

!S/kg dry 5-4pg/kg dry 5ApS/kS dry 5 4

US/kS dry 51

rrS/kS dry 10 7

ug/kg dry 5.4

udkS dry 5.4

tgtKgdry 5.4

udkS dry 5.4

ldkS dry 5.4pdkg dry 5.4

ldkS dry 5.4

!g/kg dry 5.4pg/kg dry 5.4

lgkS dry 5.4

FdkS dry 5.4pqkS dry 5.4pdrs dry 5.4

ldkg dry 53.6pdks dry 5.4pdkS dry 5.4pCl(g dry 5.4

lCftS dry 53.6

ldkSdry 5:1.6

ldkS dry 5.4

26-t4ar47 26-Mar{7 7031584 ADVolalile Oroanic Comoounds

Pfepared by method SW846 5035A Soit {low levet)76-13'1 1,1,2-Trichtorotrifuoroethane(FreoFRL6764-1 Acetone BRLl07r3j Acrylonitrite BRLt143-2 Benzene BRI-r0a€6,1 Bromobenzene BRL7497-5 Brcmochtoromethane BRL11274 Brcmodichloromethane BRL75-2*2 Bromofo.m ARL7413-S Bromomethane BRL78s13 2-Butanone (MEK) aRL1M,51rt rFButytbenzene BRL13t98{ sec_Buil/tbeflzene BRf984tr tert-Butylbenzene BRL7s 110 Carbon disulfide BRLs6-23s Carbon tefachloride BRLlo0-90-7 Chlorobenzene BRt7540'3 Chtomethane BRL67€+3 Chtorolofih BRL74-47-3 Chloromethan€ BRL954+A 2-Chlorotoluen€ aRL10e434 4chlorotoluene BRLs612.8 1,2-Dibforno.3-c}tloroprop€n€ 8RL124-46-1 Oibromodtloromethane BRLlocai-4 l,2-Dibromoethane (EOB) 8RL74-9+3 Dibromomethane BRL95-50-1 l,2-Dichlorobenzene BRL541-73-1 l,3.oichlorobenzene BRL106-.{6-/ I,rt-Oichlorobenzene BRL15 71-g Dichb.odifluoromethane (Ffeon12)BRL75'x+3 l.1-Dichloroothane BRL10746,2 |,2_Dichloroethane BRL75-35.4 l,l-Dichloroethene SRL1s6'59,2 cis-1,2-Dichloroetl|en€ BRL1s6i05 ftans-'|,2-Dbhbroeth€ne BRL78{7-5 1,2-Dichloropropahe BRL142-26-s 1,3-Dichloropropane BRL594-20,7 2,2.Dichloropropane BRL563-58-6 1 .1 -Oichloropropene BRL10061{1-5cis-1,3-Dichloropropene BRL10m1.025trans-l,3.Dichloropopen€ BRL10041-4 Ethylbenzene BRL87{&3 HexacilQrcbutiadiene BRL5ei-78€ 2-Hexanone (MBK) BRL9a{2-8 lsopropylbenzene BRL99{7€ +lsoproMoluene BRL1634{4-.{ Methyl tert-butyt ether BRL10&10-1 4-Methyl-2.pentanone(M|BK) BRL7549-2 Mettrytene chtodde BRL

SW 846 02608 2A-Mat-O7 2A-Mat-O1 70316S3 RLJ

91-2G3 Naphthalene

Page I of 165

IhLs bbo.alary fepo L\ not valu wtlhou !^ tuho.hed siE airre on the coverpage.

+ Reportable D€t€crion Limrt BRL = B€low Repo(inB Limit

Page 200: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-16 2,-4'sA5964l-01

Client Pmiect #301-88

MarixSoil

Collection Date/Time?t-Mar-07 00:00

Received22-Mat47

CASNo. Anab.z(s) Frag "RDL Dih'tion Method ReJ Prepdrcd AaalyTed Barch Aral'sl

Volatile Orgtnic Compoutrds

Volatile Oroanic ConooundsPropared by method SW846 5035A Soil (to!v tewl)10+66n n-Propylbenzene100-42-5 Styrene630-20{ 1,1,1,2-Tetrachloroethane7&34-5 1,'1,2,2-Telrachtorethane127-184 T€trachloroebene108{43 Toluenea7€1{ l,2,}Trid orob€nzenei?G€2-1 1,2,+Tdchlorob€nzene71-55{ 1,1,1-Tridtlometharle79{G5 1,1.2-Trichloroethan€Z9{1-6 Trichtoroethene

96.i8-4 1.2,3-Tricfiloropropane35435 1,2.+T.jmeftylbenz€ne108474 1,3,s-Trimethy'benzone/s-oi-4 Mnyld oridel33LAn7 m.p"Xylene95-47{ o-Xyl€ne10+99-9 T€hahydrofuran60-29-7 Ethyt ethe.991-{5{ Tert-amyt nethyl €lher637.92-3 Ethyl tert+utyl eth€r10e20-3 Di-isoprcpytether75{$o Tert€utanol/ butyl atcdtol123-91.1 1,4€bxan€

Swmgata rccgreies:460401 +Bronofluorobenzenem37-2dF5 Toluet@4St 706047-0 1, 2-Dichlotuethane4l18686Xt Dibrcnonuoronethane

Ert rcarbl€ Petrole|rm Hydrocorbotr!

Exuaclable Total Petroleum Hvdoca.bonsPrepared by method SW846 35508800e6l-s Gasolinc6e47S30-? Fuet oit #26847e31'3 FuelOit #4€ssalooa Fuel Oll [6M0980m00 Motof oilJ00rm00O Aviation Fu€/

UnidentifiedOthef OilTotal Petrolaum Hydroc€rbonsC9-C36 Aliphelic Hydrocarbons

Su/logale rccovedes:xJ86.3+2 l-Chlot@dadecene

Semlvolrlile OrErhh CompoBtrdi by cCOroanochlorins Pestbides SW846 80814Prepared by method SW846 35rt5A409-00-2 Aldrin

SW 046 82604 2&MEr{7 28{vla.47 7031693 RLJ

75-69-4 Trichloroffuorch€ltEne (Freon t 1) gRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL

8699t r6105

8RLBRLBRLBRLBRLBRL345Calculated as345345

110

pglSdry 5.4

ldkS dry 5 4

ldkgdry 5.4

|,dkg dry 5.4pgftg dry 5.4

lrdks dry 5.4

ldkg dry 5.4

Fgkg d.y 5.4pSikS dry 5.4

Ugrkgdry 5.4

ldkS dry s.4

UgkS dry 5.4

lSikS dry 5.4

udkgdry 5.4pdts dry 5.4

!Sn(g dry 5.4pSlkg d.y 1O.7pSftsdry 5.4

ldkS dry 536

udkg dry 5.4

Udk8d.y 5.4pgkg dry 5.4pEtg dry 5.4

ldlg d.y 53.6

lSrkS dry 107

7G130 %7G130%7G130%70-130 %

mg/kg dry 38.4

mgJt€ d.y 38-4

ft€49 dry 38.4

flE/kS dry 30.4

mSn(S dry 38.4

rElksdfy 39.4

tngikg dry 38.4

nBkg dry 38.4

mdks dry 38.4

firg/kg dry 38.4

40.140 %

+CT ETPH 2S-Ms,47 28 Aar07 7031513 DS

BRL t'dks dry 8.09 SltV$46 80BlA m-Mar47 ?8-Mat47 7031516 TG

This laLotulory rcporr is ,tol rditl withoqt on ottrtoded $gnelrre oa dE cat er poge.

i Repoiable D€{ection Limir BRL = Below Reporting Limit Page 4 of 165

Page 201: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple IdertificationM$F-r6 2i-4'sA5964l{ l

Client Project #30t -88

ColLection Date/Time2l -Mar-07 00:00

MatrixSoil

Received22-Mar-07

CAS No. Anabu(s) Resklt Floq Ani6 *RDL Dilution Method Retr Prepared Anabzed Bakh Atu'rystS€mivolalile Orgrnic Compounds by cC

Oroanochlorine Peslicides SW846 8081APrepaied by method SW846 35454

3J9,84$ a_BHC319€5,7 b-BHC319-86-8 d_BHC58re-9 g.BHC (Lindane)

5T-74-9 Chlordane72-544 4,4!0DD (p,p')

72-5te 4,4!DDE (p,p')

cr-2+3 4,4'-DDT (p,p.)

60-s7-1 Dielddn959,98-8 Endlosulran I33213-6+9 Endosulfan ll1031{7-8 Endosulfan Sulfatef2-2V4 Endrin7421-93-4 Enddn Ndehyde76-44-8 Heptachlor724X-5 l\rethoxychlor1024,57 3 Heptachtof Epoxide8001-15-2 Toxephene5103 71-9 a-Chlordane5,566,34-7 g_Chh|rdane

53494-70-5 Endrin Ketone

Surmgale remvenesl1a3868+2 4,+D8-Octalluorobjphenyt (Sr)2a51-24-3 Decachlorohiphenyl (So

Polvchlorinated Biphenvls bv SW846 8082

Pfepared by melhod SW846 3545A

12674-11-2 PC8 101611104_?8:2 PCB 122111141-16'5 PCB 1232$449,21.9 PCB 124212672-294 PCE 124811097{9-1 PC8 t254110e6{2-5 PCB 126037321.23-5 PCB 12621110C144 PCB 1268

Sufiog4te rccoveries:10i86812 4,4-Dgocta0uo(obiphenyt (Sr)

2051 -2at Decachlorobiphenyl (St)

Semivolatil€ Organic Compolnds by CCMS

BRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLSRLBRL8RLBRLBRLBRLBRLBRLBRLBRL

741 1 1

8RLBRLBRLBRLBRLBRL274BRLBRL

4075

udks dry 6.09pdkS dry 6.09

ugks dry 6_09pdks dry 6-09

ldks dry 30.4

lSftS dry 6-09

ldkS dry 6.0spS{(S dry 6.09

ldks dry 6.09pg/kg dry 6.09pdks dry 6.09

UdkS dry 6.09

!S/Kg dry 6.09

ugKgdry 6.09

ldKs dry 6.09pg/kS dry 6 09ps/kg dry 6.09

ugiKg dry m.4

Ug/kg dry 6.09pStxgdry 6.09pg/kg dry 6.09

30-150 %30-150 %

lrg/kg dry 12.2pg/kq dry 12.2pg/kg dry 12.2pgkg dry 12.2pgI(S dry 12.2pgkgdry 12.2pdkSdry 12.2pS/kS dry 12.2pg/ks dry 12.2

3G150 %3L150 %

sw846 8081A

Sw846 8082 2AMar-07

26-Mar-07 28-Mar-07 7031516 TG1

1

1

1

1

1

1

1

I

1

1

I

1

i

I

I

1

1

1

1

1

7031515 SM

Semivolatile Oroanic Compounds bv SW846 8270CPrepared by method SW846 35508

83.32I Acenaphthenem&96{ Acenaphthylene62-53-3 Anilin€12G12-7 Anlhracene1912.24-9 Atralne10+33n Azobenzene/Diphenyldiaznes2+7-5 Benzidine56-s$3 Benzo (a) antihracene

SW846 8270C 26-MarO7 .l.,,,ar07 7031514 M.BBRLBRLSRLBRLBRLBRLBRLBRL

usfts dry 476usrKs dry 416ugrkg dry 476!S/kS dry 476

!g/kg dry 476

ldks dry 476

!g/kg dry 416

ldkS dry 476

5

5

5

5

5

5

5

5

This laltonrory rcpoft it ,tot tlIU tlrithou ah auho.lzed sig ottte on rte co,er paEe

* Reportabl€ D€{e€tion Lirnir BRL = B€low R€porting Limir Page 5 of 165

Page 202: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiqnM8F-r6 2'-t'sA59641-0r

Client Proiect #301-88

MatrixSoil

Collestion Date/Time2l-Mar-07 00:00

Receiv€d22-Mat47

CAS No. Analy,e(s) Resull FlaC AEia *RDL Dil$i'n Method fr.tr Preparcd Aaalyed Batclt A,sN

S€mivolelil€ Orgstric Compoutrd! by GCMS

Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35508:'0n2{ B€nzo (a) pyrenem+ss-2 B€nzo (b) fluoranth€ne1s1-24-2 Bonzo (g,h,D perylon€al7-o8€ 8€nzo (k) fiuoranthene6fifl BerEoic acid10o-5i6 B€nzyl alcohol111-91n Bis(2-chloroethoxy)fiethane1i1-4.r-4 Bis(2-€filoroethyl)enh€.3s63+32-e Bis(2-chlomisopropyl)sthef117-81-7 Bis(2-€trytheryl)phhatete101-5fi 4-Bromophenyl ph€nyl ether85{&7 Butyibonzylphtttatate86-7+€ Caabazol€59-5G7 4-Chlo.GS.mefrylphenol10€4ru 4-Chtoaoanitine91-5&7 2chloonaphthalene95-57{ 2-Chlorophenoi700+72-3 4-Chlorcphenyl phenyl ether2ltl-{X.g Chrysenef3-7{}3 Dibenzo (a,h) anthiacene132$44 Dibenzofuran95-5I}1 .1,2-Dichlorobenzene

441-73-1 |,3-Dldiorobenze0e106-1e7 1,4-Dict{orobenzene9r-91L1 3,3-Didtlorob€nzidine12G?,3-2 2,+Di{rlorophenol04{G2 Diethylphthalate131-11n Dirn€thyl phthatatetotr-/{ 2.4-Dimethylpheno,lu-7+? Oi-n-buty'phhatate534-s2r {,6-Dinitc2-methyiphenols1.2&5 2,4-Dinilrophenol121-t4-2 2,4-Dinihololu€ne6OCzo.2 2,6-Dinihotoluene117€a-0 Oi-n-octylphdEtats20G44-.0 FluoEnttene8E-73-7 Fluo.eoeli6-7'l.i Hexachlotobonzene87.66-3 Hexoc+tlorobutiadGne1147 4 Hexac.hlorocyclopentadien€67-72-1 Her€doroelhane1913s-5 Indeno (1.2,3d) pyrene9{r.12-0 l-Melhy{naphthal€ne78€Sl lsophorone91-57{ 2-Metfiylnaphhslene96-4e7 2-M€lhy'phenol10F3+4, 3,+Methytphenol106-114-59t,2G3 l,laphtllat€ne

u-74 2-Niuoatnalines,rr$2 +Nitroanitine

Srt/846 8270C 2Glrar{7 28-l.lar{7 7031514 M.ABRLBRLBRL8RL8RLBRLBRLBRLBRLBRIBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBR.LBRLBRLBRL

BRLBRLBRL

!SI(g dry 476pdkS dry 476

Fdhgd.y 47€

lgl(gdry 476

rg,/}gdry 176

UdkS dry 476

ldkS dry 476

FdkS dry 476yqrgd.y 476

lJglqdry 476

!S/kS dry 476

ldksdry 476pS/rS dry 476pdkg dry 176

udkgdry 476pS/kg d.y 476

!S/kS dry 176pg/kS dry 476

ldkS dry 476

Fg/kg dry 476pgkgdry 476

#dkS dry 176

Idr(g dry 476

Fdkg d.y 476

rdksdry 476pdkg dry 476

ldxg dry 476

!g/kg dry 176

tdl(g dry 476pS^S dry 476

udl(g dry 476pdkS dry 476

ldks dry 476

[dl€ dry 476

UdkS dry 476pgl(g dry 476

Udxg dry 476psrksdry 476

lCftg dry 476

Ug/l€dry 476

lrdkS dry 476pdl€dry 476pgJkg dry 476

ldrg dry 476

ldl€ dry 475pgkS dry 476

ldl€dry 476

ugkS dry 4?6

usftSdry 476

ldksdry 176

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

This labrslory rcFEr is nol wld roithornt ad aulLodazd sig obtrc oa tha cawr poAe.

' Reportabl€ Delection Limit BRL = Bclow R€porting Limir Ptge 6 of165

Page 203: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Id€ntificationMEF-t6 2'-4'sA59641-01

Client Proiect #l0l-88

MatrixSoil

Received22-Ma.r07

Collection Date/Time21-Mar-0? 00:00

C"4S No, Anatrte(s) Resull Flag Unirt *RDL Dilution Mefiod netr Prepaftd Aturyze.l Bolch Analfst

Semtiolatile Organic Compornds by CCMS

Semivolatib Oraanic Compounds bv SWO46 8220CPrepared by method SW846 35508

10c01$ 4-Nitroanitine9A-9+3 Nitrobenzene€8-7+5 2-Nitrophenol100-02-7 4-Nitrcphenol

62-75-9 N-Nitrosodimethytamine621{4 7 N-Nitrosodi-n-propylamine86-30-6 l'{-Nihosodiphenylamine87-8es PentachtoropfEnol85{1-8 Ph€nanthrene108-95 2 Ph€nol12900{ Pyrene110{6-1 Pyridine120-821 1,2,4-Tdclilorobenzene95-95.4 2,4,tTnchtorcphenoleg46-2 2,4,6-Tichtorophenol

Suftogale Ecovedes:321-60a 2-Fluorobiphenyt

367-12-4 z-Fluorophenol

11 65404 Nilrobenzene-ds

416s 62 2 Phenot4s

BRLARLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

59474851

Completed

BRL

8RL

0.0577

BRL

0 01s3

BRL

0.0161

BRL

s4.'l

pg/kg dry 1900

rc/kg dry 476pg/kg dry 4f6

trdt(S dry 1900

UdkS dry 476pdkg d.y 476pS/kS dry 476pdks dry 476

ldkS dry 476

ldkS dry 476pdkS dry 476pS/kg d.y 476

IdkS dry 476pdkg dry 476pdkS dry 476

30-130%15-110 %n-t30%15-110 %3G130 %15-110 %

mg/kg dry 0 0309

mg/kg dry 0-976

mgr'tg dry 1,46

nE/kg dry 0 4&]

ntgr'kg dry 0.244

mgL/kg dry 0.488

rhCftg dry 0 732

mgikg dry 1.46

mSI 0.0200

mgfl 0-0150

rngl 0.0150

mSn 0.0025

mg/l 0.0150

mS/ 0.00040

mg/l 0.O15O

mgn 0 0150

%

5

5

5

5

5

5

5

5

5

5

5

5

5

5

1718-51-0 Terphenyl4l4 68118-/9-o 2,4,6-Tibromophenol Ss

Tord Metrls by EPA 6000/7000 s€ries Mfthods

7439 97$ Mercury 0 0707

Totsl M€rals by EPA 200 Scries Methods

7440-224 Sllve(

7,140,3&2 Arsenic

7440-393 Badum

7a40-419 Cadmium

7440-47 3 Chromium

7439-92-1 Leacl

778249-2 Selenium

SPLP Extraction

7440-224 Sitv€r

742t{-3€-2 Arcenic

7440-33-3 Barium

7r|{0-4$9 Cadmium

7lK0-47-3 Chromilm

7439-97-6 Merc!ry

7439-92-1 Lead

77€?-4+2 Selenium

Ceneral Ctemhtry Prrrmete.s

% Solids

1 SW846 74714 2A-Mat47 2A-Ma..07 7031495 YP

EPA 200.7 28-Mar47 28-N{ar-07 7031434 Rl.l|BRL

5 5 9

28.A

0 .615

30.4

49.7

BRL

SPLP M€talr by EPA 13l2 & 6000n000 Series M€thods

t SW8461312 26-tlaF07 26-MaF07 7031560 BD

1 SW&161312/60104 28-Mar-07 28-MaF07 7031651 HB

1 '

1 '

1 '

1 "

1 SW84613141470A ' 28-1,4a{-07 7031652 YP

1 SW846131260108 " 28JI1,a(O7 7031651 HB

1 '

1 SM2540 G Mod. 2+MaA7 24-Mat47 7031470 QP

Thb labomtutry rcport is nol volid *ithou an tuthofi@d signatwe o^ the crver paEe .

+ Reporlable Detection Limit BRL = Below Reporting Limit Page 7 of 165

Page 204: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificariotrMtF-r7 4'{'sA5964l-02

Client Proiect #301-8E

t{ahixSoil

Received2?-Mar47

Collection Datey'Time21-Mar4? 00:00

CAS No. Analflc(s) Resaa FIog *R.DL Duadon Melhod Ref, Prepatul Ansbaed Bdch Aialtsl

Vohdle Otgaet Compo|rndr

vOC Efiraclion Fiold exfacted

2ffi

ydks dry 69.2

lgrsdry t380

ugts dry 69.2

ldks dry 69.2

lgfts dry 69.2pdks dry 69.2

ldks dry 69.2

t4fts dry 69.2pgr(g dry 138

!g/kg dry 6S2

lgAS dry 69-2

UgkS dry 69-2

lSftg dry 69.2

t gl€ dry 346

Ugikg d.y 63.2

uSAgdry 6s.2pqkg dry 138pdkg dry 69.2pdks dry 138

IdkS dry 69.2

[r9lk0 dry 69.2pgkS dry 138

!S/kS dry 63.2

FS/tg d.y 63.2pykg dry 63.2pdks dry 69.2

rS/kS dry 69.2

IdkS dry 692pdko dry 13S

t'dko dry 69.2

IdkS dry 6S.2

US/kS dry &.2pCI(g dry 69.2

!g/kS dry 69.2

ldkS dry 69.2

ugts dry 69.2

lg'l(S dry 69.2

trgkg dry 69.2

Ugf(o dry 69.2

IS/r9 dry 69.2

udkg dry 69.2

udkg dry 69.2

!g/tS dry 692pgkS dry 69_2

uSn€ dry 69,2

t'dkg dry 69.2

ldkS dry 692

!S/kS d.y 692

rdksdry 69.2

26-Mer47 26 lar47 7481584 BDVolatile Oroanic ComDounds Ro5Prepared by mothod SW846 5030 Soit (high levet)76.1!1 1,'1,z-Tridtlorotriiuoroethane(FreoBRL4744.1 Acetoos BRL107.1}1 Adlbnitile BRL7113.2 BerEsrl€ BRL1&s-86-1 BronrbefEene BRL71.97-5 Broanod o{omethane BRL75-2?1 Ekornodichioromethane BRL75-212 Brornoform BRLzt++g Brornomethane BRLm.e3-3 2-Butanone (MEK) BRLro4-s1€ n-Butylbenzene BRL13598€ s6c€utylberEene BRLs{s6 ted-Butytbenzene gRL

75-1t0 Ca6on di6ulfide BRL56-2+5 Cafuoli lefachloride BRL10+90-7 Chloaob€nzffe BRL75{)G3 C,hlqoothane 8RL675G3 Chto.ofiorm BRL71{,7-X Chloromethffe BRLe5-49{ 24htoototuene BRL1rl&43-4 zl_Chtorotoluene BRLge12-€ t,2-DibromoS-{tttorcpropane BRL12+44-l Oibrcmodrloromehane BRL10c93-{ l.2-Dibomoethane(EDB) BRL7,r,9+3 Dibrodtomethane BRL95-5Gl 1,2-Dichlorobenzen€ BRL541-73-1 l,SDichlorobenzene BRLi0e'4f!7 l,+Dichlorcbenzene SRL75-714 Dichlcrodifuoromethane(F|Bonl2)BRL7t34-3 .1.1-Dichloroetfiane BRL107{6-2 l,2-Did oroethane BRL?t35rt ,1,1-Dldrloro6thene BRLr5&E€,2 cis-1.2-Oichlo.o€lhene BRL15,€io'5 t?ns-1,2oid{oroedrcn€ BRL78{7.5 1,2-Oichto.opropane BRLi42-2S9 .l,9Dichloropror,ane BRLs9+2{r7 2,2-Dictttorcplopane BRL5,6958{ 1.1-Dichlo{bpropene ARL100€t{1-5 cigl,3-Dlchlomprop€ne BRL10061{2{ tans.1,3-Dlchtoloplopene BRL10G414 Ethyb€nzene BRL87'6&3 Hexad orcbutadiene BRL591-78{ 2.Hexeion€ (MBK) BRL9€{2{ lsopropytb€nzoie BRL99{76 +lsorropyttotuene BRL1634{44 Mediy|led-bubd ether BRt_108-10.1 +Mehy'-2-penbnone(M|BK) BRL7s"{re-2 l|€tlrylen€ d odde BRI_

50

50505050

50

505050

50505050505050

50505050505050505050

50505050505050

50

5050505050

SWE|6Em0B 27^ er47 2A-$i*47 7031642 mar

s1-2e3 Naphthalene

Page E of 155

Thit labo4tory rqod b not v4lu wiahoa an aulhorizptr ig at*re on thz cor'.r page.

. Reportable Dst€ction Limit BRL = Betow R€porting Limit

Page 205: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samnle ldentificationM8F-17 4'-6'sA5964l-02

Client Proiect #301 -88

Collectioo Datc/Time2l-Mar{7 00:00

MatrixSoil

Rcceivcd22-Mar-0'7

CAS No- /tnaltte(s) Flog Uni6 +RDL Dil,'tioh Method ReJ Prcpared Analrzed Batth /lnalFt

Voladle Organic Compounds

Volalile Orqanic ComooundsPrepared by method SW846 5030 Soit (high tevet)1016t1 n-Pmpytbenzene 8RL100-42-5 Styrene BRL63G20$ |,1.1,2-Tekachloroelhane BRL79-34-5 1,1,2,2-Tekachloroethane BRL127 10-4 Tetrachloroethene 8RL108.84-3 Toluene BRL87$1€ 1,2,3-Trichtorobenzene BRL120-82-1 1,2,4-Trichlorobenzene BRL71{t6 1, |,1-Trichloroethane BRL79rlG5 1,1,2-Trichlorcethane BRL7941{ Trichloroethene BRL75$9-4 Trichloronuoromethan€ (Freon 1t) BRL96-18-4 l,2,lTrichloropropane BRL95{3{ 1,2,4-TrjmethylbenzerE BRL108-67€ 1,3,5_Tdmethylbenzene BRL75-01! Vinytchtoride133c20-7 m.p-Xytene95-47-6 o-Xylene109-99-9 Tetahydrofuren60-297 Ethylether994-05{ Ted-amylmethylether6!7-s2-3 Ehy' teft-butyl ether108-20-3 Di-isopropylether75$S0 Tert-Butanol/ butyl alcohol123-91-1 1,4-Dioxane

Surogale rccorqries:460-00-l +E|rcrnolluorobenzene

20i/-26-5 foluene-dg

1 7 06U07 -0 1, 2-Dichl orcethane-d4

1868-s3-7 Dibromofl uorcmelhane

Extractrble Petroleum Hydrocrrbons

Extractiable Total Petroleum Hvdrocarbons

Prepared by mothod SW846 35508

8006{1-S Gasolane6847430-2 FuelOil#268476 3i .3 Fu€tOi l#46Ass3f004 Fuej oil j6

M0980qlo0 Molo( oilJ0010{DC|0 Aviation Fuel

Unidentified

Other Oil

Total Petroleum Hydrocarbons

C9436 Afi phatic Hydrocarbons

Surogate recoyer'esj33aG33-2 7-Chlorooclaalecane

Semivolrlile Org'ric Compourds by CC

Oroanochlorine Pesticides SW846 8081APr€pa.6d by method sw846 3545A

309{{).2 Alddn

BRLBRLBRLBRLARLBRLBRL8RLBRLBRL

10410810199

BRLBRLBRLBRLBRLBRL8,5'10Calc!lated as8,5108,5r0

ugkS dry 69.2

lgkg dry 69.2

!S/kS dry 69.2pdkg ury 69.2

!g/kg dry 69.2

ldks dry 69 2

!S/kS dry 69.2

lsftg dry 69.2

UStkS dry 69.2

PS&S dry 69.2pSrkS dry 69.2pgkS dry 69.2

lgkS d.y 69-2

!Sn<g dry 69.2

ISAS dry 692

lSftS dry 6S.2

lSn€ dry 138

lSftS dry 69.2

ldkS dry 692

ISAS dry 69.2

!g/kS dry 69 2

lgftS dry 69.2

lSit(S dry 69.2

!S/kg dry 692pdks dry 1380

70-130%70im %70-tm%70-tm %

rq/kg dry 195

"r1€/kS dry 195

mS/kg dry '195

nr€Jkq dry 195mg/kg dry 195mg/kg dry 195mg/kg dry 195mg/kg dry 195mgftgdry 195nglkS&y 195

40-140 %

5050

5050

5050505050505050505050505050505050505050

5

5

5

5

5

5

5

5

5

5

SW 846 82608 27'Mat41 2g]vtadf 7031&2 n'al

+cT ETPH 26-[Iar-07 28-rrar-07 7031513 oS

ldkS dry 6.75 SW8468081A 2&Mer-07 28-[4rr{7 7031516 TG

Thb laborclory rcpod is nat vslid x,itholl an atdtod.ed signdture oB the cowr page .

* Reportable Det€.tion Lirnit BRL = Below R€porrinC Limit Pas€ 9 of 165

Page 206: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldendficationM8F-17,1'16'

sA59641{2

ClientProiect #301-EE

MakixSoil

Collection Date/Iime2t-Mar47 00:00

Received22-Mat47

CAS No. ,lnaltu(s) R.st U nag Urrits *RDL Diludon Llethod ReJ, Pepared Analwd Bdt h Aralfst

Semivohtile Orgrtrlc Compounds by (rc

Orqanochbrin€ Pesticides SW846 8081APrepar€d by method SW846 3545A

3t+8a{ a-BHC319{5-7 b-BHC319-€6€ d-8HCsa{se g-BHC (Lir$ane)57-744 Chlordane12-544 4,,|'-ODD(p,p'I72{rs 4,4'-DOE (p,p,)s!?Fs 4.41DDT (p,C)€057-1 Dleldrin95+9&€ End,osuijan I321165-s Erdosulfian tlt03147+ Endosulian Sutfate72-20{ Enddn7421{3-4 Endrin Aldehyde76-1-{-8 Heptadtlor72.1.3.5 MefFxychlor1024-57.3 l-bptachlor Epoide8001-3+2 Toxaphene5103.71-9 a-Otlordane5s6€-34-7 g-Ch{ordane53a94-70-5 Endrin Ketone

Sunogat€ rsror€rt6s--10386 8+2 4,4 -Dgoclenuo.obiphenyl (Sr)2+51-2+i DscachlorcNphenyl (So

Polvcnbnnated Biofisnvls W SW846 8082Prepared by method SW846 3545412674.11-2 PCB 10161r1(X-28-2 PCB 1221r1141-16,s PCB t2325315+2r-9 PC8124212672-29{ PC8 1248r1097{Fl PCB t25411096825 PCB 126037324-23.3 PCg 1m2i110cr4-4 PCB t268

Sunogal€ r€corror,esr1o?aEaa2 4,+DB&Equorobiphenyt (Sr)m51-243 Oacadlorohiphenyl (Sr)

Se mlvol.ailc Orgni€ Compound3 by GCMS

BRLBRLBRL

BRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRL

6853

BRLBRLBRLBRLBRLBRL21.6BRLBRL

50

BRL

BRI-BRLBRL8RLBRLBRL988

udxg dry

Pqxg dryIS/kS dry

ldkg dry

US/kS dry

Lrgil€ dry

PSXS d.ypgrq dry

USlkS dry 6.75

l|gl€ dry 6.75

tl{r'es dry 6.75

lCftS dry 8.75pdks d.y 33.8

udkSdry 6.75

rcn(S dry 6.75

ldrq dry 6.75

rrdkS dry 6.75

FSftSdry 6.75p$fts dry 6.75pdks dry 6.75

udks dry 6.75

t'dksdty 6.75

lSn€ dry 6 75

UCI(g dry 6.75

lgrS dry 6.75pdkg dry 33.8

!gl(S dry 6.75

Ugn€drt 6-?5pdrS dry 6.75

30-150 %301fr%

pS/kS dry 13.5pdkS dry 13.5

UCftS dry 13.5pdks d.y 13.5

ISAS dry 13.5

ldksdry 13.5

lgAs dry 13.5pdkg dry l3-5pdkg dry 13.5

so-150 %30-150 %

SW846 00814 26-Mar.O7 28{t4ar{7 7031516 TG

SW846 E082 26-Mat4? 2A-tAs47 7031515 SM

Semivolatile O.oanic Comoounds bv SW84ti 8270CPfeps(ed by me$\od SW846 35508[3.32-9 Acanaphthene20&9ffi Acenaphthylene62€+3 Anillno12G12-7 Anthracene1912-24€ Ab€zine'103333 Azob€nzen€y'Diphenyldiatne9247-5 BerEidines6,5t3 Benzo (a) anthracene

SW846 8?70C 2dMat47 ?34tat47 7031514 M.S444

444

444

444

444

444

.r04484

555555

fh6 |4ra'',loty .fjp*t b,tttral tx'ith'n tt,.tthoriid signature oDdte covctt age.

. Reportrble Derectio Limit BRL = Below Repo.ting Limit Page l0 of 165

Page 207: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdeptificationM8F-l? 4'-61sA5964l-02

CLient Proiect #301 -88

MatrixSoil

Collection Date/Time2l-Mar-07 00:00

Received2?-Mar-07

CAS No, Analy.e(s) Flo9 *RDL Dilution Method Retr Prcparcd AnalJzed Bdch Analtsl

S€mivolNtil€ Organlc Compounds by GCMS

Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35508

fo,32,B Benzo (a) pyrene

205,99,2 Benzo (b) nuoranthene191_24 2 Benzo (g,h,a) perylene207-08 9 Benzo (k) iuoranthene65J5{ Benzoic acid100'51$ Benzylalcohol111-91-1 Bis(2-chloroethoxy)methane111444 Bis(2-chloroehyl)etEr3e63e-32-9 Bis(2-chloroisopropyt)etherr17-81-7 Bis(2.edtythexyt)phthatate101'553 4-Bromophenytphenylether

8564-7 Butylbenzytphthatate86-74-6 C€rbazole59-507 4-Chtoro-3-methytphenolr0s47-8 4-Chtoroaniline91-58-7 2-Chtoronaphthatene95-57-8 2-Chlorcphenol7005-72-3 +Chlorophenylphenylether218-01-9 Chrysen€53-7G3 Dibenzo (a,h) anthrEcene132$a-9 Dibenzofurans5-50'l 1,2-Oichlorobenzene541,73-1 1,3-Dichtorcbenzene106!6'7 1.4-Dichlorobenzene91-94.1 3,3--Dichlorobenzidane120€3-2 2, -Dichlorcphenol

M{6-2 Diethytphthalale131-11n Dimethylphthalate10S7-9 2,4-Dim€thytphenolu-74-2 Oi-n-butylphthalate534-52-1 4,6-Dinitro-2-methytphenols1-28-5 2,4-Dinikoph6nol12rr,{-2 2,4-Dinitrotolueneffi-21}Z 2,6-Dinikotoluene117{4.0 Din-odylphthalat€2064-44 Fluoraothene8&717 Fluorene118-74-1 Hexachlorobenz€n€87$8,3 Hexachlorobutadi€nef7471 Hexachlorocycjopeniadiene6?.72-1 Hexactlloroethane19139,5 Indeno (1,2,3-cd) pyrene

90.12,0 1-Meth!4naphhalen€7a-59-1 lsophorone91-57-6 2-Methylnaphthalene95-48-7 2-Methylphenol

106-39a, 3,4-Melhylphenol106-114{91-2G3 Naphlttalene8a-74-4 2-Nilrcaniline99{+2 }Nitroenitine

BRL1, r40BRL930BRLBRL

BRLBRLBRLBRLBRL

8RLBRLBRLBRLBRLBRLBRL1,370BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL2,990BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARL

BRLBRLARL

!S/kS dry 444

!S/kS dry 484

pg/kg dry 484

f.ig/kg dry 444

Ugftg dry 444

pS/kS dry 444

!S/kS dry 4U

pS/kS dry 44

UdkS dry 4U

pS4g dry 484

!S,4(S dry 484

!g/kg dry 4M

!g/kg dry 484

US/kg dry 484

lgkgdry 444

!g/kg dry 4a4

!S/kS dry 4a4

ldkgdry 4A4

UdkS dry 484

pSftS dry 484

!S/kS dry 444

!Si4<S dry 4M

l.islkg dry 484

Lig/kg dry 4A4

Ug/kg dLt84

udkg dry 441

US/kS dry 4a4

!g/kg dry 444

pdkS dry {44

pg/kg dry 444

!g/kg dry 444

!g/kg dry 4U

!S/kS dry 484

USn(S dry 444

ugkgdry 4upS4$ dry 4A4pgkgdry 444ps/ks dry 484

LrgftS dry 4a4

!g/kg dry 144

!g/kS dry 444

!S/kS dry 4A4

ugkg dry 4E4

Ug/kg dry 4a4pS/kS dry 484pdkS dry 444

!g/kg dry 4a4

US/kS dry 4€4

Ug/kg dry 444

IdkS d.y 444

sw846 8270C5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

26-Mat47 28-Mat41 7031514 M.B

This labomta,! repo.t it noa whd wiahoat an atthodze.l signahne on the catter paEc .

* Reportable Det€ction Limit BRL = B€low ReportinB Lidit Page l l of165

Page 208: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple ld€ntificationMtF-t7 4'-6'

sA5964l {2

Client Proiect #301-88

MatrixSoil

Collectioo Date/Tim€2 I -Mar{7 00:00

Bessivcd22-Mar-07

CAS N^ Anallte(s) Resuk Flog Anib 'RDL Dilatia,r Method nel. Prepored Aaalyzed BdEh AMDst

Semivolstile Orgrnic Compo{nds by CCMS

Semivolatile Oroanic Comoounds bv SW848 8270C

Pr€pa.ed by method SW846 35508

ioo{i€ 4-Nito6nilin€94.95-3 Nihob€nzene€t-7t5 2-Nrtr@henol10Go2-7 +Nitlphenol62-7ts N-Nitdsodimelhylaminem1€4-7 N-Nilio6odi-n-prcpylamine463{!6 N-Nihrsodiphenyhminea7ls5 p€ntacfilorophenol

45.01{ Phenanthr€ne1089$2 Phenoli29{0{, Pyrene

ll0+1 Pyridine1m{z-l |,2,4-Trichlorcb€nzene9Cs+4 2,4,STdchloroph€nole0-0F2 2,4,GTrichlorophenol

Sunogale.ecowdes:321e-a 2-Fluorobiphenyl

?k7-124 z-Fluorophenol

1165-604 Ni'/obenzena45

116162-2 Phenol45

17 18.s1 4 Terphenyl-dl4

11e79-6 l4,6.Tribtodtophenol

Totn Med3 by EPA 60Oy7000 S€ri6 Mea$odt

BRL8RL8RL8RLBRIBRLBRLBRLBRLBRL3.020BRLBRLBRLBRL

6150705168

0 -135

BRL

6.41

46.I

0.569

38.4

7S.8

BRL

WkE dty 1940

Idl(S dry 484

Ugrsdry 444pgrs dry 1940

Ugn(g dry &4

udks dry M

US/kS dry 84

lSftS dry 4€4pdksdry 4a1pdksdry 444

!S/kS dry 464pdkS dry 444pdkg dry &4

ldkS dry &

!S/kS dry 454

30'130 %15.110 %30-130 %1*110%30-130 %15'110%

mg/kg dry 0.0318

ms/kg dry 1.17

mg/kg dry 1.76

mgikgdry 0.586

nE/kg dry 0.293

mgl(g dry 0.586

ttE/kg dry 0.880

m€it(g dry 1.76

N/A

msn 0.0200

lngn 0.0150

mgl 0.0150

n€n 0-0025

nEI 0.0150

nrg/I 0.00040

mdl 0.0150

mSl 0.0150

%

55

55

1 EPA 200_7

1 "

t '

1 "

1 '

28-lvla.-07 28.{!lar{7 7031494

28-l ar{7 7031652

2&Mar47 7031651

SW846 8270C 26.Ma.{7 2&Marfi 7031514 M.B

7439,97{ M€mrry

Toirl M€{rb by EPA 200 S€rtei Methods

?44G224 Silver

7440.3&2 Arsenic

71.1+393 Barium

7t4o-4s9 Cadmium

7440-47-3 Chromium

74i19€2r Lead

7782-4+2 Selenium

SWE46 7471A 26:Mat47 2a].',E,t47 7031495 YP

RM

SPLP Merrb by EPA l3l2 & 600{y7000 serl€s Methodr

SPIP Extra€tbn CorFleled

744$?24 Silvor BRL

Z.()'3sz Anenic BRL

7440393 Badum 0.0440

71-104+9 Cbdmium BRL

74rlo4?-3 Ctrornium BRL

743ss?{ llercury BRL

7439€2-1 Lead 00298

282-19-2 S€tiEnium BRL

CeDedl Chdnistry Prrrm€terg

% Solids 84.0

1 SW84A 1312 28{rer47 26-l €r{7 70315G0

1 SW8461312/60109 2&Mar-07 2&Mar-07 7m1651

1 '

1 "

BD

HB

t '

I s!v8,t6 1312?470A

I SW8,r{i 1312/60't0B '

1 ' ,

HB

1 SM2540 G ifod. 24.lulat47 24.Mar-O7 7m1470 OP

Thit laborurory Epott ls ,tot tdid without an rzlhorizd sigt BtE ott the coeet pqgz.

+ R@ortable D€tection Limit BRL = Below Rcptrting Limit Page 12 of 165

Page 209: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-18 2'-4'sA5964l-03

Clieot Proiect #J0l-88

Collection Date/Time2l-Maro7 00:00

MahixSoil

Received22-Mar07

CAS No, An tk(s) Resul( FbE 0nits *RDL lllethod ReJ Prepued Aubzzd Batch Antllst

Prepared by m€thod SW846 5O35A Soit (low levet)

76-13.1 1 ,1 ,2_Tichlorotrifl uoroethane (FreotBRL67s-1 Acelone BRL107-13-1 Acrylonitrile BRL714+2 Benzene BRL108-86r Brornobenzene BRL74-97-s Erornochloronrethane BRL75-274 Eromodidtloromethane BRL75-2+2 Erofirofom BRL74{3-9 Bromomethane BRL78-e3-3 2-Butanone (MEK) BRL104-sl-E n-Butylbenzene BRf13+98-8 sec-Butylbenzene BRL98{6{ tert,Butylbenzene BRt7115+ Ca.bondisullide 8Rt56-23-5 Carbon tetrachloride BRL10€-90-7 Chto(obenzene BRL75'00-3 Chloroethane BRL67sc3 Chlorofotrn ARL

14413 Chlorohethane BRL9s-4+8 2-Chlorotoluene BRL106 43-4 4-Chlorotoluene BRL96-12-8 1,2-Dibroryro-3-chtoroprop6ne 8RL124{8-1 Dibromochloromethane BRL10+e3-4 l,2,Dibromoethane(EDB) BRL74-9$3 Dibromomethane BRt

95-5c1 1,2-Dichtorobenzene BRL

541-73-1 1 ,3-Dichtorobenzene BRL106-46-7 1 ,4-Dichtofobenzene BRL71714 Dichtorcdinuoromethane(Freonl2)BRL

75 3+3 l,l-Oichtoroethane ERL

107 06-2 1 ,2-Dichloroethane BRL

75-35-4 1,1-Dicl{oro€th€ne BRL156,59-2 cis-1 ,2-Oichtoroeth€ne BRL15&60-5 trans-1,2-Dichtoro€thene BRL78{7'5 1,2-Dichlo@propane BRL

Volatile Orgrnlc Compounds

VOC ExtractionVolatile Oroanic Compounds

142-28-9 1,3-Dichlorop.opane

59420-7 2,2-Dichloropropane563-58S 1,1-Dichtoroprop€ne10(161-015 cis-1,3-Oichtoropropole1006142€ trans-1,3-Dichloropropene100a14 Ethylbenzenea7{8-3 Hexachloaobutiadiene591 786 2-Hexanone (MBK)

98{2-8 lsopropylbenzene9s{7{ 4-lsopropyltoluene

pS/kS dry 5.7

liSI(S dry 115

lig/kg dry 5.1

!g/kg dry 5.7

!g/kg dry 5.7

!g/kg dry 5.7

!g/kg dry 5.1pg/kg dry 5.7

!g/kg dry 1'1 5

!g/(g dry 51.4

!9/rg dry 5.7jJdkS dry 5.7

uS/kg dry 5.7pdksdry 28.7pdkS dry 5.7

ldks dry 5.7

UdkS dry 11.5

fS/kS dry 5-7

ldkS dry 11.s

Lig/kg dry 57

!S/kS dry 5.7pS/lAdry | 1.5pg/kS dry 5.7

lS/ftS dry 57

!S/kS dry 5.1pg/kg dry 5.7pg/kg dry 5.7

!g/kg dry 5.7

!g/kg dry 11,5pglkg dty 5.7

uS/kS dry 5.7pg/kg dry 5.7pgkS dry 5.7

FdkS dry 5.7pdkS dry s.7

uS4qdry 5.7

lqks dry 5.7

!S^S dry 5.7

ldks dry 5.7

ldts dry 5.7

tg/kg dry 57pdkS dry 5.7pS/kS dry 57.4pS/kS dry 3.7

udks dry 5.7

tSikSdrll 5.7

rd|(g dry s7.4

USn€ dry 57.4

ldkS dry 5-7

26-Ma(41 26-^/lat47 7031584 BD

27-MarO7 27-Mat-O7 7031658 RLJ

Field extr€cted voc

sw 846 82608

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

i63a+a-a ,lethyl (ert-butty' eoher 8RL108-10-1 4-Methyl-2-pentanone(M|BK) BRL75{9-2 Methylene cfilodde BRL

BRL91.2G3 Naphttlalene

Page 13 of 165

Thb labotuory repod k not volu withott! a aathorized siEnztarc o, tAe mvet page

' R€portabl€ DEtection Limit BRL = B€low R€porting Limit

Page 210: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-18 2,-4'sA5964l-03

Clietrt Proiect #301.86

MatdxSoiL

Collectiotr Date/Time2l-Mar47 00:00

Received22-MEr-07

CAS N^ AaLlrrz(t) R€sllt Fl"E Ania *ftDL Dilutbtl Method neL Prcparcd Analfzet Ba/fh Atrztrsl

Vohtil€ Orgenlc Comporod3

Volatile Orcanic C,ompoundsPrepared by rnelhod SW846 5035A Soit (bw tevel)

75{!Fr T.ichloroffuomrn€tnsne (Freon 1l) BRL

'03{5-1 n_Propylbenz€nel0H2-5 Sorene631)-20-6 t, t t 1,2-Tetrachtoroethane79.345 |,1 .2,2-Tetracl oroethano127n8.4 TetEchloaoeth€ne10&€61'3 TOlUene87616 1,2,+Tridtlorob€nzenerana2n 1,2,4-Tfjdllo.ob€nzene7l-5s |,'l,l-Trichloro€thsne79{D5'1,1.2-Tridrkro€thane?9{1{ Tii,cf oroethens

96-18-4 1,2,+Trichloaopropane95{3€ 1,2,4-Trimethylb€nzene108-67{ l,3,tTdmethylbenzene?5{14 Vinyl cfitoridel$0-m'7 m,p-Xylene95tr74 o-Xylen€10$99-9 TetahtdrofuEn@-2s7 Ethyl eherS4o5{ Tert-amy' m€(.ryl ed1ea637-92-! Edly4 tert-buryl edrert0&2o-3 Dii6opropy'ledEr754S0 l€rt-Butdnol / bultt alcohol12191-1 1,+Dio)@ne

S./t/ogale rccov€nbs,'460{0!1 4.8zomofluorcbenzene

2037-2&5 TohEna4S

lvlaat 474 1,2-Dichloroethane<!4

1 86e-53-t Dibanofl uoro,?ethane

Ertrrc{rble P€i.oleum Hydro$dons

Extradable Total Pelroleum FtudrocarbonsPrepared by m€thod SW846 355088006€r€ crasolhe6847s3G? Fu€t Oil #26&f+31n Fu€l Oil ,r408553{0-4 Fuel Oit f6iao9€000m i/iotof oilJ001m0oo Avialbn Fuel

Unid6nlifiedOtt|e OilTotal Pef olsurh HydaocadonsC+C36 Aliphalic Hydroerbons

Srrnsgl3lo recovbrbs:Atge3l2 | -Ctionodadecane

S€mivol.tile (kgrtrL Comportr& by CCOrqanocfilorine Pegticides SW846 808,1APr€pa.ed by method SW846 35,{5A309{x,-2 Aldrin

BRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRL

BRLBRtBRLBRLBRLBRLBRLBRLBRLBRLgRL

BRLBRL

95

9299

BRLBRLBRLBRLBRLBRL287Calculat€d as247

62

US/l€ drypdkg drypS^g d.y

ugl(g drypdks dry

$Snq diy

|ls/(g dry

udkS dry

uSfig dry

ldxS dry

lSrkg dry

rdkg dry

!Si*g drypgts dry

Udkg dry

ldks drypgag dry

lqxg dry

PdxS dry

ldkg dtypgkS d.y

t Sikg dry

Ugl(g dry

ldlS dry

udks dry

5.7

5.7

5.7

5.7

5.7

5.7

5_7

5.7

5.7

5.7

5.7

5_7

5.7

5_7

5_7

1 1 . 5

57,1

5 7

5.7

57.4

1 1 5

1

1

1

I

I

1

1

1

I

1

1

t

I

I

1

1

I

I

11I

I

1

1

SW 8,$ 82604 27-Mar47 27d.tac-07 7001658 RU

+CTETPH 2a^4sr-07 28-A,lar-07 7031513 DS

7G130%

7G130%

70.130 %

70-1fi %

ntg/kg dry 130r€r'I€ dry 130mg/t(gdry 130ftEftg dry 130mg/kgdry 130mdkS dry 130nrgL/kg dfy 130hgilqdry r30ftE/tg dry 130rvkg dry 13O

4G140%

55

5

5555

}|d@ dry SW846 801llA 26+,lar{7 :E-Mer{7 7031516 TG

Thi6 le&*aory rqod is not wlid pi&rou att or.droriEd signeatre on ttE cow! page.

* Reportabl. D€t€ction Lidir BRL= Below R€portiry Limit Page 14 of 165

Page 211: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-I8 2'-4isA5964l-01

Client Proiect #301-88

Collection Date/Time2l-Mar-07 00:00

MatrixSoil

Received22-Mar-0'7

C,'IS No, Analyte(s) Result FloS UniE t{e.hod ReL Prcpa.ed Atu|ted Balch Analyst

S€mivolrtil€ Orgrnic Compounds by cC

Oroanochlorine Pesticides SW846 808'tA

Prepared by method SW846 35454

31+845 a-BHC31s-8r7 b-8HC319-€6{ d-8HC58{$9 g-BHC (Lindane)

57-749 Chlordane72-544 4,4,-DDD (p,p')725ts a,4'-DDE (p,p )5G2e3 4,4,-DDT (p,p')

60-57-1 Dieldrin95s98-S Endosulfan I3321a65-9 Endosulfan ll1031{74 Endosulfan Sulfaten-2o4 Endrin7421-934 EndrinAldehyde1644 A Heptachlor7243-5 tvethorychlor1024-57-3 Heptadllof Epoxide8001-35'2 Toxaph€ne5103-71-9 +Chlorclane5s66-34,7 g"Chlodane

5349+70-s Endrin Ketone

Swrcsate rccov€nes:18ae,8+2 4,4-DB-OclafluotobiphEnyl (Sf)

2ost -z+3 DecachltJrobipheny4 (54

Polvchlorinated Biphenvls bv SW846 8082

Prepared by method SW846 35454

12674-11-2 PCB 101611104,2+2 PCB 1221111.41-16 5 PCB 12324n469-21-S PCB 1242'12672-29n

PCB 124811097,69-1 PCB 125411(L9$2.5 PCB 126031321-235 PCB 126211100-144 PCB 1268

Sunogale rccoveies10386-u-2 4,4-D8-Oclafluorobiphent4 (54

2051-2a4 Decachlorobhhenyl (Sr)

S€mivolrtile Org{nic Conpounds by CCMS

Semivolatile Omanic Comoounds bv SW846 8270CPrepared by method SW846 35508

€3n2-9 Acenaphthene:0&963 Acenaphthytene62-593 Aniline12G12-7 Anlhracene1912-24-9 Atazin€10+33+ Azobenzene/Diphenyldiazine

9247-5 Benzidinef'G5+3 Benzo (a) enthracene

svr'846 B0€rA

SW846 8082 26-Mat47 2g-Ma(O7 7031515 S[/l

SW846 8270C 26-Mar-07 28-MaF07 7031514 M.a

8RL8RLBRLBRLBRLBRLBRLBRLERLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRL

107

BRLBRLBRLBRLBRLBRL484BRLBRL

5080

BRLBRLBRLBRLBRLBRL

BRLBRL

ldkS dry 6.25

l4/kS dry 6.25

ldkg dry 6.25yg/kS dry 6.25

!g/kg dry 31.3pS/kS dry 6.25pS/kS dry 6.25pg4(S dry 6.25

!g/kg dry 6.25

!g/kg dry 6.25

!g/kg dry 6.25pS/kS dry 6.25

!S/kg dry 6.25

t g/kg dry 6.25pg/kg dry 6.25

uS/kg dry 6 25pdkS dry € 25pS/kS dry 3'1.3pg/kg dry 6.25

!g/kg dry 6.25

!g/kg dry 6.25

30-150 %30-150 %

Ug/kg dry 126

UdrS d.y 12.6pg/fq dry 12.6pdkg dry 12.6

Ug/kg dry 12.6

!S/kg dry 12.6

uS/kg dry 12.6

!g/kg dry 12.6

lgikg dry 12.6

3G150 %30150 0.4

I

1

1

I

1

1

1

1

1

1

1

l

1

I

1

1

1

I

t

1

FqkS dry 4O2

!g/kg dry 4Oz

fg/kS dry 402pS/kS dry 4O2pdkS dry 4n2pg/kg dry 4O2

!S/kS dry 4O2

Fg/kg dry 402

5

5

5

5

5

5

5

5

This labontory feporr h no. vatid withoul zrr snthofized Eigntturc on the eover poge_

' R€portable Detection Limit BRL = Below Reporring Limit Page 15 of 165

Page 212: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificatiooM8F-18 2'-{,sA5964l-03

Client Proiect #30t-88

MatrixSoil

Collection Date/Time21-Mar-07 0O:00

Receiv€d22.M^t4'l

CAS No. Adab'ta(s) Fldg *nDL Dilution Methad Retr Prepued Analwd Ear$ AnaW

ScrEivol il€ O.g.nlc Conpodtrd! by C,CMS

Semivolalile Oroanic Comoounds bv SW846 8270CPrepared by mabod SW846 3550850-32{ Benzo (s) pyrone20+99-2 B€nzo (b) fuoranhene1er.24,2 Benzo (g,h,i) p€rylenem7-l)a-9 Benzo (k) fluoranthene6'AE-O B€nzoic acid1(10-51.6 B€nzylalcotvol1114r-1 Bis{2dllorcefiory)mothanei11-.4-4 Bis(2drtoro€{iyl)ehe.396ire32-e Bis(2-d [email protected])€tf,er1r74i-7 Bis(2-ehythexyl)phthatate1OL5+3 +Buiophenyl phenyt elher85-6&7 BuM b€nzyt phthatateF71l-8 Cabezole5+5G7 +Chloro-3.m€thytphenol106-47€ +Cl{om6niline91.5&7 2-Chtomnaphthalene9s{7,8 2-Chlompt|€nolzx)5-72-3 +Chtoropheny' ph€nyl ether218-01-9 Chrysene53.7G3 Dibenzo(a,h)anthfacene132{4-9 Dib€nzofij.an!,6-5n-1 1,2-Oido.obenzene541-73-1 1.3-Dichtorcbenzene106-4G7'1.+DichloroberEene91€41 3,3'-Ok$lorobenziline120412 2,4-Didloroo€nol84€F2 Diehy,tphthatater31-i1.3 Dmetiytphhalater0tr74 2,4-oimettlytPhef|olU-7+2 Di.n-buMphtElste53+52-1 4,6loinito-2-methytphenol5l-285 2,+Dinitroph€nol12t-14.2 2,4-Oinitrtol!€n€60c2ll2 2,6-Dinihrtolu€ne1r7{4{ Di_fl-octylphhalat€alfl+o Flud.anthene0&717 Fluoa€nei1g7+1 Hex€chbrobonzene87€ll3 tb)(adtlooh,Utadienen4f1 Hexadorocydopentadiene61-72-1 Hoxad o.mthane19&3e.5 trd€no (1.2,3-cd) Pyrcnesr"12{ t_M€thytnaphthal€ne78{!}1 lsoptrorone!)id7{ 2-tlkthytnaphhaten€!r5.{&7 2-MefiylptEnd10&394, 3,4-Mebylphenol10G44-5gl-293 tlaphthaisneu.7+4 2-Nitranitin€s{s2 }.Nitoanlltne

SW84{i 8270C 26-[,lar-O7 2SJvlar{7 7031514 M.BBRLBRL

BRL8RTBRTBRLBRL

BRLBRLBRLBRLBRLBRLSRLSRLBRL

BRTBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLARLBRLBRLBRI-BRL

BRLgRL

BRL

pSftS dry 42pdks dry 402

USftS dry 42pgkSdry 4oz

ldksdry Q2

rc/(S dry 402pSl(S dry Q2

Fg^g dry &2pSlkS d.y 4O2

usfts dry 4o2pdksdry 42pgrs dry Q2

IgtS dry &2

t gftS dry 62

t SI€ dry 4O2

ldkS dry &2pqkS dry 4O2

lrg/kS dry fi2pS/kS dry Q2

lgkS dry &2

rdkSdry &2pdkg dry &2

USftS d.y 42

tdks dry 4O2

!g/kS dry 4O2

!S/kS dry 62

udlls dry &2pdkg dry &2

rcrkS dry &2

Igr(gdry 4O2pdkS dry 4o2

Fdkgdry 1O2

ld}g dry &2

US/kS dry 62

figkS dry &2pdks dry 1O2

ldkg dry 402

lgftgdry 4O2

tdksdry 4o2

ldksdry 4O2

Idkg dry 62

Idkg dry a@.

USikS dry &2

9gkS dry 42

USAS d.y 42pgRg dry N2

Fg/kg dry 4n2

l.'gts dry Q2

ldkS dry 42

@kgdry &2

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

Thir l4botutory .cpod is noa vali.I witiod r ardho.Aed slg,'tatdrc on thz cover page.

i R€portable Dete.tion Limtt BRI = Below Reporting Limit PNge 16 of 165

Page 213: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiorltfttF.l8 2'-4'sAs964r -01

Ctient Proiect #301-88

MatrixSoil 22-Mar-07

Cotlectiolr Date/Time2l-Mar-07 0t):00

CAS No- Anafute(s) Res/llr FIag Unitt ,RDL Diluion Method ReJ Prcparcd Anslyed Eatch A,uryst

Senivotatile Organic Compo'rnds by GCMS

Semivolatile Oraanic Comoounds bv SW846 8270CPfepared by method SW846 35508

100{15 4-Nitroenilihe98-95-3 Njhobenzene

08-75-5 2-Nitrophenol100{2-7 4-Nitrophenol62-1+9 N-Nitrosodimethytamine621€a-7 N-Nit.o6odi-n-propylamine66-30i N-Nilrosodiphenylamine87J6-s Pentachtoroph€hol8541{ Phenanlhrene10&95-2 Phenol12900{ Pyrene11G€6J Pyddine12l}821 1,2,+Trichlotobenzene95-9.F4 2,4,$Trichtorophenol88{6'2 2,4,&Tdchtorophenol

Sunogele recoveies:

32140-8 2-Fluorcbiphenyl

36/124 2-Fluorophenol

5 SW846 8270C 26-Ma'.o7 28-Mat-O7 7031514

5 "

5 "

5 "

5 "

5 "

5 "

5 "

5 "

5 '

5 '

5 '

5 '

5 "

5 "

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

615 1

lgkS dry 1610

!g/kg dry 62pgftS dry &2pS/kS dry 1610pdts dry &2

ldkS dry &2

!S/kS dry 62

ldl(g dry &2pgikS dry &2

!g/kg dry &2

lgftS dry 4O2

ldkS dry 4O2

tig/kS dry 42

!g/kg dry 62

!g/kg dry 4t)2

30-1W %15-110 %30-130 %1Ul10 %30-130 %15-110 %

mgftg dry 0.0319

mg/kg dry 0.936

mgl(g dry 1.4O

mgfl(g dry 0 468

mgkSdry 023/

mS/kS dry 0.468

n€/kg dry O.7O2

mg/kg dry 1.40

M . B

4165404 Nitobenzene-d5 52416542 2 Pheno!4s 521/1*514 Teryhenyl4l4 72t1A-795 2,4,6-Tibromophenol 55

Tot8l Mctrb by EPA 6000/7000 S€ries M€thoos

7439-97{ Mercury

Totrl Met{ls by EPA 200 Serier Methods

7440-22-4 Silver

7440-38-2 Arsenic

7440-393 Badum

7440419 Cadmium

7440{7 3 Chromium

74394h Lead

7182-192 Selenium

1 SW846 7471A 28-Ma''O7 2A-Ma'.Ot 7031495 YP

1 EPA2007 28-Mar07 28-Mar-07 7031494 Rl\,{

1 "

1 '

1 '

1 '

1 '

' t '

'1 SW84G 1312 26-Mar47 26-Mar-07 7031560 AD

1 SW846131260108 2A-Mat47 2g-Utal-OT 7031651 Ha

1 '' t '

1 "

t "

1 SW8461312'470A " 28-Mar.07 7031652 YP

1 SW846131ly60108 " 28-MaF07 7031651 HB

I '

0 0605

BRL

4.53

30.8

0.674

34.3

44.4

BRL

SPLP M€tsls by f,PA 1312 & 6000/7000 S€ries Methods

SPLP Ext action Comdeted

7440-224 s'ilvet BRL

BRL

0.0850

BRL

0.0312

BRL

0.0190

BRL

92,2

mg/l

msr

mgr

msnrYEn

fiur

rngrt

rng/l

%

0.0200

0.0150

0.0150

0 0025

0.0150

0.00040

0.0150

0_0150

7,t40-3&2 Aisenic

74-40-393 Barium

74!{l-13-9 Cadmium

74lo473 Chromiufit

7439-97-6 MercUry

7439-92-1 Lead

tE2-49-2 Selenium

Cenerrl Chemistry P.rrm€t€ri

SM2540 G ltl,ed. 24-Miat47 24Nar'O7 7031170 AP% Solids

Page 17 of 165

Thit laborulory report it ttot tqlid Nllhoa an alihodzed sigmture on lhe drver p.tge

' Reportabl€ Detection Limit BRL = Below Reporting Limit

Page 214: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sanpl€ ldedtificatiodMEF.19 2'-4,sA5964 t-04

Cliert Proiect #301-88

MatrixSoil

Collection Dat€/Time2l-Mar47 00:00

Received22-Mar47

CAS N^ Anolru(s) n"E UniB "RDL Dilntun M.lrad ReI PrcWen ,4nalwd Botch Atsltst

Vol{lil€ Otg.rlc Compoondf

VOC Extraction N'A

ldkS dry 6.6

udkgdry 132

uEksdry 6.6psftgdry 6_6

iJdkgdry 6.6

ugkgdry 6.6

lgr€ dry 6.6

t SikS dry 6.6

UgftS dry 13.2

!dl(gdry 66.0

ugkgdry 6.6

US/kg dry 6.6

US/kS dry 6.6pCftS dry 33.0

sgtkgdry 6.6

Ugv€dty 6.6

ttgilq dry 13.2ydlgd.y 6.6

ldkgdry 13.2

rs/kg dry 6.6pdkgdry 6.6

usirqdry r3.2psngdry 6.6pdxg dry 6.6

!g/kS dry 6.6

IqkS dry 6.6pdkg dry 6.6pdrs dry 6.6pg,/xg dry 13.2

ldkSdry 6.6pSftSdry 6.6

Udkgd.y 6.6pqkS dry 6.6

ldkS dry 6.6

!g/kS dry 8.6pdks dry 6.6pSftg dry 6-6

lgksdry 6.6

!g/kS dry 6.6pSftgdry 6.6

t S/kS d.y 6.6

USAS d.y 6-6pdksdry 66.0

UdkS dry 6,6

lqkg dry 6,6pSASdry 6-6

Pgkgdry 66.0pdkgdry 68.0

sdkSdry 6.6

2€+ilar-07 26-l'rar-07 ?031584 BDField extraatedVolatile Omanic ComooundsPrepared by method SW8,l6 5035A Sdl (low l6vet)76-1+l l,l,2.Tridtlorofinuqoetfune(FreoFRL674+1 Acebne BRL107n3-l Acrylonitile BRL7143-2 Benzens BRLt0a{6r g@nobenzen€ gRL

7447-s gromodlloaomehane BRI_ftr-274 Bomodidtlorornelhane BRLf*2r2 Bornoform BRL7:l++9 B,omom€than€ BRL7843.3 2€utanone (MEK) SRL10461€ n-gub'lberEene 8RL13+983 sec-Butylbenzene gRL

s8fi€ tert€ulytbenzene BRL7t15-o Carbofidisumde BRL58.23-5 Caabon tebachloalde BRLi0&9(l7 Chlorobenzene BRL75{03 Chlorc€fEne BRL€7€&3 Chlorotorm BRL7447-3 Ct oromefian€ BRL95-aS8 2€hlorotoluene BRL106{3-4 4-Ortorotrduene BRL9{-12€ 1,2-Dibrono-3-chloropfopan€ BRL124-4{r-1 Dibrcmod\lorcm€hane BRL'r(1693-4 1,2-Dlbrornoethan€(EDB) BRL74-9$3 DibKnno.n€thane BRL9$5{rr |,2-Dichlorobenzene BRLsi4r-73n l,3-Didi orcbenzene BRL1(E-a6-7 1,{-Oichlo|.obenz€ne BRL7t71{ Dlcfilorodifluoroftsthsne(Freont2lBRL75-34-3 i.l-Dichtoroethan€ BRL107{e2 l,2.DlcftloroLethane 8RL7t35-4 1, I -t)ic'|loloethene aRL1s6-5+2 ci9-l,2.Oichtoroethene BRL156{0.5 tEir-1,2-Dhhloro€d1ene BRL78{7.s t,2-Dichtoropop€ne BRLt42-284 l,$Diafiloropropane BRL594.e7 z,2$idrlomp[opalte BRL56$5d{ l.lolcltoropropene BRLtoo61{15 cis-1,}DichtoroF}aopen€ BRLiotl61-02$fans-1,$Oidrtoropmpene BRLl0c4i4 Ethyb€nzene BRL87€&3 Hexacfitorobutadien€ BRL5ei-78-6 2-Hexanon€ (MBK) BRL!l€{2{ lsop.opyb€nzene BRL99{7-6 Alsopropyltolugie BRL163411{4 lr€ltlyl terl-butyl ether BRL108-10-l {-Mehyl-21o6n!anone(M|BK) BRL7549'2 Methyl€ne chtoide BRL

SW 846 8il60B 27-|l'at47 nlnar4f 7031658 RLJ

91-2'3 Nsphthalene

Page l8 of t65

Ihit lzbonlorf reporl is aat vali.I Nithotd sn tathor*"i sigrutuE on &a coler pqE.

' ReporEble Deleclion Limir BRf = B€low Reportirg Limit

Page 215: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [d€otificationM8F-19 2,-4'

sA59641-M

Client Proiect #301 -E8

MatrixSoil

Receiv€d22 M^r 0'7

Collection Datc/Time2l-Mar-il7 00;00

CAS No. Analtte(s) FloS *RDL Dilutiorl Prcpdrcd Analyzed Bolch Analjsl

Volatile Organic Compounds

Volalilo Oroanic ComDounds

Prepa.ed by method SW846 5O3SA Soit (tow tevel)

103-65-1 n-Prcpylbenzene BRL10042-5 Styrene BRL630-20$ 1,1,1,2-Tetrachlorcl€thane BRL79-34-5 1,1,2,2-Tetrachlorelhane BRL127-18,4 Tetrachlorcethen€ aRL108,88.3 Totuene BRL87.616 1,2,+Trichlorobenzene BRL12C82r 1,2,4-Tdd1lorcb€nzene ERL71-s5 6 I,1 ,t-Ttid'lor.et1€ne BRL79{0-5 i,1,2-Trichloroethane BRL7941-€ Trichloroethene BRL75694 Trichlorofluoromethane (Freon .j1) BRLs6-18 4 l,2,STrichloropropane BRL95 61.6 1,2.4-Trimethylbenzene SRL10€-67-8 1,3,5-Tdmethylbenzene BRL75{1-4 Vinylchtoride1330-20-7 m,p-Xylene95-47-6 o-Xylene10s994 Tetrahydrofuran60-29-7 Ethyteher99r-054 Tert-amyl methyl ether637,S2,3 E ryi ted{utyi ether1ta-Zl-3 Di-isopfopldetherT'6to Tert-Butanol/ butyl alcohol12+91-1 |,4-Dioxene

Suftogat€ rccoveies:460-004 +Bronofluorobenzene

2037-26-s TolLEne4S

| 7o6co7 4 1, zOichloroethane-d4

1868-53-7 Dibromofluorcmethane

Ertractable Petroleum Hydrocarbo||3

Erlraclable Total Pehol€um HvdrocarbonsPrepared by method SW846 3E5OB

8006$1-9 casoiine68476-3r>2 Fu€t oil#268478-31-3 FuetOiln4

68553{0-1 Fuetoil#6rrl98000m Mobr OilJ00100000 Aviation Fuel

Unidentifed

Other Oil

ARLBRLBRLBRLBRLBRLBRLBRLBRLBRL

96921Ul103

lqkg drypdks drypSftS dry

tiS/kg dry

!g/kg dry

LiS/kS drypg/kg dry

t4/kg dry

Fg/kg dry

lqkg drypsn(g dry

Ugr'l(g dry

IJS/kS drypS,[(S drypq/kq dry

udks dry

Ug'kS drypS/kS dry

t g/kg dry

!g/kg dry

USftS d.Y

udkS drypdks drypdkS drypgl(g dry

6.6

6.6

6.6

6.6

6.6

6.6

6,6

6.6

6.6

6.6

6.6

6.6

6.6

6.6

1 3 2

6_6

66.0

6.6

6.6

6.6

6.6

66.0'132

28.428.428.42A.428.42842A.426428.428.4

1

1

1

1

1

1

t

1

1

1

l

1

1

1

l'|

1

1

1

1

1

1

1

1

SW 446 82608 27-Mat47 27-Mat47 7031658 RLJ

7G130%

70-130 %

7G130 %

70-130 %

BRLBRLBRLBRLBRL

BRL3,260Calculated as

mg/kg drymg/kg drymg/kg dryrnS/kg drynrS&S dryn€r'kg d.ymqkg d.ymS/kS drynrgfl(g drymgn(g dry

+CTETPH 26-MarO7 28-Mar-07 7m1513 DS

TotalPetroleumHydrocarbons 3,260CgC36AliphaticHydrocarbons 3,260

Sunogate rccovedes:$a6-33-2 l-Chloroocladecane tS6

Semivolatile Orgrnic Compounds by cCOrqanocfi lo.ine Pesticides SW846 8O8.lAPreparcd by method SW846 354SA$s{0-2 Atdrin BRL

40.140 %

rcI€ dry 6.16 SW846 8081A 26-Mar-07 28-{\rar{7 7031516 TG

ThLi laboratory repod is notyrldfr rou @ ar.thofited sEnatwe on lhe covc! page.

* Reponable D€tection Limit BRL = Below Rcportinc Limit Page l9 of 165

Page 216: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8F-I9 2'-4,sA5964144

Clied Proiect #301-88

MatrixSoil

Received22-M^t-07

Collectioo DatelTime2 I .Mar47 00:00

CAS No- Analrte(s) Flog Units 'RDL D atio,, Mahad netr Przparcd Amlyzd Batch A,,zlys.

Semivotrlfle Orgrdc Compoo.dr by cC

Oroanochlorine Pesticides SW846 8081APrepared by method SW846 35454319{a.6 a-BHC319-85.7 b-BHC319{€{ d_BHCsa.8+e g_BHC (Lindane)57-74-9 Chlordane72-s.a 4,4.-ODD (p,p')72.s+e 4,41DD€ (p,C)50-2s-3 4,41DDT (p.p')60.57-r Deldrin9s9-98{ Endosutfan I33213€S Endosutfan ll103r-o7€ EndosltfEn sulfate72-2O-A Endrin7421-934 EnddnAklehyde76-t!l+ tleptachlor724a5 i et|oryC* or1024,57-3 Heptachlor Epoxid€8001.3+2 Toxaphooe5100.71.9 a-chlodane5566,3+7 g_Chlordane53494-70-5 Enckin Kebne

SurDg€te re\cowrtts;1 0386-8+2 4, 4-DBoctafr @rcWhenyt (Stesl-zaa Deca$lonbhhenyt (Sr)Polvchlo.inaied giohenvls bv SW846 8082Pfepared by method SW846 3545A1267+1t-2 PCB 101611tO+28-2 PCB 122111r41n6-5 PCB 123253{6$2ia PCB 124212622-29{ PCB '|248

1rae7{$r rcB 12541r0s€-02,5 rcB 126037U+23-5 PCB tZ62t1r0Gr1.1 PCg 1268

Sanrogale rEcovsnies:1 6&e+2 4,+DB4clduoroblphe, yt (5429s1 -2aa Ogcachlorobiphenyl ( St)

Semlvolrtile Orgrtrl€ ComFounds by CCMS

SWO46 0O8tA -Mat47 284?tr47 7031516 TGBRLBRLBRLBRLBRLsRtBRLBRLBRLBRLBRLBRLBRLBRLaRfBRLBRLBRLBRLBRLBRL

6968

BRLBRLBRLBRLBRLBRL247BRLBRL

1(E

SRLBRLBRLBRL

BRLBRLBRLBRL

lgl€ d.y 6.16pdkSdry 6.16

ldkgdry 6.16

UdkS dry 6.16pCAgdry 30.8

FYkgdry 6-16

ldxS dry 6,16

rgkqdry 6.rG

ldkS dry 6.rG

!S/hS dry 6.16

t'gkg dry 6.16

IS{€dry 6.16

uSASdry 6.16

Wkg dry 8.16pg1(Sdry 6.16

udks dry 6.16

rc/kS dry 6.16

!S/ko dry 3O.8pdkSdry 6.16

t Cdqd.y 6-16ydkS d.y 6.16

m_lf l%3G1ffi%

t'dkS dry 12.3

trgkg d.y 12.3

F3iks d.y 12.3

FSikg dry 12.3

Ug,l(gdry 12.3

udks dry '12.3

pdksdry 12.3

tgtS dry 12.3

FdrS dry r2.3

3G150 %30-150 %

trdks dfy {40

tldl,Sdty 44

|lSn(g dry 440

udksdry 44O

lSftsdry 44

rdks dry 140

lJg,kS dry 44o

|rglkg dry 440

SWSrlt' 6082 2GMar-07 28-tvlar-07 7031515 SM

Semivolatile Oroanic Compounds bv SWB46 B27OCPrepared by meulod SW8,l6 35508tl:t32-9 Ac€naphthene20e9e€ Acenaphthyl€n€62.533 Aniline12G12-7 Anthraceno1912-2+9 Alrazine10$333 Arob€nzene/Diphenytdi6zine92€7{ B€nzidlne56-5t3 Benzo (a) anthaac€n€

SW848E27OC 2&Mer-07 28-lr{-07 70O15145

5

5

5

5

M.B

Thls laborabrf EFoa Is nol valid xtithoa an aalhodzpd sigfiztarc o^ thz c.re.r pa$.

. ReporEble Det€ctioo Limir BRL = Below Reporting Limir Page 20 of 165

Page 217: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SampLe IdentiftcationM6F-19 2'-4'sA59641-04

Client Proiect #l 0 l - 88

MatrixSoil

Rcceivedz1-Mar-Ol

CoLlection Date/Timc2l-Mar-07 00:00

CAS No. Analfte(s) Fl"C Unit$ *RDL D aiorl Method Ref, Prcpated Analyzed Btkh A','allst

Semivolrtitr Org|nic Compoonds by GCMS

Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 3550850-32-8 Benzo (a) pyrene205-!Xr-2 Benzo(b)fluoranthene191.24.2 Benzo lg.h,i) pet\y'ene207{8-9 Benzo (k) ffuoEnbene65410 Benzoic acidr0G51€ Benzytatcohol111 91r Bis(2-ctrtoroethoryFnethane111.4aa Bis(2-chtoroethyt)ether39638-32-9 Bis(2-aiitoroisopropyt)ether117€1,7 Bis(2-ehythexr)phthatate101,55'3 +Bromophenyl phenyl ether8568-7 Butytbenzylphthalate86-744 Ca|tazote5S50-7 +Chlorc-3-methylphenol106-474 4_Chloroaniline91-54-7 2-Chtorcnaphthalene9557-8 2_Chlorophenol700s-723 +Chlorcph€nyl phenytether218{1-S Chrysene53-70-3 Oibenzo (a,h) anthrac€ne132-q-9 Oibeflzofuran95-5G1 1,2-Dict{orobenzene541-7+1 1,3-Dichlofobenzene106116-7 1,4-Dichlorobenzene91,94.1 3,3',-Dichtofobenzidine12F8r2 2,4-Diihtoropt|FJnal3466-2 Oi€thylphthatate131-11-3 Oime$ylphhatatel0t67s 2,4-Dim€th),tpfienolu.712 Oi-n.butytphthatetes3+52-1 4,6-Dinitro.2.methyiphenol51-28-s 2,4-Dinitrophenol12r-1+2 2,4-Dinitrotoluene60e2G2 2,G-Dinitrotoluene117-84{ Oi.n-octyl phbalate2OH4{ FluofanhsneW-7+7 Fluorene11&74{ Hexachlorobenzene87{8-3 Hexachlo,robutadienen474 Hexachloroclclopentadi€n€67-f2-1 Tlexachloroethane19+3e-s Indeno (1,2,3{d) pyrcne90-12{ l-Methylnaphthalene76-59-r lsophorone91'576 z-l,letflylnaphthalene954+7 2-Methylph€nol10€-3s-4, 3,+Methylphenol1U6-44-591-20-3 Naphthalene&7+4 2-Nitroenitine99-0+2 $Nitroanitine

BRLBRLBRL

BRLBRLBRLBRLBRL8RL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRL

BRLBRL

BRLBRL

SRL

ldr€ dry 44o

lgftSdry 440

!g/kg dry 44O

Fg/r€dry 440pg/rqdry 44o

lrg/kg dry 440

wkg dry 44o

tg/kg dry 44o

Itgksdry 440pS/kS dry 440pdkg dry 44O

uvkg dry 440

u$rcdry 440

IdkS dry 44OpdkS dry 44OpSrkS dry 44OpdkS dry U0pdkS dry 440

lrSftS dry 440

ldkg dry 44O

lSftS dry 44O

ldkS dry 44O

US/kS dry 44OpS/kS dry 44O

ldkS dry 44OpdxSdry 44Dpdks dry 44Opdks dry 44O

ldkg dry 44O

lrglg dry 440

liS/kS dry 44O

PdkS d.y 440pg'lqdry 44opgkg dry 440pSlkS dry 44O

US/lqdry 440

Fdl(g dry 44O

uSftSdry 44o

udkg dry 44opgkg dry 440

ls/rs dry 440

!g/kg dry 440

tgtkg dry U0pdkS dry U0

udkg dry UOpg/kg dry 440

lSI(g dry 44O

pSIedry 44OpSftgdry 44O

lSftSdry 44o

sw846 8270C5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

This ldoruot! rcpor'a it ,tot wIA v hotlt dn auhotlz.d signoturc on ahe cover Nge.* ReFortable D€t€ction Limit BRL = B€low ReDortins Limit Page 2l ot 155

Page 218: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-19 2'-4'sA5964l-04

Client Proi€ct #301-EE

MatrixSoil

Coll€ctiop Date/Time2l-Mar-0? 00:00

Received22-MaFO1

C"4S No. A^dlyta(s) RcsaA Fl"S Ur,i6 *RDL lNuio Mdhod Retr PtzpaAd A,rilr"asd B4tch Anafust

S€mivolat e Orgroic Compoutrdr by GCMS

Semivolatile Oroanic Compounds bv SW846 8270C

Prepa.ed by method SW846 35508

10+01{ 4-Nltro6njtine98413 Nitrot enzene88-7t5 2-Nitaoph€nol10GO2.7 +Nitrophonol62.719 il-Mtrosodimethytamine621€4,7 N.Nitrosodj-n+ropylarnin€€6-30$ N-Nibo6odiphenylanxneE7{&5 Pentachlomphenol85-01-8 Phenanthr€n€10&95.2 Pftenol129{OO Pyrene11046-1 pyridine

12GE2r 1,2,4-Trichlo,ro,benzeness€5-4 2,4,tTridltofophenol8{r-06.2 2,4,FTrichlorophenol

Sufioga/E rccovedes:32140.8 2-Fhntuhiphonyl

fiz-r2-4 2-Ffuorophqol

4165404 Nitrcbenzene4s

116r.62-2 Phenol4s

1718s1-o Teehenyl4l4

118-79-6 2,4,&Ttibtoflldlphenol

Totel Metsb try f,PA 6000/7000 Serte$ Me{hod!

7439-97-6 Meroury 0.195

Tol M€trb by f,PA 20O Seri6 M€lbods

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLERLBRLBRLBRLBRL

u60715 1

lSit€ dry 1760

llg/rS dry 440

USn(g dry {40pdkS dry 1760pdkS dry 44o

UdLSdry 44Opdkg dry 44u

lSrtS dry {40pSftgdry 44O

ld*gdry .l{O

udl€ dry 44o

ldkg dry {40

rdksdry 440pSftS dry 44O

lgfkB dry 140

36130%1+110%3L1n%15-110%&130%1U110%

rngr'kg d.y 0.0342

nE4(g dry r.08

mgr'kg dry 1.62

rng/kg dry 0.540

mckodq 0.270

rngftg dry 0.5,10

mCl€ dry 0-810

mg{kgdry 1.62

t{/A

mgn 0.02tX)

mgn 0-0150

mg/l 0.0150

"En O-0O25

ftEn o.o15o

mgn 0.(Xx)40

o'dl 0.0i50

mSI 0.0150

%

55

5

55

55

5

55

SW8,l6 8270C 26-Mar{7 28+!,lar{7 7031514 M.B

7,r4G?2-4 Silvsr

744G3$2 ABenic

7440-3+3 Barium

7440-4+9 Cadmium

714G47-3 Chromium

743992-1 Lead

n824$2 Selenium

SPLP Metrk hy EPA 13 12 & 600M000 Sedes Mctftods

SPLP ExtEctbn

7410-22., glvel

74,{L3&2 Arsenic

74ilo-3+3 Banium

7440.419 Cadmium

7440-17-3 Chromium

7439€73 Mercury

?43942-1 Lead

aa8a4+2 Selenium

Ceneral Cbembtry Prr|meterl

SW8.l{l7471A 2&Mar-O7 2&lvtar-07 7mt495 YP

EPA?OO.7 2A nat47 2g]'L,,ar47 7031494 RM

'l SW84{i 1312 26+.iar-07 26-lelar-07 7031560 BD

1 SW84€ 1312/6010A 2&uar-O7 28.lvrat47 7m1651 Hg

1 "

1 '

'I SW846 131224704 ' 28-t\-l5r{7 7m1652 YP

1 SWA4€ 131zli0l0B ' 2A-Mat47 700165l HB

I '

8RL

5.68

12.7

0-735

56.9

r24BRL

Compl€bd

BRL

8RL

0.0300

ARL

BRL

BRL

0.0167

BRL

SM2540G Mod. 21+'Iid47 2 .d,at47 7031470 OP% Solit s

Page 22 of 165

Ihit lzbordoq rqon is noa rditt t&hotd at aQdrhrizcl sigdattr. o8 ,ha @ear pge.

+ R€ponable Detectiod Limit BRL = Below R€portin8 Limit

Page 219: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samptc IdentificationM8F-20 2'-4'sA5964I-05

Client Proiect #301 -88

MahixSoil

Received22-Mar-07

Collection Date/Time2l-Mar47 00:00

CAS No. Analrte(s) RestA F/"s Unirs *RDL Dilation Method Retr Prcpeat Aaalrzed Barch AMUstVolatil€ Orgrnic Compounds

VOC ExtractionVolatile O.qanic Com!ounds

lgkg dry 7.o

!g/kS dry 139pg/kg dry 7.0pdlg dry 7-0

ttqtKgdry 7_0

Ug/kg dry 7 O

Ug/kg dry 7 O

UdkS dry 7.OpS/kS dry 13 I

lig/kg dry 69 5

ldkg dry 7.opg/kg dry 7-0pg/kg dry 7.0

!g/kg dry 34 8pg/kq dry 7.O

lrdkS dry 1 O

ldkS dry 13.9pdkg dry 7.opS4<S dry 13.9

UdkS dry 7.OpgkS dry 7.Opg/kg dry 13.9

!S/kS dry 7.0

!g/kg dry 7 O

!g/kg dry 7.O

Udks dry 7.opSlkgdry 7.O

Ug/kS dry 7-0

!S/l(gdry 13.9

ldkg dry 7-0pg/kg dry 7 O

t g/kg dry 7.0pS/kg dry 7.O

fdkS dry 7.O

ldkS dry 7.opS/kS dry 7.O

tgkSdry 7.0yCkS dry 7.O

udkS dry 7.0

udkg dry 7.0pgkg dry 7.Opgks dry 7.O

ugks dry 69.5pdkS dry 7.O

lgkS dry 7.o

!g/kS dry 7.O

!g/kS dry 69.5

!g/kS dry 6S-5

fg/kS dry 7-O

Field extracted VOC 26-MaFO7 26-Mat-O7 7031584 BD

Prepared by method SW846 5035A Soit (tow t6vst)

76-141 1,'1,2-Trichlorotrifluorcethane(FreoERL

6764-1 Acetone BRL107r3-l Acrldonltrile BRL714t2 Benzene BRL103€6-1 Bromobenzene BRL71-91-5 Bfomochlorornethene BRL7r2r1 Bromodichloromethane BRL71252 Bromoform BRL7,143-9 Bromomelhane BRL78-93 3 2-Butanone (MEK) BRL104-51{ n_Butylbenzene BRL135,98r s€c_Butytb€nzene gRL

98{+.6 tert_Butytbenzene BRL75 15 0 Carbon disujfide BRL56-21s Cafuon tefachloride BRL10&90.7 Chlorob€nzene BRL7fiG3 Chloro€thane BRL67{G3 Chlomtorm BRL1447-3 Chloromethane BRL95 !r+8 2-Chlorotoluene BRL10,643-4 4_Chtorotoluene BRL96-12-8 1.2_Dibronro-3_cfiloropropafle BRL12448-1 Dibrcmo€hloromehane BRL106-e3-4 1,2_Dibronbethane(EDB) BRL74-9s 3 Dibromomethane BRL9s-5Gl 1,2-Oichlorobenzene 8RL5r1-r3-1 l,1DtrhlorobetEene BRL106-46-7 i,4-Dichlo|ob€nzene BRL75-71-8 Dachlorodifluoromethane (Freonl2)BRL7s-34-3 l,l-Dichloroelhane BRL107{G2 .1,2-Dichloloethane BRL7$35-4 '1,1-Dichloroethene BRLr 56-59 2 cis- 1,2-Oichtoroethen€ BRL15c60,5 t ans-l,2.Dicl,tlotoeth€ne BRL76{7 5 l,2-Dichloropropan€ BRL1.2'2&9 l,3-Dichloroprop€n€ BRL59420 7 2,2-Dichloropropan6 BRL563-fr95 l,1-Dichloroprop€ne ARL10061{1-5cis-1,3-Dichloropopene BRL10061{2{tran9.l,}Dichloropropene BRL10041-4 Ethylbenzene BRL8768-3 Hexachlorobutadaene BRLse1,78{ 2_Hexanone (MBK) 8RL98€2-8 tsopropytbenzene BRL99€76 4-tsopropyltoluene BRL1614.{14-1 Methy{ten+utytether BRL108-10-1 4-Mehy-2-pentanone(M|BK) 8RL7fi*2 Methylenechloride91-2G3 Naphthelene

BRLBRL

1

1

1

1

1

I

I

1

1

1

1

1

1'|

l

1

1

I

I

1

1

1

1

1

1

1

1

1

1

I

I

l

I

1

i

i

I

I

1

I

1

1

1

1

1

1

1

1

1

RLJsw 846 82608

Thb laborulory repod h rrot valid nithou an auahodaed signalure on the coter page.

* Reportrble Detection Lihit BRL = Below Reponing Limir Page 2l of 165

Page 220: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-20 2'-4'sA5%41-05

Clienr Projeci #301-88

MatrirSoil

Rec€ived22-Mafi7

Collection Datey'Time2l-Mar-0? 0O:00

CASN?. A Jlc(s) Rerak Fl"s 'RDL Dilulion Me.hod REI PnpaEd Anzlfen Bofth AMIyst

Volatil€ Orgrnic Compouodg

Volatile Oroanic CornooundsPrepared by melhod SW846 5S35A Soil (lor{ level}

10!65.1 rFPropylbenz€n€ BRL10G42,5 Strene BRL63lrm{ 1,1 ,1,2 -Tetrachloro€thane BRL79.3+5 1,1,2,2-Tehachloroehane BRL127.184 Tet€chlorootlrcne BRL10&88.3 Toluene BRL87'614 1,2,:FTrichlorobenzene BRLt20{2-1 1.2,4-Tricilorcbenzen€ BRL71-5'5-6 1,1,1-Trichloroethan€ BRL79-oG5 1,1,2-Trichloroethane BRL79-ll1i Trictlloroethene BRL75€9.4 TrichlorDfluorornethans (Freon I 1) BRL

SW €46 8260S 27-Mar{7 27{ar-07 7031658 RLJ

+CT ETPH 27-NIaFOT 8)v',ar47 7G1500 DS

96-1&,1 l,z,3-Trichloropmpan€9s,63'6 1,2,,t-limethylbenzene'ro8{7{ l,3,tTdmethy{benzene75{r-4 Mnylchlo*l€1330-2G7 m,p-Xyl€n€95-475 o.Xylene10999-9 Tebahwaofuran@-2s7 Ethylether99a-05€ Tert-anryl methyl ether637.923 Eu1yl ted-butyi edlerro+mi Dijsopropyleth€r

Te.i€uhanol / butyl alcohol12'91-l l,4oioxane

Sunogate r€cowrias:45o{04 tl-Elrornofiuorobenzene

m37-26-5 Toluene4S1 7 0eO7 4 1,2 -Dichloroethane44

l86a' -7 Abrcnof,uorcmethale

Extr.atrlrL PetrcI€um llydro...bors

Extractabl€ Total P€lioleum Hvdroca6onsPrepared by me$od SW846 355088006-61.9 Gosoline68a7e30-? Fu€loil tt268a7e313 Fuel Oil tr4e6553{0-4 FuelOjt#6M0980m00 Motor OilJ00t0oco0 Aviation Fuel

Unidendf€dOther Oil

BRLBRLBRLBRLBRLBRL8Rl-BRI-BRLBRLBRLBRLBRL

83

a399

BRLBRL

BRL8RLBRLBRL136Calculat€d Es

Fgl(g dry

Ug/kS dry

rc/kS drypg/kS dry

t rytS dry

lSlko dry

Fgkg drypgrg dry

lgkg drt

ldkg dry

ldlqS dry

tgkg dry

ldko dry

t siks dry

trgikS drypdrg drypgl(g dry

us,rs dryudks dryUS/kS drypS/t(g drypgil€ drypg/tg drypS/kg d.y

Fdl(g d.y

7.07.0

7.07.07.07-07.07.07_07.O7.07.0

7-0f.n7.O7.O13.97.0

69.57.07.O7.07_0

t39

70-130 %

70-130 %

7L1fl %

n-1m %

ftE/kg dry

ngikg dry

firg,kE drynE/kg drymgr'kg drymg/kS dryngLfl(g dry

mSftS dry

m9/k9 dryrndkS d.y

26.026.0

26.028.026.026.O28.O28.026.0m.0

ToblPettoleuml-lydrocarbons 136

C$C36 Aliphalic Hydrccatbons 136

Srrzogal,t /€covsnlrs.'$8e3+2 t-Chro.ooa{adec€.r€ 97

S€mivolrtile Org'nic Cornpoln& by cC

Oroanochlorine Peslicires SW846 8081APreparcd by method SW846 3!15A

:09{G2 Al&in BRL

40-110 %

t'EkS dry SW846 8081A z&ldarry 2Stvlsr{)7 7031516 TG

Ilrac laboralory .eport is tufl eaIA w hotd et ltthorizEtt siglotuE on ahe coeer pogc.

+ Re?odrble Detection Limit BRL = Belou Reportitrg Limit Page 24 of 165

Page 221: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-20 2'-4'sA5964l-05

Cliedt Pmiecr #301_88

MatrixSoil

Received22-M^.-07

Collection Date/Tim€2l-Mar-07 @:00

CAS No. Analftc(s) FIag "RDL Dilution L[e.hod Rel. Prepsred Analyed Batch Anotrst

Semivohtile Orgrnic Compoun& by cC

Oroanochlorine Pesticides SW846 8081APrepared by method SW846 3S45A

319-84{ a-BHC319-a5t b-BHC319-86-8 d_BHC

s84$s g-BHC (Lindane)

51-f4-9 ChlordaneT2-54-B 4,4.-DDD(p,p ' )

72-55'9 4,4.-DDE(p,p')

50-2e,3 4.4.-DOT(p,p')

60,57-1 Dietdrin

959-98S Endosulfan I33213-65-9 Endosutfan ll1031i7,8 Endosulfan sulfate72-20 a Endrin7a21'99 EndrinAtdehyde7644-8 Hieptachtor7243-5 Methoxychbr1024-s7'3 HepiachlorEpoxide8001-312 Toxaphen€s103 71-9 a-Chbrdane556c34-7 g_Chlordane

53494-70-5 Endrin Ketone

Swrcgale Ecoveries:1 038c84-2 1, 4-DB-Octafl uorobiphen yl (S t)2051-24-i Decachlorobiphenyt (Sr)

Polvchlorinated Biohenvls bv SW846 8082

Preparcd by method SW846 35454

12674112 PCB 101611104-24-2 PCB 122111141-16-5 rcB t232s3469-21 I PCB | 24212612 a4 PCB 1248110e7{s-1 rcB 1254110ee8?-s PcB i26037324.23.5 PCB 1262r110G144 PCB 1268

Ssnogaf€ recov€rbsi1 0386-84-2 4,4-DB-Octafluotobiphenyt (Sr)

ms1'2a.3 Decachtorobiphenyl (Sr)

SemivolNtile Orgrnic Compounds by GCMS

Somlvolatile Oroanic ComooLrnds bv SW846 8270CPrepared by method SW846 35508

83€2-9 Acenaphth€ne208-968 Acenaphthylene62{}3 Aniline

120-12-7 Anthracene1912-24-9 Atazine

103-33-3 AzobenzenerrDiphenyldiazine

92-€7-5 Benzidine

56-55-3 Benzo (a) anthracene

SW846 8081A 26-Mar-07 28-Mar-07 7031516 TG

SW846 8082 26-Ma.-O7 28-Mat47 7031515 SM

BRLBRLBRLBRLBRL

8RLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

67105

BRLBRLBRLBRLBRLBRL28.6BRLBRL

12595

BRLBRLBRL475BRLBRL

8RL652

pg/kg dry 6 66

!Sl(S dry 6 66

ldks dry 6 66pdl€ dry 6 66

ldkS dry 33.3

riS/l(gdry 6.66

t/dlq dry 6.66

t'sftS dry 6 66

ldkS dry 6.66

USftS dry 6.66

l.'dks dry 6.66

Ug/kg dry 6.66

t4/kg dry 6.66

!S/kS dry 6.66pSlkS dry 6.66

PSlks dry 6.66

1.|g/k0 dry 6.66

t Sikg dry 33.3

!S/kg dry 6.66pdkS dry 6.66

trdkg dry 6.66

30-150 %30-1s0 %

lrSikg dry 13.3

l.rg/kg dry 13.3

Ug/kg dry 13.3

us/kg dry 13.3

U9/k9 dry 13.3

ugkg dry 13.3pdkS dry 13.3

lsftg dry t3 3

sdks dry 13.3

30-150 %3t\150 %

1

1

1

1

1

1

1

1

1

1

1

I

I

1

1

I

1

1

I

1

!s/ks dry 322FS./kS dry 322

!S4(S dry 322

!S/kS dry 322pgl(g d'y 322

UdkS dry 322

USftS dry 322

US&S dry 322

SW846 8270C 28-Mat47 28-MaFO7 7031514 M.B

This laboralory pporl Lt aol valU witttoa! od au[odzel ignat!rc oa the cover page-

' Reportable Detecrion Limit BRL = Below Reporting Lirnir Page 25 of 165

Page 222: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldetrtincationM8F-20 2,-4'sAs964l-05

Cliept Project #30 r -88

MafixSoil

Collection Date/Time2l-Mar{7 00r00

Received22-M8J-07

CAS No- A.talrk(s) FlIe *RDL Dilution Mc.hod Retr. Prepand Anolyzd Babh Ansbtl

SeDivoletll€ Org.nlc Comporr& by GCMS

Semivolatile Orqanic Comoounds bv SW846 827(rc

Prepared by mehod SW846 355085&32{ BerEo (a) pyrenea)$S.z genzo (b) duorentrene191-21.2 Benzo (g,h,i) p€rytene207.{rE-9 Benzo (k) fuoranthene6s.a+0 Benzoic aodl0G5i€ B€nzyl alcohol11r-9i-1 Bis(2-chloroe$oxy)nEthane111-44-4 Bis(2-chloroouryl)€tler3863&32'9 Bis(2-chtoroisopropytFttEr117-8r.7 Bis(2-€hylheryl)phtlatate10r-55n +&.omophenyl Fhenyl ether85{8-7 Bu!/ benzyl phthalate8G74-€ Carbazole59{}7 +Chloro-3-.nethylphenol106-47{ +Chlorosniline91-5&7 2.Chloron€phthalene95574 24hlofophenol7005-7?.3 rlchloaophenyt phenyl eth€l218.01-9 Chrysene53.703 Dibenzo (a,h) anthracene132-64-9 Dibenzofuian9+50"1 1,2-OiclJorobenzene541-73-1 'l,3-Dichtorobenzene

106-4&7 l,+Dichtorcbenzene91-9+1 3,3'-Dichtorobenzidin€120-83-2 2,4-DichlorcphenolE4-86-2 Diehyl phhalate131-1r'3 Dimehylph(ralate105{74 2,+Dimethylphenolu-7+2 Di-nSutylphthalate$4.52-1 4,GDinitro-2{ethylphenol5!-2&5 2,4oinltrophenoll?l'i4-2 z,4-Dinitotoluenesls2$2 2,6-Dinitroto'lu6ne117{4{ Di-fi-oct},tphhalat€2&4{ FluolEn[lenelF7$7 Fluor€ne11&a-1 Hetachlo.obenzeile87{&3 Hexac}orobutradi€nen474 Hexachtorocyclopentadiefle6r-72.1 tlexachloroethanete+3s-5 Indeno ('1,2,3.cd) pyrenesG12{1-t/ iethylnapht' lalene78-5!Ir lsophoronee1-57.6 2-Mothy{naphthalenoS-{&7 2-M€6ylpienol108-39-4, 3.4-ft sthylph€nol10Frt4.591-2U3 Naphthalene&7+1 2.Nifroenjliness{$z }NiUoonilins

774778353474ARLARLBRLBRLBRLBRLSRL8RL8RLBRLBRLBRLBRLBRL412BRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1,680

BRLBRLARL8RLBRLBRL

BRLBRLBRLBRLBRL

BRLBRLBRL

!S/kS dry 322

lgr'kg dry 322pgi(g d.y 322

ISAS dry U2pgts dry 322

ldkg dry 322ydl€ dry 322pdko dry 322

t gikg dry 322

Udrg dry 322pgkg dry 322

trgtsdry 322pgks dry 322pdkg dry 322

Fgtgd.y 322pgkgdry 322pdks dr, 322

f.'dkS dry 322

lS/kSdry 322pdksdry 322

FC/kS dry 322pdkSdry 322

ldxgdry 322

udkgdry 322

ldkS dry 322pg^Sdry 322

USftSdry 322pgrsdry 322

ldkSdry 322

fjg/ks dry 322

!g/kS dry 322psikgdry 322

rcAS dry 322pdksdry 322

ldkSdry 322

!9/k9 dry X22pdkg dry 322

lrgkg dry 322pCftSdry 322

HglS dry n2

lidlsdry 322

rcfl(S dry 322pdks dry 322

lSikg dry 322

UC/tSdry 322

tidks dry 322

lgkgdry 322

!S/kS d.y 322pS/kg dry 322

US/IS dry 322

SWe46 6270C 26-lrar-t 7 28-{,t€r-07 7031514 tl.B

Thb ltbonlotf Eporl is Eot valld ellhoQ aE outtotlzed slgdsqre or the cover pqe.

' Reportabl€ Detection Unit BRL = Below Repofting Limit Pagc 26 of 165

Page 223: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-20 2'-4'sA5964t,05

Client Proiect #301_88

MatrixSoil

Received22-Mar-0'7

Collection Date/Time2l-Mar-0? 00:00

CAS No. Analrta(s) Resuh FI"g Unia *RDL tuIetho.l Retr. Pftpued AnotrzPd Bakh Atu'lrst

Semivohlile Organic Compoonds W GCMS

Semivolatile Oroanic Comoounds bv SW846 8270CPfep€red by method SW846 35508

100{1$ 4-N,toaniline98-95 3 Nitrobenzene88-715 2,Nihophenol100{2,7 4-Nitrophenol62-75-9 N-Nitrosodimethylamine

62lg'7 N-Nikosodi,n,prOpytamine8G3D-6 N-Nitrosodiphenylamine€7-€F5 pentachlorophenol

€541{ Phenanthrene

10&93-2 Ph€nol12S404 Pyrene1104€r Pyridine12G82-1 1,2!4-Trichtorobenzene95-95-4 2,4,tTrichtorophenot88{d2 2,4,G1nchbrophenol

Sunogate rccovedes:321-60-0 2-Fluorobiphdnylj6/ 12 4 2-Fluorophenol

416t6o-o Nitrobenzene4s

4165-62 2 Phenol4s

1718-514 Tetphenyf4l4

118-/9-6 2,4,6Tibromophenot

SW846 8270C 26-Mar{7 28-[,1aF07 7031514 M.A

7439-S2-1 Lead

778239-2 Sgtenium

Getrerrl Chemistry PNrrmeters

% Solids

pSi$ dry 12e0pdlg dry 322pdls dry 322

!S4(S dry 1290ps(gdry 322

!g/kg dry 322

!q/kg dry 322

!S/kS dry 322

!g/kg dry 322

ldksdry 322

ldks dry 322pdksdry 322pg/kg dry 322pg/kg dry 322pg/kg dry 322

30-130 %15-110%30-130 %15-110 %3G130 %15-110 %

mg/kg dry 0.0360

mg/kg dry 1.20

mg/kg dry 1.80

mg/kg dry 0.598

mgL/kg dry 0.299

mg/kg dry 0.598

mg'rkg dry 0.898

mg/kg dry 1.80

mg/l 0.0200

mg/l 0.0150

mg/l 0.0150

mg/l 0.0025

mg/l 0.0150

mg/l 0.00040

mg/l 0.0150

mg/l 0.0150

%

BRLBRLBRLBRLBRL

BRL8RLBRL848BRL1,700BRLBRLBRLBRL

624959497562

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

'Io{rl Mctals by EPA 6000t000 S€ris Merhods

7439-97€ Mer@ry

Tolrl Melrlr b) EPA 200 Ser;cs Methodr

7440'22r SiMer

744G38 2 AaSeniC

7440-39-3 Barium

7440-43I Cadmium

7440.47,3 Chromaum

7439-92-1 L€ad

7782-49,2 S€t€nium

SPLP M€trls by EPA 13l2 & 6tn0r000 Sedes Merhods

SPLP Extraclion Cotnpleted

7440-!2-4 Silver BRL

7440-38,2 AGenic BRL

74zro-39 3 Barium O.O277

7440-43-S Cadmium BRL

744037-3 Chrcmium BRL

7439-97-6 Mercury BRL

0.641

BRL

10.3

101

1.90

12.3

283

BRL

sw846 74714 28,Mar{7 26-Mar-07 7031495 YP

1 EPA2oo.7 2A-Mat47 2A-MarO7 7O3149d

1 '

1 '

1 '

1 '

1 '

1 '

1 SW8461312 26,Mar{7 2&Ma.-07 7031560 BD

1 SW8461312/60108 28-Mar07 28-t',lar{7 7031651 HB

1 '

1 ' ,

1 "

1 "

1 SW84613'127470A ' 28-lviaF07 7031652 YP

1 SW6461312r'60108 ' 28 tarol 7031651 HB

t '

1 SM2:140 G Mod. 24-MaFO7 24-MaiO7 7031470 0P

RM

0.0182

83.0

Thit lahorulory rcpotl b ,tol ealu nithoul oa suthofuel rigaoturc on the cove. page-

* Reporrable Detection Limit BRL = Below Reporting Limit PaAe 27 of 165

Page 224: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationMEF-2r ?'-4'sA59803-06

CtieotProiect #301-88

MatrixSoil

Cotlection DatelTime26-Mar-07 00l00

Re.€ived21-MaF07

CAS No. Aadlr6(s) RestU nag UnAs *RDL Dila,ba Method Retr. Prcpare.d Aadyzed Bzlch Anelfst

Volstil€ Org.dic Compornds

\€C Exlradion Fdd dlraded

Vdalilg oruanic Comoounds

Propa.ed by mehod SW846 5030 Soit (high tevel)

ttl$1 l,l2.Ttichbrotnfluoroehane(Fnon 8AL67 6+1 AEdOoe BFL101-13,1 Acryldurile BRL71-,13-2 €€rlzeie SRLlC&€&1 &qnob€ozene BRt7147.5 Brcmochbonethane g8L

75.tu Stdmdctftmriehal€ 8fu1VE2 Brunolorm ERL7+&9 g|Dfl|ornedlane gRL

7&e3.3 2.8uhno0e{MEK) 8RL10+513 n.Biytffzene 8nL13+94-8 sec€utyh€nzeE 8ALsnffi bn€{vbenzer€ BFL7t1fi cadon disulfide BRL&ai CattooLfacfibnG 8RLrdl-gG7 O&Obglre{ie 8FL75.0G3 Chtoruehane BnL

2&MarO7 2gMarOT ftts1767 8D

3Hiftr{7 30-frar.07 7(191675 ftr

BFL

BRL

8RL

8tu8RlBFLSRLBFL8RLBRLgnL

8ff1BNL8Rt-BRI,BAIgRL

8fi1BRL8RL8RLBRLB8L8FLBRLBRTBBLBHLB8L8RLBRL8R-

50505050505t)505050505l)505i)505050505)50505050505050505050505050505050505050

505050505050

50505t)505050

tdlq dry S.5

p9rqdty 1670

!S40 dy 83.5

!S/XS dy 85

|lglxS dy 83J

ldb dlv &15

ldXSdry 8i].5

$glgdy 835

ldkS fry 167

ldl€ dfy E35

|.gr€ fry 835

ugrs dy Ei'.5

UgrS dy 8i1.5

!9lS try 117

lgts &y €3-5

|4/rO dy 835

yClS dry t67

|lg/l(! dv {t3.5

!9lg dy 167

|dkg dtv &3.s

Wlr4dfv 83J

|.€/l€ dy 167

wk'ey $5

Wr,S d] 83.5

ljgfto dl a3.5

tgu,gfrt 83-5

pgrq dy 835

pdlq dy 83.5

lgrgdy 167

tiC4q dry E3.s

WkS d)' El.5

lgkS dry 831

Kl4q dry 83.5

uglq dry 83.5

rytS dV 83.5

|JgkS $' 83.5

t4lq dry 83.5

lSlq try SilJ

l4ilq dy 83.5

$kgd] (15

|lg/](g dr m.s

lgrh fy E3.5

tafrS dry 835

|{/rq dy &35

|lglqdy 83.5

|jgD.S dV 83.5

!g4q dy E35

!s/rs diy E€5

t41{tt E35

voc

srr{ 8{6 826{8

67{d3 Chlodofin7{-073 gtbfdnelhane

$.{+8 2ahtorcloluenel6-4iH 4-Crjorotoluenerr'r2.0 lloihomcs+lloropropans12{-r+l D.honochlommefiane10Os-4 1,zobmmo€tlan€(EDB)74-9t3 oibonomehane9650r t2od{orob€nEne5.r-7+1 1,3{tidlor'obenzen6r06-4G7 1,4-{Idoroben2enettTl € DidiorEdfluoromeuBno (Fleon t2)t5-1,1.3 1, t -otddor€thane

1ns.2 t ,2-olailom€ftlane635.1 t,l-[)iahlorodh€ne1se59.2 ciet,zok lom€thenels6-605 tsa$.l2,fidooeth€nei8{?-5 1l-DiddoproFens1e.4.9 1,$0iahloropttsn65&1207 2l.Didrtompropane50!-50-6 t,l{)idiofopropene1006r{1.5 ds.l,}Di* ompfopeft10061-02.6 tar6,lS.oidtolopop€nelqHr-1 Ehylbenzenear{&3 lloEdltorobuladen€s9r-78+ 2+terdo|r€(I,l8K)!B€-8 l!opl!p!|be en€99{7-6 4-lsogopyltoNlg1elE {4,{ ti.l6hy brt+dy{ atjerl0&l0r {-l{odryl.2{€nErcneU|BK)?@2 MehyLrF djodde01.r!.3 NaFhMene

Thb kloraraveport tE nat tal l drhonr o4 autho?izgd signzturu oi ahe aover prge.

. Reportable Detecrion Limit BRI_ = Below Reportiog Limit Fage 2E of | 54

Page 225: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificatiooI[8F-212'-4'

sA59803-06

Client Proiect #301 -88

Collection Drte/Time26-Mar-07 00:00

Received

2'7 -Mar-07Makix

Soil

CAs No. Aasble(s) Fl"e Unils 'RDL Dilurion Method ReJ Prcpa.ed Anallzed Bttch Ana|\l

Volatile Organic Compourdi

Volatile Orcanic Comoound$

Prepared by melhod SW846 5030 Soit(high tevet)

103{51 n,Prcpylbenzene 8RL1@ '12.5 StF€fls 8RL630 20 6 1,1,1,2-Tetrachloroethane BRL793,4 5 1,j,22-Tetrdchooethane gRL

121.18.{ TelrachloR|edlene 8RL1m ss.3 Totuene BRLt7t16 1,2p-f idbtdenzene Bft12G82'l 1,2,4-Tdchloroben2el|e BRL7!.55.6 l,1.1-Tichtoroe(hane BFL79{0-s 1,1,2-Trichloroethane BFL7s1r1s Tridtoroelhene sFL?5{e-t Tridllorcftroromehane (Freon i 1) BRL

BNL

OHL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

8Rl

8RL

BRL

99

102

90

94

50

50

50

5{)

50

50

50

50

50

50

50

50

50

50

50

5t)

50

50

50

50

50

50

udkSdry 83.s

!S,?,S dry &3.5

tS,lS dy &3.5

lglq dy 835

!9rS dry 83.5

uS.ftS dry 835

pgths tt 8.15

!94q dry 83.5

pdrs dry 83.5

pdkS dry 83-s

|Jg/kS dry 83.s

US4q dry 83.5

rc,kS dry 8:].5

tdkg dry 83.5

rc/kS dy 83.5

ldkS dry E3.5

pg/kq dy 167

pdq dy 83.5

lgtS dy 835

lgiq f}' 83.5

lglq dy 43.5

!9lg dy &3.5

!g4q dy 83.5

lSlq dry 835

!g/kg dry 1670

7019)%

70130%

70t30%

7019%

mSftS drymg/rq ftymEkg drymqks drynMs drymSAS drymgks dryILkS drymg^q drymqt(S dry

40140%

lgftS dy 34.8

sw 846 82608

+CT ETPH

9G18.4 l,2,3,TrichtonploPane9t6a{ 1_2,4-Trimelhy'benzene

108-67-8 l,3,5,Trimelhlbenzene75-01 4 Vinl chloridel33O2G7 m,p-Xyleoe9547 6 cxylene109 s99 Tethhydroiuran

m-2s 7 Etryteflerlr94{5{ Ten€rrylmelhylelher637 e2-3 Elh/ leftuvt eher103 2G3 Di-isoFopyl elher75t5-0 Tert Bubnol/ bqt),I almhol123-91-1 1,4-oioxane

44|tat 4BvnonuotcheEene

nJ7-265 Toluene4S

n6o4/4 l,2-Dcllorcethane44

I86ts3-7 DbrofiollwtoflEthffie

Extrsctabl€ Petroleum Hydroc{rbons

E{aclable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

S0Oe5l.9 Gasolined4%.30? Fueto *268176.31-3 Fuei oitt46rs534c1 Fu€tOit#€ms000000 Moff oilJ001o0000 Aliation Fuel

Unidenlilieii

Ohsl Oil

Totat Pstrolsum ftdocarbons

C9-C36 Alipfla[c Hydro€dons

?A6332 lcnbdxladecane

Semivotslile Orgatric Compolnds by CC

Orcanod odne Peslicides SW846 8081A

Prepa.ed by melhod SW846 3545A

309-00 2 Atddn

291\,!ar{7 3&Maf 07 7031772735 1

73.5 1

73.5 1

73.5 1

73.5 1

73.5 1

73.5 1

73.5 1

73-5 r

73.5 1

BRL

BNL

BRL

8RL

BRL

BFL

BFL

BNL

BHL

BfrL

8RL stYE46 80EtA 28-f,iar.07 02-Apr{7 7031739 TG

Thk taboruhvepo.t is notwlU withod on ttho zed sig alue on ttu cover page-

* Reportable Detecrion Limit BRL = B€low RepodnC Limir Pa€e 29 of 154

Page 226: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMAF-2r 2'4'SA59E03-0'5

Cli€ot Proiect #301-88

MatrixSoil

Collection Date/Time26-Ma.47 00:00

Received27-MaJ-07

CAS No. Aaalfk(s) ResaA F14s Uaia *R.DL Dilnioa ttethad Retr. hepared Atu4zed BQLh Anabsl

Semivo|rllk Orgrtric Compounds by cC

Ooanocft lodne Peslidtes SWE46 8081A

Prepared by method SW846 3545A

319.0,16 +BFIC

319'85-? b-BHC

319-€6.0 +EHC

5&8ei SSIE {[h&ne)5t-t1.9 Chtodanen510 4,4{)DD h,p')726$e a,A -DDE (p,p')

5G2e-3 44,-DI]T {p,p)st-1 Di€ldjin

95$S,3 Erdo6ulan I

30213{54 E ldoc|jlan ll1031117{ EndGullanSultale

n-zra Eidin7atg4 Erdrm l$*yde75-4+€ ttoptachtor

a4!5 Melhoxyd o.1utzAs/-X HepiachtorEponde

€0orn52 Tor4helD

[email protected] +Chhfdane556d!+7 g{HordEne

5349+7Ss Enddn Ketone

1M9aa 4UDeafr&tfi4tlcni@)

Mt24.3 Decdlddtplnnfl(Sr)

Polvd oniaabd Eliohswh bv SWg46 8082

Prepared by mehod SW846 3545A

126r!1r-2 PCB1016

11t01-&2 ?Ce,lnl

11111.re5 PC81E2

s34€9-2te frcB124212672?9-6 PCg 1248I'097-6+t PCB 12541 r0e602€ t c8 t2€0

3r!+45 tE8 t2621110G144 PCts 1268

103,6.t11 4,+Deo{'aflwt&phen l (g)

Ntz+3 D€.,dd0lobipltsttyl(3r)

Semlvolelile Orgmic Compo||ndi by GCMS

S.mivolatile 0ro6nic Cofiooun& bv SW846 8270C

Pr€pa.ed by method SW846 35508

8+@{, Aa6rEpfftsne2!8-46.0 A{enaphhyl€ne

6e-5+3 AnIrF

lbrzt Anhten€

192.24{ Atazjn€1@93-3 AzobenzendDipfienytd€zins

e{74 BenzilheE&s$,3 B€nzo (a) hnc€fie

8RL8RL8RLBRIBRLBFLBRLBRLER.BFLBHI.BRLBFLBFLBRLBRL8RL8RL36.339.0BFL

6491

BRLBRLBFLBRI.BRL8RL1048RLBRL

nN

BHLBRLBRLBRLBRLBRL8Ft-8Rt-

!g/f0 dy

Pg}s dv

m/lq dy

|db dv

l4lq drypsrq drypdks dy

!s4q dy

scl.{ dypgls dv

tdlq dry

!9'r€ ry

t8ao dry

|l9r! d)

|,04(g dy

rYls d)'

l4nq dry

FEtq av

l|dlq dv

lls,|q drypdlq dry

*19*1fl

pq4q dry

ugts dv

udrs dw

lgrs dv

!g/ks try

!4ts dy

t4t4 frl

|drs dlvpgre a

wtg%gl1fi%

sw846 mStA

sw846 €082

sw816 8270C

34.8

343

31.8

31.8

171

34J

34.E

34.8

343

31.8

34.8

31A

34J

34.8

34_8

34.8

34.8

3{t

34J

34.8

2g4qr47 m-Aprfl 7(x|1739 TG

?f-M?'47 30'Mar.07 70S173i SM6SG

MG

69.6

6qE

61.6

69.5

63.6

ldlq d.y

jignC dry

$/l0dy

rrgks dy|4lq dvldks rvudk dvdls rv

912

cl2

9l?

9r2

912

912

912

?9. 6r{t m-Aprc7 71101771 ttB

Thb hLorolo4 ,epo.l ls aor ratid xlithoqt ad ctrtonzed sigaalure oa the @wr pzge.

' Reportahle DetE{tion Limit BRL = BeloN Re['orring Limit Page 30 of | 54

Page 227: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiofiMEF-21 2'-4'

sA59803-06

Client Proielt #301-88

MatrixSoil

Received27 -Ma(01

Collection Date/Time26-Mar-07 00;00

CAS No. Analykls) FIag *RDL Dilution Method Rel, Prcparcd Anruzed Batch Analysl

SrmirolNtile Orgrnic Compounds by cCMS

Ssmivolatile oloanic Compounds bv SWB46 8270C

Prepared by method SW846 35508

50-32 8 B€nzo {alpyrenem5.ee2 B€nzo {b) fluoanhene1912+2 B€nzo(g,h,i)p€rytene

al7]E{ Eenzo (k) tluoranftene66.054 Senzoic add,0ost-6 8en44 at,oholnr.grr gis(2-chlorcelhDry)rnehane

11r-4r-4 8rs(2-chtoroehyt)€lher

39638.324 &s(2{hloroisop{opyDether117+r'7 Brs(2+ththexyl)phlhatare101-5s.3 4Bromophenytpheflyleiher

8s 7 Bulyl benzy,l phhatale

8674.8 Catt)azole5eso.7 4.chlof}Smethylphenol106 47 3 4{hlofooniline

915s7 2{hloronaphhalene9rr 3 2-Chlorophenol7m5 72'3 4{hlorophenyl pheflyteher219.01-9 ftrysene$'70.3 Dibenzo(a,hladhracene132 649 Dibsnzofuran95501 1,2-0idorcbenzene5,U.7&r l,3-Dicilorob€nzene10fi67 1,4{ichloDbenz€ne

91.94r S,3lDichlorobenzidins120$2 2,+Dcl o'Dphenol&1.66? Diethylphthalale131 r1-3 Din€fryl phlhalate

10567.9 2,+tlimettrylphenol

u 71-2 Di-n-butyl phhalate

534.521 4,&DinitrP2-mehylphenol51 23 5 2,+Dnibophend1X1+2 z,4-tlinihototueiemG 202 2,SDnibobluene117414 Di{{dylphfiatate206-444 Fluoranlhong86-73.7 Fluoen€

110'7+l Hexacfroob€m€n€

E/60.3 HexaCNobbutadiene

71414 Hexadiorccyclopsnladieoe97.721 Hexaclrorcslhane193-3$5 Indeno(1,2,3{d)py€ne

sr2{ 1-Methtlnaphthalen€7&591 lsophoone

91.st.6 2-Melh!,haphthdene

es-4&7 2-Methyphend

108-39-4, 3,4.Melhylphsnol

91'20 3 Naohalene

@74-1 2-Nitroarilinoee-0s-2 SNibDanitine

8BL

8RL

BRL

BRL

BRL

BRL

BffL

BRL

BFL

BRL

BRL

BRL

BRL

BRL

8RL

8RL

8RL

8RL

8RL

8RL

8RT

BRI-

8RL

BRL

BRL

8BL

BRL

8FL

8RL

8RL

8BL

BRL

8RL

8RL

8RL

BRL

8HL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

8RL

BRL

BRL

pdkS dry

W/rsdypc4q dy

us4q dy

!S.4q drytNkS dtypgkq dry

lidlq dry

|js/ks dry

|4/ts dy

us,ts dry

|lg/hs dry

t4lS d.ypgkg drv

Pdlq drypdk! drypdkS dry

rdlq dypgks dry

PS'IS dty

udls dry

ps/ks dry

pEt(s dry

pdks dy

|l94q d'l

tigtks dty

!94q dy

lJs4(s dy

pgkg dy

ls/ko dy

lJs,l(s dy

US4(S dy

uglq ry

pS,lS dy

ldks dy

pS4(S dy

tdkS dry

pgks dy

tslq dry

pdkS dry

ldks dry

p94q dry

uS4g dry

pnnq +y

Ps/kg dry

m/k! drypdko dry

pYtg drypVre dry

Udl(S dry

9 1 2

9 1 2

9 1 2

912

912

912

912

912

912

912

912

912

9 t 2

9 1 2

9 1 2g l 2

9 r 2

912

912

912

912

912

9 1 2

9 1 2

s l 2

912

912

912

912

9 1 2

9 1 2

9 1 2gtz

9 1 2

912

s 1 2

s 1 2

912

s ]20 1 2

s12

912

912

912

912

s t 2

912

912

9!2

912

sw846 8270C

This labo4tory repo.l k no, vold withoat oE authoized &ignala.e on lhe cover page .

* Reportable Detection Limit BRL = Below Reporting Limit Page .] I of 154

Page 228: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeotificatiooM8F-21 2'-l'sA5980l-06

Client Project #301-88

Collection Date/Time26-Mar-07 00:00

MatrixSoil

Receivod27-M 47

CAS Na Anzba(s) Reruh FIag UniB 1RDL Dilulion Method Retr. Prepated Auryzd Botch Anaust

Semivolalll€ Orgrnic ComFour& by GCMS

Semivdatile Oroanic Conoounds bv SW8,t6 8270C

Pr€pared by melhod SW846 35508

1o(Hrr6 4-liitroanitins$45.3 I't'Uob€ilzene

lo.tr5 2-Niuophenoi1tr{I.7 d-iliropnfiol

62,?F9 N_Nit6odmetnybminefq1417 ltNifo6od{flEpytainine861$-6 NNiurlsdph€r|/arir€F, 86s Penbct orqhenol85{1-S Phemndlr$e

l0&lG2 Pn€nd

129{lt{ P}r€ne

lrn{G1 fudnela!02-1 1,2,+Tridlloroben?ff|g

Fsrt 24STd6toqnenol80{e2 a4,STric}torophefiol

P1&4 2-Fwfiiplwyl

67-121 z+\U6@l!6nd

i16!,@4 Niflf€,lwla4'

f 1ffi? Ptl€t,ol4'

171&514 lqplEnyld4

1t&Ei Zl,enhiornqhend

sw846 82ruC

swB46 74714

EPA20'.7

s1r/8.{6 t312t4nu

sll€46 t3t2fl)r0B

8tuBFI-

BRL

8tuBRL

BHLgFL

BFL

BFL

8Rr-8RL8Rr_BfiLBELBNL

ffi

6 l

n6?

15

ldkg fy 3650

dfS dry 912

l4/rs ey 912

E4qdry 3654

ltksdry 9t2

|MS trV 912

rdlS dy gt?

l4rS dry 91?

}clq dy 912

lrg qey ,t2pg&dy 912

MSdy 012

lgft{ fy 912

WrS (Y s12pdb dv 9t2

$-ra%1r1t0%* l N %

trt l0

30.t9)%

trt10.t

mdks fV 0u385

mdbdry 1A

mgqdry r.gs

|Iqfi{ dry 0.6,44

mdrs ry 0P.

mg'lq dfy 0.6,{4

ntSnq fiy 0.$5

mglqdrY lS

n9l 0.0100

fig/l 0_0150

fldl 0.lXE0

'rE4 0.0@5

mgl 0.0125

rn!, 0.q1040

fi94 0.m75

m91 0.01s0

1

I

1

I

1

1

l

I

I

I

1

1

I

Told M€lrb by EPA 6000/7000 Seri6 M€rhodi

71t39976 lrercury

Totrl Metrb by EPA 200 Seri€s Methods

7t1o44 Sifuet

74!J}*2 A/E€nic

?4ro393 &rtrn

1141L9 C€d Um

74eaf-X Chlolnlum

7'r3&94J Lesd

0.0656

8FL

9.91

60.8

0.611

231

68{

02-Apr47 0GApr{7 7031810 YP

r7@4vz S€l€nium 2.80

SPLP Merdr by EPA r3I2 & 6tXXy7000 sertea Mcihods

SPIP Exlradion Csndel€d

14a0e4 Sfs BRL

71los.2 As€nia BFL

741{f3+3 Beriufi 0.0144

7+{!{s9 Cadnium BRL

71!o4i3 ChftrnitFn BFL

7'Il&074 lllstqrry 8RL

7n+94.1 Le3d 00080

77le.1v2 S6td um BFL

G€oerrl Che mislry Psr':rmeters

%Sdids 75.4

SW8461312 28 atn1 28-f'lar{7 7(Xll763 Bo

s:w8.46 1312/60108 3lrrarc7 02.Apr-07 701t1805 tB

@.Apr{7 70318s YP

' ll2-Apr{7 ?G1606 LR

SM254t G llod- :O-ilar.07 m{er.07 m31879 \lll,l

Thb laborulory rcpod ts tut volid Bdthou an aathnriaad signoarc on th. catcr poge-

. Reportable Det€ctioo LiEit BRL= Below RQorring Limit Page l2 of 154

Page 229: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SampLe IdentificationM8F-22 2'-4'sA5964r-06

Cliert Proiect #301-88

Collection Date/Time21-Mar-07 00:00

Matrix$oil

Received22-Mar-o'l

CAS No. Anable(s) Resah Fhs Unirs *RDL Diluliott Method ReL Prcpand Anzbzed Batch Analyt

Volrtlle Organic Compounds

VOC ExtractionVolalile Oraanic ComDounds

Fieh extracted

pdkS dry 5.4

pS/ftS dry lOA

pdkS dry 5.4

pdks dry 5.4

!S/kS dry 5.4

pSI(S dry 5.4

pdkS dry 5.4

pSrkS dry 5.4

pdkS dry 10-8

pgkS dry 53-S

pdkS dry 5.4

ldkS dry 5.4

pStxg dry 5.4

pSftS dry 27.O

pSngdry 5.4

vdks dry 5 4

usftg dry 10.8pdkg dry 5.4gsftg dry 10.8

ldks dry 3 4

US/kS dry 5.4pg/kg dry 10.8

!g/kg dry 5.4

!g/kg dry 5.4

ug/kg dry 5.4

wKgdry 54ydkg dry 5.4

ug/kg dry 5 4

!g/kq dry 10 8

lgkg dry 5.4pS/kS dry 5-4

!g/kg dry 5.4pg/kg dry 5.4

irg/kg dry 5.4

ugkS dry 5.4

lqkSdry 5.1

Udkg dry 5.4

US/kS dry 5.4

UdkS dry 5.4

Idkg dry 5.4pdkq dry 5.4pVkS dry 5.4

Udkg dry 53.9

ldxgdry 5.4

ugKg dry 5_4

ugkg dry 5 4ps/ks dry 53.9

!g/kg dry 53,9

FS/(g dry 5.4

2Gt]lar-07 26-Mar-07 7031584 BD

Prepared by method SW846 50354 Soit (tow tevet)76-111 1,1,z-Trichlorotriffuoroethane(FreoERL6144-1 Acetone SRl,107-13-1 Acrylonittite 8RL7143-2 Benzene BRL104{6-1 Bromobenzene 8RL7447-5 Bromochloromethane BRL7u2T4 Bromodichloromethane BRL75-212 Bromoform BRL74€99 Bromomethane BRL7843.3 2-Butanone (MEK) BRL1M-51{ n-Butylbenzene BRL135-98{ sec-Butylbenzene BRL9846{ teft-Burylb zene BRL75rt4 Cabon disulfide BRLS-2t5 Cabon teirachloride BRL108.90.7 Chtoroben:,ene BRI7so0.3 Chtomethane BRL67$6-3 Chloroform BRL74{7.3 C,hloromethane BRL9s-d9-a 2-Chlorotoluene 8RL106:43'1 4-Chlorotoluene BRL96-12{ 1,2-Dibromo-3-chloropropane BRL124-48-1 Oibfomodrloromethane BRL108s34 l,2-DibromoettEne(EDB) BRL74-95-3 Dibromomethane BRLs5-50-1 1,2_Dichlorobenzene BRL54r,731 l,3_Dichtorcbenzene SRL106-46 7 1,4-Dichlolobenzene BRL75 71J Dichlorodifiuoromethane (Freon.12) BRL75,34-3 1,t-Djchjoro€thane ARL107-06-2 1,2-Dichlorcethane 8RL7t35-4 1,1-Dichloroethene 8RL156-s,9-2 cis- l ,2-Dichloroethene BRL156-60-s trans- l,2.Dichtoroehene 8RL78{7-s l,2-Dichloropropan€ BRL142-28.9 l,3-DicNofoprop€n€ BRL5942G7 2,2-Dichlo{oprop€ne BRL5163'545 1,.1-Dichtoroprop€ne BRL10061-01,5Cis-1,3-Dichloroprop€n€ BRL10061-{12€tt?ns-1,3-Dichtoroprop€ne BRLi0n{14 Eh!4benzene BRL876&3 Hexachlombutadiene BRLss1-78€ 2_Hexanone (MBK) BRL98{2-a lsopropylbenzene BRL99+74 4-lsopropyttoluene BRL1634{44 Methyl tert-bug,l ether BRL10810r 4-Methyl-2-pentanone(MlBK) BRL7549.2 i,lethytene chloride BRLs1-2G3 Naphthalene

Page 28 of 165

Thit hboratory rcport is ^ot valid x,irtoaa 6 at lhoiz.d slgnaluH on the cover page.

' Reportable Der€ction Linit BRL = Below Repofting Lini!

Page 230: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 231: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-22 2'-4'sA5964l-06

Client Proiect #l0l -88

MatrixSoil

Collection Date/Time2l-Mar-07 00r00

Rcceived22-MarO7

CAS No. Analrte(s) Result FIaK Unirs *RDL Dilution Method Rel. Prcpcred Andlrzed Bdtch Annlrsl

Vobtile Orgrnlc Compounds

Volatile Oaoaoic ComDoundsPrepared by method SW846 5035A Sdl (low tevet)

BRLBRLBRL

BRLBRLBRLBRLBRL

BRI.BRLBRL

75{9-4 Trichtorofuoromethane {Freon jj) 8RL

10365.1 n-Propylbenz€ne10G42 s Styrene63G20-6 1,1,1,2_T€trachtoroethane79-34-5 1.1,2,2-Tetrachloroethane12718! Tetrachloroethene10&48-3 Tolsene87€1i 1,2,3_T.ichtoroberuene12G82-1 .1,2.+Tdchtorotlenzene

71,554 1,1 ,1-T tichhoethane794+5 1, 1 ,2,Trichtoroethane79414 Trichtoroethene

SW84682608 27-Mat47 2I-Mat47 7031658 RU

+CT ETpH 27.Mat47 29.Ma'.o7 7031590 DS

!,6-18-4 l,2,Slrichtoropropane

9543-6 l,2.4.Trimethylbenzene10&87€ t,3,tlimethytbenzene7s{11-4 Vinyl chloride1330-20 7 m,p-Xylen€95-474 o.Xylene10999-9 TefEhydrofuran

60-2+7 Ethl ether99+45-8 Tert-amyl methyl ether637,92-3 Ethytted-butry'ether10&20 3 Di-isopropyt ether7545-0 Tert-Butanot/butylatcohol123-91r 1,4-oioxane

Surogale rccovedes:

460404 4-Bromonuorcbenzene

203/-265 Tduene4S

17o6a07-0 1,2-Dic.hloroelhane-d4

1A6O-53-l Dihromof, uoromelhane

Ertrscarble Petmleum HydrocNrbons

Extractable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

800ffi1-9 Gasoline

68476-30-2 Fuetoit#2

6S47C31,3 Fuet Oil#4605,53{04 FuelOil#6

M09800000 Moto'r OilJ00100000 Aviation Fuel

Unidentified

Other Oil

Total Peholeum Hydrccarbons

C9{36 Atiphatic Hydroc€rbons

Sunogale reeoveries:

a38633-2 |-Chbftocladecane

Semivolr.ile Orgadc Comporr& hyCC

Orqanochlo.ine Pesticides SW846 8081A

Prepared by melhod SW846 3tl5A

30$0l)-2 Aldrin

BRLBRLBRLBRLBRLBRLBRIBRTBRLBRLBRLBRLBRL

93938599

BRLBRLBRLBRLBRLBRLr64

Calculated as164164

98

!g/KS ijry

!g/kg dry

!g/kg drypg/kg drypg/kg dry

Lig/kg dry

!g/kg dry

!g/Kg drypgxg dry

US/kS drypg/kg dry

lgKg dry

U9/k9 dry

ug/Kg drypg/kg dry

Pg/kg dry

!q/kg drypS/kS drypg/kg dry

ttgkq dtypdks dry

ldks drypdkS dry

!S/kS dry

lqks dry

5.4

5.4

5.4

5.4

5.4

5.4

5.4

5.1

5.4

5.4

5.4

5.4

5.4

r0.8

5.4

53.S

5a

5.4

5.4

5.4

5 3 9

108

1

1

1

1

1

1

1

1

1

1

i

l

1

I

I'I

'|I

1

1

1,1

1

1

1

70-130 %70-1W %7G130 %70-130 %

mgi Kg drymgftS drymgu4(g drymgL/Kg drymg/kg drymg/tg drym!r'kg dryndkg dr,lmdks drymgftg dry

,10.1

40.1

40.1

40.I

40.1

40.1

40.1

40.1

40-1

40.1

222

2222222

44-140 %

ugfts dry SW846 8081A 2&Mar-07 28-[,lar47 7031516 TG

Thit hbofstory @port it nol valw *ilhoq an authoizei signaturc ot the coeer page-

I Reportsble Detection Lihit BRL = Below ReportinB Limit Pige 29 of 165

Page 232: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple ldentificatiotrM8F-!2 2'-4'sA59641-06

Client Proiect #301-88

MatrixSoil

Colle€tioo Dat€/Time2 I -Mar-07 00i00

Received22-Mt-o7

CAS Nu Aaslytz(s) Resuk FrtC ,RDL Diluion Method R4 Ptpared Aaalyzel Bstch AMlttt

S€mlvol{tile Orgrnlc Compounds by CC

Oroanod orhe Pesticides SW846 8(E1A

Prepared by method SW846 3545A

319-84{ g-BHC

319-E5-7 b-BHC31$ffi d-BHC

58€$9 gFBHC (Undan€)

57-f+9 Chlordane72-51-s 4,4!DDD (p,C)

72-5+e 4,4'-DOE (p,p.)

so-2$3 4,4.-DOT {p,p.)60-57-l Oeldrin95S-944 Endosulfan I3321165.9 Endosulfan ll1031{74 E tdosllfan Suhhte72-2GE €ndrin742i.9!4 EndrinAldehyde

76-44{ H€ptacilor

72-4?5 Methoxydtlor

1024{7-3 Hoptacldd Epoxide8041-3t2 Toxaphone510!7t-9 a-Chroftlan€5666'34-7 g€hlodan€

5349+70-5 Endrin Keiono

SlnTogafe recovertss:I o38e4+2 4ja&Octdfr uotobiphonyt (Si

m5t-2+j Decachbtobiphenyl (Sr)

Polvchlorinated Biohenvls bv SW846 8082

[email protected] by metM SW846 3545A

1A1+11-2 PCB 10161110+2&2 PCB 12211i141-16{ PcB ,l232

5346r$21-9 PCB 1242126f2-?94 PCB 1248r1c97@l f,rcg t254

1100c€2-5 PCA 1260

3ft2+n 5 PCB 1262rrr0G14-. PcB 1268

Su/'oglefu rEcovrar€srt.Bea-e+2 4, 4-DB-Oddquotubipheny' (St)

msl-21-3 Deeechlombiphenyl (Sr)

S€nivolstilc Org.dc Conrpounds by CCMS

gRL

BRLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRL8RLBRTBRLBRLBRLBRLSRLBRL

69

BRLBRLBRLBRLBRLBRL

BRLBRL

35

BRLBRLBRLBRLBRLBRLBRLBRI-

lgkg dry

lgl(g drypdkS dry

US/kS dry

lrdks dry

ldkg dry

udks dry

ldkS dry

ugkgrtFJ 5.€O

udkg dry 5.80pg/tg dry sao

ldkg dry 5J0

UdkS dry 29.0

udkS dry 5.80pqkS dry 5.80ydko dry 5.80pdkg dry 5.80

ldkg dry 5.80

ldxgdry 5.80

ldlg dry 5.80pSng dry 5.00

Ugikg dry 5-80pgkg dry 5.80

lqrg dry 5-80pw6ry s.80

ldkg dry 29.0pdko dry 5.80

ldks dry 5.80pdkg dry s-80

3G1fi Yotu1 f l%

udkS dry 11.6

ldlS dry '11.6

pS/kS dry 11.6

Ug,fkS dry 11.6pdkg dry 11.6

lrdkS dry t 1.6

udkSdry 11.6pS/rS dry 11.6

ldkSdry 1l-6

30-150 %30-150 %

SWS,ltj 8O81A 2&Marfi 26{{ar{7 7031516 TG

SW846 8082 26-Mar47 2&Mar-07 7031515 SM

SUA46 8270C 26Ma.-07 28.[nar{7 7031514 M-B

S€mivolatile Orqanlc Cornooonds bv SW8,t6 8270CPrepared by nEthod SW846 355088$32-9 AcenaphltEne2G+9e8 Ac€naphttryleneE-5+3 AniIn€12{}12-7 Anthacene1912-2+9 At?in€loi!.9&3 Azobenzoneoiphenytdiazine9247-s B€nzj{tine56-5t3 Bonzo (a) anthrscene

249 5249 5249 5249 5

249 5245 5249 5219 5

Ihk labors&try ftpora ls Eot tolid tiithoU an dt thortzzd signortt e on Uc corer page.

* Repo able Det€ciion Limit BRL= B€low R€Porting Lnnit Page 30 of 165

Page 233: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdcntificationM8F-22 2'-4'sA5964l-06

Client Project #301 -88

Collection Dale/Time2l-Mar-07 00100

MatrixSoil

Received

22-Mar-07

CAS No, Anabte(s) F,oE 'RDL Dilaioh Merhod Retr Prcpared Anal!.e.] Batch Anabst

Scmivolrtile Organic Compounds by CCMS

Semivolatle Oraanic Compounds bv SWg46 BZTOCPropared by method SW846 35508

50-32-8 Benzo (a) pyrene

?0+99-2 Benzo (b) fluoranthene191-24-2 Benzo (g,h,i) p€ryt€ne207-0S€ Benzo(k)fiuoranthene65{5-0 Eenaoic acid10tr514 Eenzylalcohol111-91-1 Bis(2-chloroethoxy)methane111-14-4 Bis(2_chloroethyl)€ther3963+32€ Bis(2-chloroisopropyt)ethef117€1,7 Bis(2-ethythexyl)phthalate101-55'3 4-Brchophenylphenyleth€r8568-7 Bu!/benzylphthalate

€6-748 cabazole59-5G7 4-Chto|o-3-methylphenol106-473 4-ChloDanitine9r-s87 2-Chtoronaphthatenes5-5ru 2-Chtorophenol7005-72-3 4-Chlorophenyl phenyl ether218{14 Chrysenef,3-7G3 Dibenzo (a,h) anthEcener3244-S Dibenzofuran9s-5O-1 1,2-Dichlorobenzen€

!11-73-1 1,3-Dichlorobenzene10€-46-7 1,4-Dichlorobenzene91-94-1 3,3'-Dichtorobenzidine120-83-2 2,4-Dichtorophenolu$+2 Diethyt phthatate

131-11n Damethytphthatate10tr7-9 2,4-Dimethylph€nolu-74-2 Di-n-butylphthalate534-52-1 4,6-Dinitro-2-ineUrylphenol51-2&5 2,4-Dinitrophenol121-14-2 2,4-Dintrototuen€60e20-2 2,o-Dinitrotoluenet17€4{ Di-n-octylphlhatate206r,{{ Fluoranhene

W73-7 Fluorenel1&?4-1 Hexachlorobenzen€87$8-3 Hexachtorobutadiene

n174 Hexacltlotocyc)opentadiene

67-72-1 Hexachloroelhane

1913e-5 Indeno (1,2,3d) pyrene9G12{ t-Methytnaphthalene785$1 lsophorone

91.57$ 2-Methylnaphthalene9538-7 2_Methylphenol

10&394, 3,4-Methytphenol106-.14-59l-2G3 Naphthatene88741 2-Nitmenitine!19-0+2 S.Njtroanitine

ARL8RLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL8RLBRLBRLBRL

BRLBRLBRL

rc/kS dry 249

!S/kS dry 249pdkS dry 245

ldkS dry 249

ldkg dry 249pg/kg dry 249pgts dry 245pdkS dry 249

lgkS dry 249

lgkS dry 249

!g/kS dry 249

trg/kg dry 249

uS/tS dry 249

udkg dry 249yg/kS dry 249pg/kg dry 249pStkgdFt 249pqlkSdry 245

Ig/kq dry 249pS/kg dry 249

Udkgdry 245

USAS dry 249pdkS dry 245pdkSdry 249pg/kg dry 249

lqkSdry 249

lSikg dry 249

ldkS dry 249pdkS dry 249pS/kS dry 249pS/kS dry 249pSI(S dry 249pdkS dry 249

!S/kS dry 249

!S/kS dry 249

Ug/kS dry 249

Fg,kS dry 249pg/kS dry 249

l.idkg dry 249

ug/kg dry 249

Lig/kg dry 249

!g/kg dry 249

!g/kg dry 249

udkg dry 249

ldkg dry 249

ldkgdry 249

!C4(S dry 249

pS/kS dry 249pdkS dry 249pS/kS dry 249

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

Thh laborulory rcpon is not veld wirtoa an a!rtorized sigEature on the cover prye-

' Reportabl€ Detecdon Limit BRL = aebw ReportinC Limit Page 3l of 165

Page 234: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple ldentificationMtF-22 2'-41

sA5964l-06

Ctieot hoiect #30t-88

MatrixSoil

Collection Date/Time2 I -Mar-07 00:00

Received22-Mar41

CAS No. Atautc(s) F L g ateils aRItL Dilaion Method Retr Prcpand AtsQzed Bath Anolfst

SemivoL.lil€ Organic Comporn& by CCMS

Semivolatlle Orqanic Comoosnds bv SWe46 8?70C

Pr€pared by melhod SW846 35508

r !015 4-Mtoanitine98€5-3 Nitrobeflzene

8E-75-5 2-NibophenolIO(!!A-7 4-NitEPhenol62-754 N-Njtrosodimethylamin6621-64,7 N-Nit!5odi-Gpropylamin€BG.3G6 N-Niaosodiphenylaminea7€e5 Pentacfilorophenol85.Oi€ Ph€nanlhrenelO&€5-2 Phenol1294+0 Pyr6n6rlo{Fl f}yridhe12{}€2-1 1,2,4-Tdcf{ofobenzene

95-9+4 2,4,$Trichlo.ophenol8O{G2 2,4.dTdchlorophenol

Suiogate 'atj'\lerias

32140-8 2-Ftuor&iphenyl

367-124 2+fuorophenol

4165404 Nillobenzene4s

4165-62-2 Phqol45

1718.s14 Tephenyl4l4

1 18-79-6 2, 4,o-Ttibton@phenol

Totll MGtrli by EPA 600(y71n0 Series Merhods

SW846 a270C 2GMsrry 28lhr-07 7031514 M.BBRLBRL

BRL8RLBRLBRLBRLBRLARL

BRLBRL8RLBRLBRL

4851

54

0.0614

BRL

4.95

28.8

0.69s

40.9

4t1.9

BRL

Completed

BRL

BRL

0.0682

aRro.0214

BRL

BRL

8RL

90.6

ldkg dry 994

ldrS dry 249

Fgl(S dry 249

ldl(g dry SS4

ldl€ dry 249

ldl€ dry 24s

UgJkSdry 245

l€il€ dry 249

lSASd.y 249

UgtS d.y 249

udkgdry 249pgrs dry 249pdksdry 249

ldkS dry 249

FdkS d.y 249

3O-130 lo1UI10 %30-130 %15-110%3G130 %1+flo%

mglkg dry 0.033,0

drg/kg dry 1.04

mg/kg dry 1.56

mSn€ dry 0.519

mgn(g dry 0.259

drdkS dry 0.519

mgtg dry 0.71A

n€rkgdry 1-56

msl 0.O20o

mg.fl 0.0150

mgl 0.0i5O

rnSI 0.0025

mdr o-o150

rndl 0.00040

mdl 0.0150

mgn 0.0150

%

5

5

5

5

5

5

5

5

5

5

5

7439-S7{ lredrry

Total Mebls by EPA 200 serles Mettodt

7440-224 Silye(

Zt4lts3&2 AE€nic

74ao.393 BAriUm

7+G43-9 Cadnrium

7r.4crt/-3 Chromium

74:99?-1 Lead

7782-492 S€lenium

SPIP Afaclion

71"1G22-{ Siker

7a,|{)ie2 A6enic

Trlrl{)'3+3 Badum

7r.1O.13-9 Csdn{un

74'(F17+ Chromlum

7439-974 Mercqry

7+3s-C2-1 L@d

7?82-49-2 Selanium

Generd Chehbtry Prrsmetels

% Solids

1 Sw846 747fA 2g-n1at47 284a147 ?031495 YP

EPA 200.7 2A-Mar-O? 28-&lar{7 70314S4 RM

SPLP Mctdr by EPA 1312 & 600{y7000 S€rier Me0ods

1 SW8461312 m.Ma.-07 26-&ta.47 70315€0 BD

1 SWE|6 f31:l/60108 23'-Mat47 28.|nar4f 7031651 HB

1 '

1 '

1 SW8,|613127470A ' ?6-MEt47 7031652 YP

I SW8461312/601@ ' 284ar47 7txil651 HB

1 '

1 SM2540 G Mod. 2+Mat47 24]|n9f47 7031470 QP

Thtt lab&tury Epora ls nol eotu wi&ra!! att arthorlzd sigrratara on lhe coye page -

* Reporbble Detectiod Limit BRf = B€low Reporting Limit Page 32 of 165

Page 235: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationM8r,'-2t 2,-4'sA59641-07

Client Proiect #301 -88

MatnxSoil

Received

22-Ma(0'7

Collection DatE/Time21-Mar-07 00:00

CAS Na A"aryte(s) FIag A a *RDL Dilqtbz Merhod Ret Prepa.ed Adalr.ed Barch Analtsl

Volrtile Orgrnic Compounds

VOC ExtractionVolatile Oroanic Comoounds

Field €xtrected

Prepared by method SW846 5035A Soit (tow tevet)

76 13'1 1,1,2-ftidllototinuoroethane (Freo€RL6744-1 Ac€tone ARL

107,13-1 Aor/lonitrit€ BRL

714T2 B€nzgne BRL

108-86'1 Bromobenzene BRL

f4-97-5 Bromochloromelhane BRL

75-274 gromodichtoromethane BRL

75-?12 Bromotorm BRL

7,1+3-9 Bromomethane BRL

78-9+3 2-But6none (MEK) BRL

104-51-6 n-Butylbenzene BRL

13+9€{ sec-Butlbenzene BRL98{6-6 tert_Butytbenzene BRL

75,rt0 cabon disu tde BRL

56'23-5 Cabon tetrachtoride BRL10&90J Chiorob€^z€ne BRL75-00-3 Chloroethane BRL67€S.3 Chlororoarn BRL

74Af-3 Chloromethane BRL

9549{ 2-Chlorotoluene BRL

10643-4 +Chlorotoiuene BRL

96-12{ 1,2-Dibromo,3-chloropmpane BRL

124-48-1 DibromochloaomedMne ERL

10Gs3-4 l,2-Dibromoethane(EDA) BRL

74-95-3 Dibmmomethane BRL

95 50,1 1,2_Dichtorobenzene BRL

54173-1 1,3-Dichlorobenzene BRL106-'16'7 1,4-Dichtorobenzene BRL75-71-A Dichlorodifluoromethane (Freonl2)BRL75-34-3 1,l_Dichloroethane BRL

107{6-2 1,2-Oichlofo€thane7s-35-4 1,1-DachlofoetfEne15+59-2 cis- 1 ,2 -Dichloro€thene1s6{0-s t?ns-1,2-Dichloroelhene78{7-s 1,2-Dichloropropane142-28-9 .1,3-Djcldoropaopane

594-20-7 2,2-Dichlofopropanes61s8{ 1,1-Dichloropropene1 0{,61{1-5 cis-1,3-Dichloropaopene10tr6r{2{ taans-1,3-Didlloropropene10H14 EhylbenzeneA74B-3 Hexachlorob{,ttadiene591-78{ z-He1anone(MBK)98{2-0 lsopopylbenzene9€47{ +lsopropyltoluene1634{4-4 Methytted-butylehef

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

10&10-1 4-Med1yi-2-penranone(MIBK) BRLr5+*2 Metfiytene chtoride 8RL

pqksdry 60

lgftS dry 120

lqkg dry 6 0pqkS dry 60

lgks dry 6 0pgkS dry 60

VdkSd(y 60

lgks dry 6 0

lgks dry 120

ldks dry 59I

PgkS dry 6.0

!S/kS dry 6.0pgftS dry 6.0ggnq dry 30 0

udkg dry 6.0

USiTKS dry 6.0

US/kS dry 12-0pS/kS dry 6.0

!g/kS dry 12.0pgftg dry 6.0

ldkg dry 6.0

W/kg dry 12 0

!g/ks dry 6.0

!g/kg dry 6.0pgkg dry 6 0

!S/kS dry 6.0

ldkS dry 6.0pg/kS dry 6.0

!g/kg dry 12.Opg/kg dry 6.0

ldkg dry 6-0

tig./kg dry 6.0

ldkg dry 6 0

Fdkg dry 6 0pdks dry 6 0

udks dry 6.0

ldkg dry 6.0

ldks dry 6.0

t Sikg dry 6.0

t'dkg dry 6.0pg/kg dry 6.0

ldkg dry 6 0pdkS dry 59.S

ldkS dry 6.0pg/kg dry 6-0

HdkS dry 6.0pS/kS dry 53 IpStkSdty 599

US/kS dry 6.0

26-MaF07 26-[4ar{/ 7031584 BD

91-2G3 Naphthatene

Page ll of 165

This labo4loA ,eporl b ,rol e.tlid wilhou! on authoir?d signatare on the covr paEe-

a Reportable hection Limit BRL = B€low Reporting Limit

Page 236: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samote ldeotificationMtF-23 2'-4.sA5964l-07

Client Pmject #l0t-t8

MatrixSoil

Collection Date/Time2l-Mar-07 00:00

Rec€ived22-M,.r-07

CAS No. tuslru(s) Restll Flos "RDL Dilution Me.hod Retr hepar.d A@lyzen Bahh An4lfsl

Vohtile Orgrnic Compoohds

Volatile Oroanlc CornooundsPrepar€d by ms0|od SW846 5035A Soil (low l€ve{)103{5n GPropy'benzene BRLi00{2-s St}'I€n€ BRL63G2c6 1,'|,1,2-T€{r€cHoroethan6 BRL7s-3+5 1,'|,a2-T€Fachloroethane BRLt27-18-4 TetachloroellEne BRLt0&883 Toiuen€ 8RL87€1{ 1,2.}Tdchlorobonzen€ BRL12o"B2n 1,2,+Tdchlorobenzen6 gRL

7l-55€ 1,1,1-Td, oroetharte BRL79{G5 1.1,2-Trict' oroefhane gRL

79{1{ Trichloroethene BRL?5{9-{ Trichloaonuorcrhethane (Freofl 11 ) BRL9&18-4 t,2,$Trichtoropropane BRL95$3{ 1,2,+Tdmethytbenzene BRL10&674 .l.3.glrimethytb€nzene BRL7Fo1-4 Vinyt chtoride BRL133G20-7 m,ptsXylene BRL9s-47i o-Xylene BRL10999-9 T€trahydrofuran BRLdl"2s7 Ethylether BRLgarcs{ Tort-amylmethy' ether ERL637-s2-3 Ethyt ts -buM eher. BRLl0e?G3 Diisopropyl €ther BRL75€t0 Tert-Butanol/ butyt atcohol1?+9rr l,4-Oio,€ne

S|'rogale reovelies:1@401 +Btofitofluorottenzeie

m1z-26-s Tolucne4g

| 7060474 1,2'ichlorcethane44

186V5?7

SW8468260S 27-Mat47 27-Met47 7031658 RLJ

BRIBRLBRL

BRLBRLBRL

Calculiated as5545$4

123

pqlqdry 6.0pdxgdry 6.0

!S/kS dry 6.0

!SI!S dry 6-0

lqkSdry 6-0pdkSd.y 6.0pg^gdry 6.0

FS/&S dry 6.0

Fgtsdry 6.0pdl(gdry 6.0

!g/tS dry 6.0

ldl(g d.y 6-0

ldkg d.y 6-0

lglq dry 6.0

lrgxS d.y 6.0

lSrqdry 6.0

IC/X9 dry 12-0pdts dry 6.0

ldkS dry 59.9

UdkSd.y 6,0

ldtsdry 6.0pdxs dry 6.0pgtS dry 6.0

!g*9 dry 59.spCftS dry Im

70-130 %70130 %7G130 %70-130 %

nE/kg dry 219mgilqdry 249mgfl(g dry 249mgr'kg d.y 249rndkS dry 249meftgfty 249mdl€ dry 249msr€dry 249nE/tgdry 249nqfgdry 219

40-140 %

+CT EIPH 27-Mat47 29 lat47 7031590 DS

f'ttrft bbh Pcft oleum Hydrocrrbou3

Extractable Tdal Pelroleurh Hvdmc€rbonsPr€pared by method SW846 35508flXlftl-S Gasolinee18.476-30-2 Fuel O[ #2eaa7a31,3 FuslOil r,46855$00{ FuelOiltSM0se0@00 lroto. OllJ0l)100000 Aviation Fuel

UnidefltifedOth€f OilTotal Peboleum MrocgrbonsC9436 Aiphatic Hydr@rbons

Slnrogat€ rBcowriss:3i86-JXZ l-Chtotoocladecane

Sehivoldlc Oryrrtc Compornds by cC

Oroanochlorin€ Pesticides SW846 808'lAProparcd by method SW846 3545A3tr9-q1,2 Aldrin

BRLARL

9292u99

t01010

101 01010t0t0

t0

ygtg dry 6.26 S1418,16 SOEIA 2AMar{7 28{rar{7 7031516 TG

Thit bborulory reIofl E Eot ealld x,ithotu ta aathoiltd slgnalaE ol the caver pz$-

a Reportable Detcctiotr Limit BRL = Belo*' Reporting Limit Pase 34 of 155

Page 237: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Saftple ldenfificadon

M8F-23 2,-4,sA5964l-0?

Client Proiect #30t-88

Collection Date/Time2l-Mar-07 00:00

MatnxSoil

Reoeived22-Ma.-07

cAS No. Anab'E(s) FloC UniLs *RDL Dilation Method ReJ Prcpared AnaIWd Batch Anabsl

Semlvoladle Organlc Compounds by CC

Oroanochlorine Pesticides SW846 8081A

Prepared by method SW846 3545A

319-8,{4 a-BHC319-45-7 b-BHC319-86{ d-BHC58€e-e g_BHC (LiMane)

57-7+9 Chlordan€72-s4.4 4,4.-DDD(p,p')72-55-e 4,4-DDE (p,p')

5&2+3 a,4-ODT (p,p')

60-57,1 Di€ldnn

95998-0 Endosulfan I332J3it9 Enotosulbn ll103147-8 Endosulfan Sultate72-204 Endin7421,93-4 EndrinAld€hyd€7644'4 H€ptachtor7243-s Methoxychtor1024-57-3 tleptachlo.Epoxide80013S2 Toxaphene5103-71-9 a-Chlordane5566-34-7 g-Chlordane

53494,70-5 Endrin Ketone

Sunogtale recov€nesi1.;]8fre+2 4,{-Dgocte\uorobiphenyr (s4

m51-2+3 Decachlorobiphenyt (Sr)

Polvchlorinated Biohenvls bv SW846 B082

Pfegared by method SW846 3545A

12671,11-2 PCB 10161110d.28-2 PCB 1221111-41-16.s PC8 12325346+21-e PCB 1242126f2-4n PCB 124811097{9-1 PCB 125411096-82-5 rcB | 260x732+2r' PCB 12621110+144 PCB 1m8

Sunog€ls recow'bs:10386842 4,4-DB-Octatluorobiphenyl (Sr)

2051-243 Decachlombiphenyl (Sr)

Semivoloail. Orgraic Conpounds by CCMS

8Rt_8RL8RLBRLBRLBRL8RLBRLBRLBRLSRLBRLBRL8RLBRLBRLBRLBRLBRLSRL8RL

126

BRLBRLBRLBRLSRLARL109BRLBRL

3585

BRLSRLBRLBRLBRL8RLBRL888

pg/kg dry 6.26

PS{(S dry 6.26pg/kg dry 6.26

!S/tS dry 6.26

ldkg dry 31 3

!g/r(g dry 6.26

!g/(g dry 6 26pS,4(S dry 6.26pS/kS dry 6.26

lSftS dry 6.26

!S&S dry 6.26psftS dry 6.26pSAS dry 6.26pdkSdry 626pdkg dry 6 26

!g/kg dry 6 26

!g/kg dry 6-26

trdkS dry 31.3

!S/kS dry 6.26pg/kg dry 6.26

UdkS dry 6.26

30-150%30-151) %

UdkS dry 12 5

Fg/kg dry 12.5

!g/kg dry 12.5

t'g/kg dry 12.5

Ug/kS dry 12.5

US/kS dry 12.5

!g/kg dry 12.5

!C/kS dry 12.5

rrdks dry 12-5

30-150 %30-150 %

pdkS dry 771

lgftS dry 771

lgftS dry 771pdkS dry 771

ldks dry 771

!S/kS dry 771pS.4€ dry 771

Us/kS dry 771

SW8468081A m-Mar{7 28iL,lar-07 7031516 TG

Sw846 8082 26-Mar 07 28-MaF07 7031515 SM

SW646 8270C 26-l\rar47 26-Mar-07 7031514 M.B

Somivoiatile Oroanic Comooonds bv SW846 8270CPrepared by method SW846 355084332-9 Acenaphthene20es6{ Acenaphthylene62-5+3 Aniline120-12-7 Anthracene1912-24-9 Alrazine10+33-3 Azobenzene/Diphenyldiazine92{7-s Benzidine56.55'3 Eenzo (a) anthracene

5

5

5

5

5

5

5

Thit laborutoty rcltor'l is not uolid withotl.t sulhotized slgn^itre on lhe covr page.

' Reporta.ble Detection Limit BRI = Below Reporting Linit Page 35 of 165

Page 238: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationMEF-23 2'-4'sA5964l-07

Clietrt Proiect #301-88

Collection Datey'Time2 I -Mar{7 00:00

Received22-Mat47

MatrixSoil

C"1S No, Andlrte(s) FIag Adia *RDL Diluion M.lM Ret Prcpzrcd A&olfaad Batch Aralyst

Semivolalile O€rnk Cortrlour& by GCMS

Semivolatile Orqanic Comoounds bv SW846 8270C

Preoared by nethod SW846 35508

50-32{ EerEo (a) pyreneS-S-2 B€nzo (b) fluoran$ene191-24.2 Senzo (9,h,i) perylene20?-(E-q Benzo (k) fluo(anthene85{5-0 Benzoic acid1o,+5r€ B€nz!'lalcoholi11-911 gis{2-chloroethory)rnethane

i1l-444 Bis(2-chtorcethyt)€her39sH2-9 Bis(2{hlooisopropyl)elher117-s1.7 Bis(2_€6ylhexyl)phthatate101-55-3 4_Brofippt€nyl ph€nytether85.68.7 Butylbenrylphthalate8&74-a Cerbazole5g.5tl7 4chlorE-3-flethylphenoli06-.|7{ +Chlomaniline915&7 2-Chloronephthalene95{7{ 2.Chlorophenol700e72-3 +Chloroph€$yt phenyl ether21841s Chrysene53.7G3 Dib€nzo (a,h) anthracene132{44 Oib€nzofuran95-50-i |,z-Oichlorobenz€ne4,41-&1 l,+Oic*orobonzen€10ffi7 l,4-Dichlofobenzenes1€4-1 3.3'.Oid$orobenzidine12Gs+2 2,4-Oichloroph€nol64+s2 Diefly' phtrlalate131-11.3 Dimethyl phthalate10567€ 2+Oirnethytpherctu-74-2 fx-n-buvphthalate534-52-1 4,6-Dlnitrc-2-methylphenol51-2F5 2.4-Dinitrophenol121-14-2 2,4-Onibololuene606-2G2 2.(ioinibotoluene117{44 Dkl.octylphlhatate20G.r4-o pluot€nthene

&7+7 Ffuofen€l1&74-l Hoxachlorobeozene87{S3 Hexachlorobutadienen474 Hexachloroq/dopentadi€fle67-12-1 Hexacfiloroethane19$39-5 tfld€no (1,2,3-cd) pyrenefi.124 1-Methylnaphthatene7E-59-l lsopftorcne9157$ z.tlethynaphhatene9s$? z.Methytphenol1o&x94. 3,4-Mehylphenol106-44-59l-21>3 Naphthal€ne&-744 2-Nitroanitine9O.O+2 $lliuoanitin€

BRL1,370BRL1,180BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1,G)0BRLBRLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLgRL

aRlBRL2,090BRLBRL

BRLBRLBRLBRL8RLBRL

BRLBRLBRL

BRLsRtBRL

ldks dry TI1

udks dry n1pgrs dry nr

USrkS dry 7?1

tdl(g dry 771

tdks dry 771

t|g^g dry 771

uS&Sdry Tll

USAgdry 771pSrrS dry 771

UdrS dry 771

Ug/kg dry 7f1

!g/ko dry 771pS/kS dry 771pS/kS dry 771

l,gkgdry 771pdks dry 771

ldlq dry r7r

IS/IS dry 771

lgkg dry 771pSikS dry 771

UC/tg dry 771

uErsdry 711pdrs dry 7lr

lgrkS dry 171

US/kg dry 711

rdkS dry 771

IISA9 dry 771

tdkg dry 711pS/kS dry n1pgl(g dry 771

ldlq dry f1r

Udks dry 771pgi€ dry 771

lgl€ d.y 771pSftS dry 771

IdkS dry 711

udks dry n1pgrs dry 771

ldtS dry nl

Uglq dry 771

lqkSdry Tt'l

Itg/kg dry TI1ys/kg dry 771pg,lq dry n1pglgdry 771

ldkg dry 77r

US/kS dry n1

frgftS dry n1

Ug/kS dry 771

SW846 8270C rc-Mat47 28-l4a..0l 7031514 M.B

Trth lafuorf rqod ls t ol volid w hoa dn at lhorlzd slgnaleQ ott the coeer IraE .

' Reportable lh€crion Limil BRL = Below Reporting Limit Page 36 of165

Page 239: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeptificationMtF-23 2'4'sA5964147

Client Proiect #301-88

MatrixSoil

ColLectiotr Dato/Time2l-Mar-07 00:00

Received22-Mar-0'l

CAS No. Andr.c(s) Resa,t Fhc Unia *NDL Dilution Method Retr Preparcd Arralyzed Borch AnaQsl

S€mivohtil€ O.ganic Comp0undr by CCMSSemivolatile Oroanic Compounds by SW846 8270CPfepared by method SW846 35508

SW846 8270C 26-Mar47 2g4l,ar07 7031514 M.B

1 SW8467471A 28-MaF07 28-li,lar{7 7031495 YP

Toral Me..ls by EPA 6000/7000 Srries Merhods

7439-976 M€rcury

Total Metab by EPA 200 Sarler M€rhods

74rlct-22-4 Silver

74.rc-3€-2 Arsenic

7444-39-3 Earium

744043-9 Cadmium

7,140-17 3 Chromium

74@-92-1 Leacl

t82-49-2 Selenaum

100-0lS 4-Nitroaniline

96-9+3 Nitrobenzene

8a-7+5 2-Nitrophenol

10G02-7 4.Natrophenol62-7+9 N-Nitrosodimeihylamine621s4-a N-Nitro6odi,n-p.opylamine86-30{ N-Nitrosodiphenylamine87{+5 PentadtlorQphenol

a5-01€ Phenanthrene

108-95-2 Phenol129-00{ Pyrene11G86r q/ridine

r20-82'1 1,2,4-Tricilorob€n2€ne9s95-4 2,4,+Trichlorophenola8{+2 2,4,6-Trichlorophenol

Surrogate .sco!/€ti€s:

32140-8 2-Fluorobiphenyl

36r-124 2-Fluotophenol

416a404 Nil/obenzet e4S

116542 2 Phenol4s

1718,51-o Terphenyl-dl4

1tB n'6 2,4,6-Tibromophonol

trdkS dry 3080

udks dry 171

!s/ks dry 171

W/kS dry 3080

w/kg dry 171

W/kS dry 771

lgkg dry f71

WikS dry 771

lsiks dry 771

ldkS dry Tl1

WftS dry 771

rr9/k9 dry Tl1

!g/kg dry r71

lSftS dry 771

!S/kg dry Tt1

30-130 %1*110 %30-130 %1+110 %30-130 %15-110 %

mg/kg dry 0.0327

ddkg dry 1-02

mgL/kg dry 1 .52

ms/kS dry 0 506

mdlQ dry 0.254

mg/lg dry 0.508

ngkq,try 0.t62

mq,/kg dry 1.52

mg/l 0.0200

mgl 0.0150

mq 0.0150

nrsn 0.m25

mgLI 0.0150

mg|n 0-00040

tndl 0.0150

firg/l 0.0150

BRLBRLBRLBRLBRLBRLBRLBRLBRL

BRL2,210

BRLBRLBRL

6 l

59745 l

0 t93

BRL

6.41

39.2

0.599

29.4

99.7

BRL

5

5

5

5

5

5

5

5

5

5

5

5

5

5

SPLP Met{ls by EPA 1312 & 6000/7000 S€ri€s M€thods

I EPA200.7 28-Mar07 28-[4ar47 7031494' t "

1 '

1 "

I '

t '

1 "

1 SW84613t2 26-Marfi 26{v1aF07 7031560 BD

1 SW84613'f260108 2a-Ma(41 28-Mat-07 7031651 HB

1

1 '

1 ' ,

1 ' ,

1 SW846131274704 ' 2&Mar-07 7031652 YP

1 SW846131260108 ' 28-Mar-07 7031651 HB

1 '

1 SM2540GMod 244tarO7 24-Mat47 7031470 QP

RM

SPLP Enraction

744G22-4 Silver

7440-34-2 Arsenic

7440-3s3 Barium

74a0-419 Csdmium

7440-47 3 Chmmium

7439-97{ Mercury

7439-92-1 Lead

7ra2{92 Selenium

Gercral Chcmirtry Perar€ter!

% Solrds

Completed

BRL

BRL

0.0427

BRL

BRL

BRL

0.0336

BRL

89.9

This lahorutory rcpod is ,ot valid wilhotd a saahori.et sEnarare on thz cot'er pqge .

'Reportable Detection Limit BRL = Below Repoding Limil Page l7 of l6J

Page 240: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-242'4'sA5964t-08

Client Proiect #30t-88

MatrixSoil

Collectiotr Date/Time2l-Mar47 fr):00

Received22-Mafi7

CAS No- Adat z(s) Rett/lt Flzs A^i6 *RDL Dilatbd Method Rel Pnpand AnaIWd Bakh tut4lfsl

Volatile (kg lc Compoulds

v(,u Exlrafiron Fbld extracted

198

pg/kg d.y 102pqkS dry 2030

ldkS dry 1o2

fjdkS dry 1O2

ldksdry 1o2

lslkg dry 1o2pdkgdry 1o2

ugftsdry 1o2pSfl(g dry 203pdkgdry 1O2OpC4(S dry 1O2

!S/kS d.y 102p€lkgdry 102pdks dry 508

rdxsdry 102pdxs dry r02

ldxs dry m3

ldxS dry 1O2

!dlc! dry 2O3

!g/kg dry 102

t glS dry 1O2

!d*S dry 203

US/tg d.y 1O2pdfq dry 1o2

ldks dry 1O2

ldl(g dry 1o2

lgkS dry 102

t4k9 dry 102

ldkg dry 2O3

us/xg dry 1o2

US/kg d.y 1O2pdks dry 102pg/l(gdry 1o2

USI(S dry 1O2

UgL/kg dry 102

US/kS dry 1O2

udkgdry 1o2

us/rs dry 102pg/l(g dry 1O2

ldkgdry 102

ldko dry 1O2

$srkgdry 1OzpSJkAey 1020

ldkg dry 102

lSftsdry 102

udks d.y r02pdkgdry 1020pdks dry 10m

ugkgdry 1o2

26-Mar-07 26-t\rer{7 7(X]1584 BD

Volatile Orqanic Comoounds R05Prepared by method SW846 5030 Soil (high level)7G1$1 1.1,2-Tddrlorohifluoroethan€(FreoBRL67$+1 Ac€ione BRL107-13-1 Acrylonitrite BRL7143.2 Benzene ARl-100-86-1 Bromobstzene BRL7+97-5 Brcmochlorornethane BRL?'27-4 Brcmodichltrofiethane BRL75-2rz Bromotorm BRL74$3-9 Bomomethane BRL7&9+3 2.Butanone (MEK) BRL10+5i€ rFButylb€nzen€ BRL13t9eA sec.But!'ibenzen€ 8RL98-oe6 tert-BuMbonzen€ BRL75.1s-o Carbon disulnde BRL5&245 Carbon tebachlorid€ BRL10&907 Chlorobenzene BRL7fl1G3 CfiloroetMne BRL6756.3 Chloroform BRL74€7-3 Otlorom€thane BRL95-49{ z-Chloroiduene BRL10fi34 +Chlorotolu€ne BRL9&12{ 1,2€ibomo-3-dtloropropan€ BRL1?1-.1&1 Dibrornoohlorom€thane BRL1os$a 1,2-Dibromoehan6 (EDB) BRL7445.3 Dibromornelhane BRL95r5Gl i,2-Dichlorobenzene BRL541-73r t,3-Dichlorobenzene BRL1()6-45-7 |,4-Dichiorcbenzene BRLfar714 Dichlorodiouoromethane(Freon12)BRL75-34-3 l,l-Dicfiloroethano 8RLt07.06-2 1,2-Oicruo.oethane BRL?5-3+4 1,'t-Dichloroethene BRLi56-ss-2 crs-l:-Dichloroeth€ne BRL15{i€0-5 t?ns-1,2-Dicilorceth€ne BRL78{7'5 i,2-Dichlorcpropone BRL142-20-9 t,+Diailo.op.opade BRLs94-20.7 z,2-Dichloropmpane BRLs63-s8€ l,l{)icHoroprop€n€ BRL10061-01.5 cis-1,3-DichloropiJpene BRLl006142ibans-1,3-Oichtoropropene 8RLi0(}4l4 Ethyib€fEene BRL87{e3 tbxachb(oblt€dGn€ BRL591-7€{ 2-Hexanon€ (tlBK) BRL96-82+ lsopmpylbenzene gRL

S37{ 4-lsopropy'totuene BRL!634{4-1 Msthyl tert-tutyle$er BRLlostG1 +M€thyl-2-pentanon6(M|BK) BRL75{$2 tsl€dryl€no drloide BRL

505050

5050

5050

5050505050505050

50505050

5t)fl)50505050

5050

505050

50

505050505050

50505050

SW 846 S2608 27-[,lar{7 28+rar47 7031642 mer

91-203 i,bphthalene

Page 38 of | 65

Thii taboradq report is ,td volu ',irhotd u atrtodzsl sigt oure oa tk cot r pzge

' Repo.table Dercction Limit BRL = Bolow R€porti[g LiE r

Page 241: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationM8F-24 2'-4,

sA5964l-08

Client Proiect #301_88

MatrixSoil

Received

22-Mar-01Collection Date/Time

2l-Mar-O7 00:00

cAS No. Anahtc(s) Ft4S rRDL Dilarion Metj'od nel( Pryprren Ansbaed Balch Aralt't

Vohtile Orgrnlc Compounds

Volatile Orqanic ComooundsPrepared by melhod SW846 5030 Soit (high tevet)103{5.1 n-Propylb€nzene100-425 Styrcne63(!206 1,1,1,2_T€trachtoroethane79-3{_s 1 , 1 ,2,2-Totrachtoroethane127184 Tetrachloroethene10&84-3 Tolu€ne87515 1,2,3_Trichtorobenzene120'42-1 1,2,+JidtlorcbetEene71554 1 , t,.t _Trichtoroethane

794u5 I,1,2-Trichloroethane7941-6 Trichtofoethene

96,184 1,2,3_Tichtorcpropsne95€3'6 1,2,+TinrlethylLrenzEne10867-8 l,3,tTimethytbenzene75{r+ Vinylchloride133O-2C7 m,p_Xylene95-47S o-Xylene10s-9€-s Tetrahydrofuran@J-29-I Ethylether994{54 Tert-amytmethylether637-92 3 E$ryt tert-butyl ether10&20-3 Di-isopropytether7s-65-0 Te.t-gutanot/butylalcohol123-91-1 .l,4,Dioxane

Sufiogate recovedes:46A00-4 +Btomotluorobenzene

2037-26-s Toluene-da

1 t 060-014 1, 2Oic hlo@ethane-d4

1e6&5i-r Dibrcmofluorcmethane

Eft.rct ble P€troleum Hrdrocrrbons

Extractable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

€006{14 casoline6847e3O-2 Fuetoit#26447G31,3 FuetOit#464s53i04 Fuetoit#6M0980000q Motof oilJ00r00000 Aviatjon Fuel

Unidentified

Other Oil

Totet Pehoteum Hydrocarbons

C9-C36 Aliphatic tldrocarbons

Sdrogale rcco|€les;33eG$-2 l-Chloloocladecane

S€mivol{rik Orgrnic Compound$ by cC

Orqanochlorine Pesticides SW846 8081A

Preparcd by method SW846 3515A

309{G? Atdrin

BRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRL

BRLERLBRLSRLBRLBRLBRL8RLBRLBRLBRLBRLBRL

1021069697

BRL8RLBRL

BRLBRLBRL

Calculated as262262

125

Ig/tS drypdkS drypEr$ dry

Pq(g dry

!g/kg drypq/kg dry

!g/kg dry

)J9tK9 dry

!g/kg dry

lgkg drypdkg drypdkg dry

ugks drypdkg dry

!S/kq dry

us/ks dry

!g/kg dry

tiSi l(9 dry

9dkg dry

rrg/rQ dry

t g/rq d.ypg/kg drypdkg drypg/kg drypg/kg dry

102102102102

102102102102102't02

102102102102

102102203102102010210210210210202030

50

505050

5050505050

5050505030

5050505050505050505050

SW 846 82608 27-MBt47 2A-Mat47 7031642 mal

75€9_4 Trichlorotluoromethane(Freon.ll) BRL

70-130%7U130%70-130 %70-130%

mgL/kg dry

mgL/kg dry

mdkg dry

mdr€ dry

mgks dry

mgL/kg dry

mS/l€ dry

mg/kg dry

mgr'kg dry

mgr'kg dry

50.2

fi.2

f i 2

f i 2

502

fi.2

f i 2

50.2

50.2

50.2

+CT ETPH 27-Mat47 29.MarO7 7031590 DS

1G140 %

BRL pS/kg dry SW846 8081A 26+Iia(47 28-'./|,ar47 7031516 TG

Thit laborutory Epod k na. told wirhotr an authori.ad ignarare oa the cover page

r Reponabl€ Deta:iion Lim|t BRL: Below Reporting Limit Page 39 of 165

Page 242: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeotificationM6F-24 2,-4'sA5964l-08

ClientProi€ct #30t-88

MatrixSoil

Collection Date/Time2l-Ma.{7 00:00

Received22-MaF07

CAS No. Aaaltta(s) Floc UEIA .RDL Dihlina Method Retr, Prcpaed A^olfzed AoM ABalys,

S€mivolattle Orgrrlc Compornds by CC

Orqanochlorine Pesticides SW846 80814Prepared by mebod SW8,l6 354543i9-e4{ a_BHC319+5-7 b.BHC319-86{ d_BHC584$9 g-BHC (Undane)57-74-9 Chlotdane72-5,r{ 4,4.-DDD (p,C)72-5$e 4,4'-DOE (p,p.)50-2e-3 4,4'-DDT(p,p')60.57,1 Dieldrin95998{ Endocultan I3:121 345-9 Enclosulfan ll1031474 Enalosulfan SutFdte72-2t)i Endrin7421€34 EndrinAldehydet6.44€ HePtachlor724T5 Mettrorychlori024-s7.3 Heptachlof Epo de8001-3+2 Toxaphene510C-71-9 a-Chlo[dane5566-34-7 g-Chbrdane53494.70-5 Endrin Ketone

Sa/togale recovarrrss.'1038Gu-z 4,1-DB-OctatluotDbiphenyl (542051-2+3 Decachlotobiphenyt (St,Polvchlorinaled Biohenvls bv SW846 8082Prepared by method SW8,l6 35454t267+1r-2 PC81016111O1-n-2 PCB 1221r1141-16-5 rcB i232534€9?1-9 rcB t24212672-2e4 PQB 12481i097{e1 PCB .t254

110S82-5 PCB.t2503732+23-5 PCB 12621110Gi4-4 PCB 1268

Suftogale rEco!./€/res:I o3a6-o+z 4, 4O&OcIdfl @tobipheny' (Sr)ms1.2a3 bcechlotobiphenyt (Sr)

Senivolrt e Oigrrlc Cornpounds by CCMS

BRLgRL

SRL

BRLBRLBRLBRLBRLgRL

BRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL

69101

BRLBRIBRLBRLBRLBRLBRLBRfBRT

501n

BRLBRLBRLBRLARLBRLBRLBRL

Udks dry 8.0r

lSikS dry 8.01

lgrg dry 8.01

UC4(S dry 8.01

ldkS dry 40.0pSftg dry 8.01

rdkgdry 8.01pCftS dry 8.01pgrg dry 7.00

!d19 dry 8.01

ldkg dry 8.01pSI(' dry 8.01

ICitq dry 8.01

t dkg d.y 8.01

ldkg dry 8.01

!g/kg dry 8.0'l

tdkgdry 8.01pS/kS dry 40.0

tJg/kg dry E.Ol

FS/kgdrY 8O1

ldkS dry 8o1

3Gt 50 %3&150 %

pgkS dry 16.0pdkgdry t6-0

US/kS dry 16.0pdks dry 16.0

IgkSdry 16.0pqkg dry 16.0pdkS d.y 16.0

lS,lkS dry 16.0

ttglkedry 16.0

3A-150 %30-150 %

SW846 6m1A 26-[rar47 2&Mer47 7mi516 TG

SW84A 8082 26.|,,,a'4? 28\4ar47 7m1515 SM

SW846 8270C 27-l''a(47 27+nar47 7031592 ir.S

Semlvo|atils Oroanic Comoouods bv SW846 8270CPr€pared by method SW846 3545A&32-9 Ac€nsPhthene20+Fa Ac€naphtfil'l€ne€453-3 Adtin€12G12-7 Anth6csn€i912-24-9 Abazine10:l-3$3 AzobeozeneDlphenyldiazines2{7-5 Benzftlin€5O.5t3 Benzo (a) antftracene

pdksdry 374

Fgikg d.y 374pgkS dry 374

ldkgdry 374

udlqdry x74

ldks dry x74

t S/kg dry 374

USnlgdry 374

?hh laboruro,f ftport is naa yalid uAhaul sa atthadtad rlgddu.. od lhe cav6 poge.

'Reportable Detetion Limit BRL = B€low ReponidC Limit Page 40 of l6J

Page 243: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMtF-24 2,-4'

sA5964l-08

Clielt Proiect #l 0 r -88

MatrixSoil

Collection Dale/Time2l-Mar-07 00:00

Received22-Mar07

CAS No- Analrte(s) FIag rRDL Dilutiort lwethod Rcl Prcpared Analwed Bateh A,alyst

Semivolstile Organic Conpolnds by GCMS

Somivolatile Oroanic Comoounds bv SWB46 8270CPrepar€d by method SW846 35454

50-32-8 Benzo (a) pyrene

20s,99,2 Benzo (b) {luoEnlhene191 2a-2 Benzo (g,h,i)peMene

207,06 9 Benzo (k) fluoranthene6535-0 Benzoic acid10051-0 Benzytetcohol111,91-1 Bis(2_chtoroethory)mebane111-144 Bis{2_chtoro€thyt)eflrer

39638,32,9 Bis(2_chtorotsopropyj)ether117'41'7 Bis(2-ehythexyt)phhatEte101-55-3 4-Bromophenyt phenytether

8548 7 Buty! b€nzyl phthalate86-74-8 C€rbazole5e-50-7 4.Chto.o-3-methytphenol10647,8 +Chloroaniline91-sa7 2-Chloronaphthalene95-s7-8 2.Chlorophenot70os-72-3 4-Chlorophenyl phenyt eth6r218{1-9 Chrysene

53-70-3 Abenzo (a,hl anthlacene132{4€ Dibenzofuran95-5Gl 1,z-Dichlorobenzene

t{r,731 1,}Dichlorobenzene

106.467 1,4-Dichtofobenzene

91-94-1 3,3--Dichlorobenzidine120€3-2 2,4.Dichlofoph€nol845F2 Diehylphthalate131 113 Dimef1yl phthalate

10s7-e 2,4-Oimethytphenolu-r4-2 Din-b'ltylphthalate

534-52-r 4,6-Oinfto-2-methytphenot

sl-28-5 2,4-Dinikophenol

121-14-2 2,4-Dinitrotoluene

60G20-2 2,G-Dinitrotoluene

117-84.0 Di-n-octylphthalale206-444 Fluoranlhene

86-73-7 Fluor€ne

118-741 Hexachlorobenzene

87€8-3 Hexachlorobutadiene

Tr4T4 Hexachlorocyclopentadiene

67-721 Hexachloroelhane

19+3S-5 Indeno (1,2,3-cd) pyrene

90-r2{ 1-Methyl€pha|atene?8-59-1 lsophorone

91-576 2-Methytnaphthat€n€

951+7 2-Methylphenol

10b-j94, 3,4-Me'l.\y'pher)ol105-4{,591-20-3 Naphthalene8a-74-4 2-Nihoanilines9{9-2 }NitrDaniline

SW846 8270C 27-Mat47 27+,/tal.O7 70315S2 M.BBRLBRL

BRL6RLBRL

BRLBRLBRLSRLSRLSRLSRLSRLBRLBRLBRL8RLBRL426BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRL771BRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRL

BRL8RLBRL

!g/kg dry 374

!g/kg dry 374

Ug/kS dry 374pS/kS dry 374

ldkS dry 374

UgkS dry 374

tSftS dry 374

udKg dry 374

!s/ks dry 374psfts dry 374

lgKs dry 374ps/Ks dry 374

usftg dry 374

ldkS dry 374

ldks dry 374

lgftg dry 374

!S/kg dry 374

!g/kg dry 374pS/kS dry 374pdkSdry 374

PdKS dry 374

ldKs dry 374

lSlqdry 374

!S/kg dry 374

!s/ks dry 374

!s/ks dry 374

ldkS dry 374pg/kS dry 374

ldkS dry 374

!S/kS dry 374

tqgdry 374

UdkS dry 374pdkS dry 374pSftg dry 374pSftg dry 374

ljg/rS dry 374

!g/Kg dry 374pSikg dry 374

US/kS dry 374pS/kgdry 374

lgil€dry 374

ug/kg dry 374pgkS dry 374

FykS dry 374

usftS dry 314

LrS/kgdry 374pSLSd,y 374

pS^S dry 374

Udkg dry 374pdks dry 371

Thit litoratury rcporl B t ot ialid wuho4t dn ozlhod?ad signatwe on thc caver Fage.'ReFxtable D€tection Limit BRL = Below Reponing Limit PEg€41 of l6J

Page 244: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiouM8F-r4 2,-4.sA5964l-{}r

Clietrt Proi€ct #301-88

Mat ixSoil

Received22-Mat47

Coll€ctior DalelTime2l-Mr.47 00:00

CAS No. A"E+12(s) f,cscrt FI4S *RDL Dituion Method Retr. Pftpaed Ar,alyud Bdch Aizllsl

Semivol.lil€ Organlc Compo|rtr& by GCMS

Semivolatile Oroanic Cdnoounds bv SW846 8270CP.epared by merhod SW846 35454100{r€ +Nitroanillne98-!F3 NttrobefEen€86-75-5 2-Njtrophenoltoo42.7 +Nitrophenol62-7t9 N-Nitrosodirn€Etytamine621.6,1-7 N-Niiroscdi-rr-propylamine86.30€ N-Nitrosodiphenylarnin€87{65 Peotad oropt|gnol8s41{ Ph€nanlhEne

108-9s.2 Phenol

12s{0{ BnerE1i0.86-i tfidine120{21 1,2,+Trichlorobenzene

9$95-1 2,4,$Trichlooph€nol

88{€F2 2,4,&Trichlorophenot

S.fiogafe €couenbs.'

321a0a z-Ftudobiphenyl

SW846 4270C 27-Mar47 27.to1ar47 703153? M,BSRLBRLBRLARLBRLBRLBRLBRLBRLBRL705BRL8RL8RLBRL

68

0 .115

BRL

4 . t 1

34.9

0_701

44.9

22.O

BRL

67.0

Ugkgdry 1f,0O

!S/kS dry 374

tg/kg dry 374

!el(S dry 15(mydks dry 374

ldkS dry 374

!c/&s dry 374

ldkSdry 374

udlgdry 374

ldkS dry 374

ldkg dry 374pCikgdrv 374pqtg dry 374

lElgdry 374

!S/kS dry 374

3L130 %15-110 %30-130 %15.r10%

m-1n%1'-nO%

ftig/kg dry 0.043{

mqr'kg dry 1.36

mgr'kg dry 2.M

nE/kS dry 0.680

mdkS dry 0.340

nVkS dry 0.680

n€/tg dry 1O2

mg/kg dry 2.O4

mgI 0.02m

nrdl 0.0150

mgil 0.0150

nE,n 0.m25

n'gn 0.0150

mgl 0.mo1t0

mg/l O,015O

rrgrl 0.0150

%

I EPA 200.7

1 '

1 '

l '

1 '

1 sw8rl6 1312rr470A

1 SW€461312/60108

2A-Matr-O7 n+llat47 7031494 RM

2&Msr{7 7031652 YP

2Stlar{7 7ct166l HB

?67-124 2-Fluoropt6nol 551165404 Nihobenzene4s 63116542 2 Phenolds 561718-514 Tefpllenyldl4 77tte7 z,4,fiTtibft/'tophenol 67

Totrl Meti6 by f,PA 6lXXy7000 S€ries Methodt

74394?.6 Merqlry

Totel M€trb by EPA 200 S€ries Methods

7140-U4 Silvel

742{l-38.2 Arsenic

744S393 Baaium

7{4l).4}9 Cadmium

7,trO.47-3 Clromium

743s-9?.1 Le€d

7?82-4+2 Selenium

SW846 7471A 2&Mar-07 28-tuar{7 70314S5 YP

SPLP Mearlr by EPA t3 l2 & 60fiy?000 sed.s M€tiods

SPLP Exbacton Co,ndetod

z!r.o-2?-1 situer BRL

7!lo-3+2 AFenic BRL

7,t40-3+3 Barium 0.0300

74a04$9 c€dmium BRL

7t140.17-3 Chrcmium SRL

743$97€ Merdrry BRL

74S-92.r Le€d BRL

7782-4+2 Selenium BRL

G€||eid Chembtry P|r.mcter!

I 5r,/\/8161312 2SMEr{? 2GMar-07 7031560 AD

I Sl/V8461312/60108 2&Mrr.07 28-lrer-07 7031651 HB

1 '

1 '

1 "

'1 SM2540 G Mod. 24-l'iar47 24,llne'-07 7031470 OP% Solids

Page 42 of t65

TNlt labonlory rqod * aot valid n'Lhout oE aartodzod signauft od rte aover pago-

* Reponsble D€tectioo Limir BRL = Below Rcporring Limit

Page 245: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-25 2,-4'sA59641-09

Client Proiect #l 0 l - 88

MatrixSoil

Collection Date/Time2l-Mar-07 00:00

Receivcd22-Mar-07

CAS No- Anallte(s) Units *RDL Dilution Merhod Rel Ptepaftd Aruryzed Botch ,4mlpt

Volatile Organlc Compounds

vOC Extraction

pg/kg dry 6.3

Pgkg dry 127

US/kS dry 6.3

USAS dry 6.3

!g/kg dry 6.3

ldkS dry 6.3

Udkg dry 6.3

tiS^q dry 6.3

lEkS dry 12.1

ldkS dry 63.4

!g/kg dry 6.3ps/kg dry 6 3

liS/kg dry 6.3pgkS dry 31.1pg/kS dry 6.3pg/kg dry 6.3

LrgkS dry 12.1pdkS dry 6.3pg&S dry 12.7

lSftS dry 6.3pqkS dry 6.3

l.rdkg dry 12.7

ldkS dry 6 3pdkS dry 6.3

!g/kg dry 6 3

Lig/kg dry 6 3

ldks dry 6.3

ldks d.y 6.3

ldks dry 12.7

lgkg dry 6.3

UdkS dry 6.3pgkg dry 6.3

Pgkg dry 6.3

lgkS dry 6.3

PdkSdry 6.3

ldkS dry 6.3

lgkS dry 6.3pdkg dry 6.3pqkS dry 6.3

lgks dry 6.3pdlqd.y 6.3

!S&S dry 6.3pg'l(gdry 63.4pdkS dry 6.3pdks dry 6.3pdks dry 6-3pdksdty 634

ldkS dry 63.4

!S/kS dry 6.3

26-Mar-07 m.tlar{7 7031584 BDField extractedVolatile Orqanic Comrounds

Prepared by melhod SW846 5030A Soit (tow tevet)76-13-1 1,1,2-Trichtorotrinuoroethane (Freo€RL6744-1 Acetone aRL107-13,1 Acrylonitdte BRL714+2 Benzene BRL10&€e1 Brodrobenzen€ BRL74-97-5 Bromochloromethane BRL15-274 Bromodichtoromethane BRL75-212 Eromoform BRL7.1€3-9 Bromomethane BRL7s-e!3 2-Butanone (MEK) BRL104-514 n-Bltylbenzene BRL13t98-8 sec-Butytbenzen€ BRL9846+ tert-Butylbenzene BRL75-15-0 Carbon disulfide BRL56-23-5 Carbon tetrachloride BRL108-90-7 Chlorobenzene BRL7540-3 Chtoroethane BRL67$6-3 Chloroform aRL7447-3 Chlororhethane aRL9549-8 2-Chtorototu€ne BRL106-434 +Chtorotdu€ne BRL96-12J 1,2-Dibomo-3_chlorcpropane BRL124-1€-1 Dibromochloromethene BRL106 934 1,2-Dibromoethane (EDB) BRL7,1-9t3 DbromorDethane BRL9s'sG1 I,2-Dichtorobenzene BRL541-73-1 l,3-Dichlorobenzene BRL106-16-7 l,4-Dichtofobenzene BRL75 7 1-e Dichlorodinuoromethane (Freoni2) BRL7s-34 3 l,t-Dichtofoethane BRL107-06.2 l,2.Dichtofoethane BRL7s-35-4 1,1-Oichto.o€thene BRL156-59-2 cis-i,2-Dichloroettiene BRL15ffi0'5 trans-1,2-Dichloroethene BRL70{7-5 1,2-Dichloropropane BRL142-28€ l,lDichloropropane BRf5942G7 2,2-Dichlorcpropan€ BRL56$50{ 1,l-Dichloroprop€n€ BRL100€1{1-s cis.t,3-Dichloropmpene BRL10061{25fans.l,}Dichlorcpropene BRL10c.114 Ethylbenzene BRL07€8-3 Hexachlorobutadiene BRL5e1,70{ z-H€xanone ([,,!BK) BRL9442{ lsopropylbenzene BRL9947€ +lsopropyltoluene BRL163.1{.1-1 Methyllod-buty'ethor SRL1D+t0-1 4-Metllyt-2-pentanon€(M|BK) ARL7S0S2 Methylene chloride BRL

I

1

1

1

1

1

1

1

1

1

I

I

1

1

1

1

1

I

1

1

1

1

1

I

I

1

I

1

1

1

1

1

1

1

1

1

1

1

1

1

I

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t

I'|

SW 846 82600 27-Mat47 2a-Mar07 7031658 RLJ

91-207 Naphthalene

Page 43 of 165

Thi, bbonlory nporl is ^ot vau x,ithou al aatlrodzed signatarc on the cot er page .

{ Reporirble l)etection Limit BRL = Bclow R€poning Limir

Page 246: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMEF-25 2'-4'sA5964l-09

Clieflt Proiect #l0l-88

MatrixSoil

Colleclion Date/Time2 I -Mar-07 00:00

Received22-Mar-Oj

CAS No- Amlyte(s) FIzg 'RDL Dilutio.' Method Retr. Prcporcd AEaIwn Barh Andllst

Volrtile O.grnic Compoundt

Volatile Oroanic ComgoundsPr€pared by method SW846 50354 Soil (low bvet)

7569-4 Trichloronuoromehane (Fr€on ll) BRL

103-61 n-Prcpylbenzene10tl-42-5 Styrene630-20{ '1, | ,1,2-Totracl toro€thane

79-34-5 1,1,2,2-Totrachloro€lhane

12H8-1 Tehadlloroetlrene

108i83 Toluene

87{1{ 1,2,}Tridllorobenz€ne

12G82-l 1,2,4-Tdd o@benz€ne71{5{ 1,1,l-Trichloro€hane

79{ l }51, I ,2-Tr i* l toroethane

79{1S Tdchlo.o€th€ne

96-18-4 1.2,$Trictllorcpropan6

9gt€3{ ,|,2,4-Tdmethylbenzene

1085/{ 1,3,5-Trimethylbenzen675{r-4 Vinylchlo.ide1330-?07 m,p-Xyiene9547{ +Xylene109.!19-9 Tetahydrcfuran

6G297 Ethyl ethef9s4{s€ Tert-amy'methyletfEr637-12{ Ethy t6rt+utr.t ether108-20'3 Di.isopropyt€ther75{5-0 Tert€obnol/ butyl alcohol123-91 -1 'l

,4.{)ioxan€

Sutugate rccoldrias:46040-4 +B@ntofluotobenzene

m37-26-S Toluene4S

1 7 060474 1,2-Dichlotoethane44

186&5?7 Nbrcmofluoronelhene

Exlrrctrble Peftoleum Hyd.oc$bons

Ext.ac'table Total Petroleum Hvdrocarbons

Pr€pa.ed by method SW846 35508

800661-9 Gasoline6&tF30-2 Fuel Oil #2684743r-3 FuelOitt 4

6e5s90{}a Fud Oil #5M6doo{D0 Moto!. OlJ0O10O00O Aviation Fu€{

Unidentifed

O{h€. Oil

Total P€0oleurn Hydrocadons

C!€36 Aliphatic Hydrocarbons

Sunogts{e a9co!4er*es.'33E633-2 l-Chloroochdecane

Senlvolotil€ Orgulc Compoutrd! by CC

Orqanoctrlo.ine Pesticides SW846 8081A

P.epar€d by rnethod SW846 3545A

3O9-O0-2 Atdrio

SW 8{6 S260S 27-[,tar47 28{r,1a.47 Zm165a RllBRLBRLBRLBRLBRL8RLBRI-BRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLgRL

88

97

BRLBRLBRLBRLCalculat€d asBRL206BRL206206

t0()

USASd,y 63pgr(g d.y 6.3

ldkSdry 63

ldkS dry 6.3

!s/kS dry 6.3pSn(S dry 6.3pSI€dry 6.3

US/tg d.y 6 3pdks dry 6.3pdks dry 6.3

UgI(S dry 6.3

t'Stkgdty 6.3

tlgJksdry 6.3pgrsdry 6.3

ldks dry 6,3prytS dry 6.3

!g/xS dry 12.7

Lrdkg dry 6.3

UgJkAdry 63.4ydkS dry 6.3

$ikg dry 6.3

!S/kS d.y 6-3pdksdry 6.3

ldksdry 63.4

|]g/kS dry 12f

7L130 %7G130 %70-130 %70-130 %

rEL/kg dry 34,4mg/l!gdry 34.4mdkg dry Y.4nE/kq d.y U.4rvlg dry u.4ndkS dry 34.4mdkS dry 34.4mdfQ dry 34.4mg/kg dry 34.4rng/kS dry 34.4

'40-140 %

+cT ETPH 2t4 at47 29+nt47 703159/)

ngtg dry SW8,$ 8m1A 2&lle.O7 28-l!lar47 7031516 TG

Tttit lshoaldrf ,epod is not vU without zi althodu.I slgrratare ol lhc cover pag.-

' RQortabl€ Det€ctiotr Limit BRL = Below Repqiing Limir Page ,14 of | 65

Page 247: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samplo IdentificationMEF-25 2',-4'

sA5964l-09

Clent Proiect #301 -88

MatrixSoil

Received22-Mar-07

Collection Date/Time2l-Mar-07 00:00

CAS No, Anabre$) Resalt Fl"s Units *RDL Dilution Method Retr. Prcparcd Anaryzed Bakh AnaIJst

Semivolrtile Orgatric Compourd3 by CC

Orqanochlorino Peslicides SW846 8081A

Prepared by rn€lhod SW846 3545A

319-84{ a-BHC319{s-7 b-BHC31s6-6 d-BHC5s4+e g-8HC (Lindane)

5J-749 Chlordane72-s-a 4,4'.DDD (p,p')

72-55-e 4,4,.DDE(p,p,)

50-2s-3 4,4,-DDT(p,p.)€0-57-T Dielddn959-96{ Endosulfan I33213-65-9 Endosulfan ll1031{7,8 Endosulfan sulfate72-2O-A Endrin7421-93-4 EndrinAtdehyde76-44.8 Heptachlorr243-E Methorychtor1024-57-3 tleptachlor Epoxide8001-35-2 Toxaphene5103-71-9 a-Chlordane556€-34-7 g.Chlo.dane

53494-70-5 Endfin Ketone

Surogalg rccovedes:1N8Ge+2 4,+DB-Octafl uorobiphenyl (54

N51-2+3 Decachlorobiphenyl (St)

Polvchlorinated Biohenvls bv SW846 8082

Prepared by melhod SW846 3545A

12674 11 2 PCB 10t611to+28-2 PCB 122111141-16-s PCB 12325346s21-s PCB 124212672-?9{' PCB 12481r0s75e-1 PCB 1254110€6{2-5 PCB 126037324-23-5 PCB 12162ir100-14-4 PCB .1268

Sunogale Ecowries:fl 38 e, 84 -2 4, 4 - D &Oc I afl Llo rob i p he n yt ( Si

205 t-2+3 Decachlo.o b ip hen yl (Si

Semlvotalile Organic C0mpounds by CCMS

BRLBRLBRL8RLBRLBRLBRLARLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRL8RL

6876

8RLBRLBRLBRLBRLBRL25.98RLBRL

4570

8RLBRLBRL597BRLBRLBRL946

!g/kg dry 6.65

tig/kg dry 6 65pg/kg dry 6.65

!g/kg dry 6.65

!g/kS dry 33.3

!g/kg dry 6.65

ldkS dry 6.65pg/kS dry 6.65pgftS dry 6.65pdkg dry 6.65pS4<S dry 6.65pSftS dry 6 65

!g|4(g dry 6 65pSftS dry 6.65pS/kS dry 6.65pg/kg dry 6.65pglLg dry 6.65

!g/kg dry 33.3

!g/kg dry 6.65

!g/kg dry 6-65

!q/kg dry 6.65

30-15, %m,t50 %

pg/kg dry 13 3

!g/kg dry 13 3pg/kg dry 13 3

ldkS dry '13 3

!g/kg dry 13-3

!g/kg dry 13 3

!g/kg dry 13 3

ldkS dry 13 3

!q/kg dry l3-3

n-|50 %30-150%

iJdkgdry 4?7

pglgdry 427

pdkS dry 42f

UdkS dry 427

UgkS dry 127

UgkS dry 427

IdkS dry 427

Ug/kS dry 427

1

1'|

i

I

l

I

1

1

I

I

I

1

l

1

1

1

1

1

1

1

SW846 8081A 26-MaF07 28{,lar-07 7031516 TG

SW846 8082 2€-Mar47 28jv1ar-07 7031515 SM

Semivolatile Orqanic Comoounds bv SW846 8270CPrepared by method SW846 3545A83-32-9 Acenaphthene20FS€-€ Acenaphthylene62-s3-3 Anitine12e12-7 Anthrac€ne1912.2+9 At?ine103-33'3 Azobenzene/Diphenyldiazine92{7-5 Benzjdjoe56-55-3 B€nuo (a) anthrac€ne

SW846 8270C 274lar17 27+,/ta?07 7031592 M.B

Thk bboratory npoq is not vaIA dfiotl an d..thorizli slgaatarc o^ the cwer pqe .

' Reportable Detection Limit BRL = B€low Reporting Limit Page 45 of 165

Page 248: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdadtificationM8F-25 2'{,s45964149

Clietrt Proje€l #301-88

Collection Date./Time2l-Mar47 00:00

MatrixSoil

Received22-MaF01

CAS Na AM+k(s) Flig *RDL Dltution LLthod Ret Ptepared Anzlraetr Batch Anzfi*

Semlvoletile Org.dc Compounds by CCMS

S€mivolalilo Oaqanic Comlounds bv SW846 8270C

Prepared by rnethod SW846 3tl5A

50-32+ Bonzo (a) pyrene2otss'2 B€nzo (b) fiuorandreoeis1-242 Bcnzo (g,h,D peryle|]e20ru&9 Benzo (k) nuorsnthene65€fi Benzoic acjd10G51{ Benzy'l alcohol111-el-r Bis(2rhlom€thory)methane111-444 Bis(2{hloro€thyt)efier3963S32-s Bis(2dltoroisopfopyl)eheri17{1-7 Bis(2-ehyllr€xyt)phttEtate101-5+3 +Bromophenylphenylefiea85{s7 Auty,l b€nzyl phthatatie86-74{ Csfbazole5950-7 rlchbo-3-methylph€flol1&7{ 4-Chlo|oanilino91i$7 2-Chtoronaphhalen€9t57{ 2-Chlorophenol2005.72-3 +Chlorophenyl D,tletrlyl eiher218-th-9 Chrys€n€53-70-3 Dibenzo (a,h) snthracene1326+9 Dibenzofurei95-5G1 l,z-Dichlorobenzene541-73-1 1,3-Oichlorcbefizene10Sa&7 1,4-Dicidoobenzen€9l€{-1 3,3lDichlorobenzidine12G83'2 2,4-Dichlo1.ophenol84{62 Di€tlyl phttEtater31r1-3 Dimeflryl pht€tate105i7-9 2!4-Dimefiy,tphenolu-74-2 Di-n-butylphthalate$a-52r 4,6-Oinito-2-methylphefiols1 .2$s 2+Oinitrophondt2i-14-2 2,+Oinilro{oluene606.4)-2 2.GDinitrototuene117{4{ Di{.oclylphtnatatea)8-14-O FluorEnt1enefr-7r7 Fluorene1i&74_l Hexadrlorcbenzen€876€_3 Hexac-hlorobutradrenen174 Hexadiorocydopsntadiene67.72-1 HexeChloroefEne193-3$5 Indeno (1.2,3-cd) pyrene9012{ l-ilethy'naphthal€ne7&5$1 lsophoron€91'57{ 2-Metrylnaphoratenee5-4e7 2-trtethylph€nol10&3s-4, 3,4-tet|ylphonol10€-zK'591-zl3 Naphb\Elene

E-7,4 2-Nitroaniline

99{92 }Niuoanilin€

Sw846 0270C 27llt?{47 27-Mat-07 7031592 M.B9829804838mBRLBRLBRLBRLBRL8RLBRLBRLBRLBRL8RLBRL

BRLBRL't, t80BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL2,3fiBRLBRLBRLBRLBRL433BRLBRLBRLBRLBRL

BRLSRLBRL

VglxSdry 427

Pslts d.y 427pEtgdry 427

lg,fl€ dry 427pg4qdry 427

Udl€ dry 427

UgkSdry 427pS/kS dry 427pdks dry 427pS/kSdry 427pS4(S dry 427pdrs dry 427pdrgdry 427pdtsdry 427

UdkS dry 427

uglksdry 427pdks dry 127pdrgdry 12]

lgikSdry 427pdl(lgdry 427pdkg dry 427pdkSdry 427

Ugn(S dry 427

!S/kS dry 427

ttdV,Sdry 427

UdkS dry 127

rrykg dry 41

l4/kS dry 427

u/rSdry 427pdks dry 427pdks dry 427

ldko dry 427

ldkS dry 42r

!S/lq dry 427

US/kS dry 127psfts dry 127

lJg/ks dry 427

ldks dry 427

rdts d.y 427pdko dry 427

ldkgdry 427

!Sn(S dry 427

ldkS dry 427

ISftg dry 127

ldlg dry 127

lgl(g dry 427

Idkgdry 427

ydkg d.y 427pdks dry 427

rdkgdry 427

This ,4.hralory rcpad h not eaIU x,irhoat tE aantoriet dgao&,rc on the cote. pqE-

' Reportable Det€ction Umit 8RI = Below R€porti.g Limit Page 46 of 165

Page 249: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatia.nM8F.2s 2'-4,sA5964 | -09

Client Proiect #301-88

MatrixSoil

Received

22-Mar-01ColLection Date/Time

2l-Mar-07 00:00

CAS No. Arra4te(s) Resun Ftzg Unia +RDL Dilation Merhod Rel. Prcpand Anaqed Batch AMb\t

S€mivolatile Orgsnic Compourds by GCMS

Semivolatile Oroanic Comoounds bv SW846 B27OCPrepared by method SW846 3545A

100-01-6 4-Nilroaniline98-95,3 Nikobenzene

88-75-5 2-Nitrcphenol10G02-7 4-Nitrophenol62-75-9 N-NitrosodiaEthylamine621+-7 N.Nitro6odi-n-propylamine06-30-6 N-Nitrosodiphehylamine07-€G5 Penlachtorophenol8541-8 Phenanlhrene10&9t2 Phenol1?9-00-0 P,rene11G86-1 Pyridine12G€2r 1,2,4-Trichtorobenzene95-95-4 2,4,5-Tdchlorophenol88-06-2 2,4,6-Trichlorophenol

Sunogale rccovedes:3?1'60-o 2-Fluorohiphenyl

36/-124 2-Fluorophenol

SW846 S270C 27-Mat47 27-Mat47 7031592 M.BBRLBRLBRLBRLBRLBRLBRLBRL942

BRL2,360BRLBRLARLARL

6761

o.747

BRL

10.7

1 M

3.47

12.4

247

BRL

lSikS dry 1710

rlglkg dry 427pg/kg dry 427

!S/kS dry 1710pg/kg dry 427

ldks dry 427pdkS dry 427

lSftSdry 427

!g/kg dry 427

!g/kg d.y 427pdxgdry 427pgkg dry 427

lrg/Kg dry 427

USIkS dry 427

ldkS dry 427

30"130%15^110 %30-130 0/o

1U t10 %301m %1u l10 %

mS!4q dry 0-0352

rnS/kS dry 1.04

rnSikg dry 1.56

mg/kg dry 0 518

mg/kg dry 0.259

mdkS dry 0.518

mg/kg dry 0;l7S

mdksdry 1.56

mg,4 0.0200

nen 0.0150

rng/| 0.0150

mgn 0.0025

nEI 0.0150

nun 0.OO04O

mSI 0.0150

mg/l 0.0150

1

1

1

1,1

,1

1,l

1

1

1

1

1

1

1

4165404 Nitrcbenzene4s 64416542-2 Phenol4S 5617ft.514 Teryhenyl4ll ts118-7e.6 2,4,6-Tdbrcmophend 67

Totrl Merrls by EPA 6000/7000 Series M€thods

743+975 Mercury

Toral Metrh by 8PA 200 S€ries Methods

7440-22-4 Silver

74!0-38 2 AJ.SenaC

7440-39-3 Barjum

744043-9 Ce(lmium

74,10-47-3 Chromium

7439-92-1 Lead

?74249-2 selenium

SW846 74714 28-Mar-07 28-t.,laF07 7031495 YP

EPA 200 / 28-Mar-07 28.Ma.0/ /031494 RM

SPLP Mctels by EPA 1312 & 6000/7000 Srri€s Methods

SPLP Extraction completed

7440-22-4 SiMer BRL

7440,3&2 Arsenic 8RL

7.440,3+3 Eadum 0.0362

7440-43-9 Cadmium BRL

74.10-47-3 Chrcmium BRL

7439-974 Metcury BRL

7439-92-1 Lead 0.0230

7782-49-2 Selenium BRL

G€mr|l Chemistry Parlmet€rt

% Sol ids u.2

1 SW8461312 26-Mar47 2SMar{7 7031560

I SW8461312/60108 28-Mer{7 28]\4ar-077031651

t '

1 "

1 '

1 SWU6131Z747OA ' EMaLD7 7031652

1 SW846131260104 ' 2&Mar.07 7031651

1 '

8D

H B

H B

1 SM254O G Mod. 24.Mar47 24-Mer1f 7A31474 QP

This labontory rcporl k not ralid Hilhou sn oalhoi.el signawe on the coyer poge.

a Reportable Detectioo Limit BRJ- = Below Reporting Limir Pige 47 of t65

Page 250: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 251: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F.26 2-4'sA595l7-06

Clicnt Proiect #30t -88

MatrixSoil

Received

20-Mar-07Collection Date/Time

l9-Mar-07 00:00

CAS No- Aao+t4s) Floc *RDL Dilation MetAod Retr. Prepted Analyzed Batch Atullsl

Volatile Orgrtric Compounds

VOC Extraction

US/kS dry 7.6

!g/kg dry 152

us/kg dry 7.6pfudry 7.6ps/ks dry 7.6

trs/ks dry 7.6ps/ks dry 7.6

!s/ko dry 7.6

!g/kg dry 15.2

!s/ks dry 74.2

PqxSdry 7-6

!g/kS dry 7-6pgkg dry 7.6

sdkS dry 38.1

US/kS dry 7.6

us/ks dry 7 6

rcAS dry 15.2pg,tkS dry 7.6

UdkS dry 15.2

[dkS dry 7.6

IS/kS dry 7 6

!S/kg dry 15.2

ldkS dry 7.6

FS/kS dry 7 6

ttgtkSdry 7-6

ts/ks dry 7 6

tS/kS dry 7.6

UdkS dry 7.6pg/kg dry 15.2

IS/kg dry 7.6pS/kS dry 7.6

f.rglkg dry 7.6

t4/kg dry 7.6

trg/kg dry 7 6

trg/kg dry 7-6

!g/kg dry 7 6

ldkS dry 7-a

FS/kS dry 7-6

lS/kS dry 7.6

!S/kS dry 7-6

!g/kg dry 1.6

!S/tS dry 1.6

liS/kg dry 16 2

trSlqdry 7.6

ldkS dry 7.6

lgkS dry 7.6pqkS dry 76.2

Fg (g dry 76.2pg4qdry 7.6

21-Ma.-O7 21-MarD7 7031261 8DField extract€dVolalile Oroanic Comoounds

Prepared by method SW846 50354 Soit (tow tevet)

76 111 1,1,z-Trichlorotriiuoroethane (Fr€o8RL674+1 Acetone 8RL107-13,1 Acr-t{onitdle aRLf11r2 Benzene BRL100-86-1 Bromobenzene 8RL74,97-5 Bromochloromethan€ aRLT5-274 Bromodichlorcmethane BRL75-212 Bromoform BRL71419 Bromomethane BRL7e-$,3 2-Buhnone (MEK) BRL10+514 n8utylben?ene 8RL13+98{ seeButylbenzene BRL9A-06,6 tert-Butylbenzene BRL75,15'0 Carbon disulfide BRL56.23,5 Carbon tetrachloride BRL10&90-7 Chtofobenzene BRL75{0-3 Chloroethane BRL67{6"x Ch/orofom BRL74-47-3 Chloromethane BRL95-4!l-8 2-Chlorotoluene SRL10H3-4 4-Chloroioluene BRL9€'12_8 1,2-Dibfomo-3rhloropropane 8RL12qS-1 Dibromochloaomethane BRL106-93-4 1,2-Dibromoethane(EDB) BRL74-913 Dibfomomethane BRL95 so,r 1.Z-Dichlorobenzene BRL541 731 1,3-Dichlorobenzene BRL106,46-7 1,4-Dichtorob€nzene BRL15.71-8 Dichlorodiiuorcmethane(Freon12)BRL75-34 3 l,l-Dichloroethane BRL107-06-2 1,2_Dichloro€thane BRL75-s5-4 l,l.Oichtoroeihene BRL1s+s9 2 cis- 1 ,2_Dichtorcedrene BRLlsffio-s taans-1,2-Dichloroethene BRL7a€7-s 'l,2.Oichto.opropane BRL142-28-9 l,3-Dichlorcpropane BRL594-20-7 2.2-Dichtoroprcp€ne BRLr,615€5 .1,1-Oachtoropiop6ne SRL10061111-5 cis-1.!0rchtoropropene BRL10(}6142€ trans- 1 ,3_Oichtoropropene BRL1{n-41-4 Ethytbehzen€ BRL87{&3 Hexachlorobutradiene BRL5e1.784 z-Hexanone (MBK) BRL9a{2€ lsopropy'benzene BRL99€7{ +lsoprapyholuene 8RL1634{4-4 Melhyltert-butytether 8RL10&10-1 4-Methy'i-2,penlanone(MIBK) BRL75-0s2 Methytene chtodde BRL

SW E46 82608 22-MarOI 23-Ma.-07 7031335 RLJ

91-201 Naphthalene

Prge 27 ofl24

This laborutory repo4 is nol ualii Nllhod aa a ho.lzed s@au!rc on tfu cover ptge.

' R?dta)le Dete{tion Limit BRL = Below Replrrin8 Limir

Page 252: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sa8|Dle IdeltificationMAF-16 24'sA5951746

Clied Proiect #301-88

MafixSoil

Collection Dat€/TimeI 9-Mar{7 00:00

Received2GMar-07

CAS No- Adabte(s) Reast Flog Uai6 *RDL Diladoa Llethod Rcl. PEparcd ,ltulfzci Bqlch Ad4lfsl

Vohaile Orgrnic Compoudr

Volalile Omanic ComooundsPrepared by method SW8il6 50354 Sdl (low level)10+65-l n-Propy'lbenzene BRL1qr-42-5 Styrene BRIdrG20€ '1,t,1,2-T€trachloro€thane BRL7+34.s 1,I ,2,2,Tetrachlorffthane BRL127-18-l T€lrachloroethene BRL10&84€ Toluene BRL07{14 !,2.}Tridrtorobenzen€ BRL12G82n i,2,+Trichlorobonzene BRI7i{5-6 1,1,1-Tri{*llorcethans BRL79{G5 1,1,2-Trichloroethane BRL79-01i Trichloroethene BRL75{9-4 Trichlorofiuoromethane (Freon 11) BRLs+1e-j 1,2,&Tri€hlorooropane BRL95-634 1,2,+Trimethylbenzene BRL108-67{ 1.3,5-Trimeh},lbonzene 8RLf5414 Mnyl cikrider330-2{L7 m,p-Xylen€95-47-0 G.Xylenet0$999 T€hahydrofu€n*29.7 Ed1yt ettler994-oS Tert-€nryl mothy'l elher637s2-3 Edlyltert+ulylefllerr0e20.3 Di-isopfopyleth€r7$6+0 Tert-Butanot / but/l alcoholr2+9u 1,+Dioxene

Su,firogale rEcorrsnes:4tt04o2t 4lkomofluotubenzenee37-2A-5 Toluene4St/o6o474 r,2alchloroelhane441868-$-7 Ahrqnonuorcmethane

Ertrrctrble Petroleflm Hydrocrrbons

Extradabl€ Tolal P€troleum Hvdroca.bonsP'epared bV melhod SW846 354548O0O€1€ Gasolin€68a7+.3tl2 Fu€l Oil #26447+31J Fuel Oil #:4685s+oc{ Fu€l Oil #6rnem$oo Motof OlJoolooooo Aviaton Fuel

Unldenttf€dOttFr Oil

BRLBRL8RLBRLBRLBRLBRIBRLBR!BRL

101118102

Sw 846 82608 n4ht47 &Me(47 7031335 RU

+cT ETPH z.-|,tl€,t-O7 m^tat4I 7031284 DS

usrkg dry 7.6pglkgdry 7.6

ldkS dry 7.6

wlkgdry 7.6

tdkg dry 7.6

rdkg dry 7.a

$dkSdry 7.6

USikg dry 7.6pcrks dry 7.6

Ugkg dry 7.6

USI(S dry 7.6

tNu,S dry 7.6pdkq dry 7.a

lSikS dry 7.6p*s drY 7.6

lqkg dry 7.6

Itgkgdty 15.2

ldkg dry 7.6pdkSdry 76.2

ugkSdry 7.6

ldkg dry 7.6

lgtg dry 7.6

ldkg dry 7.6

!S/kS dry 16.2pSI(S dry 152

70-130%7L130 %7G130 %70-130 %

TotalPebdeumHydrocarbons 404C$C36 Aliphatic Hydro@bons rl()4

BRI-BRLER!BRL

BRLBRL4UCalcllat€d as

nvl€ dry t37n€/kg dry 137mg/kgdry 137nEr'kq dry 137rEngd.y 137mgdfo dry 137mdkSffy 137n€/*g dry 137mgikg dry 137nE/kg dry 137

10-140 %

5

5

sal.'ogatc aEoor€rie&_t3€Ga?-2, -Chlorooctdecarg

Scmlvol{tile Orgrtric Compoun& by cCOroanochlorine Peslicldes SW846 8081APrepared by method SW846 355083Oe-0+2 Atdrin trdks dry 7 .Os SW846 e0€1A ?2-Mato7 27-Met47 7mi275 TG

Thit brororary rcpod ls not eeli.l withos! an aud.o;aed signarw on the colv 4rye.. Reportnbb f,retection Limit BRI- = B€low Reporting Lnnit PryEzA ot 124

Page 253: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple IdentificationM8F-26 24'sAs95l7-06

Client Proiect #301-88

MaEixSoil

Collection Date,Tirnel9-Mar-07 00:00

Received

Z0-Ma(0'7

CAS No. Anabtz(s) Fl"S Unils *RDL Dila.aon Method Ref Prcpored Anauzed Barch AnaUst

Semivolrttle Organic Compoutrds by cC

Oroanochlonhe Pestrbides SW846 SOglAPrepared by merhod SW846 35508

319€a{ a-BHC

31$85-7 b-BHC319{6{ d-BHCs8-€se g!8HC (Undane)

5T-74-9 Chlordanerz-*a 4,4-DDD (p,C)72-5te 4,4-DDE (p,p')50 2+3 4,4-DDT (p,p.)60.s7,1 Oielddn95+98-8 Endosulbn I33213.6s-9 Endosuthfl ll1031-07-8 EndosulfansutfateI2-2O-A Endrin7421-eH EndrinAjdehyde76-44-8 Heptachtor124+5 Methoxychlor10?4-57-3 Heptachlof Epoxide8001-35-2 Toxaphene5103-71,9 a{hlordane5566,34-7 g-Cl o.dane53494-70-5 Endrin Ketone

Sufiogale rccoveies:10i8$8+2 44-DB-Octafluorobiphenyt (St)

2051 -2+i Decachlotubiphenyl (Sr)

Polvchlo.inated Biohenvls bv SW846 BOB2Prepared by method SW846 35508

1267411,2 PCB 101611to+28-2 PCB 1221ir141-1c5 PC8 12325346+21-s PC8 124212672-m4 PCB 124811097{S1 PCB 1254110€tr2'5 PCB 1 2603f32+23-5 PCB 12621110G144 PCB 1268

Suaogale rBcov€n'esj103aea4-2 4,+DB-Octafluorobiphenyt (St)

N51-24-3 Decachlotobiphenyt (St)

S€mlvolrtile Orgsnic Compounds by c{MS

BRL

BRLBRLARLBRLBRLBRLBRLBRL

8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLSRLBRLBRL43153.2BRLBRL

2540

BRLBRLBRLBRLARLBRLBRLBRL

ldkS dry 7.05

ldkg dry 7.05pdkS dry 7.05

ttEkgdry 7.O5

ldkS dry 35.3pEkg ory 7.05

lrgr(g ory 7.05

Fqkg dry 7.05

lEkg dry 7.00

ldkS dry 7.05

lgkg dry 7.05

lg/kg dry 7.05

udks dry 7.os

UgkS dry 7 _05pdkS dry 7.05pgkg dry 7.05pgkS dry 7-05

ldks dry 35.3

ldkS dry 7.05pdf(g dry 7.05

ldkS dry 7,05

30-150 o/L

30-150 %

pdks dry 14.1pdks dry 14.1

ldkg dry 14.1pdks dry 14.1

udkg dry 14.1

ldkS dry 14.1

FgkS dry 14.1

lqkg dry 14-1

lgkgdry 14.1

30-150 %30-150 %

1

1

1

1

1

1

1

I

I

1

I

1

1

1

I

1

1

I

I

I

SW846 8081A 22-Mat47 27-Mar-07 7031275 TG

SW846 8082 22-llkt47 244,lat-07 7031274 MP

SW846 8270C 22-Mar-O7 2A4,eF07 7031279 M.B

Semivolatile OEanic Comoounds bv SW846 8270CPrepa.ed by merhod Sw846 35008

03-32-9 Acenaphthene

200-Sffi Acenaphthylene

62-5+3 Anilino

12e12-7 Anthracene1912-24-9 Atraine103-33-3 AzobenzeneJDiphenyldiazine9247-5 Benzidine56-5i3 B€nzO (a) anthracene

pEks drypgks dry 680

tidkg dry 680

Pgks dry 680pStkS dry

udkS dry 680

udkS dry 6S0

rdkS dry 680

fhit 'storutory rcprt ir not vallil nithottl ot auihori.cll signatwe on the cover page.

' Reponable Detectiod Limit BRL = Below Repftting Limit Pase 29 of l?4

Page 254: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeotific{tio'pM8F-26 2-t'sA595t7-06

Clietrt Proiect #301 -88

Mahi{Soil

Collection Dare/TimeI 9-Mar47 00i00

R€ceived20-M^r47

CAs No. Atuba4s) FI"e A,ri'l 'nDL Dihttion t{erhod Ael. Prepdtcd Analfud Bdeh Analpt

Semivolrtlle Oryrnic Cohpouds by GCMSSemivolatile Oruanic Compouods bv SW846 8270CP.epared by qeltrod SW846 3550850-32{ B€nzo (a) pyrene20+992 B€nzo (b) lluoranhene19r-24-2 Benzo (g,h,i) peM€ne207{84 Benzo (k) flooranfiene65{5{ BerEoic acid10G51.6 B€rEyl alcohol111-S1-i &s(2-chloroetrory)dlethaner11{a{ Bis(2-chtoro€hy'Ftner394?+32-s 8tq2-chtodsopropytFtherr17{i-7 Bis(2-€tlytherythhtretatel0l-55-3 4BrodroptEnylph€oytethgr8f!€&7 B0tyt b€rEyt phtjatat€86-744 Carbezot€s9-5&7 +Chlrm-]rnehytphenol108-474 +CNoroeniline91,5€-7 2-Chloronephhalonee55/4 2-Chloroph€ool7@s72'3 4-Chlorophenyl phenyl 6fier218-014 Chrysene5$70-3 Dberuo (a.h) anthEcene132{4.9 Dbenzofuran955G1 l.2oicttorob€nz€ne511-711 1.lDichtorobenzen€10&4&7 !,+Dichtorobenzen€914t1 3,3'.Oichtorobenzidin€1m-e2 2,4-Diqhlorophenol€{{e2 Di€[1yt PhttElatet31rrn DimohylphdElatsi05{74 2.il-Diftefiy'ph6no,la+7+2 Di-n-butytphthalat€r,3452-1 4,&Dinitro-2flethytphenolsi-2&5 2,4Oinitopfienolr21n4? Z,+OiniFobtuene606.20.2 2,GDhibotoluen€iiru4{ Di_n-o4/lphthalate206-44{ Fluoran{teoe&f T7 Fluo.enel1&7,1{ H€xaclrlorobenzenea7r6&3 l-bxaclrlombutadiene7t174 HoxachlorocyclopentedieneEr-72-1 Hexachloroethane19!3+5 Indeno (1,2,3d) pyrene9Gi2{,t- lvlethytnaphthal€ne78-5s.i tsopfiorone91{7{ 2-M€{hy'naphthetene954+? 2-t €ryphenol10&3€.r, 3,4+!,tehylphenol1116-,{4-591-2G3 Naphth6l€ne8€-714 2-Niboeniliness{$2 }Nitsodniline

SW846 4270C 224n 47 261\nat47 781279 M.BBRLBRLBRIBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRI-BRLBRLBRLARLBRL8RLBRLARLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLARLBRI-

lg}'sdry 680

lgl€dry 6{mpgxo dry 680

FS/tS dry 660

lo,rsdry 640

Fdxsdry 6a0

|lgL/ks dry 680

t gn(g dry 6E0

lglqd.y 680

FgY€dnt €40

ldxsdry 680

UgkS dry 680

t€I€ dry 6€0

|lg?€dry 680

UgkSdry 680

ItSllgdry 680

ldkS dry 680pgil€dry 660

IC/tgdry 580

udkS dry 640

Fdksdry 680

UgnrS dry €a0pg/kS dry 680

lgtsdry 680

lqkS dry 680

ldxg dry 680

usl€ d.y 680pSAg dry 6a0

IS/kg d.y 680pg/rs dry 880

ldkg dry 680

ldi€ dty 6{10

|,9n€ dry 600

FSlkg dry 6€0

lsilqdry 680

ldkgdry 640

ldkg dry 680

u*q dty 680

r€/kg dry 680

Ugtg dry 680

lgkg dry 880

fldkg dry 680

!S{!S dry 680

trykS dry 6€0pdkg dry 680pdkgdry 680

ug/kg dry 680

lsftgdry 640

rdkSdry 6a0

Pgtg dry 680

I

I

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1

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1

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1

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1

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I'|

117

I

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1

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Tnb bbontory Epod is nor edld pihoat aa atntodzrd sknafirr. oE tk cow! pcEe.

'Rqoflable Detcction Limit BRL = Betow Reporting Linit Poge 30 of 124

Page 255: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole Iden tificationMEF-26 24'sA595 t7-06

Clicnt Proiect #301-88

MatrixSoil

Received

20-Mar-07Collection Dare/Time

19-Mar-07 00:00

CAS No. Analyte(t) Resuk Fl"s Unit *RDL Dilaion Method Retr. Pnparcd Anollzed Batch An lst

Semivolatile Org{nic Conpounds by CCMS

Semivolatile Oroanic Comooonds bv SW846 8270CPrepared by rnethod SW846 35508

100{1-6 4-Nitroaniline

98-913 Nilrobenzene8€,755 2-Nitrophenol100{2-7 4_Nitophenol

62-7+9 N-Nitrosodimethylamine

s2t{4-7 N.Nikosodi-n-propylamine

06-3G6 N-Nitrosodipherrylamine07{6-5 Pentachlorophenol

0541-0 Phenanthrene

10&9$2 Phenol

129-00{ Pyrene110-86-1 Pyradine

12042r t,2,4-Tfichlorobenzene9t9t4 2,4,STfichtorophenol8a-06-2 2,4,&Trichtofophenol

Su'rogate recover'esr321-60-8 2-Fluorobiphenyl

367-121 2'Ffuorophenol

4165404 Nitobenzene41

BRLBRLBRLBRLBRLBRLBRLBRLARLBRL876BRLBRLBRLBRL

836575

Compl€ted

BRL

BRL

0_o148

BRL

BRL

BRL

0.0226

BRL

80.7

lglg dry 2720

lgftS dry 680pgftS dry 680

!g/kg dry 2720pdts dry 680

udksdry 680

Ug/kg dry 660

udks dry 680

t4/kS dry 640

US/kg dry 680

!S/kS dry 680

ldkg dry 680

ldkg dry 680

tiS/kS dry 680pgkS dry 680

m-1m o/.

| 5-1tO %3c-130 %15'110 %30-130 %15-1tO %

mgr'kg dry 0 0367

mgL/kg dry 1.14

hg/kS dry 1.72

mgr'kgdry 0.572

mg/kg dry 0.286

tng/kS dry 0.572

thg/kS dry 0.858

hg/kg dry 1.72

mgn 0,0100

mgl 0,0150

mSI 0.0050

mgfl 0.0025

mS/t 0.0O5O

mgl 0-00040

mg/r i.oozsnEI 0.0150

%

1

1

1

1

1

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1

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SW846 8270C 22-Me(07 26.4lat47 703'1279 M.A

416162-2 Plhenol45 621/18-514 Terphenyt4t4 110118-79-$ 2,4,6-Ttibtu.Z]]ophenol 78

Total Mct|ls by EP.{ 6000fi000 S€ri€s Mettodr

743$97€ MeroJry

Tot{l M€tals by EPA 20O Seri€s Methods

7440.22 4 Silver

7440n6.2 Arsenic

7440-39-3 Barium

7,140,499 Cadmiuh

7411047-3 Chaomium

f13g-92-1 Lead

r7a2-4+2 S€lenium

St Lt Extractron

7a4G?2-4 Silver

7440-3&2 Arsenic

7440393 Badum

7440499 Cadmium

7440-47-3 Chromiuh

7439-9rc Mercury

7439-92,1 Lead

a/E2'4+2 S6leniun

C€n€rrl Ch€mirtry Psrsmeten

Yo Solids

0 .141

BRL

8.56

58.7

BRL

7 .11

123

BRL

1 SW846 7471A 26-Mat47 27-Marl7 7031322 YP

EPA200.7 26-Mat47 214ttaiJ7 7031321 HB

SPLP M€t|ls by f,PA 1312 & 5000,t7000 S€ries Merhods

1 SW8461312 22-MarA7 2214at47 7031344 BO

1 SW846131260104 29Mar{7 24-tlar-07 7031408 LR' t '

1 '

1 '' t "

1 SW84613127470A " 26-fr,iar-07 7031409 YP

I SW846131260108 " 24.M,aFO7 7031408 LR' t '

1 SM2540 G Mod. 2SMar07 23-Mar{7 7031429 QP

This l ontoty rcpoa is noa talid r|ithoU ad aathorked signalu?e ontlg clrvcr page.

+ Reporbble Det€.tion Limit BRL = Betow Reporting Linit P a g e J L o f l 2 4

Page 256: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-27 2'-4,sAs964l- l0

Client Pmject #l0l-68

MatrixSoil

Rec€ived22-Mar4'7

Collection Dat€/Ti.ne2 t-Mar{7 00:00

CAS No. Anatya(s) Rcs,'It Fbs 'R"DL Dilution Me,hod Rel Prcpand Analfzcn Bdch AM4EI

Vohtile Or€rnic Conrpounrls

VOC Extraclion Fieh ext'acted

BRL

N/A

lgftSdry 6.6

tSil€dry 132

tSASd.y 6,6pg|(g dry 6.6pslqdry G.6

ldkS dry 6.6

tdkS dry 6.6

ldkSdry 5.6

rcAg dry 13.2

USAS d,y 65.Spdlgdry 6.6

ldlS dry 6.6

Udksdry 6.6pdks dry 32.9psilqdry 6.6pSl(g dry 6.6

Fgrsdry 13.2pgtg dry 6.6

ldkS dry 1X.2

t,gkSdry 6.6

ISftgd.Y 6.6pdkg d.y 13.2

ugr(sdry 66ps,rs dry 6.6

Ug,fkS dry 6.6

!Sn<g dry 6.6

tjL/kS dry 6.6ygn€dry 6-6

vstkedry 13.2

Ug/r<g dry 6.6pgrsdry 6.6

UglS dry 6.6

ldl€ dry 6.6

tjr'kS dry 6.6

ldkgdry 6-6pS/kS d.y 6.6

Ug,r<S dry 6.6pg,lsdry 6.6pgr'l(g dry 6.6

Ugtqdry 6.6pS'lqdry 6.6ySn€d.y 6-6pSftS dry 85.9yqkgdry 6.6

HdkS dry 6.6

lgl€ dry 6.6

lgrg dry 65-9

ugrftS dry 65.9pqkSdry 6-G

26.MarO7 26ind47 7031584 BD

Voiatlle O.qan'rc CompoundsPrepared by mettbd SW846 5035A Soit (tow tev6t)76-13-1 1,1,2-Trid o.ofinuo.oethano(Fr€oDRL67€rL1 Acetono BRL107-rlr Aqyoniu.ile 8RL71.l.T2 Benzone BRL10&€&1 Bromobeflzen€ 8Rf71-97-s Brornod orcrnethane BRL75'214 Brornodidrlorornethane BRL7*2*2 Bomofoam BRL74{}9 Bromomethan€ BRL78-e3.3 2-&bnone (MEK) BRL104-sl{ n-BulylbefEene BRI_r3t98€ s€c€utylbenzene 8RLs€{6{ tert-Butylbenzeoe BRL75-15{ Carbondisutfidb BRL56-23{ Cafuon istrachloride BRL10&90-7 Chlorcb€nz€ne BRL75.00,3 ChlofoedEne SRL676&3 Chlo.o{orm BRL7a{7-3 Chlorgrnethano BRL96-49-A 24hlorotoluene BRL10643.4 +Chlorotoluene BRL9+1 2€ 'l ,2{)ibron}o-3d{orcpropEae BRL1?,r-4€-1 DibromoEhtoromethane BRL10G90-4 l.2oibromoefiane (EOB) BRl-74-953 Dibromomethan€ BRfs+sGl l,2-Dichlorobenzene BRL541-7$1 l,SDichlorobeEeng BRLl0G2!6-7 l,+Dichlorobenzene BRL7t7l{ Oid oddiffuo@nrethene(Freonl2)BRL7t3+3 l.l-Dicldoroethane BRL107{6-2 l.2oichloroethan€ BRL75.35-4 '1

,l Oichloro€thene BRL15€-59-2 cjs-1,2-Dkfloro€thene BRL15€€$s t?ns-1,2-Dichlorcethone BRL7E{7-5 |,2-Oidiloropropane BRL142.28€ 1,3{)ictdorc,prop6na BRL59+20-7 2,2-O[chloroplop6ne BRLr615e€ l,l-DlchloEpropen€ BRLi0061{1-5 cis-1.}Dlcfitoropropene BRL'0061{24bans.l.3_Di.hloopropene BRLroo4r4 Ehybeflz€ne BRL87€63 HeEcfibrobuhdierle BRL59r,70{ 2-Hexanon€ (MBK) BRLs8l2€ lsopropy'b€nzerF BRL9g+7-o +lsopropyttolueab BRfr69a{a{ Metfiyttert-butl ether BRL1081c1 4-Mgtryl-2+entanon€(M|BK) BRL7s.{l$2 tiehyien€ chbrid€ ARL

SW 846 82608 27-Mar-07 28- ar{7 7031650 RLJ

9l-20n Naphthalene

Page 48 of165

TIns bbontory rcpod h nat vatiil irld,ocl on aartoriey' s4naue ofi lhe @v.r page-

r Rcporhble Detectior Limit BRL = Below Reportiq Limit

Page 257: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificatigqM8F-27 2',-4's,{59641-10

Clieot Proiect #30 t-88

Collection Date/Time2l-Mar-07 00:00

MatrixSoil

Received22-Mar-07

C"1S No. Analtte(s) ResaL Flog +RDL Dilution Melhod ReJ, Prcparcd Analwd $alch Anaryst

Volatile Orgaric Compourds

Volalile Oroanic ComooundsPrepared by melhod SW846 50354 Soil (tow tevet)

75$9-4 Trichioroffuoromethane (Freon ltl BRL

103{5-1 rFPropylb€nzene100-42-5 Sty.ene630206 'l

, 1 . 1 ,2-T€trachloroelhane79-34,s 1 , 1 ,2,2-T€lrachtoroelhane1?7-18-4 Tetrachloroeth€ne10&Ea-3 Toiu€ne87414 1,2,U'fichtotobenzene120'82.1 1,2,+Trictioiobenzene71-5s I ,1 ,1-Trichloroethane79405 1,1,2_Trichtoroethane79{1$ TricHoroethene

96-18-4 1,2,$Trichloropropane95636 1,2,+Trimethytbenzene10&67-8 t,3,STrimethylbenzene75{1-4 Mnylchloride133o-2G7 m,p-Xyten€95-.17{ cxylene1099s9 Tetrahydrofufan60-297 Ethylether99+05€ Ted-amyl methyl ether63712-3 Ethy{ tert-butyl elher1oF2OJ Di_isopfopyteth€r75-6+0 Ted-Butanol/butylalcohol12!91-1 1,4_Diorane

Surogale recove.ies:46t)404 4-Bromofluorobenzene

2U7-26-s Toluene4S

1 706047 -o 1, 2-D bhloroethane-d4

186a-53-/ Dibrpmofluo@methane

Extiacaable P€trol€um Hydrocrrbons

Extractable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

8006€14 casoline6&47C30-? Fuel Oild26047ts31-3 FuetOit ft46855900-4 FuetOitt6

I'109600000 Motof OilJ00100000 Avialion Fuel

Unidentified

Other Oil

Total Peholeum Hydrocarbons

Cg-C36 Aliphatic Hydrocarbons

Surogale recovedesl33ee3}z 1 -Chlorooc(adecaDe

Semlvolatile Org.nlc Comportrds by GC

O,oanochlorine Pesticides SW846 8081A

Pr@ared by method SW846 3545A

30900-2 Alddn

SW 846 62608 27-MaGO7 28-Mat47 7031658 RLJERLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRL

BRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRL

99958295

BRLBRLBRLBRLSRLBRLBRLBRLBRLBRL

72

vgkSdry 6.6

Udkg dry 6.6

pdkg dry 6.6

t S/kS dry 6.6

pdkg dry 6.6

l.,S/kS dry 6.6

pSlkS dry 8.6

pg/kg dry 6.6

lig/kg dry 6.6

t S/l€ dry 6.6

ldks dry 6.6

!g/kg dry 6.6

tiS/kS dry 6.6

!g/ks dry 6.6

tis/ks dry 6.6

fg/kg dry 6.6

!s/ks dry '132

!q/kq dry 6.6pg/kg dry 65-SpS/kS dry 6.6pg/kg dry 6.6

tig/kg dry 6.6

ttdkgdry 6.6pg/kg dry 65.9

us/ks dry 132

70,130 %7G130 %7G130 %7G130%

T

1

1

1

l

1

1

1

1

I

i

I

I

I

1

I

1

1

1

1

i

I

l

l

mgftg dry 34.0

IrE4(g dry 34.0

nEftg dry 34.0

nEAg dry 34.0

mS/kS dry 34.0

mdkS dry 34.0

ngil€ dry 34.0

mg/ko dry 340

mSftS d.y 34.0

mS&gdry 34.0

40-140 %

Lrg/kg dry 5.85 SW846 8081A 2&Mar.07 28-Mar47 7031516 TG

This labontory relmn is tnt tqlid p hoa an rlahorir?d siEnalure on lhz coter poge

* Reportable D€ta:tion Limit BRL = Below Reporting Limil Pag€ 49 of 165

Page 258: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiodM8F-27 2,-4'sA59641-10

Client Proiect #301-88

MatrixSoil

Receiv€d22-Mat07

Collection Date/Time2l-Mar47 00100

CAS No, Anelrtz(s) Flog Uni6 .RDL Dil,Itj]o'| Merhod Rel. Prqand Andyzed Batch A@tt5'

Semivohlll€ Orgrtric Compo{nd! by ff

Orqanochlorine Pesticides SW846 8081A

Prepared by method SW846 3545A

319-84{ a€HC31e4n7 bIBHC3i9-86{ d_8HCsa39e gFBHC (Lindane)

s7'71-g Chtordane72.5.1 4,a'-DDD (p,p,)

725s.e 4,4'-DDE (p,p')

s&29.3 4.4 €DT (p,p,)

60$7-1 Oi€ldrin95$98{ En(lcsullan I33213.66.9 Endo6ulfan llro3l{ru Endosultan Sulfate12-204 Endrin?421-93-4 Endrin Aldehyde7644-A Hepiachjor72.43.5 Methoxy(hlor1021-57-3 Heptachlor Epoxide6001.3S2 Toxaphene5103-71,9 E-Chlordane55€6.3+? g-Chlordane

53494-706 Endrin Ketone

Sunogale Eco!€riesi1 woes+z 1, 4-Dgoctafl uoroliphenyl (St,

msr-24.3 Oocachlorobiphenyt (54

Polvcf orinated Biohenvls bv SW846 8082

Prepared by mothod SW846 3545A

t?674r1-2 PC8101611101-24-2 PCE 122111r4nle5 PCB 1232

5346+21€ PCB '1242

12672-2e{ PCB 1248

11097{s.1 PCB 12541r0sc0?-s PcB tmo3732+?3-5 rcB 12621110Gr4-4 PCB 1268

Sunogale /ecotcriesint:t86-8+2 1,+DB.ocffi @tobiphenl (Sr)

2o5t-21-3 Decehlotobbhenyl (54

S€nlvolrtile Orgrnic Compo|rrds by GCMS

sw846 8o81A 2&ltat47 2a4 ar47 7031516 TGBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRL

79

BRLBRLBRLBRLBRLBRLgRL

BRLBRL

5085

ERL

BRLBRLBRl-BRI-BRLBRL

BRL

pdftS dry 5.85

lg[rsdry 5.85

ldl(sdry 5.85

rdkS dry 5.85

rdksdry 29.2pS/t€ dry 5.85

ldkSdry 5.65

udkSdry 545pdksdry 535pgl(sdry 545

Ug/kS dry 5.85

IgkS dry 5.8s

Fdksdrv 5.8s

ldko dry 5.8spgtgdry 5.8spdrgdry 5.05

Fdtgdry 5-8s

udredry 292rgkSdry 5.8sggikS dry 5.85

tgkSd.y 5.85

w-|ffi %fi-I50%

I'SikS dry 11.7

Udkg d.y 11.7

lSftSdry 11.7pdts dry 1r.7

Ugkgdry 11.7

UgtS dry 11-7

UdkS dry 11.7

!g/kS dry 11.7

FSilg dty 11.7

u-lfl%30-1ffi %

FdkSdry 421

ISA9 dry 421pdrgdry 421

ldks dry 421

!gl(g dry 421

f./dkg dry 421

lgrko rtry 421

frdkS dry 421

SW846 6082 z&Lrlar{7 28{vlar47 7031515 SM

Semivolatfle Oroanic Comoounds bv SW846 8270CPr@ared by me0|od SW846 3545A

03-32-9 AcenaphthenemBsH Ac€naphthylene62-533 Aniline12G12-7 Althaec€ne1912-2+9 Afazin€103-33 Azobeflzeoe/Diphenytdiszine92{7.5 Beeidine5&563 Benzo (a) entfu'acene

SWS46827@ 2?+lar{7 2f.{nar47 703t5g2 t.B

Thit bboalory npod At ttot vobd withoat dn uthadzd slgnlurc on rhz coee, page.

'R€porhblc Det€ction Limit gRL = Below Reporting Limir Page 50 of 165

Page 259: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldenrificationMAF-27 2t4l

sA59641- 10

Client Project #301-88

MatrixSoil

Collertion Dat€/Time21-Mar-07 00:00

Received22-Ma(07

CAS No. Atnute(s) F,oC Unit. *RDL Dittrinn Method Ret Prepand Analy4ed Bdch Anallst

Semivolrtlle Organic Compouods by CCMS

Semivolatile Orqanic Comoounds bv SW846 8270C

Prepar6d by mothod SW846 354SA

50,32 8 Benzo (a) pyrene

20+99-2 8€nzo (b) fluoranthen€1e1 24-2 Benzo (g,h,i) perytene

207{8-9 Benzo(k)fluorandrene6s-as B€nzoic acidlrxr-s1{ Benzylalcohol111-91-1 Bis(2-cl{oroethoxy)mothane111-44-4 Bis(2{htoroethyl)eher

39638-32-9 8is(2d oroisopropyt)other11741-7 Bis(2€fit/hexyDphfEtste101.s5.3 4-Bromophenyl phenyl ether856&7 Butyl benzyl phthalat€

{16-74 I Carbazole59.5G7 4-Chlo.o-3-methylphenol

106-47{ 4-Chlo,roanaline

91{e7 2-Chloronaphthalene95!57-A z-Chlorophenol7m+72,3 4-Chtomphenylphenylether

218n1-9 Chrysene

53-IA3 Oibenzo (a,h) anthEcene1324.1-9 Dibenzofuran95,5L1 l,2,DichloaoberPen€541-73-1 1,3-Dichlorcbenzene10646.7 .1,4-DacNofobenzene

e1-e4,1 3,3-Dichlorobenzidine120{3-2 z,4-Dichlofophenolu4+2 Oiethyt phthalate

13f11-3 Dimethyt phhalale10ft7-9 2,4-Dim€thytphenol

u-74-2 Di-n-butytphthatate

s34,52,1 4,6-Dinito-2-melhytphenol

51,2&5 2,4-Dinitrophenol

121r4-2 2,4_Dinitrctotuen€

606-m-2 2,GDinitrototuen€117444 Di-n-oclyiphthstat€

206-144 Fluorandren€

&73-7 Fluoren€118-74-1 Hexac}rlorcb€nz€ne

875&3 Hexacfilorobutadien€

Tt17-1 Hexaafiloroclclop€ntadiene

67-72-1 HeXaCfOroethane1S3-39-5 hdeno (1,2,3-cd) py.en€

90r24 l.Methtnaphthalen€786+1 lsophoaone

e1674 2-Methylnaphthalenee5-4&7 2.Methytphenol

108€e-a, 3,4-Methylphenol106-..4-591-20-3 lGphlhatene8a-74-4 2-Nitroanitine99{9-2 }Nilroanitine

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

fg/kg dry 421

!g/kg dry 421

!S/kS dry 421ps/kg dry 421pS/kS dry 421pS/kS dry 421

Udl€ dry 421

!s/ks dry 421pS/kS dry 421

ldks dry 421pdkS dry 421pg/kg dry 421pS/kS dry 421pg@dry 421pS/kS dry 421

lgkS dry 121

US/kS dry 421

!s/kg dry 421

!S/kg dry 421

!g/kg dry 421

!S/kS dry 421pdkS dry 421pdkS dry 421pSAS dry 421pdkS dry 421

!S/kS dry 121pdks iiry 421pgkS dry 421

Pqkg dry 421pdkg dry 421

lqkg dry 421pdks dry 421

UdkS dry 421

ldkg dry 421pgkSdry 421pgkSdry 421

iJgtkS dry 421

UdkS dry 421

ldkS dry 421pdkS dry 421pdkg dry 421pdkS dry 421pCftS dry 421

ldkS dry 421

lgks dry 121pgkg dry 421

Udkg dry 421

tlSJkSdty 421

!S/kS dry 421p€/kg dry 421

sw846 8270C 27-Mar-O7 27-MaPO7 7031592 M.B

This labotaloA rcport Lt ,rol taid *irroU an autlloried signst!rc on lhe coeer page.

' Reportsble Detection Limit BRL = Below Reporting Limit Page 5l of 165

Page 260: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEFJI 2'4'sA5954l - 10

Client Proi€ct #l0l-88

MatlixSoil

Collection Datey'Time2l-Mar47 00:00

Received22-Mnr-07

CAS No. Anabte(s) Fl4g 'RDL Dilaion M..hod Retr P.epated Analytd Edch Analyst

S€mivolalile OrS.nic Compoundr by cCMS

Semivolatile Orqanic Compounds bv SW846 8270CP.epared by mehod SW846 3545A100416 +Nitroaniline98-9t3 Nibobenzene6E.7t5 2-Nibophenoll0o{2'7 +NitEpheno,l62-75-9 N-NitKrsodimethylamine6?1{4-7 N-Nihos4di-n-propytamioe86-30{ t$Nitrosodiph€nylgmine87{G5 per achlo{ophonda5{1-8 Phenanthrehetoe95.2 Phenolr29-0o{ q/r€ne

tlF€6.1 Pyridinel20{2-1 1.2,+Tddilorobenzen€95-s5-4 2.4,$TrichlorophenolS8{G2 2.4,&Tricilorophenol

Sunog|af€ rEcover'esr32ta68 z-Huotobiphenyl

357-124 2-Fhnrophenol

11654/)4 Nitrobnzene4s

416562,2 Pherbrds

171e51-0 Teeh6nyHl4

t 1e7*6 Z4,Fftibromophenol

SW84682mC 274tat47 274ar4f 7031592 M.BBRLBRLBRLBRL8RLBRL8RLBRLgRL

8RLBRL8RLBRL

BRLBRL

6158

60

ldl€ dry 16q) 1

lrytC dry 421 |

Fgtg dry 421 1

t C/Xg dry t690 |

ldkg dry 42r I

lgkS dry 421 1

UdkS dry 421 1

ugxg dry 421 Iydlqdry 421 |pSftg dry 421 I

ldfq dry 421 1

t9ft.Sdty 421 I

usl(S rtry 421 1

t4/kg dry 421 1psilqdry 421 t

30-tm o/.

11110 %30-1N%1r110%30-130 %15-110%

Totrl Metds by EPA 6m0t000 S.rl$ Methods

743s.974 Merdrry BRL

Totrl Metlk by EPA 200 S€ries Methodt

SW8.l6 7471A 28-Mar-O7 28 4a.47 7031495 YP

EPA20O.7 2&|.ner-o7 za']l'',Erif 7031,194 RM

SWE461312 26Mar{7 26.ltarfi 7031560 BD

SW846 1312r'60'l0B 2&ti,lar-07 28-Mar{7 7031651 HB

7440-2-4 SiVe.

7440n€-2 A6€nic

714G39,3 Earium

144H3-S Cadflrium

7+rc47-3 Chrcmium

7439.92-r Lead

744{F22-4 Slv€r

71.10-3&2 Arsenic

7'!tt',3+3 Badum

?4aoang Cadmium

744O'aZn Chlon um

7439€7$ Mercury

713942-1 Lead

n8a4$2 Setenium

Generrl Chemirlry P.r.meaer!

% Solids

r€/kg dry 0-0345

nrdkS dry 1.05

mg/kg dry 1-58

ntgilg dry O.ml

rngikg dry 0-263

nrgukg dry 0.527

mgr'kg dry 0.790

mgfl(gdry r.58

0.0200

0.0t50

0_0150

0.0025

0.01s0

0,ofix{)

o.ot50

o.o150

sw8{6 t9127470A

Sw846l31z6ol0a

28+!,lar-07 7031652 YF

28+!,lar.07 m31651 HB

BRL

8RL

| 1 .5

BRL

3.97

8 .18

282-4+2 Solenium BRL

SPLP Mer.k by EPA 13 12 & 6tXXy7000 Serier Methods

SPIP Ext Edion CompletEd

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

45.2

mgn

msf

lngn

msr

msrl

rncl

nrgil

mg/l

I SM2540 G l\rod. 24-Mar47 24t {-07 7031470 QP

Thls laboratory Eport ls d tdid pdlhou cn arrtot*Fd sig d!rc on Utt coee, INg.-* R€portable Detection Umir BRI, = Below REporliry Limit Page 52 of 165

Page 261: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-28 2'-4'.sA,59641-1t

Clietrt Proiect #301-88

Collectiop Date/Time2l-Mar{7 00:00

MatrixSoil

Received22-Mat-01

CIS No. Anaryte(s) Result Flas *RDL Dilution Lletho.l Rel. Prcpared Amltzed Bakh A al$t

Voletile Orgsnic Compounds

VOC ExtractionVolatile Oroanic Comoounds

Field extracted

BR,J-

ps/ks dry 6.2tigikg dry 125tiSikS dry 6.2

tig/kg dry 6.2pdkg dry 6.2

!S/kS dry 6.2

!S/xg dry 6 2

uS/kgdry 62

lSftg dry 12.5

uS/kS dry 623

!g/kg dry 6.2

!g/kg dry 6.2

!g/kg dry 62

Ir$tSdry 3r.2

!S/kS dry 6-2pdks dry 6.2

udksdry 12.5pdkS dry 6-2pSlkSdry 125

ug/kg dry 6.2

!g/kS dry 6 2

Ug/kS dry 12.5pg/kg dry 6-2pSlkSdry 6.2pdkg dry 6.2

ldkS dry 6.2pdkg dry 6.2

lqkS dry a.2

ldkg dry 12.5

udkg dry 6.2

Itdkg dry 6.2

lqkg dry 6.2

ldkSdry 62

ldkgdry 6.2

U94(S dry 6.2pg/kS dry 6 2

ldkgdry 62

ldkS dry 6-2

!S/kg dry 6.2

lSftS dry 6.2

ldkS dry 6.2pgkS dry 6.2

rc/kg dry 62.3

!g/kg dry 6.2pS/kS dry 6.2

IdkS dry A.2

FS/IS dry 82.3pS/kS dry 62.3

ldkS dry 6.2

voc

sw 846 82608

26-Mar{7 26-tvlac07 7031584 BD

Prepared by method SW846 5035A Soit (tow tevet)

76-13-1 1,1,2-Tdchtorohinuoroethane (FreoSRL6764-1 Acelone BRL107-13-1 Acrytonitdl€ BRL7113-2 Benzeno BRL108-86.1 Brornob€nzene BRL74 97-5 gmmochbrornelhane BRL15-?14 Bromodichtoromelhane BRL75-)12 Eromotorm BRL74{}s Ercmomethane BRL78$13 2-Butanone (MEK) BRL104-51J rFBulytbenzene BRL11t98€ sec_Bu!y'beruzene BRL98{6-6 tert-gutylbenzene ARL75-15:l Carbon disutfide ARLt6-23-s Carbon tetrachloide 8RL108-9G7 Chlorobenzene BRL75{0-3 Chloroethane ARL67€6-3 Chloroform BRL1447-x Chtoromethane BRL954s8 2-Chlorototuene BRL106-434 +Chlorobluene BRL96,12-8 .1,2-Dibromo-3_chloropropane BRLrea4a'1 Dibromochto.omethene BRL106.93i l.2D,brornoethane(EDB, BRL74 9t3 Dibromomelhan€ BRL95'5G1 l,2.Dichlorobenzene BRLs41-73-1 l,3-Dichlorobenzene BRL106-,16-7 1,4-Dichlo(obenzene BRL75-l1-€ Dichtorodifluoromelhane (Freon12)BRL75-34-3 l,l-Dichlofoethane BRL107-06-2 l,2-Dichloro€thane BRL75-35-4 t,1-Dichtoroethene BRL

156-59-2 cis- 1 ,z-Dichloroethene SRL

156€G5 tans-1,2_Dichloro€thene BRL

78{7-5 l,z-Dichloropropane BRL

1{2-28{ 1 ,3-Oichloropro'pane BRL

59t20-r 2,2-Dichloropropane BRf563-586 1,l-Dichtoropropene BRL

10061{l-5 cis- 1 ,3-Dichloropropene BRL1ilo6r{2{ trans- 1 ,}Dichloropropene BRL100-414 Ehylbenz€ne BRL

876+3 Hexad orobutadiene BRL

591-784 2-Hexanone (MBK) BRLssa2a tsopropytb€nzene BRL9€47$ +lsopropyltotu€n€ BRL163444-4Metfryltert-butyletf|er 8RL10&1G1 +Methyl-2-pentanone(MIBK) BRL

75492 Methyl€ne chloride 8RL9r-2G3 Naphthalene

Page 5l of 165

Thit labonlor! Eport is not vatid withaut aE zstho.ized sigtutaure on the cover paEe.

* Reportable D€rection Linir BRL: Below Reponing Limit

Page 262: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatodMtF-28 2'-4'sA5964l - I 1

ClieEt Proiect #301.88

Collectiod Date/Time2 I -Mar{7 0o:0o

Rectived22-Mt-07

MatrixSoil

C"1S No. 4narrtc(s) Flog Uti6 'nDL Dllution Method Rel, PEWed Analwd Edtch A&tyst

Vobdle Or€ooic Compot|ndr

Volalile Oroanic ComooundsPrepared by m€f|od SW846 5035A Soil (low tevel)103-6s1 n-Propylbeizone 8RL10G42'5 Styrene 8RL63G20{ I,l,'l,2-Tet€cfiloroethane 8RL7$1,L5 1,1.2,2-Tetracfiloroethane BRL127n04 Tebachloro€ltEne BRL108-8&3 Toluene ARf8761$ 1,2,$Tichlorobenzene 8RL120€21 1,2!+Tridhlorob€nzene BRL715# |,1.l-Tricfiloro6thane BRL79{0-5 1,1,2-Trid ooethane 8RL?941€ Tichloroethene BRL754S4 Trichlofofluoom€thane (Fr€on 11) BRLs.1a4 1 ,2,+Trichtoopropene BRL95-63i 1,2,+Trimethylbenz€ne BRL108-67€ 1,3,5-Trimedlylbenz€ne BRL7s414 Vinylcfiloride BRL1330-20.7 m,p-Xyt€ne BRL95-47{ Gxylen€ BRLlosss Tet.ahldmturan BRL60-2s7 EhyledEr BRLsgt{s{ Tert-amyl methyl ether BRL637€2-3 Ethy' left-butyt €ther BRLl(a-iG3 Di-isopropyl ether BRL7s€5i Tert-Bubnol/ butyt alcohol BRL123.s1-'1 l,+Dioxane BRL

&nrogals €coleresj4@40-4 +Ekoftnfruorcbenzene 86m37-2e5 TohEne4S 90,706G074 l,2iic o@ethane-d4 871868.53-7 Dibtonbf,uoromehane 98

Ertrrctable P€tml€um Hydrocrrbon!

Extractabl€ Total Petroleum HvdrocarbonsP.epared by nethod SW846 35504

BRLBRLBRLBRLBRLBRL932Calculated as

llJg*S dty 8.2

sdrS dry 6.2pg/rg dry 6.2pq*s dry 6 2pdrs dry 6.2

ldksdry 6.2

tlgtg 6ty a.2

lgkg dry 6.2

l.rdkg dry 6.2pS/rS dry 6-2

t SI(9 dry 6.2pdkS dry 62

ldkgdry a.2pdlq dry 6.2

lSftSdry 6.2

lslt(gdry 6.2

ldkS dry 12.5pcrks dry 6.2pdrg dry 62 3pdxg dry 6.2

ldkg dry 6.2

lJgn€ dry 6.2

I'dktd.y 6.2

lS^gdry 62.3

ISrI9 dry 125

70130%70-130 %70-t30 0,6

76130 %

mdkSdry 161

mgkg dry 161

flEn(gdry 161

mgn(g d.y 161

nE/kg dry 161

mg/kg dry 161

mg/t€d.y 161

mgftgdry 16'l

ngftgdry 161

ttlykg drt tG1

41114 %

SW S46 82608 27-Met47 28-Mat47 7031656 RU

8006€1-9 Gaeolin€68a7S30-2 Fuel o{l #26847s31-3 Fu€lOilt4

€€s53-0o.1 Fuel oil #6

MlNsloOoO Motor Oil$0100000 Aviglion Fuel

ljnidentified

OtlEr Oil

2

2

222

2Total P€trol€um Hydrocarbons 932

C943,6 Aliphe6c Hydrc€66n5 932

Surrogats rEcovEriosli38o-33-2 l -Chbr@cladecane 209

Semlvohlilc Org!tric Compounft by CC

Oroadochlorine Pesticides SW84ti 8081APrepared by melhod SW846 3545A3Xl9{,4 Aldrin BRL UqkS dry 6.21 SWB46 8081A 264nar47 2g-nAa.47 703151€ TG

This labrdlory |'Iorl is not valid tithou tn oadatlad slgadfi. on the cow. pate.

+ Reportabk Dete.tion Linit BRL= Below Re?orting Limii P.ge 54 of 165

Page 263: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldenttficarionNtSF-28 2,-4'sA5964l-t I

Client Proiect #30 t -88

MatrixSoil

Collection Date/Time2l-Mar-07 00:00

Received

22-Mar07

cAS No- Anaqtz(s) FbE Unia *RDL Dilutiarl Method ReJ PrEp ed A&bzed Bakh AnaDst

Semivol{tlle Organic Compounds by CC

Orqanochlorine Pesticides SW846 809.1A

Prepared by melhod SW846 3545A

31934$ a-BHC

319-8t7 b-BHC

319-863 d-8HC

5849-9 S-BHC (Lindane)51-f4 9 Chtordane

n54'a 4,4.-DDD (p,p ' )12-s5-e 4,4.-DDE(p,p.)

50-2e,3 4,4.-DDT(p,p')

60-57-1 Dieldrin

95$98{ Endosulfan I3321365-9 Endosulfan ll1031{7{ Endosulfan Sulfale72-2G8 Enddn

7421€+4 EndrinAldehyde76-44-A Heptachtof72-1.3.5 M€thoxychlor1024-5?-3 Hepiachtof Epoxide4001,35,2 Toxaphene5r03'71'!, a-Chlodane5566'34,r glchlordane

s34947G5 Endrin Ketone

Su7rogate Ecovenes:t 03a6.u.2 4,+DEoctafluorobiphenyt (Sr)

2051 -24-3 Decachlorobiphenyl (St)

Polvchlorinated Biphenvls by SW846 8082

Prepared by method SW846 3545A

12674-1r-2 PCB 1016111o4-2a-2 PCB 122111141-16-5 FCB 123253,469-21-9 PCB t 24212672-29$ rcg 124811097-69-1 rcB 1254110sG82-5 PCB 126037324,23,s PCB 12621110c14 4 PCB 1268

Sufloga/€ EcoveiEs:

103868+2 4,4-DB-Octafluotobiphenl Gr)N51-2+3 Decachlorobiphenyl (St)

S€mivolatile Orgrric Compoundr by GCMS

Semivolatile Oroanic Co'.npounG bv SW846 8270CPrepared by method SW846 3545A

83-32-S Ac€naphthene208-96{ AceMphhylene€2-53-3 Aniline12G12-7 AnthEcene1912-2+9 Attazine103-33-3 Azobenzene/Diphenyldiazine92.47-5 Benzidine

56.513 Benzo (a) anthrac6ne

BRLBRLBRL

BRLBRLBRL

SRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRL

3194

BRLBRLBRLBRL8RLBRLBRLBRLBRL

3045

8RLBRLBRLBRLBRLBRLBRL

BRL

Ug/kg dry 6.21

UdkS dry 6-21

ldkS dry 6.21

tgkS dry 6.21

ugtgdry 31.1

UgftS dry 6.21gkS dry 6.21

udkS dry 6.21pgkgdry 6.21

USftS dry 6.21

frg/kg dry 6.21pdtSdry 6.21pdkS dry 6.21

udkS dry 6.21pdkg dry 6.21

lig/tqdry 6.21

!g/kg dry 6.21pS,/kS dry 31.1pS/kS dry 6.21pqks drl 6.21pdks dry 6.21

30-150%30.150 %

!g/kg dry 12.4

!S/kS dry 124

tS/kS dry 12.4

|'s/kg dry 12.4

ldkS dry 12.4

!S/kS dry 12.4pdkg dry '12.4

Lig/kg dry 12.4

UdlS dry 12.1

3G150 %m-|50%

SW8,f6 80alA 26-Mat47 29-Mafi7 7031516 TG

SW846 8082 26-Mar-07 28-MaF07 7031515 SM

Pe/kg dry 3o0

!S/kS dry 3O0

UdkS dry 3O0

UgkS dry 300

!Sl(S dry 3fi)

ldkS dry 300

lgkg dry 300

ldkS dry 300

5

5

5

5

5

5

5

5

SW846 8270C 27-Mar-O7 27-MarO7 70315S2 M.B

Thb laborutory rcpo.t ie dot edd hilhoar an anhoned siEnature on tht co,er page.

* Reportable Detection Ljmit BRL = Below Reporting Limit Page 55 of 165

Page 264: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-24 2,-4'sA5964l-l r

Clietrt Proiect #301-88

Matrix50r l

Collectioo Date/Tih€2l-Mar-07 00:00

Received22-Mat47

CAS No- At'ctrk(t) FloC .RDL Dilaion Mdhod ReJ, Prcpuen Aaa[zed BaLh Aralw

Semivohtil€ Orgrrlc Comportrdi by GCMS

Somivolatile Oroanic Compounds bv SW846 8270C

Prepared by rnethod sv'r846 3545Aflt42-a g€nzo (a) pyrene20199'2 B€t|zo (b) fluo|anftetrei91-24,2 B€nzo (g,h,i) peryl€ne207.08-9 Benzo(k)fluoranthene65€s) Benzoic acid10Gs16 Bdlzyl alcohol1t1-s1-i Bis(2-chloroethoxylnstrEne111-44-4 Bis{2dloroehyl)eh€i3{'618-12-9 Bis(2d{oroisop.@yt)ether117€1-7 Biq2-€trfheryl)phfi€late101.s5-3 4-EEmoph0nylph€nytether8t6&7 8uM b€nzyl phlhalate86-Z+8 Ca|tazole595G7 4-Chloro-3-rnethylphenol106-4T3 +Chloroaniline915&7 2-Chh.onaphthalene95'57{ 24hbmph€nol7005-?2.3 4-Chlomphenyl phenyt ethea21641.9 Chrysene5il-z().3 Clibor|zo (a,h) anthi*ene13264€ Db€nzofLrranS-5G1 l,2OicHo@benz6n€54t-73-1 l,3-Dichlorcbenzene1HG7 l.+Dichtorobenzen€914+1 3,3',-Oh.htorobenzidine12G€3.2 2,:l-Oichloropi|€nol846rt2 Digtryiphthalate131-i1a Dime[1yiphhalater0fi674 2.4-DimethylphenolU-7+2 Di{-butylpf'tElste5{452-1 4,e>Dinibo-2-methytphenol5l-2&5 2,4-OiniEoph€nol12tn4.2 2,+Dinitgtolu€ne6ql2G2 2,GDinihrtotuene117{a{ Di-n-octylphhalate20e4-{t Fluoiondtene&7+7 Fluorenellg74.1 l-lexachlorcb€nzene87{&3 tbxad{orcblladienon474 Hexadrlo,rocyclopontadiene67-72-1 H€xaaf$orc€lhane1e+396 Indoio (1,2,3-cd) ptrene90-124 t-Methylnaphrnabne7869n lsophorOnesl-57.6 2-Methy'naphhal€n€!r5i.4&7 2-[,lgthylphenol1{I+?€4. 3,4-Methylphenol106.r.r-591-2Gl Naphthet€ne$.7+rl 2-Nitoaniline9s-O€.2 lNifoaniline

BRLBRLBRL

BRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRI.BRLBRLARLBRLBRLBRLBRLBRLSRLBRLBRLBRLARLBRI-BRLBRL

BRLgRL

BRLBRLBRfBRLBRLBRLBRL

BRLBRI-BRL

!g/kg d.y 30O

tldksdty 300

lglsdry 300

udlsdry 30o

Ug/kg dry 300

lSftS dry 300pdksdry 300

lSiks dry 300pSftSdry 3O0

lglg dry 3o0

ldksdry 30o

udks dry 300

udksdry 300

ldkg dry 300pSftS dry 30OpS/kS dry 3o0

ldrg dry 300

wllg dry 30o

Ug/kg dry 300

ISrkgdry 3OOpS/kS d.y 3tX)

IgAg dry I)0pdks dry 3o0

lcrrs drv 300

$gksdrr 30opSI(S dry 3O0

Itg/kg dry 300

W/kg dry 3tX)

llglkS dry 3fi)

[dkg dry 300

Fg/kS dry 30O

rdks dry 30opdkS dry 300

Udkg dry 3o0pgkqdry 3fl)

IS/tgdry frX)pgts dry 300pdks dry 3O0

lglS dry 300

!S/kS dry 30OpdkS dry 300pgks dry 30o

US/kS dry 3O0pqkgdry 3o0

ldkSdry 300

tdkdry 300

lSftS dry 3oo

pdkS dry

lgftsdry 300

Ug*Sdry 300

SW846&170C 27.Ma147 274td47 7031592 M-B

Thir labontarf ,qod is'rattdii p hoa aE or/[torlz.d sbt dqre on tt'E dtEr pagc.

' Reportrble Det€ction Limit BRL = Below Reporting Limie Pagc 56 of 155

Page 265: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple IdondficationM8F-28 2,-4,sA5964l-l I

Client Proiect #t0 l -88

MatrixSoil

Collection Datc/Time2l-Mar47 00:00

Received22-Mat07

CAS No. Anatye(s) Resall Fhs Anits IRDL Method Rel. Prcpand Aaalrzed Batch Analrsl

S€mivolatile Organic Compounds by CCMS

Semivolatile Oroanic Comoounds bv SW846 B27OCPrepared by melhod SW846 3545A

100{1{ 4-Nihoaniline96-9ti Nifobenzen€86-7$5 2-Nitrophenot100-02-7 4-Nitroph€nol62-7Fg N.Nitrosodim€ftrylamine621{4-7 N.Nitosodi_n_propylamine86-30{ t+Nitrosodiphenylamine87-SA5 Penlechlorophenol85{11'€ Phenanlhrene10&95.2 Phenol12+00{ Pyrene110{6-t Pyridine120{2-1 1,2,+Trichto.obenzene9s-9s 2,4,Slrichtorophenol86{e2 2,4,GTdchtorophenol

Sunogate r6covsrbs--321-6da 2-Fluorobiphenyl

36r-12-4 2-Fluorophenol

4165{04 Nilmbenzene45

116542-2 Phenol4s

171g-Sti TeMenyl4t4

118 79-6 2,4,6Tdbromophenot

ps/kg dry 1200

ldkS dry 300

uS/kg dry 300pdkS dry 1200

lr94g dry 300

Lrdkg dry 300

!S/tg dry 300

Lig/kg dry 30O

!g/kg dry 300

UdkS dry 300

lsng dry 3o0

Pg/kg dry 3O0

trg/kg drypS/kS dry 30O

lrglkg dry 300

30-t 30 %15-110 %30-130%15-110 %m-lm %15-tt0 %

rngr'kg dry 0.0329

ms&s dry 0 995

mgiks dry 1-49

mg/kg dry 0.497

mg/kg dry 0.249

ngtkqdry 0.497

mg/kg dry 0.746

mgfl(g dry 1.49

hgn 0.0200

lhgn 0.0150

mg/l 0 0150

mg/l 0.0025

hg/l 0.0150

rng 0-000d0

|ngn 0.0150

rng/l 0 0150

%

BRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

61

4A7057

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

SW846 8270C 27-Mat47 27+l,at47 7031592 M B

7440 22-4 Silver

7440-39-2 ArseniC

7440-39 3 Badum

7440419 Cadmium

71404r-3 Chrcmium

7439-92-1 L6ecl

778?-492 Seleniuft

Tot l Metds by f,PA 6000/7000 S€ries Merhods

7439 9?,6 Mercury 0.0388

To(tl M€trk hy EPA 200Srrics Metnods

1 SW846 7471A 2B.l./,at47 za-Ma4l 7031495 YP

I EP4200.7 28-Mat47 2841,a.47 7031494 RM

l "

1 '

1 '

1 "

1 '

1 SW8461312 26-Mar-07 2Gt4ar-07 7031560 8D

1 5W846131260108 28-Mat47 28+lar47 7031651 HB

1 "

1 '

1 '

1 '

1 SWU6131A747OA ' 28-Mat47 7031652 YP

1 SW8,16131?J60108 " 2&Mat47 7031651 HB

1 "

1 SM25.f0 G l\4od. z+Ma(Ot 24^iat47 7031470 QP

BRL

1.60

1S.3

0.333

7.39

25.3

BRL

SPLP Metdr by EPA 1312 & 6000t000 S€rtes Merhods

SPLP Extraction Compl€ted

7Mo-224 Sitvat gRL

7440-3&2 Arsenic BRL

7,140-393 Barium BRL

744043.9 Cadmium BRL

7440-47-3 Chromium BRL

7439-9?{ Mercury BRL

7439-92-1 L€ad BRL

7782-4$2 Selenium BRL

General Chemlsary Prrsmeters

% Solids 90.8

Thh lahoralory rcport is not valid withoat dn autltorir2d sigt,a,tcrc on thc coter pzge .

i ReponablE D€tection Limit BRL = Betow R€porting Limit Page 57 of 165

Page 266: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeotificationM8F-29 2',-{'sA5 4l-12

Cliert Project #301-88

MatrixSoil

Recaived22-M^r-O7

Collection Dat€/Tim€2l-Mar-07 00:00

CAS No- Analyaz(s) FlaB Units *EDL Diluion Method Retr, Preporcd AaqlyTsl Batch Anaust

Vobtile Orgrnic Compounds

VOC Erdraction ?s.M3{47 2iltat47 7031 584 BO

pSAS dry 64,3pgrkg dry 1290

!s/kg dfy 64.3

!4kg d.Y 64.3

ldkSdry 64.3

ldkS dry 64.3pdkS dry 64.3pS/kg dry 64-3

rdkS dry 129

IS/kS dry 643pS/kgdry d+.3

lgrsdry 64.3

lglkgdry 64.3

ldts dry 322pdkS dry 64.3

t€/ko dry 64.3

ldtS dry 129pSftSdry &1.3

lqkSdry 129pdxgdry 6,{.3

!g/k€ dry 64.3

USI(S dry 129pS/kS dry 64.3

lSlkS dry 64.3ydXS dry 64 3pdkg dry 6{.3

lCftS d.y 64.3

ldkg dry 64.3

ldkS dry r29

udks dry 64.3

@v,S dt t 64.3p9rk0 dry 6,{.3

ldkg dry 64.3

USA9 dry 64.3

lgl(gdry 64.3

lcrrs dry 64.3pdksdry 64.3

US/kS dty 64.3

lSftSdry 64.3

Fdks dry 64.3

rdkgdry 64.3

tiSikS dry 64.3pgtgdry 643

Ugkg dry 64.3

ldkgdry 64.3

!gI(S dry 64.3

ldl(g dry 643

l|gn(g dry 643

lSn€ dry 6,1.3

Field €idracredVolatile Orqanic Comoounds vocsPrepared by m€tfiod SW846 5030 Soal (high lovel)76-13-1 1,'1,2-Tdct o.otrifuoroethane(Fr€o€RL6l{+1 AEetone BRL107-13-1 Acrylonltrite BRL'114}2

B€nzene BRL1o&o€-1 Bromobenz€ne BRL74-97-5 Bro.no{filororn€thane BRL75'271 Brg.nodichloromthane BRL7s2r2 Blomoforfi BRL74{3-9 Bronomethan€ BRf78.933 2€ubnone (MEK) BRL1045i€ n-Butylbenzene BRL135-984 sec€utylbenzene BRL98-06-€ tdt€'-rtyhenzene BRL7s-ls-0 Carbon disutfide BRLs6.23.5 Carbon tebachloride BRL10es+7 Chlorobenzene BRl-75{0-3 Oilorc€thane gRL

67{e3 Chlomfolm BRL?4{71 Chlo(omethan€ BRL9t4$€ 2-Chlorotolu€n€ BRL10€-ts 4-Chlorotoluene BRL96-124 1,2-Dibromc3-ciloropropane BRL124-44-1 Dibmrhochlorcmefian€ BRL10+e3.{ 1,2-Dib,rornoethane(EDB) BRL74-95-3 Ditxomornethane BRL95-5Gl l,2-DlchloEbenzene BRL5,11-73-1 l,3.Oichlorobenzene BRL106-{6'7 l,4oidNorobenz€ne BRL75-71.6 Dicf orodifluoronretherE (Freonl2)BRL?s+,G3 1,'l-Dict$r.oethane BRLi07{6-2 l,2-Dichloroeth€ne BRL7$35-4 i,1-Dbhloroethen€ BRLi5tr92 cjs.1,2-Dichloroeth€ne SRLl5G6G5 tEns-1.2-Di(hlo.oethene 8RL7a€7,5 t,2-Dic* ofopmpan€ BRL142.24-9 l,3-Dichloroprcpane BRL5S+2c7 2,2-Dichloropropane BRLs6$584 1,|-OioHoropopene BRL1006141.5 cis-1,3-Dichloroprop€ne BRL10u61-o2€hans-1,$Diohlorcpropene BRLl0o4l4 Ethytbanz€n€ BRL8?{&3 Hexadrlombutadiene BRL591-764 2-tt€xanone (MBK) BRL9842{ tsopropylb€nzene BRL99{7{ zl-lsopmpyltoluene BRL163444-4 Modryl bd-butln edier BRL108-1$1 +Methyi-2+entamne([ BK) BRL7fis2 Meftylene chlorid€ BRL

5050505050505050505050505050505050505050505050505050505050505050

50505050

50

50

50

505050

SW 846 82604 23-Mat47 29-Ma.47 7031784 mar

9l-20.3 Nephthlene

Page 58 of 165

Ihb lalontory rcpod h ,et volitl h,lthou sn acrtorized sEnztrlre ott th. @ftr pqe.

' Reportlble Detection Limit BRL = Below RepdtiEg Limit

Page 267: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationMEF-29 2,-{'sAs964l- l2

Client Proiect #301-88

ColLection Date/Time2l-Mar-0? 00:00

MatrixSoil

Reccivcd22'M^.-01

CAS l1o. Analyte(s) Restlt FloC *RDL Di, ia'n PrcpaEd Antbwd Balch Anltlts.

voladle O.ganic Compoundr

Volatile Oroanic ComooundsP.epared by method SW846 5030 Soit (high tevet)

7549-4 Tdchloronuoromethane (Freon .11) BRL

103{5.1 n_Prcpylbenzene100-425 Sty€n€63G20S 1,'1,t,2-TetEchtoroethane79-34-5 1 , 1 ,2,2-Tetrachtoroethane12h8-4 TelEclioroethene109-€43 Toluene87616 1,2,STrichlorobenzene120-821 1,2,4-Trid,rtorobenzene71-5+6 1,1,1-Trichloroethane79{0-5 1 ,1 ,2-Trichtoroethane79414 Trichloroethene

s6-18-4 1,2,+Tric*rto|opropane95$3-6 1,2,4-Tdmethytbenzene108 67J 1,3, tTdmeflrytbenzene75414 Vinytchlonde1330,20-7 m,p-xylene9547-6 o,Xylene10s-98-9 Tetrahydrofuran@2s7 Ethyt ether9944s{ Tert-amylmelhytether637-92-3 Ethy{te(-bu9tether10s,m,3 Di-isopfop!4ether75{5{ T€rt-Butenot/butylatcohol12191-1 1,4-Dioxane

Su/ogate aecovedes:46'4tt4 4-Bromofluor1benzene

N3f -2e5 Toluena4S

I 7o6a07 -0 l, 2 -Dichloroethaoe-d4

186a-53-f Dibromofluoromelhane

f, xtraclrblE Petroleum Hydrocarbons

Extractiable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

6006{r-9 casotine6€47t30-2 Fueloit#z

6€47F31-3 FuetOi l#4

6855$00r Fueloil#6

M09800000 Motor oilJ00100000 AviationFuel

Unidenlified

Other Oil

Total Peholeum Hydroc€rbons

CSC36 Aliphatic Hydrocarbons

Sunogate recoveies:3386-3i-Z l-Chloroocledeczne

Semivol{til€ Orgrnic Compoundi by CC

Oroanochlorine Peslicides SW846 8081A

Prepared by method SW846 3545A

3090G? Aldrin

SW84682604 29-MaA7 29{.1at47 103178/ mal

+CT EIPH 27-MaF07 28-e1ar47 7031589 DS

BRL183ARLARLBRLBRLBRLBRLBRLBRLARL

BRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRL

1011019196

BRLBRLBRLBRLBRLBRL294Calculated as294294

89

!g/kg dry

trglkg drypg/kg dryyg/kg dry

!g/kg dry

!g/kg dry

Ug/kg dry

!S/lg dry

!S/kS dry

Pg/kg dry

tqKg dry

!g/kg dry

!g/kg dry

!q/kq drypS/kS drypg/kS drypg/kg dry

Pg/kg dty

!g/kg dry

UgftS drypdks drypqkg dry

rdkg drypcn(s dryp/ks dry

64.3

64.3

64.3

64.3

64.3

64.3

64.3

64.3

64.3

64.3

64.3

64.3

64.3

€d.3

64.3

u.3129

64.3

643

a+364.3ar364.3

643

1290

505050

505050505050505050

505050505050505050505050fi

fiE/kg drynE/kS drymg/kq dry

mg/kg drymg/kq drymg/kg dry

mgL/kg drymg/kg drymg/kg drymg/kg dry

70-130 %70-130 %70-130 %70-130 %

4U140%

83.683.683.6

0 3 603.603.6

03.683.6

pS/kS dry SW846 80€1A 2&Mar{7 2&MaF07 7031516 TG

fhis labontory repod as nat palu* hoat an aathodted r,jlgnatare oalhe cor psge.

* Reportable Det€clion Lirnit BRL = Below Reporting Limit Page 59 of 165

Page 268: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samule IdeotificationMrF-29 2'-4'sAs964l -12

Client Pro.iect #301 -88

Collection Date./Tim€2 I -Mar-07 00:00

MatrixSoil

Received22-Mar-07

CAS No. Analflc(s) FIaS 'RDL Dilarioa Method Rel Prcpoted Aaalyad Edch Arroltst

Semivobillc Orgrnic Codpounds by cC

Oruanochlorlne Pesticid€s SW84{i 8081A

Prepar€d by method SW846 3545A

31944{ a-BHC

3r9{t7 b-BHC

319{6€ d€HC5€{99 g-BHC (Lindane)

5r-7+9 Chlodane72-5:r€ 4.4 -DDD (p,p')72.5$e 4,4,-DDE (p,p,)

5G2e3 4.4,-ODT (p,p')

60-57-l Dieldrin959-98{ Endosulfian I33213'65-9 Endosulfen tl1031473 Endoeulfan Sufate72-a'Ug Endrin7421.93-rl Erd.inAtd€hyde76.44-8 Heptachlorf243'5 Methorychlor1024-57-3 Heptachlo. Epoxide0O0l-3S2 Toxaphene5103-71-9 a-Chtoddane5566-34-7 g_Chlodane

53a94-7G5 Endrin Ketone

Sunogate rtcoyarbsl1 qsGe+z 4,448-Oc!afl wtobiphenyl (5,)

2951-2+3 Daeachlotobiphenyt (Sr)

Polvchlorinatod Biphenvt5 w SW846 BO82Prepared by method SW846 3545A

12674-r i ,2 PCB 1016111U-U-2 rcB 122111141-1e5 PCB 12325346s-21€ rcB t24212672-2s{ PCB 12481r0e7s-1 PcB t254r10e6!2-5 PCg 12603732+23.5 rcB t262rlr0G14-,. PcB 1268

Su?oga{e a€coMeiesrt 03864+2 4,lO+Ocb,nuorcbidtenyt (Sr)

u51-2+3 De@chlorobiphenyl (Sl

Senivoladlr Olgadc Comporrds by GCMS

BRLBRLBRLBRL8RrBRLBRLBRLARLBRTBRLBRLBRLBRLBRLBRLBRLBRLBRL8RL8RL

4176

BRLBRLBRLBRI-BRLBRLBRLBRLBRL

4570

BRL

BRLBRLBRLBRLBRLBRL

lgftodry 665

ISI(1gdry 6.65pqrs dry 6.65

lgrg dry 6.65

ugkg dry 33.2

t'gfr4 dty 6 6spdkS dry 6.65

Fg/kgdry 6.65

ldtgdry 6.65

ldkgdry 6-65

rgkS dry 6.65

l€@ dry 6.65p{r^gdry 6.65pgkgdry 6.65

Lrdl1g dry 6-65

ldl(g dry 6-65

FSn€ dry 6.65

lg/lsdry 33.2

PgtS dry 6.65

IdlS dry 6.65

Uglkgdry 6.65

30.150 %3o-lf l%

pdkgdry 13.3pdkg dry 13.3

ldkg dry 13.3

ldkg dry 13.3

udkgdry 13-3

rgkgdry 13.3

tdke dry 13.3p{ykS dry 13.3

t/dlg dry '1 3.3

30-150 %30-150 %

rc^g dry 415

udkSd.y 415

Fcr19 dry 415pdlqdry 4t5pgtsdry 4'15

lgl€ dry 415

lrdkS dry 415pglqdry 415

I

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5!\446 e081A 2&ttlat4l 28-lr.,at47 7031516 TG

6W846 8062 26:Mat47 284tat47 7u]15r5 SM

SW8.r6 8270C 27.Ma147 274ta147 7ull592 M.A

Samivolatile Omanic Compounds by SW846 8270CPrepared by melhod SW846 3545483-32-9 Acon6phthenea)e96€ Acenaph$t46ne62-5$3 Anilingt20.12-7 AnttrEc€ne1912-2+9 At€zine103-33-3 Azobcnzene/Diphenyldiszinee{7,5 Benzldin€56.5$3 Benzo (e) anthracen€

2

222

2

Thb latonlary Eporl Is not volid rdthou, an uahoried slgruatr. oa the covz' page -

' Repodabl€ D€tectioE Limit BRL = BElow Reporring Limit Page 60 of 165

Page 269: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SampLe IdentiflcationM8F-29 2'-4'sA5964l-12

Clicnt Proiect #30t-88

Colleotion Date/Time2l -Mar-07 00:00

MatrixSoil

Receivcd2?-Mar-07

CAS No. Analru(s) Flag Units *RDL Dilutio^ Methotl Retr. Prcparcd A?uvzed Bstch Analjst

Semivolatile Orgsnic Compounds by CCMS

Semivolati16 Oraanic Comoounds bv SW846 8270CPreparod by meihod SW846 35454

50-32{ Benzo (a) pyrene

20+992 Eenzo (b) nuofanthene191-24-2 Benzo (g,h.i) perylene

207-08-9 Benzo (k) fluofanthene65€60 Eenzoic acid100-514 Ben2ylalcohol111-91-1 Bis(2-chtoroethoxy)methane111-44-4 gis(2-chtorcethyt)efier

3963&32-9 gis(2-chtoroisopropyl)ether

117{1-7 Bis(2€thy{heryt)phthatate101-55-3 +Brornophenyl phenyl ether85{&7 8uM benzyl phthalate86-74-8 Carbazole5s-50-7 4-Chtoro-3-methylphenol106-473 4-Chloroanitine

91-58-7 2-Chloronaphthetene9s-s7-8 2-Chlorophenol700t72-3 4-Chlorophenyt phenyt ether218{1-9 Chrysene53'7G3 Dibenzo (a,h) anhraceng132443 Dibenzofuran

96.50-1 1,2-Dichlorobenzene

5.11'731 1,3-Dichlorobenzene

10s46 7 1 ,4-Dichlorobenzene91-94-1 3,3--Dichtorobenzjdine120€3-2 2,+Dachlorophenol444f'2 Diedryfphthalet€131-11n Dimethylphthatate10tr74 2,+Damefiylphenotu-r4-2 Di-n-buvphthalate534'52-1 4,$Dinitro-2-methylphenol

51-20-5 2,+Dinitrophenoi121,14-2 2,+Dinitrotoluene60G20-2 2!6-Dinikotoluene117-84{ Di-n-octylphthalate

20€44{ Fluoranthene6-7TI Fluorenel1&741 Hexadllorcbenzene

e76A-3 Hexachlorobutadienen474 Hexachloroclclopeotadiene

6l-f?-1 Hexachloroeihane

19+3e-5 lDderb {1,2,3-cd) pFene90,12{ 1-Methytnaphthalene

78-59-1 lsophomne

91-57'6 2-M€thytnaphthatene

9s-4{-7 2-Methytphenol

108-39-4, 3,4-M€thyiphenol106,44-591-20-3 Naphthalene8a-74-4 2-Nitroaniljn€9{H)S2 }Nitroaniline

BRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRL

BRLBRLARLARL8RL8RL8RL8RLBRLBRLBRLBRLSRLSRLARL8RL8RLBRL8RL8RL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLARL

!g/kg dry 415

!g/kg dry 415

!g/kg dry 415

ugfts dry 415

!g/kS dry 415

lSi kS dry 415pSlkg dry 415

lrS/kS dry 415

rrEks dry 415

lSikS dry 415

!9ft9 dry 115

PEkSdry 415

Udks dry 4'15

US&g dry 415ps/ks dry 415pdkS dry 415pS/kS dry 415pS/kS dry 415

!g/kg dry 415

!g/kS dry 415

lSrkg dry 415

!g/ks dry 415

!g/kg dry 415

lS,lkg dry 415pg/kq dry 415ps/ks dry 415pqlkS dry 415

ldkg dry 415

Ug/kg dry 415

!g/kg dry 415

!g/kg dry 415

Ljg/ks dry 415

Pg&S dry 415

!g/kg dry 415

f.ig/kg dry 415pg/kg dry 415

!S/kS dry 415

!g/kg dry 415

ldkS dry 415

rrS/lqdry 415psfl(g dry 415

frg/kg dry 415

!g/kg dry 415

!S/kS dry 415

LigftS dry 415

i.igrkg dry 415pdks dry 415

!g/kg dry 415

ldkS dry 415

ldkg dry 41s

222

2222222222222222222222222222222222222

22222

2

222

SW846 8270C 27-Mat47 27+l,at47 7031592 M B

Thir laborato.y rcpo.t is not velA * holt an aartori.Etl sighafrne o1 the cowr page.

* R€portable Detectio! Limit BRL = Below Reporting Limit Page 6l of l65

Page 270: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-29 2'4'sA5964l- 12

Ctiepr Pmject #301-88

MatrLYSoil

Collectiofl Dat€/Time2 I -Mar-07 00:00

Received22-Mst4'l

CAS Na Anzlyk(s) FqC Uaia 'RDL Dilatinn Llahod Retr, Prcparul AMIWi Bat h A@lrsl

Semivohtil€ Organlc Conpornd! by CCMSSemivolatile Oroanic Cornoounds bv SW848 8270CPtepared by rnetFd S\tr,846 3t+5Al0{>0l4 +Nitosniline94.9t3 Nilrobenzene8&755 2-Nibophenol1('0.{2-7 +Nitophenol62.7+9 N-Nibosodimethylamine62r-€4-7 N-Nitosodi+popytamineaailo{ N-Nitrosodiphenytaminea7+4.5 Pentadoaophenol€5.{11€ Phenanthtene10e9aF2 Pharol12€{04 Pyr€ns110{6-1 Pyddine120&-1 .1,2,+Ttidllorobenzene

954t'4 2,4,$.TrfttlorophenolE8-0G2 2,4,&T.ichlorophenol

Surogde recarlsries:32150-8 z-Fluotubiphmyl367-124 2-FfuotoFllenol1165-604 Niltobenzone45411842-2 Phenot45t7lwta Toryl1enyl4l411&79-6 2,4,6-Tibtqnnpllenol

tdllg dry 1660 2

IC/tgdry 415 2

PElqdry 415 2

ldkg dry 1660 2

fldko dry 415 2pgkqdry 415 2

€iko dry 415 2pS/kg dry 415 2pdkgdry a15 2

ldks dry 415 2

udksdry 415 2

FdkSitry 415 2

UdkSdry 415 2pdkgdry 415 2psagdry 4t5 2

tu130 0k

15-110 %3tL130 %trfio %30-130 %1+1tO %

SW8468270C 27-Mat47 27iret47 7031502 H.BBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRL

676157

Totsl Metrb by EPA 60001000 Seri6 M€thod3

743+976 M€rcury BRL

Tot l Met.b by EPA 200 Seri€s Merhods

SW846 747f4 2B&la'.Ol 28.Mat47 7031€5 YP

EPA 200.7 28-lt ar{7 2g-[rar{7 7031494 RM

1 SW8461312 26-Msr47 26lrar{7 7031560 SD'1 S14/E46 1312/60108 28-Mar-07 28+vlar-07 7031651 HB

1 "

t '

1 .

1 '

1 SW8.161312'470A ' 28+,lar{7 7031652 YP

1 SW84€ 1312160104 ' 28-lrar0 7031651 HE

fitg/ko dry 0.0333

7.14(!22-4 Silver

7,r40-3S2 Arsonic

7r!0-393 Barium

744043-9 Cadmium

7440-a7-3 Chloftium

?4SS2-1 Lead

nEr'kg dry r.tl 1

org/kg dry 1.66 |

mgagdry 0.554 I

mSI(g dry 0.277 'l

flB4€dry 0.554 1

m€fl(g dry 0-831 1

nr€L/kg dry 1.66 1

BRL

BRL

15.2

BRL

7.06

t6. I

?82-1$? Selenium BRL

SPLP Metd3 by EPA ljl2 & 5000/7t00 Se.ieJ Mertrodi

SPLP ExEaclion

74,10-22-4 Silver

7rt4{t3&2 A6enic

Z.(,-3$3 Baduft

7&U){3-9 cadmium

ll40-473 Chtpnium

743947-€ Msrqrry

7tt3+92.1 Lead

Z8?-4$2 Sebolunl

G€r€ral Cbe irtry Panmeters

% Solids

mgfl 0.0200

ngl 0.0t50

mgn 0_0150

nE/l 0,m25

nEil 0.0150

rftSl 0.m04O

n'Sn 0.0150

msn 0.0150

Cornplebd

BRL

BRL

BRL

8RL

EIKl-

BRL

BRL

BRL

87.4 SM25,f0 G Mod. 24-M6147 24nnsf47 7031470 OP

Thb t,'5ordorf rqort h ,ot vdU xtitttou an oathorizal sigdraue on dr. cover p{/ge .

' R€porEbl€ Dete.tioi Limit BRL = Below R€porting Linir Page 62 of | 65

Page 271: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Salnple ldentificatiooM8F.30 2'-4isAs964l- l3

Client Proiect #301-88

MatrixSoil

Collection Date/Time2l-Mar{7 00:0O

Received22-Mar-0'l

cAS No- Anoqte(s) Flag Unil, 'RDL Dilution Method Ref. PEparcd Ana+.ed Batch Analjst

Volstile Organic Compo{nds

VOC ExtraclionVolatil,9 Oroanic Comoounds

Ug/kg dry 5I

!S./kg dry 117

!S/kS dry 5.9pdkSdry 59pg/kg dry 5IpgkSdry 5.9

ldkS dry 5.9

UdkS dry 5.9pS/kS dry 11-7pgks dry 58.6pdkS dry 5.9pdkS dry 5 I

UdkS dry 5-9

Ug/kg dry 29.3

!g/kg dry 5.9pgkg dry 5.9pgikS dry 11.7

lgkg dry 5 9pS/kS dry 11.7pgkSdry 5.9pdkS dry 5.9

lSftS dry 117pdkS dry 5.9pSftS dry 5.S

t gkg dry 5.9pC4<g dry 5.9

udkg dry 5.9pqks dry 5.9pdks dry 11.7pdts dry 5.9

!S/kS dry 5 9

ldkS dry 5-9

ldkS dry 5.9pdksdry 59

ldts dry 5.9

!g/kg dry 5-9pdkg dry 5.S

ldkS d.y 5-S

ldkS dry 5.9

UdkS dry 5-9

Lidks dry 5.9

i/dlqd.y 5.9

!g/kS dry 58.6

Lidks dry 5.9

Ug/kg dry 5 SpdkS dry 5.9

fldl(g dry 54.6

ldkS dry 54.6

UgftS dry 5.9

26.Mar-07 26'Mar-07 7031584 BDFi€ld ertEcted

Prepared by metirod SW846 50354 Soit (tow tevet)

76_111'1,1,2-Tr ichlorotr i f luoro€t fEne(FreoERL

6754 1 Ac€tone BRL10713r Acry loni t i te BRL7143-2 Benzene BRL108-86-1 Brcmobenzene BRL74-97-5 Bromochloromethane BRL75-274 Bromodichloromehane BRL75-25-2 Brcmoform ARL74{3-9 Bromomethane BRL78-93 3 2-Butanone (MEK) BRL104 5, 8 FButylbenzene BRL135 984 sec-Bulytbenzene BRL98{6-6 tert-Butylbenzene BRL7s 1s-0 carbon disutfide BRL56-2$5 Carbon t€trachloride BRL104-90-7 chlofobenz€ne BRL75-00-3 chbro€thane BRL67$6-3 CbJoaoform BRL7447-3 chloromehane BRL9519'8 z-Chlorotoluene BRL10643-4 44hiorototuene BRL96-124 1,2-Dibromo-3-chloropropane BRL124-40-1 Dibromochloromethan€ BRL106'e34 l,2-Dibromoethane(EDB) BRL74.95-3 Dibrffnornethane BRL9s-50-1 1,2-Dictllolobetwene BRLt41-7+1 l,3-Dichlorcb€nzene BRL10G4€-7 .1,4-Dichlorob€n2ene BRL15-7 1'8 Dicitorodilluoromethane (Freonl2)BRL75-34-3 l,l-Dichloroehane BRL107,06-2 i,z-Didlloroeulane aRL75'35-1 t,l-Dichloroethene BRL15e59-2 cis- I ,2-Oachlo.oethene ARL15M0'5 tran91,2-Diclhlo'ro€th€n€ aRL78{75 l,2-Dichloropropane BRL142-26+ t,3-Dichloropropane BRL59+20,7 2,z-Dichloropropane BRL5€$58'6 1,1-Dichlorop.opene BRL1006141,5cis_1,3-Oichloropmpene BRL10061{2-6tEns-1,3-Dichloropropene ARL100-114 Ethtlbenzene BRL874&3 Hexachlorobutadiene 8Rt_5sr-78€ 2-Hexanofle (MBK) BRt98 €2 8 ls(propylbenzene BRL99€7{ +lsopropyltotuene BRL1634{4-4 Methyt ted-butyt ether BRL108-10.r +Methyl-2-pentanone(M|BK) BRL7549-2 Methytene chlonde BRL

1

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SW 846 82608 27.Mat47 2A-MarO7 7031658 RLJ

91.2G3 Naphthatene

Page 63 of 165

This hno4bry rcpod Lt not ralid *,ithout zn z!rtorizeit sigaotwe on ahe cove, page

* Reportable Detecrion Limit BRL = Belo*, Repodng Limir

Page 272: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnol€ ldentificationM8F-30 2'-4.sA59641-13

Clielt Proiect #301-88

MatrixSoil

Rec€ived22-Ma.-07

Collection Date/Time2l-Mar-07 00:00

CAS Na Antu@k) Resull FW Ania *RDL Dil.lian Merhod R.tr Preparcd AnatyEd Bdch Anaryst

Vohlil€ Orgsnic Compouods

Volatil€ Oroa$ic Compour\dsPrepared by method SW845 5035A Soit (tow levet)r03{5-r n-ProPytbenzeneIOO-42-5 Styetre63(L20€ .t,1,1,2-Tei|achlorc6thane

79-3+s 1,1,2,2-Tetrachtoro€thane127-18{ T€IEd{oroelhene1offi.3 Tohtene87{1{ |,2,}Tictoaobenzener20-82-r 1,2,+Tridllorobenzene71-s+6 1, |, t -Tri{:hloroethan€79{Gs 1,t.2-Triafitoroethane79{1{ Tdchloroethene

96-1e-4 l,2.lTrichloropropane95{3-6 1,2.+Trimslhytbenzene108$7{ 1,3,s-Trimethytbenzone75-014 Vinyl c.hlorilet3$-?G7 m,pFxy'ene9s-47€ o-Xylene1c|9 99-9 T€lr€hydrofu€n60-297 E0tyt etEr994{5{ Tert_srnyl methyl eth€r637-92-3 Etiyt trsd+uvt etlEri0{120,3 Di_isopropytetfEr75{5.0 Teat-Butanot / buv atcohol123-91-1 '1,+Obxane

Sufrog€le recot€r,€s..4@-004 +B@npfluotobenzaB203/-26s Tduene4SI 706@074 1, z-Dichloroethane44186&5i-7 Abrwrloffuotumelhane

Erhrtsbh Pcfol€rm Hydroqdrons

Extraclable Tolal P€troleum HvdrocarbonsPrepared by melhod SW846 3551)8tilcr6-€1.9 Gesolin€68476-3G2 Fuel oit ,t26&+7431-3 Fuel Oiln46855100-4 Fuel Oit tt6M098o0000 Motor OilJo0100O0O Aviatiofl Fuel

UnidentifiedOther OilTotal Peboleum Hydrocarbor6Cg.C36 AliphEtic Hydrocarbons

Srnogale recoveriss--33E6-33-2 1 -ChbtRoctadecdne

Semivol$ile Orgr.tc Compounrt by cCO.oanocfibrine Pesticides SW846 8081APrepar€d by method SW846 3545A3OS(xr2 Atdrin

BRLBRLBRL

BRLBRLBRLBRLBRfBRLBRLBRL

BRLBRI-SRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRL

a6898899

BRLBRLBRL

BRLBRLBRI-475Calorlaled 6475475

110

IS/tg drypSfto dry

ldkgdryrcl(g dry

ldlg dry

v€rkodryldkg d.y

Pcrtg dry

udkg dry

ldkg dry

udkg drypdks drypolkg d.ypSftS drypgrs drypdkS dty

!S/kS dry

ldks dry

Wksdry9qtS drypg/kS dry

udks dry

UdkS d.y

lSftS dry

IgI€ dry

5.S

5.9

5.9

5_9

5_9

5.9

5.S

5.S

5_9

5.9

5_9

5.9

5.S

5.9

l1.f

58.6

5.9

5.0

5.9

5.9

5E.6

f l7

75.375-375.375.375.375.3

?5.3

75.3

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SrrV 846 82608 274n{47 zs-Mat4? 7031658 RLJ

75€+,1 Trichloronuoromethane (F.eon 1l) BRL

7u1fi%7E1n%70"130 %70-130 %

mgrkg drymgut(g drynE/kg drymg/kg drymgttg drynEI(g dry

nE/ftg dry

mgukg dry

ingr'kg dry

mgr'kg dry

+CT ETPH 27.[,lar47 28+,lar{7 ru1589 DS

BRL

,4-110 %

|ldko dry 6.11 SW846 80E1A 26-t €r{7 20-lrar47 7031518 TG

This labo.dh.f rcpod is lot vdid Nithau da aslho.iazd Jjg.totttre on the caeer IBge_a Reportable Derecrion Liorit BRL = Betow RcpqtiBg Limir P6€€ 6,1 of 155

Page 273: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationMtF-30 2'-4'sA5964 l - t l

Cliept Project #30 t.EIl

MatrixSoil

Received22-Ma(07

Collection Datc/Time2l-Mar-11? 00:00

CAS No, Aazlyte(s) Result FI"E Units *RDL Dilution Method ReL Pftpared Anabzed Balch AtutlJs.

Semivolrtile Organic Compounds by cC

Oroanochlorine Pesticides SW846 8081APrepared by m€thod SW846 3545A

31914€ a-BHC319{S7 b_8HC319€54 d_BHCs€-€$s 9-BHC (Lindane)57-74-9 Chlordane72,5,L8 4,4'_DDD(p,p')72-5*e 4,4'-ODE (p,p')50,2s-3 4,4rO0T (p,p')m-57-1 Dieldrin95+9e€ Endosullan I33?13{5€ Endosuttan ll1031{7-8 Endosullan Sutfatet2-2M Endrin7421.93-4 EnddnAldehyde76-44-€ Heptachlor7243-5 Methoxydllor1024.57,3 Heplachlo.Epoxide8001.3t2 Toxaph€ne5103-71,9 a-Chbrdane€,566-34,7 g-Chlordane

53494-70-5 Endrin Ketone

Sutrogate rccovedes:1038d842 4,4-D&Octafluotobiphenyt (So

205t2+3 Decachbtobiphenyl (Sr)

Polvchlorinated Biohenvls bv SW846 8082Prepared by method SW846 3545A

1267+11-2 PC81016111o+2s-2 PCB 122111141,16-5 PCB 123253449,214 PCB 124212n72-294 PCB 1248110S7-€9-1 PCB 1254i10e6-€2-5 PCB 1260j7324-23-5 PCB 12621110e1{-4 PCB 1268

Sutog6ls 16s6v"ti""'103864+2 4,1-DB-Octafluorobiphenyt (s4

N51-24.3 Decachlotobiphenyl (St)

S€mivotatile Organic Compounds by ffMS

BRLARL8RL8RL8RL8RLBRL

BRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRLBRLBRLBRL

45/0

BRLBRLBRLBRLARLBRLBRLBRLBRL

4575

BRLBRLBRLBRLBRLBRLBRLBRL

lguftS d'y 6.11pdls dry 6.11

lig/kg dry 6-11

US/kS dry 6.11pS/kS dry 30.5pS/kS dry 6.11

ldks dry 6.f ipdks dry 6.11pgkg dry 6.11

LrS,/kS dry 6-11

lgl(s dry 6.11

udkg dry 6.11

UdkS dry 6.11

ljg,rks dry 6.11

US/l(gdry 6.11

!g/kg dry 6.11pg/kS dry 6.1'1

ldtg dry 30.5

UdkS dry 6.11

USftS dry 6.11pdkS dry 6-11

30'150 %3Gt50%

pg/KS dry 12.2

lgftg dry r2_2

rc/ks dry 122

trS/kS dry 12.2pglkg dry 12.2pS,kS dry 12.2

!S/kS dry 12.2

US&S dry 12.2

lSftS dry '12.2

30-150 %30-150 %

1

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TGSW8468O81A 26-Mar-07 28Nar47 7031516

SW846 8082 26-Mat47 28-Mat47 7031515 SM

Semivolatilo Orqanic Comoounds bv SW846 8270CPrepared by mebod SW846 3545A8s-32-9 Ac€naphthene2oE-96{ Ac€naphthylene62-5'3 Anitine120-12-7 Anthracene1912-24S At€zin€103-33,3 Azob€nzene/Diphenyldialne92.€7-s Benzidinesss5-3 Benzo (a) anthEc€ne

pdkS drypdkS dry

!S/kS dry

!g/kg dry

ldks dry

!g/kg dry

LrdkS drypdkS dry

167

6f

467

467

467

467

467

467

5

5

5

5

5

5

SW846 8270C 27-Mar{7 274Jar-07 7031592 MB

This labontory Epotr it not ealld toithott zn authoriaed si|naturc on the eoter ple

' Reporlsble D€i€{tion Limir BRL = Belo* ReDortins Limir Paee 65 of 165

Page 274: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiorMtF-30 2'-41sA59641-13

Client P.oiect#30 t-88

MatiixSoil

Received22.l[',at47

Collectiop Datey'Time2t-Mar-07 00:00

CAs No. AnaWG) Floe rRDL Dilutiotl Method Retr. Pftpqred Aaaltud BdEh Annbs!

Semivolslile Orgrnic Compoohds by GCMS

Semivolatile Oroanic Comoounds bv SW846 8270C

ftepa.ed by method SW846 3545A50-32{ Eenzo (a} pyrene20199-2 Benzo (b) Ruofanthene191-24-2 Benzo (g,h,i) p€fylene20rc8€ Beruo (k) duoranth€ne65{5-0 Benzoic acid10G51{ BerEyleloohol111-91-1 8s(2-chloro€thory)methane1r1-414 Bis(2-ct{odo€hy)eher39638-324 Bis(2-chhroisopropyl)eh€ri17{1-7 Bis(2-ethtdhexyl)phhatats10155-3 +Bomophenyl pheflyl ethera5$&7 Butyl benzyt phthatate8&?4{ Ca.bazol€59{G7 4.chbao-}m€thytphenol106474 +Chloroaniline9r,5&7 2-ChloronaphthaleneF57{ 2-Chlorophenolruo572-3 +Chlorophenyl phenyt ether218{14 Chrys€ne5+7G3 Dibenzo (a,h) anthrac€ne132€4-9 DlbefEofuran95{+1 .1,2-Dichtorobeflzeoe

541-73-1 |,3-Dicfilarobenzene106-46-7 1,4-Did orDbenzene91-94.1 3,3'-Dichlorob€nzidinerm€:!2 2,4-Dichlo,ophenol04{+2 Dl€thyt phthllate13i-1rn Dimethyl p,hthatate105-67-9 2.+Dimetry'phenolu-7+2 Di-n-butytphhatate$a-s2.1 4,6_Dinitro-2nethytphenols1.2&5 2,4-Dinitlphenol121n4.2 2,4-Dinitrotofuene60620-2 2,6€inihotoluene117€4-0 O-n-oct!4phfialats206-,ta{ Fluoranlhsfle86-73-7 Fluorene1i8-74-1 Hexachlorcbenz€n€87-68-3 Hexachto.obutadiene11474 |lexachlorocydopentadiene67-72-1 Hexachlorcothane193'3+s Inde{ro (t,2,3-cd) prrcne9G12{t l-Me$ytnaphthalen€78-591 lsophoron€9r-57{ 2-M€thylnEphthalene95-4&7 2-M€thytphenol108-39-4, 3,4-Methylphenoli06{rt591?43 Napnhabn€€&74-4 2-Niboanillne9S{S.2 }Nitroanilin€

SW846 8270C 27+,J'€,r47 27-Mar47 703'1592 M.SBRLgRL

BRLBRLERLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRI.BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLaRtBRLBRLBRLBRLBRLBRL8Rt_BRI-BRLBRL

BRLBRLBRL

lglSdry 167

[gkS d.y 467

IdkS dry 467pdkS dry 467

FgkS dry 67pgts dry 67

lgrsdry 467

lgtS dry 467pgks dry 467

ldkS dry 67

IdkS dry 67pgtS dry 67

lgkg dry 467

ldrSdry 87

lgkgdry 447

Ug/l(g dry #7

trgks dry 67

USAS d,y 67

Isftgdry ,167pdkgdry 67pdks dry 467

!S/kS dry 467pdkS dry 467

trSI(g dry 67yqfs dry 67

tigftS dry 67pglSdry 167pdks dry 467pdksdry 467

udks dry 67

lgkg dry 467pSAg dry 67

UgrS d.y 46r

PglSdry &7

ldkS dry 67

rc/kS dry 467

ldkS dry 4G7pSikg dry 67

lgkSdry 61ygrS dry 67

lg1(S dry 67

ldkS dry 467

UdliS dry 4A7

lSitSdry 487

t dkg d.y 67pSifS d,y 67

IgrS d.y 6r

Fg/kg dry 167

fiSl(S dry 67

ldks dry 47

5

55

5

5

55

5

55

5

5

55

55

55

Thk lobomtory Eport B not vrI I wl4totd on ourhorizd sjg&trtt e od thz caeer page.

+ Reportable D€rection Limit BRL = Bdow R@ning Limir Page 66 of 165

Page 275: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationM8F-30 2'-4'sA5964l-13

Client Ptoiect #10, -88

Collection Date,/Time21-Mar07 00:00

MatrixSoil

Rec€ived22-Mar07

CAS No. Anobta(s) Re$uh FtoC Ani6 'RDL Dilation Method ReJ, Preparcd Andbzed Batch Anabst

Semivolalile Orgaric Conpounds by CCMS

Semivolatile Orqanic Cornoounds bv SWB46 B27OCPrepared by method SW846 35454

100-01s 4-Nitrc€niline9a-gt3 Nitrobenzene83-715 2-Nitrophenol100{2-7 4-Nitroph€nol62-7s-9 N-Nitrosodimethylamine621-64-7 N_Nitrosadi_n_ptopylamine86-30-6 N_NilrosodiptEDylamine87{6-5 pentachlomph€nol

85{14 phenenthrene

10&95-2 Phenol129{04 Pyrene110{61 Pyr id ine120-82-1 1,2,4-Trichtorcbenzene95-954 2.4,s_Tdchtorophenol8a-0e2 2,4,GTichlorophenol

Sunogale rccot"edes:32140-8 2-Fluorohiphenyt

36?-121 z-Fluorophenol

416540-0 Nitrobenzene'ds

416542-2 Phenol4s

1718-514 Teryhenyl4l4

118-79-0 2,4,6-Tdbromophenol

Totrl Metals by EPA 6000/7000 Seri€s Me.hods

7439-92-6 Mercury BRL

Totsl Metlls by EPA 200 Series Mcthods

27-MarO7 27 -Ma(47 7031592BRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

655758617159

BRL

BRL

12.2

o.2a4

5 .11

14_5

BRL

lSftS dry 1870pS/kS dry 67

UdkS dry 467psfis dry 1870pS/kS dry 467pEl(s dry 467pgtg dry 467

!q(g dry 461pS/xS dry 167

!S,/kS dry 467pg/kq dry 467pdkS dry 467pdkS dry 467

!g/kg dry 467

US/kS dry 461

30-130 %15-110 %30-130 %16110%30-130 %15-110 %

mg/kg dry 0_0330

mdkS dry 0.997

mgi(g dry 1.50

mg/kq dry 0.49e

mg/kgdry 0.249

mgkgdry 0.499

nStkgdry 0.748

filgi KS dry 1.50

mg/l 0.0200

mg/l 0,0150

tng/l 0.0150

mgn 0,0025

mSfl 0-0150

mg,l 0.00040

mgl 0-0150

ftr€rl OO1fi

yo

5 SW846 8270C

5 '

5 "

5 "

5 "

5 "

5 "

5 '

5 '

5 '

5 '

5 "

5 "

M-A

74t'J 22 4 Sit\tel

7440-38-2 Arsenic

741k)-39-3 Barium

7440{3-9 Cadmium

7440-17-3 Chromium

7439 92-1 Lead

n 824+2 Selenium

SPLP Metsls by EPA lll2 & 6000/7000 Sert€s M.thodi

SPLP Extraction Comp{eted

7440-224 Sitver BRL

7440-3&2 Arsenic BRL

It40-39-3 Badum aRL

74404$9 C€dmium BRL

7.1.4047 3 Chromium BRL

7439-97{ Mercury BRL

7439'92'i L€ad BRL

7824+2 S€lenium BRL

Cenrrrl Chcmistry PNrrmehrs

Y. Solids 90.5

1 SW846 7471A 28-MaF07 28-Mar{7 7031495 YP

1 EPA200.7 28-MaF07 28-l\rar,07 7031494 RM

1 "

1 '

l "

l '

1 SW8461312 2GMar{7 2fi\rar47 7031560 BO

1 SW8.{6 't 31260108 2&MaF07 28-[,laG07 7031651 HB

l "

1 ' ,

1 ' ,

1 SW8461312/7470A ' 28-MarO7 7031652 YP

1 SW846131260108 " 28+.,1ar47 7031651 HE

1 SM2540 G Mod 24-Ma'47 24-Mat47 7031470 OP

Thh lsaorclary rcpott ir nol voIAI wuh0ut an raahoriacd slgnature oa the corer page

* Reportabl€ D€tection Limit BRL = Below Repding Linit Pagc 67 of 165

Page 276: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificationMtF-312'-41sA5964l-14

Client Proiect #30t+8

MatrixSoil

Collectioll Dat€/Time2 I -Mar47 00:00

Received22-Mat41

C"1S No. A&lyte(s) FloS *RDL Dilatto.t Llcthod Rel Prcparcd llnal$,at Balch Aaalls,

Vohdle Orgrni. Compounds

Volatile Omanic ComooundsPrepa.ed by melhod SW846 5035A Soit (tow tevet)

76-13-1 |,1,2-Trid orotifuoroethane(FreoFRL SW 846 8260S 29+ne47 2g+lar47 7031779 RLJ6-l€+1 Acstone107-13-1 Adytonitite7143-2 EerEene10&€6-1 Baomoh€nzene7rt-97-5 EronrocfrloronEthane71274 Brcmodichlorcmethane712+2 Brcrnolorm74J3-9 Brcmoh€thane76-93-3 2-Butanone(MEK)104-51{ n-Bulylbenzene135.98{ s€c-Butylbenzene9S{6{ tert€utylbenzene7!15r.0 C€rbondlsutfdeg-215 C€rbontefachloride'0&SO-7 OrlorobenzenoTtrxl-3 chtoroethaoe67{+3 Chtd.oform

/dkS dry 7 _o

FsftS dry 139pSAS d.y 7.O

Fgl(g d.y 7.OpC,tSdry 7.OpdlS dry 7.O

UdkS dry 7.o

US/kS d.y 7.O

t,{,/k9 dry 'l3.9

pdkgd.y 69.5pS/kS dry 7.0

ls/ksdry 7.0pdkS dry 7 0

Udks dry 34.8pS/kS d.y 7.0

ldxgdry ropdkg dry 13.9

lg/kgdry 7.o

ldrS dry l3.g

ldkS dry 7.0

l€/kS dry 7.0

!S/kg d.y 13.9pdts dry 7.O

ldrs dry 7.0

ldtSdry 7.0

Igrkg dry 7.0

ldkS d.y 7.0

US/kgdry 7.Opgr(gdry 139

lgrs dry 1.0

ldksdry 70

$dl(g dry 7-0pdro dry 7 o

tqft,gdry 'Lo

tqtuSd(y 7.O

ldkS dry 7.o

UdtS dry 7-0

ldkS d.y 7-0

rrdks dry 7.oyS/kS dry 7.0pdks dry 7.o

fd*S dry 7.0

ldkS dry 69.5

UdlqC dry 7.0

ldkS dry 7.o

IdIg d.y 7.O

us/ks d.y 69-5pdkg dry 69.5

ldkg dry 7.o

UdkS d.y 7.0

BRL8RLBRLBRL

BRLBRLBRLBRLBRLBRLBRLgRL

BRL8RLBRL8RLBRL

1

I

1

I

1

1

1

I

I

1

1

t

1

1

I

1

1

1

I

I

I

I

1'|

1

1

1

1

1

1

1

t

I

I

1

I

I

1

I

1

1

1

I

1

1

1

1

1

1

7t-67-3 Chlommethane BRL95-49{ z-Chlorotoluene BRL106-434 +Chlorotolu€ne BRLS-12€ 1,2oib.omo-3dllorcDroDane BRL124-4ar g[bromod{ofomethane gRL

i06-$-4 1,2oib@mo€thane (EDB| BRL7+!l$3 Dibromomethane BRL95-60-1 l,2-Dichlorobenzene BRL541'73-1 1,3-DichloroberEene BRL10646'7 l,+Dlchlorobenzene BRL7t7l{ Dicf orodiffuoro.nethan€ (Freoflt2)BRl75.343 1,|-OicNoro€thane SRLi07-il6-2 1,2-Oichlo(o€thane BRL7s-35-,r 1,1-Dichlo.oeth€ne BRL15trs2 cis-1,2-Didlloireflrene BRL15640-5 l€ns-|,2-Did rroedl€ne 8RL7A47-5 l,2-Dichloropropane BRL1.2-28-9 l,3loidrloropr.opane BRL59+20-7 2,2-D{d{o.oprcpane BRL563-5e€ 1.1-Dichlo@propene BRL1{x)61{1.5 d+1,3-Diclllorcpropene BRL10061{2€U?ns-1,3-Didlloropropene BRLio0-414 Ebyt€nz€ne BRL8768-3 Hexad orobubdien€ gRL

5s1-78{ 2-Herdlono (MBK) 8RL98-82{ lsopopylbonzene BRL99{7{ +lsopropttotuene BRL163444-4 iredlyl bd-bulyl e$er BRL10e10.1 +Modltl-2fentanone(M|BK) sRL7549-2 tvlethyleie .filoride SRLfi-a}3 Naohth.len€ BRLi03€51 n.Piopylbenzene BRL

Thb lzbofllory .q,od is ,toa tdu wiahaut di ardtorw sigaurzrc on the cowt page .* R€podable D€tection Liftit BRL = B€low Repo{ting Limir Page 68 of 155

Page 277: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-31 2'-4'sA5961r -14

Client Project #30 t -88

Collection Date/Time2l-Ma.-07 00:00

MatrixSoil

Received22-Mat-07

CAS No. Analrte(s) Resuh FIag Uni,l 'RDL Dilutian Method Ref. Prcparcd Aaatrzed Ralch Andljst

Volrtile Organic Compounds

Volatile Oroanic Comoounds

Prepared by rnethod SW846 5035A Soit (tow tevet)

100-425 Styrene BRL

€n0-iD5 1,1,1,2_Tettachtoroethane BRL

79-34-s |, l,2,2_Tetrachtoroethane BRL

127-18 4 Tetrachlorcethene BRL

108€8,3 Totuene BRL

8761-6 1,2,3_Trichtorobenzene BRL

12H2r 1,2,4_Tdchlorobenzene BRL

71-5s$ l,1 ,1_Tdchtoro€thane BRL

79-oGs 1,1,2_Trichtoro€ttEne BRL

79{14 Trichloro€thene BRL75{9{ Trichlorofluorcmethane (Freon 1t) BRL

96-18-4 1,2,3.Tnchloropropane BRL

9s€$6 1,2,+Trimethytbenzene BRL

ro8{/.8 l,3,5-Trimethytbenzene BRL

7541-4 Vinyt chloride1330,20,7 m,p-Xylene95-47 6 o-Xytene109-99-9 Tetrahydrofuran

60 29,7 Ethyt ethef99,1{5{ Tert-amylmethylether637-92-3 Ethytterl-butytether10€-20 3 Di-isopropyt ether75{5{ Ten-Butanol/ butyt atcohol123-91-1 1,4-Daoxane

Sunogale recowies:4604@4 +Eromofluorobenzene

20ir-26-5 foluene4S

I 7A60 0r 4 1,2-Dichldo€thane-d4

1868-si-7 Dibrcmofluorcmelhane

VOC Extraction

Volatile Orqanic Comoounds

BRLBRLBRLBRLBRLARL

8497107107

Field extractBd

!g/kg dry 7.0

ldkS dry 7.0pdks dry 7.0

us/ks dry 7.0pdks dry 7.0pSl(gdry 7.opdks dry 7.0

lgtS dry 7.0pS/kS dry 7.0pS4(S dry 7 0

!S/kS dry 70pdkS dry 7.0

ldkg dry 7.i

UdkS dry 7.O

lgikg dry 7.O

udkS dry 13.9

ug/lgdry 7.Opg/kg dry 69.5

t4lkg dry 7 Opdkg d.y 10

ldkg dry 7.0pg/kg dry 7 O

UdkS dry 69.5

ldkS dry 139

70-130 %70-130%70-130 %70-130 %

pg/kg dry 740pg/kg dry 1480pdkg dry 74.0pdkg dry 74.o

trdkS dry 74.0

ldkg dry 74.0

ldkg dry 74-o

r€/kq dry 74.0pSftS dry 14ApdkS dry 74O

ldkg dry 74-0pg/kg dry 74.Opsn(s dry 74.0pg/kg dry 37OpdkS dry 74.O

!S/kS dry 74-O

lSftS dry 148pdkS dry 74.O

1'|1

1

1

1

1

1

1

1

1

1

I

1

1

1

1,1

l

l

1

1

1

1

505050505050505050505050505050505050

SW8460260S 2S-Msr47 29-Mar47 703177S RLJ

BRLBRL8RLARL

Prepared by method SW846 5030 Soil (high levet)

76-13-1 1,1,2-Tdchlorotdnuoroethane (Fr€o8RL67$rL1 Acetone BRL

107-13-1 Acrytonjtrile 8RL714l-2 B€nzene 8RL

108-86-1 Bromobenzene 8RL

7447-5 Bromochloromethane BRL75'271 Bmmodichtoromethane 8RL75-212 Bofioform 8RL74{}9 Bromomethane BRL78-9!3 2-Butanone (MEK) BRL104-511 n-Bulldbenzene BRL

13$98{ sec_BuMbenzene BRL

98-06-6 tert_Butytbenzene BRL

75-154 Cafton disutfide BRL

s6-23 5 Carbon tefechtoride BRL

108-90 7 Chlorob€nz€ne BRL

7tu0 3 Chloroethane BRL

67S3 Chloroform SRL

VOC 26.Mar-07 26-l ar-07 7031584

SW8468m0B 214ttar41 2g'l/,al-o7 7031642

BD

Thk labortlory report k not valid *dthoq an a.tdtoritpd sipatarc on lhe cowr prye.

* Reportable D€tccrion Limit BRL = Below ReportinC Limit Page 69 of 165

Page 278: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationMtF-31 2'-4'sA5964t-14

Cliept Proiect #301-88

Collection Date/Time2t-Mar-07 00:00

MahixSoil

Received/2-Mat41

CAS No. Anolru(s) Flog Uni.s 'RDL Dilaion Llethod Retr Preprrcd Analf.ed BaLh A8lfst

Vohlil€ Orgadc Compornds

Volalile Orqanic CommurdsPrepared by malhod SW846 5030 Soil (high levet)14-87-3 Chlorom€thane BRL9541F8 2-Chlomtoluene BRf106-43-4 +Chlorotoluene BRL9e123 1,2-Dibronro-$chloroprcpane BRLl2,Ha-1 Dibromochlorornethane BRLloH3.a i.2-Dibromoehane (EOB) ARL74€t3 Oibromornethen€ BRL95{Gl l,2.Dichlorob€nz€ne BRL54t-73r l,3oidllorob€nzene BRL106-46-7 1,4-Did{orob€nz€ne 8RL75.714 Didllomdinuorcmsthane(Freon12)BRL7+14-3 l,toichhoehane BRLr0ru6-2 1 ,2oichlo{oethan€ BRL7t354 t,t-Dichtoroethen€ BRL156-592 cis-1,2-Diciloroethene BRL15e6O5 trns-1,2-OL*tlome(nefle BRL7a€7-5 1,z-Dichloropfopane BRL142-24.9 i,3-Dichloropropaoe BRL59a-2o-7 z,2-Dichldopropsne ARL563-5€{ 1,'l-DlcHo|'opropene BRLt0061{1-5 Cis-1,}Dichloropropene 8RL10061+{ t€ns-1.}Obhloroprcpene BRL100-4r-r Ehy'b€rEene BRL476+3 Hexschlorobutadien6 BRL5e1-78{ 2-H€x€none(MBK) BRL9a{2€ lsop.opytbenzene BRL99{7{ +lsopmpylloluen€ BRL1634{4-4 l\,lethyl tort-butyl eUrer SRL10€.1Gi +iibthy'-2-p€ntanone(M|BK) BRL75{&2 ttehytene dtlodde BRL91.203 Naplrthslene 19210&6$1 tuPropylbenzeno BRLl0H2€ S0r€n6 BRL63G20€ i,1,1.2-Teb'scfiloroethane BRL79-3,1-s l.l,2,2.Tetrachloro€thane BRL127n84 T€t-achlotro€thene gRL

10€-88-3 Tdu€ne BRIa7€1€ l,2,gTdc$lorobenzen€ BRL120-82.1 .t,2,+Trichlorobenzene BRL71-55-6 1,1, t-Tri.filorcethen€ BRL79,rn!5 1,t,2-Tddtloroethane BRL79{15 Tdchlorc€thene BRL75$9-4 Trid ofoiuoronEthane (Froon 11) BRLs18-4 1,2,&Tri$lomptEp€ne BRL95€3{ 1.2,+Tdm€thylb€nzene BRL10&€7{ l,3.9Tdm€thytberEene BRL7.}071 Vinyl d{odde BRI_l33L2G7 m,p-Xylene BRL95474 o-Xylene BRLi09999 Tot-ahydrofuran BRL

pdks dry 1$

t,qikS dry 74o

ud*gdry 74.opgAS d,y 148pdkg dry 74.O

!S,/kS dry 74.O

lgtS dry 74.0

USI(S dry 74.Opdkg dry 74.O

rdks dry 74.o

lgil(g dry 148

FdkS dry 74.opdlqdry 74.o

ldkS dry 74.o

USI(S dry 74.OpglkS dry 740pgXS dry 74.0

!g/kg d.y 74.0

UdkS dry 74.O

lJgftSdry t4.opcftsdry 74.0

lcrrq dfy 74.O

ldkg dry 74.o

ldkg dry 74.O

lgkSdry 740

rgkS dry 74.0

WkS dry 74.O

Ugxgdry 74.Opyks dry 74OpgtS dry 74Opgkg dry 74.o

lgkg dry 74.0

ltgkgdry f 4.0

rdkg dry 74.0pdkg dry 74.0

lrg/kg dry 74.0

IgkS dry 74 o

lgf€dry 74.opdks dry 74.Opgks dry 71.0

ldrSdry 74.0

rc/kS dry 74.o

!S/kS dry 74.Opgikg dry 14.O

Wl(g dry 74.o

f.rgkg dry 74.O

US{lgdry 74.OpgkS d.y Ua

Lr9/k9 dry 74.O

Fdkgdry 740

50s505050505050505050

5050505050505050505050

505050505050

5050

505050

5t)5t)505050

5t)50

505050

SW 846 82608 27)'llar-O7 20+nat47 7031642 m€r

Thi' Iahonlotf rqort it aoa eaIU x,ithatt an outhoriicil slg',attarc oa rtE cover ptge.

+ R€porhble Detection Limit BRL = B€low Repdting Limir Page 70 of 165

Page 279: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatioflM8F.3t 2i-4'sA5964l-14

Client Proiect #l 0 t - 88

MarrixSoil

Collection Date/Timc21-Mar-07 00:00

Received22-Mar-01

CAS No- Analrtsb) Floq 'RDL Dilalion Method Retr. Pftparcd Analyzed Betch Analysl

Volrlile Oiganic CompoundsVolatile Oraanic ComroundsPrepared by method SW846 5030 Soit (high level)60-2+7 Ethytelher994-05{ Ted-amytmethylether637-92-3 Ethyt tedSutyj ether108-20-3 Di_isopropyiether75-6t0 Teft-Bubnol/ butyl alcohol'123-91n

1,4-Dioxane

Sunogale rccoveies:460404 +BromoflU1robenzene

203/-26-s loluene4S

1 r06co74 1,z-Dichlorcethane44

1 6EE-t+t UrDtomodlmfomethane

Ertrft table Petrol€um Hydrocarbotrs

Extractable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

S006$1-9 Gasotine68476'30-2 Fu€t Oit #26847&31,3 Fusl Oil#46855HO-4 Fuel oil #6M09600o00 Motor OilJ001o0fti0 Aviation Fu6l

Unidenlifi€d

Other Oil

Total Petroleum Hydroc€rbons lU

C9-C36 Aliphafic Hydrocarbons 1U

Sunogate rccoveies:$e6-332 1-Chloroocladecane 110

Semivolrtile Org.nlc Compounds by CC

Oroanochlorine Pesticides SW846 8081A

Prepared by method SW846 3545A

SW 846 82608 27-l\tlzt-O7 28.l.lal-07 7031642 '']'al

+CT ETPH 21-Marol 28:Mal.07 7031583 DS

SW8.46 8081A 26-Ma'-07 2a-Mat-O7 7031516 TG

BRLBRL8RLBRL8RLBRL

t03tu93s4

BRLBRLBRLBRLBRLBRL184Celculated as

lgkg dry 74.0

lgkg dry 74.0

l{r/rc dry 74.o

PgkS dry 74.opgkg dry 74O

Pgkg dry 1480

7G130%70-t30%7L1m%7G130 't

mg/kg dry 1o.2mdks dry 4o.2mg/kg dry 40.2mg/kg dry 4O.2qt/kg dry 4O.2mg/kg dry 4O.2mYkg dry 4O.2mdkS dry 4O-2mgkg dry 4O.2mg/kgdry 4o2

40-140 %

505050505050

3q9{0-2 Alddn319 84$ a-BHC319-85-7 b-BHC319,86S d€HCsa{s-e g_BHC (Lindane)57-7+9 chlordan€72-54-a 4,41DDD (p,p.)7255,e 4,4.-ODE (p,p.)5G2e,3 4,4_DDT (p,p,)60-57-1 Daeldrin9s$98€ Endosultan I33213€s-s EMosut[an tl1031.07-8 Endosuifan sutfat€72-2GA Endfin7421.S3-4 EndrinAldehyde76,4,r€ Heptachlor724+s Methoxychlor1024-57-3 HeptachlorEpoxide8001-3t2 Toxaphene5103-71-9 a-Chlofdane

!g/kq dry 7.12

ps/ks dry 7.12

f.iS/kS dry 7.12

Lig/kS dry 7.12

f.ig/kg dry 7.12

tig/kS dry 356

tig/kg dry 7.12

Ug/kg dry 7.12

tiS/kS dry f .12

t/dks dry 7-00

pdkS dry 7.12

ldkg dry f-12

Fdkg dry 7-12

lrs/ks dry 7-12

!s/kg dry 7.12

ru/kg dry 7 -12

t Sikg dry 7.12

US/kg dry 7-12

!g/kg dry 35.5

t4/kg dry |.12

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLARLARL

Thb labo&lor! reporl it notiolld rrllhou t authodze.l slgnalure on the cover pdge-

* Reportabl€ Det€ction Limit BRL = Below Reponing Limir Page 7l of | 65

Page 280: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeatificationMtF-31 2'{'sA5964 t- t4

Cli€nt hoiect #301-88

MstrixSoit

Collecrion Dat€y'Time2l-Mar-o? 00:00

Received22-Mat-07

CAS N^ Analfta(s) FW 'RDL Dtl"tion Mdhod Rel, Prcpued AE IWI Batch AnalrA

Semivol.dle Organic Compornds by CC

Oroanocfilorins Pesticides SW846 8081A

Prepared by mgthod SW846 3545A

556e3+7 g-C.h&fden€

53494-70-5 Erdrin lGtofl e

S!,rogeie rEcol€ri,gs-1 03a6a+2 4,+Dgoctafl @@Nphenyt ( 542051-2+t Cl€cachbrobipt€fl1 (Sr,

Potucfrbrinated Biohenvls bv SW846 8082Prepared by rnehod SW846 3545412674-11-2 PCB 101611tO+2&2 PCB 1n11rr{1-16{ PCB 12325346+2r-9 PCB 1242126?2,2s{ rcB 1248110974Sr PCB 125411096-82.5 PCB i26037321-?3.s PCB 12621110G14.1 PCB 1268

Sunogate recovorrbsr| 038f.8+2 4, 4-D&Octaf, uombipheflyt (So2061-2a,3 Decad otobiphonyt (Si

Semtvol.railc OiErnic Col|rporEds by GCMSSemivolatil€ Oroanic Compounds bv SW8,l6 8270CPrepared by rnelhod SW846 3545AE3-32€ Acenaphth€ne20&9e€ Acenaphtht4€ne62-53-3 Anitine12G12-7 Anthrac€nei912-24.9 Al?zjne10$33-3 AzobenzendDiphenydi6zine92{7-5 Benzidine56-513 Benzo(a)enlhrscene50-324 Benzo (a) pyr€ne2os€9-2 genzo (b) fuoranlhene1e1-242 Benzo (g,h,i) p€Mene20t{84 B€flzo (k) fluorantiene65{5{t B€nzoic acid10G51{ Eenzylalcoholr11.91.1 Bis(2.dhloroefliory)mehane11t41.4 Bis{2d o.o€thyt)ehor3963&32-9 Bis(2-chlof Disoprotrryl)ether117€1-7 Bis(2-ethylhexythhtnabte101-5$3 +BrofiDoph€nylphenylether8s6s7 Buq/ benzy phthatate&?4{ Carbazole59-5G7,{-Chbto-}methylphenoll0€.{7{ 4-Chlom,adline01{tl7 2-Chtoronaphthalenegtr?a 2-Chlorophenol7m+72'3 +Chloropheny4 phenyt ehef2181X$ Chryseno

BRTBRL

611U

SRLBRLERLBRLBRLBRL17.rBRLBRL

6080

BRLBRLBRL9298RLBRLBRL81412001,O20

1 ,160BRLBRLSRLBRLSRL

BRLBRLBRLBRI-BRI-BRLBRLBRLBRL1.390

pdks dry 7.12pgikgdry 712

30-150 %30-150 %

tgksdry 14.2

US/kS dry 14.2pdrgdry 14.2

ldks dry 14 2pgkgdry 11.2pdk0 dry r4.2

lrgts dry 14.2pdkS dry 14.2pgrS dry 14.2

361ff i%30-1il./.

SW845 8081A 26-Mar47 26-1ra..07 703'1516 TG

ldkS dry .199

Fdksdry 499p9ik0 dry 499pSn(g dry 4SgpEkg d.y 499

lgrg dry 499

FS/kS dry 499pS/kS dry 499

IdkS dry 499

tdl€dry 499

l,gAS dry 499pgkg dry 4Sg

trdks dry 40SpSn(S dry 499

tl€/ks dry 499pgikS dry 499psrts dry 499pqkgdry 499pdxg dry 4ss

!9rS dry 49€pqkg dry 499pS/l€dry 49SpS&gdry 49s

lqkgdry 499pgkgdry 499

rdkSdry 4ss

ldkg dry 499

I

I

1

1

I

I

1

I

1

I

I

I

I

I

1

1

1

I

1

I

1

I

I

I

1

I

1

SW8,l6 8270C 27-M3,t47 27.tulat47 7031592 M.B

Thls bboratt,l ..port is aal valid ttlthoat on outhodzed tignatare on lhe cots We .

i Reportable Det€cri Limit BRI- = Belour ReportiEg Limir Pag€ ?2 of 165

Page 281: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationM8F-tr 2'-4'sA59641-14

Client Proiect #l 0 l - 88

Collcctior Datc/Time21-Mar-07 00:00

MatrixSoil

Received22-Mar-07

CAS No. Anaute(s) Floq *RDL Dilution Method Rel, Prcpued Anrbzed Batch Analyt

Semivolatile Orgenic Compounds by cCNtS

Semivolalile Oroanic Comoounds bv SW846 8270CPropared by method SW846 3545A

53,70-3 Dibenzo (a,h) anthaacene132-€,{-9 Dibenzofuran9tsG1 .t,2-Dichtofobenzene

4,41-73-1 1,3_Dichtofobenzene106-467 .1,+Dichtorobenzene

91-S4-1 3,3-Oichtofobenzidane12083-2 2,zlDichlorophenol64{+2 Diethylphthatate131-11-3 Dmethyl phttialate

105-67,9 2,4-Dimelhylphenolu-7+2 Oin-butytphthalate534-52-1 4,6-Dinitro-2-nethytphenol

51-2V5 2,4-Dinihophenol121-1a-2 2,4-Dinitrotilluene006,?0-2 2,6.Dinit'otolqene117{44 Di-n-octylphhatate206-44{ Fluoranthene86-73-7 Fluorene114-74-1 Hexachlorobenzene87{83 H€xachlorobutadiene7r4T4 Hexachlorocyctopentadiene67-72-1 Hexachloroethane19il-39-5 Indeno (t,2.!cd) pyrene9{!12{ l-Methylnaphthatene78-5S1 lsophorcne91-57$ 2-Methylnaphthatenee5-48-7 z-tltethy'phenol

10+39-1, 3,4-Methylphenol106-44-591-20-3 Naphthelene8€-74{ 2-Nitroanitine99{!'-2 3-Nitroanitiner00{r1{ 4-Nitoanitin€

9€-95-3 Nifobenzene6&75-5 2-Nitrophenol100{2-7 4-Nitrophenol62-7S9 N-Nitaosodim€thytamine621S-7 l,lNitrosodi-n-propylamine86J0-6 N-NitrGodiphenylamine87€6-5 Pentachlorophenola9O1{ Phonanthrcne10&95-2 Phenol129-004 pyrene

110,86,1 Pyridine12G82-1 1,2,4-Trichlofobenzene9t95-4 2,4,$Trichlorophenol€a-0S2 2,4,elricfilorophenol

Surrogale recover'esj

i2140-l 2-Huorobiphenyl

367-124 2-Fluorophonol

41As-6o4 Nilrobenzene4s

BRLBRLBRLBRLBRLBRL8RLARLBRLBRLBRLBRLBRLBRLARLBRL3,090BRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL

BRLBRLBRI8RLBRL8RLBRTBRLBRLBRLBRL1,890BRL2,970BRLBRLBRLBRL

67

60

pg/kg dry 499

ldkS dry 499

US/kS dry 499pdkg dry 499pdks dry 499

!g/kg dry 499

!S/kS dry 499

US/kS dry 499pS/kS dry 499

Ug/kg dry 499

!g/kg dry 499

!g/kg dry 4ggpdks dry 499pdkg dry 499pqkS dry 499

!g/kg dry 499

USftS dry 499

ldkS dry 499

UdkS dry 499

US/kS dry 499pS/kS dry 499

ldkS dry 499pg/kg dry 499pg.4<S dry 49SpSftS dry 499pgkg dry 49S

ldkS d.y 499po/kS dry 499

pgiks dry 4SS

!g/kg dry 4SS

USlkSdry 499

UdkS dry 2000

!g/kg dry 499

udkS dry 499pg/kg dry 2000

lSftS dry 499ydkg dry 499

t g/kg dry 499

rrg/kg dry 499

!g/kg dry 499

!g/kg dry 499

!g/kg dry 499

!g/kg dry 499

ldkS dry 499

UdkS dry 499

UdkS dry 499

30-1s0 %15-110%30-130%

swE46 8270C 27-MarO7 27-Marn7 7031592 M.A

Thi! labotutoty rE ort h wt valid a'ithou an authorized ignatue on ths coter page

* Reporhble Detection Limit BRL = Below Reporting Limit Page 7l of 165

Page 282: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8F-312',-4'sA5964l-14

Cli€nt Proiect #301-88

Collection Date/Time2l-Mar-o7 00:00

MahixSoil

Received22-Mar-07

CAS N^ A alr,e(s) nesaU n^g UEia ,RDL DiIt4ita Method Rctr Prepared Amlyzed Batch Anaqst

Semivolrtile Orgr|rk Compounds by CCMS

Semivolatile Orqanic Compounds bv SW846 8270CPreparcd by mehod SW8il6 3545A

4166-62-2 Phenoldi 541718-514 Terphenyl4l4 75118-79-o 2,4,6-Tribmmophenol 66

Total Metrli by EPA 60fiy7000 S€rt€s Method!

7439-974 Mercury 0.753

Total M€lrb by f,PA 200 Sedes Metbodi

74,{r.224 Silver

7440'3&2 Arse'lic

74-4+3+3 gadum

7440-43-9 Cadmium

7,H047.3 Chromium

7113942-1 Lead

7782-4+2 Selenium

SPLP Exbaclion

7.40-224 Salver

74.4-3&2 AFenic

74,4G3+3 Earium

?440-4a9 Cadmium

74i[]47.3 Chromium

743$97{ Meac!ry

7439€21 Leed

202-,r+2 seleoium

G€n€ral Chemislry Prr{met€rs

% Solids

trf lo%30,130 %t1110Yn

mgL/kg dry 0.0(,69

fiigl€dry 1.m

mSikS d.y 1.E0

nEftg dry 0.599

nvl(g dry 0-299

'rB/kg dry 0.599

rE/kg dry 0.8S8

mg/kgdry 1,80

ll€n 0.O2O0

mgl 0.0'l5t)

mg,t 0.0150

rEn 0.0025

ndl 0 0150

mSI 0-fi1O4O

mSiI 0.0150

mg/t 0.0150

%

SW846 E270C Z7-Met47 27-lIiet47 7031592 M,B

SPLP Mead6 by EPA lf 12 & 600{y7000 sede3 Methods

1 SW846 7471A 26-MarO7 28-Mat47 7031495 YP

1 EPA 200,7 2A4td-O7 28-Mat47 7031494 RM

1 "

1 '

1 '

t '

I '

1 SW846l3t2 2flUaF07 26-Mer{7 7031560 6D

1 SW8461312/60108 2A:Mat47 28-[rsr{7 7031651 HB

1 '

1 "

1 '

1 '

1 SW84613'12t470A ' 2g4 d-07 7031652 YP

I Sw8,|ti 1312r'ffi108 ' 28-t a.-07 7031651 HB

1 "

1 SM254 G Mod. 24+rar-07 2+MarO7 m31470 OP

BRL

9.77

134'1.88

12.O

BRL

Comd€led

BRL

BRL

o.0242

BRL

BRL

BRL

0.025.1

BRL

80.7

Thi| lrbotuory nporl b dot tdU w holt an .uhodz.l slgadwe on thc corer page.

'R€portabl€ D€tection Lioit BRL = B€low Repoding Limit Page ?4 of 165

Page 283: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationM8F-32 2-4,sA595l7-07

Client Proiect #301 -88

MahixSoil

Rec€ived

20-Mac07

Collection Date/Timel9-Mar-07 00:00

C,4S fib. Ana|!te(s) FI0C 0ii6 *RDL DiTuio,' Method ftetr Prcparc[ Analt'zed Balch Analtsl

Voladle Organic Compourds

VOC ExtraclonVolalile Oroanic Compounds

pgtkg dry 6.2

udks dry 124

US/kS dry 6.2pSI(S dry 6.2ps/kg dry 6.2

udkS dry 6.2pglkg dty 6.2

UEkg dry 6.2

!Er(g dry 124

!g/kg dry 61 8pg/kg dry 6 zug/kg dry 6.2peksdry 6.2

US/kS dry 30.9

PdKg dry 6.2

tfg/KS dry 6.2

Ug/Kg dry 12.4pg/kg dry 6.2

@kg ctry 12.4pS./kS dry 62

!g/rg dry 6.2

WkS dry 12.4

lSftS dry 6.2pS/kS dry 6.2

r.|g/kS dry 6.2

!g/KS dry 6.2

!g/kg dry 6.2

lgrrkg dry 6.2pgkg dry 12.4

!g/kg dry 6.2

tlS/RSdry 6.2

!S./kS dry 6.2

!g/kg dry 6.2pS./kS dry 6.2

!g/kq dry 6.2pg/kg dry 6.2

tlStkgdry 6.2

t g/kg dry 6.2pg/kg dry 62pg/kg dry 6.2pS/kS dry 6.2pdkS dry 6.2pg/Kg dry 61.4

lrg/kg dry 6.2pg/k0 dry 6.2pS/kg dry 6.2

t4/k9dry 61.8pg/kS dry 61.8yg/Kg dry 6.2

21.Mat47 214J1,at4t 7031261 aDField extracted

Prepared by method SW846 fO35A Soit (tow tevet)

761T1 1,1,2-Ttichtorotdhuorcelhane (FreoERL674+1 Acetone BRL107-13-1 Acrylonitrite BRL

B€nzene BRL104-86-1 Bromobenz€ne BRL74-97,5 Bromochtorom€thane BRL75-27-4 grornodichloromethdne aRL75-25-2 Bromofom BRL74{3-9 Brornomelhane BRL78.93 3 2-Butanon€ (MEK) BRL104 s1€ n-&ltylb€nzene BRL13s-98€ sec-Butylbenzene BRL9A{6{ tert-EuMbenz€ne BRL7s-1H Carbon disulfide BRL56-23-5 carbon tetrachloride aRL10&so-7 chlorobenzene 8RL754G3 chloroethane 8RL67.{j6-3 chtoroform BRL71-J7,J Ch/oromethane BRLs5.19-8 2-Chtorotduene BRL106-434 4_Chtorotduene BRLr,6-i2,8 1,2-Dibromo_3drtoropropane BRL124'.ia'1 DabrcmochlorcmedrEne BRL106-s34 1,2_Dibromoethan6(EDB) BRL74-95-3 Oabroolomethane ARL95-5G1 l,2-Dichlorobenzene BRL5'41-73-1 1,3-Dichlofobenzene BRL106-a6'7 l,4-Dichlorcbenzene BRL15-114 Dichtorodifluoromethane(Freon12)BRL75-X4-X l,l-Dichloroethane BRL107-06-2 |,2_Bichtorcethane BRL7s-35-4 1,.1-Dichlom€thene BRL15859'2 cis-t,2-Dichtoroethere BRL1s6-60.5 t?ns_t,2_Didrtorcehene BRL78{7-5 l,2-Dichtoropropane BRL142-28-9 l,lDichtoropropane BRL594:D-7 z,2_Oichloropropane ERL563-58€ 1,1-Dichlo|.oplopene BRL1006141-5 cis_.1,3_Dichtoroprcpene BRL10061-0?6 t?ns-t,3-Didllorcpropene BRL10(!-41.1 EUtyjbenz€ne BRL87{8-l Hexachlorcbutadiene BRLs9r-76€ 2_Hexanone (MgK) BRL98{2{ lsopopylbenzene BRL99{75 4-lsopropyttotuene 8RL1634{44 Methyltert-butyteth6r BRLr0s10-1 4-Methyl-2-pentanone(M|BK) ARL75-09-2 Methylen€ chtorid€ sRL

SW 846 82608 22.Mar47 23+4ar47 7031335 RLJ

BRL91-&3 Naphthalene

Page 12 of 124

This lthorolory rcpod B not tatid *ithoul li a.!rtofiaed signatarc on the corer page .

' Reportable Det€ction Libit BRL = Below Reporting Limit

Page 284: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 285: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldetrtificatiooM8F-3! 2-4'sAJ9517.07

Clielt Proiect #301-88

MatrixSoil

Received20-Mar-o7

Collection Date/Timel9-Mar-07 00:00

CAS No. Anabte\) FI"S 'RDL Ditation Method RpJ Prepured Aulyzed Bat!:h At tstVolatile Orgrnic Compounds

Volalile Orqanic Compounds

Prepared by m€thod SW846 5035A Soit (tow levet)

10+6+1 n-Prcpylbenzene BRL'10(F42 5 Styrone BRL63G205 1,1,1,2-Tetrachloroethane BRt79-34-5 1,1,2,2-Tetrachloroehane BRL'127J8-4

Tetrachtoroethene 8RL10&€43 Toluene BRL87{15 1,2,}Trichtorobenzene BRL120€21 1,2,4-Trichlorobenzene BRL71-55-6 1,1, t_Trichloroethane BRL79{o 5 I,1,2-Trichloroethane BRL7941{ Tric oroethene BRL7549-4 Trichtorofluoromethane (F.eon 11) BRL96'14-4 l,2,3-Trichloropropane 8RL95€3-6 1,2,+Trimethylbe0zene BRL108-67{ 1,3,5-Trimed1ylbenzene BRL75{1'4 Vinyj chtoride BRL133G2tr7 m,p_xylene9547{ o-Xytene109-99-9 Tetrahydrofuran60,?9-7 Ethli ether99.-05€ Tert_amylmethytether637-92 3 Elhyttert-butyl elher108.20-3 DisopropytetfE.7s354 T€rt-Bubnol / butytalcohol123-s1.1 1,4-Diorane

Surcgate rccoveries:46040-4 +Bomofluoro,benzene

2037-26-5 Toluene4S

1 706e07 0 1,2-D bhloroelha ne.d41866-5J / Dibromofluoromethane

Ertrrctable Pettoleum Hydrorrrbons

Eidractable Total Petroleum Hvdroca rbonsPrepared by method SW846 3545A

8006-61-g Gasoline68.{76-30,? Fuet oil #26847e31,3 Fu€t Oil #468553{01 Fuet Oil #6M09800000 Motor OilJ00100000 Aviation Fuel

Unidentified

Other Oil

BRLBRLBRLARLBRL8RLBRLBRLBRL

1041061 1 5105

BRL8RLBRLBRLBRLBRL450Calculat€d as

pdkS dry 6.2pdks dry 6.2pg/kg dry 6 2pg/kg dry 6.2

ldkS dry 6.2

ldkS dry 6.2pSl(S dry 6.2pdks dry 6 2pdks dry 6 2

ISAS dry 6.2

!S/kS dry 6.2

irS/kS dry 6.2

!S/kS dry 6.2

!g/kg dry 6.2

Ug/kg dry 6.2

t/9/k9 dry 6-2pdks dry 12.4

ugksdry 62

tS,kg dry 61.8pdkSdry 6.2pg/kg dry 6.2pgikS dry 6.2

ldkS dry 6.2

!S/kS dry 61.8

lgkSdry 124

70-130 %70-130 %70'130%70-130%

nrg/kS dry 147

nlgftS dry 147

nrgr'kg dry 147

nBrk0 dry 147

frg/kg dry 187

B€/kg dry 147

mgtS dry 147

mdkS dry 147

mg/kg dry 147

wlks dry 187

44-140 %

1

1

1

1

1

1

l

1

1

I

1

1

1

1

l

1

1

1

1

1'|1

I,l

1

SW84682604 22-MarO7 23 Mar47 7031335 RLJ

+CTETPH 22-Mat47 26-Ma(47 7031284 DS

TotalPeboleumHydrocarbons 450C9-C36 Aliphattc Hyd.ocarbons 450

Sunogale ecorledes:i3eG$-2 1-Chloroocladecane 147

S€mivol.til€ Orgrnlc Compounds by CCOrcanochlorine Pesticides SW846 EoB1APrepared by method SW846 35508309{0-2 Atdrin BRL udrs dry 6-62 SW846 8081A 22-MaFO7 27-Met47 7031275 TG

Thi! Iabofatory rcpod is not valid tellhorlt 4n 4urtoriud slgnatarc oa the cotet page .

' Reporta5le D€tedion Lirnn BRL = Below Reporting Limit Pase 33 of 124

Page 286: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeotifica.tionM8F-32 2-a'sA595l7-07

Client Project #30 t-8t

Matrixsoll

Collectioo Dater'Timel9-Mar47 00:00

Rqceiv€d20-Mat4'l

CAS No. Analrb(s) Raak FI'g 'nDL Dilutinn Method Retr Pnpuen A&abzzd Barch AnalFt

Scmivol.lile Orgrdlc Comportrds by GCOrqanochlorine Pestrcidcs SW846 808.1APrspared by rnethod SW846 3550831+€a{ e-8HC319{$7 b-Bl{c319.€6-8 d€Hcsa{se g-BHC (Undane)t-1+s C-hlordane?2-54-8 4,4-DDO (p,p')72-s+e 4.4ODE (p,p')5[2e3 4,4DDT (p,p,]60{7-l DlsHnn95+98{ Endosrrlfsn I!3?13€5-9 Endo6ulfan ll103'l4T-8 Endosllfansulfate7?.20-8 Endrin7421.9!4 Endrin Mehyde78.11.8 Heptachlor72-13-5 ilbtho)rychlor1024-573 Heptact{of Epoxide80or-3s2 Toxaphene5103-71.9 e-Chlofdane5,5:6C34-7 g_Cihlofdane53a9+7G5 Endrin Ketone

Suroga{o recovsridsrt o3a6atz 4,4418-Octafl @robiphenyl (SlN51-2+3 &cachlotobiphenyt (SiPolvchlorinated Bbhenvls bv SW846 8082Prepared by method sw846 355081267+1r-2 rcB 101611104-28-2 PCB 1221r114i-t6-5 PCB 12325346921€ PCB | 24212872-?34 PCB 1248i10€7€91 PC8 12541109&e-5 PCB 12603732+n-5 PCB 1262rilq}la.l pCB 1268

St aro$le r€coyelt6$.'10i864+2 4,4-D&Odaauotobiphonyt (SiN5t-2+3 Deca&brobbhenyt (Sr)

Semlvol.r|b Orgrtrtc Compound! by GCMS

8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI.BRL8RLBRLBRL

30

BRLBRLBRLBRLBRL39.0

BRLARL

3055

BRLBRLBRL

BRl-BRLBRLARLBRL

rdxgdry 6.62pdrq dry 6.62

uqkS dry 6.62pg^gdry 6.52pqrs dry iX,.1

rdkg dry 6 62

t dlq dry 6.62

WkS dry 6.62yg^g d.y 6.62p4kg dry 6.62

ldrgdry 6.62

udkS dry 6.62

ldkS dry 6.62

tglksdry 6.62

udkgd,y 6.62

udks dry 6.62

IdkS dry 6_62pdkS dry 33,1pglkSdry 6.62

Fgtgdry 6.62

Fdkg dry 6.62

*150%3G150 %

ldlgdry 132

rdxs dry 13 2pS4€dry 13.2

ugxgdry r32pgfgd.y 13.2

ldl€dry 13.2

ldkgdry 13.2

vdkSdty 13.2pg4!g dry r3.2

so-150 %yrt50 %

pS/kS d.y 527

ldkgdry s27

uen(gdry g27

pdkS d.y 927

rcn€ dry 927

tglkgdry 927pdl€dry 927

Fgrgdry 927

1

1

1

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SW846 80814 22-l{at47 27n d47 7(]61275 TG

SW846 8062 2-1tur47 24l.i/.3tr47 7031274 MP

Semivolatil€ Omadc Compounds bv SW84€ 8270CPreparsd by moolod SW846 35508a3{2.9 Ac€naphthenez)&se€ Acenaphtlrylene6-2693 Aniline12Gi2.7 Atthlacens1912-2+9 Atazh€10133-3 Azob€nzene/Diphenyldiazine92{7's Bemijine56{+3 Eenzo (e) anthracen€

SW846 8270C ?}Mat{7 2$rar-07 7031371 M.g

22

Thb btoratory rcpo is noa ealitt uAhoal a sulhottat! signatue .m thz coeer page.

'Reportsbl€ DerectioD Limit BRL:Below Repnting Limit Prge 34 of 124

Page 287: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IderltificationM8F-32 2il'sA595l7-07

Client Proied #301 -88

Mat.ixSoil

Collection Dare/Timel9-Mar-07 00:00

Received20-Mar-o7

CAS No, Analrte(s) Flag *RDL Dilutbn Method Rej. Pnparcd AnzllEed Batch Analyt

S€miyolrtil€ Organlc Conpounds by cCMS

Semivolafile Oroanic Comoounds bv SWB46 8270CPrepared by method SW846 35508

&-32-a Benzo (a) pyrene

205-992 Eenzo (b) nuoranlhene191-2+2 Eenzo (g,h,i) perytene

m7{8-9 Benzo(k)fluoranthene65 65-0 Benzoic acid10051€ BenzylalcDhol111-91-1 Bjs(2-chloro€thoxyrnethare111-4.4 8is(2-chtoroethyl)ether3963s32-9 Bis(2-ohloroisopropyt)ether117'81-7 Bis(2-€thythexyt)phthatate101-55-3 +grcmophenyt phenyl ether456&7 Butyl benzyl phthalate86-7,L8 Cabazole595e7 +Chloro_lmethytphenol106-47-8 +Chloro€nitine9l-s&7 2-Chloronaphthatene9s-57-a 2-Chlorophenol7005-72-3 zl-Chlo.ophenyl phenyt eher218-01-9 chrysene53-7a3 Dibenzo (a,h) anthracene132{+9 Dibenzofuran95-5G1 1.2-Dichlorobenzenes41-73-1 .t,3-Dichtorobenzene

10S46,7 1,4-Dichlorobenzene91-94-1 3.3'-Dichtorobenzidine't2oat2

2,4-DichJorophgn1t8446.2 Diethylphthatate131-11-3 Dimethylphthalete105{7-S 2,4_Dimethylph€nolu-74-2 Di-n-butytphthatate53.L52r 4,6-Dinitro-2-methylphenol51-28-5 2,4-Dinitrophenol121 1,12 2,+Dinitrololuene606-20-2 2,o-Dinitrotoluene117-84{ Di-n-ocMphthalate206-44-0 Fluoranthene86.73-7 Fluorene11&74-1 Hexachlorobenzene8748-3 Hexachlorobutadiene't74r4

Hexachlorocyclopentadiene67-72-1 Hexachloroethane1s3-3e-5 Indeno (1,2,3{d) pyrene90-12{ 1-Methytnaphthalene76-59-l lsophorcne91-57{ 2-},tbthylnephthalene9548-7 2-Metrylphenol

l0&39-4, 3,4-M€thylphenol10G44-591-20-3 Naphthalene84,7{-4 2,Nitroanitines9-o+2 }Nitroenitane

BRLBRL1 , 3 1 0BRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLERLBRLBRLBRLBRLBRLBRL8RL8RLARLBRLBRLARLBRLBRLSRLBRL8RLBRL

BRL8RLBRLr,520BRLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRL

BRLBRLBRL

22?2222

2222222222222?2222??22

22222?

222222

22

222

!g/kg dry 927pdkgdry 927

lgxSdry 927pgn(g dry 927

PgkS dry 927pgks dry y27

pslksdty 927pdkgdry 927pg/kS dry 927

!g/kg dry 927

fig/kg dry 927

ridkS dry 927

frg/r(g dry 927ggks dry 927

f.igkS dry 927

Ug/kg dry 927ygks dry 927pg/kg dry 527

l4/Kg dry 927pg/&s dry 927

!g/kg dry 927

t dkg dry 927

!g/kg dry 927pdkS dry 927

ldkSdry 927

ldkgdry 927

!g/kg dry 927pdks dry 927

ug/&dry 927

!g/(g dry 927

lgkSdry 927

ldkS dry 927

uqkgdry 921

lqkg dry 927

uqkgdry 927

lJg^S dry 927

uqkgdry 921

ug(S dry 927

lqkSdry 927

!g/XS dry 927

lqkgdry 927

!g/kg dry 927

ldkS dry 927

ldkg dry 927

ldkg dry 927

Igftgdry 927

Idkg dry 927

UVkS dry 927

lgikS dry 927

lvkg dry 927

SW84E A27OC 23-Mat47 25-Mafi7 713fin M.A

Th labotutot] repod b not ealid hthhoul an aulhortzed sbnslate on the oeer Fage.r Reponable Det€ction Lnnft BRL = Below Reporting Limir Page 35 of l?4

Page 288: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeotificationM8F-32 2-{'sA595l7-07

Client Project #301-88

MarrixSoil

Received2GMa.47

Collestioo DardTime1lMar47 00:00

CAS NtL A,.abE(s) nesuh F,Ag +RDL Dilution Method Retr Prcparai ,4aalyzctt Datch Analfsl

S€divohtil€ Orgarlc Collportrds by GCMS

Somivolaiilo Oroanic Co.n@unds bv SWE46 8270C

fteparcd by merhod SW846 355081(){141 $ +Nito€niline984+3 NiboberEene84.7+5 2-Nibophenol

10G02-7 +Nitophenol62-7*9 N-Nibcodimethylarnine

62t44-7 N-NitcodirFpropyt€mine86-3t{ N-Nibosodiphenylamirc

87{G5 P€nladllofopheml

8s-01.8 PhenanthEne

r0eF99!2 Pheiol

t2s0{}.{) P},rene

11c86-i Pfidine

12GS2-1 1,2,{-Td{$lo.obenz€n€

2,4,$Trid orophenol8€{e2 2,4,6.Tdchlorophonol

S@rogale rccoveies:

3214c.8 2+hJorobipheny'

6H2a z+ludopllenol

1165-il4 Nilrobanzene4s

416s-62-2 Phenol4s

1718514 Terphe44t4

118-79-6 2,4,6Tdbronophend

Tord Mearb by EPA 6tt00/7000 seri6 Methods

7439-974 Mercury 0.0S85

Tolrl Mctrk by EFA 20O Seri€! Methods

2 SWA46 a27QC 2SMar-07 25-Ma.{7 70iI1371 M.g2 '

2 .2 '2 '

2 .

2 '2 .2 "2 '

1 SrrV846 74714 2&Mer47 27][tat47 7O3r322 YP

'| EPA?OO.I 2aMaf47 2f'dnat47 7031321 HB

1 "

1 '

1 '

1 SW6461312 22+nar.of 22itar47 70313,14 Bt)

1 SW8A6!312/6OI0B 2&tja(-07 24-Mar47 7O314OB LR

1 '

1 '

1 '

1 SWA.451312?470A ' 26.t{ar-.07 7m1409 YP

1 SW8,l6 1312€{tl0B ' 24.'.''iar47 7ml4m LR

1 '

Garerd Ch€mirtry P|]rtdetetr

% Solids

rrgkS dry 3710

rg,lg dry 921pgAgdry 927pS4gdry X710

ldkgdry 927

ldkS dry 927pdkS dry w1ygtks d.y 921pdks dry 927

ldkS d.y 927

lgrgdry 927

udkgdry {2rpg/kg dry s21

!S^0 d.y 527ps*gdry 927

n-rw%1i-fiO %36130 %18110 %30.130 %1&110 %

mg/kg dry 0.033i'

nrdkg dry 1 .0S

ntgrl€ dry 1.63

nrgikg dry 0.544

nE/ks dry 0272

n\gnqdry 0-544

mglt(g dry 0 El6

rtg/f,g dry 1.63

mg/l 0.0100

ngr 0.0150

ttrgl 0.0050

mSI 0.0025

mgur o.0o5o

flgI 0-00040

nrgl 0.m75

mgl 0.0150

%

BRLARLBRLBRL8RrBRLBRLBRLBRLBRL2,570BRLBRLBRLBRL

1A86

88

74a0,22-.t Silver

7/1403&2 Atsenic

7t40-3g3 Eadum

74-{OJ}9 C€dmium

74a0_!7-3 Ch&miun

7.1t992.1 Lead

7782-1$2 S€lenium

1 . 1 8

8_03

55.4

0.931

7,01

177

BRL

SPLP M€trk by EPA 1312 & 6000/7000 Scrt€r Metbods

SPLP Exbaction Completed

7l!l+?24 Silv€r BRL7{1{}-3&2 Arsenic BRL

7r!rG3e3 Badum 0.0126

7+r'(}4ils cadmium BRL7+{}rl7-3 Chrcmlum BRL

74N€7-6 l$€i.{llr/ BR!7:|l1942r Lead 0.0179

n82'492 S€l€niuin BRL

88.3 SM254O G Mod. 24-Mad7 24+rar-07 70314€3 OP

Ihb labodoty npoA ts nof valid x,itho4 an et hoiud stgrrdlare od ahe covrx pagc.

. Reporebl€ Derection Limit BRL = B€low Repo.ting Limit Page36 ot 124

Page 289: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SampLe IdentificationM8F-33 2'-4'sAs964l-15

Client Proiect #301 -88

MatrixSoil

Received22-Mat-01

Collection Date/Time2l-Mar-07 00:00

CAS No. Anrlye(s) Flag *RDL DiIAian t{ethod Retr. Pnpoted Adoltzed Batch A4a4st

Vohtile Orgrnic Compoundl

VOC Extraction Field extfacted

t g/kg dry 55

!g/kg dry 109

!g/kg dry 5.5pgkS dry 5.5pS/kg dry 5.5

!g'lq dry 5.5pdkg dry 5 5pg/kg dry 5 5

ldl€ dry 10I

ldkS dry 54.5pSftS dry 5 5pS/g dry 5.5

Mkgdry 5.5

!g/kg dry 27-3

lgftg dry 5.5pdl(g dry 5-5pS/kS dry '10.S

lEtS dry 5.5

!gI(S dry 10.9pdks dry 5 5pS/kg dry 5.5pg/kg dry 10.9

ldkS dry 5.5

i./dkg dry 5-5

UdkS dry 5-5

ldkS dry 5.spS/kS dry 5.5

udkg dry 5.5

ug/kg dry 10.9pg/kg dry 5.5

Udxgnry 5.5

!S/kS dry 5.5

tig/kg dry 5.5

t/g/kg dry 5.5

ldkS dry s.5

ldkS dry 5.5

IdkS dry 5.5

Ug/kg dry 5.5

uERgdry 5.5pqkg dry 5.5pg'l$ dry 5.5pgkS dry 5-5pdks dry 54-5

tigl(g dry 5-5

lgkS dry s.5pgks dry 5.5

lCeS dry 54.5

ldkS dry 54.s

FgASdry 5.5

Volalile Oraanic ComDounds

Prepared by method SW846 50354 Soit (tow tevet)

761!1 1,1,2-Trichlorotriffuomelhane(FreoERL

67541 Acetone BRL107-13-1 Acrylonitrile BRL7145-2 Etenzene BRL104-86-1 Bromobenzene BRL71-97-5 Bromochloromethane BRL75,274 Bromodicttoromethene BRL15-25 2 Bromoform BRL74-33-9 Bromomethane ERL78-93-3 2-Buranone (MEK) BRL10!-51€ n-Eutylbenzen€ BRL13t93€ sec€utylbenzene BRL98-{}64 tefi_gutylbenzene aRL7s,1s-0 cefton disullide BRLs6,23,5 Ca6on tefachtoride BRL1O8-9O-7 Chlorcbenzene BRL75-OG3 Chloroehane BRL6746-3 Chlo.oform BRL7447-3 Chlorcmethane BRL954$8 2-Chlorotoluene BRL106-43-.1 4-Chlorotoluene BRLs6-12'8 1,2-Dib'romG3-chloropropane BRL124-!€ 1 Dibrcmochlorcmethan€ BRL108,33-4 1,2-Dibromo€hane(EDB) BRL74-95-3 Dibrcmomethane BRL9+5G1 1,2-Dichtorobenzene BRL5'{1-731 l,3-Dichtorobenzene BRL10€F467 l,4_Dichtorobenzene BRLr5'71'a Dichlorodafluoromethane(Freon12)BRL75-3+3 l,l-Dichloroethane BRL10LlG2 l,z-oichloroethane BRL75314 l,1-Dichloroethen€ BRLj5e59-2 cis-1,2_Dichloro€thene BRLr5e60-5 kans-1,2-Dicfllorcethene BRL78€7,s |,2-Dichloropropane BRL142,28-9 l,3-Dichlorcpropane BRL5S4?0r 2,2-Dichloropropane BRL563'58{ l,l-Dichloroprop€ne BRL1m61-01-5cis-1,3-Dichloropropene BRL10061{2{trans-1,3-Dichloropropene BRL10G.{1-4 Ethylbenzene BRL87{&3 Hexachtorobutadiene BRL591-78$ 2-Hexanone (MBK) BRLsa€2-6 tsopropylbenzene BRL99{7{ +lsopropyltoluene BRL163{{4-1 Methyt tert-butyl eher BRL10&10-1 +Methlt-2-pentanon€(M|BK) BRL754$2 M€thylene chlorire BRL

26-Ma(O7 26-Ma.-O7 7031584 BD

27-Mat47 28-+'la67 7D31658 RLJ

voc

sw &16 82608

8RL91.263 Naphthatene

Page 75 of 165

Thh hborulory rcpod is noa wlid t4'ithod an aalhoriz,ed slgndurc on the cowr page

' Reponabl€ Dete.tion Limit BRL = Below Reporting Limit

Page 290: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMtF-33 2'-4'sA5964l-15

Client Proiect #301-88

MatrixSoil

Collcction DardTime2l-Mar47 00:00

Recrived22-Mar07

CAS Na Analfla(s) Retuu Fag *nItL Dilaion Mdhod Retr. Prcparcd Analyzcl Balch At&lfd

vokiile Org.oic Compounds

Volatile Orqanic ComooundsPreparsd by m€hod SW846 5035A Soil (lo!v tevet)

BRLBRL8RL8RLBRL8RLBRLBRLBRLBRLBRL

75-6a-4 TaichloroffuororEthane (Freon 11) 8RL

10965n n-Propylb€nzene10Oa2.5 Styren€6iXF2o5 1.1,1,2-Telrachloroethane79-3'r-5 1,1,2,2-t6trachloroethane127n84 Telrachlorc€thene108-8Ai Tolu€ns87{l{ '1,2,}Trichlorobenzene12+82-l l,2.4Triohlorobenzene7t-55-6 1.1.1-TdcfiloroettEne79{es 1.1,2-Tdd oroethsne79.01{ Trichloroethene

SW84682608 27+,lar47 28+,lEr47 7031658

BRLBRLBRLBRLBRLBRLBRLBRL8RL8RfBRLBRLBRL

97

9098

BRL

BRLBRLBRLBRLBRI-BRLSRL

'

BRLBRL

84

pdks dryldks dryudks dryUdtS dryldks dry!sn(S dryrdks dryFdkg dryrdks dry!S/kS dry

pdks drypdks dryUdkS dryUgts dry!g/kS dry

ldkg dry

l4ikS drypgikS dry

Fg/kg drypgrg drypdks dry

lisfl(g dry

rdks dry

|lg/kS dryygts d.y

5.5

5.5

t0.9

5-5

54.5

5.5

5,1.5

109

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RLJ

9€-i8-.{ 1,2.}.Tdchlofopropane95{3{ 1,2,+Tdmethylb€nzene10&67a l,3,tTrimeht'lb€nz€ne75{t-4 Vinyl cHofido133G2G7 m,pFxyleno9+47{ o-Xyler|e10$9S9 T€t-ahydrofuran@-z+7 Etty' eth€r99ffi€ T€d-amyl m€lhyl ethet637€2J Edryl teft-buhy' e{]eri00-2G3 Diisopropyl€th€r75€to TertButianol/brrtytstcoholi219r-t 1,4-Oioxane

Suoogate Ecoveries:46040.1 [email protected] Tduene-al8t7 0604t4 l,zaichloaoethane44t86€53-I Olbrornof iJoroDglhane

Ertractrble Petlohum Hydrocarboos

Eftadable Total Petroleum Hvd.oc€rbonsPr€pa.ed by m€thod SW846 355088006.61.9 Ga.6lin668a76312 FuelOl#26eaze3l-3 Fuel cll #46€6534H Fud Oil #6ir09U00000 Motor OilJ0O100mO Avialion Fuel

Unld€ntnedOO|€tr OilTotal P€troleurn HydaocarbonsC9436 Aliphatic tlydmcarbons

Srfiogsfe recul/9ttts.'?tsaeS+2 l.CttbrlJoctadecatl€

Semivoldile Orgrric Con[ouods by cC

Orqanocfilorine P€aticid€s SW846 8081APrepared by rnethod SW846 3tl5A3os.m-2 Aftlrin

TCTETPH zf-Mat4f 29.|./'a,-O7 7031590 DS

7G130 %701m%7G1fi%70-tN %

|rgftg dryntg'Xg dryntgL/kg dryndkS d.ymgl€ dryn1gk9 drymdkg dwfirgn(lg drymdks drymgl€ dry

22.1

22.122.1n.1n . l22122.1

22.1

40-11$ %

ydts d.y SW846 80614 2&t Er{7 28-tylar47 7m15t6 TG

Thit lahrratory npod it,ra, wld witho .E ardtortzd sipaAre on lhe covcr pzge.

* Reportable Deiec.ion Limit BRL = B€low R€portirrs Limit Page 76 of | 65

Page 291: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-33 2'-4'sA5964l- l5

Clieot Proiect #301-8tt

MatrixSoil

Received

22-Mat-Ol

Collection Date/Time2l-Mar-07 00:00

CAS No, Awtrt (s) FloC *RDI Dilutian PEltaten Aflalfred Darch A zllst

Semivohtlle Orgrnic Comporods by cC

Orqanochlorine Pesticides SW846 8081A

Preparod by method SW846 3545A

31+845 a-8HC31+8s-7 b-BHC319,86{ d-8Hc

58{+9 g-BHC (Lindane)

57-14'9 Chlodane

72-u-a a,4.-DDD (p,p')72-5rs 4,41DDE (p,p,)

50-2s_3 4,4!DDT (p,p')60-57-1 Dietdrins5+94€ Endosulfun I33213-65,9 Endosulran tl1031{74 Endosulfun Sulfate72-1O-A Endrin7421-93-4 EndrinAtdehyde1644-8 H€ptachtor7243-5 Methorychtol1024-57-3 HeptachlorEpoxide8001-35-2 Toxaphene5103-71-9 a-Chlordane5s66-34-7 g-Chlordane

s31F,+70-5 Endrin Ketone

Surrogals r€cor,erssr10386-e/ 2 4,4-D8-Octafl@rodphent4 64m -2aa Decechlorobiphenyl (54

Polvc$lo.inaled Biphenvls bv SW846 8082

Prepared by melhod SW846 3g5A

126?4,11-2 PC8 101611104-24-2 PCB 1221r1141-10-5 PCB 123253469-21-9 PCB 124212672-294 PCB 1248110e7-6e-1 PCB 1254110ec82-s PCB 126037324-23.s PCB 12621110G14-4 PCB . l268

Surrogaf€ r€covofl€s.'

1038&812 4,4-DB-OctalluotDbiphenyl (Si

20i1-2aa Decachtorobiphenyl (Sr)

Semivolrtile OrgsEic Compo|rtrd! by ffMS

92i7-5

5G5t3

BRLBRLARLARLBRL

8RLBRL8RLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

73

BRLBRLBRLBRLBRLBRLBRLBRLBRL

75120

BRLBRL8RLBRLBRLBRLBRL8RL

t g/l€ dry

tigks dry

!g/kg dry

!g/ks dry

t/g/kS dry

!g/kg dry

!g/kS drypdkq dty

tidks dry 5.32

ldkS dry 5.32

US/kS dry 5.32

tStkgdry 5.32pgks dry 26.6

!g/kg dry 5.32

lSrkS dry 5.32

tig/kg dry 5.32

lqkS dry 5.32

Ug/kg dry 5.32

rd*s dry s.32

USikg dry 5.32

!g/kg dry 5.32

UdkS dry 5.32

Ug/kg dry 5.32pdkgdry 532pg4(g dry 5.32pdkS dry 26.6pS/kS dry 5.32pg/tg dry 532pg/kg dry 532

30-t 50 %3A-150 %

pdkS dry 33.6pgkS dry 33.6pgkg dry 33.6

Pg/kS dry 33.6

US/kg dry 33.6

rc/kg dry 33.6

rc/kg dry 33.8

t g/kg dry 33.6

!S/kO dry 33.6

i0'15O %30-150 %

1'|

l

1

I

l

I

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I

I

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1

I

1

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1

l

1

1

1

SW8468081A 26-Mar-07 28-l,lar-07 7031516 TG

SW846 6082 27-MarO7 27-Mat47 7031591 SM

S€mivolalile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35454

83-32-9 Ac€naphthanez'o+9t13 Acenaphthytene62-53-3 Anilin€12G12-7 Anthmcene

1912-24.9 Atrazine103-33-3 Azobenzene/Diphenyldiazin€

SW846 8270C 27-Mar0t 28-Mar47 7031592 M.B5,r9 1

5,r9 |

549 1

549 1

54S 1

54S 1

549 1

549 1

BenzidineEenzo (a) antfracefle

Thb labotulory rcpo.t h ,toa valil wilhoal ot authorized sigt tlure on ahe Eover psge

' R€portable D€tection Limit BRL = Below Reporting Limit Page 77 of 165

Page 292: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldefltificationM6F-33 2'-4'

sA5964l-15

Client Project #301-88

MatdxSoil

Collection Date/Time2l-Mar{7 00:00

Rec.eivd22-Mt -07

CAS No. Arnlft (s) Fbc UEi^ 'RDL Dila.iorr Method REI, Przporcd Arnlfzett Bdch At alysl

Semlvol.lile Organic Compounds by GCMS

Semivolatlo Oroanic Compounds bv SW846 8270C

Prepared by mehod SW8,{6 3545A

5G32.8 Benzo (a) pyrenezlrr549-2 B€nzo (b) fluoranthen€191-2+2 Benzo (g,h,i) perylene2orua-s Benzo(k)fluoranhene65{5{ Bedoic acid10G51€ Benzyl alcohol11i-9i-1 Bis(2rhlorcethory)mehan€11t4a4 Bis(2-chloroe{hyl)oher39638'32-9 Bis(2ahloroisopropyl)ether1t7$1-7 Bis(2-ehtth€xytlphdrahte101'5t3 4-Brofibpll€nyl pheny' ether85$&7 Butylbenzylphthalate86.?4S C€rbazoles9-5+7 4-Chlo.o-3-m€thylphenol106-474 4-Clrlorcanilin€91-5&7 Z_Chloronaphthet€ne9s-574 2-Chlorophenol700+72-3 +Chloophenyl phenyl ether218{i4 Chrys€ne53-7G3 Dibeizo (a,h) anthracen€132€4-9 Dibenzofuran955&1 1,2-Dicilo.ob€nzene54r.73r 1,3-Didrloobenzene106-46-7 t,4-Didrlorobenzene9r-94-r 3,3:Didtlorobenzijine'rz\l{}2 23-D-rchlorophenotu&2 Dehyl ph$|slatei31-11-3 Dinrethytphthatatet0s7-s 2,+Dimethylphenolu-74-2 Di-n+utytphlhdates34.52r 4,6-Dinito-2-m€thytphenol5r-2&5 2,4{)initrophenol121-14-2 2,+Dinih.otolu€ne60G20-2 2.6aoinit'Etoluene117-84.0 Di-o-octylphthatate20G44{ Fluoranthene86-7$7 Fluolene11&Zl-1 tbxachlorobenzene67$&3 Hexachbrcbutadienen474 Her6chlorocydop€ntadieneAl-72-1 H€xeafito@ethane19!395 |rde.b (1,2,+<d) pyrcno90-12{ l-trt€thytnaphthalene70-59-t lsophorcne9157{ 2-Methy'n6phthalene95-4+7 2.iiethytphenol1o&3s4, 3,4-Metiylph€nol106-4459t-2G3 Naphthslene8€.74.4 2_Nitoanflines,l)$2 +Nitroailine

SRLERLBRLBRLBRLBRL

8RLBRLBRLBRLBRL8RLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRI8RLBRLBRLBRLBRLBRLBRT8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRL

BRLBRLBRL

fdlq dry 549

tgis dry 549

ldkg d.y 549

tS/t€dry 549ydts dry 549ygtsdry 54Spdkg dry 54SpglSdry 549

ldkS d.y 549

Idkg dry s49pdkgd.y tlgpsikodry t19ygtgdry 549pdrgdry tlgpdkS dry 549pdkS d.y 549

!Sn(S ey 549pdks dry 549

tdkS dry 549

lg/kS dry S49ggrrg dry 549pdl€ dry 54s

tdkg dry 549

dkg dry 549

ldkS dfy 549

UdkSd.y 549

ljgikS dry 549pdkg dry 549perlg dry 54S

lJdkSdry 54S

ldkS dry 549

US/kS dry 549

lSrkS dry 549

ldks d.y 549

WXg dry 549ySlrg dry 549pgkgdry 549pdkSdry 549

ldkS dry 54S

UdkS dry 549

tldksdty 549

tdks d.y 549

Wftg dry 549

lSftSdry S{9pdksdry 549

ldlq dry 549

Fdlq dry 549

lgftS dry 549pgkSdry s49

wtg dry 549

SW846 8270C 27-Met47 2a{ngtr-Ol 7031592 M.B

Thk labontorf npo.l ls tst vald wdlhdu alt duihorizcd iEitaue on iha @wt gqe.

I Reporbble Dct€ctioo Limit BRL = B€low Reporring Limit Plge 78 of 165

Page 293: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F.33 2'-4'sA5964 t- l5

Client Ptoiect #30 , -88

Coll€ction Date/Time2l-Mat4100:M

Received

22-Mar47

MatrixSoil

CAS No. A,nlyz(s) ResaIl Fl"C Ualts 'RDL Dllutbn Method Retr Pnpared Analtzed Batch AnoDst

Sehivolatile Orgaric Compounds by CCMS

S6mivolatile Oroanic Compounds bv SW846 8270CPrepared by melhod SW846 35454

100-01€ 4-Natro€niline98-95-3 Nitrob€nzene88-7t5 2-Niuophenotr00 02-7 4-Nitrophenoi62-75-9 N_Nitrosodimethylamine

621-€a-7 N-Nitr6od-n-propylamine0€-304 N-Nitrosodiphenylanine07{6-5 pentacilorophenol

05{1{ Phenanthrene

10&ss-2 Phenol14.@ PyrenellGe,6-1 Pyridine12G82r 1,2,4-Trjchlorobenzene9195-.1 2,4,$TrichlorophenolaB-o6,2 2,4,6-Trjchtorophenol

Sunogale recoveries:32140-0 2-Fluorobiphenyl

361-121 2-Fluofophenol

1165604 Nitobenzene4'

116si2-2 Phenol45

1718s14 Teryhetryl-dl4

1 1 a-/t4 2,1,6-fibromophenol

1 SW846 8270C 274J,al-o7 za-Ma..0t 7031592 M E

1 '

1 '

1 '

1 "' I '

1 '

1 "

1 '

1 '

l "

BRLBRLBRLBRLBRf

BRL8RL8RL8RLBRLBRLBRLBRLBRLBRL

665563577465

BRL

BRL

1 1 . 3

BRL

3.86

8.r6

BRL

!S/kS dry 2190

LiS/kS dry 54S

Udkg dry 549

lS,ftS dry 21S0

ldkg dry Sl9pSn(S dry 549pgkqdry 549

!g/kg dry 549pg/kg dry 549

US/kS dry 549pg/kg dry 549

!g/kg dry 549

Ig/kg dry 549

USfl(S dry 549

lSftS dry 549

30-1m %I 5-110 %30-1m %15-110 %30-1m%15'110 %

mgr'kq dry 0.0316

mg/kg dry 0.324

mg/kg dry 139

mSI(S dry 0.462

mS/Kg dry 0.231

nE/kg dry 0.62

nE/kg dry 0.693

mSik0 dry 1-39

mg/l 0.0200

mg/l 0 0150

mg/l 0-0150

mg/l 0.0025

mgn 0.01{)

mgrl 0.0(X)40

mg,1 0.0150

mg/l 0.015t)

%

Total M€tals by EPA 6000/7000 Seites M€thods

7439,97€ Mercury BRL

Totrl Metals by EPA 200 Seri€s M€lhods

1 SW846 7471A 28-Ma(47 284llacl7 70314S5 YP

1 EPA200.7 28-MarO7 28$iar07 7031494

1 ''l "

1 '

t "

l '

7440-221 Silver

7,t40-3&2 Aasenic

7440-3S3 Barium

7440-4!9 Cadmium

7c.4o47-3 Chromium

1439-921 Load

77€2-4+2 Selenium

SPLP M€trk by EPA l3l2 & 6000/7000 Seriei M€ahods

SPLP Extraction Complet€d

7440-22-4 Silver 8RL

74-{o-J€-2 Arsenic BRL

71.40-39-3 Bedum ARL

74,{0.43 9 Cadmium BRL

714047,3 Chromium ERL

7'!39-974 Merc!ry BRL

7439-92-1 Lead BRL

77824+2 Setenium SRL

Gcnerd Chemhtry Prr.|t|eiers

% Sohds 94.3

1 SW84613'12 26-Mal-O7 2U'Aar07 7031560 AD

1 SW8461312/60t08 2A-Mar07 2A-Mat47 703'1651 Ha

1 "

1 '' t "

I '

I SW84613127470A ' 28-|!lar{7 70316V YP

1 SW846131260108 . 28-Mar{7 7031651 HB

1 "

1 SM25.l0 G Mod z4-Mar0i 24{i/tat47 7031470 OP

Rt\4

This labotutory Hport is not vaIU wirhorlt an aatlioized sig aturc on the cowr prye.

* Repodable Detection Umit BRL: Below Reporting Limit Page 79 of 165

Page 294: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificarionMtF-34 4'-6'sA59ri4l - l6

Clieot Pmiect #301-88

Collection Date/Time2l-Mar47 00:00

Received22-Mar-07

MafrixSoil

CAS No- Anolyte(s) FloC A,,As ,RDL Diltdioa Lldhod ReI Prcpond Andyzztl Batch Ad4lfsl

Voktile Orgsnlc Compoonds

VOC ErlEctionVolatile Omadc ComgoundsPrepared by method SW846 5035A Soil (low l€vel)

76-1+1 1,1,2-Trid orotainuom€hane(Fteo€RLBRL

BRLBRLBRL

BRLBRLBRLSRL

70-9+3 2-Eutanone (MEK) BRL10.-51{ n-But},b€nz€ne BRL13f!98-8 sec-Buttdbenz€ne BRL9846s tert-Butylbenzene BRL75-154 Carbon disulfide aRL56-2&5 C€rbon tetehtoride BRL108.90.7 Chloroberuene BRL75oo3 Chloroethane 8RL67{&3 Chlootorm BRL7447'3 Chlofomethane BRL95-49-0 2-Chlorototuene BRL106-13-4 4-Chlomtotu€ne BRL9&123 1,2-Diblomo-3drbropropan€ BRL

Field ext-act€d

pgltq dry 5.4

FgASdly 1O7

lSftS dry 5.4pdkgdry 5.4

ldks dry 5.4

|lgn(S dry 5 4

ldks dry 5,4

$r'kg dry 5 4pgn(gdry 10.7

Fdts dry 53.6pdkg dry 5.4

ldk€ dry 5.4pdkS dry 5.4

udkgdry 26.8pgikg dry 5.4

rg/tgdry 5.4

ugl€dry 10.7pdrgdry s.4

ldkSdry 10.7

tdks dry 5.4

ldkS dry s.4pg^gd'y 10.7ygiks dry 5.4psilq dry 5.4pdrgdry s.4pdksdry 5.4

IS/kS dry 5.4

udkg dry 5.4pdlq dry 10.7

lS/|€ dry 5.4pSAg dry 5.4pdlgdry 5.4pdks dry 5.4

dkg dry 5.4

udkSdry 5!pg/kg dry 5.4pS/tS dry 5.4pdks dry 5.4

ldkgdry 5.4

[d|(10 drv 5.4

sdkS dry 5-4

!€ftS d.y 5.4

tdkg dry 53.6pS/ksdry 5.4

!S/kS dry 5.4pdkSdry 5.4pslxgdry 53.6

IdxS dry 53.6

lCl€ dry 5.4

1

1'|

I

I

I

t

1

1

I

I

1

1

1

1

1

I

I

I

1

1

1

I

I

1

1

1

1

1

E.Mat47 2 ',,,at47 7031 584 9D

674+1 Acston€

107-13n Acry,tonitrile

71432 B€nzene

10&€S1 Bromobenzene74-97-5 Bromochlorom€lhane

75-2t4 BronEdichloromethane712+2 EromoformZIJ+g Brcmolrlolhane

1244€r Oibro.nochloromethane10eF934 1,2-Dib@moehane(EDB)7{-9t3 Dibrornomethane95-50-1 l,2-Dichlorobenzene54i-73-1 1,3-Oichlorobenzene10se7 l,+Dichlofobenzene

15ffi05 trans-l,2-Dichloroeth€ne7a-67-5 1,2-Dichtoropropane142-2&9 1,3-oichloaopropane

594.20-7 2,2-Dichlonrp|.opane

56+s86 1 , | -Oiddq.optopene

10061{t-5 cis- 1 ,3-Okl{oropmpene

75-343 |,1-Dichloaoethene BRL107.06.2 I,2-Oid{oroethene BRL7s-3s4 1,1-Di.*Jtro€tfEne BRLt5F59-2 cjs-1,2-Dichlorcethen€ BRL

BRLBRL8RLBRLBRLBRL

(Freon12)BRL

BRI-aRtBRLBRLBRLBRL

10061{26tra1s-l,3.Dic.hloropropene BRfi0o4i-1 Edryibe{zehe sRL07{8-3 Hsxacilorobuuad'ene BRL591-784 2.lfe)€none {MBK) BRL98€2€ lsopmpylb€rEene BRLs€7.6 +ls@ropyltotueno BRL1634-0s Methyt bd+utytether 8RL10&10-1 4-Methyl-2-penranon€(M|BK) BRL75{9.2 Methylene cfiloride BRL9l-20.3 N€phthalgne

Page 80 of 165

Thb labodory ftpo.t X not vau N hoar zn.a&torlzed dgaaurc od dte cowr Inge.+ Reportable Detection Limir BRL = Below Reportiflg Limir

Page 295: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationMtF-34 4'-6'sA59641-16

Client Proiect #301-88

MatrixSoil

Received22-MaA1

Collection Date/Time21-Mar-07 00:00

CAS No. Arurlte(s) FlaE 0nits *RDL DiIAio Method Retr. Prepared AnabEed B ch Analyst

Vohtilc Orgrnic ComFornds

Volatile Omanic CompoundsPrepared by method SW846 5035A Soit (low l€wt)

BRL6RLBRLBRLBRLBRLBRLBRLBRLBRLBRL

75s9-4 Tdchloronuoromethane (Freon 1.1) BRL

103{51 n-Propylbenzene100-42-5 St]/rene630'209 1 , I , 1 ,2-Tetrachtoroethane79-34.5 1 , 1 ,2,2-Tetrachloroelhane127-18-a TeFechloro€lhene108-08,3 TotueneB7$1-6 1.2,3-Trichlorobenzene120-8?-i 1,?,4-TrichlorDbenzene71'5!F6 1,1,1-Trichloroethane79.00-5 1,1,2-Tridrtoroethane7341-6 Tdchloro€thene

SW84682608 28-Mat47 28-MarO7 7031693 RLJ

+CTETPH 274J,at47 29-Mar07 7031590 OS

9618-4 1,2,3-Tric*rloropropane95$35 1,2,4-Ttifiethytber'zerle108-67{ 1,3,s-Tim€thylb€nzene7s{1 4 Vinylchloride133c2c7 m.pFxylene9s47-6 o-Xylene109-99-9 Tetrahydrofuran60-29-7 Ethylethets94-05{ Tert-amytmethylether637-92-3 Ethyt tert-butyl ether10€-20-3 Di-jsopfopylether75-65-0 Tert_Butanot/butylalcohol123 91-1 1,4-Dioxane

Sucogate .ecovelies,46Mo1 +Bromofluorohenzene

2037-26-s Toluene-dg

1 7o6uo7 -o 1,z-DichlqcEthane -d4

ft6a-83-7 Dibmmolluoromelhane

Erttsctabl€ Fettoleum Hydrocarbotrs

Extractable Total Petroleum Hvdrocsrbons

Prepared by method SW846 35508

800691-9 casoline68476'3G2 Fuel Oil#z6€47S-31-3 Fuel Oil#46€553{0r Fuet Oit#6nl0960cDol Moior oilJ00100000 Avialion Fuel

Unid€ntified

Other Oil

Total PebDleum Hydrocarbons

CSC36 Aliphalic Hydroc€rbons

Surogata /ecoyei€s:

336-33-? 1-Chloroocladecene

Semivolrtilc Organic Compoudds by GC

Orqanochlorine Pesticides SW846 8081A

Prepared by method SW846 3545A

30$00-2 Aldrin

BRLARLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL

891021141U

BRLBRLBRLBRLBRLBRLBRL

BRLBRLARL

udks drypdks dry

ldks dry

!g/kg dry

UdllS dry

t4/l€ dry

ldkS dry

UgkS dty

!S/kS drypdkg drypdkS dry

ldks drypgks dry

Pstkg dty

t S/kS drypdks dry

ugks dry

ldkg drypdks dry

lldrS dry

ldks dry

IdkS dry

udkS dry

ldkS dry

udks dry

5-4

5.4

5.4

5.4

5.4

5.4

5.4

5.4

5.4

5.4

5.4

5.4

5.4

5 4

5.4

5.4

10.7

5 4

53.6

5.4

5.4

5.4

5.4

53.6

107

70-130%

7&130%

7G130 %

7G130%

mgkS dryftrgkS dryFrglkg drynsfts drymgkS drymgrxg dryhgkg drymgr'kg drymglqC drymg/kg dry

15.0

15.0'15_0

15.0

15_0

15.0

15.0

15.0

15.0't5.0

40-140 %

BRL !S/kS dry SW846 8081A 26-uat47 28 4a147 7031516 TG

That ltboratory Eport b not vaIU xtithalt aE aurhoized sigfiola/-e on the cover page.

' Reportable D€tection Limit BRL = Below R€porting Limit Page 8l of 165

Page 296: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiorM8F-34 4'{,sA5964l- r6

Clieot Proiect #301-88

MatrixSoil

Collection Date/Tirr1€2 I -Mar-07 00:00

Received22-Mar47

CAS NlL A,tolyte(s) Respk UnjaFlog *RDL D utlon Mdhod Retr Prepated ArBIyel Balch 'lna$sl

S.mlvolsiile Orgatric Compoutrds by CC

Orqanocfi lorine Pesticides SW846 E081APreparad by n€lhod SW846 3545A

319€4€ a-BHC3198s-? b-Blrc319€6€ d€HCs,B{e-e g€HC (Lindane)57-7+9 Chlordanef2-54-a 4,4'-DDD(p,p')z5+e 4,4'-DDE (p,C)50-2+.3 a,a-DDT (p,C)6tr57-i Dioldrin95S98{ Endosulbn I33219€5€ EMosulran tl1031{ru EndosulnanSulfate

7{2r-S3{ Endrin Alrtehyde7411-A Heptachlor724$5 Methorychlo.1021-57.3 Heptachlor Epoxide800135.2 ToxaptEneslo:l-71-9 +Chlordane56G63+? g_Chlordane53494-705 Endrin Kebne

Sunogale @coved6s:t03a6a+2 4,+D&Octefi@robiphenyt (Sr)2051.?+3 Deca&brcbhhenyl (Sd

PolvchlorirEted Biohenvls by SW846 8082Prepared by rnethod SW8,l5 3545A12674n1-2 PCB 10161110+28-2 PCB 1211t141-164 PCB 17325346*214 PC8 1242126n-N4 PCB 1248r1097$9t PCB 1254110s€-02-5 PCB 126037324.23-5 PCB 12621110Gr4-. rcB t268

Swmgete rccowles:103864+2 4,+D+Ociafl@rcbiphenyl (Sr)zostzaa Dacachlototiphenyl (St)

Semivolrtlle Orgrnlc Compo[nds by GCMS

S\i846 80814 26-fi,lar{7 28-l ar{7 7031516 TG8RLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLSRLBRLBRI-BRLBRLBRLBRLBRLBRL

79

8RL8RLBRLBRLBRLBRLBRLBRLBRL

70115

BRL

BRLBRLSRL8RfBRLBRLBRL

IS^gdry 5.22

udkS dry 5.22

!df(g dry 5.72

ldkS dry s.22

ls/t(gdry 26.1ps4€dry 5.22

U€ifgdry 5.22

uS/kg dry 5.22

ldkg dry 5.D

!C4(S dry 5.72

USI(S dry 5.22

lsftgdry 5.22pglk0dry 522

!S/kS dry 5.22pdt.gdty 5.U

ldko dty 5.22

lgkg dry s.22

lqko dry 26.1

Fdtgd.y 5.22

ligftg dry 3.22pgkgdry 522

3G150 %3$1tu %

pS/kSdry 32-8pdkg dry 32.9

ldkg dry 32.8

lSftSdry 32.ApSI(g dry 32.ApSftS dry 32,8pglqdry 32.8

ldkS dry 32.8psA(S dfy 32.a

3G150 %30-150 %

udks dry 371pgkSdry 371

lSftS dry 371

FdkSdry 371pdks dry X71

ldkS dry 371

ldkS dry 371

Idkg d.y 371

SW846 8042 21-Mat47 27-Md47 7031591 SM

SW8,r8 8270c 27-t\'€,t47 '8-ltat47 703'1592 M.B

S€mivdalilo Oroanlc Cornpounds bv SW846 8270CPrepared by meflod SW846 354SA

E332-g Aaenaphthene20+9GS Acenaphthylene6253-3 Anilinot2Gl2-7 Anlhracene1912-24.9 AtBzin€i0$33n Azobenz€ne/Diphenyldiazineg2€7-s Eenzidine$-55>3 genzo (a) anthec€ne

Thh laboturory rcpora it nol &lid idroa cn aut'odzed tiga ue on rle cover page.

* Rpportable Dcrecaion Li6ir BRL = Below Reporti[g Limia Pege 82 of 165

Page 297: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldenfilicationM8F-34 4'-6,sA5964r-16

Client P.oiect #301-88

MatrixSoil

CoLlection Dat€/Time2l-Mar.07 00:00

Received22-Mar-07

CASNo, Analyte(s.) Flos Utia 'RDL Dila.ion Method Rel. Prcpared Anaryzcd Bdtch Anallst

S€mivolatll€ Organic Compound! by CCMS

Semivolatile Oroanic Comoounds bv SW8rt6 8270C

Prepared by mehod SW846 3545A

50-32-8 Benzo(a)pyrene20s-99-2 Benzo(b)fluoranthene1e1 2,4 2 Eenzo (g,h,i) perylene

20748,9 Benzo (k) lluoranlhene65{5{ Benzoic acid100-514 Benzyl elcohot111,S1-1 Bis(2-chtoroethoxy)methane111-41-4 Bis(2-chloro€thyt)ether3gfi eF32-9 Bis(2_chloroisopropyt)ethe,117-81-7 Bis(2-€thythexyt)phthatate101 55-3 4-Bmmophenyl phenyl ether85{8-7 Butytbenzytphthatate86-74-A Cadazoles9'507 4"Chloro-3-methylphenot10s7{ 4-Chloroaniline91's8-7 2-Chloronaphthalene9s'57{ 2.Chlorophenol7005-72-3 4.Chlorophenylphenylether

?16-01-9 C+lrysene51.7G3 Dibenzo (a,h) anthracene132-64-9 Db€nzofuran

9!50-1 1,2-Dichlorobenzene

5.11-73-1 1,3-Dichlorobenzene10646-7 1,4-Dichtofobenzenes1-94-1 3.3loichlorobenzidine12e831 2,4,Dichlorophenol84€6-2 Diehylphthalate131-11 3 Dimethyl phthalate

10s7's 2,4-Dimefl1ylphenolu-r4-2 Di-n-butylphthalae

534-52.1 4,6-Dinitro,2-methylphenol

51-28-5 2,4-Oinitrophenol121r4-2 2,4-Oinibotoluene606-20-2 2,6-Dinitrotoluene

117-644 Di-n-oc\dDhfiatate206-444 Ftuoranlhene

86-717 Fluorene118-741 Hexachlorobenzene

87$8'3 Hexachlorobutadiene

7f4f4 Hexachlorocyatlopentadiene

61-72-1 Hexachlooethane

1e!3+5 lndeno (t,2,3-cd) pyrcne

90'12-0 1-M€thylnaphthatene

78-59r lsophomn€

91-576 2-Melhylnaphthalene

95-4&7 2-Methylph€nol

108,391 3,+Methlphenol106-44-591-20.3 Naphthalene88-744 2-Nitroanilinees{s2 }Niroaniline

BRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLaRtBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRL8RL

BRLBRLBRL

ldkS d.y

!g/kg dry

!9ks dry

Pg/kS dry

tig/ks dry

Pgkg dry

UgeS dry

ldkg drypgkg dry

lgkS dry

lS/kS dry

lgks drypgks dry

LrEKg dry

Lrdkg dry

udkg dry

ldkg drypdks dry

Pdks dry

UdkS dry

irgks dry

!g/kg dry

!g/kg dry

!E(g dry

!S/kS dry

!S{(S drypdkg dry

!S4(S dry

ldkS dry

Pgks dry

PS/kS drypS/kg dry

!g/kS dry

lEkS dry

lSi kg drypS/kg dry

t g/kg drypdks dry

!g/kg dry

Idkg dry

lsfts dry

ug/kg dry

lgkg dry

!4ks dry

!S/kS dry

lqks dry

Wlkgdry

pSftS dry

USftS dry

lgkg dry

371 1

371 1

371 1

311 1

371 1

371 1

371 1

371 1

371 1

371 1

371 '1

371 1

371 1

371 1

371 1

371 1

371 1

371 1

371 1

371 1

371 1

371 1

371 1

371 1

311 1

311 1

371 1

371 1

371 1

371 1

371 r

371 |

371 |

311 1

37r 'l

371 1

371 1

371 1

371 I

371 1

371 1

371 1

371 1

371 1

371 I

371 1

371 1

371 1

371 1

371 1

Thit ldtoratoyeport ie aol valu ''ilhoat on authorized signdue ot1 ,fu colter p4ge.

i Reportal'le Def€ction Limif BRL : Below R€portiflg Linit PaseS) ot 165

Page 298: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samnle ldeotihcationM8F-34 4,{.sA5964l-16

Clieqt Proiect #301-88

Matrix Receiv€dU-MarO1

Coll€rtiori Date/Time2l-Ma.-07 00:00

CAS No- Aaalftz(s) Resell nq A'tur 'RDL Dilaio,, Mzthott Rcl Prcpated Analyed Batxh A^aN

SemivoL.ltle Orgrtric Compoundr by CCMS

S€mivolatile Oroanic Comoounds bv SW846 8270CPr€pa.ed by mehod SW846 3545A

lo(}ol4 zl-Nihtaniline9E€rF3 NitrDb€nz€ne€&7+5 2-Nitophenol1{Xrc2"7 +Nitophenol62-7ts N-Nihosodimethylamine621-64,7 N-Nit'osodi-Fpropylamine&3|).6 N-Nilrosodiphenyl€mine87+Gs Pentacl omphenol85{i{ Phenanthr€nel0&9t2 Phenol129{lo-o Pyreneill}€6-1 Pyririn€r20{2-l i,2,4Tridito@benzene95€5-4 2,4,$Ttichlorophenol88-oFz 2,4,GTaichlorophenol

Sunogale rccowdes:32140.8 2+luor&iphenyl367424 2+luotophenol418frilA Nillobanzene4s416542-2 Phend4s171c-514 Telphenyl4l41 l8-79-O 2,4dTtib@nnphenol

7140-4!9 C€dmium

744@7-3 Ch,omium

7439-97-6 Mef@ry

7439-92-r L€ad

7782-a92 Selenium

Gene.d Cbemirary Prr|meters

% Solils

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

6282597749

lrgrkg dry 1490

!C/tS dry 371pdkS dry 371

us/kS dry 1490

|rSn(S dry 371pgftS dry 371pslqdry 371pdks dry 371

US/IS dry 311

UdtS dry 371

USftgdry 371psrxs dry 371

ldkS dry 37r

ldkS dry 371

ldkS dry 371

30.130 %t+110%3L130 %ls t l 0 %30-130 %tE f i o%

rYrgl(g dry 0.0325

mdkSdry 0 S32

mdks dy 1.40

rnS/kg dry 0.466

ms/kg dry 0.233

(E/kg dry 0.4m

ru/kg dry 0.69S

mgrlqdry 1.40

mg/l 0-0200

mgl 0-0150

r€I 0.0150

msn 0.0025

orSI 0.0150

mgn 0.0fi)40

tngl 0.0150

rEn 0.0150

%

sw846 8270C 27-|,1l€/-47 2a.l,,ar47 7031592 M-A

Tot{l Mctrb by EPA 6000t000 S€.ies Meatodt

7tl:|€l€7i MetEUry

Toral Mearb by EPA 200 Series Methods

7440-?2-4 Silver

7,t4+3&2 Arsenic

7r,qL3S3 Badum

744{4r,9 Cadmium

744G47'3 Chromium

743O.92n Le€d

ZA2-192 Selenium

BRL

BRL

BRL

t0,4

BRL

4.41

3.65

BRL

SW846 747fA ?3-Mat47 294ar47 7031495 YP

EPA 200.7 2&Mar{7 2E-Mar-07 7031494 RM

SPLP Metdi by EPA l3l2 & 600{y7000 Scricr M€thodr

sPtP Extraclion CorfiPleted

lK+22-. Silver gRL

74rloa&2 Ansenic BRL

zaG3*3 Earium BRL

BRL

BRL

BRL

BRL

BRL

91.9

1 SW8461312 26-lrsr{7 26lvl6r47 7031560 BD

1 SW8461e1Z60l0B 2&Ma.-0? 2e-[,ta(42 7031651 HB

1 '

l '

1 SW841i 13f2//470A ' 284at47 7031652 YP

1 SW8,l{i 13'1260108 ' 26-firar-07 7ffi1651 HB

SM2540 G Mod. 24-ttaq9l 2+Mafi? 7031470 QP

Thls tabo.dlorf Epod ls nol vobd wilht.d an authot:hd tlgndarc od the eeer pagE-

+ Reportabl€ Detection Limit BRL = Below R€porting Lhnit P.ge 84 of l6J

Page 299: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-3s 2'-4'sA5980l-07

Client Proiect #301 -88

Collection Date/Time16-Mar-07 00:00

MatrixSoil

Received27 -Mar-l'l

CAS No. Analyte(s) Result FloC Unib "RDL Dilutioa Method RzI. Pnpand Amlycd Bot.h Analrsl

Volrtile Orginlc Compounds

yOC €xlcction

Volabl€ Oqanic Compounds

Field enracled

!s4q dry

lCftS dry

!s.4q dry

lEkS fiY

!e4q dry

lsfts dryps,4(sdry

lsnq dry

ttdks drpsn(sdry

lsnq drypsn(sdiy

uC4q dry

l,gkc dvp$4{g dlyptkg dy

PS/rq dy

uces dy

tidks dy

fdks dry

fore dryp940 d.y

|'jdks d,y

l4ikS d,ypglq dry

!S/rs dtYydkS dry

!S,4(S dry

ls,4(s dry

!04s dry

lCftS dry

!S4q dry

uSi$ drypsas fy

MceyuS,lg drypS/kS dry

la4q dry

t€,lq dry

l4lq dry

tj$/is dry

tldrs dry

l{As drypEKg ory

t,dks dry

}4fts(yus/rsdy!9'lq dry

udrs dy

voc

sw 846 82608

28{ar.07 2b+1a'{1 1031761 B0

@'AVAI 02-Apt.07 7M1017 mar

Prepared by method SW846 5030 Soil (high lev€l)

t613.1 1,1,2-Trichtorotifluoroelhane(fleon oBL

675,{-l Acetone oRL

107191 A.qy'onitdle 8RL/14x2 Benzene SRt

1o€.0e1 &omobsuene 8RL74.97 5 Bomochlorom€thane 8RL

75-27 4 Bmrnodidlloromelhane 8RL

15-2sz Bomolofln BRL/4.83 9 Eaornomefiane o8l

n.$.3 2-Eulalone {MEK} BRL

104.s1.8 n-EuMbanzqe BRt

r3s.98.8 sec-Sulylbnzene BRL

9€{6 6 ten€uvlbnzene BRL

7+15.0 Carbor di$rllide BFL

5623.5 Ca6on letrachtoride BFL

106'!,0-7 Chlorobenzefle BFL

7rrr0.3 chtooethane BFL

67€6.3 Chlorojom BFLt4 413 Chtosn€lhan€ BFL9549{ 2{hlo{ok{Uene BRL

1m4H 4.Chtootatuene BnL

9612_8 l,2-oibrorno3 chlorotnTane BRL

r21-46.i Dibomochlonynethane BRL10G93-4 1,2{ibrofioethane (EDB) BRL

74 qe1 DblomometuF BHL

s 501 1,2-Dichlombenzene BRL

s41-711 1,3-Dic+iorobenzene BRL106-1+7 1,4-0ichtorcbenzene 8RL

7571s Didlolodinuo{trnethane (Fleon 12) 8RL

701

t(]0

701

701

701

70_t

70-1

70.r

140

701

701

70.I

70.1

351

7 0 1

70.1

110

7 0 1

14!

70.1

74.1

1.40

70.1

70.1

70.r

70,1

70. r

70. r

14rl

70. I

70.1

70_1

70.1

7 0 1

701

7 0 1

fl1.1

70.1

70.1

70.1

70.1

70.1

701

70.1

701

70.1

701

701

70_l

50

50

50

50

50

50

50

50

50

5l)

5D

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

5{)

5t)

5t)

50

50

75.3,43 1,1-Dchloro6than€107{6 2 l2-Dd oroelhane1135! 1,1-Didloroelhene156.s92 ais.1,z-orchloroeh€ne156t0-5 lra1s.l,2-0ioiloroethene7&87-5 1,?'Didtoropop6ne

142-2ss 1,3.Oichlo(opropane

59+20.7 2,2-OichloOpropane

509s€6 1,1-Dicloopopene

10061{1.s cjs.1,}Difloropropene1cd61424 lens-13.DichwoptDrye10041-4 Etrylberuene87{8.3 flexehloobutadienes91-786 2-Hexanon€(M8X)

98-82.0 bopropylb€nzene

9S-87.6 4lsoptDpyiloiuene

1634{4-1 Me$yl ten-bltyl ether10810.1 4-lirethyl-2-pentanonelMlBK)

E@2 Methyiene chlodre9r-2G3 Nsphhalene

8RLBRLBRLBBLBRLBRLBFLBRLBNL8RLBRI8RrBRLBRLBRLBFLBFLBfrLBFLBHL

Thic laborurory kpon it noteali.l h,ttfuat an autho zed sig^atwe oa the coee, page.

+ R€porlable Detection Limit BRL = Below Reponing Limit Page lJ of | 54

Page 300: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMtF-3s 2'-4'sA5980l-07

Client Project #301-88

Collectioo DatdTime25-Mar-07 0O:00

MaarixSoil

Rec€ived27-Mat47

CAS N^ Analrb(s) Resu! Fl"S 'RDL Dilatun Llertod ReJ. Prepated Anzltzel BoEh AMW

Voldile Org.dc Compoundt

Vohne Oroanic Cofitoourds

Prepared by method SW846 50A0 Soit (high levet)

lcg4tl nfmpyb€nzeng 8FLlm-42'5 Slyr€ie SRL63eAi-o 1,1,1,2-T€t-edtoaedEn€ 8RI793+5 t,l2,2.Tdrad oroeham BAL127.1s4 Tetadlkrc€$€ne BFL108Sn Tdue{le 8FL87-616 i2,+TncHoohenz€ne 8BL12O82r 1,2,+Tddhlrb€r|za1e 8FL71-566 l.l,tTricfiloroqhane BnL791tr5 1,1,2-Tridllotodlare BFL791115 Trd oroehs|g 8RL75i$'r friclllorolbolwn€bano {Freon j1) BHLsjs.4 1,2,3_Tdd oEpropsne BFLe5.63.6 I B,+Tftnerybsnzene BAL10€{/_s l,3,tTdmehylb€nzene BFL75{l-4 Vinyldrtonde BBLl330'2G7 m,Fxy'ene BFLe547{ oxykn€ BnL1@9+s T€lrahydduran BFL&'.297 Efiyt efrer BFLs€{i6.0 Tert{my fi€hyi eher 8RL637-e2-3 Efi!4 tsd{r4i €her BRIl(c2o3 oi-isoproplt etllel BeL7s5{ T€n-Bulanol/ bulyt atcohol 8FL

mnq dy 70.1

Wrq dy 70.1

|lg/lq fiy 70.1

l4lq dy 70.1

lgxS dy 70.1

ljgfrs try 70.1

!9rS ry 70.1

AE dy 70.1

|€&sdry 70.1

tlg,rs dv 70.1

lryt0 frt 70.1

!s4€ fiy 70.1

wrady 70.1

rg,lqdy 701

rgrgry 70.1

wrg fiy 7!.1

|lg/s dy 140

ldb dly 70.1rddliqty ru1

tdko trv ml

N*qd.y 70.1

|4|rC dy 7Ot

l4trgdy 70.1

lS/tSfl 701

wrs d] l{xr

7V130 %7G130%70-13, %70-1fi%

sw 846 82608 @-Apr{7 IX00175l)50505050505050505050505050505050505i)5050505{)5050

@-49t47

12+911 1,4-Doxan6

1&404 +Br'n]onrhrob€'l?c,tlle

&1.2fr TolEno4S

t7060474 l,LDicllooellane44

t8dl-5?Z oibrOmoift$(ErneEtBne

ErOrcaNble Petroleuh Hydrocarbotrs

Eitaclable Tohl Petrohum l|]ldrocadons

Prepa.ed by method SW846 35508

&B-61.9 Gssolhosa7s3c2 Fueloilt2

6817e31.3 Fueloit#4

d86s?00.1 Fu€t 0l +61096!0o0 Moh(OtJ00l0qF0 Ariation Fuel

unklsnif€d

of|er oil

Told PetrdaJm tlydrc&rhons

Cf C36 Atipl|atic l-lydrMftoru

Semlvol.tlle Org.dc Coroportrdi by GC

OEarbd orine Posticid€6 SlV848 8081A

Pfepared by me0pd SWSil(i 3545A

309@2 Alddn

8RL

97

tu94

111

BRLBRLBRt

BALBFLBRI.2,,4{0Calculated as

a,{Eo2,480

192

nvro dry 711

dMg dry r11

n'gnqdry 741

mglqdry 741

|rdrg dy 711

mE*gdry 741

mdhdy r4l

nC4qdy 741

m$4q dty 141

ndlg fy 741

4+144 %

HI€ dY

n arc7 3GUar{? nF1Z2|cT ETPH

S1VB/|6 $8lA 28lt€f47 (|z.Aprfl 7031739

Ihk labonlory Eport t$ rrorvtlid tolthou on otrthoriud sigturure od th2 dtee! pa#.

' Repo.tabl€ Detection Limit BR! = Below Reponing Limit P€e 34 of 154

Page 301: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationNI8F.35 2'-4'sA5980l-07

Client Proiect #30 | -88

MatrixSoiL

Received2'7 -Ma(O'7

Collectioo Date/Time26-Mar47 00:00

CAS No, At'abte(s) Result Flog Unils +RDI Dilu,ioi Method Rel. PEparcd Aruuzed Balch Ahallst

Semivohtil€ Organlc Compo{nds by CCOroanochlodne Pesbcides SW846 8081APrepafed by method SW846 3S45A319{4€ a-BHC3r9 S5-7 b_BHC3re-86-8 eat&5&3s s g_BHC ltindane)t'7+9 Chlofdane2,5,r_! {,4'.000 (p.p }72 5ts 4,-4LD0E (p,C)

5G2*3 a,4LDoT (p,p )6GtJ oieldnn95990'0 End6ulfan I3"13.654 Endosufan tlr@1{7-€ Endosullansultaten2as Endin71tr.934 EndrinAtdehyde7e444 Heptachlor7?135 Methoxychlor102157'3 H€ptachlorEpoxide3001-35'2 Toxaphenes103 /1 9 a{hlordane556&3f7 g.Chiordane

t3194?0 5 Endin K€tone

t0M-81, 4j-Dg&hn@djphenyl(Sl

45t.2+3 Def€$lotobiplgnyl(Si

Potuchlorinated Biohenvh bv SW846 m82

Prepared by method SW846 35454

12674 I|2 PCB 1016]lr04 2&2 pCB 122111r1rr6.5 PCB i2328t169.214 PCB t24212672'2s-6 PCB 124€110e76s 1 FCB 12541r0$82.5 PCB 12603132+tr5 FCg 129211r0cr44 PC81268

t886a+2 4,4 DB CYqnuotdiplp1l't (g )20512+3 Dec&tloafulgDyl(St)

Srmivolstil€ Orylnic Compounds by GCMS

Semivolalile oryanic ComoounG bv SWB46 8270CPrepared by rnethod SW846 35508

&L3? I AceGphhene20S-96€ Acsnephh!4ene62 53 3 Adln61n.12.7 ff{hrec€ne1912.21-9 Atrazine1@3'3 fuobedeneniphenytdiaTine9.87.t Bazllinessst3 Benzo(a)anhracen€

BFL

BRL

8FL

8RL

BRL

BRI.

BRL

BRL

BRL

BRL

BFL

BHL

BHL

BFL

BFL

BFL

BFL

B8L

BRL

BRL

67

102

BBL

BRL

BRL

BBL

BRL

8Rt

194

ERL

8RL

ffi

95

3it4

33.4

3r.,133.4

167

33.4

334

334

B 4

33,1

33,1

33.4

33_4

33.4

33_4

33.4

33.4

167

33.4

3:r.4

33.4

pg/ksdry

|'}g*S dry

wlg ey

tiS/r(g drypgks dly

!s/kq dypS,tS dy

tS4(e dy

$4q dry

!s4q dry

lsnq dry

lgftS dry

tigts dy

Ps*s dry

!SI(S dry

!s/rS dryps,ks dry

|]drs dry

lEtq dly

/9t9 dry

lrg/lq dry

w150 %

3Gtfr r.

!S/kg dy

fdkg dry

yg/rq dy

!04q dy

ys/rc (lly

lslq dy

!g/l€ dry

!s/rq dry

ldfs dry

30-1fl %

&150 %

sw846 80ErA

I

I

I

I

1

1

1

1

1

1

1

I

I

1

I

l

I

!

2E-Ma,{7 02-!Or-07 rc61739 TG

BRT

1,lffi

BRL

3,120

BRL

BRL

8RL

28,000

ldlq dy

udlq dry

!S4q dry

ldlq dly

lglq dry

ldre d'ywke &y!S4q dry

sw8.46 8$2

sw846 827m

66.8 1

66.8 |

66.8 1

66.8 |

66.8 1

516.8 1

66.8 1

66.8 r

66.E 1

919

9 1 9

9 1 9

9 1 9

9 1 9

9 1 9

9t9

s19

28{1 07 3+Mar-07 703173E SM

29{rar47 0GAprr)7 703124 M.B

thk labotulory repod is not rdlid withou! er au,horized sigt'sturc on the .orer page.

* Reportable D€iection Limit BRL = Below Reporting Linir Page J5 of 154

Page 302: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdefltificationM8F-35 2'-4'sA5980347

Client Prciect #301-88

Matri{Soil

Collection Date/Time26-Mar-o7 00:00

Received27.Mar07

CAS No. Anolyk(s) FI4S Unia *RDL Dit,tlion MelM ReJ, PEpand Arralrz"n Babh Aaalyst

Sfmivoktile Orgstric Compounds by CCMS

S€n*volalile oroar c Com!@nds bv SW846 8270C

Ptepared by msthod SW846 35508

sc3?.8 Benzo (a)pyen€20t90.2 Senzo(b)nuoanfEne1s1.2+2 &nzo(g,h,ilp€Mene207{8 9 EaEo {k)fluo€nhene6s-€6{ B€Qoicacidlql5r-6 Eenzy ajmhol111.9r-r B6{2d1lorc6hory)nehaner11.4r.1 8is(2dtoroetryl)dErwa Eias(2{tordsoprEpyl}e$er11?{t? E}is{2€t'ytr€xy')Fthehte10n553 +&omopfienylpftff/eher85{&7 suv bd[y' phtEhte

8&7,1-8 carb€zol€5S.5G7 +cHofo-9melhylpfi*tol16-.47-8 +Ctoioaniline9r-5&7 2{htoronadlhalene9'57-8 2{fitoroph€rd700$72.3 44 orophenyj phefiyleth€r

2lS!r.9 dvlsene53703 Db€ru0(a.h)antlrac€na13e{.tg Ub€nzoluanF50r t2-Dic]{orobenzene!11-7!1 l,$oidOrd€il?€ie106-{6-7 l,lH}cnloaob€nz€n€9t9r-r 3S.Ddorobeoidnerzo.slz z,4.DchtoroFh€noi3/r5G2 Dia v phhatate

131n13 Un€dM phflateh

105.674 2,l-Oimohytph€rd*7+2 Di{-butyi phhatate

53,t62r 4,6,Dinitrc-2-fi* rytph*tols1.28.s Z+firibophendt2t.t+2 a+DdhotdLlene6os2dz 2,6-0initrototuefle117€4{ Dl-n{dylphfidato2!6-140 Rro|antlr€{le*7!1 FfuoEne11&7+t Hsxfthloroberuet|ofl{&3 H€xdtkrobuhdenen471 tl€xadoro.-ydopontad€neSI-72n Hersdtoo€ aners93F5 hdeflo(1,2,$cd)pyr*r€!&t2{ 1_M€Nny'flept{hdene7!6$l tsopholo{|6

9167-6 2-fretvnap|lt1al€nsH&7 2.l'ldhgFnsNl

log3o-4, 3,+MemylpfEfrol106-44-591-rni! Nrphdlelele&744 2-Nftoaniln€9909 2 $Nlroanilin€

n,2u4,269,S036,m0BFLBRI.BRLBR].BNLgfrL

BRLBRLBfu8RLBRLBFLBRL8RL33,800BNLBRLBFLBRLSRL8FLBRLBFLBFL8Rt-8RL8RL8nLBFL8FLBRI.39,5008f,1BRLBFLBRL8Ft_ft,7nBRLBFLBFL

S,RLBRL

BHLBNL8FL

tdr{dfl

BIq dty

|ldlq dty

wqtvlsrq dv

ustg dv

|ldk dv

lclqdvudlq dryudlq rv

ril4d'rt4Wd.vl4b dry|lgks dry

Abdvldk9 fvldrs evl'9IS dv

usnq dv

l'drs d]

ldrg dY

|ldks trv

|ldh fiv

l4hdv

uslq dv

Eilq dl

ldrq dil

wrs dv|lgb d'Y

lls,lqd'v

Aks dv|Jsi|(g trv!9h dy

|JgNq fiI

ldB dv

lrybdty

tC,t S dy

|,gt(s t)'

ls4q trv

|,glq tv

|{rq dY

l4'lq dy

trdrS 4Y

|Js/tsdv

lsnq fY

Hlq r,

Elq dv

llg4q dv

lc4q trv

WkS dty

srY846 Ee70C919 |

919 1

9t9 l

919 1

919 |

919 I

919 1

919 |

919 1

919 1

919 |

91S I

9r9 1

9t9 1

9 t 9 |

91S 1

9t9 I

919 1

919 1

919 !

919 |gts I

919 |

9r9 1

srg 1

919 1

9t9 |gts I

919 |

9r9 1

9t9 1

9 1 9 I

919 t

919 1gts 1

919 I

919 1

919 t

919 |

919 |

919 I

srg 1

910 I

919 |

s1t 1

919 r

9 1 9 1

919 1

919 I

&lr?f47 0&,ptfl 7fi1n4 M.8

Tkle laborcbry repfi is not volid d!ho.!t ad acthorkd slgndur. oE rte coeer page.

I Reportable Dct€ction Limir BRL = B€low Reporting Limit Psge l5 of 154

Page 303: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Salnple JdentificationM8F-3s 2'-4'sA59803,07

Client Proicci #301_88

Collection Date/Time26-Mar-07 00:00

MatrixSoiL

Received27 -Mar-0'7

CAS No, Andyte(s) Flag Units *RDL Dilution Method Retr Pnparcd Analyzed Botch Antll.st

S€mivolatll€ Orgrnic Compourds by CCMS

Semivolalilo oruaric Compoun6 by SW846 8270CPtepared by method SW846 35508

100.01-6 4-Nitroanitine!E-95 3 N'trob€nzene0&?5 5 2-Nitropt€[email protected]/ 4-Nirrophenol6?_759 N,Nitrosodimetiylamine621.6+/ N-Nilros€di-n-propylamine8630{ N-Nilrosodiphenylamine

tr/lFs Pentadlorophend

E54r'8 Phe0anfrenelod 9.t2 Phenol129,00-0 ryrene1rGB6r ryridine12G02-1 1,2,4-Tiohlorobenzene95€s-4 2,4,5-Tnchlorophenol33{62 2,4,FTrichlorophenol

Pt-@4 2-FhJotobi*]€nyl

367-12.4 2-FhJolophenol

1165601) l&frObenzene4s

1tou62-2 PlErol4s

1/1e51-0 l6rpl6nyl-d4

lte44 2,4,6-Itb@n]opheflol

ERL

BRL

8RL

8RL

BRL

BRL

BRL

BNL

2,90n

8ff1

56,500

BFL

BFL

B8L

BFL

55

66

75

65

41)

sw8!6 6270C 29-M3r47|]g/lq dry 3670

ldkS dry 919

lsnq dry 919

fdk! dry 3670

pSAS dry 919

Irsas dry 9r9

|alls dy 919

|aAS dy 919

llg,ts dy 919

MCet 919

|l0/t0 dy 919

tloil(S dry 919

la4(sfry 919

l,qn(Sd] 9rg

uq/l(Sdry 9rg

*13,%

15-110 %

3tJ-19 %

11110%

w130%

1 1 1 1 0 %

mgaofiy 0 0366

mgkg dly 122

'ngle dry 1.83

mS4(S dry 0.610

mgrs dry 0.30s

'ng/|(S dry 0.610

mSfiS dry 0.91s

mglg dry 1.83

rngl 0.0100

mg, 0.0150

mgn 0.0060

no,l 0 00e5

mgl 0.0125

mg4 0.00041

mgl 0.@75

mgl 00150

09Apr{7 7031774 M.8

Totrl $letals by EPA 6000/7000 Sertes Merhods

Total Metal! by f,PA 20O Seri€s Methods

7440-e.4 Silrcr

744G3F,3 Barium

7140rA3 Cadmium

711447-3 Ciromium

7€9-@r Lead

rl821r2 Seledum

03'AF'{7 7031810 YP

02-Apr{7 7031809 HS

2&Mar-07 7031763 BD

02-Apr{7 7031805 LA

02-Apt{7 7031806 YP

02-tg{7 n31N5 tR

30.Md{7 7031879 YM

BfrL

17.7

7 2 4

0-957

7.53

40

2.m

0.19€ Q-Apt-07

02.4pr.07

2&l,lar 07

301',lar-07

sl/t€46 74714

EPA 2O() 7

sw&613r2

sw846 t3r?]60l0B

SPLP M€trls by EPA l3l2 & 600{/7000 Seri€s Meahods

SPLP Exlrachon Compl€led

14!+n-1 Silver BRL

744$?&2 Acenic 8RL

74|l).393 B€rium 0.0126

z4ro-439 Cadfivum BRL

74,|0-17.3 Chrc.niurn BRL

743s97$ M€rc!ry 8RL

74N42.1 tead 0 0300

n&.a9.2 Sst€nium BFL

Cenetrl Chemistry Parrmeiers

% Solids 81.3

sw8{513t2t47M

srt846 13.12/ffi106

Sll2tl0 G Mod. 30+,la147

Th labo.atory repo.l is noa vdd flilhoat aft aulhoized sigadute on the cover page

* Reporlable Detection Limit BRL = Below Reporting Limit Pege 37 of | 54

Page 304: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-36 4'{'sA59803-08

Cli€nt Proiect #30t-88

Collection Date/Time26-Mar47 00r00

Received27-Mat-07

MalrixSoil

CAs No. Aaalr'te(s) Reszlt FloS Uails 'RDL Inuion Med.od Rel, Prcporcd Anatyzed Eokh A^aIFt

Volal s oroanic Conbolnds

Prepared by method SW8,l6 5030 Soii (high tevet)

78131 t,12-Tidtlomtrifluoroehane(Fr€on BRL

@5+1 AaetoG BRL

ro7-13,j A('yloiitrile BRL71w2 Benzu€ gFL

1@€61 Bonobglz*ts BRL

7+97-5 Eomoahlom|nelhane BFL7rzr4 Eomodkfilorollletturle BRL

E&2 Eomolorn BRL7{{3€ &mdnohale 8H!

?&s-3 2-Buhnon6 (MEK) 8Rt1or-51.9 n-Butylbenlens gFL

1ffi8 s€eBulylbnzen€ BfiLsc{G-6 tert-Bulyibnzene BFL7s150 Carhsr dEllfrde BRLsn-2o5 Cadon tdraclto do 8Rt-

10&9G7 ChlotEh€nzene BFtt5+3 Chtoro€lfiare BRL

57-66-3 Ctbrotonn BRL7447-x chlotun€tl*ne BFL9549'8 2tl{orDtoluene BFL106'13-4 4-Cl*rotdu€n€ ARI

9c123 1,2-0ib.Cfilo-Jdltooprogane BRL12'1.4&l Dib.unod ololnehanB 8RL0e9+4 lz$bronoelhane (€DBl 8RL7+9+3 obrcnun€lhane BfrL96JG' 1,2-Dicl orcbenzene BFL

5/rl t+l l,C.Drcl orob€nzene BFL106',167 l,l-Did{oobenz€n€ BRL

Volstile Org{dc Compound!

VoC Ext-adion

?5.71-8 Dchtorodiffloroftetiane(Fem12)

75-3,r.j l,1-Dciboetune

1n&2 12-Did doghane?+354 1,l_ttichlflo€ltlene150{92 cis.l,2{)idoro€henor56-6Gs tans-1,2€ichloros$€n€1t41.s lp-DicfloroFopan€

1.2-?44 l,3.0id{ofop.ogane

s+a}? zl{icftloropropans5G358{ l,l-Oido@popen€

m61{r.5 cis-1,3.0idhropnDslslF€l€{ tra1s.1,3-0ichtooproFemro0-.1J EhyoeizBn€O€&3 lt€td*rDbutadenes1.74€ z+to|rldts (MBK)

S-€2-8 lsoprlDrlben!€ne9s{45 4kopropyibfusot6a4-0t-. ohy'toii.butyl€tEr1{€ro1 4-f'lettryl-2{enbndl9{MIBK)754&2 Mdtyl€ne d oidegtltt-s llepht|ql€ne

284sfA7 28-lrar{7 7m1767 BD

C2$rfl 02-Apr{7 40017 oLr

Frdd exlra.led

|4/rS dry 104

ltlqdy AEo

Ug4qdry 101

tdkCdy r04

|]dkS dy 104

us/kg try llM

pgks dy 104

ldh a r04

|.drq dy m8

Udqdy 1{X0

|lErg d) 104

!S,lS 4y t{X

lJ9k0 fy 104

yCtS dr 321

t44€ dy t04

Enqdy 104

ellqdry 208

ug/l{g dy 104

lSIq dV a)B

lgkg try 104

pd*S dry t04

t.qh d'y 208

|l€|4€dy r04

lSlqdry 104

|{irg dy l(X

lgrS dy l(X

r/9,*g dry llx

!9,rS dry 1&

lqrs dty m8

lElqdy tu

wkecy 104l,glEdy t04

!C,lq*y 1(X

lgrS fry rr]4

!S49 dry 10{

llg4S dry l(X

FCr0 dy r04

Fg/tq dry t04

US/rqdy 104

|lg/l(S dy 1(X

!e/rS dV 1(X

ldhdy 1{x

pS*S dy 1040

Uglq dy 104

Udlq dry 10t

$nqdry to4

ryrs d] 1{x0lSl]q d-y 1{X0

|lgrg d! 104

vclc

sw 8,46 82608

SRL8RL8FLBRLBfiLBFLBRLBRLBRI.BRL8RLBNLBfrLBFL

BRL

8RLBRLBHLBRL8€LB8L

g

50

50

fr5i)

50505050505050fr

5050505050505050505050505050505o50

5t)50505(l5050

5050

50505050s05t)5{)505050

This hbodo.y rcport ts not vtIU *itltot( z^ zathorizd stgt ficre oa thc cover pqe.

'R€portable Detectioo Limi. BRL = Below ReportinC Limit Page 38 ofl54

Page 305: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationM8F-36 4,{,

sA5980348

Client Proiect #301-88

Collection Date/Time26-Mar 07 00:00

MatrixSoil

Reccived27-MaPl1

CAS No. Analyte(s) FloC Unix +RDL Dilatioa Melhod ReJ PrcpoEd Atebized Balch Analrs.

Volrtile Orgrnic Compounds

Volatile Orcanic Comoounds

Prepared by method SW846 5030 Soit (high tevet)

r016t1 n-Prcpylbenzene BRL100-42-s Styrcne BFL83020{ j,i,j,2_Tetrachlorcehane BFL79.345 1,1,2,2-Telrachlooethan€ BRL12718-1 Tetrachloroehene 8RL103{3 3 Toluene BRL07{1{ l,2,3,Trichlorcjbenzen€ BRL12ss?-1 1,2,+Tridlootcnzene BFL7r-5s-6 1,1,1_Trichtoroethane BRL7s{0 5 1,1,2,Tri$loroelhale BRL79-01-6 T.idrtoroeti1ene BFL7s{+,r Tdc}torofluoromelhane (F€ofl 11) BFL96r+,r jl,3-Tdchloropropane BFL95-63-6 12,4-Timeltrytb€nzene BBL108-67.0 j,3,S,Trimelhybenzene 8BL75.0r-4 Vinytdtoride 8RL'300.207 m,Fxyt€ne BRt95-47{ oxyi€ne 8RL10s99.9 Telohydroturan BRL60 !e.7 Ettryt eher BRLs94.n5r Tenn|lrytmeiiyi elher BFLa7-e-3 Ehyl lerl-butyi eber BFL108-2G3 Ojsopfop/ elhe. BFLtus{ T€rt€ubnot/ buM ajcoitoi gFL

12&e1.1 l,-4,Dioxane BBL

16-sI1 4-Bononurmbenzene

Nt-265 Totuer,edB 1001tw474 | 2aichloroetharc44 94t36+53-/ Dihmnofluo@nehane 1'14

f, rlrrctrble Petroleum Hydrorarbon!

Exkadable Total Pelroleum Hydrocarbom

Prepared by method SW846 35508

3ao6-619 Gasoline BHL6e47 02 Fuet Oittz BRL6B47E3rn Fuet Oitt4 BRL

Er55s-00'1 Fuelol*6 BHLms€ldtoo Mo|o{Ot BRLJ0010{000 Aviafon Fuel BFL

Unid€nlified BFL

Olhero BFL

Tolal Petrdarm Flydro..adons BFL

C$C36 Aliphatc ftdocaftons BFL

ttl6-3?2 l-ClloifrE&cme It7

Semivolrtil€ Orgrnic Compouods by CC

oroanochlorine Peslicjdes SW846 8tr81A

P.epared by method SW846 35,{5A

30e{0.2 Atddn BRL

lgrlg dry 111,1

ldks dry 104

|-€AS dry 104

lElg dry r04

Udlq dry 104

Wq dry 104

lylqd] ltx

lgkg dy lrx

!g/kS dry 104

!S/rS dry I04

lstS dry 104

pSrkS dry 104

|l!r'lq dry 104

ldrq dry 10.{

pS/rS dy 104

lC/ftS ey 104

lSIq dy 20€

ISAS dy 104

lS.ftS dry 1(l4o

trS4S dry 104

ps/rs dry 104

lstS dry 104

tidr(S dry 10,1

fdkg dry 1040

pSI(S dry 2@0

7Flin %

7+130 %

/0-130%

7&13t%

sw 846 8260A

+CT ETPN

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

m'Apri7 02-Apr{/ 7040017

2J-MaA7 n-Maf{7 7031772

28{ad7 l2.Apr-07 70111733 TG

r{/tg dryrng,tg drynEaq drymg/rq drymdtq dry'nEIS drymqlq drymSn€ drymgr! drymdks dry

4+t4It%

98.2

96.2

9E.2

98.2

s.29€.298.2

982

!]a2

942

lgfts dv sw8{6 8081A

Thb labonto4t rcpotr is not edld {ithotd on authorized sipta.urc on the cnwr page.

' Reportable Detection Limit BRL = Below R€porting Limit Ps€e Jq of 154

Page 306: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeotificationM8F-36 4'-6'sA59E0l-08

Client Proiect #301-88

MalrixSoil

Rec€ived27 -Matr41

Colle€tioo Date/Time26-Msr47 00:00

CAS No. A"rlyte(s) Resatl Flag Unitt *RDL Dil ttion Method n4 Prcpared Analyzed Batch Anzlfdt

S$rivolatile Orgrntc Compoundr by CC

Ordanodllodne P€stcii€d SW846 808rAPrepared by method SW846 3545A31!IC4-6 a€ltosr$or7 b€rcsre€6.E +BHC5&se.s $BHC (Lindane)5t.7L9 O o|lhaE

72-5,r€ 4,4,-0tt0 (p,p )72-sf,e {,4'-DDE(p,p')

5G293 4,{.-DDT(p,p)60.5?n Dielddnss9{l-8 fudcufisn I3!p13.664 Edo€ulfal lltm1{7{ EndGulhnsulfaten.?!4 Endrin71214-1 Endrin adehyd€7!{,Hr H€phd{otz{3-5 tt4ethoryd orr@'Lt-3 Heghd o( E0oide8m1{9? Toraph€$e

5103,7r-9 a{ldoadale556e317 g{hla.dane

534947G5 Endnn K€tone

twe12 1l-DBMtunrdithst4(St)

,'61-21,. oed,bobifunrlBt)

Pdvd odnaled Bi*envb bv 5W8,4{i 8082

Preparcd by method SW846 35454

r26r+x4 rcB 101611104?C-2 PCE 1221111{1-16.5 rcB 1E2s346+21-9 PC812{212t72.294 PC8124811(s7-€s1 PCB 125{r1o9€€-5 PC81250Te+es Pc€IZgzr11fi!r1.,1 PCB 1266

54ro98l, /eco€rt rit@644-, 4Ae&htthr&iptenf(s4Mtas Def€f,llotoLw(*l

Semivolstile Orgaolc Compoutrdr by @M

S€mivoladle Ooadc CdnmunG bv SWt46 8270C

Propared by rnethod SW846 35508sHe{ Acamphtlgne2(+9€{ Ac€.Ephdryt€ne6e'5$3 Aniline1?!.12-7 Anfr@fi1912-2+9 A[ezino1@-B-3 Azot€ruel*/Dipf|€nytdazineq4{7-5 B€nziine56.56-3 B€rEo (a) d,hrac€ie

2t. al{7 02{pr{7 7m1739 TGBRLBRL8Ft8RL881B8LBFL

BFLBRI.

8RLBRI8Rt_BNLBfiLBFLBRLBRL8RLBRL8RLBRL

67105

8RLBNLBRLB8LBFLBRLBRLB8L8RL

td)

BRIBRI.BNLBALBRLBFLBRL8RL

lth dv!g/rq ryU91q dry

ldlq dy

u{ylq dy

Enq dry

$.sev!S,lq dy

ldh dv

|l9l€dyUSrq dry

|JEb dv

lgrq trv

udrsdvtj{i}qdvrgls dv

$re dv

rcaq dv

|lg1gdv|Jsrq dv

ldhdv!9k{ &y

ah rvrd&dyl8rgOlsitq dy

|Jg}s trv

lgts cy

!4lq dry

&150%EItfl

lgrs ry|lgrg 4y

tdftS dry

|dl€ dry

lldh dv

uglq &vt4bevPglq dl

loh d|/

* l i l t6

, t g %

sw846 8081A

sw816 8[82

sw845 8270C

43.343.34334332164i1.3

€.3431€ 34]3€ 343.3

43.3€.3€ 3€.343.3216{3.343.343.3

1

I

I

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1

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I

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1

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86.5

86.5

86,5

865

865

665

86-5

86-5

86.5

A.$w47 3& ar{7 70317"J4 SM

0!.4F.07 761771 M.B6{E

6{B

609

609

60s

609

6&

609

ThX hboralnry reporr is ao/ vdu x'ithod atr outhodrd signata.e on lhe coecr pa9.

* Reponable Detection Limit BRL = Bcbw Reporting Limh Page,(} of 154

Page 307: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-36 4'-6'

sA59803-08Cliept Proiect #

30 l -EEMatrir

Soi lReceived

27-Mat 07Collection Date/Time

26-Mar-07 00:00

C4S No. Analyte(s) F,oe Ani6 *RDL Dilutioh Method ReL Prepatert Ahulyled Batch An.tlfst

Semivohtile Organic Compounds by cCDtS

S€mivolalile Orcanic Compounds bv SW846 O27OCPrepared by method SW846 35508

s0-32-6 8€nro (a)pyf€nemtes 2 8€nzo (b)nuoranthenelel-21-2 &nzo(g.h,i)p€ryI€fle207{€-9 Benzo(k)lluoranhene55-€€4 &nzoic acidr0cs1.6 Benzyl alcohotr r r .91-t Bis(2{hlobehoxy)nEthaner11-4,t-4 Bis(zdo{o€lht)elher39c38-32-9 Bis(2+htororsopropyl)elher117.017 8bl2+htheryDphlhatale1fi-55n 4-Brcmophenyl ph6i/ €her0s{&7 &rtyt benzyl phthatate86 t r.8 Cabazole59507 4{hloro-}fistnytphend106-17{ 4-Chloroanitine91-5&7 2,Chloromphthalenssasrr z_Chtorophenol7w-12 3 +Chtorophenyt pheny' €th€r2r3{r.9 Chrysene53143 oibeflzo(a,hianftraceoe132.6,1.9 Dibffzofuran95-501 1,2-Dictoobenzenes41.?31 t,3.Ddttolobenz€net6-4+7 1,4-Ckhlorob€nzene9144.1 3,3',0ichtorob€nzidtnet1r89.2 z,1-Dtltuotgnd8466.2 Delhytphthatater31.r1.3 Dimebytphdlalate105 67e 2 4-tlmelhylpheoolw1q.2 Di_n_butylphhatale$452.1 4G0inilrG2-melhy,lphenol5r-2s.5 2,4-tlnitrophenol121-t+2 2,4-Oinitolol0ene606.2G2 2,6_0iritrotoluene117444 D_n_ftl/ph$alate2c6.14-0 Fluodnthefte

11&7+1 ll€xadotobenzene07{€.3 Hexsdorobutadienen47.4 ltexadtloncydopefilad€nett12-1 }l€xadkriE€liane1s3 3e5 Indeno (1 ,2,3{d) pyrenes12-o l-Methylnapfihateje78-591 hophomnee1-5z6 Z.irethytnaphhalene95-4&7 2-Mslttytph€nol

10s.3s4, 3,4-Meh',iphend

9!'lo-3 Naphthaleneo&7,r4 2-Nitroanitine991rsz $Nitroaniline

gRL

BFLBFLB8LBRL8RL8RL

BRL8RL

BRL8Rr8RLBRLBRL

MLBFLBFLBFLBFL8RLBRLbFLBNLBRLBBLBBLBRLBRLBRLBBL8BL

BRL8RL8RL8RL6RLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRL

8RL8RLBRL

l4kg d'y

t'SkS dy

lqkg dry

ldkS dry

lyks dy

PtrS dy

x9lq dy

rc4q fry

rgrc dry

lgtg dty

194(s dry

wkq dry

wrsdv|rs^s drvlrq/l(S dry

rcag dry

ldlq dry

uglq dry

UgfrS dry

@WevrctS dry

runq dv

!s,4q dypgks d'y

Psiq dy

trol'tq dypErq dy

tsas dypgag dq'

Ug/rg *y

I'dlq ty

ldko fy

ldks ry|lyl(s rv

!c4q dy

!S4{0 try

rcnq dry

rdkg ffy

fSIq dry

ugAS dry

lsiks dry

usas dry

!S.4q dry

tg.4q dry

fS4{ dry

!94q dry

!g4q dry

ldkg dry

ldkS drY

tdk0 dry

609 1

609 1

609 1

609 I

609 1

609 1

609 l

60s r609 l

609 1

609 1

609 1

609 1

609 1

609 1

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6 m r

609 I

6ffr 1

6C9 I

609 I

609 |

60s I

609 1qts I

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603 1

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slt/8{6 8270C 29Mar{7 03-AO.{7 7931T4 M.8

Thie laboralory rcpo is not vstid without aB zalhofiad sigaat re on ahe cover pge.

+ Reportable Derection Limit BRL = Below Reponing Limit Page 4l of 154

Page 308: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple ldentificationM8F-36 4'{'sA59803-08

Cliedt Proiect #301 -8 I

MatrixSoil

Receiv€dZ7-MaFo'l

Collechotr Dat€y'Time2GMar{7 00:00

CAS No. AnatytA(s) ft.salt Flag Ania rnDL Dilullaa Method Ret Prepared AMIWi Bateh Adzbsl

Scmivohdle Orgmlc Conpordds by GCMS

Senivolade Oqartc Cornoofids bv SW846 8270C

Pr€pared by method SW846 35508

100{13 4ltto€d[ne

s 953 Nitrobdu4fle

88 r55 2-NitroplEnol

{b{e.7 [llitroplrenol

82-754 N-Nifoooditiehylamin€@1n+1 [+Itorodi4{ropytarnine

ftiJircsodplErytanin€87llO-5 Ps\tad'lorcFh€f,d

85{1{ Phenarhrene10&9s-2 Pn€rdr29{on h/rmell0-8s1 PWin€ro-02t ',z,+Tftlorohenzene

Fls-. a{,5-Tft$brophenol8!(F2 2,a,ST'idttorophe.lol

e14-a z-nuodlnffiri

s/.121 2hn@E(d

1t65aa lliffig'zene4'

11f6{2e Pt!€tdi6

tTta-i14 ferpw44

tt'.:9-6 24,+Td4atagh*A

2949/47 tFApr{7 7O3i?4 M.8gRL

8eLBFLBRL8RL8RLBRLBgLB8L8FL8RtBFLBRIBRLBflL

4!)

n17

|l9l|(gdy 2,1.{1)

tEkSd] 6A9

|lgftS dr 6oe

tqlS dry 2U

r4h dy 609

lglqdy 609

ugtsdy 600

E/to tI m9

!!yh fI 609

lglS dry 609

la/l€ fi} 60e

Uglqdfy 609

pgdqdy mS

l{/l(g dy 603

!ELS dy 609

*130%

trfio%

&1E)%

1*110%

w130%

t5.110%

sw846 8270C1

I

1

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7,F0{7{ ltrs|ulry

Tot.l M€ads by EPA 200 Se.ies M€thods

240.224 Silver

71,{}3*2 ArEenic

zt{oost garfutn

7'|{l4gg CedriLn

71101r'3 ohro(nfum

7,lig92-1 Lsad

zle{? Sd€nium

Totrl Mctrls by EPA 6tn0/7000 Series M€tnod3

Bfu

BflL

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64.5

0.m7

3.65

212

2.30

SPLP Metals by EPA 1312 & 5000/7fi)O S€ri6 Metftodr

SPIP E$Ection Comd€led

11,0-?2-. Srlver 8H-

744!3&2 An€na BRL

7{41-39-t Bariun Om59

7{0<-9 Cadnirfi BnL

7@4-s Chsniun BFL

7'r@47t ttlerdxy BRL

ftBc2-1 LOd 8RL

na2+2 S€l€nilrn BRt

Cenc..l Ch€mirEy P.rl]Del€r!

% solds 65.5

n'grgdry 0.0452

ndlsdy i.ls

n'gftg dry 2.17

ndrs dry 0.723

"Elq dry 0.36r

mdlq dy 0.7n

'nghdy 1.0€

mgt0 d'y 2.17

mq/l 0.0100

ms4 00150

nE4 0J050

mgt o@5

mgi 0.012s

me, 0.0m40

mS4 0.qt5

'tlg/l 0i150

swB46 7471A

EPA 200.7

g2-4fI47 m-Apl{7 7031810 YP

sw84613t2 28.lrar{7 2&t49f.ll7 703176:} 8D

Sw846131260109 3!ttar47 (B-AF-07 70i11805 LR

sw!16131274704

SW8461312,&109

0e-Apr{7 TlxI$6 YP

02.AF47 T(]3lmS H

$tir2t40c$od. xlMsrfi 3rH,tur{? 7031879 YM

Thb hno.alorl EFotl is not rqli.I wi out ad iathoized sigaaure on lhe corerpoge.

r Reporbble Detection Limit BRL = Below Reportiog Limit Psge 42 of l5{

Page 309: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [deotificationM8F-37 2'-4'

sA59803,09

Client Pmiect #301_88

Collcctioo Date/Time26-Mar-07 00:00

MatrixSoil

Rcceived27-Mar0'7

CAS No. Anauk(s) Resalt F'lag L-nirr 1RDL Dik tion Itethod ReJ Prepared Analyzed Bctt:h AnarystVolalile Orgsnic Compounds

VoC Efraction

!g,tg dry 73.0

t4lrg fiy 1'!m

UgkS d'y 73.0

WkS 4 7X.0

tigtg dy 73.0

ldkS dry 710

u94g dry 73.0

Udr(S dry 73.0

!g4q dry 146

pg/|(s dry 730

J]g/is dy 73.0

pgiq dy 7t.0

lgrq dy 73.0

!C/rS dv 365

rrg4q dy 730

lgkS fy n0

!s/ks dry 146

lS.ftS dry 73.0

!S,4( dry 1€

llg4(S fy 73.0

ldkS dry 73.0

!S.4q dry 146

US/kS dry 73.0

!S.(g dry 73.0

N,4(S dry 73.0

lgftS dry nn

!q4q dy 73.0

!S4q dry 73.0

ug/kS dry 146

ugkS dry 73.0

udrs dry 73.0

|lg/kS dry 73.0

ug/l(S dry 73 0

UdrS dry 730

pdrs dy 730

Udlq dry 730

lElq dry 730

pgrs dry 733

lgrS my ft.o

lVkS dy 73.0

lglqdy l3o

!9rS dy 23.0

lgrS d!' 730

udkg dy 730

ldhdy 730

lCiq dD' 73.0

lyko dy T$

pO{ dry 730

pCAg *y 73.0

Volat-le Oroanic ComooundsPrepared by mothod SW846 5030 Soit (high tevet)76191 1,1,2-Trichlootdflrjoro€lfianelFreon BFL67611'1 ACelOne BFL107.13.1 Adytonitile BFL7r4r2 Ser'zene BBI108.861 Bonoberuen€ BRL7497-5 g|!{nodtiolo|n€lhane oRL75274 Bomadi$lolomeihane 8RL75212 Bmmoform 8RL7443-9 Brcmomehane BRL73.e'3 2.Butanone (MEK) BRL1M.s1r n-Butlt}lruere BFt135-s3€ sec-Butytbenzene BRL

led-Butylb€nzene BRL75.rs Cabon disumde BRL56235 Caoon tetmchlorjde BRL10S91'7 Chloroben2ene 8HL75-{03 Ctiorcelhane gRL

r-6F3 Chtorotom BRL7t'913 ChlorometEne BRL$-4+8 2{htorohJuene 8RL10643-4 +ChtorEtduene BRLe612{ 1,2,Dibrcmo-3drtorc9rcpane BRL1241+1 DibrodEdllo|l}mehane BRL10640-1 l,2,Dibomo€lhane (EDBI BFL71-9t3 oikofilornothane BRL95.scr l2-Drchloobenzene BRL541-7+1 1,$Dic{lorobenzene BRL10e4&7 1,4-Dichlorobenzene BRL15714 Dichloodillooromethane (Frcoil2) 8RL75343 1,l-Diciloroelhane 8RL1tr&z l,2-oichlooelhane SRL75-354 l,l-Dicitooethene 8RL15&58.2 cie1,2-0id ooefEne BRL1ffi5 trdrs-1,2-Dicilorcethene 8RL7r.87-5 l,2_Dichtoropopan€ 8RL142n.s l,$Dichtoopopane BRLwh1 22'Drchloopopane BFLs6$58.6 l,1-Drcfloropopene BRLr006r-01-s cis-1,+oid oopopene BRL10061'0?.6 ttars-1,3-Didrlooprop€ne BRLr004r-4 Ehylbenzene BRL8763-3 HdachlorEbutadene BRL

541JS.6 2+€xenone (MBK) BHL$-@_8 lsoprcfylb€nz€ne BRL99-87{ +lsopoDyfio{uene 8RL1631.04-4 [,]€$ylt€n buly erher BRL10slo.1 4.tvtethyl-Z-p€nlanone (tyfgtq 8RL75492 Me$ylene dbrile BFL

Field extaded voc

SW E46 826!8

2EMar01 26-M3r{7 7031767

@-apr-07 02-Apr-07 1140017

BHL

50

50

50

50

50

50

50

50

50

5t)

50

50

50

50

50

5!

5{

50

50

50

50

50

50

50

5{

50

50

50

5t)

50

50

50

50

50

50

50

50

50

50

50

5091-2G3 Naphhal&e

Page 43 of 154

Thit labo4tory rcpo.t is t ol vcud piihou an tuthorized signature on the corer page.

* R€portabl€ Detection Limit BRI = Below Reponing Limit

Page 310: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentilicatiorM8F-37 2'-4'sA59803-09

Clieot hoiect #301-88

MatrixSoil

Received27-Mar07

Collectiop Date/Time26-Mar-07 00:00

CAS No. AnzbE(s) Flag UalA 'RDL Dil$io6 L{etho.l Retr. Prepaied Anslwd Eatch An4ltst

Volstil€ Orgenic Compouods

Volalils oroaic CornooundsPrepa.ed by m€ltEd SW846 5030 Soil (high l€v€l)l0s.65r t}Pl[pylt€ru€.|e100-42.5 Styr€no630.205 1,I,12-To$adlloro€han€7!!3,15 t,|,22-Tdrachhroethan€127.184 Tdrddoa€fpne1088t{ Tdter\€87{1-6 1,2,gTdJ{oobg1zale12082.1 12,1-Tridorcae'uens?1-556 1,1,1_Tido|etiarcB{G5 t,1,2-Tridllofehane79O16 Tri:l ooefreng75.6s_4 Tticldo€nuoorc$ane (Frsn l l)sr8-4 12,lTridooPropanesG3-6 l2,4,TdmetrytbefPenerr,837{ l,s,lTdmsqy'ben2ene75{1-4 Vaylc.l o*t€r@e07 m,Fxyl€ns9447{ [email protected] Tetrdltdrolu6n

@-297 EryeherS1-05-s Ted€myj me0v eher87-92.1 Ery tert-hltyl eher1rF2G3 Dii6oFoBt drer753s4 Ten€lbfiC / blltyj atcohol12991-1 1,+DiOxarB

1@404 48tutpfrtuobqzene

M7-t6-s Totuene4e

t7@4t4 l,z-Adtfudlw1el4

taf'-597 AfuadofiuxutplItste

Ortr.ct ble Petrcl€{m HydroqrboE!

E*rE{aHe Total Pqtobln ttudtocadons

Prepared by m€thod SW84ti 35508

,d661.1 Gasoline0847s3+2 Fu€tOIt2

6847631j1 Fu6t otr *4

68sslo-1 Fud 0t 15

Wsd(oo ti{obr$l

J@10000 Aviati{ Flj€l

Unii€ntfi6d

on'.r OilTotd Peholdm l|}dllcartqB

C9-C36 AlFh6lh F drocaboG

.trfiolEb rBcotia'ier:

Semlvolrtile Org.nlc Comportr& by cC

oldod oihe P€sti{ii€6 SV{846 80€'lA

Prepared by metpd SW846 3545Aa09{G2 Atdrin

BFL8FLBFLBRLBRIBRI.BAt

BEL8nLBNLBRI.9Ri-BRL

BRI.BflLBALBFLBFL8RL8RL8Fi.BRI,BRLBNLBFL

991UJc4t11

505050505050505115050505050505i)5050505050s05050fl

50

wt{ trvHrq dv

dh dv

udh dv

dlqdvpo/bdty

ugre dv

H/lq dv

ldh trv

!9lr€ dy

dl'! try

drs dv

E/lq dy

UC,tq dry

dlq dv

lgls dv

|Jg/t{ dl

'Jdr€er

us,rs dy|lsnq dy

uglq dv

udl{ dv

|ryrg tl'

lqlq fr)'

lcE dt

70t3014701fi%7Vtfi%7V1n%

nglS dY f14

lr€nq dry 7t 1

rg,lqdry 7l-1

rnplqdry 7t 4

mB4qdy 71.1

mglqdy 7r.4

myxo dy 71.4

.nclq dry 71.4

'r9AS dry 7!.4

'rdE fiy 71.4

4tltlo %

l/g4S Ov

sw 846 826C9

€T E]PI1

73.073073.073.07t073.07X.073.0730

u73,0

73-0

730

73.0

73.0

t3.0

t{6

n.0730

73.0

73.0

7J.0

73.0

730

t{60

@{pf{7 0?-AFfl 790017 nr

291tar'{7 *klnf 781n2 DSBFLBnIBRIBRLBRI.BFLB8LBFLBFLBFL

sT{&6 8m1A 2'l,8147 02-Afl.47 7{X,l73{, TG

This rtldfllory repod h nor t)dM Hithon! at thor*td sEnat ue oB drz cwE p$4

* R€portable Dctccrion Limit BRI- = 8€low Reporting Limir Page 44 of 154

Page 311: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-3? 2,-4'sA5980t-09

Cliept Proiecr #30 t - 88

Collection Date/Time26-Mar-07 00:00

MatrixSoil

Received27 -Mar-01

CAS No. Ana+tz(s) Resuk FIoC Units 'RDL Di,utioa Method Rel, Prcporcd Anaryud Baich An/tlysl

Samivolatile Organic Compoundr by CCOroanochlorine Peslicides SW8{6 8081APrepared by method SW846 3545431934{ a_BHC319357 tsBHC

319-068 +BHC58.ses g-8rc (lndan€l

57.7+9 Chlodan€z-54r 4,4O0D1p,i)72-!64 4,4{DE (p,p )50.4n 4,4!0Dr(p,C)6t57.r Dieldrin95s.98-8 Endosultan I321355.9 Erdogrllan ll103107.0 EndosullanSulhtenzoa Enddn7421-s3{ E ddn Alddryde76414 H€phdlorn+95 l4ehoxycl or1024s73 HeplachlorEpoods3m1 3$2 Toxapiene5103-7r s *Chlordane5566347 gchtordane

$agl.7Gs Endin K€lone

1@6aa 4l-N.Uafrwffibheit4 (30

,,51-213 oe{aclXotobbhenyl(Sl

Polvdrlorinaled $ohenvts bv Sw846 8082

Prepared by melhod SW846 35454

12671-1 r-2 PCB 1 01 6111M-?3-2 PCB1?2111r11-16,5 PCB 12325346921.9 PCB 124212672-2+6 rcB 124611m7-6$1 PCB 125!1109s8n5 PCB 12603na!23-5 PC812621r1@r1-4 PCB 126€

103a6.84.2 44-Dg4ctafluotobwenyl(s0M1'2Lt ^e@hbrobhlcnyl(s4

Semivolatile Org{lic Compounds by CCMS

S€mivotatile &oanic Cornodjnds bV SW846 8270C

P.epared by mettpd SW846 35504

&-e4 Acenapldlene2084€.0 A.snaphfiyl€ne62.s3-3 Anilne12G12-7 Anhra4€nel9l2-2,1-9 Atrazine103+3-3 AzobenzsraoiptBrMdiazne92-87.5 B€nzidines&5$3 B€@o(a)anhrs{€ne

?3-Mal{7 t2-AN-07 7fi1rc TGBRL

BRI-

BFL

BFL

BFL

BRL

SRL

8Rt-

BRL

BRL

8fl1

8FL

BFL

BffL

BBL

8RL

8RL

8RL

BRL

BRL

BHL

122

8RL

8RL

BRL

BRI

BRL

BHL

BRL

8RL

8RL

u110

8RL

8RL

8RL

8RL

8RL

BRL

BRL

2,470

I9lS d,y

ts,lq dy

lsfro rvlJs&g drvWrsdnt!4rg dry

pglq dry

ldlq dv

pdks dv

us4q dy

pEl(sdrv

l,!As dry

|ls/ksdrv

t]s/ks drv

fvlq dry

trS4q dry

ldlq dry

!S4ts dy

ps/hl d]

!o4q (fy

ldkg dry

30-154 %

30-150 %

!91q dry

p91q dry

ugks dy

pltg dy

pgks dy

!9Xs dy

!SI(g dry

!s4q dry

pgrs dry

30t50 %30-1fr %

tlgts dry

ldks dry

lsh dv

lgng dvpgts dv

l,gftS dYpglsdv

H,lq dV

sw846 €081A

sw846 80E2

s!i18.46 8270C

36.5

365

365

t83

365

36.5

36.5

36.5

35.5

365

36.5

36.5

365

36.5

36.5

183

36.5

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?E-Mot!l 3ct'tar07 7031738 SM73.073.073.073.073.073.0730730

n o

886

8€6

8!{J

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E86

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z9Mar{7 03A!r-07 7031774 M.8

Thit lahonlo.! rcporl it ,rol vqlu x,fuhoul on atrtofized signaar/re on the col'er page.

* Repo.lrble Det€ction Limit BRL = Below Repodng Limil Page 45 of 154

Page 312: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samolc [dentificationM8F-37 2.-4'sAs980349

Clieot Prciect #301{8

Mat ixSoil

Received27 -M^t-07

Collection Dal€/Tim€26-Mar-07 00:00

C,4S No. At nlrt k) Resuh Fl4s U,,i,l *ftDL Dilutiorr Method Retr PEFored Analtzed Batch AnalBt

Semivoletilc Org.nic Compounds by GCMS

Semivolatle Olanic Compourds bv SW846 8270C

Prepar€d by method SW846 35508

5G32€ Bsnzo (a) pyrere20t9e.2 Bsuo (b) fluotanfiefle19124.2 8€nft (g,h,i) peryj€ne207{ss B€flo(k)fluo|ant|ei€ffi{ g€nntc ecidl@51{ g€nzyl ahohol11141r Bls(zdorostloxy)nE$an€i11-4,!-,1 tlis(zdrtoro€ftt)dher@Q{ etsedrbftisopqy0etEr117{1.7 Bis{2+f1},{he4r)dfl!atare10r.s:|3 +Somoph€nyl phfiyt eher856&7 Butyj bat4l pnhahb

88.74-8 CodazDlos-5G7 44hlo|'olmettry[figrd10647+ 4.Chloodlitine91-547 2{hloronaphdEhn€96.57-8 24Hofophenol7oo+72,3 +CHoroph€nyt ph€nyl ehei219{1.9 Chry!€ne5970.1 Db€atzo {a,h) anthracene132{,1-9 oibslzofuran!F5Fl 1,2-Dd1otob€nzsn6trr.7$1 l,+Dcliorobenzens1064S7 l,4-oictiombenzffe914,q 3,3--Echloroben2dn€12o€'2 l,&Dicloophenola1t&2 DidnylphfEtate131-11n oimery phhatate1ffi/€ 2,4€imoth!4phdtd*7+2 oi{+dylptrttaht€sl+52-r 4,S0inilo-Z-fi|ethyFtt€nd5r .2es 2,4$nitofi€rd121-1+2 a+Dinitrobl6ed)620.2 2,&Dnihotofu€neri7.E4{ O{1{dylphhahb?18.444 Fl]otarrlisn€8S797 Ffuo€ne11&741 H€xd omberEe{Esft&3 Hsxdlloobotadsn€n{.74 Hexactorocydopontadi€n€6'l'7*1 ftexe*boetfEne1e3.395 lndeno (11,3{dl pyreies12{ 1 -ridvnaphhal€no

78.59t lsopfiordlee.t7.6 2{rsbytmdtst€{,€6Fl&7 z{i.telhyphstol

1(r&3s-.1, 3,+Metjybh€nol106.4t59I.203 thphfdene8&7rr4 z-NitoinilnoS.(+2 $Nltgefine

21ffi

aolo8FL

2170BRL8Rt-BRTBRL8Ri-SFTBflLBRLBRLBflLBfrLBFL8FLBFL3,370BRL8R.8R-BR.BRLBRL8RL8RLBNLBRLBNLBFLBFLBFLBFLBFI

3,940BRT

8RLBRI-BRLBRLgf,L

BHLgRL

BFLB8L

BFL

8RLBRI.

NU ty 886

t.db dy 886

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lglqdy 886

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pgk0d, 885

t,g/rS d] €86

|,Ets fl 886

|jg}S try 686

tiglo 4y 886

l'ClS fy 886

uglq dy 886

E/rg fiy 886

rlgh dY 8€6

rdb dv 8E6

|'|g/b dy 866

|db dy 886

pSlqdy 885

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ldh dry 8€6

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udbdy 886

/$qA 886

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lYlqdy 886

r{tbd} 886

rurtq dry E65

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tJg](s d)' 88€

tiS,?€ 4y E86

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psftedy 8s

t{/rq dy 866

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$nqdy 886

ug,|qdv €86

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SI,Y816 8270C 2S-lr€r{7 o3.Ap.{7 m6174 M.B

Thb laho@lory rcpwl is,.ot vdd x,l toat a!, aa{toriud tigaataw ott thc coter page-

. R€portable Dete.tion Limit ERL = Below Reponing Limit Page 46 of 154

Page 313: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SampLe IdentiftcationMEF-37 2'4'sAs9803-09

Client Proiect #301 -88

MatrixSoil

Received

2'l-Mar-07Collectioo Datf/Time

2GMar-07 00:00

CAS No. Analrte(s) Resutt FloC Uni.s *nDL Dilution Me,hod Rel. Prcpand Analyed Bctch Anabtst

Semivolatile Orgrric Compounds by CCMS

Semivolatilo oroanic Compo{nds bv SW846 8270CPrepared by method SW846 3O5OB

1m{1i 4-Nitman ine9€{t3 Nifobenzene08-75 s 2-Nitrophenol100-02-7 z$tilophenol

6e-75-e N-lfirosodimehytamin€@1441 N+lilrosodi-ntropytamine86-30-6 N{,lhmsodiphenytamine37-96.5 penhdlotophenol

9t018 Phenanf[ene10s 95-2 Phenol

110-0d1 Pyddne120-02-1 1:,4-Tricr oroben2ene95.9n 2,4,5-Trichtoropienol8!-0€.2 2,4,6-Tri{*toroph€nol

a1&4 2+l@r@,ent4

36tJ24 z-Flwry,tend,(r6s-60-0 l'lilrobalzaE4s

110562 2 PlEnol4S

171&51-0 ledpnyl4l4

tt&N4 2,4,6-Trkrcnophend

29-l,lar.07 0}Ag'A1 7fA1774 M.BBRLBRLBRLBRLBRL

BRL8RL8RLBFL8RL4,260ERLBRLBRLBFT

6154n

7051

3540836886

3540886

886

8€6

886

886

686

666

686

886

886

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pyrsdvpslq dry!S4q diypdks d'v

l]s4(s dv

lglq dry

tllliA dt l

|ls^s dry

|a4(S dry

Nkq vugfrs dry

vSllS*ylsas dy

ldkg dry

rcAS dry

30130 %15-fi0%iEli0%t5-110%30-130 %15110%

sw816 8270Cl

I

1

l

l

l

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Totd M€tab by f,PA 6000/7000 Series Methods

Total Metds by EPA 200 S€ri8 M€lhods

14t+221 Sitver

714139.3 Baiurn

744e39 C3dnium

7n{H7-3 qlunjum

743$91-1 lead

nn249-2 s€l$ium 2.S0

SPLP Mctde by f,PA l3l? & 60001000 Series Mrrhods

SP|P Extiadion Compt€led

741$224 Stver 8RL

74!eM-2 A|s€flic BRL

74.{e3$3 Eadum 0.0126

74{0-43-9 Cadnium BRI

Ta447.3 Chrcmtum BRL

743e,976 l,terc1]ry BRL

zl3$92-1 Lead 0.0542

n821e.2 Sdfiium BRL

G€trerrl Chemistry Prrrmel€rs

% So$ds 82.8

1.m mSAS dry 0.0356

r'S*S dry r.16

rrE/rg dry 1.75

riS/}€ dry 0.582

m{rg dry 0.291

mdlCdry 0.582

mdlqdry 0 871

mSftS dr] 175

mgl 0.0100

mq,l 0.0lel

mq 0.0050

mgl 0.0@5

rill 0.0125

mgl 0.0{X}10

mga 0.0075

mgrl 0.0150

slrt46 7471A

EPA2W7

sw8461312

swE16I312/60108

sw8461312?470A

sw8461312/S108

SM25,l0 G Mod

1

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02-Apr0/ 09Apr{7 7031810 YP

BRL

28.8

64.5

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02'&r07

28 Lrar{7 2€- ar{7 7031753 8D

3GMar47 02-Apr07 7031805 LR

' 02-AF{7 /031€06 YP' 02.AF{7 7031805 Lq

30{lar-07 30-lrrl{7 7031879 YM

Thb labotdory rcpod k ntt talid without aa autiorizel sigwtare on ,he cover page_

'Reportable D€t€Etiofl Limir BRL = Below Repodng Limit Page 47 of 154

Page 314: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ ldentificationM8F-381'-4,sA59803-10

Cli€nt Proiect #301-88

Collectio! Date/rime26-Mar-07 00:00

MahixSoil

Received27 -Mat47

CAS No. Analra(s) R.s|,/lt Flag Uni,$ *RDL Dihttiorl Itahod R?tr. Prcpaled Aulyzed Batch Aaabst

Fdd e{rad6d

Volafle Oqanic ComoounG

Prepared by method SWE46 5O3O Soil (high l€vel)

7$13.1 l,l2.Trichtorclifluo(EtEne(Freon 88167.€+1 Acetone BRL10'-rlt Adylonitrito BILtt.tLt2 Bs|zene BFL10g-061 grofllobenzene BfiL11.911 Bomcitoromethans 8Rl-Enl BDnodchloronefiano BRL1r&2 Brornolorm 8ru-748i19 &undn€thane 8Rl-7843.3 2-Butanmo (MEK) BRL104s1{ G8utytbenzene BnL1l+98€ s€r,Blqdbenzene BnL€0s-6 lsd-hlytbenzene BRL?F15{ cedon dsutfide BRLse23.s caftonleirad{ori& BRL1(6.{l{17 Crhlorcb€nzene 8RL

28{rar-{7 2&Uar{7 1ts1757 BO

t2-1lot47 02-Apr{7 nxlol7 fiar

Volrtile Orgar|ic Compound!

!r'oc Effaclion

lSrq dry n.1

l{lqdy um

|.grq dy 73 4

lglq dy n.4

Ud{q dy n!

|clq dy 73A

ldkS try n.4ydhs dy r31

ldlq dy r47

|jg/h dy 734

l.dlS dry 73 4

Blqdry n.4

Ig/lqd} 73.4ydhtry 367

!g/]q try 73a

E qdy 7i{

B4€dy 147

IErqdI 734

ldlq dy 141

!g/kg dy nA

mlq dv n.1

Ug/rq ry u7

lglq dy n4

t'dkS dy I}4

l4h d'y n.4

|]grS dy ?3.4

|4/lS dy 73.4

Igl{ dy 73.4

|dlq dV 147

|JdkS try 73.4

|j049 dr n4

lgls dy 73.4

r{rq dy f3_4ygrqdl t3.4

|,g4q dry 73.4

lglq dy n.4

|EIq dy 7X.4

Udr0 dy lXA

H/rq dr 73.4

udt{ dy 73a

!9,rS dry ?83

ldre &y n.4

ldbd'y 7u

udr€dy 73.4

Ug,lqdy 73.4

lghdy 7x.4

lStS try 734

ldhdy ru

lClqdy 73A

505l)505050505050505{)5{t5i)50

5050

fl)

50505050505050

5050505050

50

5{)505050505050505050

50

505050

voc

s1,li 846 82608

75{l!3 Cl oroshaneeI{63 Chlorolofln11413 qtbrooellan€

51S3 20rlorotoluene106.13-4 4{l orohluae9e12€ j2-ttibromo3d oropopane124-1&1 Dbrfi|odo.ornethane1qf0}a l2-DbromoedEne(E0B)744F3 DbromomBthene95.5c1 1,2-Ddltoob€nzenes417}l l,&oidlhrob€nu€ne106-a+7 t,4oCldolobenzen€75_71-s Didiloodffrol('ndhanelFreoni2)75.34-3 1,l-Dicito|DeflanelO{Gz 1,2-Did do€thaners"3fi l,l-DicttorodhsrErs6-5$z cisl,2ok*o€ehene156-6Os lrEns-12-oldoro€ft€ne78{7.5 l,2-DdoroFopane14p.44 t,&DicHofopropane*r-tu1 2,2.DcHoropmpanes4950-€ l,toido|DproPene1@61{r5 cb-1+Di,hblop{tp€r1elm61{26 telg-1,3-0id{o.opropen€'q)-41-4 Ehy'b€nz€n€fl.593 H€rd orobutad€ne591.785 z+iexanono(tl8qs.82-8 lsoPropylbenz€i€9+e7€ +lsoproprthbd|€fiar44-4 lr€hyl tediuM €fier10&1r!1 4-tiretfiy1-2{€nhnon€(Mt8K)7S9-2 Meftylene dbdre9r-a!3 Nepnfd€n€

BRL

8FL

BNL

BAL

BFI.

BNL

BRL

BFL

BFL

BFL

BRL

B8L

SFL

BFL

BBL

BRL

BRI.

BRL

BRL

BNL

BRL

BFL

8FL

BRL

8RL

8RI

BRI

8eLBALBFLBFIBRtBRL

Tkb htofllory repott b not vatjy' Nirtoat al du&otlzd lignafitn oE thE cover prg.

. Rcptrtrbl€ Detectioo Limir BRL = Bdow ReForting Limir Page 48 of 154

Page 315: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationMEF-3E 2'-4'sA59803-10

Cliflt Proiect #30 t -88

Collection Date/Time26-Mar47 00:00

MatrixSoil

Received27-Ma(07

CAS No- Anattte(s) Resull FlzC Ani6 *RDL Dil,ltiorl Mahod Rel. PMpared Anallzed Botch Anat$t

VolNtile Organic Coft pornd!

Volalilo orqanic ComooundsPrepa.6d by method SW846 5030 Soit (high tevet)10'6+1 n-Pmpylb€nzene10042.5 Styren€64020.6 1,1,1,2-Tetradlooelhane7s3,lt 1,1,2,2-Tettachloroelhane121-tA4 TetreiloDelhene10S-Sg 3 Toluene

87.61.6 1,2,3-Tdchtorob€n?ene120121 1,2d-Tichlorobenzene7r-55.6 1,11-Triciloroehane79{0.t l,12-Trichloroehane79{16 Trdtloroelhene7*9-4 Tri*torottuoromethane (Fleon I i )96'101 1,2,+Tridto.opopanes5-53-5 12,4_Trimethytbenzen€10€{7+ l,3,5,Trimethytbenzene75{1.4 Virryldtorids133G2G7 m,Pxytene95-47-6 oxyl€rp109-999 lelrahydm{oran&29.7 Etvleher

94{Ef Ten{mylmehyleher87923 Etryt tert-bulyt etter1m-m3 Djsopop/ elher75 65.0 Tert-Eutanot / buty4 atcoholr239r r 1,4-Dioxane

#4404 4-Ercnonwrobenzarc

tu3t'26i Toluen*dB

tiM474 1,2-Dichlotoethane.A

1868-53-7 Dlbroraquorofiekane

Ertrrctrble PEtroleum Hydrocarbons

Exlnc{able Tolal Pelrcleum Mroaafton6

Prepared by method SW846 35508

80661.9 Gaso[ne

60476.3G2 Fud oil {26347F3f3 FUelOil d463s53 00-4 Fuei Oil ,6M093000fi iiolor oilJolm)oo Avjalion Flel

Unidenlified

Ot€r Oil

Total Petroloum Hydrm€rbons

C9{36 Aliphalic Mocarbons

s$3yz l{tlorccrjadecarc

Semivolatil€ Orgrnlc Compou!& by cC

organod orift". Pestidd€s SWM6 8081 A

Prepared by method SW846 3S15A

8RL8RL8RL

BNLBFL106BFLSRLBRTBRL8RL8RL8RLBRL8RrBFL

8HL8RL8RLBHLBRL8RLBRL8RLBFL

1(Ata

s?113

50

50

50

il

50

50

50

50

50

50

50

50

50

50

50

50

5{l

fll

511

50

50

pg4S dy 134

lSeS dry 734

rcfrS dry 734

pSftSdry 73.4

lSftgd] 73.4

UdiS *y 73.4

pg/lg fy 73.4

pg/\s,rv 73.4

pSIq dry 73.4

|lgn(S dry 13-4

lCftS dry 73-4

lgtS dry 734

!9,,rg fy 734

lgrS dry 734

rceS ey n.1ldks dy 73-4

lStS dry 147

lSrlq dry 13.4

pglq dry 734

pS&S fy 73.4

Wtg dy 73.4

Fs4q dy 13.4

pS4qdy 73.4

ldrS d] 7U

ldlq dy 1170

n1&%

?v1& %

70-1U %

7F1U %

dkS d,y

mdrg dy

mgtg dry

mgtS di)

motS dry

mS/xq dl

mSf.g dy

mS/rg d)

mgtq d]

mdlS diy

44.140 %

SW 846 82mB 02-Apd7

+CT ETPH

02-Apr-07 7040017

2g-Marq 3UMaJ{7 7031772 DS69.8 1

69.6 1

63.8 1

69.8 1

69.8 1

69.8 I

6T.8 1

69.8 1

69.8 1

69.8 I

sf,LBFLBRLBFLBFLsffLBFLB8LB8LBRL

8€L VgrStt 37.9 swt46 @Era a-Mu47 l}2-Apr{7 7031739 TG

Thh laborutory nFod is not valiil x,Aou an authorhed signaraE on the cover pqEe-

* Reportable Detection Limit BRL = Below Reporting Limit Page 49 of 154

Page 316: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samol€ IdetrtificationM8F-38 2'-4,

sA59803-10

Clie Proiect #301-88

MatrixSoil

Received21-Mar47

Collection Date/Time26-Mar-07 00:00

CAS No- Analrlc(s) Resdt AnibFbg aRDL Dildion t{ahod Retr. Prcpared Artalyed Bdlch An4lfs!

Semivohrile Organic Compoun& by CC

Orqanocibine Poslicides SW846 eO81 APrepared by method SW8,f6 3545A

319{,r-6 rg{C319.657 b&{CJ1$0&8 dBHC58-8e.e 0-BHC (Undane)5r.7+9 oibrdan€z.s,l-o 4,4.DDO{p,p)z ste 4,4.DDE (p,p')5lt2+3 a,1.D0T (p,p')6115|-l Di€l&in95940-€ Edoculhn I3321$6ts Endos0llan tlr03l{7€ Endosxltansulhten-244 Endnn1Qt.tt34 ErnriiAldehydetua Heptad orn115 lrefioryd or1rl24t{ HeptEd of Egotdedloli$2 ToradHe5jG71.g a-Cl{otdane

566&3+7 g4ltodane

5349+7Gs Endin KetJ|€

,Gn042 1,{DE&a0uot&dEtV(Sr)

ffir2+3 o€caE,lonbilld/rl MPotudlloiEted BioherMs bv SW846 8062

Pr€pared by nethod SW846 3545A

1267+11-2 PC81016trr0+2s2 rcB 1221t1r41n6-5 rcg l23Z

53469.21-n PC81242

B6n-?94 rc8124811ll€7€.r PCB 1254

1l0*€e.s rcB 1260

tp,+23.5 Pc81262111001+4 PCB 1m8

@8.a+2 1,+08-Uan@tdids1yl(g)

,f61"r3 l]€fEdltorcdipttr.tryl (*)

Ssthivolraile Otg.nlc Compornds by crCMS

S€r!'vdane OEanic Co.noolmds S'/YM 8270C

Prepared by method SW846 355088+32.9 Aenagh$e.r6

200-s64 AcdEphthylon€@-53€ AllilE

1&12'1 AnhacBnstg12'2,H, Alrazin€

10+3+3 AzobgnzeneDiphenyldazine

Q{7.s Benzidn€

56-5S3 8€azo (a) anhrEce|]e

8RL

8RL

BFL

8RL

BRL

BNL

BNL

BRL

BFL

BRL

8RL

8RL

88r

8Rr-

BRL

BFL

BFL

BRL

8RL

8RL

SRL

107

BFL

BFL

BRL

8RL

BRL

BRL

BRI.

BRL

8AL

m95

37.9

3 7 9

37.9

Tf.9

189

37.S

n.937J

379

37.9

379

17.9

37.9

37.9

37.9

37_g

n3l8

37.9

320

3 7 9

rdb dvpdlq dv|jgrs d'v$g/rg dVlsrq dvlgrs cy!s/}'s AlS,trS fiy

R01 |lg/tq dy

Ah dv

|ldks drypgkg dv

$rq dv

|,o/l(s dv

ldks try

ldkS dry

lglq eY

l8fr9 frv

l4balslq dly

r9tq dy

&lf l%3+1fl %

t4rs dy

|dh dy

N$eY|ryb dtypg/lq dry

Ug/lq dy

IdrS ol]s/}{ 4y

!s4q dY

30tg%#1&%

r91s dygdro dv

ldlq trv

lgls dv

I4r4 6t

!4ls dv

ah dv

t'gb dv

sw846 80814

sa{a$E@

$rY8fi A27C

75-7

75.7

75.7

757

75,7

75.7

75.7

a.|.lai.07 30r1tr{7 lfi}1738 SM

294ai-07 6t l0rl7 VBlnl M.B8RL

8RL

8RL

BNL

SFL

BRL

BFL

BHI.

845

8&5

E65

865

865

Thb lobo.aloq repod is Aot voIU vilhou aD attthorirpd sigrraure oE tLe cov, p98e.

' R@rtable Der€dion Limit BRL = Below Reptrrirg Limit Ptge 50 of 154

Page 317: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-38 2'-4'sA5980l- l0

Client Proiect #30 t - 88

Collection Date/Time26-Mar-07 00:00

MatrixSoil

Received27 -Mar-07

CAS No. ALaltte(s) Re$ah Flog Anib +RDL Dilutinn Mehod Rel. FnpaEd Analrzed Ratch Anallst

Semleolelile Orgaoic ( ompounds by cCMS

Senivdafle ofoanic Comoounds bv SW846 8270C

Prepared by method SW846 35508

so32-8 8en2o {a)pyrer€415-9$2 Ben:o(b)ltuoranlhene1s1-212 Ben:o (9 h,i) p€rytene

m7-08 e Benzo (k) fluo.anhene66-89) Benrcic acjd100-sr.6 Benzyi akohol111-9lr Bs(2rnbroehory)melhaner1r-44-4 Bs(2{hloo€lh}4)elher38638.32-9 Bis(2{htooisopropyl)efier117.81.7 Bis(zahyth€Iyt)phihataler0r.s53 4-Bromoph€nyl phenyl efEr115.60-7 Eutytbenzylphlhatale36 74-8 Caba2ole59.s0.7 4,Chtoro-&mettrytphefld10S47.8 4,Chlotoanilines1s&7 24htoronaphlhal€ne96 57{ 2-Chlorophenol700s,72-3 4_CHorophenylphenyleth6r213{r S Chrys€ne5$70-3 Dibsruo {a,h) anlhracene132t4-9 Ditrenzofuran9+50r j,2-Dchlo{ob€nzene

s4l.73r ],3-oiohlorobenzsne16467 ],4-DDhloiobenzen€sr941 3,3'-0ichlorobenzidine12aa!2 2,4-Dichtoophenol0,146 2 Dielhy,i phhatale

r3rrr3 Dim€fiylphlhataler0567e 2,4-DirEltrylphenola4 74 2 Di-n-bulyt ph$atate

53!-52r 4.&Dnilro-2-mettryloendsr.28-5 2,4-oinihoph€fld121.1+2 2,+Dnikobtuefleme20-2 2,6.Dinilrcbtuene117.8.1{ oi{{dylphtfElate4k444 Fluo€nth€ne

8St97 Fluolenell$74.1 HexaChloDb€izen€

r7{&3 Hexachlorcbtiadenen474 Hexedllorb,.yclopenladiene67 72-1 HexachloD€tErE19339s hdeno (1,2,3{d) pyrefle

9G12{ t-llelhylnaphthat€n€7!-59-1 lsophotone

91.5r-6 2-Methlnaphhatenees-44'7 2-Methyiphenol

10&39-4, 3,4-Melhylphenol

s1r0'3 l\hphhatg'le*:r+4 2-Nitfoanilnee9-09.2 }Nitroani{ne

BFL

BFL

8RL

8RL

BRL

BRT

BRL

BRL

BRL

BFL

BFL

BFL

BRL

8FL

BRL

BRL

BRL

BRL

8RL

BRL

8RL

snLBFL

BFL

BFL

BFL

BFL

BBL

BFL

BRL

8RL

8RL

sRtBRLSRLBRtBRL8RL8RtBRLBRLBRtBRIBHI.BFI.BHL

BRL8nL8nL

ldks dv

!S/iS d.ypgts dv

|lgas dry

lglq dry

lglg dry

ru4q dry

|lg}sd.vlatsdrvydks d'y

tlgft! dYpgks d]pg/rt0 dyps/]{s dv

!S4q dry

!94{ dry

!S,4(S dypdls d}pg/tg dv

|lgilq d,y

|lslrs dry

ta4€ dry

|4r'lq dry

!04q dly

lqE dv

ldlq dvpdks drypsiq dypgls drypYks trv

ugl(gdvu04q dty

|44(s dy

!g/ks dry

|Jdkg dY

!s*s dry

|]!iks dv

ldrs dty

!c4q dy

!s4q dry

lgxs sy

ryrc dvlslq dv

!S/tS dry

lsas A

lgAg dry

Ugtg dry

l4r'IS dry

wts *v|a4q dry

865

E65

665

E65

865

865

865

665

865

865

865

865

865

865

865

865

865

865

865

865

E65

865

865

865

665

865

E65

E65

865

865

865

865

865

845

865

865

865

€€6

855

8{t5

865

865

865

€65

s' €46 {270C zgllad7 03Apr-07 703174 M.8

865

855

855

Thit lalorotorx rcpon k not BIid w hoar aa authodzrit signolure on ahe cowr page.

* Reportable Deiection Limii BRL = Below R€porting Limir Page 51 af 154

Page 318: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-38 2'-4'sA59803-10

Client Proi€ct #301-88

MatrixSoil

Collectiod Date/Time2GMar{7 00:00

Receive-d27-Mat0'l

CAS No. Adalyak) Result Flas Unix 'RDL Diletion Method netr Prcpted AnrIWd Balh tusrfsl

Semlvolrlile Orgsnic Compounds by GCMS

Semivolads Orcanic ComoounG bv SWgd6 8270C

P.epared by melhod sw846 35508

10(H116 +Nitoe lne

98{,53 llilrcD€n2g|le8&7+s 2-Nitophsnotlllo-Cp-7 +Mfrophenol

6e-754 ifltt€sodimetrylamine

6er5+7 $lfrttosodi-ntropyldnine36306 tlt{tosodipn€nylarnin€

07-8s5 P$lacttloftAhenol35{1-! Ph€nanlhr*D10Fst2 Phenol129S{ Pyleno110-€d1 PyidrF!m{2.r 1,2,+Tndbrcb€{E€ne95s 2,4,tTdJ ooph€nol8ss-2 2,4.6-Tddtorophenol

eft44 2+hefuiphstyl

#f-121 2+lwtgpl'€nd

1165j04 N|@12ale6

41fia2 PW45

17tsst4 fe(M4a

1t4/96 2,4,6-frtbtunophdtd

2S sri7 0+Alr.O7 7031n4 M-BBBt

BRL

BHT

BHL

BFL

BFL

8RL

BRL

8RL

BHL

BFL

BflL

BFL

BBL

8RL

57

59

60

n75

15

pg*S *y 3460

t'gt! dy 865

a& dv 865

Udlqdy 34€o

l9,lqdy 865

lErS dy 86s

|Jgls fy 865

tdr{ dy 865

pgrS dry 865

tdh dry 865

ldlqdry 865

llgftS dy 866

tghdy 865

!g[q fy 86s

|4/k0 ry 865

30tf l%

tr t l0%

3Etg%

tt l l0%

30F130

1r110'a

mdlqdry 0!B63

rnsilqdry 121

n'gks dl 1.82

mglgdry 0m7

n'g*g dry 0.3{X

nqlqdry 0607

mghdry 0 911

mdrgdry t&

mgl 001m

n$l 0.0150

mg4 0-m50

ngr'l 0.005

ms,,l 0.0125

mg,l 0.{m40

m! 0.0075

mgf 0.0150

sirY8{6 82mC

5!118,16 74714

EPAa]f:I

Tot.l Mctrls by EPA 6001y110{ Seria Merhods

7(l$gr{ lrgdtry

Total Merrl! by EPA 200 Series Method!

7@41 Sjlv€r

7443X.2 AJsenc

?{4SS.l Baium

?44449r Cednium

71!G11-3 Chrdniun

7'B9. t t ad

r|82{!,4 Seleniurn tB

SPLP Mereb by EPA t3l2 & 6000/7000 Sed6 Methods

SPtP8hadion Cornd€r4d7@21 Situ€. 8Rt-74+&z Arsenlc SBL

71,10.3+3 B€rium 0.O1n

7'1441-s Cadniun 8AL74aO-47.3 Olodilm 8AL

713+97-6 M€rqlry mL743892r L4ed OUgzrn24.2 Sder um BRL

G€nerrl Chemi6lry Prrlmetens

% Solids 81.2

0.972 1

I

1

1

1

I

I

l

t

I

I

1

1

1

I

m-fur-o7 t)& c{7 7ts18t0 YP

BffL

m.5

0.795

299

siw8{ti13l2 2l.ll,ai{7 A.iCr{7 7qt17€0 90

SW846 i31460108 fl)ilaroT m-Apr{7 7031806 tB

sw846 131274704

s"1€46 13t2l60108

02-4pr.07 70318fi YP

(p.AF{7 ru1805 tR

Slt23l0 G Mod sGlUtr{7 g}i&r-07 7031E79 Ytl

This lanorutury rcporr is not did whhod an atlhodzd signetare oz thz coter Fage .

+ Rcportable D€lection Limit BRL = B€tow RQortidg Limir Page 52 of | 54

Page 319: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdertificationrrtSF-39 2'-4'sA5980 l - l l

Client Proiect #30 l -88

Mat xSoil

Receiv€d

27-MaFOl

Collection Date/Time26-Mar-07 00:00

CAS No. Anolrte(s) ResuA Floc Uni6 *RDL Dil'/non Method ReJ. Peparcd Arnbtzed Barch Anallst

Propared by method SW846 5O3O Soit (high tevet)

76-1x1 1 1,2 Indk rotnltuoro€$ane (Freon BRL67€,11 Acetone eRL10713 1 Acry4onitrite 8RL71.tx2 B€nzene BRLr03 35 1 BEmobenzeoe 8RL74s15 Bmmochlommelhane 8RLtt27-t BmfiEdidlordrehane 8RL75212 Bonotom 8RL7,1'019 Bromomelhane 8RL7!-e13 2-Eutanone (MEK) 8RL104511 n-Butylbeuene 8RLrx5.ss4 !€c,B{n/benzene BRLeds Gn'suvl6€nzene 8817515{ Ca6on disotfid€ BFL56 23 5 Grbon tetrachtoride BFL10&90 7 Chlorob€nzBle BFL75.00-3 chtorcethane BRL67-66-3 Chlorolom 8HL7+87.3 C,hloror€thane 8RL9549-8 24htorotoluene BRL106-43-4 44htorotoluene BFLs612r l,2-Dibronlo-3rhtompropane BFLl2lr-$ I Dibroflpchloomethane BRL106e3-4 j,2,Dibromoeihane (EoBi BFL71-e5'3 Dibroflomeihane 8ff195-m-1 j,2-Dichtorcbenzene BFL5417:1 1 l,$Dichlorobenzene BHL10&,1$7 l,+Dcntorobenzen€ BRL7171-8 Dichloodifluoromsthane (Fleofl12) BnL75-3+3 l,l.Dchtoroelhane 8RL107-{F.2 1,2-Gchtor4thane 8RL7t3t4 l,1-oichloroelhene BFL1scs9.2 cis-l,2.0ichloroethene 8RLrsml's lrans-1,2-Dichtoroelhene BRL7!-07-5 l,2-oidtoropropane BFL14c.284 l,$DichtooproparE 8RL

s4&-t 2,2-0i*,la!aprcpare 8RL

s6$s35 1,l-Dichloopropene BRL1006141-5 cis-1,3Di$hrcpopene BRL

111061{24 trars'l,O-Did{oropopene 8Rt

Volalile Orgsnic Compounds

VoC &lracliodVolalile oroanic Comoofi ds

1@414 Efrylb€nzenegl.6€3 lhxadkJobuladiene591.7&3 z_Heraflone(MBKi98.828 lsopropylbenzenet937-6 +lsoprop!4ioluene16ir4 {r44 l,t€thyl ted-butyl etherr0€.r0.r 4.Metryf2-penianom(M|BK)7s$2 t €lhyt€ne cnlodde9fal3 Naptlhal€ie

lJg4! d'y 98 z

lEfiq dry 1960

lqrS dry 1t8.2

tS4(S dry 118.2

lgrqdry s82

lg,kS dry 98.2

tltJr(! dry 9.2

rye dry 98.2pgegdry 196

yCq dry 982yvk! dry 982

IrS/kg dy 9E.2

pgtg dy g2

pS4$ dy 491

pqkS dy 982

psft! dry s82

!dk0 dy 1SG

|lg/k! dy 982

'lg,ks dy 196yg/l(o dy s2

ps/l(o dy s2

|]gn(! dy 196

pS,lq dry 9E2

Krtq dy 982

pgACdy *2

pgn(0 dv s2

pSI$ dy 98.2

ptk! dy 2ys/r! dy 196

Ps&t dy 9€.2

MS*y 9d.2

!s4(! dy 9€2

!S4q dy 9E.2

ldr! dry 98.2

!S4q &y 9E2

tlglq dry {t€2

W+get 98.2

!g,lq dry s8.2

|€/kS dry tB.2

rcnq dry S82

lgts dry 981

tlg/lq d'y 982

tt9'l,Set 082

psnq fy 082

rS*S fiy 08.2

|lg^S dry 98.2

pS/kg dry 982

liS*! dry 982

MkS dt 982

28-MN47 28-Mat41 7031161vclc

sw 846 6?608 294arc7 3GMar47 703lEN

8RI

BRT

8RL

BRL

BRL

8RL

8RL

BRL

170

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

5|)

50

50

50

50

50

50

50

to

9l

50

50

50

50

50

50

50

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5)

50

This labontory Hport k nat ,alid *ithout an authorized signatyrc o^ the cover page

a Repoftable Det€ction Limit BRr = Below RQorting LirEir Pag€ 53 of 154

Page 320: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SampLe ldentificationMSF-39 2'-f'sA5980l-11

Client Proi€pt #30 t -88

MatrixSoil

Collection Date/Time26-Mar47 00:00

Received27 -Mat47

CAS No. Andlfu(s) Resan Flds Ul',iat "RDL Ditution tc nd ReI- Pnryed Aruryzei Bdkh An4lrst

Vohltle Orgadic Compounds

Vohde Orqarfc CunmrnGPrepared by nehod SW846 5030 Soil (high l6vel)100{51 ftPopyb€nzene10G.12-5 Sty€n66x!204 1,1,1,2-TetEdoroeltEnels3r5 1,1,22,T*Edorcelf€no1n-144 T€llachbro€t|ane108{93 Toluene0761{ 12,3-Triddord€n@neu!62r 12,4.1fi$brob€nzffe71'5!r{ t,j,j.Trichloroehanet9{,G5 1,1i.Tricloo€t€ne7!.015 lddJotlc€hdE7s-694 Tdd{oronuorornetEn€ (Freon I 1)$.1E-4 1,2.+fftfibrcpopane9ffi4 1,2,4Ttimeffylb€nzfll€10s.67{ 1,3,glnne6}ib€n2€n€75{1.r vinyt d orir€133G207 r4FXy1€00!6{7-6 o|Xyi€n€r0ss4 TelEhydrotunn@?*? Ehy eher

sg$s€ Teninylmsfiy'elhe.63? 94'3 Ehryl hrt hilyl etler10&20.3 oHsapogy' €h€r756fi fed.Eulanot / h4,tatc€hol12+El-l l,{{ioxane

41ilJ,4 +gnnoflwnb$Ene

&7-&5 Tduerle{fr

11!60474 1,2-DiC q1ethane44

164-Elt DifuoflpfrJorfilelhane

f, ttrcctrble Petoleum Hydro{r.bont

Enractabl€ Total Petdeum tMroaatods

Prepar€d by method SW846 35508

{Oe61'g Ga$ohe6A|76-3C2 Fu€lc{l#26817F31-3 FUel O1#{68s53-004 Fuet0lt6MF€O0&0 Mobloil.s010o00 Aviation Fuot

t lr*rentified

ohqoil

Tdd Pdrolsim }|),droc&tons

CSC36 AlFhalic BydrGrtons

338F3+2 l4hwoMcaB

Semlvolaaile Orgr r Compounds by @

oroapd odne Peslicil€s SWE 16 8$l A

Prepared by method SW846 3545A

s{Gz Atdin

2Sl aF07 gl sr{7 761830 matBRL

BflI.

BflL

EffL

B8L

BFL

BRI.

BRt

BHL

BHI-

BFL

BFL

8RrBRLBRT8R-8RLBNLMLSBLBRL8At88LBRI.SRL

1001&)g

95

BFL

BFLBRLBRL8RL8fi1BfiLBFLBBLBRI.

90

50

50

50

50

50

50

50

50

{1

50

50

50

50

50

50

50

50

50

s05050al5050

Bfgdry g2

uykg dry 2

lgto dy 982

!$S eV 962

ldlS dry (182

pg,l€ dry 9a2

UdlSdy 982

llg,lq dry lxl,

$/rS ey 982

l4A0 dy 982

udl€&V 982

!d*S dty {lE2

l{/lt dY 982

lgr€d.y 982

lg,lqdry 982

tg/tq dy 962

t4l4ty 196

!s,to trl s82

rcnqdlY 982

|db rv 982

lSlqdy 98?

@fqdy q2

tgkg dY 982

ldkS ty W

!dk{ drY llm

7vtfr %76130 %7G130%70-td%

'!€/Iq diy ?82

mdlqdry 332

mglq dry A2

mgtgdry 332

mglSd] 332

n'Snqf} 332

nEl€ dry 3:i2

rEIq dry 3i12

rBlqdry 3t!

mSlqdy 33.2

4+140

rulq dv

sw 846 82ffi

+CT ETPfII

I

' 1

1

I

I

I

I

1

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2$tvtar{7 30Mar-07 703173 DS

BNL sw8a€ 80814 ?a41?f47 @.AF{7 mlng IG

?hk laborubr? Epo.t is ,ut vdid *ithod an aslhoizd sigAdare on the catcr poge-

! Rcporbble Detecrion Limit BRL = Below Reptrting Limit Page 54 of | 54

Page 321: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ld€ntificationM8r'-39 2'-4'sAs9803-l t

Cliert Proiect #30 t -88

MatrixSoil

Received27 -Mar-07

Collection DatelTime26-Mar47 00:00

CAS No- Analrte(s) Res,tll Flag IJnits *RDL Dilutbn Method Ref. Prcpsrcd Anslyzed Batch AhalJst

Semivolalile Orgrnic Compounds by CC

Ooanochlorine Pesticides SW846 8081 A

Prepared by method SW846 3545A

319-€4 € a.8HC319-85,7 SBIrC

319-86.8 d 8rc5e8e4 g,8HC (Lndan6)

st-74.9 Chbdanens4.s 4,a{00 (p,p')

72-5s.e 4,4r00E (p,C)

sG2e.3 4,a',00T (p,p )6G57.1 DielMn

95$9&8 Edos/fan I3321$65.9 Endosullanll103147-8 EndosulfanS0llale|Z-ZA-8 Endnn7421-s-4 Endnn Aheiyde/64,1-3 l-leplaafilora-€ s Metroxyc$lorr021t 57 3 Hedac+llor Epoide&01-35-2 Toxaphene510371.9 a-Chlordane556e34 7 g4htodane

5n4947G5 Enddn Kslo{l€

tB86aa2 1,4-Dg-0dalwtobiptent4lsr)

N6t2+3 Decachloro ptenyl (3r)

Polvdrlorinated Biphen!,ls bv SW846 80P,2

Prepafed by meihod SW846 35454

12674r r.2 PCB 1016r104?&2 PcB 1221r1r41, !6.5 PCB 1232

5345e-?1 e PCB 12rt2!2672-29.6 PCB 1248r1m7{9.r PCB 1254110e 25 PCB 12603732423 5 PCB 12621110014-4 PCB 1268

1@86a+2 4,4'D8-thafl@tDbiphenyi (St)

2051-21.J Decacllotobphenyl(Sl

Semivohtile Orgaoic Compounds by CCMS

Semivdalih Orcanic Comoounds b{ SW846 8270C

Prepared by method SW846 35508

8su{ Acef€phh€nezu46.8 Ac€mtht'yhne6A-$-3 Anilins1&-12.7 Anh€cens1912.24.9 Altazinelmnsr fuob€nz€n€/Dipheny,ldiazine92-87-5 8€ruidln€5&553 Seozo(a)anhacsn€

28'Mar{7 3qMar{7 703173a SM

211-{l&r{7 Cl}Apr{7 7031774 M B

8RL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

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8RL

BRL

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BRL

BRL

119

91

8RL

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ERL

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ta0

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n9

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4 / 8

478

47€

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478

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47.E

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239

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47.8

47.8

pvlq *vldkS dry

lgrs dvlgtg dry

lgkS dry

lgrs dry

ISAS dry

lgftS dry

lsas dry

wKs ory

lgxs ory

ldrs dry

|ls^s dry

lJgr(s drv

ldkg dry

Nag dry

lykg drypgxs ory

lgks 6y

lgks dry

ug,lq dty

30t50%3+150%

lgrs dry

lgks drypyks dry

|Js/l(s dry

udrs drypdls dry

!s.49 dry

rc4(0 dry

tgt\s dry

*150 %gr1fl%

sw846 8081A

sw846 8082

sw846 627m

95.6 I

95€ 1

955 1

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95J 1

95t 1

956 1

956 1

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u4824

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824

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BRL

8RL

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BRL

BFL

BFL

BFL

pgts d|vpsAo drvps/kg dl'

K/r.g dypdks dv

!S/kS dy

ldq dv

|lgr'iq dry

This lzboratory rcpoa is nd wlid withoat aa o!rtoized sigMlurc on the coler ldge

* Reportable Detection Limit BRL = Below Reporting Limit Page 55 of 154

Page 322: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8F-19 2!-4'sA5980l-r t

Clieot Ploiect #30 t-E8

MatrixSoil

Rec€ived2'l-Mar-07

Collection Date/Time26-Mar{7 00:00

CAS No. Anzb@g) Rcsn/l FIAC Unia rRDL Dllaian Method ReL Prcpared Analy.ed ktch Aaatfst

Semivolatilc Organlc CorhlroIn& by CCMS

Semivdalf,e Orgonic C,srEounds by SW8,{5 827@Prepared by metllod SW846 35508so.e{ Benzo (alptEne205-992 Beflzo(blf@Entrene191-242 Benzo(g,tti)parylene?!7{&9 Bg]m (k) fluoranhene66'054 Bffzdc€ci,1oc5l.6 Befl4tatcdol11 1.s1 r Eb(2+loroehory)mefiane11l1rr{ Bd2doroetryj)efEr3trs@{ Bi{2dthdsopo9},1)edrer11741.1 es{2+tr'y'trexy0PhtDtate101.553 +BffinoCt€nyt ph€nyt etherss8.7 8tjtyl b€nzt ph$a,ate

&74€ Ca66!ole595r!7 44htdo-3-mqhytpltenol10F47{ rtclrloloanlin€

91.*7 2o{o'maphhal€nes5.57-8 2{|{orcF€ndTmtz'3 +Ctdorcphqylphonyt€her

218{1-9 onys€ne5+70.3 oabenzo(a,h)anhracsb1t2419 DbenzofuEn9S501 1,2-lld't|q'obenze0os11.791 1,3.tkfih.obenzene1116-'{&7 l,,t-Dtdiorobenzene

014+1 3,3',.Dnfibrobenzidiner2G8+2 2,4,0id{(.trphsnotu&2 oierhyl ptddate

13r-110 Dmehylp+ |atale1H74 2,+Dimeihtderd*7+2 On-butyl phhelate

s3+s?r 1,6.Dinitrc-2rndhy'phend5t'2+s a4.Dinihpn€nd'121.1t-2

aa-oinitdotsl€oG2O2 2,+Diritoduene1i7{'rc tt.n-od$ph[,able&444 Fuordittgn€&7I1 Fl O|EIet1&7't.1 Helad oDh€n:E|le6/48i1 tl€xdltorDhlsdenen474 Heradllooqcbp€ntadiene6r-121 lle)@d Oroetune1e+3e5 tndem(1,2,9cd)prBns!o12i l+JrymdhdEne7&5e1 hoptFiErloe!-57J 2-M€h&apitdens95.{&7 2- dry'Dheflol

10&39{, 3,4-lirehtphend106{r!t91413 Nephmaknew71-1 2tliboaniline0s0&2 $Nitrofiif,ne

B&BFL

BHL

BAL

BAL

BFL

BFL

BRI.

8RL

BRL

BRL

8RL

BHL

BffL

BNL

BFL

BFI.

BRL

BRL

BRL

BRL

BRL

BNLgnL

B8L

BFL

BNL

BRL

8RI

8RL

8FL

BRL

8RL

BRL

BHL

8FL

BRL

BRI.

BRL

8Rt

BRi.

8Rt_

BRL

BqL

BRL

BFL

8FL

BRLgRL

BFL

$/l€dym/tq dy

ro({ d]

rgh fy

lqb dy

wrq dv

!41€ fiy

llgre dv

a'l€ dv

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ts/}0 dy

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lqis dl

riytg fy

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|lgt{ dry

|Ets fv

t4lg fry

!$4q dy

t91q dy

rdlg d)

$a! dv

lryrsdYldh d)/

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|4tqdy!g/lq dypg4q dv

|4/lq dy

|,0to dv

wh dv

ldkg trv

vglq dyysrq dy

lldlq dv

ugnq d]

$,lq dy

|lg/rqdy

824

E4

M4

824

824

824

82{pa

821

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v4824

821

@4

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82{

82,4

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024824

Ir.b labo&tory Epo.l it,tottdid wirhou.n aalhorizfd sigEaate od !h2 coter pa* -

r' Rcportrble Dete.tion Limir BRL = Below Reporting Limir Pegc 56 of 154

Page 323: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SaErple ldentificationM8F-39 2'-4'sA5980l-r r

Client Proiect #301_88

MatrixSoil

Recoivcd2'7-Mar-07

Collection Date/Time26-MaG07 00r00

CAS Na Anatrte(s) Result Flag Units 'RDL Dilation Merhod ReJ, Peparcd Anqbzed Bakh Analrsl

Semlvolrtll€ Orgrnic Corr|poundr by cCMS

Sernivolalile Ooanic Compound b! SW846 8270CPreparod by method SW846 35508

10041€ +NitDamtine BHt9s€5.3 itmb€nzme BRL

!s'25-5 2.Nitoph€not BRL10042-7 +Ni@Enol [email protected] 9 N,Nifosodinethylarnine 8RL@lt+7 N-Nilrosodi-ntropylamine 8RL

6.30{ N-Nilmsodiphenylami0e BRL

Er{6.5 pentadllorcphend BRL

6rr_8 Phenanhrene 8RL10€452 phenol BRt129{04 ry.ene BRL1lo-oc1 pyrtdine 8RL120.02-t 1Pd-Trichloroben2ene 8RL

95-991 2,4,5-Tridiorophend 8RL6.06.2 2,4,6-Trid orophenol BRL

a1{o4 2-Fhrorofuhenyl 546?-t21 2-Fhlorqvnd 571166@4 Mtt6qzene45 n1166f4-2 PheMl4s 5f17106t4 leqlwyl44 n1t&tc4 Z4,efibtonophgnd 51

Tskl Melrls by EPA 6000/7000 Series Mettodr

0.209

29-Mar{7 o&{p.{l 7031174 M.BtiSlq fiy 3300

fSfrS dry 824

pSfrS dry 824

!g4q dry 3300

p$4q dry 8?4

pdlq dry 824

fS,Tq dry 824

pdkS dry 824

lslq dry 824

!s/rq dry 824

ldlqdry 824

ldlq dry 824

pg4q dry 824

ldkS dry 824

pdkg dry 824

30.130 %

1r110%

iG130 %

t r 1 t 0 %

&130%

l 6 t l o %

ng/tq dry 0.0455

ms^S dry l.4l

r,g/kS dry 2.12

n'94(g dry 0.705

fidkg dry 0.353

nqls dry 0 705

myrs dry 106

mS,4q dry 212

mS/ 0.0100

mgl 0.0150

mgl 0.0050

mgn 0.0025

mdl 0 0125

ngil 0.0m40

mg/l 0 0075

mq,4 0.0150

sws46 8270C

o2.Apr{i 0}Apr07 7031810 YP71ls975 Merc!ry

Tolrl Metrb by EPA 200 Seri€s Methods

lt4u-al Silver

?lrl$38? AGenic

7,!lll3g3 Badum

741$4+9 cedlnium

t1,d"41,3 Cktrnium

TIEF !lz-1 Lead

[email protected] S€leflium 3.3s

SPLP Melrls by EPA 1312 & 600Ot000 Series Methods

SPIP Extaclron Corndeled

7@-?44 Silvor BRL

t440.3S2 AEenic BFL

71{0n&3 Bariom 0.m98

7440-13{ Cadmium 8RL

7lr$<^t Chomium BRL

?130.gr{ M€rolry BRL

r3ss2-l kad 8RL

782492 S€tenium BRL

Cetercl Chemfu try Parsh€terj

%Sohrh 65.7

1 i . 8

sw8.167471A

EP4200.7

sw84613r2

sw846 r31260108

sw846131274704

swM6 r3t2/6r)109

Slvl2540 G Mod.

Q AprAT

2eirar'07

3)Mar-07

HB

101

0.367

4.34

28-Mai-07 rc01763 8D

02-Apr{7 7031805 LR

02-&d7 7031 806 YP

02-Apr-{)7 70{11805 tR

3GIUar{7 30{lar-07 7031E79 Yll

This labonlory rcFod it not ealid wirhott an authori.ed signara.z oa lhe coter Fage .

I Reportable Detection Limrt 8RL = Below Repoding Limit Page 57 of 154

Page 324: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Id€ntificatio11M8F-40 2-4,sA595l7-08

Client Proieot #30t-88

Collection Date/Timelg-Mat47 00:00

MatrixSoil

Rcceived20 Mar-07

CnS No. Ana\te(s) Res l FI"S Units +NDL Dilutbn Method Retr. Prepared AnatJzed Batch Analfst

Volatlle Orgrnic Compounds

VOC Extraction Field exfacted

181

pgftg dry ts1.4pdkgdry 1230

lqkg dry 61.4

UgkS dry 61.4

!g/kq dry 6r.4

!g/kg dry 6'1.4

fdkS dry 61.4

Udkg dry 61.4pdkS dry 123

LiS/kS dry 614pg/kg dry 61,4pdkg dry 61.4pdkS dry 61 4

ldkS dry 30/

IdkS dry 61.4

Ug/kg dry 61-4

rc/kS dry 123pS/kS dry 61.4pS/kg dry 123

US/kS dry 61.4

ug/kg dry 61 4pg/kg dry 123

tgtkgdry 61.4

lrdkS d.y 61 4yg/kg dry 61 4pdkS dry 61 4

US/kS dry 61.4pdkg dry 61.4

l.dkg dry 123

US/lg dry 61.4pg/kg dry 61.4

ug/kg dry 61 4

l4/kg dry 61.4pgtkSdty 61-4

PdkS dry 61 4

tdkg dry 61.4

udkg dry 61.4pSftS dry 6'1 .4

PdkS dry 61.4pdl€ dry 61.4

!S/kS dry 61.4

tSlkgdry 61,4

!S/kS dry 614

ldkS dry 61 4

ldrg dry 61.4

i.idkS dry 61-4

!g/kg dry 614pg/kg dry 614pS/kS dry 61.4

Volatile Oroanic Comoounds vocoPrepared by method SW846 5030 Soit (high tevel)76't+1 1,1,2-fidrlotohnuorcethane(FeoERL676rr_r Acetone BRL107-13F1 Acrylonltrile BRL7143.2 genzen€ BRL108-46-l Brcmob€nzene BRL7+97-5 gromochloromethane BRL71274 Brumodichtoromethane BRLf,2r2 Brcmoform BRL74{}9 Bromomethane BRL7&913 2-Eutanone (MEK) 8RL104-514 n_Bulytbenzene BRL13S984 s€c-Butytbenzene BRL9a{G6 tert-Butytbenzene BRL7r1SO carbon disutftde BRL56-23-s Cabon tebachtoride BRL10e.s0-7 chloobenzene BRL750G3 Chlomelhane BRL67{F3 Chloroform BRLt447-3 Chloromethane BRL95-49{ 2-Chlorotoluene BRL10q3,! +chlorotoluene BRL5124 1,2-Dibromo-3-chtoropropane 8RL124-,€n Dibrornodrtorcmethane BRL10&93-1 1,2-Dibromoethane(EDB) BRL74-9t3 Dibromornethane BRLgs.slj.l l,2-Dichtorobenzene BRL541.73-1 l,3-Dicllorobenz€ne BRL10tu6-7 l,4-Dichtorobenz€n€ BRL75-71-8 Oichlorodifluoromethane (Frcont2)BRL75-31F3 1,.t -Dichloroethane BRL107{6-2 i,2-Dicthloroethane BRL75-3s4 l,l-Dichloroethene BRL15e59-2 cis-t,2-0ichtoro€hene BRL156{0-5 trans.l,2-Dichloroetf€ne 8RL7&47-5 1 ,2-Dichtoropropane BRL142-20-9 I ,3-Dichtorop.opane BRL594-m-? z,2-Dichloropropane BRL50+584 l,l-Dichloropropene BRL10ool-01{cis-1,3-Dichloropropene BRL1m61{2€ kans-1,3-Dichloropropene BRL10S,114 Ethytbenzene BRL674&3 Hexacblorobutadjene BRLs9r.784 2_Hexanone (MBK) BRL98€2-8 tsopropytbenzene BRL99-87{ +lsopropyttotuene BRL163a44a Mehyl teft_butytethef BRL10&10-1 4-Methyl2-pentanone(M|BK) BRL75{9-2 Methytene chtoride BRL

voc

sw846 8m08

21-Ma.-O7 21-l at 07 7031261 BO

27-Mar07 27-Mat 07 7031602 fiar5050505050505050505050505050505050505050505050

505050505050505050505050505050505050505050505050

505091.20.3 Naphthalene

Pss€ 37 of 124

This labotulory report k noa valid arithoat on atthoriaett signoture on ahe corer page

' Reportable Delecrion Limi. BRI- = Belovr Repsting Limit

Page 325: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Idetrtific{tionM8F-40 2-4'sA5951748

Client Pioie€t #301-88

MatrixSoil

Collection Date/Timel9-Mar-07 fi):00

Receivedzo"Mtt47

CAS No. Analrle(s) Fl"g U,zi^ 'RDL Dilutiatr n{ettud Rel, P.eprd Analturl Bdlc$ Analtsl

i0$651 n-Propylt€nzene10(82-5 Styr€no63s2o4 1,1,1,z-I€trachloroehane7s3+5 1 ,'1 ,2,2-let-ehlorce$ran€127-18-4 TetrachlO{Oehene108{&3 Tolu€ne87-6i.6 1,2,lTdthl6obenzene12G€2-1 l.2.4lrichlorobenz€ne71-s5-6 1,1,l-frichloroethane79{0-s '|.1,2-Tnc$loroethan€

79{1{ Tficfiloroethene

vohaile Orgrnic Compolndr

Volatile Oroanio CompoundsP,oparod by method SW846 5030 Soil (high level)

BRLBRL

BRLBRLBRl-r58BRL

BRLBRLBRLBRL

75-69-4 Trichloroffuoromethano (Freon 11) BRL96-10-4 l,2,3.Taichlo.opopane ARL9543-6 1,2,4-Tdmethylb€nzene BRLt08$7{ 1,3,5;Trimethytbenzene BRL

BRL1.{}

66.3BRLBRLBRLBRLBRL8RLBRL

1001A

94

BRLBRLBRLBRLBR.LBRT791C€lc{rlated as

vdkgdry 61.4

t/glkgdty 61.4

Fdl€d.y 61.4

rdkS dly 61.4

rcikS d.y 6l.4

UdkS dry 61.4pdkgdry 61.4

ldkS dry 61-4ydkSdry 61.4

rgtgdry 61.4

|,4kg dry 61.4pdkg dry 6f .4

rc/XS d.y 6t.4

USrkS dry 61.4pgftSdry 61.4pdkgdry 614

IdkS dry 123

!S/kS dry 61 4pgrkS dry 614

rdkg dry 61.4ygtsdry 61.4pgts dry 61 4pdksdry 61.4pdxg d'y 614

UdkS dry 1230

76130 %70-130 %70-130 %70-130%

mg/kg dry 17amS/kS dry 174mgn€ d.y 17amgftg dry iAmdkg dry t7a.rE/kg dry 178mgilgdry 17Amgrqdry 17ArE/kgdry 178nglagdry 178

4+140 %

50

5050

50505050505050505050505050

50

SW 846 82608 27-Mat4f zl-MaFO7 70316m mar

+CT ETPH 22-Ltur{}7 26lvlar-07 7031284 DS

7541.1 Mnyt chlo*teit3o.2cr m,p-xylengs+474 o-Xyleoe1O$9S-9 Tetrahydrofuran6{F2s-7 Ethytet}Ef9s4ffi T€ft-arnyldlethylethere37-92-3 E|hyl tan-butyl edEr10e20-3 Ctiisopr@yt€th€r75.65{ Tert-Butanol/ bntyl alcohol12$9r-1 1,+Dio)(ane

Srr,?og€le r€cov€nes:46040{ +Brcfiof,uorcbenzeae

2037-265 foltr€.t€4S

17060474 1,2-Did O@e?hane-d4

1868-gA-7 Dbtondlto@rnethane

f, nctrble Petrolatm llydrocrrbont

Extractable Total Pgtol€um Hvdrocarbons

Prepar€d by mefiod SW846 3545A

AOo€al-9 Gasoline6€{7e3cz FuelOll#26842631-3 FuetOil#466553-00-4 Fuel Ol #6Mos800o00 Moto( OilJOOI()()000 Aviatjon Fud

Unid€ndf€d

of|€r Oil

Total Peboleum Hydrocedons 797

CSC3,€ AliphElic Hydrccarhons 797

Sunog6fo f9cot ends.'$8n332 1-Chlot@ddecarE 158

ScDlvolrtil€ Orgrnlc Compourds by cCOroanochb.ine Pestbides SW846 8081APr@ar€d by method SW846 35508349{e2 Atdrtn BRL LidXS dry 6.16 SW84A 8G1A ?2't|er-Ol 27+ns47 7031275 TG

Thit laboruloq rqort &t ̂ ot uaIU *ilhout aA authotl&d dgralare on dte &rer pcge -

' R@orhbl€ Detedion Limit BRL = B€low Reponing Lirnit Page 38 of 124

Page 326: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeptificarionMtF-40 24'sA595 | 7-08

Client Proiect #:r01-88

MatrixSoil

Collection Date/Timel9-Mar-07 00:00

&!!siyed20-Mar-07

C,aS No. AMIla(s) ResaIt FI"S Units *RDL Method ReI. Prcpared Analrzed Batch Arutltst

Semivohaile Orgrnic Compounds by CC

Oroanochlodne Pesticides SW846 8081A

Proparod by method SW846 35508

31se4{ a-BHC

319+5-7 brBHC31+86{ d-BHC58{}9 g-BHC (Lindane)57-1+9 Chlordane

72-3+s 4,4-ODD (p,p')725'e 4,4,ODE (p,p')

so-2s-3 4,4-DDT (p,p')

on57-t Dieldrin95948€ Endosulfan I33213{+9 Endosultan ll1031-07{ Endosulfan sutlat€72-204 Endnn7421-934 EndrinAldehyde7641-A Heptachlor7243.5 l,bthorychlor1024.57-3 H€ptaclhtorEpoxidea0O1-35-2 Toxaphene

s1o3.71'9 a.Chlordane5,s{t6.34.7 g-Chlordane

r,3,49+70-s Endrin Keirne

Sudog€ls rscover'gsi1 03863+2 4, 4 -DB-Octaff uorobiphenyt (Sr)

mst-2a-3 Decachlorobiphent4 (St)

Polvctrlorinated Biohenvls bv SW846 8082

Prepared by method SW846 35454

1262L11-2 PCB 1016111u-28-2 PCB jZ21

11141-16-5 PCB 12325346*21-9 PCB 12421fr72.:g-B PCB 124A11rxr7-6s1 pCB 12541 109tr2-5 PCB .1 2603732+23-5 pC8 12621fi0c144 pC8 1268

Sunogale recoyeresr1 03864+2 4,4 -DB-Octan uorobiphenyl (Sr)

2051-213 Oecachlorobiphenyl (54

Semivolrtile Orgstric Compounds by CCMS

BRLBRLBRL8RLBRLBRLARL

8RLBRL

BRLBRLBRLBRLBRLBRL8RLARLBRLBRLBRLBRL

3252

BRLBRLBRLBRLBRLBRL23.4BRLBRL

4090

BRL

BRLBRLBRLBRLBRLBRLBRL

ldkg dry 6.16pdks dry 6.16

lig/kg dry 6.16pdkS dry 6.16

UdkS dry 30.8

udkS dry 6 16

UdrS dry 6.16

IS/kS dry 616pdkS dry 6 16

lgtgdry 616pg/kg dry 6-16

ldkS dry 6-'16

lgrS dry 6-16

ldkS dry 6.16

!Sn$ dry 6.16psil$ dry 6.16

lqkg dry 6 16pS/kS dry 30-8pdkS dry 6.16pgkS dry 6.16

!S,/kS dry 6.16

30-150 %30-150 %

!g/kS dry 12.3

ldkS dry 12 3

tdkSdty 12.3pdkS dry 123pq/kg dry 123

!S/kS dry 12.3pg/kS dry 12.3

!S4<S dry 12.3

!S/kS dry 12.3

30-150 %3G150%

ldkS dry 1770

ldkS dry 1770pgks dry 1T7O

lrdkg dry 1770

udks dry 1770

Uqlgdry 1770pS/kg dry 1770

lSn(g dry 1770

I

I'|I

1

1

1

1

1

1

1

1

I

1

1

1

1

1

1

1

1

SW8.f6 8081A z2-Ma.Ol 27-Mat47 7031275 TG

SW846 8082 22-Mat47 24-Mat47 7031313 l\rP

SW846 8270C 23-Marol 25-M^t47 7031371 M.B

Semivolatile Otuanic Comoounds bv SW846 8270CRepared by method SW846 35508

a&32-9 ACenaphth€ne206'964 Acenaphthyten€

Aniline12G12-7 Andl€Cene1912-24-9 Ataazine10$3$3 AzobeMene/Diphenytdiatne92-€7.5 Benzidine5645-3 Benzo (a) enthracene

22222222

Thie laborularf rcpoft b not vdiil withou an auihorized signatt rc on lhe corer page

* Reportable Del€ctioE Limir BRL = Below Reporting Limit Page 39 of 124

Page 327: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldqntificationMEF-{o 2-t'sA5951748

Client Proiect #30t-88

MatrixSoil

Collection Dat€/Timel9-Mar-07 00:00

Received20-Mat-07

CAS No. Andtrta(s) Resalt Fl"S atb +RDL DUdIfi Mdhod n4, Pry)arul Analyzd Adch Adrtyst

Semlvol.lile Orgrtric Compo(trd3 by CCMS

Semivolatile Orcanic Co.nooonds bv SW846 8270C

Preparcd by method SW846 35glS50-32{ Eenzo (a) pyiEne20tgs-? Benzo (b) nuoraMeie191-24-2 Eenzo (g,h,D perylene207-08+ Eenzo (k) fuofsnthene65-0tO BerEolc acit10+51{ Benz}'l alcohol111,91r Bis(2drlo.oethory)rnecr6ne1i1-,!4-4 8is(2d{om€hyt)etE.3.963+3?-9 Bis(2.cl' cinisopropyl)€th€rr17€r-7 Bis(2-ethyth€ryt)phthdato10155-3 +Brcmoph€nyl phenyl eth6r65{&7 Butyt benzyt phthdtate€&74-€ Carbazotessfl).7 4-Chlorclmethytphenolr06-a7€ rl_chlofoaniline9f5S7 24htoronaphlhalen€F57-A 2chtofophenol700+72-3 4oftlorcplrenyl phenyt elher21&01-9 Chaysen€53,7G3 oib€|lzo (a,h) anthracen€132-64-9 Dibenzofuran95{,G1 |,2-Dafilorobenzenesr1-73-1 1,3-Oiohloaot€nzene106:-16-7 t,+Did{orobenz€ne9r€4-1 3,3',{ichlorobenzidine1aH3-2 2.4oicHorophenol844c2 Di€f|yt phthatatei31.r1-3 Oinethylphthatate10tr7€ 2,4oimethy'ph€no,lu-74-2 Di-n+utylphthalato5'?+52-t 4,6-Dinito-2-methylphenol5l+s5 2,4oinibophonol121-14-2 2,+Dinatobhene€0G2G2 2.8-Dinitrotoluener 1 7.€1-o Di{.octyl p,hfEt€tje20Ga4-0 Fkro€ndr$ew-7T7 Ffuof€nell$Z,l-1 Hexad*lrob€rizen€€7{e3 Hex€alorobutadienen474 l-lexgchlorocydop€itadiene5f-72-1 l-lexac'troethane191395 trdem (1,2,3-cd) pyren€!lo-12{ l-llathylmphtrEtene7E€$1 lsophomn€9l-574 2.Mefirnapfihatene*48-r 2-t{etrytpt eootr0&3e-., 3,4-Methyph€nol105JH-591-20-3 NapMElene8e-74-4 2-Nitlanilines9{92 }Niloanllin€

BRLBRLgRL

BRLBRI-BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRfBRLBRLBRLSRLBRLgRL

BRL

BRLBRLgRL

2.m0BRI-BRL

BRLBRLBRLgRL

BRL

BRTBRLBRL

BRLBRLBRL

ldkS dry 17fOpS/kS dry 1nOpg/kg dry 1770

ldlSdry 1770

Fdks dry 1no

lgftSdry lno

uSn{S drJ '1770

pdks&y 1770pSikS d.y lTlO

IglaS dry 1770pgrs dry lnl

Ugkg dry l77o

UdkS dry 17ro

IrSftS dry 1f?o

Wil€ dry l77OpC/kg dry 1nOpSftg dry 1T7opdke dry 1770

udks dry 1770

ldkg d.y 1770pSI€ dry 1770pdks dry 1770pgrS dry 1no

!g/kS dfy 1770

ldks dry r77o

rcftg d.y 1770

!s/ks dry 1770

ldxSd.y 1Tl0pdkSdry 1770

fdrgdry 1170

ldkS dry 7770

rgrq dry lf?o

!9ft9 dry 1770pdkS d.y 17fo

Ug/kS dry 1T7Opqkgdry 1770

ldrgdry 1770

fldrqdry t?70

rdkS dry 1770pdko d.y 1770

US/tgdry 1Tl0pdks dry 1770

ldksdry 1770

FS/kS dry lrTO

tdfqd.y 17rO

tgftSdry 1770

!g/kS dry 1770

pS&S dry 1770

ldrgdry rno

UgkS dry l77O

22222

2

222

222

2222

2

222222

22222

2

2

2

2

2

SW846 8270C 23.Ma147 2r>^tief47 7031371 M.B

Thlt bboraloq .eporl k ,roa tditl tsithoet a, seho z.d stgdatsrc on ahe cavu pagc.

' R€portable Deie€lion Limit BRI- = B€low ReportinC Limit P.ge 40 of 124

Page 328: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [d€ntificationM8F-40 2-4!

sA59517-08

Client Prorect #l 0 r -88

Collection Date/Timel9-Mar-07 00:00

MatrixSoil

Received20-Mac07

CAS No, Anabte(s) Resqll Flog Unia *NDL Dilutian Method ReJ Prcpared Anallzed Rarch Anaryst

S€mivolrtile Organlc Compounds by CCMS

Semivol€lib Oroanic Compounds bv SW846 8270C

Prepared by method SW846 35508

10G01{ 4-Nitroaniline

98-9+3 Nitobenzenea8-7gFs 2-Nitrophenolt0tr02-7 4Ntroph€no,l62-75.9 N-Nitrosodimethytamine62r{4-7 N-Nitrcsodi.n-propytamine86-3G6 N-Nilrcsodiphenytaminel7€GS Pentachlorophenol

85-01€ Phenanlhrene10e95-2 Phenol

i2lHD{ Pyene11G86-1 Fl.idine120-02-1 1,2,4-Trichlorcbenzone

95-95-4 2,4,s.Trichlorophenolg€.{G2 z,4,GTrichlorophenol

Sufogale recoveies:

3214G8 2+luorobiphenyl

7-12-! 2+luorophenol

4r6s-6oo Nitrobonzene4s

416s42-2 Phenol4s

1718-514 Teryhenyl4l4

1I&794 2,4,6-Tibromophenol

Totd Mellls by EPA 6000fl000 Series Methods

743947{ Mercury

Toarl Mctrls by EPA 20O Series Merhods

zr4G22-4 Silver

744036-2 Aisenic

7440.39-3 B€rium

7440-4+9 Cadmium

744Ga7-3 Chmmium

7,13992-1 Lead

z7E2-1+2 S€bnium

SPLP Metrh by EPA 1312 & 6m0/7000 Serier Methods

SPLP Extrection

I{4+22-4 Silver

7,1,|I)-3&2 AEenic

74rg!393 Berium

74()4+9 Cadmium

?.r,{o-.r7,3 chromium

7439€7-€ Merc!ry

2439{2-1 Load

7782-492 Setenium

C,€n€rrl Ch€mistry Panmet€rs

222222222222222

SW846 0270C 23-Mar47 25-MarO7 7031371 M.B

1 SW846 747'lA 26-Mal-07 27-Mar47 7031322 YP

EPA200.7 26-MaFO7 27-Ma?O7 7031321 HB

BRLBRLBRL

BRLBRLBRLBRLBRLBRL

BRL2,090BRLBRLBRLBRL

108809876122106

Completed

ARL

BRL

0.0128

BRL

BRL

BRL

0.0263

BRL

89.9

pg/kg dry 7O7Opg/kg dry 1770

!g/kg dry 1770

tgkS dry 7O7O

IgftS dry 1770

UdkS dry 1770pdks dry 1770

lSftS dry 1710pdkS dry 1770pgtS dry 1770pg/kg dry 1770pdkg dry 1770

!g/kg dry 1770

ldkS dry 1nOpdkg dry 1770

30'130 %1U l10 %30-130 %15-110 %30-130 0k

1&110 %

mg/kg dry 0 0330

fitg/kS dry 1-O7

mS/Xg d.y 150

rnSftS dry 0-535

mgftg dry 0-267

nEftg dry 0-535

rE/kS d.y 0.802

ntSnq dry 1.60

mg!4 0.0100

mg/l 0.0150

mqa 0.0050

mg"4 0.0025

mg./l 0.0050

mg,4 0.00040

mg/l 0.0075

mg/l 0.0150

0 .136

'| .24

10.4

52.1

1 .00

25.0

201

BRL

1 SW8461312 22-Mar47 22-Ma.-0l 7031344 BD

1 SW846131260108 23-Mat4f z+Mer07 7031408 LR

1 "

1 ' ,

1 '

1 "

1 SW8461312t470A " 26-Mar07 7031409 YP

1 SW846131260108 " 24-Mal.O7 7031408 LR

1 ' ,

1 SM2540 G Mod. 24-Mat47 24jv.al.07 7031463 OP% Sol ids

PaBe 4l of 124

This hbodory rcpod is noa wlid arithot ! an suthorked sEnatare on the coeer poge.

I R€ponable D€.ection Limit BRL = Below Reporring Limi(

Page 329: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationM8F41 4-5'sA5951749

Client Proiect #30IJE

MatrixSoil

Received20-M^t47

Coll€ctiop DatdTime| 9-Mar-07 00:00

CAS No, Aaolytz(s) FI4g A a rRDL Dilttlbtt Method Retr Pepared A@lyzed Bat4h Analr$t

Voladl€ Orgstrlc Compounds

VOC Enra€tion MA

ldks drv 6.6

t dks dry 132

lSftS dry 6.6pdks dry 6.6

lgrg dry 6.6

flg](S dry 6.6

Wks dry 6.6

rdks dry 6.6pSftSdry 13.2

Fdks dry 66.2

lg,lqdry 6.6

Uglkgdry 6.6

lgkg dry 6.6pdkg d.y 33.1

lgxgd.y 66

uSASdry 6.6pdrg dry 13.2

ldkgdry 6.6

udkS dry 13_2

Idkg dry 8.6

tdks dry 6.6yCftgdry 13.2

Pdkg dry 6.6

tdkgdry 6.6

fldkS dry 6.6pdkg dry 6.6

tjgiksdry 6_6pSftSdry 6.6pdkg dry 13.2

tgkgdry 6.6pdkSdry 6.6

VdUvJdty 6.6

trdkg dry 6.6pdkg dry 6-6pS/*Sdry 6.6pdrg dry 6.€pdtgdry 6.6pdkg dry 6,6

tdkdry G.8

udkg drv 6.6

!S/rqd.y 6.6

rdts dry 6.6

lcrtgdry 66.2

udkSdry 6-6

ldlq dry 6.6

Igrkg dry 6.6

ldkg d.y 66.2pel{g dry 66.2

Fdrg dry 6.6

21-L.lar.07 21-llar-07 7031261 BOFreld exbacledVolatile Oroanic ComoaundsPrepared by mef|od SW846 5035A Soit (torv bvet)76n11 1,,|,2-T.id orohnuoroothane(FreoERL674+1 Acebne SRL107,13,1 Acrytonitdte BRt_f11t2 B€nzene BRL108-86-1 Bro.nobenz€n€ BRL71-91-5 Bronroafiloron€thrne BRL75-27'4 Brcmodichloronethane BRL7r2r2 BDmototrri gRL7,t{}9 Brcmcmethan€ BRL7&9!3 2-ButanorE (MEK) BRL101-51€ n-Bulylbe@en€ BRLl3tFgE{ s€eBuq/b€nzen€ BRL9€{6.6 tsft€utylbenzere BRL7!v1s4 C€rbon disulfde BRL5€-23{ Ca6on letrachlodde BRL10&$7 Cftlbmb€nzene BRL?5{G3 CHormthane BRI_676e3 Chloroform BRLA-47-3 Chloromelhen€ BRL!15-49{ 2{hlorotolu€ne BRL106-434 +Chlorctoluen€ SRL9G12€ 1,2-ubro{ytc}chtoropromne BRL124-4€.r Dibrcmochloiomediane BRLioCg3.a l,2Obrorno€lhan€ GDBI BRL744+3 Dibrchom€thane BRL96-5G1 l,2.Dichlorobe.Eene BRL54r-?!l |,3-Didrloob€nzene BRL10€-1{}-7 |,4oicfilomb€nzene BRL7s71€ Dichlorodffuoromethane(Freon12)BRL75'34-3 1,1-Oict{oroethane BRL10rc€-2 l.2-Dichtoroethane BRL74.3s l.|-Dichtoroethene BRL156-5e2 cis-'1.2-Dichloroeh€ns BRLt5G@-5 bam-1,2-Dichloroethene BRL7E{7-5 l,z-Dichloropmpsne ARL142-28.9 l,3{iclilorcpopane BRL59+20-7 2,2-Dicl{orcprop€ne BRL563-58€ i,1-DichtorcDroo€n€ BRL10061{r€ cis-1,3-Dichloroprcpene BRLi0061-o2€tEns-1,3-Didtloroprop€ne BRL100-41.1 Ethyft€nz€oe BRI674&3 Hexaailorobutadiene BRL591-786 z-Hel(anon€ (MBK) BRL9O{2{ tsopropylbenz€ne BRLs-87-6 +Lsop.opy'bluene gRL1634{s ilethylt€rt-brtylether BRL108-rct +ilethy'i-21o€i1l&one(MIBK) BRL7s4*2 M€thylene dtlodde BRL

SW 846 82608 e.-Mat47 n+tat{7 7m1335 RLJ

9l-2G3 Naphhaleno

Page 42 ol 124

Thit lzborotor! rqod is noaealld vi pat an ar.thorizey' sigdaturc o, the cora, page.

' Reporhble DotecrtuE Lindt BRL = Betow R€poning Limit

Page 330: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-4r 4-6is459517-09

CLient Proiect #301 -88

Collection Date/Timel9-Mar47 00;00

MatrixSoil

Received2I-Mat07

CAS NL Ahqlrte(s) FI"S *RDL Dilution Method Retr Prepared Anzltzed Batch Anobst

Volatlle Oryrhic Compoundr

Volalile Oroanic Compounds

Prepared by method SW846 SO3SA Soit (tow tevet)

10365J n-Propylbenzene BRL1fi82-5 Slyene BRL6:1120{ 1,1,1,2-Tetrachtoro€thene BRL?9.34's 't

,1 ,2,2-Tet.achloro€thane BRL127n4-4 T€kachtoroelhene BRL10&€43 Toluene BRL07{1{ 1,2,}Trichtorobenzene BRL1A|82n 1,2,+Trichtombenzene BRL7r{54 1,1,1_Trichloro€thane BRL79{C5 1,t,2_Trichtoroethane BRL79{1{ Trichloroethene BRL75{H Trichloronuoromethane (Freon 11) 8RL96{0-4 l,2,sTrichtoropropane BRL96-63-6 l,2.4.Trimethylbenzene BRLi0&67{ 1,3,5-T.inrethytbenzene BRL7541-4 Vinytchtoride BRL1S0-2G7 n,p_xylen€ 8RL9+47{ o-Xylene BRL10s99-9 Tehahydrofuran BRLdl-2+7 Ethytether BRLBa{5{ T€rt-amyl methyl eher BRL6fl42-3 €thytte,t_bulyt ether BRLt0&2G3 Diisopmpytether BRL7565-0 Tert-B,llanot/ butyl alcohot BRLi2341-1 l,4-Dioxane 8RL

Sanwale Gcove,i€sl4loM 4-Bromofiuorobenzene 92m3f-2e5 Toluane4S 9917060474 l,2Dichlorcethane44 109lAOA-sj.7 Dibronofluorcmathane 1O5

Extrrctrble P€troleum Hydrocrrbom

Extractable Total Petroleum Hvd.ocarbons

Pr€pared by method SW846 354SA

SW84682604 22-Mar47 2rMarOT 7031335 RLJ

+CTETPH 22-Mar47 26-Ma(OI 7031284 DS

lgkS dry

!S/kS drypdks dry

ldks dry

rrS/kS dry

!S/kg dry

l4/kg dry

lig/kg dry

tdlq dry

!g/ks dry

LrdkS dry

t'S./kg drypg/kg dry

l'dkS d.ypqkg dry

!S,kS drypS:ftS dry

LiS/kS dry

!g/kg dry

ldks dry

t4/kg dry

!g/kg dry

!g/kg dry

US/kS drypdks dry

6.6

6.6

6_6

6.6

6.6

6_6

6_6

6.6

6.6

6 6

13_2

6.6

66-2

6_6

6.6

6.6

6.6

66.2

132

I

1

1

1

1

1

1

I

1

1

1

1

1

I

1

I

I

1

1

1

1

I

I

1

1

8,Om{1-9 casdine6€47s3G2 FuetOit#26847s31.3 Fuet Oil #4€€563-{rs4 Fuel oil #6lvtlgso(o(l) Moto, Oiirl010o00o Avialirn Fuel

Unidenlified

Othef Oil

BRLARLBRLBRL

SRLBRL728

Calculsted as

70-130./o70-130 %70-130 %7G1m %

mgr'kg drymg/kg drynE/kS dryn'qkg dry.ndkg drymg/kg drymg/kg drymdkS drymSftS drymS/kg dry

40-140 %

185 1

185 1

185 I

185 1

185 'l

185 1

185 1

185 1

1 8 5 1

165 1

TotalPelroleumHydroceftons 728

C}C36 Aliphatic Hydrocarbons 72A

Sunwafe recouenes_,3?'86312 r -C h I otoo cts d eca n e

Sc]r|holstil€ Organlc Compouds by cCOroanochlorine Pesticides SW846 8081APr€pared by method SW846 355083q9{X}2 Aldrin PSi l(g dry SW84680€14 22-Mar47 27{.nat47 7O312f5 fc

Thb laboralory repo.t k not volid |9ilhoat an ouahorized signaru.e on lhe coeer paEe_

. Repodabte Detedioo Limit BRL = Below Reporting Limit Page 4l of 124

Page 331: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ IdentificationMtF-41 4-6'sA595l7-09

Clietrt P.ojec! #301-88

Mari{Soil

Collectiotr Date/Timet 9-Mar47 00:00

Received20-lvlar47

CAS No. AaalWG) Fl4e 'RDL Diluioa Me.hod Retr. Ptepated Anaryzd Balch Aaztpt

Semivolsdle Org. c Compounds byCCOrqanocf orin€ Posticides SW846 8081APrepared by melhod SW846 3550831$44{ a-BHC3rs-0+7 b,BHc31s{6{ d-BHC58{99 g-BHC (Lindane)57-7+S Ct ordane72-u-a 4,40DD (p,p,)72.5$s 4,+DDE (p.p,)5o?s3 4,4-DDT (p,p.)6{L57-1 Dieldrin959-98{ Endo6ulfan I36213-65{ Endlosulfan lll03i{74 Enclosultan &rtfet€72-20.4 Endrin7421.93-4 EndrinAtdehyde76-44{ H€ptadtlor72-.3^5 M€froxychlor1024€7r H€ptachlof Epoxide60olns2 Toxaph€ne510$71-9 a-Chlordan€5,566,3,t-7 g-Chbdan€5349|70-5 Endrin Ke{on€

Sdaog€fe r€coysnies.'103866+2 1, +Dei-Oclduotohiphenyl (Sr)m5t-21-3 Decachbrobiphenyt (Sr)Potucfibrinated Biohenvls bv SW846 8082Preparod by mehod SW8,t6 354SA12674-i1-2 PC8 t0t61110+2V2 PCB 121rr1.r-16{ PCB 12325x46$214 PCB 124212672-29+ PCB 12/|81i097$r PC8 t 254rr0e6{.5 PcB 12603732+3"5 rcB 1262r11(rc-r4r PCB 1268

S(,/rlogEle r€co|Eriesr1u#re4+2 4, 4-DSOcbf @rcbhhenyt (Sr)mq.zaa Dacadrbtobiphenyt (Sr)

Semtvolrtile O.grnlc Colr|po!trds by GCII{,S

SW846 8081A 22-Mar-O7 27n,€t47 7031275 TGBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

3589

BRLBRLBRL8RLBRLBRL8RLBRLBRL

30fi

BRLBRLBRLBRLBRLBRTBRL|,, t10

pdlqdry 6.60

ldxgdry 6.60

lS/lqdry 6.60

ldkgdry 6.60gflrg fiy 33.0

WkS d.y 6.60pSlqdry 6.60pglg dry 6.60

trgkg dry 6.60

lSftg dry 6_60

IgftS d.y 6.60

l€ k0 dry 6.60

udl€ d.y 6.60pc/rg d.y 6.60

lgl(gdry 6.60

Udlgdry 6.60

US/kS dry 6_60

ldks dry 3:i.0pdko dry 6.60

IgkS dry 6.60pqtgdry 6.60

tu1 f r%38 f l%

lgftSdry r3.2pgts dry 13.2

lrgkg dry 13.2

lgkS dry 13.2pgkg d('r 13.2

rcn(S dry 13.2gSn(S dry 1X.2

Hfil(od,y 13:

rglSdry 13.2

fr-150 %381fi%

ugkg dry s20

ldkS dry s20

ldkS dry P0pSn(S dry 920

ldkSdry !n0

udkSdry s20

Idfgdry 920

rgks d'y 920

I

1

I

1

i

I

I

I

1'|

11

17

1

I't

1

1

1

1

SW846 8082 ?2-Mat47 24lller07 7031313 MP

SW846 8270C 23-l\,larO7 2g\rar{7 7031371 M.B

Semivolatile Omanlc Cornoounds by SWB,|6 8270CPrepared by metrlod SW8,t{i 35508a3<2.9 Acenaphthene20$96{ Ac€haphthyleoe62{}3 Aniline14n12.7 Andyaoefle1912-2+9 Atrazino103-33.3 Azob€flzen€/Dlph€nytdiazine92{75 B€nzidine56-lt3 Benzo (a) anthrEcene

TLb bbralort EpoA ls not vald withoU an outhorid siF ttnne on tL. col{lr pq. .. Re?brhble DEtection Limir BRL = B.tow R€portitrg Liruit PaAe tA of 124

Page 332: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificarionM8F-1t 4-6's,A'595 t?-09

Client Pro.iect #101 -88

MatrixSoiL

Received

20-Mar-07

Collection Date/Timel9-Mar-07 00:00

CAS No, Anolr.e(s) FloE "RDL Diluttun Method Rel PrepaEd Ana+1/d Eatxh A,'absl

Semlvolrdle Orgrnic Compounds by GCMS

Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35508

50'32{ Benzo (a) pyr€ne

20t99-2 Benzo (b) lluoranlhene191-2+2 Eenzo (g,h,i)perylene

20ru8-9 Benzo (k) fluoEnthene65{5{ Benzoic acidl0c5l{ Benzytalcohollrr-91-1 Bis(2-chtoroeflroxy)mehanelllaa{ Bis(2-diloroetlhyl)etrc.39638-32-s Bis(2-cjtjorojsopropyl)ether1i7i1-7 Bis(2-€hythexyt)phthalate101-5s-3 +Eromophenytphenylether85{s7 Butylbenzylphthalate66-74-A Carbazole59,5G7 4-Chloro-3-methytphenol106-47-8 4-Chloroaniline91-5$7 2-C+lloronaphthal€no95-574 2-Chlorophenol7m6-723 +Chtorophenylphenylether21841-9 Chry,sene5$7G3 Dib€nzo (a,h) arthracene132-64-S Dibenzoluran9+5r|1 1,2-Dicf{orobenzene541-73F1 1,3-Oichtorcbenzene10qG7 1,4-Oichlofobenzene9l-94'r 3,3"Dichlorob€nzidine12033-? 2,2[-DichlorophenolE4{G2 Diethytphthalate131.113 Dirnehytphthatate105€7-s z,4-Dimethytphenolu-7+2 Di-n-butytphthalate534-521 4,6-Dinitro-2-rnethylphenols1-2&5 2,4-Dinilrophenol121-1rL2 2,.{-Dinitrotoluene6oe2G2 2,6-Dinitrotoluenei17-M{ Di-n-octylphlhalatea)G,444 Fluoranthene86-73-7 Fluorenei1&74.1 H€xachlorobenzenea7€&.3 Hexacfilombut€diene7f..7-1 Hexachlorocyciopentiadiene67-72-1 H€xachloroethane1g}.3€-5 Indeno (1.2,3rd) pyrene{rG12-O 1-MethylnEphthalene78-5Sl lsopho.oneg1{7S 2-Mehy{nephthalene9S4&7 2-Methytphenol

10&39-4, 3,4-Methylphenol106-.{4-591-2G3 Naphthalene

&744 2-Nifoanitine99{&2 3-Nitroaniline

| ,2701,670

BRL1,840

BRLBRLBRLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRLSRL2,180BRLBRLARL8RLARLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRL3,1408RLBRL8RLBRLBRLBRLBRLBRLBRL

8RL8RL

BRLBRLBRL

Ig/kg dry S20pS/ko dry 92O

lgikS dry 92Opdks dry 920pdks dry 920pgks dry 920

lS.ftS dry 920

!SI(S dry 9mpg/kg dry 92O

udks dry 920

UgkS dry 920pdks dry 920

t S/kS dry 92O

!S/kg dry S20pdks dry 92OpdrS dry 920

tigkS dry S2Opsn(g dry 92OpgkS dry 920pd,|(s dry 920pdkS dry 920

ldkg dry 920

udks dry 920

US/kS dry 92O

ldkg dry 92Oyglkg dry S20

US/kS dry 920

t'dkg dry 920

ldkS dry 920

ldkS dry 920pSn(S dry 92O

ldks dry 920

Ig/rS dry 920

ldkS dry 920

udks dry 920

UdkS dry 920pdl€ dry 920pgftS dry S20

!g/kg dry S20

!S/kS dry 920

ldks dry 920

!S/kS dry 920

tig/kg dry 920

ldkS dry 920

lgkS dry 920

!S/kS dry 920

ldkS dry 920

ldkg dry 920

!g/&g dry 920

LiS/l€dry 920

SW84€ 0270C 23-Mar0l 25-Mel-07 7031371 M A

This labodorf Eport Ir ,tol valU pithotd an au.honzed signzturc on the cover page.

I ReDortable Det€ction Limit BRL = Below ReDortjns Limir Page 45 of 124

Page 333: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF-41 1-6.sA595l7{g

Cliept Pmiecl #301-tt

MatrixSoil

Collection Dare/Timel9-Mar47 00:00

Receiv€d20-Mar-07

CAS No. Aaalrtz(s) Res,ttl Fl"C U,tj't *RDL Dilution l{dhod Retr Pep$ed Adalyzzd Both A"zlyst

Semlvolaille Otgadc Compotrtrds by GCMSSemivolatile Oroanic Comoounds bv SW846 8270CPropared by rn€thod SW846 35508l0o{1{ 4Nit|oaniline9€-9$3 Nitrobenzen€8a-7+s 2-Nitoph€noll0o{2-7 4-Nitbph€nol62.7s-9 N-NitEsodimetfiylamine62r-Ar-7 N-Mtusodi-rFpfopylamine€+'3GG N-Nitr6odiph€nylamine87{F5 Pentachlor@hsnde5{1-8 Phenanthr€n€10+9t2 Phenol129-00{ Pyrene1101+1 Pyridinel2G€2-1 1,?,+Trichlorobenzene95-95-4 z,4,sTdchtorcphenol0a4&2 2,4,GTridtlorophend

Surogate re.nwies:32140-8 2+luotobiphenyl367-tz-4 2-Fluorophenol4165404 Niiobenzet@-at,116sa2-2 Phonol45171e.514 lerpheny'4l4tte-79-6 2,1,&Tlibtottbphenol

Iot t M€trb by EPA 5000/7000 S€ri6 Mettods

BRLBRLBRLBRLBRLBRLBRL

8Rf8RL3 ,110BRLBRLBRLBRI-

108

88102s21091 1 1

0.307

BRL

9.64

40.4

0.516

9.81

15?

BRL

pgl(g dry 3680

Ug/tgdry 920

UdtS d.y C2Opgftgdry 3640

!4kgdry 920

ItgxSdry 920

ldkg dry 920

lSftS dry 920

FdkS d.y 920

Fdks dry 920

IS/kgd.y 920

lSftS dry 920

lgrsdry 920

[grsdry 920

lgr'kg dry 920

30-130 %1t110%3L130 %15-lto%311130 %t t l t 0%

mg,fkS dry 0.0340

mg/ko dry 1.10

nBikg dly 1-65

mgikg dry 0.549

.r€/kg dry 0.275

mg/kg dry 0.549

m.drg dry 0-824

rrldkS dry 1.65

msn 0.0100

mSn 0.0't 50

mg4 0.m50

mgil 0.0025

lrlsr 0.0050

mgLI 0.m(X0

fiSn 0-0075

msil 0.0150

%

743947{ Mefcury

Tot.l Mearb by EPA 200 S€ries Meahods

744G22{ Sitver

?.?10'!&2 A.senic

74,10-393 garium

74t|1l3a9 Cadmium

71,{0-47-3 Chro,rnium

7(19.92n Lead

282!9.2 seleoium

I SW846 7,f71A m-Mar47 27']l|,,et47 7031322 vP

1 EPA m0-7 ?s.Maro? 27-|nar47 7ml32l HB

1 "

1 '

1 '

t '

I '

t '

1 SW8.{6 f3'f2 2-Itar47 22,,g'47 7031344 BO

1 SW8451312/6O106 ZA-llaFo7 244.147 70ill4o8 LR

1 '

1 '

I '

t '

1 SW8461312'470A ' 2ff!,lar47 7Gl1d0O YP't SWE461312rd0108 ' 24-lrr-07 7031408 LR

1 SM25{O G Mod. 21.1nd47 24nnat47 7O31{X} QP

SPLP M€tds by EPA 13 12 & 6001V7000 Serles Methdr

SPLPExtrEdtun Comdeted714444 sjlvet BRL7't4o.3a.2 Arsenic BRL

71,(13$3 Barium 0.00907440a3.9 C€dmium gRL

744047-3 Chromium BRLzF9{7{ irerdJtY BRL7439€2-1 Lead O.D2522E2.1$2 Seienium BRI_

GEne|'rl ChembF Prrr|||€ters

% Solids 88.2

Thlj labordtarf rcpod it,rat vdupithord att astlrotitl signott r. on E @ver lq..+ RepodablE Det€crion Limit BRL = Below Relorting Limit Page 46 of 124

Page 334: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMilF42 2'4'sA59803-r2

CLient Proiect #301-88

MatrixSoil

Received2'7-Mar01

Collectiorl Date/Time26-Mar-07 00:00

C"4S No. Anolr'te(s) Resa Flac Unia rRDL Dila.ioa Method netr Prcpared Andtzed Batch Analrsl

Volalile oroanic ComoounG

Prepared by method SW846 5030 Soit(high tevet)

7G1+l 1,12-TfthtorolnjtuoroethanelF@on BRL0744-1 Aceton€ BRL107-l$1 Acrylonihite 8RL71+le B€nzen€ 8RL1G06r BrorDb$zene SRL7+97.5 BEftEchtoornelhane 8RLEnl Bomodciloomethane BRLt 2j.2 BrDrotot|n BRt7'l{3-9 godbm€thane BRL78 93.3 2€uranone (MEK) 8RL10{'51{ n-Butylbenzene BRL1354S+ sec.Buvlb€flzene BRLs1rc6 t€i,Buvbenzene BnL7$1S Cadon disultide BRL5F235 Cadon tdlad orid€ BFL1(lg9o7 Chlonrb€fzene BFL75{03 Chtooethane BFLF7-6e3 Chlorotonn BFL744t-3 Chlordnehane SFL!6-498 2{hlorotoluene BFLlllc/B.1 4thlorotduene BFL96n2€ 1,2-Dbomc3dioropopane BFL124-181 Dibromod oonelhane BRL106s-1 12-DbrDmoefEne (ED8) BffL7+95-3 DibrorbrnefEne BFL96sct 1,2-Dchtorob€n:ene BRL54r-7l.r 1,3-Dicruoobenzen€ BFL1n6-46.7 t,4-Dicttombenzem BFL7$71-8 Ddiorodmuorcmslhane (Freon12) BFL7s3,{-3 1,1-oicltomethan€ BFL107{6.2 1,2-Dcldo.oettEne BFL?5.354 1,1-oicltoroefEne BFL156.50.2 cb-1,2-Drdtlorcelhene BBLls6€G5 bafls-1,2-Dd orodhefe BRL7l.Et{ 1,2-Dkhloo0opane BRLi{z.z&s 1,3-Dddoropopane BFL5ga-d'.7 z,2-Dichloropropane BFL5615lr{ l,1-Oichloroprcpene BRL1006r'016 cis-1,3-0idlloroprlp€ne BRL1006r-025 faE-1,3-0id{oropropcns BFt100-.r-4 Efiytb€nz€ne 123g/{63 HeEdrloobutadlene BFL591-78n 2-H€nanolle {MBK) BnLs6.828 tsopmpylberuene BRLstt{ 4.lsoprop}{toluene BFL183,r.04-,1 lvlsttyl ted-buty1 eher BFL

28-l,rarfl 28-ltl€t4t 1131767 BD

02'N147 02-Apr-07 ru4m17 mal

VoLtile Orgrnic Compounds

VoC Exkaclion

1osrGr +Methy,2renlanGre(MIBK)75{F2 Mehylsne c} orides! 20.3 Naphhdm€

ldtg dy 632

!94<9dry 1260

WkS dry 632

!S&dy 632

lrdko dy 632

ug4(g d] 632

!gA0 dry 63.2

lSrrg dry 602

lElS dry 126

|.lg/rg dry 6&

|lg/rS dry 632

!g/kg dry 53.2

ldlS dry 63.2

lqkS dty 316

|lg,tS dry 632

us,lq dry 63.2

psrts dry 126

tdks dry 53.2

us4€ dry t26

|lg/lq dry 632

ldlq dry 632

pS4qdy 126

ldkS dry 632

tdrq dy f,3.2

tidks diy 63.2

lig4qdy 632

lgre dry 63.2

pdksdry 632

U94q dry 126

tdks dry 632

lql€dy 632

lCl€dy 632

pg4qdy 6il2

E/r€ dy 632

wkg dy 632

fgnq dy 632

lglq dry 632

fdl€*y 632

Mq dy 6il2

pC4q dy 632

pg,lq dy 632

!S4q d.y 632

tdEdy 632

ldrq dry 632

B4qdry 632

ldlq dry 63-2

|.€/lq dy 632

fdE dry 632

pglq dy 632

Field exirad€d voc

sw 846 8260€505050

5050

5050

505050

50

505050505050

50505050

505050

50

50s0

50

BRLSFL155

Thi! laboratory Epora is not salid withoat an oathorial signsttne on rte cover page .

. Reportable Detection Limit BRL = B€low R€porting t.imir Page 58 of 154

Page 335: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 336: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F42 2'-4'sA5980l-12

ClientProicct #101 -88

Collection Date/Time26-Mar-07 00:00

MatrixSoil

Received21-MaF07

C4S No, An rte(s) ResuL Fl"g U^i6 1RDL Dilution Method Retr Prepored Awlyzed Bttch Antltsl

Vol.tile Orgrnic Compound3

Volalile oroanic Cor'lolnBPrepared by method SW846 5030 Soil (high tevet)103191 n.Prcpyhehzene1dr,t2-5 Styrene

6SG206 1 ,1 ,1 .2-Telbchloaoettrane7$3,1.5 1,1,2,2-Tetiachloroehane

127n44 Tetraahlooeihene

10&0&3 Toluene

87.61.6 1,2,&Trichlorobenzene

1m-82-r 1,2,4-TrichloDbel1zene7r.!56 1,I,1-Trichlooethane7$0G5 1,1,2-Trichtomehane7S0l-6 Tri{t ooethene7tt9-4 TrijhtorottuoometEne (F€on j 1 )sG1S4 l23-Tichloopropane

95€-6 1,2,{-Tirn€frytbenzene108-67.S 1,3,5-Trimehytben2ene75.01-4 Vinyld oride1@,2{17 m,Pxylene95,176 exyl€nelossss Tetrahydroluan8G2s7 Ethyl ether90445{ Ten{m9 mehy' eher6fl/-Vr 3 Ehy,l lertt0tty1 elherl08.al3 Di-isopropylelher

75.654 Ted€ubnot/ buyt atcohol12'sr 1 l+0ioxane

46n-''J4 4-Btanonlo@hnzene

&37-266 Toluene4S

tTMal4 1,2-Dichbtoethane44

18fl.53-t Abrornonu,rcrEllwe

Oxtrrctehle Petroleum Hydrocrrbons

Edractable Tolal Pelroleum Mrocarbons

Prepa.ed by method SW846 35504

mo$l.g Gasoline

68{7F30-2 Fud Oilt2

a!ftt-31-3 FuolOil t4

6€554|{0-,r Fud 0( t6ti)9000{E() Moloroil

$0100000 Aviation Flel

Unidenulied

ohef oil

Total Pelloteum Hydrocadons

C9{36 Aliphatic Mroalrtons

jB1,6ip2 l4hloe&ladec4rg

Senrjvolrdle Orgroir Compolnds by CC

Or@nod orine P€slicies SW846 PO81A

Prepar€d by merhod SW846 3545A

tl9{}2 Atdrin

8RLBRL

8RL8RLBRL154BRL

BRI-8RL8RL8AL

BRL8RL

8RLBflL26379.7BRLBRLBRL8RL8RL8RL8RL

98t0t99t09

BRLBRI-BRL8RLBRL8RLn6Calorhted asTt6n6

2U

lykS ey $2

ldkS dy 632

tdlq dry 53.2

ldkg dry 53.2

tiS^S dry 632

!g(S fy 632

l1g^S dry 63 2

!S/rS dry &32

lscs dy 632

WkS dy 6:]2

!s,rs dy 632

!S& diy 63.2

F9CS dry 63.2

l€/rs dy 63.2

llg/rs ry ff2

!g/tg dry 632

!s4q dry 126

t€frS dry 612

!s/ks dry 632

|rg/kS dry 632

I'S4s dry 632

tS&g dfy 632

ldrs dy 63.2

llgAs dry 632

ldrS dry 1260

70-130 %

TEtg%

7Vt@o,L

70130%

iWrS dryrhg4g drynsfts drymg/rg drymses drymElS drymg,tS dryfilglq dryxrgltg drymglq &y

4+144%

pdlq drv

sw 816 82608

+CIEIPH

50

50

5050505050

5050

5050

50

s0

50505050l0

02.Apr{7 O2-Apt-07 J040017 n^l

29Maf-07 30-Mar-07 7031773709

709

7m7m7og

709

709

709

7Cr9

709

BFL sw&{5 80814 28-{,lar{7 02.Apr{7 7031739

Thk bbomury repoa is not wlid tlithoct an aurtoisd siF',ature on tha coyer page.

* Reportable Detection Limir BRL = Below Reporring Limit PaBe 59 of 154

Page 337: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMtF42 2'-4,sA59803-12

Client Proiect #30t-88

Collection Date/Time26-Mar47 00100

Mat.ixSoil

Received27-Mat41

CAS No- Analyte(s) Resuk Fhg A n s *RDL Diluian Method ReJ, Peparcd Atblwd Ealih Analyst

Semivolatile Org.nic Compoo||ds by CC

orqanod{odne P€slicjdes SW846 q}€1A

Prepared by method SW846 35454

3|9-0,r-6 a_Bl-tc

i1986-? b€lr

3198&S d.gHC

s8se g-BflC (tjrdane)

st-1+s Chlordano

n544 41.DDD (p,p,)

z-55s 4,{-D0G (p,p')

ss2$3 4,4-DDT lpr)6Gt-i Oslfin

Etltossualr I

$e19H E rdodjlfrn ll161.07-8 EdGjhnSuttale72.2GB Eddn7€l'g-.1 El|llin Alt€fiyde7614-8 Heptad{or1213.a l,l€ho4d{or102r'r3 l-teptad{orEpoxid€m01.352 Tox4lE06

510971.9 a.Chlordare

$8S34? g{hbdfle

5349+705 Endrin K€0one

1'3fd4+2 4,+Dgadatundiptvt4 (St)

d6te+i Decd otilirlBv (e)

Polvd*riEted Eiohenvis bv SW846 8082

Pfspared by method SW846 3545A

126?+112 PC8101611rO+2&2 PC81221fit,{1-t65 PC81262

5346921,9 rcB 12421262.2$6 PCB [email protected] PCg 1254nc6.02.s Fc8 t260tnz+2cs Pc8l26211r@r4-4 PCB 1268

lwta-z #4v4M@tiliptBnl(SlNt'21-t Mlbnbiptvrlt(Si

S€mho|'dlc Orgrtric Compounds by GCMS

Semivotade Oroanlc Cofipoonds by SW846 eB70C

Pr€pared by method SW846 35508

s+34 9 A.a0aphh6no

2n&960 Aae|taphtrylsr€€a 533 Anihe12G12.7 Andreno

t9r2-2't4 Arra&€

1@393 AzobdEeieDiphenyldarine

s2fi-5 Bsuirine

5&55.3 E€nlo(al?'ltfeie

BfiLBFL8Rr-BRT8RX-BRI.BRLBRLBNLBRLBBLBRLERLBfrLBFLBRL8RL8Ft-8RLBRLBFL

IN

BFLBFLBRLBRLBFI.BRLBFLBFLBNL

7595

69.1

69.1

6S.1

6S.1

69.1

6 9 t

€9.1

69.1

63.1

wlgdryudrc dv!cI{ dv

|lg}S dry

ldks dv

ab dv

|dredYrdrg dvpdkg dv

lgrs dy

ldrg (y

NTq dYpsnq dY

$/tq dy

|Js4(s dv

!S/ko dry

ldt0 drypgrg dv

P9& d'y

usrq cvIEt{ 4}

a>lfr%f i 150%

!s/rq d]

rj94q 4'!g/kg dry

|lsfrs dv

|dh dy

rob d'Y

|Jgrsdvlyts trY

!s4q fft

*tq%gyfi%

swE4{J 8081A34.5 1

34.5 1

34.5 |

3 l r

t n l

34.5 l

34.5 1

34.5 r

34.5 |

341 |

345 |

34.5 l

34.5 r

31.5 1

34.5 |

345 I

34.5 1

t73 1

34.5 I

3,{.5 |

34.5 |

sw816 8082 2&tl'J47 30-ttar'07 7061738 s

zS-l'ls{7 FApr{T ru31?4 M.BBBL

BFL

BFL

BFL

BFL

8RL

8RL

BNL

|dh dv

$llqdIpgrq dY

lqh dv

ldis try

tdtqt'lugnq dy

|ldlqdv

swB45 8r/0C8€0 t

880 1

880 1

880 |

EEO 1

EEO 1

&t0 I

8 & 1

This labotutory rcpo b ^otwlid wAhorn an auttotized siF tzt,lre ott lha corer page.

. REport"ble D€tcction Limit BRL = Below Reportiog Limit Pag€ 60 of 154

Page 338: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole [dentificationM8F-t2 2'-4'sA.5980l-12

Clielt Proiect #301 -88

Collection Date/Time26-Mar-07 00:00

MatrixSoil

Rcceived27-Mar01

CAS No. Anab,e(s) FloS *RDL Dilutiot, Llethod Rel. Prcpltrul ,lnalyzed Botch Atutttst

Scmivolatile Organjc Compounds by GCMS

Semivohtile Oroa' c Cohpounds by SW846 82i0C

Prepared by melhod SW846 35508

5032{ Benzo {a)pyrcnez0+r13.2 &nzolb)tuoranhene11'1-24.2 Belzo {g,h,i) perylenem1489 Be$zo {t) fluoranifiefle8S05{ 8€nzoic acid1llc51{ Bonzyt atcohol111-91-1 8is(2doroelhory|mehanet11{e 8is(2,€hlooethyl)ether3S63!-324 8isi2-chtoroisoprap!4)elhcrt174t-7 8is(2-ethylheryt)phttEtate10r6s3 4-Eomoph€ny' pheny,i edrerE 6&7 &Iytbenzyl phhatate

F74-! Cadazole5960-7 +Chtoro-3-mehytphenot106-{71 4.chtoroanitine9.58.7 zchloroiaphlhaleoe96.57-6 2{hlorophend700572 3 4-Chtomphenyt phenyi eher2r8{i4 Ch.Fene597G3 Dibenzo(a,h)anthrac$e132+4.9 oibenzofirran!,5sGi t,Z-DicfitorobenlenesilrXll j,3-Dichlorob€nz€ne

lo64tt7 1,4-Ddorobenzene913.4.1 3,3-oicltoobenzidine120++2 2,4-Ddorophenolu{62 Di€ttryl phlhalale13n!1-3 DihBftylphlhalate105-€79 2,4-Ome',h!4phenols-7t-2 Di n,butyl phthatale53,r-s2-1 46_Dinjtro-2-rnethylphenol51-28-5 2,4,Dinirrcphenol121.1+2 z,4-DinitolotuenesF2o2 2,6,Dinitrotoluensr17-&r4 Di-0_octytphtfialat€a,6r4{ F|uoranlfcne

€&737 Fluorenet1&7+r Herad oob€flzeneAr-6&3 Hexacljorobuladi€ne17471 HeracHobcyclop€nladieno

67-72-1 hetaClioro€fEnelt+39-5 InderF(j,2,$cd)pyrene

90.12{ l{,lethy'naphlhat€n€7&59-l ls4phorone01't_6 zlvlelhylnaphthaten€s6r8-7 2{dnylphenol

t@39-r, g,4-M€hlphenol106-{+591-a)n NaphthaleneW74-1 2-Nihoaniline!1941"2 $NitrDanitm

BRL

8RL

8RL

8nL

8RL

8RL

8fr1

BRL

BBL

BBL

8RL

ORL

BRL

BRI

8RL

BHL

BHL

BFL

SFL

SFL

BRL

BRL

BRL

8RL

8RL

BRL

8RL

BRL

BRL

BRL

8RL

8RL

8RL

ERL

BRL

BFL

BFL

BFL

BRL

BFL

BFL

BRL

BFL

BRL

BFL

BHL

BBL

BRL

BNL

BRL

!S/rS dry

l]drS dry

|/dlq fiv

lglg drypdkg dry

uC/rS dy

|rs4(sdyUS4q dry

!S/kS dry

llgl(s drv

lsts diy

LgfrS dry

lgrq dry

lqkg dry

!!t& drvpdkS drypgro d]

|lgrs dvpglq dv

UgtS drypdks dry

rc,tS dry

!91s drypgKq ory

ldks drypg4(S dry

udts dry

udlq drypdq dlypotS drypskg dypg/ks dry

l,94(o dv

|Js4(s dy

l,gksrv!C4e,tyISAS dry

!C4(S dry

!04(S dry

!q4(g dry

!4rs dry

tqwfit!g4q dv

lqrs fiv

$/fS dly

|ls/rsdlyArc ev

rdl€ dy

ldks d.y

A& dv

880 1

880 1

&t0 l

88{ I

880 1

880 r

880 I

880 1

8€0 I

880 |

8€0 1

880 1

880 1

8 m 1

880 1

EEO 1

660 1

E60 1

E€O I

880 |

880 |

880 1

880 1

880 1

880 1

880 1

8EO I

88{r 1

880 1

880 1

880 1

880 |

880 I

880 1

880 1

8E0 1

8Al 1

880 1

880 1

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8€0 1

880 1

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680 I

880 1

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sw845 8270C X+lar-l1 03-&f{7 7031774 M-8

Ihk labontory ?epo Lt not valil withaa an outhorir?A signatarc or the covr pzge.

+ Reponable Detection Limit BRI- = Below Reponing Limit Page 6l of 154

Page 339: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiotrM8F-42 2'-l'sA59tol-r2

ClientProiect #301-88

MatrixSoil

Collection Date,/Tirne26Mar-o? 00:00

Reoeived21-Mar-07

CAS No, Anrlyte(s) Rdr&t Flag Uni6 *RDL DUBtian Method nej PEpared Analyen Baftl, Analfsa

S€mivolrtile Orgrnic Compounds by CCMS

&nitolaltl€ oroaric Compoonds by SW8,t6 8270C

Prepared by mehod SW846 35508

100{15 {-{ifoenilire90 9r3 lfircbeu€n€0&7s-5 2-flitophenol16{2-7 +Nitrfhsndu-7$9 J\ll{ltlsoditrEhy{anne@lt+7 ltt$lrcsodin{rEpyantne8F30-6 $Nitos(dohengdnirE87{66 Pentacilooph€nd

8601{ Ph€nolhcn€1{,8-95.2 PtEnol129.00{l ry€rle110's5r PFdne1!182-1 12,+Tritoobenzenss!E-4 2,4,$Tdfloophend881162 2,4,STli*boph€nol

plat 2-Fl/lt.,iphenfl

3f,z-121 z-Fhsqlwd

4165504 ^I'tfuEelte4s

1t65@-2 Ffa.nt4s

171&514 l6tpl}3,ntl44

11e794 Zl,eftbwnophend

SwBl6 8270c ?s u{' 0&lpr-07 m81774 M.8

Sw8167471A @.AF€7 GIApr{7 7031810 YP

EPA 2m.7 024pr.07 02-Aprfl 7ulmg HB

S|V84E 1312 2&Uar.07 Ansr]Ir 71131763 B0

SW846 1312m108 30.ilar{7 m.Ag{7 7ml&5 t-H

BFLBRLBRT8RLBRLSBLBALBFLBRLBRT8RL8RLBFI.

BFLBFt

&7363n5t)

lglS dr 3520

!g,iS dy 880

ryb a 880lS,l€dy 3520

twet 880

|,grs dy 880

IEr96y 880

ljg/}S dry 8€0

lS,rc &y 880

tlg/lg dy 880

EYbdry 880

lcngdl 800

Nlqdy 880pgrq dy 880

!g/rg fiy 880

fr.l30%t5-u031}r30%trl t0%&rg)%1rt10%

'tvts dry 0.ffi2

mYrS dry 1.10

mdtgdl l.5s

tidks dry 0 551

mq^g dry 0276

r'01q dry 0-551

ndrS dry 0.&7

mo4qdry 1.65

rng.l 0.01m

nrdl 00150

mg4 0.lxl50

mg]| 0.00e5

'rwr 0.0125

mgl ojflXo

rr$,l 0.0075

rngl O01s0

sw84613r2?170A

sw84li 131260t0€

Tobl Met b by EPA 6mO/7000 Serier M.rhodj

?43!l'97.6 ilerWry

Tot l M€td! by EfA 200 S€rie3 Merhods

+e4 sifuBr

t!l(rg2 ABeric

7'!{G3+3 Bdium

74/(}499 CadDium

r4tfr4J.3 Cltunium

7$F92n bed

nV4U2 S€l€nium

SPLP Metlls by EPA lfl2 & 6000t000 Serter M€thods

SP{-P Ertadlon Compl€N€d

711r'J-?44 Slv€r oFL

tr10-l&2 A6enic BRL

z.rtll,3g-: BaJilh 0.tB&

7,!{)4}9 Cadniwn BRL

74li}.|7-3 Otomilm 8RL

7'139976 lil€Gry 8AL

7'13$92r Lo€d BFL

7t&4-2 Sel€nfum BRL

G€nersl Cbcmtuky P.trmeter'

%Soh(h 88.9

' {P.l{r{7 70S1806 YP

' 02.4F{7 ru3rgl5 tR

BNL

795

l m

0 58.1

11.7

366

1

I

1

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l

I

I

1

1

I

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1.6€

Sfl2540GMod. g).llar{r7 3&rNar{7 7[01S/9 Ytt

Thit labo.slorf report Lr ,.ot wlU withord an authotlzrl ignsturc on thz cove, page .

' Reportable D€t€.rion Limit BRL = Below Reporring Lioil Page 52 of | 54

Page 340: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdertificationMtF-43 2'-4,

sA59803-13

Client Project #30t -88

CoLlection lJate/Time26-Mar47 00.00

MatrixSoil

Received

21-Mat07

CAS No. Analy.e(s) Resalt FtoC Iinils *RDL Dilutbn Method ReI PrcpoAd Ana4zed Bdch Anabst

Volrtil€ Organic Compounds

VoC Frlraclion

Volalile orcanb Comoolnds

F 6ld exlBd€d

Prepared by method SW846 5030 Soil (high tevet)

7t1+1 1,1 2-Tichlorotnlluoroehan€ (Frcon BFL67-6rr Acetone 8RL1mr31 A.rylmirr e 8RLn 41-2 Benrene 8RL108-86.1 Brcdnobenzene BRL7497.5 Bdnmhloaomelhane 8RL7'214 B{Emodichloomelhane BRL7t 2 Bomolortn BRL7l-83.9 Bromomelhane BRL7843.3 z-BL{anone (MEK) BRL1o,r5l{ n-Bulyibal2ene BFL115-9S4 sec-Butyhenzene SFLsl{6$ Ed-Bulylben?ene BRL75.rfi Cabon dsufiide BRL5S29s Cabon tet€chtorid€ aRLlll&90'7 Chlorobenzeno 8RL

zE-Marfl z&Mar-o7 7031767 80

oz-Aprfl 02 Ap/{7 7040017 mar

BRL

BRL

BRL

BRL

8RL

8RL

8RL

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BRL

BRL

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BFL

BFL

BRL

BFL

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EFL

BFL

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BFL

BFL

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BRL

BRL

BRL

BFL

BHL

BRL

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BBL

BBL

BRL

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61.5

r630

8J.5

81.5

81.5

81.5

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103

Er5

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40€

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81.5

81.5

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50

50

5l)

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50

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50

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50

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50

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50

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5{)

50

50

50

50

50

50

50

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|Jdrs dvpgfrs dypgxs dvpgrq orv

lgrs dry

ldrg dry

lglS dryps.4s dry

lStS dry

Udlq dry

U$4rS drypStS dry

!g4q dry

uofts dv

U0,1q dry

ldlq dvps/xs fiy

lgh dry

!S4q dry

lVrS dry

!S.4(S dry

uS.4S dry

|Js4(sdr/!S4(S dry

!S,4S drypdkS dry

lgtS drypS/xS d,ypsng dry

$4q dry

w/kS dry

|gk! drv

tErt drypdks dry

ucfrs dry

udks drypS4q dry

UofrS dry

udks dy

lots dy

lsnq dvpdlq dyps,4q dy

uc4(s dy

!dr(s d4'ps4(s dl'

tiSfio dyps49 diy

lls4s flv

voc

sw 846 82608

75{G3 Chlorcethaner-6e3 Chloojofln71nL3 Chloaomelhane95.{9S 2€hlorololuene16{l-4 4{hlootoluene*12{ 1.2-Dbmlna3-dloropropane124.48r Dbrornochloomehane10ssg4 1,2-Obromoelhane(ED8i7,1€+3 Dibromomethane9+5G1 l.2-oichtorobenlene

5{r.?}1 l,}oichloroben2€ne106-467 1,4-oichlorcbenzeno

75.710 Crid orodinuoromethang (Fleofl t2)75.343 11-Dichtoroethane

1O-0e2 l,2-Diclooettlane7+114 l,l-Dichloro€lime156-5!,? os-i2-DtdtloroellEnerso5 l|ans-Il-Didoro€lt^€ne1g-s7s l,2ochtoropropane142.ws l,Soichlooprooane

504207 z,z{ichloopropane56+58$ I,Ioiohloopmpene1006r{r.5 cis-t,3-Di.hloropropene10061{2-6 l€ns.1,3-gdoopropene

1m-4r-4 Ehy'benzer€

8?683 H€xe€ilorobutadienesr1-7e.6 2+t€ranone(MBKIs-82-8 lsopropyb€nzenes-rrJ 4-hopmpyltotuerc1d34{4.4 Methylten-burylethe{10&101 4-n4ethy,t,2-penlanone(MIBK)75492 u€hyieaechtoridesr?o3 ftaphhaten€

Thb hborztory rcpod is not tqIU r,ilhod an sqlhoriz?y' signdurc on lhe coler page.

'Reportable Detection Limit BRL = Below Reporing Limit Page 6l of 154

Page 341: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiotrM8F-43 2,-l'sA59803-13

Client Proieot #30t-88

MatrixSoil

Rec€ived2"1-M^t-07

Collertion Date/TimezGMaFO'l OO:OO

CAS No. Azaly.e(s) Resljll Fhg UaUs 'RDL Dilution Method Retr Prepared Attalfzed Batch Anausl

Vohlile Orgallc CompoudsVo{a$e Organic Compoundsftepared by method SW846 5030 Soit (high t€vel)r00.6s1 n-Prcfl&enzene B8L10c1t2-s Styrera BFL60020{ l,t,t2.fetlachtoroslhane Bn[79\345 1,13,2-T€trachbrodnan€ BRI-'t21 184 Tetrsd o|ehen€ 8FL108.8+3 Tduene 8Fta/{l-6 l2,}Trirlrlonbenzene 8RLr2o{2 r 1,2,+Triilorat€ru€ne BfiL71.55.6 1,1,i-Triciloroehal1g BRL?94G5 1,1,2-Tlit ooetEns B8L790.6 Trid ofoehene B8L75'6k TddllorDlfuorofEfiane (Fl€on 11) 8FLsro_'l l,2,gTridloropropdle BRL9+6+6 1,2,4-Tirnerybenzene BR-1lIf67.ll l3s.TnrEfrtl/benzene BH_7+014 Vinytdltor*l€ BRL133+2G7 m,pxyt€n€ 8FL9sr74 oxylene 8ff1to9 9s9 Tetrahldmlu€n BFLtu2vr EUMet|el BFL994-05e Tenrnryl metiyl eh€r BRL&t 92,i Etryt t€dtlty eher BRL10&203 Di-isoprqyt etie. 8Rt-75-€s.0 T€n-Butand / hJM aLohol12$91-1 l+Doxen€

4&@Er +Brcnofrtoobenzene2@7-26-5 Tduerc.d€17M$074 l,zaidtdodlane4t186e53-7 DlbatpfllDdnetlane

Extrcclrblc Pdroleum Hydro€{rbons

E(lrachbls Total Polrolsrm l-fudl€aftoisPrepared by mEthod SW8,f6 35508em6.6r'9 &sdine6847+3C2 FFtod 1268r7$31n FlF| oit #tr68s63{0.1 Fuetot t6m€00mo MobrolJ0010{1000 Aiaton Fuel

{hld€rnifi€dOtE OlTolal Potrcleum HydocatcnsC€436 Aiipialtc Hydroca.bons

Senrivolrtile OrBrnic Compounds by cCorcanod{odn€ Pestdi€s SWB46 0081APrepared by method SW846 35454O94G2 Ahdn

B&8RL

971021@1 t 1

8Fr-BFL

BFL

BRL

BffL

BFL

BFL

BRL

BRL

8RL

lvls trvloaq ryldh ey|dh evE/l€ fiV

|4ls dry

tlq dry

Ug,lq dV

ldks dv

$rq trv

uqks ey

arc rvldl€ dvpg|q Ar9l€ dv

lrylg dy

|Jgl{ d}

lgrq dy

!g4s ry

!S/rS dry

$& dv

ljdlq dvpdqA

ll9t9dvt4r€ 4y

7&1fr%7ttil%7Gt30 %701$%

mgaq drymgrS fymdks dyrrM{ drynul€ dry|rBr€ fiymdb d'yngnq d'yr'9,1q dryorS,lq dy

4+140

sw 846 826{E

+Cr EIPIJ

8r.5

81.5

61.5

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8 1 5

Et5

Br5

81-5

8r5

€ 1 5

EI.5

8 1 1

811

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81.5

r63

8 1 5

8 1 5

81.5

81.5

815

8r5

8r5

t6B0

7 1

7.1

7-1

7_1

7_1

7.1

7.1

5i)5050

50505050505{t5n505050505t)50505050505050505050

m"Aprfi 02d[f47 704m17 mar

29-il€r{7 3l}t{al1)7 m17,ts 0S

BFL |r'cretv sw4| alSta z&ilar{7 02.tur.07 ?t31me

Thtrt labotuory relNt l is Eot vrIU pt&to.d oE cttthadeil s,gnatarc on the corer page .

. R@rtable Detection Limit BRL = Below R€poding Limit Page 64 of 154

Page 342: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldenlificationMtt-4r 2'-4'sA59803- l3

Client Proiecr #301 -88

ColLectio1l Date/Time26-Mar07 00.00

MatrixSail

Received

27-I./:a(07

CAS No. AnaIyuG) Resall Floq anib *RDL Dilktbn Method ReJ Prcprcd Analyed Batch Analyt

Semivolstile Orgrhic Compounds by CC

Oroanociiorine Pes[cides SW8{6 8081 A

Prepared by mettrod SW846 3545A

319-8{-6 a-BFIC3r+85.7 b.8HC

3rs€68 d-8ftc

58-8+e g-8tc (Undane)

7-1rq Chbrdanen543 4,4!0OD (p,p)/25s s 4,4,.00E (p,p')

5q293 4,4'O0T (p,p')qlt 1 oiddnn

s5F96-€ Endac{llan I332i+8tg Endosullan lli031{7+ End6ullanSuttaten-&4 Endin7r12t,93-4 EnddnMehyde76_.4_0 Hep|achto(72-r9s irethorycitor102+57.3 Hepiad or Epondesnor.352 Toxaphene5103719 a-Chlordan€ss663rr-7 gthlodane

534S+7C5 €nddn Xeton€

10f8eu.2 44.08-(Xhllwtobiphenyl(Srl,,61-2+3 Decaclfurcbiphenyl(si

Polvd odnatod Bbh€{vis bv SWP,46 e,082

Prepared by method SW846 3545A

12t74||-2 PCB 1018

1110420 2 PC812211fl.1-r6.5 PC812325316e21-e PCB 124112672.4.6 PC812481r097{s1 PCB 1254110${25 PCB 12603l@l-ri$s Pcg 1262111$14rt PCE 1268

1ts'641.2 4,4-DB-Octafluot&id6nyt(Sl

MtZn oecacflonitliphertyt(St)

Sehivolatil€ Orgaric Compounds by CCMS

Sed lalaltle O.oa|lic Conpol,nds by 5141846 8270C

Prepared by method SW846 35508

m-324 Acsnaphh€nsa{}*8 Ac€naphhyl€n€@-53.3 Anrfin€120-12-1 Anthlacen€1912-2+9 Altazhs1&s.7 A.4ben.f]rctapherytdezirc@.!7-s &nzidinese5+3 8€fzo (a)anhracgn€

BBL

8BL

BRL

BRT

BRL

BRL

BRL

BRL

BRL

SRL

BRL

BAL

BRL

BFL

BFL

8FL

BFL

BFL

BRL

BRL

BRL

u97

8RLBRL8RL8RL8RLBR]-BRL

BRLBRI.

70g)

39.9

399

3 9 9

39.9

199

39.9

3S.9

33.9

39.9

39.9

39.9

399

39.S

39.9

39.9

399

39.9

r99

39.9

3 9 9

399

!S.4(S dry

lsts dy

pSIq dry

$4€ dry

!g4q dry

ldks dry

tdkS dry

tidks dry

Irdlq dy

lgks try

!s4(s dry

!g4q dry

lig/tg dry

lSrtg dry

!9lS dry

lsilS dry

!s4(s dry

lVkS dI]/

ldks dry

trs,ks dry

t44(s d.y

3Et5A %

+t5a%

!S4q dry

ldlq dry

!s/kg dry

lEtq dry

lErq dry

uslq dry

ug4q dry

!S4q dry

tiC4q dty

&150 %

38150 r,

SWE46EOSIA

sw846 80€2

sw846 8270C

l

l

l

l

I

I

I

l

I

i

I

I

I

1

l

I

l

1

1

2t-i,lar{7 @-Apr'07 7031739 TG

28-Mar'07 30.Mar'07 7031738 SM

29.1,1ar.07 03.AVl7 1$1n4 M.B

79.7

79.7

79.1

79.7

79.7

79.7

19.1

19.7

19.7

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

pg/ts dry

Ps4q dry

us4q dry

Psfrs drypdks dry

WkgdPluS4q dty

Ug'k! dry

886

€86

8€5

886

886

d€6

886

886

Thit labontory rcpod is not valid tpitkoul an aartorized signzta.e on the coeu page .

+ Reportable Detection Limit BRI : Below Reporting Limit Page 65 of 154

Page 343: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-13 2,-4'sA59803-t3

Client Proiect #301,88

MatixSoil

Received27-Mar-07

Collettion Date-/Time26Mar-07 00:00

CAS N^ Analyt (s) Resl,lt FIag rRDL Dilabn Method Rel Prcpared Analfzal Bslch Analfsl

Semivolartle O.gonic Comporrds by CCMS

Semivolalil€ Oroanic Comoolods bv SW846 8270CPreparcd by m€lhod SW846 35508

5o{e-0 Bslao (alpyrens

2o$9e? B€{zo(b)fuoranthene1912+2 Benzo (g,h,t) peryten€

nr.@A Benlo ft) nuonnhen€66-854 EenZOiC add10o5r G 8en4,l alcohol111-9rr &5(2dtroeliory)mehan6't114-a

Bis(2{itu,oehyl)dlEr

396!8-32.9 gs(2dloaoisopr.o0ytle$e.

1lr'81-7 Bis(2€hy'he4)pnhatab101-55n 4-Bomophary'd€nyleh€f

c56&7 Butyl b€nzy' pnthatab

8e7+6 Cab€roles9so'7 4{hlora}meqlphenol

106-47{ +Chloroanlineel'58-7 2{hldonaph$do|e

s57-o zchlo|o0henol7tot72-3 4.ci orcpnenyi phenyteher

213i1.9 ChrFen€53?Gt Dh€mo lAh) anthra.ene13e-6+9 Dib€{Eofuran

9550.1 1.2-DdOobenz€rE

5417?t 1,+Ddtoobenzen6

loc46'7 1,4-0idio@benzene

91-941 3,3-,DicHolohenzijne1m4.'2 2,+0ii* orDpt€ml&{4, Diedvlphthatats13111.3 oiftElhy'pnthalate105.67-9 a+Dmdrypn€iol*1+2 Di+tw phhatats

53.1-52-1 4,&DinftD-2-rnethyiph€iol

51'2&5 2,4oinitEphenol121-t+2 2,4-oinitobluene6oFaE z,&Diititobluenerl?.€4i orn-odylphbatats206-,rrr{ Ffuorfl sn€8e7+7 Rlor€ito11t7+1 H€xidbDbenzene

6/-083 Hexadroobutadione

n44 Horac+{oEcyclopentad€n€

6l-12-1 HoEd orc€lhaners3e.5 Indeno {1,2,3{d) pyrsle

sl2{ l+r€dtylrBphfid€.et859.r lsaphoron€91.5r.5 2+neftltEdffidele

95-1&7 z.lre[ulpidld

100-30-,1, 3,+Mehylphenol184591.2c0 Naphhal€n€0&7r-4 2-Nitroarihe99{s2 }Nitbanifne

B€L

BFL

BFL

BFL

8FL

8FL

8FL

BFL

BBL

BFL

BRL

8RL

8Rr.8Rt-BRLBFLBHL8RLBRL8RLBRI-BRLBRLBFLBRLBFLBRL8RL8RLBRL8FLBRLsRtBR!BRLBRLBRL8FLBRL

8Rt8RLBNLBnIB8LSFLBRLBRL

BNLgaL

BFL

udks d]

!g4rS d)'

!s4s drv

|ldh dv

|a4€ A

uglq dv

|,grs dl

dkg trv

udks dy

ljdiq fiv

|rylq dv

tigr€ dy

lsls dv

wh dr

ldlq dy

wrs dv|lgh 6v

|Jgredlv|lglqdyu$S ny

wro fvlqlq fr|'

!91€ fry

t4b dY

I9tq dy

WYS dY

lgls t)'

lgks mv

lgrc eY

llgb dv

t€/rg dry

rc,!€ dtY

ugr0 dy

|dlq dl

!049 dl

$ng dv

l{/t€ dy

lo4qdv|lglqdvllsit(g dl

rgtg ry

uEtg dy

Wl4drlt4*4trvBS dry

rcIq dv

uglg dv

!$4q rY

|ldto dry

wt{ dv

886 r

886 1

886 1

886 1

886 r

886 1

886 r

885 I

886 1

886 1

8€6 |

886 1

836 r

886 1

886 1

886 1

886 |

886 r

88lt 1

886 I

6t6 1

8€8 1

886 1

886 r

886 r

886 r

8t6 I

EE6 1

8E5 1

8E6 1

8€6 |

8116 r

886 |

885 r

8€6 1

E86 I

E{t6 I

8€6 |

886 I

886 r

885 I

885 i

886 1

886 1

E€6 1

E€6 1

886 i

886 I

886 1

€86 1

sw8.{6 €2?m 2gMBr{7 c+Agr4? ?031774 M.B

This labonJory rqot k aot vali.I Nithoa! a6 althoiac.! tignature on alte cowr Ingc.' Reporrrble Detection Limit BRL = Below Repoding Limit Page 66 of | 54

Page 344: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiouM8F-43 2'-4'sA5980l-13

Client Proiect #301-88

MatrixSoil

Rcceivcd21-Mar-07

Collcction Date/Timc26-Mar-07 00:00

CAS No. Anab.e(s) Resah FIag Irzr'6 'RDL Dilution Me,hud Rel. Prcparcd Aaalyed Butth AMqsl

Semivolrtil€ Org{nic Conpounds by GCMS

Sanivol€tile Orcanic Comoounds bv SWB(; S27OC

Prepared by method SWB46 35508

1c0{1s +Nitoaniline984+3 Ntlbeozers8&7$5 z-mtropheflol10002r +NjtDphsnol62_?5'9 l{-Nitrosodrnelhlanine0216+7 N-Nitmsrdi-ntroFtamine63!_6 l{-Mlmsodiphenylaninen4&5 Peniachtonphenol&01-8 phenanlhrene

100 9t2 Phenol

fio.srl pyidine

12{182 r 1,2,4-Tricl orobenzene695"r a4,s-Tichiorophenol88.062 e4,6-Tichtorophenol

ar$t ZFhMobbhenl

fi7-t24 2-Huotophenol

t16s644 lkLnhenzene4s

41654t-2 Ptpnol4,

t7t6-51i fepfunyLdl4

t1&84 2,4,6.Tdbtoft)phenol

29Mar{7 0}Apr{7 70317/4 ti.8BHL

BHL

BFL

BFL

BFL

BFL

BFL

BRL

BRL

BFL

BFL

BRL

BBL

BRL

BRL

61

ffi

49

68

49

0 362

51.1

2 U

pS4S dry 3910

lYkg dry 886

!/fS dy 886

trg,&g dry 3540

ldlS dry 886

lgre dry 886

|ldre dry E66

ldlq dry E86

pdlq dry EE6

lgr€ dry 686

N,4(S dry E€6

pdlq dry 886

pdkS dry 886

pS/lq dy 886

Udlq dry 886

tu130 %

15110%

3+13! %

1u110%

3+1& %

15.110%

nglq dry 0.0391

m/kS dry 129

mS4(S dry 1.9,1

n'dkg d,] 0 647

ndrq dry 0.W

mdlq dry 0.6'{7

tlgt<S dy 0-970

ndkg d'y 1.94

mgn 0.0100

tng4' 00150

fi9,1 0.0050

nrg,l 00115

rnS'l 0.0125

mg,l 0.000{0

mg/l 0(D75

fi94 0.0150

sw846 8270C

swe46 747tA

EPA200.7

Total M€trls by EPA 6000/7000 s€ries Methods

Totrl M€tals by EPA 200 Series Methods

144041 S lver

7t{G3t-2 A6enic

74{0.39.3 Barium

7440-419 Cadmfum

7440-'r?,3 Chromium

7419-92-t tEad

7792.1,!2 Sdenium

SPLP Metsls by f,PA l3l2 & 5000/7000 Series M€thods

SPLP Exlraction Comdeted

ll'lnzl4 Siher BflL

z4r3&2 A/senic 8BL

7,14cx93 Ba.ilm 0.0064

71404!.9 Cadmiur BRL

144117-3 Chmmium BRI

7,F&97-6 llercury BFI

743$92-l Lead BRL

n@4*2 Sdenium BRL

Gererrl Chemislry PrrNmetera

%So4i6 750

0.0530 02.Apr.07 0& pr47 781810 YP

BFL

3.9S

53.4

02Apt-07 H8

SW8461312 2&Mar{7

SwE161312/60108 301'rarfi

sw8461312?470A

s1rvE46 r3l26r)10A

2&Mar-07 7031763 ED

q2-ApF07 rc31805 lR

02-Apr{7 7ff1m6 YP

m-Apr-o7 7031805 LR

Sii254o G Mod 30.iraq SHrcr{7 /03i8/9

This labomtory .epod is nol vold x, haA aB aalhoriaed signoture on the cowr page_

* Reportable Detection Limit BRL = Below Reponing Limir Pag€ 67 of 154

Page 345: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnole ldentificationM8F-,1.t 2'-4'sA59803-14

Client Proiecl #30r-88

Collection Date/Time26-Mar-0? 00:00

MatrixSoil

Received21-Mar-07

CAS No. Afialru(s) Resatl Fhe *RDL Dil..,ion Method Rel Prcpared Analyzet Batch Analw

Vohde organic ColrDoinds

Prepared by mettlod SW846 5035A Soit (tow tevet)

7&191 1,12-Idchlooffiuoroehane(FGon 8FL67-6+l Aaetone BRL107.r$t A{rybnede BRt7t4-2 BsEen€ 8AL100-8Gl Bromobenz€n€ BFL7t97-5 Bo|rtochlololnetrane BFL1tru B|Dlnodidlto|tlr€tlane BRL7E25.2 &unob{m BFi-74{3'9 Bromdnghan€ BFL7e$.3 2_&ranone (MEK) BRLl{l+51{ n-Buldb€ru€ne 8FL1354s0 s€c€'rlylb€nzone 8Rfs€{e6 bd&tyibenzene 8RL75rsl Cafion d&lfide gfiL

s62+s ceitfi tdEchlonde BEL10&m-7 CHombenzene BFL7s+3 drroro€hane BRLr.66.s Cnloldorm BFt7ir€?.3 Ollorofighai€ BRL6{9-s 2-cl olutoiug16 BRL1116-{3-'l +Cfihotdufie BFLs12_8 1 ,2-Dbroot}3drlorcptEpane 8RLraH+l Diirofiodbomehano BRLro6.sH tl.Dbmmoefiane (EDB) BRL7rt-95.3 DboflDm€trene SnL95.561 1,z{ichtorobffzene BFL511.73.r l,}Dtchlcrob€rEene BRL16n6.7 l,ADbhlorotJ€nzen€ BRL7571.0 Didkodi&rordn€thane (Freon12) BRtE3.r3 1,1.Diddorc€$a1e gnl

107{ez l,roidltorc€fiane BFL7535r l,l1oicildo€tler€ BFL1565&2 os.t,2-Did{oroefiene 8RLl5&6G5 ! s.1,2-Ed om€fieno 8Bt7447-i tz-tldlo{opropa'le BRLrrE-zs{ t,}Oichkro$.oDone B8L5o+zG7 2z.oidnoDpropane BFL5631&6 l,tDafildoFopene 8Rt-l@61{r-5 ds-j,310id{orcFopeno 8Rtl@€14e{ taN-1,3{kflo(opmpg1€ BRL10rH1{ Emlb€rusne B8Lsr.6r.3 H€radtorDbdBdiene BFL5€1-78 n 2+t€xsiorE (M8K) BRLs{2{ lEop|lpy6eiz€rle 8RLssar{ +t$oprop}ltoluen€ BFLl6ll.lrlt4 t ettyl tqt b{r9 st|€r BnL108rc1 a_ etryt_2-p$tanon€ (ti{BK) BRL

m4al{1 28-]lra'{7 7ffi1167 BD

29-lMBr-07 z$Mar{)7 7031790 RU

Volrtlle Orgaoic Compoords

Voc Exfadtor

|lg/ts dl 6.0

llgli! dy 120

!91€ dry 6_0

!s4€ dy 6.0

|Jo/l(s dy 6.0

ldkS df 6.0

|4/kS dy 6.0

|dh dv 6.0

Iglq dy 12.0

udrqdy 59.8

ldkg dy 6.0

t4t,Sty 6.0

gdlq dy 6.0

pdtqdy 299

uSIEdry 60

!dk0 dy 6.0

lll/lq dl' 1?.0

|.gts 6y 6.0

ISlq d) r2.0

|lgl|(gdy E0

!g/rg dy 6.0

|lg/kS trV 12.0

lldl€ dry 6.0

!04qdy 6.0

llg/r0 dy 6.0

!S/to d] 6.0

tig+€ trI 6.0

USIqdrf 6.0

l4llq dy 12n

pg/tqdy 60

ldlq dy 6.0

Wh fy 6.0

|4/rS dl 6.0

!94€ dy 6.0

rcre dry 6_0$h0 dry 6.0

lglg try 6.0

l4rS &y 6.0

tdb rv [opg,lqdy A0

|,gl{s dv 60

!S*S 'tI 6.0

$4S 'ty 59.8

pglq dy 6.0

UdkSdry 6.0

|lE},g dy 6.0

lgrs dv 59.8

Enq dy 59.8

$9ey 6-0

Fleld sarad€d vcrc

sw 846 82608

7F0s2 Me$ytene dlbdter,r.2o3 thptfd€no

BRL6RL

Thb labonror!.epon it Nrt eaIld pihout ott aulhoized siAnatart on the cawr poge.

' Refortable D€t€dion Linit BRL = Belotry R€portiag Limir Page 68 of 154

Page 346: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-14 2'-4'sA59803- t4

Client Proiect #301-88

CoLlection Date/Time26-Mar-07 00:00

MatrixSoil

Receivcd2'l-Mar-07

CAS No- Anqbte(s) Flos *RDL Dilution Method Rel Prcpared Analrzed Batch A,rallst

Volrtil€ Orgrnlc Compourds

Volalile oqanb Comoounds

Prepared by method SWM6 5035A Soit (tow tevet)

103-6tl n-Propyh€nzene 8RL1110..2.5 Styrene 8RLaG2O.6 1,1.1,2-Telrachloroethane 8RL793,1.5 1,1r,2-TelGchloro€than€ BRLtn-lg4 Tetrachlooeheno BRLt06rt8.3 Toluene BRLsr-€r.6 1,2,3-Trichlorob€rEen€ BFL1ar'82r 1,2,4-Tichtoroben2ene oRL7155,6 1,1,1-Trchlorc€thane BRL79.00.5 l,12-Tidltoroelhane BRL71413 Trbhboehene 8RL75i9-4 TridtorofluoromethenB {Freof t1) BRL!r&18.4 12,$Trichloropropane BqL95€{ j,2,4-Trinehylbenzer€ BFLr061t7-8 1,3,S_Tdmeltrytbenzene BFL7s4r-.t vinyi dttorde BFL1s'G2G7 m,Fxylene BRLs-47€ oxylene BRLr0es-s Tetahydofuran BRL4.2u7 €$ylelher 8RLes!rc5.s Td-amy' methy4 6lh€. 8RL607{2.3 Elfiyl ten-bjtyl ehef BRL1@-2r!3 Di_isopopyteher BffL75.66.0 Ten-Bulanot / botyt atcohol BFL

2gMa.-07 29-1,lar-07 7031790

29-l'rlar{7 30.r'lar-07 7031773

ugrs dv|,vrs drvrtdlq d'y

t'4kg dry

rdl€ drypdks*ypgrs drv

!91$ dry

ISAS dry

Ps/ks d.Y

ars dryudre dryldks dv

|ldfio dy

tiglq dy

!s,4q dry

ISAS drypC4(S drypg^g dw

|a,tS dry

!94!1dyu94q dryps]|,o drypgrq dypg4(s dry

70,tn%70-t30 %7trt30 %/0-130 %

mdkS dry

n'grq dly

mgeg dry

mdq ey

m$4q dry

mSAS dry

mVlq dry

rigfts dry

mqlo fiy

mS/kS d|y

&t4n%

sw 846 826086 0

6.0

6.0

6.0

6.0

6_0

6 0

6_0

6 0

6.0

6.0

6.0

6.0

6_0

6 0

6.0

12.0

6.0

59.8

6.0

6.0

6.0

6.0

59.8

\m12341'1 1,4-Doxam

1&4).4 +Srcnol|Dobapene

,,37-285 ToiEne-dg

t/ffi474 |,2-Dlchloroethane44

t8@3?7 Dibmnonuovnelhane

Ertmctabh Petroleum Hydrocarbons

Extaclablo Tolal Petroleum Hvdocarbons

Prepa.ed by method SW846 35508

8006 61.9 Gasoline@t?6no2 Fletoil f264176-3r '3 Fuel oil *4686s3-00-4 Fueloil{6|,l]98@0 Motor oilJ10100000 Avialbn Fuel

Unidentitied

Otrer oil

Told Petrdeum Hydrcc€rbcns

C9{36 Aliphalic Hydrccaftons

n8-3t+ tohlo[oxtadecane

SemivolNtile Organk Compoutrds by cC

Oqanodllorine Psqj.idss SWe,46 8ffi JA

Prepared by method SW846 3545A

F{0.2 Atdin

BFL

105

1 1 1

115

BfrLSFL

BFL

BFL

BFL

BRL

38€

Calculated as

388

388

315

{T ETPH65.0 r

65.0 I

65.0 r

650 r

65_0 r

65.0 J

65.0 1

65.0 r

650 1

65.0 1

t4tqdv s!1846 80814 2UnaA1 VAVAT 703173ts

Thk lahomlory ,eForl is nol vzld x'ithorlt aA authoi\ed slg&turc on the coeer page

* Repo.table Detection Limit BRI- = Eelow Reporting Limit Pase 69 of 154

Page 347: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeotificationMtF-{4 2'-4'

sA59803-14

Cliert Proiect #301-88

MatrixSoil

Rec€ived21-Mar07

Collectiop Date/Tim€26-Ma.47 00:00

CAS No. Andyta(s) Ressla FloE Unltl 'RDL Dilation Method Retr. Prerycd AAa4zed Batch Anallst

Semlvolatile Orgrnic Compounds by CC

Oroanodrlodno P€sdcid€s SW846 8081A

Prepared by method SW8,l6 3545A

3l9M{ a€l-|c3198&7 b-BHC3198&S dEHC5&8s{ g-8fc (Undans)

ll-744 Chlordan€72.5+s 44ODO F,p)n15.e 4a ODE (p,p')

5G2$3 d4.0DI lp,p)qltr D€lddnSS.98-8 End6ulan I3lP1+659 Endoou an llr03t{7-0 Endooulansdlat€n-&B cndin7121,93-{ EdrinAldoiyd€76{4-0 Heplaailor72{r.5 irehoryd{or1u2r-5t-3 Hspta*brEpoxjdee0135.2 Toxalhene5103t14 a-chlodane5566-a!7 $& odane5:XS+70-5 Enddn K€ld1s

t@@44-2 4,4-08-6htuhtdiptstyl (Sr)

nsla4.i DeeMeidEwl(St)

Poh&ildinated thrhsrds bv SW846 8082

Prepared by method SW846 3545A

1267+11.2 PCB 10161110+e2 PCg 1n11r14t-tFs PCB 1232534€o"1's PC8124212672.295 PC812481r@7{Sl PCB 125411096{25 PCE t2S03tt 1.2?5 PCB1Z6211t0G1r-4 ru1ft8

[email protected] 4484daflw@En1(54,,5124-3 Dec2dlot&lrtenyt(Si

S€mtvolrtile Org.tri. Compo|rtrd! by ffMS

S€mi/olade oroaric Comodnds by SW846 8270C

Prepared by method SW846 35508

8i-32€ AceiaphtEne

A8€{ Acenedhylsfte62.513 Anjlnot&r2.7 Anthraceae1912.244 Atsazing103ill-3 l"ob6nz€n€,iDilhenyldaznes2474 B€nzidine566s3 B€nzD(a)entmc€ne

2&lrar{7 02.Aprfi rulng TGBBLBRLBRT8RL8RL8RL8RLSRLBRLBffL8FLBFI.8FLORLBRLBHI-BHI.BHLBflLBFLBFL

65t06

BRLBRI.B8LBRLBffL8FLBHLBRL8RL

65tn

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sw846 8081A

sw846 8082

34.5 1

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sw846 8270C 2Sli,l€r])7 0$Apr47 7€1774 M.S

fhb laboralory ,eport is Mrt vslld Eithoul tE zathofize.I sig attft on lhe cowr page.

. Reporlable Det€ction Limit BRL = Below R€porting Linit Page 70 of 154

Page 348: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Identifica(ionM8F-44 2,.4'sA59803-14

Client Proiect #301-88

MatrixSoil

Collection Date/Time26-Mar-07 00:00

Receil'ed

27-Mat 07

CAS Na Anatytets) FI"S Units *RDL Dilution Method Reli Prcpared Amlyzed Batch Ahalyst

Semlvol.tile Org|nic Compounds by CCMS

Semivolatil€ Orqanic Compounds bv SW846 9270CPr€pared by method SW846 3O5OB

5lr?-8 B€nzo (a)pyreiealt992 Benzo(b)tluoranlhene1n.^.2 Benzo(g,h,i)pe04ene20?i)8.9 Benzo(k)fluoranlhene05{54 Benzcic acid100,51€ B€nzylatcohdIII9r1 Bis(2dtloroethoxy)ri€hane1lr-{r!r Bls{Zdfuroethy,l)ethsr3stt8 92 e BE2dioroisopropyl)€tEr117-s1.7 Bis{2€h},th€xyt)phtnahb101_5t3 +Bromophenyl pheryi eth€rel5.G8-7 Bdyl ben4,t phlhatate8&74.0 Calbazote5SsG7 +Chtoru,$methylpt|enolr0fi7-8 4-Chtooanitine915&7 A.Chloronaphhatare&57€ 2{hloroph6ndro0tz.l 4Cruorophenyt ph€nyt eher210-01'9 ChryserDs17e3 oibenzo(a,hlanthEcene132.6+9 DibenzofuEng5.5Gr l2-Dichlorobenzene541-?+1 1,3-Didtlorobenzene106-4$7 l,4,Didoobenzene91441 3,3',{ichtomben?idine1203+2 a4-Ddltorophenol

56.4 Detryt phthatate

13r,t1_3 Dmelhylphhatate10&67-s z,4-oimettrylphenol*14-2 U-n-butylphtlalat€

!!+52'r 4,6-0inrto-2fieihytph€nolsr.28.5 2,4{initrophenol1211+2 2,4{inilDlohreneo6.202 2,Foinilrolollene117-84{ Di-n{d}4phtEtateaG{4-0 FluoEnlhene

11&741 H€nchloroben2me87.6&3 FlsachloDbuladienen17.1 HeEclorocyclopenbdiene

61n-1 Helacl oroetlarc193.1$5 Indeno (1,2,3.cd) pyreno

s.12.0 't-M€thylnaphlhalene

71.59.r lsopt|oone91.5r-6 2-MethytnaphthaienelF,ls-7 2.tethytphenol

108-€9-1, 3,4.Mshylphend106'1115g1-al3 Naphhderc0e74-{ z-Nilroanifin€9t{€-2 }Nitroanilin€

BRL

BHL

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BFL

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8RL

ORL

BRL

BRL

BRL

8RL

BRL

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BRL

SRL

BRL

BRL

BRL

BRL

8RL

BRL

8RL

BRL

8RL

8RL

BRL

BRL

BRL

BHL

BRL

BRL

BRL

BRL

BRL

BRL

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BFL

Msdl

lVtS dry

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uc4q dry

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rc/kg dfy

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!s.*s dry

|lg^g drvpgl(g dry

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801 |

807 |

807 I

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sw8{6 8?70C 29-Mar.07 03'AF-07 7031774 M.S

Thk laborutory Rport Lt dot t'dd withoat an aartoized signatare on thc cover prye-

I Reportable Detection Lim'i BRL = Below Reporting Limir Pas€ 7l of 154

Page 349: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMtF44 2'4'sA5980l-r4

Client. Proiect #l0t-88

MatrixSoil

C-olleciion Date/Time26-Mar47 00:00

Rec€ived2?-MaI-07

CAS Na Anzlyu(s) Resuk FI"S Unia *RDL DilBtioft Method Ref, Prepated Ana$zcd Botch Analysl

S€mivolalile Orgrrllc Compornds by GCMS

Semivolalile Oruanic Cqnmuods bv SWer46 8270C

Prepared by method SW846 35508

r@4r{ 4-Ni!od lne

sct3 Nilrdsl?q|e

0a75's 2+lilodt4holrm{2-7 +Nitrcfiend6a-7F9 N_NiuocodkloryanineEr€+7 N-NiEosodi{.progy'arnine86n0-6 N+litosodiptErylanine

ar{6.5 P€flhchbrophenol

85{1-0 PhemnfiEne108 9t2 PlEnol129-00-0 Pyrerc1'0€Gt [email protected] 12,4-Tt*tfuidba1z€!]lee5s54 2,45,Trichtofoph€mls8-(BJ 2,4,6-Tridofophenol

P1&4 2-Fh-nrdphewt

367-12.{ 2+hffdldnd

4t55-@4 llifunene45

1165-62'2 Pheml45

t71e5t4 fqpwd4

t1&N4 24,6-ftiban@ta1d

2$Mar{7 ()+Apr{7 7(X}1774 M IBRL

8RL

BRL

8RL

8flL

8RfgRL

BFL

BNL

8FL

BFL

BFL

B8L

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57

71

65

d9

0 586

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7.m

16.2

0.461

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1 1 S

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*tg%

1Ul10%

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*13t)%

,r110

swE46 8270C

s1v8,45 t47 tA

EPA 200.7

sw84613r2/t{70A

strs46 1312/60108

Totrl Metrk by EPA 6000/70{0 Se e! Methods

713$97+ MerqJry

Iotal Metals by EPA 200 Seri€5 M€thods

f@44 Sav6r

7.Wf39.3 &iun

7rut 139 CaddLrn

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743+92n Lead

ns24.2 S€l€nium 8RL

SPLP Met.ls by EPA 1312 & 6000fl000 sertes Merhods

SruEftaclio.r comdgl€d

7@24 Sitv€r BnL

7l{+3&2 ,,lssric BRL

71,t0-39,3 Earium Omj4

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1145!,1.3 Ch|unium BRL

7a!197-6 tlelclry BRL

7439 P-t Lead ERL

77te.192 S€t€.'i,rn 8RL

Getrara.l Ch€tnirtry ParaDeaer3

% Solds 90.1

nB& dry O0@6

m94q dry 1.lE

mdtsd'y r.59

mg/kgdry 0.530

mgtgdry 0.266

mg/},gdry 0.591

mElg dif 0.796

mgfg dry 159

rigi| 0.0100

ngn 00150

mgr 0.m50

ngl 0.00es

mga 0.0125

r'1dl 0.m040

'r|gl 0.m75

mS]| 0.0i50

MM41 0$Apd7 7031810 YP

H8

' 02-Arr{7 7091806 YP' mrApr4T TllBlSlXt $

1

I

1

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1

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1

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t

I

SW8461312 284tur.07 28.t ar.07 7031763 8D

Sl'1846 1312/601G 3Glrar{7 m.Afl-07 7031805 LR

slilzto G Mod StHvtaroT 3l.t&r-07 7001879 yli{

Thit labora,ory rcpod it not volid lfithor.t q, asthoriaed signamrc on the couer poge.

r Repo.tnbl€ D€oection Limit BRL = Below Reponing Limit Pase 72 of 154

Page 350: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentiftcationM8F-45 4-6'sA595 r7-10

Client Proiect #101-88

MatrixSoil

Received20-Mar-07

Collection Date/Timel9-Mar-07 00:00

CAS No, Anolyte(s) ResuIt Fl"S Units *RDL Dilatian Method ReJ Prcparcd AnoDaed Batch Anoust

Vol.tile Organic Compounds

VOC ExtractionVohtile Oroanic Comoounds

Field €xt|acled

't77

!g/kg dry 95I

!g/kg dry 1920

Ug/kg dry 95 I

|lgkS dry 95.9

us/ks dry 95 IpdkS dry 95.9pdkS dry 95.9

!g/kS dry 95.9

!g/Kq dry 152pg/kg dry 959

!S/kS dry 95 9pg/kg dry ss.s

PgkS dry 95.9

ugr(rg dry 479

Pg/kg dry 95.9ydkS dry 95.9pdkg dry 192

!S,(9 dry 95.9ps,'xs dry 192

UdkS dry 95.9

lgkS dry 95IpgkS dry 192

lgkS dry 95.9pdkg dry 95.9

lSftg dry 95.9p94(S dry 95.9

!94q dry 95.9

ldks dry 9s.9

lSftS dry 192

!g'I(S dry 95.9pgkS dry S5.S

!/kS dry 95.9pgks dry 95.9

trg/kS dry 95.9pg/kg dry 95.SpSn(S dry 95.9pgKg dry 95.9pdkS dry 95.9

PgkS dry 95.SpdkSdry 95.9

Fg/kg dry 95.9ydkg dry 95Ipg/kg dry 959pg/kg d.y 95I

tgkSdry 959

Fg/(g dry 95 Ipg/kg dry 959

lis.ixg dry 959pdks dry 95.s

voc 21-Mat47 21-Mat47 7031261 BD

Prepared by method SW846 5030 Soit (high levet)76-1x-1 1,1,z-Trichlorotrifluoro€thane(FreoBRL SW84682608 27-Mar1l 27-Ma.{7 7031602 mar676.+r Acelone

107-13-1 Ao.ylonit^iler14+Z Benzene

BRLBRLt8a

l0&€C1 Baomobenzene gRL

11-97-s Broft'o(hlo.omethane BRL15-214 Bromodichtoromsthane BRL75-2+2 Erclnofofm BRL74.43.9 Eromomethene BRL7843.3 2-Butanone (MEK) BRL10+51{ n-Butylbenzene BRLi3t98{ sec€utylbenzene BRL9E{€{ tert.Butylbenzene BRL75-114 Carbon disulfide BRL5F2$5 Carbon tetrachloride BRLt00+0-7 chlorobenzene gRL

75{03 Chtorcethane BRL67{&3 Chlorotorm BRL744f-3 Chloromethane BRL9s49-8 z-Chlorotoluene BRL11164:lr +Chlorotoluene BRL!re12-€ 1,2-Dibromo_3_chtoropropane BRL12{-48-l Oibromoohloromethane BRL106-934 l,2-Dibmmoethane(EDB) BRL7445.3 DibromometfEne BRL95.501 l,z-Dichlorobenzene BRL3i1,73-1 I,3-Dichtorobenzene BRL106.46.7 l,4-Dichtorobenzene BRL75-714 Dichlorodifluoromethane (Freonl2)BRL7+U-3 l,l-Dichloro€tf|ane sRL10746,2 1,2-Dichto.o€thene gRL

7135!.4 l,l-Dichloro€t|€ne 8RL1s&59'2 cjs-1,2-Dichloroethene 8RL1sffiG5 t-an91,2-Dichtoroethene BRL7&1t7-5 l,2-Dichioropropans BRL142.2&9 |,3-Dichloropropane BRLs9{-2G7 2,2_Dichloropropans BRL5eF584 |,'l -Dichloopropene BRL10061{1-scis-1,3-Dichlofoprop€n€ BRLt00€t-02€taarls-1,3-Diclhlorop€pene BRLi El-4 Ethylbenzene BRL07€8-3 H€xachlorobutadiene BRL591-7eo 2-Hexanone (MBK) BRL98{2{ lsopropyibenzene BRL99{7{ 4lsopropyltoluene BRLr63a4H Methyl tert$utyl ether BRLl0e1c1 4-Methyl-2-pentanone(MIBK) BRL7$O$2 Methylene chtoride BRL

50505050505050505050505050505050505050505050505050505050505050505050505050505050505050

50505050505091.2G3 Naphthabne

Page 47 of 124

Thb loboralary report It hol wlid f ilhoul a, thoriazd signetwe onthe coeer page

* Reportable D€teclion Limit BRL = Below ReDortine l-imit

Page 351: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole [dentifrcatiotMEF-45 ,l{'sA595 t7-10

Clieot Proiect #301-88

MafrixSoil

Collection Date/TimeI 9-Msr-07 00:00

Received20-Mar-07

C"4S No- Analytz(s) FloC 'RDL Diluioa Mdhod R.J Prcps.ed Anztyzed Bdtch Anzllst

Vohdle Orgtuic Compoundr

Volotile Oroanic CompoundsP.epa.€d by mettrcd SW846 m30 Soit (high tevet)

75{9-4 Trictrlorof,uoromethane (Freon | 1) BRL

103€+i tuProF,ylbenzene1(10-{2-5 Styr€ne63G20€ 1,1,1,?-Tetsachtoroethane79.3,t-5 I , 1 ,2,2-Tetrachloroethaale12710-4 T€trachloroethenerO€-88-3 Toluene8751-€ 1,2,3-Tridorob€nzene121l€2-1 i.2,+Trid ofobenzene7165"6 I,I,l_Trid oroethan€79{1}5 I,1.2-Tnchbroethan€79{14 Tdchloroethene

sG18-4 l,2,STrtchtoropopanee5€3-€ t,2,+Tdmethytbenzen€'ros67{ 1.3,$Tdmethylberjzen€75{1-4 Vrnyt d{odds13ilG2c7 m,p-xylene95-47€ o-Xyienell)999-9 T€fahydrofuran@-297 Ehyl etiter991-05-0 Tert-emyt methyl €ther637-€12-3 Efiyl ted+ubd ether10&20-3 Di-isopmpy'ether7555rO Tert-&rtanol / butyl alcottol12+S1-r 1,4-Dioxane

sunog,a{a /ecove/lbs.'460404 +EJnmofluorcbenzene2037-26.5 TdrEne4SI 70&47 4 1, 2-Diclldoethane441s6€.63-t Dibrcnofl rbmfiethane

Ertra..Lbl€ P€trolenm Hydrocrrbof, sExbactable Toial Peboleum HvdrocarbonsPrepaEd by method SW846 354546006€1-9 Gasoline6847G3G, Fu€t Oit tt26€47S31-3 FuelOil{t468s6340-1 FuelOit#6[r0!t8oq]00 Motor OilJoolorxDo Aviatjon Fuel

Unidentifi€dOther OilTotral Pototeum Hyd.ocarbonsCSC36 Alphatic Hydroca.bons

surtogab B@vefus:3386.33.2 1-Chlor@dadecane

Semivol.all€ O.grdc Coflpounds by CCO.oanoc{lodne Pesticides SWBi{i EOgIAPrepaf€d by mehod SW846 35508:,09{G2 Alddn

SW 8,f6 82608 27-Mar47 27.{'r'lat47 7001602 marBRL8RLBRLBRLSRL333BRL

BRLBRLBRLBRL

8Rr8RLBRLBRL22499.7BRLBRLBRLBRLBRLBRLBRL

1028992

BRL

BRLBRLBRL8RLBRL203CaldJlated as203203

140

ldkS dry 95.9

$gkgdry s5.9

rcikS dry 95.9pgls dry 95.9

ldkS dry S5.9

|l9ft9 dry 95.9pdkS dry 9s.9

UCftS dry 95.9

ldxg dry 9s.9

!Sn(S dry S5-S

FdkS dry Ss.g

rdks dry 95.9

lcrls dry 95-9

US/kS dry 95.9pdkS d.y 95.9pCrkE dry 95.$pgrsdry 1s2

lrgtS d.y 95,9

t gks dry 959pdtg dry 95.9pdrgdry Ss.g

UdkS dry 95,9

rdtgdry 95.SpSftg dry S59

ldksdry 1920

7d'130 %7G130%lGtfi %76tm %

5050505050505050505050505050

5050

5050m5t)

ngftS dry 46.1

nE/kg dry 4€ 1

mgkg dry {6. I

ntg/rg d.y 46.1

otg (g dry 46-1

rnglsdry 16.1

mg/kg dry /t6.t

nt€/kg dry {6.1

rng^g dry 46j

nElkg dry 46.1

40,140 %

+CT ETPH 22-|hr-O7 26-ttat47 703128,{ DS

BRL lgtg dry 7.74 SWE46 80814 n-M4r47 271iat47 7031275 fc

This latonrorf rcpod is dor wud nAhord arr &rhorizetl slgrulc?c oE thc coeet page.

' Reportable Det ction Limit BRL = B€low R€poftiog Linir Page 48 of 124

Page 352: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F4s 4-6'sA595l7-10

Client Proi€ct #301-88

MatrixSoil

Received20-Mar-07

Colle,{]tion Date/Timel9-Mar-07 00:00

CAS No. Ahalrte(s) Resdt FloC rRDL Dila.ian Method Rel Prcpand Anabzed Bdtch Analyst

Semiyolrtile Org{ric Cohpounds by CC

Omanochlorine Pesticides SW846 8OgiAP.epar€d by method SW846 35508

319{4,6 a-BHC319{5-7 b.BHC319-864 d_BHCs8{9e gFBHC (Lindane)

57-745 Chtordane72-54a 4.4.DOD (p,p')72-5+e 4,4.DDE (p,p.)

50-?+3 a,A-DDT (p,p,)@-57-r Dieldrin95$9€{ Endosulfan I33?1$6S Endosulfan ll1031{7{ EndosulfanSulfate72-?0-€ Endrin7.121-93-{ Endrin Aldehyde7g,r{ Heptachlor724!5 Methoxychlor10445ru Heptachlor Epoxid€E00135.2 Toxaphenesr0$71-9 a_Chlodane55SGl47 glchjordane

s349.1 70.5 Endrin Ketofle

Sunogete |Bco|uEies:

10386412 4,4-DB-Oclafluorobiphenyt (54

20 -2a-3 Decachlorobiphenyl (54

Polvcilorinated Biphonvls bv SWB46 eO82Prepared by method SW846 3545A

1267+11-2 PCB 10.161110+28-2 PCEJ 122111141-165 FCB 12325346+21-s PCB 124212G72-296 PCB 124811497-6€r PCB 1254i109€{2-5 PCB 1260x1n+?6-s Pcg 1262rl lrxr-14{ rcB tm8

Sunogale reotedes:1 @ae8+2 4, logoclef, trc'atiphenyt (Sr)

2t51-2+3 Decachlorobiphenyl (St)

Ssnivoladte orgrntc Cohpounds by CCMS

BRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRL

36

8RLARL8RLBRLBRLBRLBRLBRLBRL

45

UdkS dry 7 t4

Ug/kg dry 7 74

lgkg dry 7.74

lgkg dry 7.14

t S/kS dry 38 7ps/kg dry 7.74

Pqkq dry 7.74

ud*g dry 7.74

Ug/rS dry 7.00

USftS dry 7.74pSftS dry 7.74pdks dry 7.74

!g./kS dry 7.74

Ligt(S dry 7.74

f.ig/kg dry 7.74

P$4(S dry 7.74

UdkS dry 7.74pSAS dry 34.7

Fdkg dry 7.74

PEkg dry 7.74

!s/kg dry 7.74

30-150 %30-150 %

!g/kg dry 15.5

trdkS dry 15.5

Udkg dry 15.5

FS/kS dry 15.5

!g/kg dry 15.5

trEkg dry 15.5

ldkg dry 1s.s

!s/ks dry 15.5ydksdry 15.5

30-150 %30-150 %

FSftS dry 343

!g/kg dry 343

ldkg dry 343

!s/kg dry 343yg/[g dry 343

Fs/kg dry 343

vs/kg dry 343

ldkg dry 343

sw846 8270C

1

1

I

I

1

1

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1

1

1,1

1

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1

1

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1

1

sw846 8081A 22-Mal-O7 27-Ma?O7 7031275 rc

SW846 8082 22.Mat-O7 24-Ma.-o7 7031313 IVP

Semivolatile Orqanic Camoounds bv SW846 8270CPrepared by method SW846 35508

83.32-9 ,@naphthene20&96-8 Ac€naphthylene62-513 ,{nitin€12{112-7 Anthracene1S12-2+9 Atazinet03-3+3 Azoben2ene/Diphenyldialne92{7.5 B€nzidine56'5t3 Benzo (a) anthracene

23-Mar{7 26,Mar-07 7031371 t\r-ABRLBRLBRLBRLBRLBRLBRLBRL

This laboralory tepotl is ,tol wlw vithoat zn authonTed si4nalurc on thc co|er page .

t Reponable Det€ctiol Limit BRL = Below Reporting Limit Page 49 of l14

Page 353: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentiflcaaiotrMtF-45 4i'sA595 t7-10

Client P.oiect #301-88

Mat ixSoil

Rec€ived2O-Mar47

Collectioo Date/Timel9-Mar47 00:00

C"1S No. Analt,e(s) RescU Flrg 'RDL Dilation Aefiod Rctr PQpared AMIWd Batch An&qsl

S€mivol.tne Orgrolc Compo{trds by CCMS

Serni',/olatile Omanic Cornpounds bv SW846 8270C

Prepared by me0lod SW846 3550850-32{ Benzo (a) pyrene2019$2 B€fizo (b) nuorantEne1s1-24-2 B€nzo {g,h,i) peryl€ne207{&9 Ebnzo (k) fluoranthene05€5-0 B€nzoic acidr0o-5r€ oenzyl alcohol111-91-1 Bis(2-chtoro€thory)melhan€tll-aa4 Bis(2-chi.xo€thyt)etrEr3963&u4 Bis(2d oroisopropyt)ether117{1.7 Bis(2-ehy,ltExyt)phhalate101-56-3 +Etrornolhenyt pheny' ethera5{&7 gutyl bonzyl phthatate86-74-8 C€rbazole59-50-7 +Chloro-3-rnethyph€flol10G47{ +Chloroaniline91{&7 z-Chloronsphthalen€95-57{ 2-Chlorcphenol7005-72-3 +Chto.ophenyt phenyl sther218{r€ ChryEen€53-703 Dibenzo (a,h) anthracene132€1-9 Oibenzofu.enst5G1 i,zoic{iorcb€nzenes41-73.1 1,3-Dicl{qob€nz€ne1oeF4&7 l,+Dbhloaobenz€ne91.94'r 3,3',-Dict{orob€nzidinei?0€3'2 2,+Dichlo{opheno(€4$e2 tJiefiy phtt|atate13r.rri Dimed1yl phthatate10667€ 2,4-Dirnethylph€nol8,4-7+2 D'-n+r.(ylphthetatE53{-52.1 4,6-Dinito-2-m€thytphenol51-2&s 2,+Dinkophendl2l-1+2 2.4-Oinihotolu€ne60de{F? z,&DlnitEto|ueno117{a{ Di-{r-ocoil phtnalEte2{6-14'0 Fluqanthene8&Zll Fluoione11&7+1 Hexacfrloaob€nzefle87{&3 HExadorobutadi€nen474 Hexadorocyclopentadiene67-72-1 Hexaatdoro€thane19139-5 Indeno (1,2,3-cd) pyrsn€90-12{ l-Mefiylnaphhabn€7E-5+l lsophorcne91.57€ 2-Methylnaphthatene!F4&7 2-Mettylph€nol108-304, 3,4-M€thylph6nol106-{4{g1-2S3 NaphtEleneE8-7+4 2-Nifoahitines,os.2 +Niboanitlne

BRLgRL

BRLBRLBRL

BRLBRLBRLBRL

BRLARLBRLBRLBRL8RLBRLBRLBRL

BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRI-BRLBRLBRL

BRLBRLBRLBRLgRL

BRL

BRL

BRLBRL

lgrg dry 343pdkS dry U3

ldkg dry 343pgr'kg dry 343

Idko dry 343

PdkSdrY 343

lgl(gdry 343

UdkS dry U3

UgkS dry 343

ldkS dry 34i!

ljgIlg dry 343pgrsdry 343

FgtS dry U3

udkSdry 343

rdkS dry 343

lgr'kg dry U3

lgkS dry u3

Udl€ dry 343pdtg d.y 343

liSl(g dry 343

lgkS dry 343

Ugr(S dry 34:|p9/k0 dry 343

ISfl€ dry 343pqks dry 343

!4kgdry 343

!S/kS dry 343

trdkS dry 343pgr'kg dry 343

Igkg dry 343pgkS dry 343

trdtg dry 343

t/dkS dry 343

UdXS dry U3

ldrsdry 343pg/t€ dry 343p9ik9 dty 343pdks dry 343

ldkg dry 343pgkgdry 343

IgkS ttry 343pgkg dry U3

}rdkS dry U3pCn$ dry 343

lgrgdry 343

ugtsdry 343

IS/kS dry 3,13

rcftS dry 3,13

USikg d.y 343

l,dkS dry 33

Thir ltbnbry rqort h noa edd toilhod o eudtottzd si.'l.tatc/re on the coee, pdge.

. Rcporiable Detectioo Limit BRL = Beiow Reoodng Limir Poge 50 of l!4

Page 354: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samplc IdentificationM8F-{5 4-6'sA59517-10

Client Project #301-88

Collection Date/Timel9-Mar47 00:00

MatnxSoil

Received20-Mar-07

CAS No. Ana$a(s) FIas Uttilt *RDL Dilution Method nel Prcpdnd Arnlyzed Botch Adabtsl

S€mivoladle O.garic Compounds by CCMS

Somivolatile Oroanic Comoounds by SW846 8270C

Prepared by melhod SW846 35508

10o-0t{ +Nitroaniline98-95-3 Nitrotr€nzene88-755 2-Nit.ophenol1OO{2-7 4-Nitrcphenol@'7+9 N-Nitrosodimethylamine62144-7 l+Nitrosodi-n-propylamine86-30-6 N-Nitrqsodiphenylamine474€.5 Pentachtorophenol45101{ Ph€nenthrene1O8,9s-2 Ph€nol1294t{ Pyreneri0{6-1 Pyridine

rz0+2r 1,2,4-Trichlorcbenzene95-954 2,4,$Trichlorophenolg8-0G2 2,4,G-Trichlorophenol

S4f'ogale rccoveies32140-8 z-Fluorobiphenyl

367-124 2-Fluorophenol

4165-40-0 Nitrohenz€ne45

416ffi2'2 Phercl4s

1718-514 Teryhenyl4l4

1 SW846 8270C z3'Marlr 26-Mat-o7 7031371 M.B

1 "

1 '

1 "

1 '

l '' t "

1 "

1 "

1 "

1 "

1 '' t "

1 '

1 "

BRLBRL8RLBRLARLBRLARLBRLBRLBRLBRLBRLBRLBRLBRL

106787986123

0.0948

8RL

21.6

59.6

BRL

4_50

65.3

BRL

pg/kg dry 1370

UdkS dry 343

Ug/kg dry 343pdkg dry 13'10pg/kg dry 343

!g/kq dry 343

rgks dry 343pSnq dry 343pg'{$ dry 343pS4(S dry 343

ldkS dry 343pgkg dry 343

US/kS dry 343

t g/kg dry 343pdkS dry 343

30-130 %1Ufi0 %30-t m %15-11O To30-130 %I ul10 %

mg/kg dry 0.0436

mg/kg dry 1.40

mg/kg dry 2_1O

mg/kq dry O.7O2

mg/kg dry 0.351

mq/kg dry 0.702

n'dkS dry l-05

ntS/kg dry 2.1O

mg/l 0-0100

mg/l 0.0150

mg/l 0.0050

ng/l 0-0025

mg/l 0.0050

mgn 0.00040

mg,'l 0-0075

mg/r 0.0150

t8-7*6 2,4,6Tib@mophenol 107

Totrt Merrk by EPA 6000/70{0 series Merhods

74399rc Mercury

Totrl Metsls by EPA 200 Series Methods

744G22-4 Sih/er

744-3+2 Arcenic

7,t40+9-3 Badum

7,140{3-9 C€dmium

744{47-3 Chromium

7439-92n Lead

7782-19-2 Setenium

I SW846 747'lA 264,Aa(O7 27-MarO7 7031322 YP

EPA 200.7 2f-Ma(47 27 -Ma'-o7 7031321 HB

SPLP M€trlr by EPA 1312 & 60O0t000 S€rtes Methods

SPLP Extraction Completed

7440-22-4 Silver BRL

zt40-38-2 Arsenic BRL

7.l,l0-393 Barium 0.0236

7rt4o-43-9 cadnium BRL

7440-47-3 Chrcmium BRL

74!9,97€ Mercury BRL

743$92.1 Lead BRL

t82.4s2 Selenium BRL

G€nerrl Chembtry Prrrmei€rs

68.5

'1 SW8461312 22-MarD7 22-Ma(Ol 7031344 AD

1 SW8461312/60108 23-MaAl 24-Mafi7 7031408 LR

1 '

1 "

1 '

1 '

1 SW8461312'470A ' 26-Mar07 7031409 YP

I SW846131260108 ' 24-l\,lar-07 7031408 LR

1 '

SM2540 G l\rod- 24-Mat47 241ta(47 7031463 OP% Solids

Page 5l ,rf 124

Th laborclouepod is Aot t)alid |9llhot t an authorized signsrwe on rhe cowt pcge.

+ Report ble Detection Limil BRL = Belo* Reporting Limir

Page 355: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeptificationMEF-16 2{'sA595l7-r l

Client Project #30r-88

Collection Date/Timel9-Mar-07 00100

MatrixSoil

Received20-Mar47

CAS Na A^rlrt(s) Flas 'RDL Dilution Llethod Rzl. Prcporcd Analyzed Batch Ar.dysl

Fi€kt €xtracledVolatile Oruanic ComooundsPr€pa.ed by mehod SW846 5035A Soil (lovi, level)76'1+1 1,1,2-Trichlorolrifluoroethan€(FreoFRL

Volrtile OrB.rl. Compo{Ed3

VOC Extraction

psikgdry 6.7pgr€dry 134pgkg dry 6.7

udxg dry 6.7

irdkS dry 6.7

UdkS dry 6.7

IdkS dry 6.7

udkS dry 6.7pdkg dry 13.4

USd€dry A7.2

IS/rgdry 6.7

lSikS dry 6.7

udksdry 6.7pdksdry 3i'.6pdks dry 6,7

lgkS dry 6.7

lgkS dry |3.4

ugkg dry 6_7pdkodry 13.4

ldkS dry 6-7

USikS d,y 6.7

rc/tS dry '13.4

pdls dry 6,7

Udks dry 6.7

ldkg dry 6.7

ldkS dry 6.7

Lrdl(g dry 6.7

[gkS dry 6.7

US/kS dry 13.4

udkS dry 6.7pdks dry 6.7pdkg dry 6.7

t dkS dry 6.7

IS/kS dry 6.7pdkSdry 6.7

ldksdry 6.7

ldlSdry 6.7

ldkSdry 6.7

vdkqdry 6.7

Fdks drv 6.7

UdkS dry 6.7

udkg dry 6.7

USi*S dry 67.2pgtsdry 6.1

!g^S dry 6.7

ldtg dry 6.7pglgdry 87.2

ldkSdry 87-2

ldkg dry 8.7

1

1

1

1

I

1

I

1

1

1

1

1

1

I

I

I

1

1

1

I

1

1

1

t

t

rI

t

I

1

1

1't

1

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21-Met47 214nEf47 7031261 BD

SW 846 e2608 2ilat47 23]|lat47 7031335 RLJ67{41 Ac€lone107-13r Acryo,nitrile7143'2 B€nz€nel0a€6-l Bromob€nzene7447-5 Brcmochhaomethane7s-274 Brcmodicfih.omethane75-2*2 BrOmOIOrm74{}9 Bromom€thane78€93 2-Butanon6 (MEK)

1Oa-51{ n-Bulylb€nz€n€135-9€{ sec-Butylbenz€n€98{6{ tertSuiylbenzene75-15{ Caabon disulfide56-?+5 CarbontetaacHorid€l0&9G7 Cl o{obenzeoe75.{lG3 qrbroefhane

67463 Chtoroform7rl{7-3 Chlorom€thanes5-49-€ 2-Chlorototuene10€-43-{ zl-Chlorotolu€ne

BRLBRfaRrBRTARLBRLBRLBRLBRLBRL8RLBRLBRL8Rt_BRI-BRLBRLBRLBRLBRL

9Gl2-8 1,2-Dibromo-3-chloropropane BRLr2q€-r Dbromocl{orcmethan€ BRL10&93-1 |,2-Ob.ornoeE|an€ (EDB) SRL74-95F3 Dibromomethan€ BRLs6-sG 1 l,2-Dichlorob€nzene BRLs1.73'1 l,SDictiorobenzene BRfi05-4c7 l.+Oicfllorob€rEene 8RL75-714 Dic.to.odi0uoromethane(Freon12)BRL75tL3 |,l-Dichloroethane BRL107{6.2 l,?-Dichlolehane BRL7t36-.r |,l-DicHqo€thene BRL15C59.2 cis-1,2-Obhloaoethen€ BRL15e60-s lEn91.2-Di* oroethene BRL7847-5 l,2.Oichtompropane BRLr.2-2e4 l,Soichlomp.opane BRL59+2e7 2,2-DichloroDropane BRLfr63-58{ I ,1 Oichlorcqroene BRL10061-{tr6 ds-1.}Diclrtoropropene BRL10061-02€bans.l,$Dichlorop|npene BRLrm-1i4 Ehy'benzene BRL87{&3 tbxac* orcbuhdiene BRLsol.784 2-H€xanone(MBK) BRLg8-82-E l6ogrbpy'berE€ne BRLss€7€ +lsopropyttoluene BRL1634-o4-a M6dryttsrt+ut!,1ether BRLi08-1e1 4-Mehyl-2-p€ntanone(MIBK) BRL?5{+2 Methylon€ chloride BRL

BRL91-2G3 l{aDhthabno

Paga 52 ot 124

This bbotulory rcport is Ed t@d vlthotd sd outhoriz"t signatn oa the cove, page.

* Reporiable DetectioE Limit BRL = Betow ReDorting Limit

Page 356: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sar[ple IdetrtificationM8F-{6 2-4'sA595l7-r l

Client Proiect #30 | -88

M^EixSoil

Received20-Mar-07

Collecrion DatelTimel9-Mar-0? 00:00

CAS No, A^olrte(s) Result Fl"S Uni4. 'RlrL Dilatioa Method Retr Prcparcd Analtzed Bateh Analtsl

VoLllle Orgrnic Compoundi

Volalile Oioanic ComooundsP.€pared by melhod SW846 50354 Soit (tow tevet)103€5-1 n-Propylbenzene ERLi00.42-s styrene BRLen$:D4 1,1,|,2-Tetrachtoroethano BRL79-3+s 1,1 ,2,2-Tetrachloroethane 8RL127-18F4 Tetrachtoroethene BRL10&€a-3 Tolu€ne BRL87€14 l,2,3-Trichtofobenzene BRL12G32n 1,2,4-Tdchtorobenzene BRL71str 1,1,1-Trichloroethane BRL79{r}s 1,1,2-Tricftloroethane 8RL79{16 Tdchlorcethene BRL756€_4 Tdchlorofluoromethane (Fr€on lt) BRLg.FlA{ 1,2,}Trichloropropane 8RL95{3{ 1,2,+Trimethyjbenzene BRL10e{7{ l,3,tTrim€thytbenzene BRL75414 Vinytchloride BRL1330.2G7 m,p.xylene BRL95-17-6 o-Xylene BRL10+99-9 TelEhydrofuran BRL6G2$7 Ethyt ethef BRLs€,Hrs€ Tert-emylrnethy'edler637-92n Ethytied-butytether10&aF Disopropyteher75{5-0 Tert-Butanot/butylalcotlolt23-s1-l 1,4-Dioxane

Surrogde Ecovenes:460004 4-grcfionuorcbenzene

m37-264 TokEne4S

I 706047 4 l,2-Dichloroethane44

1a68-53-7 Abromofruarcmethano

f,xtraotrble Petroleum Hydrocrrbons

ExtractaHe Total Petrcleum Hvdaoc€rbons

Prepared by method SW846 3tt5A

Amffi1-g Gasoline6447em.2 FoelOit#26{1476-313 FuelOit#468s53.{Xr.4 Fuel Oit #6lvl098o0oo0 Motof oilJ00t00o0o Aviation Fuel

Unidentifed

Oth€r Oil

Total Petroteum Hydrocarbons

Cg-C36 Aliphalic Hydrocarbons

Su?Dg6te €cover'€si33Pd-33'2 l-Chlotooctadecene

Samivolrtile Org|nic Compouods by CC

Orqanocfilodne Pesticides SW846 8081A

Pr€pared by method SW846 35508

slg.oG2 Aldrin

BRLBRLBRLBRL8RL

100102110107

Sw 846 82604 22.MarO7 23-MaFO7 7031335 RLJ

BRLARLBRLARLBRL8RL1 ,150Caldllated ast , 1501 ,150

lSftS dry

ldkS drypq/kg dry

udks dry

udkS drypgftg dry

ldks dryyqkS dry

udkg drypdks drypq/kg dry

ldkg drypdkg dty

US/kS dry

ugks dry

IrS/kS drypdks dry

ldkS drypgnq dry

udkg drypdks drypg/kg dry

!s/kg drypdks dryps/ks dry

70-130 %

7G130 %

7G130 %

70-130%

rndkS drymg/kg dryr€,4(g drymdkS drymdks drymS4(S drymdkS drymg/kg drymg/kg drymg/kg dry

40-140 %

6_7

6.7

6.7

6.7

6.7

6.7

6.7

6.7

6_7

6,7

6.7

6 7

6 7

6.7

67.2

6 7

6.7

6 7

6 7

6l.2

134

1

1

1

1

1

1

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1

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1

1

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1

1

1

1

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1

1

l

i

I

187 1

187 1

187 1

1E7 1

r87 1

r87 1

147 1

187 1't87 r

107 1

+CT ETPH 22-Mat47 aaMa(O7 7031284 DS

231

rdks dry Sw846 8081A 22-Mat47 27-llet47 7031275 rG

Thh labofttory rcport is not vlid ttlthoqr aI uthori.et ignatarc on the cover p,age

* Reportable Detection Limir BRL = Below ReportinC Linit Page 33 of 124

Page 357: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiorM8F-46 24'sA595 17-ll

Client Proiect #301-88

Collection Date/TimeI g-Mar{? 00:00

Received20-Mar07

MahixSoil

CAS No. Anabre(s) Ressh Fl"C 'RDL D ttlort Method ReJ, Prcwrcd Amlyed Bdch A,n4'st

S€mivolNtile Org|oic Conpound! by CCOroanodrhdne Pesticldes SW846 8081APrepared by method SW846 3550a319-84€ s€HC319-8t7 b€HC319t'8 +BHCs6{s.e g.BHC (UMane)57-1+9 Chlordane7z-$-a 4,4.oDO (p.C)72.5$9 4,+ODE (p,p,)50.2e-3 4,+DDT (p,p.)€o-57.r Oietdrin95+98€ Endosulfan I332i3{54 Endosutrbn ll1031-07{ Endosulfun Sulfate72-204 Enddn7421.9!.r Endrin ludehyale76-44-8 Heptachlor7243-5 lethoxychlor10?457-3 tbplachlor Epoxide60ot+5-2 Toxapheno5103-71-9 a-Chlordane5s66J4-7 gchlordan€5349+70-5 Endrin Kebne

Surrogaie,ccoyeai6s-_103864+2 4, g+Octafl uotoupherryt (Sr)m51-24.3 Deca&lorobiphenyl (Sr)

Potuchlorinated Bbhenvls bv SW846 8082Prepa.ed by melhod SW846 35454126f+111 PCB 1016111o4-U-2 PCE 122111141-16-5 PCB 1232s3.6e21-9 PCB t24212672,2e{ FCB t248rrrET-Bsn rc8 1254r1@6-s2{ PCB 12603132+??4 rc8 1262ir10c14-4 PCB 1268

Sunogale /Bcovrabs.'1 03864+2 1,4-OB-Oclafr uotobifreny (St)2ost'2$ Decachlotobipheny (54

ScEdvolslit Orgrnlc Compo{rds by crCMS

BRLBRLBRIBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

3180

BRLBRLBRLBRLBRLBRL2 l . 2BRLBRL

4070

BRL

BRLBRL8RLBRLBRL8RrBRL

pgkSdry 6.63

!SI(gdry 6.63

udksdry 6.63

rdkSdry 6.63

rdkSdry 332

ru/kg d.y 6.6i]

lgrg dry 6.63pgtg dry 6.63pdkg dry 6-63

ldkSdry 6.63

ldkS dry 6.83pdks dry 6.63pSfts dry 6.63

lSftsd.y 6.63p91S dry 6.63

Itglgdry 6.63

trdl€ dry 6.63ygas dry 33.2psftg dry 6.63

U€ftg d.y 6.63

USi€d.y 6.63

3o-tg) %361fi%

9SftS dry 13.3

Fgn(g dry 13.3

lSftS dry 13.3

|lgks dry 't3.3

lcrls dry 13.3

ldrsdry 13.3

t gl(g dry 13.3

ldks dry r3.3

IdkS d.y 13.3

3rL150 %30-tg) %

len(gdry 923

lSn€ d.y 923

llg/tS dry 923pSI(g dry 923

Pgkgdry 923

!df(s dry g23

fldksdry s23

ugftgdry 923

SWB46 8081A 22-l,d,(47 27 at47 7031275 TG

SW8l|6 6OE2 22-Met47 24^llat47 7O3t3'13 MP

Semivolatile Oroanic Comoounds bv SWB46 8270CPropa.ed by me0|od SW846 35508A3-32-9 Ac€oaphthene20&96-8 Ac€nqhthy'ene62€93 A$line12+12.7 Antfrac€ne1912{49 Atrazjne10$333 Azobenzerie/DiptEnyldiazinee€7-5 Benzidine5e5S3 Benzo (a) anhracerE

swt46 8270c 2&Mar{7 28+{larfl 7u}1371 M.B2

2

Thb laborcory Eport h nol vali! withart on althorizd sigQatue oE tlp coser page.

. R€porbble Derection Lidit BRL = B€tow R+ortitrg Lidir Page 54 ofl24

Page 358: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldetrtificationM8F-46 2-{'sA595 l?- l l

Client Proiect #301-88

Collection Date./Timel9-Mar-07 00:00

MatrL(Soil

Received20-Mar-07

CAS N^ An ye(s) nesult Fhs Units 1RDL Dilation Method Re{. Prcparcd Anal)1ed Botch Aulrsl

Scmivolatil€ Orgrnic Compounds by CCMS

Semivolaiile Omadc Comoounds bv SW846 8270C

Prepared by method SW846 35508

5G32€ Benzo (a) py€ne

mtse-z Benzo (b) ltuoranthene191-24-2 Eenzo (g,h,i) perytene

207-08.9 Benzo (k) fluoranlhene65{tu Benzoic acidi0G51€ Benzylalcohol1r1-9rr Bis(2dlloDethory)methane111aaa Bas(2.ohloroethyl)ed1€r39€38-32-e Bis(2-clhloroisopropyl)ether1i7{1-7 Bas(2-€thylhexyl)phfialate101-56-3 4€rcmophenyl phenyt ether65-6+7 Butyl b€nzyt phthatate

86-71-g Carbezole59.5G7 4-Chtoro-3-methytphenol106-a7{ 4-Chloroanitine91697 2-Chloronaphthatene95-57{ 2-Chlorophenol7005-72-3 4-Chlorophenytph€nylether

2i8-01,9 Chrysene53-703 Dibenzo (a,h) anthrac€n€132€4-9 Dib€nzofurang$snr 1,2-Dicfilorcbenzene541-731 1,3-Diclllorcbenzene10e.46-7 1,4-Diohtorobenzene9'l€+1 3,3'.Dichlorobenzidine120€3-2 2,,t-Dichtorophenol84{G2 Diethytphthatelel3i-1l-3 Oimethyl phthatate

105{74 2,4-Dimethylphenolw7+2 Di-n-butylphthatate53,1-5?,1 4,6-Dinito-2-methytphenol

51-286 2,+Dinitophenol121n4-2 2,4-Dinilrotoluene606-20-2 2,6-Dinilrotoluene1i7{4{ Di-n-oc{|/lphthalateam-44{ Fluoranthene&7T7 Fluorene11&74-1 Hexachlorobenzene874&3 ll€xachtorobutadiene

n471 tl€xachlororyclopentadi€ne87-72-1 Hexac.hloroethanet9s95 Indeno (1,2,3-cd) pyrenesonz{ 1_M€thytn€phthaleneTESSn lsophorones1574 2-M€tlylnaphthaleness-a&7 2-tl€thyiphenol

106-3s4, 3,4-Methylphenol106-44,591+G3 Naphhalene&744 2.Niuoanilin€99{sz }Nitroanitin€

8RL8RLBRLBRLBRLBRLBRLBRL8RL8RL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRL8RLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRL1,120BRLBRLBRLBRL

BRLBRLBRL8RLBRLBRLBRL

BRLBRLBRL

!S/kS dry 923pg/kg dry 923pgftSdry 923

!S/tS dry 923

IdkS dry 923pS/kS dry 923

!S/kS dry 923

ldkS dry 923pS/kS dry 923

US/kS dry 923pg/kg dry 923

ldkg dry 923

UdkS dry 923

UdkS dry 923pdks dry 923

rS/kS dry 923

!g/kg dry 923pdks dry 923

ug/kg dry 923

US/kg dry 923

rc/kg dry 923ps/qdry 923

Ug/kg dry 923pYr(S dry 923pgtS dry 923

tiSftS dry S23

!S/kS dry 923

!s/ks dry m3

ldkS dry 923pS/kg dry 923pS/kS dry 923

!s/ks dry 923pdks dry 923

IgkS dry 923pdksdry 923

!S/kS dry 923pdkg dry e23

ldkS dry 523pdks dry 923

rdks dry C23

rcAS dry 923

rc^S dry 923

USftS dry 923

Ugks dry 923

UdkS dry 923

UEkg dry 923

l.'dks dry 923

yS4<9 dry 923

tdkg dry s23

lrS/kS dry 923

sw646 8270C22

222222

22

22222222222222222222

222

22222

222222

22

222

Thit laborolory repon k aot ,alid ta,ilhout an utlhorize.l signatare on thc coyer Nge.' Reportable Det€ction Limit BRL = Below Reponing Limit Page 55 of 124

Page 359: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiooM8F-46 2-4'

sA595 t7-l l

Cli€trt Proiect #301-88

Collectioo Date/TimeI 9-Mar47 00100

MatrixSoil

Received2GMa[-07

CAS No. Analrk(s) Resull Flos Unia .RDL DiIarLrn MdM Retr, Pnpond Analyzed Batch Analfst

Semivolrlil€ O.g lc Compoundr by CCMS

Semivolatile Oroanic Comooonds bv SW846 8270CPrepared by aFlhod SW846 3550810o{1{ 4-Nibo'enilin€9a€$3 NitEb€nz€n€a&7t5 2-Nitoph6nol100-02.7 +Nit'oph€nol62.75>9 N-Nfuosodimehyiamine621€4-7 N-Nihosodi-rFpropylamine86.3{t6 N-Nitrosodiph€rrylaminea7{ss Penta(fibrophenol85{1€ Pienanlhren€108s5-2 Phenol12900{ Pyrene110{61 Py dine12G82-1 ,|.2,+Tdchlorob€nzene

95€5-4 z,4,5-Trichto|oph€nol8s{G2 2,4.6Trichloro,phenol

Sffogate €coMe/resl3?160-8 z+l@robiphonyl

367-124 2+luorophenol

1165{04 Niltob€nzene4s

416542.2 Phq10H5

1fle5r4 lerphony'44

SPLP Extradion

7"KO+24 Silver7,trgl.3&2 Arserlic

71,{0-393 Badum74-rO-439 C€dmium744G.47.3 Chromium7rB9-97S Mercury

743&92n Leacl

7782-4+2 SeleJlium

G€nerel Cbembtry Psram€ten

% Solids

pcrkg dry 3690pgxgdry 923pgkg dry 923pdkS dry 3690

!g/kS dry 923

lgkS dry 923gg/kS dry 923

IgkS dry 923

ldkgdry 923

ldlqdry s23pSil€ dry 923

t dkg d.y S23

ldts dry 923

rcrkg d.y 923pCrkS dry 923

30-1X) %1 ,nO%3t\130 %1r110z!)-130 %1*110 %

rng/kg dry 0.0336

|rrg^g d.y 1.12

mgilqdry 1.67

rE/|q dry 0-558

nEftg dry 0279

tng/kg dry 0.558

ng/ksdry 0.836

d€/kg dry 1.67

N/A

mgl 0.0100

msil 0.0150

mSI 0.0050

rnSil 0-0025

mdl 0,0050

ntgn 0-00040

mdl 0.0075

mSI 0.0150

%

BRL8RLBRL

BRLBRLBRI-BRI-

BRIBRL

BRL|,ssoBRLBRLBRLBRL

1686

122

0.363

BRL

19_7

69.0

0.457

7.42

136

BRL

2

222

2

222

SW846 8270C 23-irar47 2frt ar{7 7031371 M.B

11&794 2,l,6-Ttibrcnophenol 1Og

Total Metab by EPA 6000/7(Al S€rl€s Method!

7439-97€ MercUry

Total Metrlr by EPA 2t0 S€rte! Methods

74/o-U1 Sivel

74arH+2 A6enic

7440-3+3 Badum

7440{}9 C€dmium

71140-47-3 Chromium

7439€2n L€aCl

262-ag2 Selenium

SW6{6 7471A 2A at47 27-N|E,r47 703132. yP

EPA 200.7 -Mar47 274atr47 7031321 HB

SPLF Merab by EPA l3t 2 & 6tXW7000 S.rt$ Merhodl

Comd€bd

BRL

8RL

0.0t 30

BRL

BRI

BRL

0.0 t.t6

BRL

87.4

I SW84613f2 22 1€f47 21nEr47 761344

t SW8461312@104 €.Ma.{7 24-Ma..07 703140€

t '

t "

t '

1 '

1 SW8r1613127470A " 26.t!,lar47 7031409't SW8461312/60108 ' 24-f'rar-07 7031408

1 '

ED

LR

1 Sn425,f0 G Mod. 24411a'47 241nat47 7m146:] QP

Thit labotuory d{o.l is ^ot vslid u,ithou ta oartod@d signihE oE the coter pag. .

. Reporrrble Detection Limi. BRL = B€low Repodilg Limit Page 56 of 124

Page 360: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldenrihcationM8F-17 2-4,

sA595l7-12

Client Pfoject #101-88

Collection Date/Timel9-Mar-0? 00:00

MatrixSoil

Received20-Mar-07

CAS No. Anabte(s) FloS *RDL Dilution lvethod nel Prcparcd A,'dIWd Batch Anobst

Volalile OrSanlc Compo|rtrds

VOC ExtractionVolatile Oroanic Compounds

pSftg dry 61.Spdkg dry 1240

ldkS dry 61.9

Pgn(g dry 61.9

!9ft9 dry 61.S

!g/kg dry 61 9

Ug/kS dry 61 9

rdkS dry 61.9pdkS dry 124pg/kS dry 619

!g/kg dry 6i.9

!s/ks dry 61.9pdkg dry 61.9pS/kS d.y 310pgkg dry 6l Ipg/kg dry 61 IpdkS dry 124

!S/kS dry 61.9pSftSdry 124pS/kS dry 61 9

t gkg dry 6'l .9ygkS dry 124pdkS dry 61.3

FqkS dry 61.9pdkg dry 61.9pS/kS dry 6l-9pdls dry 6r.9

!S/kS dry 61.9

Ud](Sdry 124pgrs dry 61 I

ldkS dry 61.9

UdkS dry 61.s

ldkS dry 61.9pg/kg dry 61 Ipg/kS dry 61 9

PdkS dry 6'l .9

t gkg dry 61.9

t dks dry 61.9

usnq dry 61.9

Udkg dry 61.9

lSn€ dry 61.9pSnq dry 61.9pElq dry 819

lgkS dry 61.9pqkS dry 61.9

lgftS dry 61-9

fdkg dry 619

!g/kg dry 619pdkS dry 61.9

Prepared by method SW846 5030 Soit (high tev€t)7s13-1 1,1,2-Trichlorotrifiuo.oetrane (FreoBRL47441 Acetone BRL107-13-1 Acryjonihle BRLt14t-z Benzene 72.5108-€61 Bromobenzene BRL71-97-5 Brcmociloomethane BRL15-274 Bromodicl oromethane BRf75-25-2 Bromoform BRLzl{3.9 Bromomethan€ BRL7&9!3 2-B'ltanone (MEK) BRL10+51{ n-Butylbenzene BRL135-9€€ s€c.Butylbenzene BRL98.06-0 tsrl€utylbenzene BRL75ts1s.O Carbon disultide BRL5€-23-s Carbon tetrachloride BRL10&s0"7 chlorob€nzefle BRL75{eJ Chloroetrrane BRL67€+3 Chlomform BRL7147< Chloromethane 8RL9149-€ 2-Chlorotoluene BRL106-43-4 4-Chlorotoluene BRLS12.8 1,2-Dibromo-3-chtoropropane BRLu4-4€-1 Dibromochlo(omefrane BRL10€43-1 1,2_Dibrcmoethan€(EDA) BRL74.9+3 Dbromomethane BRLgs-sr].1 l,2-Dichtorcbenzene BRL541-7$1 |,3-Dichlorcbenzene 8RLr0G46-7 ,1,4_Dichlorobenzene BRL7$71-s Oichlorodifluoromethane(Freont2)BRL7$3+3 |,l-Dichloroethane BRL107{6-2 l,z-Dichloroethane BRL75Jt4 l,|-Dichloro€th€ne BRL1S50-2 cis- 1 ,2.Dichloro€fhene BRL15ffi tfans-1 ,2-Dichtcro€then€ 8RL78-07{ 1,2-Oichloropropane ARL'142-28€ .1,3-Ochtoropropane BRL59420-7 2,2-Oichtoropropane BRL5615€{ 1,1-Dichloroprop€ne BRL10061.01-5 cis.1,3-Didlloropropene BRL10061-02{bans-1,3-Diciloropropene BRL100-4i-4 Ehyibenzene BRL87{&3 }bxachlorobutadien€ BRL591-76{ 2-l{eranone (MBK) BRL9€{2{ lsopropylbenzene BRL!19-876 4lsopropyltoluene BRIi63r.04-4 Methyl tert-butyl etfier BRLr0&1Gr 4-Methyl.2-pentanon€(M|BK) BRL7t{)9-2 Methylene chtonde BRL

VOC 21-Mat47 21-Mat47 7031261 BO

Sw84682604 27-MaA7 27-Ma(07 7031602 mar

Field extracted

505050505050505050505050505t)5t)5050505050505050505050505050505050

5050505050505050505050505t)5050505091-2S3 NaphtlElene

Pag€ 57 of I24

Thit laborutory Epod it aot tdid t tithout aE suthori,Fd rignatarc on the cover page .

* Reportabie Det€crion Limir BRI- = Below R€porting Limit

Page 361: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sa.rnple IdentificationMtF-47 2-4'

sA595l7-12

Clietrt Proiect #30t-88

Collectiod Date/Timetg-Mar{? 00:00

MatrixSoil

Received20-Marry

CAS No. Analtta(s) R".rull FW rRDL Dilaion Method nei PnpaQd Arnllzed Beth Anrbst

Vohltl€ Org|nic Cofi pouds

Volatile Oroanic ComooundsPrepared by mothod SW846 5030 Soil (hlgh lewl)t09651 n-Propylb€nz€n€ BRL101X2-5 Styrene BRLS0.20"6 1,1..1,2-Tetrachtorcethane BRL7+34-5 1,1,2,2-T€t'echtoroethan€ BRL127-18-4 Tet?chloro€th€ne 8RL10&84.3 Toiuene 2M87{1{ 1,2,3-T,ichto|obenzene BRL120{2-1 1,2.+Trichlorob€nzene BRL71-5+6 1,'1,1-Trichlofo€thane BRL79{0-5 1,1,2-Trichloroetfune BRL7941-6 Trichloro€thene BRL7569-4 Trjchlorolluoomethan€ (Freon 1l) BRL96-18-4 .1,2,$Tddtloropopen€ BRL9563-6 1,2,+T.inethy'benzen€ BRL10&67$ 1,3,5-Trimethylbenzen€ BRL75{1-4 vinylcf oride BRL13aX!20-7 m,p_xytene 16595-47-6 o-.Xyierie 80.5l0+9S-9 T€trahlidrofursn BRL60-2$7 Ethyt sth€r BRL

Ug/kS dry

rdkS drypgkg dry

ldkg dry

lSI€ dry

lSrkg drypgts d.ypgrs dry

ldks dry

lgkS dry

[dks dry

ugfts dry

lgfts dry

t S/kS dry

tidkg d.y

ugkr drypSAg drypCng d.y

tjc/ks dry

ldks dry

UgtS dry

USn(S dry

ldkS dry

t glq drypS/kS d.y

5 1 . 9

6 1 . 9

61_9

6 1 , 9

61.9

61.9

61.9

6 1 . 9

61.9

6r .961.96 1 . 9

61.9

6 1 _ 9

6 1 . 9

61.S

124

61.S

6 1 9

6 1 . 9

6 t _ 9. 61.9

61.9

6r9t240

5050

505050

50

505050505050505050

5050

Sw 8,46 82608 27-[,lar-0727+rad7 7031602 mar

gs,rcs Tert.amylmetfiylether637-92,3 Edryl lert+utyt €th€ri0&2o3 Di+oprgpylether7s{t0 Tert-Bubnol / buq/ atcohott2+91-1 1,+Dioxane

Sunog€te recoy€res..tiGoo4 +Eitomonuorobenzenem37-2cs Toluone4St 7 0604/4 l,z-Dichlorcethane441868-5X7 Abrononrcromethane

E(Ecrrble Peftoleum HydrocrrbotriExhactable Total Petroleum HvdrocarbonsPrepar€d by method SW846 3115A806{1-9 Gasoline6&+7+30-2 Fuel Oil #26e47fi1'3 Fuel Ol #464s53{0.4 Fuel Oit #6M0980m00 Motor OilJ0ot0@@ Aviaiim Fuel

BRLBRLARLBRLBRL

9910391

BRLBRLBRLBRLARLBRL1.310Calqrlated ds

70-1n %76130 %7G130 %70-130 %

mg/kg dry 350mgr'kg dry 350flig/kg dry 350tn€L/kg dry 350mgr'kg dry 350mgttgdry 350rndkg dry 350nEAg&y 35Omo/kg dry 350nEitg d.y 350

40-140 %

+CT ETPH

unidenlifiedOth€r OilTotllPefoleumHyd@carhons 1,310C+C36 Aliphatic Hydrocadons 1.310

Surrogal€ recovgrios:fia6t.33-2 l-Chlotoocladecene zos

Semlvolirtlle Orgrnic Compounds by GC

Oeanochlorine Pesticides SW846 80BtAPropa.ed by nethod SW846 3550430eoo"2 Ald.in BRL l|g^g d.y SW846 S08tA 2.+ttat47 27,rM6tr47 7031275 IG

This tthoruta! rqort is not volid wlthod an oalhofizd sipoa.re od thz coeer page.

* R€porrable Detection Limit BRL = B€low R€Dorting Linir Page 5E of 124

Page 362: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F{7 24'sA595l7- 12

Clieot Proiect #301-EE

Collection Date/Timel9-Mar-07 00:00

MatnxSoil

Received20-Mar-07

CAS N^ Anattte(s) Result Flag Units IRDL Method ReJ. Prcpand AmDzed Batrh An lst

Semlvol.tile Orguic Conpounds by CCOroanochlorine Peslicides SW846 808tAPrepared by method SW846 355083l+oa€ a-8HC319-05-7 b-BHC319-86{ d_BHC58{$e g-BHC (Lindane)57-74-9 Chtordane72-5,t{ 4,4-DDD (p,p.)72-5+e 4,4-DDE (p,p,)5{F2}3 4,4-DDT (p,P.)60{7-1 oieldrin9599€{ Endosulfan I3321+6&9 Endosulfan ll103r{7-8 €ndosulfian Sutfater2-m4 Endrin7421,93-4 EndrinAldehyde78-444 Heptachlor72.t3-5 M€thorychlor102+57-3 HeptachlorEpoxide€0O1.3+? Toxaphenes10s-71-s a-Chlordane55€6-3+7 g-Chlordenes3aga-nr.s Endrin Kelone

Suflogale 'Etcov€des:

10386842 4,4-DB-Octefluorobiphenyl (54

2051-24-3 Decachlotobiphenyt (Sr)

Polvchlorinabd Biohenvls bv SW846 8082

Prepared by method SW846 3545A

1247+11-2 PCE 1016ltt(]!-24-2 PcB 122111111'185 PCB 1232r,346121-9 PCB 124212672-2S6 PCB .1248

11097{Sr PCB i25411096€2'5 PCB 126031324-2+5 PCg 12621r10G14-4 PC8 1268

Sunogat€ rccoveias:rowa2 4,1-O&Octafl uotobiphenyt (St)

m5t-243 Decachbrobiphenyl (Sr)

Se[rlvolelile Orgrnic Compo([ds by C,CMS

BRLBRLBRLBRLBRLBRL8RLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL

3356

BRLBRLBRLBRLBRL8RL28.0BRL8RL

5090

BRLBRLBRL

8RLBRLBRLBRLBRL

US/kg dry 6.36pdkg dry 6.36

l./gkg dry 6.36pdkq dry 6.36

ldkS dry 31.8

trytg dry 6.36

UEl$ dry 636pgn(g dry 6.36

ldls dry 6.36

ldkS dry 6.36

Udkg dry 6.36

Lig/Kg dry 6.36

!g/Ig dry 6.36pdkS dry 6.36

ldks dry 6 36pgkS dry 6 36

l,gkS dry 6-36pg/kg dry 31_8

Fq/kg dry 6.36

ldkS d.y 6.36pdkS dry 6.36

30-150 %30-150 %

lqkg dry 12.7

!S/kS dry 12.7

udkg dry 12.7

ldkg dry 12.7

trS/kS dry 12.7pS/kS dry 12.7

!S/kg dry 12.r

ldkg dry r2.7

!g/kS dry 127

30-150 %30-150 %

ldkS dry 1740

FdkS dry 1740

pSrt(g dry 1740

ydkSdry 1740

FgkS dry 1740

pgks dry 1740

ygl(g dry l74O

p94(S dry 1740

t

I

l

1

1

1

1

1

I

l

l

1

1

1

1

I

I

I

I

I

1

SW846 8081A 22-Mat4f 2741a(47 7031275 rc

SW846 8082 22-MarO7 24-Mat47 7031313 l\rP

SW646 8270C 23-[4ar{7 m-[4ar47 7031371 M.B

Semivolalile Oroanic Compounds bv SW846 8270CPrepared by method SW846 3550883-32-9 Acenaphth€ne20e4fr Acenaphthylene62.513 Aniline12G12-7 Anthracene1912-24-9 AtrazineiO$33-3 Azobenzen€/Diphenyldiazine92{7-5 Benzadine5S5+3 Benzo (a) anthiac€ne

2222

22

fhh laboruloq .epott is not valid plthou an salhoied signalarc or lhe colv pagc.

+ Reportabl€ Detection Limit BRL = Below R€porting Limit Page 59 of 124

Page 363: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentifioatiooMSF-{7 2-4'sA595l7-l?

Client Proiect #30t18

Collection Date/Timet9-Mar47 00:00

MatrixSoil

Received20-Mar47

cAs No- AnaMu(s) F"S l&DL Dilution Melhod ReJ, Prcparud Analyzlr' Bebh Anal$r

Semivoladle Orgatric Conportrd3 by GCMS

Sernivolatile Oroanic Cornoounds bv SW846 8270C

Prepared by mehod SW846 35508

50-32{ Benzo (a) pyr€ne1!+S-2 Benzo (b) nuoranthene191-24-2 Beflzo(g,h,i)p€rylene2OZ{8-9 Benzo (k) fluorenhhene

Benzoic acid10G5r€ Eenzyl alcoho'll1r€r-1 Bis(zrhloro€thory)methane111-4{-4 Bis(2-diorcethyl)€bef35€e324 Bis(2-dhlorolsopropyl)ether117{i-7 Bb(2-efhylhexyl)phfiatate101.563 +BrornoplEnylphefiyl ethel65€&7 Buty' benzyl phhalateE6'ZL8 C€rbazole5s-5G7 4_Chtora.3-methytphenollo€-47{ 4-Chloroaniline91-s+7 2-Chlorunaphthalene9t57-a 2-Chloropf€nol7oo5-72-3 4-Chloropfienyt phenyl ether2t&0i€ Chayseng5l-7G3 Dibenzo (a,h) enthracene132{4-9 Dibenzofuran95-5&1 |,z-DichloDbenzene541.73-t l,lDichlofobenzonerofi6-7 1,+DichloroberEene91-94-1 3.3'-Dichlorobenzidine120{3-2 2,4.Dlchlorophenol84€&2 Died1ytphthalatei3r-11-3 Dimehyl phthalate105-674 2,+Dimegylphenolu-7+2 Di{-butytphthatate534.52-1 4,6-Dioito-2-methylph€nol5l-2s5 2.r|.Dinitropheflol121-1a-2 2,+Oinit'otoluene€oe2G2 2,+Dinitrotoluene117-64{ Oi_n-oct/phthatate206-44{ Ftuo€nthenoa6-717 FluorenetlA-741 HexaChlorobenzene87$&3 Hexachlorobutadiene771f4 l'lexadllorocyclopentadiene67-72-1 tlexadoro9thane193-3+5 Indeno (1,2,}cd) pyrene9Gr2-0 l-Msthylnaphihslene78€Sl ls@horon€91-57{ z-Methynaphthalene95.4&7 2-Methytph6nd106-39.4, 3,4-Methylphenoli06-44-591-20.3 NapfithaleneE8-744 2-Nihoaniline9S.Os-2 $Nitroanitine

SW846 8270C ?3-Mar{7 26-tlar47 7031371 M.BBRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRL

BRLARLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRL2,770BRL8RfBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRI-gRL

BRL

ldkSd.y 1740pgrS dry 1710pgtsdry 1740

ldrg dry 1740

$gv€dcy 1140

ldks dry lf4o

ldkS dry l74O

udkg dry 1740pgr'kg dry 1740

udkg dry 1740

lgkg d.y 1740

FS/kg dry 1740pqls dry 1740pqkS dry 1740pdkgdry 1740

ldkS dry 1740

rdks dry 1740

US/kS dry 1740

tdks dry 1740pdkS dry 1740

tdks dry 1740

lg/kgdry 1740

USftS dry 1740pErq d.y 1740

lgxgdry 1740

ldtsdry t740

ldkS dry r74o

USftS dry lf40

udl(g dry 1740

Pgkg dry 1744

t gr(g dry 1740

ItS/f€ dty l74O

Udkgd,y 1740pSftS dry 1740pqkg dry 1740

Pdkgdry 1740

9d}gdry lf4i

ldks dry l74o

USI(S dry 1l4Opdks dry 1740

rdks dry 1740pdkSd.y 1740

rc/ko dry 17fi

us/ks dry 1740

[dkS dry 1f40

t'dkgdry 1f4opdkg dry t74o

lgkg dry r74O

rgkS dry t74O

IrSftS dry 1740

2

22

2222222

2

2

2222

2

2

2

2

2

2

Thts hbatuorf rcpod is Bot yslid ttitlrord sd a.tthorized signdare oz thz uver page-

. Repodable Detection Limit BRI_ = Betow Reporting Limit P'.Ee fi of 124

Page 364: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationMEF-t7 2-1'sA595l7-12

Cli€nt Proiect #30 t -88

Collection Date/Time19-Mar-07 00:00

MatrixSoil

Received

20-Mar-07

CAS Na An4lyre(s) Resuh F14s Units ,RDL Dilution Method Retr, Prcpored A.ullzed Barch Anallst

Scmlvolrdle Olgroic Compounds by GCMS

Somivolalile Oroanic Comgounds bv SW846 8270CPrepared by method SW846 35508

100-01€ +Nitioaniline

98-9t3 Nltrobenzen€

!t-755 2-Nitroph€nol

10Go?.7 +Nitophenol

i-2-7$9 N-Mtrosodimethylamine

621$a-7 N-Niblsodi-n-propylamine86-30'6 N-Mhosodiphenylamine

074&5 Pentadllorophenolg5{1-S Phenantfirene

10+9+2 Phenol

129-004 Fyrefie

11G641 Flridine

12042.1 1,2,+Tdchtorobenzenegt95-4 2,4.5-Trl$toroph€nol

$-0e2 2,4.&Tricfiloroph€nol

&nro96ta rEcoven€srj2140.8 2-Fluorobipkenyl

36t-12..{' z-Fhtorophenot

4to5j44 Nit Lrbenzentds

416642-2 Phenotr4,

1718-514 Teehenyl4l4

1&7 2,4,6-Ttibrcmophend

BRLBRLBRLBRLARL

BRLBRL

BRLBRLBRL3,260BRLBRLBRLBRL

102919196128101

Totrl Mcl.lt by EPA 60t10/7000 Series M€thods

743&97{ Mercury 0.182

SW846 8270C 23-MaA7 2 Mafi7 7031371 M.B

BRL

10.7

54.7.

0_589

8.64

183

BRL

Comdeted

BRL

BRL

0.0120

BRL

BRL

BRL

0.0261

BRL

s0.9

usn(g dry 6940

usftg '1ry 1140

lrgks dry 1140pSftg dry 6940

lYkS dry 1740pSftS dry 1740

lSftS dry 1740pSftS dry 1740pgilKg dry 1740

lrgftg dry 1740

ISftg dry 1740

lsilg dry 1740

!S/Xg dry l14O

ldkg dry '1740

!g/kg dry 1740

30-130%1s- l 10%36130 %15-110 %30-130 %15-110 %

nE/kg dry 0.0324

mg/kg dry 1.O7

mgr'kg dry 1-61

mgr'kg dry 0.535

m€/kg dry 0-268

nrg!4(g dry 0-535

mgL/kg dry 0.803

rngkS dry 1 61

ntg4 0 0100

mg/l 0 0t 50

mg4 0.m50

ng/t 0,0025

mgl 0.0050

mSI 0.00040

mg/t 0.0075

mg0 0.0150

v.

sw6461312/7470A

sw846131,y60108

222222222222222

SPLP Merrk by EPA l3l2 & 6000/7m0 S€ries Methods

Totll Mearls by EPA 200 Series Mertods

7{40.22.1 Sitv€r

7a4+3&2 AFenic

r44G3$3 Barium

?4.10-13.9 Cedmjum

7440{7.3 Chaornium

143942-1 Lead

882.1&2 Selonium

SPLP ExFacton

744G22-{ Silver

?4403&2 ArEenic

zl40-3s-3 Baaium

7440-4+9 Cadmiuh

744H7-3 c}lromium

743+97{ Mercury

743€-92-1 Le€d

ng21r2 SelBn;Dm

C€tr€rd Ctemlstry PNram€t€rs

% Solids

SW846 74714 26-Ma.-07 27iAa(O7 rO31322 YP

EPA2cn.l 26-Mar07 27-ttar47 7031321 HB

SW846 1312 2-Mar47 221.4a(07 7031344 80

SW84€ 131 0108 23-Mat47 24+lar07 7031408 LR

1

1

I

1

1

1

1

I

'|

1

1

1

1

1

1

I

1

26{raF07 70314m YP

24.lt4ar-O7 7031408 LR

SM2540 G irod. 2+Mat47 24]'4at47 7031463 OP

Thi. laboraaory report it aot volid *irhou dn altthori?pd sigrrzlure ot the coper page.

* Reportable Detection Limit BRL = Below R€porting Limit PaBe 5l of 124

Page 365: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 366: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMtF-4t 2'-4'sA5980l-t5

Client Proiect #301,88

MatrixSoil

Collection Date/Time26-Mar{7 00:00

Received2?-Mar-07

C"4S No, Analyre(s) Result Flas Uaias aRDL Dilabn Method Rel. Prepared Anolyed Batch Anaust

Volrtile Orgaric Compornds

voo Extrlclion 2E1!!ar47 z&Mar{7 7031767 Bo

29{ar{7 29Mal{7 7031790 FU

VohRe Orcanic CornooundsPrepared by method SW846 50354 Soil (low level)i6:13-r l,tl-TricntorotriiuorcethaflelFrcon BFL

BqL

BFL

BFL

BFL

BRL

BHL

BHL

BRL

BRL

BRL

8RL

8RL

BRL

8RL

8RL

8RL

BRL

BAI

BFL

BFL

snLBFL

BRL

anL8RLBRLBRLBRL

BRLBBI.BFLBFLBFLBRLBHL8BL8RLBRL8RLBFLBFLBFLBfrLBRL8RL8RLBRL8RL

107Jll Adylfiitrle71{3'2 Beozenei08-8El ED|IEienzene7+874 Bmoloahlorom€lhaneEn4 BmnFdichloomfEneE2r2 Bro(r)ofoam7|-€3{ Bormmehane?!493 2-outsnone (MEK)

l0+5r{ FE!rylb€nzeoe

135S-8 3€c-Butylbenzeflect{ffi t€rt fuMbenzenet5.r5.0 fulbdl disrltfide

56.23.s Cabont€{rachloid€16407 Otlorobenzsne75{G3 Chlo{o€lhan€5t{&3 Cl orolonn714?.3 CftbDmefiane9$4!18 24 oohluene1643-4 44lioobluene9S12{ l3-Drbomo3{htompropaneIBI-4SI Okqnehloromehanerm-sH j,2-0ibtq'n@thane(EDB)

tLEs Dh.olnor€UlaneE5-5Ol l,2-Dichlorob€nz€ne5,r1-7+r l,Soiciloob€nzene

106{G7 l,4oichlorobenzeneE.71-8 Ddhrudiffuoomethane(Freoni2)7$3,r-3 l,l.Ddooothane107.06.2 l2$Monethane750$4 i,l.Did omethene1566s2 dsl,z-olchloroehene156{lF5 trdt5-l,2-oichloroelhene?&876 1,2-0icto.opropane1{2-2lA l,$Oid oropmpane5s+2G? a2{ichtoropopane$$s8€ t,l,DichiootrolerE10061{1-5 cis-l,}Dhhloropropene1006!{e-€ rans.l,}Dichloropropene101H1-4 Ahibenz€neEr€&3 Hg)caChlorobutadene501-71-t 2-H€!anon€(MBK}s-€e{ boprq}dbeuene1F876 +tsopopyltotu€n€

lEr44+. M€hy'ted-butyledrer

1lFlsl 4- dhy'-2,pentrnone(MtBn7Hrs2 Met|}4€n€ chloide9l-2G3 |hphtt3len€

F€ld exlracted

ljdks dry

pdks dry

!s,4q dry

!4kg diy

vs/q dryvqE dry!0&S dry

tS4(S dry

!s4q dry

|lgnq dry

!S/rS dry

ISAS dry

|Jg4s dry

UglS dry

pVrS dry

!g4q dry

pSeS dry

ldrs dy

tglgt y

pgro &ypS4(S dryldtS dry

pdkS dry

pdlq&v

w)sbl

llqs dry

lgkS dry

9s/}s drv

lEhS dry

!g4q dry

!g/fg d}y

ti9kS dy

ldlrS dy

ldlq dry

!9lS dry

trSfrS dry

psl€ ey

ls^s dry

lYlS dry

pglq dry

!9h ey

lJs4(s dv

pqts dvldlq dq

udlq dvp9t9 dry

lgks dy

r94€ dlvpg4€ dry

voc

sw 846 826086.3

126

6.3

6.3

6.3

6.3

6.3

6.3

r2.6

53_1

6_3

6_3

31.5

6 3

6.3

12.6

6.3

12.6

6-3

6.3

12.6

6.3

6.3

6.3

6.3

6 3

6 3

I ? 6

6 3

6.3

6.3

6.3

6.3

6.3

6.3

6.3

6 3

6.3

63.1

6.3

6.3

6.3

63.t

63.r

6.3

Thk lohorotory rcporl is nol,wlU u,ilhost aa aalho zed signtrue on the coret page.

I R€portabl€ DelEction Limit BRL = Below Reporting Limit Page 73 of 154

Page 367: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentific.tionM8F-18 2'-4,sA59803-15

Client P.oject #30r -88

Matlix Received27-Mar-O?

Collection DattTime2GMar{? 00:00

CAS No- Analrtz(s) Resuh FloC Anilj *RDL Dilatioa Method ReJ PrepzrcC Anolyzed Bdtch Atutbsl

VoLtilc OrBanic Compo||trds

Vohtle Orqanic Codbounds

Prepar€d by melhod SW846 5035A Soit (tow tevet)

l0+nt1 |}Prcpyt6'uone 8RL100.126 slyreno Bfudrc2r}6 j,t,t,2-T€lrad{o.o€thar€ gRL

79346 1,1,2,2_T€trad{oro€tt6ne BfiLt2f-184 Tdrad olo€hen€ BFL10e€8.3 Toluene BRLl)761-6 12,&Trit orobena€h€ 8RLrz0-€?r 1,2,+Tid orob4nzen€ 8fu715s 1,1,1-TridJorootllane 8RL?r-o'-5 l,l,2.Trid oro€dwE BRL

|4t{ dV

|lgrs tr}'pgts dry

Elq dy

ug,lq dy

uSIq dy

|lgrsf}

tr9*0 &yu€n4d/|l

uCts dy

abdyligkg dy

l|gls try

are dy|4/l€ dy

|'glqdy

ldks ry

lgrq fvpdrs dy

l&tqdv|Etqdrylglq dy

!S/rq fy

t€^g dy

lElq dy

7Ut3074130%TGIN%70.1il %

mdkg dwn'g4q drytrqr€ dryngnq dryflVfg dwn'qtS dyrngh 6yngnq d'y

lrqlq dry

.'19frq dry

&.144 %

st/'l8{6 &b(8

€T ETPH

6.3

6.3

6l

6 3

6.3

6.3

6_3

6l

6 3

6.3

6.3

6-3

6.3

6.3

12.6

6.3

63.1

6.3

6.3

6.3

6.5

63.1

1 X

I

I

1

1

I

1

1

1

1

I

1

1

1

1

1

I

I

1

!

I

I

I

1

1

29{,tar{7 29-tlar{7 7031790 RU

?94r{ rddtbrc€tEfla7t69-l Tftfttomfiuoromohane (F€on I i)9610-{ 13,}Tdfbopropane

503.6 12+Ttime$ylbenzeneros5./-o l,3sTrimeryt€naene75{l-4 Vinyl dllolilj€1SG2G7 |rtFxylorp95-47-6 o.xyl€ap10s!qs Tdr*ldr0|u|an

crz+7 Etd stter9s44+0 Tedffryl mehyi ether63r{2,3 Ery bn.h(nyt olterr00-m.3 D-ijoproprt dt€r6{5-0 Tei€utaml/ buly{ alcohol123.91-1 l,4{ioxan€

@-oo-1 4-Bronor(]oobonzere

ag7'?6 5 ldueft$

1/u6oat4 1?.Dktiddt1Ere44

le6e-5r7 DMbtonekae

Ertnctable Petroleum Hydrocarboos

Extaclabie Totd Petd€um tMrccadons

Prepared by method SW84.6 35508

mo€-c1€ Geii|e6r4763tr2 Fud Oa $268476.31.3 Fuol C{ #46055340-{ Fuel0llt6

[{E&looo MoWOI,x10100m0 Atiatim Fu€t

t d€itlied

Otl€r Oil

Told P€trdelm Hy(kaartms

Ca{sE lldlaitc l{.rdisattons

Su/rqgare Ealroibis&*2 lctddl@bcdE

Semlyohdl€ Orgrllc Compounr|l by GC

Organod otin€ Pedtcijes SW8,46 8081 A

Prepared by method SW846 3545A

ff{r,'z Aldin

BFL8Rr-8BLBRIBALBRL8nLBRL8ni-881BRLBHL8Rr-8RtsFt-

1011t2117tw

8RL

Bfu

BRL

B8L

BFL

BRI.

BRI.

BRL

BNL

BAL

7.0

7 0

7.0

7.0

7.0

7 0

7_0

1 0

7 0

7.0

2g{,1€r,07 3OMar-07 781/t3 DS

|dlq dv sw8$ SmtA 28-r&r.07 @.4pr.07 7t61739 IG

This laborotorf Epo.a ls ,rol vdjd *lrhou sn surtoriz.d slgtutla.e oa the cover page .i Repo@ble Deterrioo Limit BRL = B€tow ReDortins Limit Page 74 of 154

Page 368: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-48 2'{'sA5980l-15

Client Proiect #301-88

MatrixSoil

Received

2'l -Mar-01Collection Date/Time

26'Mar{7 00:00

CAS No. Anrqte(s) FIag *RDL Dilutioh Mertod ReJ. PrcparcJ Analyed Buth A tltst

Scmlvolrtile Org ic Compounds by cC

ooanodhrins Pesticites SW846 8O81 A

P.€paEd by m€thod SW846 3545A

3r$846 +8t63r$857 b-BHC3190&6 dBuc58-s+e g_BHc (undanel

t7+9 Chtodane12.51-8 4,a-O00 @,p')7266.s d{'-DDE (p,p,)

sc?$s a,{,OoT h,p,)m'5-f'r Dleldins50-€€-8 Endogllfan I3s213ffi Endosulfan lli(B1-07{ EndcdlanSllfate72-20.0 Endin?121_93-1 EndinAHehyde?6.44_0 H€fltadtlort2,4C5 Mefidyd or10r+r3 Hsdedltor EFoidestD1.352 Toxaph€ns51@?1€ act{odflls566&347 94 orda6s14{.7o5 €ndrh (6lone

r@t1-2 44-DE-&Efruorcbiphenyl(SlM1.2ai De'tsEhlotobiplEnyl(So

Pqlvcr{ofiated Biohenlh bv SW846 8082

Prepared by method SW846 3545A

!267+11.2 PCB 10161110420.2 PCB 1221nrrt-tos PcB 1232!,r@2r'9 PCg 124212612.2$6 PC8124811097{S1 PCB 1254110€68e.5 FCB 1260rteL&s PCg 1m21110G14.4 PCB l26E

1@t6aa2 4,1D&Odatuorobipheny'(3t)

ffi114.3 b@dlot6phsjyl(64

S.ftlvolclile Orgrnic Compounds by GCMS

S€mivoladlo Ooaic Compound6 bv SWP,46 8270C

P.epa.ed by m€Olod SW846 35508

8332.9 Aconaphhone?0&*{ Acoiaphbyl€n€6e$.! Anihn€12L12-7 ,4afiaecsn€1912.24€ Alrazjne1q!$-3 AzobenzeneDiphenyldiazinesiET{ &nuidns56-ss3 &nzo (a) aa$.acene

p.4 Ip,4 Ip a 1

:2,r 1

162 1

24 1p A 1

p1 1p_4 1p.4 1gzl Ip 4 1p t 1

p a l

p.4 r

32.4 {p.4 |

162 I

9..4 1

32.4 l

e.4 |

8FL

BFL

BFL

BFL

BFL

BFL

BFL

BFL

BFL

BNL

BRL

BFL

BFL

BFL

BFL

BffL

BRL

8RL

BFL

8RL

8fl1

NkSdrlpS4€ dry

wtqoy

lEtq dry

|,s4(s drytS.l(g dry

|dksdrv

usks dry

|JgkS dry

pgkg dry

tgtS dry

|Jgfrg dry

llg4s dry

l,s,ks dry

!s'lq dry

@k9dryp4rs &y

pgKg ory

pgks dry

us,4(sdry

Ms&y

tu150 %

3,150 %

tlgks ray

!S,kg dry

[S,lq dry

p(ylq ory

pq'q qry

pdk4 dry

!94q dry

psh dry

ldtS dry

3+150 %

il.l5t %

swe,16 808tA

sw846 8082

sw846 8270C

2&Ma47 tz-Aptlt /0i179 IG

28-|'/,ar07 3Gilar{7 7031738 Sl',

29-Mar47 09Apr-07 7m1774 M.B

51

76

55

60

64.9 1

64.9 I

54.9 1

64_9 1

64-9 l

64.9 1

64.9 1

649 1

643 1

BRL

BRL

BRL

BBL

BRL

BRL

BFL

BFL

BFL

874

874

874

8r4

871

874

874

674

gRL

ORL

BRL

8RL

BRL

BFL

BAL

BFL

lsnq dy

!S/rS drypglq drypdks drypg/lg dry

fS4€ dry

us,ls ory

tigtS dry

Thb lahoratory rcpofl b not wlid withou! an aathorized signalsrc oa tht .oeer page.

+ R€ponable Detection Lirnit BRL = Below Reporting Linrr Page 75 of 154

Page 369: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldedtihca tiotrMEF48 2'-4'sA59803-15

Client Proiect #30 t t 8

Collectioo Date/Time26-Mar47 00:00

MafixSoil

Received21-Mar-07

CAS Na Aialyte(s) Fl4S *R.DL Dil ttion Method Rel, Pnpored Analfzen Ba,ch An4lfsa

Semivolatile Org.nic ComFounds by CCMS

S€mivolatle Oroanic Comoounds W SW846 8270C

Prepa.ed by method SW8,l6 35508

5one{ B€nzo (a)py€n€205-93.2 Benzo(b)fl|,anfi€ne1s1-2+2 Benzo(O,h.i)p€rytene207{8-9 B€nlo E) nuoEflhene6S850 oenZoiC acid10G5r.6 BsW atcohol111.!r1r Bis(2-chbroelhoxylrnetEne1114-1 gs(2dtofoefiyi)sttFr

3S€e324 EI5(2dOolsoFEpytle{|e'1t7.81.7 Bis{2{ht{h.dy0phlhatabr01-5s.3 4€rqnoph*vphffytetEf85,6&7 Buty h€rr4i phthahblF74{ Caft€rol€s9{}7 .t-cflo|'o-3-|nellrytdrdtol

10F47-B 4ctdoros linesr,ss7 zcllduBphfialene9$t{ 2$bophenol70572-3 lChbophffyj phenyt sh€r21&01.9 Cnays€n€s$1I3 ofr€fuo (Ah) anhEc€ne132-6,t4 DibenzoluEn$-so1 l,2{idh.abenrenB5.11-7+1 l,3[IdorobeEene16{+7 l,4Dd robei?ene91a41 g,3..Dchhrobenzidne

1Al-€+2 2,4.Didorophend8166 2 Diettrylphhdat€131.113 Dmelhylpnhalab105.67.!1 2,4{ilr|€q&h€nol*7+2 D-n-butyl phhahte534.52r l,SDinitD2fl€fltlphend5r{&5 2,4.Dnihophenol121.1+2 2,4-Unikdotr€nqoGrD2 2,6.0idtrolotu€rE117{.4 D+odyl phtEtate206-4411 Fuor3ntEnesSXt-7 Ffuo|En€1M+1 HexadilorDbqrzeneo{€a? Hexaciloohbdeno.r{r_4 Hexadoocydopeitadi€n€6r-T2-1 H€rad ooetmmrs!-9si lndem(1,4d)py@nost2{ !_f dnyl6ph$Etsne7l{$1 lsapho|ono91{7-6 2.lrohytmphdElelroe6-{&7 z{etrylphsd

108.!$4, 3,4+rdhtphoidr06r!L591203 ilapht|atqlew1+1 2.Nibofltinesos2 SNitoanilne

BRL

BAL

BRL

BHI.

BRL

BFLgFL

8fi1

BRL

8HL

8RL

8RL

8nLBNLBFLBFL8RLBRISRLBNLBFLBRL8RL8FLBRIBRLBFLBRL8RL8Rr8RLBntARLBnIBBL

9fll-

8nLBALB8L

8RL8RLBRIBNLBRLBBLBRLsfl.

8RLBnt8FL

I

1

1

1

I

I

I

1

1

1

I

1

I

1

1

I

i

I

1

i

I

I

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1

1

I

I

1

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1

1

1

I

1

1

I

I

1

1

1

I

1

I

1

i

I

lglqdy 871

wlg try 874

pd*s ev fi4

db dv 871

US,lqdy 871

$ctgdry 814

ldhtrV a74

l4kg dry a74

|dt! try tt{

lrytS dy 871

gglqdy 871

dtg dy a74

dE fy a71

l4k! fy a74

l4ts dy 874

!9lqdy 874

wrg dy 874

ldrq fy a74

ldrg dy 87,1

t446v a

dh dv E71

lg4qdy 874

tdLSdy 874

!S'kS try a74

t4ilS fy a

Wlq fy a74

dlq dy 871

Igflqdy 514

pdks dy 874

tMg dV 871

sS*S dy 874

pgtS dy 874

ldb 6y 874

$,{q dy 874

ldks dy 874

lSitS tr)' 874

!S^S dry 874

wlgdry a74

!S4€dy 871

ugfqdy 874

!dfr{ dy 871

tryxs d) €74

!g/ig dy O4

pdl€fiy 871

lgnqdry 874

Udqey 874

lgXg dV 874

lcrs fty 814

wl.gd''t a74

Kn€ dy 874

swB4€ &270c A.Illtar.07 o&AF{i 7llB1 z4 til.B

Thit laboratory Eporl it nd wlid wirhou aa ruhorded s,gnolar. oB thz cover psge.

+ Reporbble Deteqion Limit BRL = Bdow Repoding Lirnir Pag€ 76 of | 54

Page 370: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semole ldentificationM8F-48 2'-4'sA59803-15

Client Proiect #l0l-88

MatrixSoil

Receivcd2'7 -Mar-07

Collection Date/Time26-Mar-07 00:00

CAS No. Atslyte(s) Resull n"s Unils *RDL Dilation Method Rel: PrcF.el Anauzed Batch AtuIjtt

Sehlvolrtlle Ory.nlc Compounds by CCMS

Semivoktile Orqanic Coooounds bv SW846 8270C

Prepa.ed by method SW846 35508

t00{1{ +t{itroanjhsl$gl3 i|ilrcb€flzeno8&7rs 2-tlitoph{El100&-7 +Nifophflol6e7$9 fl.Nitrosodmethylarnine@14-7 &Mtoso&n-propylaffie8+30j N.Nitosodphenylamine8?.t&5 pendiorophenol

8541{ Phendlhrene10&9t2 Ph€nol1?3{04 PyEn€110-861 q/ndne

1!182-1 li,+Tichlorobenzenes54i-,t z,4,tTditomphend8&os2 aa,FTrKfilobphenol

,r?1{0{ zawebhalyl

fi7-124 z-fr-bqlard

1t65{'4 llifrofu1zflN4s

1t6&c Phenol-(ls

t7t85t4 TerptEnyl-dl4

118-194 Z4,FTtbtonophenol

s!1i84€ 8270C

sw846 74714 02-4U47

2gl,lar 07 0&ApF07 ?031774BFL

BFL

BFL

BNL

BRL

BPL

BNL

BRL

BRL

8RL

8RL

8RL

BRL

BRL

8RL

57

72

62

76

lgeS dry 35m

|SAS dry 874

l4ks dry 871

$eS dry 3500

!s^s'1ry E74

UdkSdty 874

lgftS dry E74

!S.4$ ty 874

!0AS dry 874

IS,4q lly 874

,r9ftS dy 874

lglq cty 874

pdkS diy 674

!Sr1q ory 814

pdrs (ty 874

i&134 %

11110%

3+130%

15,t10%

3+|fr %

t 1 1 t 0 %

mg4(S dry 0.0:33

mg/kQ dry 1.11

mC.4q dry 166

mgks dry 0.555

nS/kS dt! 0.277

mdE dry 0.555

rdrg dry 0.832

mg/kg dry 1.66

mg4 o.o1o0

rngn 0.0150

mg,l 0 0050

mM 0.002s

mgl 0.0125

mgil 0.00014

mql 0.0075

rng,l 0.0150

M 8

Totsl Metrh by EPA 600{l/7000 Serl6 Methods

SPLP M.rds by EPA Il12 & 6000t000 Serler Mefiod!

7139.9?4 lt€tulry

Totrt M€tsls by EPA 200 Series M€thods

7140P4 $lvel

14&&2 AFeflc

7140-39-3 Batiun

7140..C9 Ca&dtjn

7!r{!t7,3 Clhffinium

7439.t4.1 Lead

nP2.4sz Sds !m

SPLP Eftastion

741021 glv€r

74,$138-2 AFenc

7il4&S3 BariLm

7a,4049 cadni|Jn

741l|{13 Chromium

7<q974 tilomry

74$92n [.eed

7tQ1s2 Sd€nium

Gcn€trl Ctcmlstry Pr.&m€t€rs

8RL

BFL

3.43

393

0.871

10.4

28

BFL

EPA2M.7 02-&r{7

Compleled

BRL

BRL

0.0150

8RL

sw846 1312 28-l'lar{7 2&Maf{7 7031763 8D

sw846 t3rz6010B 30-MaL07 02-!{rrl7 7031805 LB

Sl{846131a7470A ' @ Aprc7 7031806 YP

SW846131260108 02-Apr{7 7031805 tt

BFL

BffL

o0210

BHL

% Solds SM2540Gitod. 30-{lar{7 3&Marfl 7031879

This labamlory .epod ie nol wlu niahout an aurtorized signature on the cow, p{ge .

r Reportable Detection Limit BRL = Below Reporting Limir PaEe l'7 of 154

Page 371: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample lde ificationM8F-{9 ?'-l'sA59464-06

Cliept Proiect #301-88

MatrixSoil

Coll€ctiotr D6te/TimeI 5-Mar47 00:00

Receiv€d19-Mat07

CAS No. Arralrtz(s) Resdt Fl4e ani6 'RDL Diluio,' Mdhod Rq tueparcd laalyen Bdch Atatl'st

Voladl€ Or$$k ComDo$ndt

VOC Enraction Field extraded

uS/kgdry 4-5pgkSdry S0.9

ugkg dry 4.5pClgdry 4.5

lSfiS dry 4.5

rdkS dry 4,5

rdkSdry 4.5

ugr0 dry 4.5pdkgdry 9.1

Ugn(gdry 45-4

Usn(g dry 4.5pS/kSdry 4.5

lCASd.y 4.5pdrsdry 22.7

US/kS dry 4.5

ldkS dry 4.5

ttgtlxsdry 9.1

rqlgdry 4.5

Pdkg dry 9.1

!dl(g dry 4.5

!Sn(S dry 4-5

rcnrg dry s-1pS/kS dry 4.5pdks dry 4.5

ldkS dry 4.5

Igl€ dry 4.5

ldkS dry 45pSilq d.y 4.5

uglg d.y I I

ldkS dry 4.5

!S/kS dry 4.5

ldkg dry 4.5

WkSdry 4.5ySAS dry 4.5pdkg dry 4.5pc4Qdry 4.5

lgkSdry 4.5pdkS dry 4.5pgksdry 4.s

t S,/kS dry 4.5

udkS dry 4.5

ldkS d.y 4.5

t g|!g d.y 45.4pgtgdry 4.5pdkgdry 4.s

ldkS dry 4.s

ldkg dry 45.4

lgkg dry 45.4ps/ks d.y 4-5

m.Maf{7 m-i[x07 7 031156 ADVolatile Orqanic ComooundsPrepa.ed by method SW846 5O35A Soil (low levet)76-13-1 1,1,2-Tddorotrifluorcetftane(Fr€oFRL674+1 Acelono BRL107-13-r Acrl'lonitile 8RL71'112 Benzen€ BRL108-05r Baoinob€nzene BRL14'w'5 Brctrmahloromelhane BRL75-271 Bromodicfiloromethane BRL7+24ts2 Bromofo.m BRL7r€99 Bromornelhane BRL78-e'3 2-Butanone (MEK) BRL104-s1{ FButylbenzen€ BRL13s€8{ sec€utylbenzGn€ BRL98{t6{ tBrl€utylbenzene BRL7t15-o Ceftondisulfde BRL56-?$s Cafuon tefachlonde BRLt0E-90-7 ChloDbenzefle BRL75{G3 Chlooethane BRL676G3 Chtorobrm BRL74€71 Chlorom€thsne BRf9s-49{ 24hlorctoluene BRL1ftr-43-4 +Chlorotoluen€ BRL9G12-a 1,2-Dib{ome3-chtoropropans BRL12{-44.1 Dibrornochlofodn€tEne BRL1c6-s3-4 1,2-Oibrono€tharF(E08) BRL7+913 Oibromomethane BRL9s-5,01 |,2_Oichlorobenzene BRLs{1-7}1 l,3-OiclronoLbenzene BRL10&6-7 l,r|.Dichlomb€rEene BRL7r71-A Dichlorcdifuoromethane(Freonl2)BRL75-34-3 |,l-Dichlorcethane BRL107{6-2 l,2-Dichlorcothan€ BRLz5<)5-4 1,l-uichtoroethene BRLr5s5g2 cis-1.2-Dichtorcethen€ BRLt5eq)-5 tEns-l.2oichtoroethene BRL7a{7-s t,2.Oichlo.opropane BRL142-28.9 l,Soichloropfirpane BRL50+20'7 2,2-Oichlo.opropene BRL56!5s€ l,l-Dchtoroplopene BRL1006r{1€ cjs- l,}Dichloropmpene BRL10061{2{ trans-1,3-OichloropoFene BRL10041-4 Edlylbenzene BRL07{6+ Hsxad orcbutadiene BRL5s1-7e{ 2-l-loxanone (MBK) BRLsa{2{ lsopropylb€nzene BRLss-€74 +lsopropyltoluene BRL1634{4-4 Mettt'l tert-b{tyt ethe. BRL'10s10-1 +Methy-2-pentanonelMlBK) BRL7s{92 Methyten€ .htodde BRL

SW 846 S?60S 21{nar-O7 22-Srar-O7 7031233 TR

9l-2()-3 l,laphthalene

Page 2E of 152

th& latotuloq r4,s'l b uot r'y'i l uitttotl, on strto;zcd sigfista.e on thz cov.r. page-

* RQortabl€ Det€ction Linit BRL = Below Reponing Limit

Page 372: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdeutificationM8F-49 2'-4'sA594&t-06

Client Project #301 -88

MatrixSoil

Collection Date/Timel5-Mar-07 00:00

Received19-Mar-07

CASND. Analfu(s) Flag Unils *RDL Diltltion Llethod R.I. PrcFa.ed tumllzed Ba!4h AnoDst

Voldle Orgrnic Compounds

Vohlil€ Oroanic ComooundsPrepared by method S!V846 50354 Soit (low tevet)'t03stl rFPropylbenzene BRLi0G42-5 Styrene ARL630-20{ 1,1,1.2.Tetrachloro€than€ BRL793{-5 1,t,2,2-Tetrachloroethan€ BRLrz7-rs-a TetEdilotoediene BRLl0S€0-3 Toluene BRL87{r{ 1,2,}Tridtlorobenzene BRL120{2-1 1,2,+Trid{orcben2ene BRL71-55{ 1,1 ,.1-Trichloroethane BRL79411.5 1,1,2-T.ict o@elhane BRL79{1{ Tdciloroethene BRL75{s-4 TridtlQrofluorornelhane (Freon 11) BRL9Gr8-4 l.2,}Trichloropropane BRL95{xf6 1,2,+Trimethylbenzene BRL10e67{ 1,3,5-Trimethytbenzene BRL75{14 Vinyl cfiloride133G20? m,p-Xylene9547-€ o"Xyl€nelo$Sq4 T€trahyd.ofurdn

@-2S7 Ethyl 6h€rs€,l{s4 Ten-ahyl m€lhyt etl€r€,3?-s?-3 Ehyltert-butytether10e20'3 Diisopr0pylether75-65{ Tert-Butanol / butyl alcohol12+91-1 l,+Dioxane

Su'rogats rBcowrtss:460-ao4 +BrcnofluorotEnzene

N3/-26-s foluene4g

t 106.0474 1,2-Dichlorcethan6-d4

186A-53-7 Abronofluarcmethane

E{reclrbl€ Peiroleum Hydrocaft ons

Extraclable Total Pet.oleum Hvdrocarbons

Prepared by method SW846 35508

800661€ Gasoline68476-30-2 Fuel Oil #268a7B3i-3 Fuel Oil #46&55$0G4 Fuel Oil #6Mm{Doo{I} Motof OilJOoloOooO Aviation Fuel

Unld6nliti€d

Orher Oil

Total Petroleum Hydroc€rbons

C9-C36 Aliphatjc Hydrocerbons

s{rrogsf'g rEc9Msniesr

$a6-33? 1-Chlooocladecane

SemlvoLlllc Orgs|lic Compo{nds by CC

Orqano€f orine Pesticides SW846 8081A

Preparcd by mehod SW846 355083090G2 Alddn

BRLBRLBRLBRLBRLBRLBRLBRL8RLBRL

9610110898

8RLBRL8RLBRLBRLBRLBRLBRLBRLBRL

u

pg/kg dry 4.5

wKg dry 4.5

tiSftSdry 4.5

pS./kg dry 4.5pgkS dry 4.5

trg/kg dry 4.5pg/kg dry 4_5

tis/ks dry 4_5

us.ixg dry 4_5

t4Jxgdry 4_5

t4iKg dry 4_5pg/kg dry 4 5

lrg/kg dry 4 5

!g/kg dry 4 5pdkS dry 4.5

t€/(S dry 15

tdkS dry I 1

FSikg dry 4.5

WkS dry 45.4

pSikS dry 4.5

t S l € d r y 4 5

PdkS dry 4.5

pq/kq dry 4.5

pg/kg dry 45 4

pg/kq dry 90 9

7G130%

70-130 %

70-130 0.1

/0-1n %

mg/kg dry 17_2mgn(g dry 17.2mryig dry 17.2mg/kg dry 17.2mgLikg dry 11.2mdkS dry 17.2m9k9 dry 17.2ftq*.S dty 17.2mg/kg dry 17.2fl|gftS dry 17.2

40-140%

I

I

1

1

1

1

1

1

1

1

1,1

,1

1

1

1

1

1

1

1

1

1

1

1

1

SW 846 82608 2t.Ma'.07 22nna47 7031233 TR

+CTETPH 21-MarO7 21-M^t41 7031167 DS

t dkg dry 5.14 SW846 8081A 2O-Ma(41 25 at47 1031068 TG

Thit laborcory repod ir noa wlu w hout an suthorhel signatun on the cowr page.

* Reportable Detection Limit BRL: Below R€po.ring Limir Pase 19 of 152

Page 373: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeEtificationMtF{9 2'-4'sAs9,t&L06

Clieot Proicct #301-88

MatrixSoil

Collecrioo Dater'TimeI 5-Mar47 00:fi)

Receivedl9-Mar-t)?

CAS No. l,raws) Retall FI4g A l l , s *RIrL Dllalian HaItod Retr, Prepor.4 ,lrslfud Barch ,lnawSemivoladle Orgaric Compounds by CC

O.oanochlorine Pesticitres SWB46 go8tA

Prepared by liethod SW846 3550831e{46 s-Bl{C31e{57 b_BHC3r9&r€ d.BHCs6{$9 g,BHC (Lindane)5/.74-9 Ct{qdan€7244s 4,+DDD (p,p,)?2€5-e 4,4-DDE (p,p)50-2+3 a,4ODr (p,p')6t -s7.1 Dieldrins5s9o€ Endosulfan I33213r-€$9 Eodosulian ll'103r-07{ Erdosulfan Sutfate72 -2Ga En&in742r{$a Endrin Ahehyde16,{44 H€ptschlorf24rs tir€horycflor1021-57-3 H€ptaclrtq, Epoxide800135-2 Toxaphene5103.7',1-9 a-Orlodane55663+7 +Chlordane*r4!r4705 En&in K€t no

Szr'og6le aecovsriies,'1 $8ea+2 4, 4OB4detutorodphenyt ( Soz05r-21.3 De@diorobiphenyt (SdPolvchlorinated Bioh€nvls by SWB46 8082Prepsred by mehod SW8rt6 355081267+11_2 PCB 10t6111044.2 PCB 122111141n6-5 PcB 1232s346+21€ PCB 124212672-294 PCB 124811097{91 PCB 12541100€-82a5 rcB t26O3f12+2+5 PCg 12621110{}14-4 PCB 126a

S|,TEgaia rgcor/a'tesr1 tEF*a+2 4,tto&Adaf, mrobiphenyt (s4ms1-243 De@c'l,tombiphenyt (Sr)

SeEivokaile Orgritc Codportrdr by GCMS

BRLBRLBRLBRLBRLBRLBRLBRL

6RLSRLBRIBRLBRLBRL8RLBRLBRLBRLaRtBRLBRL

407/

BRLBRLBRL8RL

BRLBRLBRLBRL

40

ldkS dry 5.14 1

tdkg dry 5. 14 1

pdkg dry 5.14 1

ldkS dry 5.14 I

ISftg dry 2s.7 I

l|gikg dry 5.14 1

pglgdry 5.14 1

ldkS dry 5j4 I

IdkS dry 5.1,1 1

Igikg d.y 5.14 1

lgfg dry 5.14 I

ldkSdry 5.14 t

$S/kS dr, 5.14 'l

Fg/|(g dry 5.14 1

pdxg dry 5.14 1

ldkS dry 5.14 t

tgkSdry 5.14 1pgifqd'y 25.J 1

PqXg dry 5.14 1

!rytS dty 5j4 I

ldkg dry 5 14 1

3L150 %

3L150 %

SW846 8081A 20-Mar{7 z5-lrar{}7 7m1068 TG

SW846 8082 22J,,,a147 244 at47 7031274 Mpt gl€ dry 10.3

Lrcl€ dry 10 3ydkSdry 10.3

udrS dry l0 3pgtS dry 10.3

US/kS dry 10 3

|lg4€ dry l0 3pSftSdry 10.3

Pdkg dry 10.3

30'150 %30-150%

Semivolatile Orqanic Compounds bv SW846 8270CPrepared by mehod SW846 35SOB63.32{ Aoenaphthene208-gG8 Aconehtrylen€62{}3 Anitino12G12-7 A|rU1|ECAn€1912-2+S AEai,trF10&313 Azob€rizenoy'Diphenyldiazinev47-5 B€nzldin€56-5t3 Benzo (a) anthracen€

aRrBRLBRLBRLBRLBRI-BRLBRL

pdlq dry

ldkg dry

ldq drypS4€ d.y

FgkS dry

rdks dry

ldlg drypdlq dry

427 1

427 I

427 1

427 I

427 |

427 'l

427 I

427 1

sw846 8270C 22-ltat47 2+Ma(47 7001278 M.B

This bnodoe rapad i| Eor vslitt fr ho( on aartorized signaure o^ tlE cov.r page.r R€ponable Detectio0 Limh BRI = Below R€ptrting Limit Pag€ 30 of 152

Page 374: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple ldentificationM8F.19 2'-4'sA59464-06

Client Proiect #301-88

MatrixSoil

Received19-Mar-07

Collection Date/Timel5-Mar-07 00:00

CAS No. Arlalfu(s) F|AS *RDL Dilatioa Method Rztr Pnpared Analfied Batth AnalDt

Semivolriile Orgsnic Compornds by GCMS

Sgmivolalile Oroanic Comoounds bv SW846 82ZOCPr€par€d by method SW846 3SS0a50-32{ Benzo (a) pyrene20tgq.2 B6nzo (b) fluoranthene191.2+2 Benzo (g,h,i) perytene207{8.9 Eenzo (k} fiUoranthene6545-0 Benzoic acid10G51{ Benzyl alcohollt1-91.i Bis(2-chtoroethoxy)methane1llaaa BiB(2<hloroethyl)ether3S63&324 Bir(2-chloroisopropyl)ether117S1.7 8is(2-€urylhexyt)phthalate10155-3 +BrornoFhenylphenyief|ero6{s7 Buq/| benzyl phttlalate86-7,1{ Carbszote5s5G7 +ChtorD-$methytphenolt08-47€ 4-Chtoroaniline91.5&7 2-Chtoronaphthalene95-57{ 2-Chtoophenol700$72'3 +Chtorophenyt phenyl ether21eO1€ Chaysen€53-7G3 DiberEo (a,h) anthracener 32444 Djbfizofurarl95-5Gl 1,2-Dichlorobenzenel'41-I$1 1,3-Dichlorobenzene10s€-7 1,+Dichlorobenzene91.9+i 3,3_-DichtofoberEidine121!832 2,+Dichtorophenol844&2 Disthytphthatate131-11-3 Dinr€thy'phflratate10S74 2,+Dimettrytphenolu-7+2 Di{-butytphthalete$4-s2n 4.6-Dinito-2-m€thytphenol51.2+s 2,4-Dinkoph€noli2t-14+ z,4-Dinitotoluene60F2G2 2,6:Dnib|ololueflei17{4-o Di{r4ctylphhatatemH4-0 Fluoranhene&f+f Fluoronel1&7+1 Hexachlorobenzene87{+3 ilexadtlorobutadiene71414 He)(adtlorocyclopentadiene67-72-1 Hexadoroethan€i93-39'5 In<leoo (1.2,}cd) pyr€ne90-12.0 1-Methytoaphthalene7E-5gl lsophorone91-57{ z-llethylnaphthatene96-4&7 2-Methylphenolt0&39-r, 3.+te{fiy'pfienol10€-4469-2G3 NaphthaterE

6-744 2-Nilroanitine

SNiboaniline

BRLBRLBRLBRLARLARLBRLBRLBRL8RLBRL8RL8RL8RL

BRL8RLARLBRLERLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRL447BRLBRL8RL8RLBRLBRLBRLBRLBRL

BRLARL

SRLBRLBRL

lS/kg dry 427

tg/kg dry 427

!g/kg dry 427

tdkSdty 427

Ug/kS dry 427

US/KS dry 427

!s/kg dry 427

!9/k9 dry 427

ldkg dry 427

!g/kg dry 427

trs/ks dry 427

!S/kg dry 427

lSftS dry 427

lgftgdry 427

rcrkS dry 427

Ugikg dry 427

US/kg dry 427

lSftS dry 427

lSftS dry 427

ldkS dry 427pglkgdty 427

IdkS dry 427

[qkg dry 427

UOkS dry 127

USrkS dry 427

usrks dry 127

UdkS dry 427

USAS dry 127

UdkS dry 427

lgkS dry 127

Ugkg dry 427

IgkS dry 427

Ugr(g dry 127pqxSdry 427

!g'kS dry 427

Ug'kS dry 427

u94q dry 127

ug{q dry 427

UgkSdry 127

lCl(gdry 427

!S/kS dry 427

lgrkS dry 427

USI(g dry 427

us/ks dry 427

ldkS dry 427

rc/kg dry 421

lgksdry 427

ldkS dry 427

FS/IS dry 427pS/kS dry 427

1

1

1

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1

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SW846 8270C 22-Mat47 244tta(Ol 7031278 M B

This l4boratory rcpon is ^ot vald rgllhoat ad aldroized sEnaure oh thc coyer page .

+ R€portabl€ Detedion Limit BRL = Below Reporting Limjt Pase 3l of 152

Page 375: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sa-rnple ldeotiflc.atiotrM8F-49 2,-4'sA59464-06

Cliaot Pmieci#301-r8

MatixSotl

Colleciioq Date/Tirpel5-Mar-O? 00:00

Receiv€d19-Mu-07

CAS No. thralyte(s) F"g 'R.DL Ditaion Mdhod ReJ Preparcd ANIWd Botch Anallst

Semlmlcaile Oryrnlc Compourds by GCMSSemivolatile Oroanic Comoounds bv SW846 B27(rcPrepared by ntetEd SW846 35508100{1.€ 4-Nit'od line98-9+3 Nibobenzene0+75'5 z-Nitrophenol10G02-7 4Nitropheoo62-7+9 N-Nihdsodirnethytamine6C1{+7 ll-Mtosodi.n-propytamine8630{ N-Nitrosodiphenylamine87€0{ PefltrachlorophenolE5-01{ Phemnthrenel0g-95-2 menol12900{ Pr€nE110{6r Pyrilin€120-82-i .1,2.+Trichloro6enz€ne

95-95-4 2,4,$Tricfitorophenolaa,o€-z 2,4,6-Tridttorophenol

SsnDgate aecow r€s.'321404 24uor6iphd1yl367-12{' 2+luorophenol416r{p4 Nitobenzerc451t6542-2 Phend4s171&614 Terytwvl-dt411a-794 24,6-Trib@nnphenol

lgkS dry 17rO

udkSdry 427

US/kSdry 427

ldkg dry 1710

udkS dry 427

WkS dry 427

uSAgdry 427pdrgdry 427

tgt<gdty 427pgftg dry 427pdks dry 427pgkgdry 427

FdkS dry 427pdl€ d.y 427

lEftS d.y 427

30.130 %1U110 %30'130 %l r t l 0%3Gtn%1r110 %

r€ikg dry 0.0310

nrgL/kg dry 1.0'l

n'gkS dry 1.52

ftEftg dry 0.506

mgr'kg dry 0.253

n{l/kg dry 0_506

nrgkS dry 1.01

||lgts d.y 1.52

nEil O-010O

mgd 0,0150

mgr 0.0050

mgl 0.0025

n€rl 0.0050

mgn 0.00040

ngn 0.0075

r€rl 0.0150

%

BRLBRLBRLBRLBRLBRLBRLSRLBRLBRL4€6

BRLBRLBRL8RL

7764

6387

I

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SW846 8270C 22nnat47 214tar47 703127A M.B

Totrl M€trb by EPA 6000/?000 sffie! Meahod!

743997s M€rEUry

Totd MetrtB by EPA 200 S€rie! Meahods

?41S22-r Silver

21.44.3€-2 Ars€nic

74itr!39-3 Barium

744G:t+9 Cadmium

z!():u-3 chromium

743+92-1 L66d

262{9-2 Selenium

SPLP Met ls by EPA ISrl & 6000fl)00 S€ri€r Merhods

SPLP E'tredion

71,{G22-1 Silv€f

744G3&2 AEenic

744q393 Barium

744O4$S Cadmium

7a,1r)-47-3 Ch(omium

2(|947€ i/krcury

7431)€2n Lsad

?624S2 Seldnium

C€reral Ch.tnfutrjr P|tame 1er3

% Solids

sw8,t6 7471A 234d-O7 8.t!tdt47 7031306 yp

EPA 200.7 2$Mar{7 24-fr,l{-07 7031305 HB

24-Nlef47 ' LR

24-t\.t r-07 ' HS

SW8,f61312 21*lz(47 21-ttat47 7031229 BD

SW846 13fZ60l0B 22+.,.tt47 23.Nlato7 7m1323 tR

0.0683

BRL

1_64

2t.a

BRL

4.29

23.6

BRl-

Compl€led

SRL

BRL

0.0r 8€BRL

BRL

BRL

0.0497

BRL

s4.5

swB46 r3ra7470A

sw8,t6131?J6010823.&!ar{7 7031324 yp

2 vbr-O7 7031323 LR

SM2540 G [rod- ?2-Mat47 22+J{47 7031302 YM

Ihit labtuorf Eport is natedilt'ithoat oaaudtoi4cd sigrrtan od rhe cow, page,* Report ble Detectioo Limir BRL = B€low Rsporting Limit PsAe 32 ot 152

Page 376: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8F-50 2'-t,sA59,t5447

Cli€nt Project #301_88

MatrixSoil

Receivedl9-Mar-O7

Collection Date/Timel5-Mar-07 00:00

CAS No, .4aaly.e(s) FI"C 'RDL Dilation lr{ethod R"l. Prepared Analfred Bdlch Anal!$t

Votraile Orgmic Compounds

VOC Extracton

9t-2G3 tGphthalene

pstksdry 4.opgks dry 7S.4pgks dry 4.0pSftS dry 4.0

!C&S dry 4-0

lgrkS dry 4.0pgtxgdry 4.D

!S4<S dry 4.0

!g/kg dry 7.spg/kg dry 39.7

!g/kg dry 4-0

!g/kS dry 4.Opgr<gdry 4.0

Ug/kg dry 19.8pg/kg dry 4.0

Lig/Kg dry 4.0

!g/kg dry 7 I

ldkS dry 4.0pgJkSdry 79pdkS dry 4-0

!g/kg dry 4.0

!g/kg dry 7.9

!g/kg dry 4.0

!g/kg dry 4.0pdkS dty 4.O

ldkg dry 4 0

!g/(g dry 4.0

FS/kg dry 4.0

ldks dry 7.9

US/tS dry 4.0pdkg dty t.opdrs dry 4.0pdks dry 4.0

UdkS dry 4.0

Udkgdry 4.0

!g/,1(0 dry 4.0

MkS dry 4.O

!gl(g dry 4.0

ldkg dry 4.0pdkg dry 4.0pdkS dry 4.0pdkg dry {.0pdfq dry 39.7

!S/ko dry 4.0y9/k9 dry 4,0

udK$ dry 4,0

ugKs dry 39.7

lgKS dry 39.7

,.ISlkgdry 10

20-Mar'07 m.Mar{7 7031156 BOF€ld extracled

Volatile Oroanic Compoundshepared by method SWE46 5035A Soit (tow tevet)7G1}l 1,1,2-Ttichlorotiftuoroe,i-Ene (FreoERL67€+1 Aoetone SRL107n3-r AdYlonfit€ BRL714Y2 B€nz€ne BRL106-86-1 Brcmob€nz€ne BRL74-97-5 Bromo{fitoromethane BRL71274 Brofi€dj€*tlorom€lhane SRL7+2U2 Brcmofom BRL74{3-9 B&momelhane BRL7E-S.3 2-Butanone (MEK) BRLl(X-51{ n-Butylb€(uene BRL135-98-8 s€c-Butylb€nzene BRLs-06€ tdt-BtrMbenzene BRL7+15-0 Cafbon disutfide BRL56.2$.5 Cafbon btrachtoride BRL1o+!D-7 Chlorcbenzene BRL75-Oo-3 Chloaoethane BRL67{G3 ct o.oform BRL14+7-3 Chlo.ornethane ARL95.$-e z-Chtorotolume BRL10G4il4 +Chtorototuene BRLsr2{ 1,2_Dib|brno-.3_chtoropropane BRLr24a8.1 Dibromochtoromethane BRL10e93-a i,2-Dibmlno€r,ane(EDB) BRL74-953 Dibloftofiethene BRL95-5F1 1.2-Dichlorobenzene BRLf,41-aJn 1,3_0{chlofobenzene BRL1O€F46.7 1,4-Did{Orcbenzen€ BRL7t7t{ oichlorodinuorornethane(Fr€ont2)BRL7+3+3 l,loict{o.oethane BRL107-6-2 |,2-Oiclllorcethane BRL7+35-4 l,|-Dichlofoethene BRL15e592 cis- 1 .2-Oichtoroethene BRL15d60-5 trms-i,2oichtoro€thene BRL78{7{ |,2-Didtkfopropane BRL142-26-9 l,3_Dichlorcpropane BRL5gGacz 2,2-Oidrloop.opane ARL56!58{ t,l-Dichtoropropene BRLt00€l{l{cis-1,3oict{ofopropene 8RLt00€r{2$tEns-1,3-Dichlorcpropene 8RLi0(F4i.1 Ethybenzene 8RL87{+3 lbxad orobutadiene BRL591-78{ 2-t-iexanone (MBK) SRL

lsopr@ylbenzene BRL99€76 +lsopropyttoluene BRLl€34-&-4 Meftyt ted-butytether BRL10&1G1 +Met.|yt-Z-pentanone(M|BK) BRL?5{+2 Methytene chtoride BRL

Thk lahorotory ppod is ttot volid Eirhoa an authoized siEaoture on the cover page

r Reportable Detection Limit BRL = Below Reporting Limit Page 33 of 152

Page 377: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentifrcstionM8F-50 2'4'SA5946,1-07

Clieot Prcject #301J8

MatrixSoil

Received19-lilar-07

Collection Date/Timel5-Mar-0? 00:00

CAs No. Aaabt4i FIag *RDL Dibtrion Mdhod Ref,. Prcparcd ,lMlJEd Bokh Anal}f,a

Volrtile Org'l||tc Co|npouf, dsVolatile Oroanic ComooundsPrepared by m€hod SW846 5035A Soit (tow tevet)

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

75{9-a Triclrl6oiuoromethsne (Freon 1t) BRL

i0$6tl n-Propy'ltr€rEene1{x}42-5 sgrene€3(!zt6 .l,l.l.z-Totrachloroethan€

7$34-5 J,l,z2.TeFachloroefiane127-1e4 TetadrlorcodBneio&aa-3 Toluene€7-61-€ 1,2,+TnchloroberEefle12G82n 1,2,4-Tridllorcbenzone715$6 1,1,1-Tddtloro€thsne7g{Gs 1,1,2-Trichloro€han€79{1i Trichloroeth€n€

SW 846 8260S zl-ltsf4f 22-Mat47 700123 TR

+CT ETPH 21-Mat47 21'll a147 7031167 DS

96{84 1,2,}Tfidlloropropan€95+16 1,2,+Trinethylb€nzene108{7{ L3,gTrimelhylb€nzene75{1-4 Vlnyl cfiloride133O.2L7 m,p-Xyl€n€9547S oFxy,l€|l€10999.9 Tetahtdmfuran6G2+7 Ethye$erse4{s{ Tert-smyl methy' etherfa7-92n EUlyt tert-buty' €[1er10€-20-3 Di-isoproptieth€r7a'€fl) T6rt-Bubnol / butyt stcotrol12!91-1 l.+oioxane

Srnroga{€ EcolerJbs,4&40.| 4-arcmofluorcbenzenem37-26-5 Toluene<ft)1 706047 4 l,z-Dbhtooethane4l186&$-7 Abtumonuorcnolhane

D,rtnctrble P€troleum HydrocarbontExtradabls Total Potroleum FMroca6onsPrepsr€d by method SW846 35508800631.9 casoline6847sE!2 Fue{ Oil #26847s31*! Fuel Oil ,t468ss!-{E-1 Fuol Oil #6rr098om0o Motof OilJ001@0oo A!,lalion Fuel

UnldenIifi€dOtler Ol

Total Pefoleum Hydroca.bo sC9-C36 Ajiphatic Hydrocabons

SafrolEtfo fEcot€nbsr&186-332 l4hlotoodedecarc

Scrnhohdle Orgroic Compo!trds by cCOraanochlorin€ Pesticides SW846 StAlAPrep€red by mehod SW846 35504300{0-2 Aldrin

BRLSRLBRLBRLBRLBRLBRLBRLBRLBRLsRrsRtBRL

99105113106

pdkS dry 4.0

lS^gdry 4.0ggtgdry 40

ldxg dry 4.0

ug[Qdry 4.0

lgrtS d.y 4.0

ISikg dry 4_0pgkg dry 4.0

lgLSdry 4.0

rdr€ dry 4.0pgfg dry 4.0

UCAg d.y 4.0pgkodry 4.o

udkg dry 4.O

ldl(gd.y 4.0

t{d4s dry 4.o

Ig/lgdry 7.9pdlqdry 4-0

lgkg dry 39-7

|,9,1q dry 4.0

|'/tgdry 4.Opgtg dry 4.0

tigl(g dry 4.0

t,Sftg dry 39.7

trg/fq dry 79.4

7&1U %76130 %70-130 %7G130 %

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BRL

BRLBRLBRLBRLBRLBRL8RLBRI-BRL

n4Lkg dry 19.1

dtCkg dry l9.l

rr€/ks drv 19.1

mgftgdry 19.1

rEftgdry 19.1

r€rtgdry 19.1

mgikg dry lS.l

nqhgdry 19-1

ng/kgdry 1S.1

nrgr'kg dry 19.1

44-14) %

pgl(gdry 5-5t SWE46 808fA m-Ma[47 X1tat47 7Gr1068 TG

fhis lzbratoq Eporr Is ,ot vsld tthort on outhottal sknd/|'t- on ahe uw. page.

i Reponable DetectioE Limit BRL =B€low ReDortiaa Limit Pag€ 34 of 152

Page 378: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldgrtificationMrF-50 2,-t'sA59,1at-07

Client Proi€ct #301 88

MahixSoil

Collcction Date/Timel5-Mar-07 00:00

Receivedt9-Mar-07

C,lS No. A,rolrle(s) Ft"S Uhia aRDL Dilutind Method ReJ Preparel Arrab'zed Bltch Analrsl

Sebivolrtile Orgatric Cornpo{rds by cCO.oanoc*rlodne Pesticides SW846 8O8tAPrepared by method SW846 355083190a6 +BHC319-0+7 b"BHC319-66{ d_BHC58-8$9 g'BHC (Lindane)57-7+9 Chlordane72+44 a,a-ODD (p,p')I2{+e 4,4.DDE (p.p.)5G2e.3 4,4-DOT (p,p)€o5t-l Dielddns5s€8€ Endosulbn I3321$65€ Endosulfan tl1031fi{ Endosulfan Sulfaten-m-a Endrin7421414 ErddnAldehyde76444 l-leptachlor724}5 tirethorychlorl02a-57J l-leptachlor Epoxide8001.352 Toxaph€Nre5103.71.9 a-C+ ordane55€€-3+7 gS ordane53491-705 E ldrin Kebne

Surrogale aecorcr'esrft3e 2 4,4D4-Odanuorobiphenyt (Sr)zo -2aa &cad orobiphenyl (Sr)Polvd odnated Biohenvls bv SW846 8082Prepared by method SW846 355081267+1r-2 PCB 10161110+ZE2 PCB 12211r141-16-5 PCB 123253169:21€ PCB 124212672-29€ PCB 124811007€91 PCB 12541100€{25 PCB 12603732+23-5 PCB 1262r1r0e1+4 Pc8 1268

Sunoga,' (@vedes:1 0iwc+2 1, 44 B-O ch n u orcb i p he n y' (S 02A&-2+3 Docz&lorobiphenyt (Sr)

Se dvoladle Orgr c Compounds by CCMS

ARLARLBRLARLBRLARLBRL

BRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

50a4

BRLBRLBRL

BRLBRLBRLBRLBRLBRL

5075

BRLBRLBRLBRLBRLBRL

BRLBRL

!S4(S dry 5.51

!S/kS dry 5-51

fdkS dry 5.51

!g/kg dry 5.51

Ug/kg dry 27.5

pdksdry 55l

Ug/kg dry 5.5'l

UdkS dry 5 51

IgkS dry 5.51

US/kS dry 5.51

pg/kS dry 5.51

ugkS dry s.s1tSlkg dry 5.51

t SikS dry 5.51pg/kg dry 5.51

ItgtKgdry 5.51

!S/kS dry 5.51

!g/kg dry 27.5

ug/kg dry 5.51

ISAS dry 5.51

!g/kg dry 5.51

30-150%30-150%

tiglkg dry 11.0

ldkS dry 'l1 0pqkS dry r r.0

!g/kg dry r r.0

Pg/l(g dry 11.0

!g/kg dry I l.o

lgftSdry 11.0

ldkg dry 11.0

Ug/kg dry l l0

30-150 %30-150 %

ldks dry 475

!g/ks dry 475pdkS dry 475

Lidkgdry 475

LidkS dry 175

ISAS dry 475

ISAS dry 475

ldkS dry 475

SW846 8081A 2O-MarO7 25-Mat-O7 7031068 TG

SW846 8082 22-Mat47 24-Mar47 7031274 MP

SW846 8270C 22-Mar07 24-MaGO7 7031278 M-g

Semivdalile Oroanic Comoounds bv SW846 8270CPr€pared by method SW846 355084332-9 Acensphth€ne,O&9$ ArerEphthylene€A-533 Aniline12&12-7 Anthaac€ne1912-219 Atzzjfie10$333 Azob€nz€'re/Oiphenytdi€zineg247-5 Benzidin€56{+3 B€nzo (a} anthracene

Thit labonto.! report is ,tot volid ,'Uho..t an aulhorize.I slprature on tho cover ptge .

' R€portable D€tectioo Limit BRL = Below Reporting Limit Page 35 of 152

Page 379: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeltificationM8F-50 2,-{'s459464-0?

Client Proi€ct #301-88

MatrixSoil

R9c€iv€dl9-Ma.-07

Collectioo Date/Timel5-Mar{7 00:00

CAS No- ABalW6) Resull Flag Uaix 'ML Dilalion ,Iakad netr, Prepond lnztyzpl Eatch Atubtsl

Semiyolstil€ Orgrolc Conpo|rnrls by GCMSSemivolatile Orqanic Comoounds bv SWBit6 E270CPrepared by method SW846 35508so-32€ BgfEO {a) pyrehe20$s-2 gerEo (b) fuoranthene191-24.2 BerEo (g,h.0 psylene207.0€-9 EerEo (k) nuorenthene65J54 8€nzoic aodloe51€ 8€nzylalcohol11141-1 Bis(2-chb.oodExylnetEnei1144-4 8is(2dioroeftyt)edrer39638-32€ Bi6(2dttodsopropyt)eo|e.1r7'81.7 Bis(2€drthoxyl)phthatate101-56-3 4Bmmopheny' phonyt ether05-€€-7 &ttylb€nzylphthalate8G74{ Calbszde59-5G7 +Cfiloro-3-mehylph€nol106-47{ +Chloroaniline91-5&7 2-ChbfonaPhthalene9557{ 2.Chlomph€nol7005-72-3 4-Chloaoph€nyt phenyeth€r218-ol-9 Chrysene597i1-3 DiberEo(a,h)anthrgceno132e.9 Db€rEofuran9'5G1'l ,2Sict{orobenzen€tl l-zJ-t ' .3-Dildorobenzen€106-46-7 1,4-Dichtorobenzene91€4-1 3,3'OichtoroberEidiner2G83,2 ?,4-Oict{orophenol€466-2 DiethytphfEtale131-11-3 Di.nehy phtlEtate10tr7-9 2,+Onnedrylphenolu.7+2 Dl-n-butytphthalate53452-1 4,&Otnitro_2_flethy'ph6lrol51-2s5 2,+Dinltopfienol12t-14-2 z,4-Olnltmtotuene60c2s2 2,6roiniftobiuene1r?{4.0 Di{-octytphhalate206-44{ Fluoh'rhene8&7+7 Fluoron€11&741 tbxechlorob€nzene87{&3 H€xadorobutadi€ne77474 Hexacfilorocydop€ntadiene87.12-1 ilexadrloro€thane1s33s-5 trdb.|o (l,2,3acd) ptrcne9(}i2-o l-lrlethy'naphfialene7B{9i l6ophorones157{ 2-libtlytnaphfElenes$4&7 2-Methylphenol1063€-4, 3,+Medry{phenolt06-1,1-591.203 NaphthaloneU-714 z.t*tr@nilin€99{9.2 }Nitoanilin€

BRLBRLBRLBRL8Rf8RLBRLBRLBRLBRTBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBBLBRLBRLBRLBRLBRL8RrBRLBRLBRLBRLBRL

BRLBRL

BRLSRLBRLBRLBRT

BRLBRLBRL

BRLBRLBRL

t 9rlg dry 475ydtsd.y 4tspgrg dry 475

ldlg dry 475gdkS dry 475

ldkS dry 475

WkS dr, 475

IS&gdry 475pdtg dry 475

FgrS dry 475

Igkg dry 475

lgkS dry 4rspgilq dry 475

US/IS d.y 475pqxg dry 475

ldlS dry 475

rdk€ dry 475

l|g/kg dry 475

Udl€dry 475

$I(g dry 475

trgl€ dry 475

|./, gdry 475

Idkg dry 175

IS/kg dry 475pdrSdry 475

ldks dry 475

ldkS dry 475ydkg dry 415pdkSdry 475

udkg d.y 475

udkldry 175pdr€dry 475

ldkodry 47spgkS dry 475

UCI€ dry 475pgts d.y 475pdrg dry 175

ldkg dry 175

ugkSdty 475pgkg dry 475pdkSdry 475

Pg*gdry 47spdkgdry 47s

Fdkodry 475

US/kS dry 475

lgkg dry 475

pSAod.y 475pgkgdry a1s

ld*odry a7s

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SW8468270C 22.1td47 24.1t6t47 7031278 M.B

l7'le lafuary rqorl is "ot

tldid pbho& s" aahodlzd sig/l{/'nre oE thc corer pqe.

+ Reportabl€ D€le{tion Limit BRL = Below ReportiBg Limit PBg€ 36 of 152

Page 380: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-50 2'-4'

sA5946t-07

Client Proiect #301-8$

MatrixSoil

Receivedl9-Mar-07

Collection Date/Timel5-Mar-07 00:00

CAS No. Anab'te(s) Rest/U FIag Unia lRDL Dilktbn Method Retr. Peparcd AnzlJzed 8o1ch Aulrst

Semi\ol.tile Orgmlc Compoutrdr by GCMS

Semivolatile Orqanic Comoounds bv SW846 8270C

Prepared by melhod SW846 35504rcrcot{ 4-Nitro€niline98€t3 Nifobenzene8F75-5 2-Nitroohonolt0o{?-7 +Nitophenol62-754 N+{ikosodirnelhylarnne62t{4-7 N-Nitlsodi-n-propy'amine86-30{ N-Nitrosodiphenylaminea7-46-5 Pedachlorophenolas-01€ Phenanihrene1@9s-2 Phenol129-{X)4 P},renelloei F/ridine1A)€2-1 1,2,4-Tridllorcbenzeness5-4 2,4,$Tric-hlorophenol08{€-2 2,4,GTricilorcphenol

S{]tmgElo fgcovorbs:?21.60{, 2-Fluotohiphenyt36r-t21 2+luoropheno!1t65-6p4 Nilnrb6nzene45416542-? monol4s1716-s1e Teryhenyt4l41 l0-m4 z,4,6-TihtotnoplFJnol

Totd Mctrb by EPA 6000n000 S€ries Mctftods

sw846 8270C 22-Mat47 24^!tal{7 1031278 M.BBRLBRL8RLBRLBRL8RL8RLBRLBRLARLBRLBRLBRLBRLBRL

79

63755090

o.0344

BRL

1_98

23.5

BRL

5 .12

9.99

BRL

udkg dry 1900

ldkg dry 475

UgkS dry 475

t|g'/kg dry 1900pSlkSdry 475

ttgKS dry 475pgKs dry 475pdks dry 475pg/kg dry 475

]rgkg dry 4f5

Ug/kg dry 475pEkg dry 4r5

t g/kg dry 475pSI(g dry 475pg/kS dry 475

30-130 %19110 %30-130 %11110 %3G130 %1U110 %

mg/kg dry 0.0326

mg/kg dry 0 963

dg/kg dry 147

mgfl(g dry 0 491

m$4(g dry 0.246

mdkgdry 0.49r

mgks dry 0.983

mSI(g dry 1-47

mg/l 0 0100

nEI 0-0150

mg/t 0.0050

@4 0.M25

mgl 0.0050

mg/l 0.00040

mSfl 0-0075

mg/l 0.0150

%

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7439976 M€rcury

Totll M€trb by 8PA 20O S€ris Meahods

74,u}22r4 Sifuer

7a{-3&2 A6€itiC

zt4$3+3 Badun

744(Hgg Cadmium

71.4G1t7-3 ChroLmium

743992-l Lead

f702-49? selenium

1 SW846 7471A 23-Mat47 26-Mat.ot 7031306 YP

EPA 200.7 23-MarO7 24-Ma.-O7 7031305 HB

24-Ma.-O7 ' LR

24-Mar0t ' HB

SPLP Meaals by DPA lJ12 & 6000,q00O Seri$ M.rhods

SPLPExtEction Completed

7.!r&22-i Sllver BRL

71K+3&2 AFenic BRL

7rt40-393 Barium 0.0146

7.140-{}9 Cadmium 8RL

7rt4{H7-l Chrcmlum 8RL7t3S.97{ M€rdrry BRL

7€942.1 Lead 8RL

7782{$2 Sele.nium BRL

Gcierrl Ch.mktrJ Porcm€ters

% sdids 8s.5

I SW8461312 21-Mat47 21-Mat47 703122S AD

1 SW846131260104 22-MarO7 23-Mar-O7 7031323 LR

1 '

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I

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1 SW8461312'470A ' 23.4na(47 7031324 yp

1 SW8461312/60108 " 23-|\,1a.-07 7031323 LR

1 '

'1 SM25.40 G Mod. 22-Ma(47 2241at47 7031307 YM

fhit lstotutory repo"l k ,ral tslU wuhaat an aarhodzed signdare oa tha cover page .

r RQortsbl€ lxtection Limit BRL = Below Reporting Linrt Page 37 of 152

Page 381: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Saropte tdentifrcationM8F-51 2'-l'sA5946,+{8

Client Ploj€ct #301-88

MatrixSoil

Collection Ddte/Timet5-Mar47 00:00

Rec€ivedl9-Mar{7

CAS No. Addytc(s) nq aRDL lHdiorl Mdhod Rel Prapated Arulyzen Bdch Adelftl

Vohtil€ O.grnlc Compounds

VOC Extraction Field ext-acted

BRL

pgls dry 3.5

WkS d.y 7o.7

rdkgd.y 3.5

lgftg dry 3.5

lglSdry 3.5

rslksdry 3.5

USI(S dry 3.5

ISI(gdry 3.5

lSftS dry 7.1pdks dry 3s.3

flgfts dry 3-s

Idks d.y 3.s

l,gftg dry 3.5ggkS dry 17.7

FdkS dry 3-5

r|dkg dry 3.5

lrgkg dry 7.1

Pgtg dry 3.5pdksdry ?-1

UgI(g dry 3.5

UdkS d.y 3.5pgftg dry 7.1pgks dry 3.5

Pgn(S dry 3,5

IgkS dry 3.5

lSikS d,y 3.5

lSftS dry 3.5pgrs dry 3.5

ldks dry 7-'l

lsfts dry 3.5

ldks dry 3.5

Iqtgdry 3.5

udrq (lry 3.5

flgksdry 3.5

tdksd(y 3.5pSikS dry 3.5

ldlsdry 3.5

UdkS dry 3.5

sdkS dry 3.5

t€ikg dry 3.5

lqtgdry 3.5

Pdkodry 3.5

lgkgdry 35.3

tt*g dry 3.5

$ikS d.y 3.5pdtsdry 3.5

$gksdry 35.3

!Si(S dry 35.3

IdkSd,y 3.5

zGt,lar{7 20{r€r47 7031156 BOVolatile Omanic CompoundsPrepared by melhod SW846 5035A Soil (|ow bvet)76_1$1 1,'1,2-TdcttlorotrifLroroethane (FreoDRL6754-1 Ac€tone BRL107-13-1 Acrylonihile BRL714T2 B€nzene BRI_108-86-i Bomobenzene BRL1..gt-s Bromochlororn€thane 8RL75-214 Bron|odichlorcm€thane BRL1r2r2 Bmrnoform BRL7,143€ Bornomelhane BRL78.e13 2€stanone(MEK) BRL10r|.5l4 n-Butylbenzene BRLr3t98-o sec4utylbenzene BRL90{6€ te{t-BuMbenzene BRL75-1t0 Caabon disutfide BRL56.23-5 Carbon tetrechtoride BRL108-SO-7 Chlorobenz€ne BRL75{10-3 Chloroethan€ BRL67{63 Chlo.ofoam BRL7447-3 Chtorom€than€ BRL95-498 2-ChlorDtoluene BRL106-43-4 4-Chlorototuene BRLs6-12{ 1,2-Dibromo-Sdlloropropan€ 8RL124-4€.1 Oibromochloromethane BRL106s3{ 1,2{ibrornootrEne(EDB) BRL74-95.3 Dibromomethane BRL9150-1 lJ-Dichlorobenzene BRL5,11-73-1 l,lDichlorobenzene BRL106-4G7 l,4oichtorobenzene BRL75-71-8 Didllorodinuoromethene (Freonl2)BRL75t1.3 1,l-Dichtoroethane BRL107-06.2 .1,2-Dichlorc€{fiane BRL753s..1 |,1-Didtlam6thene 8RL15€'5s-2 cjs- 1,2-Diohbro€thene BRL15e@5 tEns-1,2-Dichloroeh€ne BRL78{7.5 1.2-Dichtorop@p6ne BRf1€.29-9 l,lDic+tbropropan€ gRf

5!M-20,7 2,2-Dichtoropropane BRL56$s83 1, I Oichlorcpropene BRL10061-01'5 cis-1,3-0idilodpropene BRL100€r{25trars-1,3-Didiloropropene SRI-10{F114 Edrylbenz€no BRLfl48'3 Hexachloobutadiene BRLs91.784 2-Hexanon€ (MBK) BRL9e{2{ lsopropylb€nz€ne BRL99{7€ +lsoproDyltoluene BRf1634{.1-4 Methyt t€n-butyl ether BRLt0&10.i +MeditG2-penta one (MIBK) BRL7s49-2 Methytone .fttodde BRL

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S1^/ 846 02608 2l+det47 2]['/€t47 7031233 TR' ;

9t.iG3 Naphthelene

Page 38 of 152

Thb bbrdo4 ,epod it Aol reli.l wiahou an oathoriztd signztare a.t ake .owr gage.

' R€portable Detection Limit BRL = Below Reponing Limit

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Sample IdentificationM8F-51 2'-4'sA59464-08

Client Proiect #30t _88

MatrixSoil

Receivedl9-Mar-07

Collection Date/Timel5-Mar-ll? 00:00

CAS Na A^abt4s) Flae Ufiits 'RDL Ditution Method Rel, tuepale.d Analped Botch Analysl

YokliLe l)tgr'i. Compounds

Volatle Omanic ComooundsPrepar€d by m€thod SW846 5035A Soit (tow tev€t)

BRL8RL8RLBRLBRLBRL

BRLBRL8RL8RL8RL

75-69-4 Trichtorofluoromethane (Freon 1l) BRL

103{6-l n-Propytbenzene10r!r2-5 Styr€ne630.206 1,1,.1,2-Tetfachtotlethane7+3rL5 .l,1,2,2_Tetrachtoroethane

127.i€i fefechlorDelhene10844{ TOlUen€87{ i4 ' l ,2,STr ichlorobenzene

120-82-1 1,2,+Trichlorobenzene71-554 1,1,1-Ttid oroethane7940-5 l,l,2-Trid oroethane794t6 fricl oroethene

SW 846 62604 21.Ma.-07 22'MaA7 7031233 TR

+CT ETpH 21-MaF07 21-[rlac07 7031167 OS

96.i84 l,2,S.Trichtofopropane95.63$ 1,2,+Triftethytb€nzene10&6/€ l,3,STrimethytbenzene75.,01-4 Mnylchlo.idel3cl-zG7 m,p-Xt4en€95{7{ Gxylene10940-9 Totrahydrofuran

.6G2+7 Eftyletler90.1{5-€ Tert-amyl meth!{ ether63742J E!]yttert-hrtyteher10&21L3 Di-isoprDpylether7545-0 Tgrt-Butanol / butjyi alcohol12+9i-1 1,4_Dioxane

Sr/'rog€te a€coyGrlesj410{04 4l-Btononuorchenzene

U37-26-5 foluene4S1 7@Do7-o 1, 2-Dbhlorcelhane-d4tffi€.53-7 Abtumofluoromethane

Ertncarble Petroleum Hydrocrrbons

Efadable Total Petroleum Hvdroca.bonsPrepared by method SW846 355088006{1-9 Gasotine6847&fi-2 Fuet Oit #26847&31-3 Fu€to tf4€455100-{ Fuel Oil t oM06800000 Mo,tof oil

"00100000 Aviation FuelUnidentifiodOtre. oilTotal Peboleum HydrocarbonsC9436 Aliphatic Hydrocatons

Srnrogale ,fooyedBsj33116.33-2 l-Chlorooctadecane

SeBtvolrtile Orgmtc Comportrds by cCOroanocfi lorine P€sticides SW846 8081APrepared by mehod SW846 3550830+{h-2 Aldrin

BRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRL

1001001 1 199

BRLBRLBRLBRLBRL8RLBRL

BRLBRL

88

!S/kS d.y

!g/kg dry

lSn(g drypEtQ drypqkg dry

lgkg dry

lgkg dry

lSftg dry

IIEXq dry

lqis dry

trS/kS dry

!s/kg dry

vdks dryps/kg drypdkS drypdkg dry

lgks dry

ldks dry

ldks dryyS/Kg dryyg/lQ dry

!g/kg dry

US/kS dry

usfts dry

t/dks dfy

3.53.53.53.53.53.53.5

3.53.53.53 5

7 1

35.33.53,53,5

35.370.7

t 7 017.0r7.0

1 7 017.017.017.0

17.0r7.017.0

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70,130%70-130%7G130%70-130 %

mqks drymS/kS drymdkg drymqks drymdks dryrng/kg drymgrq dryngn(g drynE/(g drynEnq dry

BRL

40-140 %

lgkg dry 5.41 SWOtl6 8001A 20-Mar-07 25-lvlar{7 7031068 TG

Thit hbotutory rcporl is Eol vald ,,ithout zn aafioizcn sipaturc on the cover page

+ Reporlable D€tection Limit BRL = Below Reporting Limit Page 39 of | 5.2

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Sampl€ [dentificationMtF-sr 2'-4'sA5946+08

Client Proiect #l 0 l+8

MatlixSoil

Collectioo Date/TirEeI 5-Mar47 00:00

Receivedl9-Mar-07

C,lS No. Ana$E(s) Resc/l Flzc 'RDL Diluion ntdhod nel Prcpared Arslfud Bdch Aao4st

S€mivol.tile Org.tric Colnpordr by CC

Orcanochlorine Pesticides SW846 8081A

Prepared by merhod sw846 35508

319-845 a-BHC31e{S7 baBHC31$86€ d_BHC5E{99 gFBHC (Lindane)

s7-7+g Chlordane72-/4 4,4-DDD (p.C)

n.s+e 4,4-DDE (p,p.)

50-2e-3 4,4-DDT (p,p')

60.57-1 Dieldrins5$9€$ Ehdosulfan I33213€5.9 Enclosuffan ll1031-074 Endosulfan Sulfatls72-m4 Enftin7421 -934 Endrin Aldel|},de7G.14{ Heptec*{orf24r' Methoxychlor1024-67-3 Heffacl or Epoxideglol.3F2 Toxaph€n€51()3.71-9 s-Chlodane5506-3+7 gchlordane

53494-70.5 Endrin Ketone

Sunogate ecoveies:t 03868+2 4, {-o&Octaf, uorobiphenyl ( Sr)

2051.21-3 Deczchtorobiphenyl (Sr)

Polvchlorinat€d Biohenvls bv SW846 8082

Prepared by method SW846 35508

12671.11-2 PCB 1016111o+A-2 PcB 122111141-16-5 PCB t232$46+2r-s PcB 124212672-294 PCB 124811097{9-1 pCB 12aJ41r0s6-E2-5 PCB 12603712+?l-5 PCB 1V621110ci4r PCB t258

SdTogale aecolf€fres.'1 03a6.8+2 4,+DB-OcIafl tmrcbiphenyt (5.)

N5t-2+3 Decachlonhiphenyl (So

S€E volatile Orgrnlc Compo|rtrd! by GCMS

BRLBRLBRL

BRLARLBRLBRLBRLBRLBRLBRj-8RLBRLBRLBRLBRLBRLBRI.BRLBRLBRL

44

BRLARLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

BRLBRLBRLBRL8RL

lgkg dry 5.41

rdksdry 5.41pdks dry 5 41

lrg/kg dry 5.41pdkdry 27.D

ldks dry 5.41

Udks dry 5.41

ldkS dry 5.41

t gil(g dry 5 41pS^S dry 5 41pdks dry 5 41

ldkS dry 5.41

9gkg dry 5.41

trdkgd.y 541pgrkg dry S,41pgftS dry 5 41pdtS dry 5.41

udkg dry 27.O

USftg dry 5.41

$lkg dry 5-41

lgftSdry 5.41

N-150%30-150 %

Igkgdry 10.8pdlqdry 10.8

!Sn(S dry 10.8

$gkSdry 10.4pdkgd.y 10.8

ISikS dry 10I

Frylgdry 10.8

ldlg dry 10.8

UdkS dry 10.8

30-150 %3o-t& %

$ftg dry 423

ugrS dry 423

UCASdry 423pgAS dry 423

ldkS dry 423

ldkS dty 423

t dkSd.y 423pSftgdry 423

1

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Semivolai e Orqanic Compounds by SW846 8270CPrepa.ed by melhod SW846 35508E3-32-9 Acgnaphth€ne20&s&S Acenaphthylene6?.513 Anilino12Ot2-? Anttus1912-2+9 Ntainet0!33-3 Azobenzener'Diphenytdiazine9247-5 Bqnzidine5'6.55:3 B€nzo (a) anlhracene

SUA}46 8082 22-Ma(47 24+ler47 7cB1274 kP

SW046 8270C 22-lla(47 25 tar47 7@1278 M.B

Thh ,ano.alory rcpod ie t ot wlid withou sn aath ized rq,alarc oB tlrc dawr psge.

' Repofiflble Det€ction Limit BRL = B€low R@orting Lirnit Pase 40 of 152

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Samole tdentificationMtF-sr 2'-4'sA59464-08

Client Proiect #301_88

Collection Dare/Timel5-Mar-07 0O:00

MatrixSoil

Receivedl9-Mar-07

CAS No. Anaba(s) Flog 'RDL Dilutirn Method ReI- Prcparcd Anaq@d Botch Anabst

Scmirolrtilc Organic Componrdr by GCMS

S€mivolaue Oroanic Comoounds bv SW846 8270CPr€pared by method Sw846 35508

s4l-32-8 Benzo (a) pyrene

Al$*).2 B6lEo (b) fluoranthene191-24-2 Benzo (g,h,i) perytene

al7,m.9 Benzo (k) fluorantEne66-45-0 Eenzdic acicl10{i-5r6 B€nz}4alcohol111.s1-1 Bis(2d{o.o€thory)methane111-44.4 Bis{2-cl.{orcethyt)etrer3s6:l+324 Bis{2-chtoroisopropyl)ether1174r-7 8ls(2-ehylh€xyt)phthatate101-5t€ 4Bromophenyt phenyt ethera5+17 BuVbenzylphthalat€€G7.t{ Catbazole5e-5G7 4-C;ttloro-3-rnethylphenol106-47{ +Chloroanitine91$6-7 2-Chloronaphthalene9557{ 2-ChloroPhenol70{872.3 4-Chtorcphenyl pheny' ether21&014 Chrys€rEs3-703 Dib€nro (a,h) anthracenei32-€4-9 Dib€nzofuran95,5Gr i,2-Dichlorobenzenea,4l-73-1 1,3-DichlorobenzenelGa6-7 i,+Dichlorobenzene

91{4-t 3,3lDichlorobenzidinerll€3-2 2,+Dichlorophenol846&2 Diethytphthatate131-11-3 oimetht{ phthalater05167€ 2,4-Dim€thytphenol

81-7+2 Di-n-butylphlhatate

534521 4,GDinilro-2-melhylphenol

51-2+5 2,4-Dihhrophenol121-1,L2 2,4_Dinilrctotuene

@8iry2 2,6-Dinitltrtotuefle117€4{ D{-n-octytphtratateztlGl4-O Fluolandrene86.7+7 Fluorcn€11&7+1 Hexachlorobenzen€475&3 Hexadtlorobutadienen 474 llsy€Chlorocyclopentadieoefl7.72.1 ller€d oroelhans1e&3es Indeno (1,2,3-cd) pyren€

9lt-12-0 l.ldetty'naphdlalene78-5$1 lsophorone915/6 2-Mehylnaphthal€nes5-4&7 2-ttt€hylph€nol

10&3s-a, 3,4-Methylphenoll0€.!1'591-2[3 Naph$alene

8Ii-7'!-,1' z-Nitroaniline

SS4$2 3-Nihoaniline

BRLBRLBRL

ERLARLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRL

BRLBRLBRLBRLBRL

BRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

ARLBRL

BRL

Pdks dry 423

l.t{t/kS dry 423

PS/kS dry 423pS/kS dry 423

Pdksdry 423

Pdks dry 423

!g/kg dry 423

ldks dry 42Xpg/kg dry 423

udks dry 423

Lidks dry 423

f.ig/l(g dry 423pdkS dry 423

PdkS dry 423pg/kg dry 423

ldKg dry 423

USftS dry 423

Ug/kq dry 423

Udkg dry 423

rc/kg dry 423

USnq dry 423

ug/kg dry 423

Fdkg dry 423pg/kg dry 423

ISngdry 423

rc/kq dry 423

US/kS dry 423

f./S/kS dry 423

ug/kg dry 423

udkS dry 423

Ug/kg dry 423pg/kg dry 423pSn(S dry 423pslkgdry 423

ISAS dry 423

lsftsdry 423

lgftS dry 423

lSftS dry 423

PdkS dry 423

PdkS dry 423

Irdkgdry 423

ldkg dry 423

FdkS dry 423

PdkS dry 423

F94(S dry 423

tg/kg dry 423

Hdkg dry 423

ldkSdry 423pSftS dry 42X

udks dry 423

SW846 8270C ?z-Ma'-OI 25-Ma(47 7031278 M B

Thit labontor! Eport ]a tor vqld wLhod an authorizctr sfuatue on the cover pagc_

' R€Fortable Det€ction Limit BRL = Below R€porting Limit Page 4l of 152

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SantDle [d€otificariooM8F-5r 2'4'sA59464-0r

Client Proiect #301-8s

MarixSoil

Colle!tiou Date./Ti!flet 5-Mar{7 00:00

Received19-Ma.47

CAS No. Anatre(s) Res t Fl4g A l s .RDL DiTAio,I Mdhod Rel. PEpar.d Analfied Bdch Atzlysl

Semlvohaile Orgsllc Conportrds by GCMS

Semivolalile Oroanic Comoounds bv SW846 827(rc

PreparEd by method SW846 35508

100"0i€ 4-Nitroor line9&913 Ntrobonzene

88-7t5 2-Nitroph€nol

100-02-7 +Nitr@heol@-7rg N-Nitrosodirnethylamine62t€a-7 N-Nitrosodi-Gpropylamine

€F3o-6 i+Nitrosodipheny'amine

€7{F5 Pentachlorophenol

85{l-8 Ph€Mnthrene10s95-2 Ph€nolr294O{ Pyrd€ilc86-1 hrridine1?O€-1 1,2.4-Tfidllorcbenzene95-95-4 2,4,STrichlorophenol€84+2 2,4.GTrichto{ophenol

Sutogale rgcowdes:

321aoa 2-Ftuor$bhenyl

367-124 z-FlLwopl6not

416s-@4 Niltubenzone4S

416fi2-2 Phenolds

,ne-514 Terphenyl4q

ltSlCO 2,4,6-Ttibrofitophenol

Toad Metrb by EPA 6000/7000 Seri€s Mettods

7439-9ru M6rcury

Totrl Metrb by EPA 200 Serie! M€thods

744n'224 Silver

Zt40-3&2 AF€nic

74,10-3+3 Barium

741O49S Cedmium

71-4047-3 Chrondum

7iK!942n Lead

282-4+2 Selenium

1 SW846 827OC 22-Mat47 25+trat47 7SUZ7A M.Bl '

' I '

1 .

1 "

1 '

1 '

1 "

t "

1 '

1 '

1 '

BRLBRL8RL

SRLBRLBRLBRLBRLBRLSRLBRLBRLBRL8RLBRL

81678069a9

lgr'Xg dry 1690

udksdry 423pdxs dry 423

US/kS dry 1690pdlsdry 423

ldxsdry 423

udks dry 423pS/t€ dry 423

rdkgdry 423pdrg dry 423

ldl(g dry 423

lgl€ dry 123pglqdry 423pSikSd.y 423pdrg dry 423

30-130 %18110%3G130 %,5-110%30-130 %tFllo %

mg/kg dry 0.03m

mgr'kg dry r.02

nrgr'kg dry 1.53

mgr'tg dry 0.500

mgiko dry O_2U

nrS/tg dry 0.509

nCftO dry 1.O2

mg/kg dry 1.53

mg/l 0.0100

nEA 0.01fl)

rngl 0.0050

IrE l 0.m25

mgn 0-0050

mgl 0.00040

"Elt 0.0075

msil 0.01m

%

BRL

BRL

1.96

25.6

BRI

6.60

BRL

1 SWE46 7471A 23-Mat47 m4et47 7031306 YP

EPA 200.7 23li.i,at47 24-Mat47 7031305 HB

' 24+'4et47 ' LR' 24-ltd47 ' HB

SPLf Met l. by EPA l3l2 & 600O/?000 Series Meihods

SPLP ExtEclbn7440-22-4 Slver

74rt0-3s2 AEenic

7{40.3+3 Barium

7a40-4i|9 Cadmiurn2440,,t7.3 Chrorruum7139-976 Merdty

?43942-1 L6ad

r|@-492 S€lenium

C€dertl Cl€milfry Prromelers

% Solids

1 SW8461312 21.N|,j.o7 21][n 47 7031??9 eD

1 SWB/61312/60106 22+,lar47 24.llat47 7m1323 LR

1 '

Complebd

BRL

BRL

0.0064

BRT

BRL

BRL

BRL

BRL

1 '

t '

t sw84613tZ/470A

1 Siv8461312rm108

1 '

23-Mat47 7031324 W

24+Jls47 7031323 LR

1 SM25,O G Mod. 22'|.',.a'4f n$iat47 7001307 YM

ThZs lstorolory epo b nolvolid Nlthoat sd aaaho.hcd signttut on dte @e.?poge.

* Repo.table Dele*ion Litrit BRL = B€lo* Rcporting Limit P€e 42 of | 52

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Samolo ldentificationM8F-52 2'-t'sA59803-16

Client Proiect #101-88

MatrixSoil

Collectiod frab/Time26-Mar-07 00:00

Received2'7-MaL07

CAS No, AEdyteG) Result FI"g Units *RDL Dilutioa Me.hod Rcf Prcpand Anaqzed Batch A rlysl

Volalile Oeanic Conuounds

Prepared by method SW846 50354 Soit (tow levet)

7r l19l '1,1,2-Tr ichlootr i t luoroethane(Freon BFL67+l-l A.etone SFL1lt-13r fu4ionitdto BFL71-13-2 BgEene BFL108-861 &Omob€nzene BFLr+srn Eomocilorcmehane BFLEn4 &omoddrloomelhane BHLE&2 Bomotonill BRL7l-8+9 Bonomehane BRL7Eql3 z.Eutanoie (MEK) BRL104-51.8 n-ButytbsEene BRL135.{18'8 sec-Bulyli4nzene BRL

9€{6-G ted-Butylb€mzene BRL

615-0 cadofl disufide 8BI

562+5 C€don tetBchtonde BRtr@got orlorobenzene gRL

75{G3 O ometfiane BRL

67s3 O orctom BRL1147.X 0{orcm€t|ane BBLsir+8 2{ibro{otuene BBL1ft-43{ 44 orctotuene BRLsel2-€ l,2obfom+3<filorcprcpano BRL124-4s1 Sbonod oomelhane BRL'@93-r 1,zloihunoehane (EoB) BRL740s3 [lbnnruneiharE ARL9+5G1 l.2.oichtoobenzene BRL

5,ll-73.t l,3{ichlorobenzene BRLr6-1s7 1,4-Dichtorobenzene BBL671.8 Dcftorodfluosnethane (Freont2) BRL1U*3 1.1-oicldorodhrn€ BFL1n7{G2 l,2-Uclioro€hane BRL15.35-4 l.l.oicliorcqhene BFLls6-5&2 ci91,2,olcilormthsn€ BffL

156{l}5 ra$-1,2-0hhloroethene BFL78c/'5 tz.Sdibopopane BffLta44 i,+Udiomprooane s8L

5s+a!7 22-Didltoopropane SFL

56950{ i,l-Djdlbopopene BFLlrxFr-01-5 cin1,3-oiciloroprcpone BFt10(E1-@{ tfi$-l,3oicliooprop€n€ 8FL100{1-4 EryDenzene 8BLt/-6s3 Herad{srobulad;a.a BRL

sl-78i 2+lelanone (t!,i8K) oRL

28Ma@7 A'Ma47 7U1761 8D

2g4lar07 29-Mar'07 7031790 8Ll

Voladle Orgrnlc Compounds

VOCExtadtot

jrS^S dry 6 6

ISAS dry 133

!S.4(S dry 5.6

lSilq dry 6.6

lVlS dry 5.6

lStS dy 6.6

lglq d'y 66

lvkg dry 66

lqkS dy 13.3

!S,tS dry 66.4pg,*g dy 6.6

PS/rg dry 6.6

!S4€ dry 6.6

]rgrS dty fi.z

ISAS dry 6.6

!g4q dy 6.6

!S,kq dry 13.3

!S/k! dry 6.6

lS,lqdry 13.3

!St{ dry 6.6

uS4q dry 6.6

Pgb d'y 13.3

!S4q dry 6-6

lglq dry 6.6

@tg,!y 6.6

jrdkd'y 6.6

!S/kS dry 6.5

us/ks dry 6.6

pgtS dry 13.3

pS/kS dry 6.6

lSifg dry 6.6

llgrS dry 6.6

llEls dry 6.6

ISAS ey 6.6

lglq dy 6.6

!$4S dry 6.6

!C4S dry 66

|4/l(S dry 6.6

l]gilS dry 6 6

lJg4(s dry 6.6

rtkis dry 66

$Iq fy 6-6

|lg,,l(S dry 66.1

UEk! dy a6

pg*S fy 6.6

peftS dy 6.6

Udrg d)' €6-4

ldkS dy 66-rl

!g4q dy 66

Field etuadd vcf,

sw84682 AI

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$.02€ hopropyibdlzene

SF€ AbopoDyitduene

163,q,4-,r ehy,lterl+utyl€her100ncr +lirethyi-2{€nknone(Ml8K)

69 2 ff€$yi€ne dloride9l{lr3 Naph$etone

BRL

BRL

BHL

8FL

BRL

8Rf,

mb bboralorJt repo.t i' t ot vtIU vlthost an salttorizd sigftuure on the cover paEe .

' Repodable Detection Limit BRL = Below Reporring Limrt Page 78 of 154

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Sarple ldentificaJionMtF-52 2'-4'sA59803-16

Client Proiect #301-r8

MatrixSoil

Received27 MaP'l

Collection DatelTime26-Mar-07 00:00

CAS No, Adalf,c(s) Fk'g Unix 'RDL Dilutinn Method RcI, Preparcd Analfzed Bateh Analtsl

VohaihOrg ic Compoonds

Volaule Og6nb ComooundsPrepared by method SW846 5O35A Soil (low tevel)103{$t Fprop}t€nzem100-1!.5 Styr€ne000.20.6 1,I,l,2.Tetradorcelhane1\|"3,1.5 1,12,2-Tetradooethane1r.14"4 TskaElJooetlefl€108.883 TCIU€fis87414 jz,gTdcldorobenzene

120.€en j,2,+Ti{tombenzene

7_5ft 1,1,l.llicnbro€hanen00.5 1,1,2.f'i/.dttuD€d.68?901S Tddttor€fiene75{$4 Tndtlomttuoorn€lhane (Freon I 1 )s184 i2,&TricnbEp0pane

12,l.Trhelhylbenzenel@{r-€ l3,tTdmethytbenzen€tH1.4 Vinyldlonder$clc7 m,Fxylene9s.,r7€ oxylenero949-s l€tr*ydfd ran60.r$7 Eryshsr9to$8 T€rl{llMnElhyi€hera7-a{ Errytbnhrtyielherfla{0.3 Dtjsopropytether75so Ted-Buhrbl / brJtyl alcoholrzfgt,l 1,4{iorane

@404 4-E@noflwrcbenEne

2@1.&5 fduene4S

1tu6n474 1,2-Dil otod.fq''e44

11'6&9,7 Dblonafurovnelhane

Ellttctbl. PerrolcEm Hydrocrrbons

&tnalable Tobl Pdroleum Hrdrccarbons

Prepared by mothod SW846 35508qXEf14 GasOlme6€47S3C2 F$loI +2d847s3l's Fod 0l 14d06530ca FUelOi t8rr0!00m Moffoil.m10m0 Aviatbn Rlel

Unidentfi€d

of|ol oil

Total Peldeum Hldro..a6ons

Cg-c36 Alipllatic Hydreartons

38ff3? latfuadab@le

Senllolrtile Org.tric Compomds by cC

Omanodlodne Pss|itjdss SW846 8$1A

Pr€pared by moflod SW846 3545A

1F0tl2 Atddn

B8L

BFL

BRL

BRL

BRL

8RL

8RL

BRL

BRL

BBL

BRL

BRL

BRL

BRL

8RL

8RL

BRL

BRL

BRL

BFL

BFL

BFL

BFL

BFL

BRL

1U

1(n1231 1 1

lg]l(g ftv

!s4g dry

!c4q drypdks drypgls dry

lgxs di'pgt! dypsn(! drvpgts rv

!g/ks dry

UgrS drypgks dry

ugrs dry

rc.4(s dry

Psts drypEks dry

lqtS dr/

ldrs d'yyS/kSdy

lls^s fivpS4(S dry

lls/rs dry

Ktxs orypS/kS dry

!s/ks dry

7G1i0 %7V130 %7ll'130 %

7G130 %

ntS/kS dry

mgrkg dry

nAtS dry

n€ltg dry

rE/rs dryiE/rs drynVrS dryfldlq drym94s drlmS/rS dry

40,140%

sw 845 [email protected] 1

6 .6 r

6-6 r

6 6 r

6.6 I

6 6 r

6 6 1

6 6 1

6.6 1

6.6 1

6.6 1

6.6 r

6_6 1

6.6 I

6.6 l

6 6 1

1 3 3 1

66..1 1

6.6 |

6.6 I

6.6 |

66.4 1

133 I

29r,lar-07 2FMar,07 7031790 FtJ

2!!Mar{7 3Gl\rlar{7 70317736.5 1

6.5 1

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BFLBFL8FL8RLBRLBRLBRLBRLBRLBRL

+CT ETPH

1 1 8

tErs dry slirB46 8061A 28-t'lart GAprOT 70:11739

This labonlory reFort is not dA *ihout a,t authodzed sigttatan on ahe covcr ptge

'RePortable Detection Limit BRL = Below ReporringLimit Page 19 of lS4

Page 389: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldedtificationMtF-52 2'4'sAs980l-16

Client Proje€l #301-88

MatrixSoil

Collection Daje/Time26Mar47 00100

Received27-Mar41

CAS No, Analrk(s) Resalt Flag Uni,5 'RDL Diluio,. Me,hod ReJ. PrcpaQd Analfzed Bath An4lpt

S€mivolrtll€ Orgrnic Compounds by CC

@ganodlhrirF Peslicid€s SW8{6 8081 A

Prepared by m€thod SW846 3545A

319-8rt-6 +Bt|c

919-8F7 b+8C319.S&8 d€HC58.49.e +8[C (Ltndens)

lt7+s Chlordam7254-8 4,4,-DD0 (p,p,l

72.5rs 44'-0DE h,p)5G2e3 1,4'.00T {p,C}q!57-J oidddne5998{ Endosdtan I332rtt6rg E rlosjlat tl1{Bl-07-8 ErdGuffal SU al€

7421-934 Endin rJdelde

7lH4J tbdad{or72495 lretbryddorl@4-t'3 HepbdiorEpojdellDr.352 Totaph€isS1g3-rrg aSlodare5566-347 g-Ctilddane

$491m{ Erdfi (eloie

to36611.2 4,+DeMMdit hed 6t)Nt-21-3 MthtuhlEnyl(St)

Pqlvchlorinat€d giph€nvls by SW84{i 8082

Ptepared by method SW846 3545A

1267+1r-2 PC8 tot6

11101.28-2 PCBtl?l111r1-r&5 PCB 1232s0/6e"14 PCB 124212872.296 PCB 12411flc07{91 PC8.t25l{11@6-@-5 PC8126[sr-J2+29s PC8 t262r11ll$14-1 PCB t268

ttffi412 4,+D84cMM6ip@(St)

Mt-2q DecdMFlEtyl (Stl

S€mivolatite Organic Compounds by GCMS

S€mivolalile Ooaric Co.npounds by SW0,t6 8270C

P.epar€d by m€lhod SW846 35508Anq.g loonaotdld€ae+e* Aenapt'drylanee5$3 Aniir€1m.12-I Antra€ne1912-a+9 AlEzin€{}933.j Azobenzene/Diph€nyldazine92{7-5 g€nzidin€

56F3 8€nzo (a) anhr*erc

8BLBRTBRLBRLBALBFLBRLBRL8RL8tu8ft-

8qL

B8L

BNL

BnI

BRL

BRL

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BFL

BRL

B8L

d5

t19

gRL

B8L

88L

BFT

8FL

BRL

BRL

BAt

BRL

105

BRLBALBRLBFLBRL8tusRtBHL

34J

34_9

u.s34.9

n4

34.9

34.9

343

u334.9

3 4 9

34.0

31.9

34.9

34.9

34!

34-9

174

t4.9

34.9

34.0

lCbdv!c{g dy

lldlqd,lsrq dy

wh fv

lqls try

ttgtlgtyrgts dy

$aaylslq dy

utlq dv

!9h fy

ldls dv

udk{ ry

Ah fiv

tdts dy

ugnq dy

|ldko d,

sgts dy

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l4AS dY

Ttf i%EItfl%

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udh dv

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30-1fi %*150%

srw845 &81A

sw8,46 8082

sw848827tC

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6t.7

63.7

63.7

a?

89.7

637

69.7

6S.7

28.1V€r{7 30-lrar47 m31738 5M

!9,k0 fy

Brq dv

rdlq dry

lclq dv

@aevl4redvudlq dl

$& dv

€07

807gl7

807

w7

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607

wf

2$MarJt 0+AorO7 ml?4 MA

Thb lahordory tepod h ,tot eaIU tcithout an aalhodzed sigaplure oa rte cover pzEe .

* Reporlable Dckctiod Limit BRL = Below Reporting Linit Page E0 of | 54

Page 390: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldcntificationM8F-52 2'-4'sA5980l-16

Client Proiect #301 -88

CoLlcction Date/Time26-Mar-07 00:00

MatrixSoil

Received27 -Mar-07

CAS N^ Aftalrtz(s) FtoC 'RDL Dilulian Method Ret Prepared Analrzed Bctch Autrst

S€mivolafile Orgartc Compourds by CCMS

S€mivElalile organic Comoounds by SW846 pp70c

P.epared by method SW846 35508

5G@-8 Benzo (a)pyrene

205494 &nro (b) llloranlhonetst2+2 B€nzo (g,h,i) psrytene

207{!4 Eenro(k)fluonnlhene6t€5.0 EsEdc acjd10061{ Benzyl abohol1 ,91.1 Bis(2dtlofoedroxy)m€hane1lt-4,1-4 Bis(2doroetiy')ethet

39Fee4 8is(2dtlorrisopropyl)elher117-017 Bjs(2€fryhexyi)phlharate101'5'5'3 +Bomophenylpheiytstl€r

6-€s7 Eulyl b€nzyl phihaht€

8&7r€ Corba?ole

5&507 44htorc}.nethytpiend

1116{7ll tl,Chlorodliline

91.5&7 2{ttoromphliglene5t€ 2{Hofopn€nol?1F67!3 +Cflo.optEnyl phenti e$er218{l-! ftrys€ns537SJ Dibenzo (e,h) anhrscene132{,14 oib€fiZoluan

s65&l i,z-Uchbob€nzene

5.1'x!1 t,3-tXdltoob€nzeneql4s7 1,+Ddlklo&nzene

9r€+r 3,3',-0i6lJorobonzidine12043.2 a+Ddilorophenol04.€6.2 Didt\4 pl halater31.i1.3 Dm€ltytdfElate1ffi7€ Z+fimdtrytptt€nol*f+2 D-n{uty phhatate

$4{n1 46.Dnilrc2-lnethyiph€nolsr-2&5 Z+DnitrEphsnol121-1+2 a4-Uritrdotuen€6Ce202 a6{iailrlto{uen€117{4{ D.ft{clylphhalal€ffi:t+ Fluoanhene

F7$7 FluorerD1rS?+l ll€xadtxrbquene

trr€ss tl€radoobutadienen471 Hexdorccydop€rnadi€nefl-n-1 Hexd Om€lhanelsl3s5 Inddlo(1,2,3-cd)pyrcne!l{f124 l.ti,lebihapnhdene

46$1 loophomfie

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9q$7 2{ileryphenol

106.19{. q4-frefiylphe{'oli0G!+591.203 |\lethtlal€oel&7+1 2-l{itrroanilre

99.0$2 SMftanilrE

8FL

BFL

BFL

BFL

BRL

BRL

8RL

8RL

8RL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

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8FL

SFL

BFL

BFL

BBL

BFL

BRL

BBL

BRL

BRL

ERT

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BBL

BRL

BRL

BHL

8RL

8RL

8RL

BRL

8RL

8RL

8RL

BRL

BRL

BRL

8RL

8RL

8RL

8RL

8RL

8RL

BRL

WtS dry

ISAS dry

!S.4(S dry

pS4(S dry

pgks dry

pErq ory

tjg',q dry

lSfrS dry

u9k9 dry

pg4q dry

pdks dry

pgrs dry

lglq dry

!S4q d'Y

lgks dy

lsrq dy

lSrkS dy

!g/kg dry

tiglQ dry

!gt(S dry

lykg dry

!S4S dry

!94s dry

t{yKs ory

fgks dry

pdks dry

|ls/l(s dry

$rya $l

p4rs fiv

p4rs dry

|rs/rs drvpS4rS dry

Lryks dry

|rs/ks drv

lglq dry

l€&s drv

|Js/ks drvps/rs dry

ugis drypgxg dry

ugks dry

!s4q dy

!94(S dry

llses dry

t94q dry

!g,xg dl]

!g,kS dry

|Js/rs dry

|ls/rs dry

|JEls dlv

N7

&7@7

w7807

w7807

807

807

807

807

407

807

807

80/

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80/

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@7

ffi1

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n1807

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ED7

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m7807

807

807

w807

N7

m7m7

807

807

807

swe{6 8270c 2g.Ilar{7 09AF{7 7031774 M.8

This labotuaory nporl is nol ealid fl,ilhout sn zartoriaEd signttwe o^ lhe couer page.

+ Reponable D€tection Limir BRL = Below Repoding Limi! Page El of 154

Page 391: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple ldeotificationM6F-52 2'-4'sA59803-16

Clieni Proiect #301-88

MahixSoil

Collectioo Dace/Time2GMar-07 0On0

R€ceiv€d27-M^r4?

CAS No. Aaalfta(s) nesur Fl"s Ual6 +RDL Dilztion Mdhad Ret Prcparud AnaIWd Bauh Analyst

Sehivolalile Orgrnic Compounds b!, CCMS

Semivolalih Omanic Comoourds b{i SW8.46 0270C

P.epared by method SW846 35508

10on1-6 +Niboflilne

S1193 l{ffi€nz6n6

8&7F5 2-t'litbphenol100@-7 +ifttDph€not

6&7ts l.&Ntosodlnehyjflnine

6214+7 NmhDSodi-rFpoptla,nine

8e30{ tlNitcodph€ny'amine

EI-81t5 PflhcHoloftl€nol

H1{ Ph€nenhrBne1O&S52 Pt|6nol129{D{ Pylem

110-€61 Pynding

r2o{2r l,a4.Tdchtoobenzene95-54 2,4s-TrchtorcptlerEl0&06.2 a4,6.Tddttoopttnol

st&4 z+l@tewentl

$r-t2.4 z.HMM

at65{0r ttlihtrbsuened5

1t6si22 Pl1fltr/-(E

171'nt4 Tqp@-d1

t1&?sn Z4FTfironrf,pherKlt

29-luad7 II}AF-'7 7wtn4 l'n8BCt

B8L

BNL

BRI.

BRT

BRl.

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BRL

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8fi1

55

74

u

Mh d|/

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|'|g'lq trv

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tidtS fy

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rtfr%t5-t t0 %&13J%

1U|tO16

&lf i%

1Ut10

'rdb dry 0.m42

d$|ttd) 1.10

mdks dy 1.65

mS/ks dry 0-549

'rE/kg dry 0.214

rn94€ dw 0.549

rngtq dry 0.84

mg4q dry i.€,5

mgl 0-01m

mgn 0.0150

mS, 0.m50

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rng/| 0.0125

ng,l 0000,10

ng 0 m75

m0/l 0.0150

sw846 827m

sw€rt6 74714

EPA 2M,7

3230607u73e30m7

807m7u7

€r07807w7wn7807

807

Totsl Metrb by EPA 60007000 Sedca Methods

7'F+97{ lr€rory

Tot l Metrls by EPA 200 seri6 Merhods

14!,'22! S{ver

l+(t3&2 fuSenic

7,1,rd 393 B€num

7't40{}1t cadnim

71,44f.1 CfiOfliUm

743+921 l_sed

2.87 I

I

I

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1

1

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t

02-AF{7 @+pr{7 7lB18l0 YP

1.82

3.94

95.3

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102

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SPLP Mclds by EPA 1312 & 6000l'000 Se rie! Methods

SPIP E{radbn

t44q'?24 sllver

7@&2 Arsenic

7,1,1t1.393 9aaium

Comdeted

BFL

0.0110

S1V8461312 &bbtJt 2&llar{)T 7031763 BD

SW8{61312/m108 3SMar{7 02.Apr47 781805 tR

?,1r0.{ss Cadn{lm 8RL

7@114 Chromium BRI

743+ct5 MeGtry BBL

7'(FPl |t{l 00138

71le.1s2 Sds um BFL

Gerct'l Ciemistry Paremeter$

% Soldr 06.6

sw€46 t3t2t7470

sw8lf 13r2lm108

' 02.Apr{7 781806 YP

. (P-ap.{7 n81805 |.n

$,@(| G Mod. gl+4ar.07 3cMar{7 7031879 YM

This kbonrory rqn t it nut valld rcllhoaa an zuthofized stgnOtun on thc corer paEc.

' Reportable Detection Limit BRL = Below Repoding Limit Page E2 of 154

Page 392: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Identi6cationMEF-53 2'-4's459803- l7

Client Proi€ct #301 -88

Collection Date/Time26-Mar-07 00:00

MatrixSoil

Received27-MEr-07

CAS No. Anauto(s) Flog Unils *RDL Dilution Merhod Rel. P,eparcd AnalJ)zei Bakh Analrsl

Volalile Oroanh Comoolnds

Prepared by method SW846 5O35A Soil (low leyel)

7t'r$1 1, i p-Tidilo|l]tdfluorc€ban€ (Frcon 8FL

6tt+t ,cehne 8RL1|,7.1sr Adyonitde 8RL7l{3? 8€nzer€ BFL

$ad6'r Eromobenzene 8RLt 95 Bomochbrooelhane BFL

75Zt4 Eomodiciloomethane SFL75€t2 Boinolom BFL7.134 BomofiEhane BRL7&e3 2+ulanone (MEK) BRL1ot-5r{ FBuvbenzene BBL135{€-8 ss€uvlbenzene BRLson6.6 t€n€uMbenzene BRL791i4 Carbon dhutfide BRL5e23.5 Cadon t€had oide BRtlo$gG7 Chlorob€i|z€n€ 8RLTrrocs ChloroetEn€ 8RL

r/iss ftloolorm BRL71a71 Orloro.nelhane 8RL

95.4+€ 2{h+orolduene 8RL16-43{ 44hlorotCuene 8RL96128 i,2-Ebonc3dlto@propane 8RL

12'!l&1 Dibornod oomelhane 8RL10643.. 1,2_ObromoefEne (EDB) BRL74.!lt3 Dbmmom€ttEne BRLgs-silr l,2-Ochtorcbenzene BRL

54r-7$1 l,$Dd orobenzene 8RL

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1,1-Ddllorcodr€n6 8RLrsess? cisn,2ok*lloro€th€n€ BRL

i${o-s [En91,2-0iahlo(oethene BRL7!{/5 '12-Dic oropopane SRL

Volrtile Orgrnic Compounds

r{s,zFs i'3-DicntoropropaneS+zG, 22-Didtloopropane5e5€-0 |,l-Didoopopene1S€1{15 cisl,s{iciloroprop€fielm01@5 trutsl,S{|id oroorolenelGilt-l Efiyjbenz€{po4n Hexad or$Lnadene501-78{ 2+t6ranone(MBx)98{e{ bopopy'b€nuene9S{|€ 4-tsoproMdu€nerdl4-o/r{ tlr€ftyl ten_bulyl elherro&rGr 4{r6t'y'-2fenbnone(Mlg,Kl?5-(192 fi€ttye|edltoride9r.20.! Naphftakne

28{lar{7 28{ar07 7031767 B0

2S-M^t47 29{!br{7 7031790 ffUllg/ks dv

!s/ks dry

lqks dry

!91q dry

tclq drypdkr drypdlq dvpdks d]

Igks dv

!91q drypOks dy

lElo dy

lyts dv

!s4q dv

lglS dry

uS4q dry

lgftS,trylgro dry

lgrs dry

lgrs dry

r{yKg ory

lCqS dry

lSeS drypgrs dry

ugfts dry

lgftS drypS&S dry

!g/kg dry

K,tS dry

|Jg&S dry

!s^s dry

!S4q dry

tEks fry

ldks dy

Ionq dv

loikS dypsn(s dy

|}El(s drv

IS/IS dly

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ldrS dry

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voc

sw 846 8260At51 1 1

5.5

5 5

5 5

5.5

5 5

5.5

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27.7

5.5

5.5

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] ] l

5.5

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5.5

5.5

5.5

5.5

5.5

5.5

1 1 . 1

5.5

5.5

5.5

5.5

5.5

5.5

5.5

5.5

5.5

5.5

5.5

5.5

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5.5

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BFL

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This labonlot! Epo ir ,tot tlalill teithoaa an adhorized signaturc on the cowr page

* Reportable Detection Limit BRL = Below R€porting Limit Page 83 of 154

Page 393: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ [dentificationM8F-53 2,-4'sA59803-17

Client Proiect #301-88

MatrixSoil

Collection Dal,e/Time26-Mar47 00:00

Rec€ived21-MaFO1

CAS No- Analyz(t) Ftzg 'RDL Dil'lian Method Rel, Prcpzad Aazbzen Bztch A4alyst

Vol.tile Org.nic Compoutrds

Volalile Oro& c Commun&

Pr€parcd by method SW846 5035A Soil (low lovel)

103451 tufupyhHrzene BRL

100-42-5 StyHls 8RL

6s'.20.6 1,1,12-Tetrachlo.oetrhane BRt

7!|"0,1-5 1,1,22-Ie0adrlo.oelhane BRt

127-t8-4 Te{nd orcefi€ne 8FLros-€6.3 Tobene gfiL

67{1{ 1,2,}rrichtoob€flzene BRL

12OS2t l,2.+Trid oobenzen€ BRL

71-5s.€ l,1,l.Tdchlor@fiane BFL

I,l2.td$hft€hare BFL

E{1{ Tnct om€tlqle BRL

75.6s_{ Tict onlluororneha'le (Fr€on 1 l ) 8RL

sl8-a lr,STricnbrcpropane SRL

ffit6 1,2,1-Tdnefrylb€nzsne 8Rf

100-r/{ 1,A,tTdn€hylbenzsrE BRL

75414 Vinyl.tlodto BflL

$3q?G7 |l\o-Xytelle BRL

95..75 cxyjene BFL10$9+9 Tetrahdofuran BRL

80.2+7 Efiyt etrer BnL

99t{5.0 Ten-dnyl m€dryl eiher BRL

a7+2-3 Etty' bdtut{ etler BRL

29 ar{7 29-lrar.07 703179 FUldh dy 5.s

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ldlq fy 5.s

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!g4q try 55

pglq fV 5.5

$/lq dry 5 5

|l9h dry 5.s

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pgkg fy 5.s

ttgh fy 11.1

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uErqdy 55

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l,C4g dy l1l

701f l%

7&1W%

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70130 %

ms,qdry 55mg,l0dry 5.5mglqdy 5.5mdkS 4y s.stttdkS fy S.5ftdkdry 5.sn'dlq dry 5.5mdlqdry 55nvlqdry i5'tvb dry 5.5

4,t40%

!o& dv

sw 816 826{S

l@2G3 Disoprogyt et|er

7s5-o Ist-Buland / htyl al€ohd1zlt1-r t,4.CIO(ale

@@4 4.Eronofiwabenzerre

M7.&5 Tdt-Btl€49

17ffi414 1,2-DdlotcdlhaB44

186+&7 Di&MbA@OneUBne

Erlrrctable P€t.oleum Hydrocarbo||J

Erhaalable Tolsl Pelroleum tMrdaftons

P.epared by method SW846 35508

9006-614 Gasdine60r6i102 F€t Otj26s7e3'-3 F|l€t 0it*4685510(H Fueloll 16r,!0900000 t&toroilJ@104000 Aviation fuel

U\i!(,lffi€d

0dr6r Ol

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Cg{36 lfiphalic |}}drocatbolls

3nfi,*2 l-Clio/officene

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OEandlod0e Peslicides St48a6 8081 A

Prepared by mettEd SW846 3545A

3F{O2 Aktin

8RL8RLBRI

91

107

t22

t14

BRL

BRL

8RL

8Rt

8FL

BFL

BRL

8FL

BfuBFL

+CT ETPII n4luty 30.1&r{7 70elz3 DS

sw846 8001A 28-lilar{7 09lor{7 7ll3izJg TG

Thit la.torubry ,eport h ,tot volid flIhotd aa aaahoriaed Eigrrzlare oE thz cots Fage.a Reportable D€tection Limit 8RL = Below Reponing Limit Page 84 of 154

Page 394: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeotificationM8F-53 2'-4'st\5980l-17

Client Proiect #301 -88

Collectioo Date/Tirne26-Mar-07 00:00

MatrixSoil

Received2l -MaI.01

CAS No, Anallte(s) Resuh FloE Unias +RDL Dilution Method Ref. Prcpared Anaryud Batth Analysl

Semlvolrdle Orgrnic Compoun& by CC

oroanod ofte Peslicides SW846 6081 A

Prepared by m€thod SW846 3545A

3r$84+ a-BHC3rsB 7 tsBHC319-8e8 GBHC584s4 9BHC (Lhdane)t-74.9 chbdan€7}54{ 4,4.00D(p,p')71.55e a,a.DoE (p,C)ll2e3 a,a-D0T(p.p')dH7-1 o€ldin9699&3 €ndosuffan It021345 e Endosutfan tl1031{78 €fibsrjffansutfaie72-2G8 En&in74211F{ Endin Aldehyde76-4r{ Heotadlorn4s5 lilehorydlorrn2457-3 HoflacnlorEponde0oorn5'2 Toxaphene5log-714 +Ct ordane556t3{.7 g_Chlordane

s31047C5 tuddn K€tone

t0a{€'l-2 4,4oB4claflwrchjplBnl(Sl

2'6'1-2L1 [email protected]

Potucl orhslod tlioh€nvis b! sw846 8082

Prepa.ed by method SW846 3545A

l?67+11-2 ['Cg t016rr10+2&2 Pc8122111r4r-1e5 ft8123250169.21-9 PC81242ft72-296 PCg 1248rr00?{9.1 PC81254!1000€26 PC81260

a34tt5 PC31292111OOr4-r t[B t26€

Sr,|ogElp rwvrdestwa+z 4,4t8&Bnw6iphenyl(6t)

eL2+3 DefEchhnhiphenyl(Sl

S€mir,olalile Orgstrlc Compo[nds by CCMS

S€mivdetilo Oroadc Comoounds by SV'/848 8270C

PrepaEd by mehod SW846 35508

4.3?€ Aaenaphd*nerDs.966 Acq€fifrytenee.533 Anilifle124.12.f Anh|ac€fle1912.2,r-9 AtazirE100-313 A.zob€nzene/Diphenldanne4.67-5 B€nzijine!i-55-3 Beruo (a) anhnE€ne

BRL

BFL

8fl1

BRI

BRL

BRL

BHL

BFL

BFL

BFL

BFL

BRL

BFL

BFL

BFL

BRL

BFL

BffL

B8L

BFL

BFL

64

96

BFL

BRL

BRL

881

BFL

BRL

BFL

BRL

BNL

n110

lCfrS dry

14.4S dry

ug*s dy

!c4q dry

|ls/ks drv

l4/ts drv

$4q dry

t4vrq ory

udrs drypS4q dry

lSfrS dry

udlq drypg4q dry

lgfts dv

IEKS dypgts dy

!0ts dypg/kq dypgkq dypdks dv

$/kS dy

&150 %&150 %

us,ls ctyp94q dy

lls'(s dvpgxsdv

!g,tg dvpgJiq dy

ps/rs dy!g4q dv

pglq dv

iG150 %

30150 0,6

sw8.468081A320

32.0

32.0

32.0

r60

32.0

32.0

32.0

32.0

32.0

32.0

32.0

32.0

3 2 0

32.0

32.0

?.0

160

32.0

32.0

32.0

28{,lar-07 03'&107 7031739 IG

64.1

64.1

64.1

4 .1

fl.1

64.1

64.1

fl.1

64.1

sv/846 8082

SW8,l6 8270C

2S Mar07 30'Mar.07 703173E SM

2g-l'rar{7 0&Apr{7 7031774 M.BBRL

8RL

BRL

BRL

BRL

BNL

BRL

BRL

ugiiS dry

t$\Sdty

rdlq dry

FVIS dry

$4€ ftv

8,4(S dV

!S4!S dy

ysts dry

686 1

686 I

6S6 1

586 1

686 1

686 1

686 1

686 1

Thb Isboratod tepod is not wlid tdlhout an qathorizd slgr'otwe on the corpr paEe-

'Reportable Det€ction Limit BRL= Below ReportinC Limit Page E5 of 154

Page 395: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samote [deo tificationM8F-53 2'-4,

sA59803- t7

Client Prciect #l0t-88

MarrixSoil

Receiv€d27-Mu-O'7

Collection Dal€/Time2GMar-07 00:00

CAS No, Analyte(s) Result FI"S a b 'RDI Dihaiaa M?rtod RrJ tuepared Aatlfud Batch ,Amlpt

Semivolrtile Org.Eic Compounds by GCMS

Semivohne Onanic Compdrnds bv 5$/846 8270C

Prepared by mettod SW846 35508

5&32-8 Be,Eo (r)py€o€

?0$99-2 Selro 0) nuoandrene191-24'- Seizo(g,h,i)peryisE207{S9 Es|zo (k)fiuord tEno66+5{ EaflzDic acid1@{1-6 B€n4lakDM111-91-1 Bis(2dttorehory)meftano11r-4.t-.1 8is(2d\ho€trytle$\e{sS3&349 8b(2dofiisoprogyt)oherfit{r'7 Bi5{2+ttthsyt)phhatatel0l{t3 {-S|lnoptt€iyt pheoy' edlers5.6&t Butylb$zy1phhatate&71-s Carbszole59.s07 4-chloroF}mehylph€nol106-17.8 {{hloroqiline91'5e1 2-fttoromphfiat€nes+574 24htb@Pheiol7!05-72 3 4ctiorodlellyl lhent st\er218{1-9 ChryE€net97rl3 obBfto{ah}anhn(en613?-649 Dibenzofuran5{&1 l,2€ldlkob€n:€n€511-&1 1,$oidoaob€nz€n€m6.,|a7 1,+DtfoobenzerE91.9+i 3,3-oiddorobenzidnsl20rll!.2 2,4.Dido{ophenols+€e2 obtM phhatate13' 11! Direthyld\hat b105{74 2,aoiiFsrylphejolw1+2 D.nt0lylpHnahb534s2'r 4,S0nit$2-nEhylpnenol$'24.5 2,+hitrophend1211+2 a4-DniFqtoluono6G2rF2 z,6.llnitrctduener17t4{ O+odytphfiatate206-..{ FfuoGdh€n€&7J.t Ruoene11&71.1 thxachhrobqtz€ne6/.€93 Hexadoot{r'tadenen474 Ho(adorocldope.ntadioie

-n-1 Hdaddo@offune19{9-5 H€no (12,$cd) pyrenecf12.0 l-fretrytnaphtlalene785+1 hophorffeer-'|{ 2{iethy'naphttalefles&7 2{vteirylpl|gl€l

r00-r0-4, 3,+[,teh/pnndtH+5gr-2c3 Nadbdqi€0s.74.,r 2-Mroan|lneF+2 3-MtDaniur|e

BFL

BFL

BRL

BRL

BRI

BRL

BflL

BRL

BFL

8Rr8RL8RLBRLBRL8FLBFL

BFLSRLBRTB8LBflLBHLBFL8BL8ALBRI,BRLBflLBHLBFLBRL8RL8RLBRI-BRLBRLBFLBRL8Rt-BFI

8RLB8LBFLBRLBRL8RL8FI.

BBLgRL

BFL

l4lq d,

wh rvlgrg dl

lldlq dy

Wt'r!g4q dry

ljg4q dv

lry}0dy|Jqlg trv

lgfts dry

v4*s &y

E/rq fiy

f94q 4y

ilsrq dv

lsrq dfpdrq dv

|lsas &y

Nrq fv

|lgnq dv

lgkg dy

dlq dry

!g/kg trI

!s4q fy

Wks fiy

r{yh dvpdb drv

uC,lq dry

!S,rS dy

usrq dy

lgks ey

rrgcS dI

ldre dy

!s& d]

ugllq dry

B/lq dry

tgh dv

lgrs ry14is s't|lg/tg dry

|ryqs dyu9,lc dyrErg dylgrg d!

wh dvrid*S dry

Ars dy|4k ev

Udlq dry

|,grs dv!g]q dv

685

686

686

686

686

666

686

686

686

6€6

686

686

686

s6686

686

666

6€6

686

686

666

686

886

6E6

6€6

€€6

686

t€6

€E6

6€6

€ffi

686

666

6€6

686

6€6

686

6€6

686

6€6

sw846 U/0C 2glfarfl wAy TBtn4 M I

This ltbo&tory Eport it noa valil without a aathoriact! si-g'ralare on the cotet page.

. R@rtabl€ DerqrtioE Limit BRI- = Below Repdting Limit PaBe 86 of 154

Page 396: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F-53 2'-4'sA59803- l7

Client Proiect #301 -88

Collection l)ate/Time26-Mar-07 00:00

MatrixSoil

Received27-Mar-0?

CAS No. Alotrte(s) Flog Units *RDL Dilution Pnryred Analrzed Batch lnallsl

Semivolrtile Orgrnic Connounds by CCMS

Semivolail€ o(anic Cornpflnds bv SWB46 82?0C

Pr€pared by method SW846 35508

100.{1€ 4-Nitmanitine

$.9S3 Nitrobenzene

6&7$s 2-t'titrophenol100@-7 4-Nifopi€nol

e75€ N-Nilrosodimefiylamine

@1&1 il-Nitiosodi-n-popylamin€

0s30-6 il.Nilrosodiphonytamineg/.€+5 PenlachloEphenol&t-8 Phenanliaene106-9$2 Pheml129.!04 Pyrener 10.06-1 Pyridine140.€2.1 1,2,+Trjchlorobenzene

9545.{ 2,4,tTdcnbrophenol8-05'2 2,4,ATridbophenot

ic1-604 2-H@riltplEnyl

s7-t21 2'f:hhtqlend

4165.co4 Nivobenenells

11ffi2 Ptgnol4s

1718514 teeleryH4

11&7 2,4,6ftibtonoph61ol

29Mar-07 03-Apr-07 70317i4 M.88RL

SRL

BRL

BRL

BFL

BRL

BRL

BFL

BFL

BFL

BHT

8Bt

8RL

BRL

8RL

59

6t

80

51

68

133

1.81

Compleled

BRL

8RL

0.aM

BRL

8RL

BRL

0.011i

Vdr,gdry 2140

pgXS dry 686

l4^(S dy 686

lglq dy 2740

pS,lq dry 686

pdlq dry 6EG

pdlS dry 6E6

!dt(S dry 6E6

|jg,4(S dry 686

pS4rS dry 686

|lgkS dry 686

UgkS dry 685

Udksdry 686

pdkS dry 685

pS/rS dy 606

3+130 %

15110%g-1u%

1 r t 1 0 %

3Gt30 %

1 r 1 1 0 %

nrgAg dry 0 0355

nS4q d'y 1.I8

mdkS dry 1.78

mdksdry 0.s92

mglq dry 0.2s6

mdlqdry 0 592

mdrgdry 0-888

mCtS dry 1.78

mE 0.0100

nrs/ 0 0150

ngn o@50

mgl 0.0025

ngil 0n125

mgl O0{D40

rhgl 0.0075

mg4 00150

3lrl/846 8270C

Total Metlls b!, EPA 6000/7000 Sert€i M€lhods

7,ll+97-6 Mercury

Totrl Metlli by EPA ?00 Series Methods

114t22.{ Silver

7440-3/}2 A6enic

7{rl0'3$3 Baiun

7rr4!t+9 Cadnium

7!'4,J-47-3 Chtomium

743$@-r Lead

f',]2.4g2 S€l€nium

SPtP Exlaclion

114d?24 Sifuer

7,!10.3&2 Arsenic

7.r,ro3s3 Eadm

74aG€€ Cadniun

7140{n qrronfum

7'F997{ Meretry

7,$9.92'l Lead

1

I

1

1

1

1

1

l

1

I

I

I

I

I

1

st/lJE46 7471 A

EPA200.7

sw8,46 r312

SW8461312,60108

SW8,|61312'?4704

sw8461312/0108

$l/trt|o G Mod-

a2-ap1-o7 03-Apr-07 7031810 YP

BRL

4.42

98.3

0.521

02-Apr-07 HB

SPLP Melrls by EPA lll2 & 6000/7000 Serie3 Methods

7n2{$2 Sdelium 8RL

C.DGr.l Chemhtry Palameters

% Solids €4 4

2&Mar{7 28-Mar{7 70317€3 BD

30 ar0 m'Ap.{7 7031805 LF

" 02-Apr{7 7031806 YP

" (}2-Apr.o7 7031805 L8

30-Marfl 3S-MaF0/ 7031879 YM

This bboralory rcpo it not vrlid tiithout u aatho zed slgnalarc oa the cover page.

* Reportable Detection Limit BRL = Below Reporting Limit Page R? of 154

Page 397: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

APPENDIX DBallast Sample

Laboratory Reports

Page 398: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samplc lde[tificationMSFETsA5946+09

Client Proi€ct #l0l-88

Collccdon Date/Timcl5-Mar-07 00:00

MatrixBaLlast

Reccivedl9-Mar-07

CAS No. Anabte(s) Resall FI"C Uzirs *RDL Dilurian Method ReJ PEpr.ed Ans4red B ch AMryE|

Vobdlc Orgsnic Compo|rnds

Volalile Orqanic ComooundsPrepared by method SW846 5035A Soit (tow levet)76-t3-1 1,1,2-TdchloroHnuoroethane (FreoERL6744-.1 Acetone BRL107-t3^1 AcMonitrih BRL71-432 B€nzene BRL1o€&n Eromobenzene BRL74€7-5 BaornochlorometEne BRL75.274 Bmmodicfiloromethane BRL75-2U? Brornofom BRL744!9 Bronbmethane BRL76-913 2-Butanone (MEK) BRL1{M.s1€ n-Butylb€nzene BRL13s8€ sec-Burytb€nzene BRL98{€-6 tert-Butylb€nzeno BRL75-1fi Carbon dis,_tlfide BRL56-2+5 Carbon tetrachlorde BRL10840-7 Chlorobenzene BRL75{0-3 Chloroethane ARL67{8.X Chlorcform BRL7447-3 Chlorometfiane ARL9549{ 2-Chlorotoluene BRLi0G434 +Chlorotoluene BRL9612-8'1,2-Dibromo-3-chloropropane BRL124-43,i Dibrofibchtoromethane BRL1{rss3.. i,2-Dibromo€thane(EDA) BRL74-9t3 DibrcmoiEthane BRL95{G1 t,z.Oichtorobenzen€ BRL5+1-73t l,3.Oichlorobenzene BRL106-4G7 1!4-Dichlorobenzene BRL7s71-8 Dichlorodifluoromethane (Freon12)BRL75.34-3 1,1-Dichtoroethane BRL107-06.2 1,Z-Dichtoroethane BRL75-35-4 1,l-Dichtoroethene BRL15&59.2 cis-1 ,z-Dichtoroethene BRL15e60-5 trans-1,2-Dichloroettlene BRL7&€7-5 1,2-Dichloropropane BRL142-28€ 1,lDichloroprop€ne BRLS!t-20-7 2,2-Dichloropropane BRLs6$5E{ 1,1_DichloroproF,ene BRL1ar0€1.01.5 cis_1,3_Dic*llorcpropene BRL1(|061{2St-ans-.1,}Diciloropropene BRLi0H1.1 Ethylb€nzene BRL67€al H€xachtorobutadien€ BRL591.78€ 2-H6xanone (l\rBK) BRL96{?$ Jsopropy,,benzene BRL9!1.E7-B +lsoptopyftoluene BRL1eg4!1 M€hytted-buty{ eher BRL1o&i0.i 4-Methyl_Z_pentsmne(M|BK) BRL7s.{r$2 Methylenschtoridesl-zG3 Naphthalsne103{6n n-PropylbefEene

BRLBRLBRL

Ug/kg wet 5.1

Irglhgwel 1O2

pgrkg wel 5.1

pgy'kq lvet 5.1

pgy'kg wel 5.1

lgukg wet 5 1

U94(g wet 5 1

fg/kg wet 5 1

pg/kg wet 1O.2

!g/kg !!€t 50.9

!g/kg wet 5.1

rc/kq wet 5-1

|lgftS wet 5 1

pg/kg wel 25.5

pg/kg weI 5.1

!g/kg wel 5.1

!g/kg wet 1O.2

ug/kg wet 5.1

pgr'kg wet 10-2

yg/kg wet 5.1

rc/kg wel 5.1

pgr'kg wel 1O2

lqn(gwol 5-1

pg/kg wel 5.1

pgL/kg wet 5-1

pgr'kg wel 5.1

lgr'kg w€t 5-1

lgukg w€t 5-1

lgr'kg wet 10-2

!g!kg wet 5.1

!g/kg wet 5.1

!q/kg wet 5.1

lgr'kg wet 5.1

lgr'kg wel 5.1

!g/kg wet 5 1

pg(g wer 5.1

Fqkg wer 5-1

!q(9 wer 5-1

lgy'kg wet 5.1

lgyr(g wet 5 1

lqy'kg wet 5.1

u4kg lv€t 5 1

trg/tg wet 50.9

!9y'k9 wet 5.1

!g/kg wet 5.1

!gA9 wet 5.1

!g/kg wel 50.9

lgr't(g wet 50-9

lCftSwel 5-1

pgks rvel 5-1

sw 846 826091

I

I

1

1

1

1

1

I

1

1

I

7

1

1

1

1

I

1

I

1

1

1

1

1

1

I

1

1

1

1

1

1

1,1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Thit labo.alory epsrl h ,to, w:lu xtitkott sr. zzthoried iignature on thc co,eF pzge.

+ Reportable Detection Limit BRl- = Below Reporring Linit Pag€ 43 of l5?

Page 399: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ ldeptificationM8FFl

sA5%81-09

CliEnt P$iect #301-88

MattixBallast

Collection Dat€y'Tirpel5-Mar47 00:00

Receavedl9-M6147

CASNq. A^o+k(s) ncsub Flq UnlE *RDL Diluiotl Itdhod Rif, Prepsrctl Andwd B,drh A^4lfst

10(H2-5 Sryr€ne63G2OS 1,.1,1,2-TetEchloaoehene7934-s 1,1,2,2-TetrEciloroethane127-18-4 T€trachbro€thene108-a€-3 Tolu€ne876i6 1,2,9-Trichlo.obenzen€120{2-1 1,2,+Tdchlorobenz6trte71-55-6 I ,1 ,1.Ti{*toroethane79{tr5 '|.1,2-Triahloroethane

79{1{ Trichlorosthene

Vohtll€ Orgrhlc Compounds

Volatile Oroanic ComooundsPr@ar€d by method SW846 5035A Soit (low levet)

BRLBRL

BRLBRLBRL8RLBRLBRLBRLBRL

?5{9-4 TrichlorDfluoromethane (Freon 11) BRI-96-18-4 i.2,3lTrhhtoroprop€ne95-636 ,|,2,+Tdrnethytbenzene

108-67s l,3,tTimehylbenzene75414 vinyldllodde1330.20-7 m,p_Xylenes5-17{ o-Xt€ne10$e€-9 Tebah!'drofuran6{f2$7 EtVle&Er994{5{ led-amytmehyledr€f637{2-3 Edrti tert-butyt etherto&20-3 D-isopmpytether7565{ T6rt Bulaflol / butyt alcohol12191.1 1,4-Dioxane

sunDgala rEcoyer?€sr?160401 +BtufioEuorcbenzene2037-26.5 fofuene4g11otuot-o 1,2-Dichlo@elhEne441e6+$,7 Abrcfiofluo@methane

VOC Exhaction

Ertrrctrbl€ P€trolerm Hydrocarbo13

Exhadable Total Petrobum HvdmcarbonsPrepar€d by metltod SW8.l6 35508800tr1 -9 Gasoline$476.3G2 Fuel Ol f268a7e3r-3 Fu€l oal #4685s3-dla Fu€t Oit #6t1098o00o0 Motor olJ00100000 Aviation Fuel

unidenlifiedOlEr OnTotal Pddeum Hydroca6onsCSC36 Alipfialic Hydrocarhons

Suarog'at€ r9co€rbs.3306.3}2 1-Chlot@ctadeqrne

Samlvolra e Orgrdc Co|nporld! by GCOroanochlodne Peslicides SW846 80BtAPrepared by mothod SW846 355083xr40.2 Atdrin

VOC 20-Mar-O7 20-Mar47 7031156 BO

BRLBRI-BRI

BRLBRLBRLBRTBRIBRLBRLBRLBRLBRL

105107116t6

Field €xhacted

$ftS wet 5.1

$^g wet 5-1

lSrtSwel 5.1

|rgrv€wet 5.1

pg/kg w€l 5.'l

Ug/kg w€t 5.1

|lgr'ftg w€t 5.1

pg/kg wet 5,1

$/kg vrel 5.1

lg^gwet 5.1

lgr'kg wet 5.1

!g/I(S rv€t 5.1

UdkS rct 5.'l

ldkSwet 51

IdkSwel 5.1

pgftgw€t 10.2

pgr'kg wel 5.1

!9/k9l€t 50.9

$E/kgwet 5-1

gglkg $/et 5.1

pg/kg wet 5-1

rc/kg wet 5.1

lgtswel 5O.9

ldkg$€l 102

7G1iO %

70-130%

70-130%

70-t30

mg,l(g n.2mS/kS 30.2fiEI(S 30.2mg/kS 30.2n€/t€ 30.2mgn(g f i .2|rrSftS 3O.2rrrg/kS n,2mgr,xg 30.2n'gftg 3O.2

tltttlo %

1

1

I

I

1

1

1

I

1

I

1

1

1

1

1

I

I

1

1

1

I

I

I

BRLBRLBRL8RL8RLBRLBRLBRLBRLBRL

114

wn(s SV\r446 8081A 2143f47 25-Mat47 7U,1'171 TG

Ihb laborator! rqod k nd vdd *irtort a, aqdroriad dgdofrtE oa tlE cowr pagc.

' Reportrblc Dete4iod Lidit BRL - Below Rcporting Linir Page 44 of 152

Page 400: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMSFB-IsA5946449

Client Proiect #301-88

Collection Dat€/Timel5-Mar-07 00:00

MatrixBallast

Receive.d

l9-Mar-07

CAS No, Anatrte(s) Result FIsg Units *RDL Method Rrl Prcparcd AnalJ,aed Bdtth Ada4sl

Semlvol|tile Orgrnic Compoundr by CC

Orqanodrlodne Pe$ticides SW846 8081A

Prepared by method SW846 35508

319-84€ a_BHC31$asF7 b-BHC319{6-€ d-8HC58{9-9 g-BHC (Lindane)

5l-7+S Chlordane72-54-a 4,4-DDO (p,C)

72{ts 4,4-DDE (p,p')

5{F2s3 4,4-DDT (p,p.)

6{157-1 Dielddn95+9€{ Endosulfan I33213{+9 Endosulfan Ilr03r-o7-8 Endosulfan sulfate12 -m+ Endrin74Zl-93{ End.inAldehyde76-,14-{l Heptachlorn43-5 MetlErychlori021-57.3 Heptachtor EpoxideE{D1-3$2 roxaphene5103-71-g a-Chlodane5,s66-34.7 gFchlordane

53494-7Gs Endrin K€lone

S{ttwata racov€r'€sl1038f.8+2 4,1-D&Oclafluorobipheny! (54

m5t-2a3 Decachlorobiphenyl (Sr)

Polvchb.inated Biphenvls bv SW846 8082

Prepared by method SW846 35508

12G7.-r1-2 PCB 101611104-23.2 PCB 122111141-rC5 PCE 1232

$.46921 I PCB 124212872-2p4 PCE 1248i1097{9-1 PCB 125,4i1@€-82-5 PCB 126(}3732+2T5 PCB 1262i11(xrl4.4 PCB 126€

SartogEle rgcoMenesjto38c6+z 4,+DB4cbnuorcbiphenyl (Sr)

m51-2+3 Decachlorobiphentt (5.)

Senivotrtile Org.nic Compoutrdr by GCMS

SW8468081A 21-Mat47 25-Mat47 7031171 rG8RLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

BRLBRLBRLERLBRLBRLARLARLBRLBRLBRL

74130

BRLBRLBRLARLBRLBRL8RLBRLBRL

80115

8RLBRL8RT8RLBRL8RLSRLBRf

!gftSpgftg

ug/Kgpg/Kg

UEKS

lrg/K9

!grkspok9ps&9

!s/ks!s/ks!g/ks!gftgpqlks

!sftsrc/kstrs/KslJs/ts!gag!gr'(g!g/ks

14_2

14_2

14.2

71.O

14.2

14.2

7.00

14.2

14.2

14_2

14_2

11.2

1 4 2

71.O

14-2

14.2

14.2

I

I

1

1

1

1

1

1

1

1

1

1

1

1

1

1'1

1

1

I

1

30,150 %30-150 %

psr(s!sr(s!g/ksps/ts

!g/ksusftgugftg!g/Kg

trg/ks

pgfts

rrg/(gusftg

usftgug/kgPgftgpsfts

!9/kg

24.4

28.4

24.4

24.4

24.4

24.4

24.4

24.4

24.4

30-150 %30-1fi %

Somivolatile Oroanic Compounds bv SW846 g?70C

Prepared by method SW846 3550863-32€ Acenaphth€nea)a.96-8 Acenaphthylene62€93 Anitin€1AI,l2-7 Anlhracene1912.2'l-9 Atralne10333-3 lzobenzene/Diphenyidiazin€

92{7-5 B€nzidine56-5+3 8€nzo (a) anth.acene

SW846 8270C 22-Ma(O7 2UMat47 7O312A2 M.B745

749

749

749

749

749

749

749

Thh laboNtory repo.t k nol jolid toithoar an aathoriTrl signattE ol the cover page-

. R€portable Detection Limit BRL = Below Reporting Limit Pase 45 of lJ2

Page 401: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sahple ldetrtihc{tionMEFB.lsA59,16,|-09

Cliept Project #301-68

MatixBallast

Receivedl9-Mar-07

Cotlection Datc/TimeI 5-Mar47 00:00

CAS No. Ahalye(s) Flag ania 'RDL Diluiod Method Rel. Preparcd Awltr,ed Bolch Analfsl

Semivohtile Orgmic Compo{nds by GCMS

Semivolatile Oroanic Co,npounds bv SW846 8270C

Prepared by method SW846 35508

50-32{ Benzo (a) pyrene205-99-2 Benzo (b) fuoranthene191-24-2 Benzo (g,h,i) perylene207{€-9 Benzo (k) f,uo€nthene

BerEoic acid1CD-51{ B€ftzylalcoholll1€r-1 Bis(2rhloro€thory)methaner1laa{ Bis(2-chloroelhyl)etE.3efie32{ Bis(2-ohloroi6opropyl)ether117{1-7 Bis(2-edrylhexyt)phthaiate101.55'3 4€romophenytphenylelher454&7 Buty' b€nzyl fithetate86-744 Cathazole5S50.7 +Chloro-3-metrrylph€nolro6-1ru +Chloroaniline91{8-7 2-Chloron6phthalenessz{ 2-CNorDphenol7005-72-3 +Chlodopheny' phenyl €ther2i8{1-9 Chrysene53-?G3 Oabenzo (a,h) anthracene132{4-9 Dibenzofuran95.:41 l,zoichlorob€nzenes4i-7}1 .l,3oichlorcb€nz€ne

ttrF4eT 1,4-Dichlorobenzen€91-34,1 3,3--Dichlorobenzidin€12(]"83-2 2.+Dichtofophenols,!46.2 Oiedryt phhatate131-r1-3 Darnethyl phthatate105{7-9 2,4-Dimethylph€mlB1-74-Z Di-n-butylphthalatsss4-52-1 4,6FDinjtro-2fiethylphenol51-28-5 2,4{)initrophenol12r-14.2 2,Goinitrcbluene60cat-2 2,&Dinitrotoluene117-6.1{ Di-n{atylphthatetea}6-444 FkJoranthene46.732 Fluo(enei16-74.1 Hexad Oaobenz€nea7{{l-3 l-l€xachtorobutadiene77474 Hexaafilorocydopentadi€ne67-72-1 Hexactoroethane193-3ss Indono (1,2.$cd) pyrene90{2-0 i-l,l€S1g$aph(1alene7S5{}l lsophorone91-57{ 2.iletfrylnaphtfialene95-4&7 2-Mgdtylph€nolro&394, 3,4-fttethylphenol106-,t4,5sl-20-3 Naphthalene&741 2-Nitroanilane99-092 +Nitroaniline

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRfBRLBRLBRLERLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLERLBRLBRLSRL8RrBRLERLBRLSRLBRL

BRLBRLBRLBRL

BRLBRLBRL

!s/ks!gftSrsikgt gftg

ti0/t9

FqkSPg/k9!sr(sLrsftslgks|€T€us^sus/ksus/kgpElq

$srksuslks!s/kspsiks

WftsFgk9p9&9pgks

!sr(srcfts!sftsrcn(s!9ft9

usrkspcftsp4ks

!sftsusftsrcftgt s/tg!s/k9ys/kspdkgpdks

usr(s|lsfts

!sftg

Et,ksl|grkgpgl(s

I,rd*9pg/kg

|lgI(Sugftg1€ikS

749

7{9

749

749

749

749

749

749

749

749

74S

749

749

749

749

749

749

745

749

749

749

749

749

749

749

749

749

749

749

749

749

749

749

749

745

749

749

749

749

7,19

749

z,t9749

749

749

749

749

749

719

74S

SW846 8270C 22-Met47 254t,,et47 703128i1 M.8

Ihlt l4borehrf Eprt 16,tot eali.l pirhout an a hodz.d tignauE on tht qt , page.

'Reportabl€ D€tection LiEir BRL = Betow Reponing Limit Page 46 of | 52

Page 402: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarflple ldentificationMSFB-1

s459464-09

Client Proicct #301 -88

Collection Date/Timel5-Mar47 00:00

Matrl{Ballast

Received

l9-Mar-07

CAS N.L Anaut4s) Flry Ani6 *RDL Diltttion Method Retr. PnpEd AnaIWl Bot h Antllst

S€dvotatil€ Organic Conpounds by GCMS

S€mivolatile Orcanic Comoounds bv SW84ti 8270CPrepared by method SW846 3550810G0t{ +Nitro€niline98€+3 Nitrobenzen€{lll-75{ 2-Nitioph€nol10G@-7 +Nitoph€nol62-7ts N-Natmsodimef,rytamine6219-7 N-Natrcsodi-n-propytamine8e3o{ N.Nitrosodiphenytamin€07{6-5 Pentachloroph€nolC5{1{ Phenanthren€10+95-2 Phenol'l2gOO{ Pyaene11046-1 Pyridane12G€2r |,2,4-Taichlorobenzene96-954 2,4,$Trichlorophenol88{Fz 2,4,GTrichtoroph€nol

S.Jarogate recover'€s:32150-8 2-Fluorobiphenylfi7-121 2-Fluorophenol4165604 Nitr,benzene4141r,!rt2-2 Phenol4st71e5t4 Ierphenyl-d!4118-7 44,&Tibrcmophenol

Totrl Metab by f,PA 6000/7000 Scri€s Methods

7439{7€ Mercury BRL

Total Metlls by f,PA 200 Series Methodr

BRL

BRL

10.8

0.626'1.97

5.08

BRL

1 SW846 8270C 22-Mat47 2sMaFOT 7O312A2 M.B

1 '

1 "

1 "

1 '

1 '

1 "

1 '

1 ' ,

1 '

1 '

1 '

1 "

1 "

1 '

BRLBRLBRL

BRLBRLBRLBRLBRLBRL

8RLBRLBRLBRLBRLARL

392633284427

PSI(S 3000

pgftS 749

!S/kg 749

Ug/kg 3000

Ug/kg 749

l.iSftS 749

lgftg 749

!g/kg 749

lgftg 749

!g/kg 749

tS/kS 745

!g/kg 749

pg/l(g 749

lsftg 749

pS/kS 749

30-tu %

t u t 1 0 %

m-130 %

t r l t o %

30'1n %

11110 %

ftg/kg 0.0295

mg/kg 0.920

nE/kS 1.38

mg,kg 0_450

mg/kg 0 230

mg/kg 0.460

mSftS 0.690

mS/kS 1.38

mg/l 0.0100

mg/ 0.0150

rngl 0.0050

mg/t 0.0025

nE4 0.0O5O

mg/l 0 m0+o

mgl 0.0075

rhg/l 0.0150

?.4G22-4 Silver

74rr&3&2 Arsenic

I44G3&3 Sadum

744043-9 Cadmium

7rt4o-47.3 Chromium

7439-92-1 Lead

Z€?492 Se|enium

SPLP Mctrk by EPA 1312 & 6000/7000 S€ri6 Merhodt

SPLP Extraction Cornple{ed

7440-2-4 Silver BRL

71.10'3&2 Arsenic 8RL

71-40-39.3 Badum 0_0066

7rt4H$9 Cadmium BRL

71-1047-3 Chrcmium BRL

7439.97.6 M€rcury BRL

743S92-i Lead BRL

1'782-t92 Selenium BRL

1 SW846 7471A 26-Mar-07 26-Mal'07 7031311 YP

1 EPA200.7 26-Mar-07 26-MaF07 7031263 LR

1 "

1 ' ,

1 '

I '

t SW8461312 21-Ma(47 21+,/tat47 7031229 BO

1 SW846l31Z6O10a 22-Mat47 z4-Mat-Ol 7031323 LR

1 '

1 "

1 '

1 SW8,f6 131217470A " 23-Me.47 7031324 yp

1 SW846131260108 " 24-Mat47 703'1323 LR

Thh lab.elory rcpod is not valid ts hoa an authorized slgnalare on the cover page.

' Reporhble Detecdon Limit BRL = Below R€portinC Limit Page 4? of 152

Page 403: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarrple ldentific{tioflMSFB-2sA59464-r0

Clieut Proiect #301-88

MatrixBallast

Collectiotr Dat€/TiEeI 5-Mar-07 00:00

Receivedl9-Mar47

CAS Na Anebt4s) Fl"8 Unili *ADL Dltalian Mahod nej Prcpered Analfred Bdlch Analtsl

Vohlile O.gaf, ic Coupotrnds

Volatile Orqanic CompoundsPrepared by method SWa46 5035A Sdl (tow levet)76_131 t,1,z-Tndlbrctdfluoroethane(FreoBRL6744-1 Acetooe BRLt07r91 Ad.ttonitile BRI71112 BerEene BRL1o8-8s1 Brcrnobenzene BRL74.97.5 Bfomod oromefiane BRLf5-274 Brffnodidtloromethane BRL-15-25-2

Bfomoform ARL74{3-9 Bro|r|omelhane BRL78-e3-3 2€ubnone (l!lEK) BRL1lM-sl{ nlButylbonzene BRL13+96{ sec-Bu!y'b€nzene BRL9A{6-€ teft-ButytbefEene BRL75-1s{ Carbon disutfide SRL5d23-5 Carbon tsbachtoride BRL10&9e7 Ct odobeEene 8RL75-{)0.3 ChiorD€lfEne BRL67{&3 Chlorcfonh BRL74-9t.3 Chloromethane BRL!'$4+6 2-Chlorotoluene BRL10€-43.1 +Chlo{obluene BRL116-i2-a 1,2-Dabrorno-3-chloropropane 8RLt24-4-1 Dibomochlorcmehane BRL10Ge3-4 1.2-Dib6moefian€ (EDB) BRL7{{$3 Ditromo.nethane ERL95.50"1 l,2oichlorob€tEene BRL:,41-73-1 1,3-Oichlofobenz6ne 8RL106-46.7 l,+Dichlorobenzene BRL7+71-a Dichlorodifluorcmethane (Freon12)BRL75-3.{-3 |.1-Dichtoroethane BRL10746-2 |,2-Dichloroethane BRL7t35-4 |,1-Oicfiloo€thene BRL15&5e2 cis-j,l-Dichloroethene BRL156€0-5 tans.1.2-OiafitoroettEne BRL7817-5 l,2.OichlotEpropane BRL142-28€ l,3-Dichloropfop€ne BRL594-2{l.7 2.2-DichtoroF.opane BRL56358{ l, l-Dlchloropropene gRL

10061{1-sciel,3oicfgoNopropene BRL10061€{trans-l,3.DichbIopropen€ BRLioGal-4 Efiylt€nz€ne BRL876&3 Herecfilorobutadie{e BRL5e1-78-6 2-Hexanone (MBK) BRf98{2{ tsopropylbenzene BRLs&47{ +troprqyltoluene BRL1634.044 M€0iytted-buD4 eth€r BRL10&r0'r +M€thyl.2-p€ntianone(MIBK) BRL75{s2 Methybnecfilodds BRL91-m-3 Naphthalene BRLt0l€+1 n-PropylbffEeoe BRL

SW 646 8260S 22-MIFO7 22tJls47 7031291 RLJtEftg wel 5.2

pg/kgwet 104

!g|/l(gw6r 5.2

ldkg lv€l 5.2

lgL/kg w€t 5-2

pgr'kg wet 5-2

l8rkg wel 5.2

!g/kg wet 5.2

Ug&g wel 10.4

pdkS vret 51.S

f.ig/(g trst 5-2

lgr€ Yret 5-2

pgn(g wet 5.2

rdkgwet 259pg/ftg wet 5.2pdkg wel 5.2

ld lSw€l t04

ldkg Yv€t 5.2

lgtkg wet '10.4

yg/kgwet 5.2

Ig/tqs,et 5.2

lgtgwel 10-4

pgrkg wel 5.2

ldkSw€t 5.2

lgl(g r,'/et 52pS4(S Yrst 5.2

t g/kg wet 5-2

psrkgwet 5.2

pg'kgwel 10-4

!g/kg wel 5.2

ldkS !ve! 5.2

lgL/kg w€t 5.2

lgkS rY€t 5.2

lrS/kgwst 5.2

Pg*Ow€t s.2pgkg wel 5.2

!g/kS wel 5.2

Igr'kg w€t 5.2pdkSwet 5.2pdkS rYet 5.2

!g/kg v{et 5.2pgl(g rcl 5.2

lgkg w6t 51.S

!g/kg wet A2

Ugk€ v/ot 5-2

ldkS vret 5l

trtgr'kg vr6t 5t,9ySikS wel 5l.S

Fg,kg w6t 5.2

!g'kg wel 5.2

Thb labontory Eporl ie .tol vzlitl *lthout M zttdrottzd slgnalarc od ,hz {,,ver' page.

'Rcporiable Detectior Limit BRL = Bctow p.€pofting Linit Pa€e 48 of | 52

Page 404: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationM8FB.2SA5946jl-10

Client Proiect #30 t -88

Collection Date/Timel5-Mar-07 00r00

MatrixBallast

Received19-Mar-07

CAS No- A^alrte(s) Result FloC Ani,l IRDL Dilation Method ReJ PEpaRd A,nuied Balch Aiabxt

Volttile Organic Conpoonds

Volatih Oroanic ComooundsPrspared by method SW846 50354 Soit (tow tevet)100-42-5 Styrene6:10-20{ 1,t,1,2-Tetrachloroethane79-34-5 1 , 1 ,2,z-Tetmchloroethane127.184 Telr€chloroethene108{83 Toluen€

87i16 1,2,3-Trichlorobenzene12(182-1 1,2,4-Trichlorobenzene7t-sfF6 |,1 , t -Trichtoroethane

794Gs 1,1_2-Tichtorcethane

BRLBRLBRLBRLSRLBRLBRLBRL8RL

BRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

1091M105100

Field extracted

BRLBRLBRLBRLBRL

BRL8RLBRLBRLBRL

122

BRL

!g/kg wet 5.2

!g/kg wet 5.2

Ug/kgwel 5.2

pg/kg wet 5_2

pC'kg wet 5 2

pgykg wet 5.2

!S/kS wet 5.2

!g/kg w€t 5-2

pdkgwet 5.2

lig/kg wel 5.2

pg/kg wet 5.2

!g/kg wel 5.2

!g.eg wel 5.2

pgr'kg w€r 5.2

pg/kg w€t 5.2

!g/kg w€t 1n.4

Ug/kg w€t 5.2

!g/kg w€t 51.9

jJg/kg wet 52

pS/kS wet 5 2

uS/kS Yrel 52

Ug/kg wel 5.2

trg/kg wet 51-9

!g/kg wel 104

70-130 %

70-130 %

70-1m%

70-tm %

nE/tg 25.4

mSI(g 25.8

mSn(S 25.8

mg/kg 25.A

rngftS 25.8

mg/kg 25.4

mS/tS 25.8

mgftS 25.8

mg/kg 25.8

mSI(S 25.8

44-140 %

pS/tg 13.8

l

1'|

I

1

I

I

1

1

1

1

1

I

I

1'|1

I

I

1

1

1

1

1

SW846 82608 22-MaF07 22-Ma?01 7031291 RU

79{16 Trichtoro€thene BRL7s{9-{ Trichtorofluoromethane (Freon t1) 8RL96-14-4 .1,2,lTrichtoropropane

95-6ire 1,2,+Trimethylb€{zene108{7{ 1,3,s-Trimethytbenzene75-0i.4 Vinyl chlodde'1330-2G7

m,p"Xylene96-47{ G.Xylene10$€$€ TetrahydrofuEn60-2$7 Ethyiether994-09F8 Tert-amyl methyt ether637-92-3 Ethy ten-butyl etheri0&2G3 Di-isopfopytether7s€r,.{) T€d_Butanol/butylalcohol12$9in 1,4-Dioxane

Surrogale r€cou€niesi460404 A4.cmofluorcbenzene

m3r-2c|5 Toluene-dB

tr0644/4 l,2aichtorcethane-d4

1ffi8-5i-/ Abromoffuorcmelhane

VOC Extraction

Extractrble P€trolcum Hydrocarbofi s

Extrectable Total Petroleum Hvdrocadons

Preparsd by melhod SW846 35508

800ffi1-s Gasoline6€47d3o-2 FuelOil#26847+31-3 FuelOi l t4€€55+o0-a Fuel Oil l(5M09m00(xl Motor OilJA100O0O Aviation Fuel

ljnldenlified

Oth€r Oil

Total Petroleum Hydrocarbons

Cg-C36 AliphEtic Hydroc€rbons

St rTogele rEcov€riesi?3a6-33.2 1-Chlorooctadecane

Setnivohlil€ Orgrnic Conpouhds by CC

Orqanochlorine Peslicides SW846 8O8lA

Propa.ed by melhod SW846 35508

30s0G2 Aldrin

VOC 20-Mar47 20{1ar47 7031156

+CTETPH 224lla(47 26nna'{7 70312A3 DS

SW846 8081A 21-Mar47 2&Mar-07 7031171 TG

Thit labototory rcpod is aot edid taithozt an au&odzed signature on the corer page .

* Reporlable Detecrion Limir BRL = B€low Reoo{tine Limit Page 49 of 152

Page 405: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeotificationM6FF2sA594*10

Clie P.oi€ct #l0r-88

Collectiou Date/fimet 5-Mar-0? 00:00

MarrixBallasi

Receivcdl9-Mar-07

CAS No. Analyu(s) nesu! Fhs 'RDL Dilztioa Irlcthod Rctr Prepued AnolyzTn Bdch Arultaa

Semivolatll€ (kg.ric Compolrds by GC

O.oanochlorine Posticides SW846 8081A

Prepared by .nelhod SW846 35508

3l$416 a-BHC

319{5.7 b.BHC

319{6€ d-BHC

5€{+e 9-BHC (Lirdane)

57-74-9 Chlodane

7?-544 4,4-DDD (p,p,)

72{5€ 4,4-DDE (p,p')

50-2s3 4,4-DDT (p,C)

60-57-i Dl€lddn95+98{ Endosulfan I

332i$65-9 Endosulfan lli031-07€ Endosulfan Sulfate72-204 Endrin7421-93{ EndrinAjd€hyde79'114 Heptactrlo(7243-5 Methorydrlor102rL57-3 Heptachlof Epoxid€800i.3S2 Toxaphene5103.719 a-Chlodane5566-34-7 g-Chtodane

53{9+70.s Endrin Ketcne

&rTogal€ rBcaveres-,1oia68+2 4.4o&Octaf,rcmbiphenyt (54

n51-24-s Decachlotobiphenyt (Sr)

Polvchlorinated Biohenvls bv SW846 808iPrepared by rnethod SW8,'G 35508

1267+11-2 PC8 10161t1O+28-2 PCB In11r14i-16-5 PCB 12325346921-9 PCB | 24212612-E$ PCE] 1248ilo97s$r PcB 12541 r0s6-82€ PCB I m03132+*5 PCB 12621110S14{ PCB 1268

Su''ogafe rEcovdrbs.'lNse8+2 4,U)+OataflrMtobiph6nyt (54

m51-24i Decachlotobiphenyt (Sq

Semircladle Ory. c Comportrdr by CCMS

Semivolalile Orqanic Comoounds bv SW846 827(rcPrepared by method SW846 35508€g.324 Acen@hth€ne4&96-8 Aconaphthyt€ne62.s+3 Aniling1a).12-7 Anhrgcen€19i2-24-9 A!.azjne103.3?3 ArobenzendDlph€nytdiazin€9247.5 Benzidlne5ssta Benzo (a) a.lhlac€ne

BRLBRLERLBRLBRLBRLBRLgRL

8RrBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRL

76109

BRLBRLgRL

BRLBRLBRLBRLBRL

BRL

801 1 5

BRLBRLBRLBRLBRLBRLBRLBRL

Fs/k9usftst€fts!g/ksug/ksPsn(s|rsftspsfts

!s/ksPgl(s!glksyg/ks

Psftspsfto

lrsAstiS/k9pg/k9psr(9

usr(gpsrkspdrs

13.813.E1 3 81 3 868.9r 3 8r3.813.87.0013.8'13.8

1 3 I13.8t3.8r3.813_813.068.913.8r3.8r3.8

27.5

27.5

27.5

2f .5

27.5

27.5

3G150 %& l f i%

sw8.r6 80814

sw846 6082

1

1

I

I

I

I

1

1

1

I

I

I

I

1

1

I

t

1

I

1

1

21-Ma(07 2&Ma(41 7031171

FSftg

Fs/tg

Fgikg

Fs/ksPgr(strsastrgftsps./kspsft9

us/ksvcr(gPryKSps/rs!s/ksugftg|,9nlgusits

214t|a147 2d.Matr47 7031170 SM

30-150 %3Gtfl %

841

641

641

641

u1u1641

641

sw846 8270C 22+,,lar$ 25+rs{7 7031282 M.B

Thb laLodory report it @t valid t{Uhoat aa atthorizd stgnarnre on the cov.r pqe.

' Rcportable Detection Limit BRL = Below Repo.rine Limit Fage 50 of | 52

Page 406: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiorM8FB.2sA59464-r0

Client Proiect #30 t -88

Collection Date/Timel5-Mar{7 00:00

MatrixBallast

Receivedl9-Mar-07

CAS No, Anatrta(s) Resall FIag A n s *RDL Dilurian Method ReL Prcpued Anabzed Bdtch Atlalyst

Semfuol.dle Org.nic Comlounds by CCMS

Semivolalile Oroanic Compounds bv SW846 8270CPrepared by method SW846 35508

lO-32{ Benzo (a) pyrene

2os9+2 Benzo (b) ffuoranthenei91-24-2 Eenzo (g,h,i) perytenem7{8-9 Benzo (k) fuoranthene65-05{ Benzoic acid10G51{ Benzyt alcohol111-91-1 Bis(2-chloro€thory)methane111-44-4 Bis(2-d oro€thytFther3e€s32-9 Bis(2.chloroisopropyt)€therri7-e1-7 8is(2-ehytheryt)phthalatet0r-55-3 +Bronrcphenytphenylether85{&7 Butyl benzyl phthalate

E6-7+€ carbazole59-5G7 4-Chloro-3_melhylphenol106{7-8 4_Chlofoanilane91.5+7 2-Chtoronaphthatenes.s74 2-Chtorophenol700$72-3 +Chtisrlrphenyl phenyl ether2l&{11-g Chrysene53-70-3 Dibenzo (a,h) anthracene132€4-9 Dibenzofuran95-6G1 1,2-Dichlorobenzene

541-Zlr 1,3-Dichtorobenzene'106'tG7

1,4-Dichlo(obenzene91.9,r1 3,3'-Dichlorobenzidine12()'83-2 2,4-Oichlorophenolu46.2 Diethyt phthalate

13t-1tr Dirn€lhyjphthatate105,67.9 2,+Dinethytphenola4-74.2 Di-n-buvphthalate534-s2-1 4,6-Dinitrc-2-methylphenol5r{8-5 2,4-Dinitrophenol121-14-2 2,4-Dinitrototuene60+m-2 2,6-Dinitrotoluene'll7+4{

Di-n-octy,tphdrslate20fr4{ Fluo@nthene

0G7$7 Fluofene11S74-1 Hexachlorobenzene87$€-3 Hexachlorobutadienen474 Hexachlorocyctopentadiene67-72-1 HexachloroethaneiS3-39{ Indeno (1,2,3-cd) pyrene90-12-0 1-Methylnaphhatene765+1 lsophorone9157$ 2-Methylnaphthatene95rl&7 2-Methytphenol

10€-3€-4, 3,4-Methylphenolltxi-44-591-2G3 Naphthatene4l}714 2-Nitrosniline90-0!!2 lNitroaniline

BRL8RLARLBRLBRLBRLBRLBRLARLARLBRL8RLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL

BRLBRL

BRLBRL

BRLBRLBRL

!s/ksLjsftgtls/k9!s/kgrc/kspeyK9ps/ks

!g/Kgpsfts

rcftsps/ks

tjgft9

ugks!s/ks!g/ks!g/Kg

Lig/Kg

!g/Ks

ug/kslrq/Kg

LiS'"(S

us,ksugts!s/kspg/ksps/kg

Li9/Kg

Ljsftgpgfts

!sftg

|lg/r(g

!s/ks!s/rs!sr(sugksudksps,4(gpsr(s

!s/tsLiS/kgugftsLis/xs

!gftspsfts

|lglkgpg/ks

!gftg

lsik9

!s/ksus/t(s

641

a+1641

641

64'l

641

641

641

a+1a+1641

u lu1641

641

64r

&11

&t1

641

641

641

641

641

641

u 164'l

641

&t1

&{1

641

641

641

641

641

641

641

641

641

641

an1

641

641

Bl1

641

u1641

u1

641

64'l

641

SW846 8270C 22-Ma(O7 25-MarO7 7031282 M.A

Thb lsborutory rcpod ir ttol valhl withoa att aalhoriZed slgaalurc ott ihe corer psge

* Reportabl€ Detection Limil BRL = Below ReDortins Ljmit Paee 5l of 152

Page 407: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple IdcntificationMtFB.2sA5946L l0

Cliert Pioiect #30 t18

Collection Date/Timel5-Mar47 00:00

MatrixBatlast

Received| 9-Mar-07

CAS No. Andltu(s) ResuL Flae UniB 'RDL Dllutlan Lrahod Retr Prcpond Analyzcd Balch Arultsl

Semlvokdle Organic Compound! by CCMS

Semivolatile Oroanic Comoounds bv SW846 8270C

Preparod by m601od SW846 35508100{1{ +Nitoaniline98-9+3 Nifobenzene{18-75-s 2.Niuophenol10(}02-7 +Mlrophenol62-754 l,l-Nifo6odim€thytamine621€{-7 N-Nitosodi-fi-propylamine86-30{ N-Nitrosodiphenylaminee7{6-5 Pentiaciloroph€nol854i-0 Phonanthrene10&95-2 Phenol129-00{ F}r€ne110-8€-1 q/ridin€120€2-1 1,2,+Tridlorobenzen€96-95-,1 2,4,5-Tfichlorophenolaa{6-2 2,4,GTrichlorophenol

Sarzogrle a€corrgresl3214G8 2-Fluorobiphenyl367-124 2+luotwhend4165,@4 Nitobenzene4s416+s2-2 Phenol4st71A-514 Terphenyl4l4t 1 8-79-0 2,4,6Tl'}tumophenol

Torrl Metr|! by EPA 6{Xxrflt00 scries M€thodi

BRLBRLBRLBRLBRI-BRLBRIBRLBRLBRLBRLBRLBRLBRLBRL

4024303043

ISitS 2570pg/tg U1

FSftg 641pCftS 2570pgks 641pS/kS d{l

ldkS 641

Ug/kg 641

!g/kS U1

tSftS 641

tgftg 641

US/kg U1

pS,}€ 641pSrl€ 641

n-130 %l5-110 %30-1n %ttf io%36tm%15.110%

mglkg 0.0295

mS/kg 0.991

mgikg 1.49

mS/rg 0.49{t

ngts 0.248

mgkg 0.496

mg/kS 0.743

mS/kg 1.49

mgn 0.0100

rngl 0.0150

n€n 0-0050

ntSil 0.0025

mgn 0.q)50

mdr 0.m040

mS/l 0.0075

nE|4 0O15O

2 .{ar47 7@1 324 yp

23-Mar{7 7m1323 LR

SW8/68270C 22rylar{7 2grr€r-07 70:}1282 M.B

7439-97{ l\rercury

Totd Metsb by EPA 200 Serles Methods

744F.224 Silvqr

74,4G3+2 AF€nic

7440-393 Badum

zr40-4+9 Qsdmium

74.t&47-3 Chromium

744942-1 Lead

z82.rr9? S€t€nium

I SW846 7471A 26llar{7 26+ra.47 7031311 YP

1 EPAAn-7 26-|i{a.-07 26- ari7 7031263 LR

1 '

t "

1 "

1 ' .

1 '

1 '

1 SW8461312 21-tlar47 21tur47 7031229 BD

1 SW8.161312/6O108 22+'rd{7 2 vbr{7 7fi}1323 LR

I '

t '

1 '

1 '

I Sr/Ve46 131,y74704

1 SW8,16131?J€010S

BRL

BRL

BRL

0.506

3.22

BRL

SPLP M€bl! by EPA l3l2 & 6000/t00O Serte3 Meahodt

SPIP Extraction Compleied

74{n-22-1 Situ€. BRL

74-1rl3$2 Arsenic BRL

7r4O-3$3 g€rium 0.0092

744(H&9 Cadmiun SRL

7r4O-473 Chrcmium BRI

743997{ M€roury BRI_

7439€2-1 Lead BRL

z€a492 S€l€naum BRL

This labontory nwxt ls not valirl withord o eulhorledslgnatarc on tha cop.r psge.

! R€portable Detection Limit BRL = BeloF ReportiDB Limit Page 52 of lS2

Page 408: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificationM8FB.3

sA59464-l I

Cliert Projecr #l 0 l - 88

Collection Datci/Timel5-Mar-07 00:00

Mat.ixBatlast

Received

19 -Mat-Oj

CAS Na Analtte(s) Resah Floq U,riB aRDL Dilutiofi Mc.hod Retr. Prcpond Amlyel Batch Anallst

Vohtil€ Orgrnlc Compo|rnds

VOC Exlraction

75{&2 Methylenechloride91-2+3 l{aphthalen€

lSikg 52.2

tS/kg 1040

LiS/kg 52.2

f.iSftg 52.2

yS/kg 52.2

I'Silq 52.2

trS/kS 52.2

pSrkS 52.2

FS/kS 104

!g/kS 522

!S/kS 52.2

!g/kg 52.2

Ug/kg 52.2

lSftS 261

pg/kq 52.2

lg/ftg 52.2

pdks 1O4

pS/kS 522

pS/kg 104

pg/kg 522

!g/kS 52.2

f.iglkS 1O4

pS/kg 52.2

rcfto 52.2

US/kS 52.2

pg/kS 32.2

pg/kS 522

lgn(g 322

!SA9 1O4

US/t(g 52-2

udkS 52.2

pS,4(S 52.2

!g/kg 52.2

!S/kg 52.2

!g/kg 52.2

pdkS 522

lSlkg 52.2

pgftg 52.2

lSftg 52.2

!Sn(S 52.2

pgftg 52.2

lSftg 52.2

USftg 522

ldks 52.2

W/kS 522

l,g/ks 52.2

!g/kS 522

lgftS 522

pgks 52.2

Field extracted voc 20-Mar-07 20-Mar-07 7031156 BDVolatile Oroanic Compounds Ro5Prepar€d by nethod SW846 5030 Soit (high tevet)

78'111 1,1,2_lrichlorotinuoro€ttane(FreoERL67-@,1 Acetone BRL107n3r Acrytonitrile BRL714Y2 Benzene BRL104-86-l Bromobenzene BRL74.97-5 Bromochloromethane BRL75-274 Bromodichloromethene BRL7$2$2 Bromoform BRL74{}9 Brortomelhane BRL7443.3 z-Butanone (MEK) BRL104-51{ n-Butytbenzene BRL135F98i sec-Bu{ylbenzene BRLsa{16.6 tert_Bulytbenzene BRL7s-1s"{r cabon disulfide BRL56-2+5 Carbofl tefachlorjde BRLl0&S0-7 Chlorobenz€ne BRL75{G3 Chloro€thane BRL67{43 Chtofoform BRL7147-3 Chlorornehane BRL95-494 2-Chlorotoluene BRLroG4+4 4-Chtorotoluene BRL9+12€ 1,2-Dibromo-3rhtoroprcpane BRL1zr|.{a-r Dibromochloromethane BRL106-e3-4 1,2-Dibtomoefiane(ED8) ARL744+3 Dibromomethane 8RL95-51F1 l,2-Dichtorobenzene gRL

5{1-7}1 l,}Dichtorobenzene BRL106-46-7 '1.4-0achloroten2ene BRL75.7i4 Dichlorodilluoromethane(Freoni2)BRL7+343 1,l-Oichtoroethane BRLt07-62 '1,2-Dichloroethan€ BRL753514 1,l-Dichloroeth€n€ BRLi5€-59-2 cis-1,2-Dichloroethen€ BRL15G60-5 b6ns-1,2-0ichtoroethsne BRL7E€7-5 ',2-Dichloroprop€ne BRL142-28-9 l,lDichloropropane BRL5,94-20-7 2,2_Dichloroptopane BRLs6,a58€ l,1-Dichlorcpropene BRL1006101-5cis-l,}Dichlorcprop€n€ BRL10061.02€trans-I,3-Dichloropropene BRL1rlc,-414 Etht{benzene BRL87-6&3 Hexachtorobutadiene BRLs91.786 2-Hexanane (MBK) BRLg8-€a€ lsopropytbenzene BRLs37'6 4lsopropyltoluene BRLr634-04-a Metht4 ted-buhy' ether BRLroFrGi 4-Meth!'l-2-p€ntanone(MIBK) BRL

BRLBRL

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050505t)5050

SW 846 82608 21-Ma(47 22-Mat47 7031189 jro

Thit ldtoratory npod it not vzlitl h'ithoa! an aathorized signatu.e or ahe cowr page.

' Reportabl€ Detection Limit BRL = Below Reporting Limit Page 5l of 152

Page 409: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnole [dentificatiooM8FF3s459464-t I

Ctiept Proiect #l0l-88

Collection Date/Timel5-Ma 7 00:00

MatrixBallast

Receivedl9-Mar-07

CAS No. Antlru(s) Result Fhc rRDL Dilution Method Ref. PrcWed Aaztlzed Bach Aazlyst

Voletile Organic Compounds

Volade Oroanic ComooundsPrepared by method SW8,l6 5030 Soil (high levet)

7t69-4 Trichlorofllororn€thane (Freon 11) BRL

1fi65n n-Propylb€d€ne100-42-5 Styl€n€63Gm6 1,1,1,2-T€t€cftloroethane793rr-s 1,t,2,2-Tetrschloroehane12h8-4 Tet€dhloro€fEne108{all Totu€n€87{1{ 1,2,}TnchbrobenzeDe120{2-1 1,2,+Tdchlorcbenzene71-str |,I , i -Tridlloro€thane79{Gs 1,1.2-Tricftloroethane79{1{ Trichloroeth€n€

96-1S4 1,2,$T.ichloropfopane95-6!6 1,2,r1-Trimgthylben2s6s108574 l,3,tTrimethytb€nzene75{r-1 vinyl chloaide133O2G7 m,p"Xy4en€95-47{ o-Xyt€ne1099&9 Te{rahydofuran6+28-7 Ethyl eth6r99{ff Tort-amy' methy' ether637-9?-3 Ethy ten-botyt eth€r10&2G3 Di-isopropyleth€r75-85-0 Tert8utanol / buq/ atcohol12+91.1 1,4-Dbx€ne

Sunogate rccovg'les:tW41 +Bmmofluotubenzene

2o37-26n Toluene4€l

I f 06r|074 1,[email protected] 4186esH Dibromoquoaonethane

Ertrlctsbl€ P€t.oleum Hydrocrrbo$

Extraclable Total Peholeum Hvdrcca.bons

PrepaEd by method SW846 35508

€lXl6€1-g Gasolin€60476-3G2 Fuet Oit #26847G3r-3 Fuet Oit #46855+OOa FuelOil *tGlat)9&0000 Mortor OilJ()()igAOo0 Aviatiofl Fuel

Unid€nliied

Otl|e. oil

ToLal P€lroleum Hydrccalbff s

C9.C36 Aliphatic Hyd.ocarbons

Sl,to€|a{e rDcolenecr338&33-2 1 -Chlotoocdecane

Semivolrtile Org|rL Corbpord! by GC

Oroanocfihrine Pe€ftides SW846 8081A

Preparod by m€thod SW846 35508

3o+oG2 ALldn

BRLBRLBRfBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRL

1 1 21tn110102

!sftspsn(susftgus/ksps/ksru^9lrsAsrgrs!dkspdksps/ks

!g/kSug/kstrg/kgps/kspsft9

l€/ksrryk9pqr9

udks!s/ksps/ks

lsftslrgkg9Sikg

52.252.252.252.252.2

52.2

52.252.252.252.2

52.252.2t0452.252252.252.2

52.2

5221040

505050505050

5050505050

50505050

5050

SW 846 82608 21^tiat47 22 4d47 7031189 ho

rCT ETPH 22-tilar-07 26-t ar-07 7031283 OS

70-1m%70-130 %7&130%70-lw%

BRL8RLBRLBRLBRLBRL

BRLBRLBRLARL

117

nEl(Smgn(gndkomgftsmg/r(gmsfts||'rsftsrwlsor9r(gmdks

25,6

25.625.6

25.625.6

10-140 yo

BRL llslkg SW8.f6 8O8lA 21-Ms,r47 26,.,'atr47 7031i71 TG

Thb labralory rcpod is not voud rrlthout on adhorizd siEnature on the covc. Ird$ .

'R€port blc Detectiofl Limit BRL= Bclow Reponine Lirnit Page 54 of 152

Page 410: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentiftcationMEFB.3sA59464-l I

Client Proiect #30t-88

Collection Date/Timel5-Mar-07 00:00

MatrixBallast

Receivedt9-Mar-07

CAS No' Analfte(s) Result Flag *RDL Dihl.bn Method Retr. Prcparcd AMItzed Bakh Ahalfst

Sehivohtile Organlc Compornds by GCOeanochlorine Pesticides SW846 80814Prepared by method SW846 3550831944€ a"BHC319€5-7 b-BHC319{6€ d_BHCsa€+e gFBHC (Lindane)5/-7+9 Chtord€ne72r5rl-€ a.4-DDD(p,p,)72-5te 4,+DDE (p,p,)s{l-?+3 4,+DOT (p,p')6O-57J Dietdrin95$98{ Endosut{En I33213{54 Endosulfun ll1031{7{ Endo,sulfanSulfate72.2O-A Endrin7t21.9H Enddn Atdehyde7F.r4{ Heptachtor724Ts Methorychtor102457-3 Heptachlor Epoxide600t++2 Toxap,llene5t0!714 €-Chlordane5586-3L7 g4htordane53494-70-5 Endrin (etone

Sarrrogale /ecolcr'esi,03ec+2 4,4-DB4ctafruorobiphenfl (54msL2+3 Decechlorobiphent4 (SoPolvc*rlorinated Biohenvls bv SW846 808?Pr6pa.ed by method SW846 3550812674-11-2 PCB 1016rri04-2F2 PCB t22l1ri41-16-5 PCB .1232

53.*21-9 PCa 124212672-29{ rcB 124811097{91 PCB t2:}411096€-5 PCB 12603732+?3-5 PCB 12621i1(x}r,{_4 PCB i268

Suarogal€ r€cor€r'esrI 03 B€, 8 +2 4, tl- D 84ct a fl uo ro b i ph en yl ( S 4m51-2+J Decochbrobiphenyt (Sr)

Semlvolrrib Org.ric Compounds by GCMS

21-Mat47 24'Mat47 703'1170 SLl

BRLBRLBRLBRLBRLBRLBRLBRL

BRLBRL

BRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRL

76127

BRL8RLBRLBRLBRLBRLBRLBRLARL

110

,.i9/Kg

Ljgftspslkg

Lrg/Kg

!gikg

USrt(S

['Ek9pg/kg

!g/kspg/Kg

pgfts

ug/(g

ug/kgpg/(g

tjgKspEks

psfts

t S/'(st'g/ks!si(g!g/Kg

1 3 . 5

13.5

r3.5

13.5

13.5

13.5

13.5

7.00

1 3 . 5

13.5

13.5

1 3 . 5

13.5

13.5

13.5

1 3 5

67.7

13.5

1 3 . 5

13,5

27.1

27.1

27.1

27.1

27_1

27_1

27_1

27_1

27.1

30'150 %30-150 %

sw846 0081A

sw846 8082

sw846 8270C

I

1

1

1

1

1

1

1

1

1

1

1

I

1

1

t

1

1

1

1

1

trg/Ks|Js/ksug/(g!9ir(gug(g!sftsps/kgpsfts

!Eks

m-l50 %m-t 50 %

S€mivdatile Orqanic Comoouods bv SW846 8270CPfepared by method SW846 3550883-32-9 AcenaphtBne20e€6{ Acenaphthyten€62513 A,r ,ine12G12-7 Anthracene1912-2+9 Afazine10+33+ Azobenzene/Diphenytdiazine9242-5 B€nzidinefl6{ti B€nzo (a) anthracene

22-Mat4f 264nar47 7031282 M ABRLBRLBRLBRLBRLBRL

BRLBRL

!sftsLj9fts!9ftg|l9/kS!€ftgpsl(g

us/kgpsftg

635

635

635

635

635

635

635

635

This lahorolory nport lr nol wlrl vithout on onahofited signaturc on the corer page.

r Reportable Detection Limit BRL = Below Reporting Limit Page 55 of 152

Page 411: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeotificatiooMTFB.3sA59464-11

Clieot Proiect #301-88

MatrixBallast

Collection Datey'Tim€I 5-Mar-07 00:00

Recoived19-Mar-07

CAS No. Anavlc(s) Rcs'/A FIas 'RI,L Dildion Mtthod Retr. Pnpdran ArraIWd Bach An4lfsl

S€mivoblile Orgadc Compoutrds by GCMS

Semivolatile Omanic Comoounds bv SW846 8270C

Prepared by metlrod SW8,l6 35508

Benzo (a) pyrene20+99-2 B€nzo(b)f,uorsnthene191-2a-2 B€nzo (g,h,i) perylene20rc8-s Benzo (k) fuorantheneffiso Benzoic acld101>51{ 8€nzy'l alcoholr11-si-r Bis(2_Ehtoroethory)methan€11r-444 Bis(2{htoroethyt)ether3963&32.9 Bis(2<hloroisop.opyl)eth€r1r7{1-7 Bis(2-€h!'lhexyl)phttEtate101'55'3 zl-Blornophenytphenyleher85!6&7 BuV benzyl phthatatje8&74-0 Carbazole5A-5G7 4-Chlooj-methylphenol16-47+ +Chlorcaniline91-5&7 2_Chlo.ooaphhalene9s-s7{ z_Chlorcphenol70ut72-3 +ChlqoFhenyl phonyl ether218-ol-9 Chrysene53-7G3 Dib€rEo (a,h) anthracene132{+9 Dib€nzoduran9t5+t l,2-Dicilorobenzene54i-73r l,3oidhlorob€nzene106-46,7 l,4-Dichtorob€rE€neel-9,r1 3,3 -Did ombenzidine120-83-2 2,+Dichlo.ophenol0.15+2 Diebytphthalate131-11n Oimeth/ phthalate105{7a ?,+Dimethylphenot€/.7+2 Di.n-butylphthalate534.E?-1 4,6-Dinitrob2-melhylphenol51-2G5 2,4-Dinftrophenoll21r{.2 2t4-Oinitrotoluen€60620-2 2,6;Dinihotolueoer 1 ru4{ Dln-octy' pHhat€te208-1.4-0 Fluoranth€n€88.747 Fluor€n€11&74-1 HeXachlorcbenzene87SF3 Herachtorobutadiene7t.1.74 Hexachlorocyclopentadien€6:t.72-1 Hexsdttorosthan€ls3-3e-s Ind€no (t,2,&od) p,fenew12e I _Mehyin@hhat€n€78-59-t lgophoame91-57€ 2-Metryhaphttlal€n€9914&7 2-M€thylphenol10c3€-4, 3,4+redhylphenol1{16-{11.59i.2G3 Naphthalenoe4-7+4 2.Niboanitine994o-2 $HiLoanllin€

BRLBRLBRL

BRLBRLBRLSRLBRI-BRI-BRI-BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRL

BRLBRL

UdkS 635

lSitq 635

t S/tS 635

|4AS G35

|ryl(g 63spdkS 635ps/ks 635

!g/ks 635

!g/kS 635

t€,kg 63s

l€/tS 635

trC^g 635

FC,IS 635pS&g 635pgftS 605

lSftS 6il5

lgkS 635

IS/kg 835

IS/19 635

US,IS 635pS/kS 635

lgks 6il5

!SI(S 635

lSftg 535pgn(g 635

llg/r(g 635

IgrS 635

FgrS ffispg/kS 635

!g/kS 63s

l,rgkS (i15

lSftS 63s

lrSftg 635pS^S 635

USfts 635pdkg 635

[r94(S 635

!g/kg 635

rgftS 635

ugftg 63s

t€,ag 635

rs/ks 635pgkS G35

ldks 635

LrSftS 6:|5

USftS 635

lglkS 635

rSikS 635psfts 635

lrgkS 635

Ihir hh*alotf .qorl b @t voltd tothost on aathotlzd stgnatarc or lhe cover pdge.

. R€portable Detection Limit BRL = B€low ReDortios Limit Page 56 of | 52

Page 412: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [d€otificationMTFFS

sA59464-11

Client Proiect #l0l-88

Collection Date/Timel5-Mar{7 00:00

MatrixBallast

Receivedl9-Mar-07

CAS No. Analrta(s) ResuL FIag Units *RDL Dilution Mcthod Rel. P4pared Anab.td Eotch Atullrl

S rivololile Organic Compo{nds by CCMS

Semivolatile Oroanic Comoounds bv SW846 B27OCPr€pared by hethod SW846 35508

lrxr-ol6 +Nitrcenitine9&9t3 Nitmbenzene8a-7t5 2-Nihophenol100{2.7 4-Nilrophenol

@-759 N-Nitrosodimethylamine

64144.7 N-Nitrcsodi_n_propylamine86-306 N-Nitrosodiphenylamin€a7{6-5 Pentachlorophenol8s:013 Ph€nanthrene10&95-2 Phenol

129-00{ Pyfene11&86.1 Fyridine120{2.1 1,2.4-Trichlorcbenzene95-9t4 2,4,STrichlorophenol8l]-0&2 2,4,GTrichlorophenol

Sl'rogate r€co!€n€s--

32t-60-8 z-Fluofobiphenyl

fi7-121 z-Fluorophenol

SW846 8270C 22-MerO7 26-Ma.'o7 7031282 MBBRLARLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

1 7

Completed

BRL

8RL

0.0090

BRL

BRL

BRL

BRL

BRL

lSftS 2540

tiSftS 635

pSftS 635

fiS/kg 2540

pS4{S 635

ps/kS 635

pS/kS 635

UEIS 635

pg/kS 635

pSI(S 635

pS/kg 635

lSftS 635

lSftg 635

pSftS 635

Ug/kS 635

30-130 %

1U110 %

30'130%

15-110 %

30-130 %

1nl10 %

1

I

1

1

1

1

I

I

1

I

I

1

1

1

1t654co Nitobenzene4s 33416542-2 ,thenol45 29171&514 Terphenyl4l4 461t8-7 2.4dTtibftmophenol U

Tor.l Metb by EPA 6000/7000 Series M€thods

71139-97{ Mercury BRL

Tot.l Mdrb by EPA 200 Serie Merhods

ARL

BRL

13.4

0.731

2 1 2

4.70

BRL

SPLP M.tdr by EPA 1312 & 6000/7000 S€ri€s Methods

SPLP Extraction

71,{0.224 Silver

7440.3&2 Ars€nic

744G3!t 3 Barium

7t40-4+9 Cadmium

Zl40{7-3 Chromium

7€9-97,6 Mercury

7439-92r Lead

262.4+? S€l€nium

1 SW646 74714 26-Mar47 26-MarO7 7031311 YP

EPA 200 7 2GMaF07 26+4ar07 7031263 LR

mg/kS 0.029s

74sr-22-4 gtver

7j!t+382 Asenic

7,r4G3+3 Barium

7i!rs4$9 Cadmium

7,uO-47-3 Chromium

713€-52-1 Lead

?824$2 Selenium

mSI(S 0-0S'1

mg/kg 1.u

fiEI(S 0.445

mg/kg 0223

mS/kS 0.445

rng/kg 0-668

mgfts 1.34

msI 0.0100

mg/l 0.0150

mg/r 0.0050

mg/l 0.0025

n€I 0.0050

rYE/| 0.000c0

nEI 0-0075

mgit 0_0150

1 SWE461312 21-Mafi7 21-Ma'.O7 1031229

1 SW8461312/60108 22-Mar07 2X-Ma..07 7031323

1 '

1 '

1 '

1 "

1 SW8461312'470A ' 231ttar07 7oX1324

1 SW8461312r'60108 " 23{,,lar{7 7031323

1 '

BD

LR

yp

LR

Thit labo.alory rcpo.t k not yolid withoat an autho.ized sign ture od ahe dteer page

' Reporhble D€tection Limit BRL = Below Reporting Limit P^Ee 57 of 152

Page 413: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample Identifr€tiooMtFB4

sA59,t6t t2

Clietrt Proiect #30t-88

Collection Date/fimels-Mar{? 00:00

MatixBallast

Receivedl9-Mar-07

CAS No. Analyta(s) Rcsalt Flzs U,,ia 'R.DL Dilnion Merlrod Ref, P|Epared A&lyzrr' Barch Anslysa

Vohdle Organic Conpouadr

Volatile Omanac ComooundsPrepar€d by method SW846 5035A Soll (low levet)76n3-l 1,1,2-Trichtorolriiuoroethane (FreoSRL67{4.1 Acoton€ BRLi07n3-1 Adylonitil€ BRL714+2 B€nzene BRL10&€6-1 Bmnbb€nz€n€ BRL7447-5 Bromorfttorcmethane BRL7?214 Blomodidtloromethsne BRL7+212 Bronbform BRL74{3-9 Brornomethafie BRL78+$3 z-Butanone {MEK) BRL10451{ n-Eutytbenz6|1€ BRI_13198{ sec.BuMb€nz€ne BRL98{6{ t€rt-ButylberEens BRL7t15{ Carbon disulfide BRL56.215 carbofl telrachloride BRL108-90-7 Chlo@benzene BRL7s{)G3 Chtoroethsne BRL67563 Chbroform BRL74-47-3 Chloiomethane 8RL9'49{ 2-Ctrlorctoluene BRL10S.4+.4 44hlolotolusle BRL96-12{ 1,2-Dibrcnoj-chtcropropano BRL12,H€-1 Dibromochlorornehane BRIr0A93{ |,2-Dibrcrnoetham (EDB} BRI-74.9t3 Dibromofiethane BRL95-s(ll 1,2{ic* o.obenzene BRL541-73-1 l.3oichtoob€nzene BRL106-4+7 1.+Eticldorot€nzene BRL7U714 Oidllotodinuordnehar|e(Freonl2)BRL753+3 l,l-Obhloroethane BRLr07-0f'2 l.2-Oichloro€thane BRL7535-,{ l,l-Dict otoothene BRL15s59-2 ci6-1,2-DkSloroefEne BRL1sE a0-5 tens- | Joichloroe$ene BRL78{7-5 |,2-Oichloroprop€ne BRL142.28.9 1,+Dicfilo{oprop6ne BRLs9+i8.7 2,2-Didrlooptop€n6 BRL56+50{ l,'l.Didiorop{op€ne BRL10061.01-5 cj6-1,3-flichlorcprop€ne BRL1061.024trar+1,3-DichloroproDene BRLioo4i.1 Efty'benzefle BRL67€&3 HexadturDbLdadien€ BRt_591-78€ ?-Hem|}ono(MBK) BRL98{2-6 lsopoptlborBene BRLg9{?{ +lsoprgplitohrene BRL1634{4-. Medtyl bt-bltyt ehef BRLloelGl +Medrt l-2+€ntanone (MIBK) BRL75s.2 ilethyl6n6 chhride ARLs1.2s3 Naphthalene BRL10316+l rtsPrcp!4bonz€ne BRL

lg/t(gw€t 4.3

ldkgw€t S7.0

Ig/kgw€t 4.3

ldkgYY€l 4.3

ldkgw€l 4.3

FdkS rv€t 4.3

lrgl(g rY€t 4.3

ldkg vret 4.3

pg/ko vY€t 8.fggil€ wet 43.5

pgrtgwst 4-3

pg/kg w€t 4-3

!g/r(g w6r 4.3

ldtg w€l 21.7

Lrdxgwet 4.3

ldkg v,,€t 4.3

lgLfl(g w€l 8.7

IgkS Yret 4.3

pSI(g N/et 8.7

|lg4q sret 4.3

pSftg u/et 4.3

pgr'kg wei 8.7pgkgwe{ 4-3

ldkS w€l 4.3

lgll(g wel 4.3

ugy'xg wet 4.3

USn(S wel 4.3

Ug/kS Yr€t 4.3

pdkg w€t 8.7

trdkS rv€t 4-3

Ug./kg w€t 4.3

IqkS vret 4.3

Ug/Xg v{et 4.3

Ug/kg wet 4.3

pdkswel 4.3

ldkswel 4,3

pgy'kg wet 1.3

lglSwet 4.3

Idlgrvel 4.3

rcl(g u/€t 4.3

|lgl(g rr€l 4.3

ldkSwol {.3

tg/i(Sbst 43.5

pg^gwet 4.3

Fdkgwet 4.3

lSftSwet 4.3

FSrkS wet 43.5

pdkSwe{ 43.5

lcjkgwot 4,3

lgrS*€t 4.3

t

1

1

1

1

1

I

1

1

I

1

t

1

1

1

1'I

1

I

I

I

I

1

1

1

1

1

1

1'I

I

1

1

I

I

I

I

t,|

1

I

I

I

1

I

I

1

I

I'|

SW 846 g2608 z4lliaroT 22l^4a[47 7031291 RU

fhis labotuloty ,eport ls ,tot valid *llhod od dnhodzzd sfunatue aa thz cowt page-

+ Repodable Detection Linir BRL = Below Reponing LiEir Pege 58 oI 152

Page 414: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMSFB-4sA59464-12

Clienl Proi€ct #301-88

Collection Date/Timel5-Mar-07 00:00

MatnxBallast

Receivcdl9-Mar-07

CrrS No. AnsWG) Fhs Unie *RDL Dilution Llahod ReI. Prcparcd Anrbzed Bakh Anaust

Volatlle Orgrnic Compounds

Volatile Oroanic ComooundsPrepared by method SW846 5035A Soit (tow tevet)1m-42-s Styren€ BRL6ilca){ 1,.1,.t,2-Tetrachtoro€th€ne BRL7$34-5 1,t,2,2-tekacNoro€thene BRL127-184 Tetradlloroethene BRL10&{63 Totuene BRL87€1-6 1,2,3.Trichlorob€nzene BRLi2$€2r 1,2,+Tdchlorobenzene BRL71-5sG |,'l,l-T.ichloroethene BRL7!rcc5 l,l ,2-TriChlo(o€thane BRL79{1{ Trichloroethene 8RL7s6$4 Trichlofonuoromethane (Freon 1l) BRL96-14-4 1.2,3-Trichloropropane BRL9553{ 1,2,4-Tdmethylbenzsne BRL108{7-8 1,3,5-Trirnethylbenzene75414 Vinylchtoridet330-2G7 m,p-Xyl€ne9t47{ Gxylene10+90'9 Tetrahydrofuran80-29-f Ethyt etherS4-OS Tefl-amytmelhyteher637-92-3 Ethyl tert-butyt €ther10&?0-3 Diisopropylether7fifr-o T€rt-Butanol / butyl atcohol129911 1,4_Dioxane

SW8!682608 22-Mat47 224l,al-07 7031291 RLJ

VOC 20-Mar-07 m-Mar-o7 7031156 BD

+grclnofluorchenzeneToiuene4S1 ,2-Dichlotuethane-d4

BRLBRLSRLBRL8RLBRL8RL8RLBRLBRLBRL

1041D4105103

Field extracted

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

114

f.ig/kg w€t 4.3

ug/kg wst 4 3

ug/kg wet 43

lg/kgwet 4.3

pg/kg wet 4.3

pgkg wel 4.3

!g/kg wet 4-3

f.ig/kg wet 4.3

Ug/kg,ret 4.3

!g,,kg wet 4.3

pg/kg wel 4-3

rrg/kg wet 4 3

lgr'kg w€t 4.3

trg/kg wet 4.3

!94(9wet 4-3

Ugr'kg wet A-7

pg/kg wet 4.3

t/gL/Kg wet 43 5

pgr'kg wet 4-3

pg/kg wel 4.3

Wkg wel 4 3

!g/kg wel 4.3

Ugr'kg wet 43-5

Ugukgwet 87.0

7L130%

70-130%

70-130 %

70-130 %

,l

1

1

1

l

I

I

1

1

1,1

1

1

1

1

1

l

1

1

1

I

1

1

1

s|rnryars2t60-404

2037-26'5

l7wo474

1868.5X7

VOC Exlraction

Etalsclcble Petmleum Hydrocarbons

Extraclable Total Petroleom Hvdrocarbons

PEpa.ed by method SW846 35508

80lE6l-9 Gasoline68476.30-2 FuelOit#26847e*1.3 Fu6l Oit #46855300'4 Fuel Oil f6im98000ql Motor oil$or(xxloo Aviatiofi Fuel

Unidentified

Other Oil

Total Petrole{]m Hydrocarbons

C9-C38 Aliphatic Hydroca.bons

SsnDgEle recoyanbs;

3386-3+2 l-Chlorooctadocane

SeDivokdle Orgenlc Compouods by cC

Oroenochlorine Pesticides SW846 8081A

Pr€pa.€d by method SW846 35508

30!xrc2 Alddn

ft€n(g

mgfts

mq/fS

mS/kS

mS/kS

nrSlkS

m!/Kg

msftg

rng/kS

mg/(g

27.O

27_O

27_O

27.0

27 _0

27.i

27.O

27.0

27.0

27.O

+CT ETPH 22-Ma(O7 26-MarO7 fO312A3 DS

BRL

10-140%

ug/ks SW846 80a1A 21-Met47 26]lnar07 7031171 TG

Thit laborutory relgd h not vzbd NAhoat aa eulho zen ngnat re oE ahe cover poge.

r Reportable Detection Limit BRL = Below Reponing Limit Page 59 of 152

Page 415: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ ldentificrtiooMtFB.4sA'59464-t2

Clieot Prciect #l0rt8

Collectiotr Dat€/Timel5-Mar47 00:00

MacixBallast

Received19-Mar47

CAA No. Arzlye(s) Fhg A a *RDL Dilatioa L{ahod Retr. Prepared Aaallzzd Bdth Aa4lfsl

S€mivolatile OrSrnk Compoundr hy GC

Oroanochlo,ine Pesticides SW846 6081APrepared by mehod SW846 355083rgs4{ 8-BHC319-e5-7 b-BHC319-06-€ d-BHC58-89-9 gF.BHC(Lindan€)57-r+9 Chlordarls1'2 '54{ 4,4.oDD (p,p,)72-5re 4,4ODE (p,p')50.2+3 a,a{DT (p,pl60-57.1 Dieldrin9599&A En(bsulbn I3321$68F9 Endosulbn ll1031{7{ EndosulbnSulfate72-2oi Endrin742r-93-4 Endrin Atdehyde764+A H€ptacftlor724U5 ti,l€tloxyrfilor1024€7-! Heptacldof Epoxide80Ol++2 ToGphone5103-71-9 a-Chlo(dane556G3+7 g_Chb.dane5,3491-7Os Endrin Kebno

Srrroga(e /Bcown€sj103ts64+2 4,fieod^fluorobkhenyl (Sr)m5L2+3 Decechbtubiphenbt(Sr)Pohrdtlorlnaled Biohenvls bv SW846 8082Preparod by metfbd SW846 355081267+11-2 PCB 10'61110+n-2 PCB 122111141-16-s PCB ' |232

53{n9-21.s PcB t24212672-294 PCB t24811@7€e-1 PCB.t254r10s6{2.5 PC8 12603f32+zt-5 PCg 12621fl0{}14-4 PC8 1268

Suzwab recosngsjI W64+2 41484ctafl uorobiphenyt ( 34mst-21-3 tu@chlotobi@ (Sr)

Serrlvolrtile Orgrrlc Compo{n& by GCMS

21-M3r{7 26-fvlr{7 7031171 TGBRLBRLBRL

BRLBRLBRLBRL8RLBRL

BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

118

BRL8RLBRLBRLBRLBRLBRLBRLBRL

75115

BRLBRLBRLBRLARLBRLBRLBRL

pc/t9

t'gt9pry*spsrl9

!gr(9FgftSflgftSlgftspsn€l,siksE/TII

usagpsftspgtk9pdkg

rsn(gU€ftS!s/ksFs,kst gikg

us^g

t3.3t3.313.3

66.7

13.37,006.9013.313.3t3.3

13.3

13.3

13 .3r 3.313.3

ugrs!gftspgfts

wikspslks

l€/k9us/ksusftsPgrs

2A-7

m.726.7

26.7

sltt& %w150 %

sw846 mStA

S111A46 6062 21-Mat47 z4.ll,.el.Ol 7 031 1 70 SM

30-1fl %

3Gtffi %

Semit/olatile Orqanic Comoounds by SW846 g27OC

Prepared by me0Dd SW846 35508

4332-9 Acen6phtlEne20&96{ Acenaphthyl€ne62'5}3 Anllh€14112.7 Anthtec€n€1912'24-9 At?zine10+3:1.3 Azobeoz€noDiphenyldiazineq{7-5 B€fizidine56'5+3 B€nzo (a) anthraoer€

22{tr,147 25-Mat47 7031 282 M.Brsil(gusftspsftsps/kspdksps,/ks

IgksugJks

670670670670670670670

sw846 8270C

Ihis lahnhrf npoft ls aot wlid firthotd an atltorhd stg,B,t E o,r tfu @v.r page.

' Reportable DetectioE Limh BRL = Betow Reporting LirEir Page 60 of 152

Page 416: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiopII,{EFB.4sAs9464-12

Client Proiect #l 0 l - 88

Collection Date/Time15-Mar-07 00:00

MakixBallast

Receivedl9-Mar-ll7

CAS No. At'!'bta(s) Result FI"C Unit *RDL Dilaiott M4hod nctr Prcpred Anaryzc'| Balch Analrrt

Senivolstile Orgrric Compounds by CCMS

Semivolatile Orqanic Compounds bv SW846 8270C

Prepared by method SW846 35508

5032-8 Benzo (a) pyrene

i'ot$-2 Benzo (b) lluoranUrene191.24-2 Benzo (9,h,i) peryt€ne

a)7{8.9 Benzo (k) fuoranth€ne6545-0 B€rEoic acidl0o-51€ Benzylalcohol111-91r Bis(2-chlorcethory)m€thane11r-14.1 Bis(2-chloroethyl)ed1€r4963&32.9 Bis(z-chloroisopropyl)€lher11741-7 Bis{2-ethylhexyt)phthatate

101.54F3 4-Bromophenylphenytether

65-68-7 But/benrylphthatate8e7,L8 Catbazole5!F5G7 4-Chloro.3-methylph€notlrxi-47{ 4-Chtofoaniline91-5&7 2-Chloronaphthalene9+s7-B 2-Chtofophenol70osF72-3 44hlorophenyt phenyl ether210{14 Chrysene5!7G3 Dibenzo (a,h) anthracene13244-9 Dibenzofuran!F{e1 t,Z-Dichlorobenzene541-73.1 1,3-Dichlorobenzene1rxl..1€-7 1,4-Dichlorobenzene914+1 3,3--Dichlorotenzidine120-E3-2 2,4-Dichlorophenol84-66.2 Di€thytPhthalate131-i1-3 Dimethytphthataler0f|67{ 2,4.Dimeth},lphenolw7+2 Di-n-butylphlhatale53+52-1 4,6-Oinitro-2-methylphenol

51-28-5 2,4-Dinitroph€noli21-14+ 2,+Dinitrotoluene606-20{ z,$Dinitotolu€ne11744{ O-n{ctylph0ratate206-4-0 Fluoranthene

8&7+7 Fluorene

11&74-1 Hexachlofob€nzene

87{&3 H€xadtlorobutadiene77474 Hexachlorocfclopentadiene

67-12-1 Hexadlloroethene19139-5 lrdeno (1.2,3-cd) pyEne

9Sr2{ t-Methytnaphthalene78.5$1 lsophorone91.574 2-Methytnaphthalene95-1+? 2+llethylphenol

10&394, 3,4-Methylphenol10d44-591-413 Naphthatene&144 2-Nihoaniline

99-11+2 3-Niroaniline

BRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLSRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI.BRL

BRLBRLBRLARLARLBRLBRLBRLBRLBRLSRL

BRLBRLBRLBRL

BRLBRLBRL

tig/kS 670

lSftS 670

USI<S 670

liS/kg 670

!g/tS 670

!g/kg 670

pS/kS 670

Pg/kg 670

pgrkg 670

!g/.KS 670

lsftg 670

trS/kS 670

UgftS 670

Hg/kg 670

pgftS B7O

pSftg 670

rcftS 670

US/kS 670

pg/kS 670

lgr'kg 670

uSrkS 670

pS/kg 670

Ugn(S 670

!gI(S 670

!S/kg 670

pgftg 670

pg/tS 670

!S/kS 670

UgkS 670

lgftS 670

!g/kg 670

pgeS 670

UgftS 670

ISAS 670

pSnq 670

ySn<g 670

lqkg 670

!SI(9 670

pg/xS 670

tiS/kS 670

pg/kS 670

!g/kS 670

lsftg 670

!g/kg 670

pSftg 670

USftS 670

lSftS 670

ugftg

!sftsrc/ks

670670670

SW846 8270C 22-Mal-O7 25-MaF07 7031282 M.g

I

1

1

This hbotutory Epo.. iyut valid vithout a.t asthoriad s,g$aturc on the cover paEe

' R€portable Detection Umit BRt- = Below Reporting Limit Page 6l of 152

Page 417: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldrptificationM8FB.4sAs94o+"12

Ctieot Prciect #301-E8

Coll€ction Date/Timel5-Mar-07 00100

Matrl(Ballast

R€ceived19-Mar-O7

CAS No. Ana+t4s) FI4g Ania *RDL Dilaion Meahod Retr. Preryred Aaalwd Bdtch fuulfst

SemhDhdle Olgrtric Compoundr by ftMS

Semivolatile Ofqanic Comoounds bv SW846 8270C

Prepared by Elsthod SW846 35508

10G01{ +Nitoaniline9E{+3 Nitaobenzene88-7+5 2.Nitophenol10G02-7 4-Nilrcphenol62-T+9 N-l$trosodin€thyiamine@1{4-7 N-Mtro$odi-n-propylamine€6-30{ N-Nitosodiphenylemine87{G5 Pentachbophenole5{1{ Phenanthen€10S45-2 Phenol129{0{ Pyrene11G86-1 Pyridinei2{}€e-l 1,2,+Trictlorobenzen€95e5-4 2,4,$Tri:torophenol8a{e2 2,4,Gldchlorophenol

Srr.rDgatg /eaoveabs;32le-g 2-Huorobiphenyl367-12.{' z-Fluorophenol416ssa4 Mrcbnzends416542-2 Phenol4s,7 | e-514 ferphettyl-dl4| | 8.794 2,4,6Ttibronophenol

1 Sw846 6270c 724'/.3r47 ?s.l,a'{7 7031282 M.S

1 '

I '

1 '

I '

l '

I '

t "

I '

1 '

1 '

1 ''1 '

1 "

1 '

BRLBRLBRLBRLgRL

BRI-BRLBRLBRLBRLBRLBRLBRLBRLBRL

3!t

31a4221

BRL

BRL

11.4

o.775

5.95

BRL

BRL

BRL

BRL

BRL

lrgrtS 2660

t4/k9 670

Ig,tg 670

FS/tg 2680pCftS 670plt/kg 670

PgAg 670

!g/Xg 670

!9/t9 670

!S/kS 670

lSftS 670pgftS 670

trgftS 670

lsftS 670

!S/kS 670

s0-130 %t &110 %30-130 %15.110%30-130 %15.110 %

Totrl Metrb by EPA 6lXXy7000 S€.ier Mclhods

743+97{ Mercury BRL

Ioral Metrb by 8PA 200 S€ries M€tlodr

mS/k9 1 SWe,$ 7471A 26-MatA7 26-Mar47 700l3ll YP

74{0-223 Silv€r

zr.r0-3&2 Arcenic

11403+3 Baaium

7440-419 Cadmium

7440.17.3 Chromium

7439€2-1 Lead

2824+2 Selenium

SPLP Metib by f,PA l3l2 & 600M000 Serl6 Mcthod!

SPLP Extractim Completed

74r{t 22.1 Situ€r BRL

7a40-3&2 AF€nic 8RL

714G3+3 Badum 0.0072

7440-4$9 Cadmium BRL

Z!1047.3 Chromium

7'89.97€ M€rcUry

7€S92-1 Lead

77€2-{S2 Selenlum

nE/kS 0.969

mS/kS 1.45

mgikg 0.4€,r

mSftg 0242

ntSlt(S 0.4€4

ndkS 0.726

nE/tg 1.45

mdl 0.0100

mdr 0.0150

n€n 0.0050

nEn 0.m25

mgn 0.m50

msI 0.00040

me,l 0.0015

mdt 0_0150

EPA 200.7 2&Mer47 2dvlar.07 7031263 LR

1 SW846'f312 21-Mat47 21-$ar47 703122S BO

1 SW8.16 f312l60108 2-Met47 2}uat47 7031323 LR' l '

' I '

1 '

t '

1 SvrrS,ftt 1312J7470A ' 234e147 7(n1324 W

1 SV\446 1312r'80104 " 23-Merry 7061323 LR' t '

Thie labtulorf EForl b ,ut eaad withod tn aulhodzed signaturc o8 dta corer pqge ,

* Re?trtable Detectioo Limi! BRL = Betow Reporring Linir Page 62 of 152

Page 418: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8FB.5sA5946,t- l3

Client Proiect #l0l-88

I\,IatrixBallait

Rcceivedl9-Mar-07

Collectiop Date/Timel5-Mar-07 00:00

CAS No, Analfte(s) Flog Uni6 *RDL Dilutiarl Method Re/. Prcpared Analf.ed Bqlch Analj-st

Vohtile Orgrnic Cohpounds

Voladle Oroanic ComooundsP.epared by metlDd SW846 50354 Soit (tow tevet)7e-111 1,1,z-Trichlorohiffuoroethan€ (FreoERLa7$+1 Ac€tone SRL107.13-1 Acrylonitdte BRL7143-2 Benzene BRL106-86-1 Brornobenzen€ 8RL74-97-5 Bronrca$loromethane BRL75-274 Bromodichtoromehane gRL

7r2r2 Brcmoform 8RL74-€&9 BroRomethafie BRL7&93-3 2-Butanone (MEK) BRL10a.51{ rFButylbenzene BRLt35-98€ s€c-Butylbenzene BRLs€{6-6 tiert€utytb€nzene BRL75-t5-0 C€rbon disulfido BRL56.23-5 Carbon tetachloride BRL10&9$7 Chlorobenzene BRL75{0-3 chlooelhane BRL67{6.3 Chloroform BRL74{7-3 Chloromethane BRL95-49{ 2_Chlorototuene BRLi0€-43-1 4-Chlorotoluene 8RL96.t23 1,2-Dibromo-3-chloropropane ARL12,14+1 Dibromo€hloromethane BRL1693-1 t,2-Dibmmoetnne (EDB) BRL74-9'-3 Dibromomethane BRL9s-5G1 l,2-Dichloaobenzene BRLEt41.73-1 1,3_Dichlofobenzene BRLlofi-r6-7 1,+Dichtorobenzen€ BRL7+7l.8 Dichtofodiiuoromethan€ (Freonl2)BRL7t3.4-3 1,l-Dichloroethane BRLroruc2 l.2-Drchtoroethane BRL75-35-4 l.1-Drchtorcethene BRL15e592 cis-1,2-Drchtoroethene BRL15G€0-5 taans.1,2-Djchtorcethene BRL7847-s l,2oichloropropane BRL142-28-9 l,3.Dichtoropropane BRL59420-7 2,2-Dichtoropropane BRL563{€t 'l,1-Dchlo.oprcpene BRL10001{1-5 cis-1,3-Dichlorogopene BRL10061.02{trans-1,3-Dichloropropen€ ARLrqo-{r-a Ethylbenzene aRL87€+3 Hexachlo.obutadieoe BRL5€1-70{ z-Hexanon€ (MBK) BRL9842{ lsopaopylbenzene BRL9947{ +lsopmpyltolu€ne BRL16o4{q Methyllert-buv etler BRL10&10.1 +Methyt.2-pentranone{M|BK) BRL75{$2 Methytene chlodde BRL9r.20'3 Naphthalen€ BRL103{5-l rFPropyhenz€n€ BR.L

SW 846 82608 22-Mat47 22-Maro7 7031291 RLJ!g/kg w€t 4.4

lgr'kg wet 8€.8

!g/kg wet 4.4

l4/kg wet 4-4

pgr'kg wel 4.4

lgr'kg wet 4.4

pg/kg lv€t 4A

IgL/kg wet 4.4

rc/kg wet 8-S

lg/kgwel 44.4

ljg/kg wel 4.4

pgn(g wel 1.4

Pgftg wet 4.4

pg/kg \Net 22_2

pg/Kg wet 4 4

pg/kg wel 4.4

lgr'kg wet 8.9

t gL/kg wel 4.4

ligrkg w€t 8.9

!g/tg w€t 4.4

!g/kg wet 4.4

tigL/kg wet 8.9

rc/kg wet 4-4

pg/kg wel 4.4

p€y'kq wer 4.4

pg/kg wel 44ggL/kg wel 4.4

ggrkgwet 4.4

lgfl(gw€t 8-9

!g/kg w€t 4.4

!g/kg \dct 4 4

pg/kg wet 4-4

t4lkg wet 4.4

!g/kg wet 4.4

Fg/kg wet 4-4

tjgikg wel 4.4

Pg/kg wel 4.4

lJg (g wet 4.4

FdkSwet 4.4

!g/kg lv€t 4.4

!g/kg Yret 4.4

!S/kS wet 4-1

Ig/kg wet 44 4

pg/kg $/el 4_4

lSlgwel 44

lig/kg wel 4.4

lg/kgwet 44.4

lgL/kg wet 44.4

p!y'kg wel 4.4

lgr'kg wet 4.4

Thh tabonlory Epotl is ^ol vlu vifioat a^ attltorlze.l sigttattre oa the coyer page.

i Reporbble D€tection Limit BRL = B€low ReForting Limi( Page 63 of 152

Page 419: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ld.ntificatiotrM8FF5

sA5%64-13

Clieqt Proiect #301 - t8

MatrixBallast

R€ceivedt9-Mar-07

Collectioo Date/Tim€I 5-Mar{7 00:00

CAS No. A,.alrta(s) FI4C U/'i6 *RDL Dil"tion MdMRef, tuaparcd Analwn Edch ArElFt

rc'oa2-s styr€ne63S20-6 1,1,t,z-Tetachloroethane79-u-5 1,1,2,2-Tetractloroethane127-18-4 Tet€chloroefrcno10&8&3 Toluen€87€1S t,z,}Tridorobenz€ne12O-82-l t ,2 ,+f idhtorobergone7l-5:"6 1,1,l-Trichtoroethane79{0-5 1,1,2-Tfichtoroethane79{l{ Trichloro€thene

Volatite Orgrdc Compoutrr|s

Volatile Omanic ComooundsPrepa.ed by melhod SW845 5035A Solt (tow tevet)

BRI-BRL8RLBRLBRLBRLBRLBRLBRLBRL

75-691 Tricflo.ofruoromettrane (Freon 1l) BRL96,14-4 1,2.&Trichto.oprop€ne9563-6 1,2,+Trimethylb€nzene10€.67{ |,3,s-Trimethylb€nzene75{1-4 Vin, chhtrid€133(}2F7 m,p-Xylen€9547{ exylefis10999-9 Tetrahyalrofuaan60-29-7 Ethyl ether9o4jt€ Tert-amyl medly' ether637.923 Ehyltert+utylethor10&m-3 Diisopropylether75{5}0 Tert-Butanot / butyt alcohol12+91-1 1,+Dioxan€

Sl//rDgale rBcown€s:460404 +E*omofluofotEnzenem37-26.5 fdluene4S1 7 0@-o/ 4 1, 2-Dlchlo@ethene-d4ftta-s,7 Dbrcnofluorcnethane

VOC Exlraction

E tlrclsble PeEoleum Ilydrocirbons

Exuaclable Total Petroleun FMrocaftonsP.epared by rnelhod SW846 355088{xt6{1-9 Gasoline6847e3G2 Fuel Oil #26847S3r-3 Fuet oil #46S55!004 Fu€l Oil #6[rq]800000 Motof oilJoolaxxloo Aviation Fuel

UnidentifiedOth€r OilTotial P€hs m HydrocarbonsC€-C36 Atiphalic Hydrocarbons

Ssnpgat€ recoyelrbs:33aa)il2 1 -Chloroodad€cene

Scmivoleaile Orgrtric Compounds by CCOroaoochlorin€ P€s cktes SW846 BOAIAPrsparEd by mehod SW846 3550830$oG2 Aldrin

Sw 8,f6 8460s 22-Mar47 22-ltar47 7m1291 RLJ

voc 2GMar{7 20jl,!ar-{7 7031156 BO

+CTETPH 22-$al-O7 4n3tr4f 7031283 DS

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI

106105110102

Field ext-acted

pg&gw€l 4.4

pgn(gwet 4.4

l.|grl€ wel 4.4

pgrkg wel 4.4

irgr'kg wet 4.4

ldkgw€l 4.4

lgtkg wel 4.4

lgr'kg R€t 1.4

ldkgwet 4.4

ldkg rv€t 4.4

ldlSw€t 4.4

ldkg rv6t 4.4

us^gYJet 4.4

ug/kq rv€t 4.4

udkgY€t 4.1

US/kS wet 89

!S/kS wet 4.4

IdkSwet 44.4

f.rdkS w€t 4.4

pdkSwst 4-4

|,g/kg vret 4.4

l4lk9 w€lt 4.4

Igilqwd 44.4

rcikg wel 88.8

7G130%

70-130 %

70-tu %

70-tm %

mgtg 25.6

n€/kg 25.6

no/kg 25.6

rfig/ks 25.6

nE/kS 25.6

dtS/kS 25.6

mdkg 25.6

mS/tS 25.6

mS/kS 25.6

mSftS 25.6

40-1'lO %

1I

1

1

I

I

I

I

I

I

I

I

1

1

1

1

1

1

I,|

1

1,]

1

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

1 1 1

|lsfts Sw845 8O81A 21-Mat47 -Mat47 7ul117l TG

Thb labodort .eport is aal eolu waltoul zd ruthoiei Eigdstarc on tfu ct ver psge .

' R€porbble Det€ction Limit BRL = Below Reportine Limir Page 64 of 152

Page 420: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SarEple ldentificationMSFB-5s459464,13

Client Proiect #301-88

CoLlection Date/Timel5'Mar'07 00:00

MatrixBallast

Receivedl9-Mar-o7

CrlS No. Analtu(s) Fl"s *RDL Dilaiod Method Rel. Prcpued Anabzed Balch Anabst

SemivoLdle Orgsnic Colnpornds by cCOroanochlorine Pesticides SW846 8081APrepared by method SW846 3550831s&16 a-8HC31s8t7 b-BHC3te{6{ d-BHCsa{se g-BHC (Lindane)5/-7rr-9 Chlordane72-s44 4,4-DDD (p,p.)72-5+e 4,+DDE (p,p.)50-2s3 4,4DDT (p,p)EGt-1 Dleldrins5+s8{ Endosulfian I332i3-65.9 Endosulbn tlt03r.o7{ Endosullan sutfate

tsndnn7a2143-a EndrinAldehyde76444 Heptachlor7243-5 Metfrxychlori02+57-3 Heptachlor Epoxicle6001-3+2 Tou€phene5103J1-9 +Chlordane5566-34-7 g_Chlordane5s491L70-5 Endrin lGlone

sl/rogtate rBcoveaes:t 038€.8+2 1, 4ag-Oebnuorcbipt@nyl (Som5r-2a,3 Decachbrcbiphenyt (54Polvchb.inated Biohenvts bv SW846 8082Prepared by rhelhod SW846 3550812€7+11.2 PC8 10i61110+m-2 PCB 12211r141-ra€ PCB 12325X46+21-9 PCB 124212An-E$ PCg 1249r1097.6e.1 PCB 12541109€-82.5 PCB 1260T32+n5 PCg 1262111OGr44 PCB l?68

Sunogate r€cor€resr1 038d.8+ 2 4, I -D goc t a fl uoto b iphe nyl ( S t)e54a4 Decachbtobiphenyt (Sr)

Smrivoladle Or8rntc Compounds by GCMS

BRLBRL8RLBRL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLSRLBRLBRL8RL

69137

BRLBRLBRLBRLBRLBRLBRL8RLBRL

75110

BRLBRLBRL8RLBRL8RLBRLBRL

!g/kS

!S/',(S

!g/kg

Ljsfts

ug/ksus/Ks|'|sflqtlsfts

wikgug/r(g!g/tsusrkslr9/lglrgfts!siks!s/kg!g/kgtJg/l(g

Ljsftg

!sfts

|lg/ks

13.9

13.9

13.9

1 3 I

69.7

13.9

13_S

r3.s

7.00' t3.9

13.9

13.9

13.9

13.9

13.S

13.9

13.9

6 9 7

1 3 9

1 3 I

13_S

3t>150 %

30-150./.

sw846 8081A

sw846 8082

I

I

1

I

1

1

1

1

1

1

I

I

1

1

I

I

I

1

1

1

1

21 -Mat41 26-MaFO7 703117 1

psilspglxg

!sikspgKgpEks

!g',xs

Psn(sus/kspsftg

2 7 9

2 7 9

27.9

27.9

27.9

27.9

27.9

27.9

27.9

21-Ma(47 24-Mat4r 7031170 SM

30-150 %30-150 %

Semi\,/olatle Oroanic Communds bv SW846 8270CPrcpared by method SW846 35bOB

83.32-9 Acenaphthene20&9G8 Acensphthylene{12'5}3 Aniline

12012.7 Anthrdcene191?-249 Alrazine103-333 Azob€nzene/Diphenyidi€zthe92{7€ Benzidinesa5s3 BerEo(a)anthracene

22-Mal-07 25^nat47 7031282 M.Bps/ksps/ks

ug/ksl'|sftgti9/kS

Fg4(g

FSikg

lig/kS

635 1

635 1

txls 'l

635 1

635 r

635 1

635 I

635 1

sw846 8270C

This bboralory Epod is ^ot rolkl x'ithoaa en.uthoized sigratarc od lhe cowr page

' Reportable Detection Limit BRL = Below Reporting Limit Page 65 of 152

Page 421: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdetrtificationMtFB.5SA59il6l-ll

Client Proiect #301-88

MatrixBallast

Coll€ctiop Dal€/Timel5-Mar47 00:00

Rec€ivedl9-Nla.-07

CAS No. Analtte(s) FIq UniE IRDL Diluiot' Method RrJ, Prcpared Aaalyzen Bdch Atttltsl

Seorlvol ih Orguic Compourds by GCMS

Semivolalile Orqanic Compoonds bv SW846 8270CPreparod by method SWS]{6 355085{l"32-a B€nzo (a) pyrone20S+2 B€nzo (b) ffuora.drd€19r-24-2 Benzo (g,h,i)peryleoe207{8-9 8€fEo (k) fuorandlen€

Eenzoic acid10G51-6 Eonzylalcohol111-91r Bis(2-drloncebory)medEne111-44-4 Bis(2drtolitetryt)eher39€?&32-9 Bis(2-ct{ooisopropyl)eher117€1-7 Bis{2+hylheryl)phthalatel0l-55-3 +grcnrophenyl phenyl oher0$€&7 Butylb€nrylphthalate8d7rt{ Ca6azol65q5&7 +Chloo-3-m€thy'phenol106-47{ +Chloroaniline9i.5&7 2-Chloronaphthalene9$574 2-C.hbrophenol7005.72'3 +Chbrophenyl phenyt ether21&01-9 Chrysene517&3 Oib€nzo (e,h) anhracene1 32d{ OibenzoJuran95-5G1 1,2-flichtomberEene541-F1 1,3-OlcHomb€nzene106...6-7 1,4-Obl]ldob€nz€ne91-94-1 3,3'Oict{oaobenzidine120€3-2 2,+Dichloropheioli446-2 Diethylphthatate13111-3 Dimethyl phfl1alate105$7,9 2,4.Djmelhytphenolu-7+2 Di-n-buty'phthetaE$4-5ar 4,6-Dinit'q2-m€thylphenol51.2a.5 2,4-Dinibophonol'r2r-1+2 2,+Dir.litotoluefle60e2G2 2,6-Dinitotoluenei17€4{ D-n-odylphdrahte20H4{' Ffuorenhene86?!7 Fluoren€11&74-i HexsOhlororrelp€n€876a.3 H€xadorobutadienen474 Hexacfilorocydopentradiene67.72.1 Hex€dtloroethanols939r5 Indeno (1.2,3-cd) pyeoe*124 l-Lle0tyln€phtf|alene7849-1 lsophorwt€91-574 2.MetrytiaFht\aler€9s-1&7 2.Methylptl€nol10e39-a, 3.4-MethMphenolt06'44-591-2G3 t{aphthal€ne8€-71-a z-Nitroanllln€

$ttiho€nilino

BRLBRLBRL

BRLBRLBRLBRL8RLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL

BRL

BRLBRLBRL

ugftsIrsftst CikS

!gr(sttgul(gpsiksps/r9

!9aSggftsp9lts

t g/ks

t c/ks!gkspdks

!gftgtrdtsrdkspsrqtpg4(g

rg/t(spdkspgks

!dks|lgn(ST€]KS|rsfl(gusrks

rcrkspgrkg

lrS/kS!g/Kg|lsftslsftsps/ks

rurk9t4/ks!g/kspg/ks

tlgr|(guofto

ugfts

9S*9||s*st sftstt$rkspdks

t g/kS

flgr(s|,9r(Sps,ks

635

635

635

635

635

635

635

635

635

635

835

635

635

635

635

635

635

635

635

435

6it5

635

635

635

635

635

635

(i)5

635

635

6i15

SwE46 8270c 22+'!,.at47 25 nar47 7031282 M.B

ThIj l4borsb.y tepora is nd val l x,ithozr sn oaahoried sigrrauE on the awr page.

' R€Dart$tc Det€ction Limir BRL: Below Reponing Limh Fage 65 of 152

Page 422: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMtFB-5

sA594g-13

Client Proi€ct #301 .68

Collection Date/Timel5-Mar-07 00:00

MatrixBallast

Received

l9-Mar-07

CAS No. Andlta(s) ResuIl FluS Anits TRDL Itethod Ref,, Prcpued Ana,.ed Bolch AMIjst

Semivolrdle Orgrnic Compounrls by CCMS

Sernivolatile Orqanic Comoounds bv SW846 8270C

Prepared by method SW846 35508100{1$ 4-Nitroaniline9S-9+3 Nitrobenz€ne8&7+5 2-Nitrophenolic+02-7 4-Nitrophenol02-7tg N-Nitrosodimethylamine621{4-7 N-Nitrosodi-n-propytamine6&3G6 N-Nitrosodiphenytamine87{G5 Pentad orophenolas{l+ Phenanthrene10&9+2 Phenol129{0{ Pyrenet1016-1 Pyridine12G€2r 1,2,+Trichlorobenzene9&95-.1 2,4.+Trichlorophenol8846.2 2,4,STrichlorophenol

Sunog8[e r*ovedes:32140-8 2-Fluorobiphenyl36r-t21 2-Fluorophenol41e5{44 Nittobenzene45416!,62-2 Phenol4sl7le5t4 Teryhenyf4l4ll8-79-O 2,1,6-Tib.omophond

Toarl M€trb by EPA 60{0/7000 S€ries M€thods

BRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

421 936

4527

8RL

BRL

8RL

1 2 . 7

0.565

3 1 0

3 8 9

BRL

Coftpleted

BRL

BRL

0.0073

BRL

BRL

BRL

BRL

BRL

!g/kg 2540

!g/kg 635

LiSftg 635

Uglkg. 2540

!g/kg 635

u9/k9 635

pgkS 635

lSrt(g 635

pg/kg 635

pS/kS 635

pS/kS 635

!S/kg 635

ugftg 635

LiS/kg 635

pSftS 635

n-130%

15-110 %

30-130 %

1Ul10 0A

30-130 %

15- l10 %

mS/kg 0.02SG

mg/kS 0-958

mS/kS 1-U

mg/kg 0479

mSftS 0.240

nEftS 0.479

mg/kg 0 719

mS/kS 1.44

mg/l 0 0100

mg/l 0 0150

mg/l 0.0050

mg/r 0.0025

rngl 0.0050

mgl 0.00040

n€/l 0.0075

mgn 0.0150

1 SW8467471A 26-Mari7 26-lvlar{7 7031311

EPA 200 7 m-Mar-o7 26-Mar-07 7031263

SW846 8270C 22-Mar07 25-Mat Ol 7031282 l\1 B

BD

LR

743S€7€ Mercury

Toarl Met8k by f,PA 200 Seri€s Methods

74,1+22-4 Sifuer

7'|?{}-36-? Ar€€nic

74@3e3 garium

7140419 Cadmium

ziul.47-3 Chromiuft

3S-m-1 Lead

zec49-2 selenium

LR

SPLP Mctd3 by EPA l3l2 & 6000t000 Serie! M€thods

SPLP Extraction

7,t40-22-4 Sifuer

7440-3&2 ArEenic

Zl40-39-3 Barium

7r!40-4$9 Cadmium

71t{o-a7,3 Chrcmium

213997€ Mercury

7,l:|9-g2-1 Lead

77824$? S€leniurn

1 SW8461312 21-Mar{7 21-Mar47 7031223

I SW8461312/6O108 22-MaA7 23-Mat47 7031323

1 "

1 "

1 "

1 '

1 SW8.1613'f 2t470A ' z}Ma.-OT 7031324

1 SW8461312/60108 ' 23-MarO7 7031323

1 ' ,

vpLR

Thb kborstory nporl k rol volil wilhout on Quthodzed sigfltarc on the are? page.

' ReFortabl€ Dctection Limit BRL = Below Reporting Linit Page 57 of I52

Page 423: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiopMSFB{SA59?t6l- l4

Client Proiect #301-88

Mat.ixBallast

Coll€ction Date/Tim€I 5-Ma.-,07 m:00

Receivedl9-Mar-07

CAS No. Anutfie(s) Resulr Fl4S U,,i6 .nDL Dilaion Mahnd Rctr. P,tptEd A'u4aed Bdch Aaalyst

Volraile Oryr c Compoundt

Volatile Oroanic ComooundsP.epared by m€thod SW846 5O35A Soil (tow tevet)76-111 1,1,2-Trid orotrifluorcethan€ (FreoBRL8744t Acelme BRL107-13'1 Acrylonibile BRL7143-2 Benz€ne BRL108{&.1 gromobenzene BRL74-97.5 BronodllorometfEne BRL75-274 Brornodid oromethane ARL75-212 grornotorm BRL74€3-9 Bromomothane BRL7a€13 2-&rtanone (MEK) BRL1lM-513 n-Bulybenzene 8RL13+s{ sec-Butylb€nzene BRL98{6€ tert-Butylb€flzene BRL75-15-0 Carbon disutfd€ BRLf!e2+5 Carbon tofachtoride BRL10&90-7 Chlotobenzene BRL?:.{G3 Chloro€thane BRL6766-3 Chtoroform BRl-74€7-3 Chloronethane BRL95-49€ 2-Chloroduene BRL106-434 +Chlorotduene BRL9sl2{ 1,2-Dibromo-}dtloropropan€ BRLi2a-4€n Dibrormchloromethane BRLr0+$r t,2.DibfEmo€h6ne (EDB) BRL74-95-3 DibrcmonEthane BRL95'5Gl i,z-Dichbrobenzene BRL541-73-1 l,$Dichlorobenzene BRL10846-7 l,4-Dichlorobenzene BRL7s-71-a Dichlorodinuoromefiane(Fl€onl2)BRf75-3+3 |,1-Dldrloroeihane BRL107{6-2 |,2-Dichloroehane 8RL7fis-4 Ll-Dichloro€{hene 8RLi5e5o-2 ois-1,2-Olchloro€thene BRL156-60-5 t€ns-t,2.Oichloro€thene BRL7a+7€ 1,2-DichlorEpropane BRL11?-28.9 1,lDbHorcprcpene BRLss+20-7 2,2-Dhhlo{Dprop6ne BRL56}584 l,l-Dicf oroprop€ne BRLi00€1{l'5 cis-'1,3-Dichloropropene BRL1006r{2€t"ns.l,3.Dlcfiloropopene BRL1m-41-{ EgylberEene BRL€7$&3 Hexad orobutadiene 8RL59t7+6 2-Hexamn€ (MBK) 8Rf90{2{ lsopmpylbonzene BRL

4-lsopropylblueno BRL163.{4-a M€thylta.t-bug'lethe. BRLt0s10r +Methyl2+entanone(M|BK) BRL75.0$2 Mehyten€ chtoride BRL91.20-3 Nephthalenet03-65.1 n-Propyltreflzene

Idkgw€l 42

tdkg lr€l E4.6

!S/kg vr6t 4.2

t S/kS vret 4.2pgftS t€t 4.2

Ug/qwet 4.2

Fg/kg wet 4.2pCASwel 4.2pdkg rrsl 6.5pgy'kg wet 42.3

lgrkg wel 4 2

Ugl(S lr€l 4.2

USI(Swet 4.2

ldkS wet 21.2pg/kg Y/€t 4.2

t dko w€t 4.2

Idko wet 8.sygyto wet 42pdtgwel S-5

ldkgwer 4.2

lgy'tg wel 4.2

Ugkgwel 8.5

USI(9 Yrel 4.2

US/kS wet 4.2

FdrS Yret 4.2pg/kg wet 4.2

Ig/kg wet 4.2

Igkg u/et 4.2

ugy'kg wet 8-5pgxgwel 4_2

Udlgwer 4_2pgn€ w6l 1-2

Ugftgwet 4.2

lgxgw€l 42

lg/kgw€l 4.2

frgul(g wet 4.2

Fgr'kg w€t 4.2

UqkS Yret 4.2pg,/rs s.,€t 4.2pgflqwst 4.2

FC/kS wet 1_2pgftgwel 4.2pdkgwel 42.3

ldkgwel 1-2

Igkgw€l 42

!g/l(g w€t 4-2

f.,guftg wet 42-3

t gks Y/€t 42-3

t gkg wet 4.2pr/kS rvet 4.2

I

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BRLBRL

Thit taborQbry eporl is aot volid wirtord sd zafhoizel si.f.'ra$tr. oa the covs page_

. Rc?ortable Derectioo Limir BRL = Betow Repoding Limit Page 68 of 152

Page 424: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMtFB.6

sA59464-14

Client Project #301 -88

Collectiofl Datc/Timel5-Mar-07 00:00

MatrixBallast

Received19-Mar-07

CAS N^ Analytets) Resull FloS Uni6 *RDL Merhod ReJ, Prcpa.ed ,hulyze.t Buch ,ladyt

Volotile Orgrnic Compounds

Volatile Orcanic ComooundsPrepsred by method SW846 5035A Soil (lo' , level)10Oa2-5 Styrone${Fa}€ .1,1,1,2-Tetrachtoroethane

7+34-5 l,'1,2,2-Tetrachto.oethane127-18.1 Tetrachloroethene10&e0{ Toluene87€1{ 1,2,}Trichlorobenzene120{?,i 1,2,+Trichlorcbenzonell{5-6 1,'l,1-Tridtloroelhane794G5 1,1,2-Tachlomethane79{1{ Trichloroet}Ene

pgftqwel 4.2

yqy'kg wel 42

Ug/kg wel 4.2

pgL/kg wel 4.2

pg/t(g wet 4.2

lgikgwet 4.2

pg/kg wet 4.2

!g/kg wet 4.2

pg/kg wet 4.2

UgL/kg w€t 4-2

!g/kg wet 42

Ug/kg w€t 4.2

Ug/kg wet 4.2

!g/kg wet 4.2

pg/kg wet 4.2

lrg/kg $ret 8-5

pg/kg wet 4.2

Fg/kg wel 42.3

!g/kg wel 4-2

pg/kq wel 4.2

Ig/kg wel 4 2

!g/kg wel 42

t4/kg wet 42.3

lgr'kg wel 84-6

70-130 %

70-130 %

70-130 %

70-130 %

rYE/.kS 25.4

rnsftg 25_4

'rVkS 25-4

ftrSrkS 25.4

'iSftS 25.4

mSikS 25.4

nE/kS 25.4

nVkS 25.4

nE,kS 25.4

rnSrkg 25.4

40-14] %

BRLBRLBRLBRLARLARLSRLSRLBRLBRL

BRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

103t06112104

Field extractod

BRLBRLBRLBRLBRLBRLBRLBRLBRL8RL

t 1 1

I

1

l

I

1

I'I

1

1

1

1

1

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SW 846 82604 22-MaiO7 22-Ma(47 7031291 RLJ

75{9-4 Trichlorofluororn€thane (Freon 11} BRL5-r8-4 1,2,3-Tichloropropane95-63{'1,2,4-Trimethylb€nz€ne10e67{ 1,3,s-Trimethytbenz€nef5414 Vinyldlloride1330-207 rn,p_xylene5476 o-Xylene109-99€ T€fahydrofuran60.297 Ethyteth€r!l9tt-o5!8 Tert-amyt methyt ethef637.s23 Ehylt€rt-bslyjelher108-20'3 Di-isopmpyleth€l7t65{ Tert-Butanol/ butyl elmhol12+91-l l ,4.Dioxane

S0nogala /Bcovsr'es:44o-tn4 +Brcmofluolobenzene2037+G5 Toluene4S1706+074 1,2-Dbhlorcethane-d4t868-SU Dibtomofruaronelhane

VOC Extraclion

Exlirct ble P€lrolerm HydrocarboN

Extractable Total Petrol€um HvdaocarbonsPrepared by method SW846 35508

8006{1-9 casoline6e47Ho+ Fuel oil #26ea7e31-3 Fuet Oil #46e5${G4 Fuel Oil#6M0980000o Motor Oil.re010(x|0o Aviation Fuel

UnidentifedOlher OilTotal PetroGum HydrocatuonsCgC36 Aliphalic HydrocErbons

SunDgafe Ecovenbs:$e6-12- 2 I -Ch btooc Ia de ca ne

Semivobdle Orgtic Compoonds by cC

Oroanochlorine Pesticidos SWE46 8081APrepa.ed by merhod SW846 355083o+olr2 Aldrin

VOC 20-Ma.-07 20-Mar{7 7031156 B D

+CTETPH 22-Mar-o7 26-Mar477O31283os

BRL !ciks 13.7 SW846 E081A 21-Mar47 26Mar07 7031171 TG

Ih.J labororory epod Is nol eolid n ithout an arltho.ized signatare ot the cover page

+ Reporbble D€iection Limit BRL = Below Reporting Limit PaBe 59 of 152

Page 425: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeatificationMSFB{s459464-t 4

Client Proiect #30t-88

Matrl(Ballast

Collectiotr Dat€/TimeI 5-Mar-07 00:00

Receivedl9-Mar-07

CAS No- Analrte(s) Resalt Flag ania *RDL Dilatun Method Rel, Prcptred Ansbaei Bdch AMU'I

Sedivoldile Orgrtrtc Compo{nd! by CC

Omanocfi lorine Pesticides SW846 8(E1APrepared by rnethod SW846 35508319€4€ a-BHC31F€s-7 b-BHC3'l$86€ dSHCs8€ee g-AHC Gindane)57-74-s Chlordan€72-544 4,+DDD (p,p')72-5re 4,4-DDE (p,p)s0-2e.3 4.4-DDT (p,p.)6Gs7-1 D€lddn95998€ Endosjlan I332136$9 Endosulfan ll1031-07{ Endocullan Sullate7?-?0-8 Endaln7421-93-a EndrinAldehyd€76-{.1-€ Heptachlor72'a.3-5 L{etprychlor1024-57.3 Heptachlor Epoxidea0o1-3t2 loxaphene5103-7i-9 a-Chlordane566€F34-7 g-Chlordane53494.70-5 Endrin l(ebne

Su'rogate a€co@rtes;fi386a+2 44-DB4clanuo@biphenyl (Sdms1.24 Decadbtubiphenyl (Sr)Polvd orinated BipfEnvls bv SW846 8082Prepafed by mettEd SW846 3550812674.11.2 PCB 1Ot6r11o4.n-2 PCg 1221r1141-16$ PCB 1232s34€+214 PCB | 24212672-29{ rcB 124811097{S1 PCB 125411096{2{ PCB 12603732+23-s PCB 12t21l1m-14.1 PCB 1268

SlrtDgab rEcor,ct€sr1 $8e8+ 2 4,4-OB-o('anuorofipheny' (Sr)w5t-243 Decachlotobiplonyl (Sr)

Semivohtile Orgarlc Compoutrds by CCMS

21-|tb(47 26]l.natr47 703117t TGBRLBRLBRLBRLBRLBRLgRL

BRLBRLBRLBRL8RLBRLBRLBRI-BRLBRLBRLBRLBRLSRL

70128

BRL

BRLBRLBRLBRLBRL8RLBRIBRL

751m

BRLBRLBRL

BRL

BRLBRLBRL

u9/k9l.rca9Fdlq

fdkg

t,S/kg

r9ftg

ugfts

lgftst SikgtiSikSpsrkspgrr(9

rjgkg!gtsusl(s$slkspdks

t dksr{'tglgk9pcrkg

13.7

13.7

13_7

13.7

68.7

13.7

13_7

13.7

7.ffi

13.7

13.7

13.7

13.7

13.7

1 3 . 7

13.7

13.7

13.7

13.7

13.7

w150%361fi%

sw846 8081A

sw646 8062

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111II

t€ftsr€ftguqrksrsrksrgrspsrts!dks!gtsTST(g

27527.52t.527.527.527.5

1

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zl-Llarry 24-lvlar-07 7031170 SM

30-150 %30-1fi%

Semivolatil€ Oroanic Compounds bv SW846 82 rcPrepared by me iod Swgil6 3550883-32-9 Aoenaph0€dea|&964 Acenaphtirylen€@-5$3 Aniline12G12-7 An{iracaEr912-2L9 Alrazina10933-3 Azobenzen€y'Oiphenyldiatne9247.5 B€nzktine56-5+3 Eenzo (a) anthracene

2.-Met47 2*lat47 7031 282 M.BpgJks

!9/ksusftslsftspgfts

t€/K9rc/rgTSAg

629mg629

629

629

629

629

629

Sw8,l6 8270c

ThjJ lab.alory Eport ir Eat wIU withoa za aythotizd slgaaat . oa rte @wr Fage .

I Repo.table D€tection Limit BRL = Bdow R€podiog Limit PaEe 70 ol 152

Page 426: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SarEple IdentificationM$FB{sA59464-14

Client Proiect #301 -88

MatrixBallast

Receivedl9'Mar-07

Collertion Datc/Timel5-Mar-07 00:00

CAS No. Ar'alru(s) Fhc iRDL Dilatinn Dlethod Retr Prcpared Anallzed Bo!.h Analfsl

Semtvolrlile Org€ric Compounds by CCMS

Semivdatile Omanic Comgounds bv SW846 B27OCPr€pa.ed by method SW8,l6 35508

s0-32{ Benzo (a) pyrene

205t99,2 genzo (b) fluoranhene191-2a-2 B€nzo (g,h,i) perytene

20748-9 Benzo (k) fluoranthene0t65{ B€nzoic acid10G515 Benzylelcohol1 r 1 .91 r Bis(2-ctrtoroethoxy)anethanefi1-44-4 8is(2-chtoroethyl)efier3e63E.32-9 Bis(2-chtoroisopropyl)ether117{1-7 Bis(2-ehythexyl)phthatater0t-55J 4€rornophenyt phenyl elhera5{&7 Buttbenzytphthalate86.7,t3 Cerhazoles9-5{].7 4-Chloro-3-rnethylphenol10647€ +Chlorcanitine91-5€-7 2-Chloronaphthatene9+s7{ 2-Chlomphenol700+72-3 +Chlorophenytph€nytether21&014 chrysene5$7S3 Dibeflzo (a,h) anthracene132+a.9 Dibenzofuran9t5O-1 l,2-Dichtorobenzene5,41.73n l,3-Dichlorcbenzene106-46-7 l,4roichtorcbenzene91-94-1 3,3'-DichtofobeMidine1AF3-2 2,4-Dichtorophenol84-6F2 Diethylphthatatg131'r1 i Dimethylphthalate10567'9 2,4-Dimethylphenolu-f+2 Di-n-butytphthatate534-5C-i 4,6-Dinilro-2-methylphenol

51-2&5 2,4-Dinitrophenol121-r.-2 2,4-Dinitotoluenee,oe20-2 2,o-Diniliotoluene11744.0 oi-n-octylphlhalate206-44,0 Fluorenthene86-737 Fluor€ne1i&74-l H€XEchlorDbenzene

67€&3 Hexrchlorobutadiene77474 Hexachlorocyclopentadiene4772'1 H€xachloroethane19.3'3&s Indeno (1,2,3-cd) pyrcne

{,G12{ 1-Methylnaphthalene70-591 lsophorone9i5l€ 2-Methylnaphthalene95-4&7 2-Methylphenol

loe-3s-{, 3,+Methylphenol106-{4.591-2G3 ll€phthalene

88-74-4 z-NitroanilineE9{92 }Nitroaniline

ARLBRLBRLBRLBRL8RLBRLBRLBRLBRLARL8RL8RLBRLARLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRL

BRLBRLBRLBRLBRLBRL

BRLSRLARLBRL

BRLBRLBRL

!s/ts!s/Ksugr(9ugkspgfts

lrs/ks!s/xs!dks!9lksus/ks|ls?Ks

ugfts

|lg/tg

lrg/Kg

rcr(gllg/Kg

FS/kg

!dks

!sfts

!sn(spsfts

!grk9Ps/kspqksps/kspgikg

ps./kspsaspdksps/kspgikspgn(9

!sikglrs,4qpsfts

!s/ksps/kspdks

Ps/ks!siksps/kspdks

us/ksps/kspsasps*sgs/ks

t g/kS

t'S/kS!s/ks

629 1

629 1

629 1

629 I

629 I

629 1

62S I

62S 1

625 'l

629 1

623 1

629 1

629 1

629 1

629 1

629 1

629 1

629 1

629 1

62S 1

629 1

629 1

629 1

629 1

629 1

629 1

629 1

629 1

62S I

629 1

629 1

629 1

629 1

629 1

m9 1

629 1

629 1

629 1

629 1

629 1

629 |

629 1

629 I

629 1

629 'l

629 r629 1

629 1

629 1

629 1

SW646 8270C 22-MarO7 2,Mat47 7031282 M-A

Thh tahorulory rcpo,1 is .toa roIU t+itho,tt an atthorized sEntturc on the cover psAe .

+ ReDorbble Detection Limit BRL = Betow R€Dortine Limit Pa.ge'7 | of 152

Page 427: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldepdficationMtF8.6

s45946+ t4

Clieut Proiect #301-88

MahixBallast

Received19-Mar41

Collection Datr,/Timel5-Mar47 00:00

CAS No. Analfta(s) Resut ruS Urtus +RDL Diluion Method Rqf, hepared Adalfud Bckh A4lyst

S€mivol.tile Orgrdc CoBpo!trds by CCMS

Semivolatil6 Omanic Compoonds bv SW846 8270CPrepa.ed by method SW846 35508

100{r€ +Nltoaniline98-!'$3 Nitrot€nz€n€0F7+5 2-Nitropheml10G02-7 .l-Nltroph€nol

62-7tg N-Nibocodirn€thytamine62161-7 l&Nibo6odi-n-propylamine8€-30{ N-Nibosodiph€nytamine87€F5 Peota{:foroph€nol

8+O1{ Phehanth.enet0e95-2 Ph€nol12900{ Flfef1e110€&1 Pyridine120{2-1 .1,2,+Tridtlorcbenzen€

ss€s-4 23,+Trid{ofopienol8446.2 2,4,GTrichlorophenol

Surogate recoyerigsr32140-8 2-Fluotobiphenyl

3$7-12a z-Ffuarcphenol

4165-604 Mtobenzene4s

1t6042-2 Phenol45

17tes14 Teffienyl4l4

1 1E-79-6 2,1,&Tnb@fllopl'F.not

I SW846 @70C 22-Mar-Ol 25-ldat47 7031282 M.B

I '

t '

l '

1 '

1 '

1 '

1 '

t "

1 "

1 '

1 "

BRLBRL8RLBRLBRLBRLBRLBRLBRL8RtBRLBRLBRLBRLBRL

48193S284928

US/I(S 2520

lsftS 629

rc/kg 629pgAS 2520

tqlkS 629

ugl(s 629psftS 629pdks 629

!S/(9 629

lSftS 629pdks 629

WlkS 629pS/kS 629

W!l(g 629pdkS 629

&-130tsf io %36tm %1U110 %3d-130 %15-110 %

6€/k9 O.9{3

nE/kS 1.41

msfts 0.472

ntgrkg 0236

fiSl*S 0.472

org,rg O.7O7

mS/kg 1.41

ng/l 0-0100

(€n 0.0150

mg/l O.0O5O

n€I 0.0025

mSrl 0.0050

mdl O-(x}o{o

mdl 0.0075

mg/l 0.0150

EPA MO,774{G22-4 Sifuor

74-4S3&2 Arsenic

744G3$3 Eadum

7440-rgg Cadmium

7440-{7.3 Cfuomium

743992-l Lead

-/824+2 S€l€nium

Tord Met b by EPA 6000/7000 sede! M€thod!

7439€75 l,lerqjry BRL

Totd Metrk by EPA 200 S€ri€s Methodf

aRr8RL

13.2

0.707

2.42

11 -4

8RL

SPLP l{€{r|l by EPA 1312 & 60lxy70m Sert$ Method!

SPLP Exhaction Comdet€d7lKG224 Silv€r BRI_

744{F3+2 Asenic BRL

7440-393 Barium 0.0050744r}{3-9 C€dmium ERL74q!473 Chromium BRL743047€ l\r€rcury BRL7130{2-1 Lead BRL

7|&4$2 S€lenium 8Rf

mglkg 0.029] 1 SW846 74714 &lii€r47 2641,a'47 7031311 YP

1 SW84613'f2 214ta'47 21.lrlat47 7031229 SD

1 SW8461312/6O108 2-Mat47 nl{8t47 7031323 LR

1 "

1 '

1 "

1 SW&f€ 1312n4704 ' 23+.,,ar4l 7031324 yp

I SW8461312/60104 ' 23{16r{7 7fr11323 LR

Thh hbodo4 reporl ls not vstirl w hoa an oadtodaed siFtt4jare on the cov.. pqc.

'Reportable Detection Limit BRL = Below Rcpding Limit Ptge 72 of 152

Page 428: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TASK 210.SUBSURFACE SITE INVESTIGATION

New Haven RailYardTemporary M-8 Acceptance Facility

New Haven, Gonnecticut

Volume 3

ConnDOT Assignment No- 202-3464ConnDOT Project No. 301-88

Prepared for: Prepared by:

m_99:.

State of ConnecticutDepartment of TransportationNewington. Connecticut 061 31

Maguire Group lnc,One Court StreelNew Britain, Connecticut 06051

Apnl24,2OO7

Page 429: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

APPENDIX ERailroad Tie SampleLaboratory Reports

Page 430: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8FT.Is,459464- t 5

Client Proiect #3 0t -88

MatrixWood

Collection Date/Timel5-Mat01 00:00

Received

19 Mar-07

CAS No. Anc+4(s) nesqlt Flag Unlb rRDL Ditution Mertod Ref. Prepdred Anauzed Bztch Atu UstYoladl€ Orga|Iic Compouhds

VOC Extr3clion Lab extracted

6,020

yS/kS 387

pg/kS 7730

lgftS 3a7

lgrkS 387

pg/kg &7

FS/kS 387

pSAs 387

!S/kS 387

rcn(S 773

ttSkS 3870

!S/kS 387

!S/kS 387

!g (g 387

ySn(g 1930

USrkg 387

rrSftg 387

uqkg 773

!gn(S 3a7

FSrkS 773

trg^S 3aI

US/IS 387

pSi<S 713

lgkS 387

lg/kg 347

!g/kg B7

ug/kS 387

WtkS 3El

trSAS 387pg/kS 773

pg/kg 347

w(g 387

US/kS 387

t gkS 387

!S/kg 3a7

Ig/kg 87

US/kS 387

pgtkg 387

pSftS 387

pSftS 387

pS/kS 387

pSftS 3A7

!SI(S 387

€/rg 3870

pS,kS 3a7

pgAS 387

pg/'(S 387

lSftS 3870

UdkS 3870

ISftS 3a7

1

505050505u50

505050

5050505050505050505050505050505050505050505050505{)

505050505050505050505050505050

voc 20-Mar-07 20-Li1ar07 7031156 BDVolalil€ Oroanic ComgoundsP.epared by method SW846 5030 Soil (high levet)76.13-1 |,'l,2-Tdchtorotrifluoroethane (FreoERL67€4-1 Aceton€ BRL107-11-1 Adldonitnte BRL114l-2 Benzene BRL10&€6.1 Bromobenzene BRI_7197.5 B.omochtoromethane BRL15-2f4 Bfornodichloromethane ARL15a5-2 Brenoform BRL74a19 Brchomethane BRL

2-Blbflone (MEK) aRL10+51{ n-Butylbenzene BRLi3198{ sec-Butylbenzene BRL98.06{ t€rt-Butytbenzene BRL7!F1:F0 Ca.bon disu tde BRL5&2$5 Carbon tetrachloride ARL10&90-7 Chlorcbenzene BRL7fiGs Chloroethane ARL67€s3 Chtoroform BRL744f-3 Chlolqmgt!46s BRL95,{9{ 2-CblorotoJuene BRL106-43-4 4-Chlorotoluene BRL96^12{ 1,2-Dibromo.3{.hloropropane BRL12{-{t-1 Dibromochloromethane BRLi0s93-4 l,2-Oibrornoethane(EOB) ARL749s1 Dbromornethane ARL95S0-1 l,2-Oichtorobenzene ARL54t-7J-r l,3-Ocruofobenzene 8RLl{An6'7 1.4-Dichl€fo,benz6n€ BRL75.714 Dichlorodanuoromethene (Freonl2)BRL75-3it-3 1 , i Oichloroethane BRLloru6-2 1,2-Dichto.oethane BRf75\3s-4 l,l-Dichloroethene BRLi56-€s2 cis-1,2-Oichtoroehene BRL156.6{16 trans-.1,2-Dichloro€thene BRL78i7-s |,2-Dichloropropane BRL'14?-2&€ t,3-Dichlompropane BRLs+tu1 2,2-Didllorc,propahe BRLs6lse6 i,1-Dichloropropene BRL10061{1-5ci9l,3-Dichloroprcpene BRL10061{2-€ lrans.l,3-0ichlorcpropene BRLlo0r14 Ethytb€nzene BRL67$&3 l-l,exachlorobutadiene BRL591-70€ 2-tbxanone (MBK) BRL9&824 tsopropytbenzene BRL9{l{7-6 +lsopropyltoluene BRL16r'4{€ Mebyl te(-butyl ether BRL1o+rGl +Methy'-2-pentanone(M|BK) BRL7tO9? Methy!€ne cfilodde BRL

SW&+682608 21-Ma(47 22-Ll,a?0r ru1r89 jro

91-2G3 Naphth€tene

PaBe 7l of 152

Thk bboratory repod is,tot rdid wirhoar an aurtoizpt sig',eture on ttu coeet page

'Reportable Det€.ction Limit BRL= B€tow ReDorting Limit

Page 431: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ IdetrtificationMEFT-1sA59,r6t- 15

Client Proiect #l0t-8E

Matrixwood

Collection Date/TimeI 5-Mar47 00:00

R€ceivedl9-Mar47

CAS Na. Anzly.(s) Reszb Flzg .RDL Imuion Method Rctr Peparcd Aazlycd Bdkh Analtst

Voladle Orgrnic Compounds

Volatil€ Orqaoic ComooundsP.epared by rEthod SW846 5030 Soit (high tevet)103{5-1 n-Pmpytbenzene BRLroo-4z-E Sgr€ne BRL630'20{ 1,'l,1,2-Tetrachloro€tr|ane BRL79.3.1-5 1,1,2,2-Tetracl oroethane BRt127-tB-4 Tetracfitoroethene BRL108-8€-3 Toluen€ BRL87{1{ 1,2,3.Trichlo.ob€nzene BRL12G02-i |,2,{_Trid o(ob€flzene ARL71-55€ 1,1,j-Trichloroethene BRL794G5 1,1,2-Trid oroelhane BRL79{1 6 Trichlor€thene BRL?s€94 Trichto.ofruoromethane (Freon .11) BRL96-1&4 .1,2,$.lrichtoropropane BRLs633-6 1,2,+Tdmehytbenzen€ BRLio&€74 1,3,5-Trim€fiLlb€nzen€ BRL75.o1ir Mry' chloride 8RL1330.2c7 m,p"Xylene BRL95-475 o-Xylene BRLt0$9s-9 T€bahydrofuran BRL6{rzs7 Ethyt ethe. BRL99.4-05{ Tert-amyl methy' elher BRL637-92-3 Ethyt tsrt-butytelh€r BRLt0&20-3 Oj-isopropyt ether BRL7s€si Tert-&rtanot / buv alcohol BRL12+91-1 '1,4-Oioxan6

su,rogale rccovades:450401 +Bromof,uorobenzene2037-2Gs Tduene-de| 70@07 4 1,2-Dbhloroethano441868-s77 Dibtdnofluotomethane

Eitrrchble Pet|.oleum llydrocrrbons

Extractable Total P€lroleum Hvdroca,bonsPrepar6d by m€thod SW846 355088OCOS1-9 Gasoline68a7B3ez Fuel Ot #l6847e31.3 Fu€l Olt #4685s3.04-{ Fuel Oit #6M0€q)000{) Motor OilJ001oo0o0 AYiation Fuel

UnidentifiedOS|er OilTolal P€0doum Flydmcarbons@436 Aliphattc Hydocarbons

sunwab fecoveries:3386-33-2 l-Chlotwtdocene

S€mirolrtile Orgrrlc Compou||ds by ffOroanochlodne Pesticiles SW846 8081APrepared by method SW846 3550830+oG2 Atddn

SW846 82608 21-tiar47 224a-o7 7031189p949pgfts

ugksrs^9usfts!sn(9rgftgpo/k9ygrspgkg

|lsftsr8/kstryrcpgkg

rcrksrslkst oftsgslksggtspsfts

FSrkSpdr9

usftslsiksllgr(s

387

30?

307

387

382

87

387

387

3a7

A7

387

387

387

387

347

3E70

347

387

387

3t]7

3470

7730

5050505u50505050505050

50

50

50

505050

1 1 1102109103

70.130 %

7G130 %

7G13O %

70-130 %

BRL8RL8RLBRLBRLBRL1 t.600C€lc1llat€d E6| 1,6001'|.600

rcT ETPHnrSAS

mg/kS

rEftg

nsn(0'nS^9

lnglg

fiigl(g

mS/kS

o€r*g

mc^s

99.2

99.2

99.2

99.2

99-2

992

93.2

9S.2

99.2

2-Mar47 H.,',ar47 703128:l DS

4114) %

trsas SW84A 8081A 2l-Ma!-07 zs{lsr{7 7031171 TG

Thit labnloty r.tori b ,rot lolU '{'ttho,.t aE outorizd signztur. on thz co''a page.

. Rep(rtttrlc Detect'ton Limit BRL = B€low R€portinC Limia Pdge 74 of 152

Page 432: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEFT-IsAs%64- l5

Client Proiect #301-88

Collection DatdTim€l5-Mar-07 00:00

Mat ixWood

Rec€ivedl9-Mar-07

CAS No. Anelruts) F,oC Urirr +RDL Dilt'tion Method ReJ Prepued Atullzed Balch Ahaust

SedivolrliLe Or$ric Compoundr by CC

O.qaflochlorine Peslicides SW8,+6 8081APr@ared by method SW846 35508319{4-€ a-BHC31e€s7 b-BHC31S{fi d-BHCs€{s-s g-BHC (Lindane)57-74-9 Chlofdane12-54{ 4,4-DDD (p,p,)n-s+s 4,4.OD€ (p,p,)s0-2+3 4,4-DDT (p,p.)m-57-1 Dietdrin95948-8 Endosulfan I332t36ts Endosulfan ll1031ry{ EndosulfunSulfatell2-?o-A Endnn742r-9il-4 EndrinAJdehyde76-44-0 Heptachlor7243-5 uethorychjor1024-57n Heptachlor Epoxide€Ooi-352 Toxaphene51o}7i.9 a-Chlordane55ffi4-7 g-chtordane53494-rc-5 Endrin Ketrne

Su|rDgsf€ r€cor€niesr10386-812 4,4-D8-Odanuorcbiphenyt (Sr)m5t-2a3 Decachlorobiphenyl (St)Polvcfibrinared Biohenvls bv SW846 8082Preparod by melhod SW846 35508126?+11-2 PCB 10161110+25-2 Pc.B lZ2111141-16-5 PcB 12325346921,9 rcB 124212672,235 rcB 124811W7{&r PCB 1254r i096{2-5 PCB 1 m03f32+2T5 PCB 1262i1t0G11,1 PCB 1268

Srr/togats aecover'esr

SW846 8081A 21-Mat41 26-Ma(07 70311f18RLBRLBRL

BRLBRLBRLBRLBRLBRL

8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRL

843

BRLBRLBRLBRLBRL168t648RLBRL

t siksllsftsps/ksps/}s

tlg/(g

Lrg,r(9

wKg

!s/kgpgrkg

ps/kspsrqpgag

Lrg/xg!sft€pg&s

tlsiftst 9/(9pg/kspg/ng

|lsftspsfts

44.2

40.240.240.2

20140.240.2

6.210.2

6.240.240.240.240.240.240.244.220140.2

44.240.2

1

I

1

1

1

1

1

1

1

I

I

I

1

1

1

I

l

1

1

1

1

u9/tgusftg!9ft9

!9/Kg

!9/1rSps/kstrS/kSusr(suEks

3G150 %

30-150 %

sw846 8082

swE46 8270C

80.380380_38038 0 38 0 38 0 380_380_3

21-MatO7 244Jlarl7 7031170 SM

fi3e04+2 4,+DB4cbnuarchiphenyl(Sr) 65

m51-2+3 Decachlotobiphenl (S!) 95

Se.dvolalilc O.ptric Compounds by GCMS

Semivolatile Oroanic Csnoounds bv SW846 8270C

Prepared by method SW846 35508

a3{2.9 Ac€nEphthene

A)&96{ Acenaphthylene62-5!3 Aniline12012-? Atrlhrac€ne1912-21-9 Nrzzjne103333 Azobenzene/Diph€nyldiazine92€7-5 8€nzidjn€

5&5S3 B€nzo (a) anFracene

30-150 %3t)-150 %

29.00016,900BRL282.000BRLBRLBRL227.60

rc/tspsfts

!snrs!sr(s!sr(spg&spgr(s

ugts

246024602460246024AO2$O

24602460

22-Nl€t47 64 at47 7O312A2 M.B

Thls laborrlo.y Eporl ls nol valu dlhod an adhotlzctt signature on rte cowr page-

' Reportabte Detelrion Limit BRL = B€low R€porting Limn Page 75 of | 52

Page 433: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationMSFT-IsA5946L l5

Client P.oiect #l0t-88

MahixWood

Collection Date/TimeI 5-Mar4? 00:00

Receivedl9-Mar-0?

CAj N^ AMIlte(s) Resah Flig Ania 'RDL Diluttah Malad Rel PrcWed Analyzen Bach Anelyst

S€mivolalile OrScnic Compoundr by GCMS

S€n1iwlatile Oroaric Compounds bv SW846 8270C

Prepared by method SW846 35508s0-324 BerEo (a) py.eneatrFgs.z Benzo (b) fluoranthenets1-?a-? Benzo (g.h,i) perytene207-cro4 Benzo (k) nuorandnene6s€5{ Benzoic acid1oo5l{ Be62yl €laph6{1t1.e1n Bis(zddorc€thoxy)methaner1 l-aa{ Bis(2-ohloroethyt)€trer3s€r1,8-32-9 Bis{2dtloroisopf opyt)ether117-81-7 gis(2-ehylheryt)phthatate

10r-s5-3 4_BEmopheny' phenyl ethers5€8-? Butyt benzyl phtlalate86-74{ Celbazole50,50-7 4-Chloro-3-rnethylph€nol106-47{ +Chlorosnilin€9r.5€-7 2_Chlo.onaphthalenest57j 2-Clrbrophenol700$72-3 4-Chloroph€nyl phenyl eth€r216-{11.9 Chrysene53-70-3 Oibenzo(a,h)anfnracene132-€4,9 DiberEofuran95'5O-i l,z-Dichlorobenzene541-73-1 l.+Dichlorobenzen€106-,!S7 1,4_Di.fdorobenzen€91-9,1-l 3,3'-Dichhroberudine1203!-2 2,4-Oichlorophenol44s6.2 Diehyiphthatete131-113 Dirnethy' phthatete1H7-e 2.+Dim€thy'phenol8r-7+2 O-n-bu!/phthalate534.521 4,6-Dinitro-2{ethy'ph€nol51-2&5 2,4-Dinltrophenol12t-1,1-2 2,4.Dinibolotuene606-202 ?,GDinibotoluene117-844 Di-n-octylphhelate206-i|{{ Fluo€nthene&-73.7 FlUOren€llBT/t-l Heracfilorobeflzene67{&3 Hexadtlorobutadieneru74 He)@chlorocyclop€niadiene67-f2-1 HexadrlorDethane193-3$5 tndeno (.1,2.3.cd) pyr€neg0-12'o l-Methylnaphthelefle70-5+1 lsoptrorone9i57{ 2-Meby'naphdEt€ne95-,re7 2-Msfty'plronol108-3s.1. 3,4-Mefiyhhenol106-44-591-2G3 Naphhat€ne8a-71.4 2-Nitroar line99{9-2 +Nitroanillne

99,300| 60,00,034,200187,m0BRLBRLBRLBRLBRL

BRLBRL152,0(X)BRLBRLBRLBRLBRL358,000r0,90026,900

BRLBRLBRLBRLtJKL

BRL8RL8RLBRI-BRLBRLBRL876.fi1042,700BRI-

BRL

SRL40,4003,700BRLBRL

BRLBRL

BRLBRI8RL

ps/ks

!s/ko$s/kstrSikSlgftg

Fgl(spgks

!s/ksusftspg/ks

t gukg

!gftSpdks

Fs/ksu9ft9

€4qus/k9pg/rs

!sr(gusftsrc/kgps/ks

!c/ksudkslsrkglsfts|ls/kgFSAgpg/kg

ps/k9!s/tst/gfts

r$/kgt€ltg!s/ksfgks!g/ks|lgftS

u9ftgt4/tgFS/kgpdkspsn(g

wftsrslksrsrtspclks

!s/ks|lgftS

lsrts

2460

2460346024602&r)24602140246024602460246024602460246024602'4fO24ffi2{60246024602460246024602460246024$0246024602,1602460246024602#O24602415024602460246021€o

2{6024602&O246024602460

2M2,160

246024602{li0

SW846 8270C 22Jld47 m.+,,et47 7031262 M.B

n&r ldhrabry report ls aot volid t{rthobr zd 4uthoitzd dgnsafie on rtc co',a page.I R€Dortsble Detecaion Linit BRL = Betow Repfring Limit FaaE 76 of 152

Page 434: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole tdenlificati'rnMSFT-I

sA59464- r 5

Clienf Proicct #301 -88

Collectiop Drte,/Tirnel5-Mar-07 00r00

MattixWood

Receivedl9-Ma.-07

CAS No. Analtte(s) Resuk Flag Ani6 ,RDL Dilation lrlethod ReJ Preparcd AruUud Bat& AnalrslSemivolrdle OrgrDlc Compouods by CCMS

Semivdatile Oraanic Comoounds bv SWB46 8270CP.epared by method SW846 35508

i0o.{r1{ 4-Nitrcaniline98-9+3 Nitrobenzene8A-75.s 2.Nitmphenol100.{t2-7 4,Nitophenol62-75-9 N-Nitrosodimethtamine621{a-7 N-Nitosodi-n-pfopylamine86-30$ l+Nitrosodiphenylamine87{85 Pentachtorophenol8fl11€ Phenanthreno104.95,2 Phenol129{r{ Pyrene1to€6-1 ryndine12G82-1 .1,2,+Tichlorobenzen€

95-95-4 2,4,STnchlorophenol88{+2 2,4,&Tnchlorophenol

Srlrmgate Bcoveias.n140-B z-Fluorobiphenyl

367-124 2-Fluorophenol

41A5404 Nivobenzene4s

116fi2.2 Phenot45

171&514 Terphenyl4l4

118-7 2.4,6-Tibromophend

Totrl Mctrls by EPA 60001000 Series M€thod$

7439474 Merc!ry 0.(x25

Totil Melrls by EPA 200 Series Mcthodt

BRL

BRL

13.9

o.714

2.96

2 1 8

BRL

TCLP ExlEction

74rulz2-4 Silve.

7440-3&! Arsenic

71.()-393 Barium

744+4+9 Cadmium

7421047.3 Ch.omiom

7a39476 lirefcury

743S€2-1 Lead

?e2-4S2 selenium

1 SW846 8270C 22,Mar47 26.Mat47 70y2A2 M.A

1 '

1 "

1 '

l -

1 "' t '

1 '

1 '

1 '

1 '

1 '

BRLBRLBRLBRLBR.L

BRI.ARLBRL4m,m0BRL640,000BRLBRLERLBRL

492639345548

Completed

BRL

BRL

o.0761

0.0050

BRL

BRL

0.0244

BRL

!S/kg 9850

!gn$ 2$0

tg/kg 2M

USftS 9850

US/kS 24ffi

rc/kS 2460

WkS 2460

!S/kS 2460pg/tg 2460

!S/kg 2460pg/kg 2460pSilg 2460pgr'kg 2460

rc/tg 2460pSAS 2460

30-130 %15-110 %30-130%15-110 0A

30-130 %15-110 %

msftg 0 0291 1 SW846 7471A 26-Mar-07 26{v1ar-07 7031311 YP

EFA200.7 26-Mar{7 26{4a.07 7031263 lR71140-22-4 silver

74,40-3&2 A6enic

7440-3+3 Earium

74404+0 Cadmium

,44147-3 Chrcmium

7439.92.1 Lead

7782-492 Selenium

mSftS 0.904

mS/kg 1-36

mg/'l(S O 452

mS/kS 02m

mS/kS 0.452

mSftg 0.678

mS/kS 1.36

N/A

mSI 0.0100

m94 0.0150

mg/l 0.0050

mg{ 0.0025

mgn 0.0050

n SA O.N04O

nEil 0.0075

mg/l 0.0t5t)

TCLP Metals by EPA l3ll & 5000/7000 Seri€s Methods

1 SW8461311 21-l.lat47 21^ta(O7 7031227 AO

1 SW8461311/6010A 23-lrar-07 24-{4ar-07 7031325 HB

1 '

1 '

t "

t '

1 SW846 131 1/747M ' 2!Mar-O7 70;1326 Yp'f sw846 1311/60108 " 24-Mal.I)7 7031325 HB

1 '

Thk laboratory rcpoa k aot valid roithoar a^ attlhori..d tignotare on lhe cover page .

' R€porbble Det€ction Lihit BRL = Below R€porting Limir Page 77 of 152

Page 435: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationMSFT-2sA,594U-t6

Client Pro.iect #301-88

Colleclior Dat€r'Timet 5-Mar-07 00i00

MatrixWood

Receivcdl9-Mar-07

CAS No. Anatk(s) ResuL F'lag Aai6 4RDL Dilation Meahod R4 tueparc.t ,4idlwd Boeh Aaalf;a

Vohlile Orgrtric Compouod3

VOC Exbaction t',t/A

pdks 204pSAg 4090

!g/kg 2U

ugftg 204

USftS 2M

usrtg 204

Ug/lq 7)4

!gn(g 2O4pgrks 409

f.rSftS 2040

FSrkg m4

!S/tg 2O4

]JSI(g 2O4

ttgikg 1O2O

Ig,kS 204pS/kS m4gg/kg 40€

FSftS 2O4

ttgikg 409pgftS 2O4pS/kg m4

lsftS 409

tE*S 2MpgJkS 204pS/kS m4

!g/kS 204

trSftS 2O4

teikS 204

USftg 409pSI(g m4pSn(S 2O4

t gikg 204

FgrS 2Updks n4pSn(g 2M

l4/kS m4

t€/kg 204pg/kg m4

l/g/ks 2u

|rgftS 204

t4lkg 204

ISftS 2A

!gI(S 2(XO

!9I(S m4pSftS 2u

uSfiS 2O4

UCftS 2040

!g/kS 2040

!g/kS 204

LS extracted

5,690

20-Mar47 20.l}l/'447 7031156 BDVolatile Omanic ComooundsPrepaGd by method SW846 5030 Soit (high tevel)7F13.1 1,1,2-T.id orctrifr./oroethan€(FreoERL67{+1 Ac€tono gRL

t07-i3n Acrylonitrile BRL7143.2 B€nzene BRL10F€€-i Bromobenzone BRL7rl€7-5 Bromochlorcmethane BRL?5-?7{ Btonlodid ,olomellane SRL7125-2 Baomoform BRL74{}9 EromomethaDe BRL78-9+3 2-Birtanone (idEK) BRL104'51{ GButtilbenzene BRL13$9€-8 sec-Butytbenzene BRL9€{64 ted€utylbenzene BRL75-i5-0 Carbon disutfide BRL56-2$5 Calbon t€bachloride ARf10&90-7 Chlorobenzen€ BRL75-OG3 Chtorcethane BRL67{+3 Chtoroform BRL14-Af-3 Cibronethan€ BRL95-49{ 2-Chlorotoluone BRL106-43{ 4_Cf orDbluene BRL96-12.9 1,2.Dbmrno-3-cilorcpropane BRL124-a€-1 Dbrcmochto,romef€ne BRL1oe$-a l,2olbromoethane (EDB) BRL74.9t3 DibronrornefEne 8Rf9+5Gl l,z-CxoHorobenzene BRL541-7+1 l.3-Oichlorobenz€ne SRL106-16-7 l,4-Dicfilorobenzen€ BRL15-714 Dichlorcdinuorome$an€ (Freont2)BRL7$34-3 1, I OicHoroehane BRL107-uG? 1,2-Dichloro€ttune BRL7tn5-4 1,1-Diafiloro6thene BRL15€-50-2 cis-1,2-Oichloro€th€ne BRI-156€0-5 trans-1,2-Dichloaoethene BRL7E{7.5 |.2-DicHoroproDano BRL142-2e€ l,3-Dichtoroplopane BRL594-to_? 2.2-DichloroDrcD,an€r BRL56$584 l,l Oichloroprogend BRLl(106l{1.5cis-1,}OicNoroprog€ne BRL10061{26tens-1,3-Dicilbropropene BRL1oc4l-a Ehldb€nzeoe BRLA7{83 H€xad orcbutadien€ BRL59r-78-6 2-Hexanoi6 (MBK) BRL9e{2.8 lsopropldtonz€ne BRLSg47{ ,l-lsopropttoluen€ ARL16!t44-4 Mehylt€rt-bu$d edr€r BRL1oE'lGt +Metli!'f2+eotanon€(M|BK) BRL75492 Methy'ene d oride BRL

SW 8,f6 82608 21+llat47 224a(47 7031189 iro50505t)5050

50

5050505050

50505050505050505050

5050505050

50

50g)

5050505t)50

50

50505u50

5091-2G3 Naphthalene

Page 78 of 152

Thh ltfurdloty r.pod at nat tdid plthot t a asthodaed sigEttttE on th. cor.t pgL

+ Reportlbl€ Det€.tiotr Limir BRl- = Bdow Reporting Limit

Page 436: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [dentificationMSFT-!sA59464-r 6

Ctient Proiect #30 t -88

MatrixWood

Reccived19 Mar-07

Collcction Datc/TimeI5-Mar-07 00:00

CAS No, ,lnalrte(s) F,oS A n s *RDL Dilution Mahod ReJ. Preparcd Analyzed Barch AMltst

Voletile Orgrnic Colrlpounds

Voladl€ Omanic CornooundsPrepa.ed by melhod SW846 5O3O Soit (high levet)

7549-4 Tichtorofluoromethane (Freon j 1) BRL

l096tl n-Propytb€nzene1{t0{2-5 Styrcne63Gm$ 1,1 , |,2-Tetrachloroethane79_34-5 1 , 1 ,2,2-Tetrachloroethane127.18-1 TetrachloroetfEne108-8€-3 Toluene8741€ 1,2,$Trichtorobenzene120-82,1 1,2,.4-Trichlofobenzene71-55-6 I ,1 ,l _Tricfiloroethane

794G5 1,1,2_Trichloroethane7901.6 Trjchloroethene

SW 8{6 82608 21-Mat47 22.11,a.-07 7031189 jro

+CT ETPH 22-Mat47 26-Mat47 7031283 DS

BRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRL

BRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRL

110102106101

BRLBRLBRLBRLCalc lated asBRL33,600BRL33,60033,600

70-130 %

70-130 %

7G130%

70-130%

!sn(spSn(S

us.4(sps/k9

!s/kgpg/r(g

!g/kg

!g/ks!9ft9!g/Kgtstks!sfts

!s/ts!gfts

usnlgr/sast'sftgus/kgtrg/kg

trg/kgpg/kg

pg/re,

psiks

w/ksw/x9

204

204204

2442042042012M2M2042042042042042042A4092012040m4204m420420404090

50

505050

5050

50505050505050505050505t)50505050505050

$.ta-4 1,2,3-Tdchloropropanes5{34 1,2,4_Trimothytbenzene108{7.8 l,3,tTimothytbenzenefs414 Mnyt chtorider33G2[!7 m,pFxylene95-47{ o-Xylene109{9€ Tetahydrofuranfi-zs-7 Ehy' eher9gFO5{ Tert-amylftethyletheren732-3 Ethyt tert-butyl ether10&20€ Di-isopropylethef75{$o Tert-Butanot/ butyl alcohol1299't-1 1,4.Dioxane

Surogate recovedes:160401 +EJtomofluorobenzene

2037-26-s Toluene4S

1 70.@47-0 1, 2 -Dichloroethane-d4

,86&5+7 Dibrcmofluommelhane

Erthctable Petroleum Hydrocarbons

Extradable Total Petroleum Hvdrocarbons

Prepared by method SW846 35508

8069t-9 Gasoline6447+30-2 Fuel Oil#26&176-31-3 Fuet Oit#468553{0-1 Fu€loil#6i.,109800000 Motor OilJ001m000 AviatioD Fuel

Unidentified

Ot|erOil

Total Petroleum Hydrocabons

CSC36 Aliphatic Hydrocarbons

Suno€,ale rccovedes:338tF 3 3 -2 1 -C hto rooct ad e cane

Seoivohtile Organlc Compound$ by CC

Orqanocfibrine Pesticides SW846 8081A

Ptefared by method SW846 35508

30+00-2 Aldrin

mS/tS

mg/kg

ms/'l(g

rnsfl(g

mg/kg

n,gJkg

mg/kg

mg/Kg

mg/tS

fig/kg

09.0

8S.0

89.0

89.0

89_0

89.0

89.0

89.0

83.0

83.0

4G140 %

ps/tg SW8.|n E081A 21-Ma'{7 -tittat4T 7031171 TG

Thls lsbo.aloA rcpo.l is nol wlid witho4 an salhorized sEnalur. oa the cor,c, page

r Repon ble Detectjon Limj! BRL = Betow Reprxrirtg ttnjt Page 79 of l5:

Page 437: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samgle ldentificationMSFT-2sA5946+ l6

Ctieot Project #301-88

Mati{Wood

Collection DatellimeI 5-Mar-07 00;00

Rec€ivedl9-Mar-07

CAS No. AErlrE(s) Resdl Flag U'J^ *RDL Dilaion Ll.nod Rel P4parcd AMIyzd Beteh A"alyst

Sc$dvolriile Orgsdr CompouDdi by cC

O.oanochlo.ine P€sticides SW846 808'lAPr€pared by method SW846 35508

3194+{ a-BHC31S8r7 b-BHC31946-0 GBHC5849-9 $8HC (Undane)

57-74-9 Chlordane72-544 a,4-DDD (p,C)72d+s 4,+DDE {p,C)5lr2s3 4,4-DOT (p,p')

6{1.5/-1 Dieldrine5s-984 Endo6ul6n I33213{5€ Endosulfan ll1031-07-0 €ndosulbnSutfate72-2O-A Endrin7121-93.1 EndrinAldehyde

7&{.A Heptachlor

1243-s irlethoryd{or

102a-s7-3 H€plAchloa Epoxrd€80013+2 Toxaphene51091€ a-Chlodene566&34-7 g-Chlordane

s3494-705 Enlhin Keton€

Sunog€/e recowies:| 038634-2 4, 4D8-Adfiuotohiphent4 ( Sdm51.2+3 Deca&lorobtphenyt (54

Poh/chlorinated Bioh€nvls bv SW846 8OB2Prepared by rnetlod SW846 35508

1267+1i-2 PC8-l0t611104-28-2 PCB 122111111-16-5 PCB, 1232s31n9'21-9 PcB 124212672-2e€ PCB 124811097{$1 PC8 1254rr0g6-82,s rcB 126037321-235 PCB 1262i110G14-4 PCB 1268

Srn/ogate /f,cow'resifi286a+z 4, +DB-Octaf, uotot.iphenyt (54

m -2+3 Decachlorobipheryt (Sr)

Semivolatile Orgrtric Compounds by CCMS

BRLBRLBRLBRLBRLBRLBRLBRL

BRI-BRLBRLBRLBRI.BRL

BRLBRLBRLBRL8RLBRLBRL

73

3?o3

BRL8RLBRLBRLBRL402

BRLBRL

601N

trS/kSuqikgpg/ks

Fgts!g/kspsfts

rulks!dkstqr<s!s/rs!g/tgpsag

l4/k9pg/tg

t,9I(Slrltftgusrt9pdkggs,/ks

|rgftspsikg

41.1

4 1 _ l

4 t . l

4 r . l

205

41. ' !

4 1 . 1

4 t . l

41.1

41.1

41.1

41.1

41.1

4 1 1

4 1 1

4 1 1

41.1

11.1

41_1

SW846 8ollfA 21-Mar47 261nat47 7031171 TG

fr.lfi %30-t50%

|lcfts!s/'kgug[(spsfts

t4^9usaspdkg

t4/kspsrg

42.1

42.1

E2_1

82.1

82.1

42.1

82.1

82.1

82.1

SW846 8082 21-Mat47 24]li,a147 7031170 SM

SW846 8270C 22t at47 ?s1]llzt47 7lJ612a2 M.B

wt f l%m-tf i%

Semivdatile Oroanic Compounds bv SW846 8270CP.€pared by mslhod SW846 355086-32-9 Acenaphttrene208++€ Acenaphtlrylene62633 Anitin€120-12-7 AnthEcene1912-24.s AtEzine10133-3 Azob€nzene/Diphonytdiszine9231-5 B€nzidinss6.5$3 Benzo (a) anthrEcene

r5,30010,400BRL

250,000BRLBRLBRL| 37,000

!9/kg|Jsn€|lsftsusit9us/kglsiks!s/ks!g/ks

221022102210

22102210221022102210

Ihis ltborubry Npod is,tot ralU withou arla?rhart?glslg!.4la€a t,a.ouer IdIg.-* Repoftblc Deteation Limir BRL= Below ReDo{tins Limit Prge 80 of 152

Page 438: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample [denlificationM8FT.2

sA59464 16

Client Proicct #l 0 t -88

MatrixWood

Collection Date/Timel5-Mar-O? 00:00

Receivedl9-Mar-o?

CAS No. Anabte(s) Resull Flog Ani s 'RDL Dilutian Method ReJ. tuepate.l AndIWd Bafth Anabfl

Semivol.dls O.ganic CompouEds by CCMS

Semivolatile Orqanic Comoounds bv SW846 B27OCPrepa.ed by method SW846 35508

50-32-8 Benzo (a) pyren€

20lFs$2 Eenzo (b) fluo.anth€ner9t-2+2 Benzo (g,h,i) peryt€ne

207{&s Benzo (k) fluoranilr€ne6s-8f,{ Benzoic acid10G51.6 Benz/ alcohol11i'91n Bis(2-ciltoro€thoxylntethane11r44-4 Bis(2<htoroethyt)ehel3sE3&32'9 Bis(2d\loroisopropyt)etfi er117-81-7 Bis(2-ehyth€xyt)phthatate10i.55-3 q-Bromophenyt phenytether

A5{&7 Butybsnzytphthatate86-74-€ calbazol€5S-5t!7 +Chloro-3_meth/ph€nd1116473 +Chloroanitine91{+7 z-Chloronaphthalenegs{z{ 2-Chlorophenol7005-72-3 +Chlorophenylphenylether210{1-9 chrysene53-7G3 Dl,ber':o (a,h) [email protected] Diben2ofuran9s-5+1 l,2_Dichtorobenzene54r-79r l,3-Dichtorob€nzene106-46-7 1,4_Dichtorob€nzene91€4-1 3,3',-Dicttorobenzidin€12o-en-2 2,4-Dichlorophenolu$62 Dielhyl phlhalate

13r-11-3 Difnethyt phthalate

105-67-9 2,4-Dimethylphenolu.1+2 Di-n-butytphthatate5,34-52-1 4!6-Dinitro-2-methylphenol51?&5 2,+Dinitrcphenoli2l-1+2 2,4-Dinitrototuene(X)&20-2 2,6-Dinitrototuenei17-84{ D-n-oOVlph0ralate2OE-4,1-0 Ftloranuren€8-717 Ftuor€ne11&74-1 H€xechlorcb€nzene87€&3 HoxEchlorcbutadienen471 H€xachlorocydopentadiene67-72-1 H€xachloroethene1s339.5 Ind€no (1,2,3-cd) pyrene

Crlz{ 1-Methytnaphthet€ne74.5&l lsophoaone9r5t6 2-Melhylnaphthalenee+.4&7 2-Methy'phenol

r06-3s4, 3,4-Methylphenol106-1.r-59l-21>3 Naphthalene&f44 2-Nitfoanilineg9{}2 }Nitroaniline

54,300144.00021,100143,000BRLARLARLBRLaR[ARLBRLBRL199,000BRLARLBRLARLBRL44S,0006,38019,300BRLBRLARLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL369,00026,600BRLBRLBRLBRL24,4005,000BRL4,460BRLBRL

BRLBRLBRL

!s/ksLjsftgr.isftg

Lig/Kg

!g/kg

ug/kg

!s/ksU9/kSWst g/Kg

t 9ft9

!sftg

Pg/r(9

trg/kg

fg/(gpg/Kg

pg/xg

pg/Kg

t S/kg

!9ft9

llg/r(gpg/k9

lrgftspg/kg

ug/t(g

ug/r(gusftsus/ts|Jg/xg

!g/K9

trg/Kgpg/kg

!9ft9

!g/kg

!g/kg

!s/kg

ttS/kS

!gr(s!sagp9,4q

ugft9pqr9

udksusftstiS/kS

tiS/kS

Ps/kg

l.rglKg

Ps/ksrslkg

221022102210

22102210221022102210221022102210221022 tO221022tO221022102210221022 tO22 tO221022102210221022102210221022 tO22102210221022102210

2210221022102210221022102210221022102210221022102210

221022102210

SW846 8270C 22-Mar-O7 -Mat-O7 7031282 M.B

Thb laboratorJ repod k zot talid withod an zathoized signature on the cover page.

'Reportable Det€ction Limit BRI, = Below Reporting Limit Page El of 152

Page 439: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Ssmpl€ [detrtificationM8FI.2

sA5946+ l5

Client hoiect #301-88

MatrixWood

Collection Dat€/Timel5-Mar-07 00:00

ReceivedIg-Mat4'l

CAS N^ Aazbtz(t) Resah FILC Unis .R.DL Dildion Llethod Retr, Prcpned Ano$zcd Batch Anabst

Se mivolrtik O.g lc CoEpound! by @MS

Semivolatile Oiqanic Comoounds bv SW846 8270C

Preparad by msthod SW846 35508r0o-o1€ 4-Nit'oaniline9F.95.3 Nilrcb€nzene8&7t5 2-Nitrophenol1OGtr2-7 +Nibophenol62_7t9 N-MitrGodimethylamirE6?1{4-7 N-Nitlsodi{-propylamine86-30{ N-Nitrosodiphenylamine87-46-5 Pentadbrophenol85.{ti€ Ph€nanthrene10+95.2 Ph€nol129{0{ h/r€n€r10-06-1 Pyridin€i2G€2-1 1.2,4-Trichlorobenzeie9t95-{ 2,4,$Tdtrlorophenol8S{&2 z,4dTrichtofophenol

Sunogate rwtei$:32ta)-e z-Fhrorobiphenylx7-124 z+fuotophenolll6a,noi Nitrohenzene454t6ar62-2 menol4stl1e514 Terphenyl4l41te7+6 2,4,6Ttbrcmophenot

Sw846 8270C 22-Mat47 2€-Mat47 7031242 M-BBRLBRLARLBRIBRLBRLBRLBRLt51.000BRL30t,000BRLBRLBRLBRL

54374439

51

Complebd

BRL

SRL

0.t05

0.0040

BRL

BRL

0-0r35

BRL

pSAS 6830

lJSl(g 2210

!g/tS 2210

lgftS 8930

$glkg 2210

l€/tg 2210pEkS 2210

!S/tg 2210

fjSftS U1Ogglkg 2210

l€/tg 2210

t€I(g 2210

Ug/kg 2210pSI(S 2210

USftS 2210

3G130 "/61+110%3Gt30 %|Gfi0 %30-130 %1t110 %

1II

1

1I

1'|

1

1

1

I

1

t

Toarl M€.rb by EPA 6m0rl000 Seri.i M€thods

7430-97s Mddlry BRL

Tot l Mctrb by EPA 200 Series Method!

2GMar{7 26{vler-07 703131 1

26-Mar-07 26-Ila.-07 7m12637440-22-4 Sitver

t4(13e2 A6enic

744{1393 B€dum

74rt0.13-9 Cadnrium

7440-47-3 Chrcotium

7€9o2n L€ad

7782-492 Selenium

rrrdkS 0 E67

m9ft9 1.33

ftrdkS 0A44

n\g/kg 0.222

mdkg 0.444

mg/kg 0.665

rn€tkg 1.33

mgil 0.0100

nS,/l 0.0150

m€I 0.0050

ntdl 0-0025

n4/l 0.0050

nEn 0.00040

n'S/ 0.m75

mSn 0-0150

I SW845 7471A

1 EPA2m.7

1 "

1 '

msag 0-0300

SRL

BRL

5.08

BRL

8,40

BRL

TCLP Metrb by EPA l3ll & 6m(y?000 Sed€! Merbods

TCLP Exlraclion

7{4G22-4 Slh,,er

7440-3&2 AEenic

7a40!393 Barium

74404!9 Cadmium

7,t40-47-3 Olmmiun

7(}$97{ ireacury743W2-1 Lead

?02-4+2 S€l€nium

1 SW8461311 21:M?'-o7 21-Mar4f 7OXln1 BD

I SW846 t311l60f 0S 234€f47 21.+d6t47 761325 HB

1 '

I '

1 '

I Sw8461311174704 ' 2+Mar-07 70Si326 YP

I SW€,f6 1311160 f08 ' 21J.,d47 7031325 HB

LR

fhis tabarctoq repoa b aot salr! witbsr ad c'rlha;azd sigt true ot thc cave ptg..

' R@orhblc Detectiol| Limir BRL - B.low R€porting Limit Page 82 of 152

Page 440: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

APPENDIX FGroundwater SampleLaboratory Reports

Page 441: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 442: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnple IdentificationMEF.l,t cwsA595l7-13

Client Proicct #30 t -88

MarixGround Water

Collection Date/Tim€t9-Mar-07 00r00

Reccived20-Mar-07

CAS No. At alXte(s) Flag Ania 'RDL Ditatiott Method ReI Prepated Analyzed Bt ch ,Anal]'sl

VoLtil€ Org{tic Compounds

Volatile Orqanic Compounds bv SW046 82608Prepared by method SW846 5O3O Water MS

7&1!1 1,1,2-Trichlorotrifluoroelhane(FreoBRL67$rL1 Acetone BRL10713-1 Acrylonihile BRLZt4?2 Benzene BRLl0&8G1 Eromobenzene BRL74-97-5 Bromochloromethane BRL75-214 Bromodachlo{omelhane BRL75-242 Brcmoform BRL74{3€ Brcmomethane BRL78€13 2-Butanone (l\rEK) BRL10a,514 n-Butylbenzene BRL13F98+ sec-Butylbenzene BRL9&0s tert-Butylbenzene BRL7!1$0 Carbon disulfde BRL56-2$5 Carbon teirachloride BRL10&90.7 Chlorcbenzene gRL

75{0.3 Chlsro6lhane BRL67-643 Chtoroform gRL

f,147.3 Chtoromethane BRL96-4S8 2.Chtorototuene BRL106-434 4-Chloroto{uen€ BRL9Gl2-0 1,2-Dibomo-3-ciloropropane BRLi2rt48-1 Dibromodllorcmebane BRL10G93-4 |,2-Dibromoef|ane (EDB) BRL74-9s3 Dibromomethane BRL955G1 I,2-Dichlorobenzene BRL54t.73.1 I,3-Dichloobenzene BRL1061|{}.7 l,4-Dichloobenzene BRL71714 Dichlorodifluoromethane (Freonl2)BRL7t343 l,t,Dichtoroethane BRL107.06'2 't,2,Dichtofoethane aRL7535i1 1.l-Dichtoroethene BRL15Gs9-2 cjs.l,2-Dichloroethene BRL15G@s trans-1,2-Dichtoroeihene SRL78-87-5 1,2-Dichloropropane BRL142-2€-9 l,3.Dichloropropane BRL59+20-7 2,2,Dichtoropfopane BRL56+5€{ l,l.Dichlorcpropene BRL1006r{1-5 cis-1,3-Dichlorcpropene BRL10061{2-6trans-1.3-Dicitoropropene BRL100-41-4 Eth),jbenzal6 BRLE/6&3 Hexachlorobut€diene BRL591-78-€ 2-Hexanone (MBK) BRL90-82{ lsopropylbenzene BRLs{7{ +lsopropyltoluene BRL163tog Methyl teft-butyl ehsr BRL10sr0-t 4-Methy'-2tentanon€(M|BK) BRL75{92 Methytene chloride BRL91.2G3 N€Dhthatene BRL1036$1 rFFropylb€nzene BRL

!g/l

psrpsnus4lig/l

tjs4uglplyl

uEl!Er

wl!gntrg/l!gl

psnpsnpgrpsn

!srfg l

pgtl

lJ9/l

Lrgl

!El

ps4

us/lps/lpg/l

wnpgn

vgltis/lvgtl!s/ps/l

l.,silWnuElus4ItEl

ldlpdl

pdl

psrpdlpsrpdlpsn

!c4!94

1 .020.o0_51.O1.0't .o

0.51 .02.O1 0 0

1 .01 01 05.01 .01_O2.O1 02.O1 .01 .0

2.O0.50.5't .0

r 0r 0

l 02 01 .01 .01,01 .01 01 .01 .0'1.0'1.0

0.50.51 00 510.0' 1 0

1.01 010.05.0't.0

1.0

1

1

l

1

1

1

1

1

1

1

1

1

1

1

l

l

1

I

1

1

1

1

1

1

1'I

I

I'|

1

1

1

I

I

I

I

I

1

I

I

'|

I

1

1

1

1

1

1

1

SW846 82608 22-Mat47 22-Mafi7 7031296 ek

This la.toralot! repo.l is nat uotid withou att aun odzett ignaturc on tlE cover p.tge

a Reportabl€ D€tection Limit BRL: Belotr Reporting Limit PaEe 62 of 124

Page 443: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 444: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samplc ldentificatiotrM8F-14 cwsA59517-13

Client Proiect #301-88

Mal xCround Wat€r

Collection Date/Timelg-Mar 07 00r00

Received20 Mar-07

CAS No. Atuttu(s) Fl"E *RDL Dilatbn .\Iethod ReI. PMparcd Anahaed Batch Anzlpl

Vobtilc Orgrnic Compounds

Voiatile &oanic Comoounds bv SW846 82608

Pr€parcd by method SW846 5030 Water MS

10rl-12-5 Styrene BRL63oe2l)-6 1.1,1,2-Tetrachloroethane BRL79{r4.s 1,j,2,2-Tetl.achloroethane BRL127-18r Tet?chloro€thene 8RL1lr8-88.3 Toluene BRL€7-61{ .1,2,3-Trichlorob€nzene BRL12l)€2-r l,2,4,Tdchtorobenzene BRL

7t{5€ 1,1,1_Tdchtd.oefhane SRL

7945 | ,1 .2-f tichlfoethane gRL

79{1{ T.ichloroeth€ne BRL

75.€9-4 T.ichlomfluorcmethane (Freon 1.t) BRL

96-1&4 l,2,lTrichtoroprcpane BRL95€96 1,2,+Trimethylbenzen€ BRL111847{ 1,3,5-Tfimethylbenz€n€ BRL75.o1-'r Vinylchloride1330'zl-7 m,p-Xylene95'474 o-Xylen€10+9$9 Tetrahydrofuranfl-2*7 Ethylether99+05{ Te -amyi methyl etier637-S?'3 Ethyttert-butytether10&zl1.3 D-isopropylelher754s Tert-Bulanol/ butyt alcohol12191.1 1,4-Diorane

S!fiogate rccovedes:4EYn4 4-Etomofluotobenzenem37.26-s Toluene4S17060a7 -o 1, 2-Dbhloroetha ne-d 4

BRLBRLBRLBRLBRLBRLBRLBRLBRLSRL

100101931001A6A-53-7

us4 1.0pS4 1.0

pg/l 0.5

ldr 1.0

ldr 1.0

!9/ l 1.0

!g/ l 1.0

fd l 1.0

pdt 1.o

!S/l 1.0

Ug/ l 1.0

pSl l 1.0

fdr 1.0

US/ l r .0

Lig/l L0

frdl 2 O

tJSll 1-0

pS/l 10-0

USfl 1.0

IiSll 1.0

LiS/l 1.0

Lig/l 1.0

!S/ l 100

rdt 20.0

70-t n Yo70-130 %70-t 30 %70-1m %

mg/l 0.1

lng/l 0.1

mg/l 0-1

mg/l 0 1

mg/l 0.1

mgn 0.1

mg/l 0.'!

mg/l 0.1

nW1 01

mg/l 0.1

4rr140 %

Fgr'| 0.0121

Fdr 0.0121

SW846 82608 22-Marol 22-Mal-07 7031296 ek

Ertrctable Petroleum Hydro.arbons

Extractable Total Petroleum HvdrocarbonsPrepared by method SW846 3510C

000+61-9 Gasoline6BrG3o-2 Firel Oil #26047+31-3 Flel Oil tl46055100-{ FiJel Oil tl6lr0g0o000o Motor oilJ0Ol00m0 Aviation Fuel

Unidentilied

Other OilTotal Peholeum HlrCrcca.bonsCgC36 Aliphatic l-lydrocarbons

Sunogale recoverbsi3,efr'a3-z l-ChhtoocladecEne

ScDivolrtlle Orgrric Compounds by GCOroanochh'.ioe Pesticides SW846 80814Pr€pared by merhod SW846 3510C

3O€{G2 Aldrin31+8+€ a-BHC

BRLBRLBRLBRLBRLBRL

BRLBRLBRLBRL

93

BRLBRL

+CTETPH 21-Mat47 22-Mat47 7031160 DS

SW846 8081A 22-Mar47 224'iaro7 7O3127O 7c

Thit lata.tury rcpod is ,tot eclid n ithot on a,tthoriz"l ig.tztxre o.t the cover pzge.

r R€portrble Detedion Limit BRL = Below Reporring Limit Page 6l of 124

Page 445: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarole ldeotificationM8F-l4 cWsA595t?-ll

Client P.oiect #30t-88

MatrixCroutrd Wat€.

Coll€ctiotr Date/Timet9-Mar{7 00:@

Received20-M8't-01

CAs No. AtuUuG) Fl4C 'RDL D ula,, Merhod ReJ Preryed Aaalwd Botch *talyst

Semivo|'lilc Orgrdc Compoutrds by cC

Oroanochlorine Pesticides SW846 8081APrepar€d by rnetEd SW846 3510C3i9S7 b-Bl{C319€C8 d-BHC5€{+e g-BHC (Lindane)57'74'9 Chbrdane72444 4,4-ODO (p,p)72-5+s 4,4-DDE (p,p')$-2g3 4,4-DDI(p,p')60-57-1 Dleldrin95998+ Endosullan I33213{5+ Endosultan l11031.0ru Eldosutfan sulfate72-mi Endinz2l€3-4 EndrlnAldehyde76-44{ Hoptachlor72415 M€thoxycilor1024-57-3 Heptachlor Epoxid€dx)r,392 Toxaphene51U:r-7r-9 a-Chlodan€5566-34-7 g_Cftbrdane5349+706 Endrin K€tone

Surogate Gcoveries:t t|3t'68a2 4,H)&Octduorobiptlenyj (54N51-2+3 Decachforobiphenyl(Sr)Polvcfilorinated Bioheflvis W SW846 8082Proparcd by merhod SW846 3510C1?674.11-2 Pcg 1016111o+tu2 Pcig l22l11i41-i€-s PCg 1232F,3168.214 PCg 12421m72-?9s PCB 12481r097€9r PCB 12541r09c826 PC8 126037324-2&5 PC8 tt62r1r0G14-1 PCB .t268

S{fiogrs[€ lgcov€rt€si1 0386-8+2 4,4o&Octaf, uorowony' (54e51-21-3 Dec5d otobipl7d.nf, (Si

SehivoLdle Oqrric Co|trDotrtrd, by CCMS

22-l.,€,r47 22-Mat47 ]a1270 rG8RLBRL8RLBRLBRLBRLgRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLERLBRL

107

BRLBRLBRIBRLBRLBRLBRLBRLBRL

60100

0.0r210.0't21o.01210.0606o.o1?10.0121o.0121o.00240.01210,0121

0.01210.0121o_01210.01210.0121o.o1210.{m060.0121o.01210.0121

r.'dlItsAps/|

!dl$sllpdl

rglp{

!dlgsfl

pdl

wpdl

uglggnpclpcr

flgl

us/|u€n

30-1fr %3+1fi%

Sw8,l6 80alA

sw846 8082

1

1

1

1

1

1

1

t

1

l

1

1

1

I

1

1

I

I

1

!snjJgl

trdlrgltlsilps/|pdl

t d lI'94

Fdl

tsr|tdlIrgrygl

t d lIrdlt d ludl

30-150 %3O-1fr%

[email protected]

r.000.4o01.00t.m|.001.00't.00

1.000:m

22]ln 47 23 4a(07 70/J1271

Se.nivolatile Oroanic Cdnpoonds bv SW846 OAZoCftepared by method S1w846 ?,510CA3i2-9 Acansphtbene2O&9+€ Aaer6phltryleneeo-12{ t-Meth/naphthalene62{33 Andine12D12.7 AnUrA€etre1912+4-9 AtEdfl€10133-3 Azobenzefl€/Diph€rryldieztuEm47-5 Beozidine56-553 B€nzo (a) aothrac€ne

z-MEt4l 224,.147 7031272 M.BSRLBRLBRLARLBRLBRL

BRLBRLBRL

sw846 8270C

ftb lab.@ry Epo.l b ,et valld withod o oa&arizd stgnattE oa t e cowr We_I R€ptrtable hection LiEit BRL = Below R€porting Linit Page 64 of 124

Page 446: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationllISF-14 cwsA59-517-ll

Client Proiect #30r -88

MatrixCround Water

Collection Date/Tim€l9-Mar-0? 00:00

Received?0-Mar-07

CAS N^ Aftaute(s) Fhs |RDL Dilution Method Retr. Prepared Analyzzd Ba.ch A tllstS€mivolafile Orgroic Compornds by GCMS

Semivolatile O.oanic Comoounds bv SWe46 8270CPrepared by method SW846 3510C

5OJ2{ Benzo (a) pyrene20+99-2 Eenzo (b) fluoranthene191-24-2 Benzo (g.h,i) perytenea7@ Benzo(k)fllorenthene65{5{ Benzoic acid100!51{ Benzylalmhol11i'9il Bis(2-dlloroethoxy)rnetharte11taa Bis(2-chloroethyl)et er3963&u-9 Bis(2-chloroisopropyt)etherr17{1-7 Bis(2€dlylhexyl)phthalareto1-55-3 +Bromophonyt pheny' ef|er85-6&7 BuVbenzytphthatate86.74-A C€rbazole59-50.7 4-Chtoro-3-rhethylph€nol1rl&47{ 4_Chtoroanilines1.5&7 2-Chtoronaphthalene9s-s7-€ 2_Chlorophenol700972'3 +Chlorophenyl phenyl ether218{1-9 Chrys€net3-70+ oibenzo (a,h) anthracenet32€4-9 Dibenzofuran95-5Gl 1,z-Dichlorobenzene54t73-1 1,3-Oachlorob€nz€ne106-a+7 1,4-Dicthlorob€rizene91€41 3,3'-Dichlorobenzidine12G&3.2 2,4-Dichlorophenola4€e2 oiethyiphthatate131.11-3 Dameth!4phhalate10s7-9 2,4-Dimethytphenolw-74-2 oi-n-butylphthatate53Fs2-i 4,GDinrto-z-methyjphenol51-4s 2,4.Dinfophenolr2'r-14-2 2,4-Dinatototuene60€-2G2 2,GDinitrololuene117{4-0 Di-n{ctylphtialate2014{ FluorantheneE+717 Ffuor€n€11&7+1 HexaclrlorobenzeneE7€&3 Hexachlorobutadienen474 Hexachlorocfctopentadiene67-f2-1 Hexachloro€thene19139-5 Indeno (1,2,3-cd) Py.ene78-59--1 lsophoaone91€7{ 2-Methylnaphthat€ne9s-4{-7 2-ilethytphenol

10839"{, 3,4-Meth}lphenol106-{4{91-20-3 Mphth€lene@-714 Z-Nitroaniline9S{$2 }Nitroaniline1OrL0r4 +Nilroaniline

BRLBRL8RLBRLBRLBRLBRLBRLBRL

8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLgRL

BRLBRLBRLBRL8RLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRL

BRLBRLSRL

ttgl 0 200

!9r 0.200

US/l 1.(10

!S/l 0.300

pdl 1.00

lSn 1.00

pdl 1.00

pg/l 1.00

Ug/l I 00

ug/l 1.00

pg/l 1.00

!g/ l 1.00

ld l 100

lSn 1.00

lid! 1.0O

ldl 1.00

!g/r 1.00

pgt 1.(m

lgn 100

IS/l 0-200

W.il L00

ldl 1.00

[gl 1-00

pSn 1.00

LISI 1.00

liSI 1.00

!g/l 1.00

p d r 1 0 0

!S/l 1.00

tiS/l 1.00

rc/l 1.00

pg/ l 100

pS/l 1.00

ld l 1-00

pS[ 1.00

ld l 1.00

Ugl 1.00

ps/| 1.00

pSI 0.600

!9n 1-00

!9,f1 1.0O

!S/l 0.200

|JS{ ton

Ug/l 1.0O

lgn 1.00

tgn 10.0

Ugll 1.00

Itgtt LoO

t g l ' l . to

pdl 1.00

1

1

1

1

1

1

I

1

1

1

1

1

1

1

1

1

1

1

1

1

I

1

I

I

1

1

1

1,1

,1

1'|I

1

I

I

1

1

1

1

1

1

I

1

1

1

1

1'|

This labofalory rcpod k nol wlid tlithod an atdro.taed signaturc on tha cover page .

' Reporlable Detection Limit BRL = Below ReDorrine Limit Page 65 of 124

Page 447: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificationM8F-14 GWsA595l7-13

Client Proiect #301-88

MatrixGrotrod Water

Cotleotioo Date/Timel9-Mar47 00:fi)

Reo€ived20-Mar47

CAS No- AEzly.a(s) Ft"s *nDL Diluioa Method Retr. Prcpared Anzlwd Botrh Aaalpz

Semilolrdle Orgrnic Compoutrds by GCMSSemivdalile Orqanic Comoounds bv SW846 B27OCPrepa.ed by method SW846 3510Cs&9s-3 Nitrobenzene8a-7t5 2-Nibophenol100-02-7 +Nitophenol62-7s9 N-Nitrosodirnethyamine621-€4-7 t+Nitr6odin-propylamine€6-30{ N-Mtrloodiph€nytsmine87€6-5 Pentachloroph€nol8541{ Phenanthren€loerSs-2 Plienol129-110{ Pyrene110{6-1 Pyrltine1&u-1 1,2,+Trichlorgbenzene9545-4 2,4,tTddorcphcnol8a+2 23,6-Tddtloophonol

Suftogale ,Bcovotles:321a0a 2+tuorobhhqf367-124 z+luuophenol11C,a,e4 Nit ofuftene4jar65-62.2 Flt€noks1718-514 lerphenyl4!411e-m-6 2,4,6TthronophendSVOCS bv SW846 8270C SIMPreparod by method SW846 3510C8c32-9 Acsmphfi€n€

2084e8 Acenaphthylen€9G12{ l-l\t€thytnsphthalene120n2'7 Anthiaceness55-3 BerEo (a) anthracene5G32,a B€nzo (a) pyfone20+99.2 Beruo (b) f uora{l€ne1e1.24-2 gerEo (g,h,i) perytene207fi-9 B€nzo (k) nuoi-anttEn€21S-01{ Ckys€nes3.7G3 Dib€auo (a,h) anlhaaoene20fF44-o Fludanthene&717 F|uorene193.3s-5 hdeno (1.2,3-cd) pyrenee1-s7{ 2-Melhylnaphihatene91-a!3 Naphthaldne85{1{ Phefianthrene129{0{ PyrorE

Surmgsfu rEcowatasl32tes 2+hlotobiphanyl17t8-5tQ Terphenyl44

Tord Metsls by EPA 6m0/r000 S€der Method!

BRL

BRLBRLBRL

BRI-BRLBRLBRLBRLBRLBRLBRLBRLBRL

70

8060u

BRL

BRLBRLBRL0.425BRLo.7620.7380.6500.500ARL0.9t2BRL0,600BRLARL0-3500.850

BRL

0_(X)70

0.0096

Wl l.oo

USi t.oopdl 1.00pgn 1-00

t 94 1-00pSI 1.00pCI 1.00

Fdl t.00

ugt 1_00

FCI 1.00

FSd 1.00

FS/l ',1.00

Vdt 1.0o

tdl 1-oo

30-130 %1+110%3tr1f i%tun, %30-130.t1&1 tO %

USn 0.050

ldl o.o5o

Fdr 0.050

uil 0.050

Wt o.o5o

F94 0.050

Psil o.o5ogn 0.050

tgll 0-050pSi O.O5O

ttgJt 0.050pgt 0.050

ldl 0.050

ldl 0.050pgn O-05O

lsn o.o5opdr 0.050

30-130 %30-130 %

fltSrl 0.0050

"lq,l' 0.m40

n'Sn 0.0050

SW8468270C 22-ttat47 ?I2-*lat47 rOXl272 M.g

1lgil zflr,lar-07

1

1'|t

t

1

1

I

1

I

l

1

I'|

1

1

7lt ().22-4 Sitver

Z4{}382 Arcenic

7140393 Badum

I

1

1

SW846 60108 264af4f 2auat47 t13t413 LR

Thit bbordory .eprr is tnt ealil Nithou afi outLoriz.d sagrrotu. or. th. coyer page .'R€podable Det€ction LiEil BRL = Bclow Reporting Limia Page ffi ot 124

Page 448: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldenrificatiorM8F-r4 cwsA595 t7- l3

Client Proiect #l 0 l - 88

MatrixGround Water

Colledion Datc/Timel9-Mar47 00:00

Received20-Mar-07

CAS No. Aaab@k) Resdl Flag Unla "RDL D anon I4ethod ReJ Prepued Awlyed Batch Analrst

Totrl M€tits by EPA 6000/?000 Series Methods

74.4u-43-9 Cadmium

7ll40{7-3 Chromium

7439'92-! Lead

282-4$2 Selenium

Totd Merrls by EPA 200 seri€s Methods

7a3+976 MErcury

2&Mat-07 26-Mat47 7031413 LR

26-Mar{7 27-t!,laF07 7031414 YP

0.0048

15.7

BRL

BRL

0.00026

mgn

nEI

mgn

mdl

mgn

0.0025

0.0050

0.0075

0.0150

0.m020

sw846 60108

EP4,245.1t7 4704

This ttborarory Eport h dat volid wilttot/l an aUhodaeil signarure od thz cover prge-

r Reponable Detection Limit BRL = Below Reportine Limit PaZe 67 of 124

Page 449: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 450: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samplc IdentificationM$F-24 GWsA5964l- 17

Client Project #301 -88

MatrixCround Water

Collection Date/Time?l -Mar-07 00:00

Received2?-Mar-0'l

C"'tS Na An yt(s) Result Flag Unia 'RDL Diluttun Method Rel. Prepare.d Analyted Batch Adallsl

Volrdle Otglnic Compounds

Volatile Orqanic Comoounds bv SW846 82608

Prepa,ed by m€thod SW846 5030 Water MS

76-i11 1,1,2-Tdchtorotdfuoroethane(FreoERL

67{+1 Acetone BRL

107-13-1 Ao.ylonitrilo BRL

7143.2 B€nzene BRL

10&8S1 Bromobenzene BRL

7+97.5 Brornochtorcmethane BRL

7s-274 Brormdichtoromelhane BRL

l+2+2 Bromoform BRL7,t{}9 BrooEmethane ARL

78-913 2-Butianone (MEK) BRf

104-5r{ n-Bulylbenzene ERL

135-9€€ sec-gutylbenzen€ BRL

9€{)6-6 tert,Butylbenzene BRL

TaFi+o carbon disutfide BRL

&2X5 Carbon tefachloride BRL10&90.r chtofobenzene BRL7540-3 Chloroethane BRL6746-3 Chloroform BRL744r-3 Chtoromethane BRL9s"49-8 2-Chlorototuene BRL

1OH3-4 +Chtomtolu€ne BRL

96-12{,1,2-Oibromo.3_chlorcpropane BRL

124-€-1 Dibrcmochlorom€hene BRL

10c93-{ 1,2-Oibromoethane (EDB) BRL

74€t3 Dibromomethane ARL

95.5}1 1,2-Oichlorobenzene 8RL

541-731 1,3-Dichlorobenzene BRL

10ffi.7 1,+Dichlofobenzene BRL

75-714 Dichlorodiffuoromehane(Freon12)BRL75-343 l.l-Dichlorcethane BRL1074G? l,2-Dichloro€thane BRL793tt l,l_Dichtorceth€rne BRL

1a)sss.2 cjs-1,2-Dichloroethene BRL

15G60.5 tans-1,2-Dichloro€lhene BRL

78{7-5 l,2-Dichloropropane BRL

142-28.9 i,3-Dichlompropane BRL

594-2C7 2,2-oichlorcpropane ARL

56+58{ l,j-oichloroprop€ne BRL

1006i{1-5 cis- l,3oichloroprcp€ne BRL

10061-02{trans-1,3-Dichloropropene BRL

10{F414 Ehylbenzene BRL

876&3 tl,exachlorobutadiene BRL

$1-7&6 2-Hexanone (MBK) BRL

98{2{ lsopropylbenzsne ARL

99{7{ +lsopropyltoluen€ BRL

1634+1-4 Methyl tert-butytether BRL

10+10-1 +Methyt-2-pentanone(MtBK) BRL

75{92 i etfrylene chloride ARL

BRL8RL

|lglpgl

vgtl

ug,ItEl

trdl

lrEl

rEl!9rpql

pgl

r./!yl

!s/l

v9p9ntrglpg/l

ttstl

usn!g/l

ugrus,4usnpsn

us4psn

!91

!s/1

!sl

!91

!gnpq/l

pgn

Lis/l

!jsnpgl

Ljgl

!s/l

us/lt /g l

Ljgl

!sruglugl!sn!s{utyl!gltr9lLtEl

1 .0

20.o0.51.01 .01 .0

0.51 .02.Q.t 0_0t_01_01 .05.01.01.02.O1 02.O1 .0't .0

2.O0.50.51 .01 .01 .01 .02.O1 .0t . ot . 01_01 .0t . 0' t .0

1_01 .00.50.51_0

0.510.01 .01.01 .010.05.01 01 .0

SW846 82608 27-Mat47 27^1,3'47 7031617 RLJ

9r-2G3 Naphthalene10!65-1 n+ropylbenzene

This labo4tnry repod is na, volU withost M aathodzed sigalarc ofi tha covcr page .

' Reportable Detection l-imit BRL = B€low ReportinC Limit Page 85 of 165

Page 451: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sahple IdentificationMtF-24 GWsAs964l - l7

Ciiedt Proiect #301-88

MatrixGround Water

Collectioo Date/Time2l-Mar-07 00:00

Received22-MarO7

CAS No. Anabu(s) ncs/,L FI"C 'RDL Dih tion Llethid netr, Prcponl Aaalyzd Bdch Anal8

Voladl€ OrgAnic CoorpoundJ

Voiatile Orqanic Comoounds bv SW846 82608Prepared by metiod SW846 5030 Water MS

BRLBRLBRLBRLBRLBRLBRL8RLBRLBRL

15€9,4 Trictiorolluoromethane {Freon tl) BRL

10l}'ll2-S StyBne63c20{ 1.1.1,2-Tetrachloroethane79.3tr-5 | , 1 ,2,2-Tetrachloroethane127-1€-4 TetrachlofO'€thene108{a-3 Toluenee7{r{ 1,2.3-fiichlorobenzenerZG€2-1 1.2,4-Trichlorobenzen€71-sfi 1,|,1-Tdchtom€rhane79{0-5 1,I,2-Tddlloro€hane79-01{ Triahloroethen€

t,(yl

uslygl

psnttgl

usnusrudl!dl

rcn|l9/l

9gl

ps4

rcnustpdl

!c4!gltglttgll

tdl$npsnpdl

t . 0t.00_5't.0

1.01.0'1.0

1 .0t . 0t . 0

1 .01 .0

1_0'1.0

1.02.01.010_0t_01.01.01 .010.0

20.o

0.0' 4oo l r4

1

1

1

1

I

I

I

t,l

1

1

1

1

I

I

I

I

1

I

1

I

1

I

I

9O-1e-4 1,2,3-Tddtloropropane95-63{ |,2,4Taim€thytbenzene10€-67{ l,3,tTaimethytb€nzene75{r-4 vinytchhride1330-20.7 m,pxylen€964?6 o-Xylene10s99€ Tsfahydrofuran60-2+7 Ethyl einer994{5+ Tert-amyt nreth}'l ehea637-92-3 Ethyt tert-butyl ether10&20'3 O--isoprop/ etf|€r756!0 Tert-Butanol/ bu!y' alcDhol13-91n 1,4-Dio(ane

Srrtrtugate ftcoveties:1160-004 +Bmnoauorobenzenefi37-26-S fdueneiS1 70at0-o74 t, 2-Dbl lotuethane44186&59? DibrorDofuororne{hane

Exlrrctsble PeFoleoh llydrocadors

Extractable Total Pet oleum HvdrocarbonsPrepaed by rnothod SW846 3510C€006-6t-g Gasolin€6€47+30-2 Fuel Oil #26E47+31-3 Fuel Oil tt468553{0-4 Fuel Oil #6m980m00 Motor Oil,()0100000 Aviation Fuel

unidenlifiedOtlEr OilTotal P€foleum Hydro€rbonsC€{36 Aliphatic Hydrocarbons

Sunogata rccovedas:31863x2 l-Chlomocladecat:€

SemivobalL Oryatric Compourds by cC

O.oaoochlorlne Pesticides SW846 8081APrepar€d by mehod SW846 3510C

[email protected] Aldrin319€46 a-BHC

+CT ETPH 26-Mar-07 20{lar{7 7031505 DS

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

94102106105

BRLBRLBRLBRL

SRL8RL1.0Calculated as1 .0

1 .0

BRLBRL

|llgil 0.1

ftqA 0.1

mSn 0.1

ordl 0_1

mg/l 0.1

mgl 0,1

mgr'I 0.1

mgl 0.1

mSn 0.1

msr 0.1

40-140 %

|'|gn|ls4

7O-tW%70,1fr %TGtn %7G130 %

SW846 80814 26l,,,d47 26-Met47 7031497 TG

Thit labonlory reporlls Fol rsu w hoA aa ouhod.ry' sisttz!,tE oE lhe cow. pagc.

' Reporbblc Ddecrion Linir BRL = Belos, Repodng Limit PagE 86 of 165

Page 452: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ ldentificationM8F-24 GwsA59641- 17

Client Proiect #l0l-88

MatrixG.ound Wafef

Collection Date/Time2l-MaF07 00:n

Received22-lr(ar-I7

CAS Na. A,'alru(s) Resuh Floq Ania *RDL Dilution Prcpored AntlFed Batch AnalystSemivolrdle Orgahic Compornds by cC

Omanochlorine Pesticides SW846 8O8lAPrepa.ed by method SW846 3510C

319{5-7 bts8Ho319r6J d.BHcs€{ss 0-BHC (Lindane)

5f-7+9 Chlordane72-s44 4,4'.ODD (p,p.)72{+s 4,4.-DDE (p,p.)5o-2s3 4,41DDT (p,p')60{7-1 DieldrinS5998{ Endosutfun I33213-65-9 Endosutfan fi1031{7.8 Endosu|lanSulfatef2-?ca Endrin7421+$.4 EndrinAldehyde76-44-€ Heptachlor124+5 Methoxyd.tlor10245r-3 Heptachto. Epoxid€[email protected]$2 Toxaphene

5103.71.9 a-chlodane55€€.34-7 g_Chlordane

s3494-7$5 Endrin Ketone

Suarogate recor€r-es:

10386842 4lD$Ocbnuorcbiphenyt (Si2o51-2a3 DecAchlotobiphenyl (Sr)

Polvchlorinated Biphenvls bv SW84ti 8082Propared by method SW846 351 OC

1267+11-2 PCB 10161110+28-2 PCB 12211114r-rc5 PCB 12325346s21,e PcB 124212672-84 PCB 12491r09749.i PCB 125411006-826 PCB 12603741-ZI5 PCB 126j211100.144 PCB 1268

Sr.rnogale a€covereslto38&8+2 4,+Dgoctaftuoroblphenyt (Sr)

mst.2L3 Decachtotohiphenyt l$r)

Semlvolaiile Orgrnic Compound6 by CCMS

8RLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRL

5699

BRLBRLBRLARLSRLBRLSRLBRLARL

6090

BRLBRLBRLBRLBRLBRLBRLBRLBRL

!s/lpgn

ug/lp!yl

ll91psyl

!gn!gnusnusnu9ntrs,'lLig/lLj9lp9I

tr(yl

us/tpg/l

pg/l

lig/l

30-150 %30-150 %

3G150 %

30-150 %

0 0 1 1 4 1

0-0114 1

0.0114 1

0.0571 1

0-0114 1

0.0114 1

0_0114 I

0.0023 |

0 0 1 1 4 I

0.0114 1

0_0114 1

0.0114 I

0.0114 1

0.0114 1

o.o114 1

0.0114 1

0.0571 1

0.0114 I

0 . 0 1 1 4 1

0 . 0 1 1 4 1

oo229 1o.o229 I0.0229 10-0229 100229 10.0225 10.022s 10.022s 1o.o229 1

't.00 10.400 11.00 11.00 11.00 11.00 11.00 11.00 1

0.200 1

SW8468081A 26-tlar{7 26,Mar{7 7031497 TG

Sw846 8082 26-MaF07 26-Mar-07 7031496 SM!g/l

!s4pg.4

plyl

pg/l

pgrl

pg/l

Lj{yl

ugal

Semivolalile Oroanic Comoounds bv SWg46 8270CPrepared by method SW846 3510C

63-32.9 Acenaphthene2oe96€ Acenaphthylene

cF12{ l-irethytnaphthalene

@-533 Anilinel2O-12-7 AntliEcene1912-2+9 Alrazine103333 Azobenzene/Diphenyldiazines2{7.s Benzidine56-5+ii Benzo(6)enthracene

rc4u9n!94pglpg4

ug/ltrsflpEtpgn

SW846 8270C 2f,-Mat47 29.ir'tat47 7031499 M.B

Thb labotuloq rcpod is ,rna vrlid wiatour aa tshorlzed slgnttttrc ott the are? page.

' Reportable D€t€ction Limit BRL = Betow Reponing Limit Page 87 of 165

Page 453: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdefltifrcationM8F-24 cWsA5964l - 17

Cliedt Proiect #301-8E

MatrixCrouDd Watea

Callectioo Date/Time2 I -Mar-07 00:00

Received22-Mar47

CAS No. Aaalylz(s) Fhs *RDL Dilation lnefiod Rel. Prcparcd Analyzed Borch Analyst

Semlvolrtll€ Orgrnlc Compourdr by CCMS

Semavolatile Oroanic Comoounds bv SW846 8270CPrepar€d by method SW846 3510C5{}s2{ A€nzo (a)pyren€m5s2 Benzo (b) fluorenthene1ei-24-2 B€rEo (g,h,D p€rytenea)7-08-9 genzo (k) fuoran{hene65-85,0 Benzoic acid10Gs1€ Benzy{ alcoholi1r41n EIs(2-ohlorcethoxy)methane11laaa Bis(2-d{o.oehyl)€trer3S63e324 Bis(2dtloroisopmpyl)ether11731-7 Bis(2-ehylheryl)ph&atate101'55-3 +Bornophenylphenylether956€-7 BuV b€|1ryl phthalat€86-7,1{ Carbezole59-5+7 4chlom_$rnethylph€nol10H7+ 4chtorcanitine91'5&7 2-Chloronaphthalene0557-8 2-Chlorophenol7005-72-3 +chloophenyt phenyl ethef218-01-9 Chrys€neS3-70-3 Dibenzo (a,h) anthracone13?{,r-9 Oib€nzofuran95-5G1 l,z-Dichtorobenzene541-73-1 1,3-Oichtofobenzen€106-4{i-7 1,.1-Dh.htorobenzens9r-9+1 3,3loichtorobenzijine120-83-2 2,4-Didilorophenolu&2 Di€thyi phth2late131-11n Dim€fltphthatate10s-67-e 2,+Dimethytph€nolu-7+2 O-n{ut)y'phthalato$4-52n 4,6-Dlnitrc-2-methytph€nots1-2+5 z,4oinitrophenol121n4-2 2,+Dinitotoluene60e20-2 2,6-Dinibotoluener | 744.0 Di-n-odyl phthatate206-44-{' Fluoranthene86-73-7 Fluofene11&7+1 Hexacfllorobenzene€7-6E-3 l-bxadtlorobltadiene17471 HexachloocyclopentiadieneA7-72-1 Hexachtoroethane1ess5 Indeno (t,2,3d) pyfen€78.69-t lsophorone9l{7{ 2-Methylnaphthal€ne95-48-7 2-Mehy'phonol10e.39.4. 3,+Methy,bhenol106-{4691-2G3 Naphth6tene&f 44 2-Nitroanitine9!rc92 3-NitrDanitineroo-ih€ +Nikoanl n€

SW8468270C 26-Mar.07 2+Mar-07 7081499 M-BBRLBRLBRL

BRLBRLARLBRLBRL8RLBRLBRL8RfBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLERLARLBRLBRL

BRLBRLBRLBRL

vgllsnp{n

us4!srt/grt'dlt g/l

!st!dlt /g l

psn!snpdt

!dlugnpdl!sitpcn

!dlrglpdl

psil

pdl

!dl

uEl

1lql

trlyl

uc4!dl

!tyl

!dl

wlp{rnu4lugluglls/lpc4

udluglgr

ps4

us4udlwn

1lgl

t,gll

Fdl

PSA

0.2000:001.00

0.3001.O01.001 .m1.00

1.00'1.00

1.001.(f01.00

1.001.001.001.001_001_00

0.2m1.(X)

1.00r.001.001.00r.001.001.001.001.001.001.00r_001.001.001.00|.001.00

0.600'1,00

1.0002001.001.001.OO10.0

|.00't.ff)

1.001.00

':hls lefurorarf plfi it not valld toithost an au[tori?A tigttant e on tha caee? pg.

' Repodrble Det€ction Limit BRL = Below R€portinS Linit Pagc 8E of 155

Page 454: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationMEF.24 GWs4596,{ I - I7

Cliert Proiecr #301 -88

MatrixCround Water

Collcction Date/Time2l-Mar 07 00:00

Received22-Mar01

CAS No. Anolye(r) Resan Fhc "RDL Dilutian Mahod Retr, Preparcd Anabzed B ch Analpt

S€mtvolrtil€ Orgsntc Compoun& b!, CCMS

Sernivolatile Orqanic Comoounds bv SW846 8270CPrepared by melhod SW846 3510C

98-9t3 Nilrobenzene88,7t5 2-Nitrophenol100{2.7 +Nilrophenol

@.7$9 N-Nitrosodimethylamine

62164-7 it-Nttrosodi_n_propylamine

86-30$ N-Nitrosodiphenylamine87{65 Pentachlorophenol

s5-014 Phenanthrenei0&95-? Phenol

12940{ Pyrene

ri046-1 Pyridine12G62-l 1,2,4-Trichlorobenz€ne9+95,1 2,4,$Trichlorophenol8O{e2 z,4,GTrichlorophenot

Suzogate recoue4es.

32140-E 2-Fluorobiphenyt

367.124 2-Fluorcphenol

416&604 Mlrobenzene4'

416+62-2 Phenol4'

t7t&5t4 Terphenyl4l4

118-79-6 2,4,ETibmmophenol

SVOCS bv SW8a6 8270C StM

Prepared by method SW846 3510C

83.32-9 Acenaphthene

20&96{ Acenaphthylene90-r24 1-lilethylnaphthaten€l2Gr2-7 Anlhracene

56.5!3 EerEo (a) anth.acer€5G324 Benzo (a) py.ene

205-99? BerEo (b) fluoranthene191-?4-? B€nzo (g,h,i) perytenem7.084 Eenzo (k) fluoranthene218.O1-S Chrys€n€53-7G3 Dibenb (a,h) anthraceneA16-44-{l Fluoranthene8,J'73.7 Fluoaene19s.395 Indeno (1,2,3_cd) pyrene91.574 2-Mgthylnaphthatene91.20"3 Naphthelene85-014 Phenanthr€ne129{0{ Pyaen€

Sunogate rccovedes:321.tu8 2-Fluorobiphenyl

r719'5t4 Tetphonyl4l4

Tot l Metrls by EPA 60o0t000 Series Merhods

26-Mar47 29-MaF07 703149S M.BBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

747568679360

BRL

BRLSRLBRLBRLBRLBRLBRLBRLBRLBRLo.271BRLBRLARLARLBRL0.400

8292

pS/l 1.00

pg/l 1.00

pdl 1.0o

!S/l '1.00

lSn 1.00

US/l 1.00

pS/l 1-00

pg/ l 100

!S/ l 100

rc/l 1-00

US,4 1.00

USn 1-00pSn 1.00pS4 1.00

m- lm%1&flOot30-tm%| 5-110 %3G130 %| 5-110 %

!S/l 0.050

trS/l 0 050

US/l 0.050pdl 0.0s0pg/l 0.050pSn 0.050

trS/l 0.05t)pdr 0.050pg/r 0.050pglt o.o5opg/l 0.050pgll 0.050pg/r 0.050pgtt 0.050pglt 0.050pg/l o.o5opg/l 0.050pdl 0.050

30'130 %30-1n%

n1p,4 0.0300

mS4 0.fiX0

m9/ 0.0O5O

1 SW846 8270C

t "' t '

1 '

1 '' t "

1 "

1 "

1 "'1 '

1 '

1 '

I sw846 8270C/EPA625 S \4

2a-Ma?Ol

l44O-224 Silver

7ll4G38-2 Arsenic

74{}3$3 Barium

ARL

BRL

o.276

SW8.t6 60108 28)1afi7 2*tefi7 7O316n HB

This hbonlory rcpofl ls rrot valtd toltho,/r' on authodrzd sigtatarc on E cote. page

1 Reportable Deleclion Limit BRL = Below Reportjng Limi( Page E9 of | 65

Page 455: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarpple ldentificationM8F-24 GWsA59641. r7

Cli€nt Proiect #t0l-88

MatrixGroudd Water

Collection Date/fime2 I -Mar-o? 00:00

Recaived22-Mar-07

CAS No. An&lyk(s) Resalt Flag Ani6 *RDL D ctlarl tte.hod Rel. PEFarul Analtz.d Bdch At 4lfst

Totrl M€trls by EPA 6m0/7000 S€rle! Meahods

7440-4+9 C€dmium gRL

Taao-a7-3 Chromium 0.0079

743+92-1 Lead 8RL

282.4s2 S€lenium BRL

Total Mclrb by EPA 2m Srri€s Methods

7€947.6 Mercury O.O0221

SW846 60108 28-l ar.07 28-lrlar-07 7031677 HB.rr9[

nrgn

.run

flI4n

fitdt

0.0025

0.0050

0.0075

0.0150

0 00020

1

I

1

I

EPA245.|T/47OA 28-Ma(41 ?f'-lttat47 7m167S YP

7W l4bdoq npoa ls naa vzlid xfrtou aa asrtariaed signztare on th. @!e. pqe -

* Reporrable Der€ctioD Limit BRL = B€loq, Reponing Limit Page 90 of | 55

Page 456: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentiftcationM8F-42 GwsA59803-18

Client Proiect #l0 r-88

MatrixGround Water

Collection Date/Time26-Mar-07 00:00

Received2'7 -Mar-07

CAS N^ Analrte(s) Resuk Fl"S Unia *RDL Dilutiort Method Rel. Prepoted Ahary.ed Batch Analyst

Vol.tile Ory{!ic Compounds

Volalilo Oroanic Cornoourds bv SW846 82608

Prepared by method SW846 5030 Water MS

76.rsn 1,12-TrichlootriflLrroe&anslFr€on 8RL6r.6,t1 Acelone BRL107 M Ady'orx1r'te BRLnrt$2 Benzene BRt108'86-1 Emmob€nzene gRL

74-97-5 Bromod oromelhane 8RL15.271 BEmodichtorometharE BRL15.212 Brcmoform BFL7l€€ Bro,nomehane gRL

78.$n 2-Buranffe (MEK) BRL10+st.0 ft&ltyhenzene BFL135-9&0 se.-Butylbenzene BFL90{66 En-Butyibenzene BFL7$154 Carbon disrlfide BffL*&5 Cafton t€trachloride BRL10s!ro-7 chloobenz€ne BBL7540.3 Chloioeftane BRLrfiG3 Chlorolom BRL7447-3 Chlo,o.tethane gRL

95-4!10 2-chtoolotrjene BRL106.43-4 4{hlootoluene 8RL96r2.s t,2-Djbromo-3dtDropropane gRL

12441 Dibrornodtorornelhane 8RL106'93-4 1,2-fibfomoelhane (EoB) 8RL74453 Dibrornomeihane 8RL550.1 1,2-Dd orob€nzene 8RL511-7?1 1,3.O{drlsrobenzene 8FL1m-467 1,4-Uchlorob€nzene BRL871 8 Ddlorodi(uord'nethane (Fr€on1z) BRLE*3 |,l-Dchloroethane 8fu107{rG2 1 2,oichloroethane 8RLi53H 1,1-Ociloroethene BRL156'5s2 cls-t,2-Dkt o{oelhene BRL156 6G5 tans-1,2-0ichlo(oelhene 8RLn'87.5 1,2-0id o{upopane 8fu14229s 1+CId oroflopane Bfus94,2(}7 2,2.0i$loropropane BRLs6+s84 I 1-Ochtoropropene 8RL1q)614r.5 cis-1,3-DidltorcFropene 8RL10061{2{ ta1s-1,3-0hhlooprop€ie 8RL100.11{ Eht6enzene 8RLEr6s3 ftexachloobutadiene 8RL

pg/l

u94pcn

!snp9l

lr],1!!/l

!91

!94

!s4p

Wn!snrqlsnwPEtvlpsl

P9lp94

tlSll

!srl

!s4

tjs4

!s4psl

u94

u94

ust!c4!olp9!

u9lult!91psn

!c4p91

!94f9l!s.4t41!s4!s4!slfs4!s4!snw

1.0

20.0

0.5

1.0

1 . 0

1 . 0

0.5

1 . 0

2.0

1 0 0' t0

1.0

t 0

5 0

t 0

1.0

2.0

l_0

2.0

l 0

1 0

2.0

0 5

0 5

t 0

t 0

LD

t.0

2.0

t .0

1 . 0

t 0

1 . 0

1 0

1.0

t . 0

1.0

1 . 0

0.5

0 5

r.00 5

1 0 0

1.0

r 0l 0

100

5.0

l 0

t 0

sw846 82608 29lrarO7 *Ma'41 7031197 n!

59t 78-6 z-Hexanone (M8KJ

F{Z-o h{popylbenzene99S?t 0tsopropy,itoluene1604-0/14 Metrylle(-butylelher10€ rG1 +Methyl-2tenlanone (M8075n9.2 Metrytsnechtoride91.2$3 tkphhdale

lqt651 FPopylbenzene

8Rt8RLSRLBRLBRL

BRL8RL

€RL

Thh lahoftttory rcpod it nol wlU wAhout zn oulhofized signalare on the covct IMge .

+ Reportable Dereclion Limit BRL = B€low R€poiing Limit Pas€ 88 of 154

Page 457: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 458: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationMEF.42 GWsA5980l- 18

Client Proiect #l0l-88

MatrixGround Water

CoLlection Date/Time26-Mar-07 00:00

Reccivcd2'7-MaL01

CAS No. Andyte(s) nesuk Flog Uni$ 'RDL Dilation Merhod Re[. Prepa.ed AaalyTel Batch Aruryst

Volatil€ Org!ric Compounds

Vo{afle orqanic Comoounds bv SW846 82608PrepaEd by method SW846 5030 Water MS

100-{2.5 Styrene BFLdlG203 1,1,!2-Tellactlooethane BRL793{'s 1,1,2,2-Telrachloroethan€ 8RL1271M Tela*ioroefrene SRL100{s-! Tdlene 8RL3?61{ 1,2,}Trichloob€n2ene 8RL12!,82-1 1,2,4-Tri:hloroben2ene 8RL7t,55.6 1,1,1-Tdchtoroedrane 8RL79.{lG5 l,12-Triciloro€hane Sfu7!{ls Tri:hlorDelhene 8Rt75t94 Tdrhtorotluoromethane (FGon 1l) eRL96.18-4 1,2,3-TriEilomprcpane BRL

5605 1,2,4-Tdme$Vibenzene BRL108574 1,3,5-Trifl'€frylben?ene BRL?5{l-4 Vin},l chtoride BRLrd0.2o7 m,Pxy'€n€ BRL

547{ cxytene BRLl@9+S Tetr"ahydmluan

sG2l-7 Elhy' sher994{F0 Ted-amyl melhyl ehers37,gz 3 E$/ ten_hltyl elherl@2s3 Dijsopropyiether?5€54 T€rt-But not / bulyt alcoholra41n l,{-Doxane

LA@4 48tonbflwnJhenzene

2@7-?6-5 lduen*d8

tiwnl4 |,z'D6lorcetharc44

1@5+7 Dibrutolluorcmethane

Erf .ctsble Pelroleum Hydiocrrbons

Exllaclable Total Pefoleum fudrocabons

Prepared by method SW846 351 0C

Bm6-61-9 Gasoline

6E4763G2 Fueioilt2

6&l763rt FuelOit t46855+00"{ FudOB6

u0(|0e@0 Motoroil

J001O0C]0 A\ialion FUel

tlnideni{ed

Olher Ol

Total Petrolelm Hydrccarbons

C$C36 Aliphalic hydrcabons

W3?2 l4hlotoula&c e

Semivolslile Organic Componnds by cC

OEanodliodne Pesticid€s SW846 Prft1A

Prepared by melhod SW846 3510C

S9.00-2 Aldrin

39e!6 a-BHC

!g/l 1.0

lgn 1.0

!94 0.5

!E 1.0

!s.4 t_0

lSn 1.0

pE 1.0

ps/ L0

psn 1-0

fgn 10

ps4 1.0

ps4 r0

!S4 1.0

!s4 1.0

!S4 !-0

tSl 2.0

t)SA 1.0

Ugl 100

pgl 1.0

VSI l0

ps/l 1 0

t d I o

pSI 10.0

!s/l m0

70130 %

70t30 %

TGtg%

m1fi%

O I

0 . 1

0.1

0.1

0.1

o 1

0.1

0.r

O I

0.1

swE46 E26081

I

1

I

1

I

I

I

1

I

I

l

I

l

I

I

1

I

I

1

1

1

29-[far{7 ?gl{a]4l 7A31797 RU

101

108

1U

BRL

BRL

BRL

BRL

BFL

BflL

BfrL

SRL8RLBRLBRLBRLBRL8RL8BL8RLBRL

mqn

mg,l

mE

mgn

m94

mgn

mqn

mg,4

mq4

m94

4+1$%

+CT ErPH

sw8468081A

2giiaAi 30tta47 1031772

2$Mar{7 zg"Mar-{)7 7031768

9t)

BRLBRL

$4

M0.0130

0313t)

Thb bborutory rcport is not veld wilhout aE outhoized sig'natare oa the caver page.

* Reponable Derection Limir BRL = Below Reporting Limir Pase 89 of 154

Page 459: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SamplE Ide ificationM8F-42 GWsA59E0l-18

Client Proiect #301-EE

MatrixGround Water

Collection DatdTime26-Mar-07 00:00

Received2'l-MarO7

CAS No. At slru6) Fl4g UaAs rRDL Dil4llotr Mettod R.l: Pepored Aaqlgen $alch Adaltsl

Semivohtit€ Orgink Comporr& by CC

Oroanodllodne Peslicid€s SW846 eO81 A

Prepared by m€thod SW046 3510C

319{5-7 b€HC11!!06-0 +Bflc58.€e e gBrE (Lindar€)

t.?{ s ftbrbnen-$.6 44-000 (p"0,)

z.5re a,4-DD€ (p,p)

502s3 4,4OOT(p,p')6s5r,r Dieldin95$q€ 8 End6ulfan I3}213-664 Erddrllan ll10t107.8 Erdosuknsu(ate12?ljg Enddn7{21{3-r EndrinAhehyde7644 H€plact or724r-s Mghox}d{or1@4t3 Heplad or Eponde8001-3+2 TOxe{hsE5l0tl{ a-Chloftldls5655.91-7 g4htorde€53/|e47S5 Endin Keton€

1@&4+2 4,LDEMnwrMplHlyl(Sr)

n61.24!t Decm uobiplrEnyl(Si

Poh/.t odnated Eiohenvh bv Sw846 8082

Prepared by mebod SW8,l6 3510C

r?6/+11-2 PrCE 101611r04?s2 ICB 122.111r11- l6s t ,c8123250r692r-s PCB 1242126r2-2M PCB 12481109?69.1 PCB 1254

r10€e82-5 PCB 12m

r/!e+295 Pc81262rltoGt{-4 rcB 126{l

t@s+2 4,4.D8det@Miptpnl64

8ta+3 D€cedl ojilrrP{lyl (*)

S€mivolitil. Oryanlc Comportrd3 by GCMS

Semilola leorgd c Comoounds bv SW846 8270C

Prepa.ed by method SW846 351 0C

03-324 A.snapllflrgr€206.tt6-0 Arenaph$yleie9G12{ l.rrsrytnapitBlen€6e.5$3 fuilinot&12-f Anhrffin€t9\2-2+4 Al€:jn6ts-3+3 A:oh€nzeno/Dipn€nyttazine12-87.5 B€nzidines55F5 BeEo(a)anhrdcene

BNLBALBRLBFLBRLBF|-8RL8RLBALBFLBRLBRL8Fr-8RLB8tBFLBFLBRt8R_BRT

ljr!l

rylTE]lsn|lg4

!91

ts,l!g,l

tj91

Wlj$i

la4

t44

lsl

1,9r

|Jg/r

Mwldlps,l

*| fr%&tg

&150%

b-l50%

0u1300-013)0.01s0.06490.0t300_0t30031300_0026o0131)0.0i3)0.01300.0130001300 01300.01300.01300.06490.0130001300.0130

sw816 8081A

sua46 E082

sw846 €270C

Z{-Mar])7 29-llar{7 ?IB1768 IG

54

$'lpd

|jg4

Mts4wtlg4

!s4lgl

8Rr_8AL

BFL

BFL

BFL

8RrsR-BRL8RL

|4/l{grts4wltstNlttdltg4!s,

0.0260

o@60

0.86i)

0.860

0.0260

0.0260

0 0260

0.0260

om60

2g-llad? 2$Mar-07 703u69 SM

6090

8fl1BFLBRLBR-BntBRL

BAL8818nL

tgl

0.41D

1.00

1.mLm1tntI]0

1.m0.200

28-ilarc7 31.lraf{7 7C115$ M.S

fhls lab.alary zForl is aot ialid x'ithoat an.!.tho.iz?y' sigrafue on tc cowr pag..

+ RQoflablc Det€ctiod Limit BRL = B€tow Reportirg Lini. Paee 90 of 154

Page 460: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationM8F-f 2 GWsA59803-18

Client Proiect #301 -88

MatrixCround Water

Collection Date/Tipre26'Mar-07 00:00

Receive.d2'l -Mar-07

CAS No- Aaalye(s) FloC Unis +RDL Dilution Ptepared ArEUzed Batch Anslyrt

S€mivolatil€ Orgatric Compounds b) cCMS

Serhivolatt Ooanic Comoounds bv SW846 8270C

Prepared by method SW846 3510C

50-3?-8 oenzo(a)pyrene

26ss-2 Benzo(b)lluo|enhene191-2+2 &nzo (g,h,i) p€rytene

207{84 Banzo {k) ffuoanthene

B€nzaic acidu!51t B€nzyt atcohol11r-!r1-1 Ek(2{ito@thoxy)rne$ane111-.1.1-{ Bis(2dttoro€fv}elher39638.3p-9 Bis(2dttorcisopropyl)efEr11741-7 Bis(2-ehyhoxyl)phrhataE101-s53 +Bromophenylphenytelh€r

64 7 Bdl benzyl phhalale

8ri7'r-8 C€bazoles1l5c7 4-Chtorc3-melhlphe'1ot106{/3 4{hbromiline

s1.50-7 2{hloricmphthatenestr-8 2{hlorophenotftoS72'3 {{hlorophenyi phenyl ehet2r3{r€ Chrysene50'70.3 Dibenzo(a,h)anthrac€ne132-644 Dib€nzoluran9&501 l,2.Dichtorcb€nrene541.7+1 1,$oichlorobenEn€10e46-7 l,4-oichlorobsnzene9-9+1 3,3lDcitorobenzidn€120+a-2 2,+Dichtorophend8+6Gz oie$ylphlhalate131-1r-3 Dimlhylphlhatater0sr4 2,+Dine$ytphenolu.t+2 Di-n-butytphlhatale

l3+52'l 4,SDinito-2-n€lhytphffol

51.28.5 2,+Onitroph€not12t-1+2 2,4{iflitmhtu€ne

dG2G2 2"&Dmjtrototuse11t-&t0 Di{{dylphhataE2ll6-.!m Fuo€nlhen€t6.lJ.7 Buor€n€11EJ+1 Hexacltoob€nzen€87-Gt.3 HexachloDbuladj€nen't74 Hexacf{oocyclopentadi€nefl.n1 H€)acl{oost|ene1!F395 Indeno (1 ,2,3-rdJ pyrene,4.59n kophoones1.t.6 2-Methy,inafithaten€s-4!-7 z.llelhytph$ol

10s39-,1, ol.li,lffiylphenol106!i.591.2O3 I'laphbalen€

@74-l 2-Nitroaniline

F{F-z }Nitoanitiner0n{13 +l{lroanitine

BFL

BFL

BBL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

8RL

BRL

8Bt

BRL

BRL

8RL

BRL

8RL

BRL

BRL

BRL

BHL

BFL

BRL

8RL

BFL

8RL

8RL

BflL

BRL

BflL

BRL

BHL

BRL

BRL

8RL

BRL

BHL

BRL

BRL

8RL

8RL

BHL

8RL

BNL

BRL

SRL

8RL

8RL

8RL

0.2@

0.200

1.00

0.300

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$4

!94pc,!sn!sn!s4!94!dlwlps'l

trs4H,lrc/ltrs4!s4tjs4us4Wntlgl

|l9t

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PM!s,4!M

sw846 8270C 28 Mar{7 31 Mar{7 70316€0 M.B

This lfuorutory repon is not uolid withoat on aurtorized signaure on the corer page

* Reportable D€tectior Limir BRL = Below R€porting Limit Pas€ 9l of 154

Page 461: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldenti ficationM8F-42 GwsA59803-lE

Client Proj€ct #301-88

MatrixCrcund Water

Collection Dat€/Time26Mar-07 00:00

Received2'7-MarO1

CAS No. Analy@(s) Resuk FIag Aaib *RDL Dilution Mzthod Retr, heptzd A aqzed Balch Aulfst

Semivol.tll€ Orgrnic Comporn& by ffMS

S€mivolalio Ooanic ClrnoounG bv SWP,46 eB70C

Prepared by method SW846 3510C

!6-!153 Nibob€nz€ne

€E-?$5 2{,litoph$ol100{2.7 +Nitrcphenol

82-75-!r Ni,lhrocodlme$ylemine

621t47 |lMrosodi.n-pfopytemine

s.1n6 itNfosodiptErryhmine

87{6.5 Penhdbrophenol

ll5{114 Pi€na$rf€{le

l0&S+2 Phenoll2goiH PyrBne

llG€+1 h/ridne1aH2-l 1,2,4-TritoroDen2eie!6.9!1 2,4,5-Tddoopienol

0€{G2 2j,CT'ic$ofo$e0ol

e1@4 ?nwdnph$l

fi7r2r 2+luo@hstd

.J66j,4 ili6slzse4,

1166.6?-2 Pllp,tul4s

1rt&514 Terpnenyl.d4

1t&/ 2,4.6-Itbrdwttend

SVOCS bv SW846 8270C SIM

Prepared by method SW84.6 3510C

s32-9 Acomphhene

a,ssfi A.enaphbylone!s12-o t-M#ytnadtfiatenat@-127 Arliracen€5865.3 B€nlo(a)antnreerE5+32-S B€r'!o (aloyene

205s9? 8ffuo(b)fluor|1f|eng1s1-24-l 8€nzo(g,h,i)p€den€2074ss B€n:o(k)fiuoranhene2r0-r)r,9 chrys€n€53.?G3 oibenao (a,h) anhracdeaE.4,t{ HuoEnlhene

8t.797 Fluo|Erc

!B-3&5 trdeno(1,2,3-cd)py€ne

91-t.6 2.]Ueft'y'naphhetenes'-20'3 ihphthalene

F)1-8 PlEnanhem1290{ Pf6n€

S!1qSab ruvai:r

Q1a-8 ZRr,ollDifi'efl],l

1nc.514 Te$rllf,nyld4

BRTBNLBFLBRL8RL8RL8RLBqLBRLBRLBRLBRL8RLBNL

e759654

BNL

BFL8RLBRLBAL8fl18FLBFL8RL8FLBRLBFLBFLBRL

SRLBRLBRLBFL

p

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sw846 8270C

sw846 6ZI0C/EFA625 Sl[,

1

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Wil 0.05i0

tsl o.ll5l)

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wr oo5ovs| 0.060gS4 0.050

us, o.o5{)|ls4 oo$llg4 O05{)

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$ 0050

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sYi846 m10871,022.1 SlvE

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7{1+i}93 &dun

n,04

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0.u040

0.@50

3Girar{7 02.AF47 7001S23

Thit labonbrf reporl B not wUtI *tithost tA u.drorkd sE.eture on the cowr pzg..

i Reportable Detection Limit BRL = B€low R€porting Limit Pagegz of 154

Page 462: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationM8F42 GWsA5980l- 18

Client Proiect #301 -88

MatrixCround Watcr

Collection Date/Time26-Mar-07 00:00

Received27 -Mar-07

CAS No, Anal]te(s) Result Flat UniB 'NDL Dilutian Pnpand AruIrzed Ba.tch ldrlrst

Totrt Merrli by EpA 6000/7000 Series Methods

74ro-,r3-9 cadmium BRL

74rr0{7il chomium BFL

7'f39.92-r Led 0.0132

z&.432 S€ky[{D BRL

Tot l Mebls by EPA 200 S€ries Methods

743+97.6 M€rflry BRL EPA245-1114704 30-0,lar{7

m91

mg,l

mgr

mgn

0_0025

0.0050

0.0075

0.0150

0 00020

SWE4660108 30+lar-07 02-Apr{7 7031823 LR

ms4 02-A9rAt 7431424

Thir laboratory rcprl k ,tot rald plthou an sartoized sigazture on the cover ps|e-

' Reportable D€t€€tion Limit BRL = Below Reponing Limit Page 93 of 154

Page 463: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 464: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sanple IdentificationM8F-50GWs459,r64- l9

Clieot Proiect #30r-88

MatrixGround Water

Collection Date/Timel5-Mar47 00:00

Received

19-Mar-07

CAS No- Andr.e(s) Resuh Flag UniA *RDL Dilution Method ReJ Prepaied AntlfiEd Batch Atuttsl

Yohtile Orgrnic Compornds

Volatile Orqanic Compounds bv SW846 82608Prepared by method SW846 5030 Water MS76-111 1,1,2-Tricilorotrifluoroethan€(FreoERL674+l Acetone BRL107-13-1 Ao.ylonitrite BRLf11r2 Benzene BRL10&.861 Brornobenzene BRL74-97-5 Bromochloromethane BRL75-n4 Brornodichloromethane BRL7r2r2 grornoform 8RL7143-9 BrornorDethane BRL7&943 2-Butanone (irEK) BRL10+514 n-Butylbenzme BRL13f.98€ sec+utylbehzene BRLs€{€-6 tert-BrJtylbenzene BRL75.154 Carbon disutfide BRLs6.23.s Carbon tetachtodde BRLi0e9o.7 Chlorobenzene BRL75{0-3 Chloroehane BRL67{G3 Chlorofo.m BRL7{{7-3 Chloromethane BRL95-49-s 2-Chlorotoluene ARL106-43-4 4-Chlorotoluene BRL9&12-8 1,2-Dibromo-3-chloroprop€ne BRL12,88.1 Dibromochlofome$ane BRL10G93-4 l,2-Dibromoethane(EDB) BRL7445-3 Dibromonrelhane BRL9tre1 l,2_Dichtorobenzene BRLsi41.7+1 l,3-Dichlorobenzene BRL10646-7 1 ,4-Dl,c!\lotctbetuene BRL7t7r{ DichlorodiflUoromethane(Freon12)BRL7t3,F3 'l,l-Dichloro€thane BRL107-06-2 1.2-Dichlo(oethane BRL7t35-. l,|-Dichloroeth€ne BRL15e59'2 cis-'l ,2.Dichlo.oethene BRL15'6$05 h?ns-l,2.Oichloroethene BRL78€7-5 l,2-Dichlofopropane 8RL1112-2&9 l,3-Dichloropropane BRL59+m-7 2,2-Dichloropropane 8RL56!5+6 l,l-Dichlofopropene 8RL10061{l-5 cis- 1 ,3-Dichloropropene 6RLtoo6r{2$lrans-1,3-Dichloropropene BRL100414 Ethylbenzene BRL87€83 Hexachlorobutadiene BRL591.784 2-Hexanone (MBK) BRL98€2-8 lsopropylbenzene ARL99€7{ +lsopropyllotuene SRLt63141-4 Methyl teri-b{rb/ efter BRLi0&1(}r +Medryl-2-pentanone(M|BK) 8RL75{9-? Methylene chloride BRL

SW846 82604 21-Mat47 21-Maro7 7031185 ek

BRLBRL

uglusnpdlp94

!g,rl!91!91

!gnli9/l

Pg/lp9l

tr!yl

u(ylp!yl

ps/r

vgaugrt g l

t g l

ug/lpsn

!snvgtlrrgilttgllpsll

tgrltis/r!9/r!g/l

lrg/l

!g/l

!sn!g/l

psn

t g/l

!snpg/l

wl!g'l

t g l

t E l

llgl

wl

|ls,lpgl

rsrlrglIsrl|lgr'l

' t .o

20.00.51 .01 .01 .0o.51 .02.O10.01.01.01 05.01,01-02.91_02.O1.01.02 00 50 51_O1 0! o1.02.O1 01.01.01 0' 1 0

1 .01 01.01 00.50.51 .00.510.0

1 .01-01-010.05.0

1 01 .0

91?G3 Naphlhalenel03J-6$l n-Prcp!'lb€hzene

Thb l4boralory repod is ,tot vaIU fiilhou an sathorized ignatarc oa lhe colcr page .

' R€Fortable Detection Limir BRL = Below Reponing Limit Page 9l of 152

Page 465: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samol€ Id€ntificationM8F-50GWsA5%61-19

Clietrr Prciect #301-88

MarrixCround Wate.

Collection Date/Time| 5-Mar47 00:fi)

Rec€ivedl9-Mar-O7

CAS No- Aaalye(s) Fbs 'RDL Dilariot Mrlhot ReL Prcpored Analyvn Bztch Anab,sl

volrlile Orysdc Comportrds

Volatile O.oanic Comoounds bv SW846 82609Prepared by method SW846 5030 Wate. MS100-42-5 Sty€ne

63@2OG '|,1,1,2-T€tr€chloroefiane

79-34-5 i,1,2,2-T€bachtoroethahe127-184 Tetrachlo@€tlEne

10&68n Toluene

07{r-6 l,2,}Tridorohenzone

1?0J2-r 1,2,+Tdctltorobenzone71-55.6 1,.1,1-TriEfloroettEne79{G5 '|.1,2-Tricfiloroethane

79{1{ Tridior6th€$e

9618-4 |,2,lTrichloropropaneet63-6 1,2,+Trimethytb€nzene108-67{ l,3,tTrimedrytbenzene7541"1' Vinyl chtodde'33@2G7 m,p-Xyle.le96.17{ o-Xylenet0&9!|-9 T€[email protected] Efiyl ethergga-Oe€ Tert-aftyl methyl ehereB7-sz-l Efr/ ted+utyl etherr0e2()-3 oi+opropylether75$il T€rt-Butanol / buv alcolrcl12191n l,+oioxane

S{raog8(e /gcoverbsr160.004 /lBronEnuo@benzene

m37-2&5 TOhEne4Str060474 1, z-Diclioroethene-d4I8685i-7 Dibtontofluotunethene

Ertdc{rbl€ P€troleom Hf drocrrbms

Extractable Total Petrol€um HvdrgcadonsPrepared by method SW846 3510C800661-9 Gasoline6847+30-2 FuelOil #26647+31-3 FuetOlt #4f€5,5340-r FuelOil #6M0s800000 riob. oll,rc010(rc00 Aviatiofi Fudl

UnidentifedOtlEr Oillotal Pelroloum HydrocarbonsC+C36 Aliphdic Hyd.ocgrtons

SurlogtE g tgcor,glbs]g#&2 l-Chloroo{jpd€Eane

S€Dtvohdle Orgatrlc Codpound! by CCOrqanoc*rlo,rine Pesticld€s SW8,f6 8081APrepsrad by me0|od SW8il6 3510C3U9{X}2 Aldrin31s€a€ a€FlC

BRL

BRLBRLBRI-BRLBRL

BRLSRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI.BRL

1U)10295103

t .0

1.0o 5'L0

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t c lliC/lpdl

!dl

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SWE 16 82604 21+!h(47 21+[trat47 7031185 ek

75{9-4 T.id{dofluoromethane (Faeon jl) BRI_

70-1fr%70-1m%70-130 %70-130 %

BRLsRt-BRl-BRI,

BRLBRLBRLBRLBRLBRI-

94

BRL8RL

mgL/| 0.1mgr 01nlg4 0,1nE|l 0.1mgr'l 0.1rr€n o.lnEn 0.1mgL{ 0.1nqil 0-1nE/l 0-1

41110 %

pql 0_0143

lldt 0-0143

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SW846 808fA m-Mat4? 22411a,47 7031064 TG

This lahorototy .qort is ,tat ,aIU Fitlao an atthorlzcd sigmt*e on the coter page.

' Repo.toble D€rection Umit BRL = Betow [email protected] Liarir Page92 of 152

Page 466: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samrle lder!ificationMtF-s{lGWsA59464-t9

Client Prciect #t0l -88

IUatrixCround Water

Collection Date/Timel5-Mar-07 00i00

Receivedl9-Mar-0?

CAS No, Aaa+te(s) Result FloC *RDL Dilation Method netr. Pnpated .lrulfzed Bdth AnalJrst

S€mivohtile Orgrnlc Comporrds by CCOfoanochlorine Pesticides SW846 808'tAP.epared by method SW846 35iOC319_817 FBHC3198€_8 d-BHC58$ss g-BHC (Lindane)57-f4-g Chlordane72-54-a 4,4-ODD (p,p )7z-s+e 4,4-ODE (p,p.)5G2$3 4,4-DDJ lp,p')S57-1 Dieldrin95$98{ Enalosulfan I33213{+9 Endosulfan lll03i{7+ Endosulaan Sulfate72-20-A Endrin742r_e3_4 EndrinAtdehyde76-4{-e Heptachlor72-4+5 Methorychlot1024'57,3 HeptachlorEpoxade@0i-3t2 Toxaphene51037i.9 a€htodane56863,1-7 g-Chtordane53494-706 Endrin Kelone

Sil'rogate Ecoveies:103e8+2 4,+D&Octafl@rcbiphenri (Sr)2o5r-213 Decachloabiphenyl (3r)Polvchlo.inated Biohenvls bv SW846 8082Prepared by method SW846 3510Cr?s7+11-2 PCB 10t611t0+2s2 PcB 1221r11.t-r66 PCB 12325146921€ PCB 124212672.2e€ PcB 1249110€7S9-1 PCB 1254| 1i)96-€2-5 PCB .t26O

373a+235 PCB 126211100-14-1 PCB 1268

StrK]€ale aecowlias:I 0:)O6-&+ 2 4, 4 - D B-O c I efr uorf,hi phe n t4 ( S iu51.213 Decachlorobiphenyt (Sr)

S€nivoklil€ Orgsnic Co.npadrds by CCMS

8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARL8RLBRL8RLBRLBRLBRLBRLSRL

9493

ARLBRL

BRLBRLBRLBRLBRI-BRLBRL

75105

BRLBRLERLBRL

BRLBRLBRLBRLBRL

30-150 %m-150 %

0.01430_01430_0143

0,07140-01430-01430-01430,002s0-014:l0.01430.014:]0.014:]0.01,$0 01430.01,$0.01430 07140.01430.0143o.o143

o.o2a6

0.02860.02860.02860.02860.02860_02860.02860.0286

1.000.4001.00t.00t.001.001.00Lm

0200

vgtl

!gn

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tlSJl

ugrugipcnpgr

!sr!s/l!94

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!gn

!gn

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ps/

sw846 8081A m'Ma(47 22-Mar-0t /031064 rG

Semivolatile Orqanic Compounds bv SW846 8270Cftepared by method SW846 3510C

&-32-9 Acenaphthene4&96€ Ac€naphthyteheS,124 1-Mehytnaphthalene@\513 Anilmei2G12.7 Anthrac€ne1912-2{-9 Atrezine103-33-3 Azobsnzene/Diphenytdiazine@€7-5 B€nzidine56.5S3 B€nzo (a) enthrac€n€

SWa468O82 20-nnx-07 29MaG077031o63

sw846 8270C 20-Mat47 23-Ma(47 7031070 M.B

30-150 %30-150 %

!9!

fg/lpg/l

us/l!9/lpg/l

pc4

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ItEl

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t d l!sr

This lahorulory epod B ,tol ,alld wilhour ar. rulhoriu.t signsla.e on ahe corjr page-' Reportabl€ Detei:tion Limit BRL: Below R€po.ting Limit Paae 93 of 152

Page 467: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeotificationM8F-50GWsA59464- t9

Cliept Proiect #301-88

MahixGround Water

Collection Dat€/Tim€I 5-Mar-,07 00:00

Rec€ivedl9-Mar-07

CAS No- At alyt2(s) Rast/A Fl"c tRDL Dttuloa Method R.l PEWen Analfzcn Bdch Aaabtt

Semlvohlilc Orgrdc Compoun& by GCMS

Semivolatil€ Orqanic ComDoonds bv SW8,l6 8270C

Pr€parcd by rnethod SW846 35't0C$-32{ 8€rEo (a)pyaene2o5"s9-2 B€nzo (b) nuoranh€ne1el.24-2 B€nzo (g,h,i) perytene207{8.s B€nzo(k)fluoranthen€65:€tu Benzoic acjd10G515 B€nzyl alcohol1t1-91-t Bis{2<hloroeboxy)metn€ne111-444 Bis(2{filoroetM)ehe.3e6e-32€ Bis(2-dhlooisopropyl)€ttEr117-8r-7 Bis(2-€drythexyt)phthalatet0l€5-3 4-gornophenyl phenyl €fler85-6&7 BuMb€nzylphthalate86-74{ Cadezole5$50-? +CHoro-lrnehylphenolt0&47{ 4€hloroanitines1-5&7 z4hloronaphthatene9s{7-8 2+hlorophend700s-72'3 4-gtbrophenyl phenyl ethea2i8.01-9 Chryseneti-7G3 Oib€(lzo (a,h) anthra€sfle132+9 Db€rizofuran95-5G1 l,2-DichbroberEooe51ti-73-l 1.3-Oichlorobenzene1064G2 l,4oidoobenzene9l-94'1 S,3.Didllorobenzidine12033? 2,4oictrloNphenol84.66-2 Dieftylphthalate131-11-3 DidEthyt phnhahte105€7-9 2.+Dlm€6ytphenolu-7+2 Oi-n-buMphhatates31-5,2-l 4,6-Dinltro-2-rnethylphenol51-2&5 z,4oinitroohenotl2t-14-2 2,+Dhihodolu€n€f,trczs2 2,eDinitrololuenet17{4{ Di-n-oclylphthalateal€-4a{ FfuoEnthene86-717 FfuOaene11+7+1 Hexechlorobenzene476&3 He'0aarrlorobulsdieno71174 Hexrchlooc.ydopenhdiene67-12-1 Hexadoroethene1sg3ss lrdeno (1.2,3{d} pyreoe?t-591 lsophoam€e15/{ z-Molhyhaphthabne95-4&7 2-Me0vphend1o&3o.a, 3.+M66ytpheool106-44-59l-2G3 Naphthatenell8-zt4 2-Nit@nilines€{x!2 }Nitlgnilinetoo+r€ +Nitoanitine

SW8,16 8270C zGI ar-07 23-ttiar{7 7031070 M-BBRLBRLBRIBRIBRL

BRLBRLBRLgRL

BRLBRLBRLBRLBRL8Rr_BRLBRLBRL8RLBRLBRLBRLARLSRLBRLSRL8RLBRLBRLBRLBRLSRLBRI8RLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRTBRTBRL

BRL

BRL

BRL

ugtl|ldlvstl

wlus/lpdl

Wnp9nFgrlpsnrslpdl

udlpsrl

psn

usrpdI

!dludl|rs,lt s /|,snpdlpc4

rsnpdl

rrg,l

vsnps/|pdl

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wl

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tjgl!gtsdltldtgllpdl

pdl

rdlusnrs4psil

Fgl!dlusnwl

02m02001.00

0imt.00Lm1.00to01.00|.00

Lm1.001.00't.oo

1.00t.00|.001.001.00

o.2m1.00t.00t.001.00'1.00

1_001.001.00t.001.00t_001-001.00r.fi)r.00't.00

1.00'1-O0

0-€00r.fi)1,00

0.zx)1.001.OOt -00r0.0

r.00

t.001.00tr0

This lab.cory .qod b Eot s&d withod at asrtodztj sigu'tur. on de @ra page .

I R4ortable D€tection Lidir BRL = Below Rcporting Limit PEge 94 of 152

Page 468: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificaLionM8F.50GWs459.+e{- l9

Client Proiecr #101 -88

MatnxGround Water

Collection Date/Timel5-Mar47 00:00

Received

l9-Mar-07

CAS No. Anarytz(s) Resall Flog A n s *RDL Dilution Method Rel. Prcpued Anabzed Boteh Anabst

SeDivolrtilc Orgaric Compohds by cC${S

Semivolatile Oroanic Compounds bv SW846 B27OCPreparcd by methad SW846 35t0C98€$3 Nitroben4ene84.75-5 z-Nit ophenol10G02-7 +Nitophenol62-7+9 N-Nitrosodimethytamine621+a-7 N.Ni[osodi-n-propylamine863}5 l$NilrosodiphenytamineItSs Pentachlorophenol85{1-8 Phenanthrene10&9t2 Phenol1?9{XF Pyrone110-€6-1 Pyrfujine120{2-1 l,2,4.Trichlorobenzene9+9+a 2,4,STrichlomphenol€€4e2 2,4,GTriqhtorophenol

Srrzogatg recovenbsl321504 2+luorobiphenyl367-t24 2+htorophetml1165.6,4 Nilrcbenzene4S116542.2 Phenol4sth$sr4 Teryhent44l411e79.6 44,+TnbromophenolSVOCS bv SW846 8270C SIMftepar€d by melhod SW846 351 0Ca3{2.9 Acenaphhene

a)ss€;8 Acenaphthytene90-12{ 1-l/ethyhaphthal€ne12G12-7 Anthracene5G5t3 Benzo (a) anthracene50-32{ Benzo (a) pyrene4+99-2 Benzo (b) flloranthene191-2+2 Benzo (g,h,i) perylene207{€-9 Benzo (k) ffuoranth€ne21M1€ Chrysene53.7G3 Dibenzo (a,h) anthracenea)6-44{ Fluorantheneffi-7T7 Fluorene193.395 Ind€no (1,2.3-cd) pyrene9r-57€ 2-M€thylnaphthalene91-&3 NephthaleneC5{1{ Phenanthrene129{0{ Pyrene

Sunogktl€ aaooyeries:32t&4 2-FluofobiphenyltrteiQ Tefphenyl44

Toarl M€tak by EPA 6000/70010 Series Methoa!

SWE46 6270C 2o-t!4ar07 23-Mar47 7031070 M IBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

595367657444

BRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRL

BRL

5066

pSJt l.o0

Udl 1.00pgl 1.00

ldl 1.00pg/l 1.00

lig/l 1.00

ug/r 1 00

ugr 100

ldl 1.00

ldl 1.00

Ug/l 'l.00

pS/l 'l.00

ttSJl 1.00

ldl 1.00

30-130 %1L110 %30-130 %15-110 %30-130 %15-110 %

pS/l 0.050pS/l 0-050

ldl 0.050

Lidl 0.050ydl 0.050

!g/l 0.050

US/l 0-050

liS/l 0.050

uS/l 0.050

udr 0.050

lisn 0050pdl 0 050

!s/r 0.050

ldl 0.050

udl 0.050yg/l 0.050

tqll 0-050

30-130 %30-130%

n?gn 0.0050

rng/l 0.0040

mg/l 0.0050

!dl 25-rlla..oT

7!ue44 Silvet

744O'3F2 Aserlic

Zg0-3+3 gadum

8RL

0.0m2

0.0322

SW846 6010S z3"Ma'.Ol 24+.4aro7 7031315 LR

Thb tabontory rcpora ie not ealid xtlthottt sn aalhoited signaturc on the cowr page .

+ Repodallle Delection Limit BRL = Below Ref'orting Limit Pase 95 of 152

Page 469: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeotificationMtF-50GWsAs9464-19

Clielt Proiect #l0t-88

MatrixGround Water

Collectioo Date/Timel5-Mar47 00:ff)

Releived| 9-Mar-07

C.AS No, Anaqtz(s) Fhs A n s 'RDL Diluiarr Method R4 Prcpaed Antlfzrn Dahh Arutlfsl

Torrl Metlb by EPA 50O0,1U)0 Series Methods

71.4043.9 Csdmium

744G{7-3 Chrcmfum

7€9-92-l L€ad

r|S2-4+2 Selenlum

Tolrl Metal$ by EPA 200 S.rie6 Mcthods

7439.975 Mer ry

SWa46 60108 23-Mar4f 24ji1d47 7031315 LR

EPA245.In47OA 2$M€r{? 23-ti,la.47 781316 RM

BRL

BRL

o.0120

BRL

BRL

firgn

mgr

nB/t

rtSI

0-0025

0-m50

0.m75

0.0150

0.mo20mg/I

This lahodor! tzpotl it not wlld nithou an aathoi?rl EiE tttare ot lhz coeer p!{re.

+ Reponabl€ Detection Limir BRI- = B€low R€podng Limit Paee 96 of 152

Page 470: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

APPENDIX GQA/QC Sample

Laboratory Reports

Page 471: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 472: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationFB.I

s459464-17

Client Project #l 0 l - 88

MatrixBlank water

Collection Date/Timel5-Mar-07 00:00

Received

l9-Mar-07

CAs No. Analrte(s) Result FloE Unlts 'RDL Dilution lve.hod Rel. Prcpdred Antryzed Batch AMIlst

Vohdl€ Organic Compoundr

Volalile O.oaoic Comoounds bv SW846 82608Prepared by melhod SW846 5030 Waler MS7F1$1 1,1,2-Trichtorolriffuoroethane(FreoSRL67€+1 Acetone BRL107-13-1 Aciylonitrile BRLf14T2 Eenzene 8RL104-€6-1 Bromobenzene BRL7+91-5 Bromochloromethane BRL75-274 Bromodichloromethane 8RL75-2+2 Bromofoam BRL74{}9 Bromomelhane BRL7843-3 2-Buianone (MEK) BRL1(X-51-8 rFButylbenzene BRL13$98$ s€c-Butylbenzene BRL98{€4 te(-Butylb€nz€ne BRL75.1s4 c€rbon disulftd€ BRL56-23-5 Carbon tefachloride ARLi0&9{r7 chtofDbenzene BRL7$OD3 Chtoroethane BRL

BRLBRLBRLBRL

us/| 1.0f94 2O.O

ldl 0.5

!g/r 1.0

!s/l 1.0

rs4 'l -0

tstt 0 5

tlSJt 1.0

USn 2.O

!S.4 10.0

Ug/ l 1.0

|'jS/l r.0

pdl L0

pdl 5.0

p d l 1 0

p g t 1 0

l.dl 2.o

ust 1 .0!S/l 2.O

tgt 1.0

ldr 1.0

ps/l 2.op d l 0 5

I S n 0 5

pdl 1.0

p S n 1 0

!s4 1.0

lg l 1.0

!g/l 2.O

pSll 1.0

t91t 1.0

trdr 'r _0psr 1.0

N t 1 0

USn 1.0

lSn 1.0pSn 10pSn 1.0pSn 0.5pdl 0.5

!g/l 1.0

US/l 0.5

US/l 10.0

IS/l 'l.0

pdl 1.0pdr 1.0pg/l 10.0

vgl 5,0

vs,tt 1.0ydr 1.0

1

1

1

1

1

1

1

1

1

I

I

1

1

1

1

I

1

t

I

1

1

I

1'|

1

I

I

I

1

1

1,1

'|'|

1

I

I

I

I

I

1

1

1

1

1

I

1

1

1

SW846 82608 21-Mat47 21-Mat47 7031185 ek

67S3 Chloroform74{7-3 Chlofomethane95.49-8 2.Chlorotoluene10H3-4 4-Chlorototuene

-124 1,2-0ibromo_3doropropane BRL121-4&1 Dibromochloromehane BRL10e93-4 l,2-Dibrornoetr|Ene(EDB) BRL74.9$3 Dibronromethane BRL955Gr l,2.Dichtorob€nzene BRL4,41-73J l,3-Dichlorobenzane BRL10646-7 1 ,4-Dichtofobenzene BRL7+7t€ Dicfiloodiiuoromehane(Fr€onl2)BRL75-34-3 1,l-Dichtoroethane BRL107{6-2 1,2-Dichtorcethane BRL

l,1-Dichloroethene BRLt5e59-2 cis.1,2-Dichtoro€thene BRL15ffi{ trans- 1 ,2-Dichioroethene 8RL7847-5 i,2-Dichlo.opropane 8RL142-28-9 |,3-Dichtoropropane BRL59+20-7 2,2-Dicf oioprop€ne gRL

56'5+6 t,1-Dichtoropropene BRL10061{1-s cis-1,3-Dichloropropene BRL10061{24trans-1,}Didrtoropropene BRL1oq1-4 Ethylbenzsne BRL87{&3 Hexachlo.obubdiene BRLi91-78{ Z-l-texanone (MBK) BRL9832{ lsopropylbenz€ne ARLgs{7$ 4-lsopropyltolu€n€ BRL163.4{a4 Mettryttert-buhy' other BRLi0€.1e1 +Methyt.2-pentanone(IflBK) BRL75{92 MetMene chtodde BRL91-2G3 Naphth€lene BRLt09A$1 n-Propy'benzen€ BRL

This taborcoty rcport is ^ot volkl n' hou an outhofizei sig,/,aturc on the colL€r ptgc.

+ Reponable Detection Limit BRL= Below R€podng Limit Pag€ E3 of 152

Page 473: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificatioaFB.I

sA59.t6r- l7

Client Proiect #301-88

MatrixBlaok Water

Collection Date/TimeI 5.Mar47 00:00

Rec€ivedl9-Mar-07

CAS Na Adqlf,e(s) ResaU FI"S Unia .R.DL Dilatioa MEthod Rel, PEpsred Anzlwd Bach Anzlyst

Vohtile Orgrlic Compornds

Volatil€ Orqanic Comoounds bv SW846 82608Pr€par€d by method SW846 5030 Waler MS

BRLBRLBRL8RLBRLBRLBRLBRL8RrBRL

7559-4 Tri€*{oroffUoomethane (Freon 1l) 8Rl-

tolx2-s St)rcn€63G2O€ 1,.1,.1,2-T€hcl or€thane79-34-5 1,.1,2,2-TetracNoroethane127n8-4 TotladrloloeUlenelom.3 TOlUen€87-61{ 1.2,}Tridltorobenzene12oi2n ,l.2,4-T.ichloobenzene

71.55€ |,1, t -Trichloroelhane

79.0[!.5 |,1,2-Trichtorcethane79Oi5 Trichloro€thene

SW846 82604 2l-Mar47 21+larO7 7031185 ek

BRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL8RLBRL

9910296101

BRIBRLBRLBRLBRL

BRLBRLBRLBRLARL

88

BRLBRL

tstusn|lsnt'$t4t'dl$nrsfl|lsnpdl

!dlusnuglsdlusflt g/l

l€/l

pc4

|'|s4pqlpglpdl

!dlpdl

t . 0

1 .00.51.01 .01.01.0

1.0r . 0t . 0t . 01 .0r_01.01_02.n1.0't0.0

1.01 .0t . 0t . 010.020.0

o.01210_o121

I

1

I

I

1

I

I

I

I

1

l

1

1

1

I

7

I

1

I

I

1

1

I

1

96-14-4 1.2,9Tri:tlloropropane9163{ 1,2,+Tdmethylbenzenel0o{7€ 1,3,s-Trimethy'benz€ne7501-4 Vinyl chtoride133G2G7 m,p"Xylene95-.17$ o_Xyiene10+99-9 TdEhydrofuran60-2$7 Ehyl dher994-05{ T€rt-amyl methyl elher637€2-3 Ethytsft_butyleherto&mn Di-isopropytefll€r755to Tert€utanol/ buty' alcohol1?3€r-1 I,41Dio)6ne

Surogale recoveries:16oJn4 lt4honofluorobenzene

437-2e5 ToltAne4S17 06047 4 1, zaichloroethene-d41868-sv7 Abrcmofluorcmelhane

Ertrrctrble Petmleum Hydroclrbols

Ext-actable Totral Peboleuin Hvd.gc€rbonsPrepared by method SW846 3510C00064i-9 Gasolino68117&30.2 Fuet oit #26847e31-3 Fuel Oil #468553{0{ Fu€| Oil #6i,10980flm Motof Oil.()01m{P0 Aviation Fuel

UnidenlifedOther OilTotal Petroleum HydrocarbonsC!9-C36 Aliphatic Hydr6arbons

Sr/'rDgata €cot€d,es j3{je643-2 1 4hlorooctdecane

Semlvolrtil€ Org.ric Coopo|rndr by CCOroanoct orine Peslicides SW846 SOBIAPrepared by rnethod SW846 3510C3rls-oGz Aldrin3ls8a€ 6-BHC

+cT ETPH 2l-Mat47 Uia47 7031160 DS

7G130 %

70-130 %

7G130 %

7G130 %

rndl 0.ImCn 0.1mgl 0.1mSil 0.1fiigl 0.1

msn 0-1drsn 0.1mSn 0.1mg/l 0.1mg/| 0.t

4llt'to %

1'snItgl

SW€46 m81A 204.,.?d47 t.+tato? 7031064 TG

Thit laboralory .epott it no, valid tdthotd ott oizd signattte on the cavc!pag..

+ R€portable D€t€ctioo Umit BRL = B€low R€poiting Linit P.ge 84 of | 52

Page 474: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationFBIsA594er- l7

Client Paoiecr #301_88

MatrixBlank Watcr

CoLlection Datc/Timel5-Mar.07 00:00

Received19 Mar-07

CAS N^ Analrte(s) Resull Fl4C Ani6 *R.DL Dilutian Melhod Ref, Preparcd Amlyzed Bqlch A"alyst

Semivolrtih Orgrnic Compounds by cC

Oroanochlorine Pesticides SW846 8081A

Prcpared by m€thod SW846 3510C

3r+8+7 b-BHC31S{64 d-BHCsa4$e g-BHC (Lindene)

5/-74.9 Chtoadane72-544 4,+DDD (p,p')

72,55.9 a,4_DOE (p,p.)

50-2+3 a.4-DOT (p,p')

60-57-l Dieldrin95s98€ Endosutfan I3321+65'9 Endosuffan ll1031-073 Endosutfen Suttate72-204 Endrin7421.93-4 €ndranAldehyde76444 Heptachlor72-43s fttethoxychlor1024-s7-3 Heptachtor Epoxide€001-3+2 Toxaphene

5103-71-9 a-Chlordanef,a,6€,3+7 gchlordane

5349+7Gs Endfin Ketone

Su/rogate rec?ver'es:1 0386++2 1, 4 -DB-OeIafl uorobiphenyl (Sr)

mst'21'3 Decachlorobiphenyt (St)

Polycfilodnated Blohenvts bv SW846 B0B2

Prepar€d by melhod SW846 3510C

126f+11.2 PCB 101611t04-28.2 PCB 12211r14r-16.5 PCB 1232534692r-e PCB 1242126?2-29{ PCB 124811097691 PCB 125411006-82,5 PCB 1260

c7c21.23.6 PCg 1V62

111&144 PCB 12€8

Suftogaie Bcovedes:103864+2 l,4Dgoclafluorobiphenyl (50

m51-243 Decechlorobiphenyl (Sr)

Semivolrtile OrSrnlc Compounds by CCMS

2GMaF07 23.Mar{7 7031063

BRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

9781

BRLBRLBRLBRL8RLBRLBRLBRLBRL

I t

95

BRLBRLBRLBRL

BRLBRLBRLBRLBRL

!El

ljEl

!sI

FEI

FSn

us4ps4

!s{!gn

!g/l

!s/l

!gn

uEl

ug/l

!g/l

ut/l

ugl

|rg/lpgn

|rg/l

!gl

!gn

!gn

ug/l

!s/l

!gnpg/l

rsnpg/l

o.01210.01210.0121

0.06060.01210-012ro.0121o 00240.0'1210.0121

0.0121o.o121o.o121o.0121o.o121o.01210.0606o_o1210.01210_0121

30-150 %3G150 %

sw846 8081A

sw846 8082

sw846 827(rc

1

1

l

l

I

I

1

1

1

1

1

1

1

1

1

1

1'|'|'|

o.02420_0242o_02120 02420.02420.02420.0242o.02420 0242

1

1

1

1

1

I

1

1

1

3F1SO %

30150 %

Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 3510C

A3{2-9 Acenaphthene20e96{ Acenaphthylene90.12{ l-Methylnaphthalene

@-5!3 Anitine12&12.7 Aihrac€ne'1912-249

At-azine10$33.3 Azobenzene/Diphenyldiazine

9?{7-5 B€nzidine5&593 B€nzo (a) anthr€cene

2O-Mat47 2344erll 7031070 M.ApEl

Fgn

lgr'l

llEl

FgI

l|sntrgl

ll(/l

rdl

1.000 4001.001.00r.001.001.001.00

0.200

This laboratory npoa is not vafid wirtoat an ra,horized sigttzturc on the cover page .

' Reportable Detection Limit BRL = B€low ReFo(ing Limir Page 85 of 152

Page 475: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SarnDle ldentificationFB-IsA59454-t7

Client Proiect #30 | -88

MatrixBlank Water

Collection Date/TimeI 5-Mar{7 00:00

Receivedl9-Mar{7

CAS Na AnaIrE(s) Fl"s Anb *RDL Dilutbn Mdhod netr. Prcpated Analfzrd Adch An&lyfl

Sealvolraile Org.ni. Compo||||ds by GCMS

Semiwlade Oroanic Comoounds bv SW846 8270C

Prepared by method SW846 351 OC50324 Benzo (a) pyr€ne2O$9e,2 B€nzo (b) fr'Jo,rEflth€ne191-2a-2 B€fEo (g,h,i) perylene207{6-9 Benzo (k) nuorantfiene65{S0 genzoic acidl0G5l-6 B€nzylalcoftol111-9r-1 Bis.(2{hhfoEthory)mehane111-aaa Bis(2-ohlo.o€thyl)eflrer38€38-32.9 Bis(2dttoroisopropyl)ether117{1-7 Etis(2€hy,thexyl)phthatatoi0t-553 +Bromophenyi phenyl eher8s6&7 Butyibenzylphth6tEte8G743 Cgrbazole!€-50-z +cftloro-3-mehyiphenol106-47{ +Chloroaniline91-50-7 2-Chloronaphthalene95-57-8 2-Chlompheflol7005-72-3 il-Chlo.ophenyj phenyl ether218{t-9 Chrysenes3-7G3 Dibenzo(a,h)antkacene132{.t€ Dibenzofuaan9&sG1 l,2-Dichlorcbenzone541-73-1 i.3-Dichlorobenzene10c46-7 1,4-Dichloobenzeoe9i++1 3,3-Dichlorobenzijine120-€3-2 23-tlichloro0henol84{&2 Diehyt phthatate131-113 Dimethyl phth€tetetotr7€ 2til-Dimohytph€fiolu-7+2 Di-i+uMplthalat€53+s2-1 4,6-Diniko-2{nediylphenol51-2&5 2,+Dinitrophenolt2r.r,1-2 2.4olnibototuene60G2GZ 2,SoanitbIotuene117{,{.0 Okl{{t/phthshto20G44{ FluoEn$tene&-1rf Fluorenel1e74n Hexachlorobenzene87€+3 Hexachtorobutadiene71474 l-lexachlooctdopentadiene67-7?-1 Hexechloroethaoe1943s-t Indono (13,34d) pyene7€-59-1 lsophorone9l-57$ z-Merhrnaphhatenes54+7 2-Methylphenol1o€.3s-1, 3,+Methytphenol1o€-it{-5et-al3 Naphthalene8€-7.Lrt z-Nitroenitine99:0+2 $Niboaniline10O{t€ +Nitoaniline

BRLBRLBRLARf,ARLSRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL8RLBRLBRLARL8RLBRLBRLBRL

BRL

BRLBRLBRL

wlysn

FSnPdlPS/|FSrltt$wpgl

tlsAyglps4

wItdlpdl

ugl

ug/lt,qtlvgtlp$4

!dlrcnttdrpgrlpglpdl

u g l|'lsnt'q[w!s/l!94uslltlS|l

ItEl

vgtltJslpsA

ugtl|,9/lItgJl

ttgl!dl!dl|lg/l

psn

FS4psr!dlu{l

0,2000200r.00

0.3001.001.00|.0,0

L001.001.O01,001.001.001.00

1.001.001.001.001_00

o.mo1_O01.001.(m

L001.001.001.001.001.00r .m1.001.001 001_(X)r.00

1.001.001 0 00.6001 0 0

|.00

0.zx)1.001.001.0010.0

t.00

1.001-001.00

SW846 8270C 2O-Mat47 23.1t,er'7 7031070 M.A

Thh lzborotoq npo.t ls Eot eold ,rithoa att aalhot zpl ttgadare on thc covr ltzg. .

. R€portable Detection Limia BRL = B€low Reporting Linit Pagp E6 of | 52

Page 476: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldertificationFB-1sA59464- r7

Clierlt Proiect #l 0 t -88

MatrixBlank Water

Collection Date/Timels-Mar{7 00r00

Receivedl9-Mar-07

C4S No, Analyte(s) Resttll Fl"S Ani,s *RDL Diluiotr Method netr Prcpued Anauzed Batch Analyst

Semlvolrtile Orgrnic Compo||nds by GCMS

Semivolalile Orqanic Comoounds bv SW846 8270CPr€pa.ed by meihod SW846 35t0C

sB9t3 Nitrobenzene88-79F5 2_Nitrophenoli0Go2-7 +Nitrophenol62.719 N-Nitrosodamethylamine621€4-7 N-Nitfosoda_n-pfopylaminem.3G6 N-Nitrosodiph€nytamine47J6.5 pentachloroph€nol

854r{ PheMnthrene106-95-2 Pheno{12s00{ h/rene1lc€8r F'Jridiner2o-42-1 1,2,+Tdctitorobenzene9+95-4 2,4,$Trichlorophenol{18{€F2 2,4,GTncfrtofophenol

Sffrogate re€o!€ries-3214c-a 2-Fluorobiphentl

357-124 z-Fluorophenol

1165-604 Nihobenzene-ds

416162-2 Phenol4s

17tAS14 Teryhenyl4l4

118-794 2,4,GTtibtofllopheool

SVOCS bv SW846 8270C SIM

Prepared by method SW846 3510C

8332.9 Acenaphthene

2rl&964 Acenaothylene9O.12{ 1-Methylnaphlhalene120"12-7 AnthEcene56-5+3 Benzo(a)anthmcene50-32-8 Benzo (a) pyrene

?05-99-2 Benzo (b) fluoranthenelgl-24-2 Benzo (g.h,i) peryl€ne

20rc&g Benzo (k) fluoranthene?1F014 Chrysene53-7G3 Oibenzo (a,h) anthracene2{E-1,.-0 Fluo(anthene06-717 Fluorene19$39$ Indeno (1,2,3-cd) pyrene9i-57€ 2-Methylnaph0ratene9l-2G3 Naphthatene854r-g Phenanthrene129-00{ Pyrene

Surrqale reco.y€ies:321-6Go z-Fluothiphenyt

171e-514 ferphenyl4l4

Tobl Metab by f,PA 6000/?000 Serier M€thods

8RLBRLBRL8RL8RL8RLBRLBRL8RLBRLBRLBRLBRLBRL

697083638552

BRL

BRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

6176

trdr 1.00pdl 1-oo

vq 1.00

U94 1.00

!q/r 1.00

lsr 1.00

lgr ' t .00

llg/l 1.00

t)glt 1.0O

ug4 1.00pS4 1-00pdl 1.00

US/l 1.0Opdl 1.00

3G130 %15-110 %30-130 %15-110 %m- tn%15'110 %

pgn 2$Mar-07

1

1

1

I

1

I

I

I

1

1

1

I

I

I

1 SW846 8270C/EPA625 SIM

7440.224 Silver

7l4O-38'2 Arsenic

7,{403+3 Badum

rsn 0.050pgn 0 05O

l.dl 0-050

FSI 0-050

Ug/l 0.050pg/l 0-050

lgn 0.050

sdl 0.050

liS/l 0.050

tsA 0.050

$slt o.o5o

lsn 0.050

liS4 0.050

ug|/| 0.050pdl o.o5o

fdl 0o5o

US4 0.050

30-130 %3G130 %

mg/l 0-0O5O

mg/l 0.0040

lng/l 0.0050

sw846 60108BRL

BRL

8RL

23-Met47 24+/tat47 7031315 LR' 26.1,{ar{7' 24-Mat47

Ihk laboftaory repod is nor wud rslthoa oE aul'ortatd siFn,/t,,,.? on thz corer pagc

' R€podable D€teation Limit BRL = Below Reponing Limit Page 87 of 152

Page 477: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdetrtificatiooFB-Is45946+ t7

Cli€nt Proiect #30t -88

MatrixBla-ok Water

Collectiol Date/Timel5-Ma.-07 00:00

Receivedl9-Mar-07

c-as N^ ANtrE(s) Resslt FI4g Anib *R.DL uhtu'n Method ReJ. Prepued Amly,en Buctt Aazlpt

Tobl Metab by EPA 6000/7m0 S€rlci Metrorb

74.10-,13.9 Cadmium BRL

7440-47-3 Chmlitium BRL

7439-92r Lead BRL

282-4+2 Selonium BRL

Totd Mettb by EPA 200 Serlts M€thodt

743997€ t\iercury BRL

mgn

ntg/l

mql

mgr

fitsl

0.0025

o.0050

0.0075

0.0150

0.00020

SW84660108 21Mar47 2+[,lar{7 7031315 T-R

EPA245.1n4l0A 23 tafi7 Z3Jtrlar{7 7031316 RM

':hb bbontory Eport It n4t vzlil iirtoar an auttort4d slgn4urc on lh. co|9. page .' R@drble D€t€ction Limit BRL = Bdow R€porting Linit Prge 8E of 152

Page 478: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificationTLT5A59464- I8

Client Proiect #30 | _88

MatrixBlank Water

CoLlection Date/Timel5-Mar-07 00:00

Receivedl9-Mar-07

CAS Na An ytc(s) Res!k UnitsFlag *RIIL Dilurio" Method Ret:, Prupan.l Anabgd Barch AnalystVohail€ Orgrnic CompoundsVola$le Orqanic Compounds bv SWB46 82608Prepared by method SW846 5030 Water MS76-111 1,1,2-Trichlorohfuoroothane(FreogRL67€1L1 Acetone BRL1rr3-1 r'€rybnitdle BRL7143^2 Benzene BRLt0&E6-1 Bromobenzene BRL74'97'5 Bromochtoromethane BRL71271 Bromodichtoromethane BRL75-2*2 Baornofom BRL7'l{3-9 Bmmomethane BRL78-933 2-Butzr}c,re (MEKI BRL101L51+ n_Butytbenzene BRL13t90{ sec.Butytbenzene BRL98_0&6 lert-Eutylbenzene BRL75'15'0 Carbon disutfide BRLs6'295 Carbon tetrachioride BRLlosscz Chlorobenzene BRL7s-{ro.3 Chloroethane BRL67{fi Chtoroform BRL744r-3 ChlorDmethane BRL95.498 2-Chbrotoluene BRLloHg zlchlorotoluene BRL96-12{ 1,2-Dibromo-3+htoroprcpane BRL12'/H{l-1 Dbromocitoromelhane BRL16W l,2-Dibromoethane (EDB) BRL7+913 Dibromomethane BRL9l5Gi l,2.Oichtorobenzene BRL541-73-1 1,3_Dichlorobenzene BRLloe&7 l,+Dichlorobenzene BRL73'714 Dchtorodilluoromethane(Faeonl2)ARL75-3+3 l,1_Dichtoroethane BRL107+2 l,2-Dichioroethane BRL75-3F4 l.|_Oichtofoetfrene BRL156-5S-2 cis-1,2-Dichtoroeth6ne BRL'15ffi0-s

tlans-l,z-Dichloroethene BRL78{7-5 i,2-Dichloropropan€ ARL'42-2v9 1,3-Dichtorop@pan€ BRL59+20'7 2,2-Dichtoropropane BRL563-58{ I,l-Dichtoropropene BRL1o061{l-s cis-1.3-Dichtoropropene BRL1006i{?{fans-1,}Dichloroprop€ne BRL10q41-a Ethylbenzene BRL87{s3 Hexachlorobutadaene BRL591-78{ 2-t-lexanone ([/BK) BRL98€2'8 lgopopylb€nzene BRL9+87$ +bopropyltoluene BRL1634{e Methyt tert-but}i ether BRL106-10-1 +Melhyt-2-pentanone(M|BK) BRL7549'2 lrethylen€ chtoride BRL91'2G3 Naphthaten€ BRL10$6$1 rFPropylbenz€ne BRL

r9n 1.0psn 20 0pSI 0.5

pg/l 1 0

ttgtt 1-0

!9/l 1.0

pEl 0.5

lSn 1.0

!g/ l 20

@t tD.o

ttgtt 1.0

pgJl 1.0

psn 1.0

ps/r 5.0lgn 1.0pgn 1.0

rsn 2.o

trgr 1.0

!94 2.0

l g r 1 0p g t 1 0

ttgtl 20pg/r 0.5

t sfl 0.5

l.rs/l 1.0ps4 1.0

! s / l 10

Ug/l 1.0

ug/r 2.0

tsn 1.0pSn 1.0pSn 1.0

!S/l 1_0

!g/r 1_0ps / r 10

Mt 1.0

t)glt 'l.0

t/g/l 1.0pgl 0.5p!,n 0-5

!g/l 1-0

lgr 0-5

|l9r 10.0pg/l 1.0

vgt r.0psfl 1.0

!s4 10.0pc4 5,0

ldl 1,0

l d l 1 0

1

1

1

l

l

1

1

1

1

1

1

1

1

1

1

1

1

1

I

1

I

1,1

1

1

1

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1

1

1

1

1

1

I

1

1

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1'|

1

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Sw846 82608 21-Mat47 21-Ma,-ot 7031185 ek

Thb ItboratoA rcport it ,tol tdljd wdhoat dd aaihorir4d signusre on tlc covq pager Reporrrbte Detectioo Limit BRL = Betow Rwrting Linir Page 89 of 152

Page 479: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldetrtificationTB-IsA59464-18

Client Project #l0r-88

ManixBlank Warer

Coll€ction Date/Timel5-Ma.{7 00r00

Receivedl9-Mar-07

CAS Na Anabtt6) nas 'RDL Dilut& ' Merhod R.l Preparcd ADaltz,.t fulch Anott$l

Vohaile Olgrnic Compounds

Volatile Orqanic Comoounds bv SW846 82608P.epar€d by method SW84ti 5030 Water MS100.a2-s Sttrcn€ BRL63G204 1,1,1,2-Tetrachloroeihane BRL7$34{ 1,1.22-T€trachlo{oethane BRL127-18-4 Tatacfitoroeflrene BRL108{€-3 Toluen€ BRL87Si{ 1,2,+Trict orobenzene SRLl2o{2.1 1,2,+Tricfilorobenzen€ BRL71-5s Ll.l-Tridlloroethane BRL79{0-s 1,1,2-Trichl6oethane BRL79{1{ Tdchloro€lhene BRL75{94 Tdchlorofluo.omethaoe (Freon 11} BRL9G104 |,2,lTddtloropropane BRL

1,2.+Tdm€thylbenzeoe BRLt06$7{ 1,3.5-Trimethytbenz€ne BRf75414 Mrryi chlo{ide BRLr33o-2c7 m,p-Xy'ene BRL9$.17{ o-Xytone BRLlosss-g let-ahyclrofilran BRLao-2+7 Ethyt ethef BRL9ea{5{ T€rt-dnyl methytetr€r BRL637-e2n Ethy tert-but/ ether BRLi0&203 Di-lsopropyl ether BRL75$$o Tert€utanol/ butty' alcohot BRL123.9i-r l,4oioxane BRL

|ldl

lrg/l

us/lFdlpdl

!s4|ldl

|rsnpdl

ItgltsIIJqI

!dluElu$vglsrlvglpgilpdl

udlrcnt s4psit

t . 0t . 0

0.51 0

1 .0'1.0

1.0t . 01.0't .0

1_O1 .01.01.01 .02.O1 .010.01,01 .01.0

1 .010_020-0

I

t

I

1

1

1

I

I

1

t

1

1

1

1

I

1

1

1

1

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I

1

t

SW846 82608 21{nar-O7 21-tnar-07 7031185 ek

Surogate recoveies:1tu404 +B@nofluotobenzene,n37-26.5 Tduene4B

10010295102

7G130 %70-1n %76130 %70rN%

I 706047 4 1,2Obhlo(oelhane44

fiaest7

Thk bhftlarf ,cpott is not eaIU silhort an atdodzd dgnt ,re o8 th. cowr pqe .

' Reporiable D€tEcri,on Limit BRL = B€low R€porti[g Limit Pag€ 90 of 152

Page 480: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtile Organic Compourds - Quality Cortrot

Anslyqsl Resutt I lag

Source %REC

Resulr %REC LimitsUnits rRDLSpike

tevel RPDRPD

Limu

Batd 7031185 - SW8{6 5030 Waier MS

Blank fl031t85€LK1l

P.epared & AnEllzed: 21-Mar.O7

1,'l ,2-Tridrlorotdfluoroethane (Freon I l3)

genzene

Bromobenzene

Brornochlorornethane

8{omodicitororneltEfl e

B.onrolom

2€utahone (MEK)

nAutylb€nzene

s€c-BiJtylbenzene

te|l€utylbenz€n€

Ctrbon disulfde

Carhon tet achloride

Chlorobenzene

Chloroelhane

ChloIototm

Chlorom€thane

24hlorololuen€

4-Chlorololuene

l,2.Dibrorno-3-chlo.opropan€

Dibromochloromethan€

1,2{ibrDno€thane (EDB)

Dibrornomelhane

1,2-Diclllorooenzsne

| ,!Didrlorobenzene1,4{ichlorobenzene

ARL

BRL

BRL

BRL

BRL

BRL

BRI.

BRL

BRL

ARL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

ARL

8RLgRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRI.

BRL

BRL

BRL

BRL

BRL

ARL

ARL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

SRL

BRL

BRL

BRL

!gl

trdlpgl

!sn!dlLjs/|!snps/l

|lgl

Lrgl

t (yl

pgn

W/rltgtl

ugrugl!snp$4

ps4

!91

ugl

!g/l

us/ludlllgl

|ls/lpg/l

pg/r

psn

tsrl

trg4

us^yryl

u(yluglusilg€|/l

uElpEr

ugrus4uglpsnuglpdlpsn!Euql!sn!dl

!dl

tsA

' | .o

20.o0.51 .01 .01 00.51 .02.O1 0 01.01 .01 .05.01 .01 .02.01 .02 01 01 .02-00_50.51 .01 .01 01.02 01 .01 .01 .01 .01 .01 .01 .01 .0LO

0.50-5l 00.510.0't _01 .01 -010.05.01_01.01 .01_0

{Freonl2)| , | -Oiciloro€thane

I 2-Dichloroeti'ane1 , | -Dichlorelhene

cis-i,z-Di.* oro€thene

tranE-1,2{)ic* oroef\ene1 ,2.Dichloropropaie

| ,3-Dichloropropan€2,2{)ij|loropmpan€

| ,I .Oidrloropropene

cis-1,lDichloropropene

lrans-1,3-Dinbrcprop€n€

Ethytbenz€ne

Hexehbrob!tadiene

2+lexanone (MBK)

{-lssropyllolu€ne

Meoryl brt-butyl slh€r

+lrsthy]2+€ntanone ([llBK)

Methylene chloride

Naphthalene

Styrene

1 ,1 ,1 ,2-TetEchloroelfiane

Thit llbo.olory rcpod it ,toa vslrl u,ilhour an at!rtorized ngnatarc on tfu cover pzge

' ReDotuble Detection Limil BRL = B€low R€Donins Lmit Page 97 of lJ2

Page 481: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organlc Compoutrds - Ql|ality Control

Anallrds) R€sult Flag UnrrsSource %REC

Result %REC Limits.RDLSpikel,ev€1

RPD

LiftitRPD

Brtch ru 1l$ . SW846 5030 Wrt€r MS

Bl.nk a?o3 l 185€LKl I

Prepercd & Analyzedr 21+rar{7

1,1,2,2-Tellachlorethane

TekEdrbroethen€

Toluen€'1 2,lTrid orobenz€ne

I P,+TrlcSlorobenz€ns1,1,1-T.idrlorE€thane

1 , | ,2-Tri€filoro€hanel.iibloeth€ne

Tri.fi bronuorom€han€ (F.eon 1 1 )1,2,}Td.nbrwropane

1,2,+Trimethytb€nzerE

1 ,3,STrimethy'b€nzeneViny' cf dlde

m,p-Xy'ene

o-Xylen€

Telrahydofu.an

Etrryl €{her

Tert-dnyl rnethyl ether

Elhyl ten+uryl eti€r

Di-lsopopy{ eh€r

Ted-Eutanol / butyl €lcohol

l,rmioxanQ

Sunogate : 4-Bmnpfl uo@benzeneSu''oga|€] lduene4gSunogste : l,zokhfotuetane44Sunogate : Dlt*onofluorcmethane

LCS aZ031165€5ll

Preparod & AnalFed: 2l -Mar-O7'1 ,1 ,2-Tdd$rokinuoroethane (Freon 1 '1 3)

Adllonilrib

Benzen€

8mlnob€rEen€grotnocibrun6than€

Brcfirodicl{oromelhane

Bsnotoam

BrqrFfir€lfian6

2€ula0on6 (MEK)

n€r|lylb€nz€ne

s€c-ButyG€nz€ne

lert€uty6onz6ne

Carbon di$dfide

Carbon btsd oride

Chlomb€riz€ne

Chloro€$m€

Chlomfofin

ChlotDmohane

2-chb.otoluen€

4thlo{oioluem

1,2{)bronb-Sc$bropropsrF

Diho|ttod orom€then€

1,2-Dbromo€lt|ane (EDS)

BRI.BRLBRL8RLBRLBRLBRLBRLBRLBRI8RLBRLBRL8RL8RtBRLBRLgRL

BRTBRLSRLBRL19.59.844.850.8

21.921.517 .621.122.020.520_521.020.4l7.o20.4n.s22.A16.623-O2't-5r9.520.0m,121.521-517.621.620.6

pclldlpsnpdlpdl

!dl!snusnt8Arc,TEIpcn!gl

tst|lsnusnt'91ps4!Elpglpdl

!dlugl|ldlpsnpsn

!dl!dlrstIrdl|lglpg/l

lrs/l

rs4pdlpdl

tsrugrr9npdl

tjs/|!snpsnpdl

tts/|!dluglttsf,t grl

wl

0.51.01.01 .0t . 01 .01 .01.01-01.01.0t . 01 .02.O1 .010.01_01 .01.01.0t0.020.0

50.050.050.050.o

20_020.020.0m.0m.020.020.020.o20.020.o20.0m.0m.0m.020.020_020.020,020.0m.0m.om.o20.o20.0

99 7&130102 70-1309{t 70-1Wto2 7013t)

110 70.130108 41.1-1178a 7G130106 7&'130110 7G130102 7G130102 70J30105 7G130102 57J,',15185 48.9134102 7G130114 7G130114 7G130s3 7Gr30115 7G130108 70-1309A 56.$ 1,15r00 7G130100 70-1?0108 701301@ 70.13088 70-130108 61-5-142103 7G130

Thi6 bbo.dloty r.port ls ,roa vdld |4ithd.z, .n dud,oriuat slga&A,e on the cova 1ngE.i Reporlabl€ D€tection Limia BRL = Belov Relorting Limir Pag€ 98 of 152

Page 482: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Spike

L€v€l

Source

Result

R}DLimit

%REC%REC LimitsAnalyr(s,

Bdch 7031185 - SW846 5010 Wrrer MS

LCS 17031165€S.t)

Prepared & Anallzed: 21 -Mar-07

Dibrowrodl€thane

I ,2{)idrlorobeozene

l,3OiciloroberEene

1 ,4-Dichlorobenzene

Dichlorodifuoromethane (Freont 2)| ,1 .DiJ\loroethane

I ,2-Dichloroeu|aneI ,1-Oichloroelhen€

cis-1 z-Did{oroethmelrans-1,2-Dichloroethen€

l,2Oichloropropane

1,3-Dichloropmpane

22-Dirhbropropane

I .1 Oichloropropene

cas.1,3Di{:hloropropone

t'ans-l,3oichloropropene

Etrylbeozen€

Hexachlorobutadiene

2+€xa.looe (MBK)

lsopropylbenzene

iiethtl lert-butyl ether

4Jt ethyr2.pentafl on€ (MIB()

Melhylene chbride

Naphttulene

StFgne

1 .1 ,1 ,2-Tstachloroethane1.1,2,2'T€trachloroethane

T€u'achloroeth€ne

1 ,2,+Tncfibrobenzen€I ,2,+Tdchbrob€nzene| ,l , l-Triciloroethane

|,1,2-Trichloroethane

Tdc*ioroetn€n€

TrichlorEf @romethane (Fteon I 1 )1,2,$Tnchbropropan€'1,2,+Trimethy'beruene

'l,3,tTrimehylbenzene

Mny' chbnde

m,pXylene

o-Xylene

Tebahydrcturan

Erhy' elher

Ted-€myl rrehyl ethsr

EflVl ted+uv dher

Di+opropyi eth€r

T€rt€utanol / butyl alclhol'l,4.t)ioxan€

S wrog aE : 1 -B.o mo nu o ro be nzaneSunogate: Toluene4gSunogal€i 1,2.Dk'ilorcelh ana41

19.4

20.5

2 2 4

19.8

21.3

20.6

15.2

18.6

21_7

20.o

20.9

19,9

2 1 . 4

1 9 . 1

21.7

23_2

1S.0

21.1

2 1 . 3

19.5't 8.4

1 9 . 1

17.9

2 1 . 3

21.9

2 4 5

20.1

2 t 6

20,5

16_0

2 1 2

2 1 1

20.2

20.5

20.4

22.1

22.7

22.6

2 2 4

44_4

22.7

14.2

18.2

2 1 . 5

2 1 . 6

20.7

162

r93

53.549.415.8

20.020.o20.020.020.020020.o20.020.020.020_020.020.020_020.020.020.o20.020.020.o20_020.020.020.o2 0 020.020.020.020.020.o20020.o2 0 020_020.020_o2 0 020.o20.020020.040.020.o20.020_020.020.02 0 020020050.050.0500

us/ltrgl

!s/lpgl

!El

l.rg/l

!gn

!s/lpgn

!!t l

uglpsn

QC1 lSn

!s{pg/l

Lrs./lpgl

t g/l

ps/l

udlps4!9/l

iiS/lps/l

us/lu9/lps/l

lig/l

ljg,l

t/gl

tjEl

psnpsnp9l

!gnps,4

usllpgl

!s/l

}l91pg/l

!El

lig/l

!glps/l

lr9l

!cnIE!dlpdl

!91!!y1!91

97 70-130102 70,130112 70-13099 70-130106 36.6-187103 70-1309€ 70-13()s3 70-130108 70-130100 70-1301M 70-130100 70-130136 70.130103 70130107 70-13096 70n30'to8 70-130116 8.7-142s5 56.3-131106 70-130106 7013098 70-13092 55.2.12996 70-13090 70-130106 70-130110 70-130'122 70-130lfi) 70-13o108 70-130102 70-13080 70-130106 70-130106 70-130101 70-130102 70-130102 68.148110 70-130114 70-'130113 7G.130112 7G.130111 7G130114 70-13091 70-13091 57 6-132108 70-130108 7Gr30104 70-13081 70-130

45.2-132107 70-13499 7t)E13492 7G134

Ihk labontory pFod h nol wlil wilhod an at thoriaeit slgnaturc on the.awr poge

'Reportable Det€ction Li&i! BRL= B€low Reporting Limir Page 99 of 152

Page 483: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Vol.dle Organic Compounds - Qurllty Control

Batch 7031185 - Sw846 50J0 Water MS

LCS a703t185AS

Pr€parcd & Amlyzed: 2l -rdar{?

Su nngab : Afuonofu roront€fhane

LCS Duo ?03llE gsoll

P.epared & Analf2ed: 2l-Mar-OI

1,1,2-Trichlorotriflt oroathane (Frsn 1 13)

Ac.ybnitile

B€nzene

Bomobenzen€

Brornochlorornelhane

&omodi$brornehane

Brcftrolorm

Brornomelhano

2€t/hnon€ (MEK)

n€utytb€flzene

s€c-Buvbenzene

t6t-8!tylttenzene

Carbm disulfide

Carbm btracfibdde

Cldorohonzene

Chltoethene

Chlonrbrm

ChlorDrnelhane

24hlorotolu€ne

4Chlorotolu€ne

1,2€bmft o-3{hloropropan€

Dlbromochlorofir€thEn€

1 zoibrornoetnan€ (EDB)

Dibrcrnom€6lan€

1 2-Di{$lombenzene'l ,3-Dichlorobenzen€

| .4-Oichbrobenz€n€Did{,orodifl uorometrtar€ (Freon12)

| ,1-Di{$lorcetllane1,2-Oidhro€lhane'|

,1-Okl$oro€th€nsci+1,2{)id oroettEne

trans.l,2oichlom€thon€

1,z-Oichbrcpropane

1 ,3oichbmpropane2.2OiEnbmpropan€

I , I Oichloropropere

ci9l,3-Dichloroprop€ne

t-ans-1,3oicf o.op.opone

Elhylb€lEene

tlo€chlorobutadisns

2+l€xEnon€ (MBK)

lsopropylb€.Eene

4-lsopropyttolu€n€

Molhyl brl+utyl eth€r

4-lrethyL2f onranon€ (Ml8K)

li4elhylen€ .*rlorid€

l,lsphthal€ne

fi.o

19.3

r8_2

17.3

19.6

20.6

19.4

19.7

20.2

19.5

15.3

19_7

21.9

22.O

16-0

19.9

r g . 1

1E.6

20.o

20.2

17.6

20.3

10.0

19.6

21_O

18.4

r9.1

19.5

r8.8

17.r

N.2

14.2

19_9

19.6

2 4 6

18.3

20.3

18.4

19-9

20.7

t8.6

1S.6

z).g19.1ts.114.2

16.5

psn

rslt d l!dlttslugtlugrtrdlpdl

$/lFg/lvdlug/lpcnpdl

vslysll

Xyl|tdlrgltrdlpdl

rctp9lpdlpdlpdl

!dlIs/l!gruglt d l|ldludlrgl!sn!s4udlpdlpdl

vsludl!dl

|lgl

ljgl

udl|,gnlr3/lFSnllgl

50.0

20.020.020.020_o20.020020.om.020.020.020.020.020.020.020.o20_0m.020.0m.o20.o20.020.o20.020.020.o20.020.020.020_o20.0m.0m.0m.o20.020.020.020.o20.o20.020.0m.020.020.o20.0m.020.o20.020.020.0

100 7G13t)

s6 70.130 1491 41.1-147 l7m 70-130 29a 7G130 I103 7Gr30 797 7Gr30 598 7{)'130 4101 70-130 498 57-7-151 476 48.9-134 11s8 70n30 4110 70-130 4fio 70-130 4m 70-130 15102 70-130 12100 7Gr30 886 56.9-145 1396 70-t30 Is4 70-130 6100 70-130 0101 70-'t30 788 70-130 0106 61.5-142 2102 70-130 194 70.'130 39A 7G130 4r05 7G130 692 7G130 796 36.&187 1098 7{t130 5s4 7G130 286 70-130 I101 7G130 791 70-130 9100 70ns 49a 70-130 2123 70-1n t0s2 70'130 t1r02 7G130 592 70.130 4100 7Gr30 8104 8.7-142 1193 56-3-131 298 7G130 I'1& 7G130 296 7S.130 2s0 55.2-129 29t 70-130 5a2 70-13/J I

2550252525

25

5050252525

25502525

25

50252525

255025

2525252525252525

5025

255025

Thb bbonlory ftpon k not edid Niahout ad a4thortzcd tlgnatur. on th. @re. Fgc.. ReF6rtable D€tection Limit BRL = B€low Repoding Limit Pa€€ 100 of 152

Page 484: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgar c Compouads - Qualitj,Controt

Spike SourccAnalyl€(s) Resulr Ftag UDirs *RDL Lcvcl Result %REC Limjts Rpu Limrr

Brtch 70l l lEs - sw846 5010 water Ms

%REC RPD

LCS Duo (703118$BSD1l

Preparsd & Anatyzedr 21 +tar{7

tFPropylb€nzene

Styrene

1 , l ,1 ,2-Tetrachlorcethane1,1,2.2-T€trachloroethane

Tetrachloroethen€

1,2,3-Trjchlorobenzen€

1,2,+Tridrlorobenzene

I, |,1-Tdchloroehene

1 ,1 ,2-Tricnbroethane

Trlchloronuoromethane (Freon 1 I )1 .2,3-Tdchbrcpropane12,+Trim€lhyibenzene

l,3,tTrimethylbenzene

vinyl chlodde

m,p-xylen€

o-Xylene

Tetsahydrofuran

ElIy' etrcr

T€rt-€nM melhyl ether

Ethyl ted.buty eth€r

Oiisopropyl ether

T€rt€utanot / butyt alcotrct'l

,4-Oioxane

S utqale : 4 8m mofr uorcbe nte n eSqrcgate: TokEne4SS tnogate : 1, 2 - D i ch loro et h a ne 4 4SuEogEIe : Dib toltio fl uoone lha n e

iletrix Soike (7031 1 85.USl I

PtEpa.ed & Analyzed: 21-MaF07

Benzene

Chlorobenzene

l!l.Dlchloroethene

T.iJ orc€tlEne

Swwate: + Bro zmfl @ mb e n ze n aSltarogale: Tohtene4SS u rraga le : l, 2 - Dktl lo roel h a ne4 4S u nqa te : D ibrc m o n u otu m eth a ne

20.0

20.3

22.2

19.5

19.2

19.0

14.7

20.1

19.1

19.7

14.7

1 8 0

21.1

21.9

21.2

19.8

41.4

21.6

17.S

1 4 1

2 0 8

21_2

20.1

162

179

52.149.945.949.7

Sourc€: SA59.l70{l

23.324.82't .523.522349.750_44 7 4495

ps/lpsn

ugrudl!91

ugn!g l

ps/l

!94

trg/r!s/lt9lltrglusn!g l

!dt!g/1!s/lLj(yl

pg/l

tgtl

v9ulylpsntsllu9luglusnwll

20.020.020.020_020.020.020.020.020.020.020.020.02002 0 02 0 020.040.020.0?0-020.020.020.020.0200200so.o50.o50.0500

20.020.020.020.020.050.050.050.050.0

?0.020.020.020.0?0.050_050.050.050.0

r00 70-130 6 25

102 70-130 8 25

111 70-130 I 25

98 70-130 2 25

96 70-130 12 25

95 70-130 1 25

74 f0-130 6 25

100 70-130 6 25

96 70-130 10 2596 70.130 3 25

94 70-130 8 25

s0 68-148 12 50106 70,130 4 25

110 70-130 4 25

106 70-130 6 25

99 70-130 12 25104 70-130 7 25

108 70-130 5 25

90 7G130 1 25

90 57.6-132 1 50ro4 70-130 4 25

106 70-130 2 25

100 70-130 4 25

a1 70-130 0 25

w 45.2-132 6 25

to4 70'130lM 70-13092 70-13099 70-130

aRL 1' t6 70-130

aRL 124 70-130

aRL 108 70-1 30

BRL 118 70-130

aRL 112 70.130

99 7G1m101 70-13095 7013099 7G130

BRL 114 70-13D 2 30

BRL 124 70-130 0 30

aRL 108 70,130 0 30

BRL 119 70-130 0 30

BRL 112 70-130 0 30

98 7Gl3t)101 70-1U95 70-tU101 70-tg

t{atlx Solk€ Ouo fl031'185-Irl$}l) Source: SA59,tZ0.0.lPrepared & Anatyzed: 21-Marfl

B€nz€ne

Chlorob€aEene

1 , l €ichb.o€th€ne

Toluene

Taldlloro€tn€n€

S/ntwate : 4 - Brono nrc robe n zeneSuiqate: TohEne4SsJrno ga E : 1, 2 -D i dl Io rceth a ne 4 4S unogate : Dib rc mon rcroneth a n e

Brtd 7m1l$- SW846 s030 Soit (high levet)

23f

24.7

2 1 . 7

23.5

22.3

49.250.747_450.5

p9l

pgn

!q/l

!9/lpgl

!Elrg/luglps/r

!gl

ps,l

!g/ltlgJl

!g l

rcl!g/l

!s,4!sn

Thk lal0rotary rcport is nol wld wilhaar ai a!rtodast signtdtrc oa the coter Fge .

a Reportable D€tection Limit BRL = B€low Reporting Limit Pase l0 l of 152

Page 485: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgrnic Compounds - Quality Control

Br.ch 7031ttlt - sw8,t6 5030 soil (high level)Blen* 17031180€LKl)

Pr€pared & Analfred: 21 -llar47

1 ,1 ,2-Tnd{oroffiuoroethane (Freon 1 1 3)

Acrylonilrfle

Benzen€

Bromochbromethane

Bromodid oro,nethane

BrorElorm

Bromon€han€

2€utanorc (MEK)

rFBulylbenzene

sec-gutylb€nzen€

t€rt-Bu\lbenzene

C€rbon dlsutfid€

C€rbon tehad|bride

Chlomhenzene

Chbro€thane

Chlo|obrm

Chlorornelhane

2{hlorotolo€neil-Chlo.oto|uen€

l,2.Dibiomoj-drlorcpropan€

Dilbrornodbmdetlran€'1,2-Oibromoehan€ (EDB)

Dlkomomethane

1 Joichlorobenzene1 ,3-Dichbrobenz€ne1 ,4.oichlorobd|z€neDicf*omdiffuorornofi ane (Freonl2)

I,I-Di{r oroe[tane

I ,2-DiibroetEn€1,1€ichbrc[Ene

cis-l,2.Dichloroetherle

transl,2oichloroeth€n€

| ,2-Okhlo.op.opan€|,loit oropropEne

2,2Oi* oropropane

1 ,1 Oichbrwropene

.js-1 ,+Dichlo|lpmp€n€

lrans.l,3oichb.opropene

Ethy&enzens

Heiacl{orobulsdiene

2+ler€non€ (MBK)

lsopropyb€nzene

4-lsopropytbluene

lil€thY lert-butyl 6ther

4{relhyf z{€otanon€ (MIBK)

lrethylen€ drloiir€

Naphthal€n€

n+aopylbsEs|e

SVr€ne

1,1, 1,2-Tehechlormthan€

1,1,2,2-T€fudtoroothan€

BRL

BRL

SRL

BRI

8Rt

BRL

ARL

SRL

ARL

BRL

8RL

BRL

BRL

SRL

BRL

BRI

BRL

BRL

BRL

ARL

BRL

8RL

BRL

BRL

BRL

sRtBRf

BRL

BRL

BRL

ARL

BRL

8Rt-

BRL

BRL

BRL

SRL

SRL

BRL

BRL

BRT

BRL

ERL

BRL

BRL

8RL

BRL

8RL

SRL

BRL

BR,L

BRL

pdks

!dksfldksrcftsrrs^o!sftspdksudr9usn(s!g/kg@ksrgksPdkgudksps/kslsiks!sftspdlg

!drsrdkswr(gpErlspdkspdts

1 .020.01.01-O1_01.0t . 01 .02.O10.01.01.0t . 05.01.01 .02.O1 .02.01.01.02.01.01.0

ldr€ L0

udl€ 'l.0

IdfiS 1_0ps/€ 1.0

lgxg 2.0

tglq r.0

ldks |.o

ldr€ 1.0

lgr(g 1.0

rrdks 1,0psikg 1.0

UqtS 1.0

ldxs 1.0

ttgks 1.0

FSftS 1-0psrlq 1.0

tdtg 1.0

lrgftg |.0

ldkg 10.0ggrq 1.0

ldks 1-o

rdkg 1.0

FdkS 10.0pC4(9 10.0pgl€ |.0

Itglks 1.0pdkS 1-o

lrgikg

Pdllg

1.0t.o

Thb labraloo Eport ls ttd tditt utthoU on aadtorizd stgaagE ofi ahz crver Fge.+ [email protected] Derecriofl Limit BRL = B€tow R€porting Limit Page 102 of152

Page 486: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qualiay Coltrol

Arlalyte(s) Resuh Flag Units

%REC%REC Limits. RDL

Spike

l,ev€l RcsultRPDLi'nitRPTJ

Bahh ?031189 - 5118{6 50J0 Soi l (h igh teveu

Slank {7031t0!I.BLK1l

Prepared & Anatyzed: 21-Mar{7

Tehaciloroeth€ne

Toluens

1,2,$Irichlorob€nzene

1,2,+Trichlorobenzene'1 .1 ,1 -Ttichklro€than€

1,1,2-T.ichloro€thane

Trichloroethene

Trichlorolluoromeft ane (Freon 1 1)1,2,lTrichlorupropane

1,2J-Trinethylbenzene

1 ,3,$Tdmetnylb€nzeneVinyl cnlorid€

m,tsXylene

Tetr$ydrofuran

Ef'yl ether

Ten-amyl ncthyl ether

Elhyl tertnuv elhe.

Di.isopropyl efier

T€rt-Butanol / butyl alcohol'1,4-Dioxane

Chlorobenzene{5

1,4-Oichlorobenz€ne-d4

S utrog ale : 4 -*o mofl uo tobe n zeneSuftogate: Toluene-d8Sutog ate : 1, 2 -D i c h lo roetha ne 4 4Suft og ale : D ib mmo ll u oro m e th a ne

LCs f'031-t89€S

Prepared & Anal)rz€d: 21 -Mar{7

| ,'l ,z-Tricilororrinloroethane (Freon I 1 3)

Actylonitflle

Benzene

Bronoafilororhstnane

Blolnodidrloror.flehane

Bromoform

Saornomethane

2€ubnone (MEK)

n€ulyhenzen€

s€c-Butylbenzene

tert-B0tylbenzen€

Calbon disulftde

CElbon telracfibnde

Chloaotlenzene

Chloro€'1ene

Chlomform

Chloromelhane

2€trloroiolu€n€

44rlorcloluene

l.z.l)blomo3drloropropan€

BRL

8RL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

ARL

BRL

ARL

ARL

BRL

30_o

3 0 0

3 0 0

32.230.232.8$_4

20.7

2 1 6

23.1

18.8

2 1 . 6

20.2

20.8

2 3 0

19,1

20.6

1 9 3

1S.7

20.3

20.8

1 9 . 1

20.8

19.9

20.s19.920.320.42 t . o

!s/xsgEKg

ugKsFgIKg

!q(9psrKs

p94(s

LiS/kg

LjgKs

ug/Kg

t g/kg

ugxsp9Kg

!9/r(gLis/Ksp!yKgpg/kg

rjgxsuEksUEKg!gr(gps/kspg/KgpE(g

!s,Kg!gl(sugftspgks

ugKsudkspg/ks

LIEKSt/g/x9psft9

Pgkspdks

!9Kgpg/|(9

!!yKgpsfts

t gKg

t S/kg!gKgFS&Spqk9

!sftsg/ks

!s/ks!gKsygKg

l 01-O'1 01.01 .01 .01 .01 0'1.0

1.01.01 .02.O1 .01 0 01.01 .01 .01.010.020.0

30-03 0 030.030.030.0300300

20_o20.o20.020.o20.020.020.020.020.020.020.020020.020.020.020.020.020020.02 0 020.0200

u.1 50-200

76.5 50-200

85 50-200

107 70-130101 70-130109 7G130101 70-130

104 7G130

108 3 31-159

116 70-130

s4 70-130

108 70-130

101 70-130

104 70-130

115 70-130

96 50-140

103 47.7-127

96 70-130

98 70-130

102 70-130

104 70-130

96 70-130

104 70-130

100 55.9-135

1M 70-130

100 70-130

102 70130

102 70-130

105 7Gr30

Thit hboralorr repod is trot ytlid vithoat on adhonzed slgnda,e oa the .atet page

I Reporlable D€tection Limit BRL= Below R€poning Linit Page 103 of152

Page 487: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Vol'ailc Organic CompouDds - Qurlity Cooarol

Anslyt{s) Result Flag

SPike*RnL lrvel

SorEce y.REC

Result %REC Lin bUnits RPD

RPD

Limit

B.rcl 703118' - SW846 5030 Soit (high tevel)

t9s_tr93!L9935.!lPr€Fred A Anal}.z€d: 21-[,!ar-07

Dibrom€hbrom€lhane

l,2oibronoethane (EDB)

Oabromoin€lhane

I ,2oidrlorobenzene| .3-Dldrlorcbenzene| ,+Dii* orob€nz€ns

m.521.5

2r.220.420.520.120.214.?20.917.620.018-419.919.917.3r8.62 0 120.1m.,rm.3

19.220.322.319.619.019.019.221.7

19.01E-5

20_219.321.8rg .1ts.325.1N.720.41S . t40. I2 r , 123.E20.92'O2r.921.12@

rgr(gpdlqgpsfts

lgkstl/l€ps'xg

!gxs!gt€

usiksps/ksps/Bst'dts!gts!crks!gkg!dxsudkst,9Kg

|lgKs

uslksrgftsugftslrBftspExgvsikgusiks!sftsps/xgpsag

Fdkspgrspgftg

Fdkgps/ks

Fdkg

!dl(g

!g/kS

!gn(S

udts[9K9

ugftsrs/ks!s/kgpgn(sudksldkspsnq

wr€!cftsrdks!dkspgl(9

20.020.o20.02().020.o20,o20.020.o20.020.020.020.o20.020.020.o20.020.0m.020.0m.020.0m.020.020.0z).020.o?0.020.020-020.020-020.oz).020.0m.o20.020.020.020.om.0m.020.020.o40.020.020.020.020_o20.020.o2U)2m

72-12570-1307Gr307G13()7G13070-'t30

102t08r06102102100

I ,1-Didrloroethane1,2-Di$broethane'1,1-Olchloroethene

cis-1.2{)icfi loro€th€n€

t€ns-l,2oidloroethane

1,2-Dichbropmpane

1 ,3-Oidbmpropans2,2{)ichlorop|opsne

1 ,1 Oichbrop.op€ne

cis-1.3-Dichloroptopsn€

tlans-1,3oichloroprwene

Ethylbenzene

Hoxachloroduladiene

z+lexenon€ (MBK)

lsopropylbenzene

4lsoplopy4td|Ene

UetM !6n-buvl €ttl€r

4-M€f ryl2{€ntanone (MIBK)

Metlry'ene ailodde

Naphhalene

stren€

1,'1,'1,2-Tetrad oroehane

1,1,2,2-Tetrad orcethane

Tet"achloroelh5i€

1,z,}Tridrt .lbenleite

1 .2,+Tdd$robenz€ne1,1,1-Trichloroethane

1,1,2-Tichbroehane

Trichloaoehen€

Trichlorofluolome$an€ (F.eon 1 I )l,2,STrichlo.opropdn€

1 ,2,+T{ime$ylbenzefe

1 ,3,$T.im€|f|Ybel|2en€Vlnyl drlodde

m,Fxylene

o-Xylen€

Tet"ahydFfuren

Etlryl ether

Tert-aftyl rlothy' €tt*r

E{V te(-hnyl other

Oi-isoprooyl ad€r

Te.t€utand / bdyt atcohol

1,+Dioxane

(Freon12) '101 42.3-19094 70-r3o104 70-1308B 7Gr30100 7G130s2 7G130100 70-.130100 ro-1986 70-130q) 7s.130rQo 7G130100 7G130100 7u130102 7G1X7108 7G13096 7G130102 7Gt3o112 7G130s8 ,t8_5-127

95 70-13095 70-13)96 70-130108 7G130113 70-130112 70-13095 70.13002 7G.130r12 70.130101 7G'130!6 7G130r09 7G13096 7Gr 3096 66.5-1441m 7Gt3()104 7G.t30102 7Gt309G 70-130100 ?G130106 7G130118 70-130104 64.$.123110 70-130110 70.130106 7G130r00 70-130l0O ,1G134

ThB lttatuloty rqo.l,s aot ezltl Nihoa a, a.tlerid,tignetu.c on ih2 cor,t poge.

. Reporhblc Det€ction Limit BRL = Below R@orting LiEir Poge l(Xof 152

Page 488: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

%R-ECAnaltle{s) Resuk Flag Units *RDL L€vet Resutt %REC Limirs RpD l_imu

B.act 7031189 - SWA46 5030 Soit (ftigh tevet)

Spike SoDrce

LCS ff031189€S

Pre9a€d & Anal]rred: 21 -Mar{7

Fluorobenzene

ChbrotEnzene-d5

1,4-Okft lorob€nzen6.d4

Su nogale : 4 4rc mon u orc b e n ze neSurogale: Toluene4SSutlog€le: 1, 2aichloroethane44S mog ale: D i b ro no fl u o ro m e t h an e

LCS Oup ?03llag-BSOI)

Pr6parEd & Anal].zed: 21-Mar-07

1 ,1 ,2-Tdchbrotrinuo.o€thane (Freon 1 1 3)

Acrylonfie

Benzene

Bromochlorohletlane

Brotudichloaomelhan€

Brooroforrn

EronEmo[1ane

2€uhno{e (MEK)

n€u@eizene

sec-Bull/lberEme

terl€uty'benzene

Carbon disulfids

Carbon tetsc* oride

Chlorobe$zene

Chloroetian€

Cl oroform

Chloromethane

24hlorolol0€ne

44hlorololuene

l,2.t)btomo-3drloropropane

Dibiomochlorom€tf|ane

1,2-DbtornoetwE (EDBI

Dlbromornehane'l:-DiJ|lorcb€nz€rc

I ,:|-Dicuorob€nzene1,4-Oict$oobenzene

Did orodifl uorom€thane (Freonl 2)t , t Oicttoroettlane

|,2-DicHoroehane

1,l-Did oroethefle

d91 .2oichloroelhene

hEls-1.2{idtloroefhene

1,2-Dlc oropropane

1 ,Soiddoroprcpane22Jirtlloropmpane

1 , I -Didrloroprop€ne

d+1 ,$Dichloropropen€trans-1,3{ichloropropene

Ethylb€nrene

tlexac{ orobutedien€

2+lex8tEne (MBK)

30.0

30.0

30.0

32.229.631.630.6

1S.6

19.5

2 1 . 6

1 4 2

20.0

1 9 . 1

20.2

22.5

19.4

16.8

17.9

14.7

19.4

1 8 . 1

19.0

18.9

19.7

1 9 . 1

18.4

19.8

20.6'19.8

20.9

20.4

r8.7

1 9 . 7

1S.0

1 8 5

18.3

1S.S

17.4

19.0

r7.9

19.1

18.6

16.3

1 6 . 3

19.2

1 9 . 7

19_2

19.6

!s/ksps/ksJ.igK9

!9KStl(!KgtjgKss/ks

tls/ko

l.rgKs

!g/Kg

ug/K9

Lrs/Kspgt,<g

!g/rq

wxsvg/Kgug/rq!s,Kststxsl.,g/K9wl(gt s,xspgKq

lrs/Kgwxsps/ks

ug/KgtrgK9t g/Kgpg/x9pgtK9

!dksIS/KSps/K9

ug/rcr.igKs

wKs

!gKg

Ll9Kgpg/Kg

udksps?Ks

trS/kSg/K9

!gKgus/kg!qkgps/ks

FdkSpgks

30.030.030_0m_0m 0300m.0

20020_020.020.020_020D20.020020.020.02 0 02 D O20.02002002002 0 0m.o20020020.o20020_o20.020.o20.020.020020_020.D2 0 02 0 020.020.020.020.020.o20_o20.020.020.om.020.0

98

s8108

91

100

96'lo1

112

97

u90

94

97'r01

90

95

94

98

96

92

99'103

99

104

102

94

98

95

92

92

100

a7

95

90

96

93

82

92

96

98

96

98't06

r05 5G200s9.6 50-20098_3 50-200107 70-13099 70-130105 70-1fi102 70-130

70-130 6 253.31-159 10 5070-130 7 2570-130 3 2570-130 A 2570-J30 5 2570.130 3 2570,130 3 2550-140 1 50

47 7-121 20 5t)70-130 6 2570-1N 4 2570-130 5 2570-130 3 2570-130 6 257G130 9 25

55.S135 6 5070-130 E 2570-130 4 2570-130 10 2570-130 3 2570.130 2 2572-125 3 5070,13D 4 2570-130 4 2570,130 A 2570-130 4 2570-130 s 25

42.3-190 I 50t0-130 2 2570-130 4 2570-130 1 2570-130 5 2570-130 2 2570130 4 2570-130 7 257G130 5 2570-130 1 2570-130 4 2570-'f30 2 2570-130 470-137 4 n70-130 2

Thb labotuotf Eport ir not valid wirhotd an otrtodzed signattare ott lhe cover page.

a Report ble Detection Limit BRL = Below Reporting Lirnit Pas€ 105 of 152

Page 489: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qodity Cotrtrol

Spike

Bahb ?031189 - SW846 s030 Soil (high t€vet)

LCS DUD ?0!1189-BSD1l

Prepa.ed & Amtf.6d: 21 +rar47

lsop.opylb€rEene

+lsoprEpyhol!9n€

ftrethyl tert.butyl €trler

4-tvlethyl-2+€ntafl on€ (MIBK)

tirethyl€ne d\lortd€

Naphtfialene

n-Propylb€rEene

Styrene

1 ,1 ,1 .2.Totrdchlclrelhane1 , | ,2,2-TshachloroetheneTelEchlo(€then€

Toluene

1,2,3-Trid orobenzenei 2,+Triaillo,rob€ruene1 ,1 ,1-Triciloroehane1,1,2-TrichloroothanB

Trichloroethe{F

Trichkrofuoromefhano (Freon I 1 )12,}Tridlloroprlpane

1,2,4-Trim€hytbenz€ne

t,3,ST,ime'|ylb€nzene

Vinyl ct{orid€

m,p-Xy'sne

o-Xybne

T€trahydrcturan

Etiyt ether

Ten-amyl nt€hy' etrer

Elhyl te.t+ury' stherDi-isopropy' eth€rTert-Butand ./ buv atcohol

l,+Dbxane

Chlorobenzeneds

1,4-Dicfllorohen2ro€d4

S urcg ate : +gdnofl uoraf en ze neSu''-oEal€: fotuane4SSu nlj4atd 1,2 D b h I o rcet h a ne4 4S unogab : Abdrc fl uorc m eth me

B.rch t031233 - SW846 5035A Soit (low tevel)

g|enr aTo3lru€LKl)

Prgpar€d & Ansl].ied: 2l-M€r-t)7

1.1,2-Trichlortiiuom€th€ne (Fr€on 113)

Asyh{reib

Benz€'re

Bronob€nz€fle

Broftrdrlounefiane

Aromodidrlo(om6tn€ne

Aroanofofln

Brcmornelhfl|o

2€ubnon€ (MEK)

n.8ulyllbsnzene

s2 70-130 496 7G130 6105 7Gi30 696 44.5-t27 290 70-130 588 7G130 I96 7G130 0105 70-130 3tfti 70-130 6r08 70-1gt 492 76130 3go 7Gt3t) 2104 70-130 705 70-130 69t 7G130 5107 7G130 294 7G130 296 66.5n,|4 0122 7U1T 399 7G130 599 70-130 3u 70-1m 13ss 7Gr30 1r01 7G130 5'fi8 7G130 098 6r.$.123 6105 70-13/J 5iM 70-130 6100 7G130 696 7G130 4114 4$.134 13103 5&200101 5G200r05 5G200106 7o.BAtol 70-1tutos 7G1301m f+lfr

18.3

19.3

2 l . o

19.2

16,0

l f .5

1 9 . 1

21.0

2 1 . 3

21_6

t8.4

1 7 . 9

20.8

19_0

18.2

21.4

1$.e

19.1

24_3

19.8

rs.8'16.8

39.7

e3.6ts.62r.o20.820.019122930.030.030,031.830.23r.630.6

20.0m.020.020.o20.020-0m.020.020.020.0z)-0m.020.020.020_0m.0m.020.om_020-0mo20.040.020.020.0z).020.o20.020_02m20034.030.030-0fi.o30.ofi.030.0

rdksldksvdksPe/kgpdks

!gl€|ldksugtqugrgudrsLjgkg|Islksrdkg9gtSpdks

udks!clq

lrgt(g

!Et(gpcaguqksps/kspdks!dxsPglq

t/dlslrsftst ckoFs/kspgl(srdl(suglkgt srxs|ls^9!dl(gpdkg|ldkstrsfi(g

lrdkgv{et 5.0

rcAgwet 100pgtg $,et 5.0

lgtS trel 5.0

US/kS Yret 50

rur'kg 'ret t0

Igko{et 5.0

trSftSw€l 5.0

!glkg$/€l 10.0

Igl(g Niet 50-0ISftS N/st 5.0

x25255025252525

2525

252525

25

2525252525g)

25

252525

BRLBRLBRLARL8Rr-gRL

ARLBRIBRLBRLBRL

This lsbrttory eport is t ot r'llitt withou at osdtodtj signart c o,. thz coter page .

t R€portrble D€t€ction Lidit BRL = Below R.porring LiEit Page 106 of 152

Page 490: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Spike

L€vel

Source

Resull

RPDLimit

%REC

%REC LimitsAnalyte(s)

Batch 70f,1:3J - SW846 5015A So[ {hw lrvcl)

Blank 17031233€LKl)

ftepared & Analyzed: 21-J\,4ar{7

sec€uMb€nzene

{ert€ulylbenzene

Carbon disulfide

Carbon bnachbdde

Chlorokenzene

Chlorc€thane

Chloroform

Chloromelhane

2Chlo.otoluenetl-Chlorotoluene'1,2-Obmmo3-chloropropane

Dibromochlorornethane

l2oibrodoethan€ (EDB)

Dlbrornomsthane

1.2-Dichlorobenzene

t ,SDicnbrobenzene1,4-Drcnbrcb€nzene

Dichlorodif uorometharie (Freon12)

l,lOichlorcehan€

l,2oichloro€thane

1 .1 Oichloroelhen€

cis-l,2.Dichloro€th€ne

tfan+1,2.Dichloro€thene

l,2.Dicfiloropmpane

1 ,3-Did oropropane

2,2.Did orcpropan€

1 ,'l Olthloropropene

cis-1,3-Dichloroprop€ne

tr ans'1,3-Dichlotgpropene

Ethylbenz€ne

Hexachloroburadiene

2+exanone (MBK)

lsopropylbenz€neiHsopropylloluene

Lielhyt led-b'rtyl €th€r

4-lelehyl-2{€ntanorE (MIBK)

M€thy'me dbnde

Naph0Elone

n-Propylb€nzene

SVrene

1,1.'1,2-f et-dchloroe$ane

1,1,2,2-T€trEchloroethane

TetEchlorc€thene

Toluen6

1 2,lTrichlorobenzen€'1,2,4-Tdchlorob€nzene

| ,l ,1-Trichloroehane|.|,2-Tricr oroohane

Tri*{oroetlEne

Trichb.onuommelhane (Freon I 1 )t 2,STrfuhloropopan€1 ,2,+Trtnethy'b€nzene

BRL

BRf

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRI.

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

BRL

8RL

ARL

ARL

BRL

8RL

8RL

BRL

BRL

BRL

BRf

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

SRL

SRL

BRL

BRL

iig/(g wet 5.0

!g/kg wet 5-0

lgr'kg wet 25.0

!g/kg wet 5.0pgrkg wet 5.0pg/kg wet 10.0

!S/kS Yvet 5-0

!g/kg rvet 10.0

ug/kg wet 5,0pg/kg wet 5-0

!g/kg wel 10 0

Ugfig wel 5.0

!g/kg wet 5.0

!g/kg vret 5.0pS,4(S,.vet 5.0

!g/kg wet 5-0

ugL/kg wet 5.0

fg/kg wet 10.0

Ug/kg wet 5.0pgr'kg wer 5.0pg/kg wet 5.0pgr'kg wel 5.0

lgikg w€t 5-0

tS/tS rvet 5.0

t/g/kg wet 5,0

ttgL/kg wet 5.0

Ug/kg wel 5.0

tig/kg wet 5.0

!g/kg wet 5.0pg/kg w€l 5.0

pgks ',vet 5.0pgr'kg wet 5O.0

!gI(9 wet 5.0pg,rkg wet 5 0pg/kg wet 5.0

UgL/l(g wet 50.0pg/kg wet 50 0

!g/kq wet 5.0

lgrkgw€i 5.0

Ig/kg wel 5.0

tjg/kg wet 5.0pS/kS rv€l 5.0pgkgwel 5.0

lrgftgw€t 5-0

ldkswet 5_0

Pg/kg',et 5.0

Ug/tg wet 5.0pgr'kg wet 5.0

!g/kg wet 5.0

Pg/kg w€t 5.0

lglqwet 5.0

Ig/Xg wel 5.0

Thh lalotulary repon is not valid withoaa an a./hottzd s,ignalure od tht .ove! page.

* Reportable Detection Limit BRL = Betow Repoding Limit Page 107 of 152

Page 491: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgrric Compoutrds - Qudlty Control

AnalyteG) Result .RDLSpike

lllte)

R-PDLimitFlag RPDUnits

Sowre yoREC

R€8Uh %REC Limits

Batch 703123f - SW846 5035A So (tow levet)

glank 1703123€LKtl

Pre9ared & Analfr€d: 21 -Mar{7'l,3,$lrimethF€nz€n€

Vinyl drlodde

m.Fxylene

Tetrahydrofuran

Ethyl ether

Tsrl-emyl m€thyl ether

Ethyl ,e4.buM ether

Di-isopropyl etn€r

T€rt-Butanol / butyl alcohol

l,4oloxane

S u nqate : 44to nnfl uo rcbe n zaneSurogale: Tohtene4SS u nagale : 1, 2. D ich lo tueth ane 4 4S ulw ale : O i b rcmofi uo tomet harc

LCS t7031233€{ )

Preparcd & Analfzed: 21-Mar-07'1,1,2-Trichloroffiuoroethane (Freon 113)

Acrylonirile

8€nzene

Bromob€nz€ne

Bomochlorom€harF

Bromodichlorcoethane

Bromofom

BrofrEmeihane

2€utanone (M€K)

nSutybenzen€

s€c4uty'benzene

tsrt-Butylbenzene

C€rbon disulnd€

csrbon tet-adbdd€

Chlorob€nzen€

Chloroethane

Cldorofofm

Chlomm€flans

24rh,rotolu€n€

44hbmioluene

1,2-Oibromo-3dforopropan€

Dibfomochbrom€than€

1,2-oihromoolhan€ (EDB)

Dibrornorn€than€

1 ,2.t)idlbrob€nzen€1 ,3-Didbmb€nzene'l,iloicnbrob€rE€ne

Did orcdlffuorom€ttun€ (Fr€ont 2)1 ,1{)ichloroethdtel,2oiahloroethen€

1 ,1Oic*lloro€thenecis-'1,2-Didrlo.oeth€ne

rans. l,2oichloaoethene

1 ,2.Dlcfilo|opropene

8RL

BRL

8RL

BRL

BRL

BRL

BRL

ERL

BRL

BRL

BRL

52.052.756.052.0

12.9

18.0

19_1

18.3

1 6 . 5

19.9

20.o

1t -g

15.6

r9.019.4

20.0

17.2

16.0

19.3

r8.318.018.1

18.5

10_3

17.2

18.3

20.3'19-3

19-2't 8-2't8.2

t4.E19.2t7.s17.O,t9.0

r8.5t9.2

pdkS r€l 5.0

Fdkg rsl 5.0

t gts wst 10.0

lgr'kg v/et 5.0

lgkS w8t 5O.0

Ugllg x,et 5.O

Ig/kg egl 5.oygr'kg w€t 5.O

Ugdtg wet 5.0

lgr'kgw€t 5O.0

pg/t€wel 100

yg4€ wetpgr'kg wel

!g/kg wet

lgftg uret

H4kg x,et

!g'l(9 w€t

ldlS i€t

pdkS {€t

!g/kg wet

ldl(g $'st

ldkg wet

UgftS vr.t

Ugr'kg w€t

ugr'kg wEt

lgr'kg wetpqkS wet

t gftg w€l

Wikgwet

Ig/kg wel

[gl!g wel

liS/kS rst

IE?€ w€lpSrlq r4lpS/kg wel

9gkg rv€lpgltg w€l

lrgftg est

ldkS rEt

ldl€ r'/et

ldkS rvot

tgLllg wet

ugLnlg wet

|lgr'lq v',Bt

Hgr'kg wst

|lgl€ wsl

Igt'i€ vret

!gl!g w€t

Ug/t(g wet

|l€/kg w€t

101 70-130IOS 70"13t)1t2 70-1n1U 70-130

r08 70.13064 3.31-15990 7Gr 3096 70-13092 7G13082 7G130100 70-130100 7Gr30g) 5G140fB 47.7-12795 7G130s7 7G130100 7G13086 7G130s0 70-13096 70-13092 55.S13s90 7G13090 70.13092 70-13096 70-13086 7Gr3092 72-125102 70.130s6 70-t30s6 70-130s't 7G13t)91 70-13074 42.3-19096 7G130I 70-130&5 7G13095 70-130g2 70-1?096 7G130

fi_ofi.0

50.0

20,020-020.o$.02t).020.0a).020.020.o20.o20.020.020.020.020.020_o20.020.o20_020.o20_020.020.o20.020.0m.020.020.0m.020.020.020.o20.020.020.o

Thk lab.obry epoA h not salid )rlthour on osdroftd slgEatuE oz thz er.r Fsge.' Reporlnble D€r€ction Limit BRL = Below Repo{ting Limit Page 108 ofl52

Page 492: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgsnic Compounds - QuNlity Control

Sprke Sourc€ %REC

70.1303.31-15970-13070-13070.13070n 3070-13n

RPDA-uab'te(s) Result FlaB Unirs |R_DL Level Resulr o/"REC l-imirs Rpfr Limit

B{tch 70312$ - SW846 5035A Soil (low t€vel)

LCs f7031233€S

Pr€parsd E Analfzed: 21-Mar{7

1 ,3-Dichlorapmpane

2,2.Dichloropropane

| ,1 Oachloropropen€

cis-1,3.{)1*loropropene

trangl,3-Oichloropropen€

Et\/b€nz€ne

Hexachlorobuladiene

2-H6)€nooe (MAK)

4-lsopropyftoluene

Lrolhy' brt$utyl elhet

4-lrethyl-z-pentanone (MtBK)

Lr€tryl€ne cibdde

Naphlhelene

Styrena

1 ,1 , |,2-T€tachloro€tnane

1 . t ,2,2.Tetachloroethaneletradiorceth€ne

| ,2,}Td$brobe|Eene1,2,+Trichlorobenzene

1,'l,1-T.idllorcelfEne

| , 1,2-Trij{oroethane

Trichloroethon6

TdJ oiofluororn€hane (Frcon 1 I )| ,2,}Trid$ropropane1,2,+Trimethytbenzene

1 ,3,STrimeftylbenz€neViny' cfioride

m,p-Xylene

o-Xyl€ne

Tetrahydrcfuran

Ethyl ether

Terl.dhyl n€hy' ether

Ehyl hrt+utyl eher

Dl-isogopyletle.

Tort€utanol / butyl €lcohol

1,4-Oioxan€

Su noga f e : #Jro n ofr u orc be nzen eSwrogde: fduen648S,J/'og ate : 1,2 D i ch I oro eth a ne 44Sfi ogate : D lb rcmofl u o @ nelh an e

Lcs Duo ?031233.8so11

Prepared I Analf2€d: 21-t ar-07

1,1,z-Tdcnbroffiuoro€thane (Freon 113)

Aclylonitrile

Benzehe

Erooobeoz€ne

Bncmocilodorn€thsne

B{oanodichlorornethane

19_3

1 7 6

1 9 3

20.4

20.r1S.3

14.6

14.7

1 7 . 7

19.6

14.6

1 6 I'17 2

2 0 3

19.6

18.7

19_7

17.6

21_O'16.7

20.0

1 8 . 8

17.6

20.4

2 1 . 2

19.2

20.5't9.3

19.3

20.1

37.7

18.8

16.5

1S.6

21.O

20.6

18.3

150

189

49.651.849.440.8

20.4

13_2'18.8

19.4

19.2

1E.0

1S.0

lgr'kg w€t

ug/kq wel

Fg/kq wel

ug/to wetpg/kg wet

!g/kg wel

Ug/kg w€t

ugLikg wer

!g/kg wet

UgI(g wet

uS/kS wel

Ug/Kg wstpg/kg wetpg/kg wet

trgL/kg wet

Ug./kg wst

!g/Kg wet

lgftg wet

ug/kg welpg/kg wel

t g/kg wet

!g/ko w€t

ldkg wet

l./g/kg w€t

ugikg wet

!g/kg wel

Ugy'tg wel

ug/kg wel

lgr'kg w€l

ug/kg wel

Pg/kg wet

UgL/kg w€l

ugL/kg wel

Ugy'kg wet

psn(g Yv€t

Ugy'kg wel

ug/kg wet

Ug!4q w€l

Ugy'kg wet

!g/t(g w€t

lidkg v{€tpg&g wetpg!4(g wet

pgkS Yv€t

usrkg lvet

pgy'kg wet

Pgrkg lvet

pgUl(g wet

lSI(g w€l

pgrkg wet

20_020.02 0 020.020.020.020.020.020.020.020.o20.020.020.020.020.o20.020.020.02 0 020020.02 0 02 0 020,020-020.020.020.02 0 040_020.020_020.020.020.0m.020020050.050.050.o50.o

20.020020.020.020020.020.0

96 70-130

8a 70,130

96 7G130

102 70-130

r00 7G.130

96 70-130

93 70-137

74 70-130

88 70-130

98 7G130

93 70.130

u 4a.5-127

86 70-130

102 70-130

98 70.130

94 70-130

98 70-130

68 70-130

105 70-130

94 7G130

r00 7G130

94 70-r 30

88 70-130

104 70-130

106 70,130

96 66.5-144

102 70-130

96 70,'t 30

96 70-130

100 70-130

94 70-130

94 70-130

82 70-130

98 64_9-123

105 70-1f i

103 70-130

92 70-130

75 70-130

94 40-134

99 70-130to4 7G13099 70-13098 70-130

104

66

94

97

96

90

s5

3

1

9

5

50

2525

25

Thb laborutory Epod tr nal vsIU withoa, an aalhorized rtglnuure oa tha covet page* Reprtable Det€ction Limit BRL = Below ReportinB Limit Pase t09of 152

Page 493: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatlle Organic Comporrds - Quslity Control

Ai|8lytdd Result Flag Uoits 'RDLSource %RECResu.lt %REc Limits

Spikel.evel

RPDLimitRPD

Bract 703t233 - sw846 50!5A soit (tow tcvc0

LCS Dso (70312$-ASD'|l

Prepared & Anel]/z€d: 21-ird-07

Bromotoarh

Eromom€lhane

2€ubnone (MEK)

n-Butylb€nz€fle

sec€uVboruene

terl-Butylberueng

Calbon disllfide

C€rbon tebad oride

Chiolobenz6n€

Chlolo€fl€n€

CHoruform

Ct{oroneth €

24trlorotol$€rle

44hlorototu€ne'1,2-Oibon|o-3d ompropan€

Dlbmmftibmmdhane

1,2-Dibroneth6de (EDA)

Dibromonted1sne

1,2-Oi:hbmbenzene

1 ,3oichbobenzene'l ,4-Oichlorsb€rE€neDhhlnodifrrorcrnetrEne (Fr€on'12)

I,l-Did|brethane,|,2-Dblrloro6thane

1,l-DaC oroeth€ne

d$1,2-Di{* oroethene

Fans-1 ,2Oichbr@then€1 2-Oic*rloro9rooane| ,}Did orcorcpEne

2,2-Di$bmpmpane

1,l-Did otolmpene

cjs-'1,3-Ok$bopr@ene

rans-'l,3oid|bropf opene

Ethylb€nz€no

H€xachhobutadiens

2+exanono (MBK)

lsopropylb€nuone

4lsopropyibluen€

[4€Aryl tedtrty' ether4+ul6{hyl.2t€ntanone (MIBK)

MethMene chbrile

Naphlhelen€

n+roDybel\zorre

Slyrene

1,1, 1,2.Tohac5loro€than€

1,1,2,2-T€treehloro€thane

TetracilorEth€ne

1 ,2.lTridrhroO€nzen6

1,2,4-Trichbrob€nzene

1,1.1-Trichlorg€fiane

1 ,1 ,2.ldchloro€E|sne

r9.6r0.514.8

18.9

20.1

m.817.5

18.1

19_6

17.5

18.5

17.S

1S:

20.4

18.1

18.7

19-0

18.7

ls. l

19.7

14.2

20.0

19.1

18.0

16.S

14.2

1 f . 9

1 9 7

21-1

17.3

r9.5

21.O

19.7

20.3

18,4

14.9

ts.419.519.S

18.0

16.9

19.8

t9.s

m. l19.8

19.3

19-0

tE.8

19.0

18.2

21.8

20-020.0m.om.020.020.020.020.om.o20.020.020.020-020.o20.020.020.o20.020-o20.020,020.020.o20-020.om.om.o20.020.020-o20.020.0m.o20.020020.020-om.om.o20.o20.o20-020.020.020.020.020-020.020-020.020.020.0

513

4

42

07o30

0I

't0

2

326I010

77

2

1s102

13

!g/kg w€l

lgAg wetyg/tg w€l

|lg/l9 Y/et

!q/kg Yret

!d(g vret

lgutg rv€l

Ig/kg rcl

UgI(g r€l

Fgkg w€tpgfl(s wet

UdkS wet

UgLfllg w€ipg/t€ wel

lgAg w€tpgtg wetpdrs wet

lgr'kg wet

tgtkg w€t

Ug/tq wetpgltg welpdkg w€t

tdks wet

ldkg'r/etrcUkg wet

Ug/t€ wel

!g/kg wel

Idrs rvet

FdXS rvet

ldkS wst

rc/kS @l

lgr'tg lr€l

!g||(g w€lpdkg r€tpdks rvetpdkg vret

!g/kg w€t

lglkg welpdtlg rvet

Ug/19 welpdkS wet

ldkg wet

!g/,kg wet

lgll€ wel

t gag w€t

Igltg w€lpgdq wet

FSXS f,,et

|lgL/kg welggltgw€t

ru/t(g w6l

PgAg r€l

9A 7G130

92 5o-r&74 47.1-12r9t 70-130100 70130t04 7G13088 70-13094 7G.13098 70-13088 55.9-135g2 70-130so 70.1m98 70-130102 70-i30s0 70-130g 72-12595 7{t13094 7G13096 70-13098 7St3691 70-130100 42.3-19096 70-13090 7G130€4 7G13091 70-13t)s0 7G13098 70.130106 70-13086 7G13098 70-13010s 70-13098 7G130102 70-130s2 ?0-13774 70-13097 7Gt3t)98 7G130100 70-130s 4€.512764 7G',t3099 7G130100 7G130100 7Gi3099 7G13096 70-13095 7G13096 70.130s4 7G130s5 ?0-130

91 7G130f09 70-13J

5050

25

2550252525

25502525

2525

2525

252525

b

255025

25

502525252525252525

25

25

This l4bo.etuf npod it aot tofrd xt&hotd zn d,adlorkad signdt e or thz @rzr page,

* Reptrbble Detection Limit BRL = B€tow R€portins Lirnit Page I l0 of | 52

Page 494: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volaail€ Orgalic Compounds - Quality Cootrot

Brrch 703t213 - S\r8{6 50t5a S0[ (to!v levet)

LCS Duo fl031233-ASD'|l

Prepsred & Anal}.zedt 21-Mar{7

Triiloroethene

Tdchbronuorom€thane (Freon 1 1 )1,2,3-Trichloropropane

1,2,4-Trinethylb€nzem

1,3,s-Trim€thylbenzene

m,p-xylene

<}Xyl€ne

lotrahydrofuran

Ehy' €thsr

Tert-amyl mehyl ether

Ethyl terl.butyl ether

Di-isopropyl ether

Te{t€utanol / butyl alcohol

1,+Dbxan€

S u nqa t e : 4 - B ronofl u o tobe n z e neSutmgate: Toluene4SS u oog a Ie : 1, 2 -D ich lo rceth a n e 4 4S u toga I e I D ib ro m ofl u orc m eth a ne

Bdtch 70.31291 - SW8{6 50f5A So oow level)

Blant 17031291€LK1l

Pr€par€d & Anal].zed: 22-[iar{7

1,1,2-Trichlomtriff loroethane (Freon 1 j3)

Acrylonitrile

Benzefle

Bro.nobenzene

Erc{nochbronrelhane

Bromodichloromethane

Eromoform

Bromon€lhane

2-Bubnone (MEK)

n-8lllylb€nzene

soc-Butjb€nzene

lert.Butylbenzene

Carbon disulfide

Cerbor lstracnbide

Chloobenzene

ChlorE€thane

Chloroform

Chlorom€f|Ene

24hhrotoluen€lrchbrololuene

l,2Oibromo-3-c}|bmpmpane

Dibromod orom€thane

I "zolbromoethane (EDB)

Dibrqnomethane

1 .2{ictrlo{obenzene1 ,3-Dichlorobenzene| ,4Oichlorob€nzeneI)id orodifl uoromethane (Freont 2)1 , | -Oi:hloroethen€

2 1 . O

1 8 I

23.7

20.2

20.2

21.8

40.3

20.4

18.3

14.7

1 9 1

2 1 . 2

19.1

169

212

52.051.849.149.8

Spikc

20.o20.020.02 0 020.020.040.020.020.020.020.020.020.020020050_050.050.050.0

25502525

25252525502525

2525

p!/kg wel

pg/kg wet

Ug/kg wet

LrgL/kg wer

|lgkg wel

!g/Kg wel

!g/kg w€l

!g/(g wel

Fg/kg wet

lgkg wet

pdkg rYet

PdkS Yret

pg/kg wet

!g/kg wet

lgkg wet

pg/kg we1

Ugr'kg wet

lgKg wslpg/kg wel

!g/kg wet 5.0

!g/kg wel 100

lgkS vr€t 5.0

!g/kg wet 5_0pg/kg wet 5.0

t gr,kg wet 5 0

ldkS Y€t 5.0

!S,xg Yvet 5.0

!S4(g Yrel 10.0

ldkS wet 50.0

riqr'kg wet 5.0

!g/kg wst 5-0

!g/kg wet 5-0

!g/kg wet 25.0

ldkg u,61 5.0

!g/kg wet 5 0

Ug/kg w6t 10.0

pSfl(g v{et 5-0yg/kg wet 10-0

pg/kg wet 5 0

udl(| vret 5.0

!91/kg wet 10.0

!g/kg wet 5.0

t|gLitg wet 5.0

l4r'kg wet 5.0

rcr'kg wel 5.0

Ug/kg wel 5.0

lgr'kg wel 5.0

rgr'kg w€t 10.0

Ygr'kgwel 5.0

t05 70-130 0.9

s4 66.5144 2

118 70t3o 15

101 70-130 5

101 7G.t30 5

109 ?0-130 I

101 70-130 7

102 70-130 I

92 ?0-130 11

94 64 S123 4

96 70-130 I'106 70-130 3

96 70,130 4

84 70-130 11

106 10-134 12

104 70-t3t)104 70-13098 70-130100 f0-130

ARL

BRL

BRL

BRI

ARL

ARL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

ARL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

Thb lzbontory EFort ls aat lalu wdhotd on z!flto;zct sig,,ara,? on the cover pale.

' Rep'ortable D€t€ctEn Li6ir BRL = B€low ReDortine Limir Page ItI ot 152

Page 495: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtilc Org|nic Compounds - Qurlity Cootrol

Analyte(s) Result Ftag UnitsSpike

LevEl

Source

R€s t %PfC

%RECLimils RPD

RPD

Limil

Batch 7031291 - SW646 5035A Soil oow level)

Abnk ln)s11'l1€LK'll

Ptepated & futaly?€.d: 2-Mu47

1,2{ichloro€than6

1 ,1 -Dicibro€lhe.E

cisl,2-Dict oto€tlEne

lrans-1,2Oichloro€thene'l,2-Diibropropane

I,}{)ic orcpropan€

2,2-Dichbrop,opa|€

1 ,1 Oichbrop.opene

cis-l,3olchloroprop€ne

trans-l,3JichbroFopen€

Ethylbenzen€

Hexehlorcbutadiene

2-H6xenon€ (firgK)

lsopmpylbenzene

4-lsopropy'loluen€

Mehy' tertndyl ethet

4-Melhyl2-pentanone (M|8K)

Methylene chlorid€

N+hlhalen€

Styrene

1 ,1 ,1 ,.T€t-echloroethano1,1,2,2-Tstrachloroelhan6

Tetacftloro€tltone

1,2,$Tri{fibobenzen€

l,z,+Trid orobenzene

1 ,1 ,1 -Tricfibrcathane

1 ,I 2-Tdc*rb.o€than€T.idloro€then€

Trftt orofuorcmsthan€ (Fr€on l 1 )| ,2,lT.ichlotopropane1,2,4-TrimehyDenzsn€

1 .3,STrim€thylbetEenoVirM cf oride

m,FFxyle@

o-Xylsn€

lebahydroturan

Ew sther

T€rtdrryl mehyl €th€r

Etryl isd+uty' €th€r

Di-isoFopyl efte,

Ten-Butand / buv Elcohol

1,+Dioxan€

Sunogai€: l-AmneauonbenzaneSunogalg: Toh@'€48Su''ogale: l, 2ltichb@elhan644S u nogale : Dib MEfl rn @meth a ne

LCS a7rt9l29t€5r)

Prepar€d & Analfzed: 22-Mar{7

| ,1 ,2-Trichlorotdffuoro€thsne (Feon 1 13)

SRL

BRL

BRL

BRL

BRL

BRL

BRL

BRf

BRL

ARL

BRLgRL

BRL

SRL

ARL

ARL

BRL

ARL

BRL

BRL

BRL

aRf

BRL

BRL

BRL

BRL

BRL

SRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ERL

BRL

BRL

BR|-

BRL

52.757.O51.9

22.3

12.0

!g/tg wel

$fl(g w€t

lgy'kg v/et

UdkS w€t

Fg/t€ wet

$/k0 wet

pdrS w€t

lgr'kg r{!el

Ug/tg w€t

!91(S $/et

pdrq wet

Ig/kg wet

udts lv€l

pglq w€l

lgflqg w€i

|lgL/kS wet

ygrkg wet

pgi l€ wet

lgy'kg $,el

pglq,,tet

ldkS w€l

usn(s Y/etldkS wetrcn€ wetIg/kg wet

ug&g welpdkg wet

tdtg \r€t

lgr'kg w€tpdkg wetpd@ wetpgikg w€tpdkg welpdkg v!,el

!9&g w€r

Io'kg wet

lgLlkg wet

Fgrtg wet

ug/rg wet

Pg,lg wetpgts tvet

ldkg w€t

rdb w€tpgikg wet

!€/kg wetIS/1S welugftg well.rs/xs wol

Pg/kg wst

rcI€ wet

5.05.05.0

5.05.0

5.0

5_05.05 050-0

5.05.050.050.05.05.O5.05.05.0

5.05.05.05.0

5.05-05.05.05.0

10.05.050.05.05 05.0

50.0100

50.o50.o50.050.0

1O5 761mt05 70.130,14 70-1$1(U 70-130

112 7Gt3080 3.31-159

m.020.0

TIth l^borztory rato.l is not voM h'ith46 an o4lho.hd sigr'rtt&re or ahe cowr pag..

r Reportable DeEcrion Li6it BRL= Betow R€gcding Limit P.ge l12 of 152

Page 496: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quallty Control

pg/kg wet

lgL/kg u/et

!g/kg wet

lgL/Kg wet

plyr(g wet

ug/kg wet

ugkg wel

!g/kg wet

LilyKg wet

Pg'kg wet

pgrkg wel

Igtkg wel

Pqfts wel

Ug/kg wel

pg/kg wet

ug/r(g welplyKg wel

!g/kg wsl

LiEKg wel

Lig/kg wel

ugr'kg wel

pgir(g wel

ugikg wet

Uglkg w€t

pgdkg wet

Pq/kg wet

lJgrKg wet

pg/kg wet

Pg/kq ',et

!g/kg wet

!g/kg w€t

pdks wet

Llg(g wet

pdkg wet

pqkS \ /et

pgkg wet

Ig/kg w€t

ldks w€t

ug{xg wel

lEKg wel

pdkg wel

Pg/kg w€t

!g/kg wer

|rgr(9 wel

|lgi kg w€t

tr(ykg w6t

plyKg wsl

Lig/kg w€l

ldkS wet

lgr'kg wEt

pdks wet

ldkS','/et

%REC

Limits

98 70-130'r01 7G13090 70-13094 70-130104 70-1309€ 70-130101 50-14070 47.7-127104 70-13t)s8 70-130101 7{1130106 70-130100 70-130104 70-13099 559-135104 70-130s6 70-13097 70-130103 70-13084 70-13098 72-125109 70-1n93 70-'t30101 70-13096 70-13096 70-13t)112 42 3-190108 70-13094 70,13095 70-130s9 70-130106 70-130105 70.130102 70-13096 7G.130106 70-130104 70-130'r 14 7S130102 7Gt30103 70-13779 70-r 3097 70-130106 7Gt3010t 7G130s6 4a.t12794 70.130108 70-130't01 7G130102 7G130100 70-130e8 70-130112 70.130

SpikeL€veL

i

Brlch 70lI29l - SWE{6 5015a Soit tton teveu

LCS 17031Ar1€.till

Pr€par€d & Analfzed: 22-Mar-07

Acrylonitile

BerEene

Bromob€nzene

Arorho{hlommelhane

Brornodidnloromeu'lane

Brcinobrm

Eronrornelhane

2-Bulemn6 (MEK)

n€utylbenzene

sec-Buty'lb€nz€n€

tert+utylb€nzene

Ca.tton dis'rmde

Carbon t€lEchlorid€

Cl orob€nzene

Chlorcehane

Chbrofofin

Chloromethane

24hbIotoluene

44hlorotoluene

1,2{ibro,mo-3drlompropane

Dibaomochlorom€than€

1 ,2-Dibromo€Ulane (EOB)

Dibromomethar€

I ,2.oiilorobenzenel,3.0ichlorob€nzene

1 ,4-Dichlorob€nzen€Dichhrodftioromelhane (Freont 2)| , | -0ichloroethane

1 2-Dichloro€thane'l ,l -Di€hloroethene

ci9l ,2-Dlflooethenefans-1,z0ichloro€thene

l lOichloropropane

1,3Oicfiloroprcp€ne

2tOicnloropropane

1 ,1 Oichlompropene

cis-l.3.Dichloroprop€fl st-sns-l,}Dichlompropene

Elhylbenzene

H€xachlorobutadi€fle

2+lexanone (MBK)

lsoprogylb€nzene

4-lsopropyholuen€

Mehyl tert-butyl elher

4-l,lethyl-2-pentanone (M tBK)lr€tryl€ne d odde

Naphhalen€

nPropylb€nzen€

Strene'1,1, 1,2-Tetrachloroethane

t , t ,2,2-Tetacfilorc€tnansTebacfiloroelh€ne

1 9 7

202

18.0

1A.E

20.9

1 9 . 1

20_2

14.O

20.9'lg 7

2 0 2

21_2't s_s

20.7

19.8

20.f

1 9 . 3

1 9 4

20_6

16.9

19_7

2 1 . 8

19.8

2 0 2

19.3

1 9 . 3

22.4

21_6

1 8 I'19 0

1 9 8

21.1

21.0

20_5

19.2

2 1 3

20_7

22.9

20.4

20.6

15.8

19.4

2 1 . 2

20.7

19.2

1 8 7

21.6

20.2

2 0 5

20.0

17-6

22.5

20020_020.o20.020020_o20.o20.020.020.020.020-02 0 02 0 020.02 0 020.020.020.02 0 020.020020.02 0 020.020.020.o20.020.o20.020.020.o20.020.020.020.020.020.020.020.o20.020020.c20.020.020-020.020_020.020.020.020.0

Thit laborulory rcpofl k noa vald wirhod oa suthorized signature on the owr pa$e.

* Reporhble Detection Limit BRL: Below R€porting Limit Page l l3 of 152

Page 497: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatlle Organic Compounds - Qlality Cotrtrol

Analyte(s) R€sult +RDLSpikeL€vel

%RECLimits RPD

RPDLimitFlag Units

Source

Result %REC

Bstch 7031291 - Sw846 5035A Soil (low levcl)

LGS 47001291€S1)

Pr€Fred & Anatyzed: 22-li4ar-07

Tolu€ne

1,2,&Tli;lrkfob€nzene

1.2,4-Tn_d omb€nzene

I ,1 ,1 .Trt(filo.o€thane

I , | ,2-TrichlorD€dEneTri$loroeheno

Tdchtoronuorcmehan€ (F.6on 1 1 )1,2,&Tdchbropmpan€

12,4-TdfiEthylb€nz€ne

1.3,s-Taim€trylbenzene

Vinyl drlodd€

m,p-Xylene

o-Xylen€

Tetrehydrcfuran

Ethylefi€r

Tert-amyl rnethyl €ther

Ethyl bd-butyl e(tl€r

Diisopropyl 6lher

Terl-Butanol / buv atcohol

l,4oioxane

Su Eogate : 4 Bro rpfl u orcbe n zeneSurrDgElej Tolu€no-d8S u fiog a le : t, 2 -DkhloroEtha rc4 4S u fiog ele: Ditno nofl uodn ath ane

LGS Ouo?03t291+SOll

Prepared & AndFed: 22-ltlar-07

|,|,2-Trichlorotriflloroethane (Freon 113)

Acrylo. iril€

Benz€no

ErEmod{Oromehane

Brornodichlorom€thane

Bronofomgrcmomehan€

2Auhnone (MEK)

ftAdy|b€ru€ne

seo8utylbonz€ne

terl-Buvh€nz€ne

Cerbon disumde

C€fton tet'ad odde

Chloroh€nzefl€

Chlo|oetiene

Chloroloam

Chlorcn€thBne

2Chbmioluene

44hbrololuen€

1,2-DibrDmo-3d{cmpropan6

Dibromodrloron€than€

I 2-Dbrornoethane (EDg)

DlbmmoflEthane

| 2-Didlo.obenzen€

19.420.8

19.3

24-721.621.220_020.821 .738.819.417.420.1

22.4m.4r6214147.25t.a5 t . 152.0

21.412.614.620.317.817.420.419.2'ts_ I13.720_720.120.3't8.0'18.8

19.6r7.419.719.419.'l19.921.7r9.t20.318.921.0

20.020.om.020.020020,0m.020.020.020.020.040.0m.020.020.o20.020.020.020020050.o50.o50.o50.0

m.020.o20.020.020_0m.om.020.o20.020.020.020.020.020.020.020.0m.020.020.020.0m.020.020.020,020.o20.0

529I1620

302I

16

6

r 3

2t

25

7

Fdkg v'/et

ug^g wet

ldkg wsl

!g/kg w€t

!g/t(g rrel

trg/kg wet

l.,g/kg wet

lgrkg wel

|Jdko w6l

rcr'kg r€t

Fgr'kg w€t

US4(S YJ€t

ldkg "velldkS rct

!g/lq n€tpgkS 'r/et

lgtkg wst

Pdkg vJel

ldkS $/61

IgL/i(g n€l

t gkg wst

UdkS wetpSlkg wel

lgkg wel

Ig/kg wet

Pgukg w€tqR2

!g/kg wet

Idks v,€l

lrSrkg lv€t

Pg/tg wst

pg/kg wet

lrgkg w6l

Lrgy'kg wot

lgL/kg rret

pSn€ wet

pg/kg $'et

pg&g wel

ugr'kg R€t

pg/kg wet

Pgkg sret

pg/kg wstpgftg wel

ldlS wel

t gr'kg lr€t

lrg/kg wet

ygilq w€tpgts vret

lgr'kg wel

udkS w€lpgdkg w€t

97 7G130'104 70-13J110 70-13096 7G130113 7G130124 70-130108 66.S1{4106 TG13()1(X 70-130104 7Gt30108 7o-t3097 70-13097 70-13087 7G130f 00 u.g-r23t16 70-130'n4 70-130'lo2 7&13081 7G13070 .t{tt34

94 7+1m104 70-1fi102 7G1fr101 70-1u

107 70-13063 3.31-15973 70-130

102 7Gt3t)69 70-13087 7Gt30102 70-13096 7G130s6 50"1406a 47.7-127104 70-130100 70-130102 70-1fis0 7G13(194 70-13098 7G13087 55.913598 7G13098 7Gr3096 7&i30100 7G130108 70.130

72-125102 7G.t309a 7G130105 7G130

50

25252525

50

25

25

258E

g)

25

This r4borabf Epotl h ,rot vaUd withoa an aalhotirij sig darc ott the coyer page,

* Rcporrable Det€ction Limit BRI- = Below Repoltidg Limit Pige I 14 of 152

Page 498: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Anrlt'tds) Resuft RPDUoitsFlae . RDLSfrike

L€vel

Sourc€

Result %RtrC%REC

Linits

RPDLimit

Brtch 703t29r - Sw846 50t5A Soil (lo$ t€yeD

LCS Ouo 17031291-a.SD'l)

PreDarcd & Amlfzedr 22-Mar-07

t .s-DichbrobeDzene1,+0d omb€nzene

Dlchlorcdin!oromethan€ (Freonl 2)'l,l-OiJ oroelhane

1,2-DiJ oruethans

1 ,'l 'Dinbroethene

cis-1,2-Dichlo.oelhene

trans-l,2Oichloroethene

12€kt oropropane

l,SDid oropropane

2,2-Didtbr@ropane

|.r-Di{* oroprop€ne

cis-'1,3-Dichloropropene

trans-1,3-Oichloropropene

Ethylbenzsn€

Hexact orobutadiene

2-He)6none (MBK)

lsopropylbenzene

4-lsopropyltoluene

lll,ethyt bn-butyl ether

4{vlelhyl-2-p€nlaoone (MtBK)

Methylene drlorile

Naphthalene

n+mpldberEene

Styrene

1 ,1 ,'l ,2-Telrachlo.oethan€1,1,2,2-Telrachloroelhane

l,2,STdcnbrobenzene

1,2,+Tri{:trlorcbsnz€ne

I.1, l-T.ichloroethane

1 , | ,2-Trichloroehane

Trkiloroff uoromehane (Freon 1 I )| 2,&Tricitoropropane12,+Trimetlylbenzeoe

l,3,5-Tdhethylbenzene

\rrM d 6id€

m.D-xylene

o-Xylene

T€hahydroturan

EUrt 6the,

T€rt-€myi methyl elher

EthY t€n-buv €ttPr

DLboprosy' elher

fert-But€flol / butyl alcohol

t,4-Dioxsn€

I u fi Egale : +&o n1o fl u orcb e n zen eSunWa'P.: Toluene4SSunWaE : 1,2 -Dichloroethane44

Sunwa b : A b rcrnon uo a n elh e rc

207

204

2 2 4

20.1

1 8 0

1 9 9

18.6

2 1 3

20-4

19_8

18-1

1S_5

21.4

?0.9

20.5

20.2

14.0

19.2

2 1 A

i9.a

1 8 . 9

18.4

20.5

20_2

1S_7

20.9

19.0

20.4

1 9 3

2 0 9

21.1

1 8 . 6

2 t . 4

22_9

20.1

21.2

20.4

r9.9

18.4

3S_6

1 8 . 9

17.3

20.0'18 5

2 1 . 5

15.2

175

202

19.852.048.549.8

pg4(g wsl

pq(g wet

lsftg wet

Pgrkg wet

pS'kS t^rt

trgkg wet

Pg'ikg wet

l]Erq wet

pg/kg wet

!s&g wet

ldkg wet

uEr(g wet

!g/kg wet

us.4€ wet

!g/rq w€t

!q/kq wet

!g/kg wel

lgikg w€l

!g/kq wet

lgr'kg wel

pgi kg wel

lEkg wet

lgkg wel

ugftg wel

irg/kg wel

!g/kg wet

!g/kg wet

pglkg wet

Pg/kg wet

!g{(S \^/et

pgn(g wet

Lig/r(g wet

tig/kg wet

pg/kg wet

pg/kg wet

lgyrlg wel

ugr'kg wet

pgl(g wel

Fg/tg wet

!g/kg wet

!Er(g u/et

!g{(g '4et

pSI(S w€t

pgkg w€t

ug/Kg wet

!g/kg w€t

!g/kg wet

pgkg wet

UgL/kg wel

!g/Kg wel

!g,'kg wetpg,rkg wet

1D4 70-130102 70-130112 42.3-190100 70-13090 70-130100 70-13093 70-130106 70-130102 70-130s9 70-13090 7G13098 70.130r07 70-130104 7G't30102 70-130101 7G13770 70-13096 70-130109 70-1309e 70-13094 48 U12792 tO-130102 70-130101 70-13098 70-130104 70-13095 70-130102 70r 3096 70-1301o4 70-130106 70-'t 3093 70-13t)107 70-130'r14 7G130100 66.t144106 7G130102 70-130100 70.13092 70-13099 70.130s4 70-13086 70-19)'r00 64.912392 70-130108 70-13096 70-13088 7&130'101 4G134100 70-130104 7o-1N97 70"19)100 70-19

2D.O20.020020.020.020.o20.o20.020.020.o20.020.o20.020.020.020.o20.020_o20.020.020.020.020_02 0 02 0 020.o20_020.020.o20.020.020.020.o20020.020.020.020_o20.040.020.024.020.020.020.020.020020050_o50_o50.0ffio

8

6

0

I

5

6

0

3

3

8

3

I

0

2

1 2

1

3

5

2

2

6

0

4

I

I

I

0

3

5

6

I

0

2

'16

2

3

I

0

5

6

I

36

25255025252525252525252525

25502525252550252525

25252525252525255025252525252525502525252525

Thk taboraory rcport b ,tol vdU tellho.,l an auhoirztt signzture on lhe cotpr page.

* Reportable Detection Limit BRL = Below Repodng Limit Psge I 15 of 152

Page 499: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Extrrctable Petroleum Hydrocarbons - Qudity Cobtrol

Analyte(s) Resuit .RDLSpikeIavel

SouaceResult

%R-ECLimits RPD

RPDLimiaFlag n/,wcUnits

B.rct 7031160 - SWM6 3510C

A|ank 17031ler€LKll

Pr€pared: 21 -01a.{7 Analyzedi 22-Mer47

Gasolin€

Fuel Oil f?

Fuel Oil *4

Fu€lOi l#6

Moto. Oal

unidenlifcd

Ohe. Oil

Total Pet oleum Hydrocarbms

C9436 Aliphalic Hydrocarbons

Sunogale: t -Chlot@dedecane

LCS f7031160€S1)

Prepared: 21 -l\rd-07 ArElyzed: n-Met4l

CgC36 Afi phalic Hydroc€bons

SufiWate: | -Chlotooctactecl,ne

Brtch ?03116? - Swa46 3SS0B

Ahnk (7031167€LK1r

P.6pared I Analyzed: 2t-lvlar{7

Gasoline

FuelOi l#2

FuslOi l#4

FuelOi l#6

Motor oil

Unidej$ned

OtherOil

Total Petrolsum Hydrocarbons

C!,.C36 Aliphatic Hydrocerbons

Su.'ogate : 1 -Chlotoocladecane

LC€ 1706fl67€{t1}

Pr€pared & Analyzed: 21-Mar-07

CgC36 AliphBlic Hydro€rbofl 6

S u nrpate : I 4 hl otooctadecan e

Dublicat€ 470:li I dl-OUPI )

Pr€pa€d & Analfzsd: 2t -Mar{7

Gasofn€

Fu€l Oil flz

FuelOi l#{

Fuel oll #6

Mobr O{

Unld€r if€d

Oh€r Ofl

Tolal Petoleum Hydrtredons

CgC36 Allph€ltc ttydroc{bons

Sr/'rogate l{'h,j}rEd.adecane

lretrlx $rlt. {7031167{|ll)

Pr€pared & Analfzed: 21-MErry

C9436 Aliphalic Hydroca.bons

BRL

BRL

BRL

ARL

BRL

BRI.

BRL

BRL

BRL

BRL

0.04i0

1 . 4

0.0520

BRL

BRI

ARL

BRL

BRL

BRL

SRL

ARL

BRI.gRL

2.fi

84.6

3.74

Sau.ce: 5459464.07

BRL

ERL

sRt_sRr_gRL

BRL

BRL

BRL

BRL

2.08

Sourcs: 3459484{l

mgl 0.05mg 0.05rngl 0.05mSI 0.05mdl 0.0sntg/l 0.05rngl 0-05mgn 0.05.9n 0.05nEn 0.05ordl

ngl O.05t|u

mgftg wE[ l3-3(€lkgwet 13.3

fl€lkgwel 13.3

rngltgw€t 13-3

ttlSllg Yrst 13.3

r€/kg wEt 13.3

mgrkgwst 13-3

nE/kg we( 13.3

mgr'kg w€l 13.3

mgikgw€i 13.3

rngl(g sr€t

.trgftow€l t3.3

mgrkg rN€l

nSftS dry 18_9

.nSftS 6y to.S

d€tkS dry 18.9

lr€rkg dry 18.9

mgl(gdry 1&9

rEr'kg dry 18.9

nS/kS dry 18.9

nEftSdry 18-9

rtg/kg dry 18.9

nSftgdry 18.9

nEukg dry

mSftodry 14,6

o.oflo

|.40o.tR00

4+140

60.120&)-tm

86

r00104

93.33.et

40.141)

60-12060-1m

91

fi2

BRLBRLARLBRLBRLBRLBRLasu_BRLBRL

505050

50505050

79.6

,ll)-ln

5G15078BRLlo2

This tabordaucpul is twt volid sAhoat at oathotized sig,'Flfrtre ad ahe ca,!e, page.

* Repdbbl€ D€t€ction Limit BRL = Below ReponioC Limir Psgc l16 of 152

Page 500: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Extractable Petroleum Hydrocarbons - Quatiqv Conarol

Analyte(s) Result Flag UDits

%REC%RtrC Limits*RDL

Spike

I-evcl Result

RPD

LimitR}D

Brtch 703116? - SW8{6 35508

'|.rflxspikD17031t67-frsl) Sourcc:5A5946/147

P.epared & Analyzed: 21-Mar{7

Suflogste: I,Chtorooctadecane 3.Sl

i|grrfx Soike Ouo fl031167.MSD11 Sou.cs: 5A59464{7

Prepared & Anatt"edr 21-Mer-07

CgC36 Aliphatic Hydrocarbons

S u ttogale : 1 -C hl oroocl ad e c a ne

B.tdr ?031283 - SW846 3ss0B

glenk tm3t283€jLt<11

Prcpsred: 22{rar.07 Anat}zed: 26-Mar-07

Gasollne

FuelOi l#2

FuelOilrr4

FuelOi l16

Molor Oil

Unidentifted

Olh€r Oil

Tohl Pekolellm Hydrocadons

CSC36 Aliphatic Hydro€bons

Suflngate : 1 -Chloroactadecane

LCtf7031283€S

Preparcd: 22-{vlar-07 Analr.edr 26.l ar-07

CgC36 Atiphatic Hydrocarbons

Sunwele : 1 -Chloroocladecane

Prcpa/€'d 22-Mat47 Anegzed 2&t!1afi7

Ga6olin€

FuelOi l#2

Fuel Oil#4

Fu€l Oilt6

Motor oil

U. d€ntified

Othor Oil

Totd Petroleum Hydrmarbons

CS+36 Aliphatic Hydroc2rbons

S u nggal e : l - Ch lo to oclad ecan e

74.4

3.35

3,65

99_9

3 5 /

mS/kg dry

mg/kg dry 14.2mgl(g dry

96 4A-140

8RL 74 50-1a)94 40-140

115 40-140

90 60-120109 60-120

30

ARL

BRL

BRL

8RL

BRL

BRL

ARL

BRL

BRL

BRL

3.84

84.3

J-64

BRL

BRL

BRL

BRL

ARL

ARL

BRL

BRL

ARL

BRL

7 0 5

mg/kg

msftg

mgftg

mS/kS

mExg

mg/Kg

trEftS

r€/kS

mg/kS

mg/kg

ngftg

13.31 3 313.31 3 313.313.313.313.313.313 .3

r€/kS 13.3mgfts

333

93.33.33

Duoltc.t t70312E3{UptI Source: 5459rl.64-10

mS/kS

mg/xsmSI(S

mg/kg

mSI(g

fta/lr's

mS/kS

mg/kg

r,ig/kg

m9ikg

mg/kg

25.4

25.8

25-8

2 5 E

25.8

25-8

25.4

2 5 8

25.4

25_E

ARL

8RL

BRL

ARL

ARL

ARL

BRL

ARL

BRL

BRL

50505050505050505050

109 10-14n

Thb taborqtory rcpod is nol ealU wilhout oI aurtoiel sig'zztare on lhe cowr page.

* Reportable Detection Limit BRL = B€low R€porting Limit Page l l7 of l52

Page 501: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semlvolrtil€ Orgenlc Compourds by cC - Qurlity Control

Result FhS Unirs

Bstch 7t3 1063 . SW846 3510C

B|ank r/o3loB-ALKI IP.epared: 20-Mar{7 AnalFed; 2z-tula( 47PCe 1016PCB 1221PCS 1232PCB 1242PCB 1248PCB 1254PCB t260PCa 1262rc8 126aSunogalE: alae&anuoabiphenr4 (&)S u n9gete : DeoEch lqob i p he nyl ( S I

LCS n031063€8tI

Preg€r€d: 20-lrar-07 Anal:Fed. 22-Mat47PCS 1016PCg 1260Su'.ogate : 4 t+Dg4cbnuorobiphenyl ( SlSu''ogate: Decehwobiphenyl (Sf)

LCS Duo a7081061€50l lPrepared: 2Glrar-07 Analyzed : 22 -Mat 47rca 1016PCB 1260Su|'€gete : 4lABQdanuor&iplbnyt ( SiSufiogata : DEc€chbrobhkenyt ( St)

Brtch 7031061 - Sw646 3510C

Bhnk t7031064-BLfilIPrepar€d: 2SMai-07 Analyzed 2 l-tAat47

a€HCb€r.rcd€Hcg+HC (Lindan€)Chlodane4,4-DDD (p.C)4,+oDE G,p')a,+IDT (p,p')DieldrinEndosuhbn IEndos{ftan llEndosr fan SultaleEiddnE.ddn AH€hydeH€pbdrlori"lelhoxycfttcrH€ptad or EpoddeToxapftea|€aorbrdansgChlordan€

Endrin KebnoS:unogate: +,+Oeoaanro-uptmny 1S4Sufiogate : Decachlorobiphenyt (Sr)

LCS aZ0!106a€311

8RtBRIARLBRL8RLBRLERLBRTBRL0.1500.1w

2.322.35o.t4t)o.170

2_342.3Xo.1fi0.1fo

ARL

ARL

BRI.

BRL

BRL

BRL

BRL

aRl

8Rr-BRL8RLARLBRT8RL8RLBRLBRLBRLBRL8RLSRLBRL

0.01380.0191

udlpdlusxpqlrglwn!glt'$ttsnpdl!tl4

0.2m0-200o.2000.2000.2000.2000.2m0.2000.200

o.200o.m)

30-tfl30-150

,()-140

40-140tui5030-150

4G.14440-140!)-1fi30-1$

7590

t s4!s4pdlrdl

93s470a5

[email protected]

e4

65

udlpql

t9/lu9n

0.2000.200

0-2000-200

0_0r000.01000,01000,0100oo1000.05000.01000.01000_01m0.01000.o1000.01000.01000.01000,01000.01000.01000.01000.05000.01000.01000.0100

2.50250o.2uo.2m

2020

udlug/l'|ldlpsnugnpsntr9/l

!dl

wli

I,lg/l

lrsitp9n!dl

rlgr

Itdl

run!dlpdl

vgl!91ttilpsnpc4pdl

0.02000.0200

30-1tu30-1fr

6996

Thls lahrarory &port is ,rot vdid wtdna an &t^orized sigragre on the .aver page.

. R€portable Det crion Limit BRL = Beloer Repqting Limit Page I 18 of t52

Page 502: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - euality Coltrol

Spike

Brtch 113 106l - SW846 35 locPaepared: 20.1\Iar{7 Analyzed. 21-MaLO7

Aldrio

a€HC

b-BHC

d.BHC

g-BHC (Lirdane)

4,+DDD (p.p )4,4-DDE (p,p )4,+DDI (p,p')

Dieldrin

Endculbq I

Endcullbo ll

Endosuff?n Suttate

Endrh

Endrh Aldehyde

H€ptadrl,or

Hept,dt|dt Epoxide

a-Chlordaneg4nlordane

Enddn Keton€

S u noga te : 1, 4 -D & O cta lhm ro bi p hent| ( S 4S urog ate : Dec achb ro bt p he ny | ( Srl

LCS Ouo f|03106.!A501 l

P.6par€d: 20irlar-07 Ana\zed: 21-Mar-07

Aldfin

a4HC

b-aHc

d€Hc

9€HC (Lindaoe)

4,4oDD (p,p')

4.4oOE (p,p )4,4-DOT (p,p )Di€ldrin

Erdosulb4 |

Endosulfan tl

EndGulfan Sulfate

Endnn

Enddn f\k ehyde

Hepbchlor

Melhorycllor

Hoptachbr Epoxide

a-Chlordarb

g4hlordane

Enddn lGbne

S wrog a te : 4, 4 - DE-GlEfl w tobh he ny I ( S 4SuTogale : Oeca ch I o ro bj ph e n y I ( S r)

Barch 7031068 - Sw845 35fl8

gbnk 17031o€E€lt(l)

Pr€palEd: 20-Mar{7 AnalF€di 21-Msr,07

Ahdn

a-BHC

b€Hc

d€Hc

0_0160

0.013a

0.0103

0 0089

o 014a

0.0167

0 0137

0.0169

0.0164

0.0171

0.0186

0.0154

0.0173

0.0167

0.0174

0.0r62

0.0169

0.0171

0 . 0 1 5 9

0.0187

o.o105o.0236

0_0154

0.0131

0.0r21

0 0085

0.0142

0 0167

0.0134

0-0156

0 0160

o.0168

0 0171

0.0146

0.0166

0.0158

0.0153

0.0152

0.0164

0.0'tot

0.0160

0.0166

0 0 1 7 7o.o244

l,s^p9l

!gn

!g/l

u9rpEl

trgrpsnpdl

!srIrgJl!sr]l91

fg/l

!91

ug/rvqls/l

ugtlLjgl

tr9/lps/l

|ls/l

|ls/l

|'/s/luEtpg/l

pgl

pgl

|lry1

Lis/l

Irlyl

|l9/l

t /g l

usnp(yl

uglus/lusn|ls/l

irdl

|'jsa

!91!s/l

0.01000 01000.01000_01000 01000 01000.01000.01000.01000.01000.01000.01000 01000.01000.01000.0100o.01000.01000.01000.0100

0.01000_01000.0100o_D10D0_01000.01000.01000.01000 01000.01000.01000_01000.0r000.01000.01000.01000_01000 01000.01000.0't00

0.02000 0200o.02000_02000.02000-02000.02000 02000.02000.0200o.o2D00.02000.02000.02000.02000.0200o.o20a0.02000.02000 02000_0200o 0200

0_02m0.02000.0200D_02000.02000 02000.02000 D2000 02000.ozu)0.02000_02m0.02000.02000.02000.02m0.02m0.02000.02000.02mo.02000.0200

80 40-140

69 40-140

52 40-140

44 40-140

74 40-140

84 10.140

6a 40.1,ro

84 10-140

82 40-140

86 40.140

93 40-140

17 40-140

87 40-140

84 40n40

a7 40-140

81 40.140

u 40-140

86 40-140

80 40.140

94 40-140

92 4G110tlg 40-11n

77 4,-140

66 40-140

60 40-'140

42 40-140

71 40-140

84 40-140

67 40-140

78 40..t40

80 40-140

84 40-140

86 4&140

73 40-140

83 40-1{0

79 40.140

76 40.140

76 40-140

a2 40-140

82 40-140

80 4G140

94 40-140

88 10^140122 40-140

4

5

0

1

7

2

2

8

5

5

6

1 3

6

2

5

o0

2020202n20202020202020202020202020202020

BRL

BRL

BRL

BRL

!g/kg wet 14.3

lgkgw€t 14.3pgr'kg wet 14.3

lgukg wel 14-3

Thk laboratory rcport is not wlid wlthoat a aatlto zeilsEnalure on ilv.ovcr pzge.

' Reportable Detection Limit BRL = Beloy/ Repodio8 Limit Paee l19 o( 152

Page 503: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - Quatlty Cothol

Analyqs) R€suli Fhs UnitsSource ToRECR€iult %REC Limits

SpikeLevel RPD

Brtdr 7031068 - SwEa6 35508

Blank fl031068€Lxll

P(€pdsd: 20+rar47 Analfu€d: 21-irar$lq€HC (Undanol

Chlofttane

4,+Dff) (p,C)

4.4oDE (p,p')

4,4ODT (p,p')

Di6l&in

Endosul{an I

Endoertbn ll

Endcdtan Suliate

Enddn

Enddn AH€tryde

H€ptachbr

Methoxychbr

tleptacfilor Epoxide

a-Chlodaneg4hlordane

Endrin tGton€

Si/,rcgate : 1,4-D&Octanuonbiphenf (54Swqale : Decehlorobiphonyl ( 54

LCS n031068€Stl

Preparecf r 2Glrar-07 Analyzed: 2l -Mat47

Ald.in

a-BHC

b€Hc

d-BHC

g€HC (Undsne)

4JoDD (p,p')

4,4-DDE (p,p )a,+DDT (p,p )Oieldin

Endo€uthn I

Endosuffan ll

Endosulbn Suhble

Enddn

End.in Aldehyde

H€ptad or

Methoxychlor

Hepliachbr Epoxide

a4hlo.dan€

g.Chloden€

Endrh K6bne

2,4,5,CTc-l'l-Xybne (lS)

Sunagate: 4,+DB-Octafl uorobiplE]nyt (Sr)Surwata: D€cer;hlotobblFnti (54

LCS Drro O0:t106&830l )

Frepamd: 20-M€r47 Anavr€d: 21 +Jtaf47

Abrin

e€HC

b-BHC

d€Hc

gFBHC (Llidan€)

BRLBRISRLBRLBRI8RLARLBRLgRL

ARLBRL8RLBRLARLARLBRLBRLBRL19.132.0

23.423.712.623.126,025.623.924.926.9

24.426.825.827.228.5

27.726.529.20.o20tg.930.5

26.622.7

| 1 .724.O

za.a28.6

28.6

2862E.628.628.628.62A.A28.628.628.628.628.6

28.628.628,628.628_6

'r0.0

28.628.6

28.628.628.62A-6

Igr'kgwel 14.3

Ig/tgwet 71.5pgtllgw€l r4.3

lgr'kg rvet 14.3

udkSd 14.3

|Jg qwet 14.3pg/kgwel 14-3

Ugikgw€t 14.3

lcrtgwet 14.3pgr'kg w€t 14.3

Wr'kg s/et 14.3

lg/t€wol 14.3

Ugr/kg w€t 14-3pgr'kgw€l r4.3

ugr'kg wst 71.5

$gkgsret 14.3pg/kgwe{ 14-3

!g/kg wel 14-3pgl(g rv€trcr'kg w€t

!g^g v/et 14.3pdks u,€t 14.3pgn(g wel t4.3

ldkSwd 14.3

Igr'kg wet 14.3pg/kg wel 14.3

lYkg wel 14.3pdkg w€t 14 3

!g/kg wet 14 3

|rglkS wot 14.3yg/kg w€t 14.3

t g/kg wet 14.3

ldlSU€l 14.3pS/kS lret 14.3

ug €s/et 14.3

Idkg wet 14.3

t g/kg wel 14.3

ISikg w6l 14.3pdkgw€l 14.3

ldkS wet 14.3

ldhS v'iet

Ugr'kg wstUgkg w€t

lgrl0wet 14.3pgr'kg wet 14.3pdkgwet 14,3

Ig,tswat 14.3pqfgwel 14.3

6f *iil1 1 2 t u t f i

93 4&14082 &1Q83 4S r,r044 40-l4n82 4G140sl 40-14090 4Gl,lO105 ,(F140

a7 40-14/l94 40-140$ 4.0-14085 40-14094 4{}1,()s0 4G14095 40-140100 4tF14090 40-11097 ,1G1,|()

93 4G140102 .O-t40

39.9 50-2fi)70 1+141)1O7 40-t1O

93 40-14079 4G1,lO78 ,|&140

41 &.11Ou &14

7

3030303030

Thls lc6ordo4 tqorl k not volitl N'i haa e, odltorlul stgnsturc on ,he cosd peg..

' Rqortable Detection Limit BRL = Belorv Repodng Limit Pasc lmof 152

Page 504: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - Quality Control

Analyt<s) FlagResulrSpike

l€vel

%RECLimils

RPIJ

Limit+RDLUniLs

So\rrcE

Result %REC RPD

Brtch 703t068 - sw846 35508

LCS Dup O03l 068€SD1 )

Pre.pared: 20-Mar{7 Analyzed: 21 -Mat47

4,+DOO (p,p')

4,4-DOE (p,p )4,4-DOT (p,p')

Diebnn

Errdc|fian I

Endos{Ifan ll

Endosulhn Sulfat€

Endr|'|

Erdfin Aldetryde

Heptedllor

Heplachlor Epoxide

a{hlordane

g.chlordana

Endrin Kelone

S u rog ata ; 4, + D B4da nb rc bi p he n tt ( S 4S unq ate : Dac ac hb to h i ph e nyl ( 34

29.7

26.6

27.9

25.9

27_D

27.5

265

21.3

28.0

26.9

29.6

26_9

27.2

27.0

3 0 8

ft.832.3

14.3

r4.3

14.3

14.3

14.3't4.3

14.3

r4.3

14.3

14.3

1 4 3

14.3

14.3

14.3

14.3

28.6

28.6

24.6

28.6

28.6

28.6

28.6

28.6

28.6

28.6

286

28.6

28.6

2 8 6

2 8 6

2 8 628.6

303030303030303030303030303030

!9k9 w€t

Ug/kg y/et

lgKg lt€t

lEkg wet

/g/kg rrct

pEKg wet

lJgrlg w€t

lgKg wet

ltyKg wEt

lEkq wet

tig/Kg wet

ptyKg $/Et

ug/kg y/et

ugKg wet

!g/t(g yy€t

UEKgwellgkg wet

tig/kg drypdxg drypg/kg dry

ldkg dry

!S/tS dry

ldks dryJ pqks dry

lgks dry

lEkS dry

Uqtg dry

udkg dry

rdks dry

ttglkg dry

!s/Kg drypdkg drypS/kg drypg/kg dry

Idkg dry

ldkg drypg/Kg drypg/kg dry

fg/kg dry

ldkS drypqkg dry

104 40-140 13

93 40-140 3

98 40-140 7

91 40-140 4

94 40-140 0

96 40-140 3

94 40-144 10

95 40-140 1

98 40-140 I

94 40.140 1

103 40-1,10 3

94 40-140 1

95 40-140 2

94 40-140 1

108 40-140 6

66 40-140113 40-140

317I

73 3t)-150109 30-150

102 $-15088 30-'t50112 30-15044 30-15t)10t 30-15090 30-150183 30.15t)

Duolicate l703 l068nUPll SourEe: SASgL5-32

Pr€par€d: 20-lv,f ar-07 Analyzd. 22-Ma'{7

A.BHC

baHc

d€Hc

g€HC (Undane)

ChlodEns

4,4oDD (p,p )4JOOE (p,p')

4JoDT (p,p')

Dieldrin

Erdosulbn I

Endosulfan ll

Endosdfan Sdtate

Endrin

Endrin Ald€hyd€

Heptadrlor

Metrnxya*iht

Heptad or Epoxid€

ToxapherE

a4hlo{dane

gFChlodane

Endrin Kelone

S ulogate : 4, 1 -D B 4 da n uo rcb i p he n tl (S 4Sunqate: Deoschlorouphenyl (Sl

Pr€ps€d: 20+,f ar{7 Analyzed: 22{'i.at47

AHrln

aSHC

b€ttcd4HC

s€HC (LiMane)

4,4-OOo (p,p')

4,+tDE (p,p )

Hardx Spike fl031t)68{S l I So{rrco: SA5944t32

BRL

BRL

BRL

ARL

BRL

BRL

1 1 . 8

136

49.8

8RLgRL

BRL

8Rf

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

22.633.7

r 5 5

15.5

15.5

15.5

15.5

77.5

1 5 5

15.5

1 5 . 5

1 5 _ 5

15-5

15_5

1 5 5

1 5 5

15.5

15_5

1 5 . 5

15.5

77.5

15.5

1 5 . 5

1 5 . 5

BRL

ARL

BRL

BRL

BRL

BRL

1 1 . 5

1 1 6

4 S 3

BRL

BRL

BRL

BRL

BRL

8RL

8RL

BRL

ERL

8RL

BRL

SRL

ARL

BRL

BRL

BRL

BRL

BRL' 1 1 . 5

r 1 6

30303030303030303030303030303030303030303030

15_6

15-6

15.6

15.6

15.6

15.6

1 5 . 6

3 1 031.0

3 1 . 1

31.1

31.1

3 1 . 1

3 1 . 1

3 1 . r

3 r . 1

31.7 pEkS dry27.3 UdkS dry34.9 pgJkg dry13 8 pgitg dry32.2 pg/kS dry39-6 pSftS dry173 OM4x lgr'kg dry

This laboralory rcpon b nat,vld 'ithod an authoi?d signatzE on thc covet page.

' Report$le D€tection Limit BRL = Below Reporting Liftit Pase 12l of 152

Page 505: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Comlrcunds by GC - Q[allty Conarol

Analytds) R€sult Flag +RDLRPDLimitUnits

Spike Source c/oREC

Lclel Result %REC Limits RPD

B.rch 7031068 - SW846 35508

Iabri Solt€ O03l05gt{Sl) Source: SA5!M4$3:|

t r6pared: 2o-lrar{7 Analt'zed. 2+ta/47

4,4.DoT (p.p)

OiElddn

Endosulfan I

Endo6ullan ll

Erio6ullEn Sultale

Eirdrin

Endrin Ald€hyde

H€plEchlor

Methoxydrb.

HepHllor Epoxide

a-Chlord€n6

g.chlordan€

Endrin Kehf|e

2,4,5,&To-*l-Xylene (lS)

Sur/ogat€! 44-DB-Oclaf,uorowhenl (SoSunogate : Decachhtobiphenyl (50

a3-534.732.7u.o35.638_O22.1

46.545.344.o36_434.5

0.02023.636.7

l,laHx Soik€ Duo P03l068.t SOtt So{rc€: SA59rt4S.3l

P.€pared: m-Uar{7 Analyzcd: Z2+tat47

30.0

25.4

43.4

12.5

27.3

40.s

176

82.8

35.8

29-2

41-3

36.9

22.1

30.6

44.5

42.3

42.O

34.8

36_6

BRL

8RL

BRL

BRL

ARL

BRL

SRL

!s/ts dryldkg dry

rdks drytgks drytdko dry}llikg d.ypSftS dry

!C,rs dry

udkS dry

lgkg drypSJkS dryySiko dry

Vgr,S drypdkg dry

rdks dry|,€r'l€ dry

r 5_6r5.615.6

r5.615.615.6

15,6

r5.6

15.6

15.6

15.6

15.6

pdxSdry 15.4ugtSdry ls.4$S/kS dcy 15.4

t S/kg dry 15_4pC/kgdry 15_4pgkgdry 15.4

a[r4x !94€dry 15.4

Udtsdry 15.4

!S&S dry 15.4

tgkgdry 15.4pSAg dry 15 4ggkgdry 15.4

lgrsdry 15.4

rdlSdry 15.4

ldkg dry 15.4

Wfts dry 15.4

IdrS dry 15.4

Ug,l(gdry 15-4

!g/kS dry 15 4

udkg dry 15.4

t 9/k0 drytSi kS dry

Alddna-BHcb-sHcd€Hc

9AHC (Lifldane)a.aooo h,p')4.4-DDE (p.p')4,+DDT (p,C)DieldrinEndosuffan IEndosulfan llEndosul an SdfateEndrinEndnn AldehydeHeptacfilofMe0loxyd'lo.Hopbd or €poxidea4hbdar€g€hlordan€

Endrin K€bn€

Sunog6,l€: 4,4og4&f,uomwhenyt (54Su4.ogete: D9cachbtoblpheny' (54

BrLh 713 I 16l . SW846 3545A

Bl.nkrmStlAa€LKllPr@€red: 21{rlarry Analne,l: ?2-Mafi7PCB t0t6PCS 1?21PCB1?32PCB 1242PCB 1248PCA | 254PCB 1260PCB 12€2

3 l . l3 t . 1x1.131 .131 .131 .131 .13l.131.131-131.131 .137.110.031.131.1

30.830_830.430.830.830.830.830,830_830E30.830.830_830,830.830.830.830.E30_030.830.830.8

49.3BRLgRL

BRLSRLBRL6RLARLBRLSRLSRLBRLBRL

8RL

BRL

BRL

BRL

BRL

t 1-5

1 1 6

493

BRL

BRL

SRL

8RL

ARL

BRI

BRL

BRL

BRL

BRL

8Rr-Bfl-

7237t6

0.9710

m2I

7

1

6

0.9

2

1'10 30-150121 30n 50t05 3Gi 50141 30.150'114 30-t50122 3S.15073 30-150t06 30-150150 3C150146 3G150141 30-150117 30-150111 4t15091.2 50-20078 Wlfi118 3&1fr

97 30-15002 3Glso141 30-15041 30-1508S 3G.1509s 30.'150t95 3G151)109 3G150116 3S.r50s5 3tI150134 1)-150s6 30-150r20 3G15072 30-15099 3(l1 50144 3$t5o137 30-150136 3&150118 30.t501r3 3Gr5073 fi-150fig n-|ffi

3t)3t)3030303030303030303()3030303030

5050

Ig g vret 28.6

Fgn€w€t 28-6

t€rkgx€t 28,6pgrsw€l 28.6

ldkS Yrel 28.6

ldkgwEt 2B.Ayer'kg yr€t 28.6

tg,lqw6t 286

fhir labnbry rapora is ,or volld widtoa an atad',a.izd skn4ta]P' on tle covet page.

r Rcptrtrble Det€ctim Limit BRL= Below Reporting Linia PagE 122 of 152

Page 506: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - euality Control

Spike

l-evel

Source

Result

%RECLimits

RPDAnablqs)

Botch703l164 - swE46 j5,{5A

Bl.nk a?03116,t4LKlI

Prepared: 21-Mar{7 Analyzed-- 22-MarO7

PCB 1268

Suiogate: 4, 4-DB-OdanLhrcbiphs nyl (S r)Surcgate : Decachloabiphenyt (Si

LCS n031164AStl

Prepared: 21-Mar-07 Analyzgd: 22-Mat4f

PCB tot6

PCA 1260

S u nog a E : 4, +DB- Oc tafh@obi phe nyt ( 3 OS nEg eb : Dacac h I o tdbi ph e nyl (Sr )

LC.S Oup fl03ll6.|ASD1l

Prcpaed: 21 -MaA7 A^alyzed: 22.Mar47

PCg 1016

PCB 1260

Sniggate: 4lag-Octafl@rcbipheny' (54Su/rogale: Decachlorobi pha nyl ( St)

PCB to16

PCB i260

S u rrogate : 4, fi & Oc k n u oro hi phe n yl ( S IS u ftogale : D ec ac h I orobi p h e nyl ( S r)

Brht 7031170 - SW846 35508

Bbhk a?0llt70€LK'l)

Pr€pared: 21-Mar.07 Analyzed: 24-Mat47

PC€ 1016

P@ 12.1

PCS 1232

PCB 1242

PCB 124€

PCA 1214

PCB 1260

9ualicrt€ 4703'1 16+OUPI ) Source SA59tt54{1

PrEpared: 21 -ii,lar-o7 Analyzed: 23-Irar47

PCa 1016

PCg 1221

PCB 1232

PCg 1242

PCa 1248

PCB 1254

PCB 1260

PCa 1262

PCB't266

Suqogate: 4, 4 -D&Octathnrobiphent4 (S r)Sulogate : De c ac hlo ro b i ph e n yl ( St)

atrlx Solks fl Gtl lG4-tlS l) Scturce: SA59/t6441Prcp€red: 21-lvlar{7 Analfzed: 23-Mar-07

PCB 1016

FCB 1260

Su,7ogale : 4, 4-Dg-Octafl uorobiph4ny! (3r)S u ft ogEt e : Decac h I o tobi p h e ny' ( 54

124

1 5 r

5.44E.39

.ndx Splke Duo ft03ll64,tlliDll Sourco: 5A59464{1Prepared: 21-llar-o7 Anatyzed: 23-Mar{7

%REC R?D

ARL

2 1 43 0 0

427

430

20_o28.6

4 1 3

459

2 0 031.4

28.628.6

357

28.6

357

357

28.6246

| 1 . 71 1 _ 7

r50

150

12.O12_O

1 4 9

1 4 9

1 1 . 91 1 . 9

Ugr'kg wet 24.6pdkg wetpgftg wet

pglkg \Atet m.6

!g/kg wet 28.6

lgkg wet

lgr'kg w€t

!g/kg wet 24.6

Pgkg wel 28 6

trg/kg wel!g/Kg wel

!g/Kg dry 11.7

llg/kg dry 11.7pdkg dry 11.7pg/kg dry 11.7pS/kS dry 11.7

udxs dry 11.7UdkS dry '11 .7

!S/kS ory 11.7pg/kg dry 117sS/kS drypgi Kg dry

pS/kS dry 12_0pS/KS dry 120

usfts drypgks dry

pS/kS dry 11.9

!g/Kg dry 11.9pg/r(g dry!g/kg dry

75 30-1fr105 n-150

120 40-14t

120 40-140

70 30-150100 30-150

116 40-140

129 40-140

70 3&150110 30-150

55 30-15075 30-1fi

83 4G140

86 40-140

4s 30-15070 30-150

81 40-140

84 40-140

50 30-15075 U-150

3030

BRL

ARL

ARL

BRL

BRL

BRL

292

BRL

BRL

6_428.75

120

147

5.978.95

BRL

BRL

BRLgRL

BRL

BRL

21 9

BRL

BRL

BRL

21 9

BRL

21 I

404040404040404040

29

5050

BRL

BRL

ARL

ARL

8RL

ARL

ARL

!dlsgE|(s

ftdk9udksUs/kg,rgKsus/ks

28.6

28.6

28.6

24.6

28.6

28.6

28.6

Thit hbonlory rcpatl k nal yditl *ithout n oulhotited sEnalurc on the cojer page.

'R€ponable Detection LiDit BRL = Belo* Reporting Limit PaBe 123 of 152

Page 507: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mivohdle Org|tric Compounds by cC - Quallty Control

Spike

Brtch 7031170 - SW846 35508

Ahnk fl03ll70.BLKi)

Prepar€d: 21 Jrf ar{7 AnelyTf,d: 24.Me147

PCB 1262

PC8 't 268

Sunog|ale: 4, 4-O&Octet/D.oblphenyl (S!)Sunogab: De@chbtobiphdlyl (Sr)

LCS fflXIt70€StI

P.eparedr 2l- Er-07 Ahalyzed: z+ltat4t

PCB 1016

PCS 1260

Surmgate : 1,1484cbfl uotoupllent4 (54Suttoga'€j Dec&hbftbiprwtyl (Sr)

LCS Drd ato:'{ 170€SDi l

PrepEr€d: 21 {rar-07 AnEtyz€{j. 244/€147

PCS 1016

PCB 1260

Sunogate : 4, +DBactafi @rohiphenyt ( SlSu,'ogata : Decacnlot&iFhenyl ( St)

BRL

BRL

21.431.4

421

450

20.031.4

|dkgpcl(sdks

pofts

ugls|rdlisr4yksr{y$

l|sasvgts!grsvgks

Fgllsus/ks||gkgt gikg

ugl(9!grslls/kspdkgugksrgkst/dl(S

24.628.6

357

357

2 8 628.6

357

2 8 628.6

28.62S.6

28.628.6

27.4

27.1

27 _4

27.4

27.4

27.4

27 -4

27.4

27.4

24.6

28.6

42946620.o31.4

75 fi"1fi110 tu1tu

1ia 4&140126 4{tt4o70 fr-150,10 3tt1fr

120 40-140r31 44n4070 30-tg114 30-150

u) 30-150115 W-te)

3030

Dudicate fi03l I mouPt l Sourca: 3A59.16+10

Prepar€d: 21 -l,far47 Analy"€d. 24-ndet{i|

PCB t 0t6

PCA 1?21

PCB 1232

PCB 1?!2

PCS 1244

PC8 1254

PCB 1260

PCB 1262

PCB 't 268

S/,j/rcga/l6: 4,4aS4danuorcbiphenyt ( SoSunogdte: Dec'clbrohipheffll (So

Brtch ?03117r - Sr#845 3ssof,

Abok fl0illl7'lSLK|l

Pr€per€d: 21 -Mar47 AnalFed: 2SM€F07

AHrh

a€HC

b.BHC

d€Hcg€HC (U.rden€)

Chlordane

4,15DD (p,p')

4,4{OE (p,p')

4,4ODr (p,C)

Oieldrin

Endosulfan I

Endosufian ll

E ldosulfan gdfate

Erdrin

Enddn Aldehyd€

Hegtad or

M€thqydrb{

l-lEptadlb. Epoxide

ORLBRLARLBRLBRLARLERL8RLBRL21.931.4

BRL

BRL

SRL

BRL

BRI.

BRL

BRL

sRtARL

BRI-

BRL

SRL

sRr-ERL8RLBRL

BRLARL

BRL8RLARLBRLBRL8RLBRLBRLSRL

.t0

4A40&4040404040

2 7 3

pdts|lgr€ps^spgrspdksg{yr(gpsikspgl(spdkg

flgxs!dhst dkgucrts!grst/g'r(g|lgk€l{ftsvdtoItC}q

14.314.314.314.3t4.371.514.314.314.31 4 3t4_314.3t4.314_311 .314.3t4.314.371.5

Thrs taboralory rqn , k dot edtd nitttord an ald.or*ll 4MlaE on ah. cova pag._

'R@ortabl€ Detection Limit BRI= Below R€porting Limit Pagc 124 of l52

Page 508: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - Qurtity Controt

Spike

Level

%REC

Limits

Source

Result %RECRcsult Units

BRL

BRL

BRL

18.531.4

25.8

23.6

24.1

13.0

23.2

28.1

294

32.9

27.5

30.4

3 1 . 6

30.1

3r-o27.238.029.4

28.6

28.O

329

18.33 7 1

24.8

23.1

23_8

12.3

23.9

26.2

2 6 0

295

25.2

27_O

24.7

30.0

30.2

26.6

32.2

26.7

25.2

25.4

27.O

18.2

pryxgug/Kgps/ks

!g/Kg

!9/Kg

LjEKg

ptyKg

r/dksu(/Kg

!sfts

!gKq

PEKg

t/(yKg

tjlvK9

tr9/Kg

trgr(g

t/s/Ks

vslkspgtxg

!gr(sIJgKg

ugKgs/Ks

!slksfdks!9Kgp9(9

pdks

trSilqpgl(spg(g

tjgn9!dk9!s/kgug/Kgt gKs

!gK9pgKs

|lgKgpgKg

ugKgpdl(s

!grsp9xsFS/kSpgkspgkspcks

14.3

14.3

14.3

RPDLinit

303030303030303030303030303t)303030303030

FlaB RPI)

Betch ?031171 - sw846 35508

Ahnk {703ll71.BLKIl

Pr€pared: 21-lvlar-o7 Anallzed: 25-Mar{7

a1,l,Dt6a/],eg{hlordans

Endin Kebn€

S unog ale : 4, +D B 4 cI a ff uorcA p h e nyl ( S 4S unog ate : De c.ac hl o tobi ph e n yl ( S t)

LCS I7Gltt7l€S

Prepafedr 21.tvlar-O7 Analyzedt 25-Mar-07

Ald.in

a€HC

b4HC

d{Hcg€HC (tjndane)

4,4-DDD (p,p')

{,40DE (p,p')

4,4OOT (p,p')

Dietdkin

Endo8llt'Bn I

Endosulfan ll

Endosulbn Sulfate

Enddn

Enddn Aldehyde

Heptact o{

Hegtachlor Epoxide

a0{odanegFchbdan6

Endrin lGtone

S u nogate : 4, 4 O B -Octa fl @ ro bip hen yI ( S ISu.rggate: Decehlorobiphenyl (54

LCS Dup (?03li7laSDl)

Prapdted: 21{lat47 Nralyzed: 25-Mat4t

Ahdn

a€HC

b€Hc

d-BHC

g-BHC (Ljndane)

4.4-DDD (p,p)

a,a-DDE (p.C)

4,4-DDT (p,p')

Dioldrin

Endcsulfan I

Endo$ullbn 1l

Etdosuif€n Suf'ate

Endrin

Erldrin Atdehyde

HspffiilC)f

Methoxyd{or

H€ptachlor Epoxide

+Chlordane

g€hbdane

Enddn K€trn€

Su'd6la : 1,14B4cbnuo@bipheny! (SO

1 4 . 3

1 1 . 3

1 4 . 3

14_3

1 4 . 3

14.3

1 4 3

1 4 . 3

1 4 . 3

1 4 . 3

14.3

1 1 . 3

14.3

14_3' t4.3

1 4 . 3

14.3

14.3

14.3

14.3

28.628.6

28-6

28.6

28.6

za628_6

24.6

2a_6

28.6

28.6

246

28.6

28_6

28.6

24.6

28.6

28_6

28.6

24.6

28.6

28.6

28.628.6

2 8 6

28.6

28.6

28.6

286

2 8 6

28.6

246

2 8 6

28.6

28.6

28.6

28.6

2a_6

28.6

28.6

28.6

24.6

28.6

24.6

28.6

14.3

14.3

14.3

1 4 3

1 4 3

14.3

1 4 3

14.3

14.3

1 4 . 3

14.3

1 4 _ 3'14_3

14.3

14.3

14.3

14.3

14.3

14.3

14.3

65 30-150110 30-150

90 4.0-140

03 40-140

84 40-140

45 40-140

81 40-140

98 40-140

104 Q-140

115 40-140

!]6 40-140

106 40-140'110 ,$-'140

105 4G140

117 40-140

108 44-140

95 40-140

133 40-140

104 40-140

100 40-140

98 40-140

115 4A-140

64 4t)-140130 14-110

87 40-140

81 40-140

83 40-140

43 40-140

u 40-140

92 40-140

91 40-140

103 40-140

88 40-140

92 40-140

94 40-140

86 40-140

105 40-140

106 40-140

93 40-140' | 13 4G140

93 4G140

88 4G140

69 4t!.140

94 4G140

u 40-141)

3

2

1

5

6

1 1

9

1 4

1 6

20

1 l

2

2

1 6

1 l

1 0

20

Thk hborutoq ftport h aot volid withoft M aurhoriz.a signourc on the cover page

r Reportsble Deteclion Limit BRL = Below Reporting Lirni! Page 125 of 152

Page 509: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatlle Organic Compounds by GC - Qurlity Control

Analyte(s) Result Fhg

Sourc€Resuft o/&,ECUnits *RDL

Spike

Letrel

o/oREC

Limirs

RPDLinutRID

Baich t03ll71 - SW846 3ss0B

LCS Ouo fl03ll7l€SDl)

PmpaI€d: 21-{ta.{7 Analrzed: 25J;,,s'.O7

Sunogate: Decachlorohipheny' (Sl 105 4A-141)

Duollcat (7031171-DIJP1) Sourc€: SA5g.l6a-lO

30.1

SRL

SRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRI.

BRL

BRL

sRrARLaR!8RLBRI.BRLBRLBRL19.435.2

BRL

BRLgRL

BRL

BRL

ARL

ARL

BRL

BRL

20.o

13.7

1 3 7

13.7

13.7't3.7

68.4

1 3 7

13_7

r 3 7

13.1

13.7

13.7

13.7

13.7

13.7

1 3 7

13.7'13.7

68.4

13_7

13.7

13.7

ARL

SRL

SRL

Bftr

BRL

ARL

ARL

BRL

ARL

SRL

BRL

BRL

BRL

BRL

BRL

aRtBRL

BRL

BRL

8RL

ARL

ARL

Lrdks

pgxg

!sftsugK9ugx9rdks|ldkst dkspg/tgysft9

t dks!dksr9?q,|ldkous^glrgt€Fgrs!gkstrgrl€udks!dkspdkg

Fs^9t'dksFdks

Ug/kg w6l

ydkg ',v€i

Pg,ts ret

Udkg vJel

Ugr'kg';yet

lSftS wet

lglt(g w€l

!g/*g wel

lrgrkg wet

pgrs !ret

[dkS wet

Prepared: 21-lrar{)7 Aoallrzed: 25-MEr{7

Aldrin

a€tlC

b€Hc

d€Hc

g€HC (Lindane)

Chlordane

a,a.DOD (p,p')

a,a-OOE (p,C)

{,|-DDT (p,p)

Dielddn

Erdosulfan I

Endosulfan ll

Endosulbn Sulfale

Endrin

Endd4 Ald€hyde

Heptachlor

tl€pbdr|d Epoiide

Toxaphene

aChlofdane

g4hlo.dene

Endrh l(eron€

Sunlgde: 4,44a.AdanuotlDipheny, (Sr)Surogatg: Decacl ombiptuny' (5.)

Brlch 703127C - SW846 35508

Blanl O031274€LKl I

PrepaFd & An€lfzsd: 22.1'?tar{7

PCB tO16

PCB 1221

PCS 1232

PcB 1242

PCB 1248

PCB 1254

PCB 1260

PCB 1262

PCA 1268

Su'Ioga€: 4,4-DBndanrgottphenyl (St)S,;1,logate : Decehba phonyt (St)

LCS flOglz7a€Str

Ptbparod a Anslfzed: 22-lrar47

PCA tO16

PCB 1250

Sul'c{/ate: 4,'l{/B-cE.snLarobiphenyl (54Sunogate: Decachli/ohiplr€i'ryl /sr)

LCS Dup t?O3t?IaASEt)

P.epared & Ans,lyzed| 22-Md47

PCB 1016

3030

303030303030303030303030303030m303030

27.327.3

7l129

30-t5t)31 15t)

28.6

28.6

28.6

28.6

28.6

28.6

24.6

28.6

28.6

3SO

4 t 6

20.o30.0

pgagwel 28.€

Fg^gwsl 286pgr'kg r€lldkg wet

Fg/kgw€t 28.6

70 g-1995 n-lfl

i09 4G140t17 40.14070 30-t5o105 vttg

111 4G140

28.628.6

3573,tt724628.6

357&6

Trtis lsbontoryeporl it ,toa vau xtitled dtt arlthod?d dgnatt t or, the coverpge.

t R€poftable Detlclioo Lidit BRL = Bdow R€porthg Limit P.gB | 26 of | 52

Page 510: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organlc Compounds by GC - Quality Control

Analit4t Resutt Frag IRDLUnits

SpikeLevel

Source

ResDIl %REC

%RECLimits RPD

RPDLimrt

Brlcn 7031274 - SW846 3ss0B

LCS Duo O03l27adSO1lPrepar€d & Analfzed: 22,Mar-07PCB 1260S unogEle : + + D EO cta E uo.obiphen yt ( S 4S Mogale : Dec ach I o ro bi phe n yl (54

PCA 1016

PCB 1221

PCB 1232

PCB 1242

PC8 1248

PCB 1254

PCB 1260

PCB 1262

PCE 1266

Su rog aie : 4, 4O 8- Oc b n uo rcb i p h e nt4 ( Sr )Sumg ate : De c ac h brob i p h e n y I ( S 4

43320.0286

Duplicat.{70312ZOUP1I Sou.c€:SA595,|E-02

Prepared ll Anal!.zed: 22-Mar47

ARL

ARL

BRL

ARL

ARL

BRL

BRL

ARL

ARL

21.g31.3

Source: SA59YA.02

llgr(9 wel 28.6

P94(g w€tlgks vr€t

lgkS dry 31.3

Lidks dry 31.3

!g/kS dry 31.3

lVkS d.y 31.3

Lig/kg dry 31.3

lgkS dry 31 3

!g/kg dry 31.3pdkS dry 31-3pg/kg dry 31 3

!S/kS dryPgkg dry

Ug/kg dry 30.5

Pgkg dry 30.5

!s/ks drypSftS dry

LigftS dry 31-0ps/ks dry 3'r 0

Lig/kS dryPg/kg dry

' t21 40-140/0 30-150100 30-150

70 w150100 m-tfi

106 40-'t40

117 40-140

60 30-tfi95 30-150

111 {0-140

121 40-140

60 30-1fl9s m-1fl

357

28.628.6

31.33 1 . 3

381

381

30.530.5

387

387

31.031.0

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

404040404040404C40

5050

latrtx splko a703l27{-tlsl }

Prsp€rsd & A^alyzed: 22-Msr-07

PCB 1016

PCB 1260

S u nog ate : 4, 44 B- Oc ta fl u orobi p h e ny' ( Sr)S u zog ate: De c ac h lorobi p h e nyl ( S r)

405

446

18.328.9

424

46S

14.629.4

BRL

BRL

BRL

BRL

atrix Solts Duo 4031274- SDil Souice: SA50548{2

Prepared & An€bzsd: 22-MaF07

PC81016

PCB 1260

Sunogate : 4, 4-D B- Octa fl @ rob i p h e nyl ( S 4S urogale : De c ac hb tob i p hen y I (S I

Thb ltboralory rcpo.l it ,tol tdd xrlthor.! an salhofu?t sigutae od thc covet plge.

. R€portable D€t€cdon Limit BRL = Below Reporting Limit Page 12? of 152

Page 511: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgrnic Compoutrds by ffMS - Quslity Cootrol

Analyte(s) Result FhC Units

Spike

Leeel

Source %RECResult %REC Limits

RPDRPD Limit

Brrch 7031070 - swMS 3510c

Blank f?03t070€LKl)

Preparod & Analfzed: m-irar{7

Acenaphhylene

| €thylnaphthal€ne

f -il€ttryhEphtlElene

Atazln6

Azob€nze{E/Ixphefl yldiazin€

B€nzidirE

Benza (a) anthracene

Benzo (a) anthracene

Benzo (alp cne

Benzo (a) pyrene

Benzo (b) fluotanthone

B€nzo (b) ltroranthen€

Benzo (g,h,l) pery4€n€

Benzo (g,h,i) perylene

a€nzo (k) ftroranhen€

BerEo (k) fl0oranfEne

B€nzoic aclt

BenzY fuhd

Bis(2d oro60roxy)fi €tEne

Bis(2d{orGttyl)ether

Sis(2-chb'roi8oDropyl)etller

Biq2-etrylh€xyl)phlhalats

+Brorbphsnyl phenyl €ther

Butyl berEyt phthalat€

Carbazole

4-Chbm-}fnet'tyiphenol

4-Chloroailllne

2Chto.onephttulene

2.chlompheml

4-Chlorophenyl pnenyl €tner

Chrys€ne

Chrys€ne

Dib€rEo (a,h) anlhrac€ne

Dib€nzo (a,h) snthrac€ne

OlberEofu€n'1,2{bhbmb€rPene

1,lDichltrobmzene

I,4-Dir*rkroberu€n€

3,3--Dic*rffi€nzltine

2,+Did ooph€nol

Oierhyr phth€ al€

Dimethyt phtlslate

2 +Dnnetrylph€nolDi{+utyl ph0|ale{€

4,6-Oinilro-2{€thylphend

2,&Oinnroph€ml

sRtBRL

BRL

BRL

BRL

BRL

SRL

BRI,

BRL

BRL

BRL

BRL

ARL

SRL

SRL

ARL

BRL

ARL

ARL

BRL

BRL

BRL

BRL

SRL

BnlBRI-

BRL

8RL

BRL

ARL

aRI

BRLgRL

BRL

BRL

BRL

8RrBRL

BRL

BRL

BRL

BRI.

BRL

BRL

BRL

ARL

BRL

BRL

8RL

ARL

BRt

8RL

r9l|ldl

|lEl

vallustIJdIps,4l,sn|,dl!s/|usn!(t/l[!yl1ldr$llusnFgl

!dl

usrlt (yl

lrg/l

llgn

IJdI

!dl

|,dl

wFS4pql

!dlpdl

ttg/]'

lr9lpgl

psnFdltjs/|ugrll€rl$rluglFdltgllIrdl|,g/lp0,

|lg4

pdl

!dlIrdludlys4pcrl

0.0501_000_4000.0500.05t)1.001.001-000 0501.001.00t.000.0500.200o.0500.2000.2000.0500.0501.00o.3000.050|.fl)'t_t)0

l-001.001.00t.00t_001.00't.00

1.OO1.001.00|.o01.001_000.050o.0500.200|.00t.00't.00

1.001.00r.001.00t.001.00to0L00|.00

Thh lobonury repod b Eot tead withoat zn aadtotlzd igndre ott rhe coje, pogc.

* Relofbble Detection Limir BRL = Belo{ Reporring Limir PaeE t28 of 152

Page 512: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgaric Compounds by GCMS - eualify Control

An8lytqs) Result Flag UnitsSource %REC

Resulr %REC Limits

Spike

l-€vel

RPD

Limit

Brtch 7031070, SW8463510C

B|a* {m310?0€LKlt

Prepared & Andyzed: 20-MaF07

2,+Dinitotoluene

2,c-Dinibotoluene

Di-n{ctyl phthalate

Fluorene

flerac-hloroboneene

tlexachlorobuladiene

H€xachlorocyclopentad iene

Hexachloroelhan€

lrdeno (1,2,3<d) pyrene

l.deno (1,2,3-cd) pyrene

lsophomn€

2-l,lethylnaphtnabne

2-llr6tht{naphthatene

2.Metrylph€nol

3,4-trr€thylph€nol

Naphtnalene

Naph|tlalene

2-l.litroanifine

3-l{lt oaniline

4-l{iboaniline

Nilrob€nz€n€

2+litrophenol

4-a{ttropherrcl

t{-l'lilr-Godlnethylarnine

N-l'{ilroGodi-n-pmpytamine

N-l'lilrosodiphenylamine

Ph€mnhlene

Ph€ml

Pynijin€

Heradrlorobenzene

1 ,2,+f.*ttt robenzene

Peniacfiloroph€nol

2,4,s-Trid|hroph€nol

2,4,&Trld oophend

H€xadtlorobutadi€n€

Su n({/ste : 2 + I uo rob t p he n ylS,//rogate: 2+ fu o to U p henylSll,roga,€ : 2+ I tb to ph e n o I€unogelg : N ih{,,he n zen e4 5Sfiogata: Phend4sSunogate: feryhenyl4t4Suftlgab; Teryhentl4l4Sunogab : 2, 4,6. Tt b to ft ap h e nol

LCS ft031070€s1)

Plspared & Analyzed: :t()-Marry

8RL

BRL

8RL

BRL

ARL

BRL

BRL

SRL

BRL

ARL

BRL

ARL

8RL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

aR(

BRL

ARL

BRL

BRL

8RL

90,390.393.910690.o10310371.7

ps/l

l.rg/lps/l

!9n

t(yl

Fgl

lrgpgn

!g/l

!9/l

!srp(vl

pgl

psnpsnpc{pgl

!(/l

tj9l

!s/l!s/l!gnps:4ps/lp9l

!gnusllLiS/l!gnpsn

!gnugnLj9l

!gn

!gnpsrl

!gnps/l

psll

!91ps,4

!g/lpg/l

!s/lpsnps,4f s.4!c4!dlIJ9Ipdt

t 0 01_001 0 01.00o.oil1.000.0501.000 6001.001.000.0500.2001.001.000.050t,oo1 0 00.0501.001.001.001_(101.001.001_001.001.001.001 0 00.0501.001.000.0501.001.001.00r.00r.00t _001.00L000.5m

too1001001001M100100100

9090941069010310372

3o-1m30.13015,1103o-1N15-t 1030-13030-13015-110

Thit labo.alory pport h not wlid tollhouj sn atdro zed signtrlne on the covcr ttoge.r Reportable Det€ction Limit BRL = Below Reporting Limit Page I 29 of I 52

Page 513: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mivolatile Organic Compoundr by GCMS - Qustify Control

AnalyteG)Sourc€

Result

RPDLimit%REC Limits RPDR€sulr FIag Unitt

Baach ?0J 1070 - SW846 3510C

LCS t?(Bt070€S1l

Pr€psred e Analfz6d: 20-Mar{7

Acenaphthyl€lte

l -Ivlelhylnaphthalene

1 .ftlethylnaphthabn€

Azob€nzene/DiptEnyldiazine

B€nidine

Eenzo (a) entluacene

aeozo (a) anthracene

B€nzo (a) py.ene

Benzo (a) pyr€ne

Benzo (b) fuoranthene

B€nzo (b) furoraotr€d€

Benzo (g,h,a) p€rylene

Benzo (g,h,i) pery'enegenzo (k) nuoraothon€

Benzo (k) ffuofanthene

Benzoic aodgenzyl alcohol

Bis(2-dbroethory)rnethane

Bis(2.chloro€thyl)ethe.

Bis(2drloroisopropyt)ert€r

Bis(2-€try'herylE hthalate

4-Aromophenyl ph€nyl efi er

Butyl benzyl pht'halate

Carbazole

44hk ro-3flethytsh€nol

44hbru6nilin€

24hktrohaphthal€ne

24hlotEphenol

4chlotophenyl phenyl ether

Ghrysene

chrysene

Dih€nao (a,h) afl thracrne

Dlb€nzo (a,h) anhracan€

Dib€nmluran

l,2obhbrobenzone

1 ,3oichlorobenzerE| ,+Di€filo.ob€nz€n€3,3..Dlchh.obenzidine

2,+oichlorophenol

Di€thyl phlhalat€

Dhelhyl phthabb

2,4-Dimelhy'phend

Di-n-butyl phuralete

4,6onitr+2Jn€hylph€nol

2 Soinibophend

E2.882.892. r92.185.785.71 1 39r.691 .61U106

83.583.592-0s2.882.682_669.169,110510565.884-692.3

6r.8t0184-010112988.243.287.072.582.949.I89.186-786.7a7.777_O6S.479 .194.9m.090.9E6.€79.390.972.784.6

|lsnt|94!snpcl

!dl!dllrgl!c4pdl

!snrdll€4

pdlpsr!Elpdlps,lpgnpdl

udlItg!l

tjc4pdl

!9n

udlt'$tsllpdl

!sntts/l'@lvgtlpql

!snrs4|lsnItgllp9/l

!dl

Fdlpsnus4pdl

!dl

!dl

us4lrdll)glt'dl!drttglt s {

1-O0o.0500.4000.050't_00

0.050r.00t.000.050't-00

1-001.000.0500.2000.0500.2000.0500.2000.(m1-000.0500.3{x)1.00r . t o1,001.001.001.001.001,OO1.00L001.001-001-001.(X)r.fil0.0500.2000.0501.00r .m1.001_00'1.(x)

r.00r.001.mt-001.001-{X)r.00

r00100r001 m100t00100'tm1 m100t00100100100100r0010016100tmt00r00100100r00r00'tclo

100100r001001001001001001fi)1m'100

100r001001m1001001001001m100'r(x)r001001m

83 .r0-r40&, 40-1109:l 4&1.$92 4Sr4086 40-14086 4{11{0113 40-14092 4&1,1092 4G1401U G200106 40-140126 ,lO-14O

04 40-t,tt)84 40-14093 40-14093 40-1.10&l 40'1{08:t 40-14069 40-14069 40-140tos 40.140105 ,10-140

86 30J3085 40-14092 4S.'14095 ,lG1.l0

62 4Gt40101 40-14084 40-110101 4G1,10r29 ,|{).'140

88 3St3003 .$-140

a7 40-1d672 30-13003 4o.1,r089 4G14069 40-14087 4G140a7 &11088 {G1407f 40-14069 40-14079 40-14095 1S14060 3$.13091 40-14.087 1o-14I79 3G13091 ,lG14O

73 3{!rr085 3G130

This bbralo.y Eltort k ,tot tatfut $ holt ar authorfud sig',&tre oa th. cnter pqe.+ Rcporr.ble DelEcrion Umit BRL = Bclow R€Foriing Limit PaAe 13O of 152

Page 514: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semiyolatile Organic Compounds by GCMS - Quality Control

AnalyteG) Resu,l .RDLSpike

Level

TOREC

Lirni(s RPDRPDLimitFJug Units

Source

Result %REC

B{rch 70J1070 - sw846lst0c

LCS f703t070-ASrl

Pr€pared & Analyzed: 20-Mari7

2,4-Diflilrotoluene

2,GOinitrotoluene

Di-Goctyl phlhalate

H€xachlorob€nzen€

H€xschlorobutadiene

Hexadllorocychpentadien€

Indeno (1,2,3-cd) pyrene

Ind€no (1,2,3,cd) pyEne

lsophorone

z+r€thylnaphlhalene

24rethylnaphlhalen€

2{'lethylphsnol

3,4-M€th)4phenol

Naphthabne

Naphthalen€

2-Nilroaniline

3-ilitoaniltne

4+.litroEnilln€

2+li8opfi€nol

4-Nitrophenol

N-NitrosodimethYamine

N-l,lilrosodi-n-propyramine

N-Nltrosodiphenylamine

PFidin€

Hexachlorobenzene

Hexachloro€lhane

I ,2,+Tri$lorobenzene

2,4,5Trid oroph€nol

Penbchlorophenol

Hexad&aobuiadiene

2,4,&TrftJtlorophenol

S unogate : 2 + hJo n N phe nylS u nogab : 2 + I u o to bi p h e ny ISuftoga|]e.:2+l@tophenolSwrogale : N ihoben ze n e4 5Sl/froga/€: menol4sSunogata: Teryhenl4l4S u nogate : Te,p he nyl 41 4S uiog ate : 2, 1, 6 - f n brcn o ph end

Brtch 703 (278 - SW846 f5508

ehnk 1703'127E€LKIl

95.6

94.3

1 1 8

8 3 0

83-0

8.r.5

8 4 5

80.5

19.4

7 1 . 6

7s.0

59.7

55.7

s 3 8

E9_3

89.3

74.8

84.8

84.8

90.9

8S.6

1 t 5

102

80.7

5S.0

423

4 1 5

1 0 1

7 4 0

8 0 4

80.4

42.5

86.8

86.8

85.9

80.5

75.0

41.2

92.1

74.0

I9A

68.5

91.891.871.71 1 075.597.297.283.5

1_001 0 01 0 01_0000500.0501.00r.000.6001.00r_000 0500.2001.001.000.0501 0 010.00.0501_00't.00'1 00'1 001,001_001 0 01 0 01.O01.00r.001.000.050r.000.0501.001.001_001 0 01,001-001.000.5001.00

100

r00100r00100100100'100

100'tff)

100100I Cro100100100100100'| 001001001001001001001 m1 m1001001001001001001mr001001001(1t)1001001001001001M1001N1001001001(n100

!gn

us.4ugl

!91

!g/l

!s/l

!El

rc/|trg/l

!9r

ItElpsn!c4p9l

u(ylug/lrs/l|lsnvgrllig/l

uElpdlpglps,4

!gn!gn!g l

!g/l

tr9/l

us/lItgtl

lr(yr!91

us/l!g l

lrg,WnpsnpsnpsnpdlFEI!s,4ps/lLjgl

!sn!snpgl

!dlu9/lpg/l

96 ,rO-140

94 40-140

118 40-140

83 40-140

8:t 10-140

84 40-140

84 4G140

80 40-140

79 40-140

72 40-140

15 40-144

60 40,140

60 40-140

94 40-140

89 40-140

89 40-140

75 40-140

75 40,130

85 40-140

85 40-140

91 40-140

90 40,140

115 {S140

102 40.140

81 30-130

59 30-130

a2 40-140

42 40-140

r01 40-140

74 30-130

80 40-140

80 40-140

82 30-130

87 40.140

87 40-1,$

86 40-140

80 40-140

75 40-140

84 4G140

92 3G.130

74 30-130

7S 4G140

68 30-1311

92 #13092 3G13072 t5-110110 fr-13076 15-11097 3L13097 30-1mu 15-110

Thb labontu4t Epotl it ,tot vzlu i'ilhoat tE o!rtoized signainre on the cowr pge

' Ret'orirble D€t€ction Limit BRL = Below R€podng Limir Pase 131 ot 152

Page 515: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgatric Compounds by GCMS - Qurlity Control

Anflbtds) R€sulr Flae Units .RDLSpike

Level

%RECLimits RPD

RPDLimit

Sour,rResult '/oREC

Brrch 7031278- SWE{6 35508Prepa.6d: 22-MarO7 Analyz€d: 23-Mar-07

AnilinE

Ahazine

Azobenzene/Diphenyldiazanegenzidine

A€nzo (s) snthracerE

Benzo (a) pyrerEgenzo (b) iuoranhsfl€

B€nzo (g,h.i) perylene

B€nzo (k) nuoranlhene

Benzoic acid

B€nzyl alcol|ol

Bb(2drloroelhoxy)m€lhan€

Ai.s(2d oro€trY)€ber

Bis(2d oro{sopropyl)elher

Bis(2-€thylhexyl)phthalats

4€romoph€ny' phenyl ether

Butyl benzyl phtElate

Caabazole

rchb,ro-3-m6thylpheml,{-Chlo'roanilne

24hloronaphfielene

2.chlorophenol

4chlo.@henY ph€nyl elhet

ChryEene

Oibenzo (a,h) anthracene

Dlb€nzofuran'l,2Oichlorob€nzsn€

I .3oichlorobenzene'1 .+Oic+ ofobenzene

3,3'-Oidbrob€flzidin€

2 JOichloroph€nolDietryi phthalats

Dinethyl phtrialab

2,4-Oirn€thylphenol

Oi-nSuryl prtihsbt€

4,$Oinirc2.m€lhylphenol

2,lEinilrophonol

2,+Dinitololu€fl€

2,H)inihotolu€ne

Di+octyl phfialate

FluoEnlhen€

Fluoren€

H€xachlorob€nz€ne

H€xechlombutadisn€

H6xachlofi ccyclop€ntadien€

H€xschldoofn€n€

Indeflo (1 ,2,3-cd) pyren€

1 -fvlelhylnaphlhalene

lsophorde

2-t lethy'naphthsl€ns

2-M€l,hylptFnol

ARL

BRI-

8RL

BRL

8RL

8RL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

ARL

BRL

sRr-ARL

BRL

BRL

BRL

8RL

BRL

BRL

8RL

SRL

BRL

8RL

BRL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

SRL

BRT

SRL

BRL

BRf

ldkgwet 30

US/kS {v€l ix}opgy'kg v/et 330

rcL/kg vY€t 3:)0

!S/kS Y,/et 330pSr'kS wet 330

!g/kg wet 330

lrg/kg wet 330

lgikgw€l 330

rc/*g n€l 330

lg^g wet 330

!g/kS w€l 330pgftg wel 330

Pgr'kg w€l 330

ldtS lYel 330

ldrgYiel 330

ldkg Yr€l 33t)

!S,4(S rret 330!S/kg wet :}i,,0pdkS wet 330

lgL/kg {,et 30

tidkS vret 3l]0

lgr'kg wet 3il0

lgrl€ wet 330p€/t€wet 330lg/kgwet 330

Ig/kgw€t 33O

|lgr'tgwer 33oIg/?€ $/el 330

tigRg wel 330pgikgw€t 330pdkg wel 330pqkS wet 33O

!g'kg w€l :I:}0

lS&Sn€t 33O

lidks wel 330lgn(g wel :I10

IgL/kg w€t S0

Udkgvvet ai!0!S/kS vret 310lgr'kg wet 3:10

lgr'kg w€t 33Opg/kg wet 33Opg/kgwet 330

l€n€wet 330ug/kg wet 330yg/kgwet 330pgtlg w€l 330pgtg$€t 330pgrkgw€t 33t)pgftgYr€t 330

lSftgrY€l 33O

ldkgw€l 330

rcfxg wsl 330

Thb taborulorf Eporl it nat wIU uUhosr cd .uthori@d sig',,rtare on ahe coee page-

r Repntablc Dett€ion Liqrit BRL = Bclow Reporting Lioit Page l32ofl52

Page 516: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Quality Control

Analyte(s) Result Flag Units .RDLSpike

t€vel

%RrcLimits

RPI)

I - imi tResult %REC R P D

Betch 70Jt278 - SW84615508

Blank 17031278-BLKll

Preparcd: 22-i,la.{7 Anatfred: 23{,laF07

3,4+vlelhylphenol

NEphthalene

2+lit o€oiline

SNitroaniline

4+{ikosnilin€

Ntrobenzene

2+likophenol

4+liroph€nol

N-NitrGodi.r€lhylamine

N-NibGodi-n+ropylamine

N-Nibosodiphenylemine

P€ntachlorophenol

Ph€ml

Pyridine

1 2,4-T.ichlorobenzen€2,4,$Tdcnbr@henol

2.4,eTdchlomphenol

S u rogale : 2-F I uorob i p h e n ylS u ffo9at6 : 2-F ro rophe no IS u rogate : N ltobe n ze ne - d 5Sutrogate: Phenol46Suroggl€: Te9henyl4l4S u tnualE : 2, 4, 6 -T n b Mno ph en ol

LCS t7031278€5

Prepared: 22-Mar{7 Analyzed: 23-lvlar{7

Aniline

Azobenzen€/Diphenyldiazine

Benzilin€

Aenzo (a) aothracene

Bsnzo (a) pyr€ne

Benzo (b) ffuoEnthene

Benzo (g,h,l) perylene

S€nzo (k) nuoranth€ne

Bmzoic acid

8enzy' alcohol

Bb(2-d oroethoxy)methane

Bi.s(2{hloroehY FtherBE2d'lomisoprop)4Fther

Bb(2-ethylheryi)phthalate

+B@floph€nyl ptienyl etler

BUV b€nzyl phthalal€

Cabazdett4hlom-3fi ethylphenol

{-Chloroanilin€

2-Chlo.onaphthalene

2Chlo.ophenol

4€hlo.oplEnyl phenyl eher

BRL

BRL

BRL

BRL

ARL

BRL

ERL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

532052606490514062903900

5350

5910

66S0

5970

7500

6850

BRL

5'160

5700

5 1 1 0

4550

6 1 1 0

5480

5280

5780

6170

5110

6360

5170

6'r90786055205040$9045305490

667066706670667066706670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

pS./kS wet 330

lgkS Yvet :]i]0

lgr'kg wet 330

Lig/kg wet 3il0

lig/kg wet 1320pg/kg wet 330pgkswet 33O

lgL/kg wet 1320

!g/kg wet 330

Ug/kg wet 330

lgL/kg wet 330

trg/kg wet 330

Ugr'Kg wet 330pgr'kg wel 330pgn(g wel 330

Ugr'kg wet 330pg/kg wel 330

Ug/kg wel 330pgftg wet 330

!g/kg wet

|lg,/kg wet

!g/kg wetug/Kg welUgkg welpgr(g wet

ug/kg wet 330

PgL/kg ',el 330

!g/kg wet 330

Ug/kg wet 330

Ug/kg wet 330

!g/kg wet 330

!g/kg wet 330

Ug/kg wst 330pS/kg Y/et 330

!g/kg Y/et 330

ldkS wet 3il0pdkg rret :l3O

!94q Yr€t 3{}0

ldkS\det 330

ligkswet 3l]0

Ugftgw€t 330pg/kg w€l 330pg/kg wet 3i,0

l4/kg w€t :l:],0

Ug/kg wet 330

Ugltrgwel 330

lgr'kg wet 330

Ug/kgwet 330

Pg/kg we( 330pdkswet :t:|0

t'dkg wet 330

80 m-13079 1U110s7 3G13077 1U11094 30-13058 16110

80 40-13089 40"130100 40-13090 40-130112 4&130103 40-130

0-13077 4o-13o85 4G13077 10-13068 40-13092 40-13082 0-13079 40,13087 40-130s3 40-13078 40-13095 40-13078 40-13{)93 40-130118 40-13083 40-13t)76 40-13082 40n3068 40-13t)82 4.G130

Ihit bhoralary ..po.t is ,un valid vitho4 an c{&oriaed signalw on tre cot E prye -

. Reportabl€ Deteciion Lirnir BRL = Below R€poning Limit Pase t33 of 152

Page 517: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semlyolatile OrgNnic Compounds by GCMS - Qudity Control

Anflbae(s) Result Fhs Uniis RPD*RDLSpikel"evel

RTDLimit

Sourcq %WcResult %REC Lir ts

Brtch 70312?8 - SWE46 35508

LCS r703t270€: I

P.epared: 22{rar-07 AnElyzed: n.l|,€f 47

Chrys€Ile

Dib€ruo (a,h) entnrEoene

Dibenzofuran

1,z-Diihrob€nzen€

I,3.Dicl orob€nzene

1 ,4Oichbrobenzene3.3'nlcilorobenziline

2,4Oidrlorophenol

Di6fi!,1 pht|alele

DinreEtyl phthalab

2,4oimeb/pft€nol

Di{-buM phtl|a|et€

4,6-Dhitro-2{helhylphenol

2,+Dinitrophenol

2.rtDinitrotoluen€

2,6oinlUotoluen€

Di.n-*tylph8lahte

Ft orarttErE

Hexachlombsnz€ne

ilexaclrlsobutadlene

H€xschlorocydop€nlEdiene

HexacrdoroelhEne

Indeno (1,2,3d) pyrene

lsophorone

1 {rethyLtaphthal€ne

2-Melhyhephtrsbne

2-f ethylph€nol

3,+M€lhylpherol

N6phthalen€

2{.litsoanilin€

3-llilrcaniline

4+lihoaniline

Nibot€nzene

2+.litophenol

4{'{itrophenol

N-l.lito$odtn€lhylamioe

N-Nibosodi-n+rogylamin€

N+,lilrosodiphenylahine

PenLdrlorophenol

Phenol

Pyridine

1,2,+Tid*orob€rEene

2 r, tTrichbroptEnol

2.4,STric*rlo.oplEml

Sffilp,ate:2+IwmblphenylSu nogato : 2 +l @toph en otSuftogala: Nfuolj€.nzene4sSunogala: PhenoI4SSurYoga(e: Ierp|t€flydl4S uttogab : 2, 1, 6f tibtonl€ptl€nd

550052705610448042m51505&X)49505690535044105810441050705470

f5205040554050005020,1520

50r046S0s89054'70

4730487D552056,|057E0752063iX)497037605r503@O6470454050505210va04020522058404rtu56rO4"8)6560154)565048fi

6670667066706670

6670667066706670

6tt706670667064706670

667t)6670667066706{t706670667066706670

66706670

66706670667066706670

66706670667066706670

667066706670€670

467086m6470667066706670

!dl!S wet :|:}0

!q/19 wet 330

Ugikgwel 330

Udkg w€l 330

!g/kS Yr€l 330

!g/kg wet 3:10

lS/lqwst 330

Fgfkg wel 330

|Jgtg w€l 330

!9r'k9 rsi 330

Idl(S','/el :l:10pg/!g wst 330

Ugftg w€t 330pSI(Svr€t 330

ldxg vJ€l 330

ldl(g wet 3i'0

FBfkg wel 33O

Ugr'kg w€t 330

t gl(S v{el 330

UdXS wet :l:}0

lgL/xg wet :x)0

t g/|(o w€t 33O

lgkgw€l 330pg/kg wel 330

rcrxg w€i 330lgr'kg wetWftgwet 30

Ig/kg wet 330

lrqrc w€l 330tgfl(g w€l 330

lgL/kg v/et i]:10

ldkg wet 330

wrtg w€t 1320pqkgwel lio

lgftgn€l :]:j0

lgfq Y{€t 1320pg/tqwel 33Opgrl(g w6t 330pglkg Yt€t 330pgr'kg wet 330

lgks w€t 330

Fgftg wet 33O

l€/kg w€t 330

Fgrkg wet 330

$SlkSY{ct 33O

lBkg $/et 330lrgilgwet 330

tis/kg wett€/|(g wetpqto w€tUdkg vJ€ludko wetugr'kg wet

84 40-'t3079 40-13084 40-13073 4G13t)63 {0-130f7 4O-1m87 40-13074 40-13085 4Gt 3080 40-13072 40-1n87 40-13066 4G13076 4Gt3085 .tG130

s0 .40-130

r 13 {G13076 4t)-1&&3 40-13075 ,$n 3075 40-13068 40-13075 4G13070 .tGt30

88 4$r 30s2 4G14084 40.13071 4G't3073 4{}-13083 40-13085 40n 3087 40-130t13 4G130s5 4G13075 4D-13056 4{-13)77 40-13045 1r()-130

97 40"t306a 4{t13d76 40n 3078 4/l-13/l8:l 1{!,r 3060 ,r0-t3t)

78 4S1308E 4.0-13062 40.131184 3lLtfl67 tS1t09A tu19)68 15-11085 g-ln72 1U110

Ihis latorarorf rcpod it nol telitl,tithotd onz. hodztd stgnatuI:. oE tte canet pagc.

. Re.portable D€rection Limit BRL = B€tow Re-portirC Lirhit Page I 14 of | 52

Page 518: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SemivolNtile Orgrnic Compounds by GCMS - Quality Control

Spikc

E2t h m307a - sw8t6 35508Duollcatel703l27E{UPll Source:SA59S48{2P.epared: 22-{\,{ar{7 Analyzedr 23-MaF07

Alrarne

Azobenzene/Diphenyldiazine

Beozidine

Senzo (a) anthracene

Benzo (a) pyrene

Benzo (b) fuoranlhme

B€rEo (g,h,l)perytenegenzo (k) lluoranlhsne

Benzoac acid

B€nzyl alcohol

Bb(zd oroetroxy)rn€thane

Bis(2d{orueihyl)ether

Bis(2+hloroi6opropyl )€therBir(z-ethylh€xyl)phthalate

4€romophenyt phenyl elher

8uM b€nzyl phthalate

Carbazole

4-Chloro.3-rhelhylphenolrt4hloroaniline

24hlorooaphlhalene

2-Ct orophenol

44hloroph€nyl phenyl ether

Chrysen€

Dibenzo (a,h) anthracen€

Dibonzofu€n

| ,2-Dichlorcb€nzene1 ,!Dichlorob€nzene'|

,4-Dknlorobenzene3,3

--0i,chlo|ob€n?idine

2,+Didlbrophenol

Dlethyr ph{hahb

Oimelhyl phlhalate

2,aoimef\ylphenol

Di-n-butyl phtt€late

4,60iniho-2fl elhylph€nol

2,4oinrtophenol

2,+Din rctoluene

2,6-Dinitolotuene

Dl-n{cM phtt'Elate

Ruorene

Hexad orobenzene

H€xad orobuladiene

Hexadrlttocyclicpsntadiene

Ind€flo (1,2,3-cd) pyrene

lsophorone

I -l,l€thylnaphtllalene

2#ethyhephtnalen€

BRL

BRL

BRL

BRL

ARL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

8RL

ARL

BRL

BRL

ARL

BRL

BRL

8Rt-

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

ARL

ARL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

ldkS dry 231pdkS dry 231

lqkg dry 231

US/kS dry 231

!g/kg dry 231

!g/kg dry 231

!g/kg dry 231pS/kg dry 231

!g/kq dry 231!S/kS d.y n1

liS/kS dry 231

lqkS dry 231pS/kS dry 231pg/kg dry 231pg/kg dry ?31

US/kS dry 231

US4(S d.y 231

!S/kg dry 231

!g/kg dry 231lqkg dry 231pdkS dry 231pdkS dry 231pdks dry 231pg/kg dry 231

LidkS dry 231

!S/kS dry 231

!g/kg dry 231us/kg dry 231pdkS dry 231

!g/kq dry 231

lgkg dry 231pdkS dry 231pdks dty 231

ldkS dry 231pgks dry 231

ldkg dry 231

ldkS dry 231

!SI(S dry 231pg/kg dry 231pg/tg dry 231pdkS dry 231

!g/kg dry 231

!S/kS dry 231

ldkSdry 231pS/lg dry 231pdks dry 231pgks dry 231pS/kS dry 231pg/kg dry 231pg/kg dry 231

lgkg dry 231

ls/ksdry 231

ldts dry 2i1

BRL

BRL

BRL

ARL

BRI.

BRL

BRL

BRL

BRL

BRL

ARL

BRL

ARL

8RL

BRL

ARL

BRL

8RL

BRL

8RL

BRL

BRL

BRL

SRL

ARL

8RL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

ARL

BRL

BRL

BRL

BRL

BRI.

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

50505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050ff)

Thb lIbon1ory rcpoA is not laliil without za oaihoized sigrurwe on th4 cover page_

* Reportsbl€ Detection Limit BRL = Below Reponing Limit Page 135 of 152

Page 519: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgrnic Compounds by GCMS - Quality Cortrol

Analytds) Flag UnirsSpikeLevel

Br.ct 703127t. SW846 3ss0B

Ouplicater703l27&DUPI) Sourcs:SA5O5a84t

Pr€pe.€d: 22-filar4TAnalFed: 23-Msr{7

2-lr€trrylpherrcl

3,4-lrethty'phenol

Naphthslene

2-Nitroanl ne

3-Nitroanilin€

4-l.lilrosniline

Nitrobenzene

2-Nltophenol

+Nibophenol

N.Nlbosodarnenhy'anin€

N-Nitrosodi-n+ropylamine

$Nitrosodiphenylamine

Pentacibrophenol

'1,2,+Trid crobGnzene

2,4,$Tridtbmph€nol

2,4,ETndrbroph€nol

S u nogaE : 2 +tuoft bip he n ylSunogate: 2+hn@phenolSuflggate: Niffienzeoe45Suftqate: Pheno!4sSunogale: ferphenyl4l4S u zog ate : 2, 4 6-ft i bmrnop henol

l|atir Soko (7o:tl 278{Sil

Prepared: 22+vlar{7 Anal).zed: 2}Mar-07

4€hbro-kh€th/lphenol

2-Chloroph€nol

1 ,+Di{$loroh€nzen€2,+Oinilrolol!€nerH{fuophenol

N-Nilrosodi-fl -propylamin€

PentaEhbaophenol

t,2,+Trichlorobenzene

Su/rogate: z-Fhnnbiphen ytSu'rcgate: z-Fh.toft pherolSunqate:Niffinzene4'Swmgate: Phenol4,Sunogal€: Tefienyl4!4Sur'ogale : 2, 1,A- Td b ft noph et'o/

gRL

SRL

SRL

8RL

sRrBRL

BRL

BRL

ARL

BRL

BRL

BRL

SRL

BRL

BRL

BRL

BRL

BRL

BRL

BRI

1480154t)1800t6@19fit2g)

Sourc.: 3A59548{2

32r059005530293J312037403260,1430

$7035S027103r90263037502491)37n26fr

IeHx Splko OtE fl031274- SDl) SoutE i SAsgstg-O2

Pr€pared: 22-lIaF07 Analyzedt 2?-Nlar 07

pgl€dry 231pS/kgdry 231

ldkg dry 231

ldksdry 231Idlq dry 231

t dl(s dry 923t|g4!S dry n1psnq dry ZJ1

Igr(S dry 9?3pCAgdry 231

!g\gd.y 231

Udl(g dry 231

rc/kS dry 231

ld].4dry 231

FdkS dry n1

trg,ll€ d.y nl

ldrg dry 2J1pgksd.y 231pdkg dry 231rdkS dry 231

ldks dryugt{gdtypdkg drytdkS dry!S/P€ d.ypdks dry

USnqdry 231lgkS dry 231pg/kg dry 231

t SI(S dry 231lJg/kS dry 231pdkg d.y 923pdks dry 231!S,/kS d.y 231UgrS dry 231UdkS dry 231

ldkSdry 231

Idks dryldlg dryrc/kS drypdks dryfgtg d.ypdks dry

m/kg dry 233t|gr'kg dry 83lg^gdry 233

FdkS dry 233

t4fts dry 23,:]ldkgdry qli

64 30-13066 15-11077 3G1m72 15-110u 30-13053 15-110

69 40-14t)63 3o-'t3o5S 3&13063 40.14067 {114040 3G.13070 4&t404a 30-13061 3G'r30t7 4o-14o58 {0.14068 n-131)58 11110a) n-19)53 tSlto&) g)-1tu56 1S-1rO

75 4&1,O74 30'13)64 3{tt3t)65 40.t4074 4[-14t)42 3Gt30

2330B:N?33{)nn23fr23m

4660

s32093204660

4660

9320

4660

9320

9320

4660

4660

16ffi16@16@4664166046ffi

470/)

94t0

9410

4700

4700

94t0

SRL

BRL

BRL

BRL

BRL

SRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

8Rr-BRL

SRL

SRL

BRL

ARL

BRL

BRL

BRL

8RL

BRLBRL6RLBRLBRLBRLgRt

BRLBRL8RLBRL

505050505050505u505050505050505050505050

44hloro-3-|nefi ylptleml

24hlorcphenol

1 ,4-Oi* orob€nzene

2,4-Dhitrotoluene

4+.litrophenoi

35206&106010305034603040

6310

30303)3030

Thb labdory Eporl B not efllid Nithou an authadad tlgndue oa ahe covet We.* Reportablc Det€ctiotr Limit BRL = Below Reportilg Limit Page 136 of I 52

Page 520: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - euality Control

Anab,te{$ ResultSpike

Level

RPD

I- imi tFlag Units

Sour€e %REC

Resuli %REC Limirs

Brict 703127E - SW846 35508

t ardx Soike Ouo l7031278.trlsD Source: SAs9548{2Prepared: 22-{vlar.07 Anattzed: 23-MacO7

N.Nllrosodi{-propytamine

Pentad$rcpheml

| ,2,+Trinbrobenzene

Su nog ale : 2 +l tDto bi p he ny1S urog a te | 2 - F I u oto ph e notSunogate : N i t to be n ze ̂ e45Sunogate: Pheftt4sSunogale: Teehentt4l4S unogaE : 2, 4, 6 -Tn b ro nop h e rlol

Batch 70312t2 - SW846 35508

Bbnk 170312E2€LKi)

Pr€pared: 22.Mar-07 Anatyzat Z5,-M1.O7

Acenapht|€ne

Ac€nsphtfiylene

Aniline

Azoberaene/Diph€nyld jazine

8en/dlne

Eenzo (a) anthracene

B€nzo (a) pyrene

Benzo (b) f,uoranthene

8€nzo (g,h.i)perylene

B€nzo (k) fluo.anthen€

Benzoic acid

Ben2yt atcohol

Bis(2-chbroethoxy)rnethan€

Bis(2-chloroothyt )eh€rBis(2<ila{oisopropyt)erher

Bis(2-€thylheryl)phthatatezt8ornophenyt ph€nyt ether

Butyl b€avyl phthahte

C€tbazole

44hbro-3-methylphenol

44hb.oaniline

2{hloronaphthat6n€

2.Chh'roph€nol

4chlorophenyl phenyt ethe.Chrysene

Dlbsnzo (a,h) anrhrene

Dib€nzohrran

I JOlchhrob€nz€neI ,3OichbroberEene| .4-Didrlorobenzene3,3lDichlorobenzbine

2,4-Dkhlomphenol

Diethyl phthatate

Dlmethyl phth3ble

2,4-Dimethylpfi6nol

Di-n-bu!y' phhatat€

40305270641042702470347028203E502840445n2980

pS/kS dry

!g/kg dry

vsftg drypg/kg dry

Idkg dryydks d.y!g/kS drypg/kg dryldkg dry!g/kg drypdkS dry

4700941094tO47004700470047ffi4700470047m4700

40n4030-13030-13040-r4010-14030-13015-11030-13015-110u-t301Ul10

233

233233

BRL

8RL

BRL

BRL

BRL

1 5

1 1

1 7

5

3030303030

86

56

68

91

6 1

74m82609563

BRL

ARL

8RL

BRL

BRL

BRL

BRL

BRL

ARL

8RL

BRL

BRL

BRL

BRL

aRf

ARL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

us/KsUgJKg

!s/ksp9KSpg/(g

!gKsug/KgvgKsug/KgvgRgpgKsps/ks

Ljg(9

ugKgugKst g/Kg

!g/KgudksUEK9rjdkspslks

!g/KSut/KgpgKg

trg/xg!9xsgEr(9

lrdkspdks

fs/r(gl.r9/Kg!gKgugKgps/Ks

!g/r(9ugKspdkspsr(g

330330330303303303303303303303303303303303303303303303303303303303303303303303303303fi)3:}0330330330330330330330330

Thir labotuo,! r.potl it not ,otid xttrhaal an aalhorizpd sigaatarc on the caeu plage .'Reprtabl€ Derecrioo Limir BRL = Betow Reporriog Limir Pase 137 of 152

Page 521: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semlvolatile Orgaric Compounds by cCNIS - Quality Contlol

Analyiqs) Result Fl"S UnitsSource %REC

Result %REC Limits

Spike

Irvel

RPDLimit

Betch 7031282. SW846 35508

B|ank (7O31282€LKtt

P€pargd 22-lrar.07 Anavzed: z5-Mar-O74,6{)inibo-2fl etnyiphenol2.4Ohtropheool2,4-Dinibotolu€n€2.6-DinitrotolueneOa-n-oclyl ph[\abb

FluorgneHexaEfilorob€flzene

H€xachlorohJiadiene

Hgracnrorocydop€nbdiene

Hexachloro€lhan€

Indeno (1,2,3d) pyrene

1 {Iotryhaphthel€ne

2{ilelhyhaphlhalene

z-[{elhylphenol

3,+Me$rylphonol

Naphthalene

2+lfiroaniline

$Niboenflin€

4-l,,litoanihe

Nilrob€naene

2{,{ifophenol

4-tlilrophenol

N-Nibosodim6hylamhe

N-Nfi rosadi-nf ropylefi ine

N-Nibosodiph€nylamin€

Phenol

1,2,+Trichlorob€nzen€

2,4,FTdchbmph€nol

2,4.&Trichlorophend

S u 'rogata : 2- F I uotobip he nylS/uLircgale: 2-HuotophanotSufiWate: Nihobenzene45Sunoga/€] metp145Sunc€at€j Teryhenyt4l4S u nogale : 2, I,ETd Mo ipph a n ol

LCS O03'|242€Sll

Pr€par€d: 22-Mar-07 AnalFed: 2$tl€r{7

Ac€mphthene

Ac€naphthylene

Ardllne

Azobenzene/Dlph€nyldiazin€

Benldlne

B€nzo (a) anthracene

E€nzo (a) PyaeneB€nzo (b) nuolantr€rle

8RrARLBRL8RLBRL

BRL8RLBRLBRLBRLBRLBRI8RL8RLBRLBRLBRLBRLBRLBRLBRLaRt-8RL8RLARLBRLBRLBRLBRLBRL8RLBRLBRLBRtxM)71907890723098307591)

59205260B,RL63r053905490BRL430058504470

3:t0330330t30330330303303]03303,0330330330330330330303:]0

132033033013m3303303i'033030330330:l:]03:n330330

!dftsudkg|lgxs

PEK9

Itdkopsks

rgkgugl(sFdkS!dls!gl(s!gr€llgKg

udr€p€/t!9

pe/kg

FSikS

ugltsFgr(sudkgpdks

!dks|lgts|lgn(S!s4!srdksFdkstdkgps/ks

tldkgudkspdkspdks

udtsudks|ldks|lsftg!dkspsrkspdkst g/kg

pc,rsudks

m? ldkg|Jdkssdks!sftspdksggn€psftspelkg

30-13015-110wl3nt5-fi0m-tfr1EltO

{0-1fi)40-'t30{o-1304{} 1304G130,rG130

0-'t304o-r 3040-r304$ 130

330330330330330lxl0330330

frr0

13gn13W)13fi013fr0t&rot33N

66706€706G70

6670

66706670

5459547457

95

81

82

8079

6488

fhjj lahalorf r.pod b Ao, vaIU withont ., authodd stgaota'" orr thz covcr pge.

+ R@rtable D.t€dion Limi. BRI = Bdow Rcpoftine Limit Fag€ 138 of 152

Page 522: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolstile Organic Compounds by GCMS - Quatity Conarol

Analytd$) Resutt Ftaq UnitsSpike

Level Limi(sResult %REC

Brtch 7031242 -,SW846 J5fl)B

LCS r7clr282.BS1l

Pr€pated: 22-Mar{7 Analyzed: 25-MarO7

Benzo (g,h.i)p€ryI€ne

Be.uo (k) ffuoranthene

Benzoic add

Beoryl elcohol

Bis(2{hloro€thoxy)methane

Bis(2<hloroethyl)enher

Bis(2-cfi lo.oisopropylFlher

Bh(z-et'rylhexy)phthelate

4€tomophenyl phenyl eher

Bulyl benzyl phthalate

C€rbazde

4€hlo.e3{ethylphenol

44hloroaritine

24hloron+hlhalefle

2€ltoroph€noj

44hloroph€nyl ph€ny ether

Chrysene

Oibenzo (a,h) anttrracene

Dibenzoturin

1 2Oichlorobenzene1,3oid?b.obenzene

1 ,4-Othlofobeflzene

3,3 Oichbrobenzdine

2,4Oichlorophenol

Diethyl phlhalate

Ditrr€thyl phthalate

2,a€me(rylplrcnol

Di-n-butyl phthalale

4,6-{)iniho-2fl ethylphenol

2,4$inltophenol

2,4-Din botoluene

2,GDinitroioluen€

Oi+octyl phthal€te

Fluoranthsne

Hexaat$orobenzene

He)(d{ombutiadiene

Herachlorocyclopentadi€ne

Hexacirloroelhane

lndeno (1,?,3{d) pyren€

f -i,lethylnaphthalene

lsophorff\e

2-MelhylnapHh€lene

2{ilethy'pfEnol

3,:Aibrhylpr€nol

flEphthalene

2+{llrodniline

3-llilmaniline

4J,litroaniline

Nitrobenzene

2-ilitroph6nol

4{ifoph€hol

4660730038901380339054103730563055905550549050302820549041206500633040906030713032107070571043r051605020393055103690564051905710625C5790570068107410267063304090613055504410334045505810512028906010360040505050

330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330

33033033033033033033033033033033013203301101320

6670

6670

6670

6670

6670

6670

6670

6€70

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

ffi70

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

!g/Kg

!gKs

!s/kgoc2 !g/kg

!g/Kg

tis,Ks

!s/Kg

!s/kspE(9

!dkslig/Kspsr(s

tigr(s!g/kspgr(s

!g/tsugKslis/Ks!dks!s/KswKs!s/Kslrg/Kg!9/K9vg/kgrc/kswRg!9/KSt/9/Kg!g/ksugKsirs/Ks!s/ks!g/|(gpsiks

!dksug/ksudkspgr(sp(/r(spgxg

lis/Ksw(sfg/Kg

w/I€

|ls/K9

utl/KsUI/Kg

!(vKgp9/Kg

ps/tspg/r€

70 40-130

109 40-130

58 0-130

21 40-130

51 40-130

87 44-130

56 40-'130

64 40.130

84 40-130

83 40-130

82 40-130

75 40-130

42 40-130

62 40-130

62 40-130

97 40-130

95 40-130

61 4G130

90 4G.130

107 40130

4a 40-130

106 4G130

86 40-130

65 4G130

77 40-130

75 4G.130

59 40130

83 40-130

55 40-130

85 40-130

78 40.130

86 40,130

94 40-1

87 40-130

85 40-130

102 40-130

l r l 40-130

40 40.130

95 40-130

61 40-130

92 40-14r)

83 40-130

72 4O-13r)

50 40-130

68 40-130

87 40-130

77 40-130

43 40.130

90 ,|(1130

54 40-130

61 40.130

76 4G130

Thb labodory Epor, is not volitt tritho4 tn a@hoized signatare on tlE cover pzge

* Repodable Detection Limit BRL = Below Reporting Limit Page 139 of 152

Page 523: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compoun& by GCMS - Qoslity Cotrarol

Andyte(s) Resutt Ftas Unirr *RDLSpikelrvel

RPD

Limit

Source '/.REC

R€sult %REc Limi6

Brtch ?03 12t2 - Sw846 35508

LCS t7cll2€2€St I

PreDared: z+lsr{7 Anavlee 2s-Mar{7

N+lilro€odinFryamine

N-Nittosodi-n+ropylsmine

N.Nitrosod'pttentamine

Penta€$brophenol

Pyddine

1 2,+Trichlorobenzsn€

2,4,5-TrichlompherDl

2,4,&Trid orophoml

S u trogale : 2 +hn otE)h e ny'S utrogdle : 2+ fu o Eph en o ISu nogate : I'litroben nne4 5Sutr9gate: PheNl4SSunogatu: ferphonyld4Suftogale : 2, 4, 6 -f rib tu n o ph e n ol

Dupllcats oo3l282oUP1l

52503{5060903690337044tO61706't90641057303250696045e,393046706670628t)

Source: SA5945il-10

pdkg

!gkspsfts

l4^9Fg/kgpdks

Ltgt€t dl€ru/kovs/tspcftgpgkqttgksrcftspdk9tts1l(.spdkg

!dkgugl(srdksps/ks

ugkst dksTSAgpdks

!gks|ldksPs*s!grxgFS&Stdkspdks

|rsftgt€iks!sftspgks

!dtsrgkslrs/l€!dxgpdks

udks|ldkslryksTgKS

usrrcFdlSpdksp91€pdt€pgrs

6670667066706670667066706670667066706670667066706670667066706670

40.1304G1304$.13040-13t)4$.13040-1304G13{4Gr3040-t3040-r3040-130&tNt5tt0#14)15-110fr-ln15-110

79

gl

606793{xl9686491046959701(nM

3303303i]0330330330330330330330:}:10

Preparodt 22-fvlsr47 AnalFed: 2'Mar-07

Atrazine

Azoti€nzene/Diphenyldiazin€

B€nidin€

B6n2o (a) antlxacen€

B€nzo (a) pyren€

B€nzo (b) lluoranf|eneAenzo (g,h,i) p€rylene

Aenzo (k) ftDranthene

Benzoic 6cld

B€nzy' alcohol

Elis(2<hlorEtrcry)olethane

Ais(2drloro€tly')€tter

Bis(2d oroisoFopy')et|er

Ais(24tny$'6xyl)phfi alate,Sronrcph€rryl ph€fl yl erh6rButyl benzyl phtfrabte

Ca|bazole

4-Chloro-lm€t rylphenolrrchbmarilin€

24hhrcnaf*rBBbn€

2{hloropheml

44hlor@heny' phe.M eth€rChrys€ne

Drbenzo (a,h) anthraceneDlbenzofrrran

1 ,z-Di{$lorcbenzone

l.3oiJrbrob€nzene

I ,4oichlorob€nzeoe3,3'Oicrrlorob€nzldine

2,4oi('|loroph€nol

SRL

BRL

ARL

ARL

BRf

BRL

BRL

BRL

aR[

ARL

SRLgRL

BRL

BRL

8RL

BR|-

aRl

BRL

BRT

BRI-

BRL

BRL

SRL

BRL

SRL

BRL

BRI.

SRL

BRL

BRL

BRL

BRL

BRL

BRL

639

63S

639

63S

639

639

639

63S

639

639

639

639

639

639

63S

63S

639

639

639

639

639

639

639

63S

639

{r,9

63S639639639

BRL

8RL

SRL

BRf

BRL

ARL

ARL

BRI.

BRL

BRL

BRL

8RL

BRL

SRL

BRL

BRL

ARL

BRL

BRI

8RL

BRL

ARL

ORL

BRL

BRL

BRL

SRL

BRL

BR(

8RL

ARL

SRL

ARL

BRL

5050

50505050505t)5050505050505050

50

5050505050v)50

50

5050

50

Thb ,.bo.otarl' rzped ls aoa y.li.t at host on a horhd signer!rc or, ahe cover page.

r Repdtflble Dete{tion Lirnit BRI- = Betow Reporting Limit Page l40of 152

Page 524: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolati le Organic Compounds by cCMS - Quality Control

Source

Brrch 7031282 - SW84515508

Duolicate lm31282OUPlt SourEel 5A59464-10

Pr€pared: 22-[,f aF07 Analyzed. 25-Mat47

Oiethyl phtrlalate

Dimethyl phthalate

2,4-DirYEthylphenol

Oi-n-butyl phthalale

4,6-{)inibo-2nethylphenot

2,4.oi.|it ophenol

2,4-Dinilrctoluene

2,&Oinitrololuene

Oi{-octyl phdlalate

Hex&hlorobePene

Hsx{-hhobutadiene

Hexachlorocyclop€nhdi€ne

Indeno (1,2,3-cd) pyrene

1-{\rethyhaphlhalene

z+vlethylnaphthalene

2+,tethylphenol

3,+Methylphenol

Naphlhal€ne

2-l'lilro€niline

3-l.litroanilne

4-llitoaniline

Nitob€nzene

2+litophenol

4.f'libophenol

N-Nikosodimethyiamin€

N+liLosodi-n-propylamine

N-Nilrosodiph€nylamine

Phenanlhene

Pyddine

1 2,+Tichlorobenzene2,4,$Trichlorophenol

2,4,6-Tdchlo.ophenol

Su trog Ete : 2-F I uoro h i ph e n yl8u rogate : 2-F | @roph e rc ISuttogale : NifiDben za ne-d 5Sufiogals: Phercl4sSumogale: Teryhenyl4l4S utogate : 2, 4,&Tn bo no p h en ot

BRL

BRL

BRL

BRL

ARL

BRL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

8RL

BRL

BRL

8RL

BRL

8RL

8RL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

s310t03043203850574n3270

PEKg

l.rglKs

tg/Kg

!s/Ksrdkspgr(gpdks!E|<Spdks

pdks

!9Kgpgrls

pg/i(l

ps,K9

!gitqpgxs

uEk9

t gKg

pgxs

!9K9

!g/Kg

us/Ks!dksLr(yK9

|lg/Kg

us/Kspgfts

t gKops/ks

!s/kgps/ks

ugrspgts

l'|dksudksp(y(gpdrs!s/ks!s/kg!dks!9Kg!g/KgugK9ugKg!9/Kg

63S

639

639

633

639

639

639

639

639

639

639

639

639

639

639

639

639

63S

639

439

639

639

639

639

2560

639

639

2560

639

639

639

639

639

639

639

639

63S

639

639

BRL

BRL

ARL

BRL

ARL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

ARL

BRL

ARL

ERL

8RL

8RL

BRL

BRL

BRL

BRL

505050505050505050505050505050505050505050505050505050505050505050505050505050

129001290012fi0129001290012900

34-1m15-11030-13015-1103o-13015-110

3330

25

This lobo.slory Epo is not velid *llhout ar, caahofiazd signaaure oa the clrver page

* R€portable D€t€.tion Limit BRL = Below Repding Limir Page l4l of 152

Page 525: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Totrl Metals by EPA 6fi)0/7000 Series Methods - Qua[ty Cotrtrol

Anab,l{s) R€suh FIag RPDUnits IRDLSpike

L€vel

Sourc€

Re3ull %REC%p.EcLimits

RPD

Limit

Brach 703 1306 - EPA2{XySW70{0 Serica

B|8nk O031306-ALKll

P.eparcd: 23diaF07 AnalFed: 26{,tar{7

t uolicels (7031305-DUPI) Sourca: SAlsgLil{z

0-604

1_00

Sourc.: 3A5946440

BRI

Sou.ce: 3A5046+10

mSlkS rvel

OR5 mdkg dry

mg'kS dry

|rE]fg wel

89 75-125

8a 65.S132.6

8Rt

0.350

0.463

1 . 1 3

0.0292

o.033:]

0.0300

0.107

0.190

Prep€red: 23-lrar-07 Analyzed: 2&I|,tar{7

20370_0345

lratlx Solke ft03l106{31) Souicei SA5946a4

Prepored: 23-[,tar-07 AnalFed: 26-Mar-07

Mercury

Rsf..€nc. rTqll306-SRHi IPrepared: Z3-l ar{7 Anal]rred: 26-irar47

Brlch 70ll3rl - EPA200/SW70m Eeri€s

glank 17031111€LKII

Pr€pared & Analfz€d: mjvl{{)T

Duollc.t r03l3l1{ruPPrepa€d & Analyzed: m-Ma|{7

Marnx Sdk. r0313ll.ilsll

Prepared & Analyzed 2AMar-O7

Renaftnc. O031311€Rirll

Prepared & AndFed: 26-Mar-07

Bstch ?03 1315 - SW846 300sA

abnk l703r 3t s€LKt )

BRL ndks o_0292

fi€n(g

rng/kg

BRL 20

0.4440.4700.,tEso.4720.5230.4350.496

0.449o.442

mc4nE/lmg/ntsnmgilftsnmgr

r€nms,l

0.01500.00750.00250.00500.00,r00.00500.0050

o.00750,01500.m50o.00400.00s00.00500.0025

0.00750.0150

0.4t4

0,5000.5000.5000.5000.sfi)0,5000.500

0.5000.50()

SRL0,029E

0.0300

a5 71125

1't 1 65 9-132.6

P.dpar€d: 23-lrariT Analyzed 24+ii.at47SeleniumLeadCadmiumChromium

BsriumSilver

LCS fim€i5€St)

Prepared: 23{itd{7 An€lyzei 2+Mat 47LetdSekfliumChromium

BaaiumSilv€rCdmium

LCS Osp ftml3l$ASDIl

Prep€redr 23-Mar-07 Analyzed: 24-lrar{7LeadSe[,tntum

124 |rElfts

BRL msn

SRL mgL/l

BRI mgl

8RL mgl

BRL mdt

BRI .ng/l

BRL mSrI

s7 a5-11594 8911597 8911594 85115t05 8s11587 85-115100 E$115

s8 8$.115sG 85-1t5

mm

Ihb lzbororory .qort ls not valid w hru an at $orlzz.t signatar. od the cover INg... Report&ble Det€clion Limit BRL = Below Reporting Limir P.ge 142 ot lS2

Page 526: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total M€tNls by EPA 6000i?0{0 Series Methods - Qualit} Control

SpikeL€v€l

%RECLimits

RPDLimit

Sourcc

Result %RECAnab4{t RPD

Brtch 7031315 - SW846 10054

LCS Duo O031115€SDl)

Prepared: Z3-l\r€d7 Anal:Fed: 24-Mar01

Chaomium

SilYer

Barium

Cadmium

Pr€psred: 23-[{ar{7 Analyzet 21-Ma(O7

Lead

Sel€nium

Silv€r

Earium

Cadmium

Chromiuft

Prepa.edi 23-irar-O7 Analyzed: 24-Ma(47

Leed

Solsnium

Cadmitlln

Situ€r

Barium

Chroini{rfh

Selenium

ChromlumSilv€rC€dmiumgadum

Post so[(g f7(x]t 31 s+st I

0.4910.4390.4900.5830.515

ARL

ARL

BRL

0.0060

0 068a

ARL

ARL

0..{48

0.440

0.497

0.440

o.572

0.446

0.490

mg/l

mg/l

mg/I

QC3 mg/l

mgn

0.00500.00500.00400.00500.0025

0.00750.01500.00500.00400.00500.00250.0050

0.00750.01500.00250.00500.00500.00100.0050

0.0'1500.00750.00500 00500 00250_00500.0040

0.00750.01500.oo500.00400.00500.00500.0025

0.5000_5000-5000,5000.500

98 85t15 I

88 E5-115 0.9

98 85-115 4

111 85-115 11

103 85-1 15 3

6

0.4

75-125

96 75-125

99 7s-125

86 75-125

104 75-125

96 75-125

98 75125

96 75-125 0.2

96 75,125 0.8

s8 7t125 0.2

a6 75-125 0.5

99 75-125 0.4

103 75-125 0.7

11125 0

2020m2020

Duollcato lm3l3l5-DUPll Source: 5459424.01

mg4

msrmsrmg/rmg/lmgnms/l

mgnmsnms/rmg/l

msl

msfl

mgn

mg/l

ng,'l

msl

msn

msrms,4mg

mEl

nEI

r'gnfi1gI

rng/l

rngn

rngn

0.5000.5000.5000 5000 5000_5000_500

0.5000-5000.5000.5000.5000.5000.500

0.5000.50uo 5000.5000_5000.5000-500

0.00230.0otr0.0M60 00650.0892BRLBRL

0.0064ARL

0.00r60.0076o 05220 0M0ARL

BRL0 0064BRL

0.00760.00160.05220.00+0

m202020202020

t{arfi x Splk. n03r315.MSt I Source: SA5930O{I5

ll.tix gEike Duo |1031315{SO1) Sourc.: SA5{ty)0{5

Prepared: 23-t\,lar-07 Analyzed: 2+MaF07

0 481

0.4€4

0.489

0-438

0.499

0.568

0_486

Source: SA59300.O5

2020m20202020

Pr€pErcd: 23-Mar-07 Analyzed: 24{ra.-07

Lead

S6lenium

Baiium

Silv€r

Chromism

Cadmium

0.0064 102 80.120BRL 116 8G120

o.o522 111 N-1200 0040 107 80.1200.0076 88 80-120BRL 105 80-120

0.0016 108 80.120

0.5140.542o.6480.5380.4460.5240 542

Thh labodory Epnd is nor |slin w hod an aurtodzed signzlare on the .oee, page.

'R€port ble Detection Limit BRL= Below Repodng Limit Page l4l of 152

Page 527: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total M€trls by EPA 2fi) Series Methods - Quslity Cotrtrol

A""lyt.{0 Result Flag Unils .RDLSo rce %REC

Result o/oR-EC Linits

Spikekvel RPD

RPD

Limit

B{tch 1}31263 - f,PA 200 Ser{et

Bl.nk rT0ll2dtALKllPrepared & Analyled: 2AMar-07SsleniumCadnium

ChroarturhBarlJmSilv€rL€ad

Duotlcat {70312GHruP11Prepared & An€lyzed: 26-Mar-07Sel€nium

AariumCedmiumSituerChromium

Malrix Splk6 fl031263{ilsl IPrepared & AnalF€d: 26-Mad7Sel€niumC€dmlum

BdiumLeadClrromiumSll'rer

t{atlx Solk 4031269{52)PrEpared & Anal)/"2sd: 2GMar{7Sd€niumBariumC€dmiumSilverChmmium

Lead

Po3r S.tro ?03126+PSl)Prepared & Anelfzsd: 26-rrar-07S€l€r umBaaiumCedfltiumSlr€{Ctrro|nfun

Reb.t||c. O03126&,sRt{l)Prepar€d & AnBlyzod: t8+tlar{7S€l€nlun

gartum

ChromiumL€6d

Cadrdum

BRLBRLARLBRLBRLBRLaRl

SourE : S450464-lE

BRL0.stx10.2

0.5€8BRL1.S84.75

Sosrc€: SA50,l€+10

mdxgntgl(grYtSn(gmg/kgrrEJI9mcl(grgls

rngIq,nigrkgmsasmS/k9dr€n(gmSlkSmsas

lr€/kS

$tgrkg

m€rkgnlg/kgn€ftsmgt(9rEItS

mSI(S

ngrkg

firS*0

mgfts

ntSftS

mg/kg

ntg*g

msasmgasm94(gfirg^SmSrkS

1-1801,161.400.4920.4s20.9850_734

r.401.,t00.{670.2330.934o4670.700

1.40o.2341.400.4680.701o-4640-935

1.430.4760.2380.953o.1761.430.715

1.400.468o.2u0.935

0.468.t_40

1.50

1.50

0.500

0-500

0.750

o.250

BRL0,502r0.6

0.626BRL1.S75.08

0.s47o.5060_sso13.23.78

ARL

0_55346.8t . 9 lSRL9_311.242r0

o.u713.2

0.506BRL

0.590

o.465

o.57

35

3535

a5

10f

97-S

100

t 1 9

97.4

t02

1(b

Sourcs: 5A59569{i

1 t s

r60

t 1 0

1 1 0

1 1 8' 1 1 1

386

Sourr.: SA59,164-'10

nS'l(]g

mqx9mS/k9rEn(omgftsmS/kS

oM4X frE^o

100 7o-1?o95 7G13091 7G13t)92 70-13091 7G13092 70-13o148 70-130

93 81115!0 85-ll585 8t1t592 85-11565 8t1158ll 8$r 15

100 77.+12268S 80.&r',19.4N 82.7-117.305 78,$.120.566 81.&118.193 82,1-117.9

117

117

117

117

117

117

1 1 9

1 r 9

l t s

1 1 9

1' t9

1 1 S

1 1 9

117

11f

117

117

117

117

N.2

46.0

41

50.7

46.0

32.6

70-r 3070-13070-1307G13070-13)70-13070130

91E3

so80u90

't to11899.8108't03

r03

80.441.1zx)43.339.630-3

Thb hbo.obry tqor, is nat wlil flirha4 an acthori?d sk u!u. on ahe coEr pq. -

+ Reportibl. Der€ction Limit BRL = B€low fupoding Limit Page 1,14 of 152

Page 528: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Meaals by EPA 200 Series Methods - euality Cootrol

Spike Sourc€

B{tch 7031263 - EPA 200 Series

Rei.r.nce 1703l263-sRMl I

Pteparod & Analyzed: 26-Mar-07

Silver

Brtct 7frllJ05 - EPA 200 S€ri€s

gl.nk 170:11305-aLK1l

Preparedi 23{vlar{7 Anatyzed: 24-MaF07

42_240.2 m9/kg 95 66.3-133.6

Prepared: 23-l\,{ad7 Anatyzed. 24-Mar-07

SiverSeleniumLea0

CadmiumChrofti(nnBanum

Dqellcaas t7031305nUP1)

S€l€nium

Silver

L€€d

Cadmium

Chrcmium

Bariuh

l|.dr Spik 17031305{51)

Sdenium

Sllve.

Chromi(m

Cadmium

Esrium

ilatir Soik€ (703130tMS2t

Sel€t um

Silv€r

Lead

Cadmium

Cttromium

Badum

Fosl $plke fl031 305-PS1 |

BRL

BRL

8RL

BRL

BRL

BRL

ARL

Sou.c€: sA59442.{2

128

1 1 8

138

446.t4E

1 3 1

197

Sourc€: SA5950ru1

125

1 1 1

120

1 1 7

124

122

153

Sourc€: SA5946d-02

mg/kg wel

mg/kg wel

mgeg w€r

mgukg wet

ftE kg w€t

mg/kg 'fl€t

0.936

1 4 0

0 936'1.40

o.234

0.468

0.468

1.54

1.05

1.58

1_05

0.263

0.526

0.526

1.62

1.OE

1.62

1_08

0.539

0 269

0.539

1_48

0_989

0-742

o_247

0.495

1.48

0.495

1 _ t 2

1.69

0.562

1.69

0.281

1 . 1 2

0.562

135'135

135

135

135

135

135

124

124

124

124

124

124

121

141

141

141

141

141

141

141

BRL

1 . 3 7

13.1

28f

1 1 8

21.6

266

BRL

SRL

1 4 4

I

25.O

1 6 8

53.6

BRL

8RL

6.37

o o5r29 2 8

4.69

28-8

aRL ftg/kg dry0.856 J,OR4 mg/kg dry6-74 QR1 mg,fkg dry160 aRs nrg/kg dry

0.510 QRi mdks dry

18,5 mg/kg dry106 OR5 nsrkg dry

Source: 3A59116+02

46

64

57

79

1 5

86

35353535353535

P€par€d: 23-lrsr{7 Anallrzed: 24-Mar{7

Prepared: 23-l\iEr47 Anatvzed. 24-Mat47

mg/XS drymgl(g drymg/kg dry

o,v8 ng/kg drymg/kg drymS/kg dryng/kg dry

95 70{3087 70-13092 70-130132 70-13091 70-13096 70-130106 70-130

101 70-13090 70-13092 70-1A)s4 70-13093 70-r 3095 70-130100 70-130

Pre9ared: 23-llar-07 Analyzed:. 24-Mat47Sit/€rS€lertumCtuomium

CadmlumL€edBaaium

R€fe.ones {70t1305-5RilllPr€par€d: 23-fr.tar{7 Anslfzed: 24-Mar47

123

145

154

146

136

422

199

mgftg drymg./kg dryr(]g,l,(g drymgftg drymgftg drymg/kg drymgl(g dry

rng/kg dryngRS drymgl(g drynEftg drymg/kg drymSftg drymg/kg dry

aRL 87 8$115

BRL r03 85115

25.0 91 85-115

14_4 93 85-115

1.64 95 65-115

26A 10S 85-115

53.6 103 65-115

This lahorator, rcport ls nol oalu fiithoat zn zurtoi@d signztare on lha.wet page.

i Reportable Detection Limit BRL = Below Reporting Lrmit Page 145 of l \2

Page 529: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Totrl Mearls by EPA 200 Series Methods - Qtrality Cotrarol

Analyds) Result UnitsFlag Result %g.Fc Limirs RPD

B.tcb 703t305 - EPA 200 Serica

R€turence f703lm5.sRilllPrepared: 23-{\rar-O7 Analyzet 214ta(47SilverSeleniumL€ad

Chromium

Cadmlum

Barium

Bat h 7031316 - EPA200/SW7000 S€rie!

Bhnk {m3l3l6€LKt}

PrBpar€d E Anelyted: 23-lvlar{7

LCS O03l3l6331l

Pr€pared & Aialfzed: 23-ilar47

Ouolicsie r0:1131&DUPI I

Prepared & Anayzed: 23-M€r-07

t{strlx Soiko OGll3lGHSll

Prepared & AnElfi€d: 23-l{ar-07

atrtx Solke Duo fl03l3lG*lS01l

Pr€pared & Anarfz€d: 2!Mar{}7

Llercury

Posl Solke ft03l316€5l I

Prugsrcd & A^alfzed: 23-M€r47

34.574.O34.339.0

26.Srgo

fiig (gwet 1.00

nEikgwel |.50

nEril(g w6l 0.750

dElkgwet 1-50

mgfigw€t 0-500

rig/kg w€t 0.250

mgftSe/st 0.5fi)

66 &133.6l7_+1?2.481.&1r8.180.8-119.478.9120.582,1-r17.9a2_7-117.3

11_2

78.3

44.9

44-S

49.5

31.8

216

0.00250

8S1t5

64

a5877684EA

0.00265

Sourc€: SASg,lS+17

8RL

Source 345945+19

o.00266

SourE€: SA59,16+19

0.00279

So{rc€: 5459464-19

8Rr-

0.00267

0-00005

0.00005

75-125

73-125

4t115

fngn 0.00020

ITE/I 0.00020 o.00250

flr4,4 0.00020

rE/l 0.00020 o.@250 0.00005

0.00020 0.0025nm9/l 1 1 0

lr'sl o_0m20

Thb loborstory rqort h rral ecli.I tuElaat on otrtofiEd s,gntat on ttg @vd page.

'ReporEbl€ Detectioo Lini! BRL = B€low R€porting Limir PtgE ta6 of 152

Page 530: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TCLP Metals by EPA l3l | & 6000t000 S€ries Methods - Quatiay Conarot

Analyte(s) Result Ftog Units *RDLSource %REC

Resuk %REC Limits

Spike

Level

RPDLimitRPD

Bricr 70313?5 - SW8{6 30r0A

Blank n03132$ALK1)Plepar€d: 23-{rraF07 Analyzed. 24-Ma.47Selenium

ChromiumCadmiumSilv€rAarium

LCS 17031325€SPrep€|gd: 23+,,lar-07 Analyzed: 24-Ma'{ 7SeleniumL€ad

Sllver

Hmium

Cfuomium

Barium

l-CS Dup f'03132$Bsol)

Prepared: 23-{\,,lar-07 Anal)r2ed: 24-Mar-07

Lead

S€lenium

Sih€r

Cllfomium

CadiYumgadtj{n

BRL

BRL

BRL

BRL

BRL

ARL

8RL

1.33

1 . 1 3

1 . 1 3

1 . 3 1' | .25

1 . 2 1

1 . 2 1

1.08' | .27

1.07

1.20

1 r 5

1 . 2 5

1 . 1 4

0.0140BRL

0.0034BRLBRL8RL0.100

mg/l

rEnr!)9fl

m94

mg/l

mg/l

mg/l

mg/l

mgn

mg/l

nEx

mg/l

nEI

MEI

mg/l

mgn

nEn

mg/l

m9/l

mg/l

mgn

mgn

rhg/l

mg/l

mgn

rngn

mg/l

mg/l

r€nng,'l

mg/l

rng/l

ng/l

mq/l

ft9.i1

rng/l

rhgl

mgI

nE,4

rngn

0.01500_00750.0r500.00500 00250 01000.0050

0.01500.00750 01000 00250-01500-00500.0050

0.00750 01500.0't000 01500.00500.00250 0050

0_00750.01500.00250.01500.00500.01000.0050

0.00750.01500.01500 00500.01000 00250.0050

0.00750.01500_01500.00500.0r00

1_25

1 . 2 5

1 . 2 5

1 . 2 5

1 . 2 5

1 . 2 5

1.25

1 . 2 5

1 . 2 5

1 . 2 5

1 . 2 5

1 . 2 5

1 . 2 5

1 . 2 5

106 77.1-123

90 73.6-107

90 55 1-124

105 &3.4-111

100 75.+11S

97 N.7-110

97 86-117

86 73.G107'to2 77.1-123

a6 55.1-124

96 75.9-119

92 80.7-110

100 83.4-111

9 1 8 6 - 1 1 7

5

5

5

5

5

5

20202020202020

OuplicaL fi03l325nuPl I Sourc€: 345946+i6

f atrix Soik6 17031325.Ms11 SourEei SA5!146+15

Preparedi 23-Mar.07 tul€lyzei: 24-Marjt

Le€d

Sds um

Cadmium

Chrofiiufir

Sdver

B€rium

Prepared: 23.Mar-07 Analyzed' 24 -Mat 47

Selsnium

Chromiom

Sllver

C€dnium

furium

L€Ad

S€l€nium

Aasenlc

Chromium

Silv€r

t .tslr Solte Duo ft03l3z5{SDll Sourc€: 5A5946+15

Pr€pd€d: 23-Mar{7 Analyzed: 24 -Mat 47

1 . 1 2

1.27

1.20

1 . 1 6

1 . 1 0

1,25

1.25

L09

1.24

1 . 1 9

1 . 1 5

1.()9

1.25

1.25

125

1_25

1_25

1.25

1 2 5

1 . 2 5

1.25

1 . 2 5

1.25

r.25

0 0 1 3 5

BRL

0.0040

8RL

BRL

aRr0.105

o.02440.0063ARLBRLARL

o.00500.0761

4.02440.0063BRLBRLBRL

88 70.1109

101 78_8-120

96 81.4-114

94 767-115

88 59.6-115

100 a17-107

94 84 5-116

85 70_1-109

99 76.0.120

95 61.4,114

92 76.7-115

87 59.+115

32

0.83

0.9

2020202C20m20

2020202020

Thk hboratory repod it nor vdil withad on eurtoired signrtu,e od the covgr page .

' Reportable Detecrion Limit BRL = Belov ReI'odDg Limit Page 147 of 152

Page 531: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

TCLP Metals by EPA 131I & 5000/7m0 Scries Methods - Quality Control

Analyte(s) Result Flag Unr|l +R-DLSplke

L€v€l

Solllce

Result ./.RICo/.REC

Limils RPDRPDLimit

Bsrch 703r32s - SW846 3010A

tlatix Solk6 Ouo ?0313i15-t{Sol} Sou.ce: 5A!1016+15Pr€paredr 23-Md.07 Analyzed: 24-ltal{7

C€dmium

Barium0.0050 s7 It.7-1070.0761 92 84.5116

0.0063 102 79-5-122o.o241 88 75.5-102sRL S6 8'1.8-10SBRL 98 65.d-114BRr- 98 823-115

0.0050 100 81.9-t100.0761 96 M.7-fi7

122123

|r1S{

msn

flgn

mdl

ndl

nsnmsnn€,

rndl

0.002s0.m50

001500.0075o.0(500.01000.ot500.00250.0050

1-25125

1.251.251-251251.25|.251.25

2020

Posr SoH€ 47031325+St) SourE€: SAlll!l6a-15

Preparedl 2$Mar{7 Anatyzed: 24.tAet 47

Selenium

Leeo

Chromaum

Silver

Cadmium

Bsnum

Brrch ?03 1326 - EPA200/SW7000 Se.k's

Blank l?031326€LKl)

Prepared & Andyz€d: 23-Mar-07

LCS 17031326€S

Prepared & Aneiyzed: 23-Mar-O7

Dupllcate rtrutt3?6{ttPlI

Prepared I AnatFed: 23-Mar-07

matrlx Soik€ ?O3l32SllS1l

PreFred & fuiall.2ed: 23-Mar-07

[atrix Splke Duo ftoll326-f,SDll Source: SA.l9a6a-t5

nEI 0_00uo

nEn

mdl

msrl

o.0oor'o 0.00250

o.o{txo

0.00(xo 0.002so BRL t09

rftdl 0.0m40 0 00250 8RL 104

nE,l' 0.00(x0 o00250 BRL 112

0.m257

Source: SAsg,[a+lC

BRL

Sosrc€: SA5g4S{-15

r281 . 1 3

1.19

1_23

1 2 2

126

1.27

gRL

o.00273

r03 63.$124

Prepar€d & Analyzed: 23-Mar47

PGt Soike l-fl):ll 326PSl I

PreFred & Anall.zed: 23-Mar47

0.00265

Sou.c.: S4!19{6+15

53.'t-126

53-1-126

85115

m

o.oo27s

fhh ltb.otory rcport Is trot edld *irtonr tn adhoriltl sigt aitE oE th. coeq We.+ Repo.table De{.dion Lidit BRL = Below R€portirg Limit P.ge 148 of I 52

Page 532: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Metals by EPA l!12 & 600011000 Se €s Methods - Quality CoDtro.

Spike

Lev€l

%REC

Limits

RPDLimit

SourceResult %RECResul( Flas Units RTD

Bstch ?031123 - SW846 3010A

Bhnk fl03t323{LKtlPrepar€d: 22-Mar{7 Analyzed: 23-Mar-O?SelenlumLeadCado umSilver

CiromiumBadum

LCS f70313zlast I

LOa6

SelsriumCdmiumChtomlum

Situ€lgarlum

LCS Oup ft031313-BSOI )Prepared 22-tr,f ar-07 Analyzed 234,iar0zSeleniumLead

ChromiumCa(mfumSdv€rBarium

ARL

BRL

BRL

BRL

sRt-BRL

BRL

1.20' l -14

' t .15

o_771

1.25

1_09

1 1 6

1.08

1 . 1 4

1 2 l

0.900

1 _ 1 8

ntsnmqnmg/|mgnm9/lmsrmgn

mg/lmsflmg/1mg/tmsflmsnmg/l

ng/lmg/rmgrnE/lnE/llng/lmg,l

mgn

mg/l

mgr

mg/l

rngn

mgrmsil

mg,1

lngr

mg/l

mg/l

mgn

mg/l

mg/l

msrmg/lmgnmgnmgn

0_01500.00750_00250.01000.01500.00500.0050

o.00750.01500.00250 00500.01500.01000 0050

0.01500.00750.01500.00500.00250.01000.0050

0.0r500.00750_01000.01500.00500_00250.0050

0.00750_01500.00250.01000.00500.01500.0050

0.00750.01500.00500.01500.0100

1.25

1 . 2 5

1.25'| 25

1 . 2 5

1.25

1 2 5

1 . 2 5

1.25

1.25

1.25

1 . 2 5

1.25

1.25

96

91

9t)

92

91

62

100

87

93

E6

9 1

s77294

82.3-108

79.106

87.9-110

76.2-114

77.4-109

55 5-115

8 5 . 1 - 1 1 9

79-108 4

82.3-108 3

f7_4-109 5

76.2,118 0 9

87_S-110 2

55.5,115 15

8 5 . 1 - 1 r 9 6

81.&10580-4-10586.+10863_6-10981 5 -11179.2-10688.9-114

81.0-105 280,+105 281 .5 -111 279.2.106 263_6-109 0.8

OuCicaie 1703l323OUPl) Sourc€: SA59,l6a-02

20202020202020

20202020202020

flabir Sprko ft00t323-tI3t] Solrce: SA59,t6.l-o,

Prepared: 22-l,,f ar{7 Analyzed. 24 -MaFO7

Selenfum

Lead

Slver

Ghaomium

CEdr*um

Barium

Prepared: 22-ll,f a.-07 Analyzed: 23-Mat47

Lead

S€l€nium

cadmium

Silv€r

Chro|rfum

Bsrium

L€adS€l€niumChromiumArlenlcglwr

ARL

0.0512

BRL

BRL

0.0109

ARL

0.0168

1231 1 6127

0 9521.20r .16126

IaHr Solke DtE 4f031323-t{sD sourcsr sass.t6{41Prepar6d: 22-t ari7 Analyzed: 234nat47

1.21

1 . 1 4

1 . 1 6

1 . 1 4

0-9,14

1.25

1.25

125

1_25

1 . 2 5

1.25' | .25

BRL0.0507ARLARL

0 0105BRL

0_0170

o o21t8Rr

o.0004ARL

o.0122BRL

0.0120

0_0217ARL

o.0122ARLBRL

97

93

102

95

s3100

95

91

93

91

76

2020202020

Thit |tborotor! fqon is Eot vrtd h'ithou an t,tlho?ized signzlan on lhe cover page .

r Reportable Detectior Limit BRL = Below Reporting Limit Page 149 of I52

Page 533: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Metals by EPA f3f2 & 6000t000 Series Methods - Qmlity Conarol

An ytqt RPDResuh Flag UnitsSpike

trvel

So{rce

Result

RPDLimit./oREC Limits

B.tcl t03l32f - SWE45 3010A

litrdx Srlke Duo 17031323- SOt) Source: SA5!X6,!lllPreparcd: 2241er47 AndFedr 23-MarfiCadmiumBa um

m20

'100

98

Po.l Soike 170:rl 3:llPsl! Sourc6: Srt5g464{l

1.25

1.24

1 . 1 3

1.20

1 . 1 7

0.9m

124

1 1 3

1.23

msrmgn

m9/lfiEnmgnmsnnEntlEilmgn

0.00250 0050

0_01500.00750.00500.01000-00250.01500.00s0

1.251.25

1251251.251.251.251251.25

0.00010.0120

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0.oflxBRL

0.0120

66.+108

88.9114

77.7-108

80.3-108

78.1-ll4

61_7-107

86-9109

79.3-107

86.8-118

Prepared: 22-frar-07An€lyzed: 23-Mar.O7SeleniumLeadChromiumSikerCadmium

BEdum

B.hh 7fi11324 - EPA2|XySW7000 Se.ies

Ahnk rm3l324€LKl)Prepared: 22-llaF07 Analf!6d: 23-MaF07

909493t8sg90s7

8RL ng{ 0.000{0

nvn 0.00040 0.m250 109 86.&117

108

LCS r703t324-A5t)Prepared: 22-MaF07 Anal}.zed: 23-Mar{7Mercurt 0.00273

P@parcd: 22{-f€r{7 Analyzed: 23-Mat 47

Ouollr5t 17031324-DUPI ) So'rrc€: 5A5046.1-02

nrdl 0.00040 ARL

l|.tsix sotks fl03132+us1l SourE€: 5A50461.{ll

Prepared: 22-llar{7 Analyzed : 23 -lfiatrA7

ti4€rorry O_0/J272

Matrlx Soike Duo t?03l32il-llsoll Sourc€: SA59a64{t

Preparedi 22.1!lar4TAnsl].zed: 23-Mar{7

Mercury 0.00270

mg/l 0 00040 o.00250

General Cbemisary Parameaers - Qurlity Cotrtrol

76,1-111

76.t -111nE,ll 0.0@lO 0.00250 8RL o_7

Analyte(s) Reslllt

SourceResult

R.PDLi(rritFIac Units ./"wc Limits

B{tcb 7031317 - CeDeral Prep.rrtloD

Duolharel7oSlloTOUPl) Source:SA59,l5,l.OlPreptred & Anal}l.zed: 22-Mar-07% Sorids 89-1 % 87.7 2 m

Ihir lobontury Epoll ii ,,ot vzlid wirhoat an a$thoriaed ttF rzftln on thc @ru pge.

'Rcptrbble Det€ctioo Limit BRL = Below Reponing Limit Page l50of l52

Page 534: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Notes rnd Deflnitions

*TPH Calculated as

Coop Completed

FP Field Preserved

QCI Adalyte out ofacccprance fange.

QC2 Analyte out ofarceptance ratrge in QC spike but Do reportable corcentration present in sample.

QC3 The spike recovery is outside acceptable limits for the LCS. The batch was accepted bascd upon the MS and/or MSDmeeting the LCS limits cliteria.

QM4X The spike recovery was outside ofQC acceptance limits for the MS, MSD and/or PS due to anal]4e concenfiaLion a14times or gr€ater the spike concentration. The QC batch was acc€pted based on LCS and,/or LCSD recoveries wiihtn theacceptance limits.

QM8 The spike recovery exceeded the QC control Limits for the MS and./or MSD- The batch was accepted based uponacceptable PS and/or LCS recovery.

QRI Analyses arc not controlled on RPD values fiom sarnple concentrations less than l0 tim€s the reporting timit. QC batchaccepted based on LCS and/or LCSD QC r€sults.

QR2 The RPD result €f,ceeded the QC control limits; howevet, both petcent recoveries were acceptable. Sample .€sults for ihe

QC batch were accepted based on perceDt recovedes and completeness ofQC data.

QR4 ABalyses ate dot controlled on RPD values from sample conceltratioos less !ha$ thc reponing limit. QC batch acceptedbased on LCS and,/or LCSD QC results

QR5 RPD ou! ofacceptance rangc.

R03 The Reporting Limit for this amlyte has been raised to account for interference from coeluting organic compoundspaesent in the sample.

Elevatcd Reponing Limits dw io the presence ofbigh levels ofDoFtarget analytes.

The sunogate recovery for this sample cannot be accurately quantified due to interference ftom coeluting organiccompounds pr€scatt h the sample exract.

vexl Lab extracted

veto Field extracted

BRL Below Reporting Limit - Analyte NOT DETECTED at or above the reporting limit

dry Sample results reported oD a dry weight basis

NR Not Reported

RPD Relative Percent Difference

A plus sign (+) in the Method Reference columl indicarcs the method is not accredited by NELAC.

R05

s02

Thk lsbonlory rcporl k Eot volitl t ithou al authodzed signaturc on thz covet page.

' ReDortsble Deterlion Limit BRt = Below ReDortins Limit Page l5 l of 152

Page 535: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Interprctation of Total Petroleum Hvdrocr.bon Report

Petloleum ideatihcation is detetmined by cornpa.ing the CC frtrgeryrint obtained ftom the samgle with a libEry ofGC fingerprintsobtained from analyses ofvarious petrolgum products. Possible match categories are as follows:

Gasolide - inclLdes rcgular, udle{de4 premium, etc.Fuel Oil #? - includes home hearing oil, #2 tuel oil, and dieselFuel Oit #4 - itrcludes #4 fuel oilFuel Oil #6 - itrcludes #6 fuel oil and bunker "C', oilMotor Oil - itrcludes virgin atrd waste automobile oilLigoir - iocludes minerdl spirits, petroleum nE htha, vm&p naphthaAviation Fuel - includes keroseDe, Jet A and Jp-4Other Oil - includes lubricating atrd cuttitg oil, and silicon oil

At times, 6e uoidentified petroleum product is quaotified using a calibratioo that most closcly approxiEates Se distribution ofcompourds i.D tie sample. Wheo this occurs, the re$lt is qualifred as 'TpH (Calculated as).

Laboratorv Control SamDle (I-CS): A known matrix spiked with cohpouDd(s) r€prcs€otative of the targer aoalJ.tes, which is used todocument laboratory perfonnance-

Mahix DuDlicate: An intr4-laboratory split sample which is used to document the precision ofa method in a given sample matsix.

Matrix Soike: Ao aliquot ofa sarnple spiked with a known concentmtion of biget analyte(s). The spiking occurs prio. to safilpreprepa-.ation and aoalysis- A matrix spike is used to document r.he bias of a method in a givetr sample ltraEix.

Method Blaok: An anallte_free mabix to \r{tich all reagents are added in the same volumes or pmportions as used in mmploprocessin8 The method blank should be carried through the cotnplete sample pre!fiation and aoalytical procedure- The methodblank is us€d ro documeot contamination resulting from the anal)rtical process.

Method Detection Limit aMDLI: The minirBum concentralion ofa substance that calr be measued and reported witb 99oloconfid€nce that the analyte colc€otsation is grcat€r than zero and is determined ftom aoalysis ofa sample in a givetr mahix typ€cootaining th€ affilyte.

Reportabl€ Detection Limit (RDLI: Thc lo\€st codc€m.4tion that cao be reliably achieved wi$h sp€cified limib ofprecisioo arrdaccu.acy duriqg routine laboratory opemting conditions. For many analytes thc RDL aoallte conc€ntmtion is sel€cted as tho lowestDon-zero staodald h the calibration curve. While the RDL is approximately 5 to l0 tides the MDL, the RDL for each sample tak€6into account the sample volume/weight, extsact/digestate volume, cleanup procedures and, ifappticable. dry weigbt can€ction-Sample RDLs are highly matrix{ependenr.

Sunoeate: An orgaDic compound which is similar to the target alulyre(s) in chemicel compositiod and b€havior in the adalyticalprccess, but which is not Dormally found in etrvironmetrtal samples. These compounds are spiked into all blanks, staodards, andsatnples prior to analysis. Percent tecoveries arc calculatcd for each surroeate.

Validahd by;Hanibal C. Tayeb. Ph.D.Cluistopher Hall

This labo hrf ppo.l it ,tol valid l'lhoa aE aartodzd swnalara on rte cover psge

r RcptrrEble Det4€l-roE Limit BRL = B€low R+ding Limit Pw 152 ot 152

Page 536: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

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Page 537: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 538: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

r c > 9 R

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Page 539: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldeotificationFB.2sA595l7-14

Clieot Proiect 430t-88

MatdxBlank Water

Collection Date/Timel9-Mar47 00:00

Received2GMar.01

CAS No. Aulyte(s) Resall Fl"C A/''iJs *RDL Diluiatt Me od Retr. Preparcd Analfud Bdc, Anat$t

VolrdL OrgrEic Compoundr

Volatile Oroanic Comoounds bv SW8,l6 82608Prepared by metl|od SW846 5030 Water MS76-1+t 1,1,2-TrichldohifuoroetfEne (F/6oBRL67€+1 Aceton€ BRL107-l3n Ad'ylonitil€ BRL7143-2 Eenzene BRL10&8Ei grcqnq!6626ne 8RLr+57-S Itomochlorcm€thane BRL7+274 Bromodicftlorom€thane BRLE2+2 Bromofo.m BRL7rl{}9 Bronbdlethene BRL76€+3 2-Eubnone (MEK| BRLt0+5t4 n-Butylb€nzene BRL13t9&O sec-Butttlsnzene BRL98-06{ tert-Butytbenzene BRL75150 Carbofldisumde BRL8-2TS Ca.bon tefacfiloride 8RL1o&so-7 Ctdorohenzone BRL7E{X}{ Chlorcett|an€ BRf6166-3 Chlorobrm BRLu-47-3 Chlorom€tlEne BRL95-.19{ 2.Chlorototuen€ BRL1064+.4 +Chlorctoluen€ 8RL96-12-S l,2.Oibrom+3.chloropropane 8RL121-,1€r Dibromod{oad.tr€lfiene BRL106-93-{ l,2-DibfomoetEne(EDB) BRL74-95F3 Dibromorn€thane BRLs6-5o-r '1,2_Dichlorobenzene BRL541-73F1 l.SDichjorcb€.Eene BRL1064.6-7 l,+Dichlombenzene BRL71714 Oid r.odlfluddnehane (Freooi2) BRf7s-34-3 .1 , 1 Oichlorcethan€ BRI_107{6-2 l,2{Ichtoroot}|ane BRL75.3S4 1, I Oichlo.oeth€ne SRLl5$5s-2 cis-l,2-Did oroetheno BRLlscd'-s tans-'1,2-Oidtrlofoethene BRL7€-07-5 l,2.OichloroFopane BRLlrr2-284 l,3-DichloropttDano BRL5ea-2G7 2,2-Oichlorop.opan6 BRL5635q€ i,l-Didrlotoprcpen€ BRL100614iScjs-1,3-Dicl{omprope|le BRL1006t4{t?ns-1,3-Dichlo.oprEpene BRL100-41{ E{rytbenzene BRL87{s3 Hexecfitoroh,rtadief€ BRL5€1-7eG 2-Hexanc|re (irgK) BRL9€{2{ lso@pylbenzene BRLs{7{ +lsopropyltoluene BRL1634.014 M€h),i t6d-tut)4 ettrcr SRL1o&rGr 4.ireh''l-21o€rltanone(Ml8K) 6RL75-092 Methylene chtorid€ BRLgr.aH NaphtElene BRL103-6$i rFPropylb€Gene BRf

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SWa46 82608 224ar47 2+tar47 7031296 ek

This kbrslory .qod ls 6at wlid vithou att quthoi?ed signohlre oE ttE coyer pq..

' Reponable D€rection Limit BRL = Below Reporting Limia Prge 58 of 124

Page 540: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdeptificationeE-2sA595 r7-14

Client Proiect #301-88

MatrixBlank Water

Collection Date,rTimel9-Mar-07 00:00

Received20-Mar-O?

CASN0. Analytc(s) Rest/ll FloC Uni6 *RDL Dilution L[ethod Ref P,epared Anal)zed Batch Amlrsl

vohdle Org.nic Compound!

Volatils Orcanic Comoounds bv SW846 82608P.epared by rnethod SW846 5030 Waler MS

1549-4 Trichloroffuoromethane (Freon 1l) BRL

10G2-5 Sbrene63C201 1,|,1,2-Tetrachlorcethane79-3+5 1,t,2,2-Tetrachtoroethane127-19 Tebadloroethene1O8J+3 Toluene07{1{ 1,2,}Tddllorobenzene12S42-t 1,2,4-Tdchlorcbenzene7t€ffi '1, t , 1-Tddtloroehane79{0-5 1 ,I ,2-Tdcttloroethane79{14 Trichloroethene

96n84 1,2,3-Tridoropropane95435 1,2,4-rrimethylbenzene108{7{ l,3,gTrimelhytbenzene25.01-4 Viny' dtlorid€r$G2Gz m,p-Xylene95-475 o-xyleneto+se€ Tetrahtdrofu r'anqfFT Ethyl etlerS$1-o54 Tort-amylmedtylether037-9?-3 Ethyltert-butyleherro&?0-3 DiisopropyletfEr75-65-0 T€rt-Bulanol/butytatcohol12$91-1 1,+Dioxane

slnrogale rccot/€ries:160404 +B&molluorohenzenew37.66 Toluene4S1 roeoT 4 1,2-Oicliotoethane-d41ffi&5J7 Abrcmofluoromethane

Ertretrble Petroleum Hydrocrrbons

Exhactabb Total Petrpleum HvdrocafuonsPrepared by melfiod SW846 3510C€O0G€l-9 Gasoline68azciG2 FuelOil#20047e31-3 Fuel Oil #468553-{XX Fuel Oil #5[{BEoI]()Oo Motor OilJ00100000 AvjalirD Fuel

Unidenffied

Other OilTotal Peholeum Hydrocarbonsc$.C36 Aliphatic ttydmcarbons

$nwde rc./^,etus:i3€6-A?2 | -Chlorcoctadecarc

Sernlvol.dle Org.nlc CompouDdr by cC

Oroanochlodne Pesticides SW846 8081APrepared by rnethod SW846 351 0C

3o+{F2 Adrin3l+a{€ +BHC

SW846 82604 22-MarO7 22-MaGO7 7031296 ek8RLBRLBRL8RL8RLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

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This labotuloq ftporl ls noa vdid wilhaul an.ulhodzed sbnofirc on the cover poge

' Reponable Detection Limit BRL = Below Reporting Limit Pase 69 of 124

Page 541: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sah!,le Id€ntificationFB-2sA595l7-r4

Clieor Pmiecl#301-88

MatrixBlenk Water

Collection Date/Tim€I 9-Mar-,07 0O:O0

Received20-Mar-07

CAS No, AnabE(s) n"E 'RDL Dilution Mertod R.f, P.epann Antlwd Botth Afl8lyst

S€mivohtlle (kgrnic CoEpo{dd! by CC

Orqanocldodne P€stickies SW846 8081A

Prepared by rnethod SW846 3510C

3rea5-7 bFBHC31s-E€{ d-BHCsE{+g grSHC (Lindahe)

57.74-9 cl o{daoe72-54-a a,a-DDO (p,p)

.2-5s 4,4-0DE (p,p,)

50-2s3 a,+oDT (p,p')m'sr.l Dieldin96&{,&€ Endosulbn I3321$6s-9 Endosulfan ll10i11,07.8 Endoeulfan Sulfate72-244 Endrin7421€3-r Endrin Atdehyde76-44{ tbptachlorZ2-43-5 Mohorychlori02a-57-3 Heptachlor Epoxide6001-3+2 Toxaph€ne510}71-9 a4hlofdan€556&347 g,Chlo.dan€534S+7G5 Endrin Ketone

Surogde rc@veies:1 NP,64+2 1,tl-Dg-Octafl uorobFkenyt (S t)?351.2q Daca&lorobiphenyl (Sr)Polvd o.imted Biohenvls bv SW846 8082Prepared by ftethod SW846 3510C1267+11-2 PC8 t0161110/.2e-2 PCB 12211ti11-16-5 PCB 1232s3{6$2i-9 PC8 124212672-zin Pc]B 124811097{s-i PCB t254r 109d82-s PC8 12603732+23{ PCB 12621r10c14-4 PCB '|268

SunEga'e t*ayedes:, 03868+2 1,4o$Uafl@mhiphenyt (Sr)?'51-2+3 bca&lotob;Fhenyl (Sr)

Semlvolrdk Orgrtrt. Compo{ndr by GCMS

U-lht-Ol 22-lli847 7031270 fGBRLBRLBRTBRTBRL

BRLBRLBRLBRTBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

6987

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0.0r 11o_0111

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sw8.r6 80914

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S€mivolatilg Oiqanlc Cornpounds bv SW846 8270CPr€pared by m€O|od SW846 3510C

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56-ss-3 B€nzo (a) anthaac€ne

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Thb knotuory r.porl ls aot tdd *ithod an aufiotized sigtr&ltQe on rhe crver pag..

. Repodrbl€ Detectiod Limit BRL = Below Reporliog Limit Pag€ 70 of 124

Page 542: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificarionFWZsAs95l7-14

Client Proiect #l0l -88

MatrixBlank Water

Collection Dat€/Timel9-Mar-0? 00:00

Received20-Mar-07

CAS No, AMlytc(s) FloC Ani$ *RDL Dilutian Method Ret Preparcd Analrzed Batch Ano4lst

S€rdvolNtile Org.nlc Compounds by GCMS

Semivolatle Orqanic Comoounds bv SWB46 8270CPrepqred by mebod SW846 35 | 0C5032-8 genzo (a) pyrene205-992 Benzo(blduofandEne1911+2 Benzo (g,h,i) peryteno207-084 Benzo (k) fluoranthene65{5-4 Benzoic acid10G5r4 Beozyl alcohol1rl'9i-i Bis(2drloroethoxy)methane1tl.4 Bis(2<hloroethyl)ether39fi&r2-9 Bis(2{hloroisopropyt)ether1i7-81-7 Etis{z€trylhexyl)phlhajele101.5t3 +BromophenytphenyleherA5{&7 Butytbenzytphthalate8S74-8 Cerbezole5!r-5r|7 +chloo_3_methylphenol106-47.€ +chto{Daniline$.54-7 2-Chkrmnaphtfialene{16-57-a 24hlo.opfi€nol7ool72.3 4-Chloaophenyl phenyl ether218{1-S Chrysene5+7G3 Dibenzo (a,h) anthracene132€4-9 Dibenzofuran956Gr 1,2-Dichlorcbenzene51ti-7!1 t,3-Didrlorobenzene106-46.7 t,4-Didilorobenzene9l€+i 3,3',-Dichtorobenzidine1UlA3.? 2,+Dichtorophenol8a{j'2 Oi€thyl phthalate13i.1r.3 Oimethyt phthatate1os7{ 2,4-Dtn|ethl'tphenolt+7+2 oi-n-buty'phffralate534-52-1 4,6-Dinitrc-2-m€thytphenol51{8{ 2,+Dinitrophenol121-142 a4-Dinitroiolueng60G20-2 2,GDinihotoluene117-844 Difl-oci/ phhatate20€-44{ Fluormhene8&7!7 Fluorene1i&74.1 Hexachlorobenzene674&3 Hexachlorobutadienen4t4 HexadorccydopentadieneA7-72-l Hexad{orcethane19&3&5 Indeno (.t ,2,3_cd ) pyreneZ8-5$1 tsophorone9i-574 2-Metrytnaphthalene95-1$7 2+rethytPhonol10&3s{, 3,+Me{hyiphenol1o€-i!r,ssi-2r.3 NaphthalenePla-744 2-Nifoanilines-o+2 3-Nifoanilinel|x}{)r.€ +Mtoaniline

SW846 8270C z2-MarOI 23-MarO7 7031272 MBBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRL8RL8RLBRL8RLBRLBRLBRL8RL8RL

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pg/l 0 200

ugt 0.200pS/l 1.00

tsll 0.300

USn 1-00

tSn 1.00pSn 1.00

!S,4 1.00

!S/l 1.00

,lS/l | 00

!g/l 1.00

ldl 1.00

l4/l 1.00

udl 1.0o

ug/l 1.00

ldl 1.00

tiS/l 1.00

!s/r 1_00pS,4 1.00pS/ 0.200

!S,4 1-0OpS{ 100pSI 1.00

!S4 1-00

LiS/l 1O0

!S/l 1.00

!g/r 100

!g/l 1 00pS/l 1.00

liS/l 1 00

ldl 100

Udl 1.00

tidl 1 (X)

!S/l 1.00pSI 1.00

lSn 1.00

US/l 1.00

Ug/l '1.00

pg/l 0.600pg/l 1.0Opdl 1.00

US/l 0-200

ItStt 1.0O

t dl 1.0O

Vglt 1.(n

trS/l 10.0

pg/l 1.00

l,g/l 1.00pg/l 'l.00

lSI 1.oO

Thir lobnto,y rcpotl k aot ealid Nlthout a aahoizeal slgnatare on rhe co|er page.

+ Reportable D€tedion Limit BRL = Below Reporting Limit P a g e ? l o f l 2 4

Page 543: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sarnplc [deotificatiotrFB-2sA595l7-t4

Client Proi€ct #301-88

MatrixBla[k Water

Coll€ctiod Datellimel9-Mar{? 00:00

Rec€ived20-MaF07

CAS No. Aaebtqs) Resutt FlLS rRDL Duadon Mdho.l R4 Pdpa.cd lnabzd Detch A|alfst

S€Elvolstllc Oryrtrh Comporn& by CCMSSemlvolatile Orcanic Comoounds bv SW846 8270CPrepaGd by method SW846 3510C90€+3 Nibobenzene80-7t5 2-NitroPhenollOO{}2-7 +NihcFheool6?-7+9 N-Nitosodimehylamtne62t{4-7 N-Nitdsodi-ft p.opylamine8e30{ N-Niblsodiph€nylamine87{e5 Pentacfiloopheflol85{1{ Phenanthr€n€10&95-2 ph€nolr29.{n{ Fryren€110-€6-1 Flridtns12042-1 1.2.+Tri.htofob€rE6ness€t{ 2.4,tTddrtomphenol88{&2 2,4,GTddtlotopheflol

Sr,ttDgal€ /ffir€nias.'32t&A 2+luorobiphenyl$7-124 z+tuuqhenolal6aiah0 Nifunzena4s4te5€?'2 Phenordstr1es14 TqFhenyl4l4t1e"7s4 24,6-nibronaph€/rotSV@s bv S!'V846 8270C SIMPrepared by method SW846 3510ClIF324 AcenapMen€

2{E-96-0 Aaenaphthyjene9n"12{ l-M€hylnephbEton€12G12.7 . Anthaaceno5&553 Bonzo (a) anthracene50-32{ B€nzo (a} py€ne206-99-2 genzo O) nuoEndrene1s1.2r-2 Benzo (g,h,l) p€rytene207{€{ B€nlO (k} flUoaand,lene21C{1€ Chry'6€rF5+7G3 Oib€nzo (a,h) anhdcene206-44-0 Fluot€tr{En€&ll7 Fluor€no1s3-s{ Indem (1,2.}cd) pyr€nes15t€ 2-MedrylnaphhEb#9?G3 Napht|al€|1€8541{ Phonanfftreno129-q1.0 Pyr€ne

Sa7lwa{6 r€coyeriggi321-604 2-Fluo!6lphenyt17tE-514 Terphqlyl4l4

Totrl Mearl, by EPA 6mU7000 Sert ! Methodr

BRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRl-BRLBRLBRL

675579

804A

BRL

BRLBRLBRLBRLBRLBRLBRLBRLBRT8RLBRLBRLBRLBRI-BRI-

BRLBRL

49

ARL

BRL

BRL

30-1go %15-i10%30'130 %,u l10%30-1& %1u i10%

1.001.m1.001.001-001,001.00r.d)|.001.00

1_001.001.00|.00

0.0s0

o,0500.0500.05t)0.05()on500.9s00-0500.0500.0500.o50o_(mo.0500.0500.0500.o50

0.s00.o50

2*Me.47

pct

|ldlt'dl||g/r|,gnps/|pc4

udl!slpsfl

rsnrdllrcrludl

pgl

t,,dlFEAFSntts/|psil

rdltslluclrdlvsnpsnltslpsn

WA- usn

psl

Fdl

SW8.46 8270C 2.-ll[d47 23+,,ar47 f061272 t'l.B

1

tI

I'|

11I

1

1'1

I. 1

I

I

I

1

1

sw846 827oCGPA625 StM

7a'ao-?2{ Silvof

7:l4o-3e2 A6€nic

z1(L3$3 BA.ium

3o-130 %30-130 %

msrl 0.m5O

mgl 0-0O,$

.r]gA O.0O50

SW84U 60108 2A+rtrfl 2c+vler47 7031413 LR

Thit lobratory rcpod is ^ot vditt withotd oE.Qthotlttd dgazarc oa rte cota 1ngc.' R@orteble Delection Limit BRL = Bclow Rcpoftiog Limit P^Ec 72 of 124

Page 544: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdetrtihcatiooFB-2sA595l?-14

Client Proiect #301-88

MatrixBlank Water

Collection Date/Timel9-Mar-07 00:00

Received20-Mar-07

CAS No. Ana+w(s) Resall Flag UniB *RDL Dilutaon L{ethod Retr. PnF ed Aruryzed Batch AnatlstToad Melrls by EPA 6{XXy?000 Series Methodi

zr4o{}9 Cadmlumz!qx7-3 Ctromium213942-1 Lead

?02-{$2 Selenium

Totrl Met l. by EPA 200 Serte! Methods

743047.6 Mercury

26-Mar-07 26-MaF07 7031413 LR

26-Mat-O7 27-MaFO7 7031414 YP

BRL

BRL

BRL

BRL

BRL

mg/l

mg,4

ngn

nEn

lrrSl

0.0025

0.0050

0.0075

o.0150

0_00020

1

1

1

1

sw8,46 60108

EPA 245.117470A

Thh laboretory rcpoa ir not yalid wirtoa an atrtorizc.l signataru oa the coter IBge' ReDoriable Detecrion Limit BRL = B€low Repodng Limit PaEe73 oI 114

Page 545: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Saople ld€ntificationTB.2sA595l7-15

Clietrt Proiect #301-88

MaEix.Blaok Water

Collection Date/Tirp€I 9-Mar-07 0O:00

Received20-Mar-07

CAS No. Adolfle(s) Floe *RDL Diluiotr Merhod netr. Pftpor.d Anabagi Batch ,lnolN

676.-1 Acetone107.1!1 Aq!'lonitnb7113"2 Beaueno10&46-l Bromob€nzenet4-91-5 Bmflochtoromethane7+274 Bromodicfiloromethan€712+2 BmnEfonn74{}9 Baomom€thane78-93-3 2-Butanons(MEK)104-51{ n-But}'lbenz€ne13+98€ sec-Bu9lbenzenes€{)G6 tert€utylbsnzene7s-14{ C€Ibon disulfdes6-2$s carbontetrachtoride108-90.7 Chloaobenzene75{G3 Chloroethane67.€S3 Chhaoform

Vohtile Orgrtrlc Comporndf

Volalile O.oanic Compounds bv SW846 82608Prepared by method SW846 5030 Water MS76-13-t ,|.1,2-Tdcfitorotifluoroethane(FreoERl- SW845 E26OB 22-l,4€d)7 ?2-|4at47 7031296 ek

BRLBRLBRLBRL

BRLBRLBRLBRLBRLSRLBRI-ERLBRLBRLBRLBRLBRL

t(!l

ldl

wPdl

vsAlElltqllvgtlFqlPollt!94ugllgrlvglpgl

udlusnt!{!glps,l

!dlNnu{lys4

udlpsn

!s,uglpEr

Isrpdl

rslugtl|lgl

ldlItgtlpsil

!dlpgn

|tdlFSnucn.tjdl

!gl

|ldlp$

ugrlp9l

t d l!91

1.O20.o0.51 n1 .01 .0

1 .02.010.0t . 0l_ot_05.O1.01 .02_O't _02.D1 .0't ,0

2.O0.50.51-O1.01 .01 .0

2.01.0

1 .01.01 .01 .01,01 .0

1.0't .0

0.50.51_00.5r0.01_01.01 .010.0

5.0t . 0r . 0

7447-3 Chloronethane BRL9t{g-8 ?-chtoroioauene BRL10+434 il-Chloroiotuene ARL$12-€ 1.2-Oibrofto-3-dioropropene ARL124-48-1 Dibromochlofornethane BRIl0ce3.4 i,2-Dibfonro€Blane(EDB) gRL

74-9s-3 DbroanonpfEn€ BRLS{}1 |,2-Oicl orobenz€ne BRL5,{1-73-1 l,3oichlorobenzene BRL106-4G7 l!-OicHo.obenzene BRL75-714 Did orodifuorornethane(Freonl2)BRL7534-3 l,1-Dichloro€thane BRLt07-cr6-2 |,2-oichlororettEne BRL71354 |,l-Dichloroethene BRL15Cs$2 ci9.1 ,2oiclrloro€hene BRL15S60-s hans-1,2-Oic* oao€lh€ne BRL7837.5 l,2-Olchtompropane BRI_142-?trg 1,3-D'ichloropropane BRL5 2G7 2,2.Dlchtoropropane BRL56+586 l,ioichloropfopene BRL10061{t.5cis-1,3-Dichloropropene BRL10061{2at?ns-1,3-Oiohloropropene BRL100-41-4 EthYlb€flzene gRL

07€&3 tt€xad orobutadi€ne BRL591.764 2-Hexanone(MBK) BRL9A€2r tsopropy'b€nz€ne BRLs37€ +lsopropyltoluen€ BRL163a{4.4 Methyt teft-hrty{ eth6r BRLlc'&1c1 4-MethyL2-F€fltanone(M|BK) BRL7549.2 t{ehyleno d o,ride BRL91-2G3 Naphhal€ne BRL1016+l n-Propyheruene BRL

Thh Lhuolary rqod ls aot vditt lfihotd zd adfndzad slgns//are orr thz towr page .

' Reponable D€tectioo Lilnia BRL: B€low Reporting LiEit Page 74 of 124

Page 546: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sampl€ Id€ntificationTB.2sA595l7-15

Clielt Proiect #30 t -88

MatrixBlank Water

Collection Date/Timel9-Mar-{17 00;00

Received

20-Mar-07

CAS No. Analyte(s) Resalt Floq Unia XRDL Dilution lnethod Retr, Prcparcd Analyzed Batch AnalJst

Vobtile Orgllic Compoudds

Volatile Omanic Compounds bv SWE46 82608Prepared by rnethod SW846 5030 Water MS1ql4?-5 Styrene BRL63&a}{ '1,1

,1 ,2-Tetrachloroethan€ BRL7!|.34-5 1,1,2,2-Tetrachloroethane BRL127n6{ T€tEchtoroethene ARLt06{6-3 To{uene BRL4731-€ 1,2,+Trichlorobenz6ne BRL120{2-1 1,2,+Trichlo.obenzen€ BRL7r-55{ 1,1,1-Trichloroethan€ BRL79{01 1,1,2-Trichloroethane BRL79414 Trictloroethen€ BRL75{9r Trichloronuorornethane (Freon 11) BRL96-18-11 1.2,&Trichloropropane BRL9543-6 1,2,+T.imethylbenzene BRLlo€{7€ l,3,STrimethylb€nzene BRL75-01-4 Vinylcfloride BRLi33}.al.7 m,p-XyterE BRL95-47a o-Xylene ARLiogg}-e Teb.ahydrofuran BRL60-2+7 Ethylelher BRLggiros{ Teft-amyl methyt ethef BRL637- -3 Eth!4 tert-butyt €lhel10&e3 Di-isoE ropyl ether75€5-0 Tert-Butand / buty' alcohol12!91.1 1,+Dioxane

Sunogale /ecov€n€s:tl604rJt 4-BtofiofluorobenzeneU37.26-S Tduene-dg1 10@47 4 1,2'Dichlomelhane-d4

ft64-*L7

!sntsllljgnpEl

Itgtl

Lrg/l

lrEl

usnugn!91

f9l

!g/l

rr!yl

ItEl

!gn

tsll

ItEl

usnpsr!slp9l

p9/l

Ljsfl

r.iS/l

1 .0l_00.51 .01 .01.01 .01.O1_01_Ot -01 .01 .01 .0'1 02 0't .0

10.01 .01_01_0l_010_020.o

t

l

1

1

1

1

1

1

1

l

1

1

1

I

1

I

1

1

1

1

1

1

SW846 82608 22'Mat47 22-Ma.{7 7031296

BRLBRLBRLBRL

98102s3100

70-130%70-130 %70-130 %70'130 %

Thls labonlary 7sps11 ;t not val I tuittout ai outhoi.ed sigaatwe on the covet page.

' Reportabl€ Det€ction Limit BRL = Below ReportinB Limit Page 75 of 124

Page 547: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Voladle Organic CompouDds - Qrdity Control

Bstch 7031296 - SW846 3130 Wrt€r MS

Blank 17031296€LKll

Prepared & Anal}.z€d: 22-lv1ar-07

1,1,2'Trichlolotriiuoroethan€ (Fr€on 1 13)

Acrylonildl€

Benzen€

Brofiob€nz€n€

Bromochloromehane

Bromodid{orom€ih€ne

Bromoformgromomolhdre

2€uhnon€ {MEK)n€uVb€nz€ne

sec-Butylbenzene

tert€utylberEsn€

C'arbd| dislrlfide

Carbon l€trachlodde

Chlorobenz6n€

Chk!roethane

Chbroform

Chbrornethan€

2chlorotoluene

4{hlorotoluene

I J-Dibromo-3drbropropaneOibrornfthlorDrneft5n€

1,2-Dibrornethane (EDB)

Oibromomelhafie

t ,2-Olchloroo€nzs.r€1 ,lDinbrub€nzene1 ,+DichlombenzeneDid orodifluoromothane (Freonl2)

l,lOichbroethan€

l,2oichloro€than€

1 ,1 Oichloroethene

ds-l ,z.c,[email protected],2-Dichbro€thene

1 2-Dic*rloropropane1 ,$Dicfiloroptop€ne2,2okt oroprcpane

1,1-Oinbrcprop€r|e

cis- 1,3-Oichloop.opene

ttEns-1,$Dichloopropene

Elhylbenz€ne

itexachlorobuladi€ne

2+l€xanone (MB()

lsop|opylbenz€n€

4lsopropyltot €neMethyl bd-bug/ eherl-lrothyl-2.!€nlanone U|8K)i,lolhylerc ('lbrid€

Naplrthalen€

n-Propy'tr€nzene

Styr6n€

I,l, !,2-Telrachloro€o€n€

BRL

ARL

BRL

BRL

BRL

BRL

BRI

8RrBRL8RLBRLSRLARLSRLBRLBRLBRI.ARI-BRLBRI.BRLBRLBRLsRr-BRL

sRr-ARL

8RrBRL

BRL

ARL

BRL

BRL

BRI

ARL

8Rr-aR|-BALgRL

BRLBRLBRLBRL8RrARL8Rt8RL8RLBRLBRLBRLARL

tc4!dl

rgll

usnugrlps4t gtl

ugnpdl|ldl

fl41

!gl

tJ9t4

tql

||g/lpsnygl

!dl

ItSll

!dl

udlusnttgfl

t's/ltollusnusrpql

!dl

!dl

trdl

u9nItgAggil

wusnItsnpcn!dlgsfl

usnugA!dlwlt,€ll

llsil

|ldl

udlpdludludludl

1_020.00.51,01.01 .00.51.02.0t0.0t_01 .01_0

1.01.02.0t . 02_Ot.01.02_00-50.51.01.01 .0r . 02_O1.01.01.01 .01.O1.01.01 .0t.00.50.5't_0

o_510.01.01.01 .010.05.0t . 0t.01.01_0

nhit labdorf Eporl b Eot vditt i'Ehau sn aathortztl tur@lE oE the corer page.

. Rcporable Detectiou Limit BRL = Below Reporting Limit PaEe16 ot 124

Page 548: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Brlcb 7031296 - SW846 5030 Wsrer MS

Blant a?031296€LKl l

Pr€Fred & Analfzod: 22-Mar-07

|,I,2,2-Tetrachloro€than€

Telrachloroeth€ns

1,2,$Tricilorob€nzene

1z,+Tridbrobenzene

1.1,l-Trid or€taan€1 ,'l ,2-Trirfibroef|aneTriciloroetl€ne

Tddrlo(ofluorcm€tharc (Freon 1 t)1,2,}Tri:hloropropane

1 l,4.Trlmehy'b€nzene

1 ,3,&Tdm€hylbenzeneVlnyl d oride

m,p-Xy'ene

crxyl€ne

Tehahydroturan

Ethy' ether

Terl-€myt m€thy' €ther

Ehyl t6rt.b|t/ efi€rf,liisopropyl etherTert€utanot / butyt atcohol1,+Oioxen€

S ,,''ogaa6 : + Btotnofl uo mh e n ze neS|,'ogate: Totuene4gSuftgete : 1,z-Dichlorcethane44S urrcgate : Di b rononrcrc melh a ne

LCS a7qtl29€4st )Pr€pared & Analrled: 22-Mar4Z

1,1,2-Trid oromuoro€ttnane (Freon.t.t3)

A.fy'ofiit it€

B€nz€n€

BromoberEene

Bronoc||brdnethane

Brofircdidlloaoflt€[lane

Brwnotoarn

Broo|on|ethane

2-Aubnon6 (MEK)

n€otylbenzen€

s€cdu!y'b€rEene

isrr€uttbgnzene

Carbon disrltfide

Catbon tetad{onde

Chlorobs\2ene

Chb|Dehane

Ct{orDf\crm

Chloaomoflane

24hbrobtue.|e

44hlorotoftrene

l,2Olbromondrbropropane

oibfomodtlo.ome0rane

t 2-OibtDmoeu€n€ (EDB)

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRI.

aRl

BRL

BRL

8RL

BRL

BRL

BRL

BRI-

BRL

BRL

ARL

8RL

50.350.746.650.2

21.9

19.9

1 4 7

21.2

21.7

20.6

20.7

21.8

20.2' t9.1

20.5

23.0

16.9

22.8

1 9 3

20.1

2 1 0

22.2

2 1 . 2

19.2

22_1

21.1

!snLi9/l

Ljglpg/l

lr9lpsnpdlpdl

u9lpsnpsll

tj9l

ugl

!91

!gn

usnu(ylttgrllrg/luglt'|dlpg/lpElps/luglugi

psrusnpgn

!s?1!s/l!snus/lltg/tt g/lpg/l

usnusnusn!s4Lj9l

!sn!sntlg/l

rg/lp(yl

!g l

!9,usr!gl

0.51 01 .01_01 01 .0t . 01 .01 .01,01 .O1 .01 .02.O1_010.01_01 01.01 .01 0 020.0

50.050.o50.o500

20.020020.o20.020.o20.020.020.o20_020.020.020.020_o20.0m.020.o20.o20.o20.o20020.020.020-020-0

101 70-130101 70-1U93 70-130100 70-tu

110 70-130'f 00 41_1-14794 70-130106 70-130108 70,130r03 7G130104 70-130109 7Ga130101 62-.t3€96 53.9-133102 70-130115 70-1 30113 70-.t3094 70-130114 70.130108 70-13096 62.&132100 70-130105 7G130111 70-130106 70-13096 70-130110 70-143106 70-130

This labordoty .epod 8 nol wljd Hithaat on atdroriad signalarc on the eover page+ Reponabl€ D€rection Limit BRL = B€tow R€porring Limit F a E e l l o t 1 2 4

Page 549: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organir Compounds - Quallty Control

SpikeL€vel

%RECLimits

RPDLinit

Source

Result %RECResult Flag Unit! RPD

Brtct 7031296 - SW845 5030 Wrl€r MS

LCS r'031296-AS| )

Prepared & Analyred: 22-Mar-07

Dibromomethan€

l,2.oichbrob€nzen€

1 ,3-Dichbrob€nzene

I ,4-Dlifibrob€nz€neDicl{orcdiff uoromolharE (Fr€onl 2)

t ,l Olchloro€than€'l,2-Didrloro€rfiane

1.l-Dicf oroeth€ne

cis-l2.Dichbro€th€ne

Fdns-1,2-Di{* oroelhene

1 2-Dichloroplopd|e

I .SDichloropropane2,2-Dichb|Epropane

1,1-Dbhlo.opropene

cis. 1,3-Drcnbrcprop€ne

kans-1,3-Didtloropropene

Elhylbenzene

HexachloobuHi€n€

2-Hexanone (MSK)

lsopropylbenzene

4-ls@r(tpyltoluene

Methyl bn-buql ether

4-lreihyl-2f entanone (MIBK)

Itlstry'ene dbrtdo

t'laphthaleoe

Styr€ne

| ,l ,1 ,2-Telrachloroelhan€1 , I 2,2-Tetrachtoro€lhane

12,$Tricnbrob€nzene'1,2,+Tdchlorob€rEene

1.1,1-Trichloroethane

I , | ,2-TridloroethaneTricl{or€thene

Tichlorcouommehan€ (Freon 11)

1,2,!TrirJ oropropane

1,2,+TrnnehyltFflzen€

1,3,+Tdmethy'b€nzen€

Vinyl afiloride

m,tsXyl€n€

TelrEhydrofu.an

Etryl elher

TeGamyl m€fiy' €th€r

Etryl t d+utyl €fl€r

OLisopropy' ether

Tert-Butanol / b(tyl alcotlol

I,+Dioxan€

S u nog^le : lLgtonbfl uo rcbe n ze rcSu/rcgata: k @ne48Su/'ogal3: l,24bhlorodhane44

19.720.622.520.122520.719_4r8.321.720.321.520.826.020.521.9t9.321 .423.620.221.121 .3t9.9m.4.t9.7

18.921.222.2

21.522.020.514.62?.420.s

20.s21.28.022.5

44.923.220.519.221.222.121.2r7€207

50.145.5

usnlldt

l|g4

t€/lpcnPgtt/dl|lsnu9ntt$psil

pg4

pcnts/|usnudlt,€Awt'gluqt!dlTS/||lgl

ttg|t g/l

!snpdl

udlLrglIrdlrcnlrg4rgltsrpdl

!sn[gl

ldl

trgrl

tryl

!s4

us4pdl

edlttgfiuqlwl$nuql!dl!dlugl!dl

20.o20.020.020.020.0m.0m.o20.o20.0m.o20.020.Dm.020.020.020.020020_020.020.020.020_o20.o20.o20_020-o20.020.020.020.0m.020_020-o20.020.0m,020.020.020.020_o20.o100m.0m.020.020.o20-020.0200200fl.o50.o50.0

9a 7G130103 7G130112 7Gt30100 70-130112 39.&167104 70-1fi97 70.13092 7G130108 7{rr301d2 70-130104 7G130lft 70-130130 70-130f02 7v1301r0 7G1309€ 70-t3t)107 f0-130110 70n36101 56.3.131f06 70-130106 7G'r30100 70-130102 70-t3094 7G13{)94 70-130r(Xi 7G.130r11 7G130t18 7G1301o8 7Gr30110 70n30lm 7G13074 70-13rc112 70-130104 7G130102 7G130102 7&130'106 7Gr30115 70-t3o112 70-,t30112 70.10106 ?G130t12 7S1301t6 7Gr30102 zGi 30s6 7G130106 70-1301t0 7G130t06 7G130&! 7G130104 70-r3o105 70-IU100 f0-1fi9t 7E 3t)

Ika! laboelary r?pott,s frteond ''i/,,ord tn otdrodzet signat.E ot ttg cwer poge.

+ Repo.nble Dete$ioo Limit BRL= B€low Rep(trtiae LiEir Paee 78 of 124

Page 550: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgalic Compounds - euatity Conarot

Aoalyrds) Result Flag UnirsSource

Resulr %REC+RDLSpikeLevel

%RECLimirs

RPDLimilRPD

Brtct 7031296 - SW8{6 S0l0 Water MS

LCS fl031296€51)

Prepared & Anatyzed: 22,Mar-U7

S u ftogale : Di bro fi tofl u om n€th a ne

LCS Dup l703t29iBSO1l

Prepa.ed & Anatyzed: Zz-Mar{7'1,1r-Trichlo,otdf,uoroethane

(Frson 1 t3)

Aciylonihil€

B€nz€ne

Bromobenzsn€

Bao|hodlbromethane

Brornodit odnethane

Sromoform

Brcrnomehane

24ulanone (MEK)

n€utylb€nz€ne

sec€uiy'benzene

tsrt€'rtylbenz6.r€

Ca6on disulfide

CEfton bt'achlcride

Chlorobenzene

Chloroethan€

Chlolobrm

Chlomdre0lane

24hlorotoluene

44hbroioluene

I 2-Dibro.no-3rJltoropropane

Dibromochloromethane

l,2-Dibrcmoetra e (EDB)

Dibfornomethane

l2.orchlorob€nzene

I ,3Oicfilorobenzene1 ,4-Did oobenzene

Did oro<,|fl uotumerhane (Frsonl 2)|,1-Dldb.E€thane

1 ,2{)i* oro€thane

1 ,1 Oldlo.o€trene

ds-t 2{)i$broethen€t'anE- l,2Oichtoroethene

| ,2ol$loropropane1 ,$Di*k ropropane

z2-Dicl o,ropmpene

1 ,1 Oicfiloropropene

.i5-'l ,3oinbrcpropen€tans-1,$Dictloropropene

€@benzene

Hexechlorobutadiens

2+lexanone (MBK)

lsopropy'berEene

4-boproMolu€ne

Melftyl t€n-butyl etr'er4-[r6thyl-2-p€ntanone (MtaK)

MetrMarE chtoride

Na9hf|5l€ne

49.8

19.4

20.1

18.7

19_7

21.3

20.0

19.7

22.2

1 8 6

18.0

20.3

23.2

23.O

15.9

20.6

21.O

1 7 9

1S.0

1 9 4

21.4

20.7

18_0

21.2

2 0 9

18.8

20.5

21.7

19_4

1 9 1

19.6

18.8

r6.6

20.6

18.4

203

20.2

24.3

ra.4

20.7'18.3

2 0 6

2 1 . 7

1 9 4

20.6

2t .7'19.6

19.9

17.6

17 -4

pdl

pdl

!srpgl

ItEl

rcnFEI

!g l

!g/l

tgnpglpsl

tig/l

tgl

!snpgn!91pgl

us/ygtl

uglps4

!gn

vgl

lr9l

ttEl

lj94p9l

pg/l

usnpg/l

rcnpdl

pdl

!!y1

ug/l

Itgrl

IIEIpdl

udl!g/l

vtttlps4

psil

!glpdl

!sr!sl!snug/l

50.0

20_020.o20.020.o2 0 020.o20.020.o20.020.020020.o20_020020.o20.020.020.020-020.o20.0m.020.020.o20_020_020.020.o20.o20.020_020020.020.020.020.020.020.020.020.o20.020.020.o20.020.020.020.020.020.0

99 7L130

97 70n 30

100 41.1-147

94 70-t30

98 70-130

t06 70-t 30

100 70-130

98 70-130

111 70-130

93 62-136

90 53 9-133

102 70-130

116 70.130

115 70-130

60 70-130

103 70-130

105 70-130

90 62.&132

95 70-130

97 70-130

107 70-130

104 70-130

90 70-130

106 70-143

104 70,130

94 70-130

102 /0-130

108 70-130

97 7G130

96 39_3-167

98 70-130

94 70-13t)

83 70-130

103 70-130

92 7G130

102 7G130

101 70-130

122 70-130

s2 70-130

104 7G130

92 7G130

103 70-130

108 70-136

97 56-3131

103 70.130

108 70-130

98 70-t 30100 70-130

68 7{t130

a7 70-13n

13 25

0 5 0

0 2 5

8 2 5

2 2 5

3 2 s

6 2 5

2 2 5

8 s 0

6 5 0

0 2 5

0 9 2 5

2 2 5

16 25

10 25

3 2 5

5 2 5

8 2 5

4 2 5

2 2 5

6 2 5

4 g

2 2 5

4 2 5

1 2 5

4 2 5

3 2 5

l5 50

6 2 5

3 2 5

10 25

10 25

6 2 5

3 2 5

6 2 5

10 25

4 2 5

9 5 0

4 2 5

2 2 5

7 2 5

8 2 5

Thh labordory rcpofi k tot valid witho4t aa rathortz"j sign ture oa the corer ptage.* Repdable Derection Limjt BRt_ = Betow Repoding Limir Page 79 of 124

Page 551: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compouods - Quality Control

Amlyr€(s) Result Flag Units R€srlt %REC Lrmrls

B.Ntch 7031296 - SWt46 5030 Wrter MS

LCS Ouo (7Gll296€SDl )

Pr€paEd & Analfzed: 22-Mar-07

Styr€n€

1 .1 .1 ,2-T€trachloro€lhaneI , | .2,2-T€tsachloo6lhane

Tebachlorc€thene

Tolu€n€

1,2,lTrichlorob€nzene

1,2,+Tricnbrob€nzefl€

1,1,1-Tri$broelhane'1,1,2-Tridlnoethane

Trichloro€thsr€

Trichlorofl uoromet|ane (Freon 1 1 )1 2,3-Tddrbropropan61,2,+Trim€tnylb€nzene

l,3,'Trirn€drylbenzene

Vinyl chlodde

m,p-xylene

. Tet ahldofuran

Elhy' €h€r

Terl-amyl nEthyl etier

Efhyl te.ttu!y' efter

Oi-isopropy' €tier

Tert-Buianol / buv alcohol

I,4-Dioxsne

S unogate : + Bto nbfllwoh e n ze neS'l'rcgate: f(rl@ne4gS uiog eh : l, 2-Dich f oroetha n e 4 4Sutogalg: Dibmn$fluot@tethat e

Marnx Soft(€ O031 29&MSll

P.epare<t I Anal}.i€d: 22- ar.07

Benzene

Chlorob€nern€

1 , l -Dlchlorc€flens

Toluen€

Su/7ogab : 4-&otrpfl uor&EnzeneSunogote: foL/6.ne4SS.j'|ogate : 1,2OkahlomdhaE443 u tng ale: Dilbanof, uoronelh a ne

20.621.523.121.5't9.9

19.5'13_9

21-415.220.2t8.6r8.722.922.622.418.543.2

20.419.421.021.420.6r7321353_849.845.049.6

Solrrc6: SA59563{l

1{X} 7G130100 70-lm't1E 70-'130108 70.130100 70n3096 7Gr3070 7S.130107 7tt130s6 70-1010t 70n3094 70-13094 70-130114 70-130113 7Gr30112 70.t3092 70-t 3t)lm ?0-130110 7G130102 70-13xn 70-130105 70-130l(x, 7G130t03 7G13086 7&1 30106 7G130108 7G1g)100 7G1g90 70-13099 70-1m

r18 70-13t)128 70-130104 70-i30117 70.130112 7G13099 7G130tN 7G1$91 70-13099 7G1n

lt4 70-130124 70-1301ft} 70-130116 70-130r00 70-130gg 7o-tu101 70-1fig 7&1fi98 70-130

!dlugll!snydl

t s4pg/l

ug4r.'dlpdl

!dlpgr

ugtl!dtFSilugl!94pgl

tsllpdl

uglu$pdl

WIlrgnt4l4!sntd l!41psn

20.020.020.020.020.020.020.o20.020.020020.020.o20.020.020.o20.0,10.0

20.020.020,020.0200m.0zn200fr.o

fi.o50_0

20.020.020.020.020.050.050_o50.050.0

20.020.o20.020.o20.o50.050.050.o50.o

332010

65

1I120.90.9014

50

0.90.9

2525252325252525

25

50

252525

2550

25625

23.425.720.823A22.549.650.145.649.6

lrEl

wl!g/l

vslluc,4pdlpdlu9l|lgn

8RL

BRL

BRL

SRL

8RL

lilatrlx Solk Ote O031206-flSO1t So{rcr: SA5O!6J-01

Prepaed & Anal]/2ed: 22-Mar-07

B€flzene

Ct{orcb€nzen€

1 ,l .oidtlorcenhene

Toluen6

Trbhlorosthen€

Ssfogate: ttglo/noltuoloben,f,,neSu/'ogale: Td@ne4gShogale: 1,2-Dkithrcethane44S u nqate : Dibtunrcfl uotornelh a ne

Brrcb 7031335 - SW846 5035A Soil 0ow lcvct)

22.924.820_623.1

49.550.715.118.8

BRL8RLBRLBRIBRL

lrdlFSnrcn!dlpdl

rdlu9l|lsnIt

331

0.9

30

30

This labtulrq rqn.a is not vald *&hov an ,,r!rtorize.I sign,d.tre on tte cova, psge ,+ R€portable Dete{rion Limit BRL = Below Rcpqriry Limir P€e 80 of 124

Page 552: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compoutrds - Quality Control

ADalFe(s) Result Flag UnitsSource 7"RECResult %RtrC Limits

Spike

L€vel

RPD

Limi(

Brrch 7031335 - SW846 50J5A Soit {tow ter.et)Blank {70t133!t€LKtl

Preparcd & Analfzed: 22-Mar-07

I,1,2-Trid orolrifluoroethane (Freon t13)

Acrylonibil€

Benz€ne

Brdnob€nzene

Eromodrbmmelhane

Brornodk$loronehane

E.omofom

Bfomorne$ane

2€uranone (MEK)

n€utyD€nz€ne

6€c-Buiylbenzene

tett€utylb€nzen€

Cdbon disifde

Carhon lehacfilodd€

Chlo@benzen€

Chlooethe|e

Chlorofom

Chlorofir€$ane

2-Chbrololusn€

4-Chlorololuene

l,2.Dlb@mo-3-chlompropane

Dib.omo<fibromethane

1,2-Dibmmo€thane (EDa)

Oibfomomehar€'| .2-Dichbrob€nz€ne

1 ,3oicibrobenzeneI ,lLDichloobenzeneOlcft lorodiff utrom€thane (F.eonl 2)| ,1 Oi{rhloroethane'l ,2-Didtloroethanel,l.Dic$lor*then€

ds-1,2-Oic*rbmethene

t_ans-l,2Oldtloroethen€

1,2-Dldrlorcpropane

1,lDichlompropsne

2,2-Dbt{ompropane

J , l Obhbroprop€n€

cis-1 SJidrlsop.opene

ttans-l,3oid oropropene

Ethylbenzene

H€xachlo(brrtadiene

2-Hexanon€ (MBK)

lsoFopylbenzene

+lsoprorMrolu€ne

Motryl bd-buv dr€r

+M€lhytz-pentanone (tlttBK)

Methten€ crrloRte

Napha|abn€

Slyrene

1 ,1 ,1 2-T€trEchbro€haneI,I J,2-Tetrachloro€{hene

BRL

BRI.

BRL

BRL

BRL

BRL

BRL

8RL

BRI.

ARL

BRL

BRL

ARL

BRL

8RL

BRL

BRL

BRL

ARL

8RL

BRL

ARL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

ARL

ARL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRI.

BRL

BRL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

!g/kg wet 5.0pglkg wet 100pS/kS tvet 5.0pg/kg wet 5.0

!g/kg wet 5.0

lig/kg wel 5.0pg/kgwel 5.0

lgkg w€t 5.0

Ugy'kg wet 10.0

!949 wet 50-0

lgkg wet 5 0pg/kg wel 5.0pg/kg wet 5.0

lig/kgwel 25.0

!g/kg wel 5.0

P94(9 w€t 5 0pgkS vret 10.0pgr'kg wet 5.0pq/kg wet 10.0

Ligftg wet 5.0

lgkg wet 5.0

ttg/kg wel 10.0

!g/kg w€t 5.0

!g/kg wel 5.0pS/kS wet 5 0

Ugftgvret 5.0

lgukg wet 5,0pgr'kg wet 5.0

Ug/kg wet 10.0

Ug/kg wet 5.0

Ug/tg wel 5.0

Ugr'Kg wet 5.0

lgftgwet 5.0

!g/kg wet 5.0

!s49wel 5.0

!g/kg w€t 5.0

pgks lvet 5.0psrkswet 5-opdkS wet 5.0

!gl(q wel 5.0

!g/kg wet 5-0

lgL/kg wet 5.0

lgr'kg wet 5()-0

Ug/kg wel 5.0

l.rg/kgwel 5.0pgikgwel 5.0

trSikS vJ€l 50.0

!g/kg wel 50.0

Ug/kg wel 5.0

lgn(g w€t 5.0pdkSwet 50pqkS Yr€t 5-0

ldkg YJet 5.0

Thit labonlory rcpotl b not talirl xrithoul q4 aaihorizcd EiFttzturc on the cover pzEe.

* Repo.table Detection Limir BRL = Below Reporting Limit Page 8l of 124

Page 553: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volalile Orguic Compounds - Quality Cortrol

Bdch 7031J35 - SW846 503sA Soil (low levcll

Blant r|031335{LKll

PtepatEd & Analyzed. 22-Ma(O7

Tetrad$oao€h€na

1,2,3-Tric$lorob€nz€n€

1,2,+Trichlorobenzene

1 ,1 ,1 -fncnbroethan€

1 ,1 ,2-Tridrbro€than€Trici or€th€ne

Tricl orofuoromethan€ (FrEon 1 1 )1,2,$Tric*rloropropaoe

t,2,4-Tri.nehytb€nzene

l,3,STrimeftylb€nz€n€

\rmy' c* oride

m.p-XylerE

cXylene

Tetrahydroturan

Etrylether

Tert-amyt methyt €th€r

ErhY ten+utyl strr€r

Di+opropyl ether

Terl€ltanol / butyl alcotrcl

l,40ioxane

Surrcgale: laronldfrnorden zeneSunqatg: Toluen&8Sufltgate : l,2aichloftethane44S/u/tlgate : Dibro.ilo/fltlotonethane

LCS ft03t3:15€Sr I

Prspared & Anat)/red: 22-Mar-07

1 , t.2-Tricfiloro,trifluoroethane (Freon 113)

Benzene

Itomobenzen€grornod ordnethane

Erornodichlorom€hane

Baofitobfin

Brcmomelhane

z€ubnon€ (MEK)

n€utylir€nzene

s€c-Eulylbenz€ne

t€fi.Buty'b€nzon€

C€rbon disumde

C€rtoo bhacnbride

Chforcb€nz€n€

Chb&ethane

Chlooform

Chlotom€tl€n6

2Chbro{oluene

44hbrololu€n€

1 2-Dibmmo-:|-ct oropropane

Dibmmodrb(xnethane

1,2-Dibromoeharr (EDB)

Dibromonpthane

BRLBRLERLBRLARLBRLBRL8RLBRLBRLBRLBRLARLARLBRLBRLBRLBRLSRLSRLsRr-52.152.355.452.0

2006.5ls.020.417_a1E.020.218.917.914.216.819.719.417_O18.919.619.018.8t9.319.419.521.720.5m-2'| 0-6

50.050.050.050.o

20.020.020.o20.o20.o20.0m.0m.020.020.020.020.o20.020_020.020.o20.020.020.o20.o20.020.020.0m-oz)-o

Fg^gwet 5.0pgAgwet 5.0pdtSw€t 5.0pdkswet 5.0

lgftgw€l 5.0pgr'kg w€t 5.0

ldlqv,et 5.0

!g/kg wet 5-0

Ekgwet 5-0

lrgitqwet 5.0

lgr'kg wet 5.0pCftg w€l 5.0pg/kg w€l l0 0

UdkS wel 5.0

t/dkS Yret 5O.0

Ug/kS wet 5.0pg/kg wet 5,0

l1g/l€ wel 5-0

ldkg w€i 5.0

Fgftgwet 50_0

UC^gw€l 10O

ldkS w€l

!g'kg w€tldl€ wet|lgL{(g wet

!€/l€ wol

ldtS vret

l.'dks wel

pdkS trel

pdkg wet

ugr/kg w€t

tSn(g rYet

|l9fi9 wet

t gil€ wet

ugn€ w€t

lrg/tg wetpgts w€t

Iqkg wet

ldko Y.€l

lgr'kg tvet

!9Ag wet

!SI!S v{etpg/kg wet

rc/kg w€trc/kowetpSAg w6l

t'dkg YY€t

!$4q w€t

ld](S Yret

rc/kg,ret

104 70-t3t)105 7L1fi111 70-13t)104 70-130

100 70-13/)42 1.77-17595 7G130102 7Gr3089 70-r 3090 70-t3t)10t 7$13094 7G13090 55.113671 #.8-14294 7G130s8 7G13097 70-13085 70-13094 70n3096 70-13095 55.!13094 70-13096 7G13097 70-13/]98 70-t3t)lm 70-lm102 64_7-13910r 7G13093 7G130

Thls bbonbry rcpo.a k,rotvdidw hoa an auttoriud rigazute oa the covet pge.. R€Frtabi€ Detcdioo Limit BRL = B€low RcErrins Lirnit P^ge82 ot 124

Page 554: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compourds - Quality Cootrol

Analyt€(s) Result *RDLSpike

L€vel

SourceResulr

RTDLimitUnitsFlag

%REC%REC Limi6 RPD

B|ach 7031335 - Sw846 503sA Soil (tow tev€t)

LCS {7031335€3l I

Prepared & Anal!.zed: 22-ItaF07

I ,2-Dichbrob€nz€ne

1 .3oichlorob€nz€ne

1 JJid orobenzene

Dichlorodi0uoromotrhane (Freont 2)1 ,1 .I)bhlorc€than6

1 ,{i6lo.@thane

I . | -Dbnb.oef.n6n€

ci6-l,2-Di$broethene

lrans-l,2.0lc{l toroetr€n€1 ,z-Did orcpropane

| ,SDirJ ororropane

2,2okfiloropropan€

1,1-Did oroprop$e

cis-l,SOichlo.opopene

lran6-l,3 Oicnbrcprop€ne

Ethylb€rE€ne

l-lexachlorobutadiene

2+{exd|one (MBK)

lsoptopy'b€nzen€

4-lsopropyltoluene

rn€thyl lert-butyt ethe.

4+vtethyl2?€ntsnone (MIBK)

M€lhylsfle chlorde

Naphihalene

n.Propy'berE6n€

SVr€ne

1,1,t,2-TeHtloroethane

1,f ,z.z-Tet"ad oro€thane

Toluene

1 ,z,$T.ict orcbenzen€

1,2,+Trichlorob€nzene

I, I, l-T.tctrlorcethane

1,1,2-T.ihloro€thane

Tri:ib.oethen€

Tddbrofluoron€hane (Freon 1 .t )1,2,}Tri<t oropropane

1,2,+TrinlethylberEene

1,3,$lrirhethytbenzene

\rmylchlodde

m^0-Xylen€

oXylene

Tet-alryd$fu€n

Etll|rl et|er

T€nqnyl ftFthyl ether

Etlyl isrl+uM etler

Dl-lsogrepY "h",Ted-8{tanol / b(ltyl elcohol

1J-Dixar'€

S ui(va/e : 4-Bmmoll u orcb e n z e n€Slnrcg'/e: Toluene-daS,J/'rogde: l,2Olchloro€lhane44s/mt,gate: D/D,onld.fl uotomelha rn

18.8

1 8 . 1

1S_3

2 1 3

2 1 . 0' t9.0

17.9

1 8 9

1 8 8

20.4

205

17.9

1 9 . 8

19.8

19_4

1E.5

1 2 6

1 9 . 1

19-8

20.5

19.6

18.5

20.5

19..1

20.0

1 9 . 9

1 9 . 1

1 8 . 8

19.9

1 9 . 9

1 9 . 5

1 9 . 1

20.6

22..1

1 9 , 1

19.8

19.0

21.2

39.0

19,9

1 7 . S

19.2

22.0

22.8

19.4

174

177

48,551.s47.450.1

20.02 0 020020.020.020020.0m 020.020.o20.020_o20.o20.020.020.020.020020.020_020.020.o20.o200?0.020.o20.020.020.020.o20.o20.020.o20.020.o20.020.020.o20.020.040.020_020.o20.020.020.020_020020050.ofl.0fi.0ffi.0

US/kg wet

Fgtg wslpEt(g r^€t

!E(g wet

trdks wetpqhg wet

pyKg wet

Ugr'Kg wetpEkg wetpg/Kg wet

trg/kg wetpg/(g welyg/ko welpEr(g wel

Ug/kg w€lpgkS w€tpgkS vret

oc2 !g/kg wet

lEkg wet

!g/kg wetp9t(g \ /et

Irg/kg wet

tig/Kg wet

yg/tg wet

trgkg wet

ug/kg $/etpgi/kg wel

UEkg wer

Pg/kg wet

lrg/t(g wet

ug/t(g wel

Irg/l(g wet

!g/kg wet

t Et€ wel

uEr(g wet

rrg(9 w€t

!g/tq wel

ug/kg wet

Ug/kg wet

!g/kg wel

UgAg w€t

!g/kg wet

[g/kg wet

FS/kg wet

lglkg wet

uE|(g 'n€l

ygl$ w€t

ugy'kg wet

Ug/kg,,!et

!g/(g w€tt gftg w€lygftg w€lygftg w€l

94 70-130

90 70-130

92 70.130

106 U.+t67

105 70-130

95 70-130

90 70-130

94 7G't 30

94 70-130

102 70-130

102 70.130

90 70-130

99 70-130

99 70-130

r08 70-130

97 70-130

92 60.1-140

63 70-130

96 70-130

9S 70-130

102 70.130

98 46.1,145

92 7G130

102 70-1 30

96 70-130

100 70-130

100 70-130

96 70-130

94 70-130

f00 70-130

100 70-130

98 70-130

96 70-130

103 70-130'110 70-130

96 56_8-140

126 70-130

99 70-130

95 70-130

106 70-130

98 70-130

100 70-13t)

90 70-130

96 65.3-130

110 7G130

114 70-130

97 70-130

87 7G130

88 3+155

97 76130103 70-13095 7)-130100 70.130

This labodary rcport Ir ,tot valid ''tthoat zd outhoirpd siF rararc oE thz cover page .

* R€porrlbte Dereciion Limir BRI = Bclow R@nirg Ljmjr Page 83 of 124

Page 555: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

AnaMe(s) Resuh Fteg UnitJ

Spik€Level

RPD

LimitRPD!RDLSourc€ oZREC

Result %REC Limits

B.rch 701 1335 - SW846 5035A Soil (tow levet)LCS Duo r70gl33SSDil

Pepared A Ansl}rzed: 22-rvlar-07

|,1,2-Trichlorotmuoro€thane (Freon 1 13)

Acrylonitdle

Benze{|€gromoben:€ne

Bromochbromet,rane

B.oflbdichlorom€thane

Brornoform

Brcrnomelhane

2€uta.lcne (MEX)

n€utybenz€ne

s€c-Butylbenzens

tert-Buqdb€nz€ne

Carbon disulfid€

Cerbon btracnbdd€

Chlorobenzen€

ChloF€thane

Chlorofffm

CNoromettra|€

2chlomblu€ne

44hlorololuen€

1 JOibrofi b-3ddorcpropane

Oltrornociloromelhan€

1,2{ibrorno€lhane (EDB)

Dib|Emomethane

1 ,2-oichloroberEen6l,3oid irobenzen€

| ,4-DirfilorabenzeneDid orodif uoromethsne (F.eonl2)

1,1 -Obhlorc€thane

l,2obhloro€thsne

| , I Oi{$loroeth€ne

cjs-l 2-DirJ oroethene

t-ans-1,2-Dkilor@thene'|

,2-t i(,|bropropz€

1,lDicl oopropan€

22olcfrloroprop€ne

l.l -Dlcfiloropmp€ne

cis-l,3oichloropr@ene

lran9l,SDi.hbropaopen€

Ethylbenzene

Hexachlorobutadi€n€

2-tf€x8non€ (tvtBK)

lsopropylbenze'r€

4-lsopropyltoluem

lllethy' brt+uv 6lher

4-l,lethyl2t€ntanon€ (MlgK)

iretnrybne cfibril€

Nephthalen€

Sty.6ne

!, |,l,2-T€trachlorcethane

I,1,2,2-Tst'achloroethan€

21.39-818.720.318.217_421.O14.71S.912.019-719.420.518.219.5

17.319.220.119,319.31 f . 418.9

21.820.5r6.419.121-120.2r9.514.620.5'19.7

20_o20.017.120.521.321.820.019.9t3_618.620.1a).817.O18.2r9.819.4r9.8m.218.1

20.0m.020.o20.020020.020.020.o20.o20.0m.020.o20.020.020_om.0m.020.o20.020.om.020.020.020.020_020.0m.020.020.o20,0m.020.020.020.020,020.020.020.020.020_om.020.020.o20.020.020.020.020.o20-020.0m.020.020.0

Ugiko wet

lrg/Xg wel

t gks u/€l

Lrdkg Yv€l

lgr'kg {,et

pgr'kg wet

PgtS vJet

lgtS w€l

lgy'kg wet

Ug/kg wet

pg/*g wet

pg/tg w€l

Fgr'kg w€l

ugl/l(g lYel

t gtilg wst

lrgilg Yret

pgy'lq we{

!g,kg w€l

lgkS w€t

$/t(g wet

Ug/kg w6t

Pdkg $€l

UdkS v'^el

t g/kg rv€t

l,g/ko sst

Fgftg u/el

ldkS vr€l

ldkg Yrel

rc/kg vYst

|lg/kg wet

pg/kg wel

udkg vret

Lrg,fkg r€l

ldkS w€t

rc/ko wetygag wel

Fgrkg wel

rur'kg w€tlgL/kg rvet

!S/(9 wetpg/kg wet

lgkg wetQCz !g4qg vr€t

pgr'kg n et

lrg/t€ wet

Pgr'Xg wetpgukg w€l

IdkS $et

lrdlls wet

t€/ko u/et

Pg/fg welpdkg ',vel

UdtS wel

106 70-13049 1.77-115s4 70-130102 7Gt3091 70-130a7 70n3)105 7G13094 7Gr30100 55.3-13660 38.8-'t4298 70-13097 7G130102 7Gr309t 70-13098 70-13096 70.13086 55.3-130s6 70-130100 70-13096 7G.1309{t 7G13087 70-r 3094 64-7-139106 70-r 30109 70n 30102 7Gt3092 7Gt 3096 70130107 y_4-167

101 70n 3098 7G13093 70-?30102 70-13098 70-130100 7G130100 7G13087 7Gr 3{)102 70-130106 7G130109 70-130100 7Gr30100 60.7-14068 70-13093 70n 30100 7&130104 70-13085 46.1n4591 7S.r3099 7G13097 70-13099 70-130rol 70-13090 70-13n

t5 501 2 50 2 52 2 53 2 54 2 50 2 511 5017 504 2 51 2 55 2 57 2 54 2 5

10 502 2 54 2 51 2 5

2 2 58 5 05 2 5t6 25

2 X4 2 5

0.9 504 2 53 2 53 2 58 2 54 2 52 2 52 2 53 2 53 2 57 2 5

0.9 253 2 58 5 04 2 5

1 2 52 2 514 501 2 53 2 51 2 5t 2 51 2 5

Thb ,abodory ra?n.t is nol edld flithoA a4 Mthorlael [email protected] o,t the rover poge .

' Reporlablc Detectioo Limit BRL = B€l,ow Repoding Limir Psg€ 84 of 124

Page 556: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Baach ?031335- SW846 5035A Soit (low lcverr

LCS Duo (703133tASDil

PreFred I Analfzed: 22-[/ar-07

Te{rachloro€thene 20.6Toluerle 19.9l,2,lTricfilorobenzene 20 91,2,+Tridrlorotcnzene 19.9I,l,l-T.i$bro€lh€ne 19.6I,l,2.Tdchbroetiane 20 9Tdchloroe[heoe 2Z.aTridrlo.ofluomrn€thane (Freon 11) 2O.2l,2,3Tridrlo.oprcpane 21.51,2,+T.inehytb€nzene 2O.O1,3,$Tdm€f|ylb€nuene 20.1Vinyl d oride 22 7m,p-Xylene 38.8o-XYlen€ 19.0T€hahydrofu.an 18.0EtMether 21.1Tert-emyl medlyteth€r 20.6Ethyl ied$ui/t ettEr 224Di-isopropyl 6t'rer 19.6Tefl-Butanol/ butyl alcohot 1591 ,4-Diox€ne e3Su/'pgate: +BtDt pqtto@benzene 4B.gSu,togate: ToltAne4S 53.0Sunoga'€j 1,2-Dichtorcethane44 49,5Suiogab: Olbtono{Iuorcmethane 50.6

Brrch 70.3 1602 - sw846 s0l0 sott (high t€vel)

tigfl(g wet

Ug/kg wet

!S/kg w€t

lgr'kg wet

lgkg wet

lig/kg wet

pg/kg wel

lgt/kg wet

ligr'kg Y/et

pg/kg wet

t g/xg wel

Igftg wet

plyt(g wet

Ligr/Kg wet

!g/kg wet

Fdkg wet

!g/Kg werpgftg wel

pg,4(g wet

!g/kg wetQc1 pg/kg wet

ggftg wet

Pg'rg wel

!g/kg wetpg/kg wel

103 70-130 9100 70-130 0r04 70-130 4100 70-130 29E 70t30 2104 70-130 1't14 7Gr30 4r01 56.8-140 5108 70-130 15100 70-130 1100 70-130 5114 70-130 797 70-130 195 70-130 590 70.130 0106 65.3130 10103 70-130 7112 70-130 2s8 70-r3U 180 70-130 I62 34-155 3598 70-13n106 70-13099 70-t 30101 70-130

20.020.020.om.020.020020.020.o20.o20.020_02004 0 020.o20.020_o2002 0 020.0zDO20054050.050.050.0

252525

255025

25

2525

5025252525

Blant {7031602€LKl I

Prepared & Analli?ed: 27-Mar07

1,1,z-Tridrbrofiffuoroethane (Freon 1 13)

Acrylor trile

BonzenegromoberEene

BronEdrloMn€thane

Brcrnodicfiloromehane

Bmmoform

Brornomehan€

2€utarEr'€ (MEK)

n€urybenzen€

s€c-guvb€nzene

lsrl-ButylborEene

C€rbd| disifide

Cadon bbachlodde

Cl{orobenzone

ChloD€than€

Chlorobrm

Chloromehane

24hlorctolu€ne

4-ChbrobluerE

1.2-Dibrcrm€d oopropane

Dib.onochbrornethane

1 "z{]ibromo€thane (EDB)

BRL

8RL

BRL

BRL

ARL

BRL

8RL

ARL

BRL

8RL

BRL

BRLgRL

8RL

8RL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

8RL

1 02001 .01 .01_01_01_01_02.O10_01 .01 . Q

1 05_01_01.02.O1 .02.O1 .01-02.01 .01.0

!g/kg wet

!g/kg wet

pg/kg welpgr'kg wet

Ug/kg wet

pg/kq wet

pgr'kg wetpgKg wel

wkg wel

ug/kg wel

pg.4g r4€l

pg/kg wet

!g/kg wet

pg/kg wet

lgkg wel

t g/Kg wel

Fgy'kg welpqkS w€l

lrgkg r €lpEr(g wet

!gl(g w€t

Ug/kg v/st

Ig,/kg wet

t g/kg wel

Thb labarulory Hpon h noa wld withottr an aatho.iae.! siEnatuR o1 the cover page .' Reportable D€rection Limit BRL = Below ReDortins Limit Page 85 of l14

Page 557: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtile Orgaric Compounds - Quality Control

Anallte(s) Flag .R-DLSpike

Level

SourceRe$rlt %REC

%RECLimits

RPD

LimitRPD

Batch 7(Lr 1502 - SW846 5030 Soil (bign kv€l)

Bl.nk r76l6O2€LK1l

PrepaEd & An€AEed: 27-ti,tar.07

Dibromornethane

1,2-Oid orcb€izene

1,3-D-hlorob€oz6n€'l ,4-Did|hrob€rEene

Dichlo.odifl uo.om€than€ (Fr€onl2)

1 ,1 Oichbro€thane

1 ,Oichloro€thaneI ,1 Oichlorc€th€n€

ci6-1,2-Did oroellteno

tans- 1 ,2.olafibrc€th€n€| z-Dichloropropsne

t,3-Dhhbroprcpane

2,2-Ditrlorogmpane

1,1{Hrbropropene

cis-1,3Jichloroprcpeoe

tr8ns,1,3-Dihloropop€fl €

Elhylbenzene

H€x€chlo.obutadiene

2,tlexar|one (MBK)

lsopopylbenzene

4Jsopmpyltolu€ne

Methyl ted-buty' €uler

+ld€hyl-2+€nlanons (M|aK)

M€thylens d|iornle

Naphth€len€

Slyrene

1,1, 1,2-Tstrdchloroethane

l. 1,2,2-T€trachloroethane

Tetrachlcao€th€ne

Toli,,ene

1,2,+Trichbrobenzene

I,2,4-T.id orobenzsE

1 ,I ,l -T,ichbroehane

1,1.z-TtiJtlorethane

Trichloroollsle

Trk] orolluo|om€U|an€ (Freon 1 'l )'1 :3Td$brop|open€

1,2.,r-Tdmothylb€.E€ne

l,3,STrinEthylbenzene

Vlnyl.filo|Uo

m.Fxyl€ne

o-Xybtro

Tedlydrofuran

EthM elh€t

T€rt-a||y' m€hyl ether

Ethyl lo.l+utyl etl|er

Dl-lsog.opyl €t'€r

Terl-But4rol / butyl alcohol

1,+Dlxan€

Smr{iab : 4-AtonmfluotolFJnzeneSwrogale: TohEne4SSurroga63: l,zOichloto€han€4 4

BRL

SRL

BRL

8RL

BRL

BRI.

SRL

BRL

ARL

BRI-

BRL

BRL

BRLgRL

BRL

BRL

BRL

BRI.

BRL

ARL

BRL

BRL

BRL

BRI

8RL

BRL

BRL

BRL

BRL

ARL

BRT

BRL

8FL

BRL

BRL

SRL

BRL

BRL

BRL

ARL

aRf

8RL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

ARL

30.129.528.4

30.030.030.o

70-1&70-1n70-130

pdkS v{et 1.0pgkswet 1,0

t gI€ w€t 1.0p€/kg w€l 1.0

Ug/kgw€l 2.0

Ug/tqw€l 1.0

Pg/kg wel 1.0

lgrSYr€l 1.0

ldkg vJ€t 1.0

lgkg rY€t 1-0

!S/kS s/et 1-0

U€r'kg wet 1.0

!g/kg wet 1.0

Fg/kg wet 1_0

!q/l€|t,€t 1.0yg/kg w€l 1.0

!g/kg wet 1.0pdkg tv€t 1.0

Pg,kgw€l 10.0

ldkgw€r 1.0

!Sr(g Yret 1.0

tdkg w€t t.O

|rg qwet 10.0

tdkS wel 10.0

1,g1,k9 wet 1.0

Fgftg w€l 10

ldkgwel 1.0pSrkS ly€t 1.0pgftgw€l 1.0pdkg vi€l 1.0

Ug,/kS rvel 1.0pdkg Y,/el L0

!S/Fg rvet 1.0

IgL/kg wet 1.0

lgr'kg f,'et '1.0

Udkg vret 1-0pg/t€wet 1.0pg/kgwel 1.0pgfl(gwer 1.0

lgukg u/el 1.0pgkg*€t 1.0

ldkS t€t 2.Opg/tg \r€t 1.0

PgL/kg w€r 10.0

UdkSwet 1.0

lgLitg vrel 1.0

Ugi@w€t 1.0

l|grkg wet 1.0

Ig/kg wet '10.0

pg/|(rg wet m.0

Ugl(g ',r,€l

ldkg w€r

Hgr'kg w€l

1@9896

fhis latoraloA Epotl it Ed rclitl ,ritlrou aa aathorized tig&4utft otr lhe cover page.

' Repo.table Dekction Li.nit BRL = Below Rcpdiry Linit Page 86 of 124

Page 558: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qualiay Control

%RECAnalyr(s) Resuir Flag Uni6 *RDL Lcvel Resutt %RLC Limi(s RpD Limir

Batch ?031602 - SwE46 5030 Soll (high tev€t)

Spike Source RPD

Bl.nk 17fi!1602€LKlr

PleparEd & Anallrz€d: 27-Mar47

Su ttogde : Oilb ronbfl u orom elh ane

LCS {?0: 602€sl l

Pr€pa.6d & Analfzed: 27-Mar-07

1 ,1 ,2-Tric$lorolrifuoroethane {Freon t J 3)

Benzene

Bronrb€nz€n€gromochlorometrane

Eaomodicibrom€Slan€

Bromoform

Ercmomehane

2Autanon€ (MEK)

n€uvbenzene

sec-gulylbenzene

iert4utylb€nzen€

C€.bon disulfide

Carbon blrachbdde

Chlorob€nzen€

Chloro€thEne

Chlo.ofom

Chlomlfiethane

24hlorololuen€

4Chbrotoluene

1,2-[rlbromo.3<l orcpropane

Dibrornodbrornethane

I 2-Dibro.noelhane (EDB)

Dibrsnomehane

l.2Jidlorobenz€ne

l,3oiahlotrobenzeno

1 ,4oichloroberEeneDid orodifl uoron€thane (Fr€on1 2)

I ,l Oichlo.oethane'l,zolchhoelhane

1 .1 Oichloro€thsn€

cis-l ,-Di$loroodt6ne

t"ans-l,2oichbroethene

1 Joichloroprop€ne'1 .3oktlbopropane

2,2oicnhopropan€

1 ,1 .Dbhb@prop€ne

ci+1 ,lDidrldoorop€nelrEns-l,lDidrloroFopene

EthMb€nzene

H€x4hlorobutadiene

z-H€xanon€ (MBK)

fsopr@I4Denz€4e

+lsopropyllolusn€

Methyl iart{uv eiher

4-l €hyl-2-penlrnons (MIBK)

MethMei6 dlbrijo

N+hfral€rE

2 9 0

22.213 .420.423.O

22.123.024.O22.415 .120.121.622.723.119.723.420.021.421.123.422.421 .822_923.421 .S23.823.923.O23.A21.121_420.522.621.122.722.618.922.521.922.422922.31 4 021_722.O21.519,020-022.0

Lig/kg wet

p!|/xg wetpgL/kg f,,et

t/EKg wetpgkg wet

Ug/kg wet

ug/Kg wet

pg/Kg wet

!g/kg wet

Fg/'(g wet

lrg/kg wst

!g/kg wet

fgftg wetpg/kg wetpg/tg wet

!g/kg wet

!g/kg wet

!g/kg w€t

!g/kg wet

lig/kg wet

!g/xg wet

tig/kg wet

!g/kq wel

!g/kg wet

!g/kg wet

!g/kg wet

lrg/Kg wet

!g/kg wet

ttEkg wet

lgr'kg wet

ugirc w€tIg/kg wet

lgLftg wetpgLi kg wet

UEkS,,et

lgL/kg wet

Ugkg wet

pgkg wet

!g/kg wst

l.r9r(9 wet

Lig/kg wer

lgr'kg w€t

lgrkg wet

lEkg wetpg4(g w€l

Fgy'kg wel

trdkg wel

lSftS w€t

Fgftg wet

Pg/tq wet

30.0

2DD20.020_020.020_o20.020.020.o20-02 0 020_020.o2 0 020.020020.o2 0 020.o20020020020.020.020.02 0 02 0 020.020-020.020.D20.o20.02 0 020-020.020.020.020.020-020020.020.020.020.020.020.o20.020.o20.0

97 70-t 30

111 t'-130

67 1. f7 -175

104 70-130

115 70-130

120 70-130

1r0 70-130

1r5 /0-130

120 70-130

114 55.3,136

76 38.8-142

100 70-130

108 70-1K

114 70-130

116 70-130

98 70,130

117 70,130

100 55.3-130

109 70,130

106 70-1gl

111 70-130't'14 70-130

109 70-130

114 64.7-139

117 70-130

110 70-130

119 70-130

120 70-130

115 70-130

119 34 4-167

106 70-130

107 7G130

102 70-130

113 70-130

106 70-130

114 70-130

113 70-130

94 70-130

112 70-130

1r0 70-130

112 70-'130'r 14 70-130

112 G0_7-r40

70 70-130'tD8 7D-13D

110 70-130

108 70-'t 30

95 46.1-145

100 70-130

110 70.'t30

This labonrory rcpod it not valid ruithout an authon "A

fiSnotarc od the co'e, paSe.

+ Reporrable Detection Limit BRL = Belou Reporting Liftn Page Sl of 124

Page 559: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgaric Compouods - Qusllty Cooarol

AnalyteG) Resutt Ftas Unrts *RDLSpikeItvel

%RECLimits RPD

RPD

LimitSource

Re6uk %REC

Brtch 7031602 - SW845 5m0 Soil (high level)

LCS t7031602€St I

PrepBred & Analfz€d: 27Jt ar-07

n+opylbenz€n€

Slyrene

1 ,1 ,1 ,2-T€tachldoethane

| , | ,2,2-Tetrachloroeth6n€Tetrad{oroehene

1 ,2,3-Trichbrobenz€n€1 2,4-Tricilorobenzene

1 ,1 ,1-Trid!lorc€han€| . | ,2-Tdchlorelh€neTdchloro€th€ne

Tricilorolluorom€fEne (Freon 1 1)

i l,STnchbIopmpaneI ,2,+Trim€fiyib€.Eenel,3,tTrirnetnyt'b€nzen€

m,p-Xylene

cXYlene

T€bEhydrofuran

€thyt eher

Tert-amyl m€6yi ethe.

Et'ly' ierl-buv eth6r

Di-isoptopyl €th€r

Tert-gutand / butyl alcohol

1,4-Dioxane

Su.rog€l€: al-8rc.r|oduor(6€nzeneSufiogate: Toluene4SS udog ate : 1, 2-DM lo t@lh ane 4 1S unogate : Dib rofi D lfu ordi eth ane

LCS Ouo Oo3l602-A50t)

Prepa(ed & AnalFed: 27-Llar-07

1,'1,2-Tri{:r{orotrifuoroothane (Freon I 13)

Acrylonftrile

BerEerEgrqrrobenzene

Bromochbront€lhan€

Bromodidrbmrnethane

Iroftrclorm

Bronrom€lh€ne

2€'lbFone {MEK)n€utylberE€ne

E6c-&It!4benzen6

red€ltylbonz€ne

C€toar disulfde

Carboh tstEchbdde

Cuoroben:€ne

Chloroethd|e

Chlomform

Chlorcm€lhane

2{hlomtoluen6

4-Chlo'roiolueie

19.325.2

22.520-021.O72.522.520_323-'l

20.625.122.723_521.246.624.120.421.3?0.321.719.9

15730.728.727.828.9

20.511.710.321.221-8m.2

22.522.O14,4r8.115.720.417.618.121.318 .319.9'19.5

20.621_1

20.020.o20.020.020.0m.0m.020.o20.020-020.0m.020.020.020.020.o40.020.020.020.020.0m.o20.02002m30.t30.0m.030.0

20.o20.o20.o20.020.020.020.020.020.020.020.020.020.020.o20.020-020.020.020.020.o20-o

pdkS vrel

ugfl(g wetpg/ko wet

Fg/kg wel

Pqkg rv€t

lrgts vrel

!gl(g 'rv6t

lgr'kg v/st

Ug/kg wel

Yqtg w€lgglkg \rqt

ldkS wet

|,9r'k0 wetp€y'kg w6l

Idkg rvel

Fglkg wei

ldks rYet

!94(g wet

Pg/kg w€I

lgvkg wel

llgtkg wet

!g'l€ "!€t

Ugiko wetpgrtg wet

Yglg rv€lpdks Yrerug/kg w€tlgfllg wetpgr'kg wol

pdkS wet

USftS w€t

Pg/kg Y,€tpgr'kg wel

Yslkg w€l

Pgr'kg r€l

!g/kg $/et

lgLftg wet

Pg/kg '/et

Pglg w€tpdks Yret

lgrkg wet

Ig/kg wetaRs Igkg w6t

pg*g wel

PgAg wel

ldkg rwt

ldkg,r,et$r'kg wet

!g/kg wet

USftg wel

96 70.130126 7G130118 70-130112 70-130100 70-130r05 70-130112 7G.130112 7G1 30102 70-t3t)118 70-130112 70-130103 56.&140126 70-130114 7Gt30t18 70-l3t)to6 70-130tt6 7G.130120 7G130102 70-130rrxi 65.3-130102 70-130lm 70-130100 7G13098 70-13098 34-1 55102 7G13099 7$til93 70-lg96 70-tg)

102 7G.1 30 g

8 1-77-175 11s6 70-130 I106 70-130 It09 70-130 10101 70-130 I108 7G130 6112 70-t30 7110 55_3-136 47:L 8.8-142 590 70-1$ 11sB 7Gt3o 10102 7Gr30 1l88 70-t30 2790 7trtfi) I106 7G.130 t092 55.1130 I100 7Gi30 I98 7t!130 0103 7Gt3o 13106 7G130 f

25502525252525

5050

25

252550252525

Thb bhrrdoty repatt is not ,alid wirtod zn curtorizd slgdalarc oE thz cowr pfuge .

' RePo.tablc D€tection Linit BRL = Bclow Reportiog Limir Poge 88 of | 24

Page 560: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volaaile Orgrnic Compounds - Quality Control

Atrrllt4s) 'RDLUnitsFlagResultSpike

I-evel Result % REC%RECLimns

RPDLimitRPD

B{rch 7031502 - sw846 50J0 sott thigh tfvet)

lcs t uo fictt6it2€sotIPr€parcd & Amtyzed: 27,Mar-071,2-Dibromo3{hlo.opropan€Dibromochlorom€thane'1,2-Dbmmoethan6 (EDB)Oibaomonr€thans1 ,2-Dichlo'robe&eneI ,3-Oi:hfrnobeflzen€1 l-Dlchlorob€nzsh€

(F eonl2)

203

21.5

2 1 . 8

20.4

21.4

21_5

20.8

2 1 . 8

19.4

1 8 . 5

r8.4

20.2

18.7

20.6

2 1 . 3

1 7 2

20.8

20.4

2 0 7

206

1 9 . 8

13.2

19.E

20.0

19.8'17.7

'17 2

1S_8'18.0

225

2 1 . 6

21.6

1 8 . 5

19.6

2 i 1

2 0 1

18.4

2 1 . 6

2 0 6

18.S

20.6

2 t . 2

19.6

42_4

21.5

2 1 . 9

19.7

1 9 4

201

18_4

198

20.o20.020.o20.o20,020-o20.o20020.020.o20.020.020_o20.02 0 020.020_0200i {o20.o20.020.020.o20.o20.020.020.020.020020.o20.020.020-oz).020020020.020020.020.o20.020.020_o20.040.020.o20.o20.020.020020_0200

Lrg/kg wet

lrg/kg wet

Pg/kg wel

lgr'kg wer

!!y'kg wel

Pgftg rv€t

ldks wet

lgr'kg wet

!g/kg wst

rc/kg wet

pg/kg wet

Pg/kg wetygkg wel

!g/kg wetggkg w€lpgr'kg wet

!g't(g wet

lSftS YJ€t

!g/kg wetpg,,kg $/et

lgr'kg wetOcl Ug/kg wet

pg/kg wet

ug/kg wel

tig/k0 wet

ug/kg wel

lJglkg wel

lrg/kg w€lpg/kg wet

lgikg wel

tis/kg w€l

ldks vr€t

lgr'kg wet

!g/kg \ret

Udkg wet

Lig/kg wet

!gL4<g wet

lgr'kg wet

ug/kg wet

Ugr'kg wst

t gu4€ wet

ttg/kg wel

lig/kg wel

!g/kg wel

!g/kg w€l

UgAo wel

rcfig welpgrkg wel

ug!4(g w€l

rcrkg $/el

Fg{(g wel

!g (g w€l

102 70-130108 64.7-139109 7n-130'toz 70.130107 70-130fo8 70-130104 70-130109 34.4-16797 70n3092 70-130s2 70-130'101 70,130

70-130103 70-130106 70-13086 7G1301M 7G130102 70-130104 70-130103 70-13099 60.7-14066 70-13099 70-130100 70-13099 70-13088 46.1-14586 7G130ss 70-13090 70.130112 70-130108 70-130108 70,13092 70-13098 70-130100 70-130100 70-13092 70-130108 70.130103 70.13094 56_e-140120 70.130103 70-130106 70-13098 70-130106 70-130110 7G130110 70-13098 65.3-13097 70-130100 70-13092 70-130s9 70-130

7 2 5

5 5 0

7 2 5

4 2 5

1 1 2 5

1 1 2 51 0 2 5

9 5 0

9 2 5

15 25't0 25

1 1 2 5

12 25

10 25

6 2 5

s 2 5

r 2 5

8 2 5

7 2 5

1D 25

12 50

6 2 5

9 2 5

1 0 2 5g 2 5

E 5 0

15 25

1 1 2 5

6 2 5

1 2 2 5

9 2 5

4 2 5

8 2 5

7 2 5

1 1 2 5

1 1 2 5

10 25

7 2 5

8 2 5

s 5 0

5 2 5

10 25

t 1 2 5

8 2 5

9 2 5

9 2 5

8 2 5

8 5 0

s 2 5

8 2 5

8 2 5

1 2 5

1 ,l -Dichloroethane

| ,2-Oit or*thane

| ,1{)ii$loroeflene

cis. l,2.oichloro€thene

t'ans-1,2,Dicl o,?ethene

I ,2{ichlorop.opane1 ,3Oknbropropene

2,2Oictloropr@ane

I .l Oichloroprop€ne

d91,3-Dicf rloroprop€ne

t'ans-1.lDidrloropropene

Eh]dbsnzere

Hexd orobuladiene

z-Hexanone (MBK)

lsopropylb€nzen€

+bopropyllolugne

Mehyl tert.b'rvl €8ler

+Methyl2+entanone (M|BK)

Meihy'ene chbdde

Naptrthal€ne

n+ropylbenzene

Styrene'l ,1 ,1 .2.TetachloroettEn€1,1.2,2-T€t'€chloroethane

Tshsct oroetiene

Toluen6

1 .2,STricfiloroben?ene| ,2,+T.iilorot€EeneI,|,l-Tricttbro€lflan€

| , | ,2-Tri{filorcEtlraneTdi{oroethgne

Tri*bmnuoronEfune (Freon 1 1 )l,2,aTridftroplopane

1,z,+Trimetay'b€rEene

I ,3,+TdmethylbenzeneVinyl d onde

m.P-Xylene

o-Xyl€ne

T€ffahydrofr&n

Elhyl€ther

T6rl-€myl methyl €lher

Ethyl b.t-bdyl ether

Dlloopropyl ether

T€rl€ubnol / fu tyl alcohol

This lzbontory rcpod is ,at ialid *irtoat z^ aarlrodzed signttttrc on the cavu paEe

' Reportabl€ Detection Limit BRL = Below ReDortine Limir Page 89 of 124

Page 561: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Vohtlle Orgrtrlc Compounds - Quality Cotrtrol

Analiqs) Result Flag Units *RDLSpikeLevel

Sourc€

R€sult

RPDLimit

%REC%REC Limi6 RPD

B|ich 7m1502 - SW846 5030 Soil (htgh level)

LCS Duo flft'lm2€SDll

Pr€par€d & Anal!.zod: 27-lrar-o7

1.4{)ioxs|e

S/j7'oga te : 4-Srond@tdenzetES,'toga|€: Tduene4SSlJi'ogate: l,2alchbroethane44Sunoge/€ : Dibtonbfl uotgneth erc

ts6&.3fr.226.928.9

2630.030.o30.o30.o

m.0m.020.020.020.030_o30.030_o30.0

20.020.o20_020.om.030.030.030.ow.o

98

101t0190

106104100'r06

tou1011048893

lgflq w€t

Ugy'tg vretru/kg wet!g € wetpgr'kg w€l

LrgVS dry

ldl(g dry

rdkS dry

t dl€ dry

ldkg dryyqkg drypS/tS dryUglq dryldkS dry

t gllg dry

lryxo dry

lsfts dry

rdrs dry

FdkS dry

udks dryUdlq dryt'dks dryIgkg dry

BRTBRI.BRLBRLARL

BRL

BRL

BRL

SRL

BRL

3+r 5570-13070-13070-13070-1N

7t}-t307Gt307G13070-13070-13070-1fi70-tu7L1nTEtm

70-1307G1307G13070-13070-13070-1U70-19)70-13070-tfi

25

llairlr Soik6 ft03t m2.Msll l

Prcpar€d & Analfzed: 27-Mer47

Senzene

Chlorobenz€ne

1 ,1 €ichbro€thene

Toluen€

Trichloroetlt€ne

Suflogata : ttBtonpfluor$enzoneSutogata: ToltEne4SS','rcgale : 1,2 Oichlotdtane4lS u mgaE : D ib rcmofu rorcneth e rE

P.6par€d & Analfzed: 27-Mar{7

Benzen€

Chlorobenzsn€

I ,l-DichbroetheneTolu€ne

Ttid{oroeth€fi€

Sunogde: 4-ErfilonuotdenzeneS|Jl7ogate: foluene4tSu/ftgete : l,2aichloroethane44Suntga.'!- : DibtoflmfllrE.onelhane

Sdrrc.: SA59O:I9-ll

21.?20.920.1

21.230431.226.127.8

lrrtix Solks Oup t7031m2{#tot} Sou.6: SAS| &St I

19.4t9.317.7rg.419.730.331.426.127.8

s7

8a97

s8,01105a793

8

1 3

I

3030303030

Th& ldbrelarf ,Epotr b t ot fiIU wilhor,t on aulr4fiud sigaaarc ot the cowt ptgc.

* Repo.tablc Dct€ttion Limit BRL= B€low Reporting Linil Page 90 of 124

Page 562: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Extractable Petroleum Hydrocarbons - euality Control

SpikeLeveJ

Source

Result

%RTCLi')ils

RPDLi i t

And).teG)

Brtch 703t160 - SWE46 3510C

Elenk O0:ll160-E|LKl I

PrBpared: 2l -t!,lar{7 Anatil.zed: 22,Ma(07

Gasofm

Fuel Oil l?

Fu€lOi l#4

FuelOi l#6

Mqbr Oil

Aliatkrfl Fuel

Unbentfi€d

Othor Oil

Total Petroleom Hydrocabons

CgC36 Alphalic Hyd.oc€rbons

Sr/'|'ogal€j 1.Chloloodadecane

LCS a7clfi60€.st I

Pr€pared: 2 f .lvfar{7 Anatyzed: 22-Mat47

C€-C36 Aliphatic Hydrocarbons

S unqate : l -Ch lotaocl a de c a n €

Brtcn 7031281 - SW846 3ss0B

Bl.nk fl0312€1€LKil

Pt€Eaied: n+Itar47 tu tatyzed: 23-tvlaro7

G6solln€

FuelOi l#2

FuelOl l#4

FuelOi l#6

Molor Oil

Unid€ntitu

ehe. Oil

Total Peuotsrm Hydrcsrbons

ClC36 Allphatic Hydrocarbonsgmogate : 1 -Cht oroo dad e c a ne

LCS ftGI2St +rst I

Prepared: 22-{\,f ar-O7 Anat]fzed: 234tat4i

C€€36 Aliphatjc Hydrocarbons

Su,rogate: | 4hlo@o€tadecane

R}D9/,REC

8RL

BRL

BRL

BRL

BRf

BRL

ARL

BRL

BRL

BRI.

0.04m

1 . 4

0 0520

ARL

ARL

BRL

BRL

BRL

BRL

BRL

aRt

8RL

BRL

2.93

83.3

i .72

BRI

BRL

BRL

BRL

BRL

aRl

aRrARL

ARL

ARL

2.53

Sou.c€: SA595ll{l

91.4

86 40-140

100 60-120

104 60-120

mg/l 0_05msn

hgl(g w€t 13 3tng/kg wet 13-3

hg/kg'.!et 13.3

hg/kg wet 13.3

hg/kg wet 13.3

hg/kg wel 13.3

lngftgw€l 13.3

hglkgwel 13.3

mgri(g wel 13.3

rng/kg wel 13.3

hg/kg wet

nE/kg wel 13.3

tngftg wel

mgftg dry 30.3

mSI(S dry 30 3

mg/kg dry 3O.3

mg/kg dry 30.3

mg&S dry 30 3

ftg,ftg dry 30-3

mdkSdry 30.3

hg/kg dry 30.3

mgl(g dry 30.3

mg/kg dry 30-3

mg/kg dry

mSn(g dry 15.4

mg/l

mg/l

mgr

nE/l

lngd

mgn

mgl

nE4

m9/l

mg/l

mgn

0.050-050050.050_050.050.050.050.050.05

0.0500

1 . 4 0

o.o500

333

93.33.33

88 40-140

69 60-120112 ffi-120

Duollcat l703t28loupit Source: S45O511.01

Pr€pared: 22-t\,{aro7 Anatfzed: 23-Mar{7

Gasolin€

Fu€lOil f2FuelOil#4Fu€lOiltreMobr oil

Unidentifi€dOtt!€r OllTo{al Peht€um Hydroc€ruonsC9-C36 Aliphatc MrocarbonsSun<tgete: t +liotcf,daclecane

mat |I spitr aT0:1t281{st)

ARL

ARL

8RL

BRL

8RL

ARL

BRL

BRL

BRL

BRL

50505050505050505050

3.84 77 4+140

Pr€pared: ?2-lrar47 Analyzed: 23-Mar47C$(::l6 Aliphaltc Hydrocaftons 85BRL1 m

Thk labordory rcporl'B ^or valid without M aaahorizd signoture on the cover page.

* Reporlable Detection Limit BRI- = Below R€portinE Limit Page 9t of 124

Page 563: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Extractable Pearoleum Hydrocrrboos - Qurlity Control

Anal't{s) Result Flag UEits RPD*RNLSpikeIrvel

Source

Result o/oREC%RECLimits

RPDLimi(

Brl.h 703l2El - SW846 35508

a$x Spit. OO3t2Ot.ltsll

C€-C36 Aliphatic Hydacatons

Sunogate: 1 -C'rll(,'oodad€cane

Sour€e: SA595ll{l

Prepef€d: 22{tiar-07 Analyzed: ii3-Mat47

Sufiogale : | -Chlomocladecatg 3.92 101

fiatrix Solke Ouo t7031231-lrsoi) SorrE€: SASSSiI{tl

BRL

BRL

BRL

ARL

BRL

aRl.

BRL

ARL

BRL

BRL

3.26

Sourc6: SA5D455{3

86-9

3.14

mdkg dry

ntg*gdry 15-ErngftS dry

mgdqw€t 13-3mg^g w€lt 13-3mg/kgw€t 13.3.ngnqwel 13.3mgr'kgwet 13-3n{rrgw€t 13.3.r'g (gw€t 13.3mSlkS e/et 13.3ft$kgc.€t 13.3oE/kgwel 13.3nE/t(g w€l

mg/tgwet l3-3ntgftg wet

rEr'kgdry 28.5rEn<g d.y 28_5mg/kg dry 28.5rnSftS dry 2A.5nEikg dry 2A.5nrS/kgdry 28.5nE/kg dry 28.5mg/kg dry A.5nEI(S dry 28.5nE/kg dfy 28.5r'g^g dry

mg^Sdry 14.3nE/kg dry

ntgikg dry 14.4firg/t(g dry

41t140

ff)-150

4{J-110

4Ir14I)

m-lm@-1m

1+l4A

5{r15040-tlo

5Gi5o 154Irt4)

89.6

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

SRL

SRL

261

1@.

3.U

3.87

111

3.95

3.3

93.33.33

BRL

Prepared: 22-iiar{7 Analyzed: 2}t-tar-07

C9436 Af phatic Hyd.ocarbons

Suftqate : l -ChloroodEdecane

Brtct 7031!84 - SW816 3545A

Blank aZUll2MAL|(1)

PrepsrBd: 22-lrar{7 An6lrz€d: 26Mar-07

Gasollne

Fud rH #2

Fuel Oil #4

Fu€l Oil #6

Molor Oil

Unbenllfied

Othe. Oil

Tohl Petoleum tiydrocarbqE

C$C3€ Alphetic Hydrocarbons

S unogab: 1 4hloroocTadecene

LCS f703r2t4€Sl )

Preparcd: 22-lrad7 Analyzed: 26-Mar-O7

C$C36 Ailphatic t|ydrocsrbons

s u nog 4e : t 4 hl orc&ade cane

Gasolii€Fu€l Oil#2Fuel Oil {4FuelOll#6Motor Ol

Unidendf,€dOrher OlTotal Petol€um HydaocarbonsC9436 Allphalb MrocarbonsSu/rDgais: t-Cr orooajsdocare

lrrtrlx Sotk t70gt 2&Gfist )

81 3{)

78

10sf i5

Ouollcde l7O3l284rUPl I SdrrE€: SA5gil55{3Ptepdrd: ?2{4ar{7 Analyredr 26-Ms{7

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

SRL

8RL

5050505t)5050505050

3.57

1003.50

1013.61

9 l

Prepar€d: 22-irer47 Anallzedt 26-ttar47

C$'C38 Afphalic Hydrorabons 73.8

Sunoga|jj 14 o/oadadecano 3.06

tlatrlx Solk. Oulr fl0t1284. $)tl Sd|r{s: S459455{t

Prepar€di Z?-lrar-07 Anall|zed: 2&.Mer{7

BRT

SRL

74E5

308694

ThJJ lafuntory tqod ls ,td adld x,ithod on .artodtd sWMt oa the cayer pqa.

+ ReFortsble Det€ction Lisir BRL = Betow R€portine Limit Psge 92 of 124

Page 564: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semiyolatile Organic Compounds by GC - eualiq/ Conarol

Spike

[,erel

Source

R€sul(

%RECLimiLs

RPD

Lirni tAnalyt4s) %RDC

B'.ct 7011270 , SW846 i5l(rc

Blenk 47031270€LKll

Prep€red I Anal}.zed: 22-MaF07

Aldin

a€Flc

b€Hc

dSHC

gAHC (Lindanej

Chlordan€

4,{.DDo (p,p')

4,4-0oE (p,p )4,4{n)T (p,p')

Dielddn

E rdoGulfan I

Erdosullan ll

Endosultan Sutfsie

Endrin

EMdn Aldehydo

Heptedrlor

H€Orachlor Epoxide

Toxapfien€

a4filordsfle

gFchlordane

Endrin Ketrn€

S u ttog8{e : 1, 44 B4tckfl u o to b i p he n yl ( S 4Sutlog'/e: Decachlotobiphenyt ( Sl

LCS Oclt270€a1)

P.6par€d & Anaryzed: 22-Mar-07

Atdtitl

a€HC

baHc

d€Hc

g€HC (Lindens)

4,4{DD (p,p)

4,4-DDE (p.p')

a,+DDT (p.C)Disldrin

Endosufdl I

Endosdfan ll

Erdcdfan Sufble

Endiin

Endfi Ald€Me

Hept dlor

MedDrryd'Jor

Heptadlor Epoxid€

a-Chlodane

g4 odan€

Endrin Kebn€

Surqafe: 1,'11)B4clafl uorobiphenyt (54Sunogate : Dec8f.Jl t oro bi ph e nt l ( S t)

LCS Du! f7031270€SDt l

Pr€psred & Analyzed: 22-Mar{7

Aldrin

a€HC

ARL

BRL

ARL

BRLgRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

8RL

BRL

BRL

0 0 1 7 7o 0190

0 0171

0-0137

0.0126

0.0083

0_0143

0 0 1 4 8

0.0152

0.0187

0 0 1 6 0

0.0154

0.0163

0.0r46

0.0167

0.0192

0.0164

o.0183

0.0166

0.0151

0.0129

0.0168

o_o142o.0163

0.0171

0.0'r32

FEI

u9/lItgll!srpErps4

!s4pdl

lg/lug/l|lEl

!9nljg/l

tstlFSnpEt

tglps4

Lj$4

ps/pg/l

!gn

!EluEl

lgll

!gn

ItElpgn

vgtl

!gr

!sn!s4!srljdl

trglpg/l

lrSll

!gn

ugll

ttgt

tgll

ltsn

9S4

Itgtl

tlg/twl

wlpg4

3G1frwl50

40-140

40-140

40-140

4G.140.{o-140

40.140

40.140

4G140

4G140

40-140

4G140

40-140

40-140

40-140

40-r40

40-140

4G140

40-140

40-14t)

40-r40

40-141)40-14.0

40-140

40-140

0.01000 01000.01000.01000.01000.05000-01000.01000.01000 01000 01000.01000.01000.01000_01000-01000.01000.01000 05000.0't000.01000 0100

o.om00.om0

0.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000_0100 0.02000.0100 0.02000.0100 0.02000_0100 0.02000.0100 0_02000.0100 0.02000.0100 0_02000.0100 0 02000_0100 0.02000 0100 0 02000.0't00 0,02000.0100 0.02000-0100 0.02000.0100 0.02000.0100 0_02000.0100 0.0200

0.omo0.0m0

0.0100 0.02000.0100 0.0200

88

866863427274

948077a2

84s6E292u

64

84

7182

88 2020

Thir laboruory report is ,at valrl tlilhou! sn ^uthodaed sigrau.rc oa th. cover page.

'Reportabie Detection Limit BRL= Betow Reponing Limit Page 93 of 124

Page 565: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgaric Compounds by GC - Quslity Cotrtrot

Brtch 7031270 - sw846 3510c

LCS Dup ft031?0€SDll

Prepaed & Analfzed: 22-Mar-O7

b€Hc

d€Hc

graHc (Undane)

a,+DOD (p,p')

4.4ODE (p,p')

aJJDr (p,C)

Dieldnn

End6ulhn I

EndosulfEn ll

E dosuLan Suffate

Endrin

Enddn Adehyds

tieptad or

Heptad)lor Epoxide

a4hbdaneg€hlo.dane

Endin Kelon€

SunaC8/e: 4,+D&Mf, uotobtphenyt (StSvmgate: Decact otohipl@nyt (St)

8 cl7031271- SWE46 3510C

Bl.nk r?031271€LKt)

Prepa.€d: 22-l\rar-07 Analyz€d: 23Mar-07

rcB 10.t6

PCB 1?21

PCB1232

PCB 1242

PCB 124€

rcB 1254

PCB 126t)

PCB 1262

PCB 1268

S urog de : 4, +D Boclaf, @ft hiphe nyt ( S 4S mogata : Oarachlo ro hl phe n yl ( SO

LCS t700127t3{trl

Preparedi 22-f!fer{7 Anatyzeat: 2€.Iiy'.ar4l

PCg 1016

PCg 1260

Sqmgate: 4,l-DBof€,fi,0,lotiphenyt (St)Sult]ogate : De.',chlo'ohipl@nl 64

LCS Dup flfti12?1€SDll

Pr€pared: 22-lrar-07 Anal}.zed: zlt ar-07PCB 1016PCB 1260

Sunqate: 4,+OBebtuotobhtEt yt (Sr)Suno8ai€ : De(achhtfiiplEnyl (Sq

Batcb ?03127{ - SW8,t6 3s508

Ehnk lm312ra{Lxt I

Prepared & Anab,zedj 22-lrar47

PCg to16

[email protected]_01650.011€0.01430.0194.0.0t610_o1740-0't640.01,$0.01250.0t650.0152o.0164

BRL

ARL

BRL

BRL

BRI-

BRL

8RL

BRL

BRL

o.1700.21o

2.65

2_76

0.170Q-2tA

2.41

3_O1

0.1700.230

pdl

Itdlus/l!dl|lglpgrl

yg/l

psr!dl!gnt,€/lvgllpdl

rcnt d l

tgtl

l,gIpc4rcnrrdl

[email protected] 01000.01000_0too0.01000 01000.01000.01000.0too

Spikc

kvel

0-02m0.02000.02000.02000.0200o-o2m0.02000.04x)o.02(x)0.0200o,02m0.02000.02m0.m000_02000.02m0.02000.02000.o2(n0.0200

Source RPDLimit

64 40-14042 4G'14069 ,lGl.lt)

76 40-14075 4On,$a2 10-140u 4v14076 40-140a 40-14074 1o-14oE2 {014097 1{tr,r0El ,lt!140

a7 40-140a2 4o-14o71 40-14062 &-1448:l 4G14076 40-14082 40-140

o

1

r45

I

I

2

1

I

I

2

2020m202020m202020mm202020mm20

td lttgllus4pdl

t91lu$psnug4pdl

usn|ldl

02000.2000.2000.2m0-2m0_2000.200o.2000.200

ustlTgIwl$sn

0.200o.2@

udl o-20opsn 0.200F9lpcl

85 3)-150105 tu|fi

fm 4o-14/lll0 rl{!140

M fu | f lr05 tu150

't(x 4G1401m 4$t4085 tulffi115 n-lso

a.m0,2u)

2.502.500-zn02M

2.fi2.500.2000.200

20m

gRL pglkg i€l 28.6

Thb lab?abry ,"ipo.t k '@,tvalu wAhol4 o attahorizd Eig,td,ft o., thc @wr Fg]ge.* Reportable Detecdon Unit BRL = Below RcForting Lirnir Psge 94 of 124

Page 566: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semiyolaaile Orgatric Compounds by GC - euolity Control

Spike

B.tch 703I274 - sw846 35s08

Blank a70it12?4€LK1lPrepored e Analfzed: 22-Mar{7PCB 1221PCE 1232PCB 1?42PCS 12{aPCB 1254PCB 1260PCB 1262PCB t260s@ogab: 4,+Deoctafuo.obiphenyt (sr)Sur/ogab : Cgcechbrobiphenyl (Si

LCs r/0lt27a€s.trPrepared & AnalFed: 22-Mar47PCB 1016PCB 1260S trtoge te : 4, +D B4cta lhht obi p h e nyt (S iSutrwate : Decachlotokipheny' (S 4

LCS Doo 17ut1z7a-ESDi IP.eplred & Analfzed: 22-Mar-07PCB t0.t6rcg t260Suntf,ale: 4,+Dg4ctafluorobiphenyt (SlSu ggate: Decachlonbiphenyl (54

Itupltcar. am3t 27a-Dupl)Prepared & Anab/:ed: 22-Mar{7PCB 1016PCB 1221PCA 1?32PCg 1242PCB t24€PCB 1254FCB 1260PCB.t26?PCB 1268

BRL

BRL

BRL

SRLgRL

BRL

ARL

BRL

2 0 027.1

390

416

2 0 030.0

406

433

2 0 028.6

28.628.6

357

357

2 6 628.6

357

357

28.628.6

ldkS wet 28.6

pS/kS wet 24.6pg/kg wet 28.6pgL/kq wet 28.6

trgL/kg wel 28_6

!g/l€ w€t 28 6

Ug/(g wet 2E 6

!g/kg wel 28.6

Pgr'kg w€t

lSftg vJ€t

lig/kg wet 28_6

!91/kg wet 28.6

|lg/kg wet

lrg/kg wet

!g/(g wel 2E 6

Ug/kg wet 28.6

lrglg w€rpgkg wet

ldkS dry 31-3ps/ks dry 31_3ugtkgdry 31.3

Ug/kg dry 31 3

!S/kS dry 31 3

fdks dry 31.3pS/kS dry 31-3

!g/kg dry 31.3

Wkg dry 31.3pdkS dryldkS dry

udrg dry 30.5

Idkg dry 3O.5

udks dryudks dry

!o/kS dry 31.0

l.'gl€ dry 3t.0

ug/kg drypyl(S dry

70 31115095 m150

109 4G140

117 40-140

70 30-tfr105 njg

114 40-140

12't 40-140

70 30-154100 30-150

3030

Srnrcf,al€: 4,+De41afl @rcbiphenyt (Sr)Smt8,eilg : DaEEchbrohipheny' (St)

Sour.€: 5459548{2

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

ARL

2 1 . 931.3

Sd|.ce: 5A59548-{2

ARL

ARL

ARLgRL

ARL

ARL

ARL

ARL

BRL

BRL

BRL

ARL

BRL

4040404040,lo

404040

Iftlr sdk oo3t27+Ms1)ft€pafied & Anslf.ed: 22-Mar-07PCA 1016PCB 1260

70 30-150100 30-150

106 40-'140

117 40-140

60 30-15095 30-1tu

1 1 1 4 G 1 4 0'121 40-140

60 u15095 30-1fi

Su ftogate : 4, 4- D B;&tafl uo n bi phe n yt ( S r)Sunggahj OecaclfutobidEayl ( Sd

Uatk Solk Duo f/031?.|.llsolt Sorr.c6: SASSs4a.o2Pr€p{ed & Anatl.zed: 22-Mar-07

PCS 1016

PCB 1260

sunwa€: 4,+DBMfluotohiphen l (slSurftgale: Decachblobiphentl (54

Br.ct ?031275 - SW846 35508

gatrk f7031275€lJ(l!

PtEpe€d: 22+rar-07 Anal!.zod: 2$Marry

405

446

1 4 32 8 9

124

469

ft.629_4

31_331.3

341

381

30.5345

387

387

31.O31.O

5050

Thit labotuaory Epor, is ,roa iolld pllhoat an zuihoizt.l slgMture on ahe cover page

+ Reporiable Detecdon Limit BRL = Below Reoonins Linit Page 95 of 124

Page 567: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolrtlle Org8nic Compounds by GC - Qr&lity Cotrtrol

AnaMe(s) R€sult Flag Units rR.DLsource %RECResult %REC Limits

Spike

Level RPDRPDLimit

Bra€h 703 1275 - SW8,l6 3ss0B

Blank (703i279ALK1l

Prepared: 22-l\rar{7 Analyzet 25-Mat47

AIddn

a-gHC

bdHc

daHc

g€HC (U6dan6)

Chlodans

4,{-DDD (p,p)

4,aoD€ (p,p')

a,4-DDT (p,p')

Dielddn

Endosulfan I

End€s$Kun ll

Endosullan Sulfiate

Endrin

Endrin Aldehyde

Heptachlor

M€lhoxycilor

Heplachlor Epoxrde

a€t$ordane

g€hlordane

Endrin K€ione

S urog ale : 4, 4-D B4c IE fl uorob i p h e ntt ( S 4Smogata : De c ac h Mhhe n yl ( Si

LCS f7mt27s"Bs1l

Pr€pared: 22-l!lar{7 Anatyzed : 25 -Mat 47

a€Hc

b-aHc

d-BHC

g€HC (Undan€)

4,4.ODD (p,p')

4,4-DDE (p,C)

4,4-DDT (p,p)

Dieldrin

Endosulfan I

Erdosulfrn ll

Endosulhn Suttaie

Endrin

End.in Aldehyde

H€ptad or

Methoqchlor

Hoptachbr Epo{de

aChlordan€

g4t[ordan€

Enddn t(gione

2,4,5,6TC-l/l-Xylene (lS)

Sunogate: 4, +DB4ctafl @@Whed 6lSunogale: Decachlon phenyl (St)

LCS Duo fi0312? 5-BSOll

P.€pa.ed: 22-lr,,lar.07 Anal]/.zed: 25-Mer-07

Aldrin

BRLBRLBRLBRL8RLBRLBRLARLARLSRLBRLEfiI8R!ARLBfiL8RLBRLBRLBRLBRLBRLBRL17.627.1

24.922.621-9| 1.522.622.425.729-926.227-A28.026.329.927.A

31 .9

25.825.628.80.m0t7_729.9

232

28.628.6

28.62S.6

.62&628.628.628.628.628.628.628.628.628.628.628,62A.6n,628.628,628.610.028.628.6

2E.6

pdkS wet 14.3

!g/kg vr€t 14.3

!gn(g 'r,et 14.3

lgikg wel 14.3

!g/kg w6l 14.X

Ugrtg w€t 71.5

p9/k9 wel 14.3

lgfl(g w€t 14.3

!gl(g v/et 14.3

!g/tg 'aet 14 3pglt€wet '14.3

lgJkg wel 14-3

pgtgw€t 14.3pdkgYJet 14.3

!gr(g wet 14.3

ydl€ */gt 14.3

Fg/tqwet '14.3

l|g/t€ wsl 14.3

uc/ts w€t 71 3pgikgw€l 14.3pdks Yr6l t4.3pdXS wet '14.3

UdkS u/st

t g/|€ vJet

pgkgwel 143

!s/kS Y,/et 14.3

ldkSwet 14.3

Igllg $ret 14.3

lgrn(gwet 143

!9,[(g wel 14,3pg/rg w€t 14.3pgkgvr€l 14.3

lgr'kg r€t 14.3

US/kS s/et 14.3

Igr'kg wet 14.3

rcrkg wet 11.3pg/,€wet 14-3

t,gxg w€t 14.3pdxg rel r4.3

ldxg w€t 14.3

USfl(S $ct 14.3

lgikgwet 14.3

rc4tg we{ 1{.3pg/l€wet ll.3

Ig/kg wst

Ugftg w€lpgtlS w€l

F€/kgw6t 14-3

62 30-1fi96 fr-1fi

87 &14079 ,lO-1,10

77 4G14040 40-l:1079 40-14080 40-140so 40-10105 4S1,O92 ,l$1,(}

97 40-1.t0s€ 4{114092 40-140fos 4i-14097 4&1,1093 4&1{)112 ,r0-r40

96 40-140

90 4{114090 40-140tol 40-140r98 50.20082 4L140105 '4+14t)

81 4G1{O 30

T,ts l4bonlory ..pod ls aot vslid totthotl au e,trtorizd sigaaUn on thc covclr page.

' Reporbble Ddecrioo Linir BRL = Bclow REporting Limar Prye of lZ4

Page 568: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mivolaaile Orgaoic Compouods by GC - euality Control

Spike Source

Brrcl7031275 - SWE46 35508

LCS Duo ft03l275-BSD1t

fu epatd: 22^1etr47 Anal yzed : 2 54at47

a€HC

b-BHC

d€Hc

g€Hc (Lindane)

a,aODD (p,p )4J0DE (p.p')

4,4ODT (p,C)

Dleldrin

End6ulfan I

Endosdfao ll

Endosdlan Sulhte

Enddn

Enddn Aldohyde

ileptacibr

H€ptecl or Epoxide

a.ct{ordane

g4hbrdan€

Endrin Keione

Sunogale: 4, +DEOdafl uorobiplenyf ( SoSunEgate: Oecachlotobiphe nyt (Si

20.s21.4

11.7

21.3

22.9

22_f

25_4

23.4

24.5

24.8

24.1

26_3

29.6

21.4

30-3

24.5

23.4

26.6

1 7 . 127.7

Pg/kgwet 143

!!y'kg wet 14.3

Ugftgw€l 14.3

US.4q vJet 14 3

!ga$ wet 14.3pdkS wet 14.3

!g/kg wet 14.3

!g/kg wet 14.3

IgL/kg wet 14.3

Pg./kg wet 14-3

l,g/kg wet 14.3

Ug/kgwet 14.3

Ug/kg wel 14-3

l4/kg wet 14.3

Pgkgw€t 14.3pSftS$,et 14.3

Pqlg wet 14.3

!9.4(g wet 14.3pg/kg wet 14.3pglkg watUg/kg wel

lrg/kg dry 15.7

l.fg/kg dry 15 7

lgkS dry 15 7

!g/kg dry 15 7

lVkS dry 15.7

uS/kS dry 7A.3

Pg/kS dry 15.7pVkS dry 15 r

l4iks dry 15.7

LrgAg dry 15.7

UgkS dry 15.7

!$'tS dry 15.7

Hg/l(g dry 15.7

lgks dry 15.7pdkg dry 15.7

!g/r(9 dry 15.7gg/kg dry 15.7pg/}q dry 15.7

!gl(S dry 78.3

!g/kS d.y 15.7

!S/kS dry 15.7

lSftg dry 15.7

t'gkg dry

rufts dry

Ugn€ dry 15.6pdkSdry 156|lgr'kS dry 15.6

73 40-140 8

75 40-140 3

41 44-140 2

74 40-140 7

80 40n40 0

79 40,140 13

89 40-140 16

a2 44-110 11

86 ,|tt140 12

a7 40-t40 12

84 40-140 9

92 40-140 13

104 40-140 7

87 40-140 7

106 40-140 6

86 40-140 11

a2 4U140 I

83 40-140 8

93 40-140 8

60 40-t4097 40-141)

28.6

28.6

2 8 6

28.6

28.6

28.6

24.6

28.6

28.6

28.6

20_6

26-6

28.6

28.6

2A.6

28.6

24.6

28.6

28.6

28.62 8 6

30303030303030303030303030303030303030

Duplcato {7031?5O0P1 ) Source: SAs95{a.02

Preparcd: 22-Mar-07 Anatyzed: 2'Ms'-O1

Aldrh BRLaBHC BRLb€HC BRLdAHC BRLgFsHc (Lindan€)

Ct{odan€

4,+DDO (p,p')

4I-DDE (p,p')

{,1OOT (p,p )Oieldrin

EndGUltEn I

Endosullan ll

Endosulfan SuKtste

Endrin

Enddn Aldehyde

tleptachlor

[r€tr|oxydlb.

fiepLdilor Epoxile

Toxsphen€

a4hbrdanegChh{dan€

Endrin Kebne

Swogate: 1,+bBoc6]fllr,robiphenyt (54

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

SRLgRL

BRL

ARL

ARL

BRL

BRL

BRL

BRL

21.5Sunogate: Oecachtotoliphenyt (Si 38.0

tlslrlr Solk. OOlll2T$, Sl) Source: SAs9ga.02

Pr€paBd: 22-ftf ar-07 AhEl,fzed: 25-MaFO7

BRL

ARL

BRL

BRL

BRL

ARL

BRL

8RL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

ARL

BRLBRLaR[

30303030303030303030303030303030303030303030

Aldtnl

a€HC

b€Hc

2S.025.627.3

31.3

31.231:31.2

69 3G150121 3A-150

93 30-15082 30-15087 30,150

Ihh labonto4 Eporl Lt not ialid pilhoul az s$horized sigloturc oa thc cow, page .

+ Reportable D€tection Limit BRL = Below ReportinB Limit Page 97 of 124

Page 569: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivohtlle Orgroic Compounds by cC - Qurlity Control

Analyt€(t Resr.tlt FlaE Unirs Resulr %REC Limirs RPD

Brtch 7011275 - SW846 35508

tlrt lx Solt. ?03127$ilsll So{.cs: SA5O51N{2

Preoared: 22-llaF07 Anah.led: 25-Mar-07

d€Hc

g€HC (Undd|e)

4,4-DDD (p,p )4,4-DDE (p,p')

4,+DDT (p,p')

Diehdn

Erdosulbn I

Endosufan ll

Endosulfan Sulfab

Endrin

Endrin Aldehyde

H@tacfilor

Hepta.fihr Epoxir€

a4hbrdafl€

gChlordane

Enddn Kebr|e

2,4,5,GTGM-Xyl€r'e (lS)

Suftoga6 : 4.+D84cbnuor&iphenyt (SrlSufiogale : DecachlorobipllF.nyl ( Sr)

13.4

29.633.0u.732.034_832.r30.634. I3 r . 529.43 6 632.5

0,02021.641.5

Iatix Solks Dup l7031275.lrsDll Sosrc.: SA595aA-{2

Prepared: 22-lrar{7 Analrzed: 25-Msr-07

29.726.O27.413.625.931 .33t_434.730.532.134.031.7

24.730_639.030.831.040.0

21.3w.2

BRL

BRL

BRL

BRL

Ald.in

a€HC

BHC

d-BHC

g€HC (Lindane)

4,4-{)DD (p,p')

a,aoDE (p.C)

4,4-DDT (p,p')

Di€Hnn

Erdcultan I

Endosulfian ll

End6uffan Sulfale

Endrin

Endrin Ald€hyde

Hepl,adllor

Heptachlot Epoxido

adrlord€ne

g{hlordan6

Endrin K€ton€

S u nqa te : 4,'nBocb tl uotobi phen yt ( S tSu'7qar! : Decachlombiphanyl (Sr)

al.cb 7031313 - SWt45 35454

g|5nk a703lNl3€LKll

P.6parud: 22-!f ar47 Anal:fr:ed: 24 4d 47

PCB 1016

PCA l?21

PCB 1232

PCB 1242

pgrlqdry 15.6

IS&E d.y 15.6

t gkg dry 15.6

ucrrsdry 15.8

rcn(S dry 15-6

ldkS dry 1s.6

tdkS dry 15-6

Wkg dry 15.6

FdkS dry 15.6pdkgdry rs.6

ldrS dry ls.6

ldks dL15.6

IrdkSdry 15.6

l|dtS dry 15.6

US/kg d.y 15.6

irElg dry 15.6

ldkodry 15.6

Ug/l(s dry

UdI€ drypdkS dry

pgfg dry 15.8pgks dty 15.8

!Sn(S d.y 15.8

Igkg dry 15.8pS/kS dry 15 8

lS/kSdry 15.8

Uglqdry 15.8pdxodry 15.8

!Sn(S dry 15.8

[SI(g dry '15.8

lSftS itry 15.0

ldtg dry 15.8

ldkSd.y 15.6pgtg dry 15.8

liSftgdry 15.8

t/dtg dry 15.8

IdkS dry 15.8

IdkS dry 15.8lrg^gd.y 15.6

FqkS dry 15.Epdl(s dryUS/kS dry

pg/kgwel 286pdkg $€l n.6

lgr'kg rel 8,6

Udl€ w€l 28.6

43 3Gt 50E4 30-15t)103 30n50103 30-150117 3&15095 30-1m106 3G150111 30-150103 30-150112 3{1150103 30-15098 30-150122 30-150101 30-r 5096 30-150124 3S.150104 30n50126 50-20069 g-t 50133 fi,l&

91 30-15083 3G.15087 3G15043 3G15082 3(t-t5t)99 30-150100 3G150'r 10 30-150s7 30.150t02 3G150r08 3G.t 50101 30-t5t)115 3G1509t 3G150s7 3+150r24 3G150s8 3G15098 3Gr50127 30-150107 30-15068 *1fl124 30-150

31.2312312

31.23 t . 231.231.2

31 231.231.23 r .231.231.2

31.210.031.231_2

31.53r.53 t . 531_531.531 .5

31.531.53r.531 .53't .531-531.531.5

31 .531.531-531.53t.5

BRLBRLBRLBRLsRr-aRl

BRL

SRL

BRI

BRL

BRL

SRL

BRL

BRL

BRL

BRL

BRL

BRL

SRL

BRL

SRL

8RL

SRL

BRL

BRL

BRL

ARL

8Rr-BRLSRL

BRL

BRL

BRL

SRL

SRL

,1

0

3

2

2

1

2

223

30

30309030303030303030303030303050

50

fhit laloralory Eport ts ,tol rdid v hoat anz horizzd tigrrature oa th. cever pzge.

* Reportrble Dcrectiotr Limit BRL = B€low Reportin8 Limit Page 9E of 124

Page 570: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgatric Compounds by GC - euality Control

Analyt{s) Resuh Flag Unirs *RDI_ t€vel Result %REC Limits RpD Lirnit

Brtch 7031313 - SW846 3545A

Blenk lTUll313ALKilPrepared: 22-[,lar-07 Anat}rzed: 24-MeF07PCB 1248 BRLPCB 1254 aRLPCB 1260 BRLPCB1262 aRlPCB 126a BRLSunogate:4,4-D&Octafluotobiphenyt(SO 20.0Suftogate: Dqcachlorobiphenyl (Si 27.1

LCS O03t3l3€S1l

Prepared: 22.Mar07 Anatyzed: 2SMar-07

PCB 1016 400PCA 1260 436Surogale.4,44t&OchflMrcbrphanyt(Sl 2O.OSfiogale: Decachlonbiphenyt (Sl 2A6

LCS Duo 1703t313.ESp1]

Prepa.€d: 22-1,,1a..07 Anagzed: 2A-Mat47

PCA 1016 40OPCS 1260 433Surogate:4,44B4cknuombiphenyt(St) 2O.OSurogate: Ddcachlotobiphenyl (Sd j4.3

Duollcro. a7O3 | 3t30upt I So'rrce: 5459576{2

P.6pa.ed: 22-Mar47 Analyzed: 24-Mar47

PCB 1016 BRLPCB121 SRtPCB1232 BRLPCB1242 BRLPCB 1248 sRLPCB 1254 ARLPCB 1260 8.63PCB 1262 BRLPCB 1268 BRL

SunqaE;4,+O&Octall@tobtphenyt(54 22.4SuEEgab: Decachhtouphenyl (Sq 34.5

i'larrlr Soir. 4f031313-tts{ ) Source: SA595Z8{2

Prepered: 22{.iar47 Analyzed 24-MarO7

PCB 1016 419PCB 1260 533Sunogate: 4,+DgockftuotobiphEnyt (St 21 .aS,/'rogate: Decachlotobiphenyl (54 33_7

l{atir Soik€ Dup O03'l313. SOll Sourc€: 5A59578.02

Prepared: 22-l,f ar-07 Anal@d: ?A-Ma.'{l7

PCa 1016 478PCB 1260 552Suflag6l9:4,+D&Oclgflwtobipltenyt(54 20.6Sufiogale: Decaclhrobiphenyl (54 37.a

Spike

P9/kg'.vet 28 6pg/kg wet 28.6

!gA9 wet 28.6|€tkg wet 28.6!g/tg wet 28.6

Ugfl(g welpg.4q wet

!SI(S v'/€l 28.6lgr'kg w€t 28.6

!S/kS wetpg/kg trct

yqKg wet 24.6pdks wet 28.6|lg/r(g wetpg/Kg wet

!S/kS dry 34_6lg/rc dry 34-6

ldkg dry 34-6US/kS dry 34.6

Ugxg dry 34.6

UdtS dry 34-6

udks dry 34.6

USXS dry 34.6

UdkS dry 34 6ps,,tt dryUS/kS dry

ps4$ dry 35.5pglqdry 35-5pgks drypdkg dry

US/kg dry 34.4

lrgkg dry 34-1

UdlS drytidkS d.y

28.628.6

357

357

28.628.6

357

357

28.628.6

ARL

BRL

BRL

BRL

BRL

BRL

6.99

BRL

BRL

34.534.5

444 BRL

444 6.99

35535.s

430 BRL1130 6.9S34.434_4

70 3G1fi95 30-19)

112 40-140122 40-14070 30-150100 30-r 50

112 40-140 0 30121 40-140 0.8 3070 30-150120 3Gtil

404040404040404040

65 tu1AJ100 30-1fl

108 40-140

118 4D-144

60 30-15095 30-1il

110 4G140 2 gJ

127 40-140 7 50

60 30-150110 30-150

Thls laboroloty .eport ir,rot vald withou aA at/ihoitedsigE tan on the eorer ptge.

. Reportable D€tection Limit BRL = Betow Reponing Limit Page 99 of l.)4

Page 571: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organlc Compounds by GCMS - Quatlty Control

Spikekr.el

Source RPD

Limit

Bltch 70312?2 - SW846.3510C

Bbnk {m31272€LKll

Prepar€d & Analt.zed: 22-tdar{7

Acenaphth€n6

1-lr€frylnephthal€ne

I {l€t'.iylnaphthsl€ne

Alrazlne

Azobenzenefi ]|pl.ewldiazine

BenZdlne

Benzo (a) anthEcene

Benzo (a) anhrao€n€

Benzo (a) pyrene

Eenzo (a) pyreno

Benzo (b) fuo€nthene

B€nzo (b) fluot'anthene

Benzo (g,h,i) p€rylene

Benzo (g,h,i) peryene

B€nzo (k) nuoranthsne

Benzo (k) nuorantherc

B6nzob acid

Benzyl alcohol

Bi9€{nbrootrory)methane

Bi9(2d oro€thyl)ether

Sie(zd oroisopropy)€ther

Bb(2-ethylhexyl)phthalale

4€Ermphenyl phenyl ehe.

Buty' benzyt phthatarc

Ca.bazole

4-Chloro-3m€hylph€nol

44hloroaniline

2-Chloronaphthalene

2-Chlor@henol

4.chb|ophenyl pnenyl €ther

Ctrysene

Chrysme

Dibenzo (a,h) e'l|trecene

Dibenzo (a,h) Bnthracene

Dibenzofuren

l2oichlorcb€nz€ne

1 ,$Dichlorobeozen€1 ,4oict{orob€nz€ne

3,3 {)id orob€nzHin€

2,4oichloroph€nol

Die$yl thth€btsOlnetryl phtlalab

2J.DinFtr'y{phedol

Di-n+utyl phhetat€

4,&Dinibo-2{€thylphenol

2,4-Dintrophenol

BRL

ARL

BRL

BRL

BRL

BRL

BRLgRL

BRL

BRL

ARL

BRL

BRL

BRL

SRL

BRL

BRL

BRL

BRL

BRL

BRI-

SRL

8RL

ARL

BRL

BRL

BRI

BRL

BRI.

BRL

BRL

ARL

BRL

SRLgRL

BRL

BRL

SRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRI

BRTgRL

!dl

!dlpdl

lsrpsn!41utyrps4!snt'dl!dl

usll

Fdlpsnpcnpdl

u€tlpgn

ItgJlpsrusfluglpdl

vErpdl

udlu€ttlpgn

!9nFS,Itsrtt(/rtrdlrgltgr!dluglpgrl

lrsrlItsrudlrclpgtlpsnFS4!dl!s,lrgrllrsnpcn

!dludl

0.0501.000.4000.0501.00r_tx)0,0500.0501.00Lm|.001,000.o500.2000.200o_0500.0500.2000.050r.000.G500.3m1.001.m|.001.001.OO

1.001.00|.00r.001.001.001.00r.001.001_000.050o.0500.2001.00r.001.001.00|.001.001_OO1-001.00Lm1.001.00

Thb lzborotot! rcpdrt It not eetid w&hott sn zlthafuar' thr&/ta'u oE tha cova pag..

' R€porEble DEt€ction Limit BRL = Below Reportidg Limil Fsge 100 of 124

Page 572: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolrtile Organic Compourds by GCMS - euatity Control

Analytds) RcsulrSpikeLevel

RPDLimitFlrg Unih .RDL

Source %BEC

Result %REC Limirs RPD

B.lcl 7031272 -SW845 3510C

BLnk ?031272€LKtl

tuep*ed & AhdEed: 22-Mafi7

2,+Dlnit ololuene

2,6Jinilrctolu€ne

Di-n+M phthalate

Fluoranthene

Fluoranlhene

H6xachlorcbenzene

H6xachlorobutadiene

Hexachlorocydop€nhiene

Hexachloroelhan€

Ind$o (1.2,3d) pyrene

InderE {l,2,kd) pyrene

lsoplroaooe

2-lvlelhylnaphthal€ne

2Jvlelhyhaphlhal€ne

2+vlslhylphenol

3J-M€thylph€nol

l,laphthalene

Naphthalone

2-lliLoaniline

3+titroaniline

4-llitroaniiine

Nrtobenzen€

2+litroph€nol

4+litophenol

N-NirGodlhethylamine

N-Nitrosodi-r}propylamine

N-Nitosodiphenytamane

P€ntachlorcphenol

Ph€nol

Pyrldin€

H€xachlorobenzene

Hexac{loroei||€n€

I ,2,+Tricibobenz€nsPentad|brcphenol

2,4,tTdcfrlo{ophenol

Hsxef,],lorrbularliene

2,4.GTddilodophend

I u ft ogeb : 2+l@ ro b i ph e nylSu nogate : 2-F ! uoto b i phe n t4Surogai€ : 2.Fluo to ph e notSu[Dgaie. /V/tmb9/Eene{5Sunog/ate: Pherc(4sSunogal€: Teryhanyl4l4Sumgata: Teryhanyl-dl4Su nt''gel€ : 2, 4, 6 -Tti bto ft '€{'he n ol

LCS 17CI2f z€Str

P.€par€d & Anayzed: 22-MEr47

ARL

BRL

8RL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

ARL

8RL

BRL

BRL

ARL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRLgRL

BRL

BRL

BRL

BRI.

8RL

BRL

88.4u)448.810144.899.799_767.4

1.001 0 01.000.0501.OO0.0501.001.000.6001.001.000.0500,2001.001.000.0501.001 0 00 0501.001.{n1.001.001.00't.00

1.001.001.001.()01.000.0501.001.000.0501.001.00.t 001.001.001.001.000.5001.00

8888891018510010068

to0to0tuto0to0l@t@tu

!s/lygtl

ugl

t E lpgtl

psll

ugr!gl

ugrpsn

rrdl!sn!s/ltj9rpsn

!9/1

!s/lpsrl

ljEl

ugl

vgl

!g l

IS/lyg/l

rsflugtl

Lrgi

t/gl

t (yl

ugr!gl

|Jgl

Ljgl

|ls/l

|'lsnu9nLrgl

PEI

l.r9/lpgl

Ljgl

ttg

!sn!gn|J9/l!gnusluglp9lps,4!g l

3n-1n30'13015-110gtln| 5-t t03t>13030-1301Fl10

Thit lahttulory rcporl it not valit wirtav an autho.iZeA signtfrtre on thz corvr pigc.

. R€portable D€tection Linir BRL = Below Reporting Limit Page l0l of 124

Page 573: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatil€ Organic Compotrnds by GCMS - Qurlity Cortrol

Source

Brach 703122 - SW846 35lm

LCS O(li}l272€St)

Prepared & AnalFed: 22-Mar-07

Ac€mphtheno

Acemphtryler€'l +,1€ttrly'n6phthalone

1.lr€thy'naphlhabne

Anilin€

At'azirE

AzobenzonatDiph€nyldkuine

Eenzirin€genzo (a) aithfacsn€

Eenzo (a) anthrac€ne

B€nzo (E) pyrene

B€nzo {E) pyrone

Benzo (b) fluorar{h€ne

B€ruo (b) nuoranlhenegen2o (g,h,i) p€ryen€

B€nzo (g,h,i) p€rylsE

Benzo (k) Suoranthen€

Benzo (k) fluoranthene

Aenzoh acid

Benzyi alcohol

Bls(z.chloroehory)medtan6

Bis(2-€iloro€tryl)elh€r

Bb(2.chloroisopropyi)€ther

Bis(2+tlrylh6xyl)phlhabr€

4Aomoph€nyl pher\4 ether

auryl b€nzyl phfElate

Cdbazole

4-clrloro.3-methylphenolzl4hktr€niline

z4hbronaphthalen€

24hlorophenol

4-Chbropheny' phsnyt ehet

Chays€n€

Chrys€ne

DiberED (a,h) d|f|rac€r|€

DiberEo (s,h) antlu-acene

Oborlzoturan'l,2{)id$rob€nz€ne

1.3-Oil|llorot€nz€ne

1J-ttdbrob€rEene

3,3 Oichktrobe.Eitine

2,4€ldtloroph€mj

Diedr!y' phthslab

Oime0ryl phtnalab

2.4-Oinr9fiylph€nol

Dl-n{rM phthalel€

4,6-Dinitc2-m€lhylph€nol

2,4-OinihoplEnol

7S.5

78.5

87-8

8 7 8

82.2

&2.2

89_5

89-5

1 1 5

105

r0878.5

78_5

86.1

E6.1

T7.S

77.9

71,0

71.O

Eit.5

80.0

87.6

91.6

56.0

s6.4

79.1

94.5

1 1 8

82_0

80.4

a2. l

68.6

81-2

8 1 . 9

8't.g

8r.4

8t .4

83.3

74_O

64.6

76.4

s0.074.283.379.575.086. I72.2u.7

pg,l

rdl|lglpEl

vsllpsrl!dlpgl

uilItSJI

|ls4

t d l

udludltrgrlFSnpgl

tts/|

usn$gAps^pdlpdlpgl

!dl|ldl

rcIps4!dl

TMpsIt grl

ItsApdl

ItsA|ls4wlrgnpdI

!srutyrwirpgn

!srpgl!gl!glpsnItsrpc/l

t'gltrgl

0 0601.000..t000 0500.050r.001.00o,0501.00|.001.00t.00o.0500 2000.050o.2000.2000.o501_000-o500.3€00.0501.00r.001.001.00't.00

t.00r.00't.00

1.001.001.00t.001.001-001.000.0s00.0500.2m1_001.001.001.00|.001.001.001.001.00Lmi.00t_00

100't00

t00100100100100t00t00't00

1m100100t00100100100100r00100100100100tmr001001001001001(X)r001001m100100t001001m1mr001(X)r00r001001 m100r001001001m100100

78 1{)"r4D7E 40-1408€ 40J4088 ,lo-140

82 a&14002 40-140112 4{t14090 4{r1,{o90 4{t140r 15 G200105 4S.14t)108 4{t1401A 40-14078 40n,$86 4G14086 4$ 140?a &-r4t)78 4G14071 4o-1&71 44-14t)ga {G1{098 .r$.r.to

84 3013080 40-t{o88 4&1109? (t140

56 ,10-lrl0

96 40-14079 40-140s4 40.110118 4&1.10E2 3G.13080 40-140s2 40n4069 3013081 4G.1{O82 4G14082 4{t140E1 4G14081 40-14083 4O-l,O74 &1&65 4Gr4476 ,1014{1

90 40-14074 30-lfl)tx) 4&14080 4Gl,l075 3013086 4.Gr4072 3o1?o85 3&13t)

This labetory q,on is not ealld withord an aun2orized slg&atzre on tte corer lroge.i Rcportable Detection Limia BRL = Betow Repodng Limit Page 102 of 124

Page 574: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Quality Control

Anaye(s) Resull F lag Unns 'RDLSource %RECResult %R-EC Limirs

Spike

L€vel

R?D

LimitRID

ktch 7031272- SW846 3510C

LCS {7031272€5fi

Prepared & Anal]/zed: 22-Mar-07

2,4-Oinifobluene

2,Boinibotduene

Dl-n{ctyl phthatate

Fluoranlfi€ne

Fluoaen€

H€xachldob6nzen€

tl€xEchlorobutadfene

tl€xEchlo.ocvclopenladiene

llexachloretfuns

Indeno ( I,2,3-cd) pyrene

i.deno (1,2,3dipyr€ne

2+vlethylnaphlhalene

2+vlethyln4hthalen€

2-fr,ls{trylprt€nol

3 y'-M6lhylph€nol

Nsptffid€ne

2j,litro6. line

3J{itso ilineiH{itrosriline

NitsoberEene

2.1'lltrophend,l+litrophend

NJrlitosodimethyJarnine

ll-NltlosodFn{ropylamine

ll-Nitosodipft 6nylarnins

Pentachloropheml

Pflenanthrene

PlFnd

Pyridine

Hetachloobenzene

I .2.+Tridbrob€nz€neHexachbrcethane

Pentachlorophenol

2,4,+Tri{$brophenol

HexaafibrobvHiene

2,4,GT&$hr@henol

Swrogale : 2+hmobiFnenylS/J/'oga|€ : 2 + h-atubip,he n y'Sunogab: 2+fuotophenolSunogate: Nibobanzene4'Swtugabj Phercl4sSuiqale; fephenMt4Sunogale: ferpheaYd4Swft gate : 2,1,6Tn b(ono ph en o I

Iatlx SDlk. O031272.f, srl

P.€pded & Analfzedt 22-MaF07

8 4 9

89.0

1 1 6

76.9

76-S

6'1.6

8 1 . 6

76.0

75.9

70.0

7 4 2

73.0

7 3 0

88.8

84.0

84.0

70.2

72.2

8t-7

8 1 7

8 5 2

48.2

1 1 6

9 6 0

76.9

5 6 9

77.1

40.4

98.6

6S.4

76.3

16.3

79.5

a2_7

82.7

83.5

76.0

7 8 9

7 4 2

6S.4

87_0

75.9

62_7

85.945.969.O10270.249.189.176.7

Sourc€: SA5q5634t

85 40-140

89 40-140'116 4o-lulo

77 40-140

77 40-140

62 10-140

82 40-140

76 40-140

76 4+140

70 40-140

7{ 40-140

73 40-140

?3 40'141)

89 40-140

84 40-140

84 40-14{

70 40-140

72 44-130

82 40-140

82 40-14n

85 40"140

8A 40-140

116 40-140

s6 40-t4t)

77 30-130

57 30-130

77 40-140

40 40-14u

99 40-'l4r

69 30-130

76 40-140

76 40-14{l

80 30-13t)

83 40-140

83 4G140

84 40-14{)

76 40-140

79 40-140

74 40-140

69 30-130

87 30-130

76 40-140

63 3G130

86 tu13086 3lr13l)69 15-110t02 30"13070 15-11089 30-13089 3+13077 1L110

!9/lpgn

!9/lpgn

Lj!/l

u!/l

!qi I

u9/l

Lj!/l

!wlp9/l

utylgg/r

pg/l

pg/i

ttg4pg/l

pg/l

y9!l

gg/r

ugnpgnpgnpgn

trS/lpg/l

plyt

us/lug4|lg/l

pgn

pgi I

vglpgtl

!(yl

ugl

!gnps/lptufs/l!9/1pg/l

ugnpsr!s4ts4PEudrpsAuElusn

1.001 0 01.001.000.0500.0501.001.000.600r.001.000.200o.ofi1.001.000.0501.001 0 00.0501_001.001.001.001.001.001.001_OO1.00t.001.000.0501.001.000-0501.001.00.t.00

1.001.00'L00'1.00

0.5001 0 0

100100100'100

1001AOr00100't00

r001001001001001001001001001Ul1001001001001001001001DO1001001tro100'r00

100100100100100't 001001001001001001001001N1001001M1001N

Thit hboturory ftpott is dot yalid withota tn authortrpd signot',re on the coecr poge .

+ Reportl$L€ Detection Limit BRL = B€loq/ R€porting Linit Page l0l of 124

Page 575: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mivolatile Organic Compoutrdr by CCMS - Quality Conrrol

Spik€

favel%RECLimit!

RPDLimit

SourceR€sult %REC RPD

Brtch 7011272. SW816 JslOC

t{atrir aoks fl031 272.l|slr

Preperad & Anall.2ed: 22-Mar{7

4'Chloro-Smethylphenol

2-Chlo{ophenol

1,4-Olchlorob€nz€ne

2,+OtliLoioluene

4+litrQhenol

tl.t{trssodi"n+ropylarnlne

1 2,+Tdahkrob€nzene

Pe.rtaatdomphend

Suflogah. : i-Fl@nbiphenylS u nEgato : 2 + hMo biphen ylS@ogate:2+lt@tod6nolS!,tr9ga/r€: t'litohenzene4sSuftogate: Phenol4liSnogate: TeryhenYd4Suftogal€: Tephenyl44

Sourcs: SA59553-O4

78.476414113369.,176.691.783.2r0613689.569-5G4.810680.4u.465.781.36',094.894.4

81.7a1.716014359.6a2.7s0.694611415099.099.067.611483.08:t.o69.492.169,3161M74.5

wpdl

!dlggl

|rsnvilwl|lgnpdl

!gl

1|dl

lrsil

!gl

FS,l

!dl|ldl|l(ylp[ylpsnrgl!dl!dl

w!sr

aM7 pg'l

aM? lgl

ug/rygyl

ts,|ysil

FdroM7 p94

rdl|'lg,fl

@lFg/l

Fdltlsfl!dlItgAps?l

IEJIl|gilps4

71 40-14071 4Ga140127 30-130120 30-13063 4G14t)50 40.140$ 30no75 40-140ss 3&130124 30-13t)81 40.14081 40-1{05a 40-140s5 30-13072 tu1fi72 30-13059 1511079 g-1305A 1511085 *130a5 a)-19)63 l | l to

76 4614076 4Gt,O148 30-130132 30-13064 40.14071 40-14084 3G13088 4G.140106 30-i 30139 30-13092 40-1fi92 &166:t 4G140106 3$.130n tu1frn 30-1fr64 15-110a5 g-lm

N 161109a tu13098 30-13069 15-110

0-050'1.00

1.00|.00t.mr.001.001.001.00|.000_050r.001.00'LOO

1 l l

1 1 1

t 1 1

111

111

1 t 1

1 1 1'111

1 1 1' t 11

1 1 1

t i 1

1 r l

1 1 1

l t l1 r l1 1 1l t t1 1 11 1 1f l 11 1 1

108

108

108

108

r08

108

108

104

108

r08

104't08

10s'! 06108t081M1(R10410e108108

BRL

BRL

BRL

BRL

ARL

ARL

SRL

SRL

BR!

BRL

BRL

SRL

BRL

BRL

Sun9gEte: 2,1,6Tnbtunophenol 69.6

ItLlrir Spik€ Duo l703tT/2- SDll Souree SAtS9ti6$04

PreEared & A^alyzed: 2.t(et47

AcerEphthen€

44hbro-3m€fiylphenol

2{hbrophenol

| ,rt{idiorobenzen€

2,4-Dtrritrotoluen€

+Nifoph€nol

N-Niuosodi+propylamin6

Pentaddorophenol

| .2,+Trichbrob€nzenePentad orophenol

Su nW aE : 2+ I uorobi p lE n II u nEgate : 2 -F I uorobiphe nylS/,,/'cgate: 2+luorophendSuftogale : Nitrohe n zene 4 5S!/'rogde: Phenol45Sg'7Ega|i-: TeAh@yl4HSU/'$ge/€: Teryhenyl44Sl'/twete: 2,a,6-Ttib@nophanol

B.td ?01279 - SW8,l6 3ss0B

Ahnk fr0:}1279€LKl I

Prcp€re{t Z.ljar-o7 Analyzed: 23-t Er{7

Acenaphtr€n€

Ac6naphf)yl€ne

Anilino

r_000-0501.001.O01.00't.00

1_001-001.001.000.050|.001.001-00

8RL

BRLgRL

8RLgRL

BRL

ARL

8RL

ERL

BRL

BRL

BRL

ARL

BRL

m20?()mm20fr20

202020m20

77t510

t l11 61 1l 1

t 31381 1

BRL

BRL

BRL

BRL

rc49 wetrc/Xg rr'ettrg/kg r€t!94(g rel

330330330330

This labontorf rqoi ts Eat vdid i' hoa anat lhorizd stgnant}z on thz qte.r page.

'Reportable Detedion Limit BRL = Below Relorting Limir Pag€ I 04 of 124

Page 576: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivohaile Orgatric Compoutrds by GCMS - eurtir-v Cotruol

Spike

Level

Source

Result

%RECLimits

RPDLnnitAnalFe(s) %REC RPD

Brtch 70312?9 - SW846 J5508

Bl.nk O031279€LKll

Prepared: 22-Mar{7 Anatfzedr 23.MaF07

Azo!€nzene/Diphenyidiazine

B€nzidin€

8€nzo (a) antriraoene

B€nzo (E) pyreneg€nzo (b) iuoran$Ene

B€nzo (g,h,i) p€rylene

B€nzo (k) fuorenthene

Benzolc acU

B€nzyl dcohol

Bb(2-cl oro€hory)methane

Bb(2-cfi loro€tryt)€ther

Bis(2-chloroisopropylFther

ab(2-elhyltl€xyt)phthatale,l€mmoph€nyl phenyl etrer

AUV b€nzy' phthalat€

Ce.bazole

4{hbro-3-fir€thylphenol

4{hlorcan ine

24hlorooaphthalene

24hbrophenol

4-ChbroptEny' phenyl erher

Chrysene

Dlbel€o (a,h) anhracene

Dib€nzoturafl

1 t-DichbroberEeneI ,3-DlciknoberEene

1 ,4-Dictllorob€nz€ne

3J .oic* orcbenziline

2l-Dlchlorophenol

Distryl phthalaie

Dimelhyl pMalata

2l-Dlm€thylphenol

Di-niuM phthalBb

d,ruhiro-2-mebylphenol

2y'-DlnlrophorFl

2,4-Dinihololu€ne

2.G-Dlnitrotolrrene

Di-n{clyl phft.ratab

Fluoren€

H,Ex*nloaot €nz€n€

lbxad o.obutadi€ne

Hexachloiocyclop€nladi€ne

FlEx6chkro€tf|an€

Indeno (1 2,kd) pyrene

rsoptloaon9

1 +r€tryhephtral€ne

2-nl€thyhaphthalene

2-lrethylphonoi

3,4-lrefhylphercl

l,laphthalen6

BRL

ARL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

SRL

sRtBRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BFIL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

!g/kg wet 330

trg/kg wet 330

ug/kg wel 330

uglkgwel 330

lg/kgwet 330

!g/kg wot 330

Ug/kg wet 330

Pqr'kg wel 330

lgr'kg w€t 330

lsnq',vel 330

lgkg wer 330

lgikS wel 330

ldkg wet 330

lgr'kg wet 3i]0

!94Q YJ€t 33O

!q/kg w€t 330

!g/kg wet 330

Lig/kg w€t 330pq/kg wet 33O

!g/kg wet 330

!g/kg wet 330

lgr'kg wet 330pg/kg wet 330

Lig/kg wet 330

ligr'kg wet 330

pgftg wet 330pg/kg wet 330

!g/kg wet 330pS/kS wet 330

ug/kg !!et 330

Lig/kg w€t 330

Ug/kg wet 330

!g/kg tlet 330

!g/kg wet 33O

pglkgwet ?30

iJq/kg wet 330

lgr'kg w€t 33O

pg/kg wet 3:)0

!g/kg wet 3:]0

!S/kS vr€t 3:}C

pgr'kg wet 330

!g&g wel 330

ttSlkgwet 330

lgkS rvet 330

UgL/kg w€t 330

Ugr'kg w€t 330

pg&g wel 330

Ug/kg wet 330

pg/kgwel 330

t,g/kg n€l 330

!9,49 w€t 330

Igftgwel 3:)0

This laborolory rcport ls nol wliil wilhoet ar, suthoize.l cigdattue od the col'€r prye.

' Reportable Detection Limit BRL = Below Reporting Limit Page 105 of 124

Page 577: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Quelty CoDtrol

AnaMqs) FlagR€sult Unirs .RDLSpikelavel

RPDLimit

Souce %REC

R€sult %REC Limit! RPD

Brich 7031279 - SW846 35508

B|ank 170312794LKl1

Preoa.€d: 22-l1tar-07 Analyr€d: 23-&1ar47

2+litro6nilirF

3{.lilrDaniline

4-ilitroaniline

Nitrob€rEerE

2-ilitrophenolll+liuophenol

N.NitEsod-rnetrylanine

lgNitrosodi-nf ropylsmine

N-Nibosodiphenylamhe

Phemnh|gn€

Phenol

Pyndhe

1,2,4,Tridrlorobenzene

2,4,gTricilorophenol

2,4,dT.ichlorcphenol

Surcgale: 2+lrcrobid16nylSutroga te : 2 + horophenolSurcgalc: Nlhobenbne4jSrnrogator Pheno,.d5Surogate : Te.phenyl4l4Sufiogab : 2,4,eTdbrontophend

LCS f?03r279€Stl

Prepared: 22-{\rar-07 Analyzad : 23 JJ,a( 4I

Aniline

Azobenz€ne/Oiph€nytdiazine

B€nzldlne

Eenzo (a) anthracene

B€rEo (a) pyrene

Benzo (b) lluor€nthme

B€n:o (9,h,1) p€ryienegenzo (k) nuo€nthenegm2dc acid

Beozyl alcotlol

8is(2d oroe0rcryFnethane

Bis(2d{oroethyl)€6ler

Bis{2drlorolsopropt)elher

Bb(2+lht4hexyl)pht|etale

4SromoplEnyl ph€ny' o[|€r

Buqy' berEyl phhabis

Carbazol€

4-Chlorc3fiethyth€ml

4thloroenlin€

z.Chlolonaphthabn€

24hbmpl|enol,4-Chlorophony' ph€ny' ether

ChryserE

DD€nzo (a,h) anthrec€ns

BRL

BRL

ARL

BRL

8RL

BRL

SRLgRL

ARL

8RL

BRL

BRL

BRL

BRL

sRtgRL

BRL53501050489039m6140s30o

5270i9t03390521053{t043907535 t t 053S05060495058403i,504t30346t)39503520491054404720

36i103620495039805960s55052m

467086706670667066706670

667066706670

667066706670667066706670aa7066706670667066706670667066706670667048706670

w70

6€7066706670

pqkgwel 33O

Ygrlg rcl 330

udkswel l3mpg/kg wet 330

ligl€wel 330

rgrtg wel 13m

lg/kgw€t 330

Ugr'kg rsl 33O

lgAg Y{et 330

Ygtl€s/et 33Opg/rgwet 33o

Fgtgwsl 330pdkSt{€l 3:10

ldkg wet 330

lgr'kg wst 330

tglgwet 330pglkg vrel 330

Pqtg vr€tpdkg welps/ks v/etlgL/kg vretlgr'kg wetl|gilq wet

pgr'ko rrcl 330

USftg$ret 330

!g/to wet 30

Ig^gwet 330pg&g wel 3:10pdkgtvet 3ix)

!4k9 wet 330

lgL/kg wet 330

ugfl(gwst 33Op94!g wet 330pg[]g wot 33o

Fgkgrv€l 330pg1(s lnet 3:t0

Fgr'kg w€t 330

!g/t(g wel 30

l|g^g wet :l:|,0

Ig/kg wel 33O

Fdkgrv€t 33opdkg rcr 3ii0

rcr'kg Y/et 33o

ldkSwet 3i,0

Fg/t€ wBt :|i|0

Fg/kg wel 3i)0pgkg w€t 330

l.rgt/lqw€l 3li0

lgr'kg rvet 330

lgil(gwet 330pg&gurer ii:m

N 30-13061 15-11073 N-1N59 ls-11092 30'130N 11110

73 40-130?4 40-1eO51 40-13078 40-13080 4G13066 40-13011 0-130t7 44-13081 40-t3076 8.1n74 4G13088 40-13050 G13062 40-l$52 40n 3050 40n3053 4113074 4G13082 4G13071 40n30120 40-13054 40-13054 40-13074 40-13060 40-13089 40-130&, 4&13078 40-130

Thls labontory tqort it rd yald Nithod an a,/lt ottzd lngddure oD dE cot.' pagc.

. R€portsble Dele{tion Limir BRL = Below Reportiog Lirnir Page 106ofl24

Page 578: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mivolatile Org|oic Compoutrds by GCMS - Quality Control

Anal),te(s) Resu!t Flag unitsSpikc

Level

RPDLimit*RDL

Source %REC

Rcsult %REC Limits RPD

Batch 7031t79- Sw846 35$B

LCs a7031279€Sll

Preper€d: 22+4a.{7 AnatyzaX: 231,tar4t

Dib€rEoturan

1 .2oi(t|b.oberEene

1,3oic*rlorobsnz€ne

l,4oidrb.oberEen€

3,3'4{chlorob€ntdine

2,4Jidtb{ophenol

Oietvl phthalate

Dinr€thy' phtlEbl€

2,4-Olrn€0yphenol

Di-$t|nyl phttahb

4,6-Dhirro-2{ethylphenol

2+DlnltTophenol

2.4-Dk roloh/€ne

2,fl)inilrotoluene

Dl.n.octyl phihalate

Fluoranfi€n€

Hexadrlorobenzene

H€xadrlorobutadisn€

Htsxaddoroqr'cbpertadiene

Hexadlbroetlgoe

Indono (1,2,3-cd) pyrene

| +rrsthylnaphthslene

lgophorone

2-Melhylnaphthalene

2-lrr€bylphenol

3,4-lrelhy,iphenol

Naphfia{'ene

2+lit oadlin€

3-l,litroaniline

4-Nitroanllhe

Nilrob€ruen€

2i litroph€nol

4-Nltmpr€nol

N-f .libosodim€thy'amine

N-l.li[osodi-n.p ropylamine

N+lttosodiplrenylamine

Phenanth,en€

Ph€nol

Pyddhe

1 ,2,+Tridrlorcbenzene2,4,STrid o.oph€nol

2r,GTrid oroph€nol

Sunryate : 2-H twofi p h e nylSIJ''c{ate:2+lrcmpheno!Sutugete : N ilro ben ze n e4 5&fiogato: Phenol4sS|J/.ogate: TaAhany'4l4S uft gate : 2, 4, 6 f dbro noph e n ol

$40507036604730656036205 1 1 050,103100526041404470561059605160524051005710474046m43205',l7051903700414038404030381047006430672033703520443040003990555053005010366051603010440049504090525037tu3890350057405670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

8670

6670

6670

6670

6670

6670

6670

6f'70

6670

6670

6670

6670

66706670

667066706670

!g/kg wet 330

Pg/kg wet 330

rc/kg wel 330

!g/kg wet 330

lrg/kg wet 330

Mkg wet 33O

!g/kg wet 330pg/kgwet 330

lig/kg wel 330

lgikg wel 330

!g/kg wet 330

pg/kg wet 330

lglkg w€t 33O

lgr'kg wet 330

lAlkg wel 330

lig/kg wel 330

!g/kg wet 330

!g/kg wel 330

Pg^g wet 330pglkgwet 330

!g/kq wel 330

trg/tg wel 330

Fg/kg wel 330

lig/kg w€t 330

!g/kg wel 330

!g/kg wel 330pglkswet 33O

Pg/kq wel 330

Pg/kg wel 330

Fgikgwet 330

!g/kq wel 1320

!g/kg wel 330

Ug/kg wet iBo

tgRgwet 1320

Fg/kg wel 330pg/kg wet 330

t/g/kg wel 330

Pg,/kg wet 330

!g/kg wet 330

PgL/kg wet 330

Pglkgvet 33Opg/kq wet 330

!g/lg wet 330

!g/kg wst 3i]0

Fg/kg wet 330

Pg/kg w€t

!g/kg v/et!9Ag Y/et

PSI(S wet

Pgks w€t

Ugfts wst

81 40-130

76 40,130

58 40-130

71 40-13)

98 40-130

u 40-13D

77 40-1XO

76 40-130

46 40-130

79 40.130

67 40-130

67 4G130

U 4t1"130

89 40.130

77 40-130

79 40-130

76 40-r 30

86 4{t130

71 40-130

69 40-130

65 40-130

78 40-130

7a 40'14C

55 40-130

62 40-130

58 40-130

60 10'130

57 40-130

70 4G130

96 40-1 30

101 4O-t 30

51 40-130

53 4G130

66 40-r3o

60 4G.130

60 40-130

63 40'130

79 40-130

75 40-130

55 40-130

77 40-130

45 40-130

66 40.130

74 4n-130

61 40,130

79 30-13056 15-11058 30-13052 15-11086 30'131)85 15-110

oudtcar. o0: 2790uPl) Sourcer 3A59497{5

kepared: 22-t d-07 Anat'Jzd: 23.tiat47

Thb tttorrloty rcpotl ir nol r,zld withod c, otthorizad signo!fie on lhe av, pa&e.

i Reporiable Detection Limit BRL = Below Reporting Limit Page l0? of 124

Page 579: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgatric Compoutrds by GCMS - Quallty Control

Analyte(s) R€,sult RrB Unils Result %REC Linits

Bstch ?031279 - Sw8.l6 35508

Duolicarea703l279{UPl) Sourc€:Sl594S?{5P.€par€d: 22-l\,lar47 Aml}r2ed: 23-Mar{7

Acemphthen€

Acenephhyl€n€

Aniline

Azobenz€ne/Diph€nyldiazine

Bonzidiae

B6nzo (e) anth.acerE

Benzo (a) pyr€neg6nzo (b) fluoraMene

Benzo (gn,i) peryl€n€

Eenzo G) nudantherEgenzoic scid

B€nzy' slcohol

Bis{2dtloro€thdy)nElhane

Bb(2drlorcehyl)ether

Bis(2drlorolsopropy')€the.

Bis(2-€tlrylh€xy')phthalate

4-EromoplEnyl phenyl e0€rgutyl b€nzy' phthahte

Carbazolo

4{hloron{fiehylphenollLcl$or@niline

24hbronaphthal€ne

2-Chloropt€nol

44hloficph€oy' pheoyt eth€r

Chrys€n€

Dibenzo (a.h) anthrac€ne

Dibenzofuian'l 2-Oi..hl].ob€{Eene

I,3-Didtlo.oberEene

1 ,+Dic* orobenzene

3,3'Oichbroben:bine

2,4-Oi$brcpheml

Di€thyl phthdale

Diflr€ihyl phlhalate

2,+Dim€lhy'ph€nol

Di-o-butyl ph{halEte

1,GDfr {1rc-2<nathyhh6nol

2,4ohnroph€nol

2,+Dinitotoluer|e

2,6-Diniboblrerc

Di-n-octyl phth€bts

FluoranttErF

Fluor6ne

H€x8chlo(ob€nz6n€

H€rcd orobutadion€

H€xachlorocydot'€ntadi€n€

Hexachloro€[rane

Indeno (1 ,2.3-cd) pyr€ne

1 -lretrykraphttubne

lsophqofle

BRL

ARL

BRL

BRL

8fiL

BRL

BRL

BRL

BRL

BRI-

BRL

BRL

sRrBRLBRLsRrSRL

BRL

ARL

8RL

ARL

BRI

BRI

BRL

ARL

BRL

ARL

BRL

BRL

BRL

BRL

SRL

BRI

SRL

8RL

BRL

BRL

BRL

ARL

BRI

BRL

8RL

ERL

ARL

SRL

BR|-

8RL

ARL

8RL

BRL

8RL

BRL

pdkgdry E55

Udkgd.y 955

US/kS dry 855

lgko dry 855

rglgd'y 855

ldkS d.y E55pdrg dry S55

ltdkS dty 855

udkqdry 855

r4/ko dry 8s5q (g dry 855

uSftSdry 855

ldkS dry 855

Udksdry &55

ugftgdry &55

PdkS dry 8s5

lIgftS dry 855

lgrgdry 055

FdkS dry 0s5

lgl(g dry 855

|lgI(S dry 455pqkgdry 8ss

IS/kS dry 855pdksdry 855pgrgdry e55

lgkS dry 855ydks dry 855

FdkS dry 855

udks dry S55pdtg dry 855pdks dry 855

udks dry 855

ldkq d.y 855pglkg d.y 855

rdksdry a55pdkSdry 855ps/kS dry 855

LrgtS dry 855

ldkS dry 855pglkgdry 855

rdksdry a55

udrsdry 855

!S4(S dry 855

Uglkgdrr 855

udr€dry 855

udkg d.y 855

Idts dry 855pslk0dty 855

udrsdry 855

ugxgdty 855

tlglks d{y e55

Idkgd.y 855

BRL

BRL

BRI-

ARL

BRI.

8RL

BRL

SRL

BRL

BRI.

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ERL

BRL

BRL

BRL

BRI

BRL

SRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8Ft-

BRL

BRL

SRL

ARL

BRI.

BRI.

BRL

50

50

50

5050

50

5050

505050

50

50

505050505t)505050505050505050505t)5050505050505050505t)

Thb labordory rqo.t b nol vdid Ntlhout crr tttdrarized slgfi4lar. od thz .aje, p.ge.

'R@ortabl€ Detection Lirnit BRI = Below R€porting Limit P€e 108 of 124

Page 580: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semiyolatile Orgenic Compounds by GCMS - euality Control

%REC RfDAnalyte(s) Resuk Flag Units +RDL L€vel Resutr %REC Lirnirs RpD Limit

B.r.h 7031279 - SWt4615508

Duollcab (7031279OUPi1 Source: SA5S497-05

Spike Source

Prepared: 22-lrar-07 Anat\zed: 23-MatO7

2-[,lethylnaphthalene

2-l{€Urylph€ml

3,4-l-lefrr4pfi€nol

Naph[|ai€n6

2-l'lilrcannine

3-|.l loa'|iline

4-f'{itsoaniline

Nitoti€nzene

2+.lifoph€nol

+Ntrophenol

N-N ro€adnn€thyamine

N-Nfoosodin-propylamin€

N{.lilrosod{,h€oyiamine

Pentachlorophenol

Phenantfirene

Phend

ryntifl€1,2,4-TdCfi lo.obsnzsn€

2,4,$Trichlorophenol

2,4,FTrichlorophenol

Su.ftgate : 2+hMobiphetrylSuftcgeto : 2 - FI uaft ph e no IS.J ' rogabjNl funzene4sSuflEggte: Pheno!4sSunogate: Tephenyl4l4S unqala : 2, 4, 6 -nibm m o ph en o I

Matrlx Solk 4031279-MSt) Sourcer 3459497{5

Ijs/kg dry 855

USI(S dry 855pg/kg dry 855

t4ikS dry 855

Ps/ks dry 855pgkS dry 855

udks dry 3/'20lgn€ dry 855pdkS dry 855!S/kS dry 3420

!g/kg dry 855US/kS dry 8s5ldkS dry 855lgkg dry 855

LidkS dry 855prykg dry 855!S&9 dry 855

tig/ks dry 855ldkg dry 855Pdkg dry 855

us/ks dry 855l4/kg dryugks dryUgkS drytidks drylsfts dry!9&S dry

!g/kg dry 418

S/kS dry 418pg/kg dry 418

f.rgkS dry 414

ldlq dry 418

USAS dry 1670

ldkg dry 418

|ls/ks dry 418

f.igkg dry 414

ldls dry 418

lgkS dry 418

ldks d.yldkS dryt/91(9 dryrgl(s dryUStXg dryll91(S dry

t gkg dry 418

ljgkgdry 414lghg dry 418lrglq dry 418pgl(g dry 418

ARL

ARL

ARL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

ARL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

705465

776/

BRL 70

ARL 58

8RL 50

ARL 52

ARL 70

BRL 5f

BRL 47

ARL 66

8RL 44

BRL 74

BRL 72

754866420575

BRL 76

BRL 60

BRL 51

BRL 56

BRL 78

BRL

BRL

8RL

BRL

ARL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

ARL

BRL

ARL

BRL

BRL

BRL

ARL

BRL

ARL

121009350| 13008210134ffi| 1600

5S2097508460442058€0s66039801't 1007400

6070632040205530357071706344

5050505050505050505050

505050

5050505050

Preparsd: 22-l\raF07 Anal\rzed: 23-Mar{7

4.Chloro.3fi €thytphenol

2.ChloroDhenol

1 ,zt{ichlorcbenzene

2,+Ohitttotuen€

4+,libophenol

N+{ilro€odi-n-pop!4amine

PenlachlorcphonEl

Phsnol

1,2,+Trichlorobefl zene

S utogat$ : 2 -F luotob i p h e n ylSunogate : 2. F hloroph en o ISunogate : Nitoben zohe4sSumwal€j Phq,1ol45Su''oga|€: feryheny|4l4Sunwate : 2, 4,Eh bmn'f ph € n ol

173401730017300173001730017300

4440

16900

r6900

8440

8,{40

16900

84!.0

16900

16900

8440

8440

84408441)844n844n84400440

4444

16900

16900

8,t40

u&

wt 3t)15-t103{)-t m15-110n,lm15-110

40-14030-13030-13040-14040-1do30-13040-14030-13030-13040-14040-14434-13015-11030-13015-1103Gt3n15-t 10

40-1403G1303013040-r404Gt40

8 3 03 3 02 3 07 3 011 30

I.rnr So{k Duo 4703127t{SD1l Sou.ce: SA5!X97{5Pr€per€d: 22{tar-07 Analyzed: 23-Mar,07

4€hh{o-3fi6t'rybh€rlol

2€hlorophenol

| ,+Dichlorobonzeie

2,+Oinit otolu€n€

638010?00866047506550

Thit lQbofalary ,epnd is aat vald w hout sa zr/thorirrd siflt zaarc on the Eolvr prye.

' Reportable Detection Limi( BRL = Below Repodng Limi( PaCe 109 of 1 24

Page 581: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatlle Org ic Compounds by GCMS - Quality Control

Analtie(s) Flag Unils Result %REC Limils

Bdch 7031279 - SW846 35508

ilaLh 6oika Duo 12011279-LsDll gonrEc: SA3g4g?i5

PrepEtEd: 22-[16r{7 Analyz€d: z3-ldar{7

+Nilrophenol

N-Nilfosodl-n+ropylamine

Pentact oroph€rrcl

'1,2.+Trichlorotr€nzerE

S urogate : 2 + I tptob ipl?p.n ylS mogate : 2 + I uotopherr0lS unqEE : N itroben zene4 5Suft.gata: Phetul4'Surogate: Teryheny'4l4Sunlgate : 2,a,ehb@nophqnol

Batch ?0313?l - Sw846 35508

B|ank lm3l37l€tfil1

ft€paBd: 23-Mar-07 Analyzed: 24.Mat4l

Acenaphtren€

Aniline

Azob€nzendDiphenyldiazine

Benidlneg€nzo (a) anthrscen€

Benzo (E) pyren€

Benzo (b) fluoradtr€ne

BetEo G,h,il p€rylene

Benzo (k) nuoranthene

Benzic scid

B€nzyl alcohol

Bb(2-chlo.o€ft ory)methan€

Bis(2dtloroelhyl)elher

Bis(2-dtlorcisoprcpyFttEr

Bb(2+ltrylh€xyl)phthalate

4€ro.ioph€nt phenyl ether

BUV bonz/ pffi€lale

Carbaole

44hlolo-3-m€f rylphenol

44hb.oaniline

2{hbronaphthalene

2chlorophenol

44hlorophenyl pfEnyl ethsr

Ghrys€rE

Diber8o (a,h) antrlracoae

Dlbenzoturan

| ,2-Di' orohenzer|e

1,}Di{florc$onzerE

1,4-Old{orcb€nz€ne

3,3'{)icfibrobonzldin€

2,4oidllorcph€nol

Diethyt pftrh€hb

Dimethyl phflalato

2,4{)im€thl$henol

t0c001?2011000785063906220s9m644t)89405680t09009640

1670

4 1 8

4r8418d le418

169008440r6900163008,1408.t{08441)84108440S|UO844084'lI)

SRL

ARL

BRL

BRL

BRL

BRL

Fdkg dty

Pdks d'Y

udkgdrypdks dry

ugks dry

PdkS dry

PS^g d.Ypgrs dryldks dryldkg drypdks dry

clMT pg/kg dry

6a 30.13050 ,10140

65 30-r 3046 30-13076 40-14074 +1&118 3t>tg76 t5-110106 3GrW87 lSl l '129 3G1mfi4 15-110

8

6 3030303t)30

BRL

ARL

ARL

BRI.

BRLgRL

BRL

8RL

BRI-

ARL

BRI

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

aRrBRL

BRL

BRL

BRT

lgrkg wet 330

lg/ksrvet 3:10pgtg wel 330

lgtgw€l 330lgr'kg rrcl 30

FdkS vret 3]0

t€/kg wet 330ygtgw€I 330

fgtgwel 330

Idtg r^,€l 330Uglkgw€l 330pS&S rvet 3i,0pg/kg wet 330

Ug/kg wet 330

ldkgwet 330IgI(g wel 330

!s/ks t/et 30

I|SIIS wet 330tidkg wet 330

Pgr'f,g 1 '€l 330

lgkS tv€l 330lg/kqw€l 330pgdkg vret 33otig/kg wet 33Opgr'&wet :F0

lrgy'kg wer 330pdkg w€l 330

ugr'kg sl 330pg €wet 3i10Ig/kg wet 33Opdrqwet 330

ldkgw€t 330gg/kg i,r€t :Il0

rcr'kg w€l 3|0pdkSwet 3il0

Ugftgwet 33Opdksw€t 3:10

Thb bb.ototr r€pod B not v4litt *irtou da outhoizetr 6ig'Eta,e on the @wf pag...

* Reportable DeteatioD Lirnit BRI = Eetoq/ Reporting Lirnit Pag€ I l0 of 124

Page 582: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semlvolatile Organic Compoutrds by GCMS - euality Control

Spike Source %RFC R-PDAnafyle{t Resutr FtaB Unirr .RDL Level Resutr %REC Ljmjrs RpD Linit

&tch ?031371 - SWE46 3s508

Blank 170313?l€l_Kt)

Pfepa€d: 23-llrar.O7 Analyzed: 24-Ma. 47Di-rFbulyl phlhatate

4,6-Dindl$2-m€thylphenol

2,4-Dinibophenol

2,+Diniuololuene

2,&Ohilrobluene

Di-o-octyl phlhalate

Fluoranlh€n€

Hexachloaob€nzene

fl€xEchkrabutEdbne

tiex€chlorocyclof entadienetlexachlom€thane

Ind€no (t,2,3d) pyrene

t -{\rethylnadrthalene

lsoPhorcne

z+.|€thynsphthalene

2+r€thybheml

3,4-MothMphenol

Napfttnal€ne

2+.{ilr('aniline

3i,iltroonilineit-l,{itroer lihe

Nitobe.Eene

2-r.lnroph€nol

4+litophenol

N-Nihcodimethyhlhine

N+lito€odl-nf ropylamine

N{ibo6odiphenylemine

P€ntachlorophenol

Phenol

hddne1,2.+Trichlorob€nzene

2,4,tTricilo{ophend

2,4,6-Trichlof oph€nol

S mogab : 2-H tloto W h e nylS unogste : 2-F f uoro phe n o IS unogate : N it rcbe n ze n e 4 5Swmga./re: meno145Sunnga|€: letphenyl4l4S!4ft gab : 2, 4, &f n kono ph e n o I

LCS a7c'1371 ASt I

ftopaed: 23-ft-{ar{7 Analyzed: 244nd -O l

Ac€nephf|ene

A€€naphhytene

Anftn€

Atrauln€

Azob€nzei€L/Dirhenyldiazine

Bsnzidine

B€nzo (a) €nth.acsne

B€nzo (E) pyrerE

6670 776670 736670 906670 776670 906670 59

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

ARL

8RL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

ARL

BRL

5110485D6010515059703550

4030

5430

5aso548075606300BRL47005170

667066706670667066706670667066706670

30-13015-11030-13015-11030-1301U110

40-1304S.1304o-1304G13040"13040-130G13040-130.r0-130

pg/kg wet 330gSftS Y,,et 330pg/kg lYet 3l]0

tig/kg wet 330

UgL/kg wet 330

Pg/kg wet 3:10

!g/kg wel 330pg/kg wet 330

pg/kg wet 330

lgy'kg wer 330pg/kg wel 330

pgr'kg wet 330pdks wet 330

lgr'kg w€t 330

!g/kg r,/st 330

lgL/kg wet 330

trgL/kg wel 330

Ugr'kg wet 330

pg/kg wet 330

t,gkg wel 330

!g/ko w€l 330

!g/kg wel 1320

IS{9 lvel 330

l4/k9 wel 330

Ugr'kg wst 1320

pgkS vret 330

!94(g Yvet 3:}0

lgkS wet 330

lgr'kg rYet 330pgr'kg wet 330

Lig/kg,./et 33O

ligfl(g wet 330

!g/kg wet 330

!g/kg wet 330

pg € wet 330

lgL/kg wet 330

Ugr'kg wel

Ugr'kg wstUg/ko wel

ligLi K9 welpg/kg wel!g/kg wel

!g/kg wet 330

pg/kg wet 330pgiko w€l 330

!g/kg wel 330

rcy'kg w€l 330

!9y'k9 wel 330

lgikg w€t 330

usrkg lvel 330

pdkS lv€t :x}0

al88821 1 394

707A

This lanotuory rcpod Lj not w!i.L+l!ho,t! ad 4t [rorized sigrratwe on thz covet pltge .

. IGportable Detection Limit BRL: Below ReDortine Limir Page l l I of 124

Page 583: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Scmiyolatile Orgrtric Compoutrds by GCMS - Quelity Control

Anabrds) Result FlaeSpike

I,€vel Limitl

RPD

Limit

Soulce

Result %REC

B.lcb 703rJ7l - Sw846 35glB

LCS ft0313?tAStl

Prepared: ?!Mar-O7 Ana!f2€d: 24-Mar-.07

8e.Eo (b) nuoranth€n€

Eenzo (g,h,i) p€rylerE

Berzo (k) fluoranlhen€

BerEoic acid

8€nz]l alcohol

Bis(2-ciloroehoxytnethane

Bis(2.chloro€tr.lyi)ether

Bb(2{hloroisopr@y')€lher

Bis(2-elhy'hexylhht|slate,l-Brornoph€nyl phonyl eth€lBut/ benzyi phfi€taie

Carbazole

4-Chlom-3{efhMphorrclzt4hloroanftE

2Chblonaphhal€ne

24hlorcphenol

4{hlomph€nyl ph€nyl eorer

Ch.ysene

Dib€nzo (a,h) anth€c€ne

Dib€nzofuran'l ,2-Dbhbrcbenz€n€'l,3oichloroberP€ne

1 ,4-Di*lorohenz€ne3.3'Oicfi lorobenzitin€

2,4oidrlonrph€nol

DiethM phtnahle

Din|€lhyl pht|€ble

2,4oimethylfhenol

Oi-n+uy pht|alsle

4,6-Dinilro-2-methylpfi enol

2,+DiniEoph6nol

2,.1-Dinhrololuene

2,6ohh'rololuen€

Dl+odyl phthda|e

Fluo.anttlea|e

H€xachlorob€nzafl€

Hei€ctrlorobutadi€ate

Hexaclrbmqrcbp€nhdbn€

H€xachloroelhan€

lndeno (1 .2.3-cd) pyrene

lsophorcne

t -M€lhylnehtfisbne

2+.let ylnaphthalene

z-il€trylphenol

3,4-M€tt],lph€nol

NaFrr0ralone

Z+{lhooiline

3-Nilroonlline

4-Nitroanilin€

Nitrob€nz€ne

2-f.libopherlol

42S405063304620487053905sgt)4350sno41XO56007no505043404950.{260

5r60{s7047m5130460039604820509044305?,fi49204510533039SO48t052AO55m66704t00smo,t60o

1750420/J469039?05490a85052304390412052005r8047907*058701720

667066706670

6670667066706€70

66706670

667066706670667066706870G6706670

6670

66706€7046706670667068706670667066706670

6670667066706670667066706670

667066706670667066706670867066706670

ldxSwst 330

ldkg Yret 330pdkg rv€t 330

llg/t(g wet 330yg/kgw€t 330

Igut(gwel 330pg'kg wel 3[|0

Lrdkg vr6l 330

!g/kg wet 3i]0

lrgl€wet 3i]0

lrg/kowet 330pgitgwel 330

lgkg wel 330

rdkgYr€l 330

ldl€ v.el :|l}0pgr'tg $,€t 330

lgftgwet 3:t0

Ug/kgwel 330pdlS w€t 330gglkgw€t 330

ldkg$ct 330

rdkg vret 3:)o

rcrlq wet 330

Ig/kgwel 3:]0pc,19 r.€l 330

ldkgl€t 330tigftgYret 33OpdkS Yret 3lOygr'kg wet 33Opgikg w€t 330

Pglkgwet 330

tidkg wel 330

ldkg Yt€l :t:}0

Ig,kgw€t 33OpdkSwet 33opg^g w€t 330

ugitgwel 330

Pgrkg wel 330

ldkgYr€t 380

USI(S Yi€t 330pdkSwst 300

llg^g wet 3:10

Udkg we{ 330pgrts vr€l 330

trdkg Y{€t 330gdkS Y/et 330

IdkS lvet 330

Irgrkg u,et AIOpg/kgv/el 33O

lqr'kg wet 1320pg/kg w€t 330

flgrlqwel 330

64 4&1m61 4G13)95 40ng)69 G13073 40-1308t 40-13084 a&13065 4Gr 30E7 4{tt3071 40-13084 40-13{)108 40-13076 {013065 ,10-130

74 40-13]64 40-13077 40-1m75 40-13071 4G13077 4,0-13069 40-13053 40-13072 fi-I3om 4G1306S 4&13078 4$.13074 40-1U)68 4(l13o80 40-13060 40-13072 40-13079 40-'t3083 40-130100 40-13070 40-.13078 4G13069 40-13071 4Gr3064 44-13/]70 40n3060 40-13082 ()n 3073 4+1,1078 40-13t)66 4t113006 4{t13078 40-13078 4&13072 10.130'fl4 40-13()8a ,$-13t)

71 {0-130

This ,abo.dor| report b trot rditt vfuhoot qn oailoized tE aurc on the caver page.'Reportable Detection Limit BRL = Below Repoding Limir Page ll2of 124

Page 584: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivot{tile Organic CorDpourds by GCMS - euality Control

Ansltle(s) Result Flag UnitsSource %RECResult %REC Ltrnirs'RI)L

Spike

I-evelRPDLimitRPT)

Brlct 703ll7r - SW846 3ss0B

LCS {703137t€aPrepared: 23-lrar{7 Anatyzed. 24-Mat.!J74j.litrophenol

N.Nitosodimethytamrne

N+litosodi-n-propytamine

N.Nfrrosodiph€nytamine

P6nbd orophenol

Ph€nantir€n€

Ph€nol

Pyri(fins'l r,&T.ichtorobenzene2.4,$Tnchbmphenol

ZJ,GTn-d orophenol

S u iq ale : 2 - F I uo m hi p he n y !S unog ate : 2 - F I uamFke no IS mogate : N i | rcb e n zen e4 sSutogate: Phend4|Surrcgete: Teryt6nyl-d4S udogate : 2, 4, ETd bro n o p h en ot

Dupllcab 17031371 JUpl)

3320

4470

56t]0

6(H0

4130

4&t0

4850

4940

3660

4930

4640

3520

51m44106200418051504450

Sourc€: 3A59455-08

ARL

ARL

BRL

BRL

ARL

BRL

BRL

ARLgRL

BRL

ARL

ARL

BRL

ARL

BRL

ARL

ARLgRL

BRL

SRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

ARL

BRL

8RL

BRL

aRt

Lig/kg wet 1320

!g/kg wet 330

t g/kgwel 330

ug/kg wet 330pgr'kg wst 330

!94(S $/et 33O

!g/kg wct 330

pgr'kg wel 330

tlg/kg wel 330

lig/kg wel 330pgkg wel 330pS/kg wet 330

Ug/kg wet

lgKg wet!g/kg welpg/(g wet

!g/*g wel

ug/kg wel

!g/kg dry 749

ldkS dry 749pdkS dry 749

rc/kg dry 749

liglkS dry 749pdkS dry 749pdkS dry 749

USlkSdry 749

ldkS dry 749

pSftSdry 719

t g/kg dry 749

rrg/*S dry 749

Ug/kS dry 749pCn(g dry 745pdks dry 749

udksdty 749

uqtls dry 71spdl(g dry 749

ugkg dry 749pS/kg dry 749

Fg/kg dry 749

rdkS dry 749

udkS dry 74s

pgl(gdry 749pdkS dry 749

lgrSdry 749

UdkS dry 749

uslls dry 749

uS/kg dry 749

pdrs dry 749pgks dry 749

FglkS dry 749

rdks dry 749

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670667066/O667066706670

507388916270

7455147053/7609363//67

4G13040-13040-13040-13040.13040-1304G13040-13040-13040-13040,13040-130il-l3n15-11030-130t 11 t030-13011110

P reparedi ?3-Mst47 AnalFed: 24 -Mar47

Acenaphlhyten€

Aniline

Azobefi zen€/Diphenytdiazine

8€nzidin€

BerEo (e) anftraceneg€nzo (a) pyEn€

B€nzo (b) fluoEnhene

Senzo (g,h,l) peryone

Senzo ft) nutrandlene

B€nzoic aod

BerEyl atcotlol

Bls(2+hlo(o€thory)methane

Sis(2-chb'roethyl)elher

Bis{2d$foisopropyl)ether

Bls(2+thylh€xytFhthatale

4-Brdnophenyt piEny 6fl€rButyl beizyt phthatate

Cefiazol€.rchbrc$mehylphsnol

4.Chloro€nitine

2-Chloronaphdl'lgn€

2-Chlorophenol

4-Chlotropheny' phenyt eherClry€ene

Dibenzo (a,h) anthracene

DlberEofuren

1,2{H orob€nzene

1 ,3obilorobenz€ne

1.41)\.hbrc*nzene

3,3 Olcibob€nzidine

BRL

BRL

ARL

ARL

BRL

BRL

BRL

ARL

BRL

ARL

BRL

BRL

BRL

8Rr-

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

505050505050505050505050505050505050505050505050505050505050505050

Tht laborulory rcpo is fiol r'slid withoz! an dud.orizzl sigutare oa lhe covet pogc_

t R€porr[ble Detection Limit BRL = Below Reoortine Limir Page l l :1 of 124

Page 585: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatilc Org|nic Compou||ds by GCMS - Quality Control

Analytds) Result Flag Units

B.ach 70117 1 - SW846 35508

Duollc.te003l37lDUPl) Sourcs:sas9456ollPreparcd: 2'M€r-O7 Anatyzed: 24-ltat47

2,4.Okl{oroph€ml

Dielhyl phlhab!6

Dimelhy' phftlalab

2,,|-Difiethylphenol

Dh+l tyt phthatate

4.6-Dinitro-2-m€thylphenol

2,4-Dinilrophenol

2,+Dinftforoluen€

2,ooinibotoluen€

Di-n-ocv phthabb

Fluoranlftone

F&roren€

Sourc€: SAll0455-08

LrdkS dry 749

ldkg dry 749

rgkS d.y 749

trdks dry 749

Itglkodry 749

Idks dry 749pdksdry 749

ldXS dry 749

UdkS dry 749lgkSdry 749

t g/kg dry 749

ItgJkgdrf 749pc/ks dry 749

tidl(g dry 719

ldkg dry 749

lgkS dry 74s

w/l€ dry 749

ldkS dry 749pCASdry 749

PdkS dry 749!g/kS dry 749lgftS dry 749pdkg dry 119FgJtSdry 719pdksd.y 749pgksdry 3000!g/kS dry 749

!S/kS dry 749lSAg dry 30d0pgt€ dry 749

Pgrkg dry 719pgrs dry 7,tgldksdry 74s

ldkg dry 749Ug/kS dry 749pgil€dry 719!s/ks dry 749Ugkg dry 749

lgkgdry 149pdkS dry 749

lgks drypdko dry|tgikg dryllgftS d.ypgl(g dryPg/kg dry

ygikS d.y 371

PS4(0 d.y 371

Pdkg dry 371lgftgdry 371fldkSdry 371

BRLBRfBRLBRLBRLSRLARLBRL8RLBRI.8RLBRLBRLBRLaRl8RLBRLBRLBRLBRI-aR!_ARL8Rr_ARLBRLBRLBRLBRIBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLARLilst)515061do538t)5930{030

BRL

BRL

BRL

BRL

BRL

BRI.

BRL

ARL

ARL

sRr_BRL

BRL

BRI-

BRL

8RL

ARL

BRL

BRI

8RL

BRL

BRL

BRL

BRL

BRL

BRT

ARL

BRL

ARL

BRL

BRL

BRI

BRL

BRL

BRL

SRL

8RL

8RL

BRL

BRL

BRL

5050e)5050

5050505u

5050505050

50505050

505050

505050

50

505050505050

Hsxdiorobenzeno

Hex€chiorobutadi€ne

Hexachlorocydopentadlene

Hexachloaoothane

Indono (1,2,3d) pyr€ne

lsodioro(t€

I -{tlsthylnaphtialerE

2-frethyhaphthat€ne

2-lret'l]/l,rhenol

3,4-M€fiylphenol

Naphthalene

2-l'lifoadllne

SNitro8nilifl€,LNibosnilne

NitsDbenzens

2+.lltorftenollslittEphsnd

N-Nlhcdimethy'am'tlle

N-Nilroeodl-ntropylamin€

N{{itrosodFhenylamine

Penh<fllo.ophenol

Ph€nanttu€ne

Phenol

q/ddine'l,2,+Tr*,|bobenzene

z,4,tTrid o.opfienol

z,4,GTdd o{opfEnol

s/rnrjga/F : 2 -FluotobiplnnytSullDgatiei z-Flsoroph€notSu''oga/€: NiffinzeneasSufiWal': Phenol4,SunwaiF: ferytun'N4S udog ab : 2, 4, 6-T i b 'I]n1lgf,hetd

X|trlx Sllke fIO3l3?l{Sl}

75707570f57075m75707570

Prepared: 23-Mar-07 Analyzdt 2+Mat47

Acenaphh€n€,f -Chloro-Sfi ethytph€rEl

24hlorophonol

l,4obhlorob€nz€n€

t/4-Dlnitrotolu€ne

519010200921047305m0

7fiOt5()m1500075007500

ARLBRLSRLBRLBRL

$-tntul to3o-1frtF110gtl3t)1U'10

40-144

30-130

3)-130

4&l/O

4G140

67

8l7l7a

696€61

60

fhjs laborslory ryod lt natrdid tttlho,/ or onhoizrd stgitbue oa tt cowr psge.

+ Reporta6le DriectioE Limit BRL = B€low Rcporting Limit Pagc I 14 of 124

Page 586: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - euslity Controt

Analyre(s) Resrlt Flrg Units .RDLSpike

Level

Sourc€Resull %RIC

%RECLimits

RPDLimitRPD

Brtch 703l]?l - swE4615508

flrtix Solk r03l37t-Hslt Sou.cei SA59{:ig)8Prepared: 23-t'ar{)7 Ananlzed: 24-Mar4744,lbophenol

N-Nihosodi-n-propylamine

Pentad orophenol

Ph6nol

12,+Trichlorobenzene

S wogato : 2 - H @tob i phe n ytS unogdle : 2 -F I uorop h en otSurrogate : Nltoben ze ne45Sanrogaie; Plr6oor{5S!/'mga|f: Teehenyt4t4S ffi og ele: 2, 4,ETtibmm o p h e n o I

6't40557073209430587044205150423060204190622043ln

lr.Hr Soik Ouo O03l37l -tilsol) Source: SA594SS{8Pr6paGd: 23{rar{)7 Anatyzed. 2+Mat47

560010600947049505620649059108380991062804630554043906180435064904680

Ug/kS dry 1440ugkS dry 371lrSlkg dry 371tidks dry 37'l

YkS dry 371

uvks dry 371PS/kg dryt!9'l(9 drylqkS drytrgks drylgks dryPg/kg dry

|lgkg dry 368l{/kg dry 368lig/kg dry 368pg/kq dry 368Yg/kS dry 368

Ig/Kg dry 1470

l4/k9 dry 368Ugkg dry 368

PgftS dry 368pSI(g dry 368!g(g dry 368

!s/ks drylgks drygg/(s dryFq/kg drypg/kS dryLig,/kg dry

15000

7500

15000

15000

7500

7500

750075/n7500750/)7500f500

7440

14S00

14900

7444

7440

14900

7440

14900

14900

7440

7410

744074407440744074407440

30"130

40-140

3G130

30-r 3t)

40-140

40-140

30'13015.110&-13015-1103G13015-110

40-140

30-130

30r 30

40-140

40-140

30-130

40-140

30-130

30-1m

40,140

40-140

30-1301111030-13015-t 1030-13015-t 10

8RL 41

BRL 74

ARL 49

BRL 63

BRL 7A

ARL 59

695684568358

BRL 75

BRL 71

BRL 64

ARL 67

BRL 76

ARL 44

BRL 79

BRL 56

BRL 67

ARL 84

8RL 62

7459835887

,l-Chblo-3-mothy'ph€nol

24hb@'€r'ol

1 ,,loichbroberEene

2,+Oinibotoluen€il+.likoplEnd

N+lnmsodlrFpropytEmin€

Pentachloroph€nol

Phenol

1,2,+T.lcft lorob€nzen€

S ufi oge,€ : 2+ | t!o@ b i phe n ylS urryele : 2-F I uoto phen olSunogata: lhltult zE ne45SiJ/tuga/€: PhetE4sSu''ogata: faeheafr4t4&lrrngate : 2, 4, GTthro nop h e no I

8

5

6't0

7

7

6

7

5

3030303030303030303030

This hbo&lory reporl l, nal vald withod an Mthoiud sigtaturc oE the coler pqge .

+ Reportabie Detecrion Limit BRL = Below Reponing Limit P&ge 115 of 124

Page 587: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Mctds by EPA 6000i7000 Series Methodr - Qrslity Cotrtrol

Analyte(s) Result Flag

Spike Source o/oRfc

'RDL lrvel Rcsuh %REC LimitsUnits RPDRPDLirtrit

Brtch 70!1322 - f,PAr0o/SlV?0m Scrter

ghnk lm3l322€LKl)

Pr€pat€d: 26-Ma.47 Analyzedi 27 -Mar 47ilerc!ry BRL

Dupltcrt 1703132-DUPil sourei SA595l7al

fiigLl(g wet

0.232 ORs |r€ukg dry

rngtl(g dry

otgn(g dry

0.0298

0.0341

0.0333

0.0327

0.0329

0.0300

0.4fr)

0.451

20

Uarnr Soll€ t70('l 122{51 | Sourc!: SA5Sgl7.O2

Preparcd: zaMarfi Analyzer!: 27 -Mar47

Preparsd: 26-[rar47 Ananlzed: 27 -ttd47

Mercury 0.69?

Pr€psfed: 26{,f aro7 Analll?!,di 27 1,tlat47

Mo.cury 0.630

0.340 38

0.222 r03 75n25

0.182 9{t 7St25

o22 66 85,115

Larrir solk. o0313u- s2l Sou|Ee: SAlg517.t2

PoEr solk. 170313iI2+A1) So0tc€: SA595l7{2

Prepat€d: 26.ldar47 Analyzed: 27 -Ma47

RefoEnc. .7031 SZlSRlii l)

Prepar€d: 26{\rari7 Amlyzed: 27 -l.t!€to7

Brtch 7031413 - Swt46 3005A

Ahnk a703l{l3aLKtl

Prepar€d & Anal)rz€d: 26-l\rar{7

Selenium

Lead

Silver

Chrornium

Barium

Cadmium

LCS fr03t,l13€St)

Pr€pared E Anal}rzed: 2&Mar.07

0.522 ocl mS/kg dry

0.53,1 @3 mgng *"t

0.456

1 .12 4A 65.$132.6

Sel€rfum

Chrcmluln

Cadmtum

Btr|um

Sik€r

LCS oup fto:tl{13€SD{l

Prepared & Analfz€d: 26{tar-07

Selenium

Cadmium

Badum

Chromium

Silve.

Duolicaae flftll:|l3{UPl !

Proparcd A AnalFed: 2SMar47

Seleriun

0.466o.62o.4740.4860.4810.'157o.471

Sourcr: SA!iOt2.{X

BFfBRLBRLBRLBRLBFILBRL

0.4500_4530_4460.4620.4700.1480.457

lrrg,l

msrrfro/l

n'Ell

mS/l

ntgil

rrls4

mgnnsnmdl

rE/l

rE/l

ms/r'sfl

rEnrngrrf€/l

nsnngrmdl

mdl

n'SI

0.0t50o.00750.00s00.00s00.00500.0040o0025

0.00750.0t500.00500,00250.00500 0040o.0050

0-o1500.00750.00250.00400,00500.00500-m60

0.0t50

0.500o_5{x)0.5@0-5(X)0.5000.500o-500

0.5fi)0.500o_5000.5000-sfi)0.5000.500

85,115a$11585-r'! 585-11585-1't5a$1158S115

8$1r58S.1158S1158S1168$11585-t ' t585-115

90

9'l

89

s2949091

s3I

sg

9194

3

4

mm20mNm20

BRL ARL 20

ThiJ bbrqtorf rcpor, ie ,tol edlil i'irtou aa &dtoriz.d igruurc oa the cav.r pcge.

+ Reportable Det€ction Limit BRL = Belorv Reporting Lilrir Pae€ l l6 of l24

Page 588: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 6000/7000 Series Mcthods - euality Cortrol

Source

B{r.h 7031413 - SwE46 3005A

Duplicab l?031413-truP1)Pr€Dared I Anelyred: 26,t\4ar-07LeadCadmiulh

BatiumSilv€rChromium

ilruix Solk€ a703t.t13- Sl|Pre{ared & Ar|al}.red: 26-Mar.07S€l€niumLeadChromiumC€dmiumSiker

Aarium

Sourco: SASS372{4

0.01340,00060-03900 04070.00328RL

SourE€: 5A59380-01

o.473o.466o.4730.4900.4610.4700,479

Source: SA59380-01

0.469

0.464

0.1a6

0.470

0.466

0.478

0.462

fig/l

fig/l

rngnthg/l

ms4mg

mgnmg/lfignmSL/lfIE,

mgL4

mg/l

mgn

mg,l

mg4

mg/l

fitg/l

msnmgr'l

mgnmgnmg/lmg/lmg4lrE/lang/r

0.0139

0.0006

0.0384

0.0408

0.0030

BRL

ARL

0-0ma

ARL

BRL

0 002s

ARL

BRL

BRL

o.o038

0 0025

BRL

BRL

BRL

BRL

0 0038

BRL

BRL

0 0025

BRL

BRL

BRL

75-125

f5-125

75-125

75-125

75-125

75-125

71125

75-125

75-125

75-125

75-125

75-125

75-125

7U125

80-120

80-120

80-120

80-120

u-f2t80-1208&1m

0 00750.00250.00400.00500.00500 0050

0 0150 0.5000.0075 0.$00.0050 0.5000_0025 0 5000_0050 0.5000 0040 0.5000.0050 0.500

0.0150 0.500o.o075 0 5000.0050 0.5000.0050 0.5000.0050 0.5000.0040 0.5000.00?5 0.500

0 0075 0.5000.0150 0.5000.0050 0_5000.0050 0 5000.00+0 0.5000.0025 0.500o.0o5o 0.5oo

00_50.26

202020202020

0.4s70.4990.4920.5140.5040.4970.514

I.ltdr Soi(c OLp fi031413-MSO1t Source: SAE93BO{1PrepeGd & Arulyzed: 26-MaF07

S€lenium

Lea{,

Sivsr

Barium

Chromiqm

Cadmium

P6l Son(e flUr 4t 3+S1l

PrE!€r€d & Analy4d: 26-Mar.Oz

L€ad

S€lenirm

B€rium

Siver

Cedmium

c'rrornilD

999998J0310099103

95

92

94

98

9?

94

96

5

7

6

5

7

6

7

20202020202020

93s397

94

93

96

This labontor! rcporl is nottalid x,irhou ot zuthoried sigaat nc on.he cove pa*e.

+ Reportable D€t€ction Limil BRL = Betow REDortine Limit Page I l7 of 124

Page 589: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 200 Series Methods - Qurlity Cortrol

Analyte(s) Result IRDLSpikeI,€Yel

RPDLimirFlaB UniLs

Source %REC

R€sult %REC Limits RPD

Brlch 703 l32l - EPA 200 Scries

Bl.nk n031321€LKll

P@Pared & Analfred: 26-Mar-07

Sih,er

Seleniirm

Leeo

Cadfiium

Chmmium

Banum

Duolhar6 (703132l{)UPll

Preparod & Analtrred: m-irar-o7

Silver

S€ienium

Chromium

L€ad

Cadmium

B€rium

Iarnx Solke flO3l32l{Sl}

BRLsRrBRLBRLARLgRL

8Rr-

Source: SAsgslrul

m€*g w€tmg^g wetnEag w€lttg/kg welfEr'kg wetnEr'tg w€tnEI(g n€t

0.9051.36't.36

0.6790.2260.4530.453

1.091.630.5440.816o.272|.6ij

o.g4

1.08

r.610.5360.2m0-0061-61

0.538

aRrBRL

1 1 ?

0.3s4

8RL

BRL

44.5

0.490

26S

3.97

u.5

BRIBRL

0.56910.78-6,118354.7

ARLBRT.3-970.490

71 10.54aI

BRL nEAg drySRL |rElkg dry76.8 rE kg dryt3o ms/rs dry

0.3!,2 n€/kS dry6.13 OR1 n€ftg dry40-8 rE/r.g dry

Sosrc€: SA595l7{2

133 nE/kg dryr29 mg/ks dry164 msttrs dry124 nrS^g dryllb oM7 r|g,tg dry121 mg <g dryl8O ng/kg dry

35

Prepared: 26-l{ar-.07 Analyzed: 27 -t ''ts,.{7

Silver

S€lsnium

Chrcmiun

Cadr{um

Le30

Badum

P€pared: 26-l\rar{7 Analyzed: 27 -Mar47

S€l€nluln

S&€r

Cadmium

Ctt.omium

Lead

Beritnn

Pr€par€dr 26{vlar{7 Analtzdi 27 -Mat47

Silv€r

S€l6nium

Cadmium

R€feronc. l?031321€Rt l)

Pr€peedi 26-lr€r.07 Analr/rd: 27 -Met47

Selenlum

Silv€r

Chromium

L€ad

Cdmium

Barium

1341 U1341 yt3.lt34134

r2712f127127

r3513513t;135

78.21124.4,19-4

44.93'1.8214

70-1307Gr3070n3070-13{)7G1307G13)7G13{)

s9s68Sc25092101

matrlr Spike 17031 Il.t{521 SourE : 5A!9517-12

Pod Solks a70cl321+Sl I Sourcai S^st5lru:l

't t9't26

1 1 0r23't1s

335177

125129127119

03.1{4.5a5.051,54r.930-5219

mg/kg dry 1.52nErtS d.y l.O2mg/rg dry O2gmgyl€ dry 1.52rnSttg dry 0.508nEl(gdry 0.762.nSn€ dry 0.508

rElkg dry t-08mgrkgdry 152nrgr'kg dry 1.62rELI(9 dry o.mg

rE^gwel 1.50filglkgwol 1.0OrEukgw€l l-50ng (gw€l 0.500hgikg Y/et 0.750mgrkgwet 0.250.ngrtg vr€{ 0.500

94 7Gt3t)9S 70-13086 70-13088 70-13087 7G.1301m 7tri3006 70n30

tx' 8$t1596 8t11591 8tr1586 8$.115

1M 77,+1n,6108 68.+133.6rm 80.&119_4104 78.&rfts93 81-E-118-1s 92.1- 7.9101 82.7.117.3

Thls labtubry Eport ls Eot vatid d tou sD srrttodz.d d81,',aht oE fhc cow, Fqe .

+ Reportrble Detec-rioo Ljmit BRL = Below Re(ting Linir Page I l8 of 124

Page 590: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total M€tals by EPA 200 S€ries Methods - euality Control

Spike Sourcel*vel Result

RPD%RE{: RPD Limrt

Brtcb ?031414 - f,PA2al0/SW7000 Series

Blank {7031414€LKll

PrEpar€d: 26-[f a.{7 Anati 'd: 27 -Mat.4l

mg,4

LCS fr031414€StlPrepared: m-Mar{7 Anatyzed 2f -Ma(07

M€rdrry O.OO247 85-t 15

ouplicrto at03tat40uPt) Sou.ce: SA59517.13

Prepar6d: 26-fvf ar{7 Anatyzed: 27 -Mar47

M€rcury 0.00026

IatsixSplX.{703141+MS1) Sou.c.:SA59517-1.1Pr€pared: m{rar47 Anatyzed 2j -Ma.-o7

luercury O.0O2b3

,ralrix So*<. Duo (7031a14{SD1t Source: sA595t7-14Prepared: 26-{,f ar-07 Anatwe d : 27 -Met 47

Me.orry 0.00240

mg/l

mgn

' 101m9/l

lrE/l

75-125

75-125

Thls lahrutary repod k not wllil fithou c ouhonzci signaurc on the covet pzge.

' Repo(able D€tection Limit BRL = B€low R€Dorting Lirnir Pase I 19 of 124

Page 591: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Met|ls by EPA 13fZ & 6000/7000 Series Mctbods - Quality Control

Analyre(s) R€sultSpik€

Level

RPDLimitFlag +RDLUnils

Source %RECResult %REC Limits RPD

Brich 703r40E - sw846 3010A

Bhnt r7031408€txl)

Prepared: 2}Mar47 AnElyz9.d. 24 +J,at47

S€lenium

L€ad

C€dmium

silve.

Chlomiufil

Eanum

LCS f7ml400€s1l

Prep€red: 23+{ar47 Anelyzad: .Mat47

Lead

S€lenium

Silvea

Cadmium

Chromium

Batium

LCS Duo f031408-g$)t)

Prepared: 23-lt-l€r{7 Andyzed: 24.1ht47

So0rc.: SA595l7-12

mstltrEnftrgl.r€Imdlmsrlmgr'l

mgnmsn

qca r€iltrB,l.rg,AmdlNET

l|lgI

@lnqlntsltndl

OC3 mg/lmgn

mdlmglmdlmdlmgxmsnmgr

rEImgr'lmgnmgn

OR7 triSl

BRL

BRL

BRL

SRL

BRL

BRL

BRL

L l 8

t . 1 3

0.651

1_23

1 . 1 4

1 . 1 8

1.24

't.05

1.09

1.09

1,05

1 . 1 4

0-590

0.0150o.00750.m250.01000.00500.01500.0050

0.007s0.0't500.0to00,00250.01500_00500.0050

0.0r500.00750.00500.0150o.0025o.01000.0050

0.00750_01500.01500.01000.00250.00500.0050

0-0150o-00750.01500.00500.01000.00250.0050

o.00750.01s00.00250.m500.o100

1.251251.251.251.251.25125

1.251.251_251.251251 .25r.25

88.+10879108

55.+11587.+110f7.[-1097A_2-l1A85.1-' l l9

79-10882.3-t087A2-l1A771-10987T11055.S11585.1-' l lg

Selenium

Lead

Chrdnium

cedmium

Silvergadun

ouptkats n0314@{uPtl

94

s0

0891949S

s0s4s0ln54s698

9l

90q'

9'r

202020n20

n

ua7a784914Ts2

m2020

20

7

8

I

E

1 0

Xatru Solke o031{O8-lts l I SosiEs: 5A59517.{1

Pr€pared: 2+itar47 Anatyr€d. 24-MaF07Lead

Selenium

SilY€r

Cadmium

Chaomium

Earium

Pr€pdred: 23+/ar-07 Anahlzdt 244n€'47SebniumL6ad

Chromium

S{ver

Caddium

Bariu|n

L6ed

S€ledum

Cadn*lm

Chmmium

Silver

0.0280gRL

BRL0.0926BRLsRr

0_0132

r.221 . 1 4

1.24

1_18

1 . 1 4

125t151.251.25r251.251.25

1251.25t.251.251.25

0.0261BRLSRLARL8RLBRL

0.0120

BRI-00319BRL

0.0130BRLBRI

0.0rs8

0.031sBRLBRL

0.0130sRr-

80.4-10581.&10579,2n0681.5-l1163.Fr09864-10a86-9-114

8t.&10580.+10586.4-t0881.5-t | 1€i].&lm

20mmm2020

1,13 mSn1.21 mdl1.13 mg/l1..t6 msn

0.672 qM8 n€/l122 rEI1.24 mCrl

Llrlx Splke Our AOgl{OE{SDlt SourEe: SA595t741

Prepared: g3-Mar{7 Analyz€d': 24 -Met47

0-80-9

52

Thk lzbordoq rya.t it not wlld utilhottt en attfiorfuat slga4ltan oa thl .nvr l4ge .

r Reportable tt€r€cti,on Limit BRL = B€low RAo.tiEgLiEit Page 120 of 124

Page 592: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Metals by EPA l3l2 & 6000/7000 Series Methods - Quatiry Control

Flag Units

mgnm9n

frE/l

tnsnmgr'lmsnmgnmq,4

Spike Source

Level Resuft

%RECR€sult

1 . 1 5

1 . 2 7

1 . 1 4

1.23

0 958

1 . 1 5

1 . 1 S

1 2 4'1.27

0.01500.0050

0 01500.00750.01000.0150o.00500.00250 0050

1 2 5

1 . 2 5

1_25

1 . 2 5

1 . 2 5' | .25

1 . 2 5

1 . 2 5

1.25

BRL

0.0r98

BRL

0.0319

BRL

BRL

0.0130

BRL

0_0198

79.2-106

88.9.114

11.7-108

80.!108

61.7-107

79.3-107

18.1-114

86.5,109

86.6-116

I-imits

66.6-117

%RF-C

Brtch 7031{08 - SW845 30r0A

t efix Splks Oup P031108+ISO1) Source: SA59517{iPr€€ared: 23 €r-O7 Analyz€i: 24-Mat47

gadum92'r00

2020

Post Solt€ 17031 {tt8+Srl Sourc€: SA59517{l

Prepared: 23{ar-07 Analyzed: 2+Mat47

S€lenium

Lead

Slver

Chmmium

ftdmium

Eadum

Brtch 713 l4{9 - EPA200/SW7000 S€ri€s

Elank 17031409€LKll

P.€pe.ed:23-Md47 AnaIWd: -Ma?07

9 l

96

77

92

94

9!)

100

8RL ms/

mg,4

0.00040

mq,4 0.000!0

ms,4 0.000,10

0-00250

8RL

0_00250 BRL 107

Dupl|car€ fl03laogoUPll So{rce: SA595l7-12

LCs f70: 409€51)

Pr€p*€d: 23-lrar-,07 Analfred: 26-Mar-07

M€rcury 0.00255

fteptr€d: 23-lvlar47 Anavzet 26-Mat 47

Pr8p{ed: 23411 'J-07 Analyzed: 264tar -D7

Memrry 0.0$267

Pepared: 23-Mar{7 Anal]rzed: 2AMar47

M€rorry 0 00250

0 00040

l|ebir Splke flqll40g-Ms'l I Source: SA595t7-01

l|atix Splke DLb ft031rog-irsoll Source: SA59517.01

Prep{ed: 23Jutar47 AnatFed: 2&Mar-07

Merc!ry 0.00249 mgn 0.00040 0.00250 BRL

Po3t Sol*o ?031409.PS1 I Source: SA59517{1

7 6 1 - 1 1 1

7 6 . 1 - 1 1 1

66-8-'lr0ng/l 0.00010 0 00250 BRL

100

100

Ge[eral Chemlstry Parameters - Quality Control

Brtch ?031429 - cenerd PteD.r.tion

Dudicst fl031429-ouPt)Pr€par€d & AnElf2ed: 23-Mar{7

% Sollds

OuEllcat. fro3146{t.DUP1)

Prepared & Analyred: 244rar-07Yo Solidg

Brtch 7031{63 - C'e eral Preprrodotl

Source: 545051741

SourE€: SA5945l{h

87.4

% 87.4

87.8

0 1 20

20

This labontory EForl is dot vdid rvuhoA an aUhori|ed sig tature ott the cowr page _

+ Reportable Detection Limit BRl, = Belon' Reporting Lirhit Page 121 of 124

Page 593: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Notes and Definitions

*TPH Calculated as

Comp Completed

Field Preserved

QCI Alalyte out ofaccepmnc€ raoge.

QC2 Analyte out ofacceptance raage in QC spike but no rcportable concentr8tion presedt in sampte_

QCa The spike recoyery is outside ac{eptable limih for the LCS. Th€ bakh was accepted bas€d upoq the MS aod/ot MSDme€ting the LCS limih criteria.

QM7 The spike rccovery was ourside acceptance limits for the MS anvor MSD. The barch was accepted based oo acceptableLCS recovery.

QM8 The spike recovery exceed€d the Qc conhol limits for tte Ms aod/o. MSD. The batch wrs accept€d based upooacaeptable PS and./or LCS r€cov€ry.

QRI A.nalys€s ar€ oot co rolled on RID values ftorn sample conceDtmtions less ihan 10 times the r€porting limil QC batabaccepted based on I,cS and/or LCSD QC results.

QR5 R-PD out ofacceptance mnge.

QR7 The RPD exceeded the QC control limits; however precision is demoostrated wift acceptable RPD values for batchduolicate.

R05 Elevated Reporting Limirs due to the p.ese[ce ofhigh levels ofDon_target analytes.

S02 The surrogate recovery for this sample cannot be accurztely quantified due to intedererce ftom coeluting organiccompounds present in the sample exhact.

SGC Surrogate rccovcry outside of cooEol limits. Th€ data was accepted bas€d on valid recovery of the remahing suFoga@.

vex? Field eKFacted

VOC8 Reponiog limits r€flect SW846 5030 extraction tecbnique due to marrix interferetrce usitrg SW846 5035A extraotiontechdiquc.

BRL Below Reporring Limit - Anab/te NOT DETECTED at or above rhe rsportine limit

dry Sample .esults reported on a dry weight basis

NR Not Reported

RPD RelaJive Percent Difference

A plus sigfl (+) in the Method Refereqce colwnn indicates the mcthod is not accaedit€d bv NELAC.

Thb labontoq tqrort ls ,ol valid without an ea6odz.l signaa c od lt e @wr page.

. R€porrable Dctcdion Limir BRL = Below ReFoning Limir Page t22 of 124

Page 594: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

InterDretation of Total Petoleum Hvdftlcarbon ReDort

Petroleum identilication is detetmin€d by comparing the CC tLogerprint obtained from the sampL€ \\,ith a library ofGC fingerpnntsobtained from analyses ofvarious petroleum products. possible match catesories are as follows:

Gasolioe - itrcludcs regular, unleaded, prernium, etc,Fuel Oil #2 - includes home heating oil, #2 fuel oil, and dieselFuel Oil Il4 - includes #4 firel oilFuel Oil tt6 - includes 116 fuel oil and bunker ,,C" oilMoto. Oil - includes virgin and wast€ automobile oilLigroin - includes mineral spirits, petroleum taphtha, vm&p naphthaAviation Fuel - includes kerosene. Jet A and Jp-4Other Oi[ - includes lubricatirg ard cutting oil, and silicon oil

At tirnes, the unidentified petroleu.rn product is qua ified using a calibration that most closely app.oximates the disrributiotr ofcotnpounds in th€ sample- Wtren this occurs, the result is qualifisl a.jl *TpH (Calculareo as).

Laboralorv Cootrol SamDle fLCS)i A known matrix spiked with compound(s) representative ofthe target analytes, which is used todocument laboratory performa.nce.

Marrix Duolicate: Ad intralaboratory split sample which is ussl to document the precision ofa method in a given sampl€ matrix.

Matrix Soike: An atiquot ofasample spiked witha known conccntmtion of target analyte(s). The spiking occurs prior to samplepreparation atrd analysis. A matrix spikc is used to document the bias ofa method in a given sample matrix.

Method Blank: AD aDalyte-free matrix to which aLl reagcDts are added in the same volumes or proportions as Lrsed in sampleFocessilg. The method bLank should be carried through the complete sample preparation and analydcal procedure. The methodblaok is used to document contamination resulting from the analytical process.

Melhod Det€ctioo Limit (MDL): The minimum conceDtration of a substatrce that can be measured and reported with 99%coofidence that the analyte concentration is greater than zero and is determined ftom aialysis ofa sample il1 a given matrix tt?ecoEtainiag the arElyte.

ReDortable Detection Limit (RDL): The lowest concentration that can be reliably achieved within specified limits ofptecision andaccuracy durilg routinc labolatory operating conditions. For many analytes the RDL analyte conc4nt.ation is s€lected as the lowes!Doo-zero standard in lhe calibmtion curve- White the RDL is approximately 5 to l0 times the MDL, the RDL for each sample takesitrto accouot the sample volume/weight, extract/digestate volume, cleanup procedures and, ifapplicable, dry weight conection.Sarnple RDLS ate highly matrix-dependent

Sunogatel Ar organic compound which is similar to the target anal,,te(s) in chemical composition and behavior in the analyticalplocess, but which is not nolmalLy fould in environmental s|mplcs. These compounds arc spiked into all blanks, staDdards, andsamples prior to analysis. Percent recoveries are calculated for each surosate.

Validated byiHanibal C. Tayeh, Ph.D.Nicole Brown

Thk labonlory rcINrt is ^ot tlzlid ttithout aa sathotjzed slgraaure onlhe coeer poge.

' Reportable Deteciion Limit BRL = Below Reporting Limit Page 123 of 124

Page 595: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

State Of ConnecticutDeparunent of Enviro nental Protection

I^aboratory Quality Conhol and Quality Assurance Form

r The @mpounds udor.len€nts e?ortd!rc a eccificrllyiEqGsred by he clidt on rhe cl8in ofc{siodyond iD $nre cd€s tuymr hctude rhe tullatral'tc list 33 &6nsr in rh. m.'hod.

Negolive rc4tomes for 4 B ond C orc sd&essed in a cese norrulive on the cowr pqe of this rcport

I, the dndersignel, aaust andcr rte psias and perralria ofpeiary thal bssed u!,on ny penonat inquiry ofthose rcqonsiblelor oblaiaing the hformalio4 the ,,raleriol coafainod in this analyticd iqort is, b rte besr o! my h,towtedge oatt befieJqccurab Qnd con plctc-

nfr#-Hanibal C- Tayeh, Ph.D.Presideot{-aboEtory Director

D e: Y2A20O1

Labomtory Namc Spechum Analytical, Inc. - Agawam, MA Proiect Name aod Number:

Project Location: NHRY M8 Ac{eptanc€ Facility - New tlaveD, CT NHRY M8 Ac{cptarce Facility - Ne,r Haveo, CT/

Tbis Form Provides ceflifications for the following drta set:sA595L?,01 SAs9Jl7-ll

sA595t7,02 SA595r7-12

sA59517-03 S&.9517-ll

sA59517-04 SA59517,14

sAJ95l7-05 SA595l7-t5

SAJ9J | 7-rX

sA595 t 7-il7

sA595l7{6

sAJ95l7{9

s,\595l?-t0

List Sp€cific Anab'ticzl Medrods Used:

+CT ETPH

EPA 2OO.?

EPA 245.t 174704

SM254O C Mod

sw 846 E!608

s w E 1 6 l l t 2

sw8{6 L3r26010B

SWSil6l!127470A

sw845 60loB

sw846 r47lA

SWE,I6EOEIA

swE46 t0t2

swE45 82608

SW8,l6 8270C

sw845 8270(yEPA 6?5 |

voc

Sample Manices:

SoiUSedidmt

Were all samPles receiv€d by the laboiatory iD a condition consisteotwith thar described on the Chain of Custody documedtation for the dataset?

E! Yes E No

BWerc all Q'QC prccedures required for the sF,€cified anatlticalEethod(s) included in this report followed?

El Yes E No

c Were all QC performance standards ard a€commetrdations for th€specifi ed methods achieved?

E Y e s E N o

DWere iesults for all arulytelist compouddvelemeots for the sp€cifiedmethod(6) reportad? B Y e s E l N o .

This labonlorf wporr is aot voIU vdrtant da aslharized sigrentrc oE th. coret pagc .

' Repo.trble Der€ctiofl Limit BRL = Betow Repo.ting Limir Page 124 of 124

Page 596: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

E

s

5

45?

e-6 '

H@dquart^.11 Alnyer.Dtive & 830 SitvnSrEr. Acsw, MA 0l0ol . 1,800-7E9,9115 .4lt-7t9-90rE . FAx 4l l -7s9-rto?6ll rivirior: 8l E0 wodland C€nter Boulcvsld . T.mps, FL 136t4. l-888-49?-j270 .8r3-t8t-9507. FA.l( 800-48044jJ

www.6pectrum-€naltrtical.com Pege I of2

Page 597: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 598: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 599: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 600: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Saoole IdentificationFB-3sA5964 t- l8

Client Proiect #l0l -88

MatrirBlank Water

Collection Date/Time21-Mar-07 00:00

Received22-Marn'l

CAS No. Analla(s) Flag Unib tRDL Dilution Melhod Ref Prepaed Ana\,aed Eatch AnaDst

Yohlil€ Orgrnic Compould3

Volatile Oroanic Comoounds bv SW846 82608Prepared by method SW846 5030 Water MS7&111'1,1,2-Tricf i lorohifuoroethane(Freo€RL674-1 Ac€tone BRL107-13.r Acr},tonitrite BRL7113-2 Benz€ne ERL10E-86-1 BmmobefEene BRLf+97-5 gronrodlloromethane BRLf5-274 grornodichloromethaDe BRLf+2U2 grcmoform BRL74419 Brornonethme BRL7€-9!3 2-Bulsnone (MEK) BRL10+51{ n-Butylbenzene BRL13f,9€J s€c-Butytbenzehe BRL98.064 t€rt€utytbenzene BRL75-l!0 Carbon disutfide BRL56-23-5 Carbon tehachtoride SRL10&90-7 Chto.ob€flzene BRL754rL3 Clrlo{oethen€ ARL6t€83 Cftoroform 8RL1147.3 Cruoaoflehane 8RLss-4e8 2-Chlomioluene BRL10643-4 +Chlo,rotoluene BRL116-12{ 1,2-Oibroarp3-Chloropropane BRL124-4+1 Dibrornoct{oromethane BRL1fi+93-4 |,2oibrornoethane(EOB) BRL7ir€:.3 Dibrornornethane aRL96{G1 'l,2oichlorobenzene BRL54i'73-1 '1,3-Dicl{orobenzen€ BRLllE-{&7 l,4oichlorobenzene BRL7*714 Oicilorodinuoromethene (Freonl2)BRL75-34-3 'l,I Oichloroeth€ne BRLi0ru6-2 |,2-Dichloroethane BRL/5.35-4 |,l-Oid oroefi€ne 8RL1ss5s'2 cjs- 1 ,2-Dichloro€then6 BRLl5s€o5 tans-1.2-Dichlofoeth€ne BRL78i7.s l.2-Diciloropropane BRLr12-2&s 1,0-OichloroproF,ane BRL594-2e7 2,2-oichloropropane BRL563-584 1, t-Dichloropropene BRL10061{1-5 cis-1,3-Dichloropropene BRL10061{2sbans-l,3-Dictloropropene BRL100{1-4 Ehyibe{Eene BRL87{U3 Hexachlorobutadione BRLs91-78{ 2-Hexsnone (MBK) BRL98{2-g lsopropylbenzeoe BRLso{?4 +bopfopyltoluene BRL16344+4 Methyl tert-butytether BRLloercr +Methyl-2-pentanone(MIBK) BRL75{gz Methylene ctlodde BRL9l-203 Naphth6lene ARLl0l6tl n-P@pylberEene BRL

pg/lpgn

!g/l

!g/l

!El

!gn

lJ9./l

!gn

!sn!El

!gn

!91

ttgrl

!g/l

ugn

lr!yl

!dlpEl

!El

tjElpg/t

!El

t,gl

trgl

rr(yr

|lEl

rrtyl

|lEl

FS/l

!!yl

!gn

ugl

!gn

!gn

!sn!dl

!dl

t'Erpgtpgl

!gl

!g/l

!El

u9nugnpgn

u!|/luEl

Fg/l

pg/l

1 .020.o0.51 .01 .01-00.51-02.O't0.0

1 .01 .01 05-0'1-0

1 -02.O'1 02.n1_01_02.00.50.51 01 01 01 0

2.O't _01 .01_01 .01 .01 .01 .0

1 .0't .0

0.50.51 .00.510.01 .0

1 .0'1 010-05.0' | .0

1 .0

SW846 82609 2741ar47 27^tar47 1031617 RLJ

Thit hbo4lory rcpod is ,tol vau ,,ilhaqt on aulhottzcd signaaa'? on the cover psgc

' RePortable Detection Limit BRL = B€low R€poning Limit Page 9l of 165

Page 601: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationFB-3sA5964l- 18

Clieot P.oieat #30 t -88

MatrixBlank Warer

Collectiotr Date/Tim€2l-Mar47 00:00

Received22-MaF07

CAS No- A,rabac(s) R,fnI Fhc 'RDL Dilubl Method ReJ PEpamI Analyed Balch An4lfsl

volrtile Orgrtrlc Conpounds

Volatile O.qanic Compounds bv SW046 82608Prepa.ed by mehod SW846 5030 Water MS100-42-5 Styrene BRL63c2o€ 1,1,1,2-Tehachloroethan€ BRL79-345 1,1,2,2-Tetrad oro€trane BRL127.184 T€hachloroothene BRI_108-8E-3 Toluene BRL87-61-6 1,2,$Tridttorobenzene BRL12o.a2r .1.2.+Tridllorob€nzene BRL71-56.6 1.1,1-Tfidlloroethan€ BRL?g{Gs 1,1,2-Trid oroethane BRL79{1{ Tdcfilo.o€thene BRL75-69-4 Tricilorofluoromethan€ (Freon 11) gRL

96-1&.4 l,2,lTrichloropropan€ BRL95{3€ 1,2,+Trirnethylbenzen€ 8RL10s67{ l,3.5.Tdmeff.|ylbenzene BRL75414 Vinyt citoddet330,&7 m,pFxylene9f!47$ o.Xylene1099€-9 T€trahydofuren60-29-7 Ehyl eher991-05{ Tert-amyl methyl ether617-923 Efiyl left-butyl ethert0&20n Diisoproptether7t65-O Tert-Butanot / butyl alcohol12+91-1 l.+Dio/6ne

&raogats .Ecoveresr46orn4 4&ofltof,uorcbenzene

m37.26-5 Tdluene4S

I to6o474 1,24ic @@thane-d1

BRLBRLBR!BRLBRLBR,LBRLBRLSRLgRL

92101106

t03ta68-53.7

SW846 62808 274nar47 27-Mar47 7031617 RLJ

+Cr ETPH 2&Mar-07 2&l,rar47 7031505 DS

pSn 1.0

ttil '!.0

ldl 0.5

tldt 1.0

ttgfl 1.0',/gtt 1.0

t4 1.0

lgn 1.0

FSn 1.0

VSA 1.0

Vglt 1.0

Udl 1.0pdi t-0

Itgll 1-0

rc 1.0Fgl 2.opdl 1.0

Fdl 10.0

ItdI 1.O

rlglt 1.o

t!{ 1.0

t4 1.0

t'eI 10.0

t'gn 20.0

70,130 %70 tm%7o-130 %70-130 %

lrg/l 0.I

mC/t 0.1

lnSI 0.1

mg/l 0 1

mgn 0.1

mSn 01

fi€I 0.t

'nsil 0.1

m9 0.1

ngll 0.1

4L14O %

sglt(/l

Ertr.ctrble Petrcl€um Hydrocsrbong

Extractable Total Petroleum HvdrocatuonsPtepa.ed by metlod SW846 3510C8tx)6€1.9 casoline6847d-3112 FU€l C)il #26€47631.3 Fu€l Oil ,f46&553-00-1 Fu€t Oil ,t6illlggtoooo Motor Oil$olfiiulo Aviatjon Fu€l

thidentifiedOf|er Oll

Total Petoteum HydroaafionsCgC36 Aliphatic Hydroc€rbons

Sarnogal€ r€coy€nbs:3386-312 1 -Chloro@tadecane

Semivobltl€ Ory.iic Compo trdr by CC

Oroanochlorlne P€sticides SW646 8081APreparcd W mefpd SW846 3510C3094G2 Aldfin319-64{ 6-BHC

BRLBRLBRLBRLBRLARLBRLBRL

BRLBRL

119

BRLBRL

0 . 0 1 1 1

0.011'1

SW8{6 8O01A .^lsr47 &4{47 7031497 lG

Thjs labodor! rqorl is ^oa saM ',/ilho'n s.t tsthorizc.I slgn,',t re oa lhe coie Fsge -

r Repo.tdle Dotection Limit BRL = B€low Repoding Limit Prge 92 of 165

Page 602: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample JdeotiftcationFB.3sA5964r-r8

Cli€nt Proiect #l 0 t -88

MatrixBlank Water

Collection Date/Time2 t-Mar-07 00:00

Receivcd

22-Mar-07

CAS No, A"alrk(s) FIog Uni'l DiIAiofi Method Retr. Prcpated Analycd Ba.ch Aietyst

Semivolrtlle Otgrnic Compounds by cC

Oroanod odne P€sticides SW846 8081APr€pared by mslhod SW846 3510C3t9-et7 b"BHc3i9-€6{ d-BHC58499 S-BHC (Lindane)57-71-9 chlordane72-5{J 4,4-DOD (p,p')726$e 4,{.-DOE (p,p')50'2s3 4,4.-DOT (p,p,)@-57-1 Dietdrinc5$$4 Endosulfan I3321165-9 Endosufan ll1Ar{7€ Endosulfansultate72-2O-A Endrin7421€3!4 End.inAidehyde76-44.4 Heptachtor7?-435 Mefnorychlor10?4-57-3 Heptachtor Epoxidemo1++2 Toxaph€n€5108-7r-9 a-Chlodane€,566347 gchtordane53tg|70-5 Endrin Ketone

Sa|Iogate €cou.enes:1 0186-8+2 4,+DB4danuorouphenyl (Sr)mg-2+3 Decechlorobiphenyl (Sr)

Polvcfilo.inaled Biohenvls bv SW846 8082P.sparcd by melhod SW846 35i0C12674-11-2 PCB 101611104-?d-2 PCB, 12211114r-1615 PCB 1232s346+21-e PCB 124212672-2s{ PCB i24811007{+1 rcB 12541i0€6{2€ rcB 12603732+ts'5 PcB 1?621 r 1{X}14-4 rcB | 268

Slnro$l€ ,€cov€rfus:ro38e8/-2 4,4O&Octafl uorobiphenyt ( Sr)2o51-21-j Decachbrobiphenyl (Si

S€nivobdl. OrS.nic Compounds by C.CMS

BRLBRLBRLBRLBRLBRLSRLBRLBRL

BRLBRLARLARLBRLBRL

BRLBRLBRLBRLBRL

14077

ERLBRLBRLBRLBRLERLBRLBRLBRL

5085

BRLBRLBRLBRLBRLBRLBRLARLBRL

pgn

tlgllug,

FSnpEl

!9n,J(ylp9l

r91lugtlps/l

pgl

1.,91

u9/l

ugrlrg/lpdt

!g/l!sl!qn

0 0 1 1 1

0.0 '1r1

0 _ 0 1 1 1

0.0556

0 0 1 1 1

0 . 0 1 1 1

o.ot11

0.0022

0 . 0 1 1 1

0 - 0 1 1 1

0 _ 0 1 1 1

0 0 1 1 1

0 _ 0 1 r 1

0 . 0 1 1 1

0 . 0 1 1 1

0 . 0 1 1 1

0.0556

0.01'11

0 . 0 1 1 1

0 . 0 1 1 1

3rr150 %3c-154%

sw846 8081A

sw846 8082

sw846 6270C

1

1

1

I

1

1

1

1,1

1'I

1

I

I

I

I

l

1

1

1

26-Mar{7 26-l.,lar-07 7031437 TG

pg/r

pgn

t)g

l.rEl

!dl

!sflpgl

tlSJl

ugl

Wnp(yl

!g/li.isnp{vl

!g l

Ljgl

!slu94

0_02220 02220_02220 0222i_0222o_0222o_0222o 0222o_0222

2GMar-07 26-lv1aF07 7031496 SM

30-150 %30-150 %

Semivdatle Orcanic Comoo'.lnds bv SW846 8270CPrcpared by m€lhod SW846 35'l0C83-32-9 Acenaphthene2O&9H Acenaphthylen€9Gr24 [email protected] Ar ine12G12-7 Atthracenel9l2-2+9 At?zine1fi13!3 Azobenzen€y'Diphenyldiezine9247.5 Benidine56-513 B€nzo (a) anthracene

26-Ma.47 2g-Ma(O1 7031499 M.A1_000.4001_001.00.t.00

r.001.001.00

0200

Thb labontory rcport Lt ,rol .olU wirho& rE laahoriaed sbfiature on the cover psge .

' Report!5l€ D€tection Limit BRL = Below Repor.ine Limit Page 93 of 165

Page 603: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdedtificationFF3sA5964l-18

Client Pmiect #301-E8

MatrixBlank Watef

Collection Dale/Time2l-Mar47 00:00

R€ceived22-Mat4'l

CAS No- Aaslyu(s) Flag "RDL Dilation Mdhod nel. PEpand Aazlyatd Bdth At olfst

SeEdvol.lile Org ic Compouods by GCMS

S€mivolatile O.oanic Comoounds bv SW846 8270C

Prepared by rnsthod SW846 3510Cs0-324 Bdlzo (s) pfene205-9S-2 86tE0 (b) ffuoranthene191-?+2 B€rEo (g,h,i) Ferylene20ru8.9 Eeruo (k) fluoranthene65{54 g€nzoic acidlCXl51{ Benzyi alcoholr11.91-1 Bis(2-chbro€thoxy)mehane11 l-444 8is(2-cfitoroethyt)ether3so3&32-9 Bis(2rhloroisopropyl)ethe.117-81.7 Bis{2-€hylf€xyl)phhalate101.H +Bornofienyl phenyl et|6a85€&7 Butyl b€nzyl phthalato86-7+8 Carbazol€sg-sll.7 +Chloro-lm€thylphenol106-47{ 4-Cf{orc€niline91-5€-7 2-Chtoronaphhelene95-57+ 2-Chloroptr€nd7005-2-3 4-Chlomphen/ phenyt e0Erle01+ Chrlrs€ne53-703 Dibenzo (a,h) anthrac€ne13?-6,1.9 Dib€.Eofuran9s-5o-1 |,2-Dichlorobenzenos{1.?iln l,}DicNdbb€nzene105-4G7 l,4oichhrobenzene91-9.{-1 3.3-Dlchlorob€nzidine120312 2,+Oichloroph€nol8.16&2 oied.|yl phhalate131-11-3 Dimethylphthalatel0s7-s 2,+Dimethylphenolu.71-2 Di-|}S'nylphthalateS+s2-1 4.GDinitro-2{ethylphenol51-2&5 2,+Dinitrophenol12r-1il2 2,+Oinitrotoluen€60G20-2 2,G.Dinitsoitolueoe117{r{ Oin-od}dphthalaG20€-4,r{ Fhotranthene86-7+7 Fluofene11+74-l Helaclilorob€rrzene87S&3 Hexadtlorobltradi€n€n474 Heoadrlorocyclop€ntadiene6l-72-1 He)€doroethanslc+3s-s Indeno(,|,2,3d)pyrene78{s.i lsophod€9157{ ?-l{€thylnaphhalene954&7 [email protected], 3,+Melrylph€nol1&11-5si+o-3 Nephthalene8,i-14-4 2-Mbo€ndine

'NiltE€nilineioerx{ +Nltroaniin€

BRLBRLBRLBRI-BRL

sRr_BRLBRLBRIBRL8RLARLBRLBRLBRLBRLBRI-BRLBRLBRLBRLARLBRL8RLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRI-BRLBRrBRI.BRLBRLBRLBRL

BRLBRLBRLBRL

FSn!!nus/l|lsnpsn

!41pdl

Itgl|lsnugll|gr'lt4FSnw!dlpdl

!dl

eglusnudl!tylldlpsn

wltstlpsnFSn!Eltgt!dluglpgl

rrdlt c lt grl

wpgnpc4pdl

!dlfldl|ldl|lgt

pgnpdl

l€it

||gn

wEr{pcn

[email protected]

0.3001.00'1.00

1.001-001.001_00L00

1.00|.00r.00r.00r.00

1.001-001-O0

o.2001.00r.00r .@

|.001.00|.00l.oo1_001.001.001.001.001.()0t.mt .m|.00t.001.oo

0-6001.001-00

0.2001.001-001.0010,0

t.m|.00r.001.00

?:hls t4brdory ppora ls ,tot wIU *i hoar tE osrto;Z..|stgnofrtE on tha @E page.

I ReporrEble Dei€ction Li&it BRL= Below Reportine Limit Page 94 of 165

Page 604: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SafllDle ldentificationFB-3sA59641-18

Client Proiect #30r-88

MatrirBlank Water

Collection DatdTime2l-Mar-07 00:00

Received22-M^t-07

CAS No, Analru(s) FIsE |RDL Dilutioa Melhod ReL Prcparcd Ana4zed Batth Anabst

Semivolsdl€ Organic Conporndr by cCMSSemivolatile Oroahic Compolnds bv SW846 9270CRepared by method SW846 351 0C

98+s3 Nitrob€nzene88-7t5 2-Nittophenol100{2-7 4-Nitfoph€flol€-7sg N-Nitrosodinethylamine6?1{4-? N.Nltrosodi-n-propylamine86JO{ N-Nitrosodiphenylamine87{+5 Pentachtorophenol85{1{ Phenanthrene10F9r2 Ph€nol129&, ryren€11G€6-1 Pyddine120+2n 1,2,+Tnchtorobenzene95-S5-4 2,4.tTrichtorophenole6{F2 2,4,GTricilorcphenol

S.r,n€at€ recov€flbs:i2t40-o 2-Ftuuobiphenyl36'7-124 2-Fluorophercl1165404 Nitrchenzene-ds110162-2 Phend4'171a-814 Terykenyt4411d-79-5 2,4,6-TrbrcmophenotSVOCS bv SW846 8270C SIMP.eparcd by melhod SW846 3510C83-324 Acenaphthene

208-96.{ Ac€naphdrt4ene9G12{ 1-Methytnaphthatenel2Gl2-7 Aithrac€ngfG55-3 Benzo {a) anthracene$-32{ Benzo (a) pyrene2os-2 BerEo (b) fuoEnthene191-24-2 Benzo (g,h,i) p€rytene2tru8€ Benzo(k)fluorantfEne21&014 Chrys€ne5&70.3 Dibgr]zo (a,hl [email protected]]Lo Fluoranthene8&73-7 Ffuor€nei9ix9{ Indeno ('|,z,}cd) pyrene9r€74 z-Methy'naphtnalene9l-?0-3 Naphthatene85.01{ Phenanthrene129004 Pyrene

&,'|oga(e fEcov€nbsi321{0-8 2+luotobiphenyl1718-514 Tedlenyl4l4

Told M€rrb by EPA 600M000 Series M€thod3

8RL

BRL

BRL

SW846 8270C 26-Mar-07 29-I,tar47 7031499 M.BBRLBRLARLBRLBRL8RLBRLBRLBRL8RLBRLBRLBRLBRL

737780689250

BRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRL

BRLBRLBRLBRL

8398

pg/l 1-00

!g/l I 00

!S/l 1.00pg/l 1.00pdl 1.00

ldl 1.00

USx 1.00pg l 100pdl 100

Lidl 1.00

!S/l 1.00

ldl '1.00

Ug/l 1.00

l4/l 1.00

30-130 %15-110%3G130 %15-110 %30-130 %1u110 0k

!g/l 0.050

!g/l 0.050yS/l 0.050

Ug/l 0.05t)

trg/l 0.050

!g/l 0.050

!g/l 0.050pg/l 0.050

!g/l 0.050

US/l 0.050

tlglt 0.050pSn 0.050

udl 0.050

lSn 0.050pdl 0.0sopdl 0.0so

!s,4 0 050

!S/l 0 050

3G1m %30-130 %

mg/l 0.0050

mgl 0.0040

ms,4 0.0050

1 sw846 8270C/EPA625 StM

'1 "

1 "

1 '

1 '

1 '

1 "

1 "

1 '

1 "

1 "

1 "

1 "

1 "

1 "

1 "

1 '

1 '

28-MaF07

A4t-22-4 Silv€r

744ft&2 Alsenic

74,()1393 Bsrium

1

l

1

SW84660108 27-Met47 2A-Mat47 7031619 LR

Thit laborsaoq rcpon is not valid *ilhou an sulhotiae.I sigdaluft on the covet page .

' ReDortable D€tection Limit BRI- = Below ReDortins Limit P€e 95 of 165

Page 605: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole ldentificationFB.3sA5964l-18

Client Proieot #l0tt8

MaffixBlaEk Water

Collection Date/Time21-Mar-07 00:00

Received22-Mat41

CAS No. Analyu(s) FI8C 'RDL Dilattu',| Melhod Rdtr. Prepared Analwl Botth A&lys!

Torrl M€rrl6 by f,PA 6lxxy7000 s€rlfl Merhod!

zl40-43€ C€dmium BRL

7440.47-3 Chromium ERL

7439€2n Lead BRL

7782a+? Selgnium BRL

Tor.l Metrh by EPA 200 S€ricr Metftods

743947-6 Mercury BRL

sw64a 6010s 27-Ma'47 m lar47 7031610 LR

EPA245.tn470A 2t.Mat47 28.tto'47 7031620 YP

ng/l

mgn

msnmg/l

0.0025

0.0050

0 0075

0.0r50

0.00020

t

I

'|

1

mgn

Thjs bborolory repod b Nt eabd wllhot ur audtoriaeil slgn tLr. ot the coaer pag..

'ReporEble Detection Limit BRL= Below R€porting Limit P€e 96 of 155

Page 606: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificarionTB.3sA5964 t- l9

Client Proiect #30t-88

MatrixBlarl Water

Collection frate/Time2l-Mar07 qq:t 0

Reccived22-Mar-07

CAS No- Aialy,Ek) Fl"g Units 'RDL Dilation Method Retr. Preryr.ed Aaaltzed Barch Ant lrsl

Volrtil€ Org.rtc Compounds

Volatile Oroanic Compounds bv SW846 82608Prepared by rnebod SW846 5030 Wat€r t\tsu6-l+t 'l,1,2-T.ichtorotriflu6oethane (FreoBRL67{+1 Acetooe 8RLi07-13-1 Aq-ttonitite BRL714}2 Benzene BRLi0F€6-1 Bromob€nzone BRL7+Sf-5 Bromochtoromelhane BRL7+2f4 Bromodichtorornethane BRL712+2 Bromoform BRL74{34 Bromonethane BRL74413 2.&ltanon6 (MEK) BRL10+51{ n-Butylb€rEene BRL13+€8{ sec-Butylb€nzene BRL

tgrt€ltylb€nzene BRL7+rs-0 carbon disuttide BRL56-2+5 Carbon tetrachtoride €RLr08€G7 ct orobenzene BRL75{&3 chloroefhane sRLa7{&3 Chlorolorm BRL74{7.3 Chloromethane BRLs5.494 2-Chtorototuene BRLio s-4 4-Chlorototuene BRL9612-a 1,2-Dib|omo-3-chtoropropane BRLt2{-4&1 Dibmniocl{oromehan€ BRL1Fs3-4 .1,2-Dibmmo€thane(EDB) BRL7445n OiblomonEthene BRL95{+1 l,2.Dicruofobenzene BRLar4t-73-r l,3-Dichtorobenzen€ BRL106-1G7 l,4-Oichlorobenzene BRL7rf14 Dicfilorcdifluoromehane(Freoni2)BRL75-3+3 1, t-oi{:t oroethane BRL1074G2 1,2-oichlo|oethane BRL7t35>4 1,1-Oii:htoroethene 8RLt5$5€-2 cis-1,?-Dichloroethene BRL1s€-0G5 fars-.1,2-0idtloroetheno BRL7a{7-5 l,2-Dictrloropropane BRL142.2€€ l,}Dichloropropane ERL594-2G7 2,2-Dichloropropane 8Rf563.58€ 1,l-Dhhloropropene BRLlllu61.o1.5 cis-1,3-Dichloropropene 8RL100614{ h?ns-1,3-0idllofopropene BRLtot}.tl-1 Edrylb€nzene aRL87'6&3 H€xechlorobutsdiene BRL5e1-76{ 2{{exEnone ([rBK) BRL98+23 lsopropylbenz€ne BRL9S{76 +lsopr@yltoluene BRL163.44-1 Methyl left-but,,1 eth6r BRLroetGl 4-MedlM-2-pentanone(M|BK) BRLIs0s2 Methylene chlorid€ BRL91-zL3 tlapht|abne BRLl0+€+1 n-Propylb€nzene BRL

UMyg/l

!g/l

pgnpg/l

trg/l

!snlj(/r

!91

!gn

!g/l

!g/l

!91

ug./l

u g lpg/l

pg/l

!gn

!gn

!!,./lp{yl

p(yl

pql

pgl

pgl

plyl

plyl

!sl

!g/l

u9n!9n!dl

!9/l

!g/l

!9n

!gn

Lj9lp9l

tl(yl

uElysll

!Et

Lrg/l

rcnpgl

pgit

uglpg/l

pgl

ygrl

1 .020.00.51 0'1.0

1 .00.51 .02.O10.0't _01 01 05-01_O1 0

2.O1.02.O1 .01 .02.00.50.51 .01 .0l_0't .0

2.O1.01_01_0

1 01 .0

1 01 01 .0'1.0

0.50_51 .00.51 0 0'1.0

1_01 .Dr0.0

5-01 -01 .0

1

1

1

1

1

1

I

1

1

1

1

1

1

1

1

1

1

1

1

I

1

1

1

1

1

1

I

1

1

1

1

1

1

1

1

1

I

I

1

I

1

I

1

1

1

1

1

1

1

SW846 82608 2741,ar01 27.Mar07 703t617 RLJ

This lrborolory repod Is nol patd withou M tcrto ad sigaataru on the cowr page.

+ Reportable D€t€ction Limit BRL = Below ReDortins Limir Page 97 of 165

Page 607: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificatiooTE-3sA5954l- 19

Clietrt P.oiect #301-Er

MatrixBlalk Water

Colleotion Date/Time2l-Mar{7 00:00

Receiv€d22-Mar-07

CAS No, Analtre(s) Reselt FIae rnDL Dilutk'n Mahod Retr P.z?orel Ansb\ed Balch A.taryst

100425 styrene

63G20-6 1,'1,1,2-Tetachlorcethane79-3{-5 | , I ,2,2-Tetrachloroethane127-184 Tetfachloroethene108-6aJ Totuene87{t-6 '1.2,}Tddt lorob€nzef le

r20-82r .1,2,+Tdd{orob€nzene

71.5t6 1.1,l-Tfft* oro€thane79{0-5 1,1,2-Tridllofo€thane79.{)1{ Trichlofoettr€ne

Volrtile Org.nlc Compornds

Volatile Oroanic Comoounds bv SW846 82808Prepared by mehod SW846 5030 Water MS

BRLgRt

BRLBRLBRL8RLBRLSRLBRLBRL

75.6s-r Trict o(oilroromethane {F eon 1.1) BRL96-18{ 1,2,3-Tridlloropaopan€ BRL9{,€+6 1,2,4-TrinElhylbenzene 8RL108.671 1,3,5-Tfimethylbenz€ne BRL

USI 1.0

ttgl 1.0

tgl 0-5

rcil 1.0

td l 1 .0

Udl 1-0

ldl 1.0

IrSl 1.O

N t 1 0

tglt 1.0

t dl 1.0pdl 1.0

ldl 1.0

UgA 1.O

w 1 .0

rcn 2.O

Ig/l 1.0

ldl 10.0

ldl r .0

lSn 1.0

t'il 1.0

tdt 1.0

FCn 10.0

ldf 2o.0

7F130 %70-130 %7F130 %70-130 %

SW846 82604 z7-MaFOl 274nat47 7031617 RLJ

7rr{1-4 Vinylchbndel33G2c7 m,p-Xyten€95-47{ Gxylone1C'eS+9 Tehahydrofurans297 Ethyl et|er994{5{ Tert-amylm€bhyletf|ea637-92J Ethyttoft-butyt €theYr0e2G3 Oi-isoFr.opyleth€rTsso Tert-Bubnol / b'lq/ atcot|ol12$91-1 1,40bxane

SunDgaIs rEcoveriesi4F,to4o.4 +Btomofluoabenzene2$7-zes foluene4S1 70*07 4 1, 2-Dichloroethane 441868.$,7 Abrcmofruomnethaae

BRLBRLBRLBRLBRLSRLBRLBRLBRIBRL

90102105102

Thh laborubrf Epor', it ,st volid nt&lrod sn sqthodre.I slgndarc ot ahe cover ptge.

i Rcporbbie Detection Limit BRI- = B€lou' Reporting Linit P6ge 98 of 165

Page 608: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Aralytqs) Flrg Units

Source %REC

Result %RtrC Limits

Spike

Levcl

RPI)

Limi t

B.rct 7031517 - sw846 5030 w|ter MS

Bhnl r703161?€LKl)

P.epared & Anal].aed: 27.t\rar{7

1.1,2-Tricfibroffi uoroethane (Freon 1 13)

Acrytonitib

B€rrzen€

Enmobenz€n€

Bto(nod)brolnehanegromodicttloromethane

Sr('nofofm

B(xnonEfhane

2€ubrcne (MEK)

n{{rtyt,€n4.re

E€c-Buvb€nz€n€

tert-BuMbenzen€

C€tbon diermde

C€rbm b['achlodde

Chlorob€rEene

Chlo1o€thEne

Chiomform

Chlorometlane

24hbrctoluene

44hbrotoluen6

1 2.Dibronrc-Schbrcpropan€

Dlbromod{orornethane

1 2oibronDethane (EDB)

DibromorEfl€ne

1 ,zoichlorob€t|z€n€'l,3-Dichbrobenzene

l,4.f)bhlorobenzene

SRL

ARL

BRL

ARL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

8RL

BRL

BRL

BRL

BRL

ARL

ARL

BRL

ARL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

|l9/lpg/l

u9/lpdl

!Elpsl

pgl

trg/l

rr(yl

lJg4

lrs/lpgtl

lls/lps/l

p9/l

psrl

|lg/l

ugl

ut / l

|Js/l

rs/lgrl

us/lus/ltrg/lpsnp9l

Lig/l

9 lpdl

!sn!dl

lJdl

!91

tts4

ugl

!gr

!g/l

!g/lpg/l

pgn

!El

|ls/lp9/l

ugnpsn!s/lp9/l

!s4pdlpqt

1 .020.00.51 01_O1 .D0.51.02 01 0 0' 10

1_O1_O5.01.01 02 01 .02.01 .01_02.O0.50.51 01 .01 .0l 02.0r.D1 .01 .01 .01 .01.01 .01 .01 0

0 50 51_00-510.01 .01 .0'I 010.05_0t_0

1 -01 .0

(Freon12)

l,t-DidrbrDeth8'l€I loihlorcethane1 ,1 .old o.oethen€cis.'|,2-Oichbmethenefa8-i,2-Oi{t oroetherEt Z-Dichbmpmpar'€1 ,3-Dict orogopan€22-DidloropropdE1 ,l -Dlchlo@prop€n€

ds-l ,'Dld oropiopenelrahg1,3{)l.fi lo.opropeneElhy{berEenetlox8chlo.obuladiene2+ler€none (MBK)lsoprJPYS€nzone4-lsop.opytolueneMetht tert-butyl etherGid€fif2+entanone ([rlSK)Mstrylsr€ dbrijeN+ht€len€n.Prcpylbenz€neStFen€

Thh ,abo.abry rcport it no, vzlu tsithoul an aathorized signotu.e on rte cove, pdge.

+ R€ponable Det€ction Limit BRL = Betow ReForting Limir Page 99 ol 165

Page 609: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtile Organlc Compouods - Quallty Control

Analyte(s) Result Flag Units *RDLSpike Source o/"R.EC

kvcl Result %REC Limirs RPDRPDLinut

Brtch ?031517 - SW846 5030 Wrter MS

Blar|t (703161?€LKil

Pr€par€d & AnarFed: 27-Mar-07

1,1,1,z-lebad oroelhane

I, 1,2,2-Tetracl{or*thane

l,2,STrichlorobenzene

I ,2,+Tdchloroberuene1 ,1 , 1-T.icfibrGfhane

1 ,1 ,2.Tridlcro€lh€fl€

Tridrloroelhene

Trichlorofl uoror|letlene (Freon I 1 )l.2,STrichloropropane

1 2,+Trinrelhylbenzene1,3,STrid€thYb€nzeno

o-xylen€

Tetrahyd'oturan

EdIy' elher

Tert-ffrry| methyl 6th€r

Ethyl iert-butyl efler

Di-lsopropyl sth€r

Tert-Buianol / buvl alcohol

1.4-DioxEne

S u nwal€ : 4-B rono fl u oto b on zenoS',Iogate: foluene4SS unogate : 1, 2 D i ch lo rcel h arc4 4Suntga.'F- : D i h rono fl u orc n elh ane

LCS r7ftit6t7€S1r

Prepared & AnalFed: 27-Mar-07

1 ,1 ,2-T(i$k)rotifluoroethan€ (Fr€oo 1 13)

8€nzen€

Broanob€nz6n€

Bromoct oaomethane

Bromodichlorcfielhane

Brornoform

Eromo$et|an€

z-Bubnone (MEK)

n-Butylb€nz€ne

s6c-gu!/b€nzene

torl-8utylb€nz€ne

Carbon disulfide

Carbon tetaac oftt6

Chlorob€ruene

Chlor@than€

Chlorobm

Chlo(ometlan€

24hlorotolu6ne

4{hlorololuene

1,2-DibrsnGH*rrop{opan€

BRL

BRL

BRL

BRL

BRL

BRI

BRL

BRL

SRL

8RL

BRL

BRI,

BRL

BRL

BRL

BRL

BRI-

BRL

BRL

8RL

BRL

aRl-

ARL

45.649.951.251.4

'17.5

13-9

20.2

r 9 s19.4'ts.8

19.6r9.620.4

19.0'17.6

17.7

lt.o19.5r8.8r 9-7

20.820.422.7

t'$psnydl

IJdIttsnudlus4psx

tt$!dl|ldlt 9 ll€n!s4pdlgEl

u(yl]|gil!dlPdl!dludlItgtl

psrl!cnlldlIJCI

pslpsn

!s4!Ert,gltlgi!s4pdl

!sn|r9n1lg4l8/lpgl

F91!g/l

!dlIrg/ll!g/l

Pgltrdlfldllsn

1.00.51 .01 .01 .01-01.0t . 01 .01 .01 .01 01 .01 .02.0'1.0

10-01 .0t . 01 .0r 010-0m-o

50_o50.050.o50.0

20-020.0m.020.0m.020.020.020.020.0m.020.o20-0z).020.020.020.020.020.o20.0m.020.020_o

91 70-1n1M 70.1mlm 70-lm103 70-tg)

88 7G13070 11.r-147101 70-130

100 70-13t)

97 7Gl3t)g9 7G130s6 70-130sa 7G130102 62-13666 53.+133s5 7G13088 70-',t30

88 70-13086 7(}.13005 7Gr3098 7$t3094 62.0-t3it

98 70-130

r11 70.130104 7Gt301U 70-130114 m-130

Ihb hbordory reped h nor vdu Nlth*r cE aulhod,td sagnoure on lhe cow, pq. .'R€portable Detc(ti@ Lioii BRL = Below Reportiog Limit P{ge 100 of 165

Page 610: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Spike

Level

RPD

Lirnit

B.ach 7031617 - SWE{6 5030 Wrter DtS

LCS t7031617€S1l

Prepsred & AnelFed: 27-Mar{7

Dlbrbmoc'|brdn€thane

1,2€lbrorm€thane (EDA)

Dlbomomeihane

1 JSlchb.ob€nzene

1,3-Dlchlorob€nzene

1 ,4-Dici orobenzene

Did$rodif !,ofom€thane (Freonl 2)

| ,l -Di$loro€thane

1 ,2-Ornbm€thane

1,1.Dichlorc€lh€ne

ds- l 2Oicnloro€tttsne

tans, l,2oichlo(o€thene'I .2Oichlo.opropane

l Soichloropropane

2 2-Oidrloropropane

I , | -Dichlompropene

cis,l,3-Oic+ oropropene

tlans-'l,3oicnbroFropen€

Elh/b€nzene

Hexachloncbutadiene

2-Hexanone (MBK)

lsDpmpylbenzene

+l€opropyltEluetP

Ilothyl brt-buv ether

4+.relhyl2rentanone (MISK)

ftr€thybne cfilodde

Nephihabne

of.opylb€nzene

Styrene

1,1, 1,z-Tetrachloro€thane

1.1,2,2-TeUEchbroehan€

Tellacfiloroelhen6

Tolu€n6

1 ,2,&Tri'lbmb€rE€ne

| ,2,+TrtchlomberE€ne

1 , 1 ,1-Tricibroehan€

I ,l ,2-Trbhloro€tfiane

Trichloroefnene

TftJ oronuoroflEthane (Freon 11)

l2.STrichloroproDane

1,2.+Tdm€bylbenzene

1,3,$Tdm€lhy'berEene

Vtr\4 cnlorue

m,FX9€ne

o-Xybo€

Telaahydroturao

Elhyle0€.

T€d€rny' methyl €f|€r

Ehyl b.t{utyl eth€r

Diisopropy ether

T€d-gutend / butyl alcohol

1 9 . 8

20_0

19.3

21.3

20.5

19.4

20.4

19_4

19.8

17.1

2 0 7

14.7

20.4

202

18.6

18.4

21.1

22.5

202

1 9 I

1 3 . 5

18.2

1 9 2

20.7

18.4

18.5

19.8

14.2

18.8

19_5

20.s17.6

1 8 . 7

2 0 8

1S_g

17.7

rE.2

17.3

?2.6'| 9.2

18.7

22.1

39.2

19.9

20.5

20.2

19.4

2 1 . 8

20.8

205

ps/l

|lgl

psn

t/s/lusnpdl

!dlpsrljgn

rglpgl

ljg,l

!s/l

vs,4pgl

psn

!91

Ljgl

!g/l

t /g l

ps/l

IJEI

tlEl

!s/lpsnljglpgl

!snpdl

!si4rdlps,4

r.i!yl|llyl

!gl

pEl

p9/lps/r

!s,!glpgl

rs/lpg/l

wApsnpsn

tsllFSnjrdl

psn

!c4

20_o20.o20,020.o20020.o20.020.o20.020.020020.020.020.o20.020.020.020.020.020020.020.020.02 0 020020.020.02 0 020.020.o20.020_o20.02 0 02 0 020.o20.o20.o2 0 020.o20.o20020.040.020.0m.020.02i.o20_o20.0200

99 70- 143100 70.130s6 70-130106 70-130102 70-13097 70-130102 39.3-16797 70-13099 70-13086 70-130r(x 70-13094 70,r 30104 70- t 30101 70-13093 70-13092 70-130106 70-1301t2 70-130101 70-130100 70-1366a 56.3-131s1 70-13096 70-130104 70-13092 70-13092 70-13099 7G13091 70-13094. 70-13098 70-130104 70-13088 70-13094 70.130104 70-130100 70-13088 70-130106 70-13091 70-130E6 70,130113 70.130

96 70t3094 70-130110 7G13098 7G.130r00 70-130102 7G.130101 7G130s7 7G130109 70-130104 70n30102 70-130

Thh latonlary rqorl it not valid Nithout att sathoritett signat,.e on lhe cover page

r Reportable Detection Limit BRL = Below Reporting Limit P^ge l0l of 165

Page 611: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Anallt€(s) R€€ull Units .RDLSpik€Level

RPDLimitFlag

Source %RECResBft '/IREC Limib RPD

Bahh 70Jr5l? - SW846 5030 Wrter MS

LCS f70318t7.Bstl

Pr€parod & Anslyzed: 27-Ma.-07

1,4-Oio€ne

S u ftogate : 4 €,lonon uotd en n neSunoqal?-: Tohtene4SSunogata: l, zaid tbftetha'€44S u rogate : Dih ro nafl uo@n atha ne

LCS Duo (703161?.BSOil

Prepared & Ana\zed: 27.Mar{7

1 ,1 ,2-Trichlorobinuoto€thane (Freon 1 13)

AE ylonirile

B€nz€ne

gmmoct|lorornethane

Bronbdichbrornehane

Sromoforn

2€ubnon€ (MEK)

n€utylbenzon€

9€oBuMbe.Eene

isrt€utylbenzeo€

Carbon disulfde

Carbon letrachbdde

Chlorob€nzen€

ChlorEethane

Chloroform

Chlofomethane

2-Chlorclotuene

4{hloroioluene

1,2.Dibtomo3-chloropropane

Obromo{hlorom€than€

1,2-Dibromoethane (EOB)

Dibromomethane

1 ,2-Dichlorobsnz€ne1,'Oldrlorobenzen€'t ,+Di*rlorohenzen6

Didrlo.odiff uoromethane (Freonl 2)

1 ,1 Oichloroe$Ene

l,2Oichloro€tl|ane

1 ,1 Oichloroeth,ene

cis, 1,2-Dichlorcethene

trans-1,2Oichlor€th€ne

| ,2-Dl* oroprcpan€

f ,3oichlorop{opan€2,2olchhopropane

1,1-Diehloropropene

cis-l,3-ttknbroprop€fl e

lrans-l,30lat orop.op€n€

EthylblEeo€

Hexachlorcbutadiene

2+io(anone (MBK)

2m50.5

49.819.7

16-0

13_7

r9.8

rB.7

18.4

18.8

r8.6

19.0

18.2

13.6

17.3

16,6

16.2

15.6

18.4

17.7

16.8

20.7

1S.6

19.3

22.O

19.0

19.1

1 6 9

19.9

19_4

rE.4

18.6

18.3

r9.4

r5.8

19.6

17.4

19.6

19.5

17.4

16,9

21.9

19.1

17.3

t2.st 7 . l

Fgr

!dl

!dl

|lgl

|ldl

|tdl

w/lI,lEl

tsnpcnpgl

!dl

!dl

!dl

udluqlygrl

|,dlpsn

ug/lrc/lusnpqlpdl

!dluc4!dlWn|lgl

t d lFSntjEl

rglusnp9/l

tjdllrdlljdl!dlsgludl!dl|ldlpsn

20050.o50.050.050.o

20-om.o20.0m 020.020.020.o20.020.020.o20.020.020.o20.0m.020.020.020.020.020.020.o20.020020_020_020.020.0m.020.020.o20,020.020.020.0

20.020.020-020.om,0m.020.0m.o20.020.0

100

101101100

t,(yl

lldlpsil

rsrlllgn

7G13070"1Uf&13070-t 307G130

70-1fr) 10

41.1-147 3

7G130 2

7G130 6

7G130 5

7G130 57Gi30 570-130 362-t36 11

53-9.133 4

7G130 10

70-130 770-13/J 6

70-130 6

7G130 I7G130 6

62.&132 770-130 4

70-130 770-130 670-130 6

70-130 47G143 170-130 170-130 27G13) 67G130 57Gi30 5

39.1t67 S

70-130 57St30 27G130 I7G1a) 670-130 I

70-130 A

7G130 3

7G130 77G1 30 S7{}-130 4

7Gr3o 2

70-t3o 5

70-138 15

56.3-131 I7G130 6

25502525252525

5050

2525252525

25252525255025252525

50

2525

252525

25E65025

8068sg94gz

94

95916986

838178c28ll9{10498961109596s4tfl)9792gt

v9779988798s8784r02fl096

€486

Thl! labntotf Eport Is not rdu frdhoaa ad aafrorbcd stgt arta o,r lh. @ve page.

i Repotuble Detectio[ Limit BRL = Below R€poding Limil Pag€ 102 of 165

Page 612: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qualify Control

Analytqs) Resuh Flag Unjts + R D LSpike

Level

R P D

I-inrit

Souroe %REC

Result %REC Limns RPD

Bercb 7031617 - sw8,t6 5030 wrter Ms

LCS Ouo t703l6t7ASD1l

Prepa.6d & Anal}.zed: 27,Mar-O7

4lsopropyltoluene

Melhyl terttuv ether

4-fvlethyl-2-pentanone (MtBK)

M€trlyl€ne chloride

Naphthalene

Slyrene

1 ,1 ,1 ,z-Tetrachloroethane

1,1,2,2-Tetrachbrostfrane

Tatrechbro€lhene

1 ,2,3-Tdchbmb€nzene

1,2,4-Tdchlorob€nzene

l ,l ,l .Trichloroethane

1,1,2-Trichlo.oethane

Trfttrloro€tl|€ne

Trld{orcfl uoomethane (Ffeon 1 I )1,2, $Trichloropropane

| 2,+Td.nehylbenzen€

| ,3,tTrimehylt€nzene

Vinyl dd,oride

m.p-xylene

o-Xylene

T€hshydrofurEn

Etryl stfi€r

Tert-amyl rn€bryl elher

Ethyl tert{ui/ ether

Dii8opropyl ether

TsrtBubtlol / butyl alcohol

1r{ioxen€g/llggefu : /l+l to nofl uorob e n ze neSuftcgate: Tohlene4gS u fi pga/€ : 1, 2-D ich lo rcet ha rc 4 4S unqab : Di btu mof lu oro metha ne

tlatrlx Spik 17031017-{rlslI

Pr€pared & Analfzed: 27-Mar-07g6n2en€

Chlolob€nz€n€

1 ,1-Dichloroeth€ne

Toluone

Trict{oroehene

Swntgate : llStomonuor&enzene

Surcgate: Toluene-daS ulroga|€. 1, 2 -D lch h.roel h a ne 4 4S u fl og ab : Ahrcnofl uorc mel h e ne

17.7

20.5

1 8 1

17.4

18.4

1 7 2

1 8 2

18.3

20.2

16.4

1 7 . 7

1 9 4

18.3

16.4

20.7

1 6 8

1 6 . 1

1 8 . 1

r7.3

20.3

36_4

18.9

20.4

20_2

1 8 6

21_2

1 9 9

204

214

5 0 55 0 549.149.6

SourE.: 5A59642.01

!g/l

!gnp9/l

ltgtl

trs/l

ljgl

!9npdl

!snugnpgl

!snp9nItgtl

psnps/l

!sn!(yl

I.t94psn

!g/l

!g/l

!dl

ugl

Lis/l

u9/l

Itgllpg/l

pgl

PSI/l

!grpsnpsnPE

2 0 020.020.020.o20.0m.020.020.020.020.o2 0 02 0 02 0 020.020.o20.o20.020.o20.o20.020040.020_020.o20_020020.o200200200500aa.o50.050.o

20.o20.020_020.020.050_050050.050.0

20.020.020.020-0

25255025252525252525252525252525502525252525

255025252525

88 70-13t1

102 70-130

90 70,130

87 70-130

92 70-130

86 70-130

91 70-130

92 7G130

101 70-130

82 70-130

88 70-130

97 70-130

92 70-130

a2 70.130

104 70-130

84 70,130

60 7G130

113 70-130

90 7G't30

86 70-t30

102 70-130

91 70,130

94 70-130

104 70-130

101 70-130

93 70-130

106 7D-13o

100 70-130

102 70-'130

107 70.130

101 70-130101 7G1n98 70-13099 70-1m

70-13t)70-13070-13070-13070-t 3070-13070-13070'13070-1m

70.13070-13070-1307G130

I

2

2

6

7

6

3

6

3

7

7

7

8

7

2

8

7

0

6

9

8

7

6

2

0

3

4

0

7

1 9 2

1 9 . 7

21.1

19.3

19.0

46.550.751.650_4

!s/l

Fgn

!s/l

Fgn

l.i9/l

!s/lpsll

t /g l|lgl

8RL

BRL

ARL

BRL

ARL

96

9a

106

96

95

93101103101

tlat ix Solks Ouo 1703161?.|its0lt Sourc€: SA5t682jl

Pr€par€d & Analyzed: 27-MaF07

Benzene

Chloobenzene

1 ,1 Oidrloroethene

18.519.220.319_1

BRL8Rt-BRLBRL

9296r0296

30303030

rg4rglpsrlpsn

42

o

This lahorarorf reryd is not edid withoet oa attrtoized signaturc on the covet page .

' Reportable Deleclion Limit BRL = B€low Reporring Limir Ple€ 103 of 165

Page 613: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtile Orgrnic Compoutrds - Qurlity Cotrtrol

Spike

B.tct 7031617 - SW8,l6 50J0 Wrtel MS

Matrix Solk6 Dup fl03l617.ltsol) So{rco: 5A50682{1Peparcd & Analfied: 27-i.laf-O7

Tdchbrosth€ne

S ufl W ele : tt8lomon uoroben ze neSfimge|€: TohEne4SS uiogtu : 1,2 -D k:h Io rEth arc 4 ISunog e : Dlbrc nofl uomm dh a ne

BNtch ?031642 - SW846 5030 Soir (hrgh tevetl

Blank 17031€4il€LKl)

Pr€pared & Anabzed: 27-Mar47

|,|,2.Tnchlorotrifluoro€tharNe (Freon 1 13)

Acrylonitnb

B€nzs|€

Brcmob€nzsn€

Bromochbromethane

Eaomodid orofirethanegrornofom

Brornornelhan€

2€utamn€ (MEK)

n€ulylb€nzgne

s€c-Bulylbenzene

tert-Butylbenzene

Carbon disulfide

c€rboi btradlbnd€

Chbrob€nzen€

Chloro€thane

Ct{oloform

Cruo@melhane

2-chlorotoluene

44hlorotolu€n€

1,2-D0rcmo-3rhbmpropsne

Dibromo€hlorom€thane

l,2obornoethane (EOg)

Dibronlomsflan€

12-Dlchlorcbenzens

1 ,3-Dk$lorobenzene

1 ,+Ok*rlo.ob€r|z€ne

Did{orcdfl luoromethane (Freonl 2)

I,lOhhioro€lhane

l,2.Dldiloroehane

1,l{]bhbroeth€ne

ds-12oid$icrDsth€ne

lrans-l,2olciloroethen€

1 ,2ol*loropmpan6

1,3{)ir$bmpropan€

2,2-DlJ oropropang

1 .1 -Oichbropropen€

cis-1,3-Dlchloropropen€

tlan+l,lDicf oroprcpene

Ethylb€nz€ne

HexactlorobutEdi€ne

2+lex€non€ (MgK)

'18.6

46.350-651,650.4

ARL

SRL

8RL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

SRL

BRL

SRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

SRL

BRL

BRL

BRI

ARL

BRL

BRI.

aRl

EFL

BRL

BRL

BRL

SRL

BRL

ARL

SRL

8RL

8Rt_

ARL

20.0il.ofr.ofr.o50_o

BRL 70-13070-13070-13r')70-1n7G1g)

ugilpglpqlpdlpdl

sl9!l101103101

lgrkg wet 1-0

ruLrkg wet 20.0

rcI(g wet 1-0

pgllg wel 1.0

Wl(rgw€l 1.0

pg/kg wet 1.0

!g/kg wel 1.0

pC/}g tv€l 1.0

pdks wel ?.O

pdkgw€l t0.0

lg/kg\rel 1.0

!g/kg vJet 'l.0

lg/tS vJet 1.0

ldkS wst 5-0

lgr'kg wEt 1-0

lgL/kg 'r,et 1,0

pgn(g wet 2.O

pglkg wet 1-0

Ugr'kg wet 2.O

ugagwet 1.0

lgr'kg w€l 1.0

Ug/kgw€t 2.O

Fgl(g tv€l 1.0

Ugr'kg wel 1.0

PSrrS Yrel |.0

lglgtYet 1.0

pSftS w€t 1.0

UdkS wet 1.0

llgftS v{at 2.0

tdkSwEt 1-0

lgr'kg w€t 1-0

!g/kg wel 1.0

Fgikg weI 1.0

t€/kg wet 1.0

tg/ lq wol 10

rc/kg $/ol 1.0

rg/kg w€t 1.0

Pg/kg '/61 '1.0

pgkg rY€t 1.0

pS/kgr€l 1.0

pdkg Yret 1.0

ldlS Y/€t 1.0

Ugr'kg wet 10.0

Irtb laborolaty r.Ior1 b nd valid tdthottt.a altthoria.l sig,@!*re on the cover ptF -

+ Rep.rtable Detection Limh BRL = Below R@orting Limit P.ge lo4 of 165

Page 614: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgrnic Compounds - Quality Control

Analytds) Result Flag Units %REClRDLSpikeLevel

SourceResult

%RBCLimits RPD

RIt)

Limit

Brtch 7031642 - SW846 5010 Soil (high level)

Abd( {7031642.8LK1 |

Propared & Anal).zed: 27-Mar-07

4lsopropyltoluene

Mothyl t€rl-butyl €th€r

4-rvlethyl-z{entanone (MIBK)

Methyl€ne chloride

t{aphlhar,rne

Styren€

1 ,1 ,1 ,2-Tetsachloroethane

t . t ,2,2-TefachloroettEne

Tolu€ne

l,2,3'Talclrlorobenzene

| ,2,+T.kfilorob€nzene

| ,1 , l-Tri{$bro€thane

| , t ,2-Ttid orc€flane

Trichkroelhene

TdnbroRuorom€tlane (Freon 1 1 )I 2,lTricfibropropane

l,2,GTrimethyltrenzene

| ,3,$TrilnetrYb€nz€ne

Vinyl cf*oride

m,p.Xy'eno

TeHrtdroturdn

Ethyl ether

Te.t-arryl melfyl ether

Ethy' tert+ut/ etner

Di-lsopmpyl €ther

Tett€utanol / buvl alcohol

1,+Oioxane

Su/fog ale : 48 m monuo nb en ze neSwtu'a;le: fohene4Ss uif ogale : 1, 2 -Dich larcet h an e4 4Su/roga/€ : A brc rofl ttoruh elh a ne

LCS ft031AU€SI)

Prepa@d & Anal!.zed: 27-Mar-07

1,1,2-Trlchlorotrif,uoroethan€ (Fr€on 1 13)

Aqylonihlegenzene

BroanoberEene

Brornodrbmrn€than€

Bmnodichbrorfi€fEne

Brorhofoam

BroNnonrolhsne

2€ubnone (MEK)

nAdy|b€r'z€ne

s€c-Eulylb€ru€n€

l,erl€ut)4b€nzen€

Crlbon disutfide

BRL

BRL

BRL

BRL

ARLgRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

8RL

8RL

BRL

30.729.928.929_3

1 7 5

1 6 _ 1

20.4

16.5

21_2

21.5

20.2

21.O

20.6

16.0

16.6

18.3

19.3

18.O

30.o30.o30.030.o

20.020.0x.oz).020.020.020.0200z).020.020.020.020.020.0

1021009698

pS,4<S r €l 10

!g/kg w€t 1-0

pg/kg w€t 1-0

pgL4q wot 10.0

Udkg wet 10.0

pgxgwel 1-0

Lrgftg wet '1 0

!g/kg wet 1 0

lgr/kg wet 1.0

pq/kg wet 1.0

pg/kg wet 'l.0

pg/kg wel 1.0

!q!4(g wel 1.0

pg/kg wet 1.0

pg/kg wel 'l.0

!g/kg wet 1.0

!g/kg we{ 1.0

Uq/kqwet 1.0

t/g/kg wel 1.0

Ug/kg wet 1.0

Ug/kg wet 1.0

!g/kg wel i.0

!g/kq wel 2.O

!g/kg wet 1.0

Ug/kg wel 10.0

t/g/kg wel 1.0

pg/kg wel 1.0

!g/kg wet L0

pg/kg wet 1.0

Ug/kg wet 10 0

Ug/kg wel 20.0

Ugr'kg wel

ug/ko wet

!g/kg wel

LigLi kg wet

pg/kg wel

Ug/kg wet

pg/kg wel

!g/kg wet

U!r'kg wst

Ug/kg wet

lgr'kg wet

!g/kg wet

pg/kg {,et

Pg/Kg wst

lgr,l(9 wet

!g/kg v/et

FqkS Y,/et

Ugut(g w€t

88

80

to2

a2

106

108

101

105

103

80

83

92

96

90

70-1307813070.13070-130

70-130ln-17570-1n70-13070-13070-13070-1307G130

55.3-13638.8-'r427Gt307G1307G13070-130

This laborotorf Epon it ltot ealill wuhot l ar. u.horlud sigmtap on the cover page-

+ R€portable Detedion Limi! BRI = Below Reporrins Limit Prge 105 of 165

Page 615: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgstric CompotrDdr - Qurlity Cortrol

Analyt{t Resuh .RDLSpike

tevel

RPDLioitFlag RTDUnits

Soufce "/il<EL

Result %REC Limits

Br.ch 70316,12 - Sw846 3t30 soit (higb kveu

LCS {70316,{2€S

Preparcd & Anely:ed: 27-Marfl

Ca6on ietachlodde

Chlorob€ozene

Chloro€lhan€

Chloroform

Chlorom€lhens

2.Chlo.otolueil€

44hlo€toluene

1,2-obrDmo-S\lo.opro[€ne

Oibromochlorcanethane

1 ,2-Oblomostrane (EDB)

Dlbromom€hane

l,2oichloobenzen€

1 ,S Dichbrob€nzene

| ,+DichlorEbenzen€

(Fr€on12)

15.420.419_719.620.7

20.019.620.921_420.6

20-sm.3N.2r9.719.61g_120.519 .120-421 .1?5.317.219.419.619.E18.1't4.5

18-6t E 9

18.818.920.817.0

20.1

lt .718.0m_219.617.121-A20-s16-823619.720.3'r9.8

20.020.020.020.020.om.020.020.020.020.020.0m.o20.020.020.020.020-0m.0m.020.020_o20.020.o20.020-020.020.020.020.o20.020.020.020.o20.om.0m.o20.020.020.0

20.020.020.o20.020.om.020.020.020.020-020.o20.0

70-1307G130

55.3-13070-r 3070-'t 3070-13()70-13070-130

64.7-1397G13070-r3{)7G13070-r 3070-130

UgL/kg w€t

|,g/kg wst

yg/kg wet

!g/fg wel

pCAg wel

ldkg',t€l

ldkS wet

lgr'kg w€t

Udkg rv€l

t g/kg vyet

pgkg wet

U9k9 wet

pd*S wet

ldkS w€t

!g/XS Y{€t

!g/tg YJet

lgr'kg wet

pE k9 wd

!g/kg w€t

pg/tg wet

Ugrlg wol

ldkS wel

lgftg r€l

lgr'kg w€r

!94(g w€t

Wr'kg wet

Ug/kg w€t

Ugkg wet

ug/kg wel

t/dlS w€t

lgr/kg \r€t

lgr'kg wet

ldkg Yret

t dks s/etpg/tg wst

!g/kg wetydkg w6l

lrgrlq w6t

!dl(S $€l

u94(g welggltg wetpgr'kg wetpg/kg vret

Ig/t(g wet

Pg/kg wetpdkg rv€r

lgftg w€t

Ugrkg r€l

UgLtkg yrst

tlgn(g s/et

t g/kg vrst

t01 34.4-1679a 70-13098 7Gr3090 7Gr30102 70-13096 70-130102 70-130t06 70n 3076 7Gt3om 7G13097 7Gr 3098 7&130s9 70-130sx] gl,7-140

72 70-130s3 70-13094 70-130103 7G13094 46.1-145s4 7Gr30'l0{ 70-13085 70-130110 70-130t00 70-13099 70-130EE 7G13094 7G130101 70.130s8 70-13086 70n30109 70-130102 70-130a4 56,&140118 7G1309E 70-t30102 70-t3osg TGlg)

102

9898104101to098104101103'103

102102

1 ,1-Dkfilor€f|ane1 ,2-DiJrloro€han€

1.1 -DichbroouFn€

cis-1 2Oidrlo.oethen€

trans-l,2-Diciloroethene

1 ,2-Didlloropr@ane

1 ,3-Didlloropropane

2,2'Dichloropropan6

1,1Oicl oropop€ne

cis-1,3-Oinbrcprop€n€

lrans-1,3{)idlblopropene

Ethy'benz€ne

l-lexachlorobuladl€n€

2+exanone (MBK)

lsop.opylb€rE€ne

4.lsopropyltdu€ne

Methyl ed{utyl ether

4-t\46tryl-2f €ntanorE (MIBK)

Me{hyl6€ d{orlde

NaPhthalen€

Styrene'l,1. l.2.Tehachkrelhane'1,1,2,2-Tolradtk,roelhene

Tetachlofoefrlen€

Toluene

l S.STridbroben:ene

1 ,2,+Td{$brob€nz€ne'1 ,1 ,l -Tridbro€fEne

1 ,1 ,2-Tricnbro€Urano

Tri:trldo€lhen€

Triilorofluoomelhan€ (F €on 1 1)

l,2,3.TncnbrbpEpone

l2d.Trimehyb6nz€n€

1,3.:>Tdrn€thyb€nz6ne

This bLonroq .eport b nol wIU ,sithout oa c&rtodsi tignra4 oa aha covc. prg..'R€poriable Detectior Limjt BRL -Below Reporriry Limit Plge 106 of 165

Page 616: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qurlity Control

Spike

Btub 7011642 - Sll'846 sox' Soit (tigft tev.l)

LCS ft03t642€31l

Prepar€d E Anal}i"zed: 27-Mar{7

rn,Fxyl€n€

o-Xylene

Telahydrofuran

Elhyl ethor

Tert-amyl methyt ether

Ethyl brttutyl ether

Di-bopropyl ether

Tert-Buland / bulyt atcohol

1,4-Orbxane

Sunllgate : ltB ro nrcfl uofi ft e n ze neSurogate: Toluarc4gS urqete : 1, 2 -D bh lo rce I h a n e 4 4S unqeta : D ibm nofr u o lDmel h E ne

LCS Du3 at031642.ASD1l

Prepared & Analyz€d: 27-Mar47

l.|,2-Trichloroffiuoroethane (Freon 1 13)

Acrybnihile

Bonzene

Brornobenzeoe

Brorno.filoromethane

Brornodicibrorn€tnane

Srcrnofofin

Brcanomefiane

2€ubnone (MEK)

niulylbshzEne

seeguMberEene

tert€uMb€nzene

C€rbm didnde

C€rbon tehachlodde

Chlorob€nzsn€

Chloroelhane

Chloroform

Chloroamhene

2-Chbrotoluene

4Chbrololuene

1 .2Oibttho-3-chlompropane

Dibrdnodllomm€f|ene

l,2olbohoefiane (EDB)

Dib.omon€hano

l,2obhhrobenz€ne

1 ,3oichhrobeozene

t.4-DichhrDb€nz€ne

(Fr€on12)

udks wet

9&g wet

!S/kS wel

!g/tg wet

pq/kg wet

!g/kg wet

Pg/hg wet

!gl(g wet

!g/hg vret

ugL/hg wetlgL/kg wstpgn(g wetPg/kg wet

yg/kg wet

Ug/Kg wei

!g/Kg wet

LiEr(g wer

|lg/kg wet

Ug/kg wet

ugr'kg wet

uqr(q wet

Lig/hg w€t

Ug/kg wetpglkg wet

lgy'kg wet

Lig/hg wet

Ug/Kg wst

Pg/kg wet

p(y(g wet

Pgr'hg wet

Pg/hg w€t

]ld\S wet

!94q wet

!g,kg wet

ldkg vret

pE(g wet

Ug/hg w€t

Pgilg wel

!g/kg wet

Pg/kg wet

lstitg wel

Pg/kg wet

Igi k9 wet

trg/(g wst

pg/kg wet

Ug/kg wet

UgL4(g wel

Ug/kg wet

USI(S v{et

34_4.16770-13070-13070-13070n 3070-t3070-1307G130

4 0 2

20.9't9 7

20.9

19.8

20.9

19.2

1 U

1 5 1

30.730.52E.129.1

16.3

15.6

1 8 7

19_7

20.3

20,0

20.1

20.2

20.5

15.2

15.9

17.4'18.7

1 6 . 1

r 4 5

1 9 9

17.4

18.9

18.6

19.9

1 9 . 1'r9_4

20.1

20.0't 9.5

2 0 4

1 9 7

1 9 8

17.7

18.3

18.4

1 6 4

19.8

14.2

19.7

20.1

40.020.o20.o20.020.020.020.02620030.03n_03003n.0

20.02 0 020020.020.02 0 020_020-020_020.020020.020_020.020.020.o20.020.o20.020.020020.020.020.020.020.020.020-020.020.020.020.020_024.020.020.0

50

5050

50

?5?5?5

50

2525

50

2525

25

100 70,130

104 70.130

98 70130

104 65.3-130

93 7G130

104 70-130

96 70.10

92 70-130

76 U-155

102 70-t 30102 7G13094 rG13097 70-1m

82 7O-13O 7

7a 1.77-175 3

94 70-130 8

98 70-130 18

1O2 70.130 4

100 70-130 8

100 70-130 1

101 7G130 4

102 55.3.136 1

76 38.8-142 5

80 70-130 4

67 70-13) 6

94 7G130 2

00 7G.130 12

72 70-t34 7'f 00 70-130 2

87 55.3-130 12

94 7G130 4

93 70-130 11

100 7G130 1

96 70-130 4

97 70-130 1

100 64.7-i39 4

100 70-130 7

98 70-1$ 5

102 70-130 1

98 70-130 4

99 70-130 3

'l,1Olt{oroenhane

l,zoicfilaroethane1 ,l {)lchloroetfteneci8-i,2-Dichloroethenet€rls-1,2-0ichloro€thene| ,2-Oit oropropans'l ,Sohhloro0rcpane

88

s29282999198100

't4

6

6

3

5

6

Thit labo.atiry rcport is ttot ralu x'ith4t 4n aurhorlzel signarsn on the coeer psge

'Reportable D€tection Limit BRl-: Below ReFor.ing Limir Pzee 107 of 165

Page 617: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organlc Compounds - Quality Control

Anaba4s) Result Ftag Unir.s +RDLSpike sourc€ '/"REC

kve I Result '/"REC Linits RPD

RPD

Limit

Brrcl7011642. SW8,t6 50J0 So (hign kvet)

LCS Dup lIXll6a2€SD1 |

Prepar€d & Anav:€d: 27+rar{7

2,2-OictUorcproFdt€

1 ,1 {)ichlorcprop€ng

cis-1,3-Dk$lorof mpene

bans- 1,3{icib@prop€n€

Etrylb€nzene

Hexachlorob|Jbdien€

2+lexanon€ (MBK)

lsopropy'tcnzsn€

4-lsopropyltoluei6

M€lM brtbut'4 elh€r

4{r.l€ttryl-zf €nrsnono (M|aK)

MethMene d oride

Naphthalefle

n+mpylbenzene

Styr€ne

1 ,1 ,1 ,2-T€tlachldo€lhaneI , I ,2,2-Tet'achloroetheneTel,€dftroethen€

l,2,STrichlorobenzene

1.2.4-'Idcilorobenzene

1 ,1 , 1-Td.filoro€trane

1 , I ,2-Trichbro€han€

Trichlofir€thene

Trictioronuoromethene (Freon .l 1 )12,$TdchbrcFltspsrte

1,2,+Trimehylbeozene

1 ,3,tT.im€f|y'b€{rzene

m,p-Xyl€ne

o-Xyl€ne

Elhyl6ther

T€rt-€rnyl m€thyl €th€r

Ethyl ted+u[,] €ther

Diisoptopyt ether

Terr-Bl,tanol / hnyl €lcohol

1,4-Dbxane

Sutrogeb : 4 -*o nofl uor6e nzen eSu'o9ate: Toluene4SSunogale: l,2-Dicl orcelhane44S u trogde : D ibronDfl uo rcmeth ane

IahixSolke flCllA|2{S1l

Ptcpafed A Ansl]r:ed 27-[4ad7

Benz6n€

Ct{orobeaz€n€

1,1-Did{oroethene

Toluen€

Trichloro€her|e

I u nWaE : 4- Btc,rof, uotobe nze neSufiWate: Td@n048

13_9

182

18.0

17.9

18,8

13-5

17.8

14.2

19.6

16.9

17.?

19.2

15.7

2 1 . 5

19.4

19.7

16-4

17.9

19.4

18.7

15.8

20_4

19..1

r4.8

22.5

19.2

19.6

15_9

38-8

20-4

1 8 . 1

19.3

19.3

19-9

18.3

108

183

30.729.727.928.8

Sour6: SAsgli4St)2

22.a23-4

23.230.131.9

Igr'kg wEt

lrg/kg wet

lgts wel

ldkS wsl

Ugfrg Yr€l

IdkS vr€iOCI pg/kg wet

USikg vr€lpgrkg welggtkg w€t

Ugkg rvet

trgrlq w€t

trg^g wet

|lgag wel

lrg'l(g urel

lJgkg YY€l

lgr'kg rv€t

lrgikg wet

rcrrkg yr€t

pgts wel

ldrg w€l

tdkS wet

lgdkg wet

lrgrkg wet

lgr'xo w€lpdkg si€t

ldks wel

Pg/kg w€tpdkg wet

rc4(g wet

Fglkg w€(pgks w€l

Pdkg vr€tyg4(g rvetygr'kg wet

Lrg/ko w€l

Pgukg wol

ldtg wel

lgl(g rrett dkS w€tPgr''llg ''stLrdkg wet

ldks dry

YSftS dry

tlg/kg dry

uS/kS dry

Ug/tg d.ypdkg dryudks dry

70 70-130

9't 70-130

90 70-130

90 70-t30

94 70-t3)

88 60.7.14068 70-130

89 7013091 7Gr309E 70-130

u 46.1-14588 70-13096 7G1307A 70-130108 70-1309t 70-13n9B 70-13082 7G1n90 7G.r 30s7 70n3094 7G13079 70-130ro2 70-13096 7G13074 56.&140112 7G130s6 7G1309a 70-13080 7G13097 7G130102 70-13090 70-13096 65.113096 m.130100 7613092 7{rr3t)94 7G13092 34-155102 70-1349S 70-13093 TUlg96 7Gt30

774 70.130tl7 70-1xo110 71t130116 7{ll3t)116 70-130101 7G130106 70-1fi

20.020.020.o20.020.020.o20.020.020.020.o20_020.om.020.020.o20.o20,0m.020.o20.020.0200m.0m.o20.o20.020.020.o20_o40.020.020.020.o20.0z).0m.0200200fr,o30.o30.o30.o

20.020-o20.020.020.030.030.0

BRL

BRL

BRI

BRL

BRL

8

7

s52

1 1

7

8

23I

7

8

7

6

1 3

5

2

21

3

2

I

3

2

1 9

25

25252550252525

5025252525252525252525252525502525252525252550252525

This btordorf rqofl ls Dot ealld wilhoar an aulrotizpd sig,tot . on tfu .otct pege.

' R€portable Detcdion Limit BRL = Betow Reporting Limit Page 108 of 165

Page 618: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Conarol

B{tch 7031642 - sw846 s0l0 soil (trigh level}

llaHx Solk 17031642.frslI Sourcs: SA5S54tu2Prepared & Anal]/2€d: 27-Mar-07

swrcgate: 1,2Dlchlorceth ane44S urcg ate: Dlhrc n ofl u o rc m et h a n e

28.029.0

2 3 022.822422.622.930.131 .227.529.1

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

ARL

ARL

ARL

aRt

ARL

BRL

BRL

BRL

BRL

SRL

BRL

BRL

8RL

BRL

BRL

ARL

BRL

ARL

pg/kg drypdkg dry

!g/kg dryyg/kg dry

ug/kg dry

udks dfyps/}g drypg/kg dryug/kg dryudkg dryUS/Kg dry

30.030_o

20.020_020_020.020_030.030030.0300

BRL

BRL

BRL

BRL

BRL

0.93232

3030303030

93 70-13097 70-130

115 7G1 30

114 70-130'112 70-130

113 70- r 30

114 70-12t

100 7/qi13o104 704m92 7n4m97 70-tn

Iabix Spiks Duo ft031642+aSOl) Sou.ce: 3A59545-02

Prep€red I Anatyted: 27-t\,tar-O7

B6nz€ne

ChloaoberEeno

1 ,1 Oichloroelhene

Toluene

Suftcgato : I -B ronollu o ro b e n zen eSufrcgate: Toluene-d8S urcg ate : 1, 2- Dldt I orc eth a ne 4 4Sulog a|E: A b twno fl u orom e th ane

Brtch 1l3l55E - SW846 5015A Soll (low level)

Blrnk 17031658€LKl I

Preparod e Analfzed: 27-l\4ar.07

1 .1 ,2-Trichlorotriffuoroethane (Freon .l 1 3 )

Acrylonltril€

Benzene

Blomod*rroft€han€

Bromodichbrom€thane

Baomotorm

*o''oflr€thg'l€

2€utanon€ (ltlEK)

n€utylberEene

secguty'benzene

lert€uvbenu€ne

Carbon disuttde

Carbon lehachbrii€

Chlorob€nzene

Chlo@etiane

Chlorofodm

Chlolornehane

24hlorobluefle

4-Chbroblusn€

1 2Oibrcnrc-3rhloropropan€

Dibrottodrloromethane

l,2olbromo€than€ GDA)Dibroflronelhane

1 ,2-Didbrob€nz€ne

1 .St)icnbrob€nz€n€

1 ,+Oitrbrotlenzene

Dld orodnuddiet'hane (Freonl 2)

I , l -Did*rroetlEne

I ,2-Oi{Storoeth6ne

I,l-Dic* oroettEne

cis-l,2-Dicihruethen€

ban$l.2Oichlof o€thene

IrgL/kg wet 5.0

lgL/kg wpt 100

pgr'kg wet 5.0

!g/kg w€t 5-0

lqr'kg wet 5-0

pS/kS Yret 5.0

!g/kg wet 5.0

!g/kg 'ret 5.0

tgr'kg $et 10 0

pgr'kg wet 50.0

lgr'kg w€l 5.0

!g/kg wel s.0

lgy'kg wer 5.0

lgr'kg wet 25.O

!g/kg wet 5.0

pg/kg wet 5.0

!g/rg wel l0-0

pg/kg wel 5 0

pg/kg wer 10.0

aJglkg wet 5-0

pg/kg wet 5-0

!g/rg wet 10.0

pgrlq wet 5 0

pg/kg wet 5 0

pg/kg wet 5 0

!S/kS wet 5-0

!g/k€ wst 5.0

lgr'kg wet 5.0

pg/kS \,Yel 10.0

fg/kq vrer 5.0

Pqrkgwel 5.0

!g4q lvet 5.0

pgr'kg w€t 5.0

pg^g wel 5.0

Th'J lzbotuoFr Eport k not volid withour s!. suthori<ed signa/aft on the cover page .

r Reportable D€t€ction Limit BRL = B€low Reporting Lhrit Page 109 of 165

Page 619: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtile Orgrnlc Compourds - Quality Cootrol

Analytds) RBult Flug RPD*RDLSpik€L€vel

Sourc€Result

%RECLimits

RPDLirrut

Bstch 7031658 - SW846 5035A Soit oow tevet)

Blank 1703lcfA€L(ll

P.epar€d & AndFed: 27-lrar{7

I ,2-Dichbropropan6

1,'Olchloropropan€

2,2-Didrloropropane

1 ,1 Oichbroprop€ne

cis-1,3-DichloroFropsn€

trans-1 ,3oicuorcplopofle

Et'ry'b€rEene

Hexachlombuladiene

2+leEnon€ (MBK)

Iropropylb€nzsfl€

illsopropytEtlue{€

Methyl isrr-bu!/| €ther

4-!rehyl2f enlanone (M|BK)

tirethy'en€ .fitor*le

Naphlhalene

Styren€

1, 1,1,2-T6H o.oelharNe

1,1,2,2-Te{rad oroethane

Tehachloao€lhon€

1,2,$Tri*rlorobenzene

1,2,4-Tdcnbrub€nzene

1,1,1-Trid oroet'€ne

| , | ,z-Trichlorogthane

Trid oro€th€ne

Trichkrrofuoiom€thane (Freon I 't )1 ,2,lTn.filorcprcpan€I ,2,4-Tdmefr/benzane'1.3,$Trimethylb€nz6ne

Vinyl d odde

m,p-Xyi€ne

Tefdrydroturan

Elnyl€ther

Tert-anyl msthyl ether

Ethyl terl-buy €ther

Di+opropyl €th€r

T€rt-Butand / tuty' abofrcl

l,4oitxEn€

S uft ogale : 4+}.c monrcrcbe n E n eSunqate: fohJ€ne4oSu/'og E te : l, 2 -Dkhl ofoelh a N4 4S u fl ogate : Dlho nofl uoron eth dE

LCS 170:lt6s8€St)

Pr€{'arbd & AnatEedl 27-Mar{7

1,1.2-Td$bro fuoroet'ran€ (Freon t 13)

ActYonifl€

Benzene

8RL

BRL

BRL

BRI.

BRL

BRL

SRL

BRL

8Rt

BRL

BRL

ARL

BRL

ARL

BRL

BRL

BRL

BRT

8Rt-

BRL

BRL

BRL

BRI

8Rt

BRLgRL

BRL

BRI

BRL

BRL

BRL

8RL

BRL

ARL

BRI.

BRL

SRL

BRIgRL

BRL

49_249049.750.8

15.6

10.4

21.4

17.1

1g-7

t g/t€ wetpgtg wetpgr'kg w€tpdtg ret

Igkg uret

!g/kg v,/ol

t SftS ',v€t

ldkS rrer

trdkg d

!94!g w€t

Ugr'kg w€tpdkg w€t

ldtS w€tpgL/kg wet

lrdkg w€lpgl(g w6lpdkg welgL/ts vJet

pgl€ wet

!g/kg welpdks lv€t

ugts Yrel

UdkS v.,et

t g/kg we{

ugAg welpg[ts wcl

usas wet

lglq wet

w/t!g wel

Wr'kg wel

lgkg Yr€l

Lr€/kg re€t

!dl(g v,/et

Fdks wer

tigts w€l

lgtS Yrelpgkg wet

Ugfl€ wEt

Idkg w€l

Ugy'kg wet

ligts YJ6lIdkS wetpg/l(g wetIgr(1g w€t

lgL/kg w€tpgl(g wet

lgkS w€t

lgkg w€l

lgrkg w€t

70-1fr70'13070-13070-130

70.130

1.77-1757G13070-13070-130

5.0

5.0

5.05.05.050.0

5.050.050.05.0

5.05_05.0

5.05_05.0

5.05.0

5.0

r0.05.050.o5.05.05.05_0500.t00

50_o50.050.050.o

m,020.020.020.020.0

9899102

7A

109

869a

Thk labnh,r Epod is ,tot valid *ithour aE aat*orizd funaote on the covu page .+ Reporrable D€teation Limit Bht = Below Reporting Limir hge I l0 of 165

Page 620: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgenic Compounds - Quality Conlrol

Spike

Level

Source

R€sult

RPDLiflit

%RIC

%REC LinritsAnalytqs)

Btach 7031658 - SW846 50lSA Soil (to\r l€!e,,

LCS f/0fi658€S

Prepared & Analyzed: 27-Mar{7

Eromoct{oro(l|e[|ane

Brdnodi€hloronethane

Srornofofm

Bromornelhane

2€utanon€ {MEK)n€uVb6nzene

sac+utylb€nzen€

bd-Butylbenzen€

Cerbon dtsulfid€

Carbon btschloride

Chloob€nz€ne

Chlo.oelhan€

Chlomform

Chlorom€th€ne

2€hlorotoluen€

4.Chbrotoluon€

| 2-Dibrom+3.chloroprcpane

Dikomochlo,o.nef|ane

l,zobmmoelhane (EDB)

Dlbromorr€t|sne

l r.oic+ o.oberusne

I ,+Dichlorobenzen€

| ,+Dichlorobenzene

(Frcon12)

20.6

14.2

23.3

21.3

14.5

14.7

16.6

17.3

1 5 3't4.6

19.2

1 8 0

1 8 . 1

16_6

17.6

1 7 6'19.6

2 0 1

20.4

1 9 . 7

1a.a

19.5

1 7 . 5

16.0

17.0

r 7 . E

1 5 2

19.0

r7.0

14.4

1 9 . 1

1 4 . 1

15_2

1 6 8

16_9

1 7 _ 4

15.2

13.7

16.2

16.3

19.2'18.3

17.0

20.0

16,4

19.2'r 9.5

20.8

1 5 8

17.0

20.1

20.020_020.o20.o20.020.o20020-o20.o20.020.o20.020020-02 0 020.020.020.020.020.020020.020.020020.020.020.o20.o20.o20.020.020020.o20.o20.020.o20.020.020.020.020_020.020020.0m.o20.020.o20.020.020.020.o

tig/kg wel

Ug/kg wet

lgr'kg /€t

!gL/r(g wet

Ug/Kg wet

lrg,kg wet

!g/kg wel

Ug/kg wel

Pg'kg wet

!g/kg Y/et

Ugr'kg rvet

pg:/kg wel

!€y'kq wet

!g/kg wel

pSAS wet

lEkg rvet

!q/kg wet

pg/kg wet

pg/kg wer

t4/kg wet

!q/(g wel

Ug&g wel

psrtq r€t

!9,&g w€t

!S.t(g wet

Ligkg wer

!g/kg wet

pg/Kg wel

pg/kg wel

pq/kg wel

Ug4(g wet

pgkg wet

pgr'kg wet

!g/kg wet

Ugy'kg wet

!!/kq wet

!g/kg wet

Oc2 Ug/kg wet

l,g/kg w6l

!g/kg wet

Ug/kg wel

l4/k9 wel

pgks vr€t

!S/rg Yv€t

!q/kg wet

!g/kg wet

Lilt/kg wet

t/gL/kg wet

rcr'kg wel

!g/kg wet

tlg./kg wet

103 70-130

91 70-130

tt6 70-130

106 55.3.136

12 3A.A-142

74 70-13n

83 7G130

86 70-130

76 70-130

73 70130

96 70-130

90 55 3-130

90 70-130

83 70.130

88 70-130

88 70-130

98 70-130

100 64.7,139

102 70-130

98 70-130

94 70-130

98 70,130

88 70-130

80 34 4.167

85 70-130

a9 70-130

76 70-130

95 70-130

85 70-'t 30

92 70-130

96 70-130

70 70-130

76 70-130

94 70-130

94 70.130

87 70-130

76 607-140

6a 70-130

81 70-130

E2 70-130

96 70-130

92 46.1-145

85 70-i30

100 70-130

82 70.130

96 70-130

98 7G130

104 70.130

79 70-130

65 7G130

100 7G130

1 ,l Olchlorc€thane

I ,2{ichloroet'rans

1 ,1-Dichloroethene

ds-12-Dichltroethene

lr3ns-1,2oichloro€lheoe

l,2oichlo.opropane

1 ,3-Dicfilo.opmpans

22-Dichloropropane

|,|.Dii:l oropropene

d9'l,$Oi:hbmpropene

ttans-l,3.Did oropropene

EtMbenzene

Hexachlorobutadi€n€

2-He)6none (MAK)

hopropylb€rEene

4{sopmpyltoluerE

lroihyl ted-butyl efr\€.

4+vlethyl-2{€ntamne (M|aK)

liefiylene cfilorit€

Naphtrabne

n€ropyfio6nzefle

Stfen€

I,1,t.2-TelracfilotDethane

l,'1,2,2'l6Factrloo€thane

Tet'achlorcethen€

Toluene

l,2.ST.ichlorobenzene

Thit lohorulory rcpor1 is noa valid without an aathoiaed signelare on ahc cover page .

* Reporlabl€ Ihection Limit BRL = B€low Reporting Limit P a g € l l l o f 1 6 5

Page 621: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Voladle Organic Compounds - Qurlity Control

Brtch 70315s6 - SwM6 5035A Soil (low t€vet)

LCS 1703165r€Stl

Preparcd & Analyzsd: 27-Mar.07

1,2,4-Trx$lorob€nzene

1 ,1 ,1-Trid{ormtiane

1,1,2-Tridrloroethane

Tichloro€then€

Td€ilorofl uorofi*fEn€ (Freon 1 1 )1,2,3-Triciloropropan€

12,&Trifiehtbenz€ne'l,3,5.Trime$lylbenzene

Vinyl chlorid€

m,Fxyl€fle

Terahydlofurm

Ethyl elher

T€rt-€rnyl rnehf emer

Ethyl bri+uv ether

Dl+opropyl elh€r

Ted.Butanol / buv Elc.hol

1,4{ioxane

S u rDga/€ : 4 -Eto iafurc ro b en ze rcSurqate: Toh.Eno4|SufirBatg : l,2aichbroethane44Su''ogale : Dibro'''ofr u o Mn e I h ane

LCS Duo fio:ll65t€SD1l

Prepared & Aoalfied: 27-ttar-.07

1 ,1,2.Trid*rrc,ffiuoroeftme (Fleon | 13)

Ber|zen€

Eromocl oromOtiane

Brornodichloromethanegromoform

Erornofirethene

2€utamne (MEK)

n€uVlt)€nz€ne

sec.Butybenzen€

brl-Butylbenzene

Carbon disunde

CErbon tetad odd€

Chlo,obenzon€

Chloroelhan€

Chloroform

Cl ororn€thane

2Chlorotoluene

44hlorsbluen€

1,2€ibrcmGldtuopropane

Dibromocfi toaorhe(rane

1 z.Dib'omo€trlane (EOB)

Dlblonom€tran€

1 2-Dichlorob€nz€ne

1 ,3-Dichlorob€nz€fls

1E,315.2m.o16_6

14.0

22.O

14.2

17.6

17.3

19.0

20_o

20,9

16.0

18.6

17.6

14S

0.0

49_54 9 146.949.6

't 5.9

10.1

19.7

17.4

20.2

19.4'16.3

22.O

1 8 I

13.2

r 5 3

17.2

t8.0

15.7

11.7

19.6

17.7

18.2

16.6

18,1

16.1

r8.0

19.7

1S.8

18.8

18.3'19.6

20-020.0m.o20.020.020.o20.020.020-040_020.o20.020.020.020.020.02002650.050.050.o50.o

20.020.020.020.020.020,020.020.020.020.020.020.020.020.020-020.o20.0m.0m.020.020.o20.020.020_o20.020.o20.o

pdkg wel

pdkg Yr€t

ldkS y/et

UgkS {,et

Igl(g vYet

|rg € wet

lqkg w6t

l4y'kg wel

Ugkg wel

IS/kS ri,€l

pg/kg w€t

pg4(S w€t

!dl(g rvet

Lidl(g wet

IdkS wet

lgftg wet

pg/kg w€iclc2 !g/kg w6l

|lg^g welISrkg tvel

ldkS rrerpdrg vret

Ug[tS v,,et

IgkS vJet

lgr't€ we{

Ug/tg wet

pgikg wet

!g/kg rr€t

uSftg wel

Uqkg yiet

pdts yret

ldkS wet

ldkg vret

!gL[(g w€t

lgr'kg vJet

pgil€ w6l

Ig/kg w€t

pg/kg wel

lCftS YY€l

lqrg Yiet

Pgr'Ig w€t

Pg/kg wet

Fgtkg wet

pdkS v{et

#gfilg wet

Ugr'kg wel

Ugr'kg wel

Ig/kg wot

pdks w€l

92 70-13076 70-130100 70-13083 7G13070 5{t.E-140110 7Gr30

91 70-13088 70-13086 70-130

8S 70-13095 7G130100 70.130104 6s.113090 7G13093 70-13088 70-13t)74 70-130

34-15599 7G130

7G1N94 tF1fr99 70'131)

80 70-130 3fi 1.77-175 498 70-130 1187 70-130 1f01 70-13D 397 7G130 692 70-130 1fio 7G130 594 55.1136 1266 3a_&142 I76 7G13t) 386 7G't 30 4s0 70-130 57A 70-130 374 70-130 198 70'l3O 288 55.3-130 291 70-t30 |83 7Gr30 090 70n30 290 70-130 2so 70-130 Is 64.7-'139 299 70n30 394 7G130 492 TGi30 298 7Gr30 0

255t)25252525252550502525252525255025252525

50

Thb lzbodory ftpod ls ^o, eolU wiLhar/r tn dathotizrl slgnatarc on rte cover page .

. Reporreble D€rection Limit BRL = Below Reporring Limit Pagp I 12 of 165

Page 622: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volati le Organic Compounds - Quality Control

Spike

Level

SourceResult

%RF-C

Limits

RPD

LimitAnalytqs)

Birct 7031658 - SWE{6 5015A Soit (tow level)

LCS D(o f/O3l65€-BSOt I

Peparcd & AnaDzed: 27-MaF07

l,+Di{ibrobenzsne 18.0

(Freon12)

17.2

17.5

15.3

19.0

17.2

1 E . 6

16.4

1 4 4

15.4

18.5

1A_2

1 8 . 1

1 5 1'12.1

16.8

1 6 9

1 9 . 1

1 7 2

17.9

1 7 8

16.9

1 9 6

l 9 2

2C.O

1 6 2

1 1 1

18.4

17.7

1 5 6'19.2

1 6 8

14.3

21.9

1 8 3

r 8 0rE.236.5

1 9 3

17.9

19.5

1 7 1

18.6

l7.8

127

0.0

49.749.144.7496

1,1-Di.fibroerhane

l.2Oichbro€than€

l,lOicnbro€thsn€

cis.1 ,2-Dlchlor€tt€n€

trans-l,2olchloroethsn€

1 ,2oichloroprcpane,',3ol*|broprcpane

2,2.Didbropropane

l,lOidloropropene

cis-l ,!IH orcpropene

bans-1,3-Dichlo,ropropene

Ethylb€nzefi€

llexacHorobt Ladiene

2+€x8none (MBK)

4-lsof{otryltoluen€

t erhyl led+uty' ether

4-Methyl.2+enr,anorle (MtAK)

l.kry€n€ d{oride

Naphtrlalene

nPropy'b€nzene

StFene

1 ,1 , t.2-TeE&hlorcethane

1,1,2,2-Teir,(j*.rcethene

Tetrad oro€thene

Tolu€ne

I 2.STndrlorob€nz€ne

1 ,2,+Trid oroberEene

|,1,l-Tridrloro€thane

1 ,l ,2.Tnchbroetrane

T.ld{oroethefle

Tridrloro{uo$m€hane (Freon 1 1 )1 2.ST.id oropropan€

1 2,4-Trifir€thy'b€nzene

I,3,'Tnnr€ftyb€nzene

Vinyl ct{oride

m,Fxylene

o-Xylan€

Tetrahydrcfuran

Efryletr€r

T€d-erv m€Ury' €lfi€r

E6ry' bd.buty' €r'€r

DHsopropyl ether

Ted-Buranol / butyl alcohol

l,r$ioxEne

S,J'logate: 4&onpfutarobenzeneS|jl7wate: Toluene4SS|j'7ogate : 1,2 -Dichl oroo I h an e4 4S{//Iageta: Dibrutnfluorcfiethane

%RTC RPD

lig/kg w€l

lg(g w€l

IgAg wetpgftg wer

F94q wer

!gl(g vi,et

pdkS yJet

pS/kS yr€t

!g/Kg wst

lig/kg wet

lEkg wet

!Et($ wet

!g/t(g wet

Ug/kg wet

psrlkg wet

OC2 pgr'kg wet

ugkg wet

lgr'kg w€t

Ug/t(g wel

!g/t(g wel

[g/t!g wel

lgi kg wel

!g/kg wst

Fg/Xg wel

ugt(g wet

gglkg wel

trg/kg wet

lrg/kg wet

ug/kg wel

ug/xg wer

pg/kg wet

ug/Kg wel

pg/kg wel

ugfto wel

IEt(]g wel

lgkg w€l

Ugt€ wel

trg./Kg wel

lrg/tq wet

tgkg wel

|l(yKg wel

|l!r/kg wet

Ugi/Xo wel

pgdK$ welpgLi kg wet

clcl FgLnlg wet

oc2 !g/kg wet

LigL/kg n et

Lidtg rvet

ugL/kg wet

lgxg wet

90 70-13083 34.4-167 4

86 70-130 1

88 70-130 1

76 70.130 0

95 70-130 0

86 7G130 '1

93 7G130 1

92 70-130 4

72 70-130 3

77 fO-130 1

s2 70-130 2

91 70-130 3

90 70,130 3

76 60.7-140 0

60 70-130 12

84 70-130 4

84 70-130 2

96 70-130 0

86 46_t-145 7

90 7G130 6

89 70-130 12

84 70-130 2

98 70-130 2

s6 70-130 2

100 70-1K 4

61 70-130 2

86 70-130 1

92 70,130 E

68 70-130 4

78 70-130 3

96 70-130 4

84 70-130 1

72 56.8-140 3

1' t0 70-130 0

92 70n3O 1

90 70.130 2

91 70-130 6

91 70-130 2

s6 70-130 1

90 70-'130 11

98 65_3-130 6

86 70-130 5

93 70-130 0

89 70-130 1

64 70-130 14

34-155

99 7113098 70-13089 70-13099 70-130

20.020.020.020,o20.02 0 020020.020.o20.020.020.020.020.020.020.020-020.o20.020.020_020.o20.020.020.020.020.020.020-020_020.020.020.02 0 020.020.020.020.040.020.020.020.o20.020.020.020020050.o50.050.o50.o

255025

252525252525252525255025252525502525

252525252525252525

502525252525

2550

2525

25

Ihb ldton/ory repod it fiat vdlid wirtau! oE sattoriz.d sigttstzrc n rte cos.r page.

' Reportable D€tection Limit BRL = Below Rqnaing Limit Page I L3 of 165

Page 623: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgauic Compoutrds - Qurlity Control

Analyte(s) Result .RNLSprkeI*vel

RPD

LimitFlaBSource %RECResuft o/oREC Limits RPD

Barch 70f1693 - SWE{6 50JSA SoI (low tevel,

Bl.nk O031693€LKl)

Preparod & AnalFed: 2&L,lar47

t,|,2-T.idlorotifluoroethane (Freon 113)

B€trz€ne

B@mob€nzene

Bromocfilommethane

Bromodichlororn€trune

Brornoaom

Bromom€hane

2€uianoo6 (nrEK)

n-Eutylbenzene

sec€utylh€rEene

lerl€ulYbenzen€

Cerbon dF{lfde

Carbofl tretachloiide

Chlorobenzene

Chloro€than€

CHo@foan

Chklrornethane

24hbrobfuene

4-Chbrololu€ne

1 2-Dlbromo-3d$ropropan€

Dibromd$orom€thane

1,2-Dibromo€lhan€ (EDB)

Ditnomorn€ihsne

1 .z.{)itrlorcb€flz€ne

1 ,3Ol* orobenzene

1,4.Dk$loroberEene

(Frcon12)

BRL

BRL

BRL

8RL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

aR[

BRL

BRL

ARL

ARL

BRL

ea|.BRL

BRLARLSRLBRLBRLBRLBRL

ARLBRL8RLBRL

8Rr-8Rr_gRL

BRLARLBRL

pg/kg wel 5.0pgr'kg wel 100pg/kg rrel 5.0

ldkSw€t 5-0pgl€wet 5.0

Ig/kg rvel 5.0pC&g v/el 5.0

lgr'Xg rcl 5.0

lgr'kg v/et 10.0pgr'kg wet 5O.0pg/kgwet 5 0

lgr'kg wst 5.0pdtgn€l 5.0

|lg^g Yret 25.0pgL/kg w€t 5-0

t grkg wet 5.0

Fgr'kg vr€t t0-0pqrg$,el 5.0

!g/kg $€t 10_0

trdkS rvet 5.0pg/kgwet 5-0

Ug/|!gw€t 10.0pdkg wet 5.0

UdtS rrel 5.0

u€/kg wet 5.0

lgkgwet 5.0

FS/kg r{el 5.0

lig/tS wet 5.0pdl(gw€t 10.0

ISAS vrel 5.0

lgrkgwe't 5.0

t glkg wet 50pgtgw€l 5.0pc/kg lr€t 5.0pgftgw€l 5.0pdkS lvet 5.0

lgr'kg wet 5,0

tEAg wet 5.0

UdkS wel 5.0pgls r€l 5.0ggr'kg ri€t 5.0

lgL/kg wet 5-0

!g/t€ $/et 50.0

Fg/kgwel 5.0pgtgwel 5.0

lgr'*g wet 5.0

tgn(g w€t 5O.0pgr'kg wet 5O.0

ldkgwel 5.0

Pglkg ' €t 5.0

Fg (gw€l 5.0

| ,1oid{orc€thane|,2-Di.trloroettBne1 ,1 -oid oroethenecis-1,2.I)ktrloro€lhenetans-l,2Oichbroelhen€| ,2-Di{tioropropane1,$Otd{orog(opane2,2.t)it* oropropane1 ,1 .Dicilorop(opsn€

cts-|,$Di{t oroDrop€nelrans-1.3-Dldrlof opropen€Etryll}qnz€n€H€xacttorobltadien€2+lexanon€ (MBK)lsop.opylb€nz€ne4-lsoproFyltolugneMe$yl t6 +uV efi€r{-r,a€tnY.2-penhnone (M|aK)Mol,hy'€rE chbrueNephdral€nen-PropylbenzeneStyrene

TLt labratory rqorl it rot vdht wilhou an authorizty' lnt''dla'? oa 6a cavct pagz -

. Reportlble D€tcction Limit BRL = Below Repoding Limit Page I l4of 165

Page 624: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orga[ic Compounds - Quality Control

Spjke Sou.ce %REC RpDAnab't{s) Resulr Ftag Units +RDL Levet Resutr %REC Limirs RpD Linit

Edch 7031693 - SW846 5035A Soil (lo$ t€veu

Bh* 1703t€93€LXll

Pr€p€r€d & Analf.ed: 28-Mar-O7'1 ,1 ,1 ,2-Tetrachloro€lhane1 , 1 ,2,2-Tebachloro€lhaneTetlacftloloett€n€

1,2,lTricilorobenzen€

1,2,4-Tricfi lorobenzene

t ,1 ,l -Triciloro€rhane

I.|,2-Trid oroetEne

Trichloroetheoe

Trichloroff uoromehene (Freon 1 1 )1 ,2,STrid oropropan€

1,2.+T.imsflyltenzene

1,3,+T,imetnylbenzene

m,p-Xylene

GXYI€n€

T6hahydroturan

Elhyl etnel

T€.|-€myl methyt €ther

Ellhyl t€d{utt ett'€r

Di-isoproPyl elher

Tert-gulafiol / buv atcohot

1.4{ior€ne

Su fl og ate : 1 -Btoolofl u o ro b enze n eSulroga/€: Toluene4ASutr9gat9: |,z-Dichloroeth ane44Sunccale: Dibtotnffuoroneth ane

LCS r781693€S.tt

Pr€parod & Analt/.zedi 28,Mar{7

1,1 ,2-Tric*{ootrifluoroethane (Freon 1 1 3 )

Ac|yionible

Benzeie

Ercrnobenzene

BEmochloaorhelhan€

&olr|odichbromethane

Brcrmform

Bradrom€trsne

2€utanon€ (MEK)

n€ailylbenz€ne

3ec€uMbenz€n€

brt€urybenzen€Cetbon disumde

Caabon tgtrachloalde

Chlorobenz€ne

Chldgehan6

C.t ooform

Cl orom€lrrane

2.Chlo,robluerE

+4hb.obluefle

1 2-Oft mmo-kfi lo$propane

ORL

BRL

BRL

SRL

BRL

6RL

BRL

BRL

BRL

ARL

ARL

ARL

BRL

BRL

BRL

BRL

ARL

8RL

BRL

BRL

ARL

ARL

ARL

49.65 5 953.2

21.O

1 4 2

19.8

1 9 3

20.9

1 9 . 8

207

21.3

2 0 9

15. '1

19.2

19.7

19.9

20.2

18.8

20.a

18.5'19.6

21.8

20.a

20.3

20.3

50.050.o50.o50.0

2n.om.o20.020.o2 0 020.020.020020.020.020.020.020.02 0 02002002i.o20.o20.020020.020.0

lgr'kg w€l 5.0

PEkg wet 5-0

Ugr'kg wet 5-0

!g/kg wet 5.0pg/kg wer 5 0

!g/kg w€t 5.0

lqkS w€l 5-0

pqr'(g wet 5.0

LigL/kg wet 5.0

t,gkg wet 5 0

!g/kg wel 5.0

pSn(gw€t 5.0

!g/kg wet 5 0pg/kg wet 5-0

Lrgkg wer 10.0

lrgl(g wet 5.0

lgr'kg w€l 50 0

ligL/(gwet 5.0

pg4(g wet 5.0

Lig/kg wet 5 0

Ug/l(g wel 5.0

!g/kg we( 50.0

pg/kg wet 100

lrs/ts wet

!S/kS wet

!gl(g wetLig/kg wet

pg/kg wel

Pg/kg w€t

!g/kg w€t

!g/kg wet

pEKg wer

trg/kg wet

t g/ko wet

!g/kg w€t

ljEr€ wet

lgr'kg lvet

!g/kg wet

lgr'kg wet

UgL/kg wel

pg/kg wet

lgr'kg wel

ug/kg wel

ps/ks wet

!g/kg Y/st

!g/kg wet

!g/kg wet

!g/kg wet

pq/kg wet

89 70-13099 70-130112 70-tm106 70-130

105 70-13071 1.77-17599 70-130s6 70-130104 70-13099 70-1:'0104 70-130106 70-130104 55 3-13676 38 a-14296 7G13098 70-130100 70-130101 70-13094 70-130104 70-13092 55.313098 70-13010s 70-r 301M 70-130102 70-130102 70-130

Thh laborarory Epad it dot vatial *tlhoq! on aathofiaed signafuE on the cover page_

+ Reportable D€cction Limit BRL = B€low Reoortins Limit Page I l5 of 165

Page 625: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qurllty Cotrtrol

4I4f,"(") Result Flas unirsSpike

lrvelSoulce

Result %EEC Limits RPD

Brtch 703169J - SW846 5035A Soit oow levet)

LCS r703t6g3Astl

Prepercd & Anslyzed: 28-Mar-07

Dibromochboriethane

|,2{ibromoefiane (EDg)

DibEmorn€lhan€

I,2-DiJ orobenzene'l,3{)i.hbrDb€nz€ne

l,4Olchb.obsnz€n€

Dic.itlorodinuo.om€then€ (Freonl 2)1,l-Dichloro€thane

1 2Oichloro€thane

1 .l-Dbhloro€thene

cis-l,z-Did oroetheno

trans-1,2-Dicfi lorBthene

I,2.{)ichlorcpropai€

1 ,SDli oroF opan€

2"z-Dbhloropropane

1 ,1 OichloroproFene

cls.l,3.Dic'|loroprop€ne

fr€n9-t,3oia* oroprop€n€

Elhylbenzene

Hexachlorobutadiene

2-l'l€xanon€ (MBK)

lsopaopylberEon€

+lsopropyllolueoe

M€thyl brt+uM ether

a-iretttyl2+s$anone ( tBK)MerhyteGe dtbride

${6phthal€ne

StyYeng

1 ,1 ,1 ,2-T€tachbroet||ane'1,1,2,2-T€trachloro€thane

Tetrd orcethen€

ToluerF

1,2,!Trld or$Gnzene

1 ,2,+Trichbrob€nz6fle1 ,1 ,1 -TddrbE€than€

1 ,1 ,2-Tri6bro€hanc

Tdchhf€th€De

Tridrlorofuorornelhane (F.eon 't 1 )I ,2,&TdchlorDpropaneI ,2,+Tdmetrytb€nzEne1,3,tTlifiEthytbenz€ne

Vhtl dr|o.ide

m,trXy'eneo-XyloneTeLEhyd|!'ftrrdnE*|yl €therT€ri-€my' nethyt €herEhyl brt.butyl gtrtsr

Di-isopropyl ethsrT6.t-ButErd / buty atcotrol

21.6

2 r .620.221.220.319.825_419,019.7tE.4

18.220.420_717 .118-8'r9.6

20.2m.818.017.A19.620.o19.91 9 518.020.3r9.2m.721.620.820.119.720.119.4't s-021.3r9.5r9.8

23.019.819.823.341.1

21 .418.4r9.8la.720.3ts.4tm

!g/rg wet

Ug/kg w€t

|lgl(s v,/etpg/tg wet

rclkg s,etydkS v/st

F9ft9 w€tpglg wet

!g/kg wel

ldkS wel

lgL/kg n€l

!S/kS rv€tpg,tg w€tpgn€ wet

lrg/l€ wet

Ig/kg wetpdts wel

!94q w€t

!S/kg wel

USI(g vr€t

Idrrs rvet

lgrS wet

trykS vet

lrg/lq wetpglkg wetpg^g w€tpgrl(g wetpgkg wel

!S/kS Y{€lgg/kS wet

lgr'kg net

!gn(g wet

tdks wet

Irg/kg wetyg/kg wet

Pgit{g w€l

FdkS wet

ldkg u/el

lgl€ v"€t

lgr'kg w€t

!Sn(S Y€tpSlkS wd

$/kg welpgr€ wet

Igftg wet

lgrkg w€t

Pg'kg welpdkg vr€l

US/kS wel

US/kS w€l

sdkg Yret

20.020.020.o20020-020.o20.0z).0m.0m.o20.020.020.020_020.D20.om.0m.020.020.020.o20.020.020.0m.020.0zJ.020.020.020.020.0z0_020.020.020.o20.0m.0m.o20.om.o20.020.o20-040,0m.om.o20.0m.020.020,02fi

108 64_7-139108 70-130101 70-130'106 70-130102 70-13xs0 70.130127 y.+167

95 7G.13098 70-13092 70-13098 70-13091 70-1I)102 70.130104 70-13086 7G130s4 70-1 3098 7Gt30101 70-130104 70-13090 60.7-14083 70-13098 7G130100 7G130r00 7G130sa 46.1-14590 70"130102 70-13096 70-130104 7G130108 70.130rM 7G130100 70-13098 70-130100 7G.t3097 70-13095 70-t 3t)106 70-130s8 70-1309g 56.8-140115 70.1mso 70-13090 70.130116 7G130103 7Gt3ot07 70-130

92 7{rt3o99 65-913t)94 70n 30102 m-130s7 7G13090 7G130

This lonatuory ..put k not did ,ti hoct on orfrorLd dgr',ohre oE tle cor* Fege.' Repntable k€clior Umit BRI = Bdow R@orting Limit Ptee l l5 of 165

Page 626: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compouqds - Quality Control

Spike Sourcc %REC RIDAnalyt{s) Rcsult Flag Unirs .RIL L€vel R€sult %REC Limirs RpD Limit

Br|cb 7031693 - SW846 503sA Soit (low levet)

LCS flUltGStAS

Prepared & Ana\zed: 28-Mar-07

|,4-Dioxane

S urqgte : +arc n'0fl u orob e n ze n eS'']'ro,gate: Tolu@e-doS u mgale : 1, 2D bh loroe tt a n e 4 4Su rrogete : Dittn fl nfl u orcm eth a ne

LCS D{o l7(B|693€SiDt)

Pr6pe€d & Analyzed: 28-irar-07

1,1,2-Trid{otofffuoro€lhan€ (Fr€on 113)

Benzene

Bromobenzene

Bromod omm€thane

Brcmodiit*yomet.|ans

Baomofom

BrDmomelhmo

2€uhnone ([rE()

n€utylb€nzene

s€c-gu!y'benzerte

tert-ButylberEene

CE bon disulfide

Csrbon bbachlorxle

Chloobenz€ne

Chlo.oethane

Chlo.obrm

Chlommelhane

24hlorotolu€n€

4-Chlorotoluon€

1,2-Dibrom}3+ o.opropan€

Dibromod oomethane't,2-DibromosthEre (EDB)

Oitromomelhane

t ,2-Dlchlorot€nzene

1,$Okfilorcbenuene

1.+Didrlorobenzene

Did 6odif uorohethane (Freoni 2)

1,1-Di{filord€thane

1,2-Dk hloroethane

1 ,l Oicnbrc€lh€ne

cls-1P-Oid{orceth€ne

lrans-1,2Olctloro€thene

l2olchlo.opronano

I .S{)idrlo.oproFane

2,2-Dic*rktopropan€

| ,l .Dlchktroprop€ne

cls-1,3.Dldioroprcpene

trafl s- l,3-oicibropropene

Ethylbenz€ne

H€xachlorobuladi€ns

2-Hexanone (MBK)

lsopropybenzene

2M

47.250.551.350.3

15.7

19.2

14.7

20.2'19-3

19.6

19.4

21.O

15.3

21.6

19.9

20.6

19.0

202

15.2

18.9

2 2 5

20.4

20_7

20.1

20.0

19.9

20.0

20.6

21.1

19.8

27.O

18.6

1 9 . 5

18.6

19.6

14.4

19.8

19.4

17.1' t9.0

1S.0

19.3

2 0 2

1 9 9

16_0

19.4

Ig/kg wet

pgy'kg wetpg/rq wetpEKg welpExg wel

pgr(g wet

ps'kg v/et

pSkg wet

lgr'kg wet

pg/kg w€t

lgks w€t

tlg/kg wet

!g/kg wet

!Er(g wet

pg/kg wet

!g/kg wet

!g/kg wet

pg/kg wet

Lig/kg wet

pg/kg wet

!g/kg wet

pg/kg wet

trg/kg wet

!g/r(g wer

l.lg/kg wet

!g/kg wet

pg/kg wet

pg4(g wet

pS,4(S wel

pEr(g wet

pg/kg wet

pdks wet

pdks yvet

Fg{kg \,,/et

pdkg wet

pg/l(g \4,et

pqL/kg wet

pgkS wer

lg/kS wer

Ig/kg w€t

pgL/kg welpErq w€l

!g/kg wel

Ug/kg w€l

Ugftg wel

pgftg wel

pq/kg wet

t g/kq wel

lrg/Kg wet

20050.050_050050,0

20.020.020.020.020020.o20.020020020.020.o20.o20.020.o20.o20.o20020.o20020.020.02 0 020.o20D20020.020.o20.02 0 020.020.020_020.020.020.o20.02 0 020.020_020020.020-020.020.0

1O2 1415594 70-1fr101 78130103 70-130lDl 70-130

116 70-130 1078 1.77-175 Is 70-130 394 70-130 2101 70,130 396 70-130 398 70-130 697 70-130 I105 55.3-136 176 34.6-142 0'f 06 70-130 12't03 70-130 5100 70-130 0103 70-130 295 70-130 I101 7G130 396 55.3-130 494 70-130 4112 /0-130 3't04 70-130 0104 70-130 2100 70-130 2100 &.7-139 I,00 7u13D I100 70-130 1103 70-130 3106 70-130 499 70-130 0135 U.4-167 693 7G130 298 70-130 093 70-130 1

98 70-130 092 7O-13O 199 70-130 397 70,130 786 70-130 095 70-130 I95 70-130 396 70-130 5101 70,130 3100 60_7-140 11

80 70-130 11

97 70-130 1

255025

25

25

50502525

25

255025252525255025

25

5025252525

25252525252525502525

Thb leborutotr ftpo.t k ttoa volid wilhout aa aathoized sigtarure on the cover Fage.* Reportable Detection Limir BRL = Below Reporting Limit Page I l7 of 165

Page 627: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtile Organic Compounds - Qurllty Control

Analyte(s) Result Flag

Soulre %RECResult %REC Limits RPDUnits *RDL

Spikekvcl

RPDLimit

Brtch 7031693 - SWE{6 5mSA Soil (low l€vel)

LCS Dup fio:tl693"gSDl I

Prepar€d & Analfzed: 28-Mar.07

41g@ropyltLolu€ne

Methyl tert.buty' e0|€r

4-lr€fryf2-p€r,anoru (MIBK)

M€lhyl€ne c,hlorile

Naphthalene

Styrene'1

,1 ,1 ,2-TeFa.filorethane

1,1,2,2-Telract om€then€

T€trachloro€lhene

1,2,}Tri{:hlorobenzene

1,2,4-Trkt ora6€nzeoe

1,1,1-Tricnb.o€ttEne

1 ,1 ,2-Trichbmethane

Tricf orofiuommethane (Frcdr 1 1 )1 ,2,3Tdcnbropmp€ne

I,2,+TrioEth@nzsn€

1,3,s-Trimethy'b€nzen€

m,p.Xylene

o-Xylene

Etiyl ethef

Ted-amyl m€hyi ether

Elhyl tert-butyl ef|er

Oi-lsopropy' €t|er

Terl-Bulanol I bulyl alcohol

1,41)ioxane

S u1o g Ete : 4-Btonafl @roh e n zeneSunogale: Toluene4SS ufiOga te : 1, 2O ich b methane4 4Sunogate : D i h tDnE fl u oronelhane

B|tch 7031779 - SW&46 5035A Soil oow l.vet)

Bhnk 1ru31779€LXll

P.eptr€d & An€'fzed: 29{lar{7

1,1,?-Tricnbrot tffuo.odhsn€ (F.eon 1i3)

Acr/oniblb

Benzene

Erornobonzene

Srorflod oron$lhan€

Bronrodid*)ronlethane

BronElonn

8turnofit€liane

2€ubnone (MEK)

n€utylbenzen€

s€c'BuVb€rE6ne

tefl-AuvberEene

C€rbon disulfdo

20.818.816,2

19.220.020.419.819.620.519.719.920.418_920.6m.020.222.720.820.3

{0.820.418.419.6t8_119.6r9.0r7020944.850.4

50.1

BRLSRLBRLBRLBRLgRL

sRr-BRI

BRL

BRL

BRLgRL

BRL

sRt

Ugikg wet

t8/kg wel

pytS wet

PdkS Yr€r

UgkS rv€t

$grkg {ret

yg^g urel

!g/kg wel

pdkg w€t

!S/kS ret

ldkS wet

!9r'k0 wet

Ig/kg w6t

rc/kg l/t€l

lgtS wet

udkS wst

Ig/tg wst

||gitS,re{

!g/kg wel

pgkS $,el

lg/tg w€t

Ugr'kg wet

pgrkg wet

Ig/kg wet

pglq w€t

ldkg vr€t

UdtS Yret

trg/kg wet

lgr'kg wet

Fgr'kg wel

Ug/kg n6l

t g'l(g lvel

lgrkg w€tIdkg w6t

20-020.020.020.o20_020.020.020.020.o20.020-0m.0m.020.o20.020_om.om.020.020.020_o40.020.020.020_020.020.020.o200200fl.o50.o50_o50.o

10{ 70-130

94 7G130

91 46.'l-145

86 70-130

96 70n30t00 70-130102 70-130s9 7G.130s8 7G130

102 70-t30

98 70-130100 70-13)102 7G13094 7(}.t 30103 7G130r00 70-130r01 56.&140't14 7G1301ft 70-'t 30102 70-130118 70-13t)102 70.130r(x 7G13092 70-'130

98 65.3-13090 70-130s8 70.130

95 7G13085 70-130104 3+155

. 9a 7&1mt01 7L1fr101 70-130101 70-130

6756

2

6

0051322

0.9532130'I

2

2

252550

25

25

25

25252525

5025252525E25

E25

25

!S/kS wet 5.0

ldkSwd 100pgr'@wst 5.0ydkgw€l 50ygkgw€t 5.0

lgtkg wel 5.0

ldrSw€t 5.0

ldkg wet 5.0

t g4!g w€t 10.0

USASwel 50-0

trC/tSwdt 5.0

lgtg y/et 5.0gg/kg rv€t 5.0

lgr'kg wet 25.0

Thl$ latodory rqotl is not erlld nithornt n rnahor*pd sigtrsture o^ drc coee. page.

' Reportable Detection Limit BRL = Below Repodng Lioit Page lt8 of165

Page 628: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orga c Compounds - Qrality Control

Spike

Brtch 7031779 - Sw846 50JSA Soil (tow tcvet)

Elank flUllz79€LK1)

PEpar€d & An€l!.zed: 2g,t4ar47

C€6on tetachbrid€

Cl orob€{Eene

Chlo.o€than€

Chlo.olom

Chloomohane

2€hlorotoluene

44hlorotoluene

| zoib.oftlo-34dpnr'opane

Dlbrqnod{oroan€than€

l2olbromoethane (EDB)

Dibrcrnolrbthane

l,zoidrbobenzene'l ,3oi*lorobenzene

1 ,4Diclllitobslt:p/?€

(Frcon12)'1,1 -Oidrloroethane

1J-Olchloro€hane't ,1 Oidlo'roethenecjs-l2-Did oro€fn€netrans. t,?-Dichlr.oethen€1 .2-Dicfibloprooane1 .SDichloropropsne22Oi$loropropene1 .1 Oicihwropened9l ,&Dlchloropropen€t-rns- t,go,chlo.opropen€Elhtbenz€n€H€xachlorcbutadi€ne2-He,€none (MBK)lsopropylbenzene+lsopropyftolueneMstlf, brl$tltyl enr€l,grr€try!2+€rtanons (MIBK)irs0tlene chbrkieNaphfialeoen€rosrybenzeneStrenel.t . t J-TetracfdorDethan€I,1.z.2-Telract oo€than€Totr&ldoroethen€Toluene| ,z,STdflorobenzeneI 2,+Tri6brob€nzeneI .l ,l-rti.*t|f,.tlx.f'€ne| ,l ,2.TriilorsfieneTftlrloro€theneTridrlorof uorcmehane (Freon 1 1 )I,2,$T.ichloroprcpane1,2,4.Trirnehylbenzenel ,3,STrjrn€by'berEen€V|rry| cfilorid€

8RL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

8RL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

ARL

BRL

8RL

BRL

BRL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRT

BRL

BRL

BRL

BRL

8RL

BRI,

ARL

BRL

BRL

BRL

8RL

8RL

BRL

BRL

BRL

BRL

8Rr-8RLBRL

!g&g Yv€t 5.0

Pgtgilet 5.0

lgr'kg Yret 10 0

!g/kg wet 5.0

lgr'kg wet 10 0pg/kg wet 5 0

Ugr'kg wet 5.0

Pgkgwet 1O.O

pgkg we{ 5 0

ug/kg wel 5.0

lgkq wel 5.0

rc^g wet 5.0

Ug/kg wet 5.0

fdkSwet 5.O

$r'kg wel 10.0

Ig/kg wel 5.0

!g/kg wel 5.0

pg/kg wel 5.0

pg/kg wel 5.0

Wkg wet 5.O

ugkgwet 5.0

!g/kg wet 5.0

Pg/kg wet 5.0

Pg/kg wel 5.0

Ig/tg wet 5.0

pSlkgw€l 5.O

Pg/kg wel 5.0

mr'kg wel 5.0

lg.itg wel 500

lgLlkg wel 5.0

Pg/kg wet 5.0

Pg&gwet 50

!g/lq wel 50,0

pgr'kg wet 5O.0

LigL/kg $/€t 5.0

lgkg r,/et 5.0

Pdkg wet 5.0

Pglkgwet t0

Fq^g wet 5.0

pgr'kg wet 5-0

Fgtkg w€t 5.0

pdks wet 5-0

pS&gwet 5.0

P9'l(9$€t 5.0

Ig4(gwet 50

Ugn(gw€t 5.0

USt(gw€t 5.0

lgAgwet 5.0

Yg,/kg wet 5.0

llgl/tg wel 5.0

pgr'kg w€t 5.0

Thk hbontory rcpotl is not vtlid uithout tn ztthori.d sigr.arure on the cover paEe .

* Reportable Detection Limit BRL = Below Reporting Limit Page I 19 of l6J

Page 629: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qurlity Control

Analyte{t Result FlaC Units Result %REC Limils

RPD

Limit

Bsrch 7031?79 - sw845 5035A soit Cow levet)

Blank {703l7t9.BLK'll

Prepared & Anavzed: 29.Mar-07

m.p-Xylene

Tetrahydroturan

Elhyl ethe.

Ted-amyl mehyl elher

Ethyl tsrtiutyl elher

Di-isopropyl etfler

Tert-Bubnol / butyl alcohol

1,+Dicxan€

S u nogale : 4 -B mnoff uo tube n ze n eSunogale: Toluene4Ssuftogaae: 1,z-Dichlorcethane44Su ECEate : D tb rcmon M Mn dh a ne

LCS Ooiltzgast I

Prepared & AnalFsd: 29-Mar{7

1,1,2-Trichlorolriff uoroetharE (Freon I 13)

Ben:sn€

Ersnob€nzene

Brornodrbrorll€thane

Brornodlt [email protected]

Bromolorm

Eromo[€than€

2€utanone (MEK)

n-Butylbenaene

sec€utylbenzene

terl-Eutylbenz€ne

Ca6on disrJlfide

Caftofl btacnlodde

Chlo.obenzene

Chloroethane

Ct{oroform

Chkrmm€fhsne

2-Chlomtduerl€

44hlorotolu€ne

1 2-0lbromo-3drlo,ropropane

Dibro.nodrlorodnef tan€

1,z-DibronF€than€ (EDB)

Dibfomoanethan€'l

,z-Dichlorobenzene'1,3-Dichlorcbenzene

I ,4oichbrobenzeno

(Freon12)

BRLBRLBRLBRLSRL8Rt-BRLSRLARL.t&950.557.153.2

r7.410.s19.219.5

21-121.0

18.715.918.018-8't9.9

15.418.2

21.617.720_619.721.O20.319.9

20.620120.421.320.520.319.518.920.716.7m.81 9 . 1

rs.919.8

fi.0

50.050.0

20.020.020-0z).0m.020.020.0m-020.0m.02t.020.020.020.020.om.020.0m.o20.o20.020.020.0m.020.020.0m_020-020.om.om.020.o20.020_o20.o20.o20.0

34_4-167

7G130

70-130

7G.130

7Gl30

70-130

70-t 30

7G',|30

pqlgrv€t 10.0

ldkg Y/et 5-0

ugr'kg u/et 50.0

USftgwet 5.Opgr'ko wet 5.0

Fg/kgw€l 5.0

trg/kg w€t 5.0

!4kS w€l 50.0

Ug|/Xg s/et 1m

!g/kg M,elpgL/kg w6tpg/kg rv€lrc/kg w€l

|lgLnq wet

Igrkg w6tpg/tg wet

Pgtg w€l

lqlg vJ€t

!g/kg wet

lgr'kg wetpgr'ko wel

t€4(]9 w€l

USAg r€l

lgltS w€t

IdrS wet

rcr'kg wet

Igr'kg wet

l€/kg w€t

Ue^g rl€tpS/kg wel

lgrs wet

lgkS wet

lgr'kg wetpg/t€ wet

rcftg w€l

trgftg w€l

Lrgfl€ w€t

Ugr(g wet

!91fl!g wet

UdkS sret

lrg*g ' €t

Pg/tq rct

!94(g rvel

Lrglg ir€t

rcttg wet

trgr'lq.rJ€tugAg w6l

lqtg w€t

!9r'k0 w€t

9E 70-1fi101 7E1g114 7G130106 7G1m

87 70-13054 |.n-17596 70-13098 7G130112 70-r 30106 70-130t05 7{F1301oo 70-13094 55.313680 3A.&142s0 z)-r3094 70-130r00 70-13077 7c-13091 70-130108 7013t)s8 55.3-130103 7Gr30g8 70-'t30105 70.130102 70,1m100 7&130103 64.7-139t04 70.130lo2 70'13)106 7&130102 70-1301O2 7{1'l3o

I .l -Dldllo.o€thane

1,z-Di{t oroethane

1,1-DiJ orethene

cis-1 2oi$loroethefletrans-l,z{)id or€fh€og

1 ,2-Dichloroprop.ane1 ,${)lchlo{opropsne

94

104

64

104

96

100

99

Thb bbonlorf rqort b fiotr/d l ttiittout aa c$horitl sigrraure on the @wr pqe.

4 R€Fntabl€ D€t4ction Lidrit BRL = Below Rcporring Limit Pag€ 120 of 155

Page 630: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compoulds - Qoality Conarol

Spike

LCSt703t7t9€st)

Preparod & AnElFed: 29-[4ar-07

2,2oichbropropan€

1 ,1 OL+ oropropene

cis.1 ,}Di{* orQropene

trans-1,&Dicitoropropene

Efirb€nz€n€

Hexachlorobutadiene

2+lexanone (MBK)

koprofMbenzene

4{sopropyt\bluene

ldelhyl brl+Uty' ether

4.li4ethyl-29€ntanone (MtBK)

MethMene cfitodde

Naphttr€le{r€

Styrone

I ,l ,1 ,2.T€lrachloro€thane

1 , | .2,2-Tetacftloro€tfEne

Tehad oroetlien€

Toluens

1.2,'Tdcnbmbenz€ne

I ,2,4Tnct orcb€nz€ne

1 ,1 ,1-Tricibro€thane'1,1,2-Trichloroethane

Trid{oroeth€ne

Trid{orcnuomm€flane (Freon 1 1 )| ,2,STrid oropmpane

1,2,+Trimethylbenzene

| ,3,tldm€frylb€nzeneVhyl ctloride

m,p-Xylene

o-Xylene

Tetralrydtofurao

Ethylef|€r

Te.l-amyl m€thyl ether

Elhyl ied{utl eth€r

Di-i6opropyl elh€.

Tert€ulsnol / hrtyl atccfiol

1,4-Dioxane

Su''r8sle : + Brornfl u orche n E neSufioCate: Tolr6n648Sudogate : 1,2&tlorcethaoe44Suoogate : Dihrurcfluotomethar@

LCS Duo lTCll77g€SDl)

Prepar€d & Analyzod: 29.Mar47

|,|,2-Tlidiolotriff uoroedrsne (Freon 1 13)

AE ylonitil€

Benzene

Bromob€rEene

Brcnndrloro.rEtlafle

ArorFdicttboo€ttene

17.1

1 8 3

19.1

20.1

21.1'18.8

1 6 1

19.4

1 9 5

2 1 . 3

18.4

17.6

21.1

18.8

21_4

20.5

18.0

20.2

19.8

21.2

201

1 9 0

21.8

20.7

1 6 0

21.4

15.7

20.0

1 7 7

41.5

2 1 3

18.4

20.3

19.2

21.1

19_3

169

203

48.549.650.451.6

18_1

1 1 . 6

1A_7

18.6

20.0

20_4

m.3

lgrkg wet

trg/kg wet

Lrgkg wet

pg/kg wel

ug/kg wet

UgkS wet

lgkS Yv€t

!g/kg wet

pg/llg wet

!g/kg wet

ugkg w€t

ugn<g wet

pgrkg wet

pg/kg wet

Ug/Kg wst

lgL/kg wet

!g/kg wet

Ugftg wel

pg/kg wel

ldks wet

!g/kg wet

Ig/kg wet

pSI(S wet

l4/kg wet

!g/kg w€t

ug/kg wet

pg/kg wel

Ug&S wet

pg/kS lvet

Lrg/kg wet

Ult/kg wet

,lgkg wel

!g/rq wet

ugikg w€t

Ug/kg wel

Pg/kg wet

ldkS wet

lgrkg wet

ugKg wet

Pgr'kg wet

!g/Kg wetyg/kg wet

ugikg wet

pgks vret

!g,'kg wet

pg/kg wet

!g/kg wet

lgr'kg wet

ug,kg u,e(

20.o20020.020_020.020020020.020.o20.020_020_020.020.o20.o20020.020.o20.020.020.020-020_020020.o20020.o2 0 020.040.02 0 020.020.020020020.o20020050.o50050050.0

20.020.0m.020.0m.020_020_o

86 70-13092 70-13098 70-130100 70-130106 70-13094 60.7,14080 70.130s7 70-13098 7G.t30106 70-13092 461-14588 70-130106 70-13094 m-1301O7 70,130102 70-13{)s0 70-130101 70-13099 70-130106 70 130102 7G13095 70-1301m 70-130104 70-13080 56_8-140107 70-13098 70,130100 7G13088 70-'t30104 70-130'106 70-13092 70-130102 65.3,13096 70-130106 70-13096 70.13084 7G130102 3+1559/ 70-13099 7G130101 711301O3 70'130

90 70.130 35A 1.77-175 794 70-130 293 70-130 5100 70-130 11'102 70-'t30 4102 70-130 3

2550

2525

25

Brrch 70317?9 -Sw646 50JSA Soit (to$ te!e,,

This lobonro.f rcFon is zot volitl u,thout ed ddhoriztd si|Eatwe on the cowr page.

* Reportablc Det€ction Limit BRL = Below Reporhng Limit Pag€ l2l of 165

Page 631: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgaric Compounds - Quality Cootrol

SpikeLevel

%RECLimitr

RPD

Limit

Source

R€sult %RECResult Flag Units RPD

Batch 7031779 - SW846 5035A Soil (low lev€l)

LCS Ouo fl03177$aSDl)

Prepar€d & Analyzed: 29-Mar47

Baomolom

Bao|mmelhane

2€utanon€ (MEK)

nSul!,henzen€

sec-BuVbenzene

tert-gutylberEen€

Ca.bon disulfide

Carbon tet'adrtodde

Chbroti€nzeoe

Chloruethane

Chlorotorm

Chlorom€thane

24hlorotoluen€

44htorotok €ne

1 2Oibronlo-3-afi bropropane

Dibrumoc* oofirehane

1,2-Dibton'o€tha'le (EOB)

Oibrcmometlane

I ,2-Oicnbrobenzene

| ,3-Didrlorobenzene

I .+Oinlorcb€nzen€

Oicilorodinuoromethan€ (Fteont 2)

1 , 1 Oibhloroethane

1 ,OichbroefEne

1 ,1 .Dichlom€thsn€

cis-1.2-Olchloroethen€

fans-l,2oichloroethene

| ,2-Dichloropropane

l,SDldrloropmpEne

2,2-Dichlor@ropane'l,1-t)id orerop€ne

ci$1,3-Dichbropropefl e

lrans-1,$Oichloroprop€ne

Elhylb€nzene

Hexadrldobutsdiene

2-Hexanone (MAK)

lsoFopylbenzene

4-l60propyltofuerE

MetV brl+utyl eft€r

. +Mslhyf2tentanone(M|BK)

Melhylene c'|lorid€

NEphthalene

n+mptb€nzen€

Styrene

I .'l .1 ,z-Tebachloroethane1,1,2,2-Tetracnloro€[lane

TsiEchloaoeihene

l,2,}Ttichlorob€nzene

1,2,lLT,l,chlorobenzefl €

1.1.l-Trid oro€hane

20_7

17.7

14.6

1 6 3

17.5

ra.7t8.018.3

19.4

17.0

19.9

1a_7

19-0

18_6

20.0

21.0

21.0

m.019.7

19.0

10.5

20-4

16.4

20.2

r6.6

m.2

14.2

t 9 . l

19.6

16.9

17.A

19.6'19-0

17.3

15.2

17.4

l8. l

20.7

18.0

16.9

20.6

17.0

19.4

21.3

18.3

19.0

16.6

21.r

19.6

18.8

lgr'kg wet

t giko wetpg/kg $,€t

ug/rlg wel

Pslkg welpgl(s vr€l

tgl(g w€t

Fgftg rvet

lgrtg vret

ugul€ wet

Ig/l€ welpgftg wet

Ignlg wet

Fgr'kg w€t

trgikg wet

ldtS wet

ldkg wet

!g/kg wst

IgftS wet

!g/kg wetpg/kg wel

llgl(g w€t

9g/tg w€l

|lgkg wetpdks wet

ldlS rct

trgL/kg rv€tpgr'kg wet

lgr'kg wet

rc4lg w€t

Ug4!g w€l

Ig/kg wel

rgfkg welpgks w€lpdkg vret

t/dlg w€t

!g/kg w6t

IS/kS vlbtpdl.€ v{et

lroftS $€tpg/kg wel

!g/l€ vret

Ug/kg w€l

wkg tr€lpdkS welpdks Y{et

lgr'Ig wet

lgffg v/et

Itgl(s v{gt

trg € wet

lgrl(g w€r

20.o20.020.020.020_o20.0m.020.020.020.020.020.0?0.020.020.020.020.020.020.o20.020.o20.020.0m.02t).0m.020.020.o20.020.o20.020-o20.o20.0m.om.020.020.0

20.020-o20_0t0.020.0a).oa).0m.020.020.o20.020_o20-o

104 7G130 188 55.$.136 f73 38.8-142 I82 70n30 S88 70-130 794 7G130 6s 70-130 1692 70.130 r

97 70-130 1185 55.3-130 3tm 70-130 3s4 7L130 4s5 7G130 1093 70-'r3o I100 70-130 0105 64.7-139 2t05 70-130 I100 7G130 298 7Gr30 I95 70-t30 7s2 70-130 't0

102 34-+167 492 70-130 2101 70-130 38i) 7Gt30 It01 7G't30 391 70"130 5s6 70130 49a 7Gt30 164 70-130 283 70-130 396 70-130 298 70-130 295 7G130 1186 60.7-140 976 7G1 30 5E7 70-130 tl90 70-t30 I104 7Gt3o 290 46,1-t45 284 7G130 5103 70-13I) 385 7G130 1097 70-130 10f06 7G130 492 70'130 295 7G130 693 70-t30 6106 70-130 098 70-1$ 4s4 70-t3. l

25505025252525252550

252525

5{)

25

2525502525

2525252525

25

2550252525

5025E

x

2525

25

Ihis latotutory rqod tt ..ot eal I rr,fuut o,r z,ttholid sigaa&tre on the olw pgc.

. Reportable D€tEction Limit BRL = Bdow RQorting Limit Pag€ 122 of 165

Page 632: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgrnic Compoundr - Quality Control

Analyte(s) F!ag Units rRNLResult

Spikc

Level

Source

Result

RPDLimit

%REC%REC Limus RPD

Behh ?e31779 - SW846 S0l5A Soil ilow levet,

LCS Oue (7031no.aso1)

Pr€par€d E Anal\ried: 29-Mar-07

I .l ,2-Trkfilo(oetnan€Tridrloroeth€ne

TRt oroffuoromethane (Freon 1 1 )1,2,STrid oroprop6ne

1,2,+Trimehylb€nzene

1,3,tTdr€fiylbenz€ne

m,p-Xyl€$€

Tolrshydrofuran

Elhyl €th€r

Ted-6myl methyl ether

Ethyl tert-buM eth€r

Oii€apropyl ether

Te.t-Eulanol / bulyl alcotrol

1,+Dioxane

Su/'ogeto : 4 B m molfu o rc b e n zeneSunoga/€: fotuene4aSu.ro$te: t, 2oichloroethane 4 4S u noga E : Dibtono fl uorcn et h a ne

Brlcb 70317E4 - SW846 5030 Soil (high level.

Blank tt03l78,l€LKl I

P.6pared & AnalF€d: 2g-Mar-07

1 ,I J-Tridbrotrif,rroroethane (Fr€on 113)

Acayionluile

B€nzenegromob€nzefl€

Brcrnoc'lborn€thsne

Bromodicfilorom€ihane

Bromofom

Bromomelhano

2€utanon€ (MEK)

n€uvb€nzen€

6€+Buty't€nz€ne

ted.Bu!y'b6n2€n€

C€6on dislrlfde

C€6on tefachlodde

Chlombenzene

Chloloothan€

Chlomtorm

Chlorcm€han€

2-Chlorololuene

44hbrololuene

1 r-Dibrorne3d oropropane

Dibmmod ordnethane

| 2-Oibmmo€thsrc (EOA)

Obrcmornettune

|,2-Dld o.obenzen€

| ,3-Did orob€ruene

| ,4oidllorob€nzene

20.4

1 9 . 1

16.4

21.5

18.8

18.7

18_0

37.5

1 9 4

1 7 5

1 9 . 7

18.7

20.6

18.9

r65

205

4 8 950.250_451.6

BRL

BRI.

BRL

ARL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

sRr_BRI.

BRI.

BRL

SRL

ARL

pgag wet

Ugr'(g wet

!g/kg w€t

u9xg wet

rc/kg wet

!g/kg wet

Pg/kg wet

pg/kg wel

ugy'kg wel

Pg/kg wel

lgr,kg wel

pS/kS vJet

!g/kg wet

pg/kg wet

!g/kg Yi,et

!g/kg wet

r.rglkg wet

!g/kg wet!g/kg wel

lgftg wel

lgl€ wet I 0

pg/kg w€t 20.0

pg/kg wet 'l.0

!g/kg wet 1.0

pg/kg w€t 1.0

Ugftg wet 1.0

pg/lgwet 1.0

t g/kg wet 1.0

pg/kg wet 2.O

!g/kg wel 10-0

lgikg w€l 1.0

Ugr'ko wet 1.0

lgr,kg wel 1 .0

yqy'kg wel 5 0

Ug/kg wel 1.0

Ug&gwet l0

lrSftS ',Y€l 2.O

pdkSwel 1.0

ldkg Yllet 2.O

!4fS w€t t.0

pdkS v.€l 1.0

f.iS/kS vJ€l 2.O

!g/kg w€l 1.0

fgr'kg w€t 1.0

!g/kg wet 1.0

!q/kg w€t L0

!g/kg w€t 1.0

tSn(S Yr€t '1.0

102 70-130

96 70-130

82 56.8-140

108 70-130

94 70-130

94 7G130

90 70-130

94 70-130

97 70-130

88 70-130

98 65,3,130

94 70-130

103 70-130

94 70-130

a2 70-130

102 34-155

98 70-130100 70-130101 7L130103 70-130

20.020.o20.020.020.o20_020.040.020020.o2 0 020.020.o20.o20020050050.050.050_o

7

8

2

0 9

6

2

1 0

I

4

2

3

2

2

0

5025252525252525502525252525

This toborutary rcpott k nol tulU without an etthoized si?nztan on thc cover paEe.

+ Repoftabl€ Detection Lirnit BRL = Below R€porting Limit Page 123 of 165

Page 633: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Conlrol

Analytds) Result Flag Units +RDLSpikekvel

SouaceRes!ll %REC

%RECLimits RPD

RPDLirnrt

Brach 7031784 - SWa46 5030 Soil {high hvert

Blank (70317&a-gLKl I

Prepared I Ahdyzed: 29-Ma{7

1 ,1 -Di:hlor€thane

1,2-Did or€tt|sne

1 , 1 -DiJ$ro€thsns

cis-1,2-Dichloroethens

trarls-l,z-Dichloro€thene

1 ,2oidbropropane

1 ,3-Di* oropropane

2,2.Dichlorcpropane

1 ,1 .Oicnb{oprop€n€

cis-1,3.Dlcliorot|lEp€n€

hans-'l,3Oichloroproperc

E8rylb€rEene

Hexachbrubutadiene

2+lexanofl€ (n BK)

isopropylberueno

4{sopropyholuene

Msthyl bn+utyl dher

4-[,]€thyl-2-pentanone (MlBl()

Mehyleoe chloride

Naphthabne

Styren€

1 ,1 ,1 ,z-Tet.achlor*hEne1,1,22-Tefadtlorctfi ane

T€irtrhloroethen€

Toluen€'1,2.+Trichbrob€nzene

1,2,4-Trichbrobenzene

1,1,l.T.idrbro€ttEne

1,'1,2-Tridrloro€than€

Tdchbrocthen€

Trichloroff uoomethane (Freon t 1 )1,2,$Tri$broprcpane

1,2,+Tdrnehylbenzen€

1,3,tTrin€lhylbenz€rF

Vin, chloride

m,Fxyl€il€

Tet'ahydrofulEn

E[|. drr€l

T€tl-aftryl melhyl €ther

Ethyl bniut!,1 €bl€.

Dl-lsop.opyl strer

Ted-Butanol / buM alcot|ol

l,4{)ioxans

S u tqate : )tB m noff &rIJben ze neSuftqate: Tdu€ne4aSunoga|P-: 1,2 -Dichbr@thane44

S/J/twaae: OilDtonafknronqthane

LCS f7fill78,t€St)

(Freonl2) BRL

BRL

BRL

BRL

BRL

BRL

BRL

8Rt-

8RL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRI

BRL

BRL

SRL

BRL

ERL

BRL

BRL

aRI

aRl

BRI.

8RL

BRL

BRL

BRL

BRL

SRL

SRL

aRl

ARL

BRL

ARL

BRL

BRL

BRL

BRL

SRL

31.13 1 . 730.630.5

rc/l(g wel 2.OpgI€wel 1.0

lgftgwel 1.0pg/tgw€t |.0pdksw€l t.0

Fg4gw€t 1.0

ldtg vret 1.0

UgI(g wet 1.0

ldkS v{et 1.0

|,glfl€ wst 1.0

l4kg wet 1.0

lg/kgw€t 1.0

Ug4€wel 1.0

ug/l(g r{el t.0

lrgrtsYrel 10.0

ldxSw€t 1.0

lgkg rvet 1.0

rcn(g $/et 1-0

€ikg wet 1O.0pgrkg wet 10.0

lg/kgwBt 1.0

Ug^gwel 1.0

Ig/tgvrol 1.0pg/l(Su,€l 1.0

Pgr'kg rv€t i.0

t/dkSrYet 1.0

ldkg Y/et 1.0

t g/kg wst 1-0

t gl(g wet 1-0

rcfl(g wel 1.0

I€Agwet 1.0

lgrkgwet 1.0

lg/kgwet t.0

USASw€l 1.0

l.dkS w€t 1.0

!C4(g vr€t 1.0

!S/kg wet 1-0

USn(g wet 2_0

FS/IS v',et 1.0

|lgkg wet 10.0

Itgftg'rJel 1.O

lrg/kgwol 1.0

tgAgw€t 1.0

usrks rv€l 1.0pdkgw€r 10.0

iJdkg wet 2O.O

ug/kg wetmr'kg wetUgLn(g wetlgr'tg wet

30.o30.ou.om.o

70-1307G1@70-1N70-130

104106102102

T h laborulory rcpan is not valu frithod zn oa&odtd signatrt on the covet poge-

' Reporrable D€tectioo Limit BRL = B€low R€porting Limit PaBe l2,l of 165

Page 634: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qurlity Control

Spike

lrvel

%RECLimits

Source

Result %RECFlag UonsRPDLimrt

Betcb ?031781- SW8{6 5010 Soil (high level)Prcpared & Analyzed: 29-Mar47

1,1,2-Trichlo.otriRuofoethane (Freon 1 j3)

Acry'onitrils

Benzene

Brombenzene

Brdnochloromethane

Bo.nodid o,om€6anegrdnoforo

Eromomelhane

2€ubnone (MEK)

n-Buglb€rE€n€

secA'rty$€nzen€

tert€utylbenzen€

Carbod drs.rlfide

Carbon tetrachlodde

Chlorob€nzene

Cl{,oroelhans

Cttoroforn

Chloromellrane

2{hlo.otoluefle

1,2{ibrorno-3-chloropropane

Dbaomo(trlorome{hane

1,2-Dibromo€thane (E0B)

Dibromornelhane

1 ,2-Did|lorobenzene

1,$Dictlkrobenzsn€

| ,4-Dk rloroDenzeoe

Did$mdifl uoromethane (Frconl 2)

t,t-Didrloro€thane

I ,2oktior*thane

| ,l .Oichlor€lh€ne

cis-1 2-Dlctrloroeth€ne

trans-l,2Oichloroothen€

t.2-Djchjoropr@EDe

| ,SDichloropropsne

22Oicnbropr@an€

| , | -Dicnb.opropen€

ds.l,SDldiloroplopene

trans-'1,3{ichbroD.opene

Ethylbe.Een€

H€xachjorobutsdiene

2+€xanone (MBK)

lsopaopylb€nzen€

4-lsopropyltolu€ne

Metvl ta.t-hnyl elhet

4+retryl-2f entanone (MI8K)

M€thylon€ c*rbrid€

Nephthsiene

n+ropylbenzene

Styreng

1 ,1 ,1 ,2-Tet'acl*croethane

Result

16.8

13.2

18.6

20.2

20.4

1 9 4

2 1 . 4

20.1

14.6

16.9

1 8 E

19.7

1 6 0

15-6

20.1

1 f . 4

r8.8

1 8 . 5

19_1

19.5

19.2

20.5

21.1

19.8

20.5

20.6

19.3

18.5

18_3

1 8 . 0

r6.5

19.2

17.8

2 D 3

20.5

r4.6

1 8 I

1 S 0

1S-4

19.3

14.8

13.0

18.1

1 S . 1'19.8

1 6 4

16.3

19.5

17.4

21.6

20.5

!94q wet

lgr'kg wet

!g/kg wet

!g{kg rv€t

!g/kg wet

lgftg wet

tigkg wel

trgkg wet

pgkg wel

ugL/kg wel

ugkg wet

Pg/kq wet

pg/kg w€t

lSf(g eret

lgkg wel

Pg/kg wel

!g/*g w€l

t/g/kg wet

!q/kg wel

t,g/(g w€t

l./g/kg !"€t

!g/Kg wel

$g/tg wel

lqy'kg wet

!g/kg wet

tig/kg w€t

trg/kg wel

US|kS wel

Pg/kg w€t

lg^g wel

!g/kg wet

!g/kg wet

!g/xg wel

W*g wet

pg!ftg w€l

lrg/kg wel

tg/kgwet

tgr'kg wel

Fq/kg wel

Ugt(g wel

rcr'kg we(

pg'l.,€wel

ac1 Ugkg wel

trgkg wel

Ugkg wet

ugL/kg wel

tl!!4(g Yv€t

!g/kg wet

!g/kg wet

!g/kg wel

tigftg "el!g/kg wet

84 70-130

66 177-175

s3 70-130

101 70-130

102 70-130

97 70-130

103 7G134

107 70-130

100 55.3-136

73 38.8-142

84 7G130

94 70-130

98 70-130

8A 70-1n

7A 70-130

100 70-130

6/ 55.3-130

94 70-130

92 70-130

s6 7G.130

9A 70-1fr

96 70.130

102 64.7-139

106 7G130

99 70-130

to2 70-130

r03 70-130

70-130

92 U.4-167

92 70-130

90 70130

a2 70-130

96 70-130

69 70-130'to2 70.130

102 70-130

73 70-130

94 70-130

95 70-130

97 70-130

96 70.130

94 60.7-140

65 70-130

90 70,130

96 70-130

99 70.130

92 46.1-145

a2 70-13[

98 70-130

a7 70-130't06 70-130

102 70-130

20.020.020.020_020.020020020.020.o20.o20_020.o20.om o20.020.020.020.020.020020.o20.020.020020.020.o20.o20.o20.020.020020.020.o20.020.D20020.020.0m 020.020.020020.020_o20.020.020.020.020.020020.020_0

Thit hbo@ory rcpor1 is Eol vot t witho|d aE rnlhoriutt sigt alaE oa thc coeet page.

+ R€Foriable D€iection Limir BRL = Below ReDortins Limir Pag€ 125 of 165

Page 635: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatlle Organic Compoutrds - Quslity Control

Anatf,te(s) R€sult Flag Units Resulr %REC Lhnirs

Brach 703 U84 - SW846 5030 Soll (high levrt)

LCS f703t7E4asi )

Prepared E Analfzed: 29-MaF07

I , I ,2,2-TeFarhlorsthsne

Tetrachloroethene

1,2.&Trichlorobenzene

1 J,+Trichlorobeozene

1 .1 ,l.Trichloreflsne

l,1,2.Trichloro€lhane

Trilhloronuoromethan€ (Freon 1 | )'1,2,3-Tricl oaopropan€

1,2,+Trim€thyibenzene

l,3,STrilneflylb€nzene

Vinyl drlodde

m,p-Xylone

Tel€hydrEturan

Ethyl eth6r

Ted.amyl mothyl €lher

Ethyl b.t{dyl ether

Oi-isaprooyl n$er

Te.t-But nol / buM alcohol

1,+Dbxane

S u iog ate : +gronbff uo rDb e n zeneSu/'ogate: Tol@ne48Sunogate: l,2Dlchbtodhane44Su rrcgetg : Di fuomonuo@melh a rc

LCS Duo aTo3l?tt l-BSDll

Prepared & Analfr€d: 2$Mar-O7

1,1,2-Trid oroffiuoroethane (F|eon 113)

Acrylonitril€

Benzerlegrornob€nzene

gro.nochbrch€thane

Bmmodii:hloromethan€

Baomofom

Bromoftelhan€

2€ubno.|e (MEK)

n8urylbenzene

sec-gutdb€nzene

krt€utylb€nz€n€

Cshon disulfoe

C€rbon btraanbdd€

Chbrcf,grEefie

Chlo{oethane

Chlooform

Chlorcrnethane

24hlorouuene

44hbrotoluene

12oDromo-3-ct otoproperF

Oibroflod ordnethan€

20.1

17.2

18.2

19.6

19.3

16.8

21.o

r9.7

16.1

23.2'19.3

't 9.8

t6-9

39.4

20.4

24.4

19.3

18.8

214

17-0

192

30.329.827.331.5

18.8

1 l . o

2 l . t

21.2

21-9

21.9

23.3

24.4

16.5

18.4

20.1

21.6

l8-2

16.8

21.6

19.2

20.6

20.3

20.7

2 1 . 0

21.6

n.3

pgr'kg wet

pg/kg wet

Ug/Xg v.,el

uc/kg',v€l

ldkS vret

|/S/XS wet

ldkS wet

t g4!0 w€l

Idkg wet

lgixg wel

ldkS lv€l

ldls rst

ug/l(s Yret

!94{g $ret

t g/kg wel

!g/rg wel

tid*S lr€l

lgl€ Y{€t

lgr'tg w€t

pdl€ w6t

Pgifi(g 'r,et

pg/l€ wel

pgftg wetpdkg welpgl/kg u,et

!C&g vret

pg/kg w€t

pgftS {,el

lgtg w€l

ldkg w€t

ldkg Yret

pgL/kg $/et

pgL/kg wel

pg/kg wol

!g/kg wet

lidkg r€l

ldkg Y{€l

|lgl,kg vet

ldkg rvet

pg/ko vret

tig/kg w€l

t4ftg s/€t

pg/tg w€l

Idkg vret

Ugr'kg wst

t!r'kg wet

pg/kS vret

Lrglkg w6t

rs/kg w6l

m.020.020.020.o20.oal.020.020.020.020_020-020.om.040.020.020.020.o20.om.0m.0200200m.030.030.030.o

20.020.020.020.020.020.020.020.0?0.020_020.o20.020.020.0m.020.020.o20-0m.o20.020.o20.020.0

100 70-'t308A 70-13091 7G13098 70-13t)s6 7Gr3084 70-130105 7G13098 7G130ao 56.&140t16 7G13096 7o"l3t)99 70-'t3084 70-'t30s8 70-lo102 70-130122 70-13096 65.3-t3093 70-130107 7G13085 7G130106 70-13096 3+155101 70-19)ss 70-1fr91 7F1fi105 7G130

94 7G130 11

85 1.77-175 25108 70-130 151Q6 70-130 5113 7G130 10110 70-130 13| 10 7G130 7t16 7G130 I122 55.!136 2082 3a.&142 1292 70-130 9100 70-130 6t08 7G.130 10

91 7Gt30 13

84 70"130 7

108 70-130 096 553130 10to3 7G130 I102 70-130 10r(M 7G130 If05 7G.t3o 7106 70.130 12f f6 u]-139 13

502525

25

25

Ex2550

E252550

Thk lsb.olary reFod It Aol tolU p haa an aufroriz.d signzttre o, dE qe., poge.

' Repodebl€ D€t€ctioo Lirnit BRL = Below Reporting Limit Ptgc 126 of 165

Page 636: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Spike Source %REC RpDAnalyk(s) Result Flag Units .RDL kvel Resulr %REC Limits RpD Limit

Bstcl 703 1784 - SW846 y)30 Soit (high tev€r,

LCS Duo a70el 78,1€SDt I

Prep8|ed & Anatfzed: 2g-Mar{7

1,z-Dibtumo€than€ (EDA)

Dibaomorn€tlan€

1 ,2oichlorob€nz€ne

1 ,$Oid orobenzen€

1 ,4-Dichlorobenzene

Dichbrodifluorornemane (Frcon1 2)| ,l-Dichbro€th8ne

| ,2-Dicfibro€[|sne

1,1-Dit oro€ltBn€

cis-1,2-0i4fi loro€lh€ne

lrEns-1,z-Dichbroeh€ne'l.2oichlorop.opane

l,3Oichbropropane

2 2-Dicfiloropropanet,1-Dichloroprcpene

cis-|,3{iJ icropropene

trans-1,3-Dichlorl0ropene

Eq/benzen€

Hsxachlorobutadi€ne

2-Hexamn€ (MBK)

4-lsopropyltoluene

Metlryl brt.butyl ether

4+vlethyl-2-pentanone (MtBK)

M€thybne dlbfije

Naphthdene

Slyrene

1.1, 1,2-Tetehloroettlane

1,1,2,2-Tetad croethane

Telrehloroethene

1,2,'Trichlorob€{rz€ne

1,2.4-Trici orobenzens'1,'1.1-Trichloro€thane

1 ,1 J-Tricl oroetEne

Trlchloro€lhene

Tdchlorofl letom€thane (Freon I 1 )l2,STrichloroprop€ne

I J,&TrlmelhylberEene

| ,3,$Trim€hylbenzene

Vinylchbnde

m,P-Xyl€n€

o-XylEn€

Tetrahydrofuran

Ethy| ether

T*t-drM mehyl ether

EfiM brt+utyl €tn€r

oii.sopmpyl athe.

Ted€utanol / hrtyi alcohol

I,4-Oloxdle

245

2 1 8

2 1 . 8

2 1 8

21.O

2 1 . O

20.1

20_5

19.0

2 1 0

19_6

22_O

23.0

1 6 . 3

1 7 . A

2 1 _ 3

22_3

20.8

20-4

1 6 . 5

19.8

2 0 3

21.6

20.8

1 9 . 3

24.2

18.6

23.2

22.3

2 1 4

1 9 3

20.5

2 1 . 9

21.5

17.8

2 3 8

2 2 . 1

1 7 . 8

25.8

21.5

2' t .7

18.5

42.3

22_O

21.4

20.5

19.7

2 1 1

1 9 3

241

261

20.020020.020.020.020.020020_o20_020.020020.o20.020.020_o20020.020.020.020.o20020.020.020_o2002 0 020.02 0 020.020020.o20.020.020.020.020.020.020.020.02 0 020020.040.02D_020.020020.o20.ox.o200200

pgn(g wet

lgL/kg wet

!g/kg wet

Lig/kg wel

pgr'Kg wer

pg/kg w€l

pg/kg wel

Ug/kg wet

Ugr'kg wet

pg/kg wet

Lig/kg wet

!g/Kg wet

pg/kg wel

Ug/kg wel

!g/kg wet

Ug/kg w€l

ligkg wel

ps.fts wetpg/kg wet

pg/kg wet

!g/kg wet

pgL/kg wet

Ugkg wet

Ig/kg wet

!g/kg w€l

!g/Kg wet

pgftg wet

pgftS wer

Pgr'kg wet

lgr'kg wet

Pq/kg wet

pg/kg wet

!g/kg wet

!g/Kg wet

Li9Kg wel

Ugr'kg wet

!g/kg wel

!g/kg wet

t g/kg wel

lig/kg w€r

tiglkg w€t

pgr'kg wet

Udkg wet

Ugfrg wet

!g/t(S wet

!g'kg $/et

lgr'kg wet

Hqftg wet

v4@wel

lgftg wet

aRs !g/kg wet

122 70-'t30109 70.'130109 70-130109 70-130105 7G130105 34.4-167100 70-130'to2 70-13095 70-130105 70,13098 70-130110 7G130115 7G13082 70-t3089 70-130106 70-130'112 70,1301U 70-130102 60 7-14082 70-13099 70-130102 70-'130108 70-130104 46.1-14596 70-130'l2l 70-130g3 70-130116 70-130112 70,130107 70-13096 7G 130102 7G130110 70-13010E 70-13089 70-130119 70n30110 70-13089 56-0-140129 70-130108 70-130108 70-13092 70-130't06 7G130110 70-130r07 70-130102 65.+13098 7G.r 30106 7G13096 7&130120 70-130130 34-155

14 25

10 25

7 2 5

6 2 5

9 2 5

13 50

8 2 5

1 2 2 5

15 25

9 2 5

10 25

4 2 5

12 25

12 25

5 2 5

1 1 2 5

14 25

6 2 5

8 5 0

23 25

10 25

6 2 5

9 2 5

12 50

16 25

21 25

7 2 5

1 2 5

9 2 5

1 2 5

1 1 2 5'11 25

1 2 2 5

12 25

6 2 5

1 2 2 5

1 2 2 5

t1 50

1 1 2 5

12 25

9 2 5

9 2 5

8 2 5

8 2 5

1 3 2 5

6 5 0

5 2 5

0.9 25

12 25

12 25

30 25

This lahoralory repo.t k not valid Nithoat an ouihodzed signatare on thc cewr page

' ReFortable Derecrion Limit BRL = Betow Reporring Limir Page I 17 of 165

Page 637: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgatrlc Compoutrds - Qurlity Cotrtrol

Spike Source %REC RPD

R€suh Flsg Units 'RDL t-€v€l R€sult %REC Limirs RPD LimirA"a$dt

Brrct 7031784 - sw846 5010 So (high level,

LCS Dup 17031 7g,t€Soi I

PreFred & Analyzed: 29+rarJ7

S u fi ogele : .lB romo n uotd en z e neSufiogab: Toluene4SS u dog ale : 1, 2 t bh b roet h ene4 4S uno g ele : Dfuo n ofl w ro melha rc

m.731.0

293

Pg/kg Yrel

lgtS Yr€l

lgn(g w€!

lgtS wet

102103

98

30.030.030.030.o

70-13070-13070-1307G130

Ihk l4bofttuy ryNtt is t'ot tdu nithout oz authotisd signrnt". oA tlE covc, page .

+ R@ortrble Det€ction Limit BRL= Bdow R€porting Limir Pse€ 128 of 165

Page 638: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Extractable Petroleum Hydrocarbons - Quality Control

Analyle(s) Result Flag I RDLUnits

Spike

Level

Source

Resuh "/oREC

%REC

Limits

RPDLimrtRPT)

Brtch 7031505 - Swt4615loc

Bl.nk {7031505€LX

Prepared: 26-nler-07 Analyzed: 28-l\,tar-07

Gasolin€

FuelOi l#2

FuelOi l#4

FuelOi l#6

Motor oil

UnldendRed

Other Oil

Tobl Pelroleum Hydrocarbons

C9436 Afiphatc Hydroc?to.rs

Sunogate: 1 4hlotoodade cane

LCS 1703t505-BS0

Pr€pd€d: 2GMar{7 Anal]rzed: 28-Mar-07

CgC36 Aliphatic Hydrocabons

S u iqa te : 1 - C h I otoo da de c an a

Bdcb 7m1513 - SW846 35508

Blank o0r1513€LK

Prepared: 28-Mar-O7 Analyzed: 27 -Mar07

Gasolile

Fuetoi t* r2

FuelOl l#4

FuelOi l16

ti4ator Oil

Ur*tentifed

OtlErOil

Total Pefoleum Hydrocarbons

CllC36 Aliph€lic Hydrocarbons

S u tugale : I I hl oroocl a de c an e

LCg fto315r3€s

PGpared: 26-lrrar-07 Analyzed 27 -Ma.-O7

C$C36 Aliphatlc Hydroc€dons

S urcga te : l -C hl o@od a d e can e

Batcfr 703 1589 - Sw846 35508

ghnk r?O3l5ltg€LKll

P.€p6red: 27-Mar47 Anal}rzed: 28-Ma.{7

Gaso{lne

FuelOi ld2

FuelOi l i . l

Fu€lOi l t6

Mottr Oil

Uniden{6€d

OtEr Oil

TolBl Petrdeum Hydrocadons

C9436 Aliph6tic Hydrccarbons

Suro{,ala: 1 -Chlotwcladecane

LCS O03tsEgAStI

mgtt(g wel 13.3

mg./kg wet 13.3

mg (g wet 13 3

mgl(g w€t 13 3

mg/kg wet 13 3

mg/kgwet '13.3

mgl(g wet 13.3

ng/kg wet 13-3

mg/kg \N€t 13-3

mg/kg w€t 'l3-3

mgl(g w€t

mg/kg \a€t 13.3

mgl(g $/et

3.33

93.3333

mg/kg !rct 13 3

mg/kg lvet 13.3

mg/kg rrct 13 3

mgfl(g w€t 'l3.3

mg/kg lv€t 13.3

mg/kg $€t ?3.3

mg/kg wet 13.3

mg/kg \r€t 'l3-3

mg/kg w€t 13-3

mg/kgwet '13.3

mg/kgwet 3.33

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

ARL

0_0585

o 0573

BRL

BRL

BRL

BRL

BRL

8RL

BRL

8RL

BRL

BRL

2.56

7 5 8

2.83

BRL

BRL

BRL

BRL

ARL

ARL

BRL

BRL

8RL

BRL

2.24

rngl

ms.4

mg/l

mg/l

mg/l

mgrm9/l

mgn

mg/ l

mg]l

mg/l

0.050.050.050 0 50.050.050.050.050.05o.05

rng/l 0.05msn

0.0500

1 . 4 0

o 0500

40-140

60-12060-120

100115

8 1

85

40-140

60-12060-120

67 46140

Paee l29of 165

This labodo.f rcporl ir Eot ralid.,airto& ci a!rtorizcd tigaalure oa rhe coperpoge

r R€porteble Detedion Limir BRL = Below Reporting Limit

Page 639: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Exiractrble Petroleum Hydrocarbons - Quality Control

Anab,teG) FlasResult Units *R-DLSpik€l€vel

Sourc€

Result %REC%RECLimits

RPDLimitRPD

Brrch 703 1589 - SWE46 35508Pr€pared: 27-Mar-07 An€lyz€'d 2A-Mat47

C9-C36 Alipharic Hydro.erbons

Sunogate: 1 -Chlo,ooctadecane7413.3

ouollclto 1703t s8gtrtlPlI Sour[€: SA59ZI,|-03

6E.9

2_'lt)

BRLBRLARLBRLBRLBRLARLBRLBRIBRL3.(E

75.0

242

78.4

2.59

93.3

1023.63

t02

3.63

60-1ma0-120

mgftg wetn€^9 w€l

nEn(g dryrngrkg dryrngn€ dryriS/ko dryflEikg dryrERg d.yrElkg drynEtkq drymgL/ts drymgftS dryF€n(g dry

mdks dryfiig/t(g dry

mSilq d.ynE*g dry

Prepared: 27-lrar-07 Analfledr 28-Mar{7

Gagoline

Fuel Oil #2

Fu6l Oil ,r4

Fuel Oil iS

ftiolo. Oil

Avi€lion Fuel

Unirentned

Otf|er Oil

Toral Ps{rcleum Hydrocaftons

C9C36 Aliphatc Hydocarbons

Suncgate: I 4hlo,oocta.lecane

Msrdx Splke 17031589-ISll

28.92E.928.92 8 928.928.924.928.S28.924.9

ARL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

50505050505050505050

Sou.c€: SA5O724{3

8RLBRLBRLBRLARLBRLARLBRLBRLBRL2.24

70.7

8RL8RLBRLaR[ARL8RLBRL

13_313.313.313.313.313.313.313.313.313.3

BRI

BRf

BRL

ARL

BRL

SRL

BRL

ARL

4+114

50-1504L144

5G15040-14n

411144

60-12060-120

Prepa.ed: 27-Mar47 Analf2edr 26-Mar{7

CgC36 Aliphatic Hydrocarb€rE

Sufiogale : | 4hfdgocladecaneBRLt4.5 74

67

at ix Spik€ DuoOO3l589. SOll Sou.Eo: SAsgzit{t3

P teparcd: 27 4[ar47 A^alFed: 28-Mar{7

C$C36 Aliphatic Hydrccarbons

Suft''ga.'P-: 1 -Chlqoda&cane

Brlch 703l5m - SW846 35508

Blank a7031590€LKll

PreFrEd: 27-Mar{7 Analyzed: ?s-Mat47

GEsoline

FuelOi l#2

Fu6l O tA

Fuot Oat *6

Molo{ Oil

Unidonlifi€d

Other Oil

Total Petoleum Hydrocartrns

C9436 Aliphat& trydmcadons

S Mogate : I 4 h I o/ood adecan e

LCS f?03t590€slt

Prepaed: 27-lrEr47 Analfzed: 29-Mar47

CgC36 Aliphatic Hydrocarbons

S unogato : l -Chlotooc./€,deca no

30

71

14.5

rng/Kg w€tmglkg r'retmgl(g wetrnSftS welmgftg w€lrBkg welmgr'kg welmgr(g weln€L/kg w€tmgl(g welmg,t€ v{et

mglkg w€tttE/tS wst

mSn(0 d.y.rE^o dryrno,tg dryo$rkg drymg/kg drynSftS dryfiglkg dry

93.3 76

82

r3.3

Dupllcstu ft031sq)JlUPI) S'ou.€€r SA596al-16Pr€pa|€d: 2TJlrar-OTAnalt.z€d: 2g-Marry

Gasollne

Fuel Oil f2

Fuel Oil f4

Fu€l Oil #6

Motor Oil

Unid€ntifi€d

14.9

14.9

14,S

14.S

14.9

14.9'14.9

50505050505050

Thb bbo"otu ! rcpod b not jslu wllhod an aathotizd sigaatarc oa tfu ovr page.

* Reportrbl€ D€te{tion Limit BRL = Below Reptrting Limit P|ge 130 of l6J

Page 640: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Eraractable Petroleum Hydrocarbons - euality Control

Spike Source %REC RpDAnalvte{s) Rcsutr Ftag Uoits *RDL Lelet Resuit o,tREC Limns fi?r, Limir

Brtch ?0l l5q) - SW846 35508

Duolicrtl7031590Ollpil So!.cs:SAS96ai-16Preparcd: 27-lrar{7 Anat}zed: 29-t!tar-O7

Odrer Oil

Total Petroteum Hydrocarbons

ClC36 Aliphauc Hydroca.bons

S unogatd : 1 -Ch toroo ct ad e c a n e

alrir Solk€ 17031 590-MSl )

1 4 9

14.9

1 4 . 9

1.87

1 4 4 1 0 1

3.60

14.4 101 8RL

ARL

BRL

BRL

65 40-140

BRL 6a 50-150

76 44-140

Sou.ce: 5A596,lt-16

rnSI(S drymS/kS drymg/kg drymgftg dry

mdkS drynlg/kg dry

mg^S drymgl(g dry

SRL

ARL

BRL

t . 2 1

68.22 7 3

74.7

2.78

505050

Prepared: 27{\Iar{7 Anatyzed: 2g-Mat.O7

C9436 Aliphdic Hydro€ft onsS Mqete : I 4 h I o too clade c ane

rldx Splko Duo fl031590-MSDIt Source: SAS96,ri_10Prepared: 27-{rar07 An€trzed: 29.[rar-07

C$.C36 Aliphatic Hydroc€rbons

S unogate : 1 -Ch I on octade c a n e7E 50-150 14 30

77 4tr140

This labontory ft?od h floa rali.tt tritttod sn aalhoized siEnature on the cover page+ Repodable Det€ction Limit BRI = Below R€porting Limit Page l l l of 165

Page 641: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivol.til€ Orgstric CoDpourds by GC - Quality Cotrtrol

Spik€Ifvel

Betch 70r1496 - SW84{ 3s l{rc

Bbnk r7mi496€LKt)

Pftpared & Anal}/red: 26-lrer-07

PCB 1016

PCB 121

PCB 1232

PCS 1242

PCB 1248

PCA 1254

PCA t260

PCg 1262

PCA 1268

S u rog ate : 1, 4-O B -Oabtuloroh i p hen yl ( Sr )Sffiogate: Dacacnbrohiphenyl (54

LCS 47031496€31 |

ft€pared & Anal].zed: 26-Mar-07

PCB 1016

PCB 1280

Surrog€t€r 4,+DB{ctafuorobhheny, (Sr)Suno€ale : Oe c ach I oto biphe n yl ( S 4

LCS Dup ftmia96.BSDtl

Prepared & Analfzed: 26-n ar-07

PCB't016

PCB 1m0

S nogato : 1, 4 D & Oc bfl uoto biphe n yl ( Sr)SunDaae : D€cachkfobiphefl yl (St)

afl-BRLBRLBRLBRL8RL8RLBRLERL0.2000.?10

2_672.96o t30o.210

2 .713-l ro.130o.2m

ilatrirsplkoft0:11/*96{sfl source:sAst}d{$fi

Pr€parcd & And!.2ed: 2 {ar-07

llg4

rsxIStlpdl

!dl

!dlpgll

u(yl

udlpdlll€/l

0.2000.2000.2000,2000.2000.2m0_2000_2000,200

0.2000.2m

0.2000.?00

0.2350.235

o.22.o.222

!glpdlpsrludl

rgru9/llsnIrs/|

0.2u)o.2u)

2.502.50o.2uo.2f f i

2-s0250o.2000.200

2.942.940.2350.235

o.2220.222

too 3+t50tos #15{)

107 40.140118 40-140

65 30-150105 3G150

108 ,$-140

124 4{1140

65 30'150110 3G150

106 4{!1{0113 40-t40ffi 30'1fita1 3c150

t12 40-140113 40-140ffi g-150110 30-150

0.95

PCB 1016

PCB 12603. r33.72

m20

ItsA!s4pdlpdl

50pqljr4l

!91Ltg?l

BRL

0.411

BRL0.411

Su.togale:4+D&octatuorcbhhenfi64 O.t41Sutugale: Decachlorobiphenyl (Sr) 0.247

Xatdx Solke Dup 17031496{SD1} Source: SA!O659j l

Pr€pared: 26-f,1f a.-07 Analyzed: 27.Mat47

3_103-54o.133o.244

PCB 1016

PCB 12A0

Surqate : l,+OBochn uorobiphonyt ( SiSffiogaiF : Oecadlorobiqenyt (St)

Bctch 7031d9? - SW846 3510C

Blank 17031497€LKll

Prcpared & AnalFed: 26-Mar-O7

a€HC

h€Hc

dSHC

g€HC (u.dane)

Chlodarle

4,4 €oo (p.C)4,4,OOE (r,D')a{{)Dr (p,p')Di€ldrin

Endo€ufEn I

BRI.BRLBRLBRLARLARL

BRLBRLARLBRL

0.01000.01000.01000.01000.0r00o.05000-01m0.o1000.01000.01000.0100

!snusn|lgnps,l

!dl

!dl

t/(yl

|lsn

ldl

t,€llpsrl

This tzhonrory Eport h,rd eald wirharlt aa o ho.ltd tig',da.c ot rtz coverpq.-

+ Reportabl€ lkection Liruit BRL = B€low R@rting Lidit Page ll2 of 165

Page 642: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by cC - euality Cortrol

0-0120 ug/l0.0102 tidl0.010S IlS/l0 0046 z.z pg/l0 0113 pg/l0.0153 ttgtl0.0127 us40.0144 us/l0 0129 pdl0 0130 Fdlo.o153 psn0.0115 pgn0.0138 ldl0.0148 !S40.0131 pg/l0.0141 !S/l0.0132 pgll0.0128 ljs/l0.0144 ldl0-0150 pgn0.0146 !940.0196 pg/l

0 01180.01040 01090.00500_01110.01360.01250.0139o.01240.01260.01400.0120

|l94

ug/lps4

z-2 t S4!dlpgL,l

ljEl

pgl

!s.4uElwrl

Spike

Levcl

0.01000 01000_01000_01000.01000.01000.01000.05000.01000_01000.0100

o 0200o.0200

0_0100 0.02000.0100 0_02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000_0100 0_02000.0100 0.02000 0100 0 02000-0100 0 02000.0100 0_02000,0100 0.02000.0't00 0,02m0.0100 0 0?000 0100 0.02000.0100 0_02000.0100 0.0200

0.omoo.omo

0.01000.01000.0r000.01000.01000.01000.01000.01000.01000.01000.0r000.0100

0.02000.02000 02000.02000.02000.02000.02000.02000.02000.02000.02000.0200

62 30-tffi76 m-t 50

60 40'140

51 40-140

54 40-140

23 40,140

s6 40-140

76 4A-140

64 40-140

72 40-140

64 (r'r40

65 40-'t40

76 40-140

5A 40-140

69 40,14{)

74 40-140

66 .t0-140

7t 4n-u4

66 4D-14D

6,1 40-140

72 40-144

75 40-140

73 4!-14t)98 44-140

Source RPDLimit

Brtch 703t497 - SW846lsl0C

Blank fto3ta$TAlKt I

PreparBd & AnatF€d: 26-MaF07

EMosultan tl

Endosulfan Sulfat€

Endrin

Endrin Aldehyd€

H€plachlor

MeftExychlo't

Hsptad or Epo(ftte

To*aph6ne

aChlor(hn6

gChlordaoe

Enddn Ketone

Suttoga te : 1, 4. D Aid a f I uo tou p he n y I (S oSu'rogeta : Decachlotobipheny! ( 54

LCS ft031497€stl

Pr€pared & Anatfred: 26-MaF07

e.6HC

b€Hc

d-BHC

gFSHC (tindere)

4,4'ooD {p,C){,4-OOE (p,p.)

{J'{DT (p,p )Dielddn

E.dosultan I

Erdosullan tl

Eftbsulfan Suftate

Endrirl

Er|drin Aldstrydg

Hephchtor

t lolhoxychbr

Heptac$lor Epoxide

s4hlddane

g{hlodane

End|in K€bn€

Sufi E{,ele : 4, +DB-Odsf I u o rob i p he n yr F 4Sufiogele: tbtachlotobtphenyt (SO

LCS Dup r7031497-BSDll

Prcparcd & Analrzed: 26-Mar-07

Ahdn

a€HC

b€Hc

d.EHC

gEHC (LiMan€)

4,4.ODD (p,p,)

4,4,{)DE (p,p')

{,4{)DT (p,p')

Diqtdrin

Endcullan I

Endo6u an ll

Endosuffan Suff€te

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

SRL

BRL

BRL

0.o1250.0152

pgl

!gl

!g/l

!91psll

pg/r

lrlvlpg!

tig/lpdl

psnpdl

!9./l

595254255668627062631060

40-140

40140

40-140

4G140,10-140

40-140

4G140

40-140

40-140

40-140

40-140

40-140

2208011333383

202020202020202020202020

Thk leboturary Epod it not valii! wllhoU an osdto.iaci! signalurc oa the coter prge .

+ Reportable Detectioo Limit BRL = Below Reporting Linit Paee l l l of 165

Page 643: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Cotrlpounds by GC - Quality Cotrtrol

Anal''t{s) Flag Units *RDLSpikeL€vel

RPD

LimitSource o/oWC

Resuft VIFSC Limits

Batch ?031497 - SWE46 3510C

LCS Dup {703149?.4{ ll

PreP8 ed & Anal)..€d: 2&Mar-07

Endrin

End.in Aldehyde

tleptachlor

Heptad{or Epoxito

a4hlordane

g{hlordan€

Eltdrin Kebr|e

SunDgEl€: 4,+O84c|aa{ro.otrlottenl (Sr,Sunqate : DeeeHotobipheny' (50

Brrch ?031515 - SW846 3545A

ahnk fi031315€LKll

Prepared & Analyr€d: 26{vlar-07

PCB 1016

PCB 1221

PCB 1232

PCB 1242

PCS 124a

PCB 1254

PCB t260

PCa 1262

PCg 1268

Sunogd6: 4i4g4danuorcbiph€nj4 (Sr)S ur@gate : Dacechlotobiphenyl (St)

LCS O0B15t5€{ltt

Prepared & Analyzod: 2GMar.07

PCB r0't6

PCB 1260

2,4,5.€FTC+|-Xybn€ (tS)

S u nog tu : 1, 40 &OcW uotobhhe n yl (54SunDgEte: D€cachlorottphany, fS,,

LCS Ouo fioil15l$ASDI)

Prepatod: 26-Mar{7 Analyz4d: 27 -Mal{7

PCB 1016

PC8 | 260g//togata : 4,u)B&fl@rcbiptenyl (S4Su7og,ale: Docachlorotiphenyl (Sl

o.01220.0152o.01270.0r37o.0r2ao.0124o_o1420,014so.o1140.0200

BRL

ARL

BRI.

BRL

BRL

BRL

BRL

BRL

ARL

20.o32.9

401

45!3

0.0m021.435.7

476,t66

21.4

8RLBRLBRI

BRLBRLSRLsRr.BRL

3r.636.3

ugtlpdl

t,snItslps{pdl

[r9/lrdlulylItsA

0 01000.01000.0'1000.01000.01000.01000.01000-01q)

0.02000.02000.02000.02000.moo0.02000.02000.0200o0?000.0200

28.6

35710.028.628.6

35735728.628.6

31.631.6

BRI-BRI.BRLsRtBRLARLBRLBRLsRt-

61 .t{r140

76 ,10-l4t)

u 40_14068 40-14064 40-14062 {/l-1{671 &l&74 10-14072 4*^144tu) 40-14t)

1 2

3

1

1

2020mm20202020

pgkgY{€l 28.6

!S/kS rYel 28.6

ldkg rct 28.8pgko wst 28.6

t€rlg yJ€t 28-6

trgikg w€t 28-6

Ug&g wel 28.6pdtSwel 28.6

!g/Ig w€l 28.6

UdkS n€trcr'kg v/€t

Ig/kg wot 28-6

Ugkg wet 28.6pgr'kg w€l

ldkg Yret!gr*g rct

pglkgwel 28,6pg^gw€l 28.6

lrgJtg w€tpg/kg w€l

pdks dry 31.6p€ikS dry 31-6pg/kgdry 31.6

Ugl€d,y 31-6pdks d.y 31.6

lgkg dry 3'1.6

ridks dry 31.6

Igrkgdry 31.6pdhs dry 3'1.6pelg d.ylsao dry

70 *lfi115 #151)

112 4S140

127 4G140

11.6 5G200

75 &-|fl125 30-1s0

r33 4-110

131 4G140

75 *|fi1 2 5 t u l f l

30173

Dupllcet! azo315lS{uPt} SonrE€: 5450629-10

Prepared: 26'Mar-07 Analy?F,d: 27 -Mat47

PCB 10r6PCB 121PCB t232PCE 1242PCB t24ePCB 1254PC81260PCB 1262PCB 1260

sunogate : 1}o84c1fr t0mbipl'6,nyl (Slsunogate: Decachlorouphenyl (Si

6&4040444040{o

100115

Tt503o-tN

fhis lzbonlor! r.port ls ',et vaud t{'tltotd slt a!rtoded ipauft on the @vd pase-

'RrtorEble Detection Limi. BRL = Bclow ReFrting Limit Page l34of 165

Page 644: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - Quality Control

Analyte(s) Result Flag IRDLuni(sSpike

Level

Source

Result % R E C

%REC

Limit5

R.PD

t-inrit

B.rch ?031515 - swE46 3545A

Hattr Solko fl03151tMS | | Source: 5A59629-1 0

Pr6par€d: 2&Mar{7 Anarfled: 27-i{ar-07PCB 1016PCB 12602,4.5,STC-ir-Xyl6ne (lS)

S wwab : 4, 4 4B4c tafl u otob i p he n yl ( S t)S u nogala : Dec ac h lo,o,li' p h e nyt ( Sr )

aAix SFil6 O|ro i70315ts{USDI) Source: SAig629-10

Prepared: 2&Mar-07 Anatyzed: 27 -Mat-O7

426511

0.0200

2 3 /45.8

37038224.130.6

39439410.031.631 6

402402

32.232.2

BRL

BRL

BRL

BRL

pSftS dry 31.6

lgkg dry 31.6

tgks dry

tiEkS drylgks dry

gdkS dry 32 2

!S/kS dry 32 2

US/kS drypS/rS dry

Ug/kg wel 5.00

ug/kg wet 5.00

!g/tq wel 5.00

!g/kg wel 5.00

pglkgwgt 5.O0

!g/kg wel 25 0yg/kg wel 5.00

lgr'kg wet 5.00

!g/kg w€t 5.0O

!g/kg wel 5.00

!g./kg wel 5.00

Ug/kg wel 5 00

tig/kg w€l 5.00

!g/kg wel 5.00

!g/kg wel 5.00

!g/kg wel 5.00

pg/kg wet 5.00

!g/kg x,€t 5.00

!g/kg w€t 25.0

tg/kg wel 5.00

trg/kg wel 5.00

!g/kg w€t 5.00

tig/kg wetpg/kg wel

rgkgwel 5.O0

9gr'kg wet 5.00

t'|g,/kg wet 5.00

lgL/lq wet 5.00

pglkgwet 5.M

!g/kg wet 5.00

tig/kg wet 5-00pg/kg wet 5,00

pq/kg wet 5.00

!S/kS Yret 5,00

108 40-140

130 40,140

76.5 50-200

75 m-lfr145 30-1fl

92 40-140 16

95 40-140 31

75 30-15095 30-150

PCA 1016

PCa 1260

S wDga le : 4, +De!}ck]f I uotoh i p h e n y r ( S lSunogab: DecacnbnfiplEntl (54

B.hh ?031516 - SW846 l54sA

B|ank r703lSl6€Ll(1)

Prepared: 26-l!1ar.07 Anatl.zedt 28-Mar,07

Aldrin

a€HC

b4ltc

d€Hc

g!8rc Gifldar'€)Chlodane

4,4ODD (p,p )a,{'OOE (p,p')

4.4 {)DT (p,C)

Dietdrin

Endosulfan I

Endosulfan ll

Endosulbn Sufste

Enddn

Enddn Abehyde

Heptadllol

Methoryciloi

HepHrhr Epoxide

a-Chlorclen€

o4hlodaneEndrin Kebn€

Sunog,ale : 4, 4 D g-Man uarc b i ph e ntI ( S 4Sunogate : hcachlorobiphetryt 6l

LCS (70:11516€31l

Pteparedr 26-Mar-0TAnallrzed: 2&MaF07

Add4

e€HC

b-aHcdaHc9FBHC {Urdere)a,a'{)OD (p,C)4,4'-DDE (p,C)

4,4'ooT (p.p')Oelddn

Endostf& |

ARL

BRL

SRL

BRL

ARL

BRL

SRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

6.241 1 . 2

1 0 2

9 3 8

10.9

4.70

9.61

I8 '1

1 0 . 5

1 1 3

10_9't 1-0

to.010.o

'10.0

1 0 010_010.01D,D'10.0

10.010_010.010.0

62 3G150112 N-150

1O2 4O-1,1O

94 40-140

109 40-140

47 4i-140

96 40-140

98 40,140

105 40.'140

113 4n-144

r09 40.140'f10 40-14n

this laboratory rcpoA is ,tol vall.l x'ilhatl or. zkthorizcd signatare on the cover page-

* Reportable Detection Limit BRL: Below Reporting Limit Psge lls of 165

Page 645: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - Qralily Cotrtml

An&lyt(s) R€sult Flag Units *RDLSpiket.evet

o/oR_EC

Limirs

RPDLimit

SourceResult o/oREC RPD

Brtch 70J1515. SW8{6 ls4sA

LCS a703t5t6€S

Prepared: 26-fr,lar{7 A^alfued: 2&Mar{7

E rdosuffan ll

Erdosullan SuNfate

End n

Endrifl Aldehyde

Heptachlor

Heptact or Epoxirs

a4hhrdane

g4hlordane

E drin Keton€

Sunwate: 4,4-Og4danrodnpheoyt (SlSuftogate : Deead@ouplrcnl (Sr)

LCS Duo fl0gl 516€SDl I

Prepard: 2GMar.O? Analy.ed: 28-Msr-07

Alddn

a-AHC

b€Hc

d€Hc

g€HC (Li^dane)

4,4'sDD (p,y')

4,4{)DE (p,C)

4,4-OOT (p,p')

Diddnrr

Endoslllbn I

Endo6ulbn ll

Endosu(an Su$ate

End.in

Endrin Aldehyde

Heptac,lld

Hepta.t or Epoxftte

a4hlordane

g4hlodan€

Endrln KobrF

S u ncgate : 1, +D BQehfl $ nhiphen f, (Sr )Sunogeb: Dacact o.ow@nyl (Sd

11.2

10.0

9.71

10.7

10.6

10.1

10.6

10.5

13.2

11-7

6.209.27

10.3

s-31

1 1 - 0

4.69

11.2

10.7

11.2

10.9

1 1 . O

t 1.o

112

9 4 9

9.03

10.s' t t .0

10.7

10.7

10.5

13.5

1 1 . E

6.149.15

!g/kg wet 5.00

||gn€ wet 5.00pgftgwel 5.00

Igftgwel 5.00pdtSw€t 5.00

!{rg\r€t 5-00

|Jg!ftg n€l 5.0O

lgrkgwet 50O

lgn(gwet 5,0O

Fgnqwet 5OO

Wftg w€rpC^g u/€t

ldks wet 5.0o

rcL/kg wet 5.0O

Fgr'kg wet 5.0O

lrg/kgwet 5.0Opg/kgwel 5.0O

IS/kg lv€l 5.mpdrgYr€l 5.00

lgkgv.€t 500

|l€r'kg wet 5-00

ugr'kg wet 5.mpgr'kgwet 500

l€/ko wst 5.0opgy'kg we( 5.00

Udkg v,/et 5.0Opgilgw€l 500

lgtl(g w€t 5-00

rcr'kg wet t00

lgftgwet 500pg/kg wet s.fi)pg/kgw€t 5.00

ISAS vrelpdkS w€l

'112 40.140100 40n1o97 40-'144107 40-140t0€ 4G' 40101 40-140106 40-110105 40-140132 40-140117 4c-14o62 40-14093 4.0-141)

103 4n-14[93 40-140110 40-14047 40-1&102 ,lG14O

107 ,r0-t4t)

112 40-t40109 40-140110 40-140110 {0-140112 40.11035 40Lt:lO96 4G.140lff 40-110110 40-144107 40-140107 40-140105 40.140r35 40-14/J1t0 {GlrO62 4Ir1,U)94 40-141)

10,010.010,010.010.o10.010.010-o't0.0

to.010.o10.o

r0.0't0.o

t 0.0'10.0

10.010.010_0r0.0t0.oto.010.010.0'10.0

10_010.o10.010.010.010.010.0lo.olo.o

1

I

0.9

0

6

I

4

0.9

0

0

5

1

2

6

0.s02

0.9

30

303030303t)30m3030303030303030303030

Dudkd. o03l5l6aUPll SourEa: SA59€38{1

Preoaredl 26+r€r.07 Analyzed: 2eMsr{7Aldrin BRL udt(g dry 9.03a€FlC BRL pdkg d.y 9.S3b-BHC BRL $r€ d.y 9.83d.efrc BRL yg?€dry 9.83g€Hc(Urdan€) sRl ucfts dry s.t}:'Chlordan€ BRL pdksdry 4S. I4,4-DDD(p,p') BRL pd*Sdry 9.834,4'ODE (p,C) BRL ldkS dry 9.834,a'.DOT (p,p') BRL lgkS dry 9.83Dietdrin BRL ydks dry 9.93Endosulhn I BRL pSAS d.y 9.83Erdsu$an ll BRL lgftS dry g.B3Endosillbn Sulfat€ ARL pC/tS dry 0.83

BRL

ARL

ARL

BRL

SRL

BRT

8Rt

BRL

BRL

BRL

BRL

sRtARL

303030303030303030303030c)

fhb lalo$lory EFort is aottolil Nithau da allhodrpl sagn ture oE th. cowr p4ge-

J Reporlable D€t€ction LiEit BRL =Below R€poding Limit Pa€e tl6 of | 65

Page 646: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgflnic Compounds by cC - euality Control

Prepared: 2Gt aF07 Anatyzed: Z&Mar{7

E drtn

Etutdn Ald€hyde

Hepladltor

Heptachlor Epoxil€

Toxehene

aS ordane

g4hlordane

Eftdtin Keione

S/'l'wete : 1, + D & Oc laff rE rob p he n y t (S 4S/u/r9gete : Oeca.hlorobiphenyt (Sr)

tlatrtx Sbtks l'f 031stGMslt Sourc.: SA5953a4l

Brtch 703r516 - Sw8,t6 t545A

Ouolicalo O0315l6OUPl ) Sourc€: 5A59638-01

ARL

8RL

ARL

BRL

BRL

BRL

BRI

BRL

ARL

10.719.0

PreEErcd: 2AMar{7 Anatyzed: 28-Mar-07

Aldrin

6€HC

b€HC

d€Hc

g€HC (tjrdane)

4,4'{)m (p,p')

4,4-ff)E (p,p')

4,4 -OOT (p,p')

Dieldnn

Endcuffan I

Endo€uffan ll

Erdo6ulhn Sdfate

E.rdrtn

Erdrin Alliehyde

H€ptachlq

ld,6rloxydrbl

l'leplachlor Epoxide

a.chlordane

g4hbdane

Endrin Ket)n€

S unga lo : 4, +DBoctafl uo rob i phe n ta $ iS unWaE : Deca ch k,rob i ph e n yl ( 34

18.2

16.4

19.4

4.62'].2

22.4

21.1

23.4

2 l I

22.4

14.2

205

1S.6

1 8 0

1 9 . 9

2 0 3

22.8

20.5

1 1 . 420.2

X.Hx Soike Duo fo315tfitso fi Source: SA5!'€3E{1REpsred: 26-L,la.{7 Analrzed: 26-Mar-07

pdkS d,y 9.a3

PSftg dry 9.83

UqkS dry 9.83pSI(g dry I83pS/kS dry 9.83

UdkS dry 49-1pg/kg dry 9.83pdlg dry 9.83

Fdks dry S.83pdks dryldks dry

Ug/kS dry S 87

USn(g dry 9.87

!S/kS dry 9.87

ldkS dry 9.87pdks dry LAI

!g/kS dry LA7

!g/kg dry 9-87

!g/kg dry 9.87

ridkg dry 9.87

lgkgdry 9A7pS/kg dry 9.87pS/kS dry 9.87

t/s/ks dry 9.87pdrs dry 9.87pS:4(S dry 9 87

ldkg dry 9.87

!g/(g dry 9,87

!g/kg dry I87

udkS dry S.87

US/kS dry S 87

ldks dryUS/kg dry

55 34-15097 30-150

92 30-15083 30-1509a 30-15044 3G15087 30-150114 30-150'tol 30-150119 30,1501O7 30.150105 30-150'116 30-1506a 30-15092 3G150104 30-1 5099 30-15091 30-150101 30,150103 30-150116 30-150104 30,15058 ni 50to3 30-150

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

303030303030303030

Abdna€tlcb€Hcd€Hcg+HC (Llldan€)4,4'OCto (p,C)4,4'OoE (p,p )4,4{)oT (p,p')DielddnEndosutfan IEndcutFan llEnd6ufian Sulfsle

udks drypdks drypdks drypSftS dry

lgfts dry

!S/kg drypdks dry

!g/kg dry

rdks dryyg/kS drypg/kg drypgkg drypdks dryEidfi

Endrh

22.O

18_1

24.1

9.64

19.7

24.4

24.0

27.1

22.5

23.9

25.2

17.0

r8.8

20.1

r 0 . 1

1 0 . 1

10.1

1 0 . 1

1 0 . 1

1 0 - 1

1 0 . 1

10.1

1 0 1't0_1

10.1

10.1

to.1

10. ' l

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

ARL

ARL

BRL

BRL

8RL

BRL

109

90

1 1 9

4A

98

121

1 1 9

137

1 1 1

1 1 6

125

84

93

100

30-15030-t 5030-15030-15030-15030-15030-15030,15030,15030-15030.1503G1503G1503Gr 50

19.619.6

1 9 7

1 9 7

19.7

19.7

15.7

19.7

19.7

1 9 7

19_7

19.7

1 9 . 7

1 9 . 7

19.7

19.7'19.7

1 9 7'19.7

19.7

1 9 . 7

1 9 . 7

1 9 /19.7

m.220.220.220.220220220220220.220220.220_220220.2

BRL

BRL

BRL

BRL

BRL

BRL

BRL

SRL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

ARL

BRL

ARL

ARL

8RL

1 7

8

l 9

I

1 2

6

1 l

1 4

1 2

7

5

1

3030303030303030303030303030

Ikb laSonlor! ,zpotr ir not valtuI w[!hou! an oathodzed signztarc on the cover pale.

+ Reporlable Delection Limit BRL = Betow Reponing Lirnit Page 137 of 165

Page 647: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mlvolatil€ Org{nic Compounds by GC - Qurllty Cotrtrol

Analytqs) Result Ftug Utrits .RDLSource o/'frFc

Resulr YoREC LimirsSpikeL,er'el RPD

RPDLimit

Brrch 7031516 - SWE46 1545A

iratrix Solk Ouo OO3l5l&{ilSOl) SorrEs: 5A596:1841Prepared: 26,1\rar-07 Anall.zedt 28-Mar-O7

Heplachlor

Methoxy.filor

Heptachlor Epoxide

a-Chlordane

g-Chlordane

EMdn Keton€

S u fiog ate : 1, 1-D & Ocb fl uotob i phenyt ( S t)S u iog de : Oec ac h lotob i phe n yI ( S t)

B.lch 7B 1591 - SW846 3:4sA

Blrnt 17031:r!tl €LKl I

P.epared & Analyzed: 27-Mar-07

PCB 1016

PCB 1221

PCB 1232

PCB 1242

PCB 124a

PCB 1254

PCB 1260

PCB 1282

PCB r 268

S u,rogate : 4, 40 &Oclafl &n b ip hG nyl ( S 4S u nog ah : De cach Mi phe nyl ( Sr)

LCS {70:lt 591ASl }

Prepar€d & Anabrzed: 27-ttar-07

PCB t016

PCB 1260

2,a,s,&rGM-Xyl€n€ (lS)

Su ogate: 4j-DeocbnwrcNpfunyt (S4S u Eqale : Oe@c h kltl],b i phe n yl ( S t)

LCS DuoOo3lsol€sol)

P.€par€d & Anavzedr 27-Mar{7

PCB 10t6

PCB t260

Sunqale: 4, 4.Da4cki:lombidEnyl (SdSunt8,e'€': Decachbtobiplnny4 (Sr)

22.4l7.a23.022.422.621_412.321.1

BRL

8RL

BRL

BRL

SRL

8Rl-

BRL

BRL

BRL

20.030.0

396

427

0.0200

m_o30.0

394

426

18.630.0

20.228220.220.2

20.220.2N.2

28.620.6

35735710.028-6286

35735728.628.6

BRL

ARL

ARL

SRL

BRf

BRL

FdrSdry l0.l

rdl€ dry 10.1

ldkg dry 10.1pglkg dry 10.1

lgtrg d.y 10-1

Ug?€dry 10.1pS/kS dryldks dry

Ig(g lvet 28,6pdksYrel 286

[g/kS wer 28.6

Igr'kg vret n.6

!€n!g wet 2A.6

ruI€ wet 28.6

Igikg wel 2E,6pdrs vY€l 28.6pgfkg w€t 28.6

ldXS Yretugnq ',/et

yg/tg w€l 28.6

Iga,gw€l 26.6pgrs w€l

!9&g w€tFdkS rvet

pgrkgwet 28.6

Ig[(g wet 28-6pgtg welpdkg Y/el

ldkS dry 33.1

tdkg d.y 33.1

lSfiS dry 33-1

UdkS d.y 3:1.1pdxsdry 33.1

Fdl€ dry :}:}.1

uS/kS dry 31.1

lgkS dry iI!,lpdkgd.y 3:'.1pgr€ dryFdrg dry

t ' t3 3G150 13

88 30-150 3114 30-150 12

tl1 30-150 7

112 3G150 4

106 3G.150 2

6t tulillU 30.150

303030505050

Sourc.: SA5!r€:ll-16

BRL

BRL

BRL

BRI

ARL

BRI-

BRL

BRI-

8RL

t4.g21_5

70 31]'150105 3ttlffi

111 40-140120 40n40102 50-20070 30-150105 3t-1fl

1r0 4+144 0.911S 40-140 0.865 n-150105 3111il

15 n-Ifl65 30.1fr

3030

Ouolhat .z03t59lOUP|lP.epded & Analzsd: 27-Mar.07PCB 1016PCg 121PCB 1232PCE 1242PCB r24aPCB 1254PCB 1260PCB 1262PCB 1268

8RtBRLBRLBRLBRLARLBRTBRLBRL

64040

40404440{040

Su,/'agale : 4,+DBocbf,uotdiptgnyt ( 54Sunogdte : Decach lo towhen yl (Sr)

33.1

Sowcs: SAsgG4l.tAX.kir 5o (. O03l5e1{8tl

Pag€ 138 of 165

Thit lebonbt! eporl is Eot talU l*hau sd arlhorizd iig&atte od drc cowr pqe .

* Repo.table DetEction Limit BRI = Below Reporting Limit

Page 648: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgaric Compourds by CC - euality Control

B.ach 70f1s9t - sw846 354sAPrepared & Analyz€d: 27-Mar,07PCB tO16PC8 t2602,4,5,&TGM-Xybne (tS)S 6aga e : 4, 4 -D& Octaf t uo roh ip h e nyt ( S 4g-r7oga t e : De cach I o to bi phe n yt ( Sr)

tlatrlx soit. Duo fi03159t.ftsD souTc€: sA59f4.t-16Prepaed & Aflav:ed: 27+rar-07

PCB t016

PCB 1260

SuTogate: 41O& twanuotpbiphenyt (Sr)Smogate : Oocachtorobi phe nyl (SO

449

490

0.0200

24.540.8

451

490

22.8

404

408

10.0

32.632.6

407

407

32.6

BRL

BRL

ldkg d.y 32.7pS,kS dry 32.7pg/kg drypglkS drypg/kg dry

Pdkg dry 32.6

Pdkg dry 32.6

!S/!9 dry!Sn(S dry

110 40,140

12O 4l-14o

91.9 50-200

75 m-t50125 3O-15O

111 40-140

120 40-140

7D m-1fi115 m-150

0_9

oBRLBRL

5050

Thh lzbontory repo.l h ,toil edid xtdhoLt an authoized sigaature od tke cave, poge_* Reportable hactioE Limit BRI_ = B€tow Reportin8 Limir Pas€ 139 of 165

Page 649: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Qurllty Cotrarol

Analyte(s) Result FlaC UnitsSpike

Lvel

RPDLimit

Sourc€ ./.REC

Result %R.EC Limirs

Botch ?031499 - sw846 35||tC

Blank (70314${LKll

Prepared I Analyzed: 26-Mar{7

Ardllne

1 .lilelhylnaphthabne

Azobenz€ne/Diphenyldiazine

Ber\zrdirle

Benzo (a) ar hrec€ne

Benzo (a) anthrac€ne

Benzo (s) pyrene

Eenzo (a) pyrene

Benzo (b) nuorEnthene

Benzo (b) fuolanth€ne

Benzo (9,h,i) pe.y€ne

Benzo (g,h,i) perylens

Benzo (k) ffuoranthene

B€nzo (k) fluofdnther*

B€dzoic acid

Benzyl alcohol

Bis(2d{oro€thory}nelhan€

Bis(z-chbro€thyl)ether

Ais(2dtloroisoprQyl)ether

Ais(2+thylhexylhhhalale

44romoph€nyl phenyl eth€r

BUV b€nzyl phthalate

Ca.bazole

4-Chloro-3-methylphenol

4-Chloroanilin€

2-Chloronaphthat€ns

24hlorcphenol

44hbrophenl phenyl elher

Chrysene

chrysene

Oib€nzo (a,h) anhracene

Dib€nzo (a,h) anhracene

Dibenzofu€n

1 ,2-Dichlorob€nzen€

I ,3-Dicilorobenzene

1 ,4-Dichlorobenz€ne

3,3'-Dhnbrobenzldtte

2,{-Oichb'roptFnol

Diethyl phlhal€b

Dimdt\yl phthsl€b

2,4.Dim€lhylph$ol

Oi-n-brrtyl phthalate

4,6-Dhnro-z-mef ryhhonol

2Joinibophdrol

BRL

SRL

BRL

BRL

BRL

BRI.

BRL

BRL

SRL

BRL

BRL

aRf

BRL

BRL

BRL

BRL

sRrBRLBRLARLgRL

sRrBRL

BRL

BRL

BRL

BRT

sRr8RL

8RL

BRL

BRL

ARL

8RL

ARL

BRL

aR[BRLBRIgRL

8RLBRLARLBRLARL8RLBRLBRLBRLBRL

|'!g/rP9npdl

uglps/i

l4rlttdlt d lttgll|lglrcnFSnpc/t

tdlugllrc4rdlFSrlt d lLig/l

uglpdlpg/l

udlpdl

!dlttgll

||gr'lpsnt4lil

Fdl

!dl

tgl

lsn$s{usnpdl

FdlItsA|rBn!snpsn!dl!gluglI4llttsxpgl

rdl!dludl

1 .Oo2000.2000.4001.001.(n

0.200r.001 0 0't.00

1.000.2000.2000 2000.2000.2000.2 )1 .m0.200_2000.3001 0 01 .mr.00t_00't 001 0 01.00'|.00

|.001_001.001.001.00t.00|.000.2m0.2000.2001.001.001.001.001_(X)1-001.00|.001.001.00't-00

1.00

Irit labotulory rcpod it aot wlid u, ttoat a, a.trtodrd sqnala.e oa thE covet page.

+ Rrpmtable Detectioq Limi. BRL = B€low Reporring Li$ir P€e I4O of 165

Page 650: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Analyt4s)

Semivolatll€ Orgatric Compounds by GCMS - euality Control

FlrA Unitssource %REC

Rcsult %REC Limits

Berch 7031499 - Sw84635t0C

Blsnk 17031499€LKll

A€pa.ed & Anat!.2ed: 26-Mar{7

2,4-Dinikol,oluene

2.6-Dinikotoluen€

Oi-n-octyt phthatab

Fluo|antfiefle

FluoGnlhone

H€xachlorobenzene

Hexechlorobutadiene

ll€xachlortryclopentadiene

l'iex"?ctloro€then€

lrdeno (l,2,3.cd) pyrene

Ind€no (1,2,3-cd) py.ene

2-{llethylnaphthal€fl e

2-Meltrylph6nol

3,{-Ll€thylphenol

Naphfhsl€ne

2-ilitroaniline

3{.1lroanlllne,l-$lilrod line

Nirobeizefle

2{'liboph€nol

4-llifophenol

N-Nit osodlmetf tybmine

N-Nibcodi-n{ropytamine

N-llibos.di,Dhenlar.nine

P€ntachlorophenol

PherEnthrene

Phemrnhrene

Pyddine

Hexachlcob€nzene

1 ,2.{-Trid orob€nzene

z.4,tTrid oropherbl

P6ntedlloroph€nol

2r,&Tn.fibrophenol

HoxacNo.obutadisn€

Sun1&ate : 2-FluotobiphenytSl./rrogate : z-FlwohiphentlSmt8,ate: z+luo.ophenolSuEWb. Nilobenzene4sSmt:gete: Phenol4,Suftogale: Tefienyl4l4s/.lno€ak]Tefuenyl4l4gr nEgate : 2, 4, &f d bm nop he nof

LCS 17U31499€St )

P.eparcd & Analyzed: 2&MaF07

BRL

8RL

BRL

BRL

BRL

BRL

SRL

ARL

SRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRLgRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8Rl

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

ARL

8RL

BRL

BRL

87.787.79 3 510684410810869_8

81.2

81.2

ttgtl

tgtl

!sr!s/lpg/l

r91lp9/lpgl

lig/rps4p9l

!snpglpsn

Ljgn

!9nug/lps/

lig/l

rgtlugnuglpgl

!sn!s4psn

ugtl!9n|l9/l

pgn

t/gl

tgtl

trs/l

Itg

ttgl

t g l

!gn

ll(rl

v9pEl

trElvgllI'Sllwll.'dluglpsnp94

pcn!9/l

1.001_001-000.2001.000.2001.001.000.6001_00't _000.2000-2001 0 01.001.001 0 01.OO

1_001.001 0 01.0r01 0 01.001.001 .001.001.001 0 00.200'r.00

0.2001.001 .m1.001.001.(JO1_001.000.200

1.000.200

1001001(n1m1AO1001001n

100100

30'13030-1m1 1 1 1 0301JO15-11030-13030-13015-110

40-140

4G140

8888941068810810870

81

8 1

Thb labodoq rcpo.r k noa valid alithoU aa aathotlltd slgt tttre on the cover page.

* Reportable D€tocijon Limit BRL: Below ReDonins Limit P a B e 1 4 l o f L 6 s

Page 651: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semlvolatil€ Orgatric Compoun& by CCMS - Quality Control

Analyte(s) Result Flag

souce %RECResult %P.F,C Limits.R DLUniis

SpikeL€vel

RPDLimitRPD

Batch 7031499 - Sw8{6 3510C

LCS aro a99€S

Prepared & Anslyzed: 26-Mar-07

AcenaphthYen€

I -Melhylnaphthalene

Aniline

Azob€nzene/Diphenyldiazine

Benzidine

Benzo (a) anftrecenegenzo (a) anthracene

Benzo (a) pyr€n€

Benzo (a) pyr€ne

Benzo (b) fl@rdnlhene

B€nzo (b) fuo.anlhene

Benzo (g,h,i) peryiene

B€nzo (g,h,i) p€ryene

8€nzo (k) iuoranhon€

Benzo (k) fluoranthene

Benzoic acid

Benzyl alcohol

Bis(zd oroethoxy)m€fhane

Bis(2d oroeoyl)€ther

Bis(2-cnbrcisopropyl)ether

Bis(z-etry{h€xyl,phlhalate

4Sromophenf ph€nyl ether

BUV benryl phhalale

Carbazole

44hloro-3rnelhylphenol

44hloroaniline

2 4hlorunaphthdlene

24hlorophenol

44hbrophenyl phsnyl ether

Chrysene

Chrysene

Dibenzo (a,h) anth.acene

Dib€nzo (a,h) anutracene

Dib€nzofuran

1,2-DiJ orob€nzene

1 ,3-O*Ibrobenzene

13-Dichlorobenzene

3,3 --Didrbrob€nzidins

2,4-Dlchlompheiol

Di€ftryl phthalab

Dintethyl ptrthabts

2,4-Di.n6hylphef|ol

Di-n-buy phthalaie

4,&Oinito-2-rn€thylphenol

2,4-Dnitoph€nol

2,4Ohitrotolu€n6

2,6oinitroiotuerle

90_090-0ao_211694.294.2't79

10519780.6

90.090.0al2a1.262.462.89e.698.682.479.1$9.095.155.910279.098.41 1 984_377.7E1_76 9 683.786.1a6.l63.069.08{_074.66 4 877.1E5-176.S86.082.O74.768.275.582.48{i.290-5

0.2I]00.4001.001.OOl_0002001.001.00L000.2000.2000.2000.2000.2000.2001.000.2000.3000.200t.001.001.001.001.001.O01.001.001.00|.00r.001.001.001.001-000-2000.2000.2m1.001.(m|.001.001.001_00

1.001.0{)1.001.001.00|.00|.00r.(,rc

100100100100t00t00100'tfi)

1m100100100100100r00r001001m100100100100r00100100100t00100100'100

100100100t00r001001001001001001oo100t00100100100100100

100ro0't00

psntdl!dl$s,lt!{,tsrlldlt4

Ac2 ljgnt'dlp4lpdl

!dlugnudlp€rl

wltdl|lg/l

pqlpsll

udltttylttgl'ldlIdltt9,r'|us/|llgt

Pdl

!dl

!gl

r{l

|tdl

llg,l

trS/l

mnlsrlpc4

!dl

!dl

lt9rl

Irdl

ldl

wt sxpcnpsr!dlfdl|'lsn

90 4G140

90 ,lO-'1{O

80 4S140116 4.&140

€r4 4Gt40

94 ,t0-140

179 S.200t05 40-'140

197 40-140

81 ,r&14O

81 40-1{0

so 4$140

90 40-140

81 40-140

81 4tlt40

63 40-14063 40-140

99 40-140

9S 4G1{O

82 3G13079 4Gr40

89 40-14095 40-140

56 40-140102 40-14079 4O-14{J

98 4G140119 1Gl,lO

84 3G13078 .1G140

82 4{1140

70 30-13084 40-14086 40-14O86 40-'14069 4O-14O

69 {0-140

84 40140

75 4G140

65 4{rr40

n 4!-144

85 4S140

n 30.13,j

06 40-140a2 4$-14075 3&1308a 4G140

76 3G130

82 3()-130

86 4{)-l,l090 40-140

Thit lnhotuory rclorl h Eor dld N,UhoU oE axrtoized $gttttare oi the cowr prye.

'It€portable Detection Limit BRL = Below Repoftitrg Limit Pa€e 142 of 165

Page 652: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - euality Control

Spike Souce %REC RPDAtrElytqs) Resuh Ftag Units +RDL L€vet Resutt %REC Limits RpD Limit

Batch 701149{ - Sw845 3510C

LC8 1703t499€S.t )Prepared E Ansh.zed: 26-irar-07Di-n-octyl phtheleb

Fluorantlene

Fluorantllene

Fluoren€

H€xaafilomberE€n€

H€xadrloftbutadi€ne

Hexacilof ocyclop€ntadi€ne

Hexact orcethane

l.deno (1,2,3-cd) pyrene

lrdeno (1,2,3-cd) pyrene

lsophorone

2-MethylnEphthal€ne

2-M€thylpheml

3J-Medl&tlenol

Naphthalene

2-l lilroanilne

+Nilrosnilin€

4-l{ilroani{n€

Nitobenzene

2-t{iLophe{ol

4+libophenol

NJ.lib6odir|l€ihylamin€

N+titGodi-fi $opylamineN-Ntltcodlphqny'arme

Pentachbrophenoi

Phenol

Pyridn€

H€xedrlorob€nz€n€

1,2,+Triafi lorobenzene

Penla.'|broph€nol

2,4s-Tridllorophenol

2,4,GTrichlo{ophenol

Hexachk robulEdiene

Su/'o8ate: z-FhwobiptEnr4Swogate: z+tuonbiphenylSurog ale : 2+luor'o phe nolSuft g ele : N ittoben ze n e4 5S@ogale: fhe@l4sSurogale: Ta6enrt4l4S urggate : To tp l|€nyl 41 4S l/,,'€ate : 2, 4, 6 - f tibrc nop h 6 n o I

lratrlx Solko alcilaog-trls | )

Prcpar€d & Ar@lyed: 26-trar47

Acenaph0lene

Acamphh€n6

44hloro3.rn€6ylphenol

24hbrophenol

1 3 1

7 8 8

78.8

85.5

85,5

76.6

fa.4

60.4

73.9

64.2

u_293.4

85.5

71_0

86_5

85.6

8 3 7

8 8 9

114

s6.7

74.4

59.2

7 9 0

67_0

97.2

6 8 5

r7_5

77.5

7S.0

aa284.2

78.5

76_6

80.9

68.5

75.O

62.8

7 8 4

83.283.267.110067.88 9 88 9 873.6

Sou.cc: Sl5t€€9-11

73_1

73.1

143

123

pgn

trdl!s/lvglllis/l$g1luEl!ErItgtl

vs/lpsn

!gl

psn

vs]l'vsAusnpglpsA

uqrttgtlpgl

!9r

!snrgl!g/lg9l

FSn

vaJl

!El

trg4

wtl

Itg

|lg/l

ltgl

u9nPEI

!g/l

!9/lp9l

!s/lF9lpsn

!9r!9/lpsr!s/|

!grvgtl

oM7 lgnllsn

131 40-140

79 40-140

79 40-140

86 40-140

a6 40-140

71 40-140

7A 40-140

60 40-140

74 40-140

64 40-140

64 40-140

93 40-140

86 40-140

71 40-140

86 40-130

86 40-140

84 40-1l|()

89 40,140'r14 40.140

97 4O.14O

78 30-130

59 30n 30

79 40-140

67 40-140

97 40-140

6a 30-130

78 40,140

78 40-140

79 30-130

8a 40-140

88 40-140

7E 40-140

77 4O-14O

81 40-140

68 30-130

75 30-130

63 30-130

78 40-140

83 3G1m83 3F1fr67 | S1l0100 30'1m68 1U11090 3G13090 3c1fi74 15-110

7373143123

40-14040-14030-13030- 130

r.001.000.2001 0 00.2001,00

0 6001.001.00

0 2000-2001.001.00'1.00

10.o1-OO

1.00'1.00

1.001-001.001.001 0 01_001.001.001 0 00.2001.00r.00

0.2001.001.001.001.00r.001.000.200

0_2001,001.001.00

100100100'100

100'100

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100'100

1001001M1001ffi100100100100100

100100100't 00

BRL

BRL

BRL

BRL

Thit labo.Qlory repo.t is aot wlu withorlr an authoiral sigttdltne on the cover Nge' R€portable Detection Limit BRL = Below Reportiog Limi( Paee l4l of 165

Page 653: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatil€ Orgsnic Compounds by GCMS - Qurlity Control

Analyte(s) Resulr Flag *RDLSource %REC

Result %REc LimitsUEits

Spik€I.tvel

RPD

LimitRPD

Bitch 7031499 - SW846 3510C

Matdx Spits {7ml{g$irsll

Prepared A Andlz6d, 26-Mar{7

1,+oiJrhobenzen€

2,4-I)initrotoluene

4{,litophenol

N-Nibosodi-n-propylamin€

1 ,2,+Trid orob€nzen€

Pentachloropilanol

Sutrogate : 2-FhMofiphenylSutrog ale : 2 - F I @robi phen ylS u nog ale : 2 -F I uoro phe nolS u@gate : N iltobe n E rre4 5Sudogate: Phenol4sSufiqate: feryfuny'4l4Sutogat€j Teryhenyl-d4Sufiogale : 2,4,6 f ttbtumophenol

Sosrco: 5A5166S11

42.4

74.2

u.485.0114

121

s0.'l

90.1

58.3

1 1 4

74.574.56 t . l83.461.31U)10064.0

Hatrb( golkc Ouo r703la99{SDt} Sowc€: SA59669.ii

Prepared & AnEl).zed: 26-Mar47

74.8

7 4 A'146

129

64.8

77_5

86-7

E8.4

112

133

s3.1

93.1

57.4

112

7+074.0aLo79.761.798.098.063.6

BRI.ARL8RLBRIARLBRLaRt

Ac€naphfl€n€

4.chloro-3{€trrybhenol

24hlorophenol

1 ,+Dichlorobenzeri€

23-Dinibotoluen€

4+lilropienol

N-Nitrcodi-n-9lopyl€mine

Penlachloropheml

Ph€nol

1,2,4-Trichlorob€nz€ne

Pentachlo.oph€nol

S u nog ale : 2 -F I wto bi phe n ytSMogaIe:2+h$towhenylSu|'egate: z+luoropherglS uftogale : N itto be nza fi e4 5Sunogate: Pheipl4sSu''ogate: Teryh6nyl44Su.'ogate: feql6ntl4lS uiog ale : 2, 4, 6 f tibmnwh @ ol

B.tch 7F1514 - SW846 15508

Blank f7031514€lxl )

Prepared: 26-t'/ar-07 Analyzed: 27-Msr{7

,@naphh€ne

A.€naphtry'en€

Ar{lne

Azotenzens/Diphenyldiazin€

B€nzdine

pstpdl

Idl!dlps4

vElpcnpdl

rcnvd!94Fdr!dlWn|ls4pdl!glpsn

rdl!gl

qM7 pgt

!dl

vg/]'rdl!snu94ucn

aM7 pgt

tt(yi

t'ilt'dlpdl

!dlg(yl

rc4t4ltlrsxFdl!dlrdl

62 40n4074 40-14084 3G13086 40-140114 3{1130

127 3&.130

$ {G14090 4G14050 4Gr40114 30-13074 N-13074 30-13061 15-110E:J fuI3O61 t| l to1g) 30-13t)t@ 30-13064 1+110

75 4i-14075 40-14146 30-r 30ln 3Gr3065 40-140z8 40-14087 30-13088 ,l()'l{o

t12 3G130133 30-130s3 4S140

93 40-140

57 {G140r't2 3&r3r)74 3&1974 n-196' tEl10@ 3Gt3062 1&11098 fi-1fu98 n-1@64 lF1lA

1.m1.001.001.001.001.000_2001.001.001.00

1.000.200r_001.00

1.001.001.001.001.001.001 0 00.200Lm1.00

100r00'r00

rfi)100100100100r00100

1001@,N1Cl)IN1M1(ntm

't00

1001(X)1mt001m100'100

100r001001001001001001001M,an1001001001(n

BRL

BRL

BRL

BRL

SRL

BRL

BRL

ARL

BRL

BRL

6RL

BRL

BRL

BRL

BRL

BRL

BRL

BRI-

BRL

BRL

BRI.

ARL

BRL

BRL

mmmm

2020202020202020m

32

5

25

3

tidks u/€t

ldkg vrsl

$/t(g c/€l

l€ftg wet

UgkS wel

Pg/kg,.€tldkS vret

3:103303303303303ilo330

This l&torqtarf epatl ls not vdid tltdhotd s 4ttdrorhd sig,,tzture on &a coe6 N4' R€portabh kectioo LiEJt BRL = B€low R€F.ting Limit Pige l,l,l of I55

Page 654: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organlc Compounds by GCMS - eurlify Conarol

Spike

l-€vel

SourcrResult

%RECLimits RPD

RPDLimit9/OREC

B.tch 70Jl514 - Sw84d 35S0B

Alenk fl tlSl,tALKl)

Pr€p€redr 26-Mar-07 Anatyzet 27 _Ma.-O7

Benzo (a) antfiracene

Benzo (a) pyrene

Eenzo (b) fluo€nthene

Benzo (g,h,i) perylen€

B€nzo (k) fluorani\ene

Benzoic acid

Benzyl alcoholgis(2drloroerhoxy)msthane

Bls(2-chlorc€6hyl)ether

8i$(2-dloroisopropyt)ethergis(2-olhylhery')phthatare

{€romoph€nyl phenyt ethertuVl benzyl phthatate

Cetbade

4{hloro-3fi ethytphenol

4€hlo.o3nilin€

2-Chloronephthatene

24hlorophenol

4-ChlorodEny' phenyt ether

Chrysen€

Dibenzo (a,h) anthracene

Dib€rEofurao

| ,2-Did orobenzene

1,3-Oichbmbenzene

1,+Oichbrob€nz€ne

3,3'-Dichbrob6nzidine

2j-oichkrcphenot

Diethyl phth5late

Oirn€thyl phthatale

2,4-Oimethylphenol

Di-n-butyt phlhetale

4,6-Dinilro-2{eflytphenol

2,+Dinihophenol

2,+Dhihotoluene

2,o€lnibo[oluene

Di-n-oclyt phthalate

Fluorsntl|ene

H€xachlorobenzene

H€xed oobucadiene

Hexad{orccydopentadi€ne

Indeno ( 1,2,3-cd) pyrene

1-lrefrylrlaphthabn€

2-l4othylnaph$atene

2Jr4ethylphenol

3,4-Methylph€flol

Naptthalene

2-Nilrosnilin6

$Nihoani&|o

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

8RL

BRL

ARL

ARL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRI.

BRL

BRL

8RL

8RL

BRL

BRL

BRL

BRI.

BRL

8RL

BRI.

!g/r(g wet 330

ps'kg wet 330

pg/kg wel 330

pgr'kg net 33o

!g/kg wet 330

t gitg wet 330

!!r'kg w€l 330

pgllgwet 330

pqy'kg wet 330

pg/kg wet 330

!g/kg wet 330

pgkgwel 330

lgikg w€i 330

pg/kS vret 330

!gL/(g rN€t 33O

pg/kg wet 330

pdkS wet 330

Ug/kg wel 330

r4/I9 wel 330

!g/kg wet 330

Fqkg w€t 33Opdkg wet 330

fgr'kg wet 330

pg/kg wet 330

Ug/kg wel 330

!g/kg wst 330

!g/kg wet 330

lg/rc wel 3:]0

pg/kg wet 330pgks vJet 330

lgr'kg wst 330

!g/kg wet 330

Lig/r€wel 330

lgL/kg wer 330

pgkgwet 330

!g/kg r,t€t 330

!9ft9 wel 3il0

!q/kg wet 330

pdkg wet 330

pdkg wet 330

pg/kg wet 330

!g/kg wet 33O

Lig !g wet 330

Ugkg vret 330

pg^g wel 330

pg/kg wet 330

!g/lq wel 330

ugr'kg w€r 330pg'l(g wet 33O

lgy'xg wot 330

ldtS rvet 33O

This latamlory repo.t k ,nl talid drhot t oi zslhori@d sipnture on th. cover We. Reportable D€t€ction Limit BRL = Below ReDortins Limir Pag€ 145 of 165

Page 655: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Scmivolatile Organlc Compoutrds b' GCMS - Quality Control

Analyte{s) Result Flag

Sourc€

R€sult %RECUnitsSpikeLevel

%REC

Limitj

RPD

LimitRPDrRDL

Ellch ?mr514 - SW846 3ss0B

Blank t70315l{€LKt}

Prepa.ed: 26-ldar.07 Anglyzad: 2l -nnat47

4-Nitrodiline

Nilrob€uen€

2.Nllrophenol

4-Nitrophenol

N-Nitsosodim€lhy'amine

N-Nitrosodi-n{'ropylamine

t&NitroEodFhenYamine

Phenanlhren€

Pheml

Pyriline

1 2.+Trichla,roben2ene

2,4,s-Trichbmpheml

2,4,ATnchbroph€nol

Surogale: z+heobiphenfS unogafu : 2+ luotoph en o ISu/|icgat3: NillobnzenedsSuftrga/€: Phercl4sSu''ogaig: Teryhenyt4ltSuiogale: 2,4,6-Ttibrcnrcph o|

LCS a?03t51{-AS1l

Pr€p{€d: 26JL{ar-07 Anavzed| 27 4,na'.07

Acenaphtlyl€n€

Azobenzen€/Diphenyldiazine

Benziditle

B€nzo (e) snthracene

Benzo (a) pyren€

B€nzo (b) fooraothene

S€n2o (g,h,i) perybne

Benzo (k) frroranth€ne

Benzolc acid

Benzyl alcahol

Bis(2drloroet\ory)m€dlane

Bb(2dtloro€f tyl)€ther

Ais(2-dlbrcrsopropyFt[t€r

B s(2-€thyltt€xyl)ph$alale

4-gromoph€ny' phenyl 6uler

Butyl b€nzyl phthalate

Caftdzde,l4hlorclm€thylph€nol

4Chbr@niline

24hk ronaphthaler€

2€hlorcph€nol

4€hktroptEnyl ph€nyl etlr€r

Chrys€ne

Dit€rEo (a,h) anfiEc€ne

BRL

ARL

SRL

BRL

BRL

BRL

SRL

ARL

BRL

ARL

8Rt

BRL

BRL

BRL

BRL

ffig59m6660a2m6741)42m

57706380788064m96907260BRL54306090514051806al0

50306190636035406't605160611081105810sSgO5730&205S905E:1057fi

13203in3301320330330330330:It03it0330330gt0

33030

!g'xg r"et

lgr'kg $'el

rcn(g wet

Fg/t(g w€t

t gn(g wst

Fgrtg w€t

pdfg vr€t

lgxS wel

pgy'Ig wet

lglkg wet

pgtkg wet

$I€ wet

lrg/tg w€t

pqrg $el

pdlg wel

Ugr'kg $/et

rc/kg Yret

!g/t€ wet

IrgJkg w€tpg/kg wel

Ugtg w€l

ligkS Y{et

lgr'l(g wet

lgrkg wet

w'kswetqc2 !g/kg wet

udkg rv€l

pdkg v'€l

ldkg Yr€t

ldkS wet

lgLr'kg wet

pglq wet

pgiko wst

Igrkg wel

pgutg w€l

ldkg vrel

!g/kg w€t

!S/kg Y{et

lgr'kg wet

pdkS wet

pgftg wel

IdtS t!'€t

pqkg w€l

pdkg YJel

UdkS wet

ldko vret

!g/ko rYst

lrglq wet

pg/kg wet

90 30-t 30N 11110100 30-13093 1*1101O1 30'1306:J 1U110

€7 40-'t30s6 40-130118 40-13096 40-130't48 40-130109 40-13)

0n 3081 40-13091 40-13077 4r)-13078 40-130102 40-13076 0-13t)

75 4G130

93 40-13005 40-13053 40-130qz 44-1n

f7 4+1n

92 {1130122 4Gr3087 40-130

90 {1130

8€ 40n3063 {-130so 40-130

87 $-13/J86 4G130

3'0$o

3303303303303303303:10330330

330:I}03303303(i0330330330330:l:r0330330330

330330

667066706670667066706670

66706670667066706670667066706670667066706470ffi706670

667066706670667066706670667066706670€67066706670867066706670

Thit bbodoryeport ls not volid ,ithoA an aurtofiaal sFnzfiln on the coea l,age.' R€portsble Detection Limit BRL = Below Reporting Limit Frge 146of 165

Page 656: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolaail€ Orgatric Compounds by GCMS - Quality Control

Ana!,te(s) F-lsgResult UnitrSpike

Level

RPI)

LimitRPDIRDT-Source "/"RICResult %REC Limits

Batcb 7031514 - SW846 3s508

LCS {703t514€S

Prepared: 2SMar{7 Analyzed:27 -l a(41

Dibenzofurdn

l,2Oichloobenzerc

l.3ObJ orobenzerNe'I,4olaf orobenzene

3,S Oichlorobenzlline

2,4Oichlorophenol

Di€tfiyl phlhslab

Dim€thyl phth€lab

2,+Dim6thy'pt'€nol

Di-nautyl phthelate

4,6-Ohi!to-2.methylphenol

2,4-Dinihopherbl

2,4-Dinihotoluene

2,6-Dinihotoluene

Di{-fttyl lhthalatsFftroranthene

Fluoaeno

ilexachlorob€nzene

H€xachlorobutadaene

H€xechlorsydop€ntadiene

hdeno (1,2,3-cd) py€ne

1 +vtsthylnaphthalene

2-tvlethylnaphthalene

2{vlelhylphonol

3,C-n/bthylpfEnol

Nephthal€ne

2-l{ilroanitine

3{,lltroshlllne

4.$litrmhilin6

Nitrotenzene

2{.litophenol

4+tibopfi€nol

N-Nftro6odinehylamin€

N-l,litrosodi-n-propytamine

N+,{itrosodrph€nylamine

P€ntachlorophenol

Pyidin6

I ,z,+Tdd oobenzene

2,4,$Trichloroph€nol

2,4,GTridrlorophenol

S urogate : 2-F hnro b i p ha n ylSmogaae: 2-FluonphenolSunqate: Nitofunzene4sSunogete: Phenol4'Suftogale: Tephonyl4l4S wogab : 2, 1, 6-T ti b @ ft 10 p he nol

593049804270517058505260583055605 1 r 058803900479054405760710054306240509055r048005050503061006460610047905630613055S06250772066105 1 1 0359054903150671046705300530057704050562052404250643048207430191062905280

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6€70

6670

6670

6670

6670

6670

6670

6670

667066706670667066706670

!g/kg wel 330

pg/kg w€l 30

!g/kg r€l 33O

!g/kq wel 330

pg/kg wet 330

!g/kg wst 330

!g/kg r /et 33O

Ug/kg wet 33O

Ug/kg wet 330

!g/kg w€t 330

USftS vJet 330

ug/kgw€t 33O

lgr'kg wet 330

Fgkgwet 33O

lgr'kg 'Net 330

pg/kg \a/et 330

Ug,4€ wet 30

pgr'kg wet 330

tgftSwet 330

pgr'kg ret 330

pg,4(g wet 330

pg!49 wet 33O

pS/qYret 330

ISAS wet 330

pg,4qw€t 330

UgrS wet 33O

lgkg wet 33O

!g/kg wet 330

ldkS wet 330

!g/kg w€t 330

!g/kg wel 1320

rrg/ko wet 330

t/g/kg wel 330

lg/ftg wel 1320

rc/kg w€l 3n]

Ugr'kg wet 30

ug/kg wel 330

pg/kg wel 330

pg/kg wst 330

pg/kg wet 330

|Jq,,kg wel 330

!g/kg wel 330

gglgwet 330

!9r'k9 wet 330

lgr'kg wet 330

ldkg v,/et

Ug/tg wetpgfl(g wetpgks YJeipSIq vJetpdkg Y{et

89 40-130

75 4G130

64 40-130

78 40-130

Ea 10-130

79 4G130

a7 40-130

83 40-130

77 40-130

88 40"130

5a 40-130

72 40-130

82 40-130

86 40-130

106 40-130

El 40-130

94 40-131

76 4{t130

a3 40-1m

72 40-130

76 40-130

75 40-130

9l 40-140

97 40-'t30

91 40-130

72 40-130

u 10-1311

92 40-rm

84 40-130

94 40-130

116 40-130

99 4G130

]t 15130

54 4G't 30

82 411130

47 40.130

101 4G130

70 40-130

73 40.130

79 40-130

e7 40-130

61 40-130

a 40-130

79 40-130

64 40-130

96 30-13072 15-110

111 30-1m74 1511094 30-13079 15-110

Thit lnborutory ftpo.t it iat wlid dlhout 6t oaiho.ized sEnatzre o.t thz co'er Fge.

* R€ponnble Detedion Limit BRL = Below Repo.ting Limit Pase 147 of 165

Page 657: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semlvolatile Orgrric Compounds by GCMS - Quality Contlol

Analyte(s)Spike Souri;e

Flag Units Result %REC Limits

B"lch 70lrsr4 - Sw846 35glBDuollcatafl031514-ItuPll Sourca:sA5oG'71-18Prepa€dl 2&l\rar{7 Analyzed: 27 .{MaFO7

Acenephihyiene

Azobenzone/Dipheny'diazne

Bervidinegenzo (a) antlracene

Benzo (a) pyr€ne

a€nzo (b) nuoranhene

B€nzo (gll,i) p€rylene

Benzo (k) ffuorantfEne

Bsnzoic acid

Benzyl slcohol

ais(2-chbroethory)melhane

Ais(24hbro€$yl)e.tr|er

Bb(2-.*rlorcisopropyllether

Bis(2-ehyihexy')$rlelat€

4€romophenyl pheny' eut€l

BUV benzyl phlhalate

C€bazole

4-Chhro-3{6lhybhend

44hloroanilne

2-Chlo.onaphffElene

2-Cl olophenol

44hloroph€nyl pheny' etqel

Chrys€ns

txbenzo (a,h) anhr@ne

DibenzofiJaan

| ,2-DidrlorobenzerE

1,&Dicl orob€nzene

l,4orchlorobenzene

3,3'-t)id rrob€nzidin€

2,4-Dichlorophenol

Olehyl phhehte

Dinretryl pfiu|alal€

2,+Dim€tnylphenol

Di-n+utyl phtlhalab

4,6-Onilro-2<nethylph€nol

2,4Oi.nitrophenol

2,4.oinifotoluene

2,G-Dinibotoluene

DLn-octyl Atlt€labFluorantherle

Hexachbroberuene

Hexachltrobutadiene

Hexachlorocyclogentadlene

HexachloroehEne

Indeno (1,2,3d) pyr€ne

lsophorfi€

BRL

BRL

BRL

SRL

BRL

BRL

BRL

BRL

SRL

SRL

BRI.

8Rt

BRL

BRL

ARL

SRL

BRL

BRI.

BRL

SRL

BRL

BRL

BRL

BRL

8RL

SRL

BRL

BRL

BRL

BRL

BRI

8RL

BRI

BRI

BRL

BRL

ARL

BRL

BRL

8RL

BRT

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

ARL

l,gikg dry 699

lgtgdry 699pC,19 dry 699

lgtg dry 699

dkS dry 6s9pSn(S dry mgpdks d.y 6S9

tdks dry 69€pCikSdry 699pC,tg dry 699pdkg dry G99gdkS dry 6sg

USI(S dry 6eg

tdksdry 699

ldks dry 699

UCI(S dry 699

t'dlg d.y 699pdkg dry 6sg

UdkS dry

lgrSdry 699

lgkgdry 69s

Udkg d.y 6S3

ldks dry 699

Fdks dry 699

ldkgdry 6S9

ltglkSdrJ 6S9

udksdry 609

UdkS dry 699

t gftg dry 699

rdtsdry 699pdks dry 69spdl(g dry 699

ldxgdry 699

ldtS dry 699

udrsdry 699

lgkS dry 699ptS/kS dry 699pdkS dry 699pdkg dry 699pdksdry Gge

tdkS dry 699gdkS dry 699

|€iks dry 60e

Igrkg d.y 699pSftS d,y 699

ItSlkSdry 699pdkgdry 699

ldksdry 6sg

lSkSdry 699

ldkS dry 6sspS/kg d.y 699

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRT

BRL

BRL

BRL

ARLgRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

SRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

SRL

8RL

BRL

BRL

BRL

505050505050505050505050

50505050505050

5050505050

50505050505050505050505050

50505050

50

5050

Ihlt talro.atuy .qod is Aot rlau wit,,ord on aathodztd signattue o" dte towr pg..

I Repoftble Dct€ction Limit BRJ- = Betow Reporting Limir P.ge 148 of 165

Page 658: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolati le Organic Compounds by cCMS - euality Control

An.lyre(s) *R.DLFlag UDrNResultSpikefr:veJ RPD

RPD

I-imit

Sdurce %REC

Resuli %R€C Limirj

B.hh 703151{ - SW846 35508

. Duollcatd 11031 514-OUP1 | Sourc€: SASE6Tl-18

Propded: 26-t!,f ar07 Analirzed: 27 -Mat-O7

1+rehMr|aphthalene

z-avlethylnaphthal€ne

2{vlethylph€nol

3r-lvl€lhylphenol

Nspl{hal€n6

2J,lltrcaniline

3.tllhtanlhne

4J.li['o€oiline

l,lilot'enzene

2+.lit bphenolr|'|{boph€not

N+lih6odknethylamine

N-Nitrosodi-n-pmpy'amine

t[Nibosodipft enylatn'n€

Phenol

Pyridine

J J,il-Tricf rlorobenzeoe

2,4,STridrloroph€nol

2,4,&Trichloroph€nol

S urioga E : 2 -F luor&i p he n y ISuftogate : 2-Htlotodlenolsu'rosEta- /vlLoD€nzgre{sS|l'|'cf,al€: Phenol4sSlJllogate: Teryhenyt4l4S ut og ate : 2, 4, 6-hbron o p h e n ot

Pr€Fr6d: 26-lvlar{7 Analyzed: 27 -Mat 47

4-Chloro-3{€thf phenol

z{|llorcgh€nol

1 ,+Olcf[orobenzene

2,+Dhltsotolue{|e

4{ibopheml

N+.litro€odi-n{mpylamine

Ph€irol

Py.ene

1 ,2,+Tricl orcbenzene

Sutogate : 2 -Fluorobiphenyl

S/]'togrl€: z-FhJomphenolSuflogak:Nftrc&nzene4'Sunqate: Phercl4,Suno8,ete: Teryhenyl4l4S ffi qal3 : 2, 4,&T nbm n o p h €not

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

6750538063705490726043en

4940907082S043104310573051707300850055403970

uu)445058604ioo6230458o

]|rt ir Aolk. Dip a703l514-MSDi I Source: 5A596?1-18

Pr€par€d: 2Gt ariT Analyzed: 27 -Mat47

507092008430

Acenaphfieoe

C{hloro-3{ehylphenol

24hloroph€nol

pg/kg dry 699

US/ftS dry 6S9

Lig/kg dry 699

ug/kg dry 699

trg/kg dry 699

t/g/kg dry 699

trS/kg dry 699pg/kg dry 2800pdks dry 699pdkg dry 6S9pdkSdry 2800

ldkg dry 699pq/kg dry 699

!g/kg dry 6S9

ldkg dry 699

ldkS dry 699

t/g/kg dry 699

!s/ks dry 699

!g/kg dry 699

t/g/kg dry 699

!S/kS dry 699pg/kg dry 699pdks dryLig/kg dryug/kg dryugl(S dryldks drypg/kg dry

!S/kg dry

!9&S drypqks dry

S4(g dry

ldks dry

lgkS dry

ldks drypS/kS dryps/tg dry

udks dry

US/kS dry

tiS/kS drypg/kg dry!g/kg dryrcftg dryug/kg dryudkg dty

!S/kS dry

!g/kg dry

!s/kg dry

3533533533533531410353353

353353

70707070707070/o70707070

7120142001420071207120142007120142001420071207120712071207120712071m7120

707014rAO't 4100

BRL

SRL

BRL

3tLt u15-11030-1301Ul1030-13t)15-110

40,14030-13030-13040-140{o-14030-13040-'14030-13030-13040-14040-14030-130t r l t o3G1mt5tt03t]'13015-110

40-r403&1303G130

BRL

ARL

ARL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRI

BRL

ARL

BRL

BRL

BRL

ARL

8RI

ARL

BRL

BRL

BRL

ARL

505C505050505050

5050505050505050505050505050

95/69078t0362

Iafix Soite fl03151+$Sl) Source: SA5967'l-18

350350350

ma+5861

407351607A56

6282ffi8864

72

6023

30

n30

Thb laborabry Epott ls not ealid h,ithoat an authorlztd signatu. on thz covr page_

* Reportable Dekction Limit BRL = Bclow Reponing Limil Page 149 of 165

Page 659: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivoladle Organic Compouod$ by GCMS - Quslity Control

Anabte(s) Result Flag Units Result %REC Limits RPD

Brtch 7031514 - SW846 3ss0B

Matrtu Sotks Ouo ft0315t,t itso Sourte SA5967t-t8Prepar€d: 2&l\rar{7 Analyzed: 2l -Mat47

438t)144057305200783085705350,O7o

563011fi61304410666046@

BRL

SRL

BRL

BRL

BRL

BRI.

BRL

BRL

BRL

BRL

BRL

ARL

aR|-

BRL

BRL

BRL

BRL

BRL

BRI

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

8RL

ARL

aRl

ARL

8RL

l,4Oi(,|lorob€nz€n€

2,4Oini0otoluefi€

4-llitrofhenol

N+llho€cdi+proOrylamins

PenLacilorophet|oi

1 ,2,4-Tndbrcb€rEefle

Su fl ogate : 2 + I uon tiphen ylS u nEgate : 2+ luo toph enolSutogate: Nitobenzene4 5Suftogate: Phetd45Surogale: fetphenyld4S u ftog ele : 2, 4, 6-f dh @nophdtol

Brrch 113 1592 - SwE{5 3S45A

Blank 1703150?€LKl I

Pr€par€d: 27+rar47 Analyzed. 2B+td 47

Acenapht|€n€

Azobenzene/Diph€ny'diazin€

B€nzidine

Eenzo (a) antkacene

Benzo (a) pyrsi€

Eenzo (b) fuordnhene

BerEo (g,h,i) p€rylenegenzo G) nudanllEne

Eenzoic acid

Esnzyt alc hol

Bis(2-chloroethoxy)melhane

Bis(2-chlo.oehyl)€ttler

Ais(2-chlorolsopropyl)€lh€r

Bls(23trhylfi exyi)phthalate

4{romoph€nyl phenyl et1e.

BUM benzyl phthslale

Carbazole

4€hloro-3fl €Ihylph€nol

44hlor€nilin€

24hloronaphthakn€

2{hlotrophenol

44hb.ophenyl phenyi ef|€.

Ch.yEen€

Dit€nzo (a,h) anthracene

Dibenzofuran

1 2-Dichbmberuene

1 ,3-Did orobenzene

| ,4-Di{:hlorobenzene

3,3'.Didrlo'rob€nzidin€

2,,|-t)i.* oroph€rc|

tlg/ks dry 350pdl(g dry 350

ldkgdry 1400

lgkS dry 350

t dl€ dry 35Opdks dry 350pSfts dry 350pgtS dry 350

sdkS dryldkg dtYrdkg dryrdks drypdkS dryrdkg dry

62 4+14063 4G'4041 30-13075 44-14l)56 3&13061 3&13084 40-1,1058 4trr408A &-13o63 1r1to87 30-13062 15-11094 g-13066 16110

70707070141007070t4100t410070707070747070707070707070707070

BRL

BRL

SRL

BRL

SRL

ARL

BRI

BRL

2323

7

3030303030303030

lgr'kg wet 165

Ig4€wet 165

Fglkgwst 165

pdts vrel 165

Fgr'kgwel 165

t g/Xg w€l 165

trglq wet 165

$4(g wet 165

pgllg wet 165

pgikgwet 165

UgkSwel 165

lcrtswel 165

Ugr'kg wer 165

Ugfkg er€t 165

pg/kg wet 165

l4/kg wel 165

pgrn€ w€t 165

pdkgwet 165

Udkg Yr€t 165

pgL/kg v/et 165

Ugr'kg wet 165

Ug/!g wet 165

Ugil€vr€t 165

!g/kg wel '165

lg/kgwol 185

ldkSw€l 165

IdkS v,/€t 165

t|.Jr'kg 'r,et 165

Fgnqw€t 165

ggitgw€t 165

pdkgwet 165

tgr'kgw€t 165

UdkS$€l 165

!S/kS w€t 165

This laboratory rqod ls noa tsud wilhou an atdtodsy' sigrraare on the caw pqe .

' R€portoble Detectiod Limit BRL = B€low R€portine Linjr Page | 50 of 165

Page 660: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - euality Controt

Source

Brtch 1131592 - SW846 3545A

A|a.rk t703t59a.BLKt t

Prepar€d: 27+vla.47 Anal].zedt 2&MaF07

Diethy' phtharate

Dknelhyl phtheLate

2,4-Dirnethylphenol

Di-fiSrtyl phthalate

4,&Dinilro-2-methylphenol

2,4-Dinitrophenol

2,+Dinihoblu€n€

2,6-Dinibololu€ns

Oi-n-oclyl phtlnitat€

Fluo€nthene

Flrorene

Hexachlorobenzene

H€Edrlorobutldiene

H€r€cHoreyclop€ntadiene

Hexacfiloa€than6

Indeno (1,2,3cd) pyrene

lsophorone

1-lrelhylnapht\alene

2-lvl€thylnaphthal€n€

2+,lehylphenol

3,4-Melhylph€nol

NEphthel€ne

2{,litroenilins

3-llilroeniline

4{[loanlllne

NiSobenzene

2+{ilrophenol,l{'liboph€nol

N-llllrosodimethyhmine

N-Nhrosodi-n-propytamine

lJ-Niro€odiphenylanine

P€ntedlloroph€nol

Phenantfu€ne

Plrenol

Pyren€

Bdtine'l,2,+Trthbrobenzene

2,4,tTri{nbrophenol

a4,&Tnd oroDh€nol

S u fi ogele : 2+lvomb i phe n ytSunogele: z+lwtuphenolSunogab : Nibo66nzeden5Swtog6l6t Phanol-dsSurrogale: f erphsnyt-dl4S./''ogate : 2, 4,eTd fuo n o p h e n ol

LCS fl0ilt5g2gs

Prepared: 27-l,lar47 Analyzed. 2A -MarO7

Aconaphhen€

Acenapht\yien€

Andlne

Anlhracene

BRL

BRL

BRL

BRL

BRL

SRL

BRL

ARL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

6RL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

280026703250273031302180

2400

2 6 1 0

3550

2570

3330nmgm333033303330

3330333033303330

u849882

65

7278'101

77

!g/kg wet 165

!g/kg \Net i65

pg/kg re€t 165

pgltgwet 165

lgr'kg wet 165

!g/rg wet 165

pgr'Kg t'/et 165

Ug/Kg ',vet 1 65

Ugkg wet 165

Ug/kg wet 165

ygr'kg wet 165

Ugi/kg wet 165

Ugirg wet 165

Ug/Kg wet 165

lgftg wet 16s

Ug/kg wet 165

!g/kg wet 165

pgi kg wet 165

trg/kg wet 165

pgkgwet 165

UgAg wet 165

lrg/Kg wet 165

UEkg wet 165

UqL/kg wet 165

UgL/kg wet 660

ug/kg w€t 165

Ugr'Kg wet 165

Ug/kq wet 660

pg/kg wet 165

!g/kg wet 165

lgr'Kg wet 165

!g/kg rlet 660

!g/kg wet 165

!g/kg lYet 165

pgr'kg w€t 165

!91!gw€t 165

lgL/kg wel 165

tgftg wel 165

pq!4q wet 165

uEkg wetUgftg wel

Ug/kg wei

!g^g w€l!g/kg w€lUg/r€ wel

Ugr'kg wet 165

!g/kg wet 165

lgL/kg wet 165

Yg/Kg wet 165

30,1m| 5-110SGIN15-1101I1m15-110

4G130

4o-130

4o-130

40n 30

Thit hborutory rcporl b tua velid wirhout an strtorized signatue on the cover page.

* Reportabl€ lxtection Limit BRL = Below Repodng Limit Page lJ l of 165

Page 661: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Quality Cortlol

Source

B{tch 7031592 - SW846 3545A

LCS f7(Bt592€:t1)

Prepared: 27jvlar47 Anal]/"zedt 28]tlar47

Afalne

Azobenzene/Dqrhonytdiazine

B€nzidine

Benzo (a) anthracene

B€nzo (a) pyrene

B€nzo (b) fluor€nthene

Benzo (g,h,i) p€rylene

Aenzo (k) nuorar||hefle

Benzoic acid

B€nzyi alcohol

B6(z-chb{oed\oxy}nethane

Bis(2-€nbro€trnyi)ether

Bis(2d oKisopmpyl)ether

Ais(2-€thylh€xyl)phtralat€

4€ornopheny' [ft enyl ether

B0ty' benzyl phthalate

C€rbazoie

,{-Chloro-3{rEhylphenol

44hloroanilne

2-Chloronapfitl|alen€

2-Chloroph€nol

44hloroph€nyJ phenyl eher

Chry6ene

Dlbenzo (a.h) antn.ac€ne

Diben:ofuran

1 ,2Oicnlorol,€nz€ne

| ,3-Dichlofobenzen€1,4-Dlchlorob€nzene

3,3'-Dichk robenzidine

2,4-Di:hbroph€nol

Dlehyl phthabte

Oimethyl phthalate

2,4-Dlmethylphenol

Di-+butyl phlhalate

4,6oiniko-2-met\t$'heml

2.4-DiniboDhenol

2,+Dinilrotolu€ne

2,&Dinitsotoluen€

Dl-n-oclyl phthalale

Hexad orobenzene

He)(act{o.obubdion€

Hexacfi lorccydopenHi€.E

Hexachldoslhane

Indeno (1,2,3d) pyrene

1 +,tetMnepttfulene

2+ ethytEph{halene

2-tlrelhylpnenol

3,4-Molhylphenol

515029401430243026tX)2'/0

235026802!60254028002f5027AO22$'027lO3420250025802$0213{J239024602690249022702020zno28602244244025002120252024m2920282028102360214024602m02200217021202790269023tO244022302620

3{t303330333033303330333033303330333033303330333033303:X)033303l}l]033:1033303330333033i1033:'0ix)303:,303:raro3330333033303330333033:]033:103330333033iX)333033:)0333033303330333033303330

3:}:X)3330333033303:[t0:t330:Ii30

Oc2 lgn(g w€t 165

Irdkgd 165

yg^gwet 165

Ug/tg vr€t 165

!dkg',v€l 165

Ugtkgwei 165

lgr'kg u,et 165

Ig/kgwet 165

tdkgw€l 165

!gr/k9w6t 165

Ug/kg e/et 165

pg/kg $el 165

pgr'kg wel 165

pgr'kgr,€l 165

Igr'kg wet 165

lgkS !^ret 165

Fg/kgra€t 165

pdls$rel t65

Ugrlg rst 165

rdl1g t d 165

Fg/kg wet 165

Igftg wel 165pdkgw€l t65

lgrkg i,€t 165

US/kSwet 165

tgl(gwet 165pgtg wel 165

!gr'kg$,16r t65

lgkS r€t 165

$gkgwet 165

Wkg w€l 165

lgn(g wet 165

pgftow€t t65

ugkS Yr€t 165

rctkg wel 165

Ig/|(gwet 165

pgkgw€l 165

lgfl(]g rret 165

!gr!S,,{et 165

pg/kg wet 165

ygr'ko wel 165pgkgw€t 165

ldkg n€t t65

Udkgwot 165pgikgw€t 165

lgL/tg w€l 165

ldkgw€l 165

Ug/kg wet 165

UdkSwet 165

pSrlSr,r€t 165

pgr'kg wel 165

155 40-1308a 40-t30

4i, G13073 40-13078 4G.13077 40-130

n 40-1g]71 44-1n80 0-13074 4G130

76 .t{t130

84 40-13083 40.13083 40-13068 4{tr 308r 4G13t)103 40-13075 ,O-t3o

77 4613072 40-13064 40-13072 &-13074 40-13081 ,m-130

75 40-1m68 40n 3061 ,lO-l3O

69 4G13086 40n30

67 40-13073 40-13075 4G130

64 40-13076 40-13072 4A-13o88 {G13085 4G13)04 ,10-130

89 4G13073 40-13074 ,rS130

66 4$.r3o66 4+.13065 40n3064 r()-13O

84 4t)-1300r ,(rr306S 4&14073 4&13067 rl&130

79 .t{t't 30

Thb labo.olaq rcptl ls notvslitt *|t!toc! oE aatlodzd tlgn./,.E oE fie.,w. pagc.

a Reportable D€tecdon Limit BRL = B€low R€portiag Linir Page 152 of 165

Page 662: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - euality Control

Brrch 7031592 - SW8{6 3s4sA

LCS t70fi592€31l

Ptepared: 27-[rar{7 An3lyzed: 2A-Mat4f

Nsphbalene

2+liboanilinegNihosniline

4-Nilrcaniline

Nitrobenzene

2+liuoph€nol

4+{irrspfienol

N-Nibosodimethylathane

N-Nitosodi-n+r@ytaman€

N-ffi trosodiphenylahine

Pllenol

Py.idine

I 2,+Trichlorobenzefle

2,4,tTrichloroph€nol

l,4.eTdctiorophenot

S u nogdle : 2 -F I uotobi ph e n y ISunwate : 2 -F I uotoph e nolS urqate : N itto tten z e ne 4 5Sunpgate: Phenol4,S/u/rngel6: Tepheni4l4Sunrgah. : 2, 4 a-f n bmnn p henol

Ouottc.te {7031592{up1 | Sourc€: SASE6ll-16

24102620301037402410230018002410240027AO22502330213022701800232021301S30258021308D2250263023m

BRL

BRL

BRL

BRL

BRL

BRL

SRL

BRL

BRL

ARL

BRL

ARL

ARL

BRL

BRL

BRL

BRL

ARL

SRL

BRL

BRL

BRL

ARL

BRL

8RL

3330333033303330333033303330333033303330333033303330333033303330333033303330333033303330$n3330

!g/kg wet 165

!g/kq wet 165

Ug/kg Y/et 165

!g/kg wet 660

lgr'kg wet 165

lgr'Kg wet 165

!g/kg wet 660

!g/kg wet 165

!g/kg wet 165

t g/kg wet 165

pg/kg wel 660

lgkg w€t 165

lrg/Kg wet 165

!g/kg wet 165

!g/kg wet 165

pg/kg wet 165

Ug/kg w€t 165pg/kg wet 165

FEr(g welUg/kg wet

uEXg welpg/kg w€tt g/kg wetPgr'kg wel

pgkS dry 370

UgftS dry 370pg,'ks dry 370

pdkS dry 370

pgxS dry 370

[gKg dry 370

pdkS dry 370

!S/rS dry 370

UdkS dry 370

pS/kS dry 37O

pg/kg dry 37O

!s/ks dry 370!Si*S dry 370

Pg/kg dry 370

!S/kS dry 370

rdks dry 370yS/xS dry 370

udks dry 370

!g/kg dry 370

t g/kg dry 370pS/kS dry 370pdkg d.y 370

t4/k9 dry 370

Pdks dry 370

trg/lq dry 370

72 40-130

79 40-130

90 40-130

112 40-130

84 40-130

69 40-130

54 40-130

12 40-130

72 40.1fi

83 40-130

6a 40-130

70 40,130

64 40,130

68 40.130

54 40-130

70 40-130

64 40-130

58 40-'t 30

// 30-t3066 15-11092 U-t 3068 15-11079 34-19lo 15110

fuepared: 27-Mat47 Analyzed: 28&laG07

Azob€nz€n€/Diphehyldiazine

Benzidine

BerEo (a) anthrac€ne

Eenzo (a) pfene

Senzo (b) fluoranthene

B€nzo (g,h,i) peryene

B€nzo (k) fluoranfEne

B€ruoic acid

BerEyl alcohol

Bta(zdrlooethory)rnelhane

Bis(2d$roehyl)eUEr

Eis(z-€f doroisopropyl )elherBis(2-€fi Mh€xyl)phthalate4Sromoph€ny' ph€nyl ether

Butyl benzyl phth€late

C€lb@ol€

44hbro-3{etlrylphenol

44hbroaniline

2Chlorcnehthal€ne

24hbrcptEnol

ARL

BRL

ARL

ARL

ARL

ARL

BRL

8RL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

5050505050505050505050505050505050505050505050

50

Th/J laboratort 4pora is Aot dU xlthout an rulhortze.t signarae ott the .over page_

+ Rqlortable Det€ction Limit BRL = Bctow R€porting Limit Page 153 of165

Page 663: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Orgrtric Compoutrdi bv GCMS - Quality Controt

Analyte(s) Result FluC Units Result %REC Limirs

Batch 7031592 - SwE453545A

DuollcaterTfi'lsgz{)UPll Sourca:SA59C4t.t€Prepar€d: 27-Mar{7 Anal}rzed: 28-Mat47

{-Chbropheny' phenyl ef'rer

Chrysene

Dibenzo (a.h) anhrac€ne

Dib€flzofuran

| ,2-Dichlorotr€nzenet ,3-Dicilorob€nzeno

l,4oichlorsb€nzer€

3,3'-k orut €nzidine

2,4Oichlorophenol

Di€lhyl phlhalate

Dimethyl pfilholale

2,+Difi€thylph€rlol

Di-n-butyl phth€bte

4,6-Dininci-2-fi ethylphenol

2,4-Dinihopherbl

2,+Oinitrololuene

2,6-Danitrotoluene

Di-fl-octyl phthalab

Hexachlorobenzeoe

Hexachlorobutadiene

Hexachlorocydop€ntadiere

lndeno (1 ,2,3-cd) py.ene

1 -t{€f'ryidaphthal€ne

2-1!|€thylnephthalene

2+rethybhenol

3,4{,1e$rylDharbl

Naphthel€ne

2-l'lltroanilin€

!Niboanifin€

4{'lihoanilin€

Nitobenzene

2-f'lltrop|lenc,,k{ihophenol

N-t!ikosodimethylamine

N-Nilrosodi-n-propytamine

N-Nitrosodipltenylamine

Ph€nEnihren€

Pfienol

Pyridine

1 .2,+Trl.hlorobedene

2,4,STddibropherrcl

2,4,ATddbr@h€nol

Sufiogate: 2+luoabiphenylSwrcgate: 2+hrorcphenolS u nogate : N inob€ n za ne-<t 5

BRL

BRL

BRL

8RL

8RL

BRL

BRL

8Rt-

BRI.

BRL

BRL

BRLgRL

BRI

BRL

SRL

ARLgRL

BRL

BRL

8RL

sRt_BRI.

BRL

8RL

ARL

BRL

aR[ARL

BRL

BRL

BRL

SRL

BRL

BRL

BRL

BRL

sRt_SRL8RLBRLBRIgRL

BRI.BRL8RLARL8Rt2'a023103060

t€/kg dry 370pS/rSdry 370pdkgdry 370

ugkS dry 37O

Ugr'kS dry 370

lrg/tS dry 370pdks dry 37O

irdlgdry 370

ldkS dry 370

frdl€d.y 37o

Ugikg d.y 370pdksdry 37o

ldkS dry 370

ugkgdrr 37o

rcftS dry 370pgikg d.y 370pgur(gdry 370

trglS dry 370

frgts dry 37O

IrgA9 d.y 370

lSftS dry 370

ldlq dry 370

lqkS dry 370

rgko dry 370

$S/kS d.y 370

t44(g dry 37O

ldkg dry 370

UdkS dry 370

lgftSdry 37O

tgkg dry 37OpSftSdry 370

ldksdry 37o

flgl(g dry 370

UdkSdry 1480

t dkS dry 370

FSftS dry 370

Fdkgdry l4a0

udkSdry 37o

US/kSdry 370pgngdry 370

tg}gdry 1480

lgkgdry 370

USlftS dry 370

tdksdry 370

WlWdry 370

ldkgdry 370

ldksdry 370

udkSdry 370pdkS drytnlks dtyFSikg dry

sRtERIBRLBRLARLBRLSRLBRLBRLSRLBRLARL8RLBRLSRLSRLBRLBRLBRLaR-BRLBRLSRLSRLBRLgRL

BRLBRLBRLBRL8RrBRLARL

BRLBRLBRL8RLBRLSRL

BRLBRIERLBRLBRI.BRLBRI.BRLgRL

505050

5050505050505u50

505050505050505t)5050505t)

505050505050505050505050505t)5050505050

5050

3741)37103?10

3G1fi15-11030-130

58

82

Ihb letorob,y r.porr is not ealid w hoa an onlhoizc.I sigrr&tare on ahe cowr page.

* Reportdbl€ Det ction Limit BRL = B€low Reponing Lirnit P.ge 154 of 165

Page 664: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Quality Control

Spike SoLrrce

Brrch 703 1592 - SW845 ls45A

Duolicat rT03lsg2{)UPil SourEer5A59641-16

iiatrlr Soike fl0115!t2-t St) Source: 5A5964l-16

nep6[ed: 271\tat47 Ar',at\rzed: 28]\,tar{7

Sunogate: PhermI4SS@WaE: faryhenyt4t4SUl'lgate : 2, 4,&Ttibrcn o p h e not

220n29101680

2610263022tO25402650184015002090259026602460282021903340238029602420

iratsh soikc Ouo fl03t592-t{sD Source: sA59641-.t6Prepared: 27{rar47 Analrred: 28-Mar-07

27502?702400266027701920163022AO27aO28102600m0024103550250031102550

Ptepa(d: 27j{,et47 Analyzed: 28-Mar -O7

Acenaphlh€ne

44hbro-3{ethytphenol

24hlorophsnol

| ,4-Di.t orob€nz€ne

2+Lriaitrololusn€

4.Nitophenol

N+{ilro6odi-n.propyl6min€

Pentadllo'rophenol

Ph€nol

13.+TriJrlorob€nz€ne

S u ftog ale : 2 + I w rfi i phe n JtS u trog de : 2+ luotoph e n o ISufio€ale : Nltobenzene4 5SuEogate: Phenol4'Sutogale: Te@enyl44S u nog ele : 2, 4, ET i bmmo ph en ol

44 oro- 3.'nethyl pte nol

z{filorophenol

1 ,+Dlchlorobenzene

2,+Oinhrotolueno

4-l'tibophenol

N{,litrssodi-ntmpyiarn jne

Penlachlorophenol

Pheml

1,2,4-Trichhrclbenzene

S,/'rogae : 2+l uo tob ip he ny'S,//rogate: 2+luorophenolSunogete : Nittoh nz€ n e4 5Sufiogel€: Ph€nol4'Surl.c8ele: Teryhe/'444Su,tugate : Z 4,&Tnhnnophqnl

IS/ig dry!g/kg dryFS/kg dry

ldkS dry 184

UdkS dry 184

US/}S dry 154pg/Kg dry 1M

vgKgdry lu

uS/KS dry 735pg/kS dry 1M

t'dks dry 735

!S/kS dry 1U

PqlNS dry lUpdxgdry 1u

rc/kS drypg/kg dry!S/kS drypdks drytlglxS drypdks dry

pgikS dry 185

Pg4q dry 185pg/kg dry 185

Ug/kg dry 1e5pgfl(g dry 185yg/Kg dry 741

Itglkgdry 185

ug/(g dry 741

ldkS dry 185ydKg dry 185

!g/kS dry 185

!9K9 dry!9kg dryr9ll,g dryldkg dry!s/kg dry!S,4(S dry

59 1111078 30-1n45 15,110

70 44-140

71 30,130

61 30-130

66 40-140

71 40-144

50 30-130

40 40-140

56 30-130

70 30-130

72 40-140

66 40-140

/6 30-tu59 15-11090 30-t 3064 15-11080 30t3065 15-110

74 40-140

74 30-130

64 30.130

7'1 40-140

74 40,140

sl 30-130

44 40-140

6'1 30-130

74 30-130

75 40-140

70 40-140

80 3t)-13064 1$11095 3013467 15-11083 30-t 3068 15-110

374037403741)

37103710371037103710371037103710371037103710371037103710371037103710

374037403740374037403740374037403740374037403740374037403/4437403744

BRL

BRL

BRL

ARL

8RrBRL

BRL

8RL

BRL

ARL

8RL

ARL

8Rl,

ARL

ARL

8RL

BRL

BRI

BRL

BRL

ARL

BRL

6

5

4

2

l o

I

6

4

6

3030303030303030303030

Thit Mo.atotl rcpod Lt aol wIA tu hou an ourhori4d signatarc on tha cover pege.

i Reponable D€t€ction Limit BRI- = B€low Repodng Limir Page 155 of l6s

Page 665: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 6000/7000 Series Methods - Quallty Control

An&lyt€G) FiagResult Unirs 'RDLSpikel,evel

o/.REC

Limits

RPD

Limil3ourc€Rcsult %REC RPD

B{tch ?031495 - EPA200/SW7000 Se.ie*

Blrnk l7O3l49sALl(ll

Prepared A AnalFedt 2&M6r{7

Mersl(y ERI_

Duollcate a70314954UPl)

Prgpared & Anelyzed: 28-Mar{7

fdtt Solt fl031.19$Ist I

Prep€red & Anal}rr€d: 204rar.O7

r.ff x Spiko fl 0gl,€5.||S2)

Proper€d & AndFed: 2&Mar-07

Rcferunco A0ltagSSR[l)

P.spar€d A Anallaed: 2&Mar{7

Sourc.: 5A596A0{2

o_0327

Sourcs: SASgO{l{?

0.566

Sourca: SA50A|1-16

ngtkg wet

mS4(S dry

nE/kg dry

rlglkg dry

mS/kS we{

0.0299

0.0334

n.0327

0.0289

0.1s(}

BRL

20l2

820.454

0.451

1 .33

aRtBRLBRLBRTBRLBRL8RL

0.4710.4920.5210-4450.5100.{€40,471

0.0320

0.0300

0 445

1 -13

101 75-125

118 65.9132.6

Brrch 70316t9. swEl6 r005A

Abnk 1703l6l9.BLX1)

Prcparedr 27-lrar-07 Analyzp,d: 2A-Ma..07

Lead

Selenium

Sflver

Chroflfum

Barium

Ca(tmium

LCS fl031619€S

Prepa6d: 27-1 a.47 Analyzed: 28-tuler-'7

Seleniuft

Lead

B€num

Sik€r

Cadmium

Chromium

.ngImsnlns,r€rmgnms4msr

mgrtnEnmgutnBnmgnrDdlrlcrl

NETotSIdtS/l

n€nn€nms,lmcil

firgn

olgrl

Insl

lngn

0.00750-0r500.tx)500.00,$0.00500.0050o-fi)z5

0.01500.00750.00500.00500.00250.00500.0040

o0.t500.00750_0060o.00500.00250-0050o.0(X0

0.0075o.0t500-00500.0025

0.5000,5000.5000.5000.5000_5000.500

o.5000.500

0.5000.5000.5&0.5&)0.500

Barium

Silvgr

Cadmium

Chomium

Duplica|. (m3t5l9.Dt Pl)

0.517o.1140.5060.4780.467

Souir.i SASS508{1

9t 8S115

9A 85-115

t04 81115

89 85-115

1tr2 8$115

97 8!fi5

94 8$1t5

94 85-115

9€ 85-'t t5

t03 85-115

89 85115

101 8t'-t15

96 85-1t5

ltil 8s115

LCS Oup ft03l61*'BSDIt

Prepared: 27]r,1a.47 Analyzed: 2e-Mar-O7

Sebnlum 0.46SLead 0.4s9

0.60.60.8

0.81

mm202020m20

m20m20

Prepar€d: 27.1!sr-07 Analyzfd: 28-l,rl€I47

S€lenium

Si$st

Cadrlium

8RL8RL

0.00248RL

BRIBRL

o.0c27aRf

Thlt lobnbry repaa is ,rd rolil wirhoa atr audtorizd stgnaar. oi tte @je. pdge_

* Report blc k€ction LiEit BRL = Betow R€porting Limit Pag€ 156 of 165

Page 666: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 6000/70 ) Series Methods - euality Control

Analyte(s) Rcsult Flag

Source %REC

Result %REC LimitsUnits *Rl)LSpike

Levcl

RPI)

Limi tRPD

Bshh 7031619 - SW846 3005A

Ouolhat€lm3l619OUP1l Sourc€:SAsgsos.ol

Pr€pare.d: 27-lelar47 Anatvzed: 28-Mat -O7

Chrooium8€rium

frt|ir soile t703l6le+$t)

BRL

8RL

BRL

So.r.oe; SA596{l-18

0 4630.4650 .5140_464o_4370.500o 418

rng/l

rng/l

lng/l

ms/lngr'l

mgmsrmg/l

mg/l

mg/l

mg/l

mg/l

mgn

tngn

mg/l

mg/t

mgn

mgn

mgn

mg/l

rng/l

thgn

rhgn

rngn

rhgn

nE,,l

lhgn

rhg/l

lng/l

rngn

rhg/l

rhg/l

lng/l

mgn

mg

rhg/l

lngr

0.00400.00500.0050

0 01500_00750_00500.00+00.00500 00250.0050

0.00750.01500.00500.00500.00250.00500.0040

0.01500.00750.00400.00500.00500.00500.0025

0.5000.5000.5000.5000.5000.5000.500

0.5000.5000-5000_5000 5000.5000.500

0 5000.5000-5000.5000 500o-5000.500

BRL

8RL

BRL

ARL

BRL

0_001.1

BRL

ARL

ARL

BRL

8RL

BRL

BRL

0.0014

BRL

BRL

202020

Pnepar€d: 27+1€r{7 Analfled j 28,MaF07SelenlumL€Ad

Baium

Silv€rCadmiumCtuomlum

L€ed

Sel€nium

Slvea

Badum

Cadmium

Chromium

Po.t Splte O03t6t$PSl)

t{5trlr so{(€ Ooo fl031619-filsol} Sourc6: sAS964t-ta

Propared: 27-llar.07 Analyzed: 2A-Mat-07

s3 75-125

97 75-125

103 75-125

93 75.125

a7 71125

lo0 71125

95 75-125

9A 75-125 'l

75-125 1

88 75-125 0.5

103 75-125 0.4

101 75-125 1

96 75-125 0.4

94 71125 1

0.491

0.468

0.439

0.516

0.505

0.440

0.470

Sou.co: SA5964t.tE

20202020202020

P.6par€d: 27-t!lar{7 Analf?ed: 28-Mal{7Selenirm

ChromaumBariumSilverC€dmium

Brtch 113 1677 - SW846 3005A

Ahnl( O03l677ALKll

PGp€r€d & Anabzed: 28-Mar-07LeadSeleniumBariumSawrChromium

Cadmiom

LCS a?O3t€Tf .8st lPlepar€d & AndFed 28-Mar47Le€d

S6l€nium

Barium

Sft,er

Chronium

0 4760.5000.4780.445o.522o_4350.51' l

BRLBRLBRLBRL8RL8RLBRL

0.490o.4730.4450.451o.4760.48e

0.00750.01500.00s00.03000.0050o00t00.0025

0.00750.01500.0050o.03000.00400.0050

0_5000.5000.5000 5000-5000-500

BRL 95 80,120

BRL 100 80-120

BRL 96 80-120

aRL 97 80,120

0.0014 104 ao-120

BRL A7 AO-1m

BRL 1n2 80-120

98 85-115

95 85-115g7 a5i15

a5-115

95 85-115

98 81115

ThLt labontory rcFod is noa eali.l wilhoat an aulhotized sigaalure on rte cover page .

* Reportable Detection Linit BRL = Below Reporting Limit Page 157 of 165

Page 667: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total, Metlk by EPA 60([l?fi10 Series Method! - Qurlity Control

Analyte(s) ResultSpike

Lev€lRPDLiflitFlag Units *RDL

Source %WC

R€sult o/rR-Ec Linits RPD

OuElic.lsl703157OUPll SourESA5964t-t7

Pl€9ar€d & Anal}rzed: 28-Iler-0?

Brrct 70316?? - swEd6 30054

LCA 17031677€3ll

PrBpared & AnalyzEd: 2&Mar{7

Cdmium

LCS Duo f/03187ASDi)

Pr€parcd & Anatyz6d: 2&Mar{7

S€l6oium

L€ad

Bari|lm

Silver

Ch.omium

Cadmium

Selenirm

Cadmium

ClYoniumB€riumSl\,sr

l||tdrspn r7o:11677-flSl)Pr€paEd & Analfzed: 28-M€r-07LeedSel€oiumBEritffn

SnvorChrqniumCadmfum

L€€d

Sel€nium

Chrooium

B ium

Hmium

Silv€r

Pod Adke ft03-l577.Ps

P|epa€d & Ana\zed: 28-liler{7

S€l'snium

Slh/€.

Cadmium

0_500 mgn

0.464 otS/|0.,$4 ftSn0.472 nEn0,467 ms{0-43s mdlO.4f 7 mCI0.490 ndl

BRL fiS/t

0.973 qRG m97|

0-0026 -gI

0.0734 nE.Il

0.103 AR6 mg/t

0.608 aRd mSI

0.0206 J,ORa nE,t

Sourc€: SAlto532.01

O.{aO CSIT mS1|

O.47A nE/

0.760 OMz nrgrl

0.4€4 ntS,

0-447 nlg4

0.496 mgl

c.472 NI

0.492 aM7 nrgll0.4€9 mdl0.512 mCI0.79'l aM7 mg,/l0.448 '|'eA

0.5|0 rE/l0.502 mS4

So!rc.: SAsgSll?-Oi

0 0025

0.01500-0o750.00500.00400.03000.00500.0025

0.01500.00750.00250.00400.00s00 00500.0300

o.00750.0't500.00500.00400.03000.00500.0025

0,o07s0.01500.00500_00500-00250.03000.0040

o.01500.03000.0dI5

0.500

0_5000.5000.5000.5000.5000.5000.500

85-115

&1115

8$115

8S115

85.115

65-r15

85-1t5

85-115

75-125

75-125

75-r25

75-125

7U125

7$125

75-125

75-125

7*1

75-125

75-125

75-125

75-125

tu125

60-120SGlA)80-120

100

9397s4s3a79590

2I

,t

2

2

172

26

22

5

197

2020mm202020

2020202020m20

[.lrlr Solke Oop fl03167f{SDl) Source: SA59532-0i

Pregercd & Analfled: 28-lrar{7

BRLo.oo72ARL8RL

0.0079o.2760.0268

0-5{D 1.020.500 BRL0.5tn 0-6040.500 0.07560.500 0.02120.500 0.1060-500 0.0032

o.sco 1.o20.5m aRL0-500 0.1060.5m 0_6040,500 0.00320.500 0.02120.500 0_0758

0,5{x}0.5(X)0.500

BRL

o.m12o.0032

NR

3182937A94

NR9881

97s8

202020mmm20

0.4580.5410.{51

trg,lrE/lmg/l

104

Thls, ttto'{lort ,t$tt b ,tot a{f,d flirho|,, on aathodzed sig/'gd*e oE te @'er pq.-

' R€portable D€tedion Limit BRL = Below Reportiog Limir Prge 158 of 165

Page 668: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total M€tals by EPA 200 Series Methods - Quality Control

Bctch 7011494 - f,PA 200 S€ri€s

gl.nk fi031,194€LKl)Prcpared & AnalF€d: 28-li1,,lar-07

Silv€rS€lenium

Chrornium

CadmiumBarlum

Ouolicate ft03ll9{.I)UPI IPrspa€d & AnalFed: 28-[.,tar-07

SllveaSelenium

ChromiumHmiumBarium

alrix SDll. t703149+lirsr IPFpared & Andyzed: 28-Mar,07Sik€rS6leniumCfi.omlumLe€d

fumiumBadum

reHr Srtr. n03149+MS2l

Prepared & Analf:€d: 28-Mar{7

Sel€niumSitu€r

ChlomiumLeadC€dmiumasium

BRL

BRL

BRL

BRL

ARL

8RL

ARL

Sou.E€: 5A59620.02

nE/kg wel 0.938mg/kg w€l 1.41mgukq wet 0.704mgukg wet 0 469mgukg w€t 1-41mgukg w€t 0.235mg/kgw€t 0.469

mg/kg dry 1.11mg/kg dry 1.67mS4(g dry 0.43sndkgdry 1.67ng/kg dry 0.557mgfl(g dry 0-278mg/kg dry 0.557

mS/kS dry L04mg/kg dry 1.56mg/kg dry 0.522mgftgdry O 742mg/kg dry 1.56mg/kgdry 0 261mSftS dry 0.522

mgftg dry 'l -54ng/kg dry r_03mgftgdry I -:,4mgftgdry 0.515mg/kg dry 0.772nEftSdry 0-257nSftSdry 0.515

mgftgdry 1.65rhg/kg dry 1-10mg/kg dry 0.549mSI(g dry O.2f4fiE/kSdry 1.65mo/kg dry 0.549

ARL

BRL

33.9

2.90'15.2

0.368

52.9

Source: 5A5364l{7

121

132

1 5 3

218

131

120

168

Sourc€: 5A59641-16

130

130

130

130

130'130

'130

129

129

129'129

129

129

129

137'137

137

137

137

137

78.0

41.1

44.7

49.3

3 1 . 7

BRL

ARL

38.7

2.47

16.2

0.502

56.5

BRL

BRL

29.4

99.7

6 4 1

0.599

39.2

BRL

8RL

1 . 1 5

4 4 1

3.65

0 . 1 1 7

10.4

BRL

BRL

29.4

0.599

6.41

39.2

1 66317

35

3535353535

130

114

1 2 3

125

121't23

1 3 8

mgr'kg wetm9n(9 wetmgukg w€tmgtkg w€tmgukg wst

93 70-130

102 70-130

95 70-130

91 70-130

96 70n30

92 7C-130

99 70-130

101 70-130

88 70-130

70-130

93 70-130

91 70-130

95 70-130

99 70-130

101 85-115

91 E5-115

109 85-115

92 85-115

98 85-115

108 85-115

114 77 +122.6

108 66.3n$-6

101 81.8-118.1

s7 78.$120,5

101 42.1-117 _9

PoEr Sdko t703l4x+Sl I Source: SA596,H {7Propded & AnatF6dt 28-Mar-07

1 3 9

125

t 7 9

127

141'| E7

8 8 6

44.3

45.0

47.8

32.0

Sel6niumSlverChromiumCadmlum

Barium

Rrf6|E|lco O031494-SRttllPrgpaGd t Analyzedt 2B-tdar-O7S€l€niums|lverL€adChro|txumC€ddum

1.501.000.7500.500o.250

Ihis laborutoty repod is Foa vs&t Hirtotu aa aathotked signaare on the coter paEe.

' Reportable Deta:tion Limir BRL: Below Repo.ling Limit Psge ls9 of 165

Page 669: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 200 S€ries Methods - Qrality Coqtrol

AIlaryte(s) FlsgSpike Sourcc

L€vel R€sult

%RECLimifs

RPDLimit

B{tch 113 1494 - EPA 200 Series

Reter€nca ff031404-SRil I I

Pr€pared & Analfzed: 28-t ar-O7

Bsrium

ktch 70J 1620 - EPA200/SW700 S€ries

Blank (t03164€LKil

P.spared: 2 ar47 AnalFed: 28-Mar-07

46.1

219

m€rl€wet 1.50mS/kow€t 0.500

80-8-119-4

azz-177 -3

44.7

2 1 5

1(X102

LCS (?0r1620€Si\

Peparcd: 27 l!lat47 Aaatyz€d: 2g-Ma(47Mercury o.m2€s

LCS fi031679€31)

Pr6per6d & Anal).zed: z&Marfi

Dupllc'b lm3167g{UPll

Prepared & Analfz€d: 28-t1ad7

Xrt lr Soite flfi11679{S1l

Prep€€d I AnatFed: 2&Ltar-.07

srdr SolI. Duo flO316'tg*ls0lr

Prepared & AnalFed: 2&Mar-07

Po3t Sdk. O0:l1670fsir

Pr€pared & Anal}.!6d: 28-Md{7

0.m245

So{rrc.: SAsgGal-17

0.@?26

SourE.: EA596a{-17

0.00479

SourE€l SA5964l-l?

o.0048:,

Sou.E€: SAlt96al'17

nEn

nEJl

irSn 0.fin20

msn

tr'sA

msn

mgr

n€n

rngl

rvl

Duotlcate 1703tGi:m-DUP1l Source SAli965&O l

0$r'15

8 S 1 1 5

Prepared: z7-Mar{}TAnalFed: 28-Mar47

U.tix Splke l703l62G S1l SouEs: SA5O6.t1-t6

Pr€pared: 27-l'rar47 Anavzed: 284{ie47

atdr Soik€ Ouo l7031clo.t{5tr)t} Source SA5064t.18Pr6pared: 27{v,1tr47 Analyzet 2&.{l'/.at 47

Me.crry 0.m284

Port Soike {?0ll6;10+S1l So(rce: SA596al.lE

114

75-125

75-125

8&115

Pr€pared: 27-&lar-07 Anal:r2eil 2B.|i,at47Mercury o-m267

Brtch ?031679 - EPA2{XySW7000 Series

Abnk {70316794Ll(l IPr€pared & Anaifzed: 28-Mar-07

msn

r|En 0.000m

0.00221

o.(n221

0.00221

o.0022r

75.125

75-125

45115t15

This L6orco4 .qorl ls aot vztitt blrhod eE sulhorizd tlgnata?c on rtz cotet pg..

. R€portable Detection Lidit BRL = Beto$,Reporting Limit Page 160 of 165

Page 670: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Metals by EPA 1312 & 6000/7000 Series Methods - eualie Control

Spike Sourc€

B.rch 7031651 - sw8453010A

Blank 47031651 €LK1 )

Prcpared & Andyzed: 2A-Ma"{7

L€ed

Selentum

S0ve.

C€dmlum

Chromiom

Barium

LCS O03165t€Slr

P.epaed & An€l}.zed: 28-Mar{7

Lead

Selsnium

Chomium

Cdmium

Silv€r

B€dum

LCS Ouo ft03l65lSSDrl

Pr€psrEd & AnalFed: 28-MaF07

S€16nfum

Lead

Siiv6r

Cedmaum

Chrorium

Berium

ARL

BRL

BRL

BRL

8RL

BRL

8RL

1 . 1 8

1 . 1 4

1 . r 6

1 . 1 4

1 . 2 2

1.06

1.26

1 1 3

1 1 8

1 . 1 3

0.866

1 . 2 1

1 . ! 5

1.27

Ouolicatefl03l65lJuPlt Sourco:SAi96ai-is

Prep€rod E Analyled: 28-Mar-07

Leift

S€lenium

Sfver

Chromium

cadmium

Badum

I.trlx Solt ff 031oitl{tS

Prepared E Analfz€d: 28-[,lar-07

S€l€nium

Silver

Chrmhrm

Cadmium

Barium

0.0025

BRL

BRL

BRL

BRL

BRL

0.0r18

Source: SAS96a1-16

94 82.3-108

91 79-108

93 76.2-118

91 77 4-109

s8 87.9-110

85 55.5-115

1 0 1 8 5 1 , r 1 9

90 7S-108 0.9

94 82.3,108 0

90 77.4-103 0.9

69 55 $1r5 20

97 87.9-110 0.8

92 76.2-114 0I

102 85 1-119 0 8

96 0r .8-105

94 80_4-105

7S 63.6-109

94 79.2-106

94 81.5-r ' t 1

99 06.4-108

102 88.9-114

93 80.1-105 0I

95 81.8-105 0 8

94 81.5-111 0

98 86.4-108 0.8

mg/l

mg/l

mEl

mg/l

mg/l

mg/l

msr

ms4

mgr'l

mqil

mg

mg/l

mg/l

mg/l

m!

mg/l

mg/l

mg/r

mg/l

mgn

mg/l

msrmgnmg/l

mg/t

rng/l

lnsn

mg/l

mg,1

mg/l

rE/l

msi

fi€/l

filgn

mgn

mg/l

mgrm94TTE,

0.01500.01500.02000.01500.00250.0r500 0150

0_01500.01500 01500.01500.00250.02000.0150

0.01500.01500.01500.02000.00250.01500.0150

0_01500.01500.0m0o_01500.01500_00250.0150

0 01500_01500.02000.01500.01500.00250.0150

0.0t500.01500_01500.0025

1 2 5

1.25

1_25

1_25

1.25

1.25

1.25

1.25

1.25

1.25

1 . 2 5

1 . 2 5

1.25

1.25

202020202D2020

1.20

1 . 1 7

0.989

1 _ 1 7

1 . r 8

1.24

1.28

1 . 2 5

1 . 2 5

| . 2 5'| _25

1.25

1 . 2 5

1 . 2 5

1 . 2 5

1.25

1.25

1.25

0.0030

BRL

BRL

BRL

BRL

BRL

0.0098

BRL

BRL

BRL

ARL

ARL

ARL

0_0052

ARL

BRLgRL

8Rt-

1 9

20202020202020

mm2020

f,Etdx Solk. Ouo t703l651.ltsol) Source SASg6.t1-16

Prepdr€d E Analfzed: 28-Mtr{7

1 . 1 6

1 _ 1 9

1 1 8

123

Sel€niumuta0Chrc(r{rr lftdmiun

Thb laboralory ftpod h not valU withoa aA aathoirzd signalure on the cover page

* Refortable Detection Lirnit BRL = Below Reponing Limit Page l6 l of 165

Page 671: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Metsls by EPA 1312 & 6{100/7000 Serles M€thods - QuNlity Cooarol

Analyte(s) Resulr Utrit3R.PD

RPD LimitFluS

Spike Source '/"REC+RDL fwd Resuil %REC Limitr

Batch 7031651 - SWE{5 3010A

Ialrir Soiko Duo c7031651-tilSD'l I Souic€: 5A5964l-16

Pr€pared A Analyzed: 28-Msr{7

1.fi)

1 . 1 6

1.28

Sourc€: SA59G41-16

Silver

Bsrium

P€t So|te fl031G519S1)

Prepared & Anall.re.dt 28-Mar-07

Selenium

Lead

Cadmium

Situer

ChtDmium

Barium

LCS {7fi 6i2€slI

Prepared & Analyledi 28-Mar{7

Ouolic€le t703165:lOUPtl

Preptred & Anel]/"zed: 28-Mar{7

alrir Spik€ l7031652.irsll

Prepared A Analyzed: 28{vlar{7

1 . 1 7

121

1-19

1.25

t . t l

1 . 1 9

1.29

SRL

nrs/|r€/1mgn

mg/lrEnnElms/|ftrSImglmgil

mgn

fttsn

0 02000.01500.0150

0.01500.01500.01500.m250.02000.01500 01s0

1.25

125

t.25

125

r.25|.251.25

1-25

125

1.25

ARLBRL

0.0052

BRLBRLBRLBRLBRLBRL

0.m52

2020m

100-90

8793102

63.6-10979.2-1(X88.9-1'14

n.7-10a80.110E79.$t0786.5{0961.7 -107

78.1-11486.&118

94.9794100809l;103

Bstct 70f159 - EPA200,6W7000 S€ri€s

glank (7O3i652€LK1l

Prepa.ed I AnElfi€d: 2&Mar.O7

0.00244

Sou.ce: 3A59€41-15

BRL rngl 0.00040 BRt

Sou.ce: 5A39641-tG

0.00251 nrdl

0.00010

0.00040 0.00250

0.0@ro 0.00250 8RL 100

BRf 99

99

66_6-117

20

lraHx Spike Ouo 4r031652{SDl| Sourc€: 5A50641.16

76.1-111

76.1-111

E6.&110

Pr€pared & Analyzed: 2&t ar.07

Posr Soik6 O031652-PSl I

Prepared {l fu|elf2ed: 28-Mar{7

O.tn247 mgl 0.000.10 0.m25O

Sour€e: SA595al.l6

20

0.002/|a |rSI 0.mO4O 0.00250 BRL

G€oerrl Cbemistry Pammeters - Qsallty Control

Bstcb ?0ll,u0 - Ceo€rrl keper.aloo

Duollcare aTu tT0ouPt IPrepar€d & Analraed: 2+Msr{7% Solicls

So(rc€: SA59619{1

% 97.9 m

Thtt hbraro.y r.port b wt ts6d uidro!, oa oartoried tl8/,.ata!. or, rtz cover poge.+ Reportable Detection Linit BRL = Below Repodrg Limit Page 162 of 165

Page 672: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Notec and Definitions

'TPH Calculared as

Comp Completed

FP Field Preserved

QCI

QC2

QM?

QR4

QFJ

QR6

R05

s02

vela

Analle out of acccptance tange.

Analyte out ofacc€ptance ra-oge in eC spike but no reportable conceotmtion present in sample.

The spike recovery was outside accepiance limits fot the MS and,/o. MSD. Th€ batch was acc€oted based on acceotableLCS recovery.

AMlyses are not controlled otr RPD values ftom sample conceDfatioos less tha[ the reportiog limit. QC batch acceptedbased on LCS andlor LCSD QC resutts

RPD out of acceptance |ange.

The RPD exceeded the QC control limits; however precision is demonstrated with acceptable RpD values for MSA{SD.

Elevated Reporting Limits due to thc presence ofhigh levels ofnon-target analyres-

Tbe surrogate recovery for this sample cannot be accurately quantified due to interference ftom coeluting organiccompounds present in the sample extract.

Field extracted

VOCS ReponiDg limits reflect SW846 5030 extraction technique due to matrix inrerlerence using SW846 5035A extractiontechnique,

Z-2 The recovery ofd-BHC wes outside ofthe acceptatrcc range due to a breakdown ofd-BHC within the spike mixrure.The CCC is withi[ acceptable limits which demonshates that thc problem lies with the mixture, not rhe instrumentarion-

BRL Below Reporting Limit - Analyte NOT DETECTED at or above rhe reporting limir

dry Sample resulrs reportcd on a dry weight basis

NR Not Reported

R.PD Relative Percent Dilfcrence

J Deteoted but below the Reportiog Limiq therefore, result is an estimated concetrtration (CLp J-Flag).

A plus sign (+) in the Method Reference column indicates the method is not accredited by NELAC.

Iot€rpretatiod of Total Peholeum Hvdrocarboo ReDort

Peroleulrt identification is determined by comparing the GC fingery.int obtained fiom the sampte with a library ofGC fingerprintsobtrined from analys€s ofvarious pekoleum products_ possible match categories are as follows:

Gasoline - includes regular, unleaded, premium, etc.Fuel Oil #2 - includes home heating oil, #Z fuel oil, and dieselFuel Oil ll4 - includes ll4 tuel oilFuel Oil 116 - includes l/6 fi.rcl oil aod bunker "C,, oilMotor Oil - includes virgin and waste automobile oilLigroitr - iEcludes mineral spirits, pekoleum naphtha, \,ln&p oaphthaAviation Fuel - includes kerosene, Jet A and JP 4Other Oil - includes lubdcating and cutting oil, and silicon oil

At times, the unidentified petroleum ploduct is quatrtified using a calibriation that most closely approxinates the disfibution ofcompomds in the sample. Who! this occurs, the result is qualified as *TpH (Calculated as).

Thk laboraary repod is nal vol t wirhout an aurtoi4cd tripatttrc ot lhe cover pge.

* Repdlable Detection Limir BRL = Below R€podng Limir PaBe 163 of 165

Page 673: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

hboratorv Cotrtrol Sample (LCS)t A knowr mafix spiked with compound(s) r€prcs€nhtive ofthe targ€t a(atytes, which is used todocument laboratory perfonnance-

Matrix Duplicate: An intra-laboraiory split sarnple which is used to document tbe p.ecision of a method in a given samplo matrix.

Matix Soike: An aliquot of a sample spiked with a knowu concentratiotr of targEt aoalyte(s). The spiking occus pdor to samplepreparatiotr and analJrsis. Amahix spike is used ro docum€nt lhe bias ofa rnethod itra given sampl€ inahix.

Method Blaok: Atr adal)'te-fte€ nat ix to which all reageots are added in the same volumes or propo.tion$ as us€d in sampleprccessi[g The metbod blank should be canied through the complet€ sample pnqnration atrd aoal]tical procedure. Tho Eethodblaok is used to document cootamination resulting from tbe a[alyticll process.

Method D€tection Limit (MDL): The minimum concentiation ofa substance that ca! be measut€d and Eported with 99%confidence that the arullte concentration is greator thatr zero ldd is determined ftom aoalysis ofa $ample in a giveo matrix q?econtaining 6e analyte-

Reportable Dotection Lirnit (RDL): The lowest conceobation that catr be r€liabty achieved withil specilred tihits ofprecision andaccuracy duidg routine laboratory operating cooditions. For Eany analytes the RI)L analyle cotrccobation is selected as the lowestnon-zero standard itr lhe calibration curve. while the RDL is app.oximarely 5 to l0 tim€s the MDL, th€ RDL for each saGple takesinto accoutrt the sample volume/weight, exlract/digestate volume, cleanup pr<rcedures atd, ifapplicable, dry weight con€ction.Sample RDLS are highly matri[-dependent.

Surroeate: An organic compound which is similar to the targ€t analyt{s) io chemical composition and behavior in the aaalyticalprocess, but which is lot normally found in environmeDtal samples. Ttese compouods are spiked into atl blatk, stand.ards, andsamples pnor to adalysis. Perceot recoveries aae calculated for each sufiomle.

Validat€d byiHanibal C. Tayeh, Ph.D.Christopher HaltNicole Bro$1r

Thit l&boturory rqorl b nol vaful r,ltlro.t! an aythorlzed sb''{/tuE on ale coe.r poge_+ R€portable Detection Limir BRL = Beloq, Reponiog Limit Page 164 of l6J

Page 674: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

State Of ConnecticutDepartmcnt of Environmental protection

Laboratory Quality Control and euality Assurance Form

I-aboratory Name: Sp€ctrum Anal'.tical, Inc - Agawam, MA

Project lncation: NHRY M8 Acccprance Facility _ New Haven CT NHRY ME Acceptance Facilify - New Haven, CT,/Tl s Form Provides ce(iljcations fof the followlng data ser:

sa5964l-01 sA5964l_t IsA5964t{2 5A59641,t2sA5964l-0t sA596{r- l lsA5964t-04 sA596.u 14SA596{t-05 sA5964 L_ 15sAJ964t-06 SA5964t_16sA5g64t{7 5A5964I,17sAJ9641,08 SA59&t lEsA5954t 09 sA5964l_19sA596{l l0

List Sp€cific AnalyticaL Merhods Used:+(jT ETPH

EpA 200 7EPA 245.1/7470A

SM?540 C Mod.sw 8,t6 8260A

sw846 Bl?

sw8.r6l l t2/60108

swE46l3t3/7470A

sw846 50 t0BswE46 74?tA

sw846 EOEIA

sw845 80E2

sw846 8?60A

sw8468270C

sw845 82?0C/EPA 625 |voc

Werc all samples received by the laboratory itr a condition consistentwrth that described on the Chain ofcustody documentation lior the dataset? El Yes E No

Were all QA/QC procedures required for rhe spocilied anah,ricalmclhodts) included in this repod followed? El Yes E No

W€rc all QC perfonnarce standaads and recommendations for thespecified methods achieved? E Y e s E N o

Were results for all analyteJist compounds/elernents for the sDecifiedmethod(s) reported? E Ycs El No *

The mmpou(h andd €lenenl! rcPfrr.d ar€ as sPecifi@llv r€quesled bv h€ ctieflt on rhe chain ofcustody ant in $me @s6 may no( inctude rhc aulrnalyr. lis a! defin€d,n rhe m€dod.

Negqlive rcsponses lor A, R arrd C ore td.lrdsed in a case nanst re on the cover ptge ol this rcporl

I' the andenigned, anev under rhe pains .tnd penorlics olpedsry that, based tpon my percondr inquir! ol lhose ftsponsibteror oblaiaing rhe info 'ration' lhe dalerizl conrained in thb an;Irficdt r"port it,u *e best o\my kaonledge and berieJaEok rale s.rd contplela

nftd-tlaaibal C. Tayeh, Ph-D,President/LaborEtory Director

Datr: 3/29Dffi7

This taborurory rcFat h not valid Nithaat oE zy.honzad slgaa/sre on tha cove! paEe.i R€portabte D€rection Limit BRL = Below Reoortine Limit PaBe 165 of 165

Page 675: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 676: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

s b o

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Page 677: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet
Page 678: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

= b t r5 h\F4 6 :

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Page 679: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificatiooFB.4sA59t0l- l9

Client PFiect #301-88

MafixBlank waier

Collection Date/time26-Mar47 00:00

Received27-MaFO1

CAs No. Anab.z(s) Res r FIag UfiE 'RDL Dihltiot' Mahod Retr. PEparcd AnalJztd Barch Anolyst

VolEtile Orgrnic Compounds

Volalil€ organic Comoo.hds bv SW846 82608

Prepared by me$od SW846 5030 Waler MS

?6111 1,12-Tidh6tifiuor€hane(Freon 8HI6r&t Acetoi,e BnL107.1$1 Adyionitr{e BFL714!2 B6?en€ BFL108-86t Erctrjotenz€oe 8Rl7+9/-s BlollEcl{orcnethane BRL'itru

Eromodbhlooln€tlane BRLEh.2 Bornolorm BRL74+r-9 B|D|ftrnsdane B8L7818.3 2-Eulandte (MEK) BBL10451{ +Butyt€fzene 8RL13srl s€c€utylbenzene BRL90{6{ teGgr$r{tenrene BRLE1fl Cerbon dierlfide BnLs6-2+s Cafton telracdonde BFL10!-907 Chbrobenzene BFL?5{lG3 Chtorcefl'|e 8RLsl-te3 Chtonforrn BRL74.47s clioFn€hene BRLss8 24hlootdu€ns BaL1Od'13.. 4{hlorotdueo€ 8fl1F12_8 l,2{ikomo3drlorcpropane 8FLl2,l-{&l Dibrofibcl Oon€hans Bful0em-4 l,2-Diborno€hane (EDB) 8RL7+953 DibronEmethane 8RL9+5et 12-Dchtombenzene BnL511.7!1 l,O.Dichlolob€flzene BRL106.16.7 1,+oichtorob€nzene BRL75-71.8 oidtorcdiuorcrne$ane (Freffl2l BFL75-3+3 l,lSiciloroettlano BRL10146.2 l2-Dichto.o€ Ene 8Rt7t!64 j,l.Dcflomefiene BFLr5&5s z dsl.2-Did orcetlene BffLrfs-6c5 rangl2.Dicnbro€tpie BFL

BFL

BFL

8BL

BNL

BRL

B8L

BFL

8RL

8RL

BRL

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BfrLBFI.

8RL

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pdl

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Itc4

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t 0

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1.0

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?.0

05

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2.0

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1.0

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0.5

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sw846 @@A E:Mer07 z$Llar{7 7091n7 RU

n47-s t,2ochloopropane

1.d,s4 1 ,fi)id oopropaE9+*7 2,2oia dopropdne5e5€-€ l,l.Dicfitoropfopenerto€r{r-t cis-l,3{id{o,cplopene

101061423 baEl-.r{idlloilprop€n€

lo0<1-4 Eb4t€ozone87-6&3 Heradlorobdadenes01-78€ 2_HetdlolE (MB()s€2€ koorcpyb€iz€nssgaT{ 4lsopropytofuen€

1614044 Motryltert-butytdlef1oBnG1 4.$dry-2fsnlenone(MBK)7ss2 Medrylene chlodd€01_203 Naphfiaiene

1@6+t n+bpylbeflz€oe

Thb loboratoq rcpod is ^ot vdlid x'ithocl en audrodZd slg'/tCdre on thc coser page.

. R€portabl€ Dct€crion Limir BRL = Belov Repding Limit Page 94 of 154

Page 680: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole IdentificationFB-4

sA59803- t 9

Client Proiect #301-88

MatrixBlaDk Water

Collection Date/Time26-Mar-07 00:00

Received21-Mat01

CAS Na Anrb'te(s) Resull Flag Units *RDL Dilutinn PrcpoEd AndDzed Batch Ahdllst

Volrtile Orgrnic Comporndr

Volatle Oraanic Compoqnds bv SW846 82608Prepared by method SW846 5030 Water MSlq}4a5 Sryrene 8RLd!120.5 I,l,1 z-TelrachtoroetEne BRL79'3+t 1,|,2,2-Tdrachlooehane127'18.,t TeFachlooethene10!-€&3 Tofu4]er{1-6 12,3-Tichlorob€nzene120-82-1 1,2J.Trichto.ob€nzefl€71.5s 1,1,1-Trichloo€thane79{lcs 1,.t2-Tdcloo€thane79-01{ Tfuhlooeh€no

Tti*lorcf uoom€hane (Freofl 1 1)9G18-l 1,2,3-Tric$loropropane

1 J,4.Trifii€thytb€nr6ne10&€7-8 1,3,5-Trirclhylbenzefle7F0r-r \4nyt chlodler3o2o7 m,Pxy'ene96-07{ cx/enet09s6:9 Telr-afiydrotLrrana.&7 Ehyl eher90!-!64 Tgd_amylneht€ther67-!e.3 Ehyt t€d+utyl eiher10€.2rI3 Disopmpylelhef7ft54 TBrt.Bulaml / buv alcohol12391-1 j,+uoxan€

16n00'4 1-Br6pn@tobenzene

M7-6-5 TduEne4S

E0@4ra 1,2-Dic o$etAne44

tw5t7 DlxofibfrMorneuAne

Extrrc'tebl€ Pehoteum Hydrocsrbon3

Ellradalh Tolal Pelrcteun |Mrocarbo(s

Prepared by melhod SW846 3510C

&066.9 casotinE6&7e30' Fuslot#268trfl1.3 Fue{ Oit*168ts&0(|.{ Fu€l0it$6ne800c00 llotorolJilo1ll|)oo AviationFu€l

Unde0tli€d

Oh€i Ol

Tolel Psdelm Hldmcadons

CSC36 Aliphatc Hydmc€ft 016

J384$? tctMafuane

SeDivohtle Orgrnic Compoundr by cC

oroanodhdne P€didies SW846 8081 A

Prepa.ed by method SW846 35'l0C

[email protected] At&ingl9.t46 A€HC

BRL

BRT

8RL

BRL

BRL

BHL

BflL

BFL

BFL

BFL

BFL

SFL

BFL

BFL

BNL

BRI

BFL

BFL

BBL

BBL

BFL

BFL

lgl 1.0

lSn l0

la( 0.5

ps'l 1.0

USI 10

pS4 1.0

w l -0

Ug4 l-0

UCI 1.0

pgl L0

tdt r0

pg,l 1.0

pSI 10

ps,I 1.0

! M t 0

!M 2.4

pSI l0

!S, l 100

$/ 1.0

!91 1.0

lgn 1.0

lgn 1.0

!94 10.0

!S/l 20.0

7G130 %

7V130 %

7Gt3A r.

70-t3a%

0.1

0.1

0.1

0 1

0 1

0.1

0.r

0.1

0 l

0 1

sw846 82mB

rCT EIPII

sw846 811814

l

1

1

I

I

l

1

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29|'rlar{7 ?9-Ma'{7 7A31797 FU

2&Marfi 3o-Ma4l 7431122

29-Ilar47 29.Mar-07 7031768

93100108104

mg/l

'ns,l

mg,l

tng,rl

MM

mgrl

rn9l

mg,

ftq,,1

ns,'l

BFL

BFL

BFL

BFL

BFL

BfrL

Bf,L

BRL

BHL

BRL

87 1+110%

BRL

BRL1]s4pdt

0.25000.2500

This labofstory fepod is t lrt volU xtilhou aa aulhorirzd signaturc od lhe .owr poge

+ ReDo.table Detectioo Limit BRL = Below ReDortins Limit Page 95 of 154

Page 681: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samote Id€ntificationFB.{sA59E0l-19

Client Project #l0r-88

Mari,(Blank water

Collection Date/Time26-Mar4? 00:00

Rec€ived2'l-Mar-07

CAS No- Aaqlytc(s) RetuU FW Aaia *RDL Ditutioa Method Rel. Preparcd Aral$ed Balch Aaelfst

S€mivolNtik Orgrnic CompoundE by cC

Oroanochlodn€ Pe6licides SW8(; en81A

Propared by method SW846 3510C

319.S5 / b-BHC31!ltG8 d€t]c58.s$e g-BHC (Und6ne)5t-1+9 erbrdanen.544 4,4',000 {p,p')?2-55.s {,{ {DE lp,p)s0-2e3 4,4-00T (p,p)6&5l-i Di€ldinS9l-8 Endosulfsn I3913-66{ Edodjfan tl1qt1{t-8 Efth6ultarSuthte72.2G8 Endin7421-9i-4 EdinAldefryde?E-{]r.8 tbpbd{or7243-5 l.(efiorychlor1024.57.3 HeohcnbrEponds

0@1-3t2 Tcr)oph€iesr6,7r€ a.chlo'dane55663+7 g-c-l o.dar|e5C||g1-7G5 Endin Kolone

1@4, 4,4aBetuMtuiplpq4(s4

?,51-2a.3 bcactluownyl(St)

Fohd odnaled Eliphsnvh bv SW846 8082

Prepared by melhod SW846 3510C

1267+11-2 PCB 10181110+282 PCB141||11r,1€-5 PCB 123253,16&21-9 PC81242126t2.294 PCg 1244rlqr-6s1 PcE 1254Io06-ne-5 Pc812603rip4?s5 PC8126e111l)Crlr PcB 1268

IMlul 4,+DB.Maflt@r6ptcny(54

M1-21-3 'edllot@Enta(Sn

S€mlvolrlile Organic Compoundf by GCMS

Somivohdle Oroanic Comroun& bv SW8,4{t 8270C

Prepared by method SW846 351 0C

Bn29 Aaen4hh€ne200.96.8 A€nsphq/bne9012{ l.tirsttylnaphfiaJenee 53n Aniline12O.t2.7 Anhr€cene1912.2+9 AlErin€l@{+3 Arotenzen€,DiptEq,ldaine92-87-5 &nzidne5665 0 Benm (a)anhrac€n€

0RlBBI.BFIBRLBRLBNLBFL8RLBBI.BRLBHLBRLBALBFLBBL8RL8RL8Ft8RL8RL

669

8Rr,ARLBRL6RLBFI.BRLBRL8RL88t-

60IN

pC4 025&

lSI 02500

|lg'l o25oo

pEr 125)

pdl 0251I)

IS/| 025{10

lEl 0.25{0

!C4 0 05ql

pS4 025&

uS, 0251D

!S4 025{X)

8Il 025m

tS4 02500

Igtl 02500

w 02afi

M 02smt44 1.2919.'l o25oolryl 025mPS'l 02500

30.1fl%

Ttfr%

0.s{xl0.5000500

0.5@

o5&

05@

0.5@

0.s0.5d)

3t,1il %

t u 1 f l %

sw846 808t4

sw846&)82

sw8a6 827m

9ElWApc4psruc/r!sn!s.4€.4

t4

zgi.,la({? 29lrer.0? ?131769 Sl,

28{il€r.07 3r.[,t€r{7 7m1680 ltBBHI.

BRL

BFL

8FL

BFL

BRt

8Rr8RLBRI-

|lg4

wr'gl

t c IMugt't4ltdl

w

1.m

[email protected]

02m

This lsbodoq rcport is nol vali.t )tilhottt td aadtoded stg'isu.c on dre coecr psge-

' Reportable Detection Limit BRL = Bebw n€po.ring Limit Page 96 of I54

Page 682: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldentificetionFB.4sA5980l-t9

Client Proiect #l 0 t ^88

Matrixtslank Watef

ColLectio[ Date/Time26-Mar-07 00:00

Received27 -MaL07

CAS No. Atutl4a(s) Result Fl"C AniA rnDL Dilution Prcparcd Anab.ed Balch Antllsl

Scmivoletile Orgrnic Compornds b) ffVS

S€fiivolatil€ oroanic Compounds bv SW846 8270C

ftepared by mebod SW846 35'tOC

cr3'a8 &nzo (a)pyrene

at'*z Benzo (b) looranthene191.?r-2 Beozo(g,h,i)peryene2!7-@{ Benzo(k)fluoranhens66-€5{ Benzoic aaid100.5r.6 Bsqlalcot|olnl-9lJ &b(Zdoroehory)mthane111444 t|is(2doroehyi)other3Be$-324 Bis(2dororsopr@yt)ehe.11741.7 tlis(2ahylh€rylphlhatare1016$3 +&qnophenttpfienylelher8@7 Brlyl b€r141 phhatate

8G7't{ Cadezoleis5G7 44htorGlmethytphenol16-.47-€ +Chtoroan ine91.5&7 2{hlcfonaphtiatene9567{ 2{htctrophenol7!0t72.3 4{hlompheflylphenytehe(218{1,s Chrysene5370.3 Diberuo (a,h) anlhracener3a{4-9 oibenzofurans+5G1 lr-Dctiorob€nzene541-73-1 t,3.Uchlorobenzen€1q-.4+t l,4.Dchlorobentene91€+1 3,3.Dichloobentidineja4+2 z,4.Adlotopra.r,ls1-€62 Diethylphhatale131-11.3 Dimehytphhatale10557.9 a4-Ilmdhytphenol*742 Di+botyt phhalale53462-1 4,&Dnitm-2-meihylgenol5t &5 a{-Dnitrophenol121-1+2 a4.Dnitolotuene@2G2 z,6-Dinitrototuens117-8411 0i+odylphttEtat€206-4,1.0 Fluotanften€6&7+7 Fluorensr1&7't-l Hoxadolc,b€nzenett7{&3 HeEct ombdad€nen17.{ HexachloGlclop€nLadien€6t-t2-1 Hemd olwf|ai€19$30-5 h&no(t,23rd)pyreae?&ss1 hophorcne915/{ 2.li,ielhylMphthalon€6.f&7 2.t eitl;/ptje.trj

10&3+4, s,4.|r€hylphenol1n6-41-59r.20.3 Naphfide|es&7rH ?-NibDanihnecr{g€ O{ifoaniline100415 4tftoanilhe

BRL

BRL

8RL

BRL

8RL

8RL

8RL

BRL

BRL

BRL

BHL

BRL

BRL

BRL

BgL

BRL

8FL

BFL

BFL

BFL

BFL

8FL

BFL

BFL

ML

88t

BFL

BRL

BFL

BFL

8RL

BFL

BRL

BNL

BRL

8RL

8RL

8RL

snL8RL8RL8RL8RL

8RLgRL

8RL

ARLERLBRLBRL

uslus,lIMpsnpslp91

Wl

!94psn

us,4us4!sn

ttsl!s,4ps4

ugl!sn!sn!snjrs4

!s4!91lsnysn

wt)gr!s,4!s,l!srl!s,4usn!s.4!sn!E!s,4!s.4!81!sn

!9r!91lsri,sirtsrrcIttstpsl

rglu94!s4|a,I

0.2m0.mt m0.3001001 0 01 N

1.00

1.00

1.m

1.00

1 0 0

1.00

1.00

1.00

1.q)

Ltxl

1.@

L00

0.200

t.00

L00

1.00

1.0{)

uto

1.00

1.00

1.00

Lm1.00

1.00

1 0 0

1.00

1.00

1.00

1 0 0

1.00

1.00

0.600

l t D

1_00

0.2!0

r.00

r_00

t.00

10.0

1.m1.m1,00lm

sw846 8270C 2S.Llar-07 31-Mart 7m1680 M.B

Thit lzboralory rcpod h Na wU pilhoul da aatho.ized signtture on the cowr paEe .

i Reportable Derectio[ Limi! BRI- = Below Reporting Limit Page 97 of 154

Page 683: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample ldeptificationFB4

sA59803. t9

Client Proiect #l0 t-88

MatrixBlank Woter

Collectiop Date/Time26-Mar-07 00:0O

Received2'l-Mat47

CAS No. Adalrta(s) Aesull FIoe Unils *RDL Itilaian Me!*4d. ReI, P.qor.d Aitwd Boteh A"stlsl

Semivohaile Orgrnic Compoundi h,y GCMS

Semivolalilo Olanic Cqnpomds bv S$1846 @70C

Prepared by method SW846 3510C

00.9u litobffz€n€

8e7s 2+.litoph€nol

lm{2.7 +tiihophqrol

62-75-9 N.NitGodmett/aftne

6e1{,r-7 il+Ilm6od-n-propylanine

86-30+ l$l'litoEodiphenytamine&r.865 Parchlorophenoi350t-8 Phenanhr€n€

1@95-2 Ptenol1aH)0{ P}tEn€

lto'oel PFdn€12012-! 1,2,4-Tridttorob€nz€ne

*95{ 2,1,$TricnbrEphenol€3-062 2,4,ellulloropnend

3et.e.o 2-Fhwdiphent4

$7121 z+hfiqlErd

11d6jot N/itfu1?s'1e45

41f6{'-2 Ptwbl4s

t7t*i14 Tef,teryk4

11&t9i Z4,6TfuMnod1qd

SVOCS bv SW846 8270C SIM

Prepared by method SW8,+6 3510C

81324 Ac€napntEne

,08.96s Aafi\eohttyl€ne

sr2{ 1-tiddrlaghhatene

12V12-? Anfiracene5s5$il 8€n2o (a) sn$|lceneso324 Beizo (a) pyrene

h5.9+2 &nzo (b) iuorantEne1e('?+? Benzo lO,h,i) p€D'lme

?07{84 Benzo (k} lluo(anthene218-01.9 Chrysene53-703 oibenzo(Ah)anthric€oe2!6-.4,1{ Fl0oreaffi€ne0&7,7 Fbo|rn€193-3s.5 lnd€flo {1,2,}cdj pyr€ne

s1576 z-l"lehylnaphttd€ne9'-2G3 llaphftalen€

85'Oli Phenanhrur|€129.00{ Pyr6n€

a1&a z-Fnrefiatfl

t718514 faflErrj41

28{ar-07 3l.llar{7 71816{0 M.8BRLBfrL

BFLBRLBRL8RLBNLBNLBFLBNLBRI.8Rj.

BHL

BHL

67

vn100

8Fl-

BRL

BFL

BFL

8Ft

BRL

BRL

BFL

BRL

BNL

BFL

B8L

BRL

8RL

BRL

BNL

BFL

BFL

&)101

!s,1

tdl 1.m

|lg4 1.mp94 1.m

t!{t lm

!s, l.m

N,4 tm

lsn Lm

IS4 1.m

|4'l 1.m

|lsl lm

!S/f Lm

!91 1.00

!S,4 100

t4l 1.0{)

3$130 %l11 t0%*t30%trfi0%3F130 %t5-110%

rlsl 0.050

N, 0.0s0

|lg, 0-050

u91 0.050

US/r 0.050pC4 0.050

!S, 0.050

tiS4 0.(150

|4/r 0.(150

|Jg|,l 0.050

Ig1 0.050

M 0.60

Ug1 0.60

UEI 0.060

t{I 0.050pS4 0.050

I9l 01150

n-lil%tu|30%

sw845 €?70c

sa{8{6 8e70cGPA62sStM

s1t8it5 6010€

z$lrar-07I

1

I

I

I

I

I

I

I

I

I

l

1

I

I

1

Totrl Metrb by EPA 60001000 Serier M€tbodt

1445?24 Stv€r

7!rG393 Eadum

tn88L

BRL

8RL

n9[

ng,l

m9l

0.0050

oqxo

0.m50

3tlMar-07 @.AF.07 7m1823

Ihb hbotutoqE?o ls aot rali.t pilhout ot2 sulhoized sigMtlan od ahz cotw poge.

. Report ble Detecrion Limit BRL = Below ReportiEC Lirit Prge 98 ol 154

Page 684: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sample IdentificationFB.{sA59803- l9

Client Proiecr #l 0 t -88

MatrixBtank Watel

Collectiop Date/Time26-Mar-07 00:00

Rcceived2'7 Mar07

CAS Na Aholfta(s) FIoS A"is *RDL Llethod ReJ:, Prcpsred Anabzed Batch A,altst

Totrl Mcl|ls by EPA 6000/7000 Seri€s Merhao!

71.(l{34 Gdnim BffL

7,14!-473 Chrcmium BFL

7r39.C-r Lead BFL

m2+2 Sd€nium BRL

Tolrl M€lrls by EPA 200 Sedes Methods

74399|6 Merorry BRL

rnE

fi91

n]9,1

mgn

0@5

0.m50

0.0075

0.0i50

0.00@

SW81660108 3GMad7 A-Ap4/ lrB1\n LR

mq.l EPA245.lr470A :{-illar.07 02 N'{7 1031p4

This hhoratory repoa is not vd l withnct aE authoritpd sigaalwe on the coeet page.

' R€podabie Det€{tion Limir BRL = Below Reporting Limif Page 99 of 154

Page 685: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Sahple tdenrificationT84sA59803-20

Client Proiect #301 -88

Matd.rBlank Water

Collection Date/Time26-Mar{7 00:fi)

Received27-M^.-07

CAS No- ,lnolruls) n4sulr FIdS Aai6 'RDL Dilutia^ Llethod netr Prcpared Anallzpd Botch A!@fust

Volrlile Orga[ic Composnds

Volatilo Orcanic C,lllourlds bv SW846 82608

Prepa.ed by oFlhod SW846 5030 Water MS

7e131 l,I,2-friilorotdtluo.oehane(Fleon BffL6-r-6+r A€bn€ BnL107-13-1 AcrylcniHe BFL7t1V2 Berzine BRL

106.€6.1 BfttEb€nz€ie BRL744t-5 Brod|oct omm€$ane BRL7t2t4 Bomodk$toromethane BHL7t2u2 Bomoaom mL74.a99 B&moflehans BFL?ss-3 2€uunoie (MEK) BRL10451{ Fevtylbenzen€ BRL13&98-8 s€c.&rMb€ntBne BRI

BHL

BHL

BRL

BRL

BRI

8Rt

8Rr-

BNL

BFL

8RL

BRL

BRL

8RL

snlBNL

BFL

BRL

8RL

8RL

SRL

BRL

BFL

BRL

ERL

B8t

BBLgflL

BFL

BFI.

8RL

8FL

8RrBRLBRL

BFL

BHL

BRL

BflI-

|jg,l

Nl|aIps4

|ryr!s4

!s4lgl€4p9,|

ugr!s4lsrrlgl

lE4

wlr!'ltqll

tEl|4J|tdlwlttdl

!s4usiudll4/lI04ug/|us/rdrrlg/]lJgjl

ycn

|4lt

!9r!s/rlsips4

uE4p94

!c/r

lgrt,gl'llg/|

|Jg4

|lsl

udMIlsl'

1 0

20.0

0.5

t o

1 n

1_0

0.5

1 . 0

2.0

t0.0

1.0

t .0

1.0

5 0

1.0

1.0

2.0

1.0

2-O

1.0

1 . 0

2.0

0 5

t 0

1.0

1 . 0

1 . 0

2.0

1.0

t 0

t .0

t .0

1 . 0

1.0

1.0

t .0

t .0

0 5

0.sL0

0l

r 0 0

1.0

t .0

1.0

10.0

5.0

1.0

l_0

SWE46 E26OB 29.t erfl 8 n7 781791 8U

s&0&6 tefl,&nyjb€nzene75-1s{ C€bo.l disutfide5&23-5 Cabontetradltoridell)84c7 Chlorob€flZene754G3 Chloroehane6/6e3 Chtoidomj447.3 C1llordnehane!6-rs,8 Z-Chloro(du€ne10G,13-4 4{hhrolofu$€

$12-o 1.2-Dbrono3doropopane12141 oihro|nodioomshane10e9+4 l2-Dbrcmos{haie{E0€)

74€5,3 ObronFmethan€s5&1 l2-oicl{onctclEen€541-791 l,SoidtlotDbefu€neI06-4G7 1,+oidldob€nzere'is114

oidoodifluorcrn€hane(Freoniz)TrtA-1 t,1{)ichloodtan6

107{c2 t2-Did oro€dla]€75.3$4 1,1{icl{0rc€[Elt615$5+2 c6.1,2-Dic*orc€hen€156-€06 lfans.l2-oidtoo€herD7!-&/-s 1,2€ldtlo.opmpane112-2s-9 1,$Oi.|1loiopropane

*+N.r e2-DddooprcDane5d153€ l,l.Ochloaopropene1m61.01.5 cis.l,3oi1l|oopDpelsr06fil2i tra|rs-1,3{id{o&ptop€ns100:u-4 Ethylb€nzen€

6t-68i1 t{sEdoEb[dadene

591-78-6 2.Hexerone0,t8K)

98{2-8 Isopropyftonz€ieea.!7.0 +lsoplopttbtu€ne1$44,r-{ Mefiy'hnidytetlerrn8.1cr a-{,lethyl-A.pflbnorelfirgn

?s.o+e Mehylenedltodde

91-203 lhpnhdmo100-651 FPmpl/bfiz€ne

Thit lzborotdry rqort h not valld vlrhout aE arahorlz.d sigtdare on the cover page.

' ReporEbl€ Deaection Umit BRL = B€low Reporting Limir Page 100 of 154

Page 686: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Samole [dentificationTB-,1sA5980l-20

Client Proiect #301 -88

MatrixBlank Water

Collection Date/Time26-Mar-07 00:00

Reccivcd2l Mar07

CtS No- Analye(s) Result Fhs Ufii/5 *RDL Dilution Ne/ho.I Ret Prepdred AMIWd R.tkh Arulrst

Voltdle OrgNnic CoI[pounds

Volalile orcanic Cornoounds bv SWO46 82608

Prepared by method sw846 5030 watef Ms

1oo-42{ $rcie BRL

61020{ 1,1,1,2-Tetachtooethan€ 8RL

79-3,16 j,t,2,Z-Tetracl oroetham BRL121.181 TetrachlorD€herc 8RLr0€€&3 Tduens 8Ftc/s1$ 1,2,3-Trichtorbbeflzen€ 8RL120.!a-r jl,+Trichtoob€nzgne BRLir.5$ 1, t, j.Trcl./o/oshre BFL79{05 j,1,2-Trichtoro€hane BRL79{15 Tr*:hlor€frsne BRt75.69-l Td$torclbomrnethafle {Frcon 11) BRL$.16{ 1,2,}Idchtorcpopane BRL

s-€3{ 1,2,4-Tdrnebytbenzene BRL

1N47], 1,3,5-Idne0iylbenzene 8RL

75{l1rl Vinyicnbdde 8RL

133c2s7 m,p-Xytgne 8RL

s-{76 cxylene BRL

109s99 Tetahydrofu€n BRL

@-&t Ehyl eher BRL

9t4{5.€ fed-amylflEdrtt eitrer 8Rl

63?'92a? Etryt tert-buM ether BRLt@20-3 fi+oFopytdher BFL7s5{r Ted.Bubmt/ butylahohol BRL

w 1.0ps,t 1.0ps,4 0.5

trS4 r.0

us4 L0

}lg4 L0

LrS4 1.0

w 1.0

lsn r.0

PSn r.0

!S4 1.0

pS/ 1.0

!S{ 1.0

PSt, 1.0

ps, 1.0

psrl 2.0

rcn 1.0!S4 100

!s4 1.0

w 1.0

rcn 1.0

lsr 1.0

wn 10.0

!S,4 20.0

/0-130 %70-t30 %70-t3a %70130 %

st!846 82608

123€1 1 1,4-0ioxan€

1$@1 +Erdnohbr,bqzene

N?-265 tduene40

170d,474 l,2-Dichlotodlane44

1d655?/ Di'DtrDfluononethane

BRL

92103t10105

Thk laboru.orl rcpod ir not valid drhout ca dathorized l'/ig/|.a ne on the covr page.

* Repo.table Detection Limit BRL = Below Reporting Lim't Page l0 l of 154

Page 687: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtil€ Orgrtric Compounds - Quality Control

Barch 7031790 - SW846 503SA Soil {tow tevet)

tu rnEl?909tfi11

Popared & tualF€d: E-itar47

1,1,2'Trid omt ucroehano (Fr€on Il3l

B€nlene

Bomoform

z€ubnone {[GK)I}BIMb€nzena

sec4uMbenz6e

b.t€uryibenrsne

Carbcn di€uffide

Chloroehan€

Chlorolo.m

ChlordrstE'l€

24t{orohtuar6

1,2-DihDm'3{llorcpopane

0lDrcmocilorun€ttane

1 ,2-DiblolnoefEn€ (EoS)

Ddrdndn6!|ano

12{k*rc'obsl?€.r€

| +DinhxobsrzerE

1,+Dicnbrob€nzene

DiiJ orcdinuorurEhane lFreon12)1 .tDicnhosdune1 ,2.oicnbrcefiane

cis.r,2iichho€lh6i€

[en6l ,2.0i*kro€tEn61 2.oidlloropDpans

l.+Didboporan€

22.fid oroFqane

1 , nokhlo(opop€n€

cis-l3-olc orop|lp€ne

t-ar6-l,goicnioloFopen€

Ehy'b€rEene

H€Iadlhrobiadione

2+lqamn€ (lrBKl

lsoproAjbenrsns

UemM b.ttulyl 6h€i

+lr€M2.p€rteione (MIBK)

tlelvens d ofide

flaphhaleoo

Styr€n€

ARL

ARL

SRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

ARL

ORL

BRL

BRL

8RL

ARLgRt

aRI

aRt

BRL

BRL

BRL

BRL

BRL

BRL

BRI-

8RLgRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

8RL

aRl-

BRL

SRL

BRI

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

|lg|IS wst 5.0

|lgtS lrsl 100

|jgfig,^€l 5.0

tJ91S n€l 5.0

|lEAErel 5.0

lo,lg 161 50

IS,tS'Net 5.0

Nfi{gwst 5.0

t'gfig w€l 10.0

|,g4g trl s0.0

lJg/}g vrel 5-0

|lgtS i€r 5.0

UgrSrel t0

ldfq wel 25.0

tgkSv€t 5.0

Igtgu/el 5.0

lgtg u€l 10.0

lgfgvJal 50

UgtS wsr r00

ygtSrd 10

HYtsYrel 50

pstlqw€t 100

trytg$€t 5.0

|Jg/](! €l 5.0

lErS{'€1 s.0

$gldr,€l 50

llg.*S rsl 5.0

pgrs'.vel t0

|Jg/](g wel 10.0

|jg/|(S wet 5.0

|,gtg v€t 5.0

!$49 'r€l 5-0

tlgrs vlel 5 0

Hg*Sr/€l 50

pgA€ wsl 5.0

t€/tgr€l 5-0

pglqwel 5.0

llgA9 wst 5.0

|J{}rtS wet 5.0

lgtg Y/el 5.0

lEl0rdl 5.0

|4^gwal 5.0

llglrS rdt 50.0

|lgfrg wel 5.0

lglqwat 5.0

US"lqwst 5.0

|,g}swd s{1.0

|ldtS $61 50.0

WIS Y/€l 5-0

US4S wal 5I)

tlg/rs l.€| t0

Thit lzbordort rE ort is t ot valid fi'Uhoq an zathori@d sit taUe on lhc co!.t page-

+ R€Forlable Dct$tion Limit BRL = Belorl/ Reponing Limit Peg€ to2 of 154

Page 688: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compoulrds - Quality Colrtrol

Analyte{s) Resul t Flag Units .RDLSpike

Level

R}DLimit

Source %REC

Result %REC l-imits RPD

Brach 70317m - SW846 5015A Soil oow l€vel)

Elrnl aTlBlZl0€LKl I

PrBpaEd A Analyu€d: 29-Mad7

1,1,1Z.Tslrad orcefiano

1,1 22.T6trachtom€hane

Io[adt|fosf|€ne

l29T*J olod€nz€rE

r Z,{.Tftnbrct€nz€r€

I,1 ,l -Ticiloo€liarE

1,1 ,z-Tichlomshan€

Tdcn|orp€ttene

Tdci,lolbfl uc.onefi an6 (FI€m 1 I )l3$Tridlorqropam

l2+TdnE$y{b6nzene

l3FTdm€trrylbenz€{r€

VirV dlldid€

m*rxyiens

T€t"ltydolu'

E$ryl6t1q

Tsl{r'yl mery eh€r

E ryl hn bulyl st'€r

D-asopmpyl ehe.

TstB',{anol / t{tyl alcofiol

l+DioEra

Sarqab: 1at.,']{,fin'tr,tFnzefleSEt@: f&ate$gfiogelEj 1 2-9itttto@thaned4Sunq&: Dbrurolknw$hane

LCs ('ttsr ?9G8f r

Pre€arcd E Ans4z6d: 29-Mar.{7

l,1p.Trid{ootlff ljorosthan€ (Frcon 1 13)

Bgu€nt

SotuterEEne

Brcnoddlloronsh€ne

&flmfofln

Brqnon€fisn€

2€ulanon€ {LCK)n.8v!&enzena

sec€dll0€nzene

l6|i€tltlib€nrene

Cdtm dsilfde

Csbff bradtflide

Cltbo€ttne

O orolorln

chhromefEn€

2{trldollu€n€

{{hbor{L€n€

r3{ttfi o-3{,hlo0propane

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

ERL

BRL

BRL

BRL

BRL

BRL

55.258.4

2 0 4

13.7

2 r . 2

20_8' t t .1

18.9

22.9

19.8

20.8

14.4

17.A

11.7

r 8 5

1 7 8

1 9 8

17.S

17.8

2 0 4

20.2

17.8

19.1

16.f

pg4€ wel

pqfig v/et

pgfig s'et

pg,l(g viel

Pglg w€l

|lg]kgwel

lJg]l(s w€l

tiglg w€l

!g4g wel

ISAS wel

lSAg w€l

lSnq v€l

USAS wel

!s/rs v,/el

!s4s vrel

!94(S v€]

!SA! v€t

!A/l(S vJ€i

!Srl! wet

pg^S yret

pdk! yrei

rcI(S lvet

!S4S wel

pg4(S s/€4pg^0 v€l

lSnq vr€lUYlo v€l

pg/](sw€l

!9,t0 e/el

ljg,kg wet

pqi(g w€t

pgr(g w€t

pgts w€t

!S/tg wet

ldkg wet

ldkg wet

llgn(gwel

|.qftg wel

yen(g wst

ygtg rel

trgAs w6l

|lg,tS wel

US.4S YlBl

|/gl}S "€l

NAS vJel

lErg v€t

lsiks wel

!S/rO v€l

5.0

5 0

5 0

5i

5 0

5.0

5.0

5.0

5.0

5 0

5.0

t00

5.0

500

5.0

5-0

5.0

5.0

500

100

fi.050.050.050.0

105 m130flo n-130117 7Fli0fit 7et30

102 7F130

68 1n-175

106 70-1&

104 70-13!

E6 7F130

94 7G130

114 7G130

99 7G130

104 55.3t36

72 U.8-142

E9 7F130

88 7F130

92 7013{)

89 7t!13{

99 7F130

90 711130

89 55_1130

102 7S130

101 70.t3t)

89 7O.tA)

96 70rt0

E4 70131

20.020.02!.4

20.0

20.0

20.0

m.0

200

? 0 0

m.0

m_0

200

20.0

20.0

200

ml

m!20_0

200

20_0

m.0n.0

Thit labo&tnv report ir not t)zld Hithout an aathotiaed siCnalure on tha coyer page

+ Rcportable Detection Limit BRL = Below ReportiDg Limit Page 103 of 154

Page 689: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organlc Comporlds - Quallfy Control

Analyte{s) Result Flag Units +RDLSpike Source

Level Rcsutt %REC

7.RECLimits

RPDRPD Limit

Bstch 7031790 - swE{5 5035A Soil (hw levet)

l-cs ft6t7!xl86l I

Prcpared f Ana|}.edr 29.lrar{7

|,?OiDoflo€herE {EoA)0ikonlometErB

l,Slldhrob€nrene

1 ,+oid orch.nrElo

Dk$brldfl oo|Dlnehrne (F|9on12)

1,1{id{do€tlans

l20inbm€tuiE

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' Repo.lable Detcction Limit BRL = Bdow Reportiog Limit Pag€ l{X of 154

Page 690: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Conarol

Br.ch 70Jt790 - SW846 5015A Soit oow tev€,,

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Thb labonlor! reporl h ,tol rsIU without ofi oatho aed slgwturc on th4 corvr paqe

+ Reportable D€rection Linit BRL: Below Reporting Limit Pag€ 105 of 154

Page 691: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volstil€ Orgadc Compounds - Quslity Control

Analytqs) R€sult Flag Udits

Sour€e %RxC

Result '/.REC Limits.RDLSpik€LEvel

RPD

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r Rcportabl€ Det€ciioE Umit BRL = B€low Reportiqg Limit Page 106 of 154

Page 692: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgsnic Compoutrds - Quality Control

Spike

LcvclRssult FlaB

S$u.c€

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r R€portable Det€ction Limit BRL = Below Reporring Limrt Page 107 of 154

Page 693: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgrtric Compouods - Qurliay Cotrtrol

Analytds) R€iult Flag Units Resuk %REC Limits RPD

Brlch 703179 - SW8465030 Wrter MS

thrt fr(Bl797€L(l I

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104 7G130

101 ?G130

136 3.3167

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This ltbordory .epod h not vdid withotd an suthoriztd [email protected] on the coee, pqc_

I R€portable Derecdor Limit BRL = Bclow R4orting Limir Page 108 of 154

Page 694: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

\rolatile Organic Compounds - Qualiay Control

Spike Source %REC RPDAnelyt€G) Resutt Flag Units |RDL Levet Result %REC Limils RpD Limit

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+ Reportablc Detection Limit BRL = Below ReDonins Limit Page t09 of lJ4

Page 695: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volitil€ Orgenic Compourds - Qurlity Cotrarol

AnaLyteG) Result U$its

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Page 696: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volaaile Orgaric Compounds - eudity Control

Analye-(s) Rcsuk E lag Unitr .Rt)LSpike

Level

Source

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Page 697: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtil€ Organic Compounds - Qurlity Conarol

Analyte{t Result Fla8 Units +RDLSpike

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ThX hboftloryqo.l it not wld t' haul oa Mthoriatr 6tgnaur. oa the cover page

+ ReporEble Det€ction Limit BRL = B€low RoFrting Limit P.Ee I l2 of 154

Page 698: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compou||ds - Qurlity Conarol

turalyte(s) Result FlaB Result o/'REC*RDLUnits

SpikeLevet

% RECLimits

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1.0

1 0

1.0

1.0

l 0

2.0

1 0

1 0 0

1.0

1.0

t 0

i .0

r 0 0

200

1011t)tJ90

96

1 r 0

i09

107

112

1

1 1 1

o2

94

100

89

85

r06

99

r04

t05

105

t04

99

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1Q4

106

106

104

This labodory rcpod it not volid wirhoul an auhorAe.I sigt alare on th4 cowt page .+ Repodable Detecrion Limir BRL = Below ReDortine Limjr Page l l3 of 154

Page 699: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgrtric Compounds - Quality Control

Anallte(s) Resulr Flag Units rRDLSpiketevel RFD

RPDLimit

SourDe %REC

Resul. %REC Limits

Brtcb 70Jl8J0 - SW846 50J0 Soil (tigt l€vel)

LCS fi031030{Sifl

ft+'red e Amvlad: E.Mr.07

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z+lexsncne (iAK)

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1,+Oioxan8

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t C{l t}uo fiBr&F.BsDl I

20.3

20.4

19.5'19.1

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22.0

21.4

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20.4

20.4

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20.7

18_3

12_7

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22.7

21_5

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22.2

21.1

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23_6

20.4

20.7

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1S_8

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178

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pdrS s,€l

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|MS $/€l

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m020.0ft.0

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from.0,0.0,0.010.0m.0mN$.0$.0$-09.0

34.+r67

fl}130

7tI130

7G130

7G130

7D!30

70130

7G130

70-130

70-130

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70-r30

60,7n40

7S130

zllm

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7&131)( j .1n45

7G13I)

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7St30

70i30

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This labrcllrqt .cport h aot vdid nttou! on zaahorizrd sigrrttue on the cover p4ge,

i Reportable Detecliotr Limit BRL = Below Reporting Limit P€ge I 14 of 154

Page 700: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Spikc Source %REC RPI)Analt'teG) tusult Flag uoits *RDL Levet Resujr %R_EC Ljrnjrs RpD Lrntr

Batcb 703183'0- SW8{6 s030 Soit (high levet)ft€pgred t Anotyzed: 2$Uarr}7

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!S^S wet

lSlq wel

|rE4{S wel

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rclq wer

ldkg w€t

USAS w€l

p0IU wel

tSAg,Nei

ug^S u€l

lgAS uJet

!sa! rcr

lgtg Yiet

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uS,tS wel

lls/ts'rEl

lgfrg Bet

l]ql(gmr

ljs/rsmr

|Jq4q wer

!g/kg wer

!g/kq wer

UdiS v€l

!g/t(g sel

UEtg wel

!9r(S v€l

lgtS vr€i

pgrl(S $slpqtg w€l

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pgtq v,,el

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lslq $si

iryrs v€i

|Jg4q vl€l

lglS v,/€1

lJg4sv€lglS w€l

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lSfto wel

!s/kS w€tqc2 lgtg lwl

lglS v/et

UglS fl€l

lStS rcl

lgAs rvel

!SI(S w6l

UEIS vrel

|JgAsv.€l

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rrSftg yvst

20_0

20.0

20.0

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20.0

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N.0

20.0

2!.0

20_0

mn200

20.0

20.0

20.0

200

2{.0

t 0 0

20_0

20.0

20.0

20.0

20.0

20.0

20.0

20.0

20.0

20.0

20.0

zl.0

m.0

x.020.020.0

20.0

20.0

20.0

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2!.0

20.0

m.0

20.0

20.0

m.0m.020.0

n.0

90 ?ctm 4 25

52 1.77175 4 50

96 7D130 0 25

104 7F130 6 25

t06 7G130 3 25

104 70"130 3 25

106 7Gr30 6 25

111 7F130 0

10€ 55.S136 3 50

66 38.&142 0 50

80 70t30 ? 25

90 7GI30 4 25

96 7Gr30 4 25

88 70130 1 25

81 70.130 5 25

102 70t30 4 2s

92 55.3130 7 50

100 701130 4 25

97 7F130 I 25

100 7tr130 5

100 70-130 4 25

99 70-130 0 25

106 64.7-139 2 :O

111 70-130 A 25

t01 7G130 3 25

106 70-1m ? 25

102 7Ft30 4 25

102 7!-130 2 25

100 314.167 2 50

98 70130 4 25

95 7Gr30 3 25

8a 7E-r30 9 25

1@ ?11130 7 25

93 7G130 6 25

103 7G130 7 25

106 7q130 0.9 25

77 TVIU O 25

98 7G130 5 25

100 70130 2 25

104 i[130 1 25

r00 7s130 4 25

8E 60 7.140 4 50

64 70130 0 25

94 7G130 3 25

s2 7D130 4 25

99 7$tfi 3 25

91 16 r.r45 3 50

91 7G130 7 25

94 7G130 2 25

s1 7D130 6 25

r10 7G130 4 25

106 7A-130 2 25

Thh bbofarory Epoft b ,toa rolid tt ho4t 4n aallioriz.j signarurc on the cowr pge

i Repo.table D€tection Limit BRL = Below Reporting Limit Pase I 15 of lt'4

Page 701: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Voladle Organic Compounds - Quality Cootrol

Analyte(s) R€sult Flag Units R€suft %REC Li@ts

Brtch ?03lE3O- SW846 5030 Soil (high l€vel)

LCS Dl. ftlB183llBsol I

Pr€paBd I AnatF€d: E-{lr€r{7

|,122-Tst€droaoehane

Ie4.TrU oob€|lzsns

1 , t,l-Tdcnb!€fiane

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m,Fxyi€ne

Etryl etEr

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E ylbn-bry' €tr€r

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T*r€ubnor / buty' alcofid

l,+Oio€ne

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Pdt sott ooSlSf,trst)

Pr€par€d & tu$/zed: 29-lrar{7

B€nzsne

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t ,1-Dichloru€flgl€

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:rtk Splt Ouo ft@1830€ll

hEpared & Analfz€di 2SMarOT

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Sour!8: SA59E1+02

20118.818.918.71E.317.322.120.017.O23.1r9.520.214.240_621-31 9 120.1rg.419_516.01U1903t1.1n0269291

21.021.419_3

21.3g33 t76.1a 4

|lg/tg \tst

pg/kg $€l

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tiSAS dy!0tS d.y|4I(S drytlglq dry

a).0m.020.020_02n0

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[email protected]

m.0&.0m.020_0200

u.0$.03,'0fr.0

2

2

f

0.9

6

6

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5

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100 7G130

94 7G130

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98 70.130

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91 7F13t)

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106 7Gi30

96 7+130

t00 55-?t30

97 7l}1m

98 7&130

90 7F13{'

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95 3+rf6

10t m1301U 70-131)90 70-130lE 70.1n

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lot vI130t6 Titgp 7&tn98 7011J

r$ 70.130

r00 TGtglgii 70130

106 7tlr30

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21_6?2.120.421.122130331.827.78.5

Sourc€: SA5SEI3r@

881

8nL€FL8Rr.8Fr

BRT

B8L

BNL

BFLgffL

30s

0

30

N

na)3l

Brlch 70llE75 - SW8,t6 5010 Soll (high hvet)

ahnt a7altls4t-K

Prerd€d & Anaiz€d: 3GMar.07

This laboruto.r, ,eport Lr,tol wlid i'dhost aA aaho.lld sigtgturg ot th. @w. poge-

. Reportable Drtcctiotr Limit BRL = Bdow Reportine Lirnir Page I 16 of 154

Page 702: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volttile Organic Compounds - Quality Control

Analytdt Result Flug Uoits

Sourc€

Result %REC*RDLSpike

Levcl

%RECLimits

RPDLiInitRPD

Be.ct 7031875 - SWE46 s030 Soil (high tever)

Blrnt a/txlt?5.Blt(1 I

fir8pdEd I Ane@: m{ar{7

I,l 2.Tdd1lolgtiffuflE€nane (Freo.r I 13)

Adylmrtile

8&ilartsgrofiob€nu€n€

BofiodidblE|rE{lar€

Brdnobfin

2.eiaio$e (MEX)

n.8]ltb€nzeE

se8lnyD€nzsle

lsd4utyibenzsre

Carton disulfd€

Ca6on htachloide

Chlo.obenzene

Crhhf€oane

Chlo|b{ofln

24lo.obluene

1 2otosneldicropropane

fibronfiJdoomshan€

1 2.Dib.onefiane (EDB)

Dibromomelrane

lSDid oobenzone

l,SDrd orobsusne

i,,!Dichlorcbenzene

Dicfl odfl u.rom€fi ane (Freonl2)

I , Hlcn|oroemano

t,lficl ffrt|ane

I,l.llcilorosllsn€

a!.1 B.Oici,lcro€t1€n€ll8ns. | 2.oicnhro€lh€ne|,2{id oropopdr€

l,goid oropopane

2,a0ddl|o.opmldl€

l,l.Diir orop|op€n€

ct}l &Dichboprop€r€rans.t SDichlqop@€n€EhylDen2ene

z+lsxamne ([,!8K)

Itopropylbsnzsn€

4.lsoolQy'uudt€

M€'lit bn tuty4 etre.

4-Ll€ry1.2.p€lnanone {Mt8X)ti€qy'€n€ chtfide

ibplr$d€n€

SVi6ns

ARL

SRL

8RL

ARL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

ARL

BRL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

ARL

8RL

BRL

SRL

BRL

ARL

ARL

BRL

BRL

SRL

BRL

8RL

ARL

BRL

BRL

BRL

BRL

8RL

ARL

!S.49 wel | 0

!S,4S r,,El ?00

!S.4(S w6l 1.0

pg/|(g rel 1.0

lgrq Bel 1.0

llgn(gler 1.0

llg,1(S {el 1.0

lgnqBet 1.0

|J91(g yret 2.0

Ug,4qwet 10.0

UglS$€l 1.0

pSn(ow€l l0

pS,lq wel 10

pqn(g !,{€1 s 0

|Jg/tS v€l l-0

ll9rg$€l 1.0

lJgrs v/6i 2.0

l]g/tg wol L0

!S.4S Yrel 2.o

!S*S '/rsl 1-0

!c/rs wel 1 0

!S,4(S $el 20

pS,4(S wel 1 .0

US.4(S w€l 1 .0

llg&s rcl 1.0

fStS i.'el 10

!q,4(g l{el L0

!S/kS wet 1.0

US,*S ,'el 2.0

!9,*g u'el 1.0

pc4(q *el 10

|lg,/l(S wet 1.0

!S/kS wet 1.0

lgtg wel 1.0

lqrS wel 10

!q4S l'€l 1.0

p4.ts rel 1.0

pg/IS rcr 1.0

llg,4(S w€t 1.0

rrg4g wet 1.0

l]g.tgslet 1.0

llg,4(S {er 1.0

!S^q rel 10 0

pg4(S ml 1.0

|Jg/rSwd 1.0

ug.tS |€l 1 0

lJ94(S 5/el 10.0

lgtS wel 10.0

llg^9 Y{61 1.0

|lg/tS wet 1.0

lls/}S wd 1.0

Thir bborotor! rcW is ttol toud tttlhosl an sr.thorizel signalure oft te coeet page.

r Reportable Detection Limi( BRL = Below Repodng Limit Page I 17 of 154

Page 703: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volrtile Org|nic Compounds - Qu{lity Control

An"lyt€(t Resuh Flag iRDLUnitsSpiket evel

Source %REC

Resuk %REC LimitsRPD

RPD LifinI

Brtch 701lE75 - SW846 5030 Soll (high level)

BLnt ftool8rtBL(l I

Preparsd & Analyz€d: glusrry

I,l,l2.Tetrad orcehane

1, l2:-T€[adloroef 'ar€

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o-Xtsns

Tetsdrytoturan

E$yl €fri4(

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FJfM Bt-h,M ober

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Ten.8'rhd / bdyi akohol

Sufiogab: +BqnoluorcbeflErpS$t9gab: IdErEdSs,]li.oSeb: |2-tM arekne4ltulnSaE DiMtoMndr,alte

LCS ffrB|trlEstl

ft€par€d I Anda€d: e]',lar{7

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,{-Chlomblue{€

12-oihuncld{aoffo9aoe

BRL

BRL

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BRL

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BRL

BRL

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BRL

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aRf

ARL

8RL

BRL

BRL

BRL

8.64.08.5n.7

17.6

12.3

20.0

21.6

2t_1

2 1 . 9

21.4

13.8

16.2

r8.4

1S.g

21.1

16.0

19.5

20-4

20.9

20_0

m,51B.S

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|j91(s,,€lgS,lq tt€l

|lgl|(S $€l

|loksY/€l

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lIg,}Srv€l

!s/rs n€l

!S*S wd

|lgitS rcr

uo*grcrt4!tq wel

l€Itg sel

uglq wst

l4ACwol

ugftg wel

Igtg u€i

|Jg/](s s€t

WIS v€l

Ugl€ wd

EfrS wel

t84q r€t

|4ag rst

|lgfgv,st

!9r| w€l

|lgl{0 w6l

|lgllg v€l

|lg]ftg s€r

|l9*9"{€r

|lsisrcl

lgrg wel

t4k9',td

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t€|lq vr€t

li9x0 wsl

|Jgtg $€l

pEkg ln€l

l]gil(g v€t

|,glg v/€l

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tut3a

7S130

I n.175

70130

7t>13)

7!11)

?G1gl

7r1130

7G130

55.+rS

38-&r42

7013)

7D130

7&131)

70.t30

7G13)

ru13t)55.919)

7G130

7G130

7tlr30

7G13)

7+130

t.0

t .0

1.0

t 0

t 0

1 !

t_0

1.0

1.0

1.0

1.0

1.0

1.0

t .0

2nr.0! 0 0

t_0

1.0

t .0

1.0

1 0 0

A).0

fi,ofi.09.030.0

99979899

88

mt(x)ln6

t08

106

1mfi0

lo7

EI

w99

1S

m106

98

102

104

1m1m$1

200m.0m!20.0a).0200m.020.020.0m.0mom.0mnm.0m.0a)_0m.o20.0ft.020.0N.0m3

Thh bbordtary ?epoil k ,rot valiil tdlhout 4n a$rtoiql signdatE oa rhc orer poge.

I Reportable D€tection Limit BRL = Below Reponine LiEit Posc I l8 of 154

Page 704: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgahic Compounds - Quality Cotrtrol

Analyte(s) Result Flae UniLr *RDI,Source %REC

Result %REC Limils

Spik€t€vel

RPI)

Li 'n i tRID

Betch 70!1t75 - sn846 5010 soit {high levet,

[cs r0g1E7s.ast IPrepaGd & l^aked: 3trMar{7oibrDmod 6one$aner 2oihDmoe$ane Foa)Dib.dnoin€harE

I,aDid ombffzen€

13-I)icnbob€nz€ne

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I ,l.oichloro€Oan€

1 +Dhl oao€Oane

1,lllcl oroe$e4e

cb-l2-oicnhroehene

tsdrs-lz{hhJoro€fEne

1 ,2-tld o$gopane

I,Sudrlolwopins

2,ADid o{op'opane

|,fDid orogopene

cbn.$DiditroFop€ns

tralFl J.ucfloropopene

Ehylben2en6

2-HqarEll€ (tilP,|()

lsop.opylbe||!6ne

lllofi]r{ brt-bulyl €tter

4-lr€d!'tlp€{terone (Ml8K)

M€dtlsl€ dlcride

StyGne

1,1,12-TelradhrostEne

1,1,22.T€Fddnoro€har€

Tdracnlooeher|e

|3$ldc oDtenzen€

l2+TdJ o|rlhenuene

I,l,l-Trid om€han€

| ,l,2.Tr*Jdom€hans

TrhhlooolierE

Trhl'loofluo|crnotun€ (F|Eon 1 l)

I ,elTtidiorcCropan€

1 ,ecTnndrylDen2€r€

I,3,5-fihEfi9{lenzene

Yit dtlofljs

m,FXtsr€

GXYene

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fdl.emyiftshylst€r

Ehyl bn hiyl 6tl€r

tx'bogoffiol|€r

T€d€utard / bdyi elnhol

20.8

21.1

204

21.3

21.2

20.6'19.9

20_2

19.8

1 8 . 5

'r9.9

2 1 1

20.6

15.8

1 9 7

r 9 5

20.1

202

1 7 7

t 3 l

19_3

18_8

20_7

11.4

19.2

19.0

17.1

224

2 1 6

20.6

17.4

18,6

1 8 I

1 8 . 8

1t .6

21.4

20.0

17.O

23.4

20.4

20.4

18.5

41.4

21.8

16.5

2 1 4

14.7

20.1

1S_2

198

lgftg wet

!S4q w€t

pgll(s w€t

!g/rq ler

lgaq wet

$/rq wet

lsnq wer

|.€nq w€l

|4l4(gw€l

|al(s w€l

|a4s $et

!9(0 w€l

!9,19 wet

|Jgeqw€l

tgftg s€l

lgftS v,€r

Uglq wel

!9l(9 Yi€r

QCi lgr'l(q $el

!g4q wer

US,'kS w€l

l&lrg wet

lgftg wel

€ASsel

ugn(g wet

ug4(g w€t

llgts wel

lgeq Y/et

pgtg wet

Ug*g |ret

llgfrg ret

ISAS w€l

lgr{ N/et

fiAS wsl

!c4(s wer

lS.ftS w6l

Ms wel

udkswel

llg/kg wel

pg,kg !re1

ps4q r€1

lgtS w€l

lgas w€l

ug,lg w€l

!g/kg ei€r

!s4q wer

|.dlqr/er

!s,!q wet

1U 64.7-139

1116 70-130

!@ 7Gr30

106 70-t30

106 7G130

103 70-130

100 u4157

t01 7G130

99 ?G130

92 7G130

r07 7G130

r00 7G1n

106 7U130

103 7S130

79 7Gr30

98 7G130

98 7F130

100 70130

101 70130

88 60_7-140

66 70130

96 7Ur30

9{ 7Gr30

r04 7G t30

s7 461.115

96 7S130

% 70-1p

E6 7Gt30

112 7[130

108 7q130

r00 7Gt30

87 7G130

93 7G130

94 7G130

94 70130

68 70-130

1m 7Gt30

lm 7Gt30

85 56.&140

117 7&130

102 70-130

1U 70,|30

92 7F130

104 7G130

r09 70n30

92 7G130

107 dt.9130

94 7(}13t)

100 7F130

91 7}t3l)

s9 7tr130

20.020.0m020.020.020.0mimlJm020020040m_0m 0mo200

m_0

200

20n20.0m!200m 020.0200200n.020.020.020.020.0m.020.020020.020.020.020.0m.020.020.0240200,40 020.020.020.0mnmn2002m

This laboratory eporl Lt noa talid wAhoul aa rqthortzed signaturc on rte corer page

. Reportable Detection Limit BRI = Below Reporting Linit Pag€ l19of 154

Page 705: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Orgaoic Compounds - Quality Control

Analyt4s) Resul( Flag

Source

Resuh %REC.RDLUnits

Spike

Lcvcl

%RECLimits RPD

RPDLimit

Br.ch 7011t75 - SW846 s030 Soll (higb l€v€l)

LCS n03lAr5-A$)

Pr€pa€d & Arl8lyredi 30.Ma(17

1,+Dioffegrnog'&j +entuo&etAsgSu|"Sa/f;fdrdffiSr'jmagatd : t ?-D*lktbha1s44S$rqatE Etthtooffi$ondaE

LCS DUE f|tslE?t8EDl I

Pfspared & rnaFetr 3GMar{7

1,1l.TiJ orotituolefEre(Freofi 1t3)

Eenzene

8rofinlordone

BmmonE|ians

2-BuhnorE IME()n€d)4bsnzsls

s€c.€utyt€nre||e

C€|bofl dlsufrdg

Carbon bracircdde

0{oro€ha|€

Chlorofom

Chloon€t|ane

+chltro|6|ueo€

l2.DDmn}3dd6|oplopane

1 ,aDibrono€tEie (EoA)

Dibmnomsfiane

1 ,z.Did ombffz€no

1 ,yDKtisrhglzme

Dahlomdifr rorirn€flEne {F€dl I 2)

t,1.$€nb|EdtsE

t,Aoir orc€lullo

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c;n 2{kirdoedl€i€

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r 2'oifloopopsrs

|,3{it'torc0rDpatl€

2.lOititlso0.cp€ns

I,l.Did orwlpene

cbn,g0*r{0oprop€rB

bJle l.lDdiorofrop€no

EhylberEe||e

2-H.Ialons (MBK)

lsof.opylbenz€m

192

N.4249n 24.0

17.4

12.6

21.5

21,6

21-4

21.4

21.7

14.6

15_6

17,6'lg_8

1 7 4

15.7

20.7

19.2

20.0

20.3

19,1

19.6

20.4

21.7

22.4

20.7

21.1

20.5

20,3

r8.s19.5

19.2'17.9

20.8

r9_520,922.015.419.2

20.321.320_21 7 o14.5t8.5

!gr0 wel

ljgfi9 r/€l

llg,1S ael

lErg rd

llgftg "Bl

!040 $st

l]dkS 'ed

l.|g^gwel

99tg i€l

lclq 'fd

$S/tS{er

|lgtSwst

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|.€nq'.r€l

!9|(9 lrol

||g/|(g s€l

|lg1(g w€l

lglS $'El

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llgtg xel

t SIq rd

u0t9!|€r

US49 v'er

!Sn(S sr€l

|Jgfro,,vd

|Jg4S Y€l

llg]1S rsl

UE}S td

|,qlq r€l

ug/|(Swst

|jgkg erst

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!94(S (€l

lSIq Y€l

lgrg rEl

|,g4(S *d

lgfS t€l

!0/rs $bt

tJs/](gvlsr

|jgts wel

ISAS |€l

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l4r'rS wel

|.qlq rel

|lgtgr€l

!g/tg sst

200

3,"030.0fi.0fr.0

20.0m 0m.0a).020nm.0m.020.020.020.0m.0mom-0200A).0m.0m.0a).0MAm0m!m.on 020.0m.0m.020.0

nn2UON-020.020.020.06.0mlJ20.020-0200

20.020.020.020.0m.020.0

96 34.155

tlt 7L13096 70t3094 70t3t)97 7U130

EE 7F130

63 1-77.175

108 70-130

103 7(}130

108 7Dt30

1St 7S130

t07 70.130

!14 71113)

lm f6s136

73 3&8-112

78 7Sr30

EE 7lli30g.{ 7F130

87 7G130

78 7Gt30

104 70.tEl

96 563.10

100 711130

102 7t!130

96 7{t-130

98 n}13)

lm 7Gt30

r0€ u.7.18

112 7tr19)

t& 7llr30

1m 7&131)

1t2 70'13t)

1U 7G130

94 34.{167

9E 7Sr30

96 ft!19)

90 7llr30

10,1 7Fr30

9€ 7{}13{l

1U 7Gt3)

tlo 70.t30

n t$tn

06 7[130

r02 71131)

106 7G1Sl

101 70'1fl)

85 m.7t{n

72 7G130

92 7&',1!)

0

2

E

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0.9

5

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25

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a

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This ta.6orot4ry Eltort is not yolid Nirtou an aa[rorte{ siF @tE on tte cover psge.i Rcporbble Detection LiEit BRL: Below Reporting Lioir Page lmof 154

Page 706: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Vol,ttil€ Orgardc Compounds - Quality Cortrol

An€lyt€(s) R€sult Flas Units

Source %R-EC

Resuh %RlC Limits.RDLSpike

Level

RPDLimitRPD

B"tch 7031875 - Sw845 5010 Soil (high lcycl)

LCS D'io P6l8?5{SDl I

Pr€paGd & lrl€ir?edr 30{tla47

+lsopfopylduen€

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PGparEd & AmlF€d: $Mar-07

Ssrle{re

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srn|oga6j Tolth!*4fufig,/J: | ?Oti,Wra"e4{Surc4d€: f)tuudlwofidhane

Irtlr sofle Dl' 0lFr E75-[so1 |

P'eryed & Atafrzed' n4d47

B€rw€

&brob€nrdp

I,1-$cnbro€fien€

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18.0

2 1 1

1 9 _ 1

1 9 0

203

16.2

2 2 1

2 1 1

2 1 4

1 7 2'187

1 9 . 3

1 8 8

1 7 6

2 2 7

2 0 0

16.6

2 5 1'19 8

20.1

1 7 7

4 1 2

2 1 3

22.1

2 1 . 4

1 9 3

20.4

1 8 . 4

217

220

a 429.428,129.2

SoUEE: SA59E9t{l

g0 7F131)

106 7t!130

96 46.ln45

95 /G130

102 70'130

81 7013{

fio 7G13{

106 7G130

1A1 70130

86 70130

9{ 70-130

96 7G130

9.r /0J30

88 7F!30

114 70-130

100 70,130

83 56.&140

126 7F130

99 70 130

1@ IV\K

EE 7G!311

103 70130

106 7Gt30

110 70n30

107 65.'130

s6 7F!30

102 7G130

92 70130

10€ 7G13rl

110 3.4- t55

101 /tll3098 70t3494 701309/ 701fr

97 71t130

105 7G130

84 7F130

96 7t!130

97 7qll0

102 7U1UlU tv1fl92 70-13iJ10t 7G1U

104 7$130

l0€ 70130

95 7S130

104 7G130

20.4

2 1 . 8

1 9 0

20.7

p0ag wel

lSftg wel

IgAg w€l

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lig,rs wel

jrg,ks v,,el

pg^s w€i

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!grr0 Y€l

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tgas r€1

t}g*s r!€i

u0l! wel

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lgAS lvel

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N,lq *€l

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fgAg \{el

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u$,rq w€l

u91q w€lPg4q welYg4q w€l

El(q wet

P1rr|(grct

lgfig l^'et

!$aq wet

!g/rg tel

loag let

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lgrkS wei

20.0

20.0

20.0

20.0

m.0

200

m.020.0

20.0

20.0

20.0

20.0

n.020.0204m 0m.0m 02DA20_0m 0400m am.0200m 020.02002002mN.0u 0&.0$0

20020.020.0m.0m.0

fr.0fr.o300300

m.0200200a)-0

4

2

1 0

7

6

2

1

1

2

0

0

2

I

3

1

3

1 8

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2

2

l

9

25

25

50

25

25

25

25

25

25

25

25

25

25

25

?5

50

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?5

25

25

25

25

?5

25

25

25

19.4

2 1 . 0

16.9

1 9 2

1 9 4

?|0.730.927.730.3

Souftr: Etri98gl41

8AL

BBL

BFL

BBL

8FL

BRL

BRI

BBL

sRt

1

t2

8

30

N

30

This labo&tory rcport is not valid ttiahozt an althofized signzaure on lhe coyu page .

' Repodable D€t€ction Limit BRL = Below Reporting Limit Page 12l of 154

Page 707: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Voladle Orgrnic Compoutrds - Qudity Control

Analyre{s) Resull Flag

source %P.I.CResulr %REC LimirsUnit5 'RDL

slkeIrvel

RPDLiftitRPD

Brtch ?03 l87s - SwE46 5030 Soil (hisn ha€l)

Sdtrc!: llA5989lr0l

PrepaJed & AndF€d: elMar{7

Sunqab. {B@nonuototf,veneSulogaftf Tolu€rc$Sffiogabi l,z-Dic otultwE4aSunogdo: OiM)ordn$ane

Barch 704m17 - SWE46 50$ Soil (high rcvet)

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21.3fr.631.327.04.5

8RL

BRL

BRL

BRL

BRL

BRL

ARL

BRI

BRL

BRL

BRL

BRL

BRL

BRL

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ARL

BRI

BRL

BRL

BRL

ARL

BRL

BRf

ARLgRL

8Rl

BRL

BRL

BRL

BRL

ARL

BRL

8Rf

BRL

BRL

BRL

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ERL

SRL

BRL

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lgrg st€l

UgtS s€lllg^S {€t

EAg ta

lqlqs fd

ljgrS'/rsl II]

lgqS € 20.0

IEIS xd 1.0

|lglq {el |.0

Elqw€l 1.0

llg,|(Cwst 1ll

tlg/l(grt4l 1.0

!c/lq w€l 1.0

pdkS s,€l 2!

lSI'Slvd 103

ygrS id 1.0

tdks $l 1 0

pSilqw€t 1.0

lgrSw€t 5.0

tlg/t0v/61 1-0

|JgkS u/€i 10

|rytg Yle! 2n

!d*g'€l lO

lryrS f,d L0

ldlS*d l-0

t4kgx€t 1.0

l8,lq wol 2.0

ug,l{g wot 1.0

|JglxSl|el 1.0

|/g4q $,rl 1.0

|lglor,el lll

llg^{ lt,s| 1.0

l'grsxd 1.0

l{Iq wel 2.0

Hikg ftr 1.0

lSftgvtst 1.0

|lg/l(S wsl 1.0

|]g/](g $sl 1.0

lgfgY,€l li

|4^0 wd lI)

|jg/rS n6l Ii

I9&S nEt 1.0

l44qftt 1.0

lgllwet 1.0

tigfigwol 1.0

lgtS w8l 10

Msv'sl 13

lgrSvr€l 10.0

30!06

tutu9098

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Thb laboftlory rcpod ts aot rdid fithord on .athoriaei igdelure on thz coeer page.

' Reporhbl€ Det€ction Lirnit BRL = Belo{ Reporting Limit Page 122 of 154

Page 708: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Qurlity Cortrol

Analyt(s) Result Flag Units

Sourcc %REC

Result o;RIC l-imilsIRDLSpike

Level

R?D.RPD Limn

Brtch 7M)017 - SWE{6 5030 Soil (high ler et,

8l.n* Otxlx)l7.8LI1l

PGSarEd & Anal"€d: 02,Apd7

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BRL

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ARL

ARL

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sRl

28.629.532.4a 0

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22.8

22.9

20.6

21.6

246

22_4

26.0

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16.8

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20.3

23_3

gg4ig mt

lSftS wet

pg|tgwet

pgftg w€t

|,!n(q w€l

tigrq w€r

!0k! v'el

lgtg wel

!g,lq wel

lsas w€rlgilq \wl

lgrS w€]

t'g,ftsv.,erlSAg v€l

lsas rverpS*S vr8l

llgl}!.vet

!s,ts weryS,4S Yrel

|lgAS Y{el

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tS/rS {el

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lsas v/el

!S,4(S Y/el

!g/rg w6t

|lglrs y{€{

!c4(s v,€l

llg,4(s wer

us.4(s rEl

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lSAq welpsas r€rUS^S v€l

rc^S v/el

!S.4S Yr€l

!s/l(! rcr

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pgkss'€l

ugilg w€l

pglq vr€l

pq/kg wet

t .0

1.0

1.0

10.0

10.0

1-0

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1.0

1 0

t 0

1.0

l 0

1.0

1.0

t .0

1.0

t .0

1.0

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t_0

l_0

1.0

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t_0

lo0

1 0

1.0

t .0

t .0

10.0

20.0

u 030.030.0300

95 7G13070-130

1U 70t30113 70t30

r30 70130

114 1.17-175

r14 70t30

103 70.130

108 7tr130

123 7+130

112 7tr130

1t6 70t30

130 55&136

94 38.&142

94 7F130

97 7tI130

tm 7$13{)

116 7t I130

200

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Thit ,tbomlory rcpod ii ^oa vzlid nirhout M zartoized signalarc on the cover page.

I Repotuble Deteation Limit BRI- = B€low Reponing Limit PaEe 123 of 154

Page 709: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic ComporDds - Qualiay CoDtrol

Bc.ch 7M00r7 - sw846 5030 Soit (high t€vrl)

lcs r70a{x}17{sllft€Fsred & Ar€lyzed: 0A-&r-07

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Cl o|olofin

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22.622.720.719.620.320.020.722.922.222.422.323.O20.221.422.O

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tJgl(s *Et

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!s^s rJsl

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l.B{qrl!

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20.0

20.0

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20-0

m.o20.020.0n.0200mnNT20.0m!20.0a).020.0momnm.02U0$.0m.0m.020.0al.0m.0mn20.0200fl.0200m.020.020.020.0m!MTa).0

20.04.D

2 711130

100 ru-130

115 5 n30

1r7 7U130

116 7ur30

1d0 7}r3o

106 70-130

!m 7F130

110 64.7n3S'r(6 fll-t3)

106 70-130

r0 70130

106 7U130

110 70-130

lm 3{.4-167

1?2. 7G13{)

flr 70t3{t

t2t 7t}t3)

128 TGIO

ln 70130

110 7Gr30

to 70-130

1t8 711130

115 7GI30

112 fll-!3)

flE 7Gt3[

t06 78130

1{0 60 7. r10

78 7&i30

lm ru130

1m 7G131)

116 7G130

EE {6.11,15

t15 7Gr30

104 7Gi3l

85 7O130

113 7Fr30

114 70t 30

t0{ TFlg)

98 7D130'tv2 7Gt30

100 ?Gr31

r& 7Grtr)rr4 7Fr30111 7D130112 70.130112 56.&r()

5 711130

tot 7F13)

107 7Gr30110 7St30

This bnoralary Epora B Eat vdid ttlthost or. sxthoized sig tUe oa the cov€r poge.

+ Reportable Detectkm Limit BRL = Below ReportinC Limit Page 124 of 154

Page 710: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatile Organic Compounds - Quality Control

Spike

Lcvel

%REC

Limits

RPDLimit

Source

Result %REC

Bahh ?0{0017 - SwE{6 s030 Soil (high level)

LCA 0UO017-8611

Prep{ed & AnatFed: 02{pr{7

m,pXyhn€

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l,$Did ompropao€

4 3 522.221_624_218.223.82182 1 1172a 629.530.433.1

25.22 3 823.822_4

25.022.423.124.519.414.219.320_123120.122.O22.7

2 3 0'19.8

21.120.322.O21.f20.8

21 ,A22.120.824.1

24.025.624.222.221.4

!94(S llrel

!g/lg $€1

llg/tS rcl

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lgitg wel

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lgAS y€l

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rcIq wel

pSnq [€l

pgkq wel

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pgxg tYsr

lgeg t{et

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p!,'kq wet

pg/tg lr€t

lgl(g wet

|4&g wer

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llg,4(swer

tlg,4(sw€l

|4/rS $€l

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t 9ll(9 v'el

tq^g wet

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!sn$ r€t

llg,tg flel

MS r€l

i().0

20.0

20.0

20.0

m.0m.020.0

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200

304300fl.0fl.0

109 7q130

111 70 t30

r08 70 t30

12r 65_$130

9r 70130

119 70130

10s 70130

106 7S130

86 3+155

99 70-1&7F130

101 7&130110 /0-1W

126 7SI30

| l 9 1 7 7 . 1 ? 5

119 7G130

112 7013)'112 7G130

t2s 7G130

112 70,130

116 70 130

lE s5-$136

97 38.8142

itr.0

20.0

200

20.0

200

20.0

20.0

200

200

20_0

20.0

20.0

20.0

20.4

20.0

20.0

N.A

20.0

20.0

m_0

20.0

20.0

20.0

m.0

20.0

20.0

20.0

20.0

20.0

200

m_0

20.0

200

20!

m_0

20$

3

4

2

0

6

3

3

l

2

0

0 9

0.9

0.9

I

0

l

0

?

2

2

3

0

2

0.9

0.8

0

2

0.9

0

25

50

25

25

25

25

50

3l

%

25

25

25

25

?5

25

25

25

25

25

nl

25

25

25

25

25

25

70-130

96 70-t30

100 70130

116 7G130

100 7G130

110 7tlr30

114 55.9tff1

116 7t !130

1]s 7G13D

99 70130

t06 7G130

102 7Cr30

rr0 64.7-139

10a 70,130

r04 70-130

112 70.13i

1m 7G1O!

110 70-130

r04 34_4t6?

120 /tr130

112 7S130

120 7S130

128 701t0

12r 7G130

1r1 70t30

r07 ?G130

Thb labonlory rcpod is Aot vdd withtu! en aaho.izel sig,,atwe on the cover page.

' Reportable D€lection Limj( BRL = Below Reporting Limit Pag€ 125 of 154

Page 711: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volatil€ Orgrtric Compounds - Qualify Control

Anal]'te(s) Resulr FlaC Unitj

Spike

Lael

RPD

LimitRPD.RDLSouce o/.REC

Resuk %REC Limits

Batch 70400 17 - SW846 5030 Sotl (high l€vel)

LCS oup fiO300l7{EDl I

Pt€pared t tuslyred @-Apr47

?,z.Dichlooglpars

| ,r-0ldlorwop€rE

cjs.t,}k rlprnp€n€

fsrB-|.lDa oopop€n€

Et\y'b€Eene

2+loxanorE (l/ax]

+lsoF@ylbbe06

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Naphdulsfls

Strcn6

1,1,1,2-Tetrachloroehane

1,1 22-T€lrEd orc€han€

1 ,2,9Tnd o.obenz€ns

1.1 2-Tidlor!6heno

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1 ,a+TdnotitltenzF.r€

1 ,3,tlrime$tbenz€rE

Vinyldhdd€

m,Fxylen9

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DiisoprEpyt €0ter

T€n.Euhnol / bulyl atcohol

Snrq4E : 1 -atl'tio,fl uo robsnArEgnwdg: lolu s4gnogab: | zaic o@lnfie44gfiogaie: oihfit]{r'/ttfiont6dlE,ne

Iltfi sdrc flxat7{srl

PrEpar€d E An€@r (E.1Cr.07

EsEen€

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T.|IEE

Surog?/l: +&dnonuotMlz eg.n$,{€': Tdane$

23.222.922.324.021.520.016.120.119.723.,118.423120.017.3

21.3t9-6m.220.920.522.522.421822_524.120.42 r .621.843.022_422.O24.918.424.221.6

190u.3E23t5x?5

So0rc.i SAtgryl-tl

r9.418.1

22.520.7'18.8

30.9

t16 7G130

1t4 7Gr30

112 7+rC)

120 7[130

im 7F1g)

lm 60.7-14l)

m 7!1m

100 70.1s

90 TFtCl

117 7u130

94 46. r-145

116 7G130

r00 7G130

86 7S130

116 7Gr30

114 7D13I)

t6 7trr30

98 70.131)

r01 70n3)

1U TGiAl

102 7G130

112 70130

112 70-130

rm ru-14)ll2 56.814n

r20 7Gr30

1$2 70130

1d6 fl)130

10s 7tI130

110 7G1g)

ll2 7G130

flo 7Gr30

124 65+tgl

92 7G130

121 7Gr&)

lm ru.130

fl6 70.130

95 34.155

101 7Flfr97 70-1Ut6 7&1Nfiz 7V130

97 7G130

04 ?&t30

112 7F130g0 7}r3l)

9,1 711130

t8 7FlfitE 7F1g

!s,'le ll€l

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!9I0 rsl

|4ftg vr€l

!910 rrsl

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ts4swl

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Eylq rel

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|Jgfts 5,€l

!9rS i'sl

llgltq st

tiCftS s€t

l4lq wst

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tls^(s|d

t{,\9xd

llg/kgml

!g/tg mt

Ugrq wet

pg'rSwel

|jgrS v€l

| l s 4 s d

lgtS wel

pg&g $rt

l€{€ virt

p{Es vrel

|,g/tg vr€l

lls4s wel

lJsAS w6l!g/lq |'6l

|lg/tSx€t

lElS dry

rErs drylStS dry

lgrS dry

lSIq dry

lclq d'yli9tg dl

20020.0

m.020.020.020.020.020im.020020020.020.020.0m.0a).0m.0a).02n.0m020!a).0m.0&.020.0m_0m 020.020-040.020.020.0mnm-020.0m-0200

2m9.0n.09.0fi0

m.020.0mt20i20-0300$ 0

2

0.9

0

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2

0

3

0

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0s7

0.9403020I

22

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0.90s0.90{22I

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E

25

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25

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6

25

25

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25

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25

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z5

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a252525

8FL

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Thi6 leborutory eporl h Aal aoli.! wuhou aE oEttonel slgnslt.. oa rte cowr psge-

+ Repodible Det€ction Limit BRL = Below Reporting Limit Page | 26 of | 54

Page 712: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Volaaile Organic Compounds - Quality Control

Analyte(s) Resutt Fjap Units *RDLSpike

I*ecl

RPT)Lirnit

Source %REC

R€sult %RDC Limits RID

Brt h 70{0017 - sw846 5030 Soil (high lev€r)

Ilt|I5!t owl)l7.flSl)

Pcpar€d & tuatE€t @'A[r{7

Sutqzb : 1,2-0tibr@lhanees!firyb: oibranoluidnehane

tluh sdt D|Jd 0IX{xI7.xsD1l

Rrpeed & lrl3lnod @-Apr{7

8s!zm€

O oroh€n:€n€

I,lojdroroefrera

Tofuslre

Tri{r cio€tiene

Suto{,d3j4atdnotuottunzeneS/!'.'!€,,b: rotuane48SUN9,&: | 2.tthlro!@thane44Stl'logetr: offiudondhane

Sourcer SA59@h 1

Soulc€r SA5989l 1

21926624222.430.5in.4n.0i29

Mgdtl!S4S dry

llg4S dry

lSAg dry

aM7 wkgdry

lElS dry

!s^s dry

ls^s dry

lgfts dry

ls^s drylglg dry

s0.030.0

1Nfi2

112

0

107

112

102101931 t 0

30

30

30

30

30

7619701W

70n30 14

70t3{ 16

70130 17

7G13! 17

70-130 17

7G13070t307t+t3078t30

aaLg8L

88!

219

sRr

20.0

2DA

2D,D

200

20_0

N.AgJ.a

u au a

Thk lobonlory repo.t k trot vd6 flilhoul on aalhorized signaturc on thz cot'e! page

+ Repodabl€ Det€{tion Limit BRL = Below Reporting l,imit PzEe tZ1 ot 154

Page 713: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Exarachble P€troleum llydrocarbons - Quality Cootrol

Aralyt€(s) Result Flag Units Result %REC Linits

Bstch 7031722 - SWt4635l0C

ELnt fl03lm.OLK|l

Pr€pare{: 2$l\ler.07 Ala zed: g)-lrar'07

Ge.olin6

Frd Olf2

Frd Ol14

Ff lOl{6

Molor Ol

thid€nt'fied

Oll€r Ot

ToEl Pstd€(ln tly(loca'taE

C$C36 l,Iphdic tlydocaitEnsgfiqab:lA@dE

LCS tTIBl f4.8Sl)

Pr@r€d: 281i1347 AElyred: 3o-tlar{7

CS{36 Alpiadc Htd&caltans

s/l7,q,ata: l.gtutffiddcaft

Drtch ?03 l?72 - SW846 35508

8E1k O0l17z{Ll(ll

PreFredr ?9 aO7 &e!zed: 3Hi&r{?

Gasdin€

Fueloil#2

Foel Otr t4

F0sl Ol 16

Molor Oil

lli{tglffird

Otrsr Ol

Tolal Pefol€un fi ydrocartoni

CgC36 Afitiatic Hydruc€rbaE

SUqWAE' 14hlotffin

LCS ff€l?n€Slt

Pr€pared: zg{arfi lrulvred: 30lil"r{7

CgC36 Al(ot'a|jc rwoca,to|ls

Swogab:1$ sffica,p

q.ncds fr03lTz-0tPt)

Pla9ar6d: 2$t art Arulf!8d 30.tta{7

Gasdk\e

FLd Ot f2

Fii€l Oil 14

FilelOl 16

Molo.oil

Ur*lstr€d

Ot€r Ct

Tdal Pgtdoon tt(loartort'q}C36 Aiphdic HyfiEbdls

Swrc{aPjl.d1bo(t',de:;dE

lstk Sd6 fr031z2{61)

Pr€Fe(l Z$Mar{7 tudyr€d: C}.t arfl

BRL

BRLgRL

ARL

SRL

BRL

BRL

BRL

BRL

BRL

0.K3

1 . 1

o1ltr5

ow

1.10

o6m

10-t10

sl20tu129

0.05

0.05

005

035

005

0.05

oD5

0.05

0.05

0.05

'r'dl

mc/tnrElnEnsrrnS/lrndlms4mgilmg4i'E]

n'St

ngl

mS/rS w6l

rr4/tg rd

msnq v€l

mdlq w€l

mglq wot

flrS,lq *ol

ngtg |r€l

ngkq w€l

'ns/krld

rng4g ad

mglq wst

ttBtg sd

ndlq fiy

n4h dy

'Igbdv

m94q diy

mc q4v

nrglg dry

n'Srq drl

nglq dry

rnsrq dryJ,aM4 oElqdy

'rElq d]

ts8 l

BRL

BRI,

BRL

BRL

BRL

BRL

SRL

BRLgRL

ARL

2A

69.7

2.63

soulEe sa5g?u!20

BRL

SRL

BRL

BRL

BRL

ARL

BRL

eRl

BRI

25.2

J.59

Sourc.i Sl59?8Glt

1 3 3

r3.J

t13

13.3

r33

13.3

13.3

13.3

13.3

t3l

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qIlm

ffi.tm

n

nr3.3 s3.3

3.33

38.1

341

3 8 1

3 8 1

:t8.1

38.1

38.1

38.1

38.1

6-1

BFL

88r8AI

8Rt

BBI.

BRL

n. l

8RL

n,1

n.1

50g

505t)50505050cl50

Thb lobo$lory Eport b not t)oud *ilhod ot tuhottzd dgr4tyE on the covef page.

+ R@rtable Der€dion Limit BRL = B.low R€porting Linit P|ge 128 of 154

Page 714: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

f,xtrrctable Petroleum Hydrocarbons - Quality Control

Annlr€(t Result FIag UniLs

Sourc€

Resul( %REC.RDI,Spike

I rvcl

%RECLimits RPD

RID

Limit

Bitch 703 U?2 - SW846 35508

ll|ttr Sdke t6l?n {St }

PreparEd:2g- O7 Amtzed:30- aF07

CgC36 Arphdic Mro€ddrs&n@: tQ ot(frbdecaE

*o0ir Sdfte D|lo O6trn-mfi )

Pt€{.q'€d: 2g{r',xof ttdyzed: ?fr+"htn7

CSC36 Aliphdii Hyd|m€Ao{ls

tunr8ale: l{/no/off,frdecat a

Brlch 7031773 - SW8-16 35508

8b1t OtslII+aIXt )

Prep8rE(t 29+lar-07 &alyz€d: 3SMar47

GeEdins

Fud Ol S2

Frr€l Ofl {.{

Frrd Oit 16

L.!ob.0r

Unid*!fi€d

O$€r 0l

Totbl PrftlewnUydlrtr,n,t|6

C+C36 Atphalic ttdocado,ls

S.nn@E:laroftxtudecarc

Lcs frtsl7t18lt1t

Pr€pend:2$ ar{7 Ala}rled: 30+4ad7

C!}C36 Alphatc tl!/drc.stom

snncg8l€: t{ll/ofteadearc

lluDfic.ie {mrz+txptl

PeparBd: 29ilar{7 tualr2€C 3O-Mar-07

Gasolir€

Fd or 12

Frrd 0{ 14

FrDlOl t6

Mob. ol

thiienffed

O$s 0l

Totd P€tol6({n tfidocaDons

Cg.c36 Aliptslic Hldroc€rbons

tur'gsb:i'j@arE

t.tk S6lla OoSfIil}{SD

Pr6t€rbd: 291{ar-07 lnalFsdr 3CMar-07

CA{36 Aliphdk l{ydrsbofts

&nr.get6| l4t1bkffidearc

Sourc€: 5A5078&28

1.t9

3.79

Sdrrc€: SA5S78&28

aM2 6gq6o

mgt€ dy

OM2 nrdkg d/y

mdkS d]

30 5+150

4+140

26 50150

82 4G140

19.6

19.5

138

1.91

1 1 3

4.01

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ERL

BRL

?43

8 5 1

381

SouE€: S'A59807-11

216

5 W

rng/rc v'€rmgnq w€l

mq,'lq rvel

mg/kq wel

m!/kg wel

|ltgftg wel

nu/kq $€l

rnq/kq wel

Il)g*g r|€l

rig,lq Yr€l

rigftg v'€l

riqkg w€t

rngil(g ret

mgks dry

ftEIq dry

rnsas dry

ry/rs dtynVrS dryfngkg dry

nW4(S dry

i'S.4S dry

ms/ks drymslq dry

so2 mg,kg dry

hq/l(g drys02 lnsnq dry

mqts drys02 ndrgdry

n 4G140

91 @120

14 60.tn

13.3

t3.3

t3.3

13.3

13J

13.3

t3.3

t3.3

13.3

13J

137

L W

933l3l

BRL

BRL

ARL

Cal.trilaled as

BRL

BRL

121

BRL

121

121

4.53

sourcl: sA59807.1 1

1S5

5.49

Sclrcsr SAS)801-ll

23.1

23.1

23.1

23.1

23.1

23.1

23.1

n 121.1

u l

BNL

BflL

BRL

BRL

BRL

BBL

1 1 3

EfiI

l 1 3

1 1 3

50

50

50

50

50

50

50

l 0 l

360

tQ2

164

101

3.&

8 I

152

4+144

5Gt50

40141)

5G150 n

4G110

ft€pirodi 29tlar-07 Anatrred: 3&llar{7

Cg+S Aldtali: MmcaJborlsglzc4'&j ftlhtwbdacare

This laboraory ppod is ttot ralid ntithou an ltho zed si9nat re oa lhz cover page.

* Reportable Detection Limit BRL = Below Reporting Limit Page 129 of 154

Page 715: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivoladl€ Orgrnic Compounds by GC - Quality Cotrtrol

Analyte(s) ResultSpikekvel RPD

RPDLimitFlag Unirs .R'L

Source %REC

Resuft %REC Limits

Botch 7031738 - Sw845 3545A

Ahnkruti|€{LKl)

Ple9aftit 2&Mar{? Amlyled: zS-M{t{7

PCB r0r6

PCg re1

PCB t232

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ru 1254PC812fl)

rc812e

Ftr81268

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t-Gs l7)3t?ti84str)

ft€per€d: 28-Msr{ AtEgzed: 2g+{ad7

PCg 1016

rcB 12mSw'og2re: 1,+0ee6L0tu1plwyl l9t)sanllg'F: Dead1/o.o&prE/l,/ (Sn

LCS Dlo O0l1?!8.8SDl I

Pegated: 2&Mer{7 lrutyred; i,9-{ar.07

PC8 r0r6

PCA 1260

Surogala: 4,4nU)cbt$!WW $t)Sul48eb'0€fldr/Iqd.'fy]tl(Sl

DLfl c.i! a?u}t?itt-c|JPlI

Prepa€d: 28-li4a,{7 A|sfFen: C}ti{ar{

PCB 1016

PC81221

FC81232

Pffi 12!B

PCB 1248

PCB 1254

rcB 12Sl

PCB 1262

rc8 1288

sj't,lgg,ltrj4+o&+fr&dipw(St)Sr!'7c{,ab:D@dWWl(St

l'ti-r Solt aruollm,tsl)

P|epared: 2$Ma'fl ftdyr€d: Cluar{7

PCA 1016

rcB 1260

suwate. l,l 4E ocwndiptwvt (stSutt.g?b: ,€fl/dtlot@Istft $4

Irtk 30fi. O! OtEtTiE||Sol I

F!paEd::eM€r{7 Analy!6d: ?O r|-{I/

PCA 1016

PCa 1260gnostut4,+l'lffifr,@(Si

Sw@:W1tt(s)

Birch 703 U39 . SW8.l6 3S45A

aRf

BRL

ARL

ARL

BRI

ARL

BRL

ARL

SRL

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920

980

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Sour* 5159€&16

888

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47.7ffi.1

s.uft+ Elsg0&tf

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45.4767

l9/lS're|ygtg irl

!g/I4 rll

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pdkg wet

|ls/I(Swst

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!gr0 r/6l

|ryro u,B

l4'|(s$el

|,c/l(g*t

|]grssl|jg}O|6I

|4& rd

la/tglrEtlgtg rotHiq \rgt

vdls ev

lSfq drr

lsrq fiY

lto9€ ev

Krq dry

!S,|(g dty

llgtSdrywtc dv

|,gtsf}ldrs d)'Ug*g dry

Itrkgdt)rc,tg dry

{9rS dty|lgkg dv

|Js^s drv

rdrs dly

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&1W30P150

66.7

66.7

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667

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114 (}1{1)

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66.7

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8Rr

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8RL

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6t.6

6E.6

66-6

58.6

606

68.6

66.6

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10

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40

40

68.r

69.8

69t

68.5

851

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8RL

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104 4S110

113 lGr{l

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5050

10813)

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Thb Is&orolo.f Rport is not v6lilt nilttoat tn surrotl?att dgrrrtore oE the caver i?qe.. Repfitable Der€crioo Limit BRL = Below R€poding Limit Pa€e | 30 of | 54

Page 716: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mivolatile Organic Compounds by GC - Quality Control

Analyre(s) Resulr Ftag Units *RDLSpjke

L€vel

RPI)

Limi t

Source %RtrCResult %RfC Limits RPD

Brrch 7031739 - SWE46 3545AElalt floll?i)&8LKt t

Pt€par€di 28-titu-07 A,arfledr 02-Atr{7

attin

.€tlc

b€ricd0frcg-BfE (undanrl

Oftrdan€4,{ .D00 {p,p )4,{ .D0E (p,pl

4.4{DT{p,p')oioldrhEJd.6dhn I

Endcdil€n (

EndG{lhn Sulhle

Endrin

E '6i'l Aldelyda

fi€pladrlor

H€flhd or Epoide

a{tiodane

godoltan.

Endin Kebn€

tu'!g,e: l,4DE ebihnwlyl (St)tu/ogdE:Mnotwlgvlsn

LCS ft8t t3+Esil I

Pripdrd 2&Mart Analfredr 02-Apr.07

Alddn

a€HC

b-8HC

d.BHC

g.Bllc {undara)4,4{DD {p,p)4.4{0E hpl4,4{DT (p,pl

Di€ldin

Endditun I

Efitrdilan tl

Erdrdrlhn Sdfate

Edrn

Endft Alderrydo

tl€pEdrk

fre[Fryd{or

Hepb.tlor Epoxil€

a4ih(la|€

gc| 0.6r€

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LCS D|D n0fi739€Sotl

Prqa€d: 28.ai4sr{7 lrarf.€dr oz-Aprfl

Allln

BRL

BRL

BRL

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BRL

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BRL

BRL

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BRL

BRL

BRL

BRL

3 1 7526

59.4

53.4

5.4.2

22.O

54.6

62.1

56.9

55_S

58.9

6 1 _ 6

5 0 9

5 6 3

6 4 2

62.4

5 9 6

69.0

406

58.4

33.4

331

33.4

33.4

3?.4

167

33_4

33.4

33.4

33.4

33.4

33.4

33.4

33..4

33.4

33.4

334

333

167

33.1

33.4

33_4

33.4

33.4

334

33.4

33.4

33.4

33.4

$.,q

33.4

3C.4

33,1

33.4

334

33.4

33.4

33.4

33_4

334

33.4

66.7

66.7

66.7

66.7

6.1

56.7

6 6 7

66.7

66J

667

667

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66J

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66.7

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a2

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88

92

76

u96

94

94

89

88

85

103

39

l,g4(S v/ei

lsas 5/el

fglS wel

!S/rS rct

lgftg wet

p91q r€t

|8aq w€t

lgnq set

ru,rlq wet

|lg^q oel

pg4(S wel

|'gks rvet

lErS |/el

loilg r€l

ISAS *€l

!g/tg wel

Ilg,tswer

llg,frgwt

pq,rg wer

lgtg w€t

yglq v'st

!g^q wet

lgxg w€r

ug,lq vr€l

p9t9 wel

z2a !SI(S u€l

ps4(s vJel

p0lq w€l

|lgfts,v€lpgksv€t

uolq Y€l

|Jg4(S u/et

W4(S rcl

lElS v€t

lgfrg wel

lErS wel

lJgfrS "elmAS rcl

!S4(S wet

pVlS v'Bl

USAg wel

lls^s wd

!S.tS wel

lSAq v.€l

Ilg/rs r€l

ffi,7

6./

g>150

34150

4G140.{0-140

1&110

rl{l-1,10

4G140

44-140

40.140

1+140

4+ro

4+r40

40.140

4+r40

4o.140

4o.140

&14n

4S1'11)

4G140

40141)

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40.14{)

&1fl3&1fl

4t!14088 T

Thb laborqo,r rcpor. is not vald wirhoo an autho;zed signatte on the cover page-

' Reponable Detection Limit BRL = B€low R€parting Lihit Page l l l of 154

Page 717: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

S€mivolstlle Organic Compounds by cC - Quality Cortrol

AnalyteG) R€sult Flag Units .R-DLSpik€Level

RPDLimit

Source o/oREC

Result %REc Limits RPD

Batch 70J1739 - SW8463545A

tcs tuo ar(Btn+asol I

P@parod: 28.M.rfi tuallyz€d: m'Apr{7

a-BHC

b+fic

d€Hc

SS|C (Undan€)

4,4'.DDD(p,p)

4,4r0DE (p,p ) .{.DDl b,p'JIlddrin

Endosdta I

Endoeulhn ll

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Enddn

Endnn Aldef'yde

rlspbd'lor

Haphchlor E oxid€

a{hlordane

!q oturc

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Surogale: 1,1-DB-ehfluotfiiflEnt (50Swqate: Dacachtotdtpll€nl 6 t

E llc€te fiofl7le.DuPll

t'rEpercd: 28-li.ter{7 &alf.ed: O-Apr1)?

atddn

a{HC

b€Hc

d+tic

gAHC (l-intarF)

4JrDoD(p,Cl

4,4roDE {pp'),4,4r00T(p,p)

Ihdm

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Eldo6ulhn $/hb

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PEp€r€dz1- ar.07 Anryred: @-Apd}7

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a€tc

52.254.921.2

5e.456_9

55.363.159.051 356. t59.762.961.360.457.357.365.8u5

Sdrto: SA5l80+ro

BRL

BRL

BRL

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SRL

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9.163.5

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lCtS dryggts dy

usl€ dry

lglq dry

fs'lq drvpgtc fy

llc,tsd,|lgrs fiy

tlgtsdry

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Th:jJ bhtnrory repon it Eot volful l'dlto4 aI uthoized sigttaure on lhe coee, page_

'Repoftble Det€ction Limit BRL= Betow Repodng Limit Prge 132 of 154

Page 718: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolrtile Organlc Compounds by GC - Quality Cotrtrol

Spike Source %RgC RPDAnalyte(t Resul( FLag Units +RDt- Levet Resulr %REC Limits RpD Limit

ANlcfr 70Jlflt - Sw816 J5{5A

Irtk SotG O03l 7lI9{S | |

P|Epared: 28{ft r{7 Analyzed: @.fu r.0?

bgrcd+Hcg€HC (tinftna)

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54_4

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5 3 5

56.1

56.3

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267

56.5

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57.7

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57.5

56.6

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13.6678

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lsAs dry

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lsns dry

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lsnq dy

lg,rks drypglq drypqts drypvts drypSl(g dry

lgrs drypges drv

!s/ks dry

|]gISdrylgrs dry

!g,k dry

|ls^o &v

|ls/I(s dry

|lgrs dry

lyrg dryC[j,{7 lgtq dryu7 WAtl

|lgl(sdryorv!7 pg,ftg dry

ps/rs fivpgrs dry

Ugrg dryps4s dry

|jc4(s drvpsrl(g eypglq dvpgts fiv

30-150

30-r50

3Cr50

30,150

3GI50

3&150

3&150

3S150

30150

30t50

3G150

3F150

31I150

ml50

3GI50

3GI50

3S150

3G150

3+1fi3+t50

3{}t5l 2 30

3l-t3l I 30

3G150 4 30

3G150 6 30

30t31 0 30

3G150 5 t0

3G150 4 30

30t50 5 30

30150 6 m

slt50 6 30

3S150 14 30

3S150 5s 30

3!150 9 30

30.150 60 30

3qr50 1 30

30-150 19 30

3tlt50 5 30

3&150 7 50

30t50 2 50

30-150 41 50

fi-t@341fl

61.0

5 0 5

56.7

22.1

5 3 6

5 8 9

58.6

72.5

5 7 9

62_4

5 9 9

464

62_1

44.0

6 3 2

7 0 1

62.6

6 1 7

58.1

69.0

4 1 5N 4

35_0

35_0

35.0

3 5 0

3 5 0

35.0

35.0

35.0

35.0

35.0

35.0

35.0

35.0

35.0

35.0

35.0

35.0

35.0

59_9

60.9

6 9 9

69.9

69.9

69.9

69.9

69.9

6S.9

69.S

69.9

69.9

69.9

69.9

69.9

m.9

69S

69969.9

69.9

69.9

69.9

699

69.9

69-9

699

69.9

69.9

699

699

69.9

699

699

69.9

599

59.9

699

699

693

69.9699

BRL

BHL

8fl1

8fl1

BffL

8RL

88L

BRL

aBt

aat

8AL

88r

BRL

BRL

BBL

BBL

SRL

BFI

78

30

80

99

84

55

3E

B I

w

89

83

06

82

€l

65

6297

BRI-

8FL

BRL

BflI-

8RL

BRL

BRL

8RL

BFL

BRL

BRL

8Br

BRL

BRL

BRT

BBL

BRT

BNL

BRL

BRT

35_0

350

35.0

350

35.0

350

35.0

35.0

35_0

350

x5.0

350

350

35-0

350

350

350

35.0

35.0

35.0

87

72

81

17

84

84

104

83

E9

86

B9

63

90

100

90

88

93

5999

BRLBRLBRL

001m0.010000100

t]d.u9t!crl

Thir ltbo.alo4 repo.l it nol vrlu withotd sE aathoized sigaalure oa the coeer FaEe' Reportable D€t€ction Limit BRL = Below R€porting Limit Page 13! of 154

Page 719: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - Qur[ty CorFol

Spike Sourc€

Brtcb 7031?68 - SW84615l0C

t|mk mtsI76&Bt xrl

PlFarcd & Analyred: A.fiar{7

+8rc

q-BHC (Udan€)

Ctto.dan€

4,4500 (p,p ).1,4'-DDE(p,p')

4,4'.D0T(p,p')

Oiettin

Endosulfin I

Etthsuian ll

Endo$lhn Sulhb

Endin

Erdrh AH€hyd€

Heptadbr

Hepradtcr Epoxide

a-CliodarE

0{hlddansEnddr f,ebn

Stflogabi 4,4-0&&iaitso66Fn€ny' {S4Surrog€,b:Dec?dlorolbhar (St

lcs fn3r 76&8stl

P@9ar€d & Analadi 2+Mad7

Alddn

aftlc

tsBHC

dfatc

s€fic (Uodar€J

4,4LmDh,C)

4daDOE (9,p')

4,4!DDT (p,C)

Di4drn

Endoslhn ll

Enddilan Sdbh

Enddn

hdin Albntd€

HoPlacfla.

H€pbcr'|ol qodd€

a{t{odarc

g{hlord€n6

Endlh Xehn€

Sutog'dd, 4 i4,DB{fffi rot@Wt (54sifiggde: D6cachhtoryl€,]/ M

LtS Dlp t761tS€SDr)

PrEparbd & Ansly6dr2$ arfl

e.BHC

tsBHC

BRL

SRL

BRL

BRL

BRLgRL

BRL

BRL

8RrBRLBRLBRLBRLBRLBRLBRf6Rl-8RLBRLo0r090.0115

0.01320_01120.01240.00470.01200.0r250.01310.0124o.01?30-01280-01300.01050.01060.0123o.01420_01000_01360.01290 01340.0130o01310.0135

0.01400-01m0.0124

d-g|{c 0.m44 z.2a t4

Mlq4|jg,lpcl

u04

!s,!s.l!s,td!s.'lIlgIr,gt|4It4,,1l/g4lE,||/$'l!91t'sl'!dl!s,

|l$4

I9l

u04Z-2" till

!s,4t's4ttqlusl$4us4r44!o1M!9t!s{l|gll4/lm/r|Jgrlcl!s,tgl

{gl

uc/rlyr

0.01m0.01m0 05000.01m0.0100o0lql0.qpo0.0r000.0rm0J1m0.01m0J1000.0im0.01mo.fim0.05000.0rm0I]1000,0100

03100

0i1m

o0tq)

o0r00

0.01m

0.0100

0_0t00

0.0100

0.ma)[email protected]_01000.0tm

0.w0.0w

0.m10o@o)0 0e000.0200'02m0.m000 (P00

[email protected].(Bm0.m000,02000.@mo(E000.@q)0.02000.(Em0.02mow0,Mn

0lalo

0.0e00

0.@

0.@00

fitil301fl

4Sr401+140i0.140

r(}140

{&14i)

l|()-14{

4{rr40

40t40

4tr140

4$1.41)

4{1"140

{st40

10-r40(}r€r|(!r€

il+rill)

,|{.1{0

rUll,{)

{1}t{1)

4&t{0

4+r4t)4t 14t)

4G1rO

t{l-lr{)

4Gt40

4&140

a5E

66

56

s224

60

62

62

62

64

65

54

62

71

50

68

64

0i1000.0100o0tm0.01m

m6062

6

7

0g

mmm20

Thls laborulory Eport ls @l rdid xirtod aa sathorid signzn E on th. coter pagc.

. R@orlEblc D€t€ctirn Linit BRL = Below R@orting Limit PNBe I 34 of I 54

Page 720: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GC - Qualitv Control

Analyle(s) Result FtuC Unils *RDLSpike

Iavcl

Source

Resul l %REC

%REC

Limits RPDRPD

Limit

Brrch 7031?68 - SW846 351m

lcs nip fl0C1768{S011

Prepaftd & &Elyzod: ?9- arc7

g-BIIC {tjndai€)4,,1'.DDD [p.o)4,1'.DDE(p,C)

lt-DDJ lp,p)oi€rtin

EndNrf,an I

Endslrtan ll

Eados lan Suthle

Enddn

E{ddn Aldohy{e

H6@{or Epond€

ecl oiddr€

g€hhdan€

Endrin K€tul€g,iqgate. lfiebffindidw! (g)&nqdd Dsa onbiphe!ryl l&)

Brr.h 7031?69. SW846 3510c

Sb aGtTf+BtKt|

Psparsd A Anstlzsji 29-[rar{/

PC8t016

?cB 1221

PCA 1232

Pca1242

PCA 1248

PC8 t254

PCA 12m

ttB 1262

PCA 12mgfiqtu: 4+N-thn(Mobbhefit4 (Sr)Stnf{,ate: D&dtuttwwg (Sn

lcE fl{El ftg{Et)

P.€9er€d & Anelyr€di Anar{7

PCA t0t6

PCA t260

2,45&TC{t .Xyi€n€ (lS)

su/@ 4 4{Eeriuo(objd@ (9)sul@E Dgrad* otktlf,nt gt

LCS D|p ft6l769{S0ll

RspaEd & Andlyzsd: 2*Marfi

PCB 1016

PCB r2m

sr'r{'siE 1,{D9-o@,rL0robiphe,tt gtsuwqE:bttuta@Eort (st

0.01280.01400.013s0.01480 01390 0141o.o1470.01180 0 1 m0 0152D.01430 01200.0't450.01380 01470 01450.01280.0146

BRL

BRL

BRL

BRL

BRL

BRL

6RL

BRL

BRL

0 01300.02lJ0

o.227

i.264

0.0200

0.013{)0.92w

o.224

0.265

0.01300.u00

0.0tm

0.0100

0.0100

0.0'00

0.0020

0.0rq)

0.0tm

0.0100

0.0100

0.0r00

0.01[u

0.0r00

0.0100

0.0100

0.01m

0.0r4

0.02000.02000.0200o_uM0.0m00.02000.02000.02000.02000_02000.02000.02000.02000.02000.02000.02000.02000.0200

40r40

4G140

40,r10

40,10

4G140

40-140

4GI40

4$ t40

40-t40

1+140

40-J40

40r40

40r40

4S140

4+140

4Cr40

40-1404t-140

|.Er|anlslpsl

81t91!s4psl

us4t8ltcsrc/r$4ps4p94

!s4!s4,r94

64

70

70

70

70

59

63

76

72

60

72

69

14

72

u73

6

1 2

6

12

13

1 3

t 5

20

1

6

8

I O

I(]

2Q

202Q

mm20

20

?0

2A

20

n20

20

20

20

20

ts4t's,4us.4psn

!snI9,pgl

tsrps,l

u!/llsr

91

106

1 1 9

651U

$n$l

us,'ll4\!M

!srrcnNIwI

[email protected]{0.02000.02(Xl0 020{)0 0200

0.f200

0.0200

0.021{l

0.0200

0Mn0 w

025{)0.25010.0

ap000.02\m

0 2500.2500.0?{na02w

65t00

90

1md5t00

30-t50*t50

4G140

4o.140

50200

30-15038150

40-110,l{.14{

?0.150301Q

20

20

Thit labo?atory report is nol toltd x'itho.d an aihorize.l sigtt4ture on the coycr page-

r Reportable D€l€ction Lirnit BRL: Below Reponing Limir Page 135 of 154

Page 721: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Qudity Cooarol

Bstch ?031680 - Sw846 35t0C

Bhnt f/(Bl68G8LKl I

Pr€par€d: z8-lrar0T Analyzedi 29Mad7

1. €$yinapnUralen€

A:ob€n eneDih$ykii€dno

Bsuidiie

Bsr'a (4 snhracene

Senzo (a) anr||!c€n€

Eenzo (al gyren

8glm (a) pyr€m

SdrF {b) nuorafiel|€

Eenzo (D) tuordrfieno

Benzo (g,t',i) pgyl€n€

Bffzo (q,i,i) psyl€ns

B€nzo E) fuoaarUteft

B€l@ll)fi|.o he{te

Eenzoh acid

B€n:yl alohol

Eised{o@tbr' nrsdl{llle

8is(2-ctloro€hyI)€het

BE{2{hhntsoproMstlt

Eisl24bylhoxyhhhahr€

a&orEpher'/ p@ etFr

eJ|yl benzyl phtlslalo

C€rb8.zote

4-ClldD.3.rn€$ylglEnol

44nbrorn rE

20rlo|!mpttlalono

2-q\h,@ttsnd

4$boph€ny1 el'€nyl efi e.

Grrys€$6

Cl4€€iro

Djb€rto {E h) an0la.tr|a

ofr€nzo (ah) anh.a(€nd

Dib€n:ofrtan

I,2.Di*lorcb€nzen€

I ,}fidh|oben:€rE

1 ,+oi{t orobsuen€

33'{icilorabenzidhs

2,+0knoopt€nol

uMyldlflreleb

Dlnemyi ptdtdrb

2,+Dimetrtph€nol

Oil}nry phh€h6

4,6-0htF2.rn€t\,hnsEl

BR]-

BRL

BRL

BRL

BRL

BRL

aR[8RL

BRLgRr-

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARLgRL

sfiL

sRtBRL

BRL

BRL

ARL

BRL

ARL

BRL

ARL

BRL

aR|-BRL

BRL

BRL

BRL

ARL

BRL

BRL

8RL

BRL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

r 000.0500 0500.4001.000.05i)1.m1.00

0.0501.00t mt.t)00.05002000.0500?q)os002001.m0ffo03t0o601.001.m1.00t.001.0r.001.m1.mr00l.q)

t .m1.001.mLUo1.000.05002000.fio1_00Lm1.m1.001.001.mtfi1m1.001.001.m

l8l

!E]

!s/l

Wtl

l{l,l

$4

!c4

WrMtgi

!91

ljg4

!dl

tdl

llgi

|4,l

|g'l

ugrwtlpc4

jrgl

M$Jl

l44

!s,pdl

[c4

ljEl

|4,

t4N

Wr$,1

|js4

udl

|€/l

TCT

rjg4

u04!s,wlus,Ilgl

lgrM|lg/1

|g'l

wluc4tJg,ugltts4

I Lk ,abontory repod is not vabd x,irttu! aa ourtoitd tlgnaura oa {e coter pag..

I Reportable Detection Limit BRL = Below Reponing Limit Page 136of 154

Page 722: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Serniyol{tile Orgaric Cornpounds by GCMS - Quatity Controt

Anslyt€G) Result l'lag Units *RDLSourcc %REC

Result %RF-C Limirs

Spike

Level

RPDLimnRPI)

Batch 7ol1680 - SwS46 3510C

Bla|* ftll?168[8tl(l I

P.BparEd: 28{.kr{7 Anatyzed: 29Mar 0?

2,+Dhr@hefid

4+Di 'ro|()lune

2,&Dln{robluste

D4l.ody' phdbiaie

He&d{orobuhdi6ne

&ndf orocyclop€fl Edi€n€

lftl€no (1 2,&cd) pyrene

Indeno (1 ,elcd) pyrene

2. et'tjnaptlbalene

z{,lehylnapt$arene

2-tloWplrend

3,4-ll€ort&h*lol

l@ntabne

l@h$alene

2-Niroeiine

3.Nilroa ine

+Nitoenlin€

4-Nilrophenol

f !.Mtosodinslhylamine

ftNitt€odnntopy'anine

I\&Nifosodiphenytamine

Pyidna

IZ4-Td:t orcherlz€no

2,,1,s-rdnblopn€rbl

2,4,BTrulooohslol

Hexad onburadl€ne

SunrBa/'.24uotudwlgnqde:2.hJ3nbiplgnyl

Eurpg'/e: 2 FltJotophp,r/&.nog6taffl'oben 6rb.d5turq'b] ms0d45glrogda: leg&laaSu/og,it: ledwl.dlgtroge: 21,6-Ttbtd4taol

ARL

ARL

BRL

BRL

BRL

BRL

ARL

BRL

BRI.

BRL

BRL

BRL

BRL

BRL

ERL

BRL

BRL

BRL

8RL

ARL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

8RL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

ARL

ARL

ARL

SRL

BRL

BRL

BRL

433d3Ja2

78.192.492.465.?

!0r!dl

!sntglrgl!c4!snusn!s/!dl!sn!s,4!s,4!94!s,4!qlflsn!Mus.4

!snrrg/|

PEuglWllctl!s4!snpst

!s,4usnNN

H,4

tel

!s,us,4Nt!94

ldl

!91

|Jsn

vups,lps4p91!s,lPCr!!c!tjs'l|lg4

us4tdl

1.00

1.00

1 0 0

1.@

1.m

0 050

0.050

1 0 0

1.00

0.500

1.00

1.00

0.050

0200

1.40

1.00

0.050

1.00

10.0

1.m

0.050

Lm

1.00

1.mI 0 0

1.00

L00

1.00

1.m1.00

1.00

1.00

0.050

1.00

1.00

0.u60

1.00

r_001.0)t m

1_m1.@

1.00

0.500

tw1N

tfrtffi1@tm1N1ffi

83

a96n9292

3t>1N&1U15-1103A-130111103+1iA3G1Ulg1t0

Thb laho.alory rcpot is not told pUhou ad authori<ed signrrwe on the cover psge .

r Reportable Det€ction Limit BRL = Below Reporting Limit Page 137 of 154

Page 723: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolstile Organic Compounds by GCMS - Quality Cotrtrol

AnaLyt4s) UnitsResuft Flug .RDLSpikeL€v€l

%RECLimits RPD

RPD

LirDit

Source

Result %REC

Datch 7031680 - SW846 3510C

LCS A031dn}8s|l

PeparBd: 28-lrs.07 Anaryzed: 29-lrar-07

1-l,lehy'nadrtur€ne

Anllln6

lzoba'z€dDiptr€i\trdia.in€

Eendjin€

Senlo (d afirffile

Senzo (a) an$lac€n€

B€nzo (a) pyr*F

BenD {a) pyr€o€

8€r'zo (b) fr./o€ntsns

Eenzo (Dl lEant'€ns

8€trzo (q,hj) pdltene

Bsnm (ghj) pslien€

Bei.o (k) tuo€nheie

0€nzo (k| nuo€nbl€ne

Eenzoic acid

8€nzyl dcolu

&s(2+lidEsnDry)rlethane

Bii{z{ o{E$y')€trer

Biq2d{.tttisopopt)sth€r

tliX2€hyf lsxri)rf 'f 'alab

4-&onEpi$yl phen}1 etr€/

8utyl ben4l FmdabCarbezol€

a{ orF3{nefiyldlenol

4-ChldwdliE

2-ChlororBFffiat€n€

2.Chlora€h€|d

1-Chhrc9i6nyl phsnyl 6her

Ciry$n€

Chrysene

tttdlzo {a,il an$rac€n€

Dbefto (ah) snlvactn€

Dibenzottfdn

1 ,!Olt{c'!Hra€

I,+Oi$lo.obsEene

1 ,6Did orobduone

3,3 Oiddfloh€nzthe

2,4Dld1ldldBlol

OhhrylSr$e

ometryl phfuab

2,+Dinshylph€ml

tl'ntulyl fidElalo4,6Dinire2{ehly'pn€ftd

77.6

77_6

E5.1

85.1

76.5

103

86.2

E6l

174

94.2

104

80_4

80.4

a7_2

a7.2

83.8

E3.8

65.2

8 5 2

7 9 0

7S.0

77.O

76.8

85.5

92.0

61.4

91.2

77.4

90. I

1r2

83_7

8 6 1

79.7

69.4

76.A

86.6

66.6

90.0

90.0

a1.2

75.5

67_0

75.6

.2

75.2

84.0

E4_4

73.1

74.O

!94pg,l

|84p9l

|lMpdl

!s,|B4

1Jc4

ugl

lcl

rgl'rjstTETpgt

lsl!E]!E

wlt4,llalrgs4

!s,la4t44usrru/]rjEl

MMt44usrlrg4!c/l!s,ttgllq4l,clps/rldrMl&tl

t8,lpgl

uslt4l'Mtdl144

ugltl44

1.000.0500.4000 050r.000.05t)1.00100

o0501.00

1.m1.00035002m0-2m0.0500.0500200t mo0r0 05{)0.300L00Lmtsr_001.001.m1.00100r.m1_m1.00

L00

1.mI llo0.050t.m0 0500?001.001_001,001.mi001.m1.m1.mLm

1.m100

1 m100100r00lo0I F

100

1rI)

100

tm1m1m1(r0

100

t00

100

rml0o

100

!00

100

1 m

rfi)

100

lmt00l0{l

tmrtD1fI)100100100tmr001001001m1ql

r00100t00100r00tql

1m100

1m100tmlm

78 111-t10

78 4Gt4t)

E5 {}141)

E5 4$110

m 1ut-118

76 10.110

lm 4Gr40

86 411141)

66 4+140

174 G2m

91 {0.140

r04 40t40

m 40140

80 10.140

87 ,gl1rl0

E? {0-1{t)

B1 40110

84 4lIrO

85 4+r,{)

85 rl+141)

19 1Sl{n

79 €t10

77 30130

n 4+110

E6 4G140

92 (}1{

6t 4Gr4t)

91 {+140

77 48110

90 :l&140

112 ,91140

81 30-13)

EO 1&1,10

m 40.140

6{t 3}r3)

77 &-1{d

E7 (1140

E7 10-t&

9o 4014{'g0 4st40

81 4+140

76 4+1q

67 1&110

76 10-110

s4 4Gt41)

75 l}l3l)

84 4t114{l

84 {l}140

73 3Gr30

63 4S140

74 3$r3o

This labralory rqod k not ralU irllhott al au&.ofiaed signrntE on thz ctw. page.

t Reportable Detection Limi! BRI- = Below Reportine Limir Pagc l3E of 154

Page 724: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Quality Cotrtrol

An8lyt€(s) Resuli F lag

Sourc.e o/;REC

Result %REC LimitsIRDLUnitsSpik€[,evel

RPI]

LnnitRPD

Batch ?0ll6A0 - SW846 3510C

les fl031681]ost IPr€pated: 28{ilar{7 lnalyzed: 29lVaF072,1-Difi'toph€flol

2,+oinitotoluene

2,Sohitotoluone

Di-n{dyl phr'€ble

H€xacnboctdop€nhdienB

Indsno ( 12,3{d) p}r€ns

lndst'o (123.rd) Mene

z-tlebylmphllalene

2-lil€d\inarfii'aren€

2.Llstry{phend

3,4lrefrybienol

l'laplfial€n€

adrtElene

2+ItDanilitE

Sllt€dline

+ilroanithe

2-l,JitrEdlglol

a-Mrogt€noJ

N{.litosodimeliylanoe

l}lffiosodintropYanlne

r[l|iro&ditl€nylamin€

Fflitr'ne

lbxacl o@benzene

l24.ftichloobeo?erl€

2,4,$IriJtoro{ha|ol

2.4,STdt{orodEnd

Hexaciloobutid€rEgnrogd4: 2+tfiotiplpnylg,nqaE2+wt.t4,,W

s/dr'oga&] z+tro@Ialr/S{''{{l'{f.: ltlt/.1(ff/t2dtx,45Suro4€te:Pffi6g]/7os'iF.:TadBMaagl/'i4eh:Tetfi€vaa

st'ttc@:2,a,eT@rpnol

8 9 5

95.2

92.5

94.9

80.2

80.2

79.9

79.9

75.1

74_5

66.2

63.3

u.784.7

9 0 3

8 2 0

8 2 0

71.7

7 9 2

7 8 9

7 8 9

87_3

86.4

102

95.1

77.6

59_6

al.2

42.7

91.5

73.3

76.8

7 6 8

67.9

75_3

75.3

81 '1

75 '1

63.3

79.8

72.6

73.3

63.0

74.5

m 674.3tu71.64.14.1n.9

v94

!94

UE|lgn!s4lsn!s4usnus4pg4

!s4p94

!s]lps,l

!4,'l

Bn!sn!Egs4

!EtrE!s.4!{t'Kn!sn!c4!cn!dl!s4psnpg/].

vt/]'!dltsrr!grME4trs4!E9SrlsnPE!s4!c4!s/]!04!91w]TSI!sr!91ugl

1.00

1.00

1.00

1 0 0

1 0 0

0.05{

0_050

l_00

1.00

0.600

1.00

r.00

0.050

0200

1.00

1.00

0.050

1.00

10.0

0.050

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1 0 0

0 050

1.m

1.00

0.050

1.m

Lm1.00

1_00

1.00

1.00

1.00

1 m0$0

100

100

100

r00100

100

100

100

100

100

100

100

100

100

100

100

1 @

1m1Ul

100

100

100

100

100

t0l

100

100

100

t00

100

100

100

l m

l m

100

1m

to0

r00

100

t00

100

1 m

100

100

1U1&1N1N1N1N1001N

90

95

95

80

60

80

€0

75

74

6€

63

65

a5

90

@

E2

nt9

79

79

a7

86

102

95

78

60

81

€3

92

13

77

n6E

75

81

75

63

EO

73

73

F

74

aa

t0472uuN

30,13040t404{"1411rl{.140

4G14{

4Iliro

1111411

4G1411

4{f140

4&140,(F140

4tr1it{l

r(}1rll)

rlGI40

{f140,|G1,1{l

4(}140

411,140

1Gi30

,lGl40

rt+t40

4G140

10l,li)

4&t40

4G140

3$130

3+130

40.140

rr0l40

4i}140

3&130

4+140

40140

3D130

4+r40

4S140

40.140

4GI'o

4{t140

1&110

3G130

3G1:0

3G130

4Gl4{l

fr-t&30-130tr l l0#ti015-110*130*13011110

This lahontory rcpon k ,ot wlu x,ithod M aa{.odzed tigarurc on the cover page -

* Reportable Detecdon Limit BRL = Below Reporting Limir Pase ll9 of 154

Page 725: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semiyolatile Orgrnlc Compoutrds by GCMS - Quality Cortrol

Analyte{t ResuhSpike

t€vel

Source

ResultUnitsFlag %REC Limits

B.rc! 703t774 - SW846 35508

ah oanT4€LKll

Preg€redr 29-lrar-07 Anatfu€d 02-lpr{7

Al.n€u€ft ,oihs{tyHiarng

8€nzllne

S€nm (a) antlacone

8€nro (4 prem

8€izo (b) ftDlentlefle

B€nlo {o,h,i} pdylsr€

B€nzo (r) fluolanh€r€

8€nmic ard

8snzy' ahohol

&s(2{hlol€nlory)m€ftm

Ers{zrl o!4ldr€t

Brl2rht dsoFwl)€ts

Bis{2{hyt'edFmrahte

+BMEpienyl plrsrrl e0€r

Butyl !€n4l d'r'aksC€ftazol€

&CfilorF}IIEtryblEnat

l{1 oroanilin€

z4lorcmC El€ns

2-oioropherEl

4{Horophenyl ptt€frt ef'er

Chrys€ne

Eb€nu o (Ah) antrdr€ne

Dibenzoiran

1 2.Di{ttomb€nzen€

1 ,loir{orob€nzerEl,4oichlorcbenzsrE

3,3 -Did ctrob€rliinn€

2,+D{rn|o.aphenol

Dery d'haH€Dimefiyt ptt'alab

2,+Dimsd'tdErd

tx-n-butyt pnhabb

I,S0hr62{rcfiyhh€nd

2,4lhi[ophrtol

Z+Oirlrottuen6

4StJirilrolot$e

D-r'.odyl ptddab

liored orohiEdkn

ri6|(adblDcrdoponhd€r€

lrd€no (1,2,9d)prone

I dlstryinapt$€hi'e

BRL

ARL

BRI

BRL

BRL

8RL

BRL

BRL

SRL

BRL

BRL

BRL

BRL

BRL

SRL

BRL

BRL

BRI

BRL

SRL

BRL

BRL

ARL

BRLgRf

BRI.

ARL

8RL

BRL

ARL

BRL

BRL

aRtBRL

8Rf

BRL

ARL

SRL

ERL

8RL

8RL

SRLgRL

BRL

ARL

SRL

BRL

BRL

BRL

8Rt-

BRL

|,drg rv€l

lqrg ',v€l

Igr! rd

lglis ]rEt

lErg '|0l

|J!,rS wst

mliC vrgl

UoAS nsl

|lgtg I'sl

|jgrs wd

!Sr(9 wd

lgrg *l

HllqtrT

|4|lqwsl

UCA! r*l

|lgkgY€I

|lErgwd

tlsts wd

!9brcr

l4|t8r€t

l8,lq\$t

|lgkgwel

|lg}S $,€t

|4/lg rrd

!s,4q 'd

|js/rgwl

lSIq I€!

pSnq rct

|9 q vrel

|jgr'|(S s'sl

uErsffil

l8fts,€l

|lgltg $/sl

US*S ftl

Ug/tq $el

tlgtSwel

llgllqwel

|ld?.9lv€l

|lgkS v/et

|]grg v,El

l]grsl'd

|js/rS Td

|afrSmt

Igrq $et

|ldtgwet

|lg,tS s€l

ug]kS tJ€l

ryrs t{€l$Er! llel

|jg,'|(S f,31

|,dhlrei

330

330

3c0

330

3:]0

330

330

3t0

330

330

$0

3]0

33O

3g)

310

330

340

330

330

331)

33{)g[

cto3303303303:)033t)3m33{33030330330sto3303m3(t0330

3303303i!03it033033{)30330330330330

This labarolary .eport is ^ot rolld flitho$ zd a4ahoiud slgrata.e or, the cover pag

' Reportable D€t ctioo Limir BRL = Below ReportinC Linir Pagc I,{}of 154

Page 726: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - euality Control

Spike

Level

%RECLimits

RPDLimrt

Source

Result %RECAnallte(s)

Brtch 7031774 , SW846 35508

Bhnr fl€l?+At(l1

Preparcdi 29.fi erfl aEI.!€d: 02-Ap.-07

2.rlshF€phhalone

z. 6trlphen0l

3,4- on4{Fend

tlapfitteg€

2-l{uoal tino

9Nnr!€niln€

4-ruto8nili||e

t{tDbsEErE

2.t{i@l€{rol

+Nitldr€r'ol

ll.l{ibDrrdi'rrdl}lanirE

li-Ntt6.di.nf .opyl€min€

l'l-l'rltEs.dplE|tamin6

PttilitE

I 2,1-Tn:t orobe||,ene

2,4,tTri*'lordrsnd

2,4,&Tdilo@End

S$qtte: 2'flndifaqASrnryE:anffc{,h1rtr,ls/n/ogate l:$tMt2etE45

griogats; feryhql4aS6roge/f.: 2lEltbwnoptPJnol

tcs oBt z+asrl

PreFEd: 2+Md{7 Arulyz€d: 02-Atr-07

ANINE

Afa2fE

Azob€nzedlXph€nyldiazine

B€nzidfls

B€nzD (4 anfFrc€n€

&rEo (4 pfD te

B€nro (b) lud-antEne

B€nm (g,h,i) psyl€ne

Berllo (l) [t o,rlbsrE

BsnDk std

8€Iuyl ebohd

Sq2dforccfroxylm€$ans

8q2d$roiryl)€$er

Sq2dbotrproprtl€fl€r

Sb{2€t}4@)pl'lhatalo

4&DllEdl€ny' ph€nyi otEr

I'Jtl bsnzyl drtahl€Cartazde

BRL

BRL

BRL

BRL

ARL

ARL

ARL

ARL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

ARL

56405t@65fr

6An

4850

5170

4990

5430

7910

6030

BRL

5000

5500

4720

4840

6380

5620

4780

5340

6000

3600

6170

4680

5940

7030

lj0ks wel

!gl(g flel

!9,4(s wel

llg4(Sl{et

!91(g wet

llgn(qwet

|4,l(9 wel

ugtg w€l

l$tg !$l

trll(g w€ty9k9 rrcl

ruL&o nre,

pg/rs v.el

p0/ksv€l

lyrg wet

|'s(s wel

p!,{(s v€l

tig/*S Y'st

!g'rg wel

!S*g wet

lg.rks mt

p$^g wet

|lg,r(swetil{r4(SwstN/kg nettrgkg welp$4q wer

Pgts w€t

tig/kQ wel

PS*S r €l

Ug/Kg rl€l

Pgnq Yrsl

!g&g s€l

pgr(g $€l

!q^s l^€1

tigr(S r€1

ug4q vr€l

P!,lq w€]

P94q r€1

l]9[0 r'€l

ISAS !,€l

Ig4q rcr

Pg/lq r,El

Pg,lq w€l

PSIq wel

l|g,kS we1

IS40 w€l

IS4q !rel

IBIq v€l

alo

111)

30

330

330

330

330

1320

330

330

1320

330

300

330

331)

330

330

330

330

330

330

33{l

330

330

330

330

330

lB0

330

$0

tr|0

330

x30330330$0frto331)3303303m3:10331

6m6n

66,746m6ft

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6670

6i70

6670

6670

6670

6€70

6670

6670

6670

66m

6670

85

98

9962

73

78

75

81

1 1 9

90

75g2

7t

96

E4

80

90

54

9l

70

89

106

3U1301rt103013015 t t03+tfrt r t t0

4Gr30

10-130

4+130

4& 130

€-130

10.130

Gt30

40-t30

4G130

4S130

40r30

4&130

cr30

4+r30

4&r30

4&130

4&130

4+130

4Gr30

40130

4&130

RPD

This labontory rcpoft is not t)olid tellhout aa outhori&d s@narare on tha aecr page

' Reporkble Detection Limit BRL = Belo* Reporting Limit Pase lal of 154

Page 727: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - Quality Cotrtrol

Analyt€(s, Resull Flas Units *RDLSourc€ %REC

Result o/oREC Limirs

SpikeLevel

RPDLimitRPD

Barct 7031774 - SW846 35508

tcs iro!1744so

PreFarEd: :€.lra {7 Analr2€{: 02-AF-07

4.Chlom+m€$rylphad

a{|lbDanili|E

?{tloDriaphtu|€ne

2-Cnhopfiffd

4o{croplEfiyl dEnyl €ter

Cnrysene

ttb€nzo {a,hJ anfinc€n€

Dib€nzdu"n

1 ,2-Didcrob$zen€1 ,SDiilorobsrz€n€

l.4Dicnbrcbffzsng

3,3,.olrlffobonzidire

2,+Did oopiend

oiotryl Tlitle|oleDii'eftryj pltHare

2,4{iret4#l€nol

D.rlbutyl C'ttalats

4,ADrrdro-2{€hylph€rEl

2,+DitFopn€rDl

2,+0initoltus€

2,FDintot u€ns

Di-n{dy' prd€hh

HexacnhlE$hpenladene

Ind€no (1 ,2,3rd) py€n€

l.tit€hyinsphhal6€

z{rdbrnapht'al€ne

2-frdMptEnd

3,+M€tYpt€nol

2-llildriline

3+Urodtlh€

4i\ftoanilin€

Mlro!€nzene

2.lftbpnenol

4.t{itopisnol

N.NiEa€odin€fiylarnnE

N+lit!60d-nf .opybn-ms

&NitNd'ph€r'ybrnlie

q/Yijin€

134.TdJ oroben:ene

2,4,5-Trid &qll6id

52ffi3600193045r0157051m5330fi704€r''04?3049105.t0046605320511044'&053()040804a{m54m

70304t7051301540,$40

40404704700474057505230477054'r051205170,1S90

64t0509047703650{a5044405no43904610504019703?3048805210

6670

66m

667t

6670

6670

6670

667(l

6670

6671)

6670

6670

E6fll

66m

66m

6€70

6670

6570

66?0

6670

66fl1

fiim

6670

6670

6670

6671

6670

m?0

6670

6670

6671

6670

65m

6670

6670

66m

6670

6670

66m

6670

66/0

66m

66/0

66fl)

€671)

66n

6570

n54

74

6€

nm

73

74

EI

70

80

n67

79

6 l

t2

E1

t06'73

n68

70

5t

67

70

71

86

78

n8 t

TI

78

75

96

88

72

55

73

67

a7

66

6r

75

42

n78

|rylq wst 330

|lg/r9 wr 330

|4,Is {sr 3g)

!9{0rld s3n

tgXS wd 330

l{l€ Yr€l 3q)

mfi0$ol 3:b

ryto wd 33)

!9*gv/€1 330

lgtg f/El 310

E CrEt 3X

E qret 330

|lg,}g$l 3]0

|,glrsrci 3m

lgtsnsr 330

!9r9 r€l 330

|.€qrct $0

llgAg$ct I|l)

|4|lq rcl 330

WtSrct 330

|4,tgrq 300

|lgllq tr€l 330

lgLSwst 330

|lgkS wsl 330

|Jg/lo {/€l 330

Ug,lS r€l 30

rrSAS $r 330

lgl|q *€t n0

Igrg$,ot 330

|lg/l(S rcl 330

|]d}s t€l 330

lJq/rS rEr 30

|lg qtrol 330

BkSw€t 330

llg/kS,/{et fr10

|]gftg wd 330

lgrStld 330

ydb{sl t?0

l{l€rir 380

lgtgwet gl0

H/lq $/el 1320

M9 rvel 330

lgrs v'q 330

E q'ml 330

|A@*et 3s

EAg vrot x|0

lglg w€l 330

lg*SrEl 33[

tg4S*e{ 30pSr€w€l 330

|jgilq teet gE

(}130

4&1304$130,r$13)

4G13010-r304e13041}r30{}13011I13)

40-13010-13040r30,!0-1fl).t0-130

40r3010-r304&r304Grg)4$130(}r30

10-t3040t304G1g){s1304G13),(llgl

4&130

4tlr3l)

4+140

4l)"1{l

,{11,130

10-130

4tlr30

4$130

4$130

4G13)(}rgl

4G130

40r31)

4$130

41I13)

rG130()-r30

4$130

4+130

4$130

4r!13n

1{l-r30

(}r30

4t!r3l)

ThB lahoqtory rcN., is not vali.t ttithou sn anahorlzed sig,,zt,.re da the cora page.

. R€portable Detecriofl Limit BRL = Below Reirortinc Limit P{ge 142 of 154

Page 728: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatile Organic Compounds by GCMS - euality Control

Soike Sourc€ %RrC RPDAnalyte(s) Resulr Flag Units *RIIL Level Resutt %REC t_imits RpD I_irnir

Barch 703 U74 - SW846 35508

LCS mfi7l+BSll

P'€p€/d: a4u47 ttu zfd. AL-AF 4 l

2,4STriflo'opnolbl

Slr'l'.{,,e:2'frlotoMgil&n.galr:2.neryherdgno$b: NttlMnzdc4,

Sutt'g8e: leri6nt44Su/ogag : 2,46I tltuornqhald

Or.ilcfb rlFlZl{tUP1l

Pr€Fared 29-tilar{7 Anat"€d: Cz-Apr-it7

Ani|jn€

AxtenzendoiFonyl{arine

EonziirE

Equo (.) an$nE€n€

Eeoro (a) pyr6€

G€ruo (b) i'rorambene

B€nzo Gh,t psylene

8€ru0 (I) tuorantls{le

Be|Eoi acid

Eanrtt ehohol

ee(?-clloroehory)n€tlane

tIE{2-c ctro€tfl€mer

8is{2r}broislpop}i)€f 'er

tli{z+hyDer}4)phhalh!e

+&qnophstj pngly et€r

Bttyl bsrzyl pitalaia

C€rbade

1{ orc}n@ptHd

4cloroantrne

2+{oaonadlhal€no

2{llo.opnerd

a{ odphenylphsryl e{ler

Cirysd|e

ObaEo {ei) enfirac€r€

ob€nrolurdn

|+Oitlollt nr€n€

I+oiJ o.otd|r€n€

|,a{thlorat€nzeneq3 .Ditddotsruidirs

2,+DidlooCr€flol

U.diI d$atdeD'n€fi'r pffiEbls

a+Dim€q@r€.rol

Il-tt{tly' d'6alaie

4&Dirft c2{ishylplr€nol

2,+DittuEplrsrol

2,4-tli{rotrll€ne

2,SDindrohU€ne

3930

52W4410644046705574

Soun : 5A5925.02

!g/rq 8ei

llqks wel

lgfts lvet

!s4(s v{et

uExg werUtlq R€l

rs^s dry!S.4(g dry

ushl dryps,4s dry

!S/kS dry

!S/tS dry

!!trg dry

lsrs orypslq dry

PsrNs dry

t]9rr9 drypglq dry

lslq dry

PE& dtY

!c&s dry

|l9\g dry

fS,tg dY

tyxs,rypsas drypsnq dry

lslq dlypgts dryp0,tS (fyps4q dry

!9k0 dy

!S/tS dy

tqxs dry

ls4q dry

lgrq dry

lrS4q dry

lgkg dry

!S'rS dry

ISAS d']

|js4(s dry

l44(s dry

!g&g dry

lqes dry

!s4c dry

tS4q dry

us4(s dy

ldts dry

|Jg4(s dy

66m

ffin6n670ffi7466/0ffi70

59

n679770af l

{0t303t11301U1103+13015-1tA30130IG110

BRL

BRL

BRL

ARL

ARL

ARL

BRL

73.4

42.4

74_9

49_6

84_'l

BRL

ARL

BRL

BRL

BRL

8RL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

BRL

1 1 8

BRL

BRL

BRL

BRL

BRL

BRL

BRL

ARL

BRL

BRL

ARL

BRL

BRL

BRL

BRL

2&5

285

285

2E5

285

285

285

285

285

255

205

285

285

285

285

285

285

n5

2€5

2E5

285

2E5

285

a5

285

2E5

a5

285

n5

a5

a5

2E5

a5

245

245

285

285

a5

285

285

n5

285

BFL

8fl1

BRL

881

BRL

BAI

BAL

8RL

8RL

SRL

BF!

8R!

EBT

8Rt_

BRL

BRL

8RL

8nL

BRL

BFL

BNL

BFL

BFL

8FL

BRL

B8L

BFL

BFL

9FL

B8L

8FL

8FL

8FL

SBL

BFL

BRL

BBT

BBL

BRi-

BBL

BFL

8FL

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

fl)

J

J

J

rhb bboruloryeporr b tot ,)olu *ilhott tD earhorized signoure oa the cover ptge

* Reportable Dekation Limit BRL = Belov,. Reporting Lirdit Page l4 l of 154

Page 729: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolatlle Organic Compounds by GCMS - Quelity Cotrarol

A$alyids) Result Flag Unit5 Result '/oREC Limirs RPD

Brtch 703 1?74 - Swt46 35tlB

olllh3le filFlr'4-lXlPll

Prepsr€d 29{ilar{7 lr|a|}r4d: m-}pr{7

Di{{ctyl pht'dah

H€Iacnbiobuhdene

ll€Ischlofmtdopenbdiens

lndeno {1,2,}{d) pyene

l -Mot'tlnaphfialeno

2-fi€hylnaphtlal6n6

2.Ilsdrybiend

3*M€dlyipnent

ilaoht\rkrs

?.t{illoaniIne

}llirosniline

,l-l,litdriirc

Nilrobenzen€

2.r'Ilofleool

4-Nrophenol

N+litorodnn€0tlamiF

f &Mro€di{rFopyiariin€

N- iEosodiphenylamine

I Z{-Tdchlorobenuene

2,rsTdcllomph€rEl

2,4,STidb.ofi€nol

Sunryt,2-FatfienytSrr'/I.oga/.a:z€/btopll€tlf,lSurgga@:Nittuvefted6Slnogab: Phstd$swqattIdit ttl44Sufi Wan : 2,1,e ldbtonophefl I

Ltsk Sd(. frlBlTl.tlsr I

PrEp€red:z$ ar{7 InaiEd 0}Agr{7

44thro-3{nsr'riptFnol

2.Chh|wh€d

l,il-0*t{dobffzene

2,+Oiiibrtulus'e

+r'tuplr€td

N+I'fosodi{rFEptlamlno

I g4.Trtci{orob€nz€ne

SurqaE:z-Fk$didwag/f'rgatg:z-Fk)orqtud

Sou'la 54597854

9RL

91.0

BRL

BRL

BRL

BRL

BRL

47 -3

BRL

BRL

BRL

ARL

SFL

8RL

BRL

BRL

BRL

BRLgR'L

BRL

BRL

BRL

BRL

BRL

BRL

130

BRL

BRLgRL

BRL

22N?310264021fr8101n0

Sorr€: SA5g78FtP

lgts dYygkgdry

!9r(9 dry

ugl(g d)

|lEIg dy

!S.4q dry

|lgls drvpdls dry

Elq &ypgl€ dry

Wgt'rpgrs tr}

rMsdr!/lsrts dY

rc{q dlv

|4Iq d'Y

|lgtsdtv|lgl(s dv

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uul!drflErg fiv

lSIq drypg,lq dry

P9r9 dry

|lgl(s dY

|'slksdv|lgrgdrvljcrs drr

lgtg dty

t!/lq dry

l4,lq dry

UCrg dry|rylls d]lgrg f}ah drv|JgAS drylgks dry

ugts drv

|lg}s dry

|lgts drv

!gl{ fi}

udh dv

Hlqdrypdrs dry

Irg,lq dy

|Jdrsrv|Jgrsdrv

rg*g drt

!gt! drylErs dry

2E5

a5

285

?85

285

2&t

2E5

2&5

45

285

285

285

245

&26

r t40

?85

2E5

ffi

285

2E5

245

285

285

285

245

245

245

285

?88

nl

288

288

288

1150

266

288

2U

N

28€

8N2PEO2E&28lI'2W28&

5810

116&

11600

5810

5€10

r16m

5€10

it6m

116m

5810

5810

fil05810

ff130trfi0tutatrt103E1W1Ul lO

40.140glrg)

3St30

4&140

41!140

3I130

40t10

clt3n-130

()-r{04$14{)!r-13JlU110

BRI

63l

BRI-

BFL

8FL

8FL

BRL

BAI

Bft

8Rt

BRL

881

8fft-

BRI.

BRL

BBI.

BAL

8FL

SFL

8RL

8Rt

BRT

8RL

8RL

BEL

€a[r0€BRI.

BFI.

mt_8RL

50

50

50

50

50

fl)

5i)

50

50

5l)

50

50

50

50

50

50

50

50

50

50

50

st)505050505050

80

99

4250860074303A70417046705520650076105160350i1M37N

BffL

saL8RL

BRI.

BFT

8nL

8AL

EHL

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r0€8Fr.

n74

64

67

72

40

95

56

87

60

N65

Thls lahotuldry Eport B not wlu ''ilhoua a!, outhodzed slgnatcr. od the co!|€r pzge.

. Reportable D€tectioo Umit BRL = B€bw RepGting Limit Page l,{4 of | 54

Page 730: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Semivolati le Organic Compounds by GCMS - Quatity Control

SoLrrce

Brfth 7m1fl4 - SW846 35508

tt'th Soll(g f|tslz4{Si) So{rE€r Srf,5gt8,i{ePr€pared 2$Mar1)7 &at!€d: 03-Afl{7

Sr/rogEbi{bD6srzeE{5 S14O&r?o!ebi Pl€dJS 37&Swrr8tu: re$anyl44 SA0gnftgakjl4iniesnophend fi&

fllt|t SE{{. 0rr t'l(Bl7|+l|S0t) Sotirc€: 5A59785.02P€p&€{ 2$li4ar.{7 lnelyzod: m-Apr{7

4390

ss707870

4070

4260

{490

5950

6960

8140

5480

3800

49n39W569o4m583041ffi

ps/I(s dry|Jsfts drypv}sdry!S.4(g dry

!S/rS dry

tsft9dry!gt(S drypgls dry

lStS drypS*S dry

!SI(S dry

Msnrylsas dryps4(sdry

lgxg dry

ISAS dry!S*S dryps^s dryISAS drylglg dryliS^S dry

291

2€r

€1

291

291

t 160

291

n1

zJ1

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291

58t05810581058 t0

5€70

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11700

5870

5870

11700

5€70

11700

11700

5870

5870

58n5E705An58/058n58n

30.1U1511430-13!15-110

4G140

3t 1g

30-130

40r40

4!t4{

3013!

40t40

30r30

3!-130

4+l'10

4tr140

3EtW151103A-1301tfiq3Gt301t110

88659768

44ltrF3{eOy9n€nol

2{rbmph€{d

1,4{ii{orctsuene

2,+OinlrolDlusn€

+iftolheml

NNitGodi{-pmFybmin€

Ph€flol

I Z+Td$ffienzene

Su/.{ae. 2.F{nlbiplanylSrn4&,tsl2fl'ro'q'.igr/Srrao!€bi Lltoben:wE-d5

Sullgffi:ralpllf, aaSwrr{a& 2,4,eTtihlr/nopl)€r,ol

ABL

SRL

8frt

aBt

88L

aaL

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BRL

1m8RL

75

t7

67

69

73

42

t0t

59

7A

92

846/977tlN

3

5

3

1

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6

5

6

6

I

30

30

30

30

30

30

30

30

30

Thh labotulory repod ls ,tot pau N hoa! an adho zed signaturc on the coter page

* Reportable Detection Limir BRL = Below Reponing Limil Page 145 of 154

Page 731: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 6000/70fi1 Series Metbods - Quality Cotrtrol

Analytqt Resul. Flug UnitsSpikeLevcl RPD

RPDLimiilRDL

Soulc€ %REC

Result %REC Limits

Batch 7031810 - OPA20{ySW7000 S€ri.s

Bldrk l?tl3181GBL(Il

Pr€pared: 02.Apr47 AnalFsd: BAp|{)7

udlcat€ 176t8to.lxrP1l

Propar€d: 0z-Aprt lnalyzed 0&&rc7

{dlr sott oml0to#t}

Pr€parcd: 02 Apr{i Analy!€d: 0}&[.07

llrtk so{o fflxttllGlG2l

Prspa,€d: oz.AFfl AnrtF€d O3-Al.fl

Rd.|t|H frofl8tDSRI1 l

PrEp€r€d: (B-Apr-o7 Analyz€d: 0l rr{7

Batch 7031823 - SW846 3105A

thr 4ru018?3€t(1 I

Pt par€d: 30fftr-07 tualyzed: m-Apr{?

Sdgtim

Strvet

Chrdni,m

Cadmiun

Aarium

LiCS tm3l02:|E{t1l

P€pa4d 3&Mar{7 inarr"ed: 02.&r{7

S€l€niurn

SilY€r

Asrium

Ch,trrnium

Cadnlufir

LCS D{o nmis2$8gttl

PriF:lEd: 3o-lrsr1)7 Analf2edi 02-tF-07

S€l€rium

r.eao

Csdnirn

Clroflium

Betum

Sto€t

DlE{ic{. n$1823JUP11

PtED.rid: 3olra'iT An0I"€d: 0e.Apr{7

Sdsftm

t€€d

C]lrcnium

aRf

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1 _ 1 9

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0.53s

1.23

0.0289

0.0702

a-cmo

0.479

0 {83

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0.5000.5m0.5fr)0 5{x)0.500o5000.500

[email protected]{00.gx)o5m

ryl€rel

aRl hgrkgdry

ot"l7 rngkgdry

ivr4 dry

nglq w€l

'ndl

m9rm94

'ru14

fl'dl

mc4

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mdl

0.9r2 5E

0.0841 93

15-125

7U1E

669132t

'|,11

BRLARLBRLBRLBRLSRLARL

0.4660.4610.4760_.t890.4600.4910.4s4

0.4790.4€40.5090.5040_4750.5030.534

Sdin : 5A5863+@

0.m78

8RLgRL

0.0030

iEn

rdl

n91

lndl

msrfr's,'I'97

J nBrlmgllrrgl

J.ORa rpl

0.0t500!0750qEo0.rIN00.0660.0(p5q00g)

0.00750.0r500n0500.00500.m,()ou0500fies

o01500.00750.00250.fi800.frx00.m500.m5)

0.01500.m750.mo0.tD50

8+r 15

85-t 15

e$l15

E5.t15

89115

8$115

E5,fi5

89115

8S115

E5-115

E5.115

88 115

8S115

8$115

s.{92s698Is99

0.m64

BRT

8FL

0.mr8

96

97

l@

r0l

95

10r

107

33333

l l

2020m20

20

20

N

m&n20

Thh hho&/trtf r!0od is nor vali.l r&lrotd tn rutlrotl4ed slgnal,,rc oB thc cov.' pqe.

. t(Eporrrble Deledion Limit BRL = Below RepoftinB Limit PagE 146 of | !,4

Page 732: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 6000/7000 Series Methods - eualitv Cooarol

Ana\te(s) Result FlagSourc€ %REC

Result %REC t,imits+RDLUnitsSpike RPD

l,inritRPt)

Brich 7031823 - SW846 3m5A

thllhde fflFlE2!0UP1l

PlEpa€dr 3Glrar{7 A,llJyzel: O2-&ru7

C€drnirn

$lwr

Earium

Iltlx Sdo ft03llzl.U81 t

PeI€red;3G ar{7 ft€ry?ed: 02,Atr-07

S€l€rium

Le6d

Cadniu,n

Chrodro

B.riun

Slver

flsti So{l{E ouo ?(E1624|tS0i I

Pt€parBd: 3l}ftro7 tualyr€d: 02-Ap'{7

S4leninn

Bri'in

ftdrMrn

St!,s

Orcnirn

Pbrt soltG f|(BtEalPslr

Pt€pdEd: 3GMar-07 Analyzedr m.Apr 07

lE€d

A€riim

C€dmium

Sihllr

C}Yodtum

ARL

ARL

BRL

So|rtt.: S459652{t

Soucc: SA59S3-02

rngl

mg/l

n'M

ngl

m91

in91

m9n

m94

nrg,l

no4

0.w25

0.@50

0 0050

0.01s0

0.0075

0.0010

0.0025

0 0050

0.0051)

0.m50

0.0150

0 0075

0 00cl

0.0025

o0050

0.r)060

0.0(X0

0.0075

0.0150

0.0,050

00025

0 0050

0.0050

0.0040

0.5@

0.5'lo

0.5@

0.500

0.500

0.500

0_500

0.500

0.500

0_5{10

0.500

0 w

0.5m

0.500

0.500

0,5110

0.500

0.500

0.500

0.500

0.500

BB!

BBL

BRT

BRL

8nL

SFL

BFL

a8L

00198

BFT

BFL

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0.0198

BRL

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8nL

BFL

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00198

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BAL

8AL

95

94

1m97

100

108

95

95

1 1 0

101

112

99

96

93

94

98

99

100

98

94

n2A

20

o 413

0_469

0.473

0.498

0.4E7

0.518

0.53S

Source: 5A59652{,1

o.477

0.476

0.571

0 504

0.559

0.496

0 478

So|llc.: 5459652{1

m94

fl'S4

ngl

mgl

ag'l

tng'i

nel

75125

75-125

75-125

75.125

75-125

75,t25

78125

75-125 0 E 20

7U125 1 m

7ts125 l0 20

15-125 1 m

75125 4 n

75-125 2 20

7t125 | 20

6q120

* t m

8G120

80120

E0-r20

mrm8GI20

0.466

0 468

0 509

0.495

0.498

0.492

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RSn

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ru/lmq4

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Thk labrctory npon is not uolid tr'i*rou a authodzed signalurc oa tha coeer pzge

* Reportable Detectioo Limit BRL = Below Reporting Ljmit Page 147 of 154

Page 733: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Totrl Met{ls by EPA 200 Scries Methods - Quallty Control

Ar'alyt(t Result Flag UniG Result %REC Limits RPD

Bstch 7O3t809 - OqA 200 Scries

Bbnk mEl00lS1Kll

P€t€red E Aralyredi lp.Apr'07

Silwr

Sd€dwn

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Aanum

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Pregacd & Aiatzed lP-Ap.{7

Siitv€r

Sel€niun

C{dn'rrn

Chrc[nun

Barinn

lldtL Sdt fr!31809{Glt

Pr€ps€d A Andrzed: e-&r-07

Selenin

tiilr€t

ftrc|nim

cadftiun

Badum

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PrEFared t Analyzed: {B-Apr-07

SiL€r

S€l€nrum

Clroniufi

Cadnarn

Bari!fl

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Plepaled A Adyrsd: @-a$r{?

Sd€nium

sihl"r

L€iTd

Cdnhln

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Pt€pat€d & Aftlfled; (2.Apr1)7

S€l€dum

SilvEr

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0.88022692.3

So|jrl!: SA5SE{E{

146

145

145

135

140

t62

147

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143

143

144

138.lB6

135

210

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SRL

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BRL

BRL

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ARL

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trEltg*d 0.7j1

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mdtsdf r.55

@lq dy 3.11

mdlgdry 0.518

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mg^gdy 0.563

rnEhdy 0282

ftg/fg dty 1.68

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rrB4{ dry 0-54€

rrytg dry 02f4

fiSlqdry 0.822

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mE?,! Ot 0148

ndhdry 1.n

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ng^S dry 0573

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rn$Ag wot

mgJtg n6t

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3535353535

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98

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8$t158+t1585-1158+r 15&;11585t l58F115

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103i6

96

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Thb leboratoq fepod b not valLl tt'ilhout a, rr/.horhed sigaatare ol the Eover page.

* Reportrble DetectioD Limit BRI = Below Reponing Limit Page 148 of 154

Page 734: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Total Metals by EPA 200 Series Methods - Qualitv Control

Analyt€(s) Resuh Flag UnitsSpike Source

Level RcsultIRDL %REC%RICLimits

RPD

LimitRPD

Bracft 7031809 - EPA 200 Series

Ber.rrrce ttBl80g+Blt)

Prepflld & Ar€rf2edr (E{pr47

Cadniun

Saium

&acli 703182.1 - f,PAl00/S$'7O00 Sede!

Bldrl ftlElla4€Lxt I

Rep6red: 30+ra{7 &'alEed: m,ApFo7

LCS fr61@+Sltl

t"€FEd: I{rar tualyzsd: m,Apr-07

olllc.ts ao€fia€uPl I

PlrF 6A 30-r/|3r{7 tuatyz€d: 0e-Apr,07

Ltrh s{h fimst8z4{st)

R€pdEd 30{r€r{7 AnalF€d: Cr2-Aprfl

Llr SoL Olj! a7|Bl02+{SOt l

Prefercd: Sl ar{7 l.mt ed: 02-Apr.07

P.d 9d|{e flBrg2cPsil

45.833_6235

rngilg wel

mgAg lrel

rngl(g wel

1 m

0.2500.500

80.8-119.482.1n17.982.7t17.3

443

31.E

215

rg2

r06

109

8RL mg/ 0.00020

mg/l 0 00020

mg,4

0.0fr20

mg4

0.m020

0.0 0 8RL

0.00250

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0.00005

S.rilt : SA$a!}tg

o w249

So{rcs: SA508O}19

0 00260

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208Rr

8nLn'g/

75-125 20

Preps€d:3G lr{7lnalyred: o2-Apr{7

€(.1ry 0 00226 05-t 158ff1ngn

Thit laboralory report is ,tot ealid Hithou r taahoriNcd signaturc o^ the coter page.

* Reportable Det€ction Limit BRL = Below Reporting Limit Pag€ 149 of 154

Page 735: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Metals by EPA l3f2 & 6000t000 Seri€s Methods - Qrality CoDtrol

Analylqs, Result UniLs .RDLSpike

Level

%RECLimits

RPD

LimiaFlag

SourceResult %REC RPD

Betch 703lEt)5 - sw6{6 30t0A

ahnl ar(BlqE€u(1)

Prepa@di 3&ller{7 Analyredr m.Apd7

Lead

Sel€niun

Sd$er

Cirorhirn

C€dniun

Ealiltn

rcs fmr!6.4s1.)

Prepared: 3&Mar.07 AEtyz€d: (z.Aprfi

SelBniun

Sllvor

Cadnim

dllonium

Eariun

LCS Ap i7ml8{F8g)l)

Popar€d: gl-lrr{7 edyzed: m-Apr{7

S€lenhJm

Loird

Ciromium

Srh€r

kniun

Badum

u/oti.{. {7(Btg}stxP

Prepared: 30lrar.{7 lr|3 zed: @.Apr.07

Le.ad

Sddiun

SikE

Cdflkrn

Ctronium

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* Re!'{rtabl€ Det&tion Limit BRL= B€low ReportinB Limit Page l5Oof 154

Page 736: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

SPLP Metats by EPA l3l2 & 6000/7000 Series Methods - euality Control

Spike Source

B.tch 7031805 - SW846 3010A

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General Chemistry Parameaers - Quality Collarol

Andvte(t UnitsFlasResultSpike

L€vel LimirsResult %REC

Bract 7031879 - Cetr€ral Preprrrtion

o|btcrt a?tBlETgoupr)Pr€pe€d E AnalFed: 30.Mar-07% SdidE

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ThIs lahorAory reFod Lt aol valid htilhoul aB oathorited sigdaturc on the cowr page-

+ Reportable Detection Limit BRL = Below Reporting Limit Page 15l of 154

Page 737: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Noles and Delinitions

*TPH Calculated as

Comp Compl€ted

FP Field Pres€rved

QC I Analyte out ofacc€plance range.

QC2 Afilyte otrt of aEceptance tulge itr QC spike b(ll tro rcponable €ooce ratiotr preser in sample.

QCa The spike recovery is outside acceptable limils for the LCS. The batch was accefrted based upon the MS ard,/or MSDrn€eting the LCS lihirs crireria-

QM2 The RPD and/or percent recovery lior this Qc spike sample cannot be accurately calculated due to the high concetrhatiooofaoalyte irhereot in lhe sample.

QM4 Visual evaluation ofth€ sample indicales th€ RID is above the control limit due to a non.homogeneous sample matrix-

QM7 The spike tecovery was outside a{ceptatrce limib for the MS and,/or MSD. The barch was accept€d based on acceptableLCS recovery-

QM8 The spike recovery exceeded the QC coohol liEits for the MS atrd/or MSD. The batch was accepted based upotracc€ptable PS and/or LCS recovery.

QRI A-oolys€s are not conholled on RPD values ftffn sarDple concentsatio[s less than | 0 times the reporting linil QC batrhacceptsi baed on LCS and/or LCSD eC resultl.

QR2 The RPD result exceeded the QC control limits; however, both percent recoveries werc acceptable. Sample rcsults fo. theQC batch were accepted based on perceDr recoveries and completeDess of eC dar&

QR4 Analys€s are not controlled on R-PD values ftom sarrple mnceotralions less tharr th€ reporting limit. QC batch aco€pr€obased on LCS and,/or LCSD QC iesuls

QR5 RPD oul ofacccptance range.

Rol The ReportiIlg Limit for this analyte has been .ai$ed !o account for matrix ioterf€rence.

S02 The sunogate rcrovcry for this sample caotrot be accurately quaatified due to interfereuce ftom coeluting organiccompounds preseot io th€ sample ext act.

vex2 Field eKtrBcted

VOCS Reporting limits reflect SW846 5030 extraction t€cbnique due to mahix ilrt€rference usitrg Sw846 50354 €xtractiontechnique.

Z-2 Th€ MRL for this allallte bas increased due to the limited sanple yolume provided for analysis-

Z-2a The recovery ofd-BHC was outsid€ oftbe accepbrce raqge duD io a breakdou! ofd-BHC within the spike Eixtl|r.e.The CCC is within acccptable limitg, which d€monstrates rhat t[€ plobled lies wi6 tbe mixture, not the i[strumentatiotl

BRL Below Reporting Limit - Analyr€ NOT DETECTED er or above dle r€porting limit

dry Sarbple resulrs rcported oo a dry weight basis

NR Not Reported

RPD Relative Percent Differeuce

J Deteoted but b€low the Reporthg Litrril aherefore, result is atr estimated cotrce ratioD (CLp J-Flag).

A plus sign (+) io the Method Referetrc€ colunur indicatcs the method is oot accrcdited bv NELAC-

Thk [email protected] rcport B not ldtd to hoa an atthotizel dgnoUre on t*e covcr prge.

' RQortrble D€tectiotr Limit BRL = Below Reporting Limit Page 152 of 154

Page 738: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

Intemretation of TotaL Petroleum Hvd.ocarbon Report

Petrol€um ideotificatiol! is determined by coEpanng the GC firgerprint obhired liom th€ sample with a libmry ofGC fingerprintsobtained from an Vses ofvarious p€troleum products_ possible hatch categories are as follows:

Casoline - includes regular, unleaded, premium, ecc.Fuel Oil #2 - includes home heating oil, #2 tuel oil, and dieselFuel Oil it4 - includes #4 fuel oilFuel Oil li6 - includes #6 tuel oit and bunker "C', oilMotor Oil - itrcludes virgin and waste aunomobile oilI-ig.oin - idcludes mineral spirits, pettuleum naphtha, vm&p naphthaAviation Fuel - includes kerosene, Jet A turd Jp-4Other Oil - includes lubricating and cutting oil, and silicon oil

At times, fte uddentified petroleum ptoduct is quantified using a calibratior that most closely approximates the distribution ofcompounds ir the sample. When this occun, the result is quaLified as *TpH (Calculated as).

I-aborEtow conhol samDle (LCS): A krown rnatri( spiked with compouod(s) reprcs€ntativc of rhc targer analytes, which is used rodocument laboratory performance.

Matrix Duolicate: An intra-labo.atory splir samplc which is used to document the precision ofa method in a giveD sample matdx-

Mahix Soike: An aliquot ofa sample spiked with a known conceoaation oftarget a1aLyte(s) Thc spiking occurs pnorto samptepreparauml and analysis. A matrix spike is usedto document the bias ofamethod in a sivm samole malrix.

Method Blank: An anallte-free matrix to which all reagents arc added io the same votumes or proportions as [sed in sampleplocessing The method blank should be carried through the oomplete sample prepatation and analyrical procedure- Tbe methodblsnt is used to document contamination resuLting from the analltical process.

Method Detection Limit (MDL): The minimum concentrario! of a substance that carr be measuted and reponed with 997oconfidence that the analyte concentration is greater than zero and is detemined from analysis ofa sample in a given matrix typecontalning th€ analyte,

ReDortable Detection Limil aRDL): The lowest concenration that ca, be reJiably achieved within specified limirs ofFrecisioD andaccuacy durbg routine laboratory operating conditions. For many anatytes the RDL analyte conccntratioo is selected as ihe lowesttron-zero standard in the calibmtion cutve- While the RDL is approximately 5 to l0 times the MDL, the RDL for each sample takesidto account the samPle volumdwcight, exftact/digestate volurne, cleanup procedures and, ifapplicable, dry weight cofiection.Sample RDLS are highly matrixdependenr.

$qpgg@; Ar organic compound *.hich is similar to the trrger anal)4e(s) in chemical composirion and behavior ir the a@lyticalprocess, but which is not normally found in etvirormental samples_ These compounds are spiked into all blanks, standards, aods,arnpl€s prior to eielysis. Percent recovclics are calculated for each surroqate,

Validated by:Hanibal C. Tay€h, Ph.D.Nicole Brown

Thb laborulory.q,orl is not valu w hout an aurtorked sipstarc ol the corfrr page.

* Reportable Det€ction Lirnit BRL = Below Reponing l-imit Prge 153 of 154

Page 739: TASK 210: SUBSURFACE SITE INVESTIGATION - Biznet

State Of ComecticutDepartrnent of Environmental Protection

Laboratory Quality Conhol and Quality Assurance Form

' The compoands ando. elemts rcporled tre s W€cifi@lly .qu6red by dE cticnt on dE Chlin of Cudody lnd io sonE cs€s nay nor inctud€ rh€ tuttelyte list d delined in the m€thod

Negotive rcsponses lor A, B and C arc addressad in a ctse narative on the c.rrer page of rtis repo.l

I, lhe tndersigne4 attesl ander lhe pains and pnnallies ofpelaty thol btsed upon t tlt pedonal inqtit! oflhov respottsiblefor oblaining the inron ratian, rhe male.ia! codraidad irr rhis cna{.r'll.,ll re|nn 4 ro ,*e besr of my hnotrledge stut Mietaccatrqu and codplele

ffieHanibal C. Tayeh, Ph-D-Presidetrt/Labo.atory Director

Datei 414/2007

labomtory Name: Specrrum Aoalytical, Inc. - Agawam, MA Project Name aDd Number:

Projecl Location; NHRY M8 Accepbsce Facility - New tlaveb, CT NHRY M8 Acccptarce Facility - New Haven, CTl

This Form Provides cerrifrcations for the followinS dua set:sA5980l{l sA5980l-Ll

sA59E0l{2 SA59E0I-12

SAJ9EO3,03 SA5%01-13

sA59E03-04 SA59E03-|4

sA59803-05 5459803-15

sA59803-.{b SA59E03-16

saJ9803{7 SA5980l_17

SA59E03-0E 5.{5960l-t8

sA59E03-09 SA59E03-19

sA5980l-t0 sA59E03-20

List Sp€cific Analltical Methods Used:

+CI ETPH

EPA200,7

EP!. 245_tn410A,

SM254O G Mdr

SW 8,15 8?608

sw846l l l2

swE46 t]tz60LoB

sv,rE46 l3t2n470A

sw846 60108

swtil6747lA

swE45 808 | A

sw846 8062

sw846 82608

sw8ut6 E270C

sw8{6 E270CIEPA 62J I

voc

Sample Matnces:

SoiYseditunt

Were all samptes received by the laboratory ia a conditiol consisienrwith that describ€d otr the Chain ofCustody documentation for the dataset?

El Yes E No

BWere all QA"IQC procedures required for rhe rpcified analyticalmethod(s) iflcluded in this reDort followed?

El Yes E No

c Were all QC performalce stardards and r€aommeodations forrhespecifi ed methods achieved?

E Y e s E N o

DWere results for all anal)rt€-list coslpouDdv€lemetrts for the specifiedmethod(s) reporcd? E Y e s E N o *

Thit raborulory Epotl ls ,rol volitt xttdro.tt sn asthodzd sigaat'.E oa tht @ee, page.

'Rel'dtable Detection Limit BRL = Beloin Reponing Limit Page 154 of 154