Page 1
TASK 210:SUBSURFACE SITE INVESTIGATION
New Haven Rail YardTemporary M-8 Acceptance Facility
New Haven, Gonnecticut
Volume 1
ConnDOT Assignment No. 202-3464ConnDOT Project No. 301-88
Prepared for:
@State of ConnecticutDepartment of Transportation
Prepared by:
iltGfiOT'|P
Maguire Group Inc.One Court Street
Newington, Connecticut 06131 New Britain. Connecticut 06051
April24,2007
Page 2
t . 0
2.0
3.0
TABLE OF CONTENTS
INTRODUCTION
SITE DESCRIPTION
LOCAL ENVIRONMENT & RECEPTORS
3. I Groundwater
3.2 Surlace Water
3.3 Geology
SUBSURFACE INVESTIGATION
4.1 Geoprobe€) Soil Borings & Soil Sample Analyses
4.2 Ballast Grab Sample Collection & Analyses
4.3 Railroad Tie Grab Sample Collection & Analyses
4.4 Groundwater Grab Sample Collection & Analyses
4.5 Project Quality Assurance/Quality Control Practices
DISCUSSION OF SAMPLE RESULTS
5. I Regulatory Critcria
5,2 Results of Geoprobe@ Boring Soil Sample Analyses
5.3 Results of Ballast Grab Sample Analyses
5.4 Results of Railroad Tie Grab Sample Analyses
5.5 Results of Groundwater Grab Sample Analyses
5.6 QualityAssurance/QualityControl Samples
DISCUSSION OF AFF'ECTED RESOURCES
6.1 Soil Areas of Bnvironmental Concem
6.2 Railroad Tie Area of Environmental Concem
6.3 Groundwater Area of Environmental Concem
RECOMMENDATIONS
LlMITATIONS
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Figures
Figure I - Site Location Plan
Page 3
TABLE 0F CONTENTS (continued)
Figures (continued)
Figure 2a Task 2 10 Project Area & Sampling Locations
Figure 2b Task 210 Project Arca & Sampling Locations
Figure 2c Task 2 l0 Project Area & Sampling Locations
Figure 2d Task 210 Project Area & Sampling Locations
Figure 2e Task 2 l0 Project Area & Sampling Locations
Figure 2f- Task 210 Project Area & Sampling Locations
Tables
Table l(a) to l(n) Results ofGeoprobe@ Boring Soil Sample Analyses
Table 2(a) & 2(b) Results ofBallast Sample Analyses
Table 3 Results of Railroad Tie Grab Sample Analyses
Table 4(a) & 4(b) Results of Groundwater Grab Sample Analyses
Appendices
Appendix A Boring Logs (Volume 1)
Appcndix B Tables from MGI's 2005 hrterim Shop (Running Repair Shop)
Task 210 Investigation (Volume t)
Appendix C Soil Sample Laboratory Reports (Volume2)
Appendix D Ballast Sample Laboratory Reports (Volume 2)
Appendix E Railroad Tie Sample Laboratory Reports (Volume 3)
Appendix F Groundwater Sample Laboratory Reports (Volume 3)
Appendix G Q.drQC Sample Laboratory Reports (Volume 3)
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Task 210 - Subsurface Site Investigation ConnDOT Project No. 301-88
1.0 INTRODUCTION
on behalf of the connecticut Department of rransportation (connDor), Maguire Group Inc.
(MGI) has conducted a Task 210 - Subsurface Site Investigation in association with the New
Haven Rail Yard remporary M-8 Acceptance Facility project in New Havcn, connecticut. The
project will involve the construction of an acceptance area for the new M-8 rail cars and will be
locatcd to the east and southeast ofthe existing EMU Shop building. Figure I clepicts rhe project
area.
This Task 210 - Subsurface Site Investigation was conducted in areas of anticipated construction
activities for the New Haven Rail Yard remporary M-8 Acceptance Facility project. The
purpose of thc Task 210 - Subsurlace Site Investigation was to verify the absence or presence
and location of subsurlace contamination, and to assess the potential pollutant impacts to be
encountered during construction. It is anticipated that Task 310 Plans and Spccifications will
subsequently be prepared to assess construction related activities (i.e. proper storage,
classification, transport and disposal of contaminated materials), in relationship to the
envtronmental conditions prevalent within the project limits, as well as to specify remedial work
to be includcd in the Contract Bid Documents.
2.0 SITE DESCRJPTTON
This Task 210 - Subsurlace Site Investigation was conducted at the New Haven Rail Yard in the
area of the proposed Temporary M-8 Acceptance Facility. The proposed Temporary M-8
Acceptance area will be constructed to the east and southeast ofthe existing EMU Shop building
on land owned by the State of Connecticut Department of Transportation. The site area is
depicted in Figures 2a through 2f-Task 210 Project Area & Sampl.ing Locations.
ConnDOT Assisnmenl No. 202-14f,4 Page t
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Task 2 l0 - Subsurfac. Sire Inveslisarion ConnDOT Prqect No. 301-88
Numerous environmental investigations completed at the New Haven Rail Yard property have
indicated the widespread presence oftotal petroleum hydrocarbons, volatile organic compounds,
polycyclic aromatic hydrocarbons (PAHs), and RCRA 8 metals contamination, as well as
isolated occurrences of polychlorinated biphenyls (PCBs) in on-site soils and groundwater. Thc
contaminated soil has been encountercd at depths ranging from the surface (0) to approximately
eight (8) feet below the ground surface. The soil and groundwater contamination detected
exceeded the applicable Connecticut Department of Environmental Protection Remediation
Standard Regulations. In addition, the concentrations of leachable lead previously detected in
on-site soils at the site have exceeded the RCRA hazardous waste concentration in isolated areas.
3.0 LOCAL ENVIRONMENT & R.ECEPTORS
3.1 Groundwater
The 2005 edition of "Environmental GIS Data for Connccticut" provided by the CTDEP, depicts
the groundwater classification for the area as "GB." A "GB" groundwater classification
indicates that the groundwater has been adversely impacted by waste discharges, spills or leaks
of chemicals, or land use impacts. The groundwatcr is not suitable for direct human
consumption without the need for treatment and a public water supply source is available.
Groundwater was encountcred at the site at depths ranging from approximately 4 to 6 feet below
the ground surface. The New Haven Rail Yard and its surrounding properties are all connected
to the South Central Regional Water Company's public water distribution system and the City of
New Haven sewer system. In addition, there are no public water supply sources within a one-
mile radius of the Site, according to the CTDEP Bulletin 4, "The Atlas of the Public Water
Supply Sources and Drainage Basins of Connecticut," June, 1982.
ConnDOT Assienment No. 202-3464 Page 9
Page 13
Task 210 - Subsurface Site Investisation ConnDOT Project No, 301-88
3.2 Surface Water
There are no surface water bodies sinrated on the New Haven Rail Yard property- The project
area is located within the South Central Shoreline Regional Drainage Basin, within the South
Central Coast Major Drainage Basin. The general topogaphy of the site is relatively flat. Based
upon previous investigations conducted at the site, the infened direction of groundwater flow is
south,/southeast, towards Long Island Sound. Long Island Sound is located approximately %
mile southeast of the New Haven Rail Yard.
3.3 Geoloqy
The 2005 edition of "Environmental GIS Data for Connecticut" provided by the CTDEP, depicts
the surlicial materials at the site as Artificial Fill, which is described as earth materials and
manmade materials that have been artificially placed. Soil encountered during this investigation
consisted of brown to red-brown sand units, and fill comprised of black ash and cinders. The
Bedrock Geological Map of Connecticut, compiled by John Rodgers in 1985, indicates that the
bedrock unit underlying the site area is the New Haven Arkose, which is a red-brown arkosic
sandstone. Bedrock was not encountered during this investigation.
4.0 SUBSURFACEINVESTIGATION
Due to the contaminants previously detected in the soil and groundwater on the New Havcn Rail
Yard property, a comprehensive sampling program was conducted within the proposed
construction areas to be impacted by the Temporary M-8 Acceptance Facility project. The
following subsections detail the investigation.
ConnDOT Assignment No. 202-3464 Page l0
Page 14
Truk 210 - Subsurface Site Investisation ConnllOT Projcct No. 30t-88
4.1 Geoprobe@ Soil Borines & Soil Sample Analyses
On March 15, 19,21, ail26,2007, tifty{kee (53) Geoprobe@ soil borings (M8F-l to M8F-53)
were advanced in areas of anticipated construction activities for the Temporary M-8 Acceptancc
Facility. The Geoprobe@ borings were advanced by Logical Environmental Solutions, under the
direction ofMGI. The locations ofthe Gcoprobe@ soil borings are depicted on Figurcs 2ato2f-
Task 2 l0 Project Area & Sampling Locations.
The Geoprobe@ soil borings were advanced to a depth of 8 feet below grade. Continuous soil
samples were collected utilizing a 4-foot long, 2-inch diameter Macro Core Sampler with
dedicated acetate liners. Thc soil samples were visually inspected in the field for staining, and
described as to physical characteristics and soil type. In addition, the soil samples were screened
in the field for total volatile organic compounds utilizing a Photovac photoionization detector
(PID). Soil boring logs were generated in the field by Maguire field personnel. The boring logs
denote the types of soil encountered, the depth to groundwater and./or bedrock, the total depth
reached in each boring, and the highest observed PID reading. Copies of the boring logs are
included at the end ofthis report in Appendix A.
Based upon freld screening results and visual observations, one soil sample from each boring
was placed in glassware supplied by Spectrum Analytical Laboratory, and stored in an ice-filled
cooler. The shallow soil sample (2' to 4' below grade) was selected for laboratory analyses if
field screening and visual observation did not indicate the presence of contaminants in the other
sample intervals- The analyses for each soil sample included volatile organic compounds
(VOCs) utilizing EPA Method 8260, semi-volatile organic compounds (SVOCs) utilizing EPA
Method 8270, petroleum hydrocarbnns utilizing the Connecticut ETPH method, pesticides
utilizing EPA Method 8081A, polychlorinated biphenyls (PCBs) utilizing EPA Method 8082,
and total and SPLP RCRA 8 metals.
All Geoprobe@ soil borings were back-filled upon completion utilizing clean sand and/or
hydrated bentonite. All down-hole sampling equipment was decontaminated in accordance with
MGI's February 2007 Task 210 - Subsurface Site Investigation Work Plan.
ComDOT Assiunment No. 202-3464 Page I 1
Page 15
Task 210 - Subsurlbce Site Investisation ConnDOT Project No. 301-88
4.2 Ballast Grab Samnle Collection & Analvses
SLx (6) ballast grab samples were collected from selected locations where existing tracks will be
removed. The ballast grab samples were placed in glassware supplied by spectrum Analltical
Laboratory, and stored in an ice-filled cooler. The analyses for each ballast grab sample
included VOCs (EPA Method 8260), BNAs (EPA Method 8270), petroleum hyrlrocarbons
(Connecticut ETPH), pesticides (EPA Method 8081A), PCBs (EPA Method 8082), and total and
SPLP RCRA 8 metals. The locations of the ballast sample poinrs (M8FB-l rhrough M8FB-6)
are depicted on Figures 2d and2f Task 210 Prqect Area & Sampling Locations.
4.3 Railroad Tie Grab Samole Collection & Analyses
Two (2) composite railroad tie wood grab samples were collected at selected locations where
existing tracks will be removed so that specifications regarding handling and disposal of the
material can be provided. The railroad tie wood grab samples were placed in glassrvare supplied
by Spectrum Analltical Laboratory, and stored in an ice-filled coolcr. The analyses for each
wood sample included VOCs (EPA Method 8260), SVOCs (EPA Method 8270), petroleum
hydrocarbons (Connecticut ETPH), pesticides (EPA Method 8081A), PCBs (EPA Method 8082),
and total and TCLP RCRA 8 metals. The locations of the railroad tie sample points (M8FT-l
and M8FT-2) are depicted on Figures 2d and 2f Task 210 Project Area & Sampling Locations.
4.4 Groundwater Grab Samnle Collection & Analyses
Groundwater grab samples were collected from borings M8F-14, M8F-24, M8F-42, and MSF-
50. The groundwater grab samples were collected by inserting one-half inch diameter, schedule
40, l0-slot, PVC well screen and riser casing into the borehole. The 5-foot section ofwell screen
was temporarily installed approximately 4 feet into the observed water table depth. Dedicated
polyethylene tubing was placed into the temporary well and the groundwater sample was drawn
through the hrbing using a low-flow peristaltic pump.
ConnDOT Assignment No. 202-3464 Page 12
Page 16
Task 2l0 - Subsurface Site Investisatio[ CourDOT Projcct No. i0l-81t
The groundwater samples were collected for laboratory analysis of VOCs (EPA Method 8260),
SVOCs (EPA Method 8270), petroleum hydrocarbons (Connecticut ETPH), pesticides (EPA
Method 8081A), PCBs (EPA Method 8082), and roral RCRA 8 metals. The groundwarer
samples were placed in laboratory-supplied glassware, and stored in an ice-filled cooler.
4.5 Proiect Quality Assurance/Oualitv Control Practices
To assess the collection of samples in the field in terms of the sampling techniques and
decontamination procedures followed, quality control and quality assurance samples werc
collected. Four (4) trip blank samples (TB-l through TB-4) were prepared by Spectrum
Analytical Laboratory and four (4) field blank samples (FB-l tkough FB-4) were collected in
the field one on each day of sampling.
The trip blank samples were stored with the daily samples in the sample cooler until subsequent
delivery to the laboratory for analysis of VOCs. The FB-l and FB-3 field blank water samples
were collected by pouring laboratory supplied de-ionized water tluough an acctate liner and
macro-corc cutting shoe, and collecting the rinsate in appropriate sample containers. The FB-2
and FB-4 field bla* samples were collected by directly pouring the laboratory supplied de-
ionized water into the appropriate sample containers to check the quality ofthe de-ionized water,
glassware, and laboratory sample handling and analyical procedures. The field blank samples
were stored with the daily samples in the cooler until delivery to the laboratory, and were
analyzed for the same parameters as the daily samples.
All samples collected in the field were stored in a manner that preserved the integrity of the
sample chemistry. Samples intended for organic analyses were stored in an ice-filled cooler until
delivery to the laboratory. Chain-of-Custody (COC) forms were filled out and accompanied all
samples collected as a legal record of possession of the sample. The COC was initiated in the
field and accompanied the containers during sample collection, transportation to the lab,
analysis, and final disposal of the sample. All sampling equipment was either dedicated to a
specific sample or was decontaminated prior to and between each use. Sampling equipment was
not placed near solvents, gasoline, or materials that may impact the integrity of the samples.
ConnDOT Assisnment No. 202-1464 Page 13
Page 17
Task 210 - Subsurface Site tnvestigation ConnDOl' Prqcct No. 301-li8
5.1
5.0 DISCUSSION OF SAMPLE RESULTS
Regulatorv Criteria
The CTDEP adopted Remediation Standard Regulations (Regulations of Connecticut StateAgencies, Section 22a-133k-l to 3 and 22a-133q-l) as of January 31, 1996. The Remediation
Standard Regulations (RSRs) apply to any site undergoing voluntary remediation under Public
Acts 95-lf:13 or 95-190, a transfer ofan "establishment" under public Act 95-183, or any sire as
ordered by the crDEP commissioner. The Regulations also outline the processes for
establishing altemative site-specific numerical standards for certain sites, upon approval by the
CTDEP.
The RSRs criteria applicable to the soil and groundwater sampled during this investigation arc
summarized below. The application of these RSRs to the results of the laboratory analyses from
this investigation is discussed in subsections 5.2, 5.3,5.4, and 5.5 of this section.
Soils Criteria: The RSRs are organized into two sets of criteria: the Dircct Exposure Criteria
(DEC) and the Pollutant Mobility Criteria (PMC). The DEC and pMC arc briefly explained in
the following sub-sections, in relation to how they would be applicable to the t]?es of analyses
conducted on the soil samples collected for this investigation. Please refer to the RSRs for a
complete explanation of the Regulations.
Direct Exposure Criteria
The purpose ofthe DEC is to protect human health from risks associated with the direct contacr
with or ingestion of various common soil contaminants. The DEC are applicable to soil within
approximately 15 feet of the ground surface. Concentrations of contaminants are evaluated
based upon mass-based analyses and different criteria are established for residential and
commercial/industrial properties. The use of the less stringent commercial/industrial standards
requires the placement of a land use restriction on the property.
ConnDOT Assignment No. 202-3464 Page 14
Page 18
Task 210 - Subsurface Site Investigation ConnDOT Project No. 301-88
Thc DEC are not applicable to inaccessible soils, including soil more than 4 feet below theground surface, 2 feet below pavement greater than 3 inches thick, or below an existing building,provided that an Environmental Land Use Restriction (ELUR) is placed in e ffect for thepropeny.
Pollutant Mobilitv Criteria
The purpose of the PMC is to evaluate the potential for contaminants to leach from the soil inconcentrations that may degrade groundwater quality. Dilferenl numerical criteria areestablished for GA and G.dA groundwater areas, versus GB groundwater areas. since theproject area is situated within a GB groundwater area, the least stringent criteria apply.
Groundwater Criteria: Contaminants in the groundwater are compared either to backgroundquality or the Groundwater Protection Criteria (GPC), the Volatilization Criteria, as well as theSurface water Protection criteria (SWPC). The Gpc, Volatilization criteria, and SWpc arc
briefly explained in the following sub-sections, in relation to how they would be applicable to thetypes ofanalyses conducted on the groundwater samples collected for this investigation.
Grou0dwaler Prorection Criteria
The purpose of the GPC is to protect the groundwater quality in areas thar have the potential to
use gjroundwater as a drinking water resource {GA & GAA groundwater classification areas).
Since the project area is situated in a GB groundwater area, the GPC do not apply to this Site.
Volatilization Criteria
The putpose of the Volatilization Criteria standard is to ensure that volatile organic compounds(VOCs) in groundwater do not pose an unacceptable risk to human health due to the inhalation of
Vocs that may enter into a structure on the property. The Volatilization criteria only apply
when impacted groundwater is located within 15 feet of the ground surface or any structure.
Different criteria exist fbr residential and commerciaVindustrial properties. The use of the less
stringent commerciavindustrial standards requires the placement of an ELUR on the property.
Since groundwater was within 15 feet of the ground surface, the Volatilization Criteria apply to
this Site.
ConnDOT Assignment No. 202-1464 Page 15
Page 19
Tark 2 l0 - Subsurfhce Site Invcslrgation ConnDOT Project No. J0 | -88
Surface Water Protection Criteria
The purpose ofthe SWPC standards is to ensure that groundwater discharging to a surlace water
body will not adversely affect surface water quality. Since groundwater likely discharges to
Long lsland Sound, the SWPC apply to contaminants detected in the groundwater.
5.2 Results of Geoprobe@ Borins Soil Sample Analvses
soil samples collected during the advancement ofthe Geoprobe@ borings were sent to Spectrum
Analytical Laboratory for laboratory analyses. Summaries of the laboratory results from the soilsamples are presented in Tables l(a) to 1(n), which are located at thc cnd of this report, and
copies of the soil sample analytical results are included in Appendix c- The fo owing
summarizes the results of the analyses conducted on the soil samples.
Petroleum hydrocarbons were detected in the soil samples at concentrations ranging from Below
Reporting Limits (BRL) ro fl,5 l0 parrs per million (ppm). The following fifteen ( I 5) soil
samples contained rPH at concentrations that exceed the crDEp Residential DEC of 500 ppm:
MgF-'7,2' to 4' (5,070 ppm); M8F-8, 2' to 4' (3,020 ppm); M8F-9, Z' to 4' (2,450 ppm); M8F-
1 0 , 2 ' t o 4 ' ( 2 , 6 6 0 p p m ) ; M 8 F - 1 3 , 2 ' t o 4 ' ( 8 9 9 p p m ) ; M 8 F - 1 7 , 4 ' t o 6 ' ( 8 , 5 l 0 p p m ) , M 8 F - 1 9 ,
2' to 4' (3,260 ppm); M8F-23, 2' to 4' (5s4 ppm); M8F-28, 2' to 4' (932 ppm); M8F-35, 2' to 4'
(2,480 ppm); M8F-40, 2'to 4' (797 ppm), M8F-41, 4' to 6' (128 ppm); M8F-42, 2, to 4, (776
ppm); M8F-46, 2' to 4'(1,150 ppm); and M8F-47,2, to 4, (t ,310 ppm). The petroleum
hydrocarbon concentration detected in the M8F-7, 2' to 4,, M8F-8, 2, to 4,, M8F-10, 2' to 4',
M8F-17, 4' to 6', and M8F-19,2'to 4' samples also exceed the CommerciaVlndustrial DEC of
2,500 ppm. No other sample contained petroleum hydrocarbons at concentrations that exceed
any applicable CTDEP RSR criteria.
The VOCs benzene, ethylbenzene, isopropylbenzene, naphthalene, n-propylbenzene, styrene,
tetrachloroethene, toluene, 1,2,4-trichloroethene, and total xylenes were detected at varying
concentrations in the soil samples collected from borings M8F-5, M8F-14, M8F-15, M8F-17,
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Tas l 210 - Subsur lacc S i te Inves t tea t ron ConnDOT Project No. 301-81i
M8F-19, MBF-24, M8F-29, M8F-31, M8F-38, M8F-39, M8F-40, M8F-42, M8F-45, and M8F-
47. The 2 to 4 foot sample collected from boring M8F-14 contained the VOC benzcne (1.52
ppm) at a concentration that exceeds its GB PMC of 0.2 ppm. No other soil sample contained
VOCs at concentrations that exceed any applicable CTDEP RSR criteria.
Various concentrations of SVOCs were detected in the soil samples, and total SVOC
concentrations ranged from BRL to 289.93 ppm. Twelve (12) soil samples contained
concentrations of SVOCs that excecd applicable CTDEP RSR Criteria. The 2 to 4 foot sample
from boring M8F-l contained the compounds benzo(a)anthracene (1.12 ppm), benzo(a)pyrene
(1.09 ppm), benzo(b)fluoranthene (1.12 ppm), benzo(k)fluoranthene (1.16 ppm), and chrysene
(1.38 ppm) at concentrations that exceed their respective GB PMC. In addition, the compounds
benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene were detected at concentratlons
that exceed their respcctive Residentral DEC. The compound benzo(a)plrene was detected at a
concentration that also exseeds its Commercial/Industrial DEC.
The 2 to 4 foot sample from boring M8F-7 contained the compounds benzo(a)anthracene (3.85
ppm) and chrysene (4.9 ppm) at concentrations that exceed their respective GB PMC. In
addition, the compound benzo(a)antluacene was detected at a concentration that exceeds its
Residential DEC.
The 2 to 4 foot sample from boring M8F-8 contained the compounds benzo(a)anthracene (1.74
ppm) and chrysene (2.17 ppm) at concentrations that exceed their respective GB PMC. In
addition, thc compound benzo(a)anthracene was detected at a concentration that exceeds its
Residential DEC.
The 2 to 4 foot sample from boring M8F-9 contained the compounds benzo(a)anthracene (1.7
ppm) and chrysene (.2.21 ppm) at concentrations that exceed their respective GB PMC. In
addition, the compound benzo(a)anthracene was detected at a concentration that exceeds its
Residential DEC.
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Task 2 l0 - Subsurfacc Srte lnvestiea(ion ConnDOT Proyect No. 301-88
The 2 to 4 foot samplc from boring M8F-14 contained the compounds benzo(a)anthracene (1.51
ppm), benzo(a)pyene (l .89 ppm), benzo(b)fluoranthcne ( l.tl6 ppm), benzo(k)fluoranthene (2.03
ppm), and chrysene (1.84 ppm) at concentrations that exceed their respective GB PMC. In
addition, the compounds benzo(a)anthracene, benzo{a)pyrene, and benzo(b)fluoranthene were
detected at concentrations that exceed their respective Residential DEC. The compound
benzo(a)pyrene was detected at a concentration that also exceeds its CommerciaVlndustrial DEC-
The 2 to 4 foot sample from boring M8F-17 contained the compounds benzo(b)fluoranthenc
(l.la ppm) and chrysene (1.37 ppm) at concentrations that exceed their respective GB PMC. In
addition, the compound benzo(b)fluoranthene was detected at a concentration that exceeds its
Residential DEC.
The 2 to 4 foot sample from boring M8F-23 contained the compounds benzolb)fluoranthene
(1.37 ppm), benzo(k)fluoranthene (1.18 ppm), and chrysene (1.09 ppm) at concentrations that
exceed their respective CB PMC. In addition, the compound benzo(b)fluoranthene was detected
at a concentration that exceeds its Residential DEC.
The 2 to 4 foot sample from boring M8F-25 contained the compound chrysene (1.18 ppm) at a
concentration that excecds its GB PMC.
The 2 to 4 foot sample from boring M8F-31 contained the compounds benzo(a)pytene (1.2
ppm), benzo(b)fluoranthene (1.02 ppm), benzo(k)fluoranthene ( l.l6 ppm), and chrysene (1.39
ppm) at concentrations that exceed their respective GB PMC. In addition, the compounds
benzo(a)pyrene and benzo(b)fluoranthene were detected at concentrations that exceed th€ir
respective Residential DEC. The compound benzo(a)pyrene was detected at a concentration that
also exceeds its Commercial/Industrial DEC.
The 2 to 4 foot sample from boring M8F-35 contained the compounds benzo(a)anthracene (28.0
ppm), beuo(a)pyrene (28.2 ppm), benzo(b)fluoranthene (29.2 ppm), benzo(k)fluoranthene (36.3
ppm), chrysene (33.8 ppm), indeno( 1,2,3-cd)pyrene (12.7 ppm), and pyrene (58.5 ppm) at
concentrations that exceed their respective GB PMC. In addition, the compounds
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Task 210 - Subsurface Site lnvestisation ConnDOT Projcct No. l0 | -t j8
benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, and
indeno( | ,2,3-cd)pyrene were detected at concentrations that exceed their respective Residential
DEC. The compounds benzo(a)anthracene, benzo(a)plrene, benzo(b)fluoranthene, and
indeno( 1,2,3-cd)pyrene were detected at concentrations that also exceeds their respective
Commercial/Industrial DEC.
The2to 4 foot sample from boring M8F-37 contained the compounds benzo(a)anthrac ene (2.47
ppm), benzo(a)pyrene (2. I 5 ppm), benzo(b)fluoranthene (2.61 ppm), benzo(k)fluoranthene (2.47
ppm), and chrysene (3.37 ppm) at concentrations that exceed their respective GB PMC. In
addition, the compounds benzda)antkacene, benzo(a)pyrene, and benzo(b)fluoranthene were
detected at concentrations that exceed their respective Residential DEC. The compound
benzo(a)py,renc was detected at a concentration that also exceeds its Commercial/Industrial DEC.
The 4 to 6 foot sample from boring M8F-41 contained the compounds benzo(a)anthracene (1.41
ppm), benzo(a)pgene (1 .27 ppm), benzoib)fluoranthene (1.67 ppm), benzo(k)fluoranthene (1.84
ppm), and chrysene (2.18 ppm) at concentrations that exceed their respective GB PMC. In
addition, thc compounds benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene were
detected at concentmtions that cxceed their respective Residential DEC. The compound
benzo(a)pyrene was detected at a concentration that also exceeds its CommerciaVlndustrial DEC.
The pesticides 4,4-DDD, 4,4-DDE, 4,4-DDT, a-chlordane, g-chlordane, and dieldrin were
detected at varying concentrations in the M8F-4, M8F-21, and M8F-15 soil samples. The 2 to 4
foot sample from boring MBF-35 contained the pesticide dieldrin (0.0625 ppn) at a
concentration that exceeds its the GB PMC of 0.007 ppm and Residential DEC of 0.038 ppm.
No other pesticides were detected at concentrations that exceed any applicable CTDEP RSR
criteria.
PCBs (total) were detected at varying concentrations ranging from 0'0171 ppm to 3-5 ppm in the
soil samples collected from borings M8F-2, M8F-4, M8F-5, M8F-6, M8F-12, M8F-13, MSF-16,
M8F-17, M8F-18, M8F-19, M8F-20, M8F-21, M8F-22, M8F-23, M8F-25, M8F-26, M8F-31,
M8F-32, M8F-35, M8F-40, M8F-46, and M8F-47. The 2 to 4 foot samples from borings M8F-
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TasL 2 l0 - Suhsurfice Site lnr esrisarion ConnDO'l' Projecr No. 30l-88
12 (2.12 ppm) and M8F-13 (3.5 ppm) contained total PCBs at concentrations that exceed the
Residential DEC of I ppm. No other sarnple contained PCBs at concentrations that excced any
applicable CTDEP RSR crircr ia.
Total concentrations of the metals arsenic, barium, cadmium, ckomium, lead, mercury,
selenium, and silver were detected at varying concentrations in the soil samples tkoughout the
site. The following seventeen (17) soil samples contained total arsenic at concentrations that
exceed the CTDEP Residential and CommerciaVlndustrial DEC of l0 ppm: M8F-5,2' to 4'
(14.4 ppm); M8F-6, 2' to 4'(13.6 ppm); M8F-7, 2' to 4' (10.4 ppm); M8F-t2, 2' ro 4' (12.2
ppm); M8F-l 3, 2' ro 4' ( l 3. I ppm); M8F-15, 4' ro 6' (29.3 ppm); M8F-20, 2' ro 4' (10.3 ppm);
M 8 F - 2 5 , 2 ' t o 4 ' ( r 0 . 1 p p m ) ; M 8 F - 3 5 , 2 , t o 4 ' ( 1 7 . j p p m ) ; M 8 F - 3 6 , 4 ' t o 6 , ( l 1 . l p p m ) ; M 8 F -
J7, 2' to 4' (28.8 ppm); M8F-38, 2' to 4' (20.5 ppm); M8F-39, 2' ro 4' ( l 1.8 ppm); M8F-40, 2'
to 4' (10.4 ppm); M8F-45, 4' to 6' (.2t.6ppm); M8F-46, 2' to 4' (19.j ppm); and M8f-4'/, Z'
to 4' (10.7 ppm). The following three (3) soil samples contained total lead at concentrations rhat
exceed the CTDEP Residential DEC of 500 ppm: M8F-13, 2' ro 4' (518 ppm); M8F-15, 4, ro 6'
(841 ppm); and M8F-21, 2' to 4'(694 ppm); No orher sample contained total metals at
concentrations that exceed any applicable CTDEP RSR criteria.
Leachab.le co centrations (via SPLP) of barium, chromium, and lead were detected at r.arying
concentrations in the soil samples. However, the concentrations of leachable metals detected in
the soil samples do not exceed any applicable CTDEP RSR criteria.
f,.J Results of Ballast Grab Samole Analvses
The six ballast grab samples (M8FB- I through MSFB-6) collected during rhis Task 2 l0
investigation were sent to Spectrum Analyical Laboratory for laboratory analyses. Summaries
of the laboratory results from the ballast grab samples are presented in Tables 2(a) and 2 (b),
which are located at the end of this report, and copies of the ballast grab sample analy.tical results
are included in Appendix D. The following summarizes the results of the analyses conducted on
the ballast grab samples. For the purpose of comparison, the results of the ballast grab sample
analyses were compared to the CTDEP RSR soil criteria.
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Task 210 - Subsurt'ace Site Invcstisation ConnDOT Project Nr-r. l0l-88
Petroleurn hydrocarbons, VOCs, SVOCs, pesticides, and PCBs were not detected in the ballast
grab samples. Total and leachable concentrations of the metals barium, cadmium, chromium,
and lead were detected at varying concentrations in the ballast grab samples. However, the
samples did not contain total or leachable metals at concentrations that exceed any CTDEP RSR
criteria.
5.4 Results of Railroad Tie Gtab Sample Analvses
The two railroad tie grab samples (M8FT- I and MSFT-2) collected during this Task 2 l0
investigation were sent to Spectrum Analytical Laboratory lor laboratory analyses. Summaries
of the laboratory results fiom the railroad tie grab samples are presented in Table 3, which is
located at the end of this report, and copies of the railroad tie grab sample analltical results are
included in Appendix E. The following summarizes the results of the analyses conducted on the
railroad tie grab samples. For the purpose of comparison, the results of the railroad tie grab
sample analyses were compared to the CTDEP RSR soil criteria.
Petroleum hydrocarbons were detected in the M8FT-l (l1,600 ppm) and M8FT-2 (33,600 ppm)
samples at concentrations that exceed the GB PMC and Residential DEC of 500 ppm, and thc
CommerciaUlndustrial DEC of 2,500 ppm. Both of the railroad tie samples contained the VOC
naphthalene at low concentrations of 6.02 ppm and 5.69 ppm, which do not exceed any CTDEP
RSR criteria.
The railroad tie samples contained several SVOCs at varying concentrations. The M8FT- I
sample contained the SVOCS benzo(a)anthrac ene (227 ppm), benzo(a)pyene (99.3 ppm),
benzo(b)fluoranthene (160 ppm), benzo(k)fluoranthene (lti7 ppm), carbazole (152 ppm),
chrysene (358 ppm), dibenz(a,h)anthracene (10.9 ppm), dibenzofuran (26.9 ppm), fluoranthene
(876 pprn), indeno( 1,2,3-cd)pyrene (40.4 ppm), phenanthrene (463 ppm), and pyrene (640 ppm)
at concentrations that exceed their respective GB PMC. The compounds benzo(a)anthracene,
benzo(a)pytene, benzo(b)fluoranthene, benzo(k)fluoranthene, carbazole, chrysene,
dibenz(a,h)anthracene, and indeno( 1,2,3-cd)p),rene were also detected at concentrations that
exceed their respective Residential DEC. In addition, the compounds benzo(a)anthracene,
CorurDOT Assisnmenl No, 201-1464 Page 2I
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Task 210 - Subsurface Site Investisation ConnDOT Project No. 30t-U8
benzo(a)pyrenc, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)antkacene, and
indeno( 1,2,3-cd)pyrene were detected at concentrations that exceed their respective
Commercial/Industrial DEC.
The M8FT-2 sample contained the SVOCs benzo(a)anthracene (137 ppm), benzo(a)pyrene (54.3
ppm), benzo(b)fluoranthene (144 ppm), benzo(k)fluoranthene (143 ppm), carbazole (199 ppm),
chrysene (449 ppm), dibenz(a,h)antfuacene (6.38 ppm), dibenzofuran (19.3 ppm), fluoranthene
(369 ppm), indeno( 1,2,3-cd)pyrene (24.4 ppm), phenanthrene (l5l ppm), and plrene (301 ppm)
at concentratlons that exoeed their respective GB PMC. The compounds benzo(a)anthracene,
benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, carbazole, chrysene,
dibenz(a,h)anthracene, and indeno( 1,2,3-cd)pyrene were also detected at concentrations that
exceed their respective Residential DEC. In addition, the compounds benzo(a)anthracene,
benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthcne, dibenz(a,h)anthracene, and
indeno(1,2,3-cd)pyrene were detected at concentrations that exceed their respcctive
Commercial/Industrial DEC.
The railroad tie samples did not contain detectable concentrations of pesticides. Total PCBs
were detected in the MSFT-I (0.332 ppm) and M8FT-2 (1.255 ppm) samples. The PCB
concentration detected in the MIIFT-2 sample exceeds the Residential DEC of I ppm.
Total and leachable (via TCLP) concentrations of the metals barium, cadmium, chromium, lead,
and mercury were detected at varying concentrations in the railroad tie grab samples. However,
the samples did not contain total or leachable metals at concentrations that exceed any CTDEP
RSR criteria.
Results of Groundwater Grab Sample Analvses
The four (4) groundwater grab samples (M8F-14 GW, M8F-24 GW, M8F-42 GW, and M8F-50
GW) collected from the site during the advancement of the Geoprobe@ borings were sent to
Spectrum Analytical Laboratory for laboratory analyses. Summaries of the laboratory results
from the groundwater grab samples are presented in Tables 4(a) and 4(b), which are located at
ComDOT Assignment No. 202-3464 Page 22
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Task 210 - Subsurface Site lnvestisation ComDOT Project No. 301-88
the end of this report, and copies of the groundwater anal)tical results are included in Appendix
F. The following summarizes the results of the groundwater grab sample analyses.
The groundwater samples did not contain detectable concentrations of VOCs, pesticides, and
PCBs. The M8F-24 GW sample contained petroleum hydrocarbons at a concentration of 1.0
ppm, which does not exceed any applicable CTDEP criteria. No other groundwater sample
contained detectable concenfiations of oetroleum hvdrocarbons.
SVOCs were detected in varying concentrations in the M8F-14 GW and M8F-24 GW samples.
The M8F-14 GW sample contained the compounds benzo(a)anthracene (0.425 parts per billion
[ppb]), benzo(b)fluoranthene (0.762 ppb), bcnzo(k)fluoranthene (0.65 ppb), and phenanthrene
(0.35 ppb) at concentrations that exceed their respective SWPC. No other SVOCs were detected
at concentrations that exceed any applicable CTDEP RSR criteria.
The groundwater samples contained total arsenic, barium, cadmium, chromium, lead, and
mercury at varying concentrations. The MSF-14 GW sample contained total arsenic {0.007 ppm)
and total chromium (15.7 ppm) at concentrations that exceed their respective SWPC of 0.004
ppm and 0.11 ppm. The M8F-24 GW sample contained total mercury (0.00221 ppm) at a
concentration that exceeds its SWPC of 0.0004 ppm. The M8F-42 GW sample contained total
lead (0.0132 ppm) at a concentration that exceeds its SWPC of 0.013 ppm. The M8F-50 GW
sample contained total arsenic (0.0062 ppm) at a concentration that exceeds its SWPC of 0.004
ppm. No other metals were detected at concentrations that exceed any applicable CTDEP RSR
criteria.
5.6 Ouali tyAssurance/Quali tvControlSamples
The field blank samples (FB-l through FB-4) did not contain detectable concentrations of
contaminants. In addition, the trip blank samples (TB-l through TB-4) did not contain VOCs at
concentrations that exceed any laboratory detection limits. Copies of the anall'tical reports
associated with the quality assurance/quality control samples are included in Appendix G.
ConnDOT Assisnment No. 202-3464 Page 23
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Task 210 - Subsurface Site Investieation ConnDOT Project No. 301-88
6.0 DISCUSSION OF AFFf,CTED RESOURCES
6.1 Soil Areas of Environmental Concern
Based upon the results of laboratory analyses perfomed on the soil samples for this Task 210
investigation, as well as the analJtical results of soil samples collected from within the projcct
area during MGI's February 2005 Task 210 for the Interim Shop (Running Repair Shop), four
(4) soil areas of environmental concem (AOECs) have been identified where contaminants are
present at concentrations that exceed applicable CTDEP RSR criteria. In addition, the remainder
of the project site has been designated as a low-level area of environmental concern (LLAOEC)
for soil. In these areas contaminants were detected at concentrations below applicable CTDEP
RSR standards, but above laboratory detection limits. The locations of the AOECs within the
project area are discussed in the following sections. Tables summarizing the analy'tical results
from soil samples collected during MGI's February 2005 Task 2 l0 for the Interim Shop
(Running Repair Shop) are included in Appendix B of this report. In addition, the locations of
the 2005 borings (denoted as IS-#) are depicted on Figures 2a and 2b Task 210 Project Area &
Sampling Locations.
AOEC #l: Area Encomnassing Borings M8F-l & 15-6:
Analfical results from the soil samples collected from borings M8F-1 and 15-6 indicate the
presence ofSVOC contamination at slightly elevated concentrations in shallow soil ranging from
2 to 4 feet below grade. The contamination detected exceeds the GB PMC, Residential DEC,
and CommerciaVlndustrial DEC.
AOEC #2: Area Encompassing Borings M8F-5. M8F-6. M8F-12. M8F-13, M8F-14,
M8F-15. IS-8 . IS-10 . IS-11 . IS-12 . IS-13 . IS- ls . & IS-18 :
Analytical results from the soil samples collected from borings M8F-5, M8F-6, M8F-12, M8F-
i3, M8F-14, M8F-15, IS-8, IS-10, IS-11, IS-12, IS-13, IS-15, and IS-18 indicate the presence of
total arsenic, total lead, petroleum hydrocarbon, VOC (beruene), SVOC, and PCB contamination
ConnDOT Assierunent No. 202-3464 Page 24
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Task 210 - Subsurlace Sirc Investieation ConnDOT Project No. l0l-88
at elevated concentrations in shallow soil ranging from 2 to 8 feet below grade. The
contamination detected exceeds the GB PMC, Residential DEC, and Commercial/lndustriai
DEC.
AOEC #3: Area Encomoassine Borings M8F-7. M8F-8, M8F-9. M8F-10. & M8F-11:
Analytical results from the soil samples collected from borings M8F-7, M8F-8, M8F-9, and
M8F-10 indicate the presence ofpetroleum hydrocarbon, SVOC, and total arsenic contamination
at elevated concentrations in shallow soil ranging from 2 to 4 feet below grade. The
contamination detected exceeds the GB PMC and Residential DEC. This AOEC also
encompasses boring M8F- I l, although contaminants at this location were detected at
concentrations slightly below CTDEP RSR criteria.
AOEC #4: Area Encompassing Borines M8F-17. M8F-19. M8F-20. M8F-21. M8F-21,
M8F-25. M8F-26. M8F-28, M8F-31. M8F_32. M8F-35. M8F_36. M8F_37.
M8F-38. M8F-39. M8F-40. M8F-41. M8F_42. M8F_45. M8F-46 & M8F_47:
Analyical results from the soil samples collected from borings M8F-1?, M8F-19, M8F-20,
M8F-21, MnF-23, M8F-2s, M8F-28, M8F-31, M8F_35, M8F_36, M8F_37, M8F_38, M8F-39,
MBF-40, M8F-41, M8F-42, M8F-45, M8F-46, and M8F-47 indicate the presence of toral arsenic,
total lead, petroleum hydrocarbon, svoc, and pesticide (dieldrin) contamination at elevated
concentrations in shallow soil ranging from 2 to 6 feet below grade. The contamination detected
exceeds the GB PMC, Residential DEC, and CommerciaVlndustrial DEC. This AOEC also
cncompasses borings M8F-26 and M8F-32, although contaminants at these locations were
detected at concentrations slightly below CTDEP RSR criteria.
ConnDOT Assignment No. 202-3464 Page 25
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Task 2 i0 - Subsurfacc Sire Inveslisation ConnDOT Projcct No. 301-81{
6.2 Railroad Tie Area of Environmental Concern
Analytical results from the railroad tie grab samples indicate the presence of petroleum
hydrocarbons, SVOCs, and PCBs at elevated concentrations that exceed the GB PMC.
Residential DEC, and Commercial/lndustrial DEC. The concentrations however, do not exceed
the RCRA hazardous waste toxicity concentrations. All areas where railroad ties will be
removed from the project site have been designated as a Railroad Tie Area of Environmental
Concern (RTAOEC).
6.3 Groundwater Area of Environmental Concern
Analytical results from the groundwater samples collected from borings M8F-14, M8l.-24, M8F-
42, and M8F-50 indicate the presence of SVOCs, total arsenic, total chromium, total mercury,
and total lead at concentrations that exceed the SWPC. In addition, the M8F-24 groundwater
sample containcd petroleum hydrocarbons at a concentration that does not exceed any applicable
CTDEP criteria, but may impact allowable discharge permit limits. Therefore, the entire project
area has been designated as a Groundwater Area of Environmental Concem (GWAOEC).
ConnDOT Assisnment No. 202-1464 Page 26
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Task 210 - Subsurface Site Investigation ConnDOT Pro.lect No. -10 t -88
7.0 RECOMMENDATIONS
The results of the Task 210 - Subsurface site Investigation for the New Haven Rail yard
Temporary M-ll Acceptance Facility project in New Haven, Connecticut indicate the presence of
petroleum hydrocarbon, VOC, SVOC, PCB, pesticide, total arsenic, and total lead contamination
in shallow soil samples collected from the project area, at concentrations that exceed the
applicable RSR criteria. Soil samples collected from within the project area in 2005 by MGI
during the lnterim Shop (Running Repair Shop) Task 210 indicated similar results. The
contamination was detected in soils ranging in depth from 2 to 8 feet below grade. Railroad tie
samples collected from areas where the railroad tracks will be removed indicate the presence of
petroleum hydrocarbons, SVOCs, and PCBs at concentrations that sxceed the CTDEP RSR
criteria, but not the RCRA hazardous waste toxicity concentrations. Groundwater collected frorn
the site is also contaminated with SVOCs and total metals at concentrations that exceed
applicable RSR criteria. In addition, concentrations of petroleum hydrocarbons were detected in
the groundwater collected from within the project area, which may impact discharge permit
requirements. Four (4) Areas of Environmental Concern (AOECs) for soil, a site-wide Railroad
Tie Area of Environmental Concem (RTAOEC), and a site-wide Groundwater Area of
Environmental Concem (GWAOEC) have been identified within the project area. In addition,
the remainder of the project site has been designated a Low Level Area of Environmental
Concem (LLAOEC) for soil. Special considerations for treatmenVdisposal, dewatering
activities, and worker health and safety must be given to these areas in order to ensure
compliance with all local, State and Federal laws. Task 310 Plans and Specifications are
therefore recommended for the areas of construction within the Areas of Environmental Concem
and Low-Level Areas of Environmental Concem addressins the soil. railroad ties and
groundwater described in Section 6.0.
ComDOT Assisnmenr No. 202-3464 Page 27
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Task 2 t0 - Subsurface Site Investisation ComDOT Prqiect No. 301-88
8.0 LIMITATIONS
All work product and reporls provided by Maguire Group Inc. (MGI) in connection with the
performance of this Task 210 - Subsurface Site Investigation are subject to the following
limitations:
I . The observations described in this reporl were made under the conditions stated therein. The
conclusions presented in the report were based solely upon the services described therein,
and not on scientific tasks or procedures beyond the scope of dcscribed services provided to
ConnDOT.
2. In preparing this report, MGI has relied on certain information provided by State and local
offrcials and inlormation and representations made by other partics referenced therein, and
on information contained in the files of State and/or local agencies made available to MGI at
the time of this investigation. To the extent that such files are missing, incomplete or not
provided to MGI, MGI is not responsible. Although there may have been some degree of
ovcrlap in the information provided by these various sources, MGI did not attempt to
independently verity the accuracy or completeness of all information reviewed or received
during the course of this investigation.
3. The conclusions and recommendations contained in this report are based in part upon the
data from subsurface explorations. The nafure and extent of variations between these
explorations may not become evident until further explorations are completed. If variations
or other latent conditions become evident, it will be necessary to re-evaluate the conclusions
and recommendations of this reoort.
4. The water level readings made lor this investigation were made at the times and conditions
stated on the boring logs. However, it must be noted that fluctuations in the level of the
groundwater may occur due to variations in rainfall, passage of time and other factors.
Should additional data become available in the future, these data should be reviewed by
MGI, and the conclusions and recommendations presented herein modihed accordingly.
ComDOT Assignment No. 202-3464 Page 28
Page 32
Task 2 l0 - Subsurface Sile lnvesrisation ConnDOT Project No. 30 i -llll
5. Where quantitative laboratory analyses have been conducted by an outside certified
laboratory, MGI has relied upon the data provided, and has not conducted an independent
evaluation ofthe reliability ofthese tests.
6. If thc conclusions and recommendations contained in this report are based, in part, upon
various types of chemical data then the conclusions and recommendations are contingent
upon the validity ofsuch data. These data have been reviewed and interpretations made in
the reporl. It should be noted that variations in the types and concentrations of contaminants
and variations in thcir flow paths may occur due to seasonal water table fluctuations, past
disposal practices, the passage of time, and other factors. Should additional chemical data
become available in the future, these data should be reviewed by MGi and the conclusions
and recommendations presented herein modified accordingly.
7. Chemical analyses were performed for specific parameters during the course of this
investigation, as described in the text. However, it should be noted that testing for all known
chemical constituents was not performed. The conclusions and recommendations contained
in this reporl are based only upon the chemical constituents tbr which testing was
accomplished.
The following qualifications apply to the undersigned's opinton:
The activities described and opinions included herein are based on information gathered during
this subsurface site investigation, which was limited in scope in adherence to the terms of our
agreement. The professional opinion provided herein is based on the information described in
this report.
ConnDOT Assigrrment No. 202-J464 Page 29
Page 33
Task ? l0 - Subsurface Sitc Investisation ConnD0T Project No. 301-88
The inlormation contained herein was prepared for the use of ConnDOT solely in conjunction
with the task descriptions for this assignment. The conclusions and recommendations set forth in
this report are based on site conditions at the time of the investigation. Future studies and
findings could change the contents of this repoft. The professional opinions presented in this
report have been developed by using that degree of care and skill ordinarily exercised, under
similar circumstances, by reputable environmental engineering consultants practicing in this or
similar localities. No other warranty, expressed or implied, is made as to the professional
opinions included in this report.
Prepared by: Approved by: Reviewed by:
Jane Witherell, P.E., L.E.P.Principal EngineerLogical Env. Solutions
David R. Stock, P.E.Program Manager
ConnD0T Assisnment No. 202-3464 Page 30
Page 35
TABLE l(a) - Results ofceoprob€@ Boring Soil Sample AnalysesNew Haven Rail Yard M-8 Acceptance Facility
New Haven. Connecticut
Boring I.D-:
Sample Depth:
M8F. I M8F.2
2',-4'
M8F-3
z'4'
M8F-4
z',-4',
CTDEP PMC GBGroundwater
Area
CTDEP DEC ResidentiaUCommercial & Industrial
CT ETPH - (ppm) t 5 9 83.5 BRL 67 .4 2,500 ppm 500/2,500 ppm
VOCS - Method 8260 (ppm) BRL BRL BRL BRL
SVOCs - Method 8270 (ppm)
tsenzo(a)antkacene
Benzo(a)pyrene
Benzo(b)fluoranthene
B€nzo(k)fluoranthene
Chrysene
Fluoranthenc
Pyr€ne
Total SVOCs
1.12
r.09
1.12
l. t6
I.3E
2 . 1 5
2 . 1 3
t 0 . l 5
BRl-
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
I ppm
I ppm
I ppm
I Ppm
I ppm
56 ppm
40 ppm
l/7-ti ppm
Ul ppm
l/7.8 ppm
8.4/7ll ppm
84/780 ppm
1 ,00012,500 ppm
1,000/2,500 ppm
Pesticides - Method 8081 (ppm)
4,4-DDD
4,4.DDE
4,4.DDT
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
0.0082
0.00871
0.0142
None Established
None Established
None Established
2.6i24 ppm
1.8/17 ppm
1.8/ t7 ppm
PCBS Method 8082 (ppm) BRL 0.0588 BRL 0.0219 Not Applicable l /10 ppm
Total RCtu{ 8 Metals ppm
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
3.16
37.3
0.3 94
82.6
t t7
0.34
3.9'7
44.5
0.49
44.3
269
0.222
8.1
18.2
BRL
1 .93
3 5 . 8
BRL
9.9
52.4
l . t 9
26,2
t't 6
0 . 1 5 8
Not Applicable
10/10 ppm
4,700/140,000 ppm
34/l,000 ppm
100/100 ppm
500/1,000 ppm
20/610 ppm
SPLP RCR,{ 8 Metals - ppm
Barium
Cbromium
Lead
0.0198
0 . 0 1 3
0.0319
0 . 0 2 1 I
0.0148
0.0424
0.01 I
BRL
BRL
0.012
0.0t22
0.0217
10.0 ppm
0.5 ppm
0.15 ppm
Not Applicablc
BRL - Below Reporting Limits (see labofatory reports for compound specihc detection limits)
The compounds listed above ar€ those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.
Page 36
' I ABLE 1(b) - Results of ceoprobe@ Boring Soil Sample AnalysesNew Haven Rail Yard NI-8 Acceptance Facilit-v
New Haven, Connecticut
BRL - tsclow Reporting Limits (see laboratory reports for compound specihc detection lirnits)
The compounds listed abovc are those that were detected - please see laboratory reports for full lists ofcompounds and their specihc detection limits.
Boring I.D.:
Sample Depth:
M8F-5 M8F-6 M8F-7 M8F-8 CTDEP PMC GBGroundwater
Area
CTDEP DEC ResidentiaVCommercial & Industrial
CT ETPH - (ppm) 2 5 1 205 t,070 3,020 2.500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm)
Tetrachloroethene 0.00?5 BRL BRL BRL 1.0 ppm l2l I 10 ppm
SVOCs - Method 8270 (ppm.)
Benzo(a)anthracen€
Chlysene
Fluoranthene
P].rene
Totat SVOCS
BRL
BRL
BRI-
BRL
BRL
BRL
BRL
BRL
BRL
BRL
3.85
4.9
9 . 3 7
r 0.228.32
1.74
2.17
4 . 1 1
) .o)
t3.6'7
I ppm
I ppm
56 ppm
40 ppm
1/7.8 ppm
84/780 ppm
1,00012,500 ppm
1,00012,500 ppm
Pesticides - Method 8081 (ppm) BRL BRL BRL BRL
PCBs Method 8082 (ppm) 0.0399 0,0713 BRL BRL Not Applicable 1i 10 ppm
Total RCRA 8 Metals - ppm
Arsemc
Barium
Cadmium
Chromium
Lead
Mercury
14.4
53.6
1 . 6 8
25.0
268
0. t9
13.6
5 S . l
t .91
297
0.208
10.4
91.6
0 . 8 1 8
22.5
5'1.4
l . 7 t
4.86
47 .0
0.4t1
l0. t
28.3
0 . 9 1 2
Not Applicable
10/10 ppm
4,700/ t40,000 ppm
34/ 1,000 ppm
100/100 ppm
500/1,000 ppm
20/610 ppm
SPLP RCRA 8 Mctals - ppm
Barium
Chromium
Lead
0 . 0 1 7
0.0105
0.0507
0.0155
0.007
0.0454
0.0106
BRL
BRL
0.012
BRL
BRL
10.0 ppm
0.5 ppm
0.15 ppm
Not Applicable
Page 37
TABLE l(c) - Results of Geoprobe@ Boring Soil Sample AnalyscsNew Haven Rail Yard M-8 Acceptance F'acilify
New Havcn, Connecticut
Boring I,D.:
Sample Depth:
M8F-g M8F- 10 M8F- l I
2'4',
M8F-12
2'-4',
CTDEP PMC CBGroundwater
Area
CTDEP DEC Residcntial/Commercial & Industrial
CT ETPH - (ppm) 2,450 2,660 BRL 263 2,500 ppm 500/2,500 ppm
VOCS - Method 8260 (pFm) BRL BRL BRL BRL
SVOCs - Method 8270 (ppm)
Benzo(a)anthracene
Chrysene
Fluoranthene
P1rene
Total SVOCs
1 . 7
2.27
3.6r3.94
I 1 . 5 2
BRL
BRI-
2.68
2.94
5.62
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
I ppm
I ppm
56 ppm
40 ppm
l/7.8 ppm
84i780 ppm
1,0002,500 ppm
1,000/2,500 ppm
Pesticides - Method 8081 (ppm) BRL BRL BRL BRL
PCBS - Method 8082 (ppm)
PCB-1254
PCB-1260
Total PCBs
BRL
BRL
BRL
BRL
BRL
BRL
BRI-
BRL
BRL
1.15
0.91
2.12
Not Applicable
Not Applicable
Not Applicabte
l/10 pptn
l/ l0 ppm
Ulo ppm
Total RCRA 8 Merals - ppm
A-rsenlc
Barium
Cadmium
Cbromium
Lead
M€rcury
Silver
3.38
33.9
0.4t I
8.49
26.2
0.631
BRL
6.54
5 2 . 1
0.52
7 .28
87.5
0.3'7 5
l0. t
7.89
7 6.0
0 . 5 t 5
9.03
t52
0.342
BRL
12.2'72.3
1 . 3 5
t 6 . 0
3 3 9
0.908
BRL
Not Applicable
10/10 ppm
4,700i 140.000 ppm
34/1,000 ppm
100/100 ppm
500/1,000 ppm
20/610 ppm
340/10,000 ppm
SPLP RCRA 8 Metals - ppm
Barium
Chromium
Lead
0.0106
BRL
BRL
0.006
BRL
BRL
0.0335
BRL
BRL
0.0263
BRL
BRL
10.0 ppm
0.5 ppm
0.15 ppm
Not Applicable
BRL - Below Reporting Limits (see laboratory r€ports for compound specific detection limits)
Thc compounds listed above are those that were detected - please see laboratory repofts for fulI lists ofcomoounds and their soecific detection limits.
Page 38
TABLE l(d) - Results of Geoprobe@ Boring Soil Samplc AnalysesNew Haven Rail Yard M-8 Acceptance Facility
New Hay€n, Connecticut
Boring I.D-:
Sample Depth:
M8F- l3 M{rF- t4 M8F- t5
4'-6'
M8F- r6 CTDEP PMC GBGroundwater
Atea
CTDEP DEC Rcsidcntial/Comrnercial & lndustrial
CT ETPH - (ppm) 899 180 BRL 345 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm)
Benzcnc
Ethylbenzene
lsopropylbenzene
Naphthalene
n-Propylbenzene
Toluene
1,2,4-Trimethyltrenzene
Xylenes (total)
BRLBRLBRLBRLBRIBRLBRLBRL
1.520,3090.07530.4470.1433.O20.209t . 4 1 3
BRLBRLBRLBRLBRL0.008BRLBRL
BRLBRLBRLBRLBRLBRLBRLBRI
0.2 ppm10.1 ppm132 ppm
56 ppml4 ppm
67 ppm70 ppm19.5 ppm
2l1200 ppm
500/ I,000 ppm500i 1,000 ppm1,000/2,500 ppnr500/ 1,000 ppm500/ 1,000 ppm500/1,000 ppm500/ I,000 ppm
SVOCs - Method 8270 (ppm)Benzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChlyseneFluorantheneIndeno( 1,2,3-cd)pyrenePlreneTotal SVOCs
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
L 5 11.891.86
0.9s82.031.842.82
0.9682.45
t6.326
BRLBRLBRLBRI,BRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
1 pPm1 ppmI ppm42 ppm
I ppmI ppm56 ppmI ppm
40 ppm
l/7.8 ppm
Ul ppm1/7.8 pprn
1,000/2,500 ppmli.4/78 ppm84i780 ppm
1.000i2,500 ppnrI i7.tt ppm
1,000/2,500 ppm
Pesticides - Metlod 808 t (ppm) BRL BRL BRL BRLPCBs - Method 8082 (ppm)
PCB-1254PCB-1260Total PCBs
2.261.243.5
BRLBRLBRL
BRLBRLBRL
BRL0.02740.0274
Not ApplicabteNot ApplicableNot Applicable
li l0 pprnl i l0 ppml i l0 ppm
Total RCR{ 8 Metals - ppmArsenlcBariumCadmiumChromiumLeadMercury
13.166_4t . l 820.55 1 8
0.242
9.0r96.60.628.3?q?
0.2'l
29.3156
0.56134.',7841
0.0698
5.5928.8
0 . 6 1 530.449.'l
0.0707
Not Applicablc
10/10 ppm4,700/140,000 ppn
34/1,000 ppm100/ 100 ppm
500/1,000 ppm
?0/610 ppm
SPLP RCRA 8 Metals - ppmBariumChromiumLead
0.0216BRL
BRL
0.0142BRL0.031
0.04180.012BRL
0.05710.0 t930 . 0 1 6 1
10,0 ppm0.5 ppm0,l5 ppm
Not Applicable
BRL - Below Reporting Limits (see laboratory reports for compound specific d€t€ction limits)
The compounds listed above are those that were d€tected - please see laboratory reports for full lists ofcompounds and thet specihc detection limits.
Page 39
TABLE l(e) - Results of Geoprobe@ Boring Soil Sample AnalysesNew Haven Rail Yard M-8 Acceptaoce Facilit!
New Haven, Connecticut
Boring LD.:
Sample Depth:
M8F-17
4'-6'
M8F-18
2',-4',
M8F-19
?'4 '
M8F-20 CTDEP PMC GBGroundwater
Area
CTDEP DEC ResidentiaUCommercial & [ndustial
CT ETPH - (ppm) 8 , 5 1 0 287 3,260 136 2,500 ppm 500/2,500 ppm
VOCs - Method 8260 (ppm)
Naphthalene 0.268 BRL 0.0067 BRL 56 ppm 1,000/2,500 ppm
SVOCs - Method 8270 (ppm)
Anthracene
Benzo(a)anthracene
Benzo(a)p)'rene
Benzo(b)fluoranthene
Bcnzo(g,h,i)perylene
Benz-o(k)fluoranthene
Chrysene
Fluoranthene
Phenanthrene
Plrene
Total SVOCs
BRL
0.988
BRL
1.14
BRL
0.93
1.3 7
2.99
BR]-
l .o2
10.438
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.4'75
0.652
0.77 4
0 ; 1 7 8
I ' .J)J
0.674
0 . 8 1 2
t .68
0.848
t . '1
8.746
400 ppm
I ppm
I ppm
I pPm
42 ppm
I ppm
I ppm
56 ppm
40 ppm
40 ppm
1,0001?,500 ppm
lr.8 ppm
1/1 ppm
1/7.8 ppm
1,000/2,500 ppm
8.4/78 ppm
84/780 ppm
1,000/2,500 ppm
I,000/2,500 ppm
1,000i2,500 ppm
Pesticides - N{ethod 8081 (ppm) BRL BRL BRL BRL
PCBs - Method 8082 (ppm) 0.0216 0.0484 0.247 0.0286 Not Applicable l /10 ppm
Total RCRA 8 Metals ppm
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
6.41
46,1
0.569
38.4
79.8
0 . r 3 5
4.53
30.li
0.6'74
34.3
44.8
0.0605
5.6tt
42.7
0.735
56.9
124
0 . 1 9 5
t0.l
l 0 l
1 .9
12.3
283
0.641
Not Applicable
10/10 ppm
4,700i 140,000 ppm
34l1,000 ppm
100/100 ppm
500/1,000 ppm
20/6 l0 ppm
SPLP RCRA 8 Metals - ppm
Barium
Chromium
Lead
0.044
BRL
0.0298
0.085
0.0312
0.019
0.03
BRL
0.0161
0.0277
BRL
0.0182
10.0 ppm
0.5 ppm
0.15 ppm
Not Appticable
BRL - Below Reporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits-
Page 40
TABLE l(f) - Results of Geoprobe@ Boring Soil Sampl€ AnalysesNew Haven Rail Yard M-8 Acceptance Facility
New llaven, Connecticut
Boring [,D.:
Sample Depth:
M8F-21
2 ' 4 '
M8F-22
2'4',
M8F-23 M8F-24
2 ' 4 '
CTDEP PMC GBGroundwater
Area
CTDEP DEC Residential/Commercial & Indusrial
CT ETPH - (ppm) BRL t64 554 262 2,500 ppm 500i2,500 ppm
VOCs - Method 8260 (ppm)
Naphthalene BRL BRL BRL 0 . 1 9 8 56 ppm 1,000/2,500 ppm
SVOCs - Method 8270 (ppm)
Benzo(a)anthrac€ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Fluoranthenc
P1,re ne
Total SVOCs
BRL
BRL
Bzu-BRL
BRI-
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.888
1.37
t . I8
1.09
2.09
2 . 2 1
8.828
BRL
BRL
BRL
0.426
0.'77 L
0.705
t.902
I PPm
I PP.''
I PPm
I PP*
56 ppm
40 ppm
l/7 .8 ppm
li 7.ti ppm
8.4/78 ppm
It41780 ppm
1,000/2,500 ppm
1,000/2,500 pprn
Pesticides - Method 808 | (ppm)
a-Chlordane
g-Chlordane
0.0363
0.039
BRL
BRL
BRL
BRL
BRL
BRL
None Established
None Established
None Established
None Established
PCBs Method 8082 (ppm) 0. t04 0.0354 0.109 BRL Not Appticabte l /10 ppm
Total RCRA 8 Metals - ppm
Arsenlc
Barium
Cadmium
Chromiunr
Lead
Mercury
Selenium
9.91
60.8
0.61 I
7 . 3 1
694
0,0556
2.8
4.95
28.8
0.695
40.9
48.9
0.0614
BRL
6.41
39.2
0.599
29.4
99.7
0. t93
BRL
4 _ 1 1
34.9
0.70 t
44.9
22.0
0 . t t 5
BRL
Not Applicable
l0/10 ppm
4,700/140,000 ppm
34/l,000 ppm
100/100 ppm
500/ 1,000 ppm
20/610 ppm
340/10,000 ppm
SPLP RCRA 8 Metals - ppm
Barium
Chromium
Lead
0,0144
BRL
0.0088
0.0682
0.0214
BRL
0.0427
BRL
0.0336
0.03
BRL
BRL
10.0 ppm
0.5 ppm
0.15 ppm
Not Applicable
BRL - Below Reporting Limits (see laboratory reports for compound specifrc detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcomoounds and their sDecific detection limits.
Page 41
TABI E 1(g) - Results of Geoprob€@ Boring Soil Sampl€ AnalysesNew Haven Rail Yard M-8 Acceptance Facilit-v
New Haven, Connecticut
Boring I.D.:
Sample Depth:
M8F-25
z'-4'
M8F-26 MgF-27 M8F-28 CTDEP PMC CBGroundwater
Area
CTDEP DEC ResidentialCommercial & Industrial
CT ETPH - (ppm) 206 404 BRL 932 2,500 ppm 500/2,500 ppm
VOCs - Method 8260 (ppm) BRL BRL BRL BRL
SVOCs - Method 8?70 (ppm)
Anthracene
Benzo(a)anthrac€ne
Benzo(a)pyrene
Benzo(tr)fluoranthene
tsenzo(g,h,i)perylcne
Benzo(k)fluoranthene
Chrysene
Irluoranthenc
lndeno( 1,2,3 -cd)plrene
Phenantfuene
Pyrene
Total SVOCs
0.59?
0.946
0.982
0.98
0.483
0.88
1.18
2.3 5
0.433
0.942
2.36
1 2 . 1 3 3
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.876
0,876
BRL
BRL
tsRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
400 ppm
I ppm
I ppm
I ppm
42 ppm
I ppm
I ppm
56 ppm
I pp-
40 ppm
40 ppm
1,000i2,500 ppml / ? R n n m
l i I ppm
l/?.8 ppm
1,000/2,500 ppm
8.4/78 ppm
84/780 ppm
1,000/2,500 ppm
1,000/2,500 ppm
1,000/2,500 ppm
Pesticides - Mcthod 8olt I (ppm) BRL BRL BRL BRL
PCBs Method 8082 (ppm)
PCB-1254
PCB-1260
Total PCBs
0,0259B R L
0.0259
0.43 I
0.0592
0.4902
BRL
BRL
BRL
BRL
BRL
BRL
Not Applicable
Not Applicable
Not Applicable
I /10 ppm
li t0 ppm
l/10 ppm
Total RCRA li Metals -ppm
AISenlc
Barium
Cadmium
Chromium
Lead
Mercury
10.7
t44
3.4'l
1 2 . 4
287
0.7 4'7
8,56
58.7
BRL
7 . t I
123
0 . 1 4 1
BRL
| 1 . 5
BRL
3.97
l { .18
BRL
1.6
r 9.3
0.33 3
7.39
25.3
0.0388
Not Applicable
l0/10 ppm
4,700/140,000 ppm
34/l,000 ppm
100/100 ppm
500i 1,000 ppm
20/610 ppm
SPLP RCRA I Metals - ppm
Barium
Lead
0.0362
0.023
0.0148
0.0226
BRL
BRL
BRL
BRL
10.0 ppm
0.15 ppm
Not Applicable
BRL - Below Reporting Limits {see labomtory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and thcir spccific detection limils.
Page 42
TABLE l(h) - Results of ceoprobc@ Boring Soil Sample AnalysesNew Haven Rail Yard M-8 Acceptance Facility
New Haven, Connecticut
Boring I.D.:
Sample Depth:
M8F-29 M8F-30
2' -4 '
M8F-3 I
2',4'
M8F-32
2',4'
CTDEP PMC GBGroundwater
Aiea
CTDEP DEC ResidentiaUCommercial & lndustrial
CT ETPH - (ppm) 294 475 184 450 2,500 ppm 500/2,500 ppmVOCS - Mcthod 8260 (ppm)
Naphthal€ne
Stlrene
BRI-
0 . t 8 3
BRL
BRL
0.192
BRL
BRL
BRL
56 ppm
20 ppm
1,000/2,500 ppm500/1,000 ppm
SVOCs - Method 8270 (pprn)
Anthacene
Benzo(a)anthracene
B e nzo( a)pyene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
tscnzo(k)tluoranthene
Chrysenc
Fluoranthenc
Phenanthrene
Pyrene
Total SVOCS
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.q2q
0. rJ l4
1.2
1.02
0.53
1.16
1.39
3.09
1. t t9
2.97
14.993
BRL
BRL
BRL
BRL
t . 3 t
BRL
BRL
1.52
BRL
2.5',1
5.4
400 ppm
I ppm
I PpmI ppm
42 ppm
1 ppm
t Ppm56 ppm
40 ppm
40 ppm
1,000/2,500 ppml/7.8 ppml/ l ppm
U7.8 ppm
1,000/2,500 ppm
8.4/78 ppm
84/780 ppm
1,000/2,500 ppm
1,00012,500 ppm
1,000/2,500 ppm
Pesticides - Method 8081 (ppm) BRL BRL BRL BRL
PCBS - Method 8082 (ppm)
PCB-1254
PCB- 1260'fotal PCBs
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.017 |
0.017 t
0.039
0_0185
0.0575
Not Applicable
Not Applicable
Not Applicable
l i l0 ppm
ti l0 ppm
l/10 ppm
Total RCRA 8 Metals ppm
Arsenlc
Barium
Cadmium
Chromium
Lead
Mercury
Silver
BRL
t 5.2
BRL'7 .06
r 6 . l
BRL
BRL
BRL
t 2 . 2
0.284
5 . 1 I
1 4 . 5
BRL
BRL
9 ; 1 7
1 3 8
1 . 8 8
l2_0
266
0.753
BRI-
8.03
0.931
7.01
t7'7
0.098 5
| . 1 8
Not Applicable
l0 i l0 ppm
4,700/140,000 ppm
34/1,000 ppm
100/100 ppm
500/l,000 ppm
20/610 ppm
340/10,000 ppm
SPLP RCRA 8 Metals - ppm
Barium
Lead
BRL
BRL
BRL
BRL
0.0242
0.0254
0.0 t 26
0.0179
10.0 ppm
0.15 ppm
Not Applicable
BRL - tse lou' Reporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and thek soecific detection limits.
Page 43
' I 'ABl,E l{i) - Results of Geoprobe@ Boring Soil Sample AnalysesNew Hayen Rail Yard M-8 Acceptance Facility
New Ilaven, Connecticut
Boring I.D.:
Sample Depth:
M8F-33 M8F-34
4',-6',
M8F-35 M8F-36
4',-6',
CTDEP PMC GBGroundwater
Area
CTDEP DEC Residential/Commercial & [ndustdal
CT ETPH - (ppm) BRL BRT, 2,480 BRL 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm) BRL BRL BRL BRLSVOCs - Method ti270 (ppm)
Accnaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
B enzo(b) fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Chrysene
Fluorantle ne
Indeno( 1,2,3-cd)pyrene
Phenanthrene
Pyrene
Total SVOCs
BRL
tsRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
7.'76
3 . t 2
28.0
28.2
29.2
9.95
36.3
33.839.5
12.7
2.9
58.5
289.93
BRL
BRL
BRL
BRL
BRL
BRL
BRI-
BRL
BRL
BRL
BRL
BRL
BRL
84 ppm
400 ppm
I ppm
I ppm
I ppm
42 ppm
I ppm
I pP-
56 ppm
I ppm
40 ppm
40 ppm
1,000/2,500 ppm
1,000/2,500 ppm
l/7.8 ppm
1/1 ppm
1/7.E ppm
1,000/2,500 ppm
8.4/78 ppm
84/780 ppm
1,000/2,500 ppm
U7.8 ppm
1,000/2,500 ppm
1,000i2,500 ppm
Pesticides - Method 8081 (ppm)
Dieldrin BRL BRL 0.0625 BRL 0.007 ppm 0.03E/0.36 ppm
PCBs Method 8082 (ppm) 8zu, BRL 0.194 BRL Not Applicable l/10 ppm
Total RCL{ 8 Metals - ppm
Arsenlc
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
BRL
I l . - )
BRL
3.1t6
8 . l 6
BRL
BRL
BRI
10.4
BRL
4.41
3.65
BRI
BRI
1 7 . 7
72.4
0.957
7 .53
230
0 . 1 9 8
2.03
I 1.1
64.5
0.607
3.85
21.2
BRL
Not Applicable
10/10 ppm
4,700/140,000 ppm
34/l,000 ppm
100/100 ppm
500/1,000 ppm
20/610 ppm
340/l0,000 ppm
SPLP RCRA 8 Metals - ppm
Barium
LeadBRL
BRI
BRL
BRL
0.0126
0.03
0.0059
BRL
10.0 ppm0.15 ppm
Not Applicable
BRL Below Reporting Limits (see laboratory reports for compound specific d€tection limits)
The compounds listed above ar€ those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.
Page 44
TABLE l(i) - Resulls of Geoprobe@ Boring Soit Sample AnalysesN-ew Haven Rai[ Yard l\I-8 Acccptancc Facility
New Hay€n, Conoecaicut
Boring I.D.:
Sampte Depth:
M8F-37
2',4',
M8F-38
2'-4'
M8F-39 M8F-40 CTDEP PMC GBGroundwater
Area
CTDEP DEC ResidentiaYCommercial & [ndustrial
CT ETPH - (ppm) BRL BRL BRL 797 2,500 ppm 500/2,500 ppm
VOCs - Method 8260 (ppm)
Naphthalene
Toluene
Xylenes (total)
BRL
BRL
BRI,
BRL
0.106
BRL
0 . 1 7
BRL
BRL
0 . 1 8 1
0. t 5lt
0.2143
56 ppm
67 ppm
19.5 ppm
I,000/2,500 ppm
500/1,000 ppm
500/1,000 ppm
SVOCs - Method 8270 (ppm)
Bcnzo(a)anthracen€
Benzo(a)p5,rene
Benzo(b)fluoranthene
tscnzo(k)fluoranthene
Chrysene
Fluoranthene
Pyrene
Total SVOCs
2.15
2.61
3.37
3.94
4.26
21 .27
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
tsRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
2.03
2.09
4 . 1 2
I ppm
I ppm
I ppm
I pp-
I ppm
56 ppnr
40 ppm
l/7.8 ppm
Ul ppm
1/7.8 ppnr
8.4/78 pprn
84/780 ppm
1,000/2,500 ppm
I,000/2,500 ppm
Pcsticirles - Method 80xl (ppm) BRL BRL BRL BRL
PCBs Method 8082 (ppm) BRL BRL BRL 0.02_]4 Not Applicable l /10 ppm
Total RCRA 8 Metals - ppln
Afsenlc
Barium
Cadmium
Chromium
Lead
Me rcury
Selenium
Silver
28.8
64.5
0.937
1 4 . t
102
1 . 0 3
BRL
20.5
58.6
0.'795
7 .41
299
0.872
J , J J
BRL
I1.8
l 0 l
0.367
4.34
233
0.209
3 . 3 5
6.73
10.4
5 2 . 1
1 . 0
25.0
201
0 . r 3 6
BRL
L , 2 4
Not Applicable10/10 ppm
4,700i 140,000 ppm
34/1,000 ppn
100/100 ppm
500/1,000 ppm
20./610 ppm
340/10,000 ppm
340/10,000 ppm
SPLP RCRA 8 Metals - ppm
Barium
Lead
0.0126
0.0542
0.0121
0.0492
0.0098
BRL
0.0128
0.0263
10.0 ppm
0.15 ppm
Not Applicable
BRL - Below Reporting Limits (se€ laboratory reports for compound specific detection limits)
The compounds listed above are those that \acre detected - please see laboratory reports for full lists ofcompounds and their specihc detection limits.
Page 45
TABLE 1(k) - Results of Geoprobe@ Boring Soil Sample AnalysesNel Haven Rail Yard NI-8 Acceptalce Facility
New Haveo, Conn€cticut
Boring I.D.:
Sample Depth:
M8F-4 |
4'-6',
M8F-42 M8F43
z',-4'
M8F44
1' , -4 '
CTDEP PMC GBGroundwat€r
Area
CTDEP DEC ResidentiaVCommercial & Industrial
CT ETPH - (pprn) 728 776 BRL 3 8 8 2,500 ppm 500/2.500 ppmvocs - Method 8260 (ppm)
EthylbenzeneNaphthalene
Toluene
1,2,4-Trimethylbeznene
Xylenes (total)
BRL
BRL
BRL
BRL
BRL
0.1230. r550 . 1 5 4
0.0696
0.342',7
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
tsRL
10. I ppm
56 ppm
67 ppm
70 ppm
19.5 ppm
500/l,000 ppm
t,000/2,500 ppm
500/1,000 ppm
500/1,000 ppm
500i | ,000 ppm
SVOCs - Method 8270 (ppm)
Bcnzo(a)anthracene
Benzo(a)pyrene
Benzo(tr)fluoranthene
Benzo(k)fluoranthene
C@sene
Fluoranthene
Pyrene
Total SVOCs
1.41
1.27
1.67
1.84
2.18
3 . t 4
3 . 1 I
14.62
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
tsRL
tsRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
1 pp-
I pp-
1 ppm
1 ppm
I ppm
56 ppm
40 ppm
l/7.8 ppm
1/l ppm
1i7.8 ppm
8,4/78 ppm
84/780 ppm
I,000/2,500 ppm
1,000/2,500 ppm
Pesticidcs - Method 80li | (ppm) BRL BRL BRL BRL
PCBs Method llOlt2 (ppm) BRL BRL BRL BRL Not Applicable l/ l0 ppm
Total RCRA 8 Metals ppm
Arsenlc
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
9.64
40.4
0.516
9.8 rt52
0.307BRL
'7 .95t09
0.584It .73651.021.68
3.98
53.4
t t . lo2
4 . l l
5 l . l
0.0532.22
1.O
76.2
0.46r9.6
I t 9
0.586
BRL
Not Applicable
l0/10 ppm
4,700i 140,000 ppm
34i 1,000 ppm
t00i 100 ppm
500/1,000 ppm
20/6 10 ppm
340/ 10,000 ppm
SPLP RCRA 8 Metals - ppmBariumLead
0.009
0.0252
0.0962BRL
0.0064
BRL
0.0914
BRL
10.0 ppm
0.15 ppm
Not Appticable
BRL Below Reporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory repotts for full lists ofcomtounds and their soecific detection limits.
Page 46
TABLE 1(l) - Results of Geoprobe@ Boring Soil Sampl€ AralysesNew Hayen Rail Yard M-8 Acceptanc€ Facility
New Haveo, Connecticut
Boring I.D.:
Sample Depth:
M8F-45
4' -6 '
M8F46
z'4'
M8F-47
2',-4'
M8F48
2'-4'
CTDEP PMC GBGroundwater
Area
CTDEP DEC Residential/Commercial & Industrial
CT ETPH - lppm) 203 I,I50 1,310 BRL 2,500 ppm 500/2,500 ppm
vocs - M€thod 8260 (ppm)
Benzene
Naphthalene
Toluene
Xylenes (totat)
0 . 1 8 8
0 . t 7 7
0.339
0.3237
BRL
BRL
BRI,
BRL
0.0725
0 . r33
0.202
0.24ss
BRL
BRL
BRL
BRL
0.2 ppm
56 ppm
67 ppm
19.5 ppm
2l1200 ppm
1,000/2,500 ppm
500/l,000 ppm
500/1,000 ppm
SVOCs - Method 8270 (ppm)
Fluoranthene
Plrene
Total SVOCs
BRL
BRL
BRL
t . 1 2
t .99
3 . 1 I
2.'77
3.26
6.03
BRL
BRL
BRL
56 ppm
40 ppm
1,000,'2,500 ppm
I,000/2,500 ppm
Pesticides - Method 8081 (ppm) BRL BRL BRL BRL
PCBs - Method 8082 (ppm) BRL 0.02t2 0.028 BRL Not Applicable l /10 ppm
Total RCRA li Metals ppm
Arsenrc
Barium
Cadmium
Chromium
Lead
Mercury
21.6
59.6
BRL
65.3
0.094rJ
19.7
69.0
0.457
7 .82
1 3 6
0.363
10.7
54.7
0.5 89
8.64
t 8 3
0 . 1 8 2
l .6 l
39.3
0.87 |
10.4
228
BRL
Not Applicable
l0/10 ppm
4,700/l40,000 ppm
34/1,000 ppm
100/100 ppm
500i 1,000 ppnr
20/610 ppm
SPLP RCRA 8 Metals - ppm
Barium
Lead
0.0216
BRL
0 . 0 1 3
0.0146
0 . 0 t 2
0.0261
0 . 0 1 5
0.021
10.0 ppm
0.15 ppm
Not Applicable
BRL - Below Reporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory r€ports tbr full lists ofcompounds and their specific detection limits.
Page 47
TABLE l(m) - Results of Geoprobe@ Boring Soil Sampte AnalysesNew Hayen Rail Yard M-8 Acc€ptance Facility
New Haven, Connecticut
Boring I.D.:
Sample Depth:
M8F-49 M8F-50
2'-4',
M8F-51
2',4',
M8F-52
2',4',
CTDEP PMC GBCroundwater
Area
CTDEP DEC ResidentiaVCommercial & Industrial
CT ETPH - (ppm) BRL BRL BRL BRL 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm) BRL BRL BRL BRL
SVOCS - Method 8270 (ppm)
Fluoranthe ne
Pyrene
Total SVOCS
o.447
0.486
0.933
BRl-
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
56 ppm
40 ppm
1,000i2,500 ppm
1,00012,500 ppm
Pesticides - Method 8081 (ppm) BRL BRL BRL BRL
PCBs - Method 8082 (ppm) BRL BRL BRL BRL Not Applicable l/ l0 ppm
Total RCRA 8 Metals - ppm
Arsenic
Barium
Cadmium
Clromium
Lead
Mercury
Selenium
Silver
l . &
2t.6
BRL
4.29
23.6
0.0683
BRL
BRL
1.98
23.5
BRL
5 . t 2
9.99
0.0344
BRI,
BRL
I .96
25.6
BRL
6.56
6_6
BRL
BRL
BRL
3.94
95.3
0.499
t0.2
320
2.87
1.82
t .62
Not Applicable
10i l0 ppm
4,700/140,000 ppm
34/l,000 ppm
100/ 100 ppm
500/1,000 ppm
20/610 ppm
340/10,000 ppm
340/10,000 ppm
SPLP RCRA 8 Metals - ppm
Bsrium
Lead
0.0186
0.0497
0.0r46
BRL
0_0064
BRL
0.01 t8
0.0138
10.0 ppm
0.15 ppm
Not Applicable
BRII- Below Reportng Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompound.s and their specific detection lirnits.
Page 48
TABLE l(n) - Results of G€oprob€@ Boring Soil Sampl€ AnalysesNew Haven Rail Yard M-8 Acceptance Facility
New Haveo, Connecticut
Boring I.D.:
Sample Depth:
M8F-53 CTDEP PMC GBGrourdwater
Area
CTDEP DEC Residential/Commercial & Industrial
CT ETPH - (ppm) BRL 2.500 ppm 500/2.500 ppm
VOCs - Method tt260 (ppm) BRL
SVOCS - Method 8270 (ppm) BRL
Pesticides - Merhod 801{ I (ppm) BRL
PCBS Method 8082 (ppm) BRL Not Applicable l/10 ppm
Total RCRA 8 Metals - ppm
Aisemc
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
4.42
98.3
0 . 5 2 1
5.68
333
2 . 2 1
t . 8 t
Not Applicable
l0/ l0 ppm
4,700/140,000 ppm
34/ I ,000 ppm
100/100 ppm
500/ 1,000 ppm
20/610 ppm
340/10,000 ppm
SPLP RCRA 8 M€tals - ppm
Barium
Lead
0.0208
0 . 0 1 I I
10.0 ppm
0.15 ppm
Not Applicable
BRL - Below Rcporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that w€re detected - please see laboratory reports for full lists ofcompounds and their specific dctection limits.
Page 49
TABLE 2(a) - Results of Ballast Samplc AnalysesNew Haven Rail Yard M-8 Acceptance Facility
New Hayen, Connecticut
Sample l.D.: MSFB-1 M8FB.2 M8FB-3 MI]F8.4CTDEP PMC GB
GroundwaterArea
CTDEP DEC ResidentiaVCommercial & Industrial
CT ETPH - (ppm) BRL BRL BRL BRL 2,500 ppm 500/2,500 ppm
vocs - Method 8260 (ppm) BRL BRL BRL BRL
SVOCs - Method 8270 (pprn) BRL BRL BRL BRL
Pesticides - Method 808 | (ppm) BRL BRL BRL BRL
PCBS Method 8082 (ppm) BRL BRL BRL BRL Not Applicable t/10 ppm
Total RCRA 8 Metals - ppm
Barium
Cadmium
Chromium
Lead
10.8
0.626
1.97
5.08
13.2
0.506
3.22
3.78
t3.4
0.731
2 . 1 2
4.'l
l 1 .4
0.775
) t )
5.95
Not Applicable
4,700/140,000 ppm
34/1,000 ppm
100i 100 ppm
500/ I,000 ppm
SPLP RCRA 8 Metals - ppm
Barium 0.0066 0.0082 0.009 4.0072 10.0 ppm
Not Applicable
BRL - Below Reporting Limits (s€e laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits-
Page 50
TABLE 2(b) - Results of Ballast Sampte AnalysesNew Haven Rail Yard M-8 Acceptance Facility
New Haven, Connecticut
BRL - Below Rcporting Limits (see laboratory reports for compound specihc detestion limits)
The compounds listed above are thos€ that were d€tected - please se€ laboratory reporls for full lists ofcompounds and their specific detection limits.
Sample [.D.: M8FB.5 M8FB-6CTDEP PMC GB
GroundwaterArea
CTDEP DEC ResidentiaUCommercial & Industrial
CT ETPH - (ppm) BRI BRL 2,500 ppm 500/2,500 ppm
VOCs - Method 8260 (ppm) BRL BRL
SVOCs - Method 8270 (ppm) BRL BRL
Pesticides - Method 8081 (pprn) BRL BRL
PCBs - Method 8082 (ppm) BRL BRL Not Applicable l/10 ppmTotal RCRA 8 Metals ppm
Barium
Cadmium
Chromium
Lead
12.7
0.565
1 . I
3.89
t3.2
0.707
2.82
I 1 . 4
Not Applicable
4,700/140,000 ppm
34l1,000 ppn
100/ 100 pptn
500/l,000 ppm
SPLP RCRA 8 Metals - ppm
Barium 0.0073 0.005 10.0 ppm
Not Applicabte
Page 51
TABLE 3 - Results of Railroad Tie Samplc AnalysesNew Haven Rall Yard M-8 Acceptance Facility
New Haven, Connecticut
BRL - Below Reporting Limits (see laboratory reports for compound specific detection timits)
The compounds listed above are those that were detected - please see laboratory repofts for full lists ofcompounds and their specific detection limits-
Sample I.D.: M8FT.1 M8FT.2CTDEP PMC GB
GroundwaterArea
CTDEP DEC ResidentiaUCommercial & Industrial
CT ETPH - (ppm) 11,600 3 3,600 2J00 ppn 500/2,500 ppmVOCS - Method 8260 (ppm)
Naphthalene 6.02 5.69 56 ppm 1,000/2,500 ppmSVOCs - Method 8270 (ppm)
AcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneCarbazolcCluyseneDibenzo(a,h)anthraceneDitrenzofuranFluorantheneFluoreneIndeno( 1,2,3 -cd)pyrcnc
l -Methylnaphthalene
2-MethylnaphthalenePhenanthrenePlreneTotal SVOCs
29.0t6.9
282.0227.099.3r60.034.2187.0152.0358.010.926.9876.042.140.43.78BRL463.0640.0
3,649.08
| 5.310.4
250.0137.054.3
144.02 t . lI4J.O199.0449.06.JE19.3
369.026.624.45.0
4.461 5 L 0301.0
2,330.24
84 ppm84 ppm
400 ppmI ppmI ppmI ppm42 ppr\I ppmI ppmI ppmI ppm
5.6 ppm56 ppm56 ppmI ppm
None Established9.u ppm40 ppm40 ppm
1,000/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm
1/7.8 ppm1/1 ppm
li7.E ppmI,000/2,500 ppm
8.4/78 ppm311290 ppm84/780 ppm
lil ppm270/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm
U7.8 ppmNon€ Established474/2,500 ppm1,000/2,500 ppnI,000/2,500 ppm
Pesticides - Method 8081 (ppm) BRL BRLPCBs - Method 801i2 (ppm)
PCB-1254PCB-1260Total PCBS
0 . 1 6 80.1640.332
0.4020.8531 .255
Not ApplicableNot ApplicableNot Applicable
1/10 ppml/10 ppml/10 ppm
Total RCRA 8 Metals - ppmBariumCadmiumChromiumLcadMercury
13.90.7 t42.962 1 . 8
0.0425
5.0uBRLt.768.4
BRL
Not Applicable4,700/140,000 ppn
34l I,fi)o ppm100/100 ppm
500/1,000 ppm20/610 ppm
TCLP RCRA 8 Metals - ppmBariumCadmiumLead
0,07610.0050.0244
0.1050.0040.0135
10.0 ppm0.05 ppm0. 15 ppm
Not Applicable
Page 52
TABLE 4(a) - Results of Groundwater Grab Sample AnalysesNew Haven Rail Yard M-8 Acceptance Facil ity
N€w Ifuyen, Connecticut
Sample I.D.: M8F-14GW
M8F-24GW
CTDEP SurfaceWater Protection
Criteria
CTDEP Volatilization Criteria
ResidentiaVCommercial & Industrial
CT ETPH (ppm) BRL 1 .0 None Established Not Applicable
VOCs - EPA Method 8260 (ppb) BRL BRL
SVOCs - EPA Method 8270 (ppb)
Benzo(a)anthracene
Benzo(b)fluoranthenc
Berzo(g,h,i)peryle ne
Benzo(k)fluoranthene
Chrysene
Fluoranthene
Indeno(1,2.3-cd)plrene
P he nanthrene
Pyrene
0.42 5
0.762
0.73 8
0.65
0.5
0 . 9 1 2
0.6
0.35
0_85
BRL
BRL
BRL
BRL
BRL
0.27 |
BRL
BRl-
0.4
0.3 ppb
0.3 ppb
None Established
03 ppb
None Established
3,700 ppb
None Established
0.3 ppb
I10,000 ppb
None Established
None Established
None Established
None Established
None Established
None Established
None Established
None Established
None Established
Pesticides - EPA Method 8081A (ppb) BRL BRL
PCBs - EPA Method 8080 (ppb) BRL BRL
Total RCRA I Metals ppm
ATSENIC
Barium
Cadmium
Cfuomium
Mercury
0.007
0.0096
0.0048
15.7
0.00026
BRL
0.276
BRL
0.0079
0.00221
0.004 ppm
None Established
0.006 ppm
0.11 ppm
0.0004 ppm
Not Applicable
BRL Below Reporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.
Page 53
TABLE 4(b) - Results of Groundwater Grah Sample AnalysesNew Haven Rail Yard M-t Acceptance Facility
New Haven, Connecticut
Sampte I.D.: M8F-42GW
M8F-50
GWCTDEP SurfaceWater Protection
Criteria
CTDEP Volatilizntion CriteriaResidenrialCommercial & Industrial
CT ETPH (ppm) BRL BRL Nooe Established Not Applicable
VOCs - EPA Method 8260 (ppb) BRL BRl-
SVOCs - EPA Method 8270 (ppb) BRL BRL
Pesticides - EPA Method 8081A (ppb) BRL BRL
PCBs - EPA Method 8080 (ppb) BRL BRL
Total RCRA 8 Metals - ppm
Arsenic
Barium
Lead
tsRL
0.058
0.0132
0.0062
o.0122
0 . 0 1 2
0.004 ppm
None Established
0.013 ppm
Not Applicable
BRL llelow Reporting Limits (see laboratory repofts for compound speciiic detection limits)
The compounds listed above are those that werc det€cted - plcasc see laboratoqr reports fbr full lists ofcompounds and their specific dctcction limits.
Page 54
APPEI\DIX ABoring Logs
Page 55
EIgiggI Temporary M-8 Acceptance Facitity
Location: New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: MgF-l
Inspector: C. Criscuolo
Date:3-19-07
l 0t l l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Por'F, e A ATv/Backhoe-Moun6d Geoprcbes
E 6e a )o =
E
o
Description €.ao oo =
c ) o -o - 5
Sample Interval
Ground Surface 0.0
1 .0 -
2.0-
3.0-
4.0-
5.0-
6.0-
7.0-
Gray medium to coarse GRAVEL (BALLAST)
0.2 Macro Core 0'-2'
Dark-Brown fine to coarse SAND, trace Ash, Cinders, Concrete,Brick, & Wood (FILL)
Groundwater at 6'6.0
1 . 2
0.2
Macro Core 2'-4'
i . ! . . i l l t i -+ i: :q: ; : :q: l : : :q: i
::"::;.:r. i j;".:ii ! : . i ! j i - ! .
: :q: i : : { : i : . : :q: i
::r;:;_ :q.;i:j:".i
: :q:a :t:ij :i :q:l
:{:a:{:a:i:q:i
::q:ii:q:i:;:q:i
r,"-;r :qi; j :q:i
Macro Core 4L6'
8.0
0 .1 Macro Core 6'-8'
9.0-
10.0-
I t . u -
12 .0 -
End of Eoring at 8'
Soil Oescriotion: and = 35-50% some = 20.35% litlle = 10-20o/o trace = 1-10V"
Driller: W Lineberry
8k' Geoprone 540U
Depth to Water: 6'
Borinq Depth: 8'
Borinq Dia.: 2"
eAgg, 1 of 1
Page 56
GEOPROBE SOIL BORING LOG l 0- r\ t I
Logical Environmental Solutions354 South River Road
Tolland, CT 06084f ru c k, Port a b I e & A TV/ B ac kh oe-M o u n tecl Ge oprobes
Proiect: Temporary M.8 Acceptance Facility
lgggE$, New Haven Rail Yard
g.Igq! Maguire croup lnc.
Borinq: l,l8F-2
lnsp€ctor: C. Criscuolo
g9!g 3-19-07
E 6{ r @
o
o
Descriptionc L oo o 6 a
F C L
Sample Interval
Ground Surface 0.0lv q\i,D-o1 Gray medium to coarse GRAVEL (BALLAST) 0.5
0 Macro Core 0'-2'{:i;:.qi
l:td j-!1
t:i i:{:
s,-.:.d.:
q:i!:/:
4 i : : :
{:i"':q:r
cris.: :.::". i
(:if :q:i
?ri.r :i:q. :i
{ : i : ; :q. i
?:i{ :,::ol:i
ft:;:q:i
,i.i'.tti
qi i -q: i
i i r : ; .c: i?'..d rt.!:{:i i.{:i
?i i :c: i
Dark-Brown fine to coarse SAND, trace Ash, Cinders, Concrete,Brick, & Wood (FILL)
Groundwater at 6'6 .0
0.8 Macro Core 2 -4'
0.3 Macro Core 4'-6'
8.0
0 .1 Macro Core 6'-8'
9.0-
10 ,0 -
| | .u -
1 2 . O -
End of Boring at 8'
Soil Description: and = 35-500/6 some = 20-35% little = 10-20% trace = 1.10%
Driller: W. Lineberry
!!9. Geoprone 540U
Deoth to Water: 6'
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: I of I
Page 57
rei$li Temporary M.8 Acceptance Facility
Location: New Haven Rail Yard
e.Igg! Maguire Group Inc.
Borinq: M8F-3
Inspector: C. Criscuolo
Date:3-19-07
ifLogical Environmental Solut ions
354 South River RoadTolland, CT 06084
Truck, Pottable & AfylBackhoe-Mountecl Geoprobes
; : io o
o
ct)
Description 5.a3,s
Fo a; i c r
Sample lnterval
Ground Surface 0.0
1 .0 -
3.0-
4.0-
c.u-
6.0-
7.0-
.v q rhv
p"CI.# Gray medium to coarse GRAVEL (BALLAST) 0.5
0.4 Macro Core 0 -2'Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete & Brick (FILL)
t . 3
t . . ll t
Red-Brown fine Sand, little Silt2.5
2.4 Macro Core 2'-4'ii;::t*1::i,i'ii .e ii.o.:i
'.d.::;.qi;::ni
t :d : l :a : iq : r'.?:; .z i .::z i
:qi :{ i : ;qi
-! :a:! .1: i . ! :
:q: i :{ : i : j :q: i
r:q:aY:i:;:q:i
;:o.:i ti, :;:'.:i
r:q:i;qri::;:q:i
Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
Groundwater at 6'6.0
2.O Macro Core 4'-6'
8.0
0.5 Macro Core 6 -8'
9.0-
10.0-
1 1 . 0 -
12 .0 -
End of Boring at 8'
Soil Descriotion: and = 3S50% somo = 20-35% little = 10-20% trace = l-10%
Driller: W. Lineberry
gg; Geoprone 540U
Depth to Water: 6'
Borinq Oepth: I'
gg!i!s-B.is- 2"
Paoe: 1 of I
Page 58
GEOPROBE SOIL BORING LOG t - ^
i o| I '
Loqieal Environmental Solutions354 South River Road
Tolland. CT 06084Truck Porleue & ATv/gackhoe-llounted ceoo.obes
Plgigg!' Temporary M-8 Acceptance Facility
Location: New Hav€n Rail Yard
Client: Maguire Group Inc.
Borinq: M8F4
Inspector: C. Criscuolo
Date: 3-l S7
E 6o c to g
o
oDescription Fg6 a
d g
Sample Interval
Ground Surface 0 .0
' t .0-
2.O-
3 ,0 -
4.0-
5.0-
6.0-
.::q-i:qa::q:
iii:iEl: o - . o . . : <
j ; f l . . .9 . . , j l_+ :_or'.c_a :.10 . . o . ' . . : (lo "o :co.-:r.o-. .q..: j .{.o : .o. ,co :' : o . . o . . : {:O. ' o- :Co -
t3.=&tjt - E - . r ' ,
.': 'q^.+l
.F:-1;--#i. o lri :l. i
$,w"$l io ld 'i: i
F,u'$ir,lu a.t.f :-1l,"'.Ft, o.f" :?, t
.f "+"..f', o 9; .?, t'9;,;*i s;
ASH & CINDERS, little fine to coarse Gravel (FILL) 0.5
0.3 Macro Core 0'-2'
Dark-Brown fine to medium SAND, little Silt, Ash & Cinders,trace fine to coarse Gravel (FILL)
3.03.4 Macro Core 2'-4'
Red-Brown fine to coarse SAND, little Silt
Groundwater at 5.5'c . J
1 . 1 Macro Core 4'-6'
8.0
0.2 Macro Core 6 -8'
I 0-
1 0
1 1 . 0 -
12.0-
End of Boring at I'
Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-l0olo
Driller: W. Lineberry
Elgj Geoprone 54Ou
Depth to Watgr: 5.5'
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: I of 1
Page 59
GEOPROBE SOIL BORING LOGProiect: Temporary M.8 Acceptance Facility Borino: MgF-s
!9991!iS, New Haven Rail Yard Inspector: C. Criscuoto
Client: Maguire Group Inc. Date: 3.15.07
l o\J I
Loqical Environmental Solut ions354 South River Road
Tolland. CT 06084fruck, Poftahle & Afv/Beckhoe-Mountd Ceoryobes
: i :o oo g
Eo
Description -aEo o o o -
Sample Interval
Ground Surface 0.0
1 .0-
2.O-
3.0-
4.O-
5.0-
6.0-
7 .O-
F:i,I:i,;:iiih-!:d:f:t:i-l:t6ii:'';;.:. -o . . o - : . ' - c: o i o : C o l
i : oj' l;; :. . o . . + . . . . n:O r ' 0 : dq l;i P-. .q...;;.1o : o , _ {o :. _ .o . . 4 . . ' _o: O r ' O : C O _r : 9 . q . r : a
t - 8 . . ) . .
oY.9;.ol-F.ii".Ft - F . . r - .
oY.9-.o!*f :i.;-.rf. o lft :?i iE : . - : : . . s :.r V.rl ,<1ft: i ; ts -.- S-.f.'.r".ff ,o io.?1i :
$,";$f, o lo :?1t:'e; ;i s-
ASH & CINDERS, little fine to coarse Gravet (F|LL)
o.2 Macro Core 0'-2'
Dark-Brown fine to medium SAND, lit e Silt, Ash & Cinders.trace fine to coarse Gravel & Concrete (FILL)
3.04.4 Macro Core 2'-4'
Red-Brown fine to coarse SAND, little Silt
Groundwater at 5.5'5 .5
0.9 Macro Core 4'-6'
8.0
0.3 Macro Core 6'-8'
9.0-
10.0-
11 ,0 -
't2.o-
End of Boring at 8'
Soil Descriotion: and = 35-50o/o some = 20-35% tittte = 10-20o/o trace = 1-10%
Driller: W. Lineberry
B!S, Geoprone 540U
Deoth to Water: 5.5'
Borino Depth: 8'
Borinq Dia.: 2"
Paoe: I of 1
Page 60
GEOPROBE SOIL BORING LOG l 0( t l
Loqical Environmental Solut ions354 South River Road
Tolland, CT 06084fruck, Podable & ATv/Backhoe.lloune l Geop.obes
elgiggli Temporary M-8 Acceptance Facitity
Location: New Haven Rail Yard
Client: Magui16 Group Inc.
Borinq: M8F-G
lnsoector: C. Criscuolo
Date: 3-15-07
=aao oo =
E
oDescription -o.6
o { ) o Eo - 5
Sample Interval
Ground Surface 0.0
1 .0 -
2.0-
3.0-
4.0-
5.0-
6.0-
7.0-
:?:ij:'.:iii!:i
:".:; :D. ir :.: :o.:i
Gray medium to coarse GRAVEL, little Elack Ash & Cinders u.5
0.3 Macro Core 0'-2'
Red-Brown to Olive-Brown fine to coarse SAND. trace fine tocoarse Gravel & Ash (FILL)
3.01 . 6 Macro Core 2'-4'': e.9ft :{. i
. 9 : . - j s :
"f:1j".F' :91* '?: t. $ : . - ; i i l :
" rU.F'.,i'Y;);,:$ 9; .?, rS
- . : - S:
.F:-1r".F':5 9; .?; r
F,"sil, it 9; .1, t
.f -1).f1:6 9; .f, t
Red-Brown fine to coarse SAND, some Ash & Cinders {FILL)
Groundwater at 5'5.0
0.6 Macro Core 4'-6'
8 .0
0 Macro Core 6'-8'
9.0-
10 .0 -
11 .0 -
12.O-
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = 1-10%
Driller: W Lineberry
B!$. ceoprone 540U
9ed[!4@s'
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: 1 of 1
Page 61
ElgiCgl! Temporary M-8 Acceptance Facility
!99a!!9![ New Haven Rait yard
Client: Maguire Group lnc.
Borinq: M8F"7
Inspector: C. Criscuolo
9a!9, 3-26-07
I
i o\, I
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Portable & ATv/aackho*MounEd Geoprol,t.s
c L oO C '
o
U'
Oescription E.Eo oo 5
6 ao - =
Sample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
4.O-
5.0-
6.0-
7.0-
rv rl \r|,,'r\.a).ff;-RX;r:y--qb*v_o : .o:t .co :- : o . . o 1 . . <o - o : c o l: l d . : q . ; j Jo : o : . 4 0 :. : o . . o - 1 . : <o r 'o' :co .-: ' .o' . .q . j : Ja : 4 j . c 0 - j' : o - . - o . : : (
r . p-. .q' . . i , Jo : g ; . ( a :: o . . o . . : <
r, p-. .q.. .1i1.0 : 9 r ' . ca :- : o . . q - . - : (
Gray medium to coarse GMVEL (BALLAST)1 . 0
0 Macro Core 0'-2'
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick, trace Concrele & fine to coarse Gravel (FILL)
5 .0
0.8 Macro Core 2'4'
o.2 Macro Core 4'-6':i,;'::1,t':i;1:".:;-;:'.:ij.i:ol
Y.!:{.t:i.s:q:a:4:i:.::q
:"::;e.:i:::'l
:q:l:4:!;::q
:F.:;::'.:iri:el
Black ASH & CINDERS, little fine to coarse Sand & Gravel(FrLL)
Groundwater at 6'6.0
8.0
0 Macro Core 6'-8'
9.0-
10.0-
1 1 .0 -
12.0-
End of Boring at 8'
Soil Descriotion: and = 35-50% some = 20-35% liftle = l0-20o/o trace = 1-10%
Driller: W. Lineberry
B!$, Geoprone 540U
Depth to Water: 6'
Borino Depth: 8'
Eorinq Oia.: 2"
Paqe: I of I
Page 62
GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility Borinq: MgF-g
!9ga!!9!j New Haven Rail Yard lnspector: C. Criscuolo
Client: Maguire Group Inc. Oate:3-26-07
t , ^
i oi t l
Loqical Environmental Solut ions354 South River Road
Tolland, CT 06084Truck, Portable & ATv/Backho*lllounted Caoprcbes
E a6 g
E
tt,
Descriptionc L o
3 g o 6 .Sample Interval
Ground Surface 0.0
1 .0 -
2.O-
3,0-
4.0-
5.0-
6.0-
7 .0-
$rHGray medium to coarse GRAVEL (BALLAST)1 . 0
0 Macro Core 0'-2'g_ :.ol '_4.o :. : o . - - + . : : cO r ' O : C o l1 ; { . 9 : . , ; {o : o . . a d :
9 .:1o.:.cq ri , q . 9 . i , . 1. d i P : - Jg :' : o . . o . : . 4o : o : c o lr,9: q..r;-1.o : Pr ' .4 t :. : 0 . . o . . : a
r;r,...9:.. i i t. o : _ o j . c _ a :. :o . . o . . : co ._ a .co- .
:q:a:q:i i:qi:".i'j:o. i,j j:'.:i
?.1:{.r:;.s-1:qi;q: i : :qi
:"jj:". ij-j :'. t
:r. i :/. i: ::q:i
:r.:;'::t,:iij:?.:i
:q:ii.{ri::.::q:i
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick, trace Concrete & fine to coarse Gravel (FILL)
5.0
0.2 Macro Core 2'4'
0 Macro Core 4'-6'Black ASH & CINDERS, little fine to coarse Sand & Gravel(FrLL)
Groundwater at 6'6.0
8.0
0 Macro Core 6'-8'
9.0-
10.0-
1 1 .0 -
12 .0 -
End of Boring at 8'
Soil Description: and = 35-50% some = ?0-35% little = 10-20% trace = 1.10%
Driller: W. Lineberry
Eigj Geoprone 5/t0U
Depth to Water: 6'
Borinq Deoth: 8'
Borinq Dia.: 2"
Paqe: I of 1
Page 63
GEOPROBE SOIL BORING LOG I
i o( t l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truc R, Pottable & AMEactihcE-M ounEd Geoprobes
EIgiCgl! Temporary M-8 Acceptance Facitity
lggetig![ New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: M8F-g
InsDector: C. Criscuolo
Date: 3-26-07
E t oo o
o.(lcg,
Description E 5( r o o a Sample Interval
Ground Surface 0.0
1 .0 -
4.0-
c.u-
o_u-
7 .O-
l"r-%lGray medium to coarse GRAVEL (BALLAST)1 0
0 Macro Core 0'-2'.o-i.ii' : o . . - o . . :: O . + : c a,, .--. ..c..., :a : o : ' : . { a' : o . . - q . . . ::A r 'O : gq: j 9 . . .q . . ; ;
b : o r t . 4 { _.10 . . ' o . : . :
, j .9 . . . .9 . . , io : -4. .C_O
0 : _o. .c_o
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick. trace Concrete & fine to coarse Gravel (FILL)
5 .0
0.4 Macro Core 2 -4'
0.2 Macro Core 4 -6'
l: .. :!1 i:i +:
:{:i;{:i:i:{:
Black ASH & CINDERS, little fine to coarse sand & Gravel(FtLL)
Groundwater at 6'6 .0
8.0
0 Macro Core 6!8'
9.0-
10.0-
1 1 .0 -
12.0-
End of Boring at I'
Soil Description: and = 35-50% some = 20-35% little = 10-20o/o trace = l-10%
Orill€.: W. Lineberry
Elgj Geoprone 540U
Depth to Water: 6'
Borinq Deoth: 8'
Borino Dia.: 2"
gggei I of 'l
Page 64
GEOPROBE SOIL BORING LOG I
A O| I l
Logical Environmental Solutions354 South River Road
Tolland. CT 06084Truck, Portable & ATvl8eckhoo+lount .l ceoprcbes
e!gi$j[ Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
Client Maguire Group Inc.
Borinq: M8F-10
lnsoector: C. Criscuolo
Date: 3-26-07
-o. 6
o d )o g
o
oDescription
o . oo o o a Sample Interval
Ground Surface 0.0
1 . 0 -
2.O-
3,0-
4.0-
5 .0 -
6.0-
7 .O-
av grhv's^o1t3no.€r:\./--qb+\4o : + r ' - c 4 :. : o . . - o - . : <' a _ . + : c o l; : p . . . o . . i r Ji l: or'io' :. .o . . o . : :<
, ; .8 . .q . . r ,J.o : .or'.c9 :. - . 4 . . o . . : <o . c . c + . ': , .o . q . . i j t.o : .ar-.c.0 :. - -o ._ o - : - : (
::.ol .o..-., lt.o' : .ar'.cf :. - -o . . o . : :<
Gray medium to coarse GMVEL (BALLAST)1 . 0
0 Macro Core 0'-2'
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little 8rick, trace Conc.ele & fine to coarse Gravel (FILL)
5.0
Macro Core 2'-4'
o.4 Macro Core 4'-6'-q:i :{:l l:q:'.o.ti
.qi;.i .21
s.';14 ;a:i a..{:i :r':.:i:q:
:c.:; :". i.i:'.:i-!1'. :! .! :i.!'.:qr i :{ i : ; :q: ii.{1ri:l:i:i.{::o.ri:'.:i!.:;:q:ii.i1.:l:.i:i.!:
:q:l::{:Ii'q:i
Black ASH & CINDERS,(FrLL)
Groundwater at 6'
little fine to coarse Sand & Gravel
6.0
8.0
0 . 1 Macro Core 6'-8'
9.0-
10 .0 -
1 1 . 0 -
' t2.o-
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = 1-10%
Driller; W. Lineberry
8!S, Geoprone $40U
Depth to Water: 6'
Borinq Depih: 8'
Borino Dia.: 2"
Paqe: I of I
Page 65
r a .
i o( t l
Loqical Environmental Soluiions354 South River Road
Tolland, CT 06084Truck. Podaue & A|U/B ackhoe-tttounted Geoprohes
Proiect: Temporary M-8 Acceptance Facility
Egql!!g![ New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: M8F-l I
Inspector: C. Criscuolo
Date:3.26-07
tL clo o .n
Description €.aI E o a
Sample Interval
Ground Surface 0.0
1 .0 -
2.0-
4.0-
5.0-
6.0-
7.0-
1v q rhv
/(\ /)/c;kvhiv-qts'-vd : o : - . c o -' _ o . ' o . : . : <
; : o ' ' . c ; ' :. : o . o . : : <
r ; .9 . . . .q . : ; r-o :.o j:.c.o :. - .o . . o -1 : (. : o . - o . . : <.a j 9: I .1.o-:. : 0 . . o 1 . - <' o r ' o : co l. : d - d . . : <
i : 0 , ' . i i ' ::o . . o . . .<
Gray medium to coarse GRAVEL (BALLAST)1 . 0
0 Macro Cor€ 0 -2'
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little Brick, trace Concrete & fine to coarse Gravel (FILL)
5.0
0 Macro Core 2'4'
0 Macro Core 4'-6':q:a:qiii:;:q:i
:q:;:q:il:j:q::i
'x.'at4 .'it;v .':C:i.{:i.:r:{:i:o_D: :e. :iri i :"1:i
.q: i :q: i i :q: i
;q:i: :?. :ir: :j :qi
Black ASH & CINDERS,(FrLL)
Groundwater at 6'
liftle fine to coarse Sand & Gravel
6.0
8.0
0 Macro Core 6'-8'
9.0-
10.0-
1 1 .0 -
12 .O-
End of Boring at 8'
Soil Doscriotion: and = 3t50% some = 20-35% little = '10-20% trace = 1'10%
Driller: W. Lineberry
E!$, Geoprone 540U
Depth to Water: 6'
Borino Depth: 8'
Borinq Dia.: 2"
Pggg 1 of 1
Page 66
GEOPROBE SOIL BORING LOG I
i.ot r l\ t l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Portaue & AruBackhoe.Mounted Geoprobes
&i99$ Temporary M.8 Acceptance Facility
!999!ig![ New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: MgF-12
Inspector: C. Criscuolo
Oate:3-15-07
: : :o oo 3
cU)
Description . c ^E 6o c to g
o aSample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
4.O-
5.0-
6.0-
7 .O- <i.F-+:-L-..fi r ' d . . r " ,: r J . f t . 1 : i
Black ASH & CINDERS with little to trace Red-Brown fine tocoarse SAND & fine to coarse Gravel (FILL)
Groundwater at 5.5'5.5
0 .1 Macro Core 0'-2'
0.4 Macro Core 2'-4'
0 .1 Macro Core 4 -6'
8.0
0 Macro Core 6'-8'
9.0-
10.0-
11.0-
12.0-
End of Boring at 8'
Soil Description: and = 35.50o/o some = 20.35% little = 10-20% traee = l-10%
Driller: W. Lineberry
!!g Geoprone 540U
Depth to Water: 5.5'
Borinq Depth: g'
Borinq Dia.: 2"
Pggg. 1 of 1
Page 67
iiLoqical Environmental Solutions
354 South River RoadTolland, CT 06084
Truck, PorTahle & AfvlBackhoe-Mounted Geoprohes
Proiect: Temporary M-8 Acceptance Facility
Locaiion: New Haven Rail Yard
Clienl: Maguire Group Inc.
Borinq: M8F-13
Insoeclor: C. Criscuolo
Date: 3-15.07
1 .
a
J .
A
5 .
6 .
Black ASH & CINDERS with little to trace Red-Brown fine tocoarse SAND & fine to coarse Gravel (FILL)
Macro Core 0'-2'
Macro Core 2'4'
Macro Core 4'-6'
Macro Core 6'-8'
5.5
0
o.2
0 .1
0
End of Boring at 8'
Soil Description: and = 3s50% some = 20-35% little = 10-20o/o trace ='l-10%
Driller: W. Lineberry
8!gj Geoprone 540U
Depth to Water: 5.5'
Borinq Depth: 8'
Sil$b-2"
Paqe: 1 of 1
Page 68
GEOPROBE SOIL BORING LOG t ^
i of l l
Logical Environmental Solutions354 South River Road
Tolland, CT 06084f ruck, Pothble & AlylBackhoe.tlounte<I Geopfobes
&i$!: Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: MgF-14
Inspector: C. Criscuolo
Date: 3.19-07
a 6o { ,o 5
o
at,
Description E ^7 1o oo 9
o ad - 5
Sample Interval
Ground Surface 0.0
'1.0-
2.O-
3.0-
4.Q-
5.0-
6 .0 -
7 .O-
Gray medium to coarse GRAVEL (BALLAST) 0.5
0.3 Macro Core 0 -2'
Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete & Brick (FILL)
4 ,0
Macro Core 2'-4'
Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FlLL, wet)
6.0
4.0 Macro Core 4'-6'
Red-Brown fine to medium Sand, trace Silt
8.0
0.4 Macro Core 6 -8'
9.0-
10.0-
1 1 .0 -
12.O-
End of Boring at 8'
Groundwater Grab Sample Collected
Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = 1-'10%
Driller: W. Lineberry
Elgj Geoprone 54lU
Depih to Water: 4'
Borinq Depth: 8'
Borino Oia.: 2"
Paqe: 1 of 1
Page 69
Elgigg! T6mporary M-8 Acceptance Facility
!999!!9q. New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: M8F-15
Inspector: C. Criscuolo
Date: 3-19.07
l ^
i o( t l
Loqical Environmental Solutions354 Souih River Road
Tolland, CT 06084f ru c k, Poda b I e & A TV/B ac k hoe- rll ou nte.l G e o probe s
E 6q r o
o
U'
Description 5.aq ' { 'o g
o ao - =
Sample Interval
Ground Surface 0.0
1 .0 -
2.0-
3.0-
4.0-
5.0-
o-u-
7 _0-
rv q.h\.,/(\ n,/(ilrPri8:q:-Y:i;::q::o::ij ,F. +j;::o. :
;q:a:q:a;:q:'.o.t:q :i;i'.o.:
:q:l':q:iJ:::q:' .2$:qi; . ; .7:
:qi:qd:::q:
: i : ; : i : i t i : :
i{,'i-i{-'ritF. :'.4,i.q.i .:.r.1
i-l:r:!:.:i):'./.:i:qi:.1:
'.F.i:q i .: .a.1
:q:l':q:i:;::q:
....:
Gray medium to coarse GRAVEL (BALLAST) 0.5
0. '1 Macro Core 0'-2'
Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete & Brick (FILL)
4,0
3.4 Macro Core 2 -4'
Black Ash & Cinders, lattle fine to coarse Sand, trace fine tocoarse Gravel {FILL, wet)
6.0
3.4 Macro Core 4 -6'
Red-Brown fine to medium Sand. trace Silt
8.0
0.6 Macro Core 6'-8'
9.0-
10.0-
11 .0 -
12.O-
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-10%
Driller: W. Lineberry
8!gj Geoprone 540U
Depth to Water: 4'
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: I of I
Page 70
GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility Borinq: M8F-16
Location: New Haven Rail Yard Inspector: C. Criscuolo
9U9!l[ Maguire croup Inc. Date: 3-21-07
toa r .
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Portable & ATvlBackhoe-Mounbd Geoprcbes
€a6 E
o
o
Description - c ^X r i@ a Do g
o a- o .
Sample Interval
Ground Surface 0 .0
1 .0 -
2.O-
3.0-
4.0-
5.0-
6.0-
7 .O-
':i+: ii,i: i ii.
: { i : { i j i : { :'.d..j;:2i; .;.4:
:c:ii :q:i:i:q:i
+i:,i::4.:l
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
0 Macro Core 0'-2'
0 Macro Core 2'4'
_ d : . o : - . t t :. -o . . - a . . . .4' O r ' q : C O l
: ; .9.. ..q. .; ; .19 : .o:: . i9 :- : o . . o . . . : 4:O r 'O ;CO l9 ' : a : . c l :. : o - . o . : . : 4' O j O : d O . -
, ' .o , . .q . . . , , {
Red-Brown fine to medium SAND, little Silt, trace fine to coarseGravel
Groundwater at 4'4.0
5.00 Macro Core 4'-6'
ffiGray Clayey SILT
8.0
0 Macro Core 6'-8'
9.0-
10.0-
1 1 . 0 -
12.0-
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% littte = 10-20% trace = 1.10olo
Driller: W. Lineberry
BiS. Geoprone 540U
Deoth to Water: 4'
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: 'l of 1
Page 71
r a .
i o\!t I
Loqical Environmental Solut ions354 South River Road
Tolland. CT 06084Truck, Portable & AfV/Ba*hoe-M ounted Geopmbes
Proiect: Temporary M-B Acceptance Facility
Location: New Haven Rail Yard
Client: Maguire Group lnc.
Borinq: MgF-17
Inspector: C. Criscuolo
Date:3-21-07
E 63 e jt
Description cl oto q , 6 a
E E
Sample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
4.0-
c.u_
o . u -
7.0-
i3:'.:b.'.'i :i]:t:aj;.i.;:'.zti
r:q:i:{ii:q:i
r:o.:;j:9i..j .q:i
i'-i:iFj. : o - . c l . . c
, .O .q . . : IA :9 : . 4 -d :' : o . . - o . . : i
+ i i ' i ' c b i'1o. . - c . : (r , 9 . . q . r , . 1; . ; . . ; .
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
2 .5
0 .1 Macro Core 0'-2'
1 .9 Macro Core 2'-4'Red-Brown fine to medium SAND, little Silt, trace fine to coarseGravel
Groundwater at 4'4.Q
5.03.6 Macro Core 4'-6'
W4
+1Gray Clayey SILT
8.0
0 Macro Core 6'-8'
9.0-
10.0-
| | . u -
12.0-
End of Boring at 8'
Soil Descriotion: and = 35-50% some = 20-35% little = 10'20% trace = l-10%
Driller: W. Lineberry
Blgj Geoprone 540U
geslL@ls4'
&4!s-9s88'
Borino Dia.: 2"
Pgge:. I of 'l
Page 72
I
i ol r l
Loqical Environmental Solul ions354 South River Road
Tolland. CT 06084Truck, Portable & ATUlBackhoe-MounGd Geoprcl€s
elgigli Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
gliqli Maguire Group lnc.
Borino: MgF-18
USpCglgC, C. Criscuolo
Date: 3-21-07
=;ao ( ,o = o
Description t L oo o o a
o - - =
Sample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
4.0-
J . U -
6.0-
7 .O-
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
0 Macro Core 0'-2'
0 Macro Core 2'4'I : .O- .C.O. : o . . o . . . 'Q . o : c O
o : -o. ,+o. 1 4 . . q . . . :o . _ o : c oo :.o;i.!.o'' ' o - o . : . '
Red-Brown fine to medium SAND,Gravel
Groundwater at 4'
little Silt, trace fine to coarse
4.0
U Macro Core 4'-6'w)ffi+r4
Gray Clayey SILT
8.0
0 Macro Core 6'-8'
9.0-
10.0-
t z , v '
End of Boring at 8'
Soil Descriotion: and = 3$50% some = 20-35% little = 10-20% trace = l-l0o/"
Driller: W. Lineberry
B!$. Geoprone 5/()U
Depth to water: 4'
Borinq Oeoth: 8'
Borinq Dia.: 2"
Pgge: I of I
Page 73
Proiect: Temporary M-8 Acceptance Facility
Egel!g![ New Hav6n Rail Yard
Client: Maguire Group Inc.
Borinq: M8F-i9
Insoeclor: C. Criscuolo
Date:3-21-07
I
i of l i
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084T ruck, Podable & ATv/Backhoe-Mounted Geoprobes
E 6o o
6
Description E 6o oo =
. r iSample Interval
Ground Surface 0 .0
4.0-
6.0-
':ii::ii"::i;
:F-ij .9ii :;:el:
:i:; :'. iJ j:"1:i.t:a:l:rt.l:
:q:i;q:i-j:q:
:{j.:q:ii:q:
:;.i::t:;r :;:i::'l:;'::q :i.r i:el:
:q:ij:o. iij:e.:
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt, mlxed with Gray to OliveBrown Clayey Silt (FILL)
Gtoundwater at 5'5.0
0 . 1 Macro Core 0'-2'
2.6 Macro Core 2'4'
Macro Core 4'-6'5.5
Black ASH & CINDERS {FILL)
8.0
0,3 Macro Core 6'-8'
9.0-
10.0-
I t . u -
12.0-
End of Boring at 8'
Soil Descriotion: and = 35-50o/o some = 20-35% little = 10-20% trace = t-10%
q!0!9! W. Lineberry
8!g: Geoprone gou
Deoth to Water: 5'
Borinq Depth: I'
Borinq Dia-: 2"
@ , 1 o f 1
Page 74
Plgigll[ Temporary M-8 Acceptance Facility
kggll$ New Haven Rall Yard
gljgq! Maguire Group Inc.
Borino: M8F-20
Inspector: C. Criscuolo
@3-21-07
I
0Loqical Environmental Solut ions
354 South River RoadTolland, CT 06084
Truck, Podable & ATV,/B atkhoa-Mounted Geoprobes
E L Oo o
E
o
Description z ,rio oo g
o dSample Interval
Ground Surface 0.0
1 .
2 .
3 ,
4,0-
5.0-
6.0-
7.0-
:qi:qi i;qj
rir''?+ j:ii
i .11.:f :ait-: ;q:i :{:i j ;{:1 ...i .z i; j .zl
t.q:tr:i:.::/.:
: .ai:q i .; .2)
::q: i :{+:.r:q.
t:d.t;:z ii .i:o.l
;:q:i :{a:.::q:
i'.d.i:iii!:d.:
i'.l:i.(t ,i:o.t
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt, mixed with Gray to OliveErown Clayey Silt (FILL)
Groundwater at 5'5.0
0 .1 Macro Core 0 -2'
0.4 Macro Core 2'-4'
0 .1 Macro Core 4'-6'5.5
:q:ii:qi i:q:ir:cl:i ?:i.l :.:I:ii.!1t+:! :i-lt--.::q:iit:ii:;.q:i
::"-;j :e ir :;:qji
: :'.:i:'.i i:.:i: :'::;_: :D. :i.r j:ol:i
Black ASH & CINDERS (FILL)
8.0
0 Macro Core 6'-8'
9.n -
0-10 .
1 1 . 0 -
12.O-
End of Boring at I'
Soil Descriotion: and = 35-50% some = 20-35% little = 10-20% trace = l-10%
g[er: W. Lineberry
Big: Geoprone 54(lU
Deoth to Water: 5'
gpfjls-qellE8'
Borinq Dia.: ?"
Eegg, 1 of 1
Page 75
GEOPROBE SOIL BORTNG LOG l 0f I r
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, PorAble & ATU/Backhae-t ounled Geoprobes
Proiect: Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
Client: Maguire Group Inc.
Borino: M8F-2'l
hslector: C. Criscuolo
Date:3-26-07
sg U'
Description 5 ac L o{ r o o o -
Sample Interval
Ground Surface 0.0
'1 .0-
2.0-
3.0-
Gray medium to coarse GMVEL (BALLAST) 0.5
0 Macro Core 0'-2'
Black ASH & CINDERS, little Brick & Gray Sitt (FtLL)
4.0
U Macro Core 2'-4'
Refusal on CONCRETE at 4'
Soil Descriotion: and = 35-50% some = 20-35% little = 10-20% trace = 1-10%
Driller: W. Lineberry
BiS, Geoprone 540u
Depth to Water: Dry
Borinq Depth: 4'
Borino Dia.: 2"
Paqe: I of 1
Page 76
GEOPROBE SOIL BORING LOG | -il
i ot t l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Tructr, Portable & Afv/Backhoe-Mounte.l Geoprobes
e!gig!: Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
gliClg Maguire Group Inc.
Borinq: MgF-22
Uaso€ctor: C. Criscuolo
Date: 3-21.07
o o
o
oDescription
cL (lto (tt c I 0 -
d g
Sample Interval
Ground Surface 0.0
i-!1r,1:ali!'.:F. : ; j : ' . i : : ; : ' . :
i-qld,! i:i!:
Black ASH & CINDERS, liule fine to coarse Sand, trace fine tocoarse Gravel {FILL)
1 . 0
3.0
0 Macro Core 0'-2'i'-F:;l. : 0 . . - o . 1 . : <'o , . o :co . .
i :.o..i.ii '-:. 1O ._ - O : . : <' a
. . q : i . a lrr P: : .q.. : : Jo : 6 . ' ; b - :
Red-Brown fine to coarse SAND
0 Macro Core 2'-4'
:'jj :d. rii ::?.:
: .r'.i !:4 .; .t l
Dark-Gray to Black fine SAND & SILT, little Ash & Cinders{FILL)
Groundwater at 6'6.0
Macro Core 4'-6'
:i,;::c,.:i:q:i;".:i:'.i.j:"..ii ! : i i :5: i i i l l.q:! :{i:.r :q:
r:q:i::t:i :,::q: 8.0
Macro Core 6'-8'
9.0-
10 ,0 -
1 1 . 0 -
I z . u -
End of Boring at I'
Soil Description: and = 35-50o/o some = 20-35olo little = 10-20% trace = 1-10%
Driller: W. Lineberry
8jg, Geoprone 5,40U
Depth to Water: 6'
Borino Depth: 8'
Borinq Dia.: 2"
Paqe: I of 1
Page 77
elgiegE Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
Clieni: Maguire Group Inc.
Borinq: M8F.23
Inspector: C. Criscuolo
Date:3-21{7
l 0!7 1
Loqical Environmental Solut ions354 South River Road
Tolland. CT 06084Truck, Poitable & AMBackhoe-Mounte<t Geoprobes
€ ao oo g o
Description ; :o a bo g
o ao - =
Sample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
4.0-
5 .0 -
6.0-
7 .O-
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
1 . 00 Macro Core 0'-2'.1-Fi.6t' : o . . o . : : (
4 . q : c O . -_ : o . - o - , : (a', o.lsi'-,. ' _o . . o . : : (O r ' O : C O .. : 4 . O . : <
_o : .o: _c.o :
Red-Brown fine to coarse SAND
3.0
6.0
0.4 Macro Core 2'-4'
i.a.t:..'.t::{:i:{i
::eli::".':i.l
::q:a:{:i
i.+:.:+:!
li.4.:;.q:
:i::.:: t -1:
:.:.q:
t,:ti:
Dark-Gray to Black fine SAND & SILT, little Ash & Cinders (FILL,Detroleum odor)
Groundwater at 6'
0.3 Macro Core 4'-6'
8 .0
0 Macro Core 6'-8'
9.0-
10.0-
1 '1 .0 -
12 .0 -
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-10%
Driller: W. Lineberry
Blgj Geoprone 540U
Depth to Water: 6'
Borinq Depth: 8'
Borinq Oia.: 2"
Eggg, 1 of 1
Page 78
Elgi$h Temporary M-8 Accepiance Facility
!999!!9!j New Haven Rail Yard
Client; Maguire Group lnc.
Borino: M8F-24
EgE!g!' C. Criscuolo
Date:3-21-07
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Ponable & ATv/gackhoe-Mounted Geoprcbes
E 6o q ,
o
Description c L oo oo = -
o ao - ' =
Sample Interval
Ground Surface 0.0
l1 .0 - l
2.0-
3 .0 -
4.0-
5.0-
6.0-
7 .0-
Black ASH & CINDERS, little fine lo coarse Sand, trace fine tocoarse Gravel (FILL)
1 . 00 Macro Core 0'-2'
o o . . t _ o : l. 4 . - " o l
: c o
o . c,oa'o r ' o , gq
; : ; , . ' ' ; ;
Red-Brown fine to coarse SAND
3.0
o . u
1 . 6 Macro Core 2'-4'
Dark-Gray to Black fine SAND & SILT, Iittle Ash & Cinders (FILL'petroleum odor)
Groundwater at 6'
u.o Macro Core 4'-6'
8.0
0 Macro Core 6'-8'
9.0-
10.0-
1 1 .0 -
12.O-
End of Boring at 8'
croundwater Grab Sample Collected
Soil Description: and = 35-5oo/o some = 20-35o/o little = l0-20o/o trace = 1-10%
Driller: W Lineberry
Eig= Geoprone 540U
Depth to Water: 6'
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: I of 1
Page 79
GEOPROBE SOIL BORING LOGProiect: Temporary M"8 Acceptance Facility Borinq: M8F-2S
Location: New Haven Rail Yard Inspector: C. Criscuolo
Client: Maguire Group Inc. Oate: 3-21-07
t ^
i oq t l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Portabte & ATvlgackhoe'Mounte<l ceoprobes
se (t
Description 5 ac L oo o o a
o - =
Sample Interval
Ground Surface 0.0
1 0 -
2.0-
3.0-
4.0-
5.0-
o-u-
i-!1J:!12:i-!1
i-!1.:!11:i-U
:q:i-c:i:;;q:
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,littfe fine to coarse Gravel, trace Silt, mixed with Grav to OliveBrown Clayey Silt (FILL)
Groundwater at 5'5.0
0 .1 llacro Core 0'-2'
1 . 1 Macro Core 2 -4'
u.c Macro Core 4'-6'5 .5
;:q:i:q:ir:;.{:i
::".:;r: u.;r;;:'.:i
: :q, i :qi i :qi
: :" . :d:r. : i i :q.: i
:q+:{: i : :q: i
:o. i: :'. i:i:F. I
Black ASH & CINDERS (FILL)
8.0
0 Macro Core 6'-8'
9.0-
10 .0 -
1 1 .0 -
' t2.0-
End of Boring at 8'
Soil Descriotion: and = 35-50% some = 20-35% liftle = 10-20% trace = 1-10%
Ddller: W. Lineberry
Bj$. Geoprone 540U
Depth to Water: 5'
Bodnq Deoth: 8'
Borino Dia.: 2"
Paoe: 1 of 1
Page 80
r a .
O\ t l
Loqical Environmental Solut ions354 South River Road
Tolland, CT 06084fruck, Poraa e & ATvlBackho*Mounted Geoprobes
Proiect: Temporary M-g Acceptance Facility
tggali$. New Haven Rail Yard
glg!l!: Maguire Group Inc.
Borino: M8F-26
Inspector: C. Criscuolo
Daie:3-19-07
€ crL ol
3 E (t
Description o. o,o oo =
O C LSample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
4.O-
5.0-
o_u-
7 .O-
Dark-Brown to Black fine to coarse SAND, little Ash & Cinders,trace Concrete. Brick & fine to coarse Gravel (FILL)
2.0
0.3 Macro Core 0 -2'
:q:l,{:ir:.;:q:
:?l:i ?|i.j i3. :
:"j;-::''.:ii:::ol: Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL. wet)
Groundwater at 5.5'5.5
0.9 Macro Core 2 -4'
.f:i.:";{:.ij
Macro Core 4'-6'
8.0
0.2 Macro Core 6'-8'
9.0-
10.0-
'1 1 .0-
12 .0 -
End of Boring at 8'
Soil Descriotion: and = 35-50% some = 20-35% little = 10:20old trace = 1'10%
Driller: W. Lineberry
Elgj Geoprone 540U
Oepth to Water: 5.5'
Boiinq Depth: 8'
Borinq Dia.: 2"
Eggg! I of I
Page 81
Slgigg[ Temporary M{ Acceptance Facility Borinq: MgF-27
!99el!!9![ New Haven Rail Yard Inspector: C. Criscuolo
g!!g!: Maguire Group Inc. Date: 3-21-07
I
i o\7 I
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Portable & ATvlBackhoe-Mounted Ceoprobes
E 6q r oo g
Eo
Description €.ao o6 =
o aE g
Sample Interval
Ground Surface 0.0
i.i.
i.t.
i.q.
,..t,
' :..:
o
9
o i c a'. :q . : ;.ar ,Jg
.a,l.ii,_ .o . : - :' o : c o' ' o . :i r r ' ; i
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
?.5
Macro Core 0'-2'
0 .1 Macro Core 2'-4'Red-Brown fine to medium SAND, little Silt, trace fine lo coarseGravel
Groundwater at 4'4.0
5.00 Macro Core 4'-6'+1
uGray Clayey SILT
8.0
0 Macro Core 6 -8'
9.0-
10.0-
1 1 . 0 -
12 ,0 -
End of Boring at 8'
Soil Descriotion: and = 35-50% some = 20-35% little = 10-20% trace = 1-10olo
Driller: W Lineberry
Bigj Geoprone 5,40U
Deoth to Water: 4
Borinq Oepth: 8'
Borino Dia.: 2"
Paqe: 1 of 1
Page 82
GEOPROBE SOIL BORING LOG l 0r I '\ y l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Po.lable & Aw/Aackhoe-Mounted Geoqobes
Proiect: Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: M8F-28
Insoector: C. Criscuolo
Date:3-21-07
E 6r D o
o
IJ'
Description x ?o o o a
o - s
Sample lnterval
Ground Surface 0.0
1 .0 -
2.0-
3.0-
4.0-
5 .0 -
6.0-
7 .O-
:q: l ;{ : l r :ql
:{i;;q:ii:qi
:". :;:j :o. :;rj .;?:l
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
2.5
4.0
0 Macro Core 0'-2'
0,6 Macro Core 2'4'i":iJiF::o . . o . . . :<'o .. a :co.-
, { . ,9. . i r '1o a . c 9 ;' : o . . o - . . : (o . -o .co - 'o : o j i t o :' : o . . o - : . : (
,1 o.,. ,9..ir '1
T+)i l l+r)| l l
){)i l ll)- |
Red-Brown fine to mediumGravel
Groundwater at 4'
SAND, little Silt, trace fine to coarse
5.00 Macro Core 4'-6'
Gray Clayey SILT
8.0
Macro Core 6'-8'
9.0-
10.0-
1 1.0-
12.0-
End of Boring at 8'
aoil Description: and = 3$50% some = 20-35% fiftfe = 10-20% llace = 1-10o/o
Driller: W. Lineberry
&, Geoprone 540U
Depth to Water: 4'
Borino Depth: 8'
&dry-Pjsn2"
Paq€; I of 1
Page 83
Plgigg Temporary M-8 Acceptance Facility
!99a!!9!j New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: M8F-29
Inspector: C. Criscuolo
Date:3-21-07
Logical Environmental Solut ions354 South River Road
Tolland, CT 06084fruck, Portahle & AfvlBackhoe-Mounte.l Geoprobes
* eo q t
E
o
Description E 6o o6 g
o a Sample Interval
Ground Surface 0.0
1 . 0 -
2.O-
3 0 -
4.0-
5.0-
o.u-
7 .O-
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
1 . 00 .1 Macro Core 0'-2'a-Fii
. - . o . . o . . :
j ; P . . - q . : ;
C: .or'J.o.-_o.. o.'. ..
- : 4 . O . . :
b : o , ' - 4 i' : o . . o - . :- : o ' . - o - . :
i : i : ' .ai. -_o . . o - ' . . .g- : o. .co. : o . _ o . 1 . -O r ' O i C O; ;9 . . 9 . . ; ;pi4-;# Aq : o . c g. : o . . - o . . -o - o : c o::.9. ..9...: lg_ : o : : . co' : o . . - o . . :q . -o : c .o; i .9 . .1 . . , ;9_ : -o r : .4O' 1 0 . . ' o . :
; , .o . . .q . . : ;O : _or1.cO' t o . _ o . . . :
:9
n:
1:
9I9o
:.
Red-Brown fine to medium SAND. little Silt. trace fine to coarseGravel
Groundwater at 4'4.0
1 . 1 Macro Core 2'-4'
0.5 Macro Core 4'-6'
Dark-Brown medium to coarse SAND. trace Silt
8.0
0 Macro Core 6.-8'
9.0-
10.0-
1 .1 .0-
12.O-
End of Boring at 8'
Soil Description: and = 35-50% €ome = 20-35% little = 10-20olo trace = 1'10%
gfi!!g' w. Lineberry
E!S, Geoprone 5401J
Depth to Water: 4'
Eel!!s-ge&8'
Borino Dia.: 2"
Pegg. 1 of I
Page 84
GEOPROBE SOIL BORING LOG
elgigq!: Temporary M-8 Acceptance Facility Borinq: M8F-30
!Egl[g$, New Haven Rail Yard Inspector: C. Criscuolo
g!C!l!i Maguire Group Inc. Date: 3-21-07
I
l o( t l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Poraaue & ATv/Backhoe-Mounbd Geoprcbes
E 6o o
E
.n
Description : :o oo 9
o aSample Interval
Ground Surface 0.0
I
' o-l
2.O'
3.0-
4.0-
5.
6.
7.0-
;;;,:;;f J:il:'-:ij :t i: :i :"::
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
1 . 00 Macro Core 0'-2'i'-Tdil' - .o . o . .q
o r ' d : C a l;; P-. .q . : ; {o : o . 4 0 :- : a . . o - : . aO r ' O : { O jrr p- ..9 .i;.t-o : .o: .c.o :. ' .o . . 'o . : . :o
: , P . . q . . j ; . {b: + : ' -co ' :. : o . . o . . . : 0c : c : . q g ,. : o . . 0 . : . : a'o r'c .c.o --, ,n. . lq. . ; , . !4r i+ c:o : c . c a :: o . o - : . : o
' : a . o . : to : .0 : . c .o :' .o . . 'o . : . -4' o : o ' : c o r, 'O . . .q . ; i .1_d : .o r ' .4 .o :- :o . . o l . c: o - o : 4 q . .t : 9 : . . q . j : Ib ; o r ' . c b :. o . o : t (
Red-Brown fine toGravel
medlum SAND, little Silt, trace fine to coarse
Groundwater at 4'4.O
0.3 Macro Core 2 -4'
5.0
8.0
0.1 Macro Core 4'-6'
Dark-Brown medium to coarse SAND, trace Silt
0 Macro Core 6'-8'
9.0-
10.0-
1 1 . 0 -
12.0-
End of Boring at 8'
Soil Description: and = 35-5{rolo some = 20-35% little = 10-20% trace = 1'10%
Driller: W. Lineberry
Bigj Geoprone 540U
Deoth to Water: 4
Borinq Deoth: 8'
Borinq Oia.: 2"
Paqe: 1 of 1
Page 85
Proiect: Temporary M-B Acceptance Facility
!994!!9!! New Haven Rait Yard
Client: Maguire Group Inc.
Borinq: M8F-31
Inspector: C. Criscuolo
Date:3-21-07
I
A O\!t I
Logical Environmental Solutions354 South River Road
Tolland. CT 06084f.uck, Pottable & ATvlBackhoe-Mounted Geoprohes
=aao oo g o
Description a 6o o6 g
o ao - =
Sample Interval
Ground Surface 0.0
'1.0-
2.O-
3.0-
4.O-
o.u-
i.qld:l:jit.l
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt {FILL)
1 . 00 Macro Core 0'-2'
$ : .o:. .4.d. : o . . - + 1 . .o : o : C o. : o . - o - , . :
_o : _o: ,c_d: o . . o . . . :
' : o ' - o . - :
_o :qi .c9'' : o . . q . . . :
i i -o:. .:C... i;o : .c ; . co. : o . o - : . 'o - o ; c ci;d. .9... i jo : 9 ; . 4 9. - o . . o . . . 1-^--:at it, , .w .w.v. ' _o . . + . :o r ' o : c o. : o . o , :9 :.o j:.{.o. : 0 . - o . 1 . -
:;o: ' :4..:;o : a : r . a q' :a - . + . . - - .a : o c o
0 : a r ' . c 4' 'o . o ._ . . :
Red-Brown fine to medium SAND. little Silt. trace fine to coarseGravel
'. Groundwater at 5'
1 . 7 Macro Core 2'-4'
0.5 Macro Core 4'-6'
8.0
Dark-Brown medium to coarse SAND. kace Silt0 Macro Core 6'-8'
9.0-
10.0-
12.0-
End of Boring at 8'
Soil Description: and = 35-50o/o some = 20-35% liftle = 10-20% irace = 1.10%
Driller: W. Lineberry
[!91 Geoprone 540U
Depth to Water: 5'
Borino Deoth: 8'
Borinq Dia.: 2"
Paqe: 1 of 1
Page 86
elgiglE Temporary M.8 Acceptance Facility
!9ga!!9!! New Haven Rail Yard
gljggE Maguire Group lnc.
Borinq: M8F-32
Inspector: C. Criscuolo
Date:3-19-07
l / l
l oC l r
Loqical Environmental Solut ions354 South River Road
Tolland, CT 06084Truck, Porlattle & AruEackhoe-Mounted Georyobes
E 6o o
o
E
at
DescriptioncL dto oo 9
o a Sample Interval
Ground Surface 0.0
1 .0 -
7 .O-
: :q:a;q: i i :q: i
: t i t i i , i i : i . : i
::q:ari-::q:i: :". :;: F. ir j:cl:i
;:t:it_-:i:::n
Dark-Brown to Black fine to coarse SAND. little Ash & Cinders,trace Concrele, Brick & fine to coarse Gravel (FILL)
2.0
o.2 Macro Core 0 -2'
Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FlLL, wet)
Groundwater at 5.5'5.5
1 . 1 Macro Core 2'4'
0.5 Macro Core 4'-6'
8.0
0 .1 Macro Core 6'-8'
9.0-
10 .0 -
1 1 . 0 -
't2.0-
End of Boring at 8'
Soil Descriotion: and = 35-50% some = 20.35% little - 10-20% trace = l-10%
pd!!e! w. Lineberry
!!g; Geoprone 540U
Oepth to Waler: 5.5'
Borino Deoth: 8'
Borinq Oia.: 2"
Begg, 1 of 1
Page 87
GEOPROBE SOIL BORING LOGelgigg! Temporary M-8 Acceptance Facility
!99a!!9I[ New Haven Rail Ya.d
Client: Maguire Group Inc.
Borinq: M8F-33
InsDector: C. Criscuolo
Date:3-21-07
I
i ot t i
Logical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Po.table & Afv/Backhoe-Mounted Georobes
E 6C ' O
oll
o
Description : :o oo g
o ao - =
Sample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
4.Q-
5.0-
6.0-
7 .0-
:q,!:{:i:.::q,i
i,tii:F:' t o . . - o . . . : {, ,O. .q. . : i .1g : 9 . . . c o :. : o - . + . . . : 4o : - o d+ l,,O. :q .. i!.1o : o ; . c o :. : o . . + . . : 4'c ..-o : c? ..: , .o-. .:1 ...; .1-+ : 9r'.C-O :' o . - o : c a l;,.9.. .q...,; IO : o : r . 4 9 - :. : o . . - 4 . . . : i
: j .o-. .q .i:.10 : o r ' ' + o :: o . . o . . - : c' q . . - c g a l
:' o;. .1, :,1.o : 9; .c.4 :' ' o . _ o . : . : 4' O
r - O : C O . .rl.9- -y1..:r I
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL)
5.5
0 Macro Core 0'-2'
Red-Brown fine to coarse SAND, trace Silt & fine to coarseGravel
Groundwater at 5.5'
0.1 Macro Core 2'-4'
0 Macro Core 4'-6'
6.5
0 Macro Core 6'-8'I+))+)Gray Clayey SILT
8.0
9.0-
10 .0 -
1 1 . 0 -
12 .O-
End of Boring at 8'
Soil Descriptlon: and = 35-50o/o some = 20-35% little = 10-20% trace = 1'10%
Driller: W. Lineberry
Sigj Geoprone flou
Depth to Water: 5.5'
Esrus-gs48'
Borinq Dia.: 2"
Paoe: I of 1
Page 88
Plgiggltj Temporary M-8 Acceptance Facility
!99at!9!! New Haven Rail Yard
g!jg!l!: Maguire Group Inc.
Borinq: MgF-34
h9p9q!9! C. Criscuolo
Date:3-21-07
r / l
i of l l
Logical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Portabte & Afv/Beckho*Mounte.I Geoprcbos
o o! r oo g
oco
Description 6.6o oo g
o ao - g
Sample Interval
Ground Surface 0.0
1 .0-
2.0-
3.0-
5.0-
6 .0 -
7 .O-
:i,i':.'i,r'::i:
!riiF:- : o . . o . . : {j , .o - . .9 . . i , I0 :_or,.c.o :
; , .o - .9 . . . , , Io : 9 : . 4 9 ,- t o . c . . . : (
r r .9 . . .9 . . i ; Io : q : : . + o :' 1 0 . . c . . : (
r , .9 . . . .q . . : i .19 : 9 . . 4 9 :' ' o . . c . . : <' : o , o . , : <
9 : . o j . c 9 :
r r ' - o . q , : j lo : .or'.{4 :
r . . 4 . - . q - . ; ; J
Dark-Gray to Black fine to medium SAND, some Ash & Cinders,little fine to coarse Gravel, trace Silt (FILL) 0.5
5.5
0 Macro Core 0'-2'
Red-Brown fine to coarse SAND, trace Silt & fine to coarseGravel
Groundwater at 5.5'
0 Macro Core 2'4'
0 Macro Core 4'-6'
6.5
0 Macro Core 6'-8'W)k)
Gray Clayey SILT
8.0
9.0-
10.0-
1 1 .0 -
12.0-
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% liftle =10-20% trace = l-10%
Driller: W. Lineberry
E!S, Geoprone 540U
Depth to Water: 5.5'
Borlno Deoth: 8'
Bodnq Dia.: 2"
Paoe: I of I
Page 89
GEOPROBE SOIL BORING LOG ioC l l
Logical Environmental Solutions354 South River Road
Tolland. CT 06084Truck, Portable & ATvlBackhoa-Mounte.t Geoprobes
Proiect: Temporary M.8 Acceptance Facility
Location: New Haven Rail Yard
glblE Maguire croup Inc.
Borinq: M8F-35
Inspector: C. Criscuolo
Date:3-26-07
-*E6 s \o
Description E O
o ( , o 5 .Sample Interval
Ground Surface 0.0
5.0-
6.0-
7.0-
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
2.0
0 Macro Core 0'-2'
; :q : i .q+ : j :q : l
;:c.:;j:o. i,;:;:".ri
;:q:i-q:ir:i:q:i
i . l : . : l r i . i . t : :
i.5.'. i:+'.a it.i:
r .q l r :+1! . t l : r
i .q: . q l i ; i9 : :
:l:.:4.; ":qi
i . ! : . : l . i : i . ! : r
Black ASH & CINDERS
Groundwater at 4.5'4.5
Macro Core 2 -4'
0.4 Macro Core 4'-6'
8.0
0 Macro Core 6'-8'
9.0-
10.0-
12.0-
End of Boring at 8'
Soil Description: and = 35.50% some = 20.35% little = 10-20% trace ='l-10%
Driller: W. Lineberry
Bigj G€oprone 540U
Deoth to Water: 4.5'
Borino Depth: 8'
Borinq Dia.: 2"
Eggg. 1 of 1
Page 90
GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility Borinq: MBF-36
Location: New Haven Rail Yard Inspector: C. Criscuolo
Client: Maguire Group Inc. Date:3-26-07
t l
i of l l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, P ottable E Afvlaackhoe-Mounted Geoprcbes
t ^E 6o o
o
Description E 6o o o A
- c rSample Interval
Ground Surface 0.0
'I .0-
2.0-
4.0-
5.0-
6.0-
7 .O-
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
2.0
0 Macro Core 0!2'
Black ASH & CINDERS
Groundwater at 4.5'4 .5
0 Macro Core 2'-4'
0 Macro Core 4'-6'
8.0
0 Macro Core 6'-8'
9.0-
10 .0 -
1 1 . 0 -
12.0-
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% tittle = 10-20% trace = l-10%
Drill€r: W. Lineberry
Ejgj Geoprone 54Ou
Depth to Water: 4.5'
Borinq Oepth: 8'
Borinq Dia.: 2"
Paqe: I of I
Page 91
llgigglE Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
gI!S!l[ Maguire Group Inc.
Borinq: MgF-37
InsDector: C, Criscuolo
Date: 3-26-07
I
A O( t l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Po,TaNe & ATv/Backhoe.Mounte.l Geoqobes
Macro Core 0 -2'
Macro Core 2L4'
Macro Core 4'-6'
Macro Core 6'-8'
Black ASH & CINDERS, Iittle fine to coarse Sand, trace fine tocoarse Gravel (FILL)
2.0
4.0
0
0.4
0.3
0
End of Boring at 8'
Driller: W. Lineberry
Elgj Geoprone 540U
Depth to Water: 4'
Borinq Depth: 8'
Eorinq Dia.: 2"
eg$,1 of 1
Page 92
GEOPROBE SOIL BORING LOGelgigli Temporary M-8 Acceptance Facitity
!99a!i9E New Haven Rail Ya.d
Client: Maguire Group lnc.
Borino: M8F-38
Inspector: C. Criscuolo
Date:3-26.07
l 0a t l
Logical Environmental Solut ions354 South River Road
Tolland, CT 06084Truck, Portable & Afv/Backhoe-Mounted Ceoprobes
a 6q r oo g o
Description E E{ r oo g
Fo 6 .
Sample Interval
Ground Surface 0.0
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
2.0
0 .1 Macro Cole 0'-2'
:q:i:4i:i:q:i
:,::; :'. i. :i :'. :ii.!:r:!:rilr
,q;i :{rf I :q:ii3:-. 1:l :i!-.:q: : : t : ; i : i : " . : i
:q:i:q:ia:i:q:i
:ql:ir :o. i: :l :q:i
:q:i:qi j:q:i
:cl;::o. i'::i:P::i
:q: i :q: i i :q: ii-!1.:l1J:i-!i: " . : ; :F. : i : ;X: ii-t1.,:l:t :i-!ir:q:i:{ri:;:qri
;:". :i:'. :;i :;:9 :i
Black ASH & CINDERS
Groundwater at 4'4.0
o.2 Macro Core 2'-4'
8.0
0 Macro Core 4'-6'
0 Macro Core 6'-8'
9.0-
10.0-
1 1 . 0 -
12.O-
End of Boring at 8'
Soil Description: and = 35-50% some = 20-35% liftle = 10-20% trace = l-'10%
Driller: W. Lineberry
BlS Geoprone 540U
Depth to Water: 4'
Borinq Depth; 8'
Bodnq Oia.: 2'
@ , 1 o f 1
Page 93
Elgiggl! T€mporary M-g Acceptance Facility
Ee!!S, New Haven Rail Yard
gljgllE Maguire Group Inc.
Borinq: M8F"39
InsD€ctor: C. Criscuolo
Date:3-26-07
I
i o\ J t
Logical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Porlable & Afv/Backhoe-lt ounted Geoprcbes
1 .
3 .
A
5.
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel {FILL}
Black ASH & CINDERS
2.0
4.O
0
0 .1
U
0
Macro Core 0'-2'
Macro Core 2'4'
Macro Core 4'-6'
Macro Core 6'-8'
End of Boring at I'
Driller: W. Lineb€rry
Eigj Geoprone 540U
Depth to Water: 4'
Borinq Oepth: 8'
Borinq Dia.: 2"
Paoe: 1 of I
Page 94
Plqipd! Temporary M-8 Acceptance Facility
!9pq!!9!: New Haven Rail Yard
g!!q! Maguire Group lnc.
Borinq: MgF40
Inspector: C. Criscuolo
Date: 3-19-07
I
i.oLoqical Environmental Solutions
354 South River RoadTolland, CT 06084
Truck, Por'3ble & ATvlBackhoe-Mounb l Geoprobes
=aao oo g
co
Description E 6o o o a
Sample Interval
Ground Surface 0.0:i:i::i:i::::il:C:i- :t':i.r j :q:
:r-:; :r. :; r :r.:
rSirliir.{n
Dark-Brown to Black fine to coarse SAND, Iiftle Ash & Cinders,trace Concrete, Brick & fine to coarse Gravel (FILL)
2.0
0.9 Macro Core 0'-2'
:qi ! :q: i l :q: i
:"::i.r:".':i.::i:".:i
:c:i :q:ii :.: :q:i
:o::;r :o. i: :::'l:i
:q:i:q:i:i:q:ii - ! ' . . : l1i : i ! :
.{:i:qi i:qj
:". j;r :'. :;.j :;:'. :i
:qr i :q: i : ! : i;:q. :;.. :'. :iJ :;:q. :i
r:q:iJ:{ri,::::q:i
;:q. :;j ?:ij:;:q, :i
: :q: i :q: ir : . :q: i
::?:;r:a.:irij:q:i
Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
Groundwater at 5'5.0
J . O Macro Core 2'-4'
1 . 3 Macro Core 4'-6'
8.0
0.4 Macro Core 6'-8'
9.0-
10.0-
1 1 .0 -
12.O-
End of Boring at 8'
Soil Description: and = 35-50o/o some = 20-35% liftle = 10-20% trace = l'10%
Driller: W. Lineberry
B!g: Geoprone 540U
@!sg5'
Borinq Depth: I'
Borinq Dia.: 2"
gggCj 1 of I
Page 95
GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facitity Borinq: MBF-41
Location: New Haven Rail Yard Insoector: C. Criscuolo
Client: Maguire croup Inc. Date: 3-.19-02
r i
i o( t l
Logical Environmental Solut ions354 South River Road
Tolland, CT 06084Truc& Porlable & ATvlBackhoe-Mounted Geoprobes
€a3 E
occ,
Description * ao o o a
; i c L
Sample Interval
Ground Surface 0.0
1 .0 -
2.0-
3.0-
4.O-
5.0-
6.0-
::ii'?:ii: : t;a.ql'dl:t r.!:i:e. ii :qir j:'. ii.q:d.1.:t:i9:
:r:i;q:ai:qi::p.:i tq t;i tzi
' :qi :{ : i : :q: i
::q+j:{i j:qi
::F.ij:c. iji:".:i
::qi:r*:.::q:i
::c.:i,-:r.:;j::.ci
:.i.i"4ii:'...tii -+:. ! : t t ! :
:q:i:{i j:q:i
Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete, Brick & fine to coarse Gravel (FILL)
2.O
0.6 Macro Core 0'-2'
Black Ash & Cinders, liftle fine to coarse Sand, trace fine tocoarse Gravel (FILL)
Groundwater at 5'5.0
1 . 8 Macro Core 2'-4'
Macro Core 4'-6'
8.0
o.2 Macro Core 6'-8'
9.0-
10.0-
1 1 .0 -
12.0-
End of Boring at 8'
Soil Oescription: and = 35-50% soms = 20-35% little = 10-20% trace = 1-10o/"
Driller: W. Lineberry
Elgj Geoprone 540U
Deoth to Water: 5'
Borinq Deoth: 8'
Borinq Dia.: 2"
Paqe: I of I
Page 96
BgiggE Temporary M-B Acceptance Facility Borinq: M8F-42
Location: New Haven Rail Yard Insoector: C. Criscuolo
g!ig! Maguire Group Inc. Date: 3-26-07
r l l
i oLoqical Environmental Solutions
354 South River RoadTolland, CT 06084
fruck, Potable & ATvlBackhoe-Mounted GeoprctEs
E t oo o
E
tt,
DescriptioncL olo d t O C L
o - =
Sample Interval
Ground Surface 0.0
1 .0 -
2.O-
3.0-
: ;q: i :qr j i :q:
::o. :;::". j; i:o. I
::(:l :{i :.::4:
"4:i:4i;.::d,'
ASPHALT U.J
0 .1 Macro Core 0'-2'Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
ii:d:l:a:i.i:
i.l: r :|:ii :i-! .
: :q: i : ' . : ; r i : ' . : i
::q:a;q:i:.::q:i
r:q:it:i;::q:i
::'. ij trir :i:o::i
r:q:i:q:i:i:q:i
;:'l:i:". :i :i:q:i
::q,i::q:i jr:i
r:c.:;i:o.:ii:;r:ii.qlii:.b:ii :i-!1
:q:i::{:ij :;:q:i
BIacK ASH & CINDERS
Groundwater at 5'c.u
8.0
3.5 Macro Core 2'-4'
2.2 Macro Core 4'-6'
0.2 Macro Core 6'-8'
9.0-
10.0-
1 1 . 0 -
12.0-
End of Boring at 8'
Groundwater Grab Sample Collected
Soil Description: and = 35-50% some = 20-35% little = 10-20% trace = l-10%
Driller: W. Lineberry
B!g: Geoprone 54oU
Depth to Water: 5
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: { of I
Page 97
GEOPROBE SOIL BORING LOG I
O( t l
Logical Environmental Solutions354 South River Road
Tolland, CT 06084T I u c ?' P orlEb I e & ATU/Bac kh oe- M o u nted G eo p rc be s
Elgigg!: Temporary M-8 Acceptance Facility
!994t!9!! New Haven Rail Yard
Client: Maguire Group Inc.
Borino: M8F43
Inspector: C. Criscuolo
Date:3-26-07
E 6o o
o
Description E 6o o 6 a
Sample Interval
Ground Surface 0.0
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
2.0
0 Macro Core 0 -2'
Black ASH & CINDERS
Groundwater at 5'5.0
0 Macro Core 2'-4'
0 Macro Core 4'-6'
8.0
0 Macro Core 6'-8'
9.0-
10.0-
12,0-
End of Boring at 8'
Soil Description: and = 35-50% some = 20.35% little = 10-20% trace = l-'10%
Driller: W. Lineberry
B!$, ceoprone 540U
Deoth to Water: 5'
Borinq Depth: 8'
Borina Dia.: 2"
egE 1of 1
Page 98
glgi9g! Temporary M-g Acceptance Facility
!9ga!!9!: New Haven Rail Yard
Client: Maguire Group Inc.
Borinq: M8F.44
Inspector: C. Criscuolo
Date: 3-26-07
r ^ .
i o( J I
Logical Environmental Solutions354 South River Road
Tolland. CT 06084Truck, Porlable & ATv/Backhoe-Mounted Geoprcbes
E 6o oo g
oE
@
Description E aE g o A
Sample Interval
Ground Surface 0.0:q: i :{ i
:".:;:?:i
:q:;r:{:i
:":il:".:ii . l . . : l : i
:q:i:{:i
:q.:;j:?:i
:q:a:q:i
: " . : ; :o . : ;.q-{:q:i
:qi:q:i
i : i : { :
i:,::'::
::l:"::
::.::q:i:i.1.: i :?. ii:i.9.
:i:q::i
:--::q:ii:i.+.a-.:ql:i
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
4.0
0 Macro Core 0'-2'
0 Macro Core 2'-4'
Red-Brown fine SAND & SILT, trace fine Gravel (wet)
8.0
0 Macro Core 4'-6'
0 Macro Core 6 -8'
9.0
10.0
1 1 . 0
12 .0
End of Boring at 8'
Soil Description: and = 35-50% som6 = 20-35% little = 10-20% trace = 1-10%
Driller: W. Lineberry
Bj&, Geoprone 540U
Deoth to Water: 4'
Borino Deoth; 8'
Borino Dia.: 2"
Paqe: 1 of 1
Page 99
| -il
i of r t
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Podable & ATvlBackhoe-Mounted Geoprcbes
Proiect: Temporary M-8 Acceptance Facility
@3!9![ New Haven Rail Yard
Client Maguire Group Inc.
&!iE&. M8F-4s
Inspector: C. Criscuolo
@.3-19-07
€.ao oo g .A
Description 6.6It, oo g
o ao - 5
Sample Interval
Ground Surface 0.0
'1 .0-
2.O-
3.0-
4.0-
5.0-
o .u -
7 .0-
:ol; :D_ :;,r :i:ol:
'.n1.41i .: ..1
:'. :i t:i :; t:
:q:; .q:a:;:q:
:q: i :q: i : . : :q:
Dark-Brown to Black fine to coarse SAND, little Ash & Cinders,trace Concrete, Brick & fine to coarse Gravel (FILL)
2.O
1 .0 Macro Core 0'-2'
Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
Groundwater at 5'5.0
3 . 1 Macro Core 2'-4'
4 . 5 Macro Core 4'-6':".:;::o.:;- i;q.i
:q: i : { . j j ;q i
'9i .s :4 .: tz'.i
r:q:i:q:a:i:q:i;:q:;r :r. :i.: :l :r. :i
: :q : ; i :o . : i r : i :o . :
8.0
0.9 Macro Core 6'-8'
9.0-
10.0-
11.0-
12.O-
End of Boring at 8'
Soil Description: and = 35-50o/o some = 20-350/. little = 10-20% trace = 1-10%
gfi!!er: W. Lineberry
8!gj Geoprone 540u
Deoth to Water: 5'
Borinq Depth: 8'
Borinq Dia.: 2"
Paoe: I of I
Page 100
Elgigq[ Temporary M-8 Acceptance Facility
!9!g!94j New Haven Rail Yard
q!!gq! Maguire croup Inc.
Borinq: M8F.46
Inspector: C. Criscuolo
Date: 3.19-07
GEOPROBE SOIL BORING LOG
Soil Description: and = 35-50% some = 20-35%
r ^ .
i o( t rLoqical Environmental Solutions
354 South River RoadTolland. CT 06084
fruck, Poftable & ATvlAeckhoe-Mounbd Geoqrobes
cL olo d ,
o
o
Description!t 9l o a
Sample Interval
Ground Surface 0.0
1 .0 -
2.0^
3.0-
4.0-
5.0-
6.0-
7 .Q-
Dark-Brown to Black fine to coarse SAND. little Ash & Cinders.trace Concrete, Brick & fine to coarse Gravel (FILL)
2.0
0 .3 Macro Core 0'-2'
Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel {FILL}
Groundwater at 5'J .U
0.9 Macro Core 2'-4'
o.2 Macro Core 4'-6'
8.0
o.2 Macro Core 6'-8'
9.0-
10.0-
11.0-
End of Boring at 8'
little = 10-20% trace = 1-10%
Driller: W. Lineberry
8iS Geoprone 54DU
Depth to Water: 5'
Borlno Degth: I'
Borino Dia.: 2"
Paqo: 1 of 1
Page 101
&igq!: Temporary M-8 Acceptance Facillty Borinq: MgF47
!9e!!!9!j New Haven Rail Yard hsElq, C. Criscuolo
Client: Maguire Group Inc. Date:3-19-07
I
l o( t l
Loqical Environmental Solut ions354 South River Road
Tolland, CT 06084f ruck, Porta e & ATvl8ackhoe-ll ounted Geoptube$
=aarl, oo g
co
Description E to oo g
o 6 .o - =
Sample Interval
Ground Surface 0.0
, t n-
4.O-
5.0-
6.0-
Dark-Brown to Black fine to coarse SAND. little Ash & Cinders,trace Concrete, Brick & fine to coarse Gravel (FILL)
2.0
1 . 2 Macro Core 0'-2'
Black Ash & Cinders, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
Groundwater at 5'5.0
Macro Core 2'-4'
0.9 Macro Core 4'-6'
8.0
0.4 Macro Core 6'-8'
9,0-
10.0-
1 1 .0 -
12.0-
End of Boring at I'
Soil Description: and = 35-50o/o some = 20-35o/o little = 10-20% trace = l-10'/"
Driller: W. Lin€berry
&, Geoprone gou
Dsoth to Water: 5'
Borinq Depth: 8'
Borinq Dia.: 2"
Paoe: 1 of 1
Page 102
GEOPROBE SOIL BORING LOGrei$! Temporary M-g Acceptance Facitity Borinq: M8F-48
lgggl.iglt New Haven Rail Yard hspgglg! C. Criscuoto
g!g!! Maguire Group Inc. Date:3-26-07
t l
i of l r
Logical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Ponable & Afv/Backhoe-Mounted Geoprcbes
Black ASH & CINDERS, little fine to coarse Sand, trace fine tocoarse Gravel (FILL)
Red-Brown fine SAND & SILT, trace fine Gravel (wet)
4.0
0
0
0
0
Macro Core 0 -2'
Macro Core 2'-4'
Macro Core 4'-6'
Macro Core 6'-8'
End of Boring at 8'
p!i!!q' w. Lineberry
!!91 Geoprone 540U
Depth to Water: 4'
EI!s-g€&8'
Borino Dia.: 2"
egge:. 'l of 1
Page 103
GEOPROBE SOIL BORING LOGProiect: Temporary M-8 Acceptance Facility
Location; New Haven Rail Yard
Client Maguire Group Inc.
Borinq: MeF.49
Inspector: C. Criscuolo
Date: 3-15-07
r ^ .
i oq t l
Logical Environmental Solutions354 South River Road
Tolland. CT 06084fruck, P oftable & ATvlBeckhoe-tlou nted Geoqobes
E 6o oo g 6
Description E 6o oo g
o Eo - =
Sample Interval
Ground Surface 0 0
'1 .0-
3.0-
4.0-
5.0-
6.0-
7.0-
Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)
1 . 50 .1 Macro Core 0'-2'
ro'Ji.s .:'-:- .s.F:i).t':6 1; .?..t.sl .--ASl
.f '";"..f: v f t . 1 . t
E: . - - ; - . i l
,ts'i;-.f' u
f t t rs :; sls.ir--F', tr 9; .?, t.lt . -.;l -g
.n.".;-.E'r6'ft ?;t
..f .-1r-.F:el ; '?r t
F,.;i' ;1 9* .?: t
Red-Brown fine to coarse SAND. trace Silt
Groundwater at 4'4.Q
0.4 Macro Core 2'-4'
8.0
0.1 Macro Core 4 -6'
0 Macro Core 6'-8'
9.0-
10.0-
'1 1.0-
12.0-
End of Boring at 8'
Soil Description: and = 35-500/" some = 20-35% liftle = 10-200/" trace = l-10%
Driller: W. Lineberry
Big: Geoprone 540U
Depth to Water: 4'
Borinq Deoth: 8'
Borinq Dia.: 2"
gqg.l of 1
Page 104
!g9l9g[ Temporary M.8 Acceptance Facitity
Location; New Haven Rail yard
Client Maguire Group Inc.
Borinq: M8F-50
Insp€ctor: C. Criscuolo
@,3-1s-07
GEOPROBE SOIL BORING LOG
$eil Description: and = 35.500/" some = 20-35%
I
l of r i
Logical Environmental Solutions354 South River Road
Tolland, CT 06084fruck, Ponable & ATvlBackhoe-Mountoct ceoprcbes
r f 0 'o o
o
c
oDescription * a
o o o ao - . =
Sample Interval
Ground Surface 0.0
1 .0 -
2.0-
3.0-
J . U _
6.0-
7.O-
Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)
t . J
0 Macro Core 0 -2'
.:o l;- r,-.i
$,i.'*f .69ot ) t. s : . - : : - s :-F:"*r"..#f .6 9o . f , t, S : . - . ; : S :
.r.t'.r1,6 l ; .?, t
$,i"'}l, tr 9; .?, t
$',vo$'16 9n f: t
;";o'}f .6 9o .?, ta : . - : . $ :.f ::r**ff ,6 ?; 1?, ts : . : - : - s :
Red-Brown tine to coarse SAND, trace Silt & fine Gravel
Groundwater at 4'4.0
Macro Core 2 -4'
8.0
Macro Core 4 -6'
0 Macro Core 6'-8'
9.0-
10.0-
1 '1 .0 -
12 .0 -
End of Boring at 8'
Groundwater Grab Sample Collected
l i t t le = 10-20% trace =1-1070
Driller: W. Lineborry
8!gj Geoprone 540U
Deoth to Water: 4'
Borino Depth: I'
Borino Dia.: 2"
EAgg. 1 of 1
Page 105
elgiggl[ Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
glgllE Maguire Group Inc.
Borinq: M8F-51
lnsoector: C. Criscuolo
Date:3-15-07
t ^
i oU I
Loqical Environmental Solut ions354 South River Road
Tolland, CT 06084T I uc k, P o da b I e & A f VlB a c P,ho.- M ou n Ed G eo p rcbe s
c L oo o
o
E
.t>
Descriotion -oEo o o a
- o
Sample lnterval
Ground Surface 0 0r:ii''::i:ii:::i;i::q.:;:'. iji:o.:i
r:q:a:q:i:.::q:i
r:q:;:o.:i::.::q:;
Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)
1 . 50 Macro Core 0L2'
1;6 9; .l i
$,";.}' ,0 9; .2, t
F,";&:o-9e .?.!.i:j*lao.lu .'.!
e1J'51re lo 'l;t
,F,.;i1:6 9* .l: t
.e:1).ts1 '6?; l : t$,vo.}l . n9 f t : f : i. s : . : - l s
Red-Brown fine to coarse SAND. trace Silt & fine Gravel
Groundwater at 4'4,0
0 Macro Core 2L4'
8.0
0 Macro Core 4 -6'
0 Macro Core 6'-8'
9.0
10.0
1 1 .0
12.0
End of Boring at 8'
Soit Description: and = 35-50% some = 20-35o/o little = 10-20% trace = t'10%
Dri er: W. Llneberry
E!$. Geoprone 540U
Depth to water: 4'
Borinq Depth: 8'
Borina Dia.: 2"
eegg, 1 of I
Page 106
Proiect: Temporary M-8 Acceptance Facility Borinq: M8F-52
Location: New Haven Rail Yard Inspector: C. Criscuolo
Client: Maguire Group Inc. Date:3-26-07
I
i oLoqical Environmental Solutions
354 South River RoadTolland, CT 06084
Truck. Podable & AfvEackho*Mounted Geoyobes
-o to 6 )a g
ocU>
Description = :o ( | lo g
a EA =
Sample lnterval
Ground Surface 0.0
t . u -
2.0-
3.0-
4.0-
c .u-
6.0-
7.0-
:q: i :qr i : ; :q:
:". ; :'. :;: i :q. :i!:t,!14:i !:
:cf :{: i i :4,: " : i : r : i " :q l :
Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)
1 . 50
0
Macro Core 0'-2'
', tr ?; .1, t:
$"J$..Y:.Q;'ols:1;-*f' 6 f t . 1 1 ts. ' -- .$.f :1-".f1:6 9o .?; r
*f :";-.fl, tl ?o .?, t
$,";o$1:e 9; ' l : is : , : - s..f -L-.rt . - q . . t , ,' t
f l . 1 : rs : . : r t s :.P.".''r--.ff, tr 9o .1, t. S ;
- . : S :
Red-Brown fine to coarse SAND, trace Silt & fine Gravel
Groundwater at 4'4.0
Macro Core 2'-4'
8.0
0
0
Macro Core 4L6'
Macro Core 6'-8'
9.0-
10.0-
11 .0 -
12.0-
End of Boring at 8'
Soil Description: and = 35-500/" some = 20-35% Iiftle = 10-20olo trace - l-10%
Driller: W. Lineberry
8!q: Geoprone 540U
Depth to Water: 4'
EgEls_EcElh:8'
Borinq Dia.: 2"
Paqe: 1 of I
Page 107
elgigg! Temporary M-8 Acceptance Facility
Location: New Haven Rail Yard
9lgl! Maguire croup Inc.
g!49. M8F-53
Inspector: C. Criscuolo
Oate: 3-26-07
| -/l
i o\ t l
Loqical Environmental Solutions354 South River Road
Tolland, CT 06084Truck, Portable 4 AfvlBackhoe-Mounted Georobes
E 6{ r o
o
oDescription E : i
o oo =
o a Sample lnterval
Ground Surface 0.0
:9.:;_:F.:i.::j:o.
:L:i':.c:i -:.{
Brown fine to medium SAND, little Silt, trace fine to coarseGravel & Ash (FILL)
1 . 50 Macro Core 0'-2'
t . : d : . t ;I u . t t . 1 1s . : r s :
.F j:j".F
i r n l f t : ? . i
$+.}lr o.lft :?r t
Fe;i , o . ) . .I u._ft .1: 1
S"ri' ' u - f l . - as l . : l $ ..f :'.r"..fi - a . ) ,' t v f t . 1 : ts : . - : : - s :.f :j".Fljo li :?: r' E t . . - ! . S l
.r",.}.Fi , o l ; ' ? , t.s: . ' . - -s:
Red-Brown fine to coarse SAND, trace Silt & fine Gravel
Groundwater al 4'4.0
0 Macro Core 2'-4'
8.0
0 Macro Core 4'-6'
0 Macro Core 6'-8'
9.0-
10.0-
I L U -
12.0-
End of Boring at 8'
Soil D$criotion: and = 35-50o/o some = 20-35% little = 10-20% trace = l-10%
Driller: W. Lineberry
Ei$ ceoprone 540U
gsP![!@4'
Borinq Depth: 8'
Borinq Dia.: 2"
Paqe: 1 of I
Page 108
APPENDIX BTables from MGI's2005 Interim Shop
(Running Repair Shop)Task 210 Investigation
Page 109
MGI's 2005 Task 210 InYestigationTABLE 1(a) - Results of Geoprobe Boring Soil Sample Analyses
New Haven Rail Yrrd Interim ShopNew Htven, Conn€cticut
Boring LD.:
Sample Depth:
GPIS.3 GPIS4 GPIS-5
2' ,4 '
GPIS.6 CTDEP PMC GBGroundwaier
Area
CTDEP DEC ResidentiaVCommercial & lndustrial
CT ETPH - (ppm) t75 168 BRL 68.8 2.500 ppm 500/2.500 ppmVOCs - Method 8260 (ppm) BRL BRL BRL BRLBNs - Method 8270 (ppm)
Acenaphthene
Acenaphthylene
Anthmcene
Benzo(a)anthracene
Benzo(a)pyrene
B enzo(b) fluoranthene
Benzo(k)fluorantbene
Benzo(g,h,i)perylene
Dibenz(a,h)anthracene
Dibenzofuran
Chrysene
Fluoranthene
Fluorene
Indeno( 1,2,3-cd)plrene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Total BNs
BRL0 . 1 80.3460.6370.5 750 . 5 7 l0.5250.3650.672BRLBRLt.72BRL0.292o.212BRL0.952o.8't47.921
BRLBRLBRL0.4220.3970.5330_3610.2850.558BRLBRL0.786BRL0.2510.399BRL0.6770.6075.276
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL0.3 260.53L051.071.2 7
0 . 7 t 20,695BRLBRL1.132.85BRL0.6'12BRLBRLt.251.97
l3_525
84 ppm84 ppm
400 ppml ppmI Ppo'I pprnI ppm
42 ppmI ppm
5-6 ppmI ppm56 ppm56 ppmI ppm
9.8 ppm56 ppm40 ppm40 ppm
I,000/2,500 ppm1,000/2,500 ppmI,000/2,500 ppm
1/7.8 ppm
Ul ppm1/7.8 ppm
8.4/78 ppm1,000/2,5ffi ppm
l/l ppm270/2,500 ppm
84/780 ppm1,000i2,500 ppn1,000/2,500 ppm
1/7.8 ppm474/2,500 ppm
I,000/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm
Pesticides - Method 8081 (ppm) BRL BRL BRL BRLPCBs - Method 8082 (ppm) BRL BRL BRL BRL 0.005 ppm li l0 ppmHerbicides - Method 8l5l {ppm) BRL BRL BRL BRLTotal RCRA 8 l{etals ppm
Arsenlc
Bariurn
Cadmium
Chromium
Lead
Mercury
BRL25.81.029;12200BRL
BRL62.62.78 . 7 4tt2
BRL
BRL18.6BRLt t - l
8.5{iBRL
BRL
BRL) _ J O
62.3BRI
l0/10 ppm4,?00/140,000 ppm
34/1,000 ppm100/100 ppm
500i 1,000 ppm201610 ppm
SPLP RCIRA 8 Metals - ppmBariumLead
0.0248BRL
BRL0.0224
BRLBRL
BRLBRL
10.0 ppm0.15 ppm
BRL Below Reporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.
Page 110
MGI's 2005 Task 210 Inv€stigationTABLE l(b) - R€sults ofGeoprobe Boring Soil Sample Analy$es
New Haven Rail Yard Interim SbopNew Hav€I|, Conncciicut
Boring I.D.:
Sample Depth:
GPIS.7
4',-8'
GPIS-8
2 '4 '
GPIS.9 GPIS.I O CTDEP PMC GBGroundwaier
Area
CTDEP DEC ResidentiaVCommercial & Industrial
CT ETPH - (ppm) BRL 1,460 1 0 8 t 8 8 2.500 ppm 500i2,500 ppmVOCs - Method 8260 (ppm)
AcetoneTetrachloroethylcne
BRLBRL
0. t440.033
BRLBRI
BRLBRL
140 ppmI ppm
500/1,000 ppmt 2/1 10 ppm
BNs - Method 8270 (ppm)
Acenaphthe neAcenaphthyleneAntfuaceneBenzo(a)anthraceneBerzo(a)pyrcneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(g,h,i)peryleneDibenz(a,h)anthraceneDibenzofuranChryseneFluorantheneFluorenelndeno( 1,2,3 -cd)pyrene
2-MethytnaphthaleneNaphthalenePhe nanthrenePlreneTotal BNs
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRL
0.6940.6632.88s.034.1I4.673.212.6?0.53 |0.7884.461 8 . 5
0.5382.261 . 2 7| .07t0.'19.72
73."t t4
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL0.22BRLBRLBRLBRLBRL0 . 1 6 70.387
BRLBRLBRL0.3660.3660.4440.33o.272BRLBRL0.4440.736BRL0.244BRLBRL0.2920.5444.038
84 ppm84 ppm
400 ppmI ppmI ppmI ppmI ppm42 ppmI ppm
5.6 ppmI ppm56 ppm56 ppmI pp-
9.8 ppm56 ppm40 ppm40 ppm
1,000/2,500 ppm1,000/2,500 ppm1,000i2,500 ppm
1/7.8 ppmUl ppm
l/7.8 ppm8.4/78 ppm
I,000/2,500 ppml/1 ppm
270/2,50O ppm84/780 ppm
I,000/?,500 ppm1,000/2,500 ppm
l/7.8 ppm414/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm1,000i2,500 ppm
Pesticides - Method 8081 (ppm) BRL BRT, BRL BRLPCBs - Method 8082 (ppm)
PCB-1260 BRL 0.0465 BRL 0.0566 0.005 ppm 1/10 ppmHerbicides - Method 8l5l (ppm) BRL BRL BRL BRLTotal RCRA 8 Metals - ppm
ArsenrcBariumCadmiumChromiumLeadMercury
BRL1 3 . 9BRL4.863.96BRI
7 . t lt022.623 1 . 0280l . 5 l
BRLl1.6BRL38.914.2BRL
BRLt9.'r0.5349.343. tiBRL
l0/10 ppm4,700/140,000 ppm
34/1,000 ppm100/100 ppm
500/1,000 ppm20/610 ppm
SPLP RCRA 8 Metals - ppmBariumChromiumLead
BRLBRLBRL
0.0726BRLBRL
BRL0.0 r06BRL
BRL0.0090.0078
10.0 ppm0.5 ppm0.15 ppm
BRL Below Reporting Limits (see laboratory reports for compound specific detectian limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific detection limits.
Page 111
NIGI's 2005 Task 210 InvestigationTABLE 1(c) - Results of G€oprobe Boring Soil Sample Analyses
New Haven Rail Yard Interim ShopNew Haven, Connecticut
Boring I.D.:
Sample Depth:
GPIS-I 1
2 ' -4 '
GPIS.12
2'4',
GPIS. I3
4 ' -8 '
GPIS.15
7',4',
CTDEP PMC GBGroundwater
Area
CTDEP DEC ResidentiaVCommercial & Industrial
CT ETPH - (ppm) 1,120 r,670 1,070 330 2,500 ppm 500/2,500 ppmvocs - Method 8260 (ppm)
Acetone
Tetnchloroethylene0 .1260.0376
BRL0.0143
BRL
BRL
tsRLBRL
140 ppmI pPm
500/l,000 ppml2i I l0 ppm
BNs - Method 8270 (ppm)
Acenaphthylene
Anthmcen€
Benzo(a)anthracene
Ben2o{a)p}rene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylenc
Chryscne
Dibenz(a,h)antkacene
Fluoranthenc
2-Methylnaphthalene
Naphthalene
Phenanthrenc
Pl,rene
Total BNs
0.3 9BRL0_359BRT-0.394BRLBRL0.541BRL0.6431.05
0.8790 . 8 1 20.4645.532
BRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLtsRLBRLBRLBRLBRLBRLo.542BRL0.4910.97',7BRL0.8
0_4521.262
0.920.8572.2
t . / J
1.470 . 3 1 9
6.991.290.33) L 1
4.4829.866
84 ppm
400 ppmI ppmI ppm
I ppmI ppm
47 ppmI ppmI ppm
56 ppm9.8 ppm56 ppm40 ppm40 ppm
1,000/2,500 ppm1,000/2,500 ppm
l/7.8 ppml/l ppm
l / 7 R n n m
8.4i78 ppm1,000/2,500 ppm
84/780 ppm
l/l ppm1,000/2,500 ppm47412,500 ppm1,000/2,500 ppm1,000/2,500 ppmI,000/2,500 ppm
Pesticides - Method 8081 (ppm) BRL BRL BRL BRLPCBs - Method 808? (ppm)
PCB-1260 1.21 BRL BRL 0.005 ppm 1/10 ppmHerbicides - Method 8 t5l (pprn) BRL BRL BRL BRLTotal RCRA 8 Metals - ppm
Ars€nlcBariumCadmiumChromiumLeadMercury
BRL1722 . 3
21 .02581.03
BRL52.2
0.8029.0349.1BRL
8.8 880.10.75845.lJ3542.32
BRL64.3l . t 46.7 |t36
0.295
l0/10 ppm4,700/140,000 ppm
34/1,000 ppm100/100 ppm
500/l,000 ppm201610 ppm
SPLP RCRA 8 Metals - ppmBariumChromiumLead
0 . t l 9BRLBRL
0.0234BRI,BRL
0.0160.007t0.026
0.019BRLBRL
10.0 ppm0.5 ppm0.15 ppm
BRL - Below Reporting Limits (see laboratory reports for compound specific detection limits)
The compounds listed above are those that were detected - please see laboratory reports for full lists ofcompounds and their specific dctection limits.
Page 112
MGI's 2005 Task 210 Investigation'IABLE l(d) - Rcsults ofGeoprobe Boring Soil Sample Analyses
Nerv Haven Rail Yard Interim ShopNew IIaven, Connectlcut
Boring LD.:
Sample Depth:
GPIS-18 CTDEP PMC GBGroundwater
Area
CTDEP DEC ResidentiaYCommercial & Industrial
CT ETPH - (ppm) 2,500 ppm 500/2,500 ppmVOCs - Method 8260 (ppm)
Tetrachloroethylene 0.0367 t ppm l2l I l0 ppmBNs - Method 8270 (ppm)
AcenaphthencAcenaphthyleneAnthraccncBenzo(a)anthraceneBenzo(a)pyreneBeuo(b)fluorantheneBenzo(k)fluorantheneBe nzo(g,h,i)peryleneDibenz(a,h)anthraceneDibenzofuranChryseneFluorantheneFluorenelndeno( 1,2.3-cd)pyrene2-MethylnaphthaleneNaphthalenePhenanthrcnePlreneTotal BNs
0.3 392.412.536.3 36.165.764.923.49
0.9820.8466.061 6 . 8| _021.140.737t.0'79.1 '7t 0 .6
82.164
84 ppm84 ppm
400 ppmI ppmI ppml ppmI ppm
4? ppmI PP-
5.6 ppmI ppm56 ppm56 ppmI ppm
9.8 ppm56 ppm40 ppm40 ppm
1,000/2,500 ppmI,000/2,500 ppm1,000/2,500 ppm
l/7.8 ppml/l ppm
1/7.ti ppmIt.4/7li ppm
I,000/2,500 ppml/l ppm
27012,5O0 ppm84/780 ppm
1,000/2,500 ppm1,000/2,500 ppm
l/7.1t ppm47412,500 ppm1,000/2,500 ppm1,000/2,500 ppm1,000/2,500 ppm
Pesticides - Method 8081 (ppm) BRLPCBs Method 8082 (ppm) BRI 0.005 ppm l/10 ppmHerbicides - Method li l 5 ! (ppm) BRL
Toral RCR{ 8 Metals - ppmAIsenlcBariumCadmiumChromiumLeadMercury
10.61 7 8
34.41,3400.949
l0ll0 ppm4,700/140,000 ppm
34/1,000 ppm100/100 ppm
500/1,000 ppm201610 ppm
SPLP RCRA 8 Mctals - ppmBariumChromium[,ead
0.04160,01
0.0785
10.0 ppm0.5 ppm0.15 ppm
BRL Below Reporting Limits (see laboratory r€ports for compound specihc detection limits)
The compounds listed above are those that were detected - please s€e laboratory reports for full lists ofcomoounds and their soecihc detection limits.
Page 113
TASK 210:SUBSURFACE SITE INVESTIGATION
New Haven Rail YardTemporary M-8 Acceptance Facility
New Haven, Connecticut
Volume 2
ConnDOT Assignment No. 202-3464ConnDOT Project No. 301-88
Prepared for:
@State of ConnecticutDepartment of TransportationNewington, Connecticut 06131
Prepared by:
IilRiliEGnouf
Maguire Group Inc.One Court StreetNew Britain. Connecticut 06051
April24,2OO7
Page 114
APPENDIX CSoil Sample
Laboratory Reports
Page 115
Report Date:2'7 -Mar0'l t1 :35
Logical Environmental Solutions354 South River RoadTolland, CT 06084Attnr Cindy Knight
SPECIRUM ANALYTICAL, INC.f.atarihg
HANIBAL TECHNOLOGY
Laboratory Report
gtrE
Final ReportRe-Issued ReponRevised Report
Project: NHRY M8 Acceptance Facility - New Havel, CT
Project 301-88
Lrboratorv lDsAs9464-01sA59464-02sA59464-03sA59464-04sA594&-05sA594g-06sA594g-07sA5946t-08sA594A-09sA5944r0s45946+l ISA59,16.f-12SA59.164- I lSA59,l&l-14sA594fl- l5SA5946.1-16sA59,r64- t7SA59,164-18SA59,l6,l- I9
Client Sample IDM8F-4 2'-4,M8F-5 2'-4,M8F-6 2',-4'M8F-12 2,4'M8F-11 2,4'M8F-49 2'-1'M8f-50 2'4'M8f-5I 2'4'M8FB.1MSFB-2MTFB-3MSFB-1M8FB-5M8FB-6MSFT-IMSFT-2FB-ITB-IM8F-50CW
Matdx
SoilSoilSoi lSoi lSoilSoilSoilSoi l
BallastBallastBallastBallastBallastBallastWoodWood
Blank WaterBlank Water
Ground Water
Date Ssmpledl5-Mar-07 0D:00l5-Mar-07 00r00| 5-Mar-07 00r00l5-Mar-07 00:00l5-Mar-07 00:00l5-Mar-07 t)0:00l5-Mar-07 00r00l5-Mar-07 00r00l5-Mar-07 00:00l5-Mar-07 00r00l5-Mar-0r 00r0015-Mar-07 00r0015-Mar-07 00:00l5-Mar-07 00:00l5-Mar-07 00:0015-Mar{7 00r0015-Mar-07 00r00l5-Mar-07 00:0015-Mar-07 00:00
Drte R€celv€d
l9-Mar-07 l-5;33l9-Mar-07 15:3319-Mar-07 l5:3319-Mar-07 lJ;3319-Mar-07 l5:1319-Mar-07 l5:33l9-Mar-07 l5:33l9-Mar-07 l5:ll19-Mar-07 15:3319-Mar-07 l5:13l9-Mar-07 15:33l9-Mar-07 15:33l9-Mar-07 l5:33l9-Mar-07 15:3319 Mar-07 15:33l9-Mar-07 15:33l9-Mar-07 15:31l9-Mar-07 15:33l9-Mar-07 15:31
Headgud e^: 11 Almgen[)live & E10 Silv€r Str€€1. Aga\esm, MA 0100t . t-800-?89-91l5.4lt-789-90lE. FAX 4t3-.t9-40j6fl, Divnidz:8180 Wedland Cstq Bouldard. TatIpd, FL 33614. l-E8E49?,52?0. Elt EEt,9io7. FIX 800-4t0 643i
www-spectrum.analylical.com Pag€ I of 152
Page 116
I atest f|at the ilfo.rnatioD contaioed within the report bas been reviewed for accuracy and checked ogaitrst the quality conholrequirements for each merhod. Thes€ results rclale only to thc sample(s) as rcceivedAll applicable NELAC .equirements have beetr m€LPleas€ oote that this nepoft contalns 152 pages of analytical data plus ChaiD of Custody documen(s).This repon may not be reproduced, except in full, withour written approval from SpecFum Analytical, Inc-
Massachus€tts Certifi cition #Coorccticut # PH4777Flo'ida # E8'76(Jf,n87 936MriDe # MA138New Hampshire # 2538/2972New Jersey # MAol I A{A012New York # 11393/11840Rio& tsland # 98usDA # s-51435VerEotrt # VT-l l39l
M-MAt38MAt I l0 Authorized by:
nfrd-Hanibal C. Tayeh, Ph.D.President/l^aboratory Director
Technical Reviewels Initial:
Spectrnn Analyticdl, Inc. it o NELAC accredited laboralory or4anization and meets NELIC tellting sr.rndflrb. Use of the NELIICloSo howewr does not ittsure that Spe.lrum rs cunently accrcdiledfor the sryilc method or anal@ indicated. PteaEe refer lo our"QualiE web page at www.spectrnmaralytical.confor alu tisting ofour current ceftirtca ons andJields ofat:creditation. Statet inwhich Spechm Anolytical, Inc. holds NELAC cerlifrcation are New york, New Hampshire, New Jersqt and Floida. Alt anatytiea!worklol Yoldlile Orgdnic and Air analysis ue lrarsfefted lo and con&rcted at our 830 Silver Srreet tocation NH-2g72. Ny-l1840.FL-E879 3 6 and NJ - MA1 I 2).
ThB ,abonatry Epor, is aot polful ui aal ad azrtodzd stg.raatre o" thz coter psse.
. Reportiblc Dsr.ction Limit BRL = Below R€pniing Linit Ptg.2of 152
Page 117
Report Date:28-Mar-07 09;55
Logical Environmertal Solutions354 South River RoadTolland, CT 06084Attn: Cindy Knight
SPECTRUM ANALYTICAT-, INC.Fedta,ing
HANIBAL TECHNOLOGY
Laboratory Report
gtrtr
Final ReportRe-Issued ReportRevised Repon
Project: NHRY M8 Acceptance Faciliry - New Haven, CT
Project 301-88
nfrd-Hatribal C. Tayeh, Ph.D.President'I-aboratory Director
Technical Revieweis ILritial:
Speclntm Analyti.al, Ihc. ts a NELAC accredited laboralory organizalion and meets NELAC testing standards- Use ofthe NELAClogo however does not itlsLtre that Spec!rum is currently accreditedfor lhe speclic metlnd or anab,te indicated. pleare rcfer lo our"Qualily" web page at www.spectrun-analytical.comfor afull tisting ofour curren! certifcalionr andfielde oJaccreditatioa. Sl.lres inwhich Spectrum Analyticul, Inc. holds NEL4C certificalion are New Yorh New Hampshire, New Jersey and Florida. All analyticalworklor folatile Otgarlic and Air analysis are trunslefied to ond conducted at our 830 Silvel Strcet location NH-2g72. Ny-l1E40.FL-887936 and NJ-M40 I 2).
Laboratorv ID Client Sample IDsA595t7-01 M8F_124 'sA595l7-02 M8F_2 24'sA595r7-01 M8F-3 24'sA595l7-04 M8F-14 2_4sA595l?-05 M8F-15 +6'sA595l?-06 M8F_26 2-4'sA595r?-07 M8F-12 2-4'sA595t?-08 M8F-40 2_4'sA595l7-09 M8F-41 4_6'sA595l7-t0 M8F-45 4_6'sA595t?-l I M8F46 2_4'sA595 | 7- t2 M8F47 24'sA595l7-ll M8F-14 cWsA595 t 7- l4 FB-2sA595 t?- l5 TB_2
Matrix
SoilSoilSoilSoilSoil
Soi lSoi lSoilSoi lSoi lSoi lSoil
Grouod WaterBlank WaterBlank Water
Date Sampledl9-Mar-07 00:00l9-Mar-07 00:00l9-Mar-07 00:00l9-Mar-07 00:00I9-Mar-0? 00:00l9-Mar-07 00-00t9-Mar-0? 00:00l9-Mar-07 00:00l9-Mar-07 00:00l9-Mar-07 00:00t9-Mar-07 00i00l9-Mar-07 00:00I 9-Mar-07 00:00l9-Mar-0? 00:0019-Mar-0? 00:00
Date Received
20-Mar-O'7 14:4820-M^r-0'l 14:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4;4E20-Mar-07 l4:4820-Mar-07 14:4820-Mar-07 l4:4820-Mar-07 14:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 l4:4820-Mar-07 14:48
I atlest that thc information contaiDcd within the repon has b€en rcviewed fo. accuracy and checked against the quality co rolrequirements for each method- These results relate only to the sampl€(s) as received.All applicable NELAC .equirements have be€n met.Please Dote that this reporr contains 124 pages ofanalytical data prus chain ofcustody document(s).This repon may not be reproduced, except in full, without witten approval from Sp€ctrum Anallrical, Ioc.
Massachusetts Certification # M-MAl3BA{Al I l0 Authoriz€d by:Comecticut # PH-0?77Florida # 8E7600/E8?936Maine # MA 13 8New t{ampshire # 2538/2972New Jersey # MA0l lMAol2New York # I l39l l 1t840Rhode Island # 98usDA # s-51435Vermont # VT-l1393
fltur'q@t4tst ll Alng.€t Drivc & 810 Silv€.Sr@r . Agaearq MA0t00t . l-S0O-789-91t5 .4lj-789-90It . FAX 4Lj ?89 40?brZ Ddridr: E lE0 Woodland Cent€r Boulward . Tamp4 FL 31614 . l-888-497-52t0. 813-888-9507 . FAli E00-4E0 6435
wv,w'3 pectaum-analytical-com Page I of 124
Page 118
Report Date:29-Mar-07 16:45
Logical Envitonmental Solutions354 South River RoadTolland, CT 06084Attr: Cindy Knight
SPECTRUM ANALYTICAL, INC.F.at!.ing
HANIBAL TECHNOLOGY
Laboralory Report
gutr
Final ReportRe-Issuql ReportRevised R€port
Project: NHRY M8 Acceptance Facility - New Haven, CT
Project 301-88
Laboratorv lDsA5964l-0tsA5964l-02sA5964l-01sAs964l -04sA5964l-0ssA5964r-06sA5964l-07sA5964l-08sA5964l-09sA5964l-10sA5964l-11sA5964l- r2sA5964r-tlsA5964t-t4sA5964 t -15sA5964l- t6sA59d,!l-17sA5964l-18sA5964t-19
Cli€pt Semple (D
M8F-16 2,-4'M8F-17 4'-6,MEF-lE 2,-4,M8F-19 2,4'M8F-20 2'-4'M8F-22 2,4'M8F-23 2,4,MEF-24 2,4,M8F-25 2'4'M8F-27 2'-4,M8F-28 2,-4,M8F-29 2'4'M8F-10 2'-4'M8F-3 t 2'-4'M8F-31 2'-4'M8F-34 4-6'M8F-24 CWFB-:}TB-]
Mrtrix
SoilSoilSoilSoilSoilSoilSoi lSoilSoilSoilSoilSoilSoil
SoilSoi lSoil
Cround WaterBlank WatetBlank Water
Oate Sampled2l-Mar-07 00:002l-Mar-07 00:002l-Mar-07 00-002l-Mar-07 00:002l-Mar-07 00:0021-Mar-{7 00:0021-Mar-07 00:0021-Mar-07 00:002l-Mar-07 00:002l-Mar-07 00:0021-Mar-07 00:002l-Mar-o? 00:0021-Mar-0? 00-0021-Mar-07 00:002l-Mar-0? 00:002l-Mar-07 00:002l-Mar-07 00:002l-Mar{7 00:0021 Mar-07 00:00
DrJc ReceiY(d
22-Mar-07 l5:3 5
22-Mar-07 15i35
22-Mar-07 15r3522-Mar-07 I513522-Mar-07 15r3522-Mar-07 15r3522-Mar01 15135
22-Mar-07 l5:35
22-Mar-07 l5:3522-Mar-07 15r35
22-MaF07 l5:3 5
22-MaF07 l5:35
22-MaF07 15i35
22-MaF07 15i35
22-M^t-07 1513522-Mar-07 15r3522-Ma(07 l5:i522-Mar 07 15:3522-Mar-07 | 5135
Ha.kluutn: tr AlnB.enDrive & 8J0 Silver SrMt. Agawsfl. MA 01001 . I-8On ?E9,91l5 .4ll-789-90tE. FAX 413-789,,1076F, Drysio,:8180 WoodLand Center Borlevard . Tamm" FL136l4. L,EEE 497-5270 .613-888-9507 . FAx Eoo 480-6435
www.EF€ctrumnnalttletl.comPage I of 165
Page 119
I attest that the information contained within the report ha' beetr rcviewed for accumcy and checked against the quality colltrolrcquircmeots for each method These r€sults .elate only to the sampl{s) as received,Atl applicable NELAC rcquiremeDts hare been met.Please note tlMt this reporr contaios 165 pages ofana.lytical data plus Chain of Custody documen(s)-This .eport may oot be reproduced, except in full, witho r+Titteo app.oval from Spectrum Anal)4ical, Inc.
Massacbusetts Certificarion # M-MAI38MAI I l0 Aurhorized by:Connectiout # PH-0777Florida # E87600/E87936Maine # MAl38New Hampshire # 2518/2972New Jersey # MAol lMAol2New York # I 1393/ 1 1840Riode Islaod # 98usDA # s-51435Vermodt # VT-I1393
nfrd-HaDibal C. Tayeh, Ph-D.
Presideff/Ilboralory Dir€cior
Technical Revi€wels Initial: .eSIEctn/m Analtlical, Inc. is a NELAC arcrediled laboralory organizatiok and meett NELAIC testing staruh t. IJse of the NELAClogo however daas ̂ ot irLsure thal Epectrufi is canently accredited for the spectlrc method or aaalye indicated- Pleose rckr to our"Sualit!' web page al ww'w.specttlrm-qnallti4al.comlor afull listing ofour cutenl certifications andftelds of@credilarion. States inrihich Spectrum Analytical, Inc. holds NELAC certification are NeN, york New Eampshirc, New Jersey and Florida. Alt anolyticalworkfor Volatile Organic and Ail analysis are trarrilerred to and cohducled at our 830 Sifuer S|eet location (NH-2972, NY-t 1840,FL-E87 9 j6 and NJ- MA| I 2).
Thk loboftlory Eport b ,rot talU withotd aE aslhotigll sigaoure ot, the cove'. pag..
' R€pottabl€ f,)etectioo Limi. BRL = Below R€portine Limit Page 2 of 165
Page 120
Report Date:04-Apr-07 13:06
Logical Environmenhl Solutions354 South River RoadTotland, CT 06084Attnr Cindy Knight
SPECTR(IM ANALYTICAL, INC.Fealu,ilg
HANIBAL TECHNOLOCY
Laboratory Report
gtrtr
Fin:rl ReporiRe-lssued ReportRevised Rcport
Project NHRY M8 Acceptance Facility - New Ilaven, QT
Project 301-88
Laboratorv lDsAs980l-01s459803-02sA59803-03sA59803-04sA59803-05sA59803-06sA59803-07sA59803-08sA5980l-09sA5980l-10sA5980l-l IsA59803-t2sA59803-tlsA59803-14sA59803- l5s459803- t6sA59803-17sA59803-t8s459803-t9sA59803-20
Client Srmple lDM8F-7 2,-4'M8F-8 2'4'M8F-9 2'-4'M8F-10 2'-4'M8F-l t 2'-4,M8F-21 2'-4'MEF-35 2,-4'MEF-36 4,-6,M8F-37 2,4,M8F-38 2,-4'|\f8F-J9 2-4,M8F42 2'4'M8F-43 2,-4'M8F-44 2,4,M8F48 2,-4,M8F-52 2,-4,M8F-53 2,-4,M8F-.{2 cwFB-4TB4
Metrix
SoilSoilSoilSoi lSoiLSoilSoiLSoiLSoilSoilSoilSoilSoiISoi lSoi lSoi lSoi l
Groutrd WaterBlank WaterBlank Water
Date Sampl€d26-Mar-07 00:0)?6-Mar-07 00:0t)26-Mar-07 00:0026-Mar-0? 00:l}l26-Mar-0? 00:0026-Mar-07 00:0026-h{ar-07 00:0026-Mar{7 00:0026-Mar-07 00:0026-Mar-07 00i0026-N4ar-0? 00:0026-Mar-07 00:0026-Ma.-07 00:002GMar-07 00:0026-Mar-07 00:0026-Mar-07 00:0026-Mar-0? 00:0026 Mar-07 00:0026 Mar-07 00:0026-Mar-0? 00:00
Date Received
27-Mar-07 l2:502'1 -M^r-O1 12-502'1 -M^t-O'7 12:5027 -Mar-O7 12:5027-M^t-07 12.502'1-Mar-07 12.5027 -M^t-07 12.502'l -M^t-07 12.502'l-Mar-l1 12:50
2'l-Mar-I1 12:502?-Mar-07 12:5027-Mar-07 1?:502'7-Mat17 l):502'7 -Mar-07 12:502?-Mar-07 l2:50
2?-Mar-07 l2:5027-Mar-07 l?:502?-Mar-07 l?:5027-Mar-07 l?:5027-Mar-07 I2:50
HaadquaFte.s: ll Alngrcn Dtirc & Elo silvdsf.€et. Agavam, MA 01001 , I,Eoo-7E9 9l 15,4ll-789-9018 . FA-Y 4t]-78940?6F, Divjsid': 8180 Wmdl t Ccnre. Boulevard . Tanpa, FL 316 t 4 . t -E8B-497,5?70 . E ll-E88-9jo? . FAX 800-480{415
www.spectaum-analytical.comPage I of 154
Page 121
I attest that tbe itrformation cortiined within the repoft has been reviewed for accuracy aDd checked against the quality controlrequirements for each method. Thes€ results relate only to tte sam!,le(s) as receivd.All applicable NELAC requiremenas have beetr met_Please Dote that this report cofltains 154 pages ofsDalyticnl data plus Chain ofcustody documeEt(s)-This repon may not be reFoduce4 except in full, witbout writtei approval from Speotrum Analytical, ltrc.
Massachusetts Certiftca.ion # M-MAllt/MAl I t0 Authorized by:Couecticut # PH4777Ilorida # E87600iE87936Maine # MAl38New Hampshire # 2538/29?2New J€rs€y # MAol l/MAol2New York # I t39l/t 1840Rhode lsland # 98usDA # s-51415V€rmont # VT-l1393 &
-ffi a^d-Hanibal C. Tay€h, Ph.D,PresideEt/Laboratory Direator
Technical Reviewedr ltritiali
speclrum Analytical, Inc- Lg a NELAC rrccredited laboratory organi rtion and meers NELAC tesling standards. IJse ofthe NELACIogo however daes not insurc lhat Spectrum is cuftehtly occrelited for lhe specific method or otallte indicdeA. Please eJer to our"Quality" web page at www.spechlm-atu ylical.con Jor alutl listing of otr cunent certilcatione atd felds oJ aecredianion. Sta/€s inwhich SPeartufi Analytical Inc. holds NELIC certijcation are New York, Nei' Hampshirc, New Jersqt and Florida. All analyticalu,orkfor Volatile Organic and Air dnalysis are translened lo and coflducted at our 830 Silver S\eet locarion (NH-2972, Ny-|1840,FI- 88 79 3 6 a nd NJ- MA0 l 2 ) -
Ihb lsbordaA ryort b not eaM l,|a6otd tn a4tlur.iael siptntre on ,hc caver pge.
' RQortable Detection Limit BRL = Belo* Reponing Limil Pag€ 2 of 154
Page 122
Sample IdenrificationMtF-l 2-4'
sA59517 0 l
Client Proiect #301 -88
Collection Date/Timel9-Mar-07 00:00
MatrixSoil
Received20-Mar-07
CAS No. Anslyte(s) Flag Ania 'RDL Dilu.ion Method R4 PEparcd A aryzed Borch Analptvolalil€ Org.nic Colhpornds
VOC Exkaclion Field extracted
PS/kS dry 6 5
PS/kg dry 130
!s/kg dry 6-5
PStkSdry 6-5
!S/ko dry 6-5
Pg/kg dry 6 5
LIVkS dry 6.5
!s/ks dry 6.5
lSftS dry 13 0
Ugks dry 6{ 8
lrdkgdry 6.5
Ug/kg dry 6.5
Pg/kg dry 6.5
Pg/kg dry 32.4
ldkq dry 6.5
rc/tS dry 6_5
Ugkq dry 13.0u€/kS dry 6 5
ldkS dry 13.0
ug/kS dry 6.5
US/kg dry 6.5ps/rg dry 13.0
udkS dry 6.5p94q dry 6.5
IjSAS dry 6.5pdkS dry 6 5pdkg dry 6.5
!S/kS dry 6.5
!S/kS dry 13 0
!g/kg dry 6 5
LiS/kg dry 6.5
!S/kg dry 6-5
!g/kg dry 6.5
Pdkg dry 6.5
l./sfts dry 6.5
US/kg dry 6.5
Pgks dry 6.5pg/kg dry 6.5
!g/kg dry 6.5
t4fts dry 6.5
t'g/kq dry 6.5
t'dks dry 6 5
ttSilq dry 64.8
t S/kS dry 6.5
ldkS dry 65
lsl(gdry 6.5pgkS dry 64.8
UdkS d.y 64.6
Isfts dry 6.5
21'[r€r07 21-ft4ar 07 7031261 BDVolatile Ofoanic Compounds
P.epared by method SW846 5035A Soit (tow tevet)
76-13-1 1,1,2-Tdchtorohfluoroethane(FreoBRL67'64-1 '@tone BRL107,13-1 Acrylon(rile BRL714-2 Benzene BRL108{€-1 Bromobenzene BRL74-97-s Bromochlommethane BRL15-214 Bromodichtoromelhane BRLT5-2+2 Bromolorm BRL74-€39 Bromomethane BRL78-sg3 2-Butanone (MEK) BRL1o4-5J+ n-Eutylb€rEene 8RL135-98{ sec-Eutylbenz€ne SRL98{c6 ten-Butylbenzene BRL75-15-0 Carbon disllfide BRL56'23-5 Carbon teEachtoride BRL108-90-7 Chtorobenzene BRL75-00.3 Chtoroethane BRL6766-3 Chlototo'm BRLf4 a7-3 Chtoromethane BRL95-49-8 2.Chtorototuene gF.L
106-43-4 4-Chloroto{uene BRt96-12{ 1,2-Dibromo-3-chloropropane BRL124-48-1 Oabomochloromethane BRL10c434 1,2-Dibromoet ane (EDB) BRL74-9t3 Dibrornomethane ARL95,50,1 l,2-DichlorobeMen€ BRL5)41,73 r I,3-Dichtorobenzene BRL106-46-7 l,4-Dichtol.obenzene BRL7s'71-8 Dicilorodifluoromethan€(Freon12)BRL7s 3'l-3 1,l-Dichtoroethane 8RL107{6-2 l,2-Oichloroedune BRL75-3F4 l.l.Dichloroethene BRL15€-5€-2 cjs-1,2-Dichtoroethene BRL1ffi-s trans-1.2-Dichtoroethene BRL7Bi7-5 1.2-Dichloroprcpane BRL142-28-9 1,3-Dichtorcprop€ne gRL
594-20-7 z,2.Dichtomprcp€ne BRL4,6+s8{ 1,l-DichtorcprcPene BRL10061{1.5 cis-1,3-0icthlorcpropene BRL10061-02€tans-l,lDicthloropropene BRL100-a1-a Etht'lbenzene BRL87{0-3 ller€chloobutadiene BRL5s1-78{ 2-t-lexanone (MBK) BRL98424 lsopropylbenzene BRL9947,6 +lsopropyttoluene BRL1634-04-1 Methyl tsd-butyl ethe. BRL10e-r0-l 4-Mehyl-2-pentanone(M|BK) BRL75-09-2 Methylene chtoride BRL
SW84662604 2z-Marlt 22'Ma(47 7031335 RU1
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191'2G3 Naphthabne
Pa€e 2 of 124
Thh tabonlory rcpon k not wlid st hoa an aathod?rd signrrlre o.t the coser page.
t R€portable D€tection Limit BRL = Belo* Reporting Limir
Page 123
SamDle ldenril_rcationM8F,l 2-4'sA595l7-01
Client Pmiecr #301 -88
Collection Date,'fimel9-Mar{? 00:00
MahixSoil
Received20-Mar-0?
CnS No- A,'aryte(s) FloS Unirl *RDL Dilutioa L{ethod ReI. Prcparcd Antryzcd Bakh Anebst
103-65-1 n_Propylbenzene10G:t2-5 Styrcne63S20$ |,.1,|,2-Tetachloroelhane7934'5 t, 1 ,2,2-Tetrachloroethane12718-1 TekachloDethene10844-3 Toluene87{1$ 1,2,}Trichlorobenaener20,e2-1 1,2,4-Tdchlorobenzene7155$ t,1 , t -Trichtoroethane
7940r I ,1 ,2-TrichtoroetMne79{1€ Trichloroelhene
lblstile Orgrnic Compounds
Volalile Oroanic Comoound!Pfepared by me{hod SW846 5035A Soit (tow tevet)
BRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRL
75494 Trichtorofluoromethane (Freon '11) BRLs6-18-4 i,2,3-lrichtoropropane BRL9543-6 1,2.+T methylbgnzene BRL10867i 1,3,5-Trimethytbenrene BRL7s{1-4 Vinylchtoride BRL1330-2+7 m,p-xylene BRL95-475 o_Xylene BRL10*9{r-9 Tetrahydrofuran BRL60-2*/ EthyrerfEr BRL99+05+ Tert-amyl methylether BRL637-92,r Ethy,t ted_butyl eher BRL1oe2o 3 Di_isoptopyt ether BRL7545,0 Tert_Butanot/ butyt atcohol BRL123-91J t,4-Dioxane BRL
Sumgate rccov€neE:460401 4-Bromofluorcbenzene
2@7-2eS Toluene4g
1 706407 o 1, z-Dichlorcethane 44
1A6A-53-7 Abrcmofluorcmelhane
Extmctrble Pearolesm Hydftrcrrhons
Extractable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
8006$1,9 Gasoline6847+3G2 FuetOit#26847G31-3 Fuet Oit #468s53{O-4 Fu€t Oit #6M09800r)00 Motof oilJ00100000 Aviation Fuel
Unidentified
Other Oil
Tolal Peboleum Hydrocarbons
Cg-C36 Aliphatic Hydrocarbons
Sutogate recovdies:3ieG$-2 1-Chlorooctadecane
S€mivohtile Orgalic Compoundr by CC
Orqanochlorine Pesticides SW846 8081A
Prepared by method SW846 35508
3090l)!2 Atddn
Lig/kg dry
udks drypdts dryLig/kg dry
!S/kS dry
ldks dry
!S/kS dry
!gl(g dry
usnlg dry
ldkS dry
|lg/ks dry
pg/kS dry
usftg drypstkg drypS/kg dry
lEkg dry
!s/ks dry
ug/kg drypdks dry
lgr(s dry
ldl€ dry
PdkS dry
!s&s dry
UdkS drypSllg dry
6.5
6_5
6.5
6.5
6-5
6_5
6.5
6.5
6.5
6.5
6 5
6-5
13.0
6.5
64.8
6-5
6_5
6.5
6.5
6 4 8
r30
SW 846 82608 22-Ma.47 224,AarO7 7031335 RU
+CTETPH 22-Mat47 234 a147 7031281 DS
99106107105
BRLBRLBRLBRLC€lqrlated asBRL159BRL153159
7G130%
7G130 %
70-130 %
70-130%
.t€/kg drytrE/kg drynq/kg drymg/kg drymdkg drymg/kg drynvkg dryrngkg drym9k9 drym€/kg dry
2632432 6 32A.328.324.328.328.328.328.3
40-140 %
!S/tg dty SW846 8081A 22.Mar{7 26.tlar{7 7031275 TG
Thir loboralo|! Epatt is not vaIU withotr.n au^oriud siga,,ture on tha dtrer pnge
' Reportable Detection Limit BRL = Below Reponing Limit Page 3 of 124
Page 124
Samole ldeotificationM8F-l 2-41sA595l7-01
Cli€nt P.oiect #301-88
MatrrxSoil
Received20-Mar-07
Cotlcction Date/TimeI +Mar-07 00:00
CAS No, Ahtlrt (s) FI"C 'RDL Dilutloa Method netr Prcparcd Adalwi Balrh Ad4bst
Semivoladle O.grtric Compouods by CCOmanochlodne Pesticides SW846 8081Aftepared by mehod SW846 355083i9{4{ a€HC319-85-7 b-Bt{c319€€.€ d€Hc58-8+9 g-BHC (Undane)57-7+9 Cl orden€72.54-s 4,4-DDD (p,C)72-s5.s a,+ODE G,p.)so-2e-3 4,4-DDT (p,p')60-57-r Di€ldrin95$9E{ Endoculfan I$21345-9 Endo$lfan llr03i{7-8 EidosulfanSullaten-2oi End.in7421-93-4 Endrin AJdehydeIG-44{ H,sptachlotf24Ts Melhoxychlor1024-57-3 H€placHor Epoxjd€ ..8001-3t2 Toxapfi€nesi03.71-9 a-Chlodane5s66.3+7 g.chlodene539470.5 Erukin Ketone
Su7Dgate rccoveies:1038& z l,QBndaiuorobiphenyl (Sr)ms1-2a7 Docechtotobiphenyt (Sr)Polvchlodnated Biohsnvb bv SW846 BOB2Prepared by mehod SW846 3S5OB12674-11-2 rc810t61110/-2&2 PCB 122111i41-16-5 PCB 12325346e2r-9 PCB 124212672-?95 PCB 124811097{Sn rcg l2s110€€{25 PC8 12603n2+n4 PCB 12621r10cr44 PCE 1268
Surrog€16 /ecovs/iesi1 03&4+2 4, 4 -D&OdaEuorobiplr€nyt (SrlN51-2+i Dacachlorobipltenyt (Sr)
Sendvohdl€ Org.dic Compounds by GCMS
BRLBRTBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRI-BRLBRLBRLBRLARLBRLBRLBRLBRL
43106
BRLBRLBRLBRLBRLBRLBRLBRLBRI-
BRLBRLBRLBRLBRLBRLBRL1,120
pSftS dryrqtg drytig[l(g dry
U€/kS d.y
tgts drypgkg dry
Fgl(s dry
ldlg dry
Idtsdry 6.01
!gl(g dry 6.01
lgl(S dry 6.01
ldks dry 6.01pdko dry 30.0
PSftSd.Y 6.01
ldkS dry 6 01
IgkS dry 6.01
lCftS dry 6.01
Ig/kg dry 6.01pClqdry 6.01
lS,/tgdry 6.01
Ltdkg dry 6.01pSikg dry 6.01
Ig/kg dry 6.01pgtSdry 6.01
udksdry 6.01pSi(S dry 30-0
ldks dry 6.01
ligftsdry 4.01
ldrS dry 6.01
30-15030-150 %
udksdry 12.o
!g&s drv 12.o
lrgkgd.y 12.0
FgkSdry 11.0
ldkgdry 12.0
Ugh€dry 12.O
rs^g dry 12.0pdks dry 12.OpEtg dry 12.o
N-150 %30-1fr %
'|t
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SW846 806fA 22-MaFO7 26-l,,ef47 7031275 TG
SW846 6082 22.|,,,a'47 24 lar47 7031271 MP
Semivolatil€ Omanic Compounds bv SW846 8Z?OCPrepared by metiod SW846 35508&13?-9 Ac€naphtEne20cs6-8 Ac€iaphhyl€n€@€+3 Aniine1412-7 Attl|?cdne1912.249 Afazineto3-3:r-3 AzobenzendDipfienytdiatne92{7-5 BerEjdine56-5+3 Benzo (6) anthracen€
70r I
701 |
701 I
701 1
701 I
701 '|
701 1
701 |
SW84G 8270C 2.-Mat47 24.lli'd47 781279 M.g
Thit lthotutoq Eport ls not vatU Hirtoet rn atthortaal 1igrutap on th. @e.r poge.
+ Reportable Detectioo Limit BRL = B€low Reporting Linir Page 1 ot 124
Page 125
Sample IdentificarionMtF-l 24'sA595l7-01
Cliont Proiect #l 0 l - 88
Collection Date/Timel9-Mar-0? 00:00
MatrixSoil
Received
20-Mal-07
CAS No. Aaagte6) Fl"s Unia *RDL Diluiotr Prepdnd Analfzed Batch Anallst
Scmivol{tile Organlc Compounds by CCMS
Semivolatile Oroanic Comoounds bv SWO46 9270CPrepared by method SW846 35508
50-32{ BerEo (a) pyrene20199,2 Benzo(b)fluoranthene1s1-2a-? Benzo {g,h,i) perylene207{Sg Benzo (k) lluofanthen€65{50 Eenzoic acid100-s1€ Benzylalcohol1r1-91-t Bis(2rhloroethory)mehane111-.lt-a Bis(2-chloro€thyl)€ther39638.3"-9 8is(2.chloroisopropyt)ether117-81-7 Bis(2€gylheryt)phthatate101-55-3 4-Bromophenyjpbenyl€the/8s6a-7 Butyl benzyl phthatateE6'74-B Carbazole59'5G7 4-Chloro-3.methtiphenol106-47-8 4-Chloroaniline91-54-7 2_Chtoronaphthalene95 573 2-Chtoropt|enol7005-72 3 4-Chtorophenyl phenyl ether218{19 Chrysene53-70'3 Dibenzo(a,h)anthEcene13254-9 Dibenzofuran9s-so-1 1,2-Dichtorobenzener,r1-73-1 1,3-Dichlorobenzene106-46-7 l,4.Dichlorobenzene91-94'r 3,3lDichlorobenzadane120-83-2 2,4_Oichtorophenol84S6-2 Diethylphthatate131-11-3 Dim€thyl phthatate
105{7-9 2,4_Dimethfphenolu-74-2 Di-n-butylphthelates34-s2-1 4,6,Diniho-2_methytphenols1'28'5 2,4-Oinitroph€not121-14-2 2,4_Oinitrotoluene60+20-2 2,6-DanatrotOluene117+a{ Di-n-octytphthalate20Ha{ Fluoranlhene86-73-7 Fluorene11t-7rl'l Hexachlorobenzene87-6&3 Hexachlorobutadiene71474 Hexachlorocyclopentadiene61-72-1 Hexachbroethane193-39-5 Indeno (1,2,3-cd) pyrene9G12rl 1-Methylnaphthalene78-591 lsophorones1,5rc 2-Metlrylnaphthatene95-48,7 2-Methytphenol
108-39-4, 3,4-Methylphenol106-44-591-20-3 Nephthatene8A-74{ 2-Nilroanitine99{9'2 }Nitroanitin€
1,0901,120
1 ,160BRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLARLBRLBRL1,380BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RL2.150BRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRL
BRLgRL
SRL
ldkS dry 7O1
ldftS dry 7o1
!g/kg dry 7O1
!g/kg dry 7ol
ldks dry 701
UdkS dry 7O1
Ug/kg dry 701
Ug/kg dry 701
ldkS dry 101
PS/Kg dry 701pq|kgdry 7O1
!S/Kg dry 701
tlgkS dry 701
9Ekg dry 701
f.rs/Kg dry 1o1
Vgkgdry 7O1
ldKs dry 7o1
UdkS dry 701pgkS dry 701
ldkS dry 7O1
lSftS dry 701
Ig/KS dry 701
|lgkg dry 701
ugkg dry to1pdKs dry 7o1
UgkS dry 7O1
lig/kg dry 7O1
!g/kg dry 701
ldkg dry 7o1pgxgdry 7D1
ug/Kg dry 7O1
!g/kg dry 7O1
!g/kg dry 701
!gr(g dry 701
uqftg dry 701pS/kS dry 7O1
ldkg dry 701
ldkg dry 701
ldtS dry 701
S4{S dry 701psn(g dry 7O1pdkS dry 701pEkS dry 7O1
llgkgdry 7O1
rcAS dry 7O1
ldkS dry 7O1
ldkS dry m1
lgko dry 7O1
PgkS dry 7O1
t4/kS dry 7O1
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SW846 8270C 22-Mat47 24.ilaF17 7031279 M.a
Thh laboralory reporl it nal wlid roilhod on aartorized sigdzlure on ahe cover paEe .
' Reporiabte Oetection Limit BRI. = B€low Repoffng Limit Page 5 oa l24
Page 126
Samole ldentificationMtF-l 2-4'sA595 r7-01
Cli€nt Proiect #301-88
Matri{Soit
Received20-Mar-07
Coltectiod DatelTimel9-Mar-o7 00:00
CAS No, AnaIY.(s) Resdt Fl4g rRDL Dilu.iol L{ethod nel, Prepared ,lrralXzpd Batch Atelyst
S€mivoladle Orysnh Compoundr by GCMSSgmivolatile Oraanic Comoounds bv SWBit6 8?70Cft€pared by melhod SW846 35508100fi6 +Nilroaniline
9&9t3 Nifob€nzene€&755 2-Mtophenol10G02'7 +Nihoph€nol@-7!9 N-Nitrosodirhethy'amin€621q-7 N.Nitac6odi_n_pfopylamin€{16-10{ }SNitrosodipheflylarfilne
€7€F5 pentachloroptEnoi
85{l-6 Phenanhr€ne
i0&95-2 Phenol
r29{x}.0 n/rene1ro{6n Pyridine120{2n 1,2,+Trid{ombenzene95r.Ss4 2,4,tTridorophenol88{€F2 2,4,GTridoropnenol
&r?Dga*e /rougrbsr12t-6o.a 2-Fluorobhhentlfi7-124 2-Fluorophenol1t65404 Nitrobenzene4s4165"62 2 Phefiol45171&s14 Teryhenyt44lts-79-6 2,1,enib,!,t1ophofid
Totll Met li by f,PA 6000/7000 Series Mettods
743947{ I\rerc!ry
Tot{l M€{{b by EPA 20o S€rt€s Mcthodj
7444-?24 Silvet
7440{{12 ArgerilC.
7440n+3 Badsm
744{14}9 Cadmiun
71.1{}47-3 Chromium
7439-92.1 Leqd
rr82492 Selonium
SPLP Metals by EPA l3l2 & 6000/7000 Seri€r Method6
sr.LF Enrad|on
Z4&22-a Sllver
74,10-3&2 AF€nic
74r{},3$3 Barium
7440-449 Cadmfum
Zt4{}|7n Cho.hium
7439-9rc Merqlry
749-92-1 Lead
7782-4$2 S€'l€flium
Ge trerrl Ct€mbtry PerrDea€rr
% Sollds
1 SW846 8270C 22'&1atr47 24l"',a(47 7q|1279 M.B
t '
1 '
t '
1 '
1 '
I '
t '' l '
1 '
I SWA4i 74llA zGMar{7 27-N[ar-07 7m1322 Y?
I EPA 200.7 26.Mar-07 26+,lar47 7031321 HB
1 '
1 -
I '
1 '
1 '
1 sw8461312 ?2-MaFO7 22-MaA7 7m1344 BD
I SW8.f{l 1312/G0'108 2341Ff47 24-ttaF07 703l4og LR
1 '
I SW84813121/470A ' 26-lra.-07 7031409 YP
I SW84A 1312/60i08 ' 24.|i,.at.ol 70314S LR
BRLBRLBRL8RLBRLBRLBRLBRLBRLBRL2,130BRLBRLBRLBRL
806779529078
0.340
BRL
37.3
0.394
82.6
117
BRL
Co.npletsd
BRL
BRL
0.0198
BRL
0.0t 30
BRL
0.m19
BRL
87.4
lgl(sdry 2800pgr'kg dry 7O1
WJkSdry 701
UCrtS d.y 2m0
lgl(gdry 7o1
US/kS dry 7O1
Ekgdry 7O1
FgftSdry 7O1pgts dry 7o1
LrdkS dry 7O1
lryro dry 7Ol
frd?€dry 7O1pglsdry 7O1
ttgltgdtJ lO1
trg/kS dry 7O1
*130%,s110%30-r30 %1+11004*130%tg r l 0 %
mgftgdy 0-0340
fitgr'kg dry 1.14
mgn(g dry 1.71
rngrlg y 0.570
mgftg dry 0.285
m€r'kg dry 0.570
mg/€ d.y 0-856
mgikg d.y 1.7r
N/A
t',lSil 0.01m
mgd 0.0150
flEn 0.0050
rEif 0.0025
n€t 0.0O5O
mg/l 0,00040
trEl 0.m75
mSn 0.0150
% SM254OG Mod. 2}l',€t47 23-Met47 7031429 QP
Thit ldhonlorf .qod is ^ot tdful *tthaul aE authorizcd dgionte on ttE .av., pzge.
+ Reportlblc D€tectioo Limit BRI_ = Betoc, ReDorting Limit Paec 5 of I24
Page 127
Sample ldertificationM8F-2 2-4'sA595l7-02
Client Proicct #301 -8E
MatrixSoil
Received20-Mar-Oj
Collection Date/Timel9-Mar-07 00:00
CAS No, Anolyte(s) FloS Units *RDL Dilutiorl Method Retr. Preryed Analrzed Eotch ,4ntlltst
Volalile Org.nlc Compounds
VOC Extraction 21-Mat47 21-l,Lar07 7031261 BDField exkacted
Volatile Orqanic Compouhds
Prepared by method SW846 50354 Soit (tow tevet)
76-13-1 1,1,2-Trichlorotrinuoro€thane (FreoERL67 64 1 Acetone BRL107 13 1 Acryionitrile BRL7113-2 Benzene BRL10&8F1 Bromobenzene BRL74-97-5 Brofilochloromethane BRL15-2f4 Bromodichloromethane BRL75-25-2 Bromoform BRL74{3-9 Bromomethane BRL78,s3-3 2-Butanone (MEK) ARL104-51-8 rFBuMbenzene BRL13.198-8 sec-Butylbenzene BRL98116-6 t€rt-Bulytbenzene BRL7s,15.0 Carbon disulfide BRL56,23 s Carbon telrachloride BRL108-90-7 Chlorob€nzene BRL75'00-3 Chtoroethane 8RL67€6-3 Chlofoform BRL74.a7-3 Chloromethane BRL95-49-8 2-Chlorotoluene BRL106-43-4 4-Chtorotoluene BRL96-12-8 1,?-Dibrorno-3-chbroproF,ene BRL124481 Dibromochloromehane BRL106-e3-1 1,2-Dibromoethane(EoB) 8RL74 9s-3 Dibromom€thane BRL95-5G1 1,2-Dichlorobenzene BRL541-73-1 l,3-Dichlorobenzene BRL1096-7 '1,4-Dichlorobenzene ARL
T5-7 l-a Dichlorodifluoromethane (Freon.l2)BRL75-34-3 1,1-Dichloroethanero74G2 i,2-Dichloroethan€7535-4 1,1-Dichloroethene154F59-? cis.1,2-Dichlorcethenet56-60-5 hans-'t,2-Dichloroethene7A-57-5 1,z-Dichloropropanet42-28'9 1,3-Dichlorcpropane
59420,7 2,z-Dichlofopropane583-58$ 1,1_Dichtorcpropene1m61{1-5 ds-1,3-Dichlorop.opene10061-02{ trens-1,3-Dichloropropene100-114 Ehylbenzene
87S&3 Hexachtorobutadiene
591-78$ 2-Hexanone(MBK)!t8€2t lsopropylbenzene9947-a +Eoptopt/ oluene1634.{M-4 Methyl ted-b{jlyl eflref
BRLARLBRLBRLARL8RL8RLBRLBRL8RLBRLBRL8RLBRLBRLBRLBRL
108n0-1 4.t\tethyt_2+enlanon€(M|BK) BRL7sn 2 M€thylene chloride BRL
pSftS dry 5.9pdks dry 118
!g/kg dry 5.9
!S/kS dry 5.9pdkq dry 5 9
ldkS dry 5 9
!g/kg dry 5.9pS/kS dry 5-9
!g/kg dry r'r.8
ldks dry 59.0pS/kS dry 5 S
FS/kS dry 5.9pdkg dry s.9pqkS dry 29 5pSftS dry 5.9pSikg dry 5.9pqkSdry 114
Fg/(g dry 5.9
!g/kg dry 11.8
!S/kS dry 5.9
ldks dry 5.spg/kg dry 11.8pg/kg dry 5.9pdkS dry 5.9
Ig/kg dry 5.9
rc/kg dry 5.9
UgkS dry 5I
US/kS dry 5 9
Ug/kg dry 11 I
UdkS dry 5 I
!g/kg dry 5-gpg/kg dry 5.9
!g/kg dry 5.9
l,g/kg dry 5.9pSftSdry 5,9ps/ks dry 5.9
ldkS dry 5.9pg/kg dry 5 IpqkS d.y 5.9pdkg dry 5 I
!g/kg dry 5,9pg/kg dry 5,9
t g/kg dry 59.0
ldkSdry 59pelkgdry 5.9pdksdry s.9
t'dkg dry s9.0
Fs/kg dry 59.0pdkSdry 5.9
SW846 82604 22-MarOI 22-Ma(4f 7031335 RLJ
91.2G3 Naphihalene
Pagel ol 124
Thb labonlory Rpod i| not valid Nihou aa &arhorl@l slgaa,urc on the cot)e, page .
* Reportable Detection Limir BRL = Below Reporring Limit
Page 128
Sarnple IdetrtificationMtF-2 2-4'sA595 | 7-02
Client Proiect #301-88
MatrixSoil
Collection Date./Timel9-Mar-07 00:00
ReceivedzGMar-07
CAS Na, A','dE 4s) Resdt Flzg Afits *RDL Dllulian Method Retr. Pnparcd Analwd Bateh Anrtfst
Volatile Org.nic Compoun&
Volaf le Oroanic ComoouodsPrepd.ed by n€thod SW846 5035A Soit (tow teve{)
75'49-4 Tric*rlorofiuoromethane (Faeon l1) BRL
103-6$' GPrcpylb€nzeoe100-42'5 Slylen€€0-20{ 1,1.'1.2-T€b_acf oroethane?9,345 1,1,2,2.T€trdcHoroethane127-18-4 Tet€d omethene10&88-3 Toluene€7{1{ 1,2,}Trichlorob€nzene120{2-1 1,2,4-Taichltrobenzene71-5$6 l,l,l.Trichloro€tEne7e{P5 1,1,?-Tdchloro6thane79{1{ Trkt orcefien€
s6-18-4 1,2.+Trichlorop.opane95496 i,2,4Trimethylb€nzene10867{ l,3,tTrimethylbenzene7fr{1-4 Vinyl drtoride133G2G7 m,p-Xyteoe9147€ o-Xy'on€10+99-9 Tet(drydrofucan60-2$7 Ethyl elh€r994{5}a Teft.amylmethytether637-e23 Etry4 teft-buM 6d1€r10&20-3 Diisopropylether75{s{t Tcft-Butsnol/ h.rqy' abotlol123-91-1 1,4-Dioxane
Sutrogate tecovedes:46040.4 +Btufioauorcbenzene2037-26-s Tolueno4St 7o@-o/ -o 1, 2$ichbrcathane44fi 68-s 3,7 D itttdrlof, uo to n€th a n e
Enrrct ble Petrolcrm Hydroc.rtrons
Extractable To{al Pelroleum Hvdroc€rbonsPrepa.ed by method SW846 355088006i1-9 Gasoline6847630-2 FuelOil #26047F31.3 Fu€l Oit #4605s$0{r4 Fuet oil #6M0€8fim00 Motoi oil$0100000 Avislion Fuel
Unid€nlifiedOhe. c)ilTotal Pebol€um HydrccarbonsCS436 Aliphatic Hydrocarbons
Sa,nog|ab r€co!,,arbsr1u,6-33-2 1 -Chloroodealecano
Selr|irohttle Orgrnlc Compouldr by CCOroanochlorine Posticides SW846 8081APrepared by melhod SW846 35508309-00.2 Aldrin
SW 846 82808 22+tar47 22t4*47 7031335 RLJBRL
BRL
BRLBRLBRLBRL
BRLBRLBRLBRL
8RLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RL
99104
110
BRLBRLBRT8RLCalqilated asBRL
BRL83.583.5
115
pdts dry 5,9pdkg dry 5.spdkg dry 5.9pStkg dry 5.9pdkSdry 5_9pg/l(gdry 5-9
lglsdry 5.9
USI(S dry 5.9
ItSJkSdty 5.9
WI€ d.y 5.9pCAS dry 5.9
ugtgdry s.9
ldxS dry 5.9
ldkS dry 5.9
!g/kS dry 5.9
ttgJkgdry 5.9pErgdry 11.8pdl€dry 5.9pdkgdrt 59.O
VdkSdty 5.S
tl4/ks dry 5.9
Udks dry 59
Fgtg dry 5.9pdkgdry 59.0pS/XS dry r18
70'130 %70'1i0 %70-130%70-1fi %
mglkg dry 27.4ntdkS dry 27.4o€rkg dry 27.4mg/kgdry 27.4ndkS dry 27 -4n'dkS dry 27 .4mdkg dry 27.4mg/kg dry 27 .4rEikgdry 27.4nEfl(g dry 27.4
4)-140.A
1II
I
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1
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1
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7
I
1
1
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I
+CTEIPH 22',l',a'47 23-$9f-07 70312A1 DS
BRL ldkS dry 6.13 StrE46 80AlA ?2-MaIo7 8 tiat47 7G11275 TG
Thb lahotuory Epon is ,tot eolil Nlthott z, auahotlz.d sigdslare oE ,h2 coear ltoge.' Reportslrle Delaction Limit BRL = Below R€porting Limir Pag€ 8 of 124
Page 129
Sample [dentificationM8F-2 2-4'
sA59517-02
Client Proiect #301 -88
MatrixSoil
Received20-Mar 07
Collection Date,,Timel9-Mar-117 00:00
CAS No. Anabte(s) FloC Unatr *RDL Duutian PPparcd Autltzed Bath Analpt
S€mivolatile O€adc Compounds by cC
Orqanochlorine Pesticides SW846 808 tA
Prepared by melhod SW846 35508
319 84s a,8HC319-Br7 b_gHc319-863 d_BHC58{+e g-BHC (Lindene)5T-74I Chlodane72 54-a 4,4.DDD (p,p )72-5ss 4,4-DDE {p,p,)50-2+3 4,4{DT (p.p.)60'57 1 Dieldnn959-98{ Endosulfan I3321355-9 Enclosulfan ll1031-07,8 EnctirsulfanSullate72-2O-B Endrin7421-s3-4 EndrinAtdehyde76'44€ HeptachtorI24us l\,,lethoxychlor1024-57-3 Heptachtor Epoxideeo01-3t? Toxaphene510171,9 a_ChlordEne5,566,34,7 g-Chlordane
53494-70'5 Endrin Ketone
Sunogate rccoveries:103868+2 4,4-DB-Ochnuombiphenyt (Sr)
2051 2z j Docachlorobiphenyt (Sr)
Polvchlorinated Biohenvts bv SW846 8082Prepared by melhod SW846 35508
12674-11 2 PCB 101611104-28-2 PCB 722111141-16-5 PCB t23253463-21-9 PCB 124212672-294 Pc:B 12481to9t6s-1 PCB 12lA11096-82,5 PCg 126037324-23-5 rcB | 26211100-14-4 rc8 1268
Suftogale rcco@ies103868+2 4,4DgoclaflLtotobiphenyl (St)
m5t?+3 Decachtotobiphenyt (Sr)
Semlvolrtile Orgrnic Compouods by CCMS
BRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
89
BRLBRLBRLBRLBRLBRL58.8BRLBRL
7090
BRLBRLBRLBRLBRLARL
BRLBRL
pStkSdry 6.13
t SIq dry 6.13
!g/kg dry 6.13
!g/kg dry 6-13
IiS/kS dry 30.6
ldkS dry 6-13
ldkS dry 6.13pdkg dry 6.13
UdkS dry 6.13pdkS dry 6.13pS4g dry 6-13
t gks dry 6.13pSftS dry 6 13
ldkS dry 6.13
Pdks dry 6.13
FdkS dry 6,13
liS4q d.y 6.13
USftg dry 30.6pSlkS dry 6 13pdkS dry 6 13pS4(S dry 6.13
30-150 %30-150 %
psfts dry 12.3
Pg/kg dry '12-3
Ig/kS dry 12.3pdks dry 12.3
fidks dry 12.3
t S,/kS dry 12.3
lYkS dry 12.3
!g/kg dry 12-3
lgkS dry 12.3
30-150%io-150 0,4
ldkg dry 679
ldkS dry 679
!g/kg dry 679
UgkS dry 679
tig/kg dry 679
!g/kg dry 679
!S/kS dry 679
lgkS dry 679
swa46 80814 22-1,1ar47 26-Mat-07 7D31275 IG
SW846 8082 22-MaA7 24'Ma?O7 7031274 MP
Semivolatile Orqanic Cofioounds bv SW646 8270CPrepared by method SW846 35508
83-32-9 Acenaphthene208-s4 Acenaphthylene62-5!3 Anitin€120-12-7 Anlhracen€1912-24-9 Atrazin€10133-3 Azobsnzen€y'Diphenytdiazine92{7-5 Benzidine56-55.3 Benzo (a) anthracene
SW846 8270C 22-Mat47 214nat07 7031279 M-B
Thit lzborztory rcpon ir not valU x'ithoat aE o!rtofi.ed signeture on the @ter page .
+ Reportable Detection Limit BRL = Below Reponing Limit Page 9 of 124
Page 130
Samole [deotihcationN{EF-2 2-4'sA595l7-02
Cliedt Proie€t #301-88
Collection Date/Timel9-Mar{7 fi}:00
MatrixSoil
Rec€ived20-MaF07
CAS No. Anaryb(s) Resalt Flag *RDL Diluittr Mdhod Rel. Prqued A,,alwn Bdch Antlysl
S€mivol.tlle Orgonic Compoundr by ffMS
Semivolatile Oroanic Comoosndg bv SW846 B2Z0CPrepared by mglhod SW846 355083)-324 Benzo (a) py.oneat99l Benzo (b) ffuoranfhener9r2,1-2 Elenzo (g,h,i) perytene207{&9 BerEO (k) fruo|antlenett545-0 Benzoic add10G51{ Benzylalcohol11r-91-1 Bis(2-chlomethory)methan€11141.4 Bis{2-cruoro€thyt)etE.3963s32,S Bis(2+hlorcisoprcpyl)e0Er117-81.7 Bis(A.ethy,lh€)qt)phthalate101.553 4_Bromopheny' phenyi elh€r8s.64-7 Bu!/benrylphthatate8G74{ Csrbazole59{Gz 4-Chtoro-3-fiethyiphenol10€-4?{ +Chtoroaniline91-5&7 2-Chloronaphthatens95'57-8 2.Chlorcphenol700$72.3 4-Chloroph€nyl phenyt ether2t8{1.9 Chrysenes3-7{t3 Oibeozo (a,h) anthrac€ns132444 Oibenzofuran95{Gr |.2-Dichlorob€nzen€54i-73n 1,3-Oichlorobefizene10€-{6-7'1,4-Oidhlorobenz€ne9l-94-1 3,3'-Didtlorobenzidine120-8!2 2,+Dbhloropheflola4{&2 Diethytphthatate13rnt-3 lImethylphthatale1ffi7-e 2,4loirnetiyldlenolu-r4-z D-n-bUVphthalate53+52-1 4,6-Dinilro-2-methylphenol51-20-5 2.+Dinitrophond12i{+2 2,4-Dinilrotoluene60G20-2 2,6oinitrototuene117-e4.o D-fl-octyl phhatale206..(+0 FluoranttEne8&7+7 Ffuorsne11&7+l Hoxachlo@benz€ne07{&3 Hex€ctorobutadieneT1474 Hexachtorocydopentadiede67-72-1 H€XaClOroethane1e'396 Indeno (l,2,3-cd) pyrenes0-12-0 t-i,trethylnaphthaleno7&s*l lsophoaono91.t$ 2-Methytnaphhateno
4$7 2-ldethylph€nol10&39-1, 3,4-Methylph€nol1ftr-4.r.591-2c3 Naphthatene&744 2.Njtroaniline99{$2 }Nitroanitine
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRIIERLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLERL
BRLBRLBRL
ldkS dry 679
ldlq dry 67S
|Jg/kS dry 679
Ugl*qdry 67S
ldtgdry 679
ugkSdry 679
trg./kg dry 679
lrSikS dry 679
lqkS dry 679
ldkSdry 679
!Sn(S dry [email protected] 670
FSftSd.y 679pdksd.y 679pdks dry 67S
UdkS dry 679
t Sl(rgdry 679pS^S d.y 679pg19 dry 679pdkS dry 679
t dkg dry 679pgikS dry 679
Igr(g d.y 679pdrqdry 679
UdlSdry 829
IdkS dry 679pSil€ dry 679
udks dry 679
Lidrgdry 679
ug/kg dry 679
t'dksdry 679pgfts dry 679
rsrks dry 679
rgls dry 679
Ugr'kg dry 679
rcrkS dry 679pg/kg dry 673ps,ts dry 679
ldtSdry 67s
lgkg dry 679
$gnKS dry 673
Fgrtg d.y 679ps/ks dry 67s
ldkS dry 67S
[dkS dry 679
lldko dry 679
t sikg d.y 679
pS,/kS dry 679
lgrsdry 679
IdkS dry 079
1
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SW846 8270C 2-Met47 24+,i,a147 7O3r279 M-B
Thh labodoq rqo.l it ^oa eqlAl lrtoet qtt aalhoriad dgnafune od tlt coter pag..
'Rcportable Detectim Limit BRL = Below R€porting Limit Page lO of 124
Page 131
Sample [dentificarionM8F-2 2-,tl
sA595l?-02
Client Proiect #30r -88
CoLlection Date/Timel9-Mar-07 00:00
MatrixSoil
Received20-Mar-o7
CAS No. An4utc(s) Flog Unia *RDL Dilulinn Method Retr. Prepared Aru$'zed Rzt.h Andlrst
S€mivolrtil€ Orgrnic Compounds by CCMS
Semivolatle Orqanic Compounds bv SW846 8270C
PEpared by melhod SW846 35504
100-016 4-Nitroaniline
9O-9t3 Nikobenzene
00-7t5 z-Nitrophenol
100-02-7 4-Njtrophenol
62-7re N.Nitrosodimehytamine
62144-7 N-Nitrosodi-n-propylamine
€G3G6 N.Nitrosodiphenylamine
87€s5 Pentachlorophenol
8F1-8 Phenanthrene
108-95-2 Phenol12s0.o Pfene11c86-1 Pyridine12{)!821 1,2,4-Tddllorob€nzene
s5-efl 2,4,STichlorophenol
€3-0+2 2,4,6-Tricftlorophenol
Swrogale rccoveries:3214Ga z-Fluot&iphenyt
367-124 2-Fluorophenol
116,4a4 Nitrcbenzene45
1165-62-2 menol4s
1718 51 0 Terphenyl4l4
11a-794 Z4,ETibrcmophenot
Total Metals by EPA 6000n000 S€ries Methods
7,139 97-6 Merc!ry 0.222
Total Metds by EPA 200 S€ri€s Methorts
sw846 8270C 22-MarO7 24-Mat4/ 7031275 M.B
1 SW8467471A 26-Mar0l 2741at47 7031322 YP
BRLBRLBRLBRL
BRLBRLBRL8RLBRL
8RLBRL8RLBRLBRLBRL
786378528574
BRL
3.97
44.5
0_490
44.3
269
BRL
Comdeted
BRL
BRL
0 .0211
BRL
0.0148
BRL
o.0/24
BRL
90.0
pdkS dry 2120pg/kg dry 679pg/kg dry 679pdkgdry 2720
!g/kg dry 67S
ldkS dry 679pdkS dry 679
!q/kg dry 679pdkS dry 679
!g/kg dry 679pg/kg dry 679
!g/kg dry 679
ldkS dry 679
!Sn(S dry 679
!g/kg dry 679
30-tm o/,
1rf l00A30-130 %t 5-110 %30-130 0/o
15-110 %
nu/kg dry 0.0327
mdkS dry 1-07
mg(s dry 1.60
mg/kg dry 0.533
mg/kg dry 0 266
mg/kg dry 0.533
rirgftS dry 0.799
mg/kg dry r.60
mg/l 0.0100
mSl 0.0150
.'r,q[ 0.0050
mgn 0.0025
mgn 0.0050
mSI 0.00040
.r€l 0.0075
nE/l 0.0150
%
1
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7440-22-4 Silver
7440-38-2 AFenic
7440-39-3 Eadum
7440-43-9 Caclhium
744047-3 Chromium
743s92-1 Lead
778?4+2 Selenium
EPA200-7 26-Mat47 274,Aa( 07 7031321 HB
SPI,P Metsls by EPA ll12 & 600fl7000 Sert€s Methods
7440-224 Silver
7440-3&2 Arsenic
744{-39'3 B€riuft
744{143-9 Cadmjum
7440-47-3 Chromium
7439-976 Merotry
7a39-92-1 Lead
7782-49-2 Sel€nium
General Chemlstry Parrmetets
% Solids
1 SW8461312 22^nar.07 22-MaA7 7031344 8D
1 SW846131260108 z3-Mal.Ot 2{.Mar0l 703'1408 LR
1 "
1 "
1 ' ,
1 SW846131217470A " 2€{,lar{7 7031409 YP
1 SW846131260109 " 244nat47 7031408 LR
1 '
1 SM2540 G Mod. 23-t4ar-07 23-Mar-07 7031429 QP
Thb lahontlory fepora is not ttlld toithoul dn outhoriie.I sigAatare on the cover page
+ Reportable Detec.tior Li Di! BRL = Berow Reporrjng Limil Page 1l of 124
Page 132
Sample ldentificationM8F.3 2-a,sA595l7-03
Client Proiect #301-88
Collection Date/TimeI 9-Mar{7 00:00
MatrixSoil
Received20-Mar-07
CAS No. Analrte(s) Flae aRDL Inaitn Method Rtl PEWed Aaalr'?.ed Bdch Analysl
Volrtile Orgmic Compounds
VOC ExtractionVolatile Orcanic ComooundsPrepared b!' method sw846 5035A Soil (tow tevet)7e.i3-l l,l:-Trkhlorofinuoroothane(FreoPRL67i+t Acetofi€ BRLio7nll Adylonibile BRL71!32 Benzen€ gRL
i08.6€-1 Bromobenzen€ BRLra-97-5 Bro.nodllorofiethane BRL
75-2+2 Brornofofln BRL74{}9 Bromo0elhane BRL70-9+3 2-Buhnone(MEK) BRL104'51{ rl-Bu9lbenzene BRL13t9&€ s€c€utylbonzene BRL9e{6-6 tsd€utylbenzen€ BRL7t154 Carbon disulfde BRL50.23-5 Carbon lebachloride 8RL10990-7 Chlorcb€n2ene BRL75{0-3 Chb.o€thane BRL67€&3 Chlorobrm BRL7447-3 Chlommothene BRL9s-49.a z-Chlorotolu€n€ BRL10fF43-1 +Chlorctolueno BRL96-12-8 1,2-Dbro.no-3-chloroprop€ne BRL12.r-4{-1 Dibromod oromethene BRL1c'6934 l,2-Dibromoethane(EDB) BRL74-9!3 DibomometrEne BRLg+s(l.l l,2-Dichtofobenzene BRL541-7311 l,3-oichlorobenzene ARL106-46-7 l,+Dichlorobenzsne BRL75-7 1-8 Dicfilorodifluoaomeihane (Faeonj2) BRI75-34-3 1,'1-Dichlofoethane ARL107-Oe2 1.2-Dict{oro€thane BRL75-35-,! .1.1-Oichtoroethene BRL1se592 cis-1,2-Dlchloroetheie BRL15Sq],s ten6-l,2.Didhloro€hetre SRL7€{7-5 1.2-Oid orcpropane BRL142-28-9 '1,3-Dichlofopropane BRL59{-2F7 2,2-Dichloropropene SRL561584 1,|-Dichtoroprcp€ne BRL1006i41'5 cis"1,3-Dichlorogrop€ne BRL1006142{ tan91,}Dichlo.ogrop€ne BRfl0G41-. Ehy'bsnzfie 8RL8z€+3 Hexachto.obuladhne BRL5Sr-70S 2-t{6xanone (MBK) BRL
lsotropylberEen€ 8RL€{7{ +tsffropy'btu€ne SRL1634{4-4 Methyl ted+oty'l €trer BRL10&rcl +Me&yl-2.pentaftne{M|BK} BRL754e-2 irethylene chtoride BRL
21-iiar-o7 21-l4ar{7 7031261 8D
22-ll,.at47 22+taFO7 761335 RLJ
BRL
Field e)daactod
UdtSdry 7.5
trslt(S dry 151
FSI€dry 7.5
U919dIy 7.5
ldkg dry 7.5
rd*S dry 7.5
rc/kg dry 7.5pdrs dry 7.5
ldls dry ts.ipdkgdry 7s.4
IdkS dry 7.5
Fgtkg dry 7.5
FSftSdry 7-5pdkS dry 37.7
tdkS dry 7.5
lgkS dry 7.5
l4k0 dry 15.1
Fgtgdry 7.5
!4k9 dry 15.1
rglxSdry 7.5pSn(S dry 7.5pglqdry 15.1
US&S dry 7 _5pgrSdry 7.5
Idkg dry 7.5
!gl!s dry 7.5pgftgdry 7.5
US/kgdry 7.5pdkgdry ls. l
udlgdry 7.5
ugtsdry 7.5
lrSlkg dry 7 5pS/kg dry 7.5
Ugl(gdry 7.5
udkSdry 7.5
t gkS dry 7.5
FS/kS dry 7.5
US^S dry 7-5
$g/kSdry ? s
tdkg dry 7.5
Ug/kS dry 7.5
Fg/t€ d.y 7.5
ISftS dry 75.4
fgkg dry 7.5
ldkS dry 7.5
rcn(S dry 7.5
F€ikgdr, 75.4
f.fSikgdry 75.1pC/kS dry 75
voc
sw 846 82608
9t-u}3 Naphthalane
PagE l2of 124
fhk laboratory Epotl h not vdtd wiahoa ae surtorited slgnatsre ol the cowr 1,q..' Reportable DEtection Limit BRL = Below Re!|orting Limir
Page 133
Sample ldentilicationM8F-3 2-4'
sA595l7-03
CLient Proiect #30r,88
Collection Date/Timel9-Mar-0? 00-00
MatrirSoil
Received20-Mar-o7
cAs No. Anfute(st Res,h F,aE Unia ARDL L[e,ltod ReI. Preta4d Analrzed Balch Ana|.st
Volrtile Orgrnlc CompouEds
Volatile O.qanic ComooundsPrepared by method SW846 50354 Soit (tow tevet)
75€94 Trichtorofluorcmethane (Freon .t 1) BRL
1o}gs-t n-PrcpylterEene10G12 5 Styrene630205 1,1,'l,2_Tetrachtoroethane79{4_s I,1,2,2-Tetrachlorcethane127n8-4 Tetrachbro€thenel0a€4,3 foluen€87.€16 1,2,lTrichtombenzene120€2-1 1,2,4-Trichtorobenzene71-s5{ l,1,t_TrirhtoroetfEne79{tr5 1,1.2_Trichtoro€thane79{l€ Trichloroelhene
96-18-4 t,2,STrichloropropane9s43{ 1,2,+Trimethytbenzene108€7-6 1,3,+Trimethytbenzene75414 Vinylchtoride1330-2G7 m,p-Xylen€95-47-6 +Xylene109-9s9 Te{rahydrofuran60-?s7 Ethytether994{5€ Terl-amyt methyl ethef637.92-3 Ethytled-butytetf€r108-20-3 Di_isoprDpytether75{5{ Ted-Butanot/ bntyt alcohol12391-1 1,4-DioxeDe
Surrogale ,€cover'es_160a04 +Brcnofluorcbenzene
m37-26-s Tduene4S
1 1066074 1,2-Oichloroethane-d4
1868-sAr Dibr'ofllolfufrrcmethane
ExtyNctable Petroleum Hydrocrrtons
Exlractable Total Petroleum Hvdrocafuons
Prepared by method SW846 35508
800€-61,9 Gasotine6847&30,2 Fuetoit#26847e31-3 FuelOil#468553{0-4 Fueloil#GirogSomaJo Motof OilJ00100000 Avjaijon Fuel
Unidentified
Olh€r Oil
Total Pekoleum Hydrcc€rbons
C9-C36 Aliphatic Hydrocarbons
Sunoga6 ,ecovedes'3386-3}2 l-Chlotoodadecane
S€mivobtile Oryrnic Comportrdr by GC
Oroanochlorine Pesticides SW846 8081A
Prepared by method SW846 35508
3OlO0-2 Aldrin
SW 846 82604 22-Ma47 22-MaF07 7031335 RLJBRLBRLBRLSRLBRL
SRLBRLBRLBRLBRLERL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRL
9410110998
WkS dty 7.5
UdkS dry 7.5
ldkS dry 1.5
pdkS dry 7.5
ldkS dry 7.5
!94(S dry f_5
pg/kg dry 7.5
pg/kg dry 7.5
pg/kg dry 7.5
f.ig/kg dry 7.5
lSftS dry 7 5
f.iS/r€dry 7_5
!g/kg dry 7 5
UdkS dry 7 5
Ug/kg dry 7.5
lrSlkS dry 7_5
udks dry 15.1pg/kg dry 7 5
US/Kg dry 75.4
IgkS dry 7 5
USftS dry 7 S
lgkS dry 7.5
ldkS dry 7.5
ldkS dry 75.4
,rgkS dry 151
7L130 0t
70-130 %70-130 %70-130 %
mdkS dry 44.1
mSI$ dry 44.1
mdks dry 44.1
mgLikg dry 44.1
.ng!4q dry 44.1
lrglxgdry 44.1
mg!4(g dry 44.1
mgL/Kg dry 44-1
mgr'kg dry 41.1
mg(g dry 44'.1
40-140 %
pdkq dry 7.11
1
1
I
I
I
1
1
1
1
1
1
1
1
1
1
l
I
1
1
I
1
1
1
1
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
120
+CTETPH 224JtaA7 2}Mafi7 7031281 DS
BRL sw8,r6 8081A 22-Mat47 27-Mar47 7031275 TG
Thir ltbororor! ftFod is not eoIU xlithoat an auhortted sigrroitw on the covr page .
+ Reportable Detection Limit BRL = Below Reporring Limit Page l l of 124
Page 134
Sample ld€otificationM8F-3 2-4'sA595l7-03
Client Proiect #l0l-88
MatrixSoil
Collection Dat€/Tirnel9-Mar47 00r00
Received20-M^r-07
CAS Na Aulru(s) Fhc *RDL Dilulo', Mdhod Rel. Pnpared Addlyzed DatEh Atulfsr
Semivolrtile OrggDic Compolrnds by CC
Orqanocfilorine Pesticides SW846 8081A
Prepared by rnethod SW846 35508
319{4-€ E-BHC319457 b"BHC319-86{ d-BHC
58{Bs +BHC (Lindan6)
tl-74-9 Chlordan€72€4{ 4,,1-ODD (p,C)
?2.s5.9 A,+DDE (p,C)
5o-2s-3 4,4-DOT (p.p')
60-57-1 Oehrin95$!Xl{ EndGulfan I332133$9 Enalo€ulfan lllq3t{7+ Endo6ulhn Sulfab72-204 Enddn742143-4 EndrinAldehyde76414 Heptad or72435 Methoxydtlorl02a€7-3 tl€ptachlof Epoxide8t1o1.3.t2 ToxapfEne511)0-71-9 aql|ordan€5s66-3+7 g-Chlordanes3494705 E ldrh Ketrn€
Srrzog6l€ '€ooyr/bs--1 uae&a2 1,1,&Ociaf, @@biptenyl (Sr)
m51-243 @cdchlorobiph4nyl (St)
Polvdrlodnaled Biohenvls bv SW846 8082
Prepared by rnethod SW846 35508
1267411-2 Pcg 10161110+28-2 PCB lzl11r41n65 PCg 1232534&+21-s PCB 1242
12672-?34 PCB 1248i1097€$1 PCB 12541109€-82-5 PCB 12603ru423{ PCB 12621n0sr1-4 PcB .t268
St'rogEfe rgcovenbsirc38e8+z 4,4Dg-Ocdluorobipheni (Sr)
tu51-21-3 Decachbrobbhqnyl (Sr)
SelIivd.liL Orgsnic Cornlorf,ds by CCMS
BRLBRLBRLBRLBRLBRLBRLgRL
BRLBRLBRLBRLARL8RLBRLBRLBRLBRLBRLBRL8RL
4180
BRLBRLBRLBRLBRLBRLBRLBRLsRt
4070
BRL
BRLBRLaRrBRLBRLBRLBRL
l,gr'ko dry
USikS dry
lrgrkS dry
FS/kg dry
usl(g dD/
rcfts dry
us& drypsftg dry
FgkSdry r.t1
ucrls dtv 7.11gdXS dry 7.1rpdlq dry f .11pgl€ dry 35.6
FS{(g dry 7 11pdkS dry 7 'l1
pdksdry t. tr
IrS/kS dry 7-0O
!€ €dry 711
leit(g dry 7.r1pg/rS d.y 7.11
lJdks dry 7.1r
udxS dry 7 -11pSftg dry 7.11pg/kg dry 7.11
rdrgdry 7.11
lglqd.y 3s.6
ldlS dry 7.11
UdkS dry 7-11
UdkS dfy 7.11
3It-150 %*150%
IS/kg dry 14-2
FgrSdry 14.2
lgllqdry r4.2
Ugr'kg dry 14.2pS/kS dry 14.2
lgl€dry 14_2pdksdry 142
ldlS dry 14.2
rdks dry 14.2
3G150%30.150 %
SW8{6 80€1A 22-lhr-O7 Z7+,,ar4f 7031275 TG
Sernivoladlo Oruanic Comoounds bv SW846 8270CPrepar€d by metlEd SW846 35508&3-32-9 Aconaphth€ne2n&scs Apen€phthybn€62{}3 Anfline14n12-7 Anthrecene19'12.2+9 Atsazine10$33-3 Azobenzens/Diphenyldiazine92{7-5 Bonzidln€5€.5$3 Bonzo (a) anthrscane
97 1
547 1
547 1g7 1
547 |g7 1
97 1
97 1
SWa,{6 8082 n.Maf{7 24-MatA7 7081274 MP
SW846 8270C 22^4,tr47 24-t'6t47 7031279 M.B
Thb bbrotiry rqod is ,tot tdd pidroo att ouhorid signJ,t tE on tIE co16 page.
r R-epo.table DetEctbtr Limit BRL = Below Reporting Limit Pagc 14 of 124
Page 135
Samolo IdentificationM6F-3 2-4'sA595l?,01
Client Proiect #l 0 l - 88
Collection Dare/Time1g-Mar 07 00r00
Mat.ixSoil
Received20-Mar-07
CAS No. Anzlrte(s) Resul! FlaE Unia *RDL Dil@ion Method ReJ Ptepared Analyed Ectch Analrsl
S€mlvolatlle Orgenic Compounds by CCMS
Semivolatile Orqanic Comoounds bv SWO46 8270CPrepared by method SW846 35508
50,32+ EerEo (a)pyrene
20+99-? Benzo (b) lluot?nJ1e,le191-24-2 Benzo (9,h,0 perylenem7-08 9 Eenzo (k) nuoranthene6545-0 EerEoic acid10(l-s15 Benzylalcohol11r!'1J Bis(2dlloroethory)methane111-44-4 Bis(2-chioroethyl)€drer39638-32-9 Bis(2_chloroisopropylFther117{l 7 8is(2-€Uiythexyt)phthatate101'553 4-Brcmophenyl phenyl ethera55a-7 EuVl benzyl phthaiatem-74-A carlrazoles9-m-7 4-Chtoro-3-methytphenol10eF47{ 4-Chlo{oaniline9i-sa-7 2-chloronaphdalene95-s7-a 24htrrophenol?005-72-3 4-Chtoropllenylphenylether
218{1-9 chrysene53-t0-3 Dibenzo (a,h) anthracene13?$43 Dibenzofuran95,5G1 1,2-Dichlorobenzene:t41-731 1,3_Dichlombenzene106-46-7 1,4-Dichtorobeflzene91-941 3,3'-Djchlorcbenzidjde120S3-2 2,4,Dichlorophenol&46G2 Dierhylphthalate131-11-3 Dirnehyl phthalatre
10s7-s 2,4-Dimethylphenolu-74-2 Di-n-butylphthatate53.1.52-1 4,6-oiniko-2-inethylphenol51-28-5 2,4_Dinitrophenol121r4-2 2,4-Dinih.otoftJene
606-20-2 2,6-Dinitrototuene117-84{ Di_n_octy'phfralate206-444 Ftuoranhene86-7!7 Fluorene11&741 Hexachlorubenzene474&3 Hexachkaobutadien€77174 H€xacfilorocyclopentadiene61-12-1 H€Xechloro€lhene1913S-5 InderE (t,2,3d) pyrcn€!10'12{ l,tlethy'naphthalene78.59.1 lsophoronee1.57-6 2-Methylnaphhalenee54a-7 2-tr,,tehylphenol
10H$4, 3,4-Methylphenol106-44-5e1-2G3 f{aphthalene8a-74-4 2-Nitroanitine99{92 3-Nitroaniline
sw846 8270C 22-Ma(O7 24-Ma(O7 1031279 M.BBRLBRLBRLBRLBRLARLBRLBRLBRL
BRLBRLBRLBRLARLBRLARL8RLBRLBRLBRLBRLBRLBRfBRLBRLBRLBRL
BRLBRLBRLSRLBRLBRLBRL
BRLBRLBRLBRLARLARLBRLBRLBRLBRLBRLBRL8RL
BRLBRLBRL
pg/Kg dry 547
ldksdry 517
!g/kg dry aA7
lrsiKg dry u7
lsixs dry 547
lrgxs dry 547
tr9/k9 dry 547
lSftS dry 547
!S/kS dry 547
PYko d.y 547
ldkS dry 547
ldkS dry 547
!S/kg dry 547
!S^S dry 547pS/kg dry *7gSJkgdry 547
trS/kS dry 547
UdkS dry 547
ldkS dry 547
lgkg dry 547
!S/r€ dry 547
ligKs dry 547
lgikg dry 517
!g/kg dry 541pSJtrS d'y 547
lrg/kq dry la1pS/kS dry 547gdks dry 517
rc/kg dry U7pg/kg dry U7
lS.ftg dry 547pdkg dry 547pg/kg dry 547pdkgdry aalpdKs dry 547
f.iS/kS dry aA1
!g/kg dry g7
!S/kg dry 547
ttgtKsdry aa7
!9I(S dry aA1
FSI(S dry Y7psfts dry 547
USftS dry 547
lSftS dry g7
!S/1S dry 547
ldtS dry 547pdks dry 547
!g/kg dry 547pdkS dry 547
lgikS dry 547
th& Iabonroo' Eport ir nat uzlid ,oirtod .n aartorivd signaitrre oh ahe co4, pagc -
' Report{ble D€rection Lirnit BRI- = Betow Repotting Limir Page l5 of 124
Page 136
Sample IdetrtificationM8F-3 2-4'sA595l7{l
Clieot P.oiect #301-8r
Matri{Soil
Collection Date/Timel9-Mar-07 00:00
Received2O-Mat41
CAS No. Adab',e(s) Res t FIog |RDL Diluion Mefiod nctr. hepand Awlwd Batah Analysl
Semlvohtile Orglnic Compoundi by GCMS
Semivolatil€ Omanic Comoouods bv SW84ti 8270CPr@ar€d by m€thod SW846 35508
10G01€ 4-Nitoaniline98{+3 Nifob€nzene08-7SS 2-NitIoph€nol100{2-7 4-Nitlphenol€a-75-e l+.Nbosdimethyiamine6?r€a-7 N-Nitrosodi-n-propylamine0F305 t+Nitooodiph€nylamine87{6{ Pefitaahlorophenol85-01{ Ph€flenthene10&9+2 Phenol129{0{ Pyrcne110-8t1 F)tidiner2o82-l li,+Trid oobenzene
2,4,$Trichlor@h€nol8&062 2,4.$T.ichloroph€not
Surrogate r€cgveres:32160-8 2+tuotobiphenyt
7-124 2-Fluorophenol41 6!,6ILO Nitobenzene45416542-2 Phenol4strts-o|a Teffienyl4l4t1&7*6 L4,&Ttihtofllophenol
SW6,f6 827{rc n rat47 2+Mat47 7031279 M,B
1 SW8467471A 26.Mar$ 2l-irarfi 7031322 YP
1 EPA 200.7 26+td47 2741ar47 7031321 HB
I '
1 '
1 '
1 '
1 '
1 swe46 f312 22{d6147 ?']l[ar4T 7031344 BD'1 SW8461312160108 2 nat47 24-Mar47 7031408 LR
Z1|()-3+2 Arc€nic744on93 B€dum74{04$9 Cadmium
7,140-47-3 dlromium7€9.973 tbrcury74394+1 teadr/82492 S€tenium
Ce trerrl Chemlstry PrEmcteas
% Solids
Ugr'kg dry 21fi
udks dry s7
Udkgdry 547
ugkg d'y 2190p4kS dry 47gSlkS dry g7
ldrg dry 547pS4€ dry g7
US/kg dry 547pg,lgdry 547
udksdry s47
udks dry 547pdks d,y 547
UdkS dry 541pdks dry 547
tulm%16110 %30-130 %1+110%30-130 %trtt0 %
mglkgdry O.O3?3
nqtg dry 1 .'1 9
mdlgdry 1.78
hgr'kg dry 0.594
m€/kg dry 0-410
mdkS dry 0.594
rE/ks d.y 0.890
mgnqdry 1.7a
nEI 0.01m
rE/I O-015O
'ngn 0.0050
mgl 0.0025
mSn 0.0O5O
nrdl 0-m040
mgL/l 0.0075
mdl 0O15O
%
sw8461312|,4704
SWS46 13121160108
26-Mar-tY 781{0s YP
2{-l.i3r{7 7q}l.l0A LR
BRLBRLBRLBRL
BRLBRLBRfBRLBRLBRLBRL8RLBRLBRLBRL
8I)58
188977
Total Metrlr by EPA 6000/7000 S€ries Methods
743+975 Mefcun/ BRL
Totd M€rrb by EPA 20O Sed.s Mettods
7,{4G22r Silver
744G3&2 AFenic
744{}3$l Badum
7,1404+9 Cadmium
744047,3 (hromium
7€9€2-1 Lead
282-492 S€tenium
BRL
8.30
74.2
BRI-
7.93
BRL
SPLP M.Lh by EPA 1312 & 6001y70m Seri6 Methods
SPLP Exhadirn Compl€bd
7440-22-a Silv6r BRL
BRL
0 .0110
aRrBRL
BRL
BRL
BRL
80.3 SM2540GMod. 2UMar47 23+'tar47 7o3flm @
nhit lab$loA r@d b ,tat edu flirtout .n au{rotitd slg',ad . orr dt @er pag.,
'R€po.€ble h.ction Linit BRL = Below Reporring LiDir Pegc 16 of 124
Page 137
Sample IdcotificationM8F-4 2'-4'sA59464-01
Client Proiect #301-88
Collection Date/Timel5-Maf-07 00:00
MatrixSoil
Receivq!l9-Mar-07
CAS No. Analye(s) Resuk Fl"g Units *RDL Dilution Method ReJ, Prcpared Analr,zzd Bdlch Antbst
Volatile Organic Compo nds
VOC Ext actionVolalile Orqanic Comgounds
UdkS dry 4-7
lS^gdry 94_3
lsixs dry 4_7
lgks dry 1.7
tigiko dry 4.7
!g/kg dry 4.7pg/kg dry 4.7pSlkS dry 4.7
!S/kS dry 9.4pS/kg dry 47.2pS/kS dry 4.7pS/tS dry 4-7pg/Kg dry 4.7
!g/kg dry 23.6
,Jdhs d.y 1.7
lgkg dry 4.7
!g/kg dry 9.4pg/kg dry 4.7pq/kg dry 9.4pdkS dry 4.7pS/kS dry 1.7pdkS dry 9.4
fgkg dry 47
tsksdry 4.7pSnqdry 4.7
us/ks dry 4.7
rc/kg dry 4.7
ldkS dry 4.7pS/kS dry 9,4
UdkS dry 4-7pS/fS dry 4 7
uSn(S dry 4 7
udkgdry L7pg/kg dry 4_7
ldkS dry 4.7
lqkS dry 4.7
lglkg dry 4.7pSAg dry 4.7
US/kg dry 4.7
lSikS dry 4.7
ldkg dry 4-7pgkg dry 4.7
ttdkS dry 47.2
udkS dry 4.7
l||dkS dry 4.7
ldkg dry 4.7
ldks dry 47-2pgftgdry 47.2
US/kS dry 4.7
2GMar47 m+1afi7 7031156 BD
Prepared by melhod SWM6 5035A Soit (tow tevet)
76-13'1 |,1,2-Trichlorotriffuoroethane(FreoERL
67€4'1 Acefone BRL107-13-1 Acrytonitrile BRL7143-2 Benzene BRL10&G1 Bromobeozene BRL7447-5 Bromochloromethane BRL7s-274 eronodichloromethane BRL7s2+2 eromofom BRL74€3-9 Bromomethane BRL78-e3-3 2_Bubnone (MEK) 8RL104-51€ GButyJbenzene 8R{_13tsa€ Sec.Butylbenzene 8RL98{6{ tert-Eutylbenzene ARL/5-1+0 Carbon disulfide BRL56-23-5 Carbon tetrachloride BRL10&9G7 Chlorcbenzene BRL7s4+3 Chtoro€tEne BRL675e3 Chbroform BRLt4.97-3 Chbromethane BRL954$a 2_Chlorotoluene BRL106-43-4 ,4-Chlorctoluene BRL96'12'8 1,2-Dibromo-3-chlo.opropane BRL124-4{l-l oibrcmochlorcmehane BRL106-sr3-4 |,z-Oibromoethane(EOA) BRL7+913 Dibromomethane BRL
95-6G1 l,2-Dichlorcbenzene BRLar41-73r l,3_Dichtorobenzene BRL106-.46,7 l,4_Dichtorobenzene BRL15-7 1 4 Oichtorodif uoromethane (Freon12)BRL75-14-3 |,1-Drchloroethane 8RL107-06,2 l,2-Dicldoroethan€ BRL75-35-4 1,.1-Dichloroethen6 BRL1se59-2 Cis-1,2-0ichtoroethene 8RL15€40-5 trans- l ,2 -Oichloro€th€ne BRL7447-5 1,2-Dicl{oropropane BRL142-28-9 1,3-Dachloropropane BRL591-?!.7 2,2-Dic6lotop6lane ARL56's€s I,I -Dichloropropene BRL1m61-01-sCis-1,3-Dichloropfopene BRL10061{2€tEns-.1.3-Didlloropropene BRL10(|414 Ethylbenzene BRL8r€8-3 Hexachlorobutadiene BRL
591-78{ 2-HexarDne (MBK) BRL
9€{2-8 lsopfopylbenzene BRL
s€{76 4-tsopropyltoluene BRL
163.r{44 Methyt tert_butyl etl|er BRL108.10-1 4-Methyt-2-pentanone(MIBK) BRL75{S2 Methyleno chloride BRL
SW 846 82608 21-l at-O1 22-+,ta(o7 7031233 TR
BRLs1-2G3 Naphthalene
Page 3 of 152
Thb btorrtaq rcpofl is nol taIU *irhout tn autho.irerl sigaaturc o^ tha cover lmge.+ Rcportable Det€ction Limit BRL = Belo{'Reporting Limit
Page 138
Sample ldentil-lcntionMEF{ 2'-4'sA59464-01
Clieot Project #301-r8
Collection Date/TimeI 5-Mar47 00:00
MatrixSoil
Rec€ivedl9-Mar-07
CAS No- Aaalfta(s) Flae 'RDL Dilation Mdhod ReJ Paparcd /lnatad Bslch Analfst
Vohlile org.tric Corpoundr
Volalile Oroanic CoinpqundsPrepared by mehod SW8,{6 50354 Sdt (tow levet}1014+1 n-Prcp!'lb€nzene BRLr0G42-5 styrene BRL63,G206 1,1,1,2-T6hectoroetfEne BRL79-3L5 1,1,2,2-T€t-actdoro€hane BRL127.18-.r fet€drlorcellrene BRL108-84-3 Toluene BRL67616 l,2.S.Tdchlorobenzene BRLi21>82.i l,2.4Trlchlorobenzene BRL71.55€ 1,1.1-Trichloroethane BRL7$0G5 1,1,2-Tddlloroethane BRL79.01€ Tridtloroethen€ BRL7559-4 TricfiloroflUorornethane (61gon 111 BRL96n8-.1 1,2,&Trichboprop6ne BRL9S16 | ,2,,{-Tdm€thylbenzene BRL10&67{ l.3,tTrimedty'benzene BRL75{11 Vinyl cfiloride BRf1330-20-7 m,p-Xyl€rE BRL9547$ o-Xyl€n€ BRL10+99-9 Tet?hydrofuran BRL6t)-297 Ethyl ethe.s94{5{ Teft-dry'm€thytehef
fi7-92n Edryi ted-butyl eherr08-2G3 Di-isopropt e €r75€5{ Te.t-Blthnol / butyl alcohol12+91-l l,4oioxane
Surogate rccolr'€des:4a04o'4 +Bawttofluorcbenzene
toiT-26-5 Totuene4S
1 706041 4 1, 2 -Dhhloroethane-d4
186A-5?7 Abrcnof,uo@nethane
E raoLblo P€foleum HydrocrrboN
ExtEdable Tolal Peboleum tMrocarbon!.
Prepared by method S1V846 35508
8006-61-9 cas€line
6€a7F3c2 Fuet Oil #268a7G31-3 FustOit #4€8s5il-(B4 Fuet Oil #6iro90o000o Motor oil.jOOToOOOO Aviatid F@l
Unidenlified
ohe. Ol
BRLBRLBRLBRLBRLBRL
1N1041 1 7103
ldrSdry 4.7
ldko dry 4.7ygikS d.Y 4.7
udlq d.y 4.7
udkg dry 4.7
ldkS dry 4.7
ldtgdry 4.7pS4qdry 41
USikg dry 4.7pgl(gdry 4.7
lgtSdry 4.7
!Sn(S dry 1.7
l|gnls drv 4.7
FgtS d.y 4.7pdks dry 4.7
rdkS dry 4.7
UgkSdry 9,1
tr/kgdry 47
XCftg dry 17.2pdkgdry 4.7
tdl<S dt't 4 7
ldkS dry 4.1
FdkS dry 4.7
lgksdry 11.2
Lrgl(gdry 94.3
70-130 %70-130 %7&130%70,1n %
sW 845 82608 214tiat47 22-Mar47 7031233 TR
BRLARLARLBRLBRLBRL67.4Calqrlated as
msASdry 21.9mg,kg dry 21.9mdks dry 21.snE/kg dry 21.9mgkSdry 21.9drgr(rg d.y 21.9mgikg dry 21.9'ngr'kg dry 21.9dtdks dry 21.9mg/kg dry 21.9
40-t$ %
+CT ETPiI 21-Msr-07 2t-I.lar47 7031187 DS
TotalP€ElleumHydrocarbons 67.4C9C36AliphaticHydrocs.bo.ts 67.4
St,|rogate €coyerl?ri338&33-2 l-Chlomodadecane
Sejlivolldle Orgrdic Compo[trdr by CC
O.oanoafilorine P€stcides SW846 8081APrepared by m€rt€d sw846 355083Os-O0-2 AJd.in t'dtg dry SWE f6 80alA m.+'li,ato7 25*let47 703t06a TG
nirit l4br@ry ,qort iE "at
eolitt fthou an aartorid sigt dat ot, the coter INg..i RlporEble DetedioD Limit BRL = B€lol,v R€porting Limit Page 4 of 152
Page 139
Sample ldentificationMEF-4 2'-41sA59464-0r
Client Proiect #301 -88
MatrixSoil
Reccivedt9-Mar-07
Collection Date/Timel5-Mar{? 00:00
C,4S No. An ye(s) Flag Antus *RDL Dilution Method ReJ. Pnpared Aaallzed Botch Aru\st
Semivolrtile O.ganh Compounds by CC
Orcanodrlorine Pesticid€s SW846 8081A
Prepared by method SW846 3f508
319{4{ a_BHC31s5-7 b-BHC31+86-8 d-BHC58{s-e g_BHC {Lindane}s7-f4'9 Chlordanef2.s-6 a,4_DDD (p,p')72-ss-e 4,4_DDE (p,p.)so-2s-3 a,4_DDT (p,p.)60-57-1 Dietdrin95S-98{ Endosutfan I33213-65-S Endosutfan ll103147-8 Endosutfan Sulfatel2-2O-A Endrin742r,934 EndrinAldehyde1644 a Heptachtor7243-s Metlrcxychlor102a'57-3 Heptachtor Epoxide8001-3+2 Toxaphene5103-71-9 +Chlordane5566-34-7 g-Chlordane
534!14-10-5 €nddn Ketone
Sutogde rccoveries:103BFe+2 4,+DE-Octafluotobiphenyt (54
N51-2+X Decachlorohiphenri (Sr)
Polvchlodnated Eiohen!,ts by SW846 8082Prepared by method SWB46 3545A
12674 11,2 pCB 1016111o4-2v2 PCB 122111141-rE 6 PCB 12325346e-214 pc81242
12672-29€ PC8 1248110s7{9-1 pc81254
110ec€2-5 pcB 12603732+23-5 PCB 1262'r1100-11-4 PCB 1268
Sunogal€ /.cmv€nes:10386 842 4,4-DB-OctafluoroNphenyl (Sr)
2051-2+3 Oecachlotobipheny' (St)
S€mivolstile Organic Compounds by GCMS
BRL
BRLBRLBRLARL
8.208.7114.2BRLBRLBRLERLBRLBRLBRLBRLBRLBRLBRLBRLBRL
49103
SRLBRLBRLBRLBRLBRL21 .9BRL
BRL
4586
BRL8RL8RL8RLBRL
BRLBRLBRL
!g/Kg dry 5.93
Lidks dry 5.93
!g/l{9 dry 5-93
uglkg dry 5.93
us/ks dry 29.6
ldkS dry 5.93
!g/kg dry 5.S3
ldkg dry 5.93pdkS dry 5.93pSIq dry 5.S3pS/kS dry 5.S3pslks d'y 5.93pg/kg dry 5-S3
PgkS dry 5.93
l.rgks dry 5.93
lEkS dry 5.93
!S/kg dry 5.93
ldkS dry 29.6
!s/(s dry 5.93
t/gkS dry 5.93
ldkS dry 5-93
30-150 %30-150 %
UdkS dry 11.9
tig/ks d.y 11.9
t!91k9 d.y 11.9
ldkg dry 11.9
ldkS dry 11.9
!SI(S dry 1l.SpS/kS dry | 1.9pSlkS dry 11.9
FdkS dry 11.9
30150 %30-150 %
Ign(g dry 543
US/kS dry 543
ldkS dry 543pdkS dry 543psJkgdrt 543
!Sl(S dry g3
ps/ks dry 543
!94(S dry 54:]
1
1
1
1
1
1
1
1
1
1
1
I
I
I
l
I
1
1
1
1
sw846 8081A 20.Mar{7 25-L,lar47 7031068 TG
SW846 8082 21-M€F07 23-MaG07 7031181
SW8,r6 8270C 22-Mat47 244.t1et47 7031278 MB
Semivolatilo Oroanic Comoounds bv SW846 g27OC
Preparod by m€thod SW846 3SS0B8+32-9 Acenaphthene20e96{ Acenaphfiylene62-5+3 Aniline12012-7 AtltlxAcene1912-2+9 Al,raine10+33-3 Azobeozene/Diphenyldiatne92{7-5 Benzidine5C5+3 Benzo (a) antttaacene
This lahomtory reporl ir ttot voIU ttuuA dn 4rdtoried signsrure on the cove. Nge.i R+ortrble Detection Limit BRL = Below Reporting Linir Page 5 of 152
Page 140
Sample ldetrtificationM8F4 2,-{',sAs9.164-01
Clieot Pmiect #301-88
MatrixSoil
Collectiod Date/TimeI 5-Mar-07 00:00
Receiv€d19-Ma!-07
CAS NtL An4lftc(s) Result Fl4E Unia |RDL Dilutiot Mahod Retr Prcpated Adsltzztl Botch 'lnalfs,
Semivolatile Organic Comlnlrds by CCMS
Semivdatle Orqanic Compounds bv SW846 8270CPrepared by melhod SV\t846 355085{L32{ Benzo (a)pyreaemS99-2 Benzo (b) ffuoranth€neisr-24-2 Benzo (g,h,i) p€rylene20748€ BeMo (k) fluo.anthene65€$0 Benzoic acid,0G51{ Benzyl alcohol111'91r Elis(2-cft loroethory)rn€tnanei1tr4-. Bis(2drtoroethyl)eh€t3963e32{ 8is(2-{trh.oisop.opyt)€lher1174t-7 Bis(2-etryihexyl)phtElate101.Sr5-3 +B@mophenylphenylether05€8.7 BuVbenzytphtElate8B-71-a Carbazole5e-50-7,t-chtom-3-methytphenol106474 4-Chlooanilin€91-s&7 2-Chloronaphthetene9+57€ 2-Chlorophenol7005-72'3 +Chlotrophenyl ph€nytethet2r${14 Chrys€ne5!7G3 Dib€nzo (s,h) anthracene132+l-9 Oibenzofuran95-5Gl 1,2-oichtorobenzen6541-73-1 1,3-DichlorobefEene106-1&7 l,+Dichlorobenzene91€+1 3,3'-Dichlorobenzidine1?0-ar-2 2,4-Didrlorophenol84SG2 Di€hytphthalate13r-11-3 Dinrethyl pfithalatei05F6?-9 ?,+Oime$rytphenol&4-74-2 fx-niutylphthatate$4-s2n 4,6-Dinit'o-2{n€Uryloenol51-2&s 2,4-Dinitrophsnol121-i4.2 214-t)inibototuene606-2().2 2,eDinitEtoluene117€4-0 DLn-OdMp,hthstatem6-{44 Ffuoranhen€&f+7 Fluoreoe11874-1 Hexadrlorcb€nzene87€&3 l-lexachlorobutsdien€n47-1 Hexachlorocfdopentadiene67-r?-t H€xaafitoaoetlEn€19!3+5 Indeno (1,?,3-cd) pyrene90.t2{ l-M€fiyloaphthatene786+1 lsophororE91-57{ 2-Methylnaphhalenee5-{+? 2-ltedryiPh€nolt0&39-{. 3,+Me0rytphenolr06-44-69t-2G3 Naphthalene08-144 2-Nihoanilin€99{+2 }Nitroanilane
SW8,f6 827(rc 2]lns47 U4ld47 7031278 M.BBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRLBRI-BRLBRLBRL
8RLBRfBRLBRLARLBRLBRLBRL
BRLBRL8RL
BRI.
BRTERL
t4il€ dry 5.lA
!g/kS dry Yg
lJgkg dry 543
lgkS dry 543
UdkS dry 543
t,g/ko dry 543
ldtg dry 543
Psrksdrv 543
UdlqS dry 54i)
ldkS dry 543pdko dry 543
US/kSdry 543
Fdkgdry 543
Fdkg dry 543
ldkg dry 543
WkS dry 543
rc/kS dry 543pgl(gdry 54:,
ldtsdry 54:l
UdkSdry 543
tdkS dry 543pgks dry 543
lrdlS dry 543
ldkS dry S43
rdkg dry 543
lgr'Xg dry 543
UdtSdry At3pgrsdry 543
Ug,l€ drt 543
lgkgdry 543pgks d.y 543
uSikg dry 543
Fgl*gdry 543
lidkS dry tl3
|,9n€ dry 543
t Sikg d.y 543
UdtS dry 543pdkg dry g3
ldkS dry 543
Idllg dry $43
rsrtgdry 543
rsaSdry 543
Fdkg dry 543
ldkSdry 543
Udkgdry 543
Fdkgdry 543
ldtSdry 543
FdkS dryugkg dry||gikg d.y
t4:]
5439t3
Thit lab.ohrf Epott b ,et wlid tellhost .tt auLorizcd sEn@trc on ahe coter poge.
+ RQorbble Delection Limir BRL = B€tow Repqting Limit Pegc 6 af t5?
Page 141
Sample IdentihcationM8F-4 2'-,1'sn.594&-01
Client Proicd #101_88
Matrl{Soi l
Receivedl9-Mar-07
Collection Date/Timel5-Mar-07 00:00
cAs No. Anautz(s) ftesull FIag Uaits *RDL Dil,/tion lwethod ReJ. PEprrcd AruIWd Balch Analpt
Semilolalile Organic ComFounds by CCMS
S6mivolatile Ofoanic Cornpounds bv SW846 B2ZOCPrepared by method SW846 35508
100{14 4-Nitrc6nitine3€-95-3 Natrobenzenem-75,5 2_NitrophenolloGoz 7 4-Nitro,phenol62-7+s N-Nitrosodimethylamine621-84-7 N_Nilrosodi-n_propylamanea63o-6 N-Nitrosodiphenylamine87{SS pentachlorophenol
85418 PhenEnthrene10s,95-2 Phenol129-m4 pyren€
11G86-1 pyridine
120-82-1 1,2,+Trichlorobonzene95-954 2,4,tTrichlorophenol8arl6-2 2,4,GTric+rtorophenol
SurrDgal€ r€coy€aes:321-@-a 2-Fluor&iphenyl
367-124 2-Fluorophenol
4165404 Mrcbenzene4s
416u62-2 Phenot4s
1718-St4 Terykenyl4l4
118-79-6 2,4,6-Tnbtumophenol
1
1
1
1
1
1
1
1
I
I'|'|
1
1
1
I SwE46 74714 23-MarO7 26-Mar47 7031306 YP
EPA200.7 23-MaF07 24-l\,4ar{7 7031305 HA
SPLP Extraction
74a{l?24 Sitvef
744034-2 Ans€nic
7440393 Barium
7410-4!9 Cadmium
744G47-3 Chromium
743F97€ Mercury
7439€2-1 Lead
7782-4+2 SelenaiJm
C€neral Cbemistry PNrumeters
% Solids
!g/kg dry 2170pg/kg dry 543
t/g/r(g dry 543
UdkS dry 2170
!g/kS d.y 543
rg/kg dry 543
t Sikg dry 543pgkS dry 543pg/Xg dry 543
!S/kg dry 543
PgKg dry 543
lgkS dry 543
ldkS dry 543pS/& dry 543pdkS dry t13
3Gt 30 %15,110 %30-130 %1Ut10 %3&t 30 %t5-110 %
nrg/to dry 0.0341
rYE/kS dry 1.O2
mgkS dry 1-52
msftg dry 0.508
frEikg dry 0.254
ndkS dry 0.508
rYE/t(S dry 1 02
lwkS dry 1.52
nEn 0.0100
nEn 0.0150
mgl 0.0050
mgn 0.0025
nE/l 0.0050
nEn 0 0{040
rngil 0.0075
mSn 0.0150
%
BRLBRLBRLARLBRL
8RL8RL8RLBRL8RLBRL
BRLBRLBRLBRL
7662
598375
'| otrl Metlls by fPA 6000/7000 Serier Methods
743$9rc l\rercury
Totrl ltetrb by EPA 200 Serirs Mrftortt
7440-22-4 Sitver
lr4o-382 Arsenic
74.10-39,3 Badum
7440.43-9 Cadmium
7.{{047-3 Chromium
7439-92r Lead
282-4$2 Selenium
SPLP Metals by EPA 1312 & 6000fl000 Sertes M.thods
0.158
BRL
9.90
52.4
1 . 1 9
26.2
176
BRL
Completed
BRL
BRL
0.0120
BRL
0.0122
BRL
0.0217
BRL
81.7
I SW8461312 211,ttar07 21-MEt47 7031229 BD
1 SW846131260108 22-MarO7 24-Mat-O7 7031323 LR
1 "
t "
1 "
1 SW84613127470A ' 23-lii€147 7031324 yp
'l SW846131260108 ' 24-[4ar{7 7031323 LR
1 '
1 SM2540 G Mod. 22-Mat47 22-Met47 7031307 YM
This taborqloqt ftpn ls ^olecla *ithaua an oatho.ateC sign,'lure onthe coltar page.
{ Reportable Det€ctior Limir BRL = Below Reforting Limit Page 7 of 152
Page 142
Samole IdentihcationM8F-s 2'-4'sA594#1-02
Client Proiect #301-88
MatrixSoil
Collectiop Data/Timel5-Mar-0? 00:00
Receiv€dl9-Mar-07
CAS No. Anrlyte(s) Resall Flag Aaia *RDL Dlhnion Melhod R.J PEpaled Arralfzld Aafth Anzltst
Volrtile Orgrnit Com!'oundr
VOC ExtractionVolatle Orqanic Comoounds
pdrg dry s.3
lgv€dry 105
Ug/tg dry 5.3
Udkg dry s.3
tr9/k0 dry 5.3
liS4qdry 5.3pSrkS dry 5.3
lgrgdry 5.3
!g/kg dry 10.5
ttglkgdty 52.6pdlq dry 5.3
tdkgdry 5.3
FS/tgd.y s3pCASdry 26.3pgxgdry 5.3
!SI(g dry 5.3
rcftg dry 10.5
la/kS dry 5.3
usAodry 10.5pdks dry 5.3
lgl(g dry 5.3
|lgI(S dry 10.5
Igkg dry 5.3
t S/kS dry 5-3
Idkg d.y 5.3
USftSdry 5.3
lgksdry 5.3
ldxS dry s.3
rcIqC dry 10.5
ug,l€ dry 5.3pg/ko dry 5.3
rdkg d,y 5.3pgtSdry 5.3
lg/lqg dry 5.3
FdkS dry 5.3p9/€ dry 5.3pdkS dry 5.3
lgkSdry s.3pSASdry 5.3pglqdry 5.3
US/kgdry 5.3
USI(S dry 5.3
rc4q d.y 52.6
lSilg dry 5.3
lSikgdry 5.3pgls dry 5.3
ldkSdry 52.6
ldkS dry 52.6
IdkS d.y 5.3
2o-[,lar47 2o-Marfi 7031156 BDField ext"acted
ftepared by mehod SW8,l6 5035A Soil (low levsl)76-1$1 1,1,2-lricfilorotriffuoroethene(FreoERl_67{+1 Acetona sRL107-13-1 Acrylonitib BRt_714}2 Benzen€ BRL108{G1 Btonobsnz€ne BRL7+97-5 BtoriochloronEthane BRL7r2f1 BrodEdictlloromethane BRLf5-zuz Bromobfm BRL71419 Brcmohelhane SRL7&913 2-Bubnone(MEK) BRL104-514 n-Butylbenzen€ BRLi35-96-€ sec-Butylbenz€ne BRL9a{6{ tert€Utylbenzen€ BRL7t15-0 C€rbon disutfde 8RL5G235 Carbon tefachlorid€ BRL'10&90.7 Chlofob€rEefle BRL75{0-3 Chlo@othane BRL67{+3 C o.ofonn BRL741?-3 Chlorornethane BRL95-49{ 2-Chlorototuene SRL106-434 +Chlorotolu€ne gRL
!a't2€ 1,2-Dibrorno-3dtloropaopan€ ARL124-44-1 Dibrornodllorom€thane BRLt0ce3-1 l,2-Ofrfomoehane (EDB) BRL7+95-3 Dibmmomelhane BRL95-SO-1 i.z-Dichlorobenzene BRL411.73-1 i,3-Dichlorob€nzene BRL10re-7 |,4-Diohlorob€nzefle BRL75-71€ Dicitorodinuoromethane (Freonj2)BRL75-3rl-3 'l,l-Dichloaoethane BRL107.06-2 1,2-Dichlo{oethane BRL7t35-4 1, t-Dichloroethene BRL15+5*2 d!-1,2-Dichloroetheoe BRL15€-60.5 lrans-'1,2-Dichloroethene BRL7&.47.s 1,2-Dichloropr@ane 8RLi42-2E'9 1,3-DicHo,opropane BRL.re4-207 2,2-Dichlo.oprop6ne BRL4|615&6 1,1-Dichloropropene BRL10{r€1{1{ ds-1,3-Dichloropopene BRLi006i{2€tlans-1,3-Dichloroprop€ne BRLt00-41-4 Ehy{b€nzene BRL876&3 Hexed*rrobutadiene BRL4,91-78{ 2-Ho6none(MBK) BRL98{2-a lsoproptb€nzene aRL99{7{ +lsopropyttoluene BRL1634{1--{ iledryl tert-bulyt edler BRIloelo.i +Metht't.2fentanone(Ml8K) BRr75{9-2 Methylene chtoride BRL
SW 846 82608 2l-Mar47 224a147 7031233 TR
91-?G3 Naphlhalene
P{ge 8 of 152
Thi! laborzto.f.qoi is not valAl wllhoet an a.tdrati@4 sigEate oa dr2 cowr IMge.. R€portable Dck{rion Limit BRL = Below R@orting Limir
Page 143
Sample [deotificationM8F-5 2'-4's459464-02
Client Proiect #301 -88
MatrixSoil
Receivedl9-Mar-07
Collection Date/Timel5-Mar-07 00:00
CAS No. Analrfu(s) Resull Floe a n s *RDL Dilation Method ReJ Prcparcd Analttzed Balch Anallst
Vohtlle Orgrnic Compounds
Volatile Oroanic ComooundsPrepared by method SW846 50354 Soil (tow lever)
BRLBRLBRLBRL
BRLBRLBRLBRLBRLBRL
7559-4 TrichlQrofluoromethane (Freon 1t) BRL
103{5-1 n-Propylbenzene10H25 Styrene630-20€ 1,1,1,2-Tetrachlor€thaneT9-34-5 1 , 1 ,2,2-Tetrachloroethane12H6-4 Tet€d{oro€thene1$.€a-3 TOlUene47s16 1,2,3-Trichtorobenzene120€21 'l,2,+Trichlorobenzen€
71 s5 6 1,1 ,l-Trichloroethen€79{0 5 1,1 ,2-fticttlo.oethene7s{1-6 Tdchloroethene
SW 846 82608 21-Ma.-O7 22-MaG07 7031233 TR
+CT ETPH 21-Ma(47 21'!lar07 7031'167 DS
{1618-4 1,2,}Trichtoaopropane
95{3{ 1,2,4-Trimethylbenzene
108{7+ 1,3,5-Trjmethy,benzene15414 Vinylchlorider33O-2G7 m,p_Xylene95474 o-Xylene
109993 Tekahydrofuran
60-23-7 Ethytether
991H15€ Tert-atnytm€thytether637-923 Ethylted_bstytether108-20-3 Di-isopropyleher75€s-0 Tert-Butanol/butylatcohol12991r '1,4-Diorane
Surragalg recovaties:46040-4 +Bromofluorcbenzene
2037 26-5 Toluen*d8
1 f o6Go t 4 1,2-Dichloroelhene<!4
1a68-5x7 Abromofluorcmethane
Extrrctrble Petroleum Hydroc.rbons
Extractable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
800641-9 Gasoline6847e30-2 Fuet OiJ #?6847S31-3 Fuet Oil#46855!09 Fuel Oil t[6M0980m00 Motor OilJ00100000 Avialion Fuel
unidentified
Otr|€r Oil
Total Petroleum Hydroc€rbons
C9-C36 Aliphatic Hydrocarbons
Suaogale recoyehies:
$e6-33-Z l-Chloroocledecene
S€mivolrtite Orgrnic Comporrds by cC
Oroanochlorine Pesticides Svry'846 8081A
Prepared by method SW846 35508
3OS-00-2 Aldrin
BRLBRLBRLBRLBRLBRLBRIBRLARLBRLBRLBRLBRL
88101102110
BRLBRLBRLBRLCElorlat€d as8RL251BRL251251
!g/ks drypgkg dry
lgts dry
ldks dry
tt4k9 dry
tidkg dry
Fgftg dry
tiSlq dry
FSnq drypgtks dry
lSftS dry
lSftS dry
US,kS dry
ldks dry
I!9*.S dry
lgftS dry
lgftS drypg/kg drypgKg dry
!s/ks dry
ldks d.y
lEkg dry
wks drypg/kg dry
trSlkS dry
5.35.3
5.35.3
5.35.35.35.310.55.352_65.3
5 352.6105
70-130 %70'130 %7G130 %70-130 %
mgLi kq drymgkg drymdks dryrYEAg drynEftg dryms/kg drynE^g drymdkg drymdkg drymgn(g dry
24.1
24_1
24.1
21_1
24-1
24_1
24.1
24.1
24.1
24.1
40-140 %
ldKs dry SW8{6 8081A 20'ti,lar47 25+lar{7 7031068 TG
This labo&bry rcpod k not Jelid ilithout en oalhorivd signatarc dE lhc aver page.
'Reptrhbl€ D€tection Limit BRI= Below Reporting Limit Page 9 of 152
Page 144
Sample IdcntificationM8F-51'-4'sA5946442
Client Proi€ct #301-88
Collection Dare/Time1 5-Mar-07 00:00
MatrixSoil
R€ceivedl9-Mar{7
CAS No, Analye(s) Floc 'RDL Dilution Llahon Retr, Prcpee Aazlyat Batt Aa44s1
Semivohttle Orgatric Compodtrds by GC
O.oanocfilo.ine P€sticides SW846 8081APrepared by me6od SW846 35508
319++€ a-BHC3t9€5-7 b-BHC319-864 4BHC58499 gFBHC (Undane)57-7+9 Chlordanen-544 a,ADDo (p,p')72.s+s 4,+DDE (p,p.)5&i'+3 4,+DDT (p.p,)EilL57-1 Diohrin95+9€{ Endosulfan I3321165.9 Endosultan ll103147'8 Endbgullan Sultatle
742143-4 EndrinAtdehtdo7644-a Heptachlor7243-5 Metlorychlori0?4s7.3 H€9tacHor Epoxlde8001+tz Toxaph€ne5103-71-9 a4hbrdanefi566-34.7 g-Chtordan€s349rL?G5 Enddn Kelong
surDgata tecolldrrbsj103e64+2 44-Dg-Odan@robiphenyt ( Sr)20s1-213 Ddcachlotobiphenyl (Sr)
Potvchlodnaled B-rohenvls bv SW8,td 8082Preparcd by method SW8il6 3545A12674,1r-2 PC81016111O1?l-2 PCB 1221i1141-16-5 PCB t232536e21-9 PCE t24212672-2s{ PCg 124811097{e-1 PCB 12541i096+2-s PCB.t2603732+23.s rcB 126?1110G14-4 PCB 1268
Ssnqg€le a€coFrigs:1 03E04+2 4, 4ae-Octafl @robiphenyl (Sr)mstu-3 Docechlorcbipheny, (St)
Sesivolrtile Org.nic Compoutrds by mMSSemivolatile Omanic Comoounds bv SW846 827(rcPrepa.ed by method SW846 355088332{ Acenapht}Eno2O&S{ Acenaphthyteng6a-5}3 Anllne12Gi2-7 Allhrac€ne19r?-21L9 At?inei0!33+ Azobenz€ne/Dphenytdiatnes2€ru Bertzidin€s6-5$3 BerEo (a) anhrec€ne
sw846 80814 2{}i,lar-07 2s.fvlar{7 7fi1106a TG
SW846 8082 21][trat47 23 td47 703116/
sw846 6270C 2:$d47 2{-Mat47 7031278 M.A
BRLBRLSRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL8RLBRLBRLBRLBRL
44
BRLBRLBRLBRLBRLBRL39,9BRLBRL
45
BRLBRLBRLARLBRLBRLBR!BRL
Udl(g dry s.87
Ws dtv 5.87
ldks dry 5.Alpg[r(gdry 587
lgrs dry 29.3
$slksdry 53?
UdkS dry 5.87
rdkg dry 5.87
ldkg dry s.87pgl(g dry 5.87
ldkS dry s.87
UdkS dry 5 87
ldkS dry 5 87pdkg dry 5.87pdko dry 5.87pEtg dry 5 87
lrdkgdry 5.87pg/Ig dry 29-3
USI(S dry 5.87
UgkSdrY 5.67
lSfts dry 5.87
30-1fi %30-154 %
wrxg dry . . 11 .7
USAS dry 11.7
Ugr'*O dry 11.7
ldlS dry 11 7pgkC dry 11.7
uS/kg dry r1.7
t Sftg dry r1.7
ISrkg dry 11.7pg/tg dlt 11-7
30-150 %3G150 %
FdkS dry 597
usftgdry 597g/kodry 5s?
FS/kg d.y 597pdts dry 5€7pgkgdry 507
Ugn(g dry 597
tglkgdry 597
fhb bborubry npod b ,et ttdli.I tsidrold ott oa&ortzed sigdafur? on d,e @va poge.
* Reportable Detecriotr Limit BRL = Below R?orting Linir Page l0 of 152
Page 145
Sample IdentificationM8F-5 2'-4'
sA59464-02
Client Proiect #301-88
MatrixSoil
CoLlection Date/TimeI 5-Mar-{)7 00i00
Receivedl9-MaG07
C''lS No. Analr,e(s) Fldq 'RDL Dilatian Mdhod Rel. Pnparcd Analyed Ealch Anebst
Scmivolrtilc Orgrnic Compoundr by CCMS
Sernivolatile Oroanic Comoounds bv SW846 8270C
Prepared by method SW846 35508
Q-32-s BEtEo (a) pyrcne20+9s-2 Benzo {b) fluoranthene1s1-24-2 B€nzo (g,h,i) pefylene207-0€-9 Benzo {k) fluo.antfEne65-85-0 B€nzoic acid100-51€ B€nzylalcohol111-91-1 Bis(2_chloroethoxy)methane111<4-4 Bis(2_chloroethyl)eher3963&32-e Bis(2-chlofoisopopyl)ether117{1-7 Bis(2€ft,rytheryt)phthatate101-55-3 +Brornophenylphenylether
85-6+7 Butylbenzylphthalate86-748 Carbazole59-5G7 4_Chtoro_lmethylphenol106{{ +Chtoroanitines1-5&7 2-Chloronaphtrabne95-57{ 2_Chlorophenol7005-72-3 +Chlorophenylphenytether2r8-O1-9 Chrysene53-7G3 Dibenzo(a,h)anthrecen€1325{,9 Oibenzofuranssa5Gl 1,2_Dichlombenzene541-t3-1 1,3-Dichlorobenzene10646,7 1,4-Dichlorobenzenes1€4,1 3,3_Dichtorob€nzidine120+3,2 2,4-Dichtorophenol8446 2 Oiehyt phlhatate
131-11-3 Oimethylphthalate10+679 2,4-Dimethylphenplu-74-2 D_n_butylphthajales34-52r 4,6_Dinitro-2_methytphenol51-2€-5 2,4-Dinilrophenol121 14 2 2,4-Dinitrotoluene606-202 2,6-Dinitrotoluene111444 Dij:,4dyl phhatate
206-444 Fluoranlhene6-TVI Fluorener18-74r Hexachtorobenzene8740-3 Hexactorobutadiene17474 Hexachlorocyclopentadlene6T-12-1 Hexachloroethane1e3-3e-5 Indeno (1,2,3_cd) pyren€
s0-1?{ 1-Methylnaphthalene78{91 lsophorones1{rc 2.Melhy{naphthalene95-48-7 2-Methylphenol
100-39-4, 3,4-lt4ethylphenol106{4-591-20-3 Naphthatene0a-74-4 2-Njlroaniiine99{S-2 3-Nitroanitine
BRLBRLBRLBRLBRL
8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL8RLBRL8RLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
tdksdry 597
ldks dry 597ps/ks dry 5s7
IdkS dry 507
rdks dry 597
IS/kg dry 597
Ig/kg dry 597
rdks dry 87
[dkS dry 5S7
US/kS dry 597
uS/kg dry 597
IgkS dry 597
uS/kS dry 597
Udkg dry 597
tiS/kS dry 597
!94!g dry 597
Lrg/ks dry 597
ldkg dry 597
ldks dry 597
!S/kg dry 597
!Sn(S dry 5S7
ldkS dry 597
!g/kg dry 597
!g/kg dry 597
!g/kg dry 597
!S/kS dry 597
Fqkg dry 597pgks dry 597
!SI(S dry 5S7
lSftS dry 5S7
USftS dry 597
rc/kS dry 597
rc/tS dry 5S7
!S/kg dry 597pSlkSdry 557pS/rc dry 597
t S/kS dry 597
Udko dry 5S7
ugnlg dry 597
Vskgdtt 597
!S/tS dry 597
!Sn(g dry 5S7
FdkS dry 597
ldkS dry 5s7pgks dry 597
FqkS dry 597
lgks dry 597
uqkgdry 597
Wkgdry 597pS/kS dry 557
SW&46 827OC 22-Ma(07 24-Mar47 7031278 MA
Thb laborotory rcpod is nal wli.l toithout on arahorired signrtare on the corer page.
* Reporiable Deteation Limit BRI = Below ReoortiEs Limir Page I I of 152
Page 146
Sampl€ [dentihcatiodMrF-s 2'-4'sA59464-02
Client Proiect #l0l -88
MatrixSoil
Collection Date/Timel5-Mar47 00:00
Rec€ivedl9-Mar-0?
CAS No. Arralfuk) Rcsuk FI"t *R.DL Dilution Methad Rel, Prepand AnaflEed Balch Attzlrst
Semlvoletile Org.ni€ Cotrrpo{nd! by GCMS
Semivo{atil€ Oroanic Compounds bv SW846 8270C
Prepared by method SW846 35508ro(}or{ 4Niro6nilirE{l&95-3 Nitrobenzone8S75-5 2-Nboph€nol100{2-7 +NitEpheflol€A-7Ss N-Nitrcsodi.nethylamine621{4-7 l$Nih6odi-nfropylamine88i10$ N-NitEeodiphanytamirE87€45 Pentac+llorophonolE5{14 Phenanthrene10&9+2 Phefiol!29{04 Pyreneil{}s&1 FlrUino12G@-r 1,2,4Tdcl{o.obenzene95.954 2,4,STdchtorophonol86{$2 2,4,GTricfilorophenol
Sttnogale dcoveies:afio-g 2+luq6wenrdfir-121 2+fuoropltqol1lf,!,e4 |tilrohenzene45116552-2 Phend4s171&514 TerpheryI4l411$79.6 2,4,6-Trb.omophenol
1 sW846 8270C ?2-Mat47 244nat47 7031278 M.B
1 '
t '
l "
1 '
1 '
1 "
1 "
1 '
1 '
1 ' ,
l '
I SraJ846 7471A 23-0/ta(-07 26'trta(-07 70313ffi YP
1 EPA 200.7 z3-Met47 24-Mar47 7031305 HS
1 '
I '
1 "
1 '
1 SW8,{61312 21-Mar47 214a.47 703129 BD
1 SW846131260108 22-ltar47 2X tat47 70313?3 LR
1 ' ,
8RLBRLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRI-
BRI'BRL
8063
1588
t gkg dry 2390
t dko dry 597pgrtSdry 597
ldl(g dry 2390
ldkdry s97
ugkSdry s97
US/kSdry 5S?
ldkgd.y s97
Fqrcdry s97
ldkgdry 507
r€l/kS dry 597pdkg dry 597
t€ikg d.y 597pg/kg dry 597
ldtg dry |87
30-130 %15-110 %il-130 %t *110 %30-130 %lU I tO%
nryrg dry 0.0340
nE/kg dry 1.05
mgftg dry |.57
n'gkS dry 0.524
mdks dry 0.262
mglkg d.y O.5
m€L/kg dry 1.05
n|g/kS dry |.57
mg/] 0.0100
mgl 0.0150
nEn 0-&)50
mgr'I 0.0025
mSn 0.0050
mgLI 0.00040
mSI 0.0075
odl 0.0150
%
I '
1 '
1 SW8461312r|470A
1 SW84€ 1312/@'t0B
1 '
23+r€r-07 7031324 yp
23Mar{7 7031323 LR
74eU1 Sibel
7440-38-2 AE€nic
?{40'33.3 Earium
?,t4Gals Cadmium
1|{}47.3 Chromium
743€F92n Le€d
Ir82-492 S€bdum
Totrl M€trk by EPA 600u7000 serl€3 M€rhod!
74399rc Me&rry 0.190
To.rl Met{b by f,PA 200 Series Methodt
BRL
14.4
53_6
1.68
25.O
BRL
SPLP M€trl! by EPA l3l2 & 50{0n000 S€rtes Meahods
SPLP Extraction Compleled
71,40-?2-1' Situet BRL
744t!3&2 AFenic BRL
744039-3 B6dum 0.0170
r!s)-43-9 C€dmium BRL
7.rlo-47-3 Chrcmiurh 0.0i0S
7,138-97-6 Mercury BRL
7€9€2n Lead 0-0507
Zg2-4s2 S€l€nium BRL
Ccrctrl ChcDirtiJ Prrrmet€r!
SM254 G Mod. ?,{at47 2-Md47 703 1 307 YM% Solids
Page l2 of I J2
Thl| Iabonlory qn t is rrot vdid ei&ott.a aulhott1rtr signararc oa the oter page.
'R€porfibl€ DetectioE Limit BRI = Below Repo.tinS Limir
Page 147
Samp[€ IdentificationM8F{ 2'-{'sA59464-03
Client Project #301 -88
Collection Date/Timel5-Mar{7 00r00
MatrixSoil
Receivedl9-Mar-07
CAS No. ,4n4te(s) Fl"C *RDL Dilutio,, ,[ethod Rel. Prcpued Aadyei Bolch Adaljst
Volatile Oigrnic Comp,orndr
VOC Extraction
!g/kg dry 5_8
!sn(S dry 116
ugKg dry 5.8
lgKs dry 5.8
tg/Kg dry 5.8
!g/kg dry 5 8
uglkg dry 5 8
!g/kg dry 5.8yg/xg dry 1r.6
FyKg dry 57_9
Ug/kS dry 5.8ygkS dry 5.8
Ug/rcdry 5.8pgrc d.y 29 0pgkS dry 5.8pdkS dry 5.8
UdkS dry 11.6pSftS dry 5.8
lgkS dry 11.6
lgkS dry 5.8
HqkS dry 5.8
lqks dry 11.6
Fgfl(g dry 5.8
Ltglkgdry tE
ldkS dry 5.8pdks dry 5.Apg/kS dry 5-8pS/kg dry 5-8pdkedry 11.6
!S,&S dry 5-S
!94(g dry 5.8
fgkS dry 5.8
tS/kS dry 5.8
lglqdry 5.8
ldkS dry 5.8pdkS dry 5.8
ldkS dry 5.6psAS dry 5.8pdks dry 5.6
PgkS dry 5.8
PS&S dry 5.8pSn(g dry 5.8
Ug'l(gdry 57.9
USftS dry 5.8
UdkS dry 5.0
USAS dry 5.8
ugkg dry 57.9pS/kg dry 57.9
ISAS dry 5.8
20-1,/aF07 20-Mar-07 7031156 BDField erhectedVolatile Orqanic ComDounds
Prepared by method SW846 5035A Soii (torv tevet)
76-11-1 1,l,2,Tdchlorotrifluoro€thene(FreoBRL674-j Acetone BRL107'13-1 Acrylonitrile BRL714+2 Benzene ARL10s{6-1 gromobenzene BRL74'9r'5 Bromochloromethane BRLr5-2t4 Brornodichloromethane BRL15-212 Bromofofin BRLz4{3-9 Bromomethane BRL70-9!3 2-Butanone (MEK) BRL104-51{ n-Butytbenzene gRL
13+9€{ sec-Butylbenz€ne BRL9€{6s tert_Butylbenzene BRL75-154 Carbon disutfide BRL56'23'5 Carbon tetrachloride BRL104-90-7 Chtofobenzene BRL?5-00-3 chtoroetfEne BRL674$3 Chloroform BRL74i'-3 Chtoromehane BRL95-49-a 2-Chlorototuene BRL1oe-43-4 +Chlorctoluene BRLs6-12-a 1,2-Dibronro-3-chtoropropane ARL124{a-1 Dibrcmochlo.omeflane BRL10F93-4 t,2,Dibrornoethane(EDB) BRL74-9$3 Dibromomethane BRL95-50-1 l,2-Dichlorobenzene ARL5.1173-1 l,lDichtorobenzene BRL106-46-7 1,4_Dichlorobenzene BRL75-7 1 -g Dictrlirrodifluoromethan€ (Freonl 2IERL75-3zl-! 1 ,l-Dichtoroethane BRL107.06,2 1,2_Dichtoroethan€ ARL75-35-4 1.l-Oichloroethen€ BRL15F5+? cis-1,2-Dichloroethene ARL156{0.5 taans-1.2-Oichloroethene ARL78s7-5 1,2_Oichtoropropane BRL142 ?8-9 j,3-Dichtoroprop€ne BRLss4-20-7 2,2-Dichtoropropene SRLs63585 1,l-Dichloroprop€ne BRL1o061{1.s cjs- l,3.Dichloropropene BRL10061-02€ trans-l,lDichtoroprop€ne BRL100-41-4 Ehylbenz€ne BRLB76E-3 Hexachlorobutadien€ BRL141-78{ 2-Hexanone (MBK} BRL9€{2{ tsopropytbenzene BRL99{7+ zl-lsopropyftoluene BRL16349a'4 Methyt tert-butyt elher BRL108-10-1 4-l\,lethyl-2.pentanone{M|BK) BRL7s-o92 Methytene chtoride BRL
1
I
1
I
1
1
1
1
1
1
I
1
1
1
1'I
I
1
1
1
1
1
I
1
1'|I
I
1
1
1
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1
1
1,1
1
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1
1
1
1
1
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1
1
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SW8468m0B 21-Mat47 22 naFO7 7031233 TR
BRL91-2C3 Mphthalene
Page 13 of 152
Tht lohoratoe rcW is aot wlitl toithou ttn 4athori1ad sigtature on rhz cowr palc -
* Reportable Detection Limit BRL = Below Reporring Limir
Page 148
Sample ldeptificationMEFS 2'-{,sA59464{3
Clieot Projgct #l0l-88
MatrixSoil
Receivedl9-Mar-07
Collertio'$ Dat€/Timel5-Mar47 00:00
CAS No. Anatrte(s) Resuh Fhc *RDL lxlulloa Mdhott Rel. Prepsred Analfzed Borch Aialfst
Vohlite Orgonlc Com0o{trdi
Volat-.b Oroanic ComooundsPrepared by melhod SW846 5035A Soil (ton, levet)io3{tr n_ftopytbenzgne BRL100-42-5 Styrene 8RL63020{ i,1,|,2-Tehsd om€thffe BRL79-3+5 1, 1,2,2-Teb'6chloro€thane BRL127-1E{ Teha.hloroethene 8RLroSje{ Toluene BRLA?€15 l,2,3-Trid orobenz€ne aRLi2G82-l 1,2,+Trichlofobenz€ne BRL71-55-€ 1,1,1-Trid,toroethan€ BRL79oG5 1,1,2_Triatrtoroethan€ BRL79416 TdchloroettEne BRL7si9-4 Tidllorofiuoronethane (Freon fi) BRL{,6-16-4 l,2.S.Trict oropropane BRL95-€3-6 l,2,,fTdm€thytbenzene BRL108-67{ I,3,5-Trimeflrytbenzen€ BRl-?s{14 Vint ctllodde1330-Z+7 |TlFFXyle{1e95-47{ o-Xylene1099€-9 T€trahydrafuran60-2S7 E8ryl elhergs4-Otr Tert-dnytmethylether637-92J Etry t€Nt_butyt ether10&20-3 Diisopropyteti€r7tr5-o Tert€utanol / butyl alcohol123.91J 1,4obxane
St rmgaie tecowrnrs--461,404 +Btumofluorcbenzqnem37-26-s TdtGna4S| 7 060474 l,?Qichlot@thane44
BRLBRLBRL
BRLBRL8RLBRLBRLBRLBRL
1041@1G)
ta6a5.:lz
Ettrrctrble PetaoleuIr| HydrocrrborsEdi"actuble Total Pol.oleum HvdrccarbonsP.epared by rneltbd SW84{i 355088006{1{ Gasoline68476-30.2 FuolOlt #26847&313 Fqel Oll fi46455!0Ga FuelOilt 6trogtfrooo tbto. OilJoo1dxloo Avialion Fuel
UnidentifedOd|€r oillol,al Petroleum HydrocarbonsC9436 Aliphatic Hydrocarbons
SuTDgare recorr'gnss--33BB-3.}2 |-Chlotwcladecene
Semlvolrailc Ory{nh CoEpo[n& by CCO.oanochlodne Pesticidos SW8,16 808 1 APrepared by rnethod SWE46 35508309-OG2 Aldrin
pg/kS dry 5.8
lg,irsdry 5.8
lqkS dry 5,8
ldko dry 5.8
lrykg dry s.6pgl,l(gdry 5,8pCrlg dry 5.8
lgr'kg dry 5.8pdks dry 5.8
tdkg dry 5.8
uqlqdry 5.8
PdkSdry s.8
IdkSdry s.8
ldkg dry s.8
Igkgdry 58pCftgdry 5.8
LidfS dry 11.6
ldkg dty 5.8
ttgtkSdry 57.9
USikS dry 5-8
t'dksdry 5.8
t/dkS dry 5.8
!g/kg dry 5.8
t dkS dry 57.9
USftSdry 116
TG lm%7G1m%7G134%7G130 %
1
1
1
1
1
1
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1
1
1
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1
1
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1
SW846 82608 2l-Mar47 22{.',,at47 7m123:| TR
BRLBRfBRLBRLCdculabd asBRL205BRLrc5205
144
BRL
msftsdry 25.4mgikS dry 25.4nWkS dry 25.4rEftg dry 25.4figr'kg dry 25.4mdkgdry 25.4n'g/kS dry 25.4nE/kg dry 25.4mdrgdry 254nrdlq dry 25.4
40-l40 %
+CT ETPfI 21-Mar47 21]lngf'o7 7091167 DS
US/f,S d.y 6.27 SW846 8081A 20+lar-07 25-lrer47 7o3l06a TG
Thts labotutuq rypod is ,rot l'dtd uih4d .a authoriztd funzntre on &a @Er prg..' Rrportable Detection Umit BRL = Below RQortinC Linir Page 14 of 152
Page 149
Samgle IdentificatiooM8F-6 2'-1'sA59464-01
Client Proiect #301-88
MatrixSoit
Received19-Mar-0'l
Collec!ion Date/Timel5-Mar 07 00:00
CAS No, Analyte(s) Resull Fhs A n s *R.DL Dilution Method Ret Pteparcd Aaalrzed Bakh At'agrt
S€mivolrtile Orgrnic Compounds by CC
Orqanochlorine Pes0cides SW846 8081A
Prepared by melhod SW846 35508
3198a€ a-BHC31e{+7 b-8HC31e-86€ d_8HCs€-aee g-BHC (Lindane)
s7-74'9 Chlordane72'54.a 4,4-DDD (p,p,)
72 s+e 4.a-DOE (p,p,)
so,2e-3 4,4DDT (p,p')
60-57-1 Dielddn959'983 Endosulfan t33213S5-9 EndosLujtan,l1031{7{ Endosulfan Sutfate72-20-a Endrin7421-93-4 EndrinAtdehyde76.1+A Heptachtof124!5 Mefiorydtlor1024-57-3 Heptachlof EFoxade8{X,1-3tz Toxaphene5103-71-9 a-Chlodane5566-3.4-l g-Chtodane
5349+70!5 Enddn Keione
Suftogale rccoveies:103a6-8+? 4,+D&Octallwrcbiphenyl (Si
2051 -2+3 Decachbtobiphenyl (Si
Polvcf o.inated Eiohenvls bv SW846 8082
Prepared by method SW846 35454
12674.11-2 PC8 10t61110.4.n-2 PCB 122111141-16-5 PCB 1232
53469-21-9 PCB 1242
12672-294 PCB 1248
11097€91 PCB .1254
1109C€2,5 PCB 12601f u4-2r5 rc8.f621r10e14-4 PCB 1268
Suarogale r€@ligriesl1Na68+2 4, +DB-Oclelluorobiphenyl (Sr)
2051-2+3 Deeachlotobipheny4 (54
Sernivolrtile Organic Compounds by CCMS
BRLBRLBRLBRLBRLBRLBRLBRL
BRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
45108
BRLSRLBRLBRLBRL8RL
BRLBRL
4075
pgKS dry 6 27
US/KS dry 6-27pS/kS dry 627
ugkg dry 627
ldkg dry 314pdkg dry 6.21
udkS dry 6.27
f.ig/kg dry 6.21
!g/kg dry 6.27pg/kg dry 6.27
!g/kg dry 6.27
!g/kg dry 6 27p$ftg dry 6 27
lSn(g dry 6 27
sdkg dry 6.27pS/(g dry 6.2/
lSixq dry 6.27
ldkg dry 31.4
ldkg dry 6.27
lig/kg dry 6.27pdkS dry 6.27
30-150 %3Gl5O To
lSftS dry 12.5
ldkS dry 12.5pg/kg dry 12.5
udkg dry 12.5
lSikg dry 125pdkS dry 12 5pg/Kg dry 12 5
!g/kg dry 12.5
ldkS dry 12.5
3U150 %30-150 %
pS/kS dry 630
uS/kSdry 630
Ug/kg dry 630pg/(g dry 630
!S/kS dry d30
lgks dry 630pdks d.y 630
lSftS dry 630
1
1
1
1,l
I
1
1
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1
1'|1
1
1
I
1
I
1
1
1
SW846 8081A 2O-Mat47 25-Mat47 7031064 TG
sw846 8082 21-Mat47 23+Jlar07 703116/'
Semivolatile Orqanic Comoounds bv SW846 8270CP,epared by method SW846 35508
83-32,9 Ac€naphthene208,964 Acsnaphthyiene62-5!3 Anilin€i2G12-7 Anthracene1912-24-9 At€zine103-331 Azobenzene/Diphenyldiazine9247-5 Benzidine56-5t3 B€nzo (a) anthracene
8RLBRLBRLBRLBRLBRLBRLBRL
SW846 8270C 22-Ma(07 24-Maro7 7031278 M.B
Thh labontory ftporr k not vald v'irhout or auahotiz.l slpatarc on tha cotu Fage .
a Reporlrblc D€tection Limit BRL = Below ReportinC Limit Pag€ l5 of 152
Page 150
Samole ldcntificationMtF{ 2'-4's45946443
Client Proieca #301-88
MatrixSoil
Collection Dare/Timel5.Mar{7 00:00
Receivedl9-Mar{7
CAS No. Anolrte(s) Resalt Flag *RDL Dilation Melh4d Ret PrcWed AaaIWd Batch A,'/'lyt
Semlvolraile Org{trlc Cohportrd! by GCMS
Semivolalile Orqanic Co$pounds bv SW846 8270C
Prepared by method SW8,t6 3550850-32{ Benzo (a) pyrene20599-2 Benzo (b) fruoranthene191-24-2 Eenzo (g,h,i) perybne20748-9 Benzo (k) fuoraohene
Benzcic acilr0G51€ Benz!4 ekof|1cl11i-91-1 Bis(2rhlooettpxy)m€lhane1tt-,4-4-4 Bis{2-chh.etryt)€66r3963e32-9 Bis(2-chloEisoprop!'l)etheri17-81-7 Bis{2-€hylhexyl)phbetatetol-5t3 +Ekornophent pheny' ethers5{&? BuM benzyt phhatate86-74-8 C€rbazoles9.5o7 44lloro-!ft€tttytphenol10647r +chloroanilin€91{$7 2-Chloronaphthab{re9+s7-a 2€htofahenol7006-72-3 4-Chlclophefl yt ph€nyt ether218{1-9 Chrysene53-?G3 OiberEo (€,h) anthrac€nei32-64-9 Dibenzofuran96.:!Gt l.2.Oid{oobenzene541-73-1 l,3,DichlofoberEene1OM-7 t,4,Dichlorcbenzene9144-'1 3,3:Dichlordenzjdine12C43-? 2.+Dichlotrophenolu&z Diehyt phhatate13r-1r-3 Dimehyiph0rstatei05-67-9 2,+Dlnefftylphenola+74.2 Di-n-butylphrletat€534-s2-l 4,6-Dinito-2-mefiylphenol5t-2&5 2,4-Oinitrophenol121-t4-2 2,+Dinitotoluen€60e20.2 2,&Dinitotoluene1 rru4{ Di-fl-oc{yl phthaht€2t6-444 Fluoranthen€86-7$7 Fluorerig11+74-1 H€xa€l{orcbenzeno87{&3 }texEdbrcbutadisne71474 Hexadorccydopentadien€67-72-1 H€r€c*tlorcethane193-s9-5 Indeno (1,2,3{d) pyr€ne$t2{ t.tlodrynaphthalene7&1t91 lsoptubne91'57-6 2.Llofrytnaphthatene95-4&7 2-Mgthytphenol10s38a, 3,+M€thy{phenol106-44-5e1-2G3 Naphthalene8€-744 2-Niboaniline9s{+2 }Nltroanitine
BRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLSRLARLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLARLBRLBRLBRL
BRLARLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
pqkgdry 630 1
ldkS dry 600 1
ugksdry 630 1pS/kg dry 630 |
trSf€d.y 630 1
PsrkS dry 630 1
ldkgdry 630 |
ldlq dry 630 I
ldkg dry 630 |pSlkgdry 630 1ySAS dry 630 1pdkSdry 630 |pdkgdry d30 1
ldkS dry 630 1pdks dry 630 1
t4/ks dry 630 1pgrsdry &,0 t
tgr(g dry 630 1
ldkS dry 630 1
Ug@dry 630 1pS/kg d.y 630 1pcftS dry 630 I
lidl(gdry d30 |
ldkS dry 6il0 1
USrkS dry 630 1
lrSikS dry 630 1
FSAgdry 630 1
PS/kg dry 630 |
ldkgdiy 630 1
|lSn(S dry 6il0 1pdksdry 630 1
ISikSdry 630 1
FC^S dry 630 1pdksdry 630 |
IdkS dry 630 1pdkS dry 630 1pSftS dry 6:10 1
FSftS dry lI)0 1pdks dry 630 |
ldkgdry 600 1
rcfl(S d.y 6il0 I
Ug/kS dry 630 1
ISilqdry G30 1psilgdry 630 |
Fdkgdry 630 |
fldkSdry I
ldkg d.y 630 1
IdtSdry 630 1pCftS dry 630 I
Idrgdry 630 |
Thit lzbontery tqorl is r@t ialu wAhoa .n aalhodTd sigaate oa lhe colet pqe .
+ Reportrble Detection Limit 8RL = Betow RcForting Limir Page 16 of lJ2
Page 151
Sample ldsotificationM8F-6 2'-4,
sA59464-03
Cli€nt Proi€ct #301 -88
MatrixSoil
Received
19-MaF07
Collection Date/Timel5-Mar-07 00:00
CAS No. Analrte(s) Resull FIag Uzis ,RDL Method ReJ PQpored Anabzrd Bokh Anarysl
Semivoletll€ Orgaric Conpounds by CCMS
Semivolatile Omanic Compounds bv SWg46 8270CPrepared by method SW846 35508
100-01{ 4-Nito6hiline98-95-3 Nikobenzene8a-75-5 2-Nitrophenol100{2-7 4-Nttrophenol
62-7+9 N-Nitrosodirnethylamine
621$4,7 N-NitrcGodi-n-propylamine86-30-6 N-Nitrosodiphenylamine87{6-5 penlachloropfEnol
8541.8 Phenanthfene10&95 2 Phenol129'004 Pyrene110-m-1 Pyridine120.82-1 1,2,{-Trichtofobenzeness-9t4 2,4,tTrichtorophenol86{G2 2,4,&Trichtorophenol
Suftogate reco|,En€'s:32140-a 2-Fluorobiphenyl
367-'2-4 z-Flu(nophenol
41654a4 Nitrobenzene4'
4165-62-2 Phenol4s SO1718-514 Teryhenyt4l4 8611e79-6 2,4,6-Thbronoph6nd 7l
Torrl Metats by EPA 6000f10o0 S€ris Methods
BRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
77
71
Compl€ted
BRL
BRL
0.0r55
BRL
0 0070
BRL
0.0454
BRL
86.0
ug/kg dry 2520
ug/ks dry 630
ldkS dry 630
!s/ks dry 2520pdk0 dry 630
lig/kS dry 630
lSikS dry 630
lis/ks dry 630
t s/kg dry 430
PSn(g dry 630
lgil(g dry 630
lqkg dry 630
!S/kS dry 630pdkS dry 630pdkS dry 630
m-130 %15-110 %30-130 %trl t0 0A
30-130 %15-110 %
mg/kg dry 0.0342
mg/kg dry 1 13
mgr'kg dry 1.7o
ng/kg dry 0-566
mg/kg dry 0.203
ogr'kg dry 0.566
mgftSdry 1.13
mg/kg dry 1.7O
mgfl 0.0r0o
mg/l 0.0150
mgl' 0.0050
mg/l 0.0025
mSI 0-0050
mg/l 0.0o(Xo
mSl 0.0075
mg/l 0.015t)
%
I
I
l
I
I
I
1
1
1
1
1'|
1
1
SW8{6 8270C 22-MatsO7 24-Mat47 7031278 M.B
7439-97$ Mercury
Totrl Metds by EPA r00 Series Methods
74'lO 22t Salver
74.10-38-2 Arseoic
7440.393 Earium
7,r4or3-9 Cadmium
74-4047-3 Chromium
7a39-921 Lead
7782-492 Selenium
SPLP Extraction
7440,224 Sitver
7440 3A-2 Arsenic',440-39-3
Baium
7440-43-9 C€dmiuh
7440]7-3 Chromiqm
7439-97{ Meac1lry
7439-92-1 Le€d
7782-4$2 Selenium
C€deral Cft etni3ary Psrsmeasrs
% Solids
o.208
BRL
13 .6
59.1
1 .97
23.1
297
BRL
1 SWE467471A 23-Mar47 26-tvlar{7 7031306 YP
EPA200.7 23-Mat47 24+,4a(47 7031305 HB
SPLP Metalr by f,PA I I | 2 & 60001000 Sertes Methorts
1 SW8461312 21-Mat.o7 211\lat47 7031229 BD
1 SW846131260108 22-Mat-O7 23.tr\Aa(47 7031323 LR
1 ''1 "
t "
1 '
I SW84613127470A ' 23-Mat47 7031324 W
1 SW8{6131260108 ' 23-Mat47 7031323 LR
1 "
1 S[,f2540 G Mod 22-Mat47 22-Mat47 7031307 YM
Thls laborulory rcport is aal tclU wirto( an aulhoriaed signatarc on the @ve, page.
+ Reportable Dercction Limit BRL = Below Reporting Lidl Page l7 of l52
Page 153
Sample ldentificationM8F-7 2'-{'sA5980l-01
Client Proiect #30r-88
MatrixSoil
CoLlection Date/Time26-Mat-07 00:W
Received27 -Mar-07
CAS No. Ana\,te(s) Resall Flos A n s *RDL Dilution Method Rel. PEpored Awlrzfll Bach AnalJts!
Vol.til€ Organic Compornds
VoC Extracrion Field exLacted
Volalile organic Camoounds
Prepared by method SW846 50354 Soil (low levet)
76131 1,1,2'Tidrlootdnuoroehane{Fr€on 8RL6I+41 Acetcne BRLr07.1$r Acrylonitate 8RLJ14+2 Benzene 8RL
100{61 Bomobenzene 8RL
1447-5 Bromoc+ioromelharE BRL7}274 Bomodichlommelhane 8RL
15-25-2 &omofonn 8RLt4-83'9 Bornomehane 8HL784+3 2-Butanone (MEK) 8RL
10,1.51-3 n-BltylbB.rzene BRL135.98-8 sec-gL{ylbenzerE BRL
98464 lerl-Butylbenzene BRL75-15,0 Carbch disutfrde 6fl1
IUA
p4rs dy 21.0
PS4€ dry 421
$/kS dry 21.0pS4S dry 21.0
$*S dry 2l.0pglrg dy 21.0pdr(S dry 21.0
rcAS dry 21.0pdls dry 42.1
Pg/tS dry 210
llg/kS diy ?1.0
rrgls dry 21.0
ldkS dry 21.0
trS4S dry 105
pS4S dry 21.0
}4^S dry 21.0
l4AS dry 42.1
|Jg/rS dry 21.0
pdxs dry 42.1
lgtS dry 21.0
pVlS d,y 21.0
|EtS dry 42 |
$/ks dry 21.0
!S/fS dy 21-0
IAAS dy 21.0
lSftS dy 21.0
ptsdy 21-0
Msdry 21.0
pSAS d,y 42.1
pgr(! dy 21.0
!dk! dry 21!
Udlq dry 21.0
ldkq dry 2l.0
ldfS dry 21.0
|4,tS dry 21.0
iVtS dry 21.0
ldkS dry 21.0
!s/rs dry 21 0
tS,& dy 21.0
MSey 21.0
t]oAS dy 21.0
lgrq dV 21-0
llgAsdv 210
pSf.S dV 21.0
tj['t!0dy 2ln
l'dlq dry 21I
UdlS dry 210
pdlq dry 210
pdts dry 21.0
voc
sw 846 82608
28-Mar-07 28-Mar-07 7m176?
5Fr+5 C€rbchteiEchtodde10S.90-7 Otlorobenzene7s{l}3 Cfiloro€l}€n€6/{6 3 Chlorofom71-87.i Cilorofieharc96-49.0 z-Cruorotduene10641-4 4{Hoaololoene
9t!12-s 1,2-Dibrom+Sdtloropropane
124-!41 Dibromodoron€har€106sH l,2-Dbrcmo€thane{EDB)
749s3 DibronEmethanegtscr 1,2-Dsorobenzene
54r.73.r 1,3-Di$toob€nzene10e.{67 lj-Didtlorob€nzere75_71-8 oichloodilluoromethane(Fre!ni2)E*3 1,l-Dichloroelhane
10746-2 l,2-Drchloroelhane
75-35-4 l,l-Drchloro€lhene
156592 os-1,2-0ichloroethene
156@5 tans-l,2-Didooelhene73{7.s 1,2-Oc.iompropar€
1{2 26e 1,3{)id oroprcpar€
s942G7 2,2-Dichtoopmpane
s63.s8-6 1 I -oic+toroprcpene
10061{1.s cist,S.Didlo.opropene10061-t2€ trans-l,g0ictilooptopene10041-4 Eryb€nzene
875&3 Hexachtoobutadiene
5e1 73 6 2-H€xa1on€ (MgK)
98-6e-8 kopropytb€n:€ne
e9-8/j +lsopropy'lduefl€r&4-04-4 Msttyt t€n-blty' €th€r10€nGr 4-l,lethyf2-penbnone{M|BK)
7549-2 ft,telhylenechbrtje
91.20-3 Naphhalen€
BRL
8RL
8RL
BRL
8R!
8HL
BRL
BRL
BRL
8RL
8RL
8RL
BRL
BRT
BHL
BRL
BffL
BRL
BFL
BRL
BRL
BHL
BHL
BRL
BRL
BRL
8RL
8RL
8RL
BRL
B8L
BFL
BFL
881
BRL
Thb labo4to,J, rcpod b nol talu fiUhoU aa authortzed sigdtttu.e on lhe cot$ page.
+ R€podable Det€crion Limit BRI = Below Reporting Limit Page 3 of 154
Page 154
Samol€ IdentificationM8F-? 2'-4'sAs980l-01
Client Proiect #30t-t8
Collection Date/Time26-lvlar4? 00:00
Rectived27-MaF07
MatrixSoil
CAS No. Analrtz(s) Result Flog Uait **DL Dilatio.t Mdhod Rc[. hepated Anabzed Bath A^olW
Voldile Orgrnic Compounds
Volane Orcanic C!.ruounds
Prepared by method SW846 5035A Soil (low t€vet)
1@{5.1 $-PnflA€nreie BfrL
lllc'P.5 SlyrEne BRL
6s!20{ 1,1.11-Tetraohloodnane BnL
?83,t6 1,l2r-Telradlorodl3ne 8RL
1n-1s1 T€fad ooghene BRL
106-0&3 Tduefc BRL
'I{1-€ 12,}T J olob€n2ene BFL
120-82-1 I,2+T*t oobejlzen€ 8RL
7l-5s 1,1,1-TdJ oroetlane 8fi1
?Bs6 1 ,'12-Tfthloroe$a1e BFL
19{16 Td* otoet\ore BRL
Td$lonftrorofirehane (F€dl ll) 8ft-
$l8t tz$Td$lorQropane BRI
96-63.6 1,2,+Tft1€hylbenzene BRL1n06't0 1,3,$Tdmstrytbenzefle BRL
?v14 Vhy' chlod& 8RL
133+2ol n,pxtle0o BRL
9t17.6 exyi€fie BRL
1099s4 T€lrafi@uran 8RL
6G2e7 Eryeher BfrL
99{453 T€n-anyl meftyj s$er BFL
637{J-3 Ehyll€d+dy'ef€l 8FL106?l!3 Di+opmgyletitor 8RL7$5q) f€rl-gutanol/ buM alcord BRL12+s1.1 1,40i(*arc BRL
d6t @r +EflNitMobenane 95
M7-h-t fdudv$ 16170f,474 1,2-hfilotd11dE44 I$Etttnil Dkryr'fir{'onahme !)6
f, xlrlct{ble Petrolerm Hydrocirbons
Enradabl€ Totd P€trcle0n |Mrc.aftoos
Prepard by .nehod SW846 35508
BRL
BRL
8R-
BRI-
BHL
BfrL5,070Colc{lahd as5,0705.070
t'Vhgdr) 21-0
|Jg4SdY 21.0
lgkS dl 2r.o
tgrS dry 21.0
ldts dy 21.0
|'Er'lq dy 2!ll
tgrgd'y 21.0
lrylq (} 21.0pyto dry 21.0
lgrS d') 21.0yg&dy 21n
uc4q dy 2r.0
USIq df x.0
lglq d! 210
lg/kdy 21.0
lsl€ dy 21.0
ldEdry 210
|lyrSdy 210
lgkSdy 2t.0
lErS dy 21.0
lgtS dy 21.0
tryl€try 21.0
lSIq dy 210
lalrg st 421
7lllg 70
7F l f i%
701f i%
7tr1& %
rWkS dr, 1240rldh dry 1210msredry 1244mylSdry 1240mg/lq dy 1240nS.,kS !q' 12{0mq/rg dry l24onE/l€dry l21omgrqdry 1244mgtSdry 1240
1e140
s'vt 846 &604
|cI EIPH
I
I
l
I
I
I
1
1
1
I
I
I
1
I
1
I
1
1
1
I
I
29-ltrri{7 2$Uarfl ffi1?S0 ru
&661.9 GardinB6s4?G.!-2 F!elo{f26847e31'3 Fu€t 0d*46ss}00-4 Fuelol +61f91100000 l,lotorol
ro1w0 Alialih FLd
unil€nt'fiod
ohe. olTdd Potden tidocarboGC!.c36 Alirhatic Mrcaitons
Semivolrlil. Org.nic Compo!trds by CCorganodh{in€ Psdi.ites SV{8,46 8081APrepared by method SW846 3g5As]D2 Aktin
2g-llar{? $}l|3I{7 700177?
BRL ldlqdy 6t9 swB,{6 808rA zg-,lizrnT 02.Apr{7 7m1739 IG
Thb lahonlary rqoti it rrot ttdid w&hod an auihatizel ipatuE on aha coea page.
' Repotuble D€tection Gmn BRI: Belos, ReDorririg Limit Page 4 of t54
Page 155
Sample ldentificatiooM8F-? 2',-4'
sA5980l-01
Client Proiect #30t -811
Collcction DatelTime26-Mar-07 00:00
MatrixSoil
Received
27-Mar-07
CAS No. AnalJte(s) FloC Units *RDL Dilutiot' lrlethod Ref. PrepaEd Ancbzed Bot..h Anavsl
Semivolatilc Orgrnic Connounds by CC
oeanochlorineFesricides SW8468081A
Prepared by method SWB46 3545A
319-84-6 &BHC31+8s-7 b-Bflc319-86.0 dBHC58.8e.e *BhC (Undane)tt-7+9 Chlordane?.s+8 4,4"O0D (p,p)
72.55-e 4,4!00E (p,p')
s02s3 4,4L0DI h,p,)60.tr Dieldlin
95+9{l-0 Endosulfan I
30213-619 Endosllfanrm147'8 EndosulfanSulfale72-20-6 Er in74214X-1 Enddfl Atddyde76-r,13 Heptachtor
2415 Mef|orylhlo(102+57 I H€llachlor Epoxide&Il13t2 Toxaphene5r@719 a{hlordde550e34.7 g{hlordate
53,194.705 EfidinKelone
1e?raa.2 a,a.D84cEnuotobbhenl(54
N1++3 Decehtonbipheny)(k)
Polvchlodnated Biohenvls bv SWe,46 8082
Prepared by method SW846 3545A
1267411.e PCB 1015111M2e2 PCB 1?2|l l14r 165 PCB 1232$16921-e PCB 124212672 As PC812481r0e7 6+r Pc8125411mfi25 PC81260373242+5 PCB 12621110s14-1 PCB 126g
1038644.2 1,4-D84clafluottu0lgnl64
2051.24.3 Decd otobiptEnyl(*)
S€mivolrtit€ Orgrnic Compounds by CCMS
S€mivolalil€ orcanic Comoounds bv SWB46 8270C
Prepared by m€thod SW846 35508
3$349 Acemphhene20s46 0 Acenaphthytene
62 t13 Anillne12n121 Anlhfacene1912-21-9 Alra2ine1q!$-3 Azobenaene,Diphef4ldiaane
9{7.5 8€nzidine566$3 B€{Eo(a)anthrac€ne
SFL
BNL
BFL
BNL
BffL
BFL
BFL
snLBRL
BHL
BFL
BFL
BHL
BRL
BRL
BRL
BRL
8RL
8HL
BNL
BRL
59
108
8RL
8RL
BRL
BRL
BRL
BRL
BFL
BFL
BRL
fl
fl
BRL
BRL
BRL
BffL
BHL
8Rt
BRL
3,e50
65.9
65.9
65.9
65.9
33{)
65.9
65.S
65.9
65.9
65.9
65.9
65.9
65.9
65.9
€ 5 9
65.9
65.9
sto659&59659
ps,'lq dy
ldks dry
!S/iq dry
fdks dry
!s4q dy
lsxq dyps q dry
lsnq dry
!g4q dry
uc4q dry
udkg dry
uqks dly
lqks dry
ldlq dry
ldlq dy
lE|q dry
|lg/ks dry
|.dks dry
|lg,lg dry
$4q dry
|ls^sdry
3A-154%
3Gt50 %
!SI(g dry
!g/lq dry
pglq dy
pyrq dy
usnq dy|lglq dry
pdkg dry
wts drypdkS dry
# t f l%
fr-150%
s',Y846 8081 A
sw846 E08?
sw846 8270C
I
I
I
I
I
I
I
I
I
1
1
I
l
l
1
1
1
2E4a"{7 02-Atr47 7031739 TG
132
r32
t32
132
132
132
132
132
1 U
z&l',lar{7 30-Mar.07 7031738 SM
usks dy
usiq dyp9rk9 dv
Fdkg dry
$/rs dry
lsl|(s auStS dry
ldks dly
768 r768 I
768 I
768 t
768 1
768 1
768 I
768 I
29+1arc7 0!Apr'07 703124 M.B
Thb laborulory rcpo4 is trot valid without an zaahoized sigaature on thc eovcr prge .
' Reportable D€tection Limit BRL = Belo,x Reponing Limit Page 5 of 154
Page 156
Sample [dedtificationM8F-7 2,-{'s459803{l
Client Project #301-88
MatrixSoil
Collection Dat€y'Time26-Mar-o7 00i00
Received21-lia.-01
CAS Na Anotytc(s) Resa,A ntg Unis 'RDL Dilltio,t Lldh4d Retr, PrcWed Analfzed Boftk A,,4lfst
Semtvolrtile Orgrnic Compoobdi by GCMS
Semivolatls oroglic Comoounds bv SW846 eB70C
Prepared by m€thod SW846 35508
:G!a{ 8€rED {a) pyrene
a5{9.2 Benm(b)fluoranhone191.2,1.2 B€nzo (glli) peryl€ne
207{a9 8€nzo (k) ffuoranhe'les6ss{ &natc a.id1@516 Ssqlrtcotol111€rr As(2d|hroatloxy)n'€han€111-414 Bis(ldllordfit)efief
$s.!e-D 8js(2drlooi6oproptl)g$er1r7-0r.7 8i{2€ryhoxyt}phfidale101_563 4€dmph€ny' phenyt etEr85.6&? &rMbst4tpfifElale8F744 Csbazolesgsr}.',r {4hloo.3{rBlfuphend
10G47-8 44hlo.oddhe
s1-s&7 2€Hq,onafht|d€ne
s7{ 2{hlo.opha,ld
ruF72-3 {act orcdrsyl phg]yl€tref
210{1-9 ChryE€n€597G3 Dibonzo (e,h) anilEcae13e{49 ob€luotulan
S5Gl 12-Ddloob€nzene5417$1 l,3-Odltotot€fterc106.1&7 t,4{)icilo.ob€nz€fle
91€+1 3,3'-Dichbltrenzidne120-€+2 23{ktotophonolat&2 oiefM pafietaie
13rr1.3 Dicttyl pfthahb
106'6-r.9 2,4.Orn#rylpheflol&112 D-n-h4yl phfiatals
$4521 4,eDiniu.!.2meryphenot
51'28-5 2+fini[lphCtoll2r-l+2 e4.oiritobtusne6{6,2!-2 e€{hitoblt e{err7-€r{ o-n{dt pnhalab
a6444 Fluordrfi€ra{St$? Fluorrlo
11&7+1 H€xddoobgrz€n€
E7{8-3 }tsxddJo|ohJhd€n€
17171 Hexadtoroqcbpenladiene
6l-721 lleiad OO6U€IErs30-5 h&no (1,a3<4 pyEneqr12{ l{,tstttitnaFfial€ie781&1 lsophorfie9r5/-t 2{r€{tylneph{rahrcs{€.7 2.t{dtt}dphed
10G3!'-4, 3,4-l,tst$&h{rdtEn45S1.203 t{aFtDlffF&fu 2{nroaflfln€9rF2 }t{itwnilne
8fit-BRL
B8LBFLBFL8R-BRL
BFLBFL8RL8FlBRLBNLBNLBRL8RLBFLBFL4,9008RL8Ft
MLBfiLBFLBRLBRL8RL881BRI.8RLBRI8RL8nLBFL8RL9,370gRL
BNL
BFLBRI.Bft-BRLgfiL
B8L8FLBFLBH.
8FLBFLBRf
lc|qA$/tq d)
|]9r9 tryudkg dyab dvFS{q dy
r4rc dy|jgls d]
lgls dy
Ars *y!91€ dy
|lg/t€ dl
wts dvlglq dv
ugts dy
IJdE A
!S,lq dV
lgrq dv
tdlq dy
|dlq d'v
|,glq dry
ldrs dy
lgxS d)
ti4kS dy
Uglrg dy
|dE dv
abdvldks dy
|Jdis ey
ryrg dry
|dhdry0lg dv
ldh aldlq dy
wk! dv
E/lq dy
|lglqd]
|Jdlq dy
ldlq rt
vllt dy
t{/l€ dry
$,lqdy
|{lq dV
!g/lq dy
Elq dy
|dh d-y
@ev
|4ts rvlgb dy
lglq dv
766
m!
768
76E
766
768
7€8
768
766
766
768
768
766
768
ru7e76€768
76t
768
7€8
7t8
76€
7€f
7€E
768
768
768
768
ru768
768
768
768
768
768
768
7€8
7€8
768
766
768
76€
sw846 8270C 29.1'rer.07 o3-t{'47 7031774 lil.B
Thh leborultry report Lt aot rdU withnct on salhoizcd slgnals.e od thz cover psgd .
+ Repofbble Detection Limit BRL = Belo* Reponing Limit P.ge 6 of 154
Page 157
Samolc IdcntificationMEF-7 2'-4'sA5980l-0t
Client Proiect #30r-88
Collection Dare/Time26-Mar-07 00:00
MatrixSoil
Received
2'7 -Mnr-07
CAS No. Analrteq) Result Flos Uni6 *RDL Dllurbn Method Rel. Prcpated Analyzed Batch Anabst
Semivohiile Org{[ic Cohpornds by CCMS
Semivolafle orqanic Comoounds by SW846 8270C
Prepared by mothod SW846 35508
100{1{ 4-Nilrcaniline98-9s'3 Nilrob€nzene88-75-5 2,Nitrophenol!0042.7 +Niliodenol627t9 N-Nirosodimefrytanine621447 N-NiEosodi-n-propytamine8630{ llNihosodiph€nytanine678e5 P€nlachlooph€nol85{l-8 PlEnanlhr€ne10e95 2 Phenol
110+6.r Pyddn€120-8p-r 12,4-Tnchtomb€rEene
9G954 2,4,5-Trichtorcrphenot88-0G2 2,4,6-Trichlomphenol
3216o4 2-Flwohiphenyl
3n7-124 2-Fluotophgnol
{165JG! llitdenzene4'
4te6-62,2 PtEt1ol4,
1713 5r1) TeAhenylaC4
tt&Ni 2,1,&Tribnnophenol
2941at41 03-Apt41 lb1-t74 M.88RL
BHL
BHL
BflL
BHL
BflL
SRL
BRL
BFL
BHL
10,2n
BflL
BRL
BRL
BRL
u58
n60a4n
sw846 8270Cug^s (y 3o7o
|lg,{S ry 768
|4/ks &y 7€8
lS,rc dry 3070
WkS dry 768
!S/kS dry 768
WkS dry 766
udkS dry 7€E
pq/tg dry 7€€
llg^s dry 76E
rgtks $y 78
lC(g fy 76€
lqrs dry 768
UgftS ry 7€a
fgftS fy 768
34130 %
15110%
3+1@ %
t5-110%
30-130 %
t5-1tD%
mdks dry 0.0704
mo/kg dry 2.21
rndhdry 332
rgAgdry 1r1
nrg,lq diy 0 553
mdkg dry Ll1
nSftS ey 1.66
mCfto dry 3e
mgn 0.0100
mg/I 0.0150
ng.4 o oo5o
mgl 0.0025
mgl 00125
firg/r odlMl
mga 0.0075
rngl 00150
sw846 7471A
EPA200.7
sw8451312
sw846 t312/60108
sw64613t274704
sw8.461312]6010a
Sll2540 G Mod.
Toaal Metrt! by EPA 6m0/7m0 seri.s Merhods
Total M€trls by EPA 20{ Scrier Methods
714t.22-4 Sitver
7{,O.3S2 dsenrc
74|+393 Eaium
7110-43-9 Cadmium
I44o47l Chromium
743992'1 L€ad
[email protected] ? Selenilm
A2-4.{n47 03-Apr-07 7031810 YP
BBL
10.4
91.6
o0 l8
n.5
574
8Rt
02-Apr{7 HB
SPLP M€t ls by EPA 1312 & 60007000 Sert$ Methods
SPLP Exlr&lion compl€l€d
4J-n4 Sitver BRL
714I3&l Ars4nic BRL
7.{rl! 3+3 Badum 0.0106
744G'|}g Cadnium BFL
7,110-4/-3 Ctrornium BRL
zlss 97-6 Merc!ry BRL
74!+Se,r Lead BRL
nv4s2 Sslenium SRL
Gen€ml Chemislry Prtrmeters
% Solids 41 5
2B-Mar07 2&mr-07 7031763 BD
30-ttar{7 02-AF{7 7031806 Ln
" @'Apr{7 7031806 YP
' C-Apl{7 7031E05 La
3&tuar{7 3&Mar.07 7011879 YM
This hnonhry Epo,l ir not vdu withod ar cuthottud sigatan on thc cover page .
* R€porlable Detection Limir BRL = B€low Repolting Limii Paee 7 of 154
Page 158
Sample lde[tificationMtF-8 ?'-4's,A59803-02
Clieot Proiect #30t-88
MatrixSoil
Collectiop Date/Time26-Msr{7 00:00
Received27-Mafi7
CAS No. Anavta(s) ncstdl Flos Ani6 *RDL Dihttion Method Retr. Prcporcd Arebapd Bouh Anabst
Vohdle Orgsnic Compounds
VoC Eiffaditn
Volatile OKanb Comoqln&
Field e!(ad€d
lglq dv
rigkS fy
|4h dv
|8lqdv
|lgIq dY
|ldl€ d]
wl'gdt
!dk! dtl
B/tq dy
EIq dy
rrtbdtugh rvHAo dlwrgtlrt4l4dyudl(etvidlqdY
wks trv!S/fq dV
ldlq dry
Ah *v
r4h d'y
!91q dry
!9lq dt
Irgt0 fy
!g4q dv
H/lq dry
|dh d'v
rdk d'y
!04q d]
tlgts fv
Eq t r ylsrq fry
|!lq dry
I{i€ dry
!o/Iq dV
lgrS dry
lsnq dry
|dkg dry
rdbdvtdlq dry
|4rg 4v
|Js/ks d)'
us,/rs Y|ldb fy
l4lqdv
US,lq dy
$fig fv
t'gkS &y
voc
sw 846 82ffi
28+&r{7 28.lrar{7 781767
Prepared by method SW846 50354 Soil (low l€v€l)
76.111 1,1,2-Tricntootiffuooehane(F.eon BRLBFL
BFi.
BRL
B8I.
sRrsnlBFLBFLBRL88L8RL8nL8RLSFLBRLBFI.BRIERLBALBFLBRL8RL8RL8RLBRLBFLBFLBRL8tu8Rt-B8tB8L
8FL8RLBRLBRL8RLBFLBFLBRLBRL
BRLENL
BFLEFL8Rt-SHt.8FL
614+1 Aaeloie10r'1$1 k4ionlt'iten4E2 E€i2en€rc6.06n BrcnobgEsl€71171 0r([md orolr€hene.827.4 Srcrsdidrkd(rr\€t1al]e74.2t2 &onoloim7'r.839 Brundnetfte]€?&e-3 2-Buanoio (MEK)
10rr51-8 n Buybqrqn135.98-8 sec-Eulylben2ao€
l€n-0ulylbenz$€
75.1s Ce|bofl di$lfida
5e295 C€don lelEd{dide1084G7 ollod€rEgro7S0.3 chboohane6/,663 cttbotom71'X7 3 ctdo|lln€he/rq$.!$8 2{l{o|ottu€ns106<H a{tlorolduene
9@12_8 l2-Dbromo3diomprqane
124_,1&1 $bromod{O|unetlane1d ss4 l2oib.omoot'an€ (EDB)7445-3 Dhbnomehane9t5G1 1,2.0i$lorobenrene54r-7+r t,$oidllomb€nzene106-{&7 l,+ttdtlorob€nzene
?5714 t&torodiffuoromethane(Freonlz)
lS4 3 l.l{)ichloDe$Ene10/{6-2 l2oidttsogthane
75.39 1,1-0lctoro€tlEn€156-592 cigl,2oid{oroefpne15ffi taansn 2-Dct o.o€tlFn€7B.Er-5 lJ.Dcnlorcpropar€112-289 1,3oidlic@gmFane
t91207 22OirildoFop6ne5A+566 t,t.Oidllorqrope|re
10061{1-5 ciel,3{*liorcpropsn€1[(6]+2J talg-l,alDidr oropr,op€nelllo41{ E$tlbeEeno87{&3 Hoxddoobuhdiec591.78.6 2-Har4tone(MgK)ss&€ hoerlpylb€nzg]€s87{ +&ot oMolu€n€1034{t-r l{ehyitod{rfyleber
10SrG1 4-lrotlylz{€rnEDon€(M8n16,4!2 freh ere dloddBsr{G3 t{apht'aien€
65
tzg
6.5
6.5
1E
&.7
129
6.5
123
6J
55't29
6.5
6.5
6.5
6_5
6.5
5.5
129
6.5
6.5
6.5
6_5
6.5
6.5
6.5
6.5
E.5
6.5
u.7
6.5
84.7
64.7
6.5
This lrfutzloq rqon it noa ed@ w hoa an dtttloizd signonlre oE the cover pgg..
+ Reporbble D€{ectioo Limir BRL: Below Reporting Limit Psge I of 154
Page 159
Sample IdentificationM8F-8 2'-4'sA59803-02
Cliert Proi€ct #l0 r-88
MatrixSoil
Rcceived2'l-Mar01
Collection Date/Iime26-Mar{7 00:00
CAS No. AnalJE(s) Resuk FIAS anils *RDL Dilution Method ReJ. Pnpared Anal].Zetr Eatch AMh,\t
Volraile OrgaIic CortrFo{rds
Volatle Orqanic Cornpounds
Prepar€d by m€lhod SW846 5035A Soit (low levet)
103-6t1 nfrcpylbenzene BRL
1m 42 5 Styreoe BRL
630-?0 6 1,1,1,2-T6lradlloroelhan€ BRL
1+t+5 1,1,2,2-Telrachtoroethane BBL
12t.144 Telrachloro€bEne BBL
103 3&3 Tduene BBL
e7{r-5 l,2,3Tn€nbmb€nrene 8FL
lm-6e-r l,a4-Tti{* oroberDene BFLrr 516 1,1.1_Tti*toroehane BRL
7s{0.5 l,l2.Ticitoroshene BRLrs{r$ Tri{:htorD€tn€ne BBL
BRL
BFL
B8L
SFL
BRL
BRL
BFL
BFL
BFL
BRL
8RL
BRL
8RL
8RL
97
103
1ffi
N
BFLBFL8RL8RLBRLBRL3,m0Caid.ilated as3,m03,m0
160
!4ts dy
Lrg^g dy
l4/ts dry
llg/rs dv
9SrrS 6y
$/xS dry
!S4S dryp4kS dry
ur4s dy
lgtg drypdk{ dfy
|ls^sdrypglsdrv
!g4q dry
!g4q drv
!g4q dry
!gt! dry
ISAS dry
us&sdry@xs ev
lSilS (ty
lglq dy
lsfrs dy
lqtS dry
wn$ dv
7V130 %7013/%7G130%70tg%
mdt(s dry 667
mSitS dry 667
mg*g dry 667
mdks dy 67
mElgdry $1
nSI(S dry 67
mgl(g dry 67
mgas dry 667
mdlq dry 667
rnglq dry 667
4+140 %
UglS dry 2
sw 8{6 8260A
+CTETPH
6.5 l
6 5 1
6 5 1
6.5 1
6 5 1
6 5 1
6 5 1
6 5 1
6.5 I
6.5 1
6.5 1
6 5 1
6 5 1
6 5 1
6 5 1
12.9 1
6.5 1
u.7 1
a 5 r
6.5 |
6.5 |
a 5 r
4.1 1
12S r
E 6sl Trirhlorolluoromethan€ (FGon 1 1 )s13-r 1,z,3-Tdchtorcprcpanee533'6 l,2,tt.Trinehytben2ene108-678 1,3,5-Trimellrylbenzene75.01-4 Viny' dtodde17tu 7 n,p-Xylene9547-6 Cxylene109999 TetaMofuran
60?9'/ EthylefBr
994{58 Ted€my mehyi efier63742 3 Ethyl lsrt-buM e$€rlG 2G3 D,hopropyl sther75654 Ten€{lanot / butyl alcohol123-911 l,4-Dioxane
4ta-N4 4-g@nofludobenzene
2tA7-26.5 Tdler,e.fr
t7o@4r4 l,28icl d@tlqtE44
I46JS|7 Dibrcnmiuonnethane
f,raractable Petroleum Hydrocarbons
&lraclable Tolal Petroleum ltdroaarbons
Prepared by method SW846 35508
m0G6!.9 Gasoline
684rC3G2 Fuelotl2
6847631 '3 FU! CljJ J4
6€6$aH Fu€lo( 16ms€mcoo otoroil
J001qFI Avialion Fu€l
Llnidentifed
orher ol
Total Petolsrn Hydrocarbos
C$C36 Alipf lalic l-lydr@rbon€
338F33? 14hwo6ldeca1e
Semivolrlile Orgrnk Compoundr by CC
oroamd oflilo Pestiides SW846 8081A
Prepared by method SW846 3545A
@4G2 Atd.in
29Mar-07 &.lt^t47 J0$n2
BRL sw846 8031A 28-1rfffl Oe-AprO7 m31?39 TG
This ltbonloA reporl is ttol vald withost aa aaahoiratt signzrurc on the cryu page
* Reporiabl€ Detection Lirnit BRL = Below Reporting Limit PagE 9 of l54
Page 160
Sample IdetrtificationM8F-t 2'-{'sAJ9803-0?
Clielt Proiect #l0r-88
Collection Dale/Time26-Mar-0? m:oo
MatrixSoil
Received27-Mar{7
CAS No. A"zlrk(sJ Res l Fl{g Ania *RDL Dilation Method Rel Pnpated Anaiwd BtEh AnAttst
Semivolalile Orgrnic Compo|rnds by CC
Oruanodiodne Pe6licide6 SW846 8081A
Prepared by m€thod SW846 35454
319-8:16 D&lC319057 tsBHC3r$063 dSHC58{e s gBfC (tjndarc}
,.7+s cltodne12 5,13 a,4{00 (Ap )72 55-s 1,4,O0E(p,C)5c2s.3 4,4!DT1p,p16Gt.1 Uetdrins5998-€ Endo6ufian I321s65.9 Endcudan ll1031-07{ Endog/fansdhto72-@-8 Endin7t21.934 Endfln Abehyde?9{48 Hegtad{or724!s M€fioryd or102+57-3 H@d'torEponde3{,01i,S2 Tdaphd|e510c7r-9 achtordane556 r-7 g4hlodan€
E!4s.{-7r"t Eddn Kelms
te4-84a 4,4-Dg4cbftbtdidwl(54
Nr21.i Der,fJlht&ipw (St)
Pohahlorinald Bid€nvts bv SW846 808?
Prepared by method SW846 35t5A
1267+112 PC810161t1o+2E2 PC91E1rr14r.165 Pcg lzllsr.r6$21-9 PCE 12421A72.En PCg12481109t+e 1 PCB 1254fi(,€632.5 PC81260fie+2$ PCg 1Z&[email protected] { PC8 t2f8
1N&.84 1,+08.&'eiwteMyt(Srl
N12.:3 De{a./,otc6ip]l€nl(54
Scmivolrtlle Orgroic Comporndr by GCMS
Semlvolatl€ Oqanic Comoour6 by SW846 e27OC
P.epa.€d by method SW846 35508
al@4 A.enapfibs|e1846.8 Aconaphtlylons82-s3.3 AnitirEl&\2-7 fuhracdE191?+4{ Afazin€10933-3 Alobon2€i€/Diph€ny'da2ine94.C/.5 8fiidin65G5F3 SduD(a)uihracerE
BNL
8RL
BHI
BHI.
BNL
BRL
BRI
BRt
8FI-
SHL
BRL
BRI
BRL
BF(
8nL8ALBFLBFI.8RLBFLBRL
58ttt6
BNL
B8L
BFL
BRL
BRI
8n_8RL
BNL
BFL
fi
BRI.BRL8RLBRL8fi18Ft-BRL1,f6
2t2262x2x2r31
26.2282x2x2a2626.2ffi2x2x26262t3 l262
2%2
!91€ dypdls dv
!c/rs d]
|ls,fts dlv
lgilq trvpdlq dvpc4q dry
usrq dv
|jdks rv
tilgdrlt4l4d.v|.€/lq dy
ugrq dY
lgrq trv
ldks dv
alq fv
l4lq dv
lgre dv
|,c4s dv
lgtg tv
tigAg dy
*150x*tg%
!s4q dY
llElS trv
lglq dY
$g{q dY
lyxs dY
!04q dry
lgkS drypS/tS fy
|rylqdy
*1flgrlfl %
|lBredY|Jdrs dv$/tg dY
$!Iq eY
rdEdvI'd& dry
Arg dv
lgrg dv
surE46 8081A
sw846 8082
sr!a46 @70c
I
1
1
I
I
1
I
1
I
I
I
I
1
I
I
I
I
1
I
I
2$l,lar{7 @-4p|{)7 7@1739 rG
523
52.3
5L3
52.3
52.3
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52.3
5L3
827
u7
e7827nf827
u7
?€]l,Eto7 3{l.l{ar.07 7031738 SM
z$M3r{t O3dIV{7 ?lB1l/4 lr.B
This tzboraurry rqod b noa ealil wirhou an a4dr4ded stg'@tE on th. @eer page .
. Repo.table D€tectiotr Limia BRL = Beiow R€porting Limia Pag€ l0 of 154
Page 161
Sample ld€ntificationM8F-8 2,-4'sA59803-02
Client Prciect #l 0 l - 88
Collection Date/Time26-Mar-07 00:00
MatrixSoiL
Received27 M -0'7
CAS No, An lte(s) Resu Flag U^i6 aRDL Dilatioa twethod Ref Prepa.ed Ana!]qed Batch Analtst
Srmivolrtile Orgrnic Compoutrds by GCMS
Ssmivolal B oroanic Comoounds bv SW846 8270CPrepared by mehod SW846 35508
5qe.0 B€n:o lalpyrene205-9s.? Berl:oiblfluoranthenels124.2 B€nzo {g,h,i) perytenem?-00-e B€rEoik)fluoranth€n€6ts5.o B€nzoic acidrm51$ B€i4laltohdrrl411 Bis(2drlorc€lhory)rnetEne111.14.1 Bis(2dttoro€h/)ether3s8.4 e Bis(2dtlorois€protyl)eher117.81.7 Etisl2sttytheryl)phthatate101-55,3 +Brcmoph€iyt phenyt ehere6-68.7 Buttb€nzyphthatateuj.74-8 calbazole5$50-7 4{hlorc}m€thytphsdl{16-473, l ,ChlorDeni l inB
91-s&? 2-Chlorcnaphhalene9557-8 z.Chtolopnenol7D05-72 3 4-Chloro9henyl phenytehet
218{14 Chrysenes+r03 Dibenzo la,h) anlha.en€132-64,9 Dibenzofuran95.50.r l,2,Didtorob€nzene54173'1 l,3,Didtlorob€nz€n6116.1$7 l,4,Dichlorob€nz€n691-9,1-1 3,3'.Didombenzidne120.33, 2,4,Ochloroph€nol34{6-2 DielhylphtEtate13i-11-3 Dimefvhhdale10567-9 2,4omehytphend8r-74.2 D-n-bryphihakte
534-52.1 46-Dinitr62{ehylphsol51.2&5 a4-DmtoDh€ml12114.2 2,4-tlnjlrotoluenem6m2 2,GDinitrotdu€ne117_&.0 D{-fl_odyllhfiatatea6-440 Fluo€ntfisne
110'7+1 Herachloob€nzene
tr€!.3 HexacntorDbuladenen414 HexachloMycbpenhdiene
6r rzt Hexact{orDehanere+3e 5 Ind€no (1,2,3-€d) pyr€fl€90.12{ 1+r€thy'naphhal€ns78.59-r lsophorcnosr-t$ 2-frehytnaphhat€|lee&,r&? z_Meftylpheiol
10s39-4, 3,4-Mehylphenol106.14-591.2c3 Naphhelslos&7,r,4 2_Nitroa ines${9-2 +Nilroenitine
BffL
BFL
BFL
BFL
BfrL8RLBFL8RL8RL8FL8RL8RL8fr18RLBRLBRLEHLBHL2,170BHLBRL8RL8RLBRL8RL
BRLBBLBRLBRLBFLBRLBFLBRLBRL8RL4 , t108RLBRLBFLB8LBFLBRL8RL8RLBRLBFLBRf,
BRL
8RLSRL
!94€ dry
!c4q dry
ldks dry
t94q dry
udrq dry
|lg/rq dry
udkS dry
|lg4rS dry
lqfts dry
ugrq dry
ldlq ry
|{y|q dry
!E*4 dry
!S4(S dry
tdrs dry
liS,tS dryp91q dry
US,tS dry
lStS dry
l4,4(s dryydls my
lsas dryps,4(sdrypsiq dry
lgts dy
lgkS dry
rcn.S dv
ldkS d'y
lgks dypqrc d,y
|l9fr9 dry
tS4q dry
!4rs dypSlq dry
!Sn{ dry
US4(S dryps/ksdry
lio/kg dry
lgrs dy
IS,lq dyp4lq dypgrs dryps4q dy
lSeS drv
t4/rg dry
trylq dy
lSftS dry
lJg,4(s dry
lldks dry
l]dks dry
827
827
827
827
627
827
8?7
8?7
827
827
E27
E27
821
827
827
827p7
827
827
421
v1
e7
821
827
MI
827
827
827
827
8?7
w7
827
827
827
427
&1
427
@7
&7
827
427
82f
u7827
827
827
827
&7@1
e7
sw846 8270C
This labomlory repod is ,rol wIU teilhou an aathorized signsture on dte cot)er pagc .
* Repqiable Detectioo Limir BRL = B€low Reporting Limit P a g e l l o t l 5 4
Page 162
Sample IdentificationM8F{ 2,-4,
sA59803-02
Clie Proiect #301-88
MatrixSoil
Colle€tion Dat€lTime26-Mar{7 00i00
Received27 -Ma.-07
CAS Nd Analrte(s) Resuh Fl8 Unia rRDL Dilutio| Merhod Rel, Prepared Anzb.d Bdch Antlyst
Semivolatile Org.nic Coopound! by CCMS
S6mivolalile oroaric Comodnds bv SW846 8270C
Pr€pared by m€thod SW846 35504
100{1{ 4Nitroan'lir}6ga.Osil l.ftobenzslE
8|175.5 2-Nitfopfi€nol
100-n2-7 {-i6lroph€nol
62-754 N-tlitrosadhdMamin€
@14+7 N-iSlrosdi-l}poptlanin€
EG30-6 N.NEosodpienylanin€
E/€G5 P€l achhrophenol85{1-8 PlEnadfi@ne
1(F952 Plt€nol
t2940{ PWerE110{s1 Pyidnetm-€ar 12,+fridorcbenrene
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gta-a 2+Iwobiplldlyl
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29+&r-{f7 @A{47 7ff11n4 M.BBRLBRL8RL8RLB8L8FL8Rt-8RL8RL8RL5,65,0BHLBRLBF!BRt
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%50116 86.6
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' Reportrble tltection Limit BRL = Below Rcporting Limit Page 12 of 154
Page 163
SampLe IdentificationM8F-9 2'-4'sA5980l-03
Client Proiect #301-88
Collection Date/Time26-Mar-0? 00:00
MatrixSoil
Received
27-Mar Q'7
CAS No, Anabtte(s) Result Fl4S Anits 'RDL Dilutinn Mcthod Eetr. P4pared Anabzed Batch AMIFI
Volatile Organic Compounds
VoC Efiraclion
Volatile Oroanic Compolnds
Field €nraded
Prepared by mettod SW846 5030 Soit (high tevet)mr': 1,1,2-Trid orotrifluo.oethane (Freon BRL67-6+r Acelone BFL107-13 r Acrytcjnitdte BFL71-492 Benzene BFL10316 | BomobHzene BFL14 915 Bbmochloomslhane BFLfin4 BromodichtoronefEne BFL14252 Srcmdom BFL7.1-&3I Emmom€tlan€ BFL7&93.c 2-8utanofls (i,tEK) BFL104.s1-8 n-Sutylbenzene BnL13+90.8 sec.Srybenzene BFL9846.6 led-futy,berz€ne BBL7'1s4 Carton disullid€ 8Bts623.s Celbon tdBchlodde BRL
VOC z})Jat4l 28tl,a47 7031761 BD
!C4q dry 61.7
pS4qdry 1230
lglqdy 61.7
pg4q dry 61.7
US*S d'y 61.7
PSIq dv 61.7
US4iS dy 6lJ
W^g dy 61.7
lgftg dy 123
|{Asfy 617pg/l(0 fry 617
tJg4(g dry 6lJ
I0ft9 dry Bt.l
|lg/l(S dry 308
!gA0 dry 617
tCIq dry 61.7
pCIq dry 123
|lvtS dry 617
Msdry tn
lMS dry 611
lrytgdry 51.7
lJgftS dry 1a
|1g^g dry 6l-7
lglq dry 61.7
tyls dry 6r.7
pglT(S dry 61.7
PSAS dr!' 61 7
p!4q dy 617
psAS dry 123
usilq fy 61.7
pS,?.S dy 61.7
!s/ks dy 61.7
pgrcdy 61-7
t'drq dy 61.7
ldlq dy 61.7
tgtlq6,J 61.7
lJdlq dry 61.7
fdksdy 61.1
lo4€ dy 61.7
9dhdry 61.7
l44q dy 61.7
yEre dy 6t.7
lSlq dry 617
!S4S dy 61.7
ru4q ey 61.7
Mq dry 61.7
tgts &y 617
tidh dy 617
tidhdry 617
sw 816 02608
108.9G7 Chlorobenzene75ill3 Chloro€lhane6756 3 Chlorolom/147.3 ChtoromettEne!r5.t9 3 2{hlorotduene10e'|3-4 ,l{hlorctctuene
9e12.0 [email protected] Dibomo4hloromefian€106.93-4 l,2,Obromoehane(ED8)7495.3 Dibornomelhane9+501 1,2-0ichlo(ObenZene54173r l,3.oichloaobenzen€106-45 7 I,4_Dic+ oj.obenzene75-71-8 Dichtorodnuoromelhane(Freon12)16.34-J l, t Oichtoro€than€107{S2 1,2{id1lorc€than€75-35-4 jl-Dchloo€lhsne
15sss.2 ciel,2.Dichtoosthene156rt0.5 tans,l2-Dchloroelh€nen874 l,2.Oc.l{oopropane142-28.9 l,?nidnooproo€rcs9+2G7 2,2.0ic1{oopropanes695€.6 l,1-Didomprcpone1061{1-5 cis-l,S.Didlloropropdl€1006l.02-6 rans-1,3-DidioropDpsne100-tl-4 Ehylbenzene6r{&3 f{exadttoobubdiene591784 2_He|anone (MB(|
S-!?-8 lsopropyftenz€ne99.€7-6 4lsop.opyltoluene1q',1{4.,r Mehyll6nbutyleflerr0&1cr 4+retiyl-2f€nlanooe([{BK)75{9-2 Mehytenechloride91-2!.3 Naphhat€ne
8FL
881
8Rt-
BRt
BBL
8BL
BRL
8RL
BRL
BRL
B8t
B8L
BRL
BFL
BFL
BFL
BFL
SFL
SRL
BAL
BET
BfrL
BRL
8nL
BRL
8RL
8Rr
BRT
BRt
8RL
8RL
BRL
BRL
BRL
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
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50
50
50
fi
50
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This laboftlory rcpod h ,tol tald v had an althodztl signat!rc on tfu cowr psge
* Reportable Dete.tion Limit BRL = Belovr Repofling Limir Page l l of 154
Page 164
Samole ld€trtificationM8F-9 2'-4'sA5980t{3
Cli€nt Proiect #l0l-88
MatrixSoil
Received27-Mar-0'7
Collection DatdTime26-Mar-07 00:00
CAS No. Aaolrta(s) Resak FloS Unirs rRDL Dllaliaa trIethod Rctr Prcparcd Analyud Bzlch Argtyst
Vol.tile OrgE tc Co|Ipourds
Vdaile Organic Cofilo0nds
Prepared by method SW846 5030 Soil (high tevet)
1q]-6rr ftPrcpytodone 8RL1m{25 StyrcE 8RL630roi |,t,1,2-Telract{oro6lhan€ 8RL?9.3't5 t,t,2,2-T€trac orc€thene 8RL121.1n1 Tet|adrlooef|ene BRL1os.€r.3 Tolueoe BFL
!761'6 l2,$Trinbrob4nzene 8FLr2o-xar 1,2+Tri* orcbemeno 8RL
7r-s5+ 1,1,1-Tricldoro€tEne BRt
a+5 1,1,2-T J oEe$ane gR[
7941{ lri*brdn€ne BRL
T**{orofiuororcftele (Freon 111 BFL
Flo{ 1,2,}Trit oropmpane BnL
S.6+6 lz+Tf,mghylbenz€ne10s.6I{ 13,$Ttifl*tlylbeozeneTsor-4 Vinydthrids1@&7 m,Fxyleie9647{ DXytaE10!r"9$e Tetr*ydDtuan
@&7 Eqt{et€rg€,HE-8 Teil€myl medry' eltter
67q2-X E$yl brt-tdyt edler1@al3 O-rsoprwyl eh€f
7s3fl1 Tert-Sutenot / hiyt alcohol,'91n 1,+otorane
A,40.4 +ErffiofrN$en|ene
&7161 [email protected]
ttM474 |,2-Ac otoelhene44
l@-5J-/ Dibtonofi@rhalhane
Exlrsctrble Pelrolcum Hydrocsrbons
Eftaclabl€ Total Pgdeum tlydrccarbons
Pr€Oared by method SW846 35508
ffi31.9 Gesdne
6.76{02 Ft€toil*z
6t17+i|ln Firel Ol *4685t${+4 FUelOtt6li0806jo0 it otoroil
"m100mo Aviati)n fuel
t nt sttitd
odl€rOl
Tot l P€totEUm Hydrearbdls
CS{36 AiiDrlaUc Mmarborts
Ne&2 l4ttM&ca1e
Semivol..dl€ Orgretc Compoutrd! by GC
Ouenod odn€ P€sli.ii€s SWE46808'lA
Prepared by method sw846 3545A
3@{l}2 A|ddn
8Rt-
BRI.
8RL
BAL
8FL
BFL
8Rf
BRT
8R|
BNL
BNL
BFL
97
101
v109
8RLBRLBRI.BRLBFLBBL
2450Cdqihbd as2,4S02,450
14:J
pg4q dy 61.7
lqredy 61.7
UdkS d'y 61.7
$/rqdy 61.7
tlgrstt 61.7
r4/hfy 61.7
l4/ts dt 61.7
lryrS d.y 61.7
udhd] 517
l4/lqdy 61.7
tJgU dy 61.7
tlE}gay 6r.7
dts fy 61.1
llg/rs fy 61.7
|lg/tq dy 617
Blqdry 6r.7
lgLS *y tz3
tg4q fy 61 7
l4^Sdy 61/
p0/t€ay 611
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7Gl$ %
701f i%
701f l%
76130%
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1t 40 %
|lgrg dy 333
sw 8{6 82608
+CT ETPII
5050503)505050tu505{l5050fi5l)505050505050505n65050
02dtr-07 oe.tpr{7 7040017 rn€r
2gn ar.07 30lilar{7 7mln2m5 16{b 1
605 1
605 1
605 1ql5 I
m5 1
66 I
606 1
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sRt s1846 80814 ?€4a-07 {P.AorO7 7G17JB TO
This labonrorf Eqorl is 60l valid l'ithotd dl zurtodad dgEthtn oa the cawr page.
. Reporbble Delectior Umfi BRI- = Bdow Reporring Lirbil Page 14 of 154
Page 165
Sarnple IdentiticationM8F-9 2'4'sA5980l-03
CIient Proiect #301-88
Collection Date/Time26-Mar-117 00;00
Mat.ixSoii
Received27-Mar07
CAS No. At'alyte(s) FoS Unir: 'RDL Dilarinn Method R4 P,elnnd Amlfzed ga!(h Anabtt
Scmivohtil€ Orgenic Compounds by cC
ooanocilodne Pesbcides SW846 0081 A
Prepared by method SWM6 3545A
319-84-6 a-BHC31s85.7 ts8HC319-aS0 d.BHC5&8e-e +BHC (Ljndane)
671+9 Chlordane7?-54-8 4,4'O0D (p,p')
?l.ss-s 4,4LD0E (p,p')
50-2$3 a,a'{oT (p,p i6S57-1 Diet&in959-93{ EnCjoSUIan I3213{5-9 Endo6ulla0 ll1031{7 0 Endostllan Sutlabn2!8 Endin71219X.4 EMin Aldehyde76-44-0 Heptachlor72-.13.5 Mefioxycitor1024 t-3 HeptadrJor Epoxide3mr.3r2 Toxaphsne51037r-9 a.chlodan€tt66.34-7 gthlordan€
5las4 7c5 Endrin Keldre
t0w41, 4,4oe4dafl|&tofulEnt4 l9l,051.2+3 DecehlooMhenyl(St
Polyoh/o[?aled Eiphends bv SW846 8082
Prepared by method SW846 35454
1267+1r.e PCB !016111042+2 PCB 122111r4r.r&5 PCB 123253469.219 rcB 12421267129-6 rcB 1 24€r !097 69.1 PCB 1254]1096{2-5 PCB 1260t:1321-21-5 PCB12621 1 r @ r 1 { P C 8 1 2 8 8
1t30644? 4,4-DSoclanuodiplEnyllsl
20s124-3 Deachl1tohohenyl(St)
Semivolrtile Organic Compounds by CCMS
Semivolalib Orcanic Comoounds bv SWg46 8270C
Prepared by method SW846 35508
83.32-9 Ac€naphh€n€208.96.8 Acenaphthylene61.53-3 Aniline1N.12-7 Anhracene19122+9 Afaane10133-3 Azobenzene/Dipheq4diarine9e-87-5 &nzidine56-5t3 Eenzo (a) adhracene
BRL
BEL
8RL
BRL
ERL
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8RL
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104
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105
BRL
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BRL
8RL
1,700
611
67.7
67.7
671
87.1
67.1
671
677
671
750
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750
750
750
750
750
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tgr(g ory
tCL ! dry
rSfrS dry
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lsnq dv
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!94q dry
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!dl(g dry
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tqtS dry
wl f l%
&1f l%
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3G1fl %
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!sr'{ dyps,'lg dry
ldks dry
ldred,ylsnq fy
sw846 8081A33.6 1
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169 1
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sw8{6 8270C
28-Mar-07 30Mar.07 7031738 SM
?9tt^t47 c&Apr 07 7031774 M.B
Thb laboruaory rcpod k ,toa tolid wAhoul ad a.llho.ized slpzlarc on the coter page.
' Reportable Delection Limit BRL = B€low Reporting Limit Page 15 of 154
Page 166
Sample ld€ntificatiooM8F4 2'4'sA59803-03
Client Proicct #30 t-88
MatrixSoit
Collection Drte/Time2GMar47 00:00
Received27-Mar-07
CAS N.L AmlrE(s) Fl"C Unlb *ADL Dilaion Method ReJ hepued A tlwi Bdch An^lyst
S€tr|ivolatile Otgrnic Compounds by CCMS
S€mivdatle Oruanic Cdnooun& bv SW846 6270C
Prepared by rnelhod SW846 35508
50n2{ 8€izo (alpyrcnem5.992 o€nzo(b)ffuoranfieoe191242 Bel\Io (g,hj) perji€ie
Ar.0s9 8€{zo(k}lhroanh€fe65'85{ &nzoic ejd1651{ B€nzyj ahoholtrr.!r1.1 Bis(2dfurethoxy)rnetEne11r-4r4 Bir(2d'loroot{)ater386!e32.9 9ie{A.dlbdscpropyl)€fier11t41.1 8b(Z€httrsxyi)phrhdatorn5s.3 +B{crnotaHyt pherryt efter0F4s 7 Bulyt beryl phhatete
s.?'t-8 Cadszolos$sc7 ,t4hlotoFlne{Vph€nol
10Ga7ll 4.chloro€nifin€sl,5+7 z.chlotdBstfulei\ee$r{ Z-ChtolEpl,€nolM5-12-3 44ldorcFheny dslyi etr€r21041.9 OlrySen€51ti!3 Ob€nzo (a,hl antracene132-64.9 oibduofurans5so1 t2-Dicfilorobsdsr€5.1-73-1 r,ltkhlorobenz€nerc€..{e7 l,4{idbrcbenz€n€s1{+1 33--Dbhloroben2ljfl€12!.03? 2,+D**ttrophenols[6e2 Deftylphhatale|31-1r.3 Otr'€fttpftflalat€105+7-S 2,4-Dm4ph€nolw7+2 D,n+ulyj phhatate
a+52-r 4,MinitD2-mdhylpnenolsr.2o-s 2,+Dinitoptend121.14-2 2,+Dinitohtlene@2FZ z,FDnitobfu€ne117€,t-o oi.tuody pfit slate206{,{i FUoGn l€rE6n7 fl-orene1rs7+l ltBxichkcbe$lene&/$83 Hoxad{oobuladenen..74 HgxadoDalrlopentadi$efl-12.1 Hgx# oo€dUne1cl3ss ld€no {j2r3{d) pyrdt€$r24 l.lretldrBphfutae7&5$ | lsdlorqjo9157-6 2+ldiylfiNph$at€nec5.{&7 2lre$rylph€nol
toeiF{, 3,4.lr@phendl{t6-,4+5sr-20-3 t&phfid$e!+74.1 z.Nir@rilinos{s" fi,lito€n ins
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750
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750
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750
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750
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Thh toborubrf rqtod &r not asld fit hotd M atrrhodrrd sBnaUre od lhe cova page-
' R€portable Der€dion Limit BRL = Bebw Repodng Limit Page 16 of I54
Page 167
Sanple IdedtificationM6F-9 2'-4'sAs980l-01
Client Proiect #l0 r-88
Collectiop Date/Ttme26-Mar-07 00:00
MatrixSoil
Reccived27 -Mar-0'l
CAS No. Anatrte(s) Result Flas Units *RDL Dilutinn Metholt Rel, Prcporcl Aaalyetl Batch Ana\'rt
S€mlvolrtil€ Orgrnic CoInpornds by CCMS
Semivolatjle orcanic Corflpounds bv SWg46 8270C
Prepared by method SW846 35508
100-01-6 +Nitroeniline90.95.3 Ntdenzenen475 5 2,Nitroph€nolrm{2 7 4-Nilrophenol62'759 N-Nitro€odimelh!4amine621.617 N-Nillosodi-n-Fopyhmhes6 o 6 ttNilrcsodiphenylamine8r-36.5 pentachtoophenol
85"018 Phenantkenel@9$2 Phenol14940_0 pyaene
110-66r Pyn:dine120{21 l,2,+Triclorobenzenese954 2,4,5-Trid{oopherml3S062 2,4,6-Ticnbfophenol
gt@-o 2-Htbtobipherryl
6/-12-4 2-Fluotjphenol
1165404 M1$qzene4s
4t6542.2 Phenol-ds
t7t&514 Teryh€'ry|-d4
tt31 2,4,6Ttib@noghend
zJNar|T @lvo? 7031774 M.BBFL
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BRL
BRL
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3,9.10
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BRL
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57
52
72
50
66
45
754
751)
7fl
7il
1il
751)
750
750
750
750
750
750
750
udks dry
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fS.ftS dry
Udlq dry
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pdrq dry
pS/kS dry
lgks dry
!s/lq dry
ldkS dry
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pdkg dry
l01q dry
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30-1U%
15-110%
30-130%
tr l t0%
30-130%
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sw846 8270C
S1iv846 7471A
EPA 2t]O 7
Totrl Metrls by IPA 50{0/7000 S'€ries Methods
743€.97-6 Mero!ry
Total M€tlts by EPA 200 Serics Method$
74!0!224 Silver
74,|0.39.3 Badum
7440-43.9 Cadmium
14!o.11.X Chromium
iB$P,1 Lead
BNL
3 3 8
339
0.411
8.€
26.2
ndrq dry 0.43?2
n'9fr9 drr/ 1.08
mdkS dry t62
mg/kg dry 0.541
mgAS dry 0271
mS,ftS dry 0.541
mglg dry 0 812
n0,4qdry 1.62
mg/l 0 0100
m94 0.015,0
mM 0.0050
mdl 0.0025
nM 0.0125
ngl' 0.m040
mM 0.007s
rng,r 0.0150
@-Aprfl 6SAtr07 7031810 YP
H8
ns2.1s-2 Sdenium BRL
SPLP }Idth by EPA 1.312 & 6000t000 Series Methods
SPLP Extraclion ftmdeted
7440.24 Silver BFL
7,t4G3S2 Ajs€rjc BBL
71!0.39-3 Badum 00106
7140<r.9 cqdmium 8RL
7411047-3 Chromium BRL
713$t-6 Lle{c!{y 8nL
7€S9ar Lead BRL
na24s.2 setenium 8RL
C€nerrl Ch€mistry ParNm€tcrs
% Soiids 90.6
Sw€461312 ze.lna4i 2&i,lar{7 7031763 BD
SW84613126010g 3&i,lar{7 @.Apr{7 7031805 LB
Svfi$1312t74794 ' 02-Arr{7 7031806 YP
SW8461312/€0108 ' 02-A9r{7 7031805 tR
SMzslocirod. 3041a47 n-Nal'07 7031879 YLl
This la.bofatoueport is not raIU x'ithout an aahottad sig&nne o" the uee. page .
. Reportable Derection Limit BRL = Below Reporring Limir Page l7 of 154
Page 168
Samole IdcntificationMtF-r0 t'-4,sA59803-04
Client Prciect #301-88
Collection DatdTime26-Mar-07 00;00
MatrixSoil
Received27-MaF07
CAS No. Anolra(s) Resul! nag U,'i'l *RDL Dih tion Methad ReI, Prepann Adrlyzed Bdch Analfst
Volafl o OLlanic Cqrmunds
Pr€pared by method SW845 50354 Soit (lorr levet)
Tsiil-1 1,12-TrichlorotdfluoEefiano(Freon BFL@&1 Acelone BRLron$r Acryl6nfie BRI71<f2 Benzene BRL1@-0G1 BDmlbg'Eene BFL7447.5 Brcmodlloaomelhane SRL7s271 godDdichbomefEne BFtEE-2 Brcnotoin BHL7r-899 &Dmcrn€liEno BnL78lIr-3 2-Bulanone (MEK) BFL10rs1{ ltsBuiytdlz€ne EFL
trr€6{ s€c€{Vt€nzone ERLgs{fi tert-Eutylbenzone 8RLE1i4 Ca6on diejlfide BFL5&?+s Cartd\ tsirad{odde BRL10&s'7 Chbptjsnz€ne 8RL?5.0c3 Chtofoe0lane 8RLlt{6.3 Cfilorofonn SnL7a{7-3 Chloro.nehan€ BFLs49.6 2-Cl orotolueno BRl,1(F-43-4 4-Ch'ofotdu$o BFt9612-8 tj_Obromo3d o.opropane BHI12'14!1 oibronbdioomeham BFL106!B-1 l,z.Dbrornoefiane (Eog) BFL7{-es3 Dbofibn|9hane 8RLsG501 j2{icnbrob€filene BHt541-7x1 1,$tlihlorooenzer€ BflL116_{$7 l+Ocf oobenzsne BffL7t7r-€ Dchhrodifuofdnethans (Freon t2) BBLIn34 3 l,l-oidllorceftane BRL107.0+2 j.?.0ichlordtlan€ BRL?!54 .1,1-ganlofo€tEne €,qL15&59-2 chl,Z-Dk orDotlone Bntrs6.6os fians.1z.Dcnto|Ddhgne BRLn&'s 1 2old oopmp€ne 8RLrtr2-r8{ i&D.fttsopro0ane 8Rt*2J-7 2:.D0t oropropang BnL5e50.6 l,l Ochtorogogare BFL10{6t{'-5 cts-.t,gDidloroprc!€ne BRL10061{2{ hans-lSoiohtooFDp€ne BRLl0o4r.. E$ytbenz€rE SRL
2&4a/{7 28.lllar{7 7031787 80
?9.{l/'u47 2$irt07 7m1790 RU
Volatile Org40ic ComFounds
vOC E{rftibn
07&3 fleEdloobLiadene
501-70€ 2-Hodlore(MBtqs-€e{ kopf4}tbstz€.I€&E/t 4lsogopythbffe
16314,r"l omy' t€+butt sttlgr1@rG1 4-M€dty1.2{*rb]q1e{MIBK)r5'G-2 lr€trliho€diorid€Er'2O-3 tlaptihals€
ldlq dy 7.4
l44q dy 141
i4/lq dy 7.1
!C4q dy 7.1
lgrS dy 1.4
la4q dry 7.4
ld& drY 1.4
tg/|qdry 7.1
wb dy 14.7
IrEh try 73.5
K/tq dy 7 -4
udbdy 1a
lglqdy 1.1
rrSASdy 368
ldh ff, 7.4
@r0frt 7t
lslqdy 117
IEIS dy 7.4
lErStu 14.7
ystS dry 7.4
uc4€ ('t 7a
E lqdy 141
|Jg/lg dy 7.4
lg4qtry 1.4
ldlS try 7.4
uc4q dy 7A
dl€dry r.1
lElS dy 7.4
lgrlg dy 14.?
Fdlq dy 74
Irdbdry 74
H&a 1.4lgrq dV 74FSIEtrl' 7.1
144€ dy 7.4
Uqnqdry 7 A
lClqdry 7.4
lg/rqdy 7.4
l4rg Ay 7.4
ldlS dy 1-4
lj9k dry 7.4
lgtg dy 74
lElq fy 735
lglq try 7.4
Fglq dy 7.4
pdlqdy 7.4
!919 dy ?3.5
!S/fS dy ns
pdlq d)' t.4
Fidd sxt'd€d voc
S'/V 846 82mI
1
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8R-8RL8nLBRLgFt_
Ihh llbo.atory ?qa|t is ,td yalid wiahod ad oartoitqd :tignafrare on the cowr We.i Repoftahle Detection Lirit BRI = B€low Repoaing Lirnit Page 18 of 154
Page 169
Samole IdentificationM8F-10 2,-4'sA59603-04
Client Proiect #301-88
MatrixSoil
Collection Date/Time26-Mar47 00:00
Receivsl2'7-M^t-0'7
CAS No. Analyte(s) Resuk FloS Unkt rRDI Dilu.ioa Itethod Rel. Prepoled Ann\rzed Barch Araltst
Vol.tlle OrBanlc Compounds
Volalile Ooanic Comoo{ndsPrepared by method SW846 50354 Soit (tow tevet)r03i!r n_propr,lb€azgn€100-42-s Styre$eff10 204 1, t,1,2.Ieta{htoroethene7s 3rr-5 1, j ,2,2_Tetlachtoroelhane12710.4 Tstrad onethene100 8€-3 Toluene0t.61-6 1,2,!Tri$torob€n:ene12{.8t,1 1,2,+Tdcilorob€flzene7r-55-6 1.1,1.Tridttorelhane7e.oo_s 1,1,2_Tri$torelhane7+01$ TricNoroeh€ng75 6e-4 Trlchlorolluoromehane (Fleon l 1 is1&4 1,2,3-Tdchloropropan€9543-6 1,2,+Tdmelhyibenzer€100t7-8 t,3,5.Trimeh!,jbenrene7Ir01{ Vinyldloride
1310.?G7 n,Fxylene95-47'6 oxylene109.9$9 Tetrahydoluran
60'29-7 Efrvlelher9e,L{s3 Tedamyl melhy ether637.9?-3 E$yttsrt-bl]tyi€lherr0s.20.3 Di,istprop/€lh€r7s{5{ Ted_Butend / bLrtyt almholrzJ.Sr-t 1j-Dioxar€
464CA1 4-Er1mon\O@beizene
to3/-26-5 Tdrcne$
17060474 1,2-IicllwoellBne-d4
186&53-7 Dihbfionwonahane
Exlrrctrbl€ P€troleum Hydrocarbons
ExlEclable Total Petrolefin Hvdrocarb$s
Prepared by method SW846 35508
m06-61.9 Gasolir€6617S1G2 Fuelol {?
6847631-3 Fu€lOl {4685s3{0-. FuelOl#6M)9€r)0c00 MolorollJ00]0OC0 Avjal'on FUel
unid€ndi€d
oher Ol
fotal Petole{rm l-lydrocarbons
C9{36 Aliphatic Hydrocadons
3J86-i3-2 lohlon$tadecane
Semlvol.tlle Orgsnlc Compoln& by GC
Orcanochlodne Pesliddes SW846 8{]81 A
Prepa,ed by method SWM6 3545A
$94G2 Al(trii
8RL
8RL
8FL
BRL
BFL
BFL
BRL
8ff1
BFL
BAL
BFL
BFL
BfrL
BRL
BNL
BFL
BFL
BFL
BRL
BRL
BHL
BFL
8RL
8RL
8RL
95
105
122
76
8RL
BBL
BFL
BFL
BFL
BFL
2,660
Calculaled as
2,660
2,660
151
Nrs$y 71
lgeg dry 7.1
lgkg dry 7.4
!S,lq d.y 7.4
lgrq dry 7 4
UdkS dry 7.1
pgkS dry 7.4
ldlq dry 7.4
|rg,,ltg d,] 7.4
!dk!@ 7.4
!S,1rS dry 7 4
ldlq dry 7.4
ligrq dry 't.4
fdlqdry 7.4
ldlq dry 7.4
pdks dry t.4
lEtS dry 14.1
ldksdry 1.4
ldrS dry 73-5
Uglgdry 7 4
ldlqdry 7.1
|Jdlq dry 7 4
pdkS dry 1.4
f4ts dry ?3.5
tdkS dry 147
7trt30 %
7c-t30 %
7G134 %
70tw%
ms/rs &ym94q dy
mYtg dry
mdkg dry
mg/k! dry
|ngnq dry
mgrq d'y
m94q dry
ndtg dry
n€/rg dry
4+110%
lSnqty 39.0
sw 6.16 82608
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n-M3t47 8-Ma4l 7431t90 RU
724
124
724
724
t24
724
724
721
724
721
29+lad7 3GMar07 7031772
BNL slli8{6 m81A 28.!larq ()q-Apr{7 m3173S TG
This lehorulory rcFnrt is aol wlu *ilhod an or.lhoti?eil signoine on lhe cover page .
t Reportable Deiection Limit BRI- = Below Reporting Linit Page 19 of | -54
Page 170
Samole [dentificationM8F-r0 2'-4'sA5980l-{x
Client Proi€ct #301-88
MatrixSoil
Collectiolr Dat€/Time26-Mar-o7 00:00
Received27 -Nlato7
CAS No, .4nslyt (s) Flas ,RDL DiIUion LTdhod ReJ Prcpa?cn Aaalwd Bateh A^zW
Semivolctile Orgrnlc Coflpound! by CC
Oroanodlorin€ Pesticides SWE45 8081 A
P.€pa.ed by method SW846 3515A
319.84{ +8HC319.95.7 bBl.tc319.06S dBHCss{$e gtsBHC (Undans)
t.11.9 Chlodane?2-5,r+ 1,4,-D0O (p,p )7as-!r 4J,-D0E{p,C}
502s3 4400T{p,p)m'5/-1 fiddin
Erd@jlEn I102r3{t9 EdGuIan ll1@r{7{ Endo6u[d| Sdlab,2-2n{ Enddn
7rr21-s-4 Edrh Atd$yde76-448 H€pracl or72"(3-5 il€Eroxyd orrE+r3 HeFfudJor Eponde8EO13t2 Tof,aphs€51ll!71.9 a{ihadan€s66t47 gchloadane
5i!94705 Endnn Keloalo
1@8641-2 A,+DB4cbtu athptenyt (Sr)
Nt2+3 Decachlotofiolw (St)
Poh/d odnated Ephenvls hi/ SW846 80€2
Prepared by method SW846 3545A
126r&1r? PC810161110+?42 l\812111141-16.5 rcB1232s.6+21-9 PCB 124212612-293 PCB 124S11qr-6s1 PC8l25!l11096-€?-5 PC81260tt3e+4s Pcg1V621t1@1rt-1 PCB 1268
rM44z 1,4{8-odatufr6iptsg$l
M144 D*J/ctiht(t,ifrr.,1yt F4
SeElvolrdle Orgroic Comporn& by (rcMS
S€mivoladlo Olanic Conoounds bv SW846 8270C
Prepared by method SW846 35508
lo.aa{ AcemphtErE208.96-0 [email protected] Aniline1 .t2-7 Anfirdc€ng1912.2+9 Atazirc1B.1go Azobgnz$oDiphorryktazines4875 Bquidine56'55t BsEo (a)anhresne
39.039.0
38.01S539-031339.03S0$i39.039.039.03S0393!9.039.01{153€O33.039-0
BRL
BHI
BNL
BFL
BFI.
BRL
BR.
BBL
BflL
BRL
BRL
8RL
BRL
8tuSFL8RLBRL8RLBNLBFLORL
$Ig dYpgrg dY
wrg dI
lglq dv
|lgl€ ffv
|ldlqdvtAtg dY
lglq frY
$nrg dy
lgrq dY
udls dv
udlq dv
lglq fv
uSftS dry
W*edryldts d'y
lgkdvrgh trY
lls/}s dv
$/tS fy
|a4q dv
*1fl
* | f l%
u94q dy
tgts tr),psrs fitlg/lq dy
udh drvpglq dry
dro d]!s.4q fvtiSAS dy
3Gtfi%
*l f l%
s1{6,16 8081A
sw846 8082
sw8l6 82Zr
2&llarfl l}2-Apr{7 7(Bi7Jg TG
?,-|.e/41 3&Mdr{7 7031736 Stt!
E ei47 &1947 1fi1n4 M.8
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898
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Ikh tobonbry rqod is rrd idid wirtou ar, tr/,thodqd tUnaare on the coyer page
t Reportable D€iestion Limit BRL = Below Rcporting Linil Page 20 of I t4
Page 171
Sample IdentificationM8F-10 2,-4'sA5980l-04
Client Proiect #301 -88
MatrixSoil
Rcceived21-Mat-0'1
Collection Date/Timc26-Mar-o7 00:00
CAS No. AttlJ,te(s) FIoC UEib *nDL DilutiDrt Prcpuel Amltz?t Bdth Andbst
Semivolatile Orgstric Compound! by GCMS
Semivolalils oroanic Cornoounds bv SW846 B2Z0C
Prepa.ed by melhod SW846 35508
50-32{ B€nro (a)pyrene205.e9.2 Eenro F) nuoranthene19124.2 Bs02o (g,h,i) perytene207-0s s 8€flzo {k)ffuol?rihene6t-85{ 8€nzoic acidl0csr 6 Benzyt ahohol1 r 1-s r ' r Bts(2{htoroethory)nelhate11 1 .14 4 Etis(2{hlomeh}4)ether39633 324 &s(2drtodsopropylielter1r73'7 8ts(2+fiyiheryt)piihalate101-55.3 +Brunophentlphenyle$eret-6€-7 tuMb€n4iphhalate96-74-8 Calbazole595.!7 +Ctioto_xlrldhytr'?f,l(r''10647.S 4{hloroanilin€91.5&? Z{hloomphthatene9&s7-8 Z-Chloophe{ol7005.72-3 4-Chloophen!4phenyleth€f218{1.9 Chrysene5?/0-3 oibenzo(a,hlanthracen€132'84.9 Dtbon2ofuan9+sG1 1,2-Didorobenzenes41731 l,3-Didrlonberuene10616.7 l,4_Dichtorcbenzene9r'g,{-r 3,3-Dcfitorobenzidne120.33.2 2+Dicnbrcphenolu{62 oiethyl phlhaiate
131-1r-3 oimehgphf\aiale105674 2,4.Dimelhyiphsldu.74.2 oi-n-butylptihatates34.52-1 4,6-0ioitrG2-melhylphatd51.20.5 2,+Dnivophenolt21.1+2 2,4{iniuotohrenem6.2G2 2,6{iniEololuene117.€4.0 Din-odt4phthatale2C5-14 0 Fluofafllh€ne
r18 74 1 Hexachlofobenzene37-€&3 flexehloobdadienen414 HexehloD€yd@eflladiene6J:/7-1 Hexachlorcethanere13s5 Indeno 11,a3{d) pYrcne
9G124 l-M€tiylnaphlhdene7!-59-1 lsophoronesr.575 2-MslhylnaphtEtene96.{&7 2_ €thylFh€nol
10t.3s-4, 3,+Mehylphsnol$G.4-5s1-2O3 lhphthaleneN.7+1 2-Niboan ins99{92 }Nitroariline
BRL
BFL
BHL
BFL
BFL
BFL
BFL
BFL
BFL
BFL
BFL
BFL
BFL
BEL
BRL
881
BFL
BFL
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8RL
SRL
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BRL
SRL
8RL
8RL
8RL
8RL
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SRL
8RL
8RL
2,680
BRL
BBL
BFL
BFL
BFL
BFL
BFL
BRL
8RL
8RL
8RL
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8RL
us^s dylgfu my!S^S dry
lls/}sdryps^sdry
us^sdrypglsdrytld](sdrypg}sdrvpsfts dry
rcAs dry
!S4S dry
lgks dry
lrat\S drl
|]s^s dry
lEkg dry
!Yt(q dry
us^s ryl'ls/ls dry
Nksd!'l!S.4q dry
llgts dry
uqts d.y
ldkS dry
lgra dy
lJs4to dy
ldle *v
lgts dypgtsd'ypyrs dy
!91tS dry
|Jgt€ drypcts dry
Utlq dry
udts dry
rclq ftv
ldlq dry
lqkS drypSeS dfy
t44q &y
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$ts dy
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lStS dry
lgkg dry
!c/k dry
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ps4(sey
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838
898
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This lzborzaory rcpon k ,oa jvlU xtithoat tn asthoriud slgnalarc tA the rver psge-
* Reportabt€ Detection Limit BRL = Below Report'ng Lirnit Page 2l of 1J4
Page 172
Sample Identific6tiopM8F-10 r'-4'sA5980l-04
Client Proiect #l0 t-88
MahixSoil
Collection Date/Time26-Mar-07 fi):00
Received27-Mar-07
CAS No, Analyk(9 R.sdt FIAS Urrits *ADL Dthttioa Mahod ReI, PEpaRi Analfeed Botch An4lrsl
Semivslrtile Organic Comportr& by GCMS
Sentuolane Or-Eanic Comoounds bv SVlS4li 82mC
Preparcd by method SW846 35508
100.011 +NitofltiirF$115.3 l,llrob€iEgle8s755 2-ilitoph€nollsdat +NirophdDl@-754 NM.r6Odim€hyiam{l€@1417 MMtocodi-ngopyhnine&3ll-6 N+,litosodipneqdernine874$5 pg]bd oaophenol86-{114 PhemnlhGrei0&9+2 Pnenolla}{l-o pyYene
trH&1 foidneral82.r 12,+Tri*lorobenz6n€9€'o5.. a4,tTri$lorcphenols{e2 2,4,eTridttooph€nol
@1&3 2-Fket@
fi7-124 "Fhgqlwot116ai@4 'VfooDedle-ds
41654a-t Pt|€ro,ns
tn&514 lotdwrJl44
n&84 zl$nbrq@t€nd
8Rr-BAL
BFL
BRL
sRt-88L
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g
47n,E
66
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1 0 1
6.54
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rdkg dv
ldkq r!/
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*130%
15.l10%
xt lN%
t r n 0 %
Ttn%
t6n0%
mdks dty 0'(B68
mdkg dry r.!l
mg,Iq dry 1.65
mgag dy 0.553
'ng/hdry 02n
rtlS/r,g dry 0553
mdlqdry 0 830
mtrsdry t 94
mgl 0.0100
ngl 0.0150
mS, 0.0050
ngr! 0-ll0?5
mS, 0.0125
ng4 0.(m1{]
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sw846 6270C
sr{E46 7171A
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2$Mar{7 0}Apr$ 7031114 MB
Totd Merrts by EPA 60o{V7000 Scrt€s M€rhods
7(19.s76 MeroJry
Tot{l Merrb bt EPA 200 S€ri6 MEthods
7a,044 SituEr
?{4}9&2 Als€oic
7|l$59n Baiun
7l{0-4}9 CadtiuT
,4{0{7-3 Olmmiom
7r3+4.r Lead
v82+2 s€lerfum BRL
SPLP Mel.b by EPA 13 12 & 60001000 S€ris M€thodt
SPtPExftrdon Comdd€d
14{044 Sih€r BFL
741(1.3&2 Alsenrc BRL
t4('-393 gaiun 0.q160
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7(89|.6 tii6rury BFL
[email protected] Leed BRL
7,12.'192 S€l€ntum BR.
Cencrsl Ch€sistry Farsmt{crs
M-,{r47 034pr{7 70318t0
7.8
8 7 5
@.&r{7
80.1
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Sw845131260108 3!luar{7 m-Aprl)7 7081805 LH
SW8461312/14704 ' m-Apr{7 71181806 YP
SW8461312/6016 ' 024pr-07 m3i805 |.n
$12!t{l G ilod. 3} ar{7 30'liladT ru1879 Ytil% Solids
P4e22 ot 154
Thh |a.!toto.t fp*t X rrrtadU NAhoar an auhortzzd signeoe oE the coj6 pagc.
i Reptrrable Detecrion Limit BRL = Betow RepodinC Limit
Page 173
Sample ldentificatiorM8F-l l2'-4,
sA5980l-05
Clielt Proiect #l 0 l - 88
MatrixSoil
Received
27-Mar-0'1Collection Datc/Time
26-Mar-07 00:00
CAS No- A"alrk(s) Resutt FIag Unia 'RDL Dilutil,rl Method ReJ Prcporcd Anallzed Betch Ahabal
Volatle orcanic Comoounds
Prepared by m€lhod SW846 5030 Soil (high levet)
7r.r3r 1,l2-Trichtorotdfluoro€hffB(Freon 8RL61.*1 Acetone 8RL107r3-r AcMonilnle BRL714!2 8€nzene 8RL103-3t1 8mfi\ot€nzene 8RL7'l s7 5 Bo|rlochloro'n€than€ BRLrr27-1 Eono(ichtoromethane 8RL
ErDndlom BRL74.03-s BrDmom€flane BRL78 e3 3 2-8ubno{€ (MEK) 8RL10,ts1-8 n-Buvtbenzene BRL135-9&3 sec-Eutylbenzene BRLs{6.6 terl-$rtyibenzene 8RL75154 Ca6on dtsdftde 8RL
56.2$s Ca6on telEchtoride BRL
108.9G7 Chlorotrejzme BRLi5{G3 Chtomefiane BRL
67{6-3 Chtorolonn BRL
14.8r-3 Chb,o'rledian€ BBLFe B 2-Chlorcbluene BBL10G.434 {-ftiorohluene BFLF12 3 1,2{ikome3drloropropane BBL124-181 DbomodrtorcnEthane SFL
106.93.l i,2,Dikonoelhane (EDB) BffL
?44s.3 Dibronhelhane BFL
9+50.1 1,2-oichtoobenzene BFL
541.711 l,3-DcHorcbenzene BffL
'06:45-7 l,4-Dtciloobenzene BFL
757rr Dichtorodifluoromethane (Freon12) BHL
7534,3 t,t-Dd oroethane BHL
1cr!$.2 l,2-Dichloroethane BRL
7s354 l,l nidbroethene BRL
28.{farfl 2l-Mar47 7031767 B0
O2-4W47 02-ApF07 70,{0017
volNtite Orgrnic Compourds
VoC Enraction
pSAS dry 67.3
ldks dry 1350
PdkS dry 67.3p94q dy 67.3
!g4g dry 673
ldkS dry 673
|lgr'tS dry 67-3
lgkg dry 67.3
p94q dry r35
Pdre dry 673
lSredry 673
ldq dry 67_3
!S4(S dry 67 3
gg&griry 336
ldkS dry 67-3
pdks dry 67.3
lyq dry 135
p9?€ dry 67.3
vdtodty 135
t€/rS dry 67.3
P$S dry 673
|]g4S dry r35
lgkS dry 67.3
|Jg,4(S dry 67J
lsrls dry 613
lS.ftS dry 67.3
!S^g dry 67.3
ISAS dry 67.3
lClq dy 135
!g4q dy 67.3
!SI,.S dy 67.3
|lg4S dy 67.3
pdks dry 67.3
lsnq dy 67.3
p91q dry 67-3
ldkS dry 67-3
lStS dfy 67.3
pglq dw 67.3
|44q dry 673
Pdrq dry 671
!9+S dry 673
pg*s dry 67.3
lS.ftS dry 673
lgnq dry 67.3
!{it.cdy 67.3
!9rg dry 67 3
U0Iq dy 673
ldk€ dy 673
pplqdy 673
F eld exlraded voc
sw zu 8260a
BRLBRL8RLBRLBRLBBLBFLBRLBFLBflL8RLBRL8RtBRLSFLSRLBRL
50
50
50
50
50
50
50
50
50
50
50
50
50
50
5D
50
50
5t)
50
50
50
50
50
50
5l
5l
50
50
50
50
50
50
5{)
50
50
50
50
50
50q
50
5{l
50
r5e5s.2 cis-1,2,Drdoroetkne
1545 tlans-1,2-DidoD€lhene
4S7-5 l,2,Dichtorcpropane142.2s9 l,$Dichtoropopan€
w.2ot 2,2-Dichlorcpropane
563.rS4 l,1-Didoropop€ne10061{r'5 ci5-1,}Didiorcgropene10061{2-6 lran6,j,}Didlo€prop€ne100-111 Efrybenzen€0753 3 H€xaal Oobuladien€59r.73-6 2-Hsx one (MBK)
9A{2-3 lsopmpybsnzsn€998/{ +lsopropylofuene1641.0,r-4 [4etvltM-tulyleherl0&io'1 4-[telhyl.2?edanorc(MIBK)
7s2 Mehylene dioride91-2G3 llapittdqe
Thk laborutory repor, it not jslid wilhoua an euthoi.ed sigdatun on the cowr page
t Reporrable Derection Limit BRL = Below Reporting Limir Page 23 of 154
Page 174
Samole ldentifica6onM8F-u 2.4,sA5980l-05
Client Pmiect 4301-8E
Collection Date./Time26-Mar-07 fi):00
Received21-Mar07
MatrixSoil
CAS No. An!b@(s) Resuh FIag Uatb *RDL DUsliad Met'od R4. Pftpued Anzlyzed Bd.h Andlfsl
Yol.tlle Orgrnic Compourds
Vohtle Oroania Comoo|'l(lg
Prepared by method SW846 5030 Soit (high tevel)
lm.6'1 n+@pylbqzeno BRL
100-,125 slyreje sRt-
ac2ll$ t,1,1,2-Tetladtoroeflane BnL7+34-5 t,1,Zl.T€trad oroethane BffL1n-10.. Tetnd oo€fion€ BFL108-$-3 Tofuae BBL
87-€1{ 12,3-Tnchbaooenz€n€ 8RLt20€2r 't2,{-Trid oro0€{zeno BfiL7r_sE-G 1,1,1-Trid o.oghans Bf,L,9rxt5 1,i,2-Ti*bro€dlan€ 8FLII4I3 TftfiDrc€dl E BFL7s94 Tndlordluorfi|gbane {Frmn 1 t, 8Rf9618-4 lz,STridrloropl'opano gnl
s4$.6 1,2,+Tdm€fny'benzene BFL100.67{ l,3,FTnrnedrylbenzene BRL75-01{ \.hy' d orftle 8RL1SO.2G7 m,Pxt6ne 8RL95476 oxylene SRLlollllrse Tefahydofuran BFLdr2s7 Etryefw BRL
99{45-8 T€nsrrylmohylehd BRL697s2'3 Ehylhn-hlu eher 8FLr06a!3 oii$popytdt|or BFL75-65{ Ted-B{hrbt/ hrylatcoftrt BnL1&91-1 1,4{io{afi6 BRL
1@@1 4BonofrJoobenalE fiNr-4-5 ldtwc4S 101t706oa74 lz'ok:ltbrEfndne44
t8dn-tt7 Di&ottofiw@|€tlr€ne lM
Ertrctable Petroleum Hydrocrrbons
Edraciable Tod Peudqrn hdrocadons
Pr€pared by merhod SW84ti 35508
oe.Aprfl m.AF{7 7(Kxlt7 nalwh dy 67.3
|jg/k! dy 671
l4lq dy 57.3
$Iqdy 67.3
lglq dry 67.3
|lglS dV 673
|4/l€ dry 671
$lq dy 67.3
$/lq dV 67 3
lgrq dy 67.3
pg/kS fy 67.3
lglqfy 67J
|lglkg dy 623
ldlq dy 613
UdkS trt' 67.3
pghdrv 673
lg4qdry 135
|lg/|(! dy 673
|Jg/}S trI 673
ldlS dY 67.3
|4irg dy 671
$/t€ dy 673
lglq dV 67J
|gl(s rv 6nug*get 1s0
TVtn %
7r\1&%
7813t) %
70-ti4 %
n'S*Sfi 6s2
IIdh dy 652
ngilqdry 65.2
'nglq dry 652
rfldkgdv 652
fldkS dry 652
mdlqdry 452
mgnqdry 65.2
mytg d] 652
mg/kq dq 65?
4+110%
sw 846 82608
+CT ETPti
50
50
50
50
50
50
50
50
50
50
50
5n
50
e)50
50
5t)
50
50
50
50
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mlF614 Gssolme6{|e3C2 Rl€t Ott268476-11-3 Fueloil#40166!{0-1 Fu€lo{t t6r,{98c0000 li,lotoroilJ0010@0 Aviatio|| Fu6l
uilidsnifi€d
ober 0dTdd P6lrole./m gdocadois
CS{36 Alqffic Hydr@fto(B
&rrD@e rd@latrsi
J386it1? 14lfutwta&eE
Semivolatile Orgrdc Compootrds by cC
oroanod odne Pesticil€s 5$/846 8081A
Prepar€d by method SW846 3tt5A
$s+2 Aldrin
BFLgRL
8RL8qLBFLBRLBRL8Rr,BRLBRL
ta
BRL pglq dry swB46 808rA n$alo7 u2-4cl{7 7IE173g
Thb ,obo.alory rcpod k not yoli4 tdrhoal a arlhodzad signafine on lhz cove.IRge.
i R€portrble D€tection Limit BRL = Below Rcpding Limit Pag€ 24 of | 54
Page 175
Sample IdentificationM8F-lt 2L4'sA59803-05
Client Proiect #301 -88
Collection Date/Time26-Mar-07 00:00
MatrixSoil
Rcccived27-Mat07
CAS No. Anatyeb) Rcsult FloC Ania *RDL Dilation Llzthod Rel. Prcpored Arc$zed Balch AruLtsl
Scmivolrtile Organic ComFornds by CC
orcanodibrine Pesticlies SW846 8081 A
Prepared by method SW846 3545A
319r4i a_BHC31s85 7 tsBHC31946-3 dBHC5ars s 9BHC (Lindane)
'/-71.9 Chloidanep.54.n
4a _oDD lp,p )72-56.s 44-DDE (p.p')
s0-el3 a,a -00r lp,p,)6G57.1 Dieldin951,.9€.8 Ericdlllan I332196+9 Erdosutan ll1061-07.8 Endosullanslllate72-20-n Endrin7,r?r,s4 Erdin AtdehyGfi44 a kdacntoru3.5 Metlorychtolroe4 573 Heplachtor Epoxrde0001 15, Toxaphenes103 71-9 a-Chlordan€5566-3,17 g-Chlordane
53494.7'5 Endin K€lcme
103t6-81-2 4,+D&(Nanuorcbi$entt (Si
fr51-24-t De.a orcbiphe / (Sr)
Potuchlorinated Eiphen!,ls bv SW846 8m2
Prepared by method SW846 3545A
!257+1r ! PC81016r 04.2s2 PCB 12211114r 165 rc8123i2$169.2r-9 rc81242p6n-2+6 PCB1248r1os76+1 PC81254110s6S2-5 PC8 126037u4-23-5 PC81m21r1m 11-4 PC8 1268
t03&-8+2 4,4-Dgl,aanuoronFtunt4(St)
m5t-21-3 UcachknobiofEnl$|
S€nivolrtile Organic Compounds by c,CMS
Semivolatil€ orqanic ComoounG bv SW846 8270C
Prepared by method SWB46 35508
33'32 9 Acsnaphh€ns203-963 Acenaphfiyieno62-53-3 Aniline1tu12.1 Anfr&€ne19122+9 Alrazine103333 A2ob€02€n6,Diph€nyldialine92-87-5 genzidine
Benao (al anhraccne
BRLBRLBRLBRLBRLBRLBRLBRL8RL
BRL8RL8RLORLBRLBRLBRLBRLBRLBRLBRLBRL
62107
BFLBFLBFLBFL8FLBNL8FLBRLBRL
ffi
105
33.2
33.2
33.2
332
165
332
33.2
33.2
33.2
13.2
33.2
33.2
33.2
n233.233.28.2166
33.2
33.2
332
lyks dy
!s4q dy
!s.4q dypg4q dry
lsnq dy
tig.4q dry
us.4q dypS/kS drypSikS dry
!s4q dry
!S/kS dry
lsas dry
US/kS dry
!gl$ dry
lllas dry
!s&s dry
ldk€ dry
!s/ks my
tr!/kQ dry
lgeg d]
!s4q dry
fi-150 %
3+150'n
!s4q dry
!g]|(S di]
pdxg dry
PqtS dty
lgkq dry
!s4q dry
tjs,ks dry
r{vlq dry
!S/kS dry
wt50%
3+1f l%
!s,4q dy
t/gftsdylgrq dryps,tsdry
tgks dy
xtlq dry
lgkg dry
tCksdty
su,/846 €081A
sw€46 Er)82
swt46 E270C
664
664
66.4
6 6 4
66.4
66.4
66.4
66-4
66.4
28-Ma(07 02.Apr07 703173s
28tta(07 30-Mar-0i 7031738 Slvl
ZS+,laro7 03'Apl47 7031774 M.8808
80€
806
808
808
808
sm808
BRLB8lBRL
BFLBFLBFLBRL8Rt
Thit laboratory repod h nol ealA n'ilhou an auhoriud siqrutlure on lhe corcr page .
a Reporoble Detection Limit BRL = Below Reporting Limit Page 25 of 154
Page 176
Sample ldendficationM8F-ll2'-,1'
sA59803-05
Client Proiect #301-88
MatrixSoil
Collection Dat€/Tifte2GMar-07 00:00
Received21-Mar47
CAS No. Anatflz(s) Fbg |RDL DiIuiM Method ReJ Paparcd Analwn Babh Anoltst
Semivol.tile Org{tric Compoltrds by GCMS
Serivdalil€ Orcanic Comlouds bv SW846 Pe70C
Prepared by method SW846 35508
$'32 s Eeruo (a) plmng
20ss2 Sgnzo (b)ffUo{v hene191-242 Bgnro {g,h,i) D€rftne207{&9 B€rEo(k)0uoranh€ne6C85 0 BdnrIJiC rcid10r!51{ BsEyta|conol11141-1 Bis{2dlloroehory)fiFt|€ne111-4,t4 Bis(2dorcery)dhe.s€48-32{ 8is{2dordsop&pi)dh€r!17+1-7 8E{2€hyh€xy)pt{hahtel0r-5s3 +Ercrnoph€rM pl€ryt slherBffi'7 &M bon4l phthdale
&f44 Calbazol€5s,5{r7 44oo+melhylpt€nol106-471 d4 oloatitino915&7 24tfuonaphtha/sne96t8 24Ho(ophetd7m6.72-3 {{llsoohe$ytph€ny'stlei210.01-9 Chrysenes0-?u3 Dibsruo i4h) arthfacon€l@6,14 Dben2ofurin9&5G1 1,2{)idlo|Db€.Eenes,rr-7iir 1,$Uanbrobeftene16.467 l,4ohlorobsnr€ne91€4r SSoidiorob€flridne120.83.2 2,+DdtorophsEl04{6-2 D€fly' drtuJalo13111-3 D{nrehylphhalate105{ttt 2,a.0inehMph$d&r+2 Di4-bdyi ptdEtate
531-52'1 4,eDinib+24$dtrylphexol5r2&s z,4.0rtffophsnol121112 2,4.0iduobtueisoG2O2 2,GJiriroblueneIri-o/}{ Dfl.ttphhahte?!6144 FuoraJ,|,tst€
!S7J7 FluOtEn€l1€.7+l tlenclorob€nzeie87€.3 Hemd*l@butad€n€tu74 Hexado@qdop€{ndiere
-n1 H€xaddoE€haae1s+3e5 Ind€m(1,2,3{d)pyrsle
s12{ 1{.|€dryjnphfial€ne7€.59r lsootlo|one91-rt 2+t€dvtrleshhalei€1646-7 2-lrofttiht'arol
1fi-39{ 3,1.fr€0ryhhstd10€-4i.59r.20.3 llaphfralene
0&7r-a 2.1{itmnit'fls00-0+2 3{tt(rdrttrn€
BFLBRLBR.8FT8RLB8LB8LBRLSRLBFIBnI
snlB8LBRL8RL8RL8RL8RLB8L8FLBRI8RLBFI.BHLBflLg8L
BFLBRI.BR.BFL
BRLBflLBFLBFLBRL0R-8RLBNLBALBFLBRL8RL8RL8RLBRLBRLBFL
8Rt-B8L8H-
ugrq dy
lgrq dv
!g/rg dly
tdrg dv
|rsnq dv
rsre dv$4q dv
!s4q dr)'
uc4q dy
|ldkS dty
|dhdv
uglq dYpyrsdv
$gks dv
wh evrjdh dv
lrylq frvpE/l€ dy
!gL0 dl'
lgls dv
lgk fiv
!g/1€ rYpgh dY
ldks d'Y
ugtq dv
lErs fy
!E]q fiv
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lldksd'YUS,lq dy
|jg}s dy
lErg fv
!S/rS dy
|ldts dy
rcnq dY
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fhis lztontory rcpott is ,rd vaUd uahout an a&l*otlz.d signaure o,. the coecr page.
. Reportable Det€.rion Limit BRL = Betow Reooding LiEir Page26 of 154
Page 177
Sample [dentificatiopMtF-lt 2'-4'
sA59803-05
Client Proiect #l0r-88
MatrixSoil
Rcccivcd2'7-Mar-01
Collection Date/Time26-Mar-07 00:00
CAS No. Analytc(s) Resull FIaS Uaits *RDL Dilu tn Prcparcd Andwn Bztch Analrsl
Semivolrtil€ Orgrnic Compounds by GCMS
Semivolalile oroanic Compounds bv SW846 8270C
Prepafed by method SW846 35508
100'01$ 4-Lljlroaniljru 8BL9€'9ss NiFob€nzene 8RLo&7ss 2-Natophenot BRL100-02-7 4-Nitophenol BRL62_75_9 N-Nitrosodmehylamin€ 8RL@1-6+7 l{.Niliosodi-n-propylemin€ BRL06-10-6 N.Nitrosodrpl^e.Mamine BRLflt6-5 Penlacilorophenot BRL05{1,8 pherEnhrene 8RL100-9t2 phenol BRL12940-0 pyrene BRL110.0F1 4rndine 8RL1n'a21 1,2,+Tichtoobenzene 8RL9ss-4 2,4,5-Trichbrophenol 8RL$116-2 2,4,6-Tridrlorophend BRL
@160-a 2-Fhnobiphenyl 5,fi/124 2-FluoroplBnol Sa4t65nM Nitrcbenrseds n1185n2-2 PheMUS 4t1/1e51-0 feryhent+da 75lt'ns 2,4iTtihornophend 49
Totrl Metals by EPA 6000,rru0 S€rie5 Method!
€-Mad7 03Apr{17 7031774 M.BlJg+tSdry 3230
!94q dry 808
ldkq dry al8
lgrq diy 3-?30
u94q dry zu
u94q dy 808
USrkS dry 8{l€
ti9kS dy EoE
lsas dy 80€
lsAs dy E0€
!9ks dy EoE
PSI(S ('y m8
lEkS dy 808
pslq dry m8
lSIq dy 808
3+130 %
15110 %
3U130 %
15-110%
3&130 %
15-110 %
r'q?{ dry 0.0338
mqkS dry 1.10
mS,?.S dry 1.64
rnS,1q dry 0.51|8
"dkg dry 0274
mdrq dry o.:l'E
m94q dry i-|n
tn9,k9 dry 1.€4
mgn 0.0100
mqn 0.0150
n91 0 0050
mql 0.0185
mg,l 0.0125
mg4 0.0@10
m!,,1 0 m75
'ngrl 00150
sw8,46 8270CI
I
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7139-97{ _ Metcury
Toaal llet ls by EPA 200 S€ries M€rhodr
74{o-u4 Silver
?,rlG3$a Badum
7,t4I1439 Ca*niun
71rra 47 3 Chrcnium
/aq.92r Lead
]?l!492 S€lenium BFL
SPLP Metrts by EPA l3l2 & 6000/7000 Sedes M€thods
SPIP ExtrJclion Compleied
7414-22-4 Silver BRL
71.4033 2 A6enic BFL
74{G39 3 Barium 0.0fi}5
7'llo-43I Cadmium BRL
t41a!7 x Chromium BHL
7it3e9?{ l,lerorry BRL
7+lser Lead BRL
r@-ae 2 S€leflium BRL
G€nerrl Chcmistry Prrametetr
% Solids 88 6
0 342
BRL
7.8S
760
o515
s08
152
st{846 7471A
EPA2M-7
SW8,161312
s-w&61312/60t08
sw8461312Ir470
sw846 t31 Z60t0B
SM2540 G Mod.
02-&r{7 03-Apr,07 70lr8l0 YP
H8
28-l'1a47 28.ilar-07 7031763 80
30-Mar{7 02'AF-07 7031805 LR
' @.Apr{7 7031806 YP
' 02-Apr47 7031805 LH
30.{'lar.{7 3$Mar-07 761879 Yl',!
This lsbomtory HNd h ^ot vald withrlt aE s$thorized slgnalurc on the cowr prye
I Reportable D€rection Limit BRL = Below Reporting Limit PaE 27 ot 154
Page 178
Sarnple ldenti ficationM8F-t2 2'-{'sA59464-04
Clietrt Proi€ct #30t-88
Mat ixSoil
Receivedl9-Mar-07
Collection Datel[imel5-Ma.-07 m:0o
CAS No. Aqrlyt4s) Resak Flas Aab *RDL Dihtthn Llahod netr Prcpared AnaPzed Bdch Analfsl
Vol.til€ Org.nic Compounds
VOC Extraction
ISlkgdty 4.9
t,€ikgdty 9E.6
PSn(g dty rt.g
ldks dry 4.9
Fgts dry 4.9
ldks dry 4.9
ldks d.y 1.9pg/ls dry 4.9
!g/kg dry 9.9
ldkS dry 49-3
t dks dry 4_9
IdkSdry 4_9
ldkgdr, 4.9
ldkS dry 21.6
Ueftg dry 4.9pdkS dry 4.S
Ug/lqdry 9.9
Idtg dry 4.9
rcr(S dry 9-9
ldkS d.y 4.9
tidks d.y 4.9pg/r(g dry 9.9
lSfl(gdry 4.SgdkSdry 4.9
lSlkS dry 4-9pg/tg d,y 4.9
IdrSdry 4.Sygrsdry 4.s
[gtS dry 9.9
t grko dry 4.9
ldkgdry 4.9
|lgn(g dry 4.9
ldkgdry 4.9
!s/kg dry 4.9
t g@ dry 4.9
Ig/kgdry 4.9pdksdry 4.s
ldkS dry 4.9
fldlg dry 4.9
I'gkS dry 4.9
t4/*S dry 4.gydkgdry 4.9
ldrg dry 49.3
ldkSdry 4-9
lSit€dry 4-9pS/Xgdry 4.9
ldkgdry 49.3
ldkg dry 49_3
ldtsdry 4-9
20-ltat47 20''.,ar4? 7031156 8DField extracledVolalil€ O.oanic CompoundsP.epa.ed by rnetlnd SW846 5035A Soit (tow tevet)7F111 1,1,z-Tri€frlorcfinuoroelhane(FreoSRL6?€+1 Ac€lone 8RL107-1+1 Aq,ylonible BRL71-4+2 Eenzen€ BRL108{6-1 Bromobenzene BRL714r-5 BmmochhrometlEne BRL71274 Brcrnodiclloromethane BRL75-2+2 Baornoform BRL74{}9 Bromomethaoe BRf78-9+3 2€utanone (MEK) BRL10,!-51+ tuBulylbenzone BRL13+9€{ sec.Bulylbenzone 8RL98{66 te(€utylbenzene BRL75-l$o C€rbon disulfide 8RL56.23-5 C€rbon tetehtoride BRL1O8-Cr7 Chlorcbenz€oe BRL75.oGs Chloroethane BRL67€6.3 Chtoroform BRL74{7n Chbromethane BR!95-19{ 2-Chtorctotuene BRL10643-4 4chloobluene 8RL96-12{ l.2oibrono-ktloropropane BRL124.18-1 Dib@rnocf$oromethane 8RLioca34 l,2oibromoef|ane (EOB) BRL74-9rF3 Dibromome$€ne BRL95{01 l,2Srchlorobenz€ne BRL541-73r 'l,3tichlorpbenz€ne BRLl06a6-7 I .+Dichlorobenzen€ BRL75-714 DdJorcdifuoromehan€(Freon12)BRL75{4n t,lohNoroe$tane BRL107.06-2 1,2-Dichlorc,€thane BRL7+3s4 1, I Obhlofoeth€ne BRLl5€-5s2 cis-tJ-Dichloro€th€n€ BRL156{cs t€nel,z-Oidttotuethene BRL78{7€ |,2-Oichloropfopane BRL142-2€.9 l,3oichloropaopane BRL59a-2Gr 2,2-Dichloropropan€ BRL563-58€ l,l.Dichloropropene BRf10061415 cis-1,3-Dichloropropene BRLt0c6r{2$ bans.1.}Dichloropropen€ BRL100.41.1 Efiylbenz€ne BRL87{&3 Hexachlorobutadiene BRL591-784 2-He,€none (MBK) BRL9€{2{ lsopropyibenzene BRL99-€7{ +tsopropyltoluen€ BRL1634{4-4 tvl€thy' tert-buFy' eher BRL10s10r +Meury'l-2.pentanone(Ml8K) BRL7s+r.2 Methy'€ne chtoride BRI_
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SW 846 82608 21 -ttla.-o7 22Jt €r-07 7031 233 lR
9l-i+3 tlaphthEbne
Page lE of lJ2
Thb lzbortroq rqo.t is ro! ealid wifua ad dtdtori?td slgfi tke oz th2 coeer ?tagc.' R@rfable Dctecrio{ LiEir BRt = Bclow Reporting Limit
Page 179
Sample IdentiftcatiolMtF-I2 2'-4,
sA59464-04
Client Proiect #301-88
Collection Date/Timet5-Mar-07 00:00
Mat ixSoil
Rec€ivell9-Mar-07
CAS No. Anzbte(s) Resull Fhs Uni/5 'RDL Ditaaion Meahod Retr. PPpaHd Atubaed B eh AnalFt
Vohlile Org.nlc CompoInds
Volatile Oraanic ComooundsPrepared by method SW846 50354 Soit (torr,/ tevet)
7s59-4 Trichlorofluoromethan€ (Freon 11) BRL
10165r n-Propylbenzene10042-s Styrene630-206 1,1,1,2-Tetrachlorcethane79-34-5 1 . 1 ,2,2-Tetrachloroethane127-184 Tetrechloroelhene104{€-3 Toluen€87-614 l,2,STrichtofobenzene120-82,1 1,2,4,T.ichtorobenzene71'5s'6 I,I,l.Trichtoro€thene79-oG5 1,l,2.Trichtofo€thane7941-6 Trichloreth€ne
s6-18'4 l,2,3.Trichloroprop€nes5€35 1,2,4-Trimethylbenz€ne108-67-8 1,3,s-Trimethylb€nz€ne7s{1-4 Vnylchlorider33O,?C7 m.p_Xytene95-475 O-Xylene1(A-99-9 Tetrahydrofuran60-2+7 Efrylettlersg4{€.0 Tert-amy' methyl ether637-92-3 Ethyltert-butylether1D&2!-3 Di-isopropylethe.7s€t0 Tert-Butsnol / butyl alcohol123,91-1 j,4_Diolane
Sunogate rccowdes:1604t14 +Bromolluorobenzene
m3r.2€-5 Toluenedg
1 7 0604? 4 1, zDichlorcethane44
186&53-7 Dibromofluorcmethane
Extrsctrble Pelrole|rm Hydrocarbons
Exlractable Total Petroleum HvdaocarbonsPrepe.ed by melhod SW846 35504qxl641-9 Gasoline58174302 Fuetoit#26847&313 Fuetoit#46€55100-1 Fuet oil /{15l\.109800000 Motor OilJ001 00000 Avietion Fuel
unid€ntified
Otl,er Ol
Total Petloleuft Hydrocsrbons
C9-C36 Atiphetc Hydroc€dons
Su/rogate recoveaiesl
338+33-2 1-Clrlotoodedecane
Semirolatlle Orgrnlc Compourldr by GC
Oroanochlorine Pesticidos SW846 8081APrepared by mettEd SW846 35508
309{+2 Aldrin
SW84682608 21-Mat47 22-Ma(07 7031233 TRBRLBRLBRL
BRLBRLBRLBRLBRLBRLSRLBRL
BRL8RLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRL
103105101104
BRLBRLARLARLBRLBRL263Cal laled es263263
pgkS dry 4.9
ldks dry 4.9
lgikg dry 4.9
!g/kg dry 4.9
ldks dry 4.9pg/kg dry 4.9pSl(S dry 4-9
ldkS dry 4.S
lgftS dry 4.9
UgkS dry 4.9
ldkS dry 4.9
lig/kg dry 4.9
lCkg dry 4.9
!g/kg dry 4 9
!9kS dry 4_9pcks dry 4I
UgftS dry 9.9
lgkg dry 4.9
ldkg dry 4s.3pqkg dry 4.9pStkgdry 4.9pS/kS dry 4-S
ldkS dry 4.Spg/kS dry 49-3
ldkS dry 98,6
70-t m %70-130%70.tm %70-130%
mgfl(g dry 34. I
ndl(g dry 34.1mg/kg dry 34.Inglkg dry U.Img/kg dry 34. ImdkS dry 3. ImS/kS dry 34 1'rldxg dty 34.1m€/kg dry 34-1['SI(S dry Uj
40-140 %
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+CTETPH 21-Mar{7 2 '1+vlar{77031167 DS
ldkg dry sw846 8081A 2O.Mat47 25-Mat47 7m1068 TG
Thh lsbotuaary nFo.t is ttot ldU trithou an auhodzed sigaature on the coeer page* Reportabl€ Detection Limir BRL = Below Reporting Limit Page l9 of 152
Page 180
Sample IdetrtificationM8F.12 2,-C'sA59464-04
Clint Proiect #l0l-88
MatrixSoil
Collectioo Dste/TimeI 5-Mar47 00:00
Receivedl9-Mar-07
CAS No- A,uiyz(s) ResJ|h Fleg aalts iRDL Dihriat Maho,l Rel Prcpa.ed ,lazalz"i Batch ,laalyst
S€mivol{tlle Orgetric Comporrdr by GC
Omanochhdne Pesticides SWA46 808 | A
Prepard by mehod SW846 35508
319€44 a€HC3r9.S5-7 b_BHC319-86-8 d-BHC58{99 gFBHC (L,ndane)s7-7+9 Chlordane72s+8 4,4-DDD (p,9')
72-55-s 4,4.DDE (p,p.)
5o-2e-3 4,4-DDr (p,p')dr.57-r Dieldaln95s-98$ Endosulfen I$2ra65.9 Endosulfan tlt03t474 Endosultensultatef2-2o4 Endain7421-93-4 ErdrinAldehyde76-14€ Heptad ori24+s Mehoxydtlor1024-57,3 flsplachlor EFoxide8OOl3t2 Toxapltene5103-714 a-Chlordane5,566-3,t-7 g_Chbrdane
s349+705 Endrin Kebne
SurrogaG €couEnies.1o38M+2 4, 4'&Oclan uorcbiphenyt (St)
2051 -zaa Decachhtobiphenyt (Si
Polychlo.inated Biohenvls bv SW846 8082PrepaEd by rnettbd SW846 3545A
1267411-2 PCB t0161110+28-2 PciB,12lI1tl,rr-16,5 rcB 12325346s21-9 PCB 124212672-84 PCB 12481toq74s1 PCB t2541t096{2-5 rcB 12603732+?3-5 PCB 1262ii10G14-4 PCB 1268
Sutqele Bcot/Elks:| 0386a+2 444goclaf u?,'ohiptlFJnyt (Sr)
2051-24,i Decachlotubiphenyt (Sr)
Serdiyolrfle Orgrtrtc Conpounds by GCMS
BRLBRL
BRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRL8RL8RL8RLBRLBRLBRLBRLBRL
47109
BRLBRI.BRLBRLBRL1.150970BRLBRI-
4045
sw8{6 8061A
sw846 8082
udkSdry 6.48
IrgkS dry 6.48pgftgdry 6.48
fdkS dry G.48
rdkSdry 324
WkS dry 6.48
US/IS dry 6.48
ldrg dry 6.48
usftsdry 6.4€pSikg dry 6.40ps^gdry 6-41)
Udrgdry 6.40
lgkS dry 6.48pdkSdry 6.48pdkgdry 648
FS/kS dry 6.48
ldksdry 6.4a
rgks d.y 32.4
Pg/kS dry 6-,18
lglS dry 6.48
ISrkg dry 6.4a
30-t 50 %3Gt 50 %
pgrsdry 13-0
TSrkS dnl 13.0
P+ftS dry 13.0
Ig/kg dry '13.0
lCAgdry 13.0
ldkS dry 13.0pdkgdry 13.0
rcftS dry 13.0
lgrsdry 13.0
3G150 %3f.150 %
1tI
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?o-I!,.ar'47 2$te(47 7m1068 TG
21-Mat47 23ttlar47 10311€/.
22-t\-tar{? 24-i&f47 ?0312?g M,B
Semlvolatile Oroanic Comoounds bv SWe46 B27OCftepar€d by method SW846 3550883t2.9 Acen@htlEne21ls968 Acenaphdly'ene€A-5t3 Aniline12Gt2-7 Anthracefle1912.2+9 At€dne10333-3 Azob€nzent/Dipheny'diazines{7-5 B€nzidine5d€+3 B€nzo (a) dnlhrEcofie
8Rr_BRLBRLARLBRLBRLBRLBRL
ldlg dry
ISftg dry
rcas dryt S/kg dry
t4lkS dry
FS/IS dry
|lgiks dry
ldks dry
846
E46
846
8,tos468468466,16
sw848 A270C
Thk lzbordory Eport ls nea yalid withadt on qstt oried slgrrdtue on thc cava page -+ R€porbblc Det€ction Limit BRL = Below Repofting Linit Psge 20 of 152
Page 181
Sample ldentificalionMtF-r2 2'-4ts45946+A
Client Proiect #301-88
MatrixSoil
Collection Date/Timel5-Mar-07 00:00
Receivod19-Mar-07
CAS No- Aaolrtz(s) Resull FloS a n s IRDL Dilatioa Method Ref Prcpffed Anaqrrd Eatch Analrst
Semivolalile Organic Compounds by GCMS
Somivolatile Oroanic Compolnds bv SW846 O27OCPrepared by method SW846 35508
50 32-€ Benzo (a) pyrene
205-99,2 Eenzo (b) nuoranthene1e1-24-2 Benzo (g,h,i) perylene
207 08 9 Benzo (k) ffuoranthene65rto Benzoic acad100-514 Benzytalcohol111-91-1 Bis(2dilorcethory)methane11r-444 Bis(2-chloroehyl)eth€r3963&32-9 Bis(2-chloroisopropyl)eth€l1 1 t-81 -/ Bisl2-ehylhexyl)ph&ratate101-s5l 4-Bmmopheny phenyl €ther8564-7 Butyt benzyl phthalate86-743 CarbaZole595G7 4-Chloro-3-methylphenoi106173 +chtoroanijjne9158-7 2-Chtoronaphthalene9s,57-8 2-Chtorophenoi7005-72'3 4-Chtorophenytphenylether218 01-9 Chrysene53-70 3 Dibenzo (a,h) anthracene13?s-9 OibenZofuran9t5G1 1,2_Dichlorobenzene
4141,73-1 .t,3-Dichlo|obenzene
106-{67 1,4_Dichlorcbenzene91-941 3,3'-Dichtorobenzidine120-832 2,+Dichlofophenoln466-2 Oiethylphthatate131-11-3 Dmethylphthatate1r)5{7'9 2,4-DimeUrytphenolu-7+2 Dt-n-butytphthatete534-52-1 4,6-Dinitrc-2-methytphenol51-28-5 2,4-Dinitrophenol121-14-2 2,4-Dinitrotolu6ne606-4t-2 2,6-Dinilrotoluene117€4{ Di-n-octylphthalat€206444 Fluo@nthene6-7Tl Fluorene
11€-74-1 Hexachlorobenzene
87{s3 Hexachloaobuiadiene
77-4f4 Hexachlorocyclopentadi€ne
67-72-1 Hexachloroethane
193-39'5 Indeno ('l,2,3-cd) pyren€
90-124 f-i,lethylnaphthalene
78{9-1 lsophorone
91-57€ 2-Methy'naphthalene95-.{8-7 2-Mett\ylphenol
100-394, 3,4-Methytphenol106-4-t-591-20-3 Nephthaiene
E8-744 2-Nilroaniline
99-0+2 3-Nitoanitine
BRLBRLBRLBRLARLBRLBRLBRLBRL8RLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLARLBRLaRtBRLBRL8RLBRLBRLBRLBRL
BRLBRLBRL
lgkg dry 846
ldks dry 846
tidkS dry 8,16
USiftS dry 846
Ug/kg dry 846
ldks dry 046
IrS/kS dry 846pdkS dry €46pSn(S dry 846
ugKs dry a6
uS/r(g dry 846
Ugi@dry E46
lqKg dry 846
lsiKg dry 846
lrglkg dry 646
!q/kg dry 846
t SikS dry 846
!S/kS dry 846pSlkS dry 846
rcftS dry 846
ldkS dry 846
PSKS d.y 846
rs&s dry 846
rgkg dry 846
uSr(g dry 846
t4,'k9 dry 846
USftS dry 846
USftS dry 846
!g/kS dry 846pgftS dry 846
Ug,ttg dry U6pSftS dry 846
!g/kS dry 846
uSftg dry 846ydkg dry 846
tghSdrl 846
l,gkg dry 046y9ft0 dry 846
udkg dry 846
!s/kg dry 846
US/kg dry 846
US/kg dry 846pdrS dry 846
Ugikg dry 846
lslks dry 846pS/kS dry 846
t€ftS dry 846
pslqdry S46
r|dks dfy 846
!S/kg dry 845
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SW846 0270C 22-MarO7 24-Mat47 7O3127A M.B
Thit lzbontory npod it t ot vzlid withoat ad r horiAtt sigt ztuc on the covr Nge.* Rqortable Det€ction Lirnit BRL = Below Reporting Limir Pag€ 2l of 152
Page 182
Sample Idg ificationnfiF-r2 2'-{'sA59464-04
Clietrt Proiect #l0l-88
MatrixSoil
Receivedl9-Mar47
Colleqtiotr Date./TimeI 5-Mar47 00:00
CAS No. Analyte(s) Flq 'RDL Diluio Method Retr. Prcparul Analyzen Bdch Anabtsl
S€mivoltdle Olganic Comporrds by GCMS
Semivolatile Orqanic Comoounds bv SW846 8270CPrepared by method SW846 35508100{1€ +Nltnoanitine96€+3 Mtob€rEene8$7t5 2-Mtropftenol100-02-7 +NiaEphenolE?.75!9 N-Nitiosodimethylanxn€621{+7 lgl{trosodi-rFpaopytemine86-30{ t&NitrosddiFhenylarnine87{e5 PeotachlorophenolB54l€ Ph€mnthrene10&95t Ph€nolr2$oo{ pyrene
110-86-r Pyridine12(W-r 1,2,+Taicl{ombenzene95-954 2,4,tlrichlofophenol88{fF2 2.4,GTricftlorophenol
S{nrogate /€corrdries,'izlaas 2-Fluotobiphenyt67-t2a 2-Ffuorophenol1165$04 Nitobenzene4s1t65$2-z Phenol-ds1718.514 Tedlenyql4t1&794 2,1,€>Tribrcmophend
Totd Me{rk by EPA 60{M000 Serte3 Metbodi
I SW84A 8270C 22-l,llar9l 2+Met47 7031278 M.A
1 '
1 "
1 '
I '
1 '
1 '
1 '
1 '
1 "
1 '
1 "
8RLBRL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
766d67
u76
0.908
SRL
12.2
72.3
1 .35
16.0
339
BRL
Cornd€ted
BRL
BRL
0.0253
BRl-
BRL
BRL
BRL
BRL
82_8
Pgl(S dry 3380
UdkS dry 846pdkS dry 846pglkSdry 3380pdkSdry 8,16
ldkg dry 646
Igks dry M6
lgl€ d.y 8,16
ldksdry 846pgkS d.y 846
vgkgdty 846
ldkS dry 846
Fdkg dry 8,16pSAgd.y 846
ldkgdry 846
3L1fi%t r t t 0%30-130 %1s l10%30-130 %,81 r0%
mg/kgdry 0 0352
mS/ko dry 1.21
nrdkS dry 1.81
mS,kgdry 0.603
n4r'kg dry 0.301
mg/kg dry 0.603
nElkg dry 1.21
mgtkg dry 1.6r
r€I 0.0100
mgl o.015O
mg/l 0.0050
fign 0.0025
mgn 0.0050
mg/l O.00o{0
msil 0.m75
ftigl 0.0150
yo
743,9-976 Me.ojry
Toad M€lrb by EPA t00 Seri$ Metbods
7,14G22-4 Silv€r
74.40-3€,2 Arsenic
74{+3+3 Barium
7i!40-43-9 Cadmium
7,140{7-3 Chromium
7439.92-l Lead
7?8?-{s2 selenium
I SW846 7471A 23-tUar{7 2&Mar-07 70013ff} YP
1 EPA20O-7 2r+],€,t-Ol 24+tat47 7031305 HS
1 '
1 '
t '
t '
1 SWa46'f312 21-Vlar47 21+n€f47 7031229 BD
1 SW846 f31z6ol0E U+lat47 tuMet47 7U!1323 LR
1 '
1 "
1 ' ,
1 Sw846131217470A " 23+1.?r47 7031324 n'1 sw8461312i60108 ' 2$Mer{7 70313,i13 LR
1 '
1 SM25,l0 G Mod- 2-lht47 2+nef47 7031307 YM
SPLP Meldr by EPA lJ 12 & 60001000 S€ries Methods
SPI-P Exhadion71.10-22-4 Sllv€tr
7r40it&2 Arsanlc
Zr4{)393 Badum7.l,l04$9 Cad[ Um7140-47-3 Chro.nlum
7€e.97{ lfercury
743942-1 L€ad
n824S2 S€lsnium
Generrl CherDtlry Psl'metels
% Solids
Thft bfu@4ry .epF1 is naf wlid ulthout an ad@dzd signottre on tha @js '[ge.' Reporrabl€ Detecbn Limit BRL = Below Reporting LirDit PaAE2Z ot 152
Page 183
Sample IdentificationM8F-I3 2'-4'sA59464-05
Client Project #301-88
MarL{Soil
Receivedl9-Mar-07
Collection Date/Timel5-Mar-07 00i00
CAS No, AnalJte(s) Resuk Flos U.'its 'RDL Dilation Method ReL PEparcd ,4nal!.ed Bach AnalytVolatile Org.nic Compounds
VOC ExtractionVolatile Oroanic Comoounds
!g/r(g dry 3.3
UdkS dry 66 5
t S/kg dry 3 3
lrglq dry 3-3pgr$ dry 3.3pgl$ dry 3 3
tigkS dry 3.3pdks dry 3.3pSikS dry 6.7
Pg/kg dry 33-3
!g/kg dry 3.3
!g/kg dry 3-3
Ug/Kg dry 3.3
!g/kg dry 16.6
Uglkg dry 3 3
UdkS dry 3.3
!g/ks dry 6.7pdkS dry 3.3
lVftS dry 67ug/Kg dry 3.3
UEkg dry 3.3
lgkg dry 6.7gqkg dry 3.3
trgkS dry 3.3ggr'(S dry 3.3
UgkS dry 3.3
US/kS dry 3.3pdkS dry 3.3
WxS dry 6.7
PgkS dry 3-3
l4lKg dry 3.3
trg/kg dry 3.3
ljg(S dry 3.3pS/kS dry 3.3
W/kg dry 3.3pg/kg dry 3.3p.gKS dry 3.3pg/Kg dry 3.3
PdkS dry 3.3pgrs dry 3.3
lgkg dry 3.3
!Sn(S dry 3.3
tdkedry 33.3
!Sl(S dry 3.3
US/kS dry 3-3
!g/kS dry 3.3
!g/kS dry 33.3
!S/kS dry 33.3pdks dty 3.3
Field extracted VOC 20-Ma.-07 2clvar-o/ /031156 BD
Prepared by method SW846 S03SA Soit (tow tevet)76-'i3-1 l,l,2.Trichlorobifluoroethane(FreoSRL67{4-1 Acetone BRLr07-13-i Acry4onitrite BRLn1T2 Benzene BRL10e-86-1 Bromobenzene BRL74-97-5 Brcmochloromethane BRL7s-zr4 Bromodichtoromethane gRLT5-25-2 Bromoform BRL74{3-9 Eromomelhane BRL78-s3-3 2-Butanone (MEK) BRL104-51i n-Butylbenzene BRL135-98€ sec_Burylbenzene gRLga{ffi tert,Butylbenzene 8RL75-15{ Carbon disulfrde BRL5G23-5 C€rbon tetrachtoride BRL108-90,7 Chlorobenzene BRL7s-00-3 Chtoroethane BRL8746-3 Chtorcform BRL74€r-3 Chtorcmethane gRL95498 2-Chlorctotuene BRL10643-{ 4_Chlorotoluene BRL96-12+ 1,2-Dibromo_3_chtoropropane BRL124-4€-1 Dibromoc* oromethane BRL10G93-{ 1,2_oibromoethene(EDB) BRL74'95'3 Oibromom€thane BRL95 5o-1 I ,2. Oichlorobenzen€ BRL5.11-73-1 l,3-Dichlorobenzen€ BRL106-46 7 1,4_Dichlofobenzene BRL75-71-8 Dichlorcdifluoromethane(Freont2)BRL75-34-3 1,l-Dichtoroethane BRL10746-2 1_2_Dichtoroe$:'ane gRL7s-35-4 l,l.Dichtoroethene BRL15G5S? cis-1,2-Dichtorcehene BRt15ffio-5 trans-1,2_Dichtoroe{hene BRL78€7-5 l,2.Dichtoroprcpane BRL142-28,9 1,&Dichtoroprcpane BRL594-?0 r 2,2_Oichbrcpropane gRt563-58{ 1,l-Dichloropropene BRL10o61{1-s cis.l,3_Dichtorcpropene BRL10061{2{ t€ns-1,3_Dichtorcpropene BRL10@1a Ethylbenzene BRL€7€&3 Hexachloobutadiene BRL591-78+ 2-Flexanone (MBK) ARL98€2€ lsopropylbenzene BRL99{7{ 4_lsopropyltoluene BRL1634{a-4 Mehyt tert.butyl ether BRL108-10.1 4-Meffnyt-2-pentanone(M|BK) BRL7549-2 Methylene chloride BRL
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I
1
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1
1
1
1
1
1
1
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1
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191-2(!3 Nsphthalene
Page 2l of 152
Thit ttboralorf rcporl is not wli.l withod aa aahorhad stgaafurc on the cowr page.
' Reportable Der€ction Limir BRL = B€low Reporting Limit
Page 184
Samole ldentificationM8F-13 ?'-4'SA59,16f05
ClieftProiect#30r-88
Coll€ctioq Date/Timel5-Mar-07 00:00
l,tatdxSoil
Received19-Ma.47
CAS No. naabac(s) Fl4e 'RDL Dllutiatr Itahod Retr. Prcporcd Aubzed Borch Analtst
Volalile OrgoDic Compoutrds
Volatih Orqanic CompoundsPrepared by rn€thod SW846 5035A Soit (tow tovet)103{5-1 n-Propylbenzene BRLr0o-42,5 sb,rene63420-6 1,1,1,2-Tstrachloroethane79-3?L5 |,l.a2-T€Fadorcethane12 6a Tebachloroethene
YdxS dry 3.3
ldkS dry 3.3
ldrS dry 3.3pglSdry 3.3
Fdl(g dry 3.3
udkS dry 3.3pglro ffy 3.3pgtsdry 3.3
lgr(s dry 3.3
Idl€ dry 3.3p9/k0 dry 3.3ygkS dry 3.3
ldkg dry 3.3
ttgfiodry 3.3
ldkgdry 3.3
usil€dry 3.3pdlgdry 6.7
ls/kgdry 3.3
tNkS dry 33.3
$dkgdry 3_3pdkgdry 3,3
ldkgdry 3.3
tg4(e dry 3.3
t'gl/kgdry 33.3
rgkgdry 6G s
7Gt 30 %70-130%70-130 %70-1m%
BRLBRLBRLBRLBRL
BRLSRLBRLARLBRL8Rr8RLBRLBRLBRL
1011U114105
8RLBRLgRL
BRI-
BRLBRL8SSCatculsbd as899899
sw 846 826081
I
1
1
I
1
I
I
1
I
1
1
I
t
1
21-Ma(47 2trlet47 7031233 TR
i0B€83
87{1€
Toloene
75ir-4 vinytd{oride133G?G7 m,p.Xyt€nes647$ o-Xy,leflei0+9$g T€t€hydrofursn60-2s7 Ethylether99+@ Tert amyl m€thyl ether637-e2-3 Ediyl tert-but/ etheri08-20-r Di_isopmpylether75-65{t T€rt-Bubnol/butyjalcotlol12+91-1 1,4-Oioxane
Sa,,riDgate raco€abs--16040', +&omofluorcbenzene,w7-26-5 foluene4Slf 06047 4 l,2oichlo6ethane44t 868-5,+7 Abrunofr rfr lo m o th ane
f,xtrrcarbl€ lclrol€ m Hydrocarb{ns
EfJ9ctabl€ Total Peboleum Hydroca.bonsP.epared by method SW846 355088006414 Gasolin€68476-30-2 Fuel Oit #26847s31n Fu€l Oil f46855toc4 Fuet Oil #6M0e800000 lvlotof oitJ00100000 Aviadon Fuel
Uoidentifiedotta( oilTotal Petroleum Hydror4rbonsC$C36 Aliphalic Hydrocarbons
Surrogate /oooy€r,esi3J8el3'z 1-Chlotooctdde@ne
Semtvol.db Orgrdc Cohpo[I|rk by cCOroanochlo.in€ P€stic les SWE46 6Od1APrepared by mothod SW846 355083'o+ca Aldrin
1,2.$Tricftlorobenzene BRL12G€?r 1.2.+Trichloobeazeno BRL71.5rF6 l,t..l.Trichh.oethane BRL79{lr5 1,1,2-Tdchloroethane BRL79{t1{ Trichlorcei}Ene BRL7s{9-4 Trichlorof,uorofirethan€(Freonl.l)BRL96-18-4 l,2,$Trid oroproFne BRL95€3-6 .l,2,+Trimethylb€nzeno BRL1oS€7€ 1,3,5-Ttimehylb€nzene BRL
|ltsr(o dry 148mgrtg dry r4Emgffgdry 144mgikg dry 148nlg/kS dry 148oE/kg d.y 148nrgr'kg dry 148r'grkg dr/ 144mgilqdry 148dEl/kg dry l4a
4tr140
5
5
5
5
5
5
+cT ETPH 214a14't 2l-tttato7 f81167 DS
lryko dry 6.14 SW8,r6 808iA 2Gli.led7 2fliar{7 7l}31068 TG
This,abotuloq repod ls hot tatid tdthak! za rathorlaet sEnrturc on ahe coec, paE -' Reporhble Det€ctioo Limit BRI = B€low Repo.ting Linit PtgE 24 ot 152
Page 185
Samole ldentificationM8F-13 2'-41sA59464-05
Cliflt P.oiect #l 0 l - 88
Collection Date/Timel5-Mar-07 00:00
MatrixSoil
Receivedl9-Mar-07
CAS No. Analyt4s) Result Flae Units +frDL Dil,ltioh Method ReL Prepoted Anaryzed Belch AatlrstS€mtvolatiLe Orgroi. Cornpoutrds by cC
Oroanochlorine Pesticides SW846 808.1APreparod by method SW846 35508
319-84€ a-BHC319{5,7 b-BHC31$€6€ d-BHC58{9-9 g-BHC (Lindane)
5I-7+9 Chlordane72,54-€ 4,4-DDD (p,p')72-5rs 1,4-DOE (p,p.)
fi-2s3 4,4-DDr(p,p')@-57-1 Dietdrin959-98{ Endosulfan I33213-65-9 Endosulfun ll1031-07-8 Enctosulfan SulfateT2-2O-A Endrin7421 914 Endrin Atdehyde76-44{ Heptachtor724+5 Methoxydrtor1024-57-3 HeptechtorEpoxide4001-3+? Toxaphen€5103-71-9 a-Chlordane556614-7 gchlordane
53a9470's Endrin Ketone
Sunogate rscover'esr1038d8+2 1,4-D*Octafluorobiphenyl (Sr)
2051 -21-3 Decachlorobiphenyl (Sr)
Polvchlorinated Biohenvls bv SW846 8082Prepa.ed by method SW846 3545A
12674-11-2 PCB 101611101-24-2 PCB 122111141r6-s PCB , |232
5y6s-21,s PCB 124212612-294 PCB 12481r0s7{91 PCB 125411096-€2-5 PCB 12603732+2X PCB 12621110G14-1 PCB 1268
Surrogate recoysflesito38G8+z 4,4-D8-Octafluorobiphent4 (Sr)
2051 -2+3 Decachlorobiphonyt (St)
Semivolatile Orglnic Compoutrds by GCMS
BRLBRLBRLBRLBRLBRLBRLBRLBRLARLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRfBRL
4653
BRL
BRLBRLBRLBRL2,2601,240BRLBRL
4040
t4lkg dry 6.14
!S/kS dry 6.'14
!s/ks dry 6_14pdkS dry 6.14
lqkS dry 30.7
!g/kg dry 6.14
!g/kg dry 6.'t4
!g/kg dry 6.14
ldkS dry 6.14
Ug/kg dry 6 14pS/kS dry 6.14
ldkS dry 6.14
Ug/l(S dry 6-14pdkS dry 614pgks dry 6.14
!S/kS dry 6.14pS/kS dry 6.14
!g/kg dry 3O.7pg/kg dry 6.14
lgkS dry 6.14
UdkS dry 6.14
30-150 %30-150 %
lrs/'(g dry 12-3
lgkg dry 12.3pdkS dry 12.3
ligkg dry 12.3
lqkg dry 12.3
!g/kq dry 12.3
ldkg dry 12.3
us/ks dry 12.3pg/kg dry 12.3
30-150 %s0-150 %
t SIlg dry 736pg/kg dry 736
Lidksdry 736
ldkg dry 736
rdks dry 736
rcnS dry 76
US/IS dry 736
Ig/tS dry 736
sw846 8081A1
1
1
1
I
1
1
I
1
1
1
1
1
1'|
i
1
I
I
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m-Mar47 2541'ai-07 7031058 TG
sw846 8082 21-Mafi1 2rMafi7 703116/
Semivolatile Orqanic Comoounds by SW846 8270CPrepared by rn€lhod SW846 35508
a3'32-9 Acenaphthene208-964 Acenaphthyiene62.53'3 Aniline120-12,7 A,rthfacene1912-24-9 Atrazine103.333 Azobenzeneoiphenytdiaane92{7-5 Benzidines6-5+3 Benzo (a) anthracene
BRL
BRL
BRL
SRL
BRL
SRL
BRL
BRL
sw646 8270C 22'-MarO7 264llat47 7O3127A M.B
fhit lfionloq rcpoa k not vdid wirtoa aE azttoipn signaturc on rhe cot!4 page.
* Reportable Detecrion Limir BRL = Belov/ ReportinB Limit Page 25 of 152
Page 186
Sample ldentificatiotrM8F-n 2,-4'sA59464-05
Clietrt Proiect #301-88
Collectiotr Date/Timel5-Mar-07 00:00
MahixSoil
Rec€ivedl9-Mar-07
C,lS No. AQzlrte(s) Resull Flag 'RDL Dilution Melh4dRetr, heparcd AnzlWA Both Anoust
Semivolrlil€ Organlc Comportr& by CCMS
Somivolatile O.qanic Comoounds by SW846 8270C
Prcpared by method SW846 3550850.324 Benzo (a) pyr€ne20199" Benzo 0) nuoEntlrener9r-2+2 Benzo (g,h.i) pery,tene20ru84 Benzo (k) firorantEne65{5{ Benzoic acjd1ql516 Be(uylalcohol1 i 1 -91 -1 Bis(2-d1lorcethory)nEthanet11-444 Bis(2-d{oroethyt)€0Er3963&32.9 Bis(2d&Kisogropytlethef117€r-7 Bis(2-etrtheryl)phthalatet01-513 +Bromoph€ny phenyt ethef€sa'7 Butyl berEyl plfihalatE86'7rr€ Carbazol€59's0.7 +Chloro-&methylph€nol106-47{ +Chtoroaniline91'5+7 2-Ch*c.onsph$alene95-57{ 2-Chlorophenol700172-3 4chloroph€nyt phenyl ether21841{ Chrysene53-703 Obenzo (a.h) enthracenej32-64.9 Dibenzofuran95-5Gl 1.2{)icilorcbenz6n€541-rcn 1,3-Dichlorcbenzen€l06..ez 1!-DichlorobefEene91-9+1 3,3'-Oic+orobenzidin€120-83-2 2,4-Did{q.ophenol8,ri&2 Oiethylphu.ratate131-11,3 Dime{lyl ph[iatate10s7-9 2,4-Dimedrylphenolu-r4'2 Di-n-butylphthalate534-52-1 4,SDinife2-methytphenol51-2&s 2,+Dinitroph€nol121-141 2,+Dinitniotuene60@2G2 2,6-Dinll.otohrene11741-0 Di-n-octylph$alat€206,44{l Fluoranhene86.7$? Fluorenet1&711-1 Hexadllorob€nzenea76a-3 Hgxschlo.lbut6diem7r4r4 llExec*tlorocyc.lopentiadieoe67-72-1 H€xachbroetlune193305 lrdeno (1,2,3-cd) pyrcne9G12{ l.Mohylnaphthalone78-59-1 lsophoroneel-57{ 2-i,l€thylnephthatenes6-4&7 ?-tiiethylphenolio&3s-1, 3.'l-Mcthylphenol106-,14-591-2G3 Naphthalene88-74-4 2-NitoanilinelE{x}2 }Nitroaniline
SW846 8270C 22+{iaf'o7 zstrtat47 7031278 M.BBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRI-8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBR|-BRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRL
BRLBRf8RL
ldkS dry 736pSilg d.y 736p{kS dry 736
ldrSdry 736
ISAS dry 736
UgkS dry 736
lgkS d.y 7SygkS rtry 736
$dtsdry 736psftSdry 736pdks d.y 736pdkgdry 736
FdkS dry 736pSn(S dry 736
t'dksdty 736
ldks dry 736pdks dry 7fipgft€ dry 736
!gl(9 dry rupdts dry 736
lgkgdty 736
lgftS dry 736
Wit€ d.y 736pS/kS dry 73{ipS/kS dry 736pdrsdry 736
ldtg dry 736
ldkS dry 7
!Sn(S dry 736pgltlg dry 734
Fdkg dry 736
lSftSdry 736
FglS dry 736perlq dry 736
ldkSdry 736
udkg dry 736
USftS dry 7
udkg dry 736p€ikS dry 736
ldksdry 736pdkS dry 736pgrS dry 736
ldl(gdry 736
ldks dry 736
ldkS dry 736
lgrkg dry 736
t4Jkgdry 736
rd*gd.y 736p4ksdry 736
|JdXo dry 736
T rtts labodorf rcpod b ,tot vdid vahoa an suthoid signrttn oA t a coter pege.
' Repodable D€recrion Limit BRL = Below Reporting Limit Page 26 of 152
Page 187
Sample ldentificarionM8F',.r3 2'-4'sA59464-05
Clie Proiecr #30t -88
MatrixSoil
Received
l9-Mar-07Collection DatdTime
l5-Mar-07 00:00
CAS No. Analyte(s) Resah FloC Unib *RDL Dilulinn Metho.l ReJ Preparen Ana\zed Batch AnabslSemi!oletil€ Orgrnic C0mpounds by CCMS
Semivolatite Orqanic Comoounds bv SW846 8270CPrepa€d by method SW846 3S5OB
100{1€ 4_Nitroanitine9€-9+3 Nitrcbenzene88-/n5 2-Nitrophenol10r),02-7 4.Nitrophenol62-7tS N-Nilrosodimethytamine621.64,7 N-Nitrosodi-rFpropylemine8G306 N-Nitrosodiphenytamine87{e5 Pentac*tlorophenol85{1-8 Phenanlhrene
108 95-2 Phenol129-00 {t Pyrene110{6-r Fyridine120€2-1 1,2,4-Tdchlorobenzene95-954 2,4,s-Trichtorophenol8a-06-2 2,4,GTrichtorophenol
Sumgale rccovelies,32140-8 z-Fluorobiphenyl
36H24 z-Fluorophenol
41 654co Nitrobenzene-ds
416542-2 PhenoHS
1718-514 Teryhenyl4l4
118-79-6 2,4,6Tibtoflnphenot
Ug/kg dry 2950
uS/kS dry 736
!$'l(g dry 736
!S/kS d.y 2950
ldtS dry 736
!g/kg dry 736
!g/kg dry 736
UdkS dry n6
!g/kq dry 736
!S/kS dry 736
t/S/kS dry 736
!S/kg dry /36pSn(S dry 736pSftS dry 736
ldkS dry 736
30-130 %t5-110 %30.130%15-110 %3U130%15.110 %
mg/kg dry 0.03.44
mg/kg dry 0.990
mg/kg dry 1.48
mg/kg dry 0.495
mS/kS dry 0.247
fi'SAS dry 0.495
rE/kg dry 0 990
nlg/|.g dn/ 1.48
msil 0.0100
mg/| 0.0150
mgn 0.0050
m9 0.0025
m9 0.0050
m9 0.00040
mSI 0.0075
rhg/l 0.0150
yo
I SW846 8270C
1 '
1 '
1 "
1 '
1 '
1 '
1 '
1 "
1 "
1 "
1 "
I '
l '
1 SW846 7471A
22-MarO7 2s-+l,ar07 7031278 MBBRLBRLBRLBRLBRLBRLARLBRLBRLBRLSRLBRLBRLBRLBRL
77
661M79
0 242
BRL
13 .1
66.4' 1 .18
2 0 5
5 r8
8RL
Totrl Metrls by EPA 60{0/?000 Series Methods
7-43947{ Mercury
Torrl M€tNts by f,pA 20{ seri6 Merhods
7440 22-4 Sifuer
74'tG3&2 Arsenic
7440-393 Badum
7440-43 9 Cadmium
74,{)-47-3 Chromium
7439,92-1 Lead
778249-2 Selenium
23 Mar-07 26.tlar-07 2031306 YP
EPA 200.7 23-lvar.07 24-Mar-07 7031305 HB
BO
LR
LR
SPLP Metdr by EPA 1312 & 6000/?000 S€rics M€rhods
SPLP Exhaction
74-40-22-4 Silver
7440-3&2 Arsenic
7"40-3+3 Badum
7440-4+9 Cadmium
7440473 Chromium
7439-97{ Merstry
743+92-1 Lead
7782-49-2 S€l€nium
Cen€rd Chemistry Param€ters
% Solids
1 SW8461312 21-Mat47 2141,aA7 7031229
1 S'/v8461312/60108 22.1,iat47 23 ltarl7 7031323
1 '
1 '
1 '
1 '
1 SWM6'131217470A " 23+,nar47 7031324
1 SW84613126O108 . 23-Mat47 7031323
1
Completed
BRL
BRL
0.0216
BRL
BRL
BRL
BRL
BRL
86.9 1 SM25.f0 G Mod zz-Ma..oi 22.$ia'-Ol 703t307 Yl\4
This loborulory rcpod is not vdd ithoa 4n aalro zed sign tan on the cover page.
* Reporlrble Detection Limir BRL = Below Reporring Limit Paze 21 ot 152
Page 189
Samole IdenfificationM8F-I4 2-{'sA595l7-04
Client Pro.iect #l 0 l - 88
Collectior Date/Timel9-Mar-07 00:00
MatrixSoil
Received
20-Mar-07
CAS No, Anob.e(s) Result Ftoe Unik *RDL Mahod Ref, Prepued Anolyttd Batth Atu\st
Volrtile Orginlc Compounds
VOC ExkactionVolalile Oroanic ComDounds
Ug/kg dry 67,8
Ug/r(g dry 1360
PgKS dry 67.8
lgKs dry 67.8
US/Kg dry 67.8
!g/kS dry 67.8
!S/kS dry 67.8
!g/kg dry 67Ipg/kg dry 136pSlkS dty 67Apg/kg dry 67.8pg/(g dry 67.8pg/kq dry 67.8pg/kg dry 339pg/kg dry 67.8
US/kS dry 67.8
!g/kg dry 136pg/kg dry 67.8
!g/kg dry 136
B9/K9 dry 67.8
rc/kg dry 67.6
!g/kS dry 136pS/xS dry 67.4
WBS dry 67.4pS/kS dry 67.8
Wkg dry 67.8pg/kS dry 67.8pg/kg dry 67.8pgikg dry 136pg/kg dry 67.8
!S/kg dry 67.8
!g/kg dry 67.8
!g/kg ory 67.8
lgkS dry 67.8pg/kg dry 67.8
IgKg dry 67.8
!g/kS dry 67.8
tgkgdry 67.4
ldkS dry 67.8
lgftS d.y 67.8
ldkS dry 67.8
!S/kS dry 67 I
liS/kS dry 678
!S,4(S dry 67.8
trS/tS dry 67.8pS/kS dry 57-8pdks dry 67e
ldks dry 678
Lrdkg dry 67_8
21-Ma.{7 21-Mar-07 7031261Field extracted
Prepared by method SW846 5030 Soit (high tevet)761t1 1,1,2-Tricfilorotnfluometftane(Freo€RL67-64-l Acetone107-13r Aoylonitile7143-? Benzene
SW 846 82608 2r-Ma.-O7 274taFO7 7031602 mar8RLBRL1,520
505050505050505050505050505050505050505050
50505050505050505050505050505050505050505050505050505050
108{6-1 Bronrobenzene BRLT4-97-5 Brormdtloromethane BRL75-274 Bromodichloomethan€ BRL75-212 Brormform gRL
7443-9 Bromomethane BRL78-93-3 2.Eutanone (MEK) BRL10.F51€ n-Buvlbenzene BRL13ts8€ sec€utylbenzene BRL9€ 1)6-6 tert_Buvlbenzene BRL75'1t0 Carbon disultide BRL56 23,5 Carbon tebachtorade BRL108-90-7 Chtorcbenzene BRL75{0-3 Chtorcethane BRL6766-3 chloroform BRL7447-3 Chloromethane sRL95-4S-8 2-Chlorototuene BRL10H34 4-Chlorotoluene BRL96-12{ t,2-Diblomo-3rhloropropan€ BRL12+46-1 OibromochloromefEne BRL106-e3-4 t,2_Dibromoefiane(ED8) BRL74,9S3 Dibromomethane BRL95-s0'1 t,2-Dichtorobenzene BRL541-731 t,3_DicJatorobenzene BRL10616'7 t,4-Dichtorobenzene BRL75'71-a Dichlorodifuoromehane(Freon12)gRL75-34-3 1,1 . Dichloroethane BRL107{6 2 l,2-Dichloroehane BRL75-3+4 .l,l-Dichloroethene BRL1s6-5s2 cjs- 1 ,2-Dichlorc€theyte BRL156+5 rans- 1,2-Dichloroethene BRLTA-47-5 l,2-Dichloropropan€ BRL142-28-s l,3-Dichloropropane BRL594-2G7 2,2-Dichloropopane 8RL56$58€ t,1-Djchlo{op{Dpene BRL1061{1-5ds_1,3_Dichloropropenc BRL10061{?5 tans-1.3-Dichloropropene 8RL10$41-4 Ethylbenzene 309875+3 Hexachlorobutadiene BRL591-76€ 2-Hexanofte (MBKI BRL9€42-8 lsopropylbenzene 75.399+74 +lsoPropyitoluene sRL1634{44 Methylte(-but\y' ethe. BRL108-10-1 4-Methyt-2-pentanone(Ml8K) BRL7s{92 Methylene chlodde BRL
44791.20.3 Naphthatene
Pa€e l7 of 124
This labontory report it not wliil htlthout on ashoizctt signorurc on the cowr pdge
r Reportable Detection Limit BRL = Below Reporting Limit
Page 190
Sample IdcntifrcationMtF-l{ 2-l'sA595t7-04
Cli€ot Project #301-88
MatrixSoil
Colle€tion Date/TimellMar{7 00:00
Received2O-Mat-01
CAS No. Analyt2(s) Resal FI"S 'RDL DiIatL'n Merhol Retr, Pepaled AMIWd Batch Aizlt\.
Voladle Organlc Co|npounds
Volatile Oroanic ComooundsPrspared by mettbd SW84.6 5030 Soit (high levet)
7t69-4 Trichlorofluomm€tEne (Freon 1l) BRL
10s-65r n-P|opylb€n2erlel0o-42'5 Styrene63()'Al€ |,1,1,2-Tetrachtoroethans7s34-5 t,i.2,2-Tetrac+lloroethan€127-18-a Tet€chlometh€ne108{83 TOlUenO87{1{'1,2,}Tfidt lorobenzene12G€2n |,2,+Trichlo|obenzene7l{5{ 1,1,1-Tridofo€lhane79{G5 1,1,2-Trichloro€thane79{1{ Trichloroethene
9+18-4 l,2,3.Trichlompropane956+6 1,2,+Tdmethylb€nzene10&67€ 1,3,5-Trimethylbenzene7541'1 Vlnylcfitoride1 3ilo?G7 m,p-X!,t€ne95-47{ o-Xylene'109€99 TetEhydofuran@'29-7 Ethyl ofEr99as€ T€d-amylmeulytether637-9?3 Ed1yt terttutyl €d1e10&?0-3 Diisop.opylelh€r7565{ Tert-Butanol / but},t alcohol123-31,1 .l,4-Dioxane
sltrog|ab ,Bcoverbsj4&-@1 +Brcmolluotubenzene2037-2&5 Toluene4E1 lffi 047 -o 1, z-Dicl' o@ehane441 gJoIrS+l Abromofl uotonethane
f,ltract ble PctrolflI|l Hydrocfibons
Ettra.lable ToUl Petroleum HvdrocarbonsPr€pa.ed by m6hod SW846 355088006{1€ Gesoliat€€8,17G30-2 Fu€t Oit #26447G313 FuetOit #46€553.0il4 FuetOit#6u090000o0 tilobf oilJ00100il0O Avlatioo Fuel
Unlr€ndfiedOt|€ OilTotal Peboleum HydrocgrbonsC9436 Aliphatic Hydroa€.boos
sl/rDg|ale aecor,en€ar$tr633-2 l-Chlofiloctadecano
Semlvolrtile ()rgrdc Coltrpoutrd3 by cCOrlanocfilorine Peslicid€s SW846 8081APrepared by method SW846 3550930$llG2 Aldrin
$W 846 82608 27-Ma(07 274at-O7 7031602 marr43BRLBRL
BRLBRI-3,020BRL
BRLBRLBRLBRL
pg/kS dry
LrdkS dry
ugko dry
!s/*s dry
PgkS dry
lgks dty
ugvadrypgks dry
FdkS dry
ldks dry
!94!S dry
Itdkg dty
FgkS dry
lglqS dry
Idkg drypdks dry
US/rg dry
ldls dry
UgkS dry
ttSJkS dryyg/kS drypdks dry
rcftS dry
lgkS dry
UgkS d.y
67.8
67,8
67.8
67.6
67_8
67.8
67.a
67.8
67.8
67.6
67.8
67.8
67.E
67.8
67.8
136
67.8
674
67.8
67.8
67.4
678
1360
BRL2@BRLARL906507BRLBRLBRLBRL8RLBRLBRL
s91079295
505050505050
505050
5050505t)50505050
50
50
7t).1fr%7G130 %70-130 %7Gt30 %
BRI-BRL
BRLBRLCdoJliaiad asBRL380BRL3803m
drykg drynE/kg drynrgL/kg dayrrlgnlg dry.ns/ks dfymdks drynE (g drymgikg dry.ng/kg dryr|gkg dry
30_530,530.5
30.5
30.530.5
+CT ETPH ?2-Mat47 234Ja(47 7031281 DS
BRL
40.140 %
pS/rS dry 6.41 SWE ft SOatA 22+nt47 Z7ilar47 703t275 TG
This labotubry Eporl lt not tat t utthottt ott dhorirpd sFt ttttft on,hc cow. pate.
+ Reportrbl€ Dete.lion Limit BRI- = Below Reporting Limit P a g e l S o f l 2 4
Page 191
Samole ldentificationM8F-14 2-4'sA595l7-04
Client Proiqct #301-88
Matri(Soil
Collectioq Datc/Time19-Mar-07 0O:00
Received20-Mar07
CAS No. Anatrte(s) Flag U r s *RDL Dilution Merhod Ref, P,eparcd Ansbzed Batch Anat!:st
Semlvalrtile Orgrnic Compornds by cC
Orqanochlofine Pesticides SW846 SOBIAPrepared by .r€thod SW846 3SSOB
319-845 a-BHC319{5-7 b-BHC31e-8ffi d-BHC5,4{e-e g.BHC(Lindane)
s7-74-9 Chlordane7251{ 4,4-DDD (p,p.)72'5te 4,4-DDE {p,p')5{r2e3 a,4-DDT (p,p,)6O-s7,1 Dietdrin959-98{ Endosulfan I3213$5-9 Endosulfan tl1031i?-8 Endosutfan sutfuteT22GA Endrin7421-934 EndrjnAtdehyde76-44-A Heptachlor724?5 Methoxychtor1024-s7'3 Heptachlo{ Epoxide8001-35-2 Toxaphene5103-71-9 a-Chlordane5566-3,|'7 g-Chlordane
5349.-70-5 Endrin Ketone
Surogale rccowies:1we68+2 4,4og-Octafluotobiphenfl (542051-243 Decachlorobjphenyl (Sr)
Polvchlorinated Biphenvls bv SW846 8Og2Prepared by method SW846 35508
r2674 11-2 PCB l0 l611104-28-2 PCB 122111141-1es PCB.t232s34€+21-s PC8 124212672-2en PCB 124811097{9-1 PCB 12541109F€2-5 PC8 12603732+23-5 PCB 12621110C14{ PCB 1268
Suftogate .scoveias:
10386-84.2 4,4-O8-Octaf,uotobiphenyt (Sr)
2OSt-?4-i Decachlorobiphenyl (3r)
Semlvolrtlle Orgrnic ComponEds by cCMS
SW846 8081A 22-Mat47 27-Mat-07 7031275 TGBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLSRLBRLBRLBRL8RL8RLBRLBRLBRLBRL
3258
BRLBRLBRLBRLBRLBRLBRLBRLBRL
50
BRLBRLBRLBRLBRLBRLBRL1 ,510
pdkS dry 6 4tpdks dry 6 41
!g/kg dry 6.41
USI(S dry 6 41
ttStkgdry 32.O
US/kg dry 6.41pg/kg dry 6.4'l
Udkg dry 6.41ps/ks dry 6.41pS/tS dry 6.41
PqkS dry 6.41pdkSdry 641pg/kg dry 6.41
PdkS dry 6.41
ldkg dry 6 41
ldkg dry 6 41
UdkS dry 6.41
lSlkS dry 32.0
tig/kg dry 6.41
Pg/kg dry 6.41
l4/kg dry 6.41
30-150 0a
30-150 %
US4q dry 12.4
Ugks dry 12.8
UqkS dry 12.4
UgkS dry 12.4
Ug/kg dry 12_a
Udkg dry 12.Apgkgdty 12.8pg/kg dry 12.4
ldkS dry 12.a
30-150 %30-150 %
USn(g dry 757
lgl€ dry 757
lSftS dry 757
ttglqg dry 757
PeJkgdty 757
rglls dry 757pSn(S dry 757pSlqdry 757
1
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SW846 8082 22-Mat41 24-Mat41 1031274 MP
Semivolatile Oroanic Comoounds bv SW846 g27OC
Prepared by method SW846 35508a3i2-9 Acenaphthen€20&96-€ Acenaphhylene62,53-3 Aniline120-12-7 Anthacene1912-24-9 Atazjne10133,3 Azobenzene/Diph€nytdiazine92-s7-5 Beruidine56-5!3 Benzo (a) anthracene
SW846 8270C 22-Mar07 24-Mar-O7 7031279 M.B
Thb lqbotulory EForl as,rotvsltl 'ithout an raahod?ld sigrrddtrc on the coter page.
. Ret onable Detecrion Limir BpL = Below Rgporinl Limit Prge 19 of t24
Page 192
Salnple IdefiificatiopM8F-l{ 2-4'sA595l?-04
Client Proiect #301-88
MaFixSoil
Collectioo Date./Time| 9-Mar{7 00:00
R€ceiv€d20-Mar-07
CAS No. Anslrta(s) Flos Unib *RDI Dilutioa Method Rctr. Prepated Adalyed Bdch An4lrst
Semlv0hltl€ Oryrnlc Compoun& by GCMSSemivolatile Orqanic Compouods bv SW846 82ZOCP.epared by method SW846 355085O32,a Benzo (a) pyren€205'9$2 Benzo O) ftioranthene1sl-24-a 8€nzo (g,h,i) perytene207{r!r.9 Benzo (k) f,uoranhene65{s-O B€nzoic acjd10{}.51.€ Berizy alcoholilt-91_l Bis(2€hloroethoxy)methaneIfi-{.44 8i6(2-ddotpehytFher3963&32€ Bis(2d{oroisopropyt)ether117-01-7 Bs(2-€thyltleryl)phfl€tater0l-5+3 4-Brofttophenylphenylefter85{&7 Bu!/benzytphfiataie8t?4{ Carbazole59,5G7 +Chtoro_g-methyiph€nol106-47{ 4chloroenitine91-5€.7 2_Chloonaphthalene!15-57{ 24hbrophenolnE5'72-3 +Chlo.oph€nyl phenyt €ther2i8-01.9 Chrysene5+7G3 Dibenzo (a,h) antrrrscen€i32{4€ Dib€izofuaan95-5Gt l.2-Diof orobenzen€541'73-t l,lDichtorobenzens10646-7 1,4-Dichlor.obenzene91€4,1 3.3'-DichlorobefEidinei2o{3-2 2,4-Oic orophenol04{c2 oiethyt phfElat€13i-1r-3 Dimethy{phthatale105-67-9 2,+Dim€drylph€noto+7+2 Di-n-buty'phfiatats53+,52-1 4,6-DiniblF2-[rehytphenol5l-?&5 z,+Dinifoptrend12r-14.2 2,4_Dioilr,otoluene60c20-2 2,6-Dinitrhiu€ne117{4{ D-n{d}tphhatat€m6-{4-O Fluo.€ndEne8€-73-7 Fluor€ne1l&7+l llexachloiobenzene874&3 HexadJombutsdiener|474 Hexet orocyclopentadi€ne6r-72-1 Hexadlloro€thane19&3$5 Indeno (1.2,4cd) pyr€ne9G12{ l.Methy'nryhthalen€78-5+1 lsophoavt€9157.6 2-irGhytnaphthatene9+4&7 2-M€byhhenol10&3s.a, 3,+M6thylphenol1oc44-s91+03 Naphtla|€.|€&7.1-4 2-Nitro€r{he994+2 $Nltroendine
1,8901,8609582,030
8RLSRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLr.840BRIBRLBRLARL8RLBRLBRLgRL
SRLBRI-BRI-BRLBRLBRLBRLBRL
2,820BRLBRL
BRLARLBRL968
BRI-
BRLBRL
BRI-
BRLBRLBRL
UdkSdry 757pdks dry 757
WkSdry 757pg,rs dry 157
ldkgdry 757
ldkg dry 757
tdkgdry 757
lSftgdry f57pCftSdry 757
ldks dry 757pdkgdry 757pSlgdry 757
FS/kS dry f57pglsdry 757
ldkS dry 757
lgl(g dry 757pCxS dry 757pqkg dry 757p4kgdry 757
Uglkgdry 757pSI(S dry 757
t4,lksdry r57ygts dry 757
ldrsdry 757
llg/kS dry 757
US/kSdcy 757
Igil€dry 757
rdkgdry 757
['dkg dry 757
rdksdry 7s7
ItSlkqdty 757
uqlSdry 757p91(9 dry 757
USeSdry 757
udkS dry 757pdkS dry f'f
Fdkgdry 757pdks dry 757
FdkS dry 757
!9rS dry 757
sgko dry f57gtlqdry 157
tytS dry 757
ldks dry 757pdkS dry 757pSJRgdry 757
us/kgdry 757
pgjkgdry 757
!dl(S dry 757
ldkg dry 757
t
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SW8,'{18270C 22 tar0l 24+lat47 7O3l27S M.6
Ihls ,4brobry Epott is ,',ot ttdld withod att aalho.iael twEdue oa the cow! page.
* Repo.table Der€ction Limir BRL = Below Reporting Limir P€e 20 ofl24
Page 193
Sample IdentificationM8F-14 2-4,sA595 t7-04
Client Proiect #301-88
MatrixSoil
Collection Date/Tirne| 9-Mar-0? 00:00
Received20-Mar-07
CAS No. Analrre$) Fl4S Ani6 *RDL Diluliot Method Retr Preparcd Analyzed Bakh AMUst
S€mivolattle Orgsnic Compoutds by GCMS
Semivolatile Oroanic Comoounds bv SW846 B27OCPrepared by melhod SW846 35508
100{14 4-Nitrcaniline98-9t3 Nitrobenzene€8-7$5 2-Njtrophenol10GO2-7 +Niroph€not62-7t9 N-Nitrosodimethytamine6216{-7 N-Nihosodi_n_propylamine86-3G6 N-Nibosodiphenytamine87{e5 PentacfilorcphenolB5{1 I Phenanlhrcne108-95-2 Phenol129{0{ Ptrone110-86-1 P,yridin€120{21 1,2,4_Trichtorobenzene95-9s4 2,4,5,Trichtorophenol08{6-? 2,4,GTrichlo.ophenol
Sufiogale rccoveies:321a0-8 2-Fluorobiphenyl
367-124 2+luoropheool
4165-60-0 Niuobenzene4s
116U62-2 Phenol4s
1718-s14 Tery,leny'4l4
1ra-79 6 2,4,6-Trbrcmophenol
Tord Merrts by EPA 6000/7000 series Methoos
743997$ Mercury
Totrl Metals by EPA 200 Seriti Methods
744G22-4 Salver
7.4401&2 ArsenaC
7440-3+3 Barium
7440-4+9 Cadmium
71{r)-47,3 Chromium
743+92-1 Lead
77€2-49-2 Selenium
SPLF Metrls by f,PA l3l2 & 6000/7000 Sert€r Merhods
SPLP Erdraction744C22-4 Silvef
744G3e2 A6enic
744C3*3 Barium
7.1,10-4!9 Cadmium
f 44(47-3 Ch.omium
743S97€ Mefcrrry
7439.92,1 Lead
7182-4+2 Selenium
Generol Chemistry Param€ters
% Solids
BRLBRLBRLBRL
BRLBRL8Rr_BRTBRLBRL2,450BRL
BRLBRLBRL
57725180
0.270
BRL
9_01
0 600
28.3
292
BRI
Comdeted
BRL
BRL
0.0r42
8Rt
BRL
BRL
0.0310
ARL
86.3
pdr(g dry 3030pS&S dry 757pqkSdry 757
!$ftS dry 3030
lgkS dry 757
PdkS dry 757
fdkg dry 757
lidKS dry 757
PsftSdry 757pg/kg dry 757
ldks dry 757
trErq dry 757pS/kS dry 757
!d(g dry 757
f./dkS dry 757
30-130 %1G|10 %a-130 %15-110 %34-130 %15110 %
mgr'kg dry 0.0342
rYtgfl(g dry 1_14
mg/kS dry 1.71
m$ftg dry 0 571
nEukg dry 0 206
msfts dry 0,571
mgks dry 0.857
mgikg dry 1 71
mgn 0.0ro0
mS,4 0.0150
mg/l 0.0050
mg/l 0.0025
nV, 0.0os0
mg/t 0 00(X0
mg/l 0.0075
mg/l 0.0150
%
1
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SW846 8270C 22-Mat47 24.n|/,a(O7 7031279 M.B
1 SW846 7471A 26-Mafi7 27.Ma..oI 7031322 YP
EPA 200.7 26-Ma'-07 27-Mat-07 7031321 HB
1 SW8461312 22-Mat47 22-Ilar'O7 7031344 BD
1 SW846 1312/60108 23-Mar-07 24-Mar-07 7031408 LR
1 '
1 '
1 "
1 '
1 SW8461312/7470A ' 26-Mar-07 7031409 YP
1 SW84613't260108 ' 24-Mar{7 7031408 LR
1 '
1 SM2540 G irod. 23-Mat47 23-inal.O7 7031429 QP
Thb labrutoq fcpofl is not vdid withoa at ot/rtoized signatuE on the cover pge.
' Reporfrbl€ Detectbn Limi BRL = Below R€?or,tng Limir Page 2t of 124
Page 194
Sample ld€ntificationMtF-15.1-6'sA595t7-0J
Client Proiect #301-88
MatfixSoil
Collectioo DatdTimel9-Mar47 00:00
Re{eived20-|.tlat-07
CAS No. ,!nable(s) Flag rRDL D aaA'" iterhod Retr PrepoQl Attalfzd Bat h Ana$st
Volrtile Org lc Cmpoundi
VOC E.xtraclion Field o)draded
Volatile Orqanic CompoundsPrepared by m€thod SW846 5035A Soit (tow tewt)7&1!1 l,l,2.Trichtorotriffuoroothane(Freo€RL474+1 Acetone BRL10?.13-1 A.rtonitdl€ BRL71<.T2 B€nzene BRL108€e1 Brcmb€nzene BRIZt€75 Eromo<filoromethane BRLfr271 Brornodichloromethane BRL7+212 S.oanoform SRL7a{}9 Broflrdnethene BRL78.e!13 2€ubnode (MEK) BRL1(X-sl4 rFButylbenz€ne BRL13+S{ sec-Butt4benz€ne ERL98{6-6 t€rt€utylbenzen€ 8RL75-15.0 Cer0on disuhde BRL5G215 C€rbon teb&hlorftte BRL10&90-7 O o{obenz€ne BRL75{G3 Chloroethsno BRL67{6-3 Chtoloform BRLzr{7-3 chlolofir€Ersne BRL95{9{ 2-Chlorctolu€ne BRI1o6-4i14 4-Chlorctoluon€ BRL9€_12{ 1,2-Oibrorno.3.c}o@propan€ BRLl2a-48-1 Dbromochbromethane BRL10e9+. l,2-DibromoedEn€ (EOB) BRtz,t-9+3 Dibro.nomethane BRL9s5G1 l,2oidllorobenzene BRLs41.?:lr l,3oicHofob€nzene BRL106-{s7'1,4-Obhlo.ob€nzene
uglkgdry 7.3
t dkS dry 146
trSikg dry 7.3
Pgkg d.Y 7.3
ldkgdry 7.3
ustkgdry 7.3
vdkgdry 7,3
Fg/kgdry 7-3
lrsjkg dry 14.6
lgkg dry 73.1
IdkS dry 7.3ygkS dry 7.3
lg,tSdry 7.3pdkS dry 36.5
t/dkS dry 7.3
ldkg dry 7.3pg/tg dry 14-6
lCftS dry 7_3pOkS dry 14.6
UgkS dry 7.3
ItgkS dry 7.3
t dkS dry '14.6
UCAS dry 7-3pdkS dry 7.3
rdks dry 7.3pdkS dry 7.3pgkS dry 7.3pS^g d.y 7.3pg/kg dry 14.6
sdkS dry 7.3
FSftS dry 7.3
ldkS dry 7.3pgAS dry 7.3
FgkS dry 7.3
trS/kS dry 7.3
FdkS dry 7.3
USilg dry 7.3
lgrS dry 7.X
!gl(9 dry 7.3
IdkS dry 7.3
ldks dry 7.3
IBAS dry 7.3pdkgdry 73.r
tglqdry 7.3
|lgftS dry 7.3pSfl€dry 7,3yqkgd.y 73.1pdkS dry 73.1
UgXSdry 7.3
21-Mat47 21'l[ta'.07 7031261 BD
7s-7t+ Dchtorcdifrloromethan€(FGont2)BRL75-3+3 l,l-Dichlofoethsne BRI_107S-2 |,2oichloro€thane BRL7s-35-4 1,l -ttictdo.o€thsne BRLls&59-2 cis-i2-Dicfdorcethen€ BRLlsf!6o{ bans-l,2oichtoroethene BRL78{7.5 l,?-Dicl oroFopane BRI-t42-2&9 t,3-Did{o|tpropsne BRL59+41"7 2,2€icHorcprcpane BRL56450{ 1,l-Dichtoropropen€ BRL10061{1-5 cigl,3-oichloropaoD€ne BRL10(E1.02{hane.t,3oidrlorcpmpede BRL10041-4 EthytbqE€ne BRL874s3 Hexacfibrobutadbne BRLi91-78{ 2-H6xanm€ (MBK} BRLs{2{ tsop.@ytbeiEen€ BRLse{7{ 4-tsopropyltoluene BRI10:x{4{ M€hyt t€rtrbuM €sler BRLloslGl +Mefiy&2-p6nlanooe(MIBK) BRL75.{)!}2 Meth}4€n€ drloride BRL
SW 846 82608 22+nar07 2X4ar47 70313:15 RU
BRL
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Pagezz of 124
Thb bborolory tqod ie nd pallt wlthotd on zulho.iaed sigrrrt/re 06 ,he covu page.
'Reporbbl€ Detectim Limit BRL= BelowRrportiag Limit
Page 195
Sample ldentificationM8F-I5 44'
sA595l7-05
Client Pmject #301-88
Collection Date/Timel9-Mar-07 00:00
Received20-Mar-07
MatrixSoil
CAS No. Anoqta(s) Flog 'RDL Dilatioa Itethod Retr. Prcparcd Analfzed Batch Analjts/
volatile Organic CompoundsVolatile Oroanic CompoundsPrepared by method SW846 5035A Soit (tow bvet)
75$9-,{ Trichlorofluoromeltune (Freon 11) BRL
10!6tl n-Propytbenzene100-42 5 Styrene63C20$ 1,1,|,z-Tetrachloroethane793.1-5 1,1,2,2-Tetrachloroethane127'18-4 T€tEchloroeihene10&€&3 Toluehe87$1$ 1,2,3-Trichlorobenzene120-821 1,2,4-Trichlorobenzene71_55_o 1.1 , t_Trichloroethane79{0-5 1.1,2-Trichlorcethane79{1-6 Trichloroethene
96,18-4 1,2,3-Trichlorop.otEne95$36 1,2,4-Trim€thylbenzene108-67{ 1,3,gTdm€thytbenzene75414 Mn/chlodde13m-20-7 m,p.Xylene9s-47-6 o-Xylene10+994 Tetrahydrofuran60-29-7 Ethylether99€tr Tert-amyl meftyl ether6r7-e2-3 Ethylte(-butytether10&20-3 Di-isopropylethef756t0 Tert-Butanol/ but/i alcohol123-91-1 1,4-D:bxene
Suri.ogato recol€oesi
41040-4 +Bromofluorcbenzene
203/-2cs Tduene4S
| 7 @G074 1, 2-Dbhlotoe.Ihane44
1E6a-5?7 Dibrotnofluoromethane
Erhact ble P€koleum Hydroqrbons
Extractable Total Petroleum Hvdrocadons
Prepared by method SW846 3545A
8006{l-9 Gasoline6ea7+30-2 FuelOil#260476-31-3 Fuel Oil #46€55+00-{ FuelOil #6il09e{0000 Motor OilJo01 00000 Avialion Fuel
Unidentified
Ohe(Oit
Total Pe&oleum Hydrocabons
C9.C36 Atiphatic Hydrcc€rbons
Suftqde recovedes:fia63?2 l-Chlotooctdecaie
Semivolatil€ Otgrnlc Compounds by cC
Orqanochlorine Pesticides SW846 8081A
Prepared by method SW846 35508
309{0-2 Aldrin
SW 846 82608 22-Mat41 23'llr''a147 7031335 RLJ
+CTETPH 22-MaF07 26.M€47 7031284 DS
BRLBRLBRL
BRLBRL
8.0BRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARL
99107100101
BRLBRLBRLBRLBRL
BRLgRL
BRLBRLBRL
75
uSi kS drypdks dry
US/kg drypdks dry
ldko drypdkS dry
ldkS drypdks drypdks dry
ldks drypdks dry
lSftS dry
fg/kS dry
!g/kg dry
Pg/kg drypg/kg drypdks dry
US/kg dry
Ug/kg dry
IdkS dry
!S/kS d.y
udks dry
Ug/kg dry
ldks dry
Pdkg drl
7.37.37.37.37.37.3
7.37.37.37.37_37.37.37.37_3
14,6
7.373.17.37.37.37 373_1144
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/0-130%7G1m %/0130 %70-130"a
mdkS dry
mg/kg dry
mg/kg dry
mgL/kg dry
ftg/kg dry
mgL/kg dry
mg/kg dry
.tWkS dty
'rs!ftS dry
'YVks dry
20.620.620.620.620.620.6
2 0 6m.620.620-6
40-t44 %
lgikg dry 7.1O SW6.f68081A 22-MaFO7 27-Ma(O7 7031275 rG
This labo ttory ppod ls not,old *ilhoul an azthorhel si4nrture on the coeer FzEe.+ Reportabte Der€cdon Limir BRl- = Below Repordng Limit Pzse 23 ot 124
Page 196
Sahpl€ [dentificationM8F-15 4{'sA5951745
ClietrtProiect #30t-88
MatrixSoil
Collection DatdTimeI 9-Mar47 00:00
Rec€ived20-Mar{7
CAS No. Adalyte(s) Fhs Anht rRDL Dilution Method Rttr, hepoted Analytd Bozh Ansllrt
Se$rivohtile Orgrrlc Compound! by CC
Oroanochlorine Pesticid€s SW8,+6 808 1 APreparBd by melt|od SW846 3550831$e4s a-BHC319-e'7 b"BHC
31986{ d-BHC
50{se g€HC (Lindan€}
57-74-9 Cfilordane12-544 a,+DDD (p,C)
72-s5a 4.+DDE (p,p,)
5o-2s3 4,+DDT (p,p,)
60-57-1 Dield.in95$9F€ Endosulhn I332116'9 Endoeutfan ll103r{7{ Endoslltan sulfate72-204 Eoddn7421.93-4 Endain Ald€hyde764+A Heptacruor724Y5 MethorycNoi'1024-57-3
H€ptachlof Eporide0001,3$2 Toxapheoe
5ro3-71-9 a-Chlordane4,56fi+7 g-Chtordane
53a9+70{ Endrin Kelone
S/J/rogab reeovedes:1 038Gw-2 1j.D8-M uotpdphenyl (Si
m51-24-3 De@chbrobiphenyl (Sr)
Polvchlorinated Bbhenvls bv SW846 8082
ft@ared by mehod SW846 35508
i267+11-2 PCB 10161110+28-2 PCB 12211i14r-t6-s rcB 1232s316+21-9 PCB 124212872.n4 PCB 1248'110s7-€9-1 PcB 12541109e82-5 PCB 126031:t24'n.s PCB 126211t0+r4-4 rcB 1268
Sfimg /e rccovedes:| 0386.342 4, 4D*Octafl uotobipl6nyl (Sr)
mst-2+j Deca&torobiphenyl (Sr)
Seftivolrtile Org.dc CodrpouEdr by G,CMS
BRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRfBRLBRLBRLARL
36127
BRIBRLBRLBRLBRLBRLBRLBRL
BRL
50
SRLBRLBRLBRL
BRLBRL8Rr-BRL
US4(S d.y 7.1OpdXS dry 7.1O
lsASdry 7.10
ldxgdry 7.1O
UdkS dry 35.5
rgks dry 7.10
rgts d.y 7.10
ldkg dry 7.10
udkodry 7.m
UdkS dry 7.1O
lrgn€ d.y 7.1OpdkS dry 7.1o
ldkS dry 7.1O
Udks &y 7.1o
l|gikg dry 7.10
ldkS dry 7.1O
!s,nq dry 7.r0ydl€ dry 35.5
rdkg dry 7.10
f.fS/tg dry 7.1O
Fdkgdry 7.10
30.150 %w-lf i%
IrSlkS dry 14.2
US/tSd.y 14.2pgrkg dry 14.2
ldkS dry 14.2pS/kS dry 14.2
trgr*gdry 14.2
FSrlgdry 14.2pdksdry 14.2
!S/kS dry 14.2
30.150 %30-1fi%
1
I
1
1
1'|
I
1'1
I
t1'1
1
t
1
1
1
I
I,1
SW846 80014 n-Maro7 27l',,aFO7 7031275 TG
SW846 8082 2z-lhtof 24-Mat47 7031214 MP
S€rnivolatile Oroanic Comoounds bv SWg46 8220CPrcpar€d by method sw8,t6 35508a3{2-9 Ac€nephthene20&964 Acenaphtrylefle6?-533 Aniline12G12-7 AnthrEcene
1912-243 At€inel0$S3-3 Azob€nze{r€Oiphenyldiezine
9247'5 BerEidine5€513 B€nzo(a)anthrac€ne
SW846 E270C T2-Mat47 21,l'',a147 7frr279 M.BpdxSdry s10
WkS dr, 51O
IdkS dry 510
Igit€d.y 5t0pgutg dry 510
ldkg dry 510
t dkS dry 510
tgkg dJy 510
This l4brelorf repo.t it tut valld toilholt a asrtoriztl siguarc oa thc uvet ptge.
* Reptrtable kectiorr Limit BRL = Below Reporting Limir PaEe 24 of 124
Page 197
Sample IdentificationM8F-15 4i'sA595l7-05
Client Proiect #301-88
Collection Date/TimeI9-Mar-07 00:00
MalrixSoil
Received2O-Mar-07
CAS No. Azalj-k(s) Resall Fl"e *RDL DiIt/tiorl Method ReJ Prcparcd Anatrzed Balch Antlysl
Selnlvotalile Organic Compounds by (;CMS
Semivolatile Orqahic Comoounds by SW846 8270CPrepa.ed by method SW846 35508
s0-32{ Benzo (a) pyrene
20ts92 Benzo(b)fluo.anthen€1s1-24 2 Eenzo (g,h.i) perytene
207 08 I Eenzo (k) fluoranthene65{54 Benzoic acid10os15 Benzytalcohol111-91 1 8is(2drloroethoxy)rnethane111.44i Bis(2-chtorce$yt)et1er3963&32-9 Bis(2-chloroisopropyt)ether117-81-7 Bis(2-ehyth€xyt)phthatate101-5s-3 +Brcmophenyl phenyi ethefA54A-7 Butt| benzyt phthatate86-74{ Carbazoles9-5|}7 +chlord3-rn€lhylphenol106-473 +Chlo|oaniline9r.58-7 2-Chloronaphthalene
95-57{ 2-Chlorophenol7005-72-3 4,Chtorophenylphenylether21&01-9 Chrysene
53,70-3 Dibenzo (a,h) anthracen€132{4 9 Dib€nzofuran95-5Gl 1,2-Dichlorobenzene
541-73r 1,3-Dicl.{orobenz€.r€106-46-7 1,4-Dicj{orob€nz€ne91-94.1 3,3'-Dichk'roberErdine12033-2 2,4-Dichloropheool445+2 Diethy,jphthatate
131-11-3 Dirnethytphthalate109,67-9 2,4-Dimethylphenol
w-14-2 O-n+utytphthalate531-52'1 4,6-Dinilrc-2-mehylphenol
51-2&5 2,+Dinitroph6nolr21-14-2 2,+Dinitrctoluene
60e20-2 2,6-Dinit'otolu€n€
117{,{{ Di-n_octylphhatate
206-,4{ Fluoranth€n€
86-7$7 Fluoren€118-7t-1 Hexacfilo/ob€nzene87iA-3 Hexachlorobutadi€n€77471 Hexadllorocyclopentediene
67-72-1 Hexachloroethen€193-39-5 lndeno (1,2,3-cd) pyreneso.12-0 l-Methylnaphthat€n€78-5+1 lsophoronee1-57{ 2-Methylnaphthaleness-48-7 2-Methylphenol
l0&3s-a, 3,4-Methylphenol106-.{4-5gt-2o-x Naphthalene
8a-744 z-Nitroaniline99{$2 }Nitroaniline
SW846 8?70C 22-Mar07 24-Mat47 7031279 M.BBRLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLARLARLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRL
BRL
BRLBRL
ldkSdry s10
tls/ks dry 510gikg dry 510
ldkS dry 510
trSftS dry 510
trgftS dry 510
Udkg dry 510gdkg dry s10
USftS dry 510
US4$ dry 510
UdkS dry 510pgkSdry 51O
UdkS dry 510
UdkS dry 510
tr9'k9 dry 5to
UdkS dry 510
USn(g dry 510
UdkS dry 510
USftS dry 510
USftS dry 510
UgkS dry 510
ugks dry 5r0
USftS dry 510
UdkS dry 510pqkgdty 51o
US/l(q dry 510
US,4<S dry 510
ldkS dry 510
Wn(g dry 510pS/kS dry 510pS,to dry 510
Ug/kS dry 510pg/kg dry 510
UgkS dry 510
!S/kS dry 510
US/kg dry 510
ldkg dry 510
Uglkgdry 510
!S/kS dry 510pdkg dry 510
ldkS diy 510
llg/kg dty 510pg/kg dry 510
ldks dry s10
ldkS dry 510pdkS dry 510pS{(S dry 510
USftS dry 510
lSftS dry 510
!S/kS dry 510
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
I
1
I
l
1
1
1
1
I
I
I
I
I'1
1
1
1
1
1
I
1'|
1
1
1
1
This labontory rcpod is aot valid wirhour za authoized sigtutarc on the cot)er ptge _
+ R€portable Detection Limjt BRL = B€tow Reporting Limit Page25 of 114
Page 198
SaEple ldentificatiotrM8F-r5 4{'sA5951745
ClieDt Proiecl #301-88
Collection Date/Timet+Mar47 00r00
MatrixSoil
Rec€ived20-Ma.r-07
CAS No- Aialyta(s) Ratuk Flog 'RDL Dilut*trt Method Retr, Prcpred Anzlyed Batch Aazlyst
Semivolrtile Orgroic Compoutrdr by cCMSS€mivolalile Oroanic Comoounds bv SW846 8270CPrepa.ed by method SW846 35508
10rrc1{ 4Nitoaniline
9€-9+3 Nitrob€nzen€
08-75_s 2-Nitrophenol
10G02.7 4-Nitroph€nol
62:1us N-Nitrosodimethytamine
€41+a.7 N-Nitrosodi-n-propylamin€863ts N-Nitrosodiph€nylamine07.06-s Penlacibr@h€nd85-01i Phensnthrene100-9s-2 Ph€hol129{0r' P}rfierlG€Fl B/ddin€12O-e2-1 1,2!-Trichlorobeflrene95-954 2,4.STrichtoroph€nol884&2 2,4dTncfibrophenol
Sufiogale rffivedes:321-604 z+fuotobiphenyl
367.124 2-Ftuprophenol
4165-604 Ni'&enzene4s
416542-2 Phenol4s
1118-514 Telphenyl4l4
1 1&794 Z4,$Taibtomophenol
Toarl M€trb by EPA 6000t000 S€ri€3 M.ttods
'l SV'1848 E27DC 2:n1at47 24{ie E 7 001 279 M.A
t '
1 't '
1 '
1 -t 't '1 '1 "
I gwg46 7471A 26+16-07 27-Mar$ 7031322 YP
1 EPA2OO.l z&tir€r{7 27-lrat-07 7031321 HB
1 ' ,' t "
t "
1 '
1 "
t '
I SW8,r61312 22-iiar-O7 22-itar-07 7031344 8D
I SW8461312/60108 ?3-Mar-07 24+larry 7(B14m LR
1 '
t '
1 '
1 '
I SW8{6131274704 ' 26l,re-07 7031409 YP'l S1rV8.l6 1312180109 ' 24+vlar47 7031408 LR
1 '
I SM2540 G ttod. 23-ldar.07 23-$lerry 7031429 qP
BRLBRLBRLBRLBRLBRLBRI-BRLBRLBRLgRL
BRLBRLARLBR|-
f7
64a4
0.0698
BRL
29.3
t56
0.s61
34.7
841
BRL
Co.npleted
BRL
BRL
o.0418
BRL
0.0t20
BRL
BRL
BRL
9glk9 dry m40
ldks dry 510
t!r'kg dry 510
t gkg dry 2lX0
lrgrkg dry 510
t/dXSdry 5'10
YdkS dry 51o
ldko dry 5lopdfs dry 510p4lqdry 510
UgkS dry 510
ll84€ dry 510peig dry 510pgr(g dry 510
ldkS dry 510
30-t3lt %t5-110 %fi-1$%15-110 %30-130 %tutl0 %
org/kgdry 0-0382
rngftg dry 1.28
mgrkg dry l.9l
rflg/kg dry 0.638
mdko dry 0.319
'rEAg dry 0.638
mg,kSdry 0.357
mgLfl(g dry l-91
N1A
firvl 0.0100
mg/l 0.0150
mgLt 0.0050
rnSI 0.0025
msn 0.0050
msn 0.000,tt)
rrBn 0-0075
mgl 0.0150
%
7439-974 Merdry
Tohl Mctrb by EPA 200 S€rier Metlods
7440-224 glver
71,4G33-2 Als€stic
744n.393 g€dum
74aG4$g Cadmium
7440.47_3 Chrcmium
?43{l-92n Lead
za2-4$2 Selenium
SPLP Metrk by EPA l3l2 & 60001000 S€.ics Mcttods
SPLP Exhac{ion714{1224 Sifu€r
7440-3&2 Arsenic
7440nF BA um744043t9 C€dmiutn
74(X73 Chrornium
7€9.9rc i,l€rcury
7439€2-1 Lead
77&492 Selenium
Cen€rll Chehlslry Pr.rmctets
% SolkJs
Thb kbordary .epod ti ,tot vdid witho'd .a .lthothd sbndnrc on thc cawr pag.
. R@rtable Dcteclioa LirEi! BRL = Berore R€po.tinC Linir Page 26 of 124
Page 199
Sample ldentifications{8F-16 2'-4'sA5964l-01
Client Proiect #301 -88
Collection l)alelTime2l-Mar-07 00:00
Mari\Soil
Received22-Mat0l
CAS No. Ahabtz(6) Resu& Fhs *RDL Dilution Method Ref, Prcpared Analt'a,ed Batch Analrsl
Volalile Orgrnic ComtrN)undf
VOC Extraction Field extracled
BRL
!S/kg dry 5.4pg/kg dry 1O7pdkS dry 5.4pdkSdry s.4
r.ig/kg dry 5.4pg/kg dry 5.4
US/kS dry 5.4
lSlkg dry 54
IdkS dry '10 7pg/kg dry 53 6
|JS/kg dry 5.4
VqlkSdry 5.4
|,g/kg dry 5.4pg/kg dry 26I
Ug/kg dry 5.4gdkSdry 5.4pg/l€ dry 1O.7
tdkg dry 5_4
t S/kS dry 10.7
Vqkgdry 5.4
ug/kg dry 5.4pg/kg dry 10 7
Irdkg dry 5.4
llStkSdry 5.4
!S/kg dry 5-4pg/kg dry 5ApS/kS dry 5 4
US/kS dry 51
rrS/kS dry 10 7
ug/kg dry 5.4
udkS dry 5.4
tgtKgdry 5.4
udkS dry 5.4
ldkS dry 5.4pdkg dry 5.4
ldkS dry 5.4
!g/kg dry 5.4pg/kg dry 5.4
lgkS dry 5.4
FdkS dry 5.4pqkS dry 5.4pdrs dry 5.4
ldkg dry 53.6pdks dry 5.4pdkS dry 5.4pCl(g dry 5.4
lCftS dry 53.6
ldkSdry 5:1.6
ldkS dry 5.4
26-t4ar47 26-Mar{7 7031584 ADVolalile Oroanic Comoounds
Pfepared by method SW846 5035A Soit {low levet)76-13'1 1,1,2-Trichtorotrifuoroethane(FreoFRL6764-1 Acetone BRLl07r3j Acrylonitrite BRLt143-2 Benzene BRI-r0a€6,1 Bromobenzene BRL7497-5 Brcmochtoromethane BRL11274 Brcmodichloromethane BRL75-2*2 Bromofo.m ARL7413-S Bromomethane BRL78s13 2-Butanone (MEK) aRL1M,51rt rFButytbenzene BRL13t98{ sec_Buil/tbeflzene BRf984tr tert-Butylbenzene BRL7s 110 Carbon disulfide BRLs6-23s Carbon tefachloride BRLlo0-90-7 Chlorobenzene BRt7540'3 Chtomethane BRL67€+3 Chtorolofih BRL74-47-3 Chloromethan€ BRL954+A 2-Chlorotoluen€ aRL10e434 4chlorotoluene BRLs612.8 1,2-Dibforno.3-c}tloroprop€n€ 8RL124-46-1 Oibromodtloromethane BRLlocai-4 l,2-Dibromoethane (EOB) 8RL74-9+3 Dibromomethane BRL95-50-1 l,2-Dichlorobenzene BRL541-73-1 l,3.oichlorobenzene BRL106-.{6-/ I,rt-Oichlorobenzene BRL15 71-g Dichb.odifluoromethane (Ffeon12)BRL75'x+3 l.1-Dichloroothane BRL10746,2 |,2_Dichloroethane BRL75-35.4 l,l-Dichloroethene SRL1s6'59,2 cis-1,2-Dichloroetl|en€ BRL1s6i05 ftans-'|,2-Dbhbroeth€ne BRL78{7-5 1,2-Dichloropropahe BRL142-26-s 1,3-Dichloropropane BRL594-20,7 2,2.Dichloropropane BRL563-58-6 1 .1 -Oichloropropene BRL10061{1-5cis-1,3-Dichloropropene BRL10m1.025trans-l,3.Dichloropopen€ BRL10041-4 Ethylbenzene BRL87{&3 HexacilQrcbutiadiene BRL5ei-78€ 2-Hexanone (MBK) BRL9a{2-8 lsopropylbenzene BRL99{7€ +lsoproMoluene BRL1634{4-.{ Methyl tert-butyt ether BRL10&10-1 4-Methyl-2.pentanone(M|BK) BRL7549-2 Mettrytene chtodde BRL
SW 846 02608 2A-Mat-O7 2A-Mat-O1 70316S3 RLJ
91-2G3 Naphthalene
Page I of 165
IhLs bbo.alary fepo L\ not valu wtlhou !^ tuho.hed siE airre on the coverpage.
+ Reportable D€t€crion Limrt BRL = B€low Repo(inB Limit
Page 200
Sample IdentificationM8F-16 2,-4'sA5964l-01
Client Pmiect #301-88
MarixSoil
Collection Date/Time?t-Mar-07 00:00
Received22-Mat47
CASNo. Anab.z(s) Frag "RDL Dih'tion Method ReJ Prepdrcd AaalyTed Barch Aral'sl
Volatile Orgtnic Compoutrds
Volatile Oroanic ConooundsPropared by method SW846 5035A Soil (to!v tewl)10+66n n-Propylbenzene100-42-5 Styrene630-20{ 1,1,1,2-Tetrachloroethane7&34-5 1,'1,2,2-Telrachtorethane127-184 T€trachloroebene108{43 Toluenea7€1{ l,2,}Trid orob€nzenei?G€2-1 1,2,+Tdchlorob€nzene71-55{ 1,1,1-Tridtlometharle79{G5 1,1.2-Trichloroethan€Z9{1-6 Trichtoroethene
96.i8-4 1.2,3-Tricfiloropropane35435 1,2.+T.jmeftylbenz€ne108474 1,3,s-Trimethy'benzone/s-oi-4 Mnyld oridel33LAn7 m.p"Xylene95-47{ o-Xyl€ne10+99-9 T€hahydrofuran60-29-7 Ethyt ethe.991-{5{ Tert-amyt nethyl €lher637.92-3 Ethyl tert+utyl eth€r10e20-3 Di-isoprcpytether75{$o Tert€utanol/ butyl atcdtol123-91.1 1,4€bxan€
Swmgata rccgreies:460401 +Bronofluorobenzenem37-2dF5 Toluet@4St 706047-0 1, 2-Dichlotuethane4l18686Xt Dibrcnonuoronethane
Ert rcarbl€ Petrole|rm Hydrocorbotr!
Exuaclable Total Petroleum Hvdoca.bonsPrepared by method SW846 35508800e6l-s Gasolinc6e47S30-? Fuet oit #26847e31'3 FuelOit #4€ssalooa Fuel Oll [6M0980m00 Motof oilJ00rm00O Aviation Fu€/
UnidentifiedOthef OilTotal Petrolaum Hydroc€rbonsC9-C36 Aliphelic Hydrocarbons
Su/logale rccovedes:xJ86.3+2 l-Chlot@dadecene
Semlvolrlile OrErhh CompoBtrdi by cCOroanochlorins Pestbides SW846 80814Prepared by method SW846 35rt5A409-00-2 Aldrin
SW 046 82604 2&MEr{7 28{vla.47 7031693 RLJ
75-69-4 Trichloroffuorch€ltEne (Freon t 1) gRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL
8699t r6105
8RLBRLBRLBRLBRLBRL345Calculated as345345
110
pglSdry 5.4
ldkS dry 5 4
ldkgdry 5.4
|,dkg dry 5.4pgftg dry 5.4
lrdks dry 5.4
ldkg dry 5.4
Fgkg d.y 5.4pSikS dry 5.4
Ugrkgdry 5.4
ldkS dry s.4
UgkS dry 5.4
lSikS dry 5.4
udkgdry 5.4pdts dry 5.4
!Sn(g dry 5.4pSlkg d.y 1O.7pSftsdry 5.4
ldkS dry 536
udkg dry 5.4
Udk8d.y 5.4pgkg dry 5.4pEtg dry 5.4
ldlg d.y 53.6
lSrkS dry 107
7G130 %7G130%7G130%70-130 %
mg/kg dry 38.4
mgJt€ d.y 38-4
ft€49 dry 38.4
flE/kS dry 30.4
mSn(S dry 38.4
rElksdfy 39.4
tngikg dry 38.4
nBkg dry 38.4
mdks dry 38.4
firg/kg dry 38.4
40.140 %
+CT ETPH 2S-Ms,47 28 Aar07 7031513 DS
BRL t'dks dry 8.09 SltV$46 80BlA m-Mar47 ?8-Mat47 7031516 TG
This laLotulory rcporr is ,tol rditl withoqt on ottrtoded $gnelrre oa dE cat er poge.
i Repoiable D€{ection Limir BRL = Below Reporting Limit Page 4 of 165
Page 201
Sarnple IdertificationM$F-r6 2i-4'sA5964l{ l
Client Project #30t -88
ColLection Date/Time2l -Mar-07 00:00
MatrixSoil
Received22-Mar-07
CAS No. Anabu(s) Resklt Floq Ani6 *RDL Dilution Method Retr Prepared Anabzed Bakh Atu'rystS€mivolalile Orgrnic Compounds by cC
Oroanochlorine Peslicides SW846 8081APrepaied by method SW846 35454
3J9,84$ a_BHC319€5,7 b-BHC319-86-8 d_BHC58re-9 g.BHC (Lindane)
5T-74-9 Chlordane72-544 4,4!0DD (p,p')
72-5te 4,4!DDE (p,p')
cr-2+3 4,4'-DDT (p,p.)
60-s7-1 Dielddn959,98-8 Endlosulran I33213-6+9 Endosulfan ll1031{7-8 Endosulfan Sulfatef2-2V4 Endrin7421-93-4 Enddn Ndehyde76-44-8 Heptachlor724X-5 l\rethoxychlor1024,57 3 Heptachtof Epoxide8001-15-2 Toxephene5103 71-9 a-Chlordane5,566,34-7 g_Chh|rdane
53494-70-5 Endrin Ketone
Surmgale remvenesl1a3868+2 4,+D8-Octalluorobjphenyt (Sr)2a51-24-3 Decachlorohiphenyl (So
Polvchlorinated Biphenvls bv SW846 8082
Pfepared by melhod SW846 3545A
12674-11-2 PC8 101611104_?8:2 PCB 122111141-16'5 PCB 1232$449,21.9 PCB 124212672-294 PCE 124811097{9-1 PC8 t254110e6{2-5 PCB 126037321.23-5 PCB 12621110C144 PCB 1268
Sufiog4te rccoveries:10i86812 4,4-Dgocta0uo(obiphenyt (Sr)
2051 -2at Decachlorobiphenyl (St)
Semivolatil€ Organic Compolnds by CCMS
BRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLSRLBRL8RLBRLBRLBRLBRLBRLBRLBRL
741 1 1
8RLBRLBRLBRLBRLBRL274BRLBRL
4075
udks dry 6.09pdkS dry 6.09
ugks dry 6_09pdks dry 6-09
ldks dry 30.4
lSftS dry 6-09
ldkS dry 6.0spS{(S dry 6.09
ldks dry 6.09pg/kg dry 6.09pdks dry 6.09
UdkS dry 6.09
!S/Kg dry 6.09
ugKgdry 6.09
ldKs dry 6.09pg/kS dry 6 09ps/kg dry 6.09
ugiKg dry m.4
Ug/kg dry 6.09pStxgdry 6.09pg/kg dry 6.09
30-150 %30-150 %
lrg/kg dry 12.2pg/kq dry 12.2pg/kg dry 12.2pgkg dry 12.2pgI(S dry 12.2pgkgdry 12.2pdkSdry 12.2pS/kS dry 12.2pg/ks dry 12.2
3G150 %3L150 %
sw846 8081A
Sw846 8082 2AMar-07
26-Mar-07 28-Mar-07 7031516 TG1
1
1
1
1
1
1
1
I
1
1
I
1
i
I
I
1
1
1
1
1
7031515 SM
Semivolatile Oroanic Compounds bv SW846 8270CPrepared by method SW846 35508
83.32I Acenaphthenem&96{ Acenaphthylene62-53-3 Anilin€12G12-7 Anlhracene1912.24-9 Atralne10+33n Azobenzene/Diphenyldiaznes2+7-5 Benzidine56-s$3 Benzo (a) antihracene
SW846 8270C 26-MarO7 .l.,,,ar07 7031514 M.BBRLBRLSRLBRLBRLBRLBRLBRL
usfts dry 476usrKs dry 416ugrkg dry 476!S/kS dry 476
!g/kg dry 476
ldks dry 476
!g/kg dry 416
ldkS dry 476
5
5
5
5
5
5
5
5
This laltonrory rcpoft it ,tot tlIU tlrithou ah auho.lzed sig ottte on rte co,er paEe
* Reportabl€ D€{e€tion Lirnir BRL = B€low R€porting Limir Page 5 of 165
Page 202
Sample ldentificatiqnM8F-r6 2'-t'sA59641-0r
Client Proiect #301-88
MatrixSoil
Collestion Date/Time2l-Mar-07 00:00
Receiv€d22-Mat47
CAS No. Analy,e(s) Resull FlaC AEia *RDL Dil$i'n Method fr.tr Preparcd Aaalyed Batclt A,sN
S€mivolelil€ Orgstric Compoutrd! by GCMS
Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35508:'0n2{ B€nzo (a) pyrenem+ss-2 B€nzo (b) fluoranth€ne1s1-24-2 Bonzo (g,h,D perylon€al7-o8€ 8€nzo (k) fiuoranthene6fifl BerEoic acid10o-5i6 B€nzyl alcohol111-91n Bis(2-chloroethoxy)fiethane1i1-4.r-4 Bis(2-€filoroethyl)enh€.3s63+32-e Bis(2-chlomisopropyl)sthef117-81-7 Bis(2-€trytheryl)phhatete101-5fi 4-Bromophenyl ph€nyl ether85{&7 Butyibonzylphtttatate86-7+€ Caabazol€59-5G7 4-Chlo.GS.mefrylphenol10€4ru 4-Chtoaoanitine91-5&7 2chloonaphthalene95-57{ 2-Chlorophenoi700+72-3 4-Chlorcphenyl phenyl ether2ltl-{X.g Chrysenef3-7{}3 Dibenzo (a,h) anthiacene132$44 Dibenzofuran95-5I}1 .1,2-Dichlorobenzene
441-73-1 |,3-Dldiorobenze0e106-1e7 1,4-Dict{orobenzene9r-91L1 3,3-Didtlorob€nzidine12G?,3-2 2,+Di{rlorophenol04{G2 Diethylphthalate131-11n Dirn€thyl phthatatetotr-/{ 2.4-Dimethylpheno,lu-7+? Oi-n-buty'phhatate534-s2r {,6-Dinitc2-methyiphenols1.2&5 2,4-Dinilrophenol121-t4-2 2,4-Dinihololu€ne6OCzo.2 2,6-Dinihotoluene117€a-0 Oi-n-octylphdEtats20G44-.0 FluoEnttene8E-73-7 Fluo.eoeli6-7'l.i Hexachlotobonzene87.66-3 Hexoc+tlorobutiadGne1147 4 Hexac.hlorocyclopentadien€67-72-1 Her€doroelhane1913s-5 Indeno (1.2,3d) pyrene9{r.12-0 l-Melhy{naphthal€ne78€Sl lsophorone91-57{ 2-Metfiylnaphhslene96-4e7 2-M€lhy'phenol10F3+4, 3,+Methytphenol106-114-59t,2G3 l,laphtllat€ne
u-74 2-Niuoatnalines,rr$2 +Nitroanitine
Srt/846 8270C 2Glrar{7 28-l.lar{7 7031514 M.ABRLBRLBRL8RL8RLBRLBRLBRLBRLBRIBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBR.LBRLBRLBRL
BRLBRLBRL
!SI(g dry 476pdkS dry 476
Fdhgd.y 47€
lgl(gdry 476
rg,/}gdry 176
UdkS dry 476
ldkS dry 476
FdkS dry 476yqrgd.y 476
lJglqdry 476
!S/kS dry 476
ldksdry 476pS/rS dry 476pdkg dry 176
udkgdry 476pS/kg d.y 476
!S/kS dry 176pg/kS dry 476
ldkS dry 476
Fg/kg dry 476pgkgdry 476
#dkS dry 176
Idr(g dry 476
Fdkg d.y 476
rdksdry 476pdkg dry 476
ldxg dry 476
!g/kg dry 176
tdl(g dry 476pS^S dry 476
udl(g dry 476pdkS dry 476
ldks dry 476
[dl€ dry 476
UdkS dry 476pgl(g dry 476
Udxg dry 476psrksdry 476
lCftg dry 476
Ug/l€dry 476
lrdkS dry 476pdl€dry 476pgJkg dry 476
ldrg dry 476
ldl€ dry 475pgkS dry 476
ldl€dry 476
ugkS dry 4?6
usftSdry 476
ldksdry 176
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
This labrslory rcFEr is nol wld roithornt ad aulLodazd sig obtrc oa tha cawr poAe.
' Reportabl€ Delection Limit BRL = Bclow R€porting Limir Ptge 6 of165
Page 203
Sample Id€ntificationMEF-t6 2'-4'sA59641-01
Client Proiect #l0l-88
MatrixSoil
Received22-Ma.r07
Collection Date/Time21-Mar-0? 00:00
C"4S No, Anatrte(s) Resull Flag Unirt *RDL Dilution Mefiod netr Prepaftd Aturyze.l Bolch Analfst
Semtiolatile Organic Compornds by CCMS
Semivolatib Oraanic Compounds bv SWO46 8220CPrepared by method SW846 35508
10c01$ 4-Nitroanitine9A-9+3 Nitrobenzene€8-7+5 2-Nitrophenol100-02-7 4-Nitrcphenol
62-75-9 N-Nitrosodimethytamine621{4 7 N-Nitrosodi-n-propylamine86-30-6 l'{-Nihosodiphenylamine87-8es PentachtoropfEnol85{1-8 Ph€nanthrene108-95 2 Ph€nol12900{ Pyrene110{6-1 Pyridine120-821 1,2,4-Tdclilorobenzene95-95.4 2,4,tTnchtorcphenoleg46-2 2,4,6-Tichtorophenol
Suftogale Ecovedes:321-60a 2-Fluorobiphenyt
367-12-4 z-Fluorophenol
11 65404 Nilrobenzene-ds
416s 62 2 Phenot4s
BRLARLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
59474851
Completed
BRL
8RL
0.0577
BRL
0 01s3
BRL
0.0161
BRL
s4.'l
pg/kg dry 1900
rc/kg dry 476pg/kg dry 4f6
trdt(S dry 1900
UdkS dry 476pdkg d.y 476pS/kS dry 476pdks dry 476
ldkS dry 476
ldkS dry 476pdkS dry 476pS/kg d.y 476
IdkS dry 476pdkg dry 476pdkS dry 476
30-130%15-110 %n-t30%15-110 %3G130 %15-110 %
mg/kg dry 0 0309
mg/kg dry 0-976
mgr'tg dry 1,46
nE/kg dry 0 4&]
ntgr'kg dry 0.244
mgL/kg dry 0.488
rhCftg dry 0 732
mgikg dry 1.46
mSI 0.0200
mgfl 0-0150
rngl 0.0150
mSn 0.0025
mg/l 0.0150
mS/ 0.00040
mg/l 0.O15O
mgn 0 0150
%
5
5
5
5
5
5
5
5
5
5
5
5
5
5
1718-51-0 Terphenyl4l4 68118-/9-o 2,4,6-Tibromophenol Ss
Tord Metrls by EPA 6000/7000 s€ries Mfthods
7439 97$ Mercury 0 0707
Totsl M€rals by EPA 200 Scries Methods
7440-224 Sllve(
7,140,3&2 Arsenic
7440-393 Badum
7a40-419 Cadmium
7440-47 3 Chromium
7439-92-1 Leacl
778249-2 Selenium
SPLP Extraction
7440-224 Sitv€r
742t{-3€-2 Arcenic
7440-33-3 Barium
7r|{0-4$9 Cadmium
7lK0-47-3 Chromilm
7439-97-6 Merc!ry
7439-92-1 Lead
77€?-4+2 Selenium
Ceneral Ctemhtry Prrrmete.s
% Solids
1 SW846 74714 2A-Mat47 2A-Ma..07 7031495 YP
EPA 200.7 28-Mar47 28-N{ar-07 7031434 Rl.l|BRL
5 5 9
28.A
0 .615
30.4
49.7
BRL
SPLP M€talr by EPA 13l2 & 6000n000 Series M€thods
t SW8461312 26-tlaF07 26-MaF07 7031560 BD
1 SW&161312/60104 28-Mar-07 28-MaF07 7031651 HB
1 '
1 '
1 '
1 "
1 SW84613141470A ' 28-1,4a{-07 7031652 YP
1 SW846131260108 " 28JI1,a(O7 7031651 HB
1 '
1 SM2540 G Mod. 2+MaA7 24-Mat47 7031470 QP
Thb labomtutry rcport is nol volid *ithou an tuthofi@d signatwe o^ the crver paEe .
+ Reporlable Detection Limit BRL = Below Reporting Limit Page 7 of 165
Page 204
Sample IdentificariotrMtF-r7 4'{'sA5964l-02
Client Proiect #301-8E
t{ahixSoil
Received2?-Mar47
Collection Datey'Time21-Mar4? 00:00
CAS No. Analflc(s) Resaa FIog *R.DL Duadon Melhod Ref, Prepatul Ansbaed Bdch Aialtsl
Vohdle Otgaet Compo|rndr
vOC Efiraclion Fiold exfacted
2ffi
ydks dry 69.2
lgrsdry t380
ugts dry 69.2
ldks dry 69.2
lgfts dry 69.2pdks dry 69.2
ldks dry 69.2
t4fts dry 69.2pgr(g dry 138
!g/kg dry 6S2
lgAS dry 69-2
UgkS dry 69-2
lSftg dry 69.2
t gl€ dry 346
Ugikg d.y 63.2
uSAgdry 6s.2pqkg dry 138pdkg dry 69.2pdks dry 138
IdkS dry 69.2
[r9lk0 dry 69.2pgkS dry 138
!S/kS dry 63.2
FS/tg d.y 63.2pykg dry 63.2pdks dry 69.2
rS/kS dry 69.2
IdkS dry 692pdko dry 13S
t'dko dry 69.2
IdkS dry 6S.2
US/kS dry &.2pCI(g dry 69.2
!g/kS dry 69.2
ldkS dry 69.2
ugts dry 69.2
lg'l(S dry 69.2
trgkg dry 69.2
Ugf(o dry 69.2
IS/r9 dry 69.2
udkg dry 69.2
udkg dry 69.2
!g/tS dry 692pgkS dry 69_2
uSn€ dry 69,2
t'dkg dry 69.2
ldkS dry 692
!S/kS d.y 692
rdksdry 69.2
26-Mer47 26 lar47 7481584 BDVolatile Oroanic ComDounds Ro5Prepared by mothod SW846 5030 Soit (high levet)76.1!1 1,'1,z-Tridtlorotriiuoroethane(FreoBRL4744.1 Acetoos BRL107.1}1 Adlbnitile BRL7113.2 BerEsrl€ BRL1&s-86-1 BronrbefEene BRL71.97-5 Broanod o{omethane BRL75-2?1 Ekornodichioromethane BRL75-212 Brornoform BRLzt++g Brornomethane BRLm.e3-3 2-Butanone (MEK) BRLro4-s1€ n-Butylbenzene BRL13598€ s6c€utylberEene BRLs{s6 ted-Butytbenzene gRL
75-1t0 Ca6on di6ulfide BRL56-2+5 Cafuoli lefachloride BRL10+90-7 Chloaob€nzffe BRL75{)G3 C,hlqoothane 8RL675G3 Chto.ofiorm BRL71{,7-X Chloromethffe BRLe5-49{ 24htoototuene BRL1rl&43-4 zl_Chtorotoluene BRLge12-€ t,2-DibromoS-{tttorcpropane BRL12+44-l Oibrcmodrloromehane BRL10c93-{ l.2-Dibomoethane(EDB) BRL7,r,9+3 Dibrodtomethane BRL95-5Gl 1,2-Dichlorobenzen€ BRL541-73-1 l,SDichlorobenzene BRLi0e'4f!7 l,+Dichlorcbenzene SRL75-714 Dichlcrodifuoromethane(F|Bonl2)BRL7t34-3 .1.1-Dichloroetfiane BRL107{6-2 l,2-Did oroethane BRL?t35rt ,1,1-Dldrloro6thene BRLr5&E€,2 cis-1.2-Oichlo.o€lhene BRL15,€io'5 t?ns-1,2oid{oroedrcn€ BRL78{7.5 1,2-Oichto.opropane BRLi42-2S9 .l,9Dichloropror,ane BRLs9+2{r7 2,2-Dictttorcplopane BRL5,6958{ 1.1-Dichlo{bpropene ARL100€t{1-5 cigl,3-Dlchlomprop€ne BRL10061{2{ tans.1,3-Dlchtoloplopene BRL10G414 Ethyb€nzene BRL87'6&3 Hexad orcbutadiene BRL591-78{ 2.Hexeion€ (MBK) BRL9€{2{ lsopropytb€nzoie BRL99{76 +lsorropyttotuene BRL1634{44 Mediy|led-bubd ether BRt_108-10.1 +Mehy'-2-penbnone(M|BK) BRL7s"{re-2 l|€tlrylen€ d odde BRI_
50
50505050
50
505050
50505050505050
50505050505050505050
50505050505050
50
5050505050
SWE|6Em0B 27^ er47 2A-$i*47 7031642 mar
s1-2e3 Naphthalene
Page E of 155
Thit labo4tory rqod b not v4lu wiahoa an aulhorizptr ig at*re on thz cor'.r page.
. Reportable Dst€ction Limit BRL = Betow R€porting Limit
Page 205
Samnle ldentificationM8F-17 4'-6'sA5964l-02
Client Proiect #301 -88
Collectioo Datc/Time2l-Mar{7 00:00
MatrixSoil
Rcceivcd22-Mar-0'7
CAS No- /tnaltte(s) Flog Uni6 +RDL Dil,'tioh Method ReJ Prcpared Analrzed Batth /lnalFt
Voladle Organic Compounds
Volalile Orqanic ComooundsPrepared by method SW846 5030 Soit (high tevet)1016t1 n-Pmpytbenzene 8RL100-42-5 Styrene BRL63G20$ |,1.1,2-Tekachloroelhane BRL79-34-5 1,1,2,2-Tekachloroethane BRL127 10-4 Tetrachloroethene 8RL108.84-3 Toluene BRL87$1€ 1,2,3-Trichtorobenzene BRL120-82-1 1,2,4-Trichlorobenzene BRL71{t6 1, |,1-Trichloroethane BRL79rlG5 1,1,2-Trichlorcethane BRL7941{ Trichloroethene BRL75$9-4 Trichloronuoromethan€ (Freon 1t) BRL96-18-4 l,2,lTrichloropropane BRL95{3{ 1,2,4-TrjmethylbenzerE BRL108-67€ 1,3,5_Tdmethylbenzene BRL75-01! Vinytchtoride133c20-7 m.p-Xytene95-47-6 o-Xylene109-99-9 Tetahydrofuren60-297 Ethylether994-05{ Ted-amylmethylether6!7-s2-3 Ehy' teft-butyl ether108-20-3 Di-isopropylether75$S0 Tert-Butanol/ butyl alcohol123-91-1 1,4-Dioxane
Surogale rccorqries:460-00-l +E|rcrnolluorobenzene
20i/-26-5 foluene-dg
1 7 06U07 -0 1, 2-Dichl orcethane-d4
1868-s3-7 Dibromofl uorcmelhane
Extractrble Petroleum Hydrocrrbons
Extractiable Total Petroleum Hvdrocarbons
Prepared by mothod SW846 35508
8006{1-S Gasolane6847430-2 FuelOil#268476 3i .3 Fu€tOi l#46Ass3f004 Fuej oil j6
M0980qlo0 Molo( oilJ0010{DC|0 Aviation Fuel
Unidentified
Other Oil
Total Petroleum Hydrocarbons
C9436 Afi phatic Hydrocarbons
Surogate recoyer'esj33aG33-2 7-Chlorooclaalecane
Semivolrlile Org'ric Compourds by CC
Oroanochlorine Pesticides SW846 8081APr€pa.6d by method sw846 3545A
309{{).2 Alddn
BRLBRLBRLBRLARLBRLBRL8RLBRLBRL
10410810199
BRLBRLBRLBRLBRLBRL8,5'10Calc!lated as8,5108,5r0
ugkS dry 69.2
lgkg dry 69.2
!S/kS dry 69.2pdkg ury 69.2
!g/kg dry 69.2
ldks dry 69 2
!S/kS dry 69.2
lsftg dry 69.2
UStkS dry 69.2
PS&S dry 69.2pSrkS dry 69.2pgkS dry 69.2
lgkS d.y 69-2
!Sn<g dry 69.2
ISAS dry 692
lSftS dry 6S.2
lSn€ dry 138
lSftS dry 69.2
ldkS dry 692
ISAS dry 69.2
!g/kS dry 69 2
lgftS dry 69.2
lSit(S dry 69.2
!S/kg dry 692pdks dry 1380
70-130%70im %70-tm%70-tm %
rq/kg dry 195
"r1€/kS dry 195
mS/kg dry '195
nr€Jkq dry 195mg/kg dry 195mg/kg dry 195mg/kg dry 195mg/kg dry 195mgftgdry 195nglkS&y 195
40-140 %
5050
5050
5050505050505050505050505050505050505050
5
5
5
5
5
5
5
5
5
5
SW 846 82608 27'Mat41 2g]vtadf 7031&2 n'al
+cT ETPH 26-[Iar-07 28-rrar-07 7031513 oS
ldkS dry 6.75 SW8468081A 2&Mer-07 28-[4rr{7 7031516 TG
Thb laborclory rcpod is nat vslid x,itholl an atdtod.ed signdture oB the cowr page .
* Reportable Det€.tion Lirnit BRL = Below R€porrinC Limit Pas€ 9 of 165
Page 206
Sample ldendficationM8F-17,1'16'
sA59641{2
ClientProiect #301-EE
MakixSoil
Collection Date/Iime2t-Mar47 00:00
Received22-Mat47
CAS No. ,lnaltu(s) R.st U nag Urrits *RDL Diludon Llethod ReJ, Pepared Analwd Bdt h Aralfst
Semivohtile Orgrtrlc Compounds by (rc
Orqanochbrin€ Pesticides SW846 8081APrepar€d by method SW846 3545A
3t+8a{ a-BHC319{5-7 b-BHC319-€6€ d-8HCsa{se g-BHC (Lir$ane)57-744 Chlordane12-544 4,,|'-ODD(p,p'I72{rs 4,4'-DOE (p,p,)s!?Fs 4.41DDT (p,C)€057-1 Dleldrin95+9&€ End,osuijan I321165-s Erdosulfian tlt03147+ Endosulian Sutfate72-20{ Enddn7421{3-4 Endrin Aldehyde76-1-{-8 Heptadtlor72.1.3.5 MefFxychlor1024-57.3 l-bptachlor Epoide8001-3+2 Toxaphene5103.71-9 a-Otlordane5s6€-34-7 g-Ch{ordane53a94-70-5 Endrin Ketone
Sunogat€ rsror€rt6s--10386 8+2 4,4 -Dgoclenuo.obiphenyl (Sr)2+51-2+i DscachlorcNphenyl (So
Polvcnbnnated Biofisnvls W SW846 8082Prepared by method SW846 3545412674.11-2 PCB 10161r1(X-28-2 PCB 1221r1141-16,s PCB t2325315+2r-9 PC8124212672-29{ PC8 1248r1097{Fl PCB t25411096825 PCB 126037324-23.3 PCg 1m2i110cr4-4 PCB t268
Sunogal€ r€corror,esr1o?aEaa2 4,+DB&Equorobiphenyt (Sr)m51-243 Oacadlorohiphenyl (Sr)
Se mlvol.ailc Orgni€ Compound3 by GCMS
BRLBRLBRL
BRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRL
6853
BRLBRLBRLBRLBRLBRL21.6BRLBRL
50
BRL
BRI-BRLBRL8RLBRLBRL988
udxg dry
Pqxg dryIS/kS dry
ldkg dry
US/kS dry
Lrgil€ dry
PSXS d.ypgrq dry
USlkS dry 6.75
l|gl€ dry 6.75
tl{r'es dry 6.75
lCftS dry 8.75pdks d.y 33.8
udkSdry 6.75
rcn(S dry 6.75
ldrq dry 6.75
rrdkS dry 6.75
FSftSdry 6.75p$fts dry 6.75pdks dry 6.75
udks dry 6.75
t'dksdty 6.75
lSn€ dry 6 75
UCI(g dry 6.75
lgrS dry 6.75pdkg dry 33.8
!gl(S dry 6.75
Ugn€drt 6-?5pdrS dry 6.75
30-150 %301fr%
pS/kS dry 13.5pdkS dry 13.5
UCftS dry 13.5pdks d.y 13.5
ISAS dry 13.5
ldksdry 13.5
lgAs dry 13.5pdkg dry l3-5pdkg dry 13.5
so-150 %30-150 %
SW846 00814 26-Mar.O7 28{t4ar{7 7031516 TG
SW846 E082 26-Mat4? 2A-tAs47 7031515 SM
Semivolatile O.oanic Comoounds bv SW84ti 8270CPfeps(ed by me$\od SW846 35508[3.32-9 Acanaphthene20&9ffi Acenaphthylene62€+3 Anillno12G12-7 Anthracene1912-24€ Ab€zine'103333 Azob€nzen€y'Diphenyldiatne9247-5 BerEidines6,5t3 Benzo (a) anthracene
SW846 8?70C 2dMat47 ?34tat47 7031514 M.S444
444
444
444
444
444
.r04484
555555
fh6 |4ra'',loty .fjp*t b,tttral tx'ith'n tt,.tthoriid signature oDdte covctt age.
. Reportrble Derectio Limit BRL = Below Repo.ting Limit Page l0 of 165
Page 207
Samole IdeptificationM8F-l? 4'-61sA5964l-02
CLient Proiect #301 -88
MatrixSoil
Collection Date/Time2l-Mar-07 00:00
Received2?-Mar-07
CAS No, Analy.e(s) Flo9 *RDL Dilution Method Retr Prcparcd AnalJzed Bdch Analtsl
S€mivolNtil€ Organlc Compounds by GCMS
Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35508
fo,32,B Benzo (a) pyrene
205,99,2 Benzo (b) nuoranthene191_24 2 Benzo (g,h,a) perylene207-08 9 Benzo (k) iuoranthene65J5{ Benzoic acid100'51$ Benzylalcohol111-91-1 Bis(2-chloroethoxy)methane111444 Bis(2-chloroehyl)etEr3e63e-32-9 Bis(2-chloroisopropyt)etherr17-81-7 Bis(2.edtythexyt)phthatate101'553 4-Bromophenytphenylether
8564-7 Butylbenzytphthatate86-74-6 C€rbazole59-507 4-Chtoro-3-methytphenolr0s47-8 4-Chtoroaniline91-58-7 2-Chtoronaphthatene95-57-8 2-Chlorcphenol7005-72-3 +Chlorophenylphenylether218-01-9 Chrysen€53-7G3 Dibenzo (a,h) anthrEcene132$a-9 Dibenzofurans5-50'l 1,2-Oichlorobenzene541,73-1 1,3-Dichtorcbenzene106!6'7 1.4-Dichlorobenzene91-94.1 3,3--Dichlorobenzidane120€3-2 2, -Dichlorcphenol
M{6-2 Diethytphthalale131-11n Dimethylphthalate10S7-9 2,4-Dim€thytphenolu-74-2 Oi-n-butylphthalate534-52-1 4,6-Dinitro-2-methytphenols1-28-5 2,4-Dinikoph6nol12rr,{-2 2,4-Dinitrotolueneffi-21}Z 2,6-Dinikotoluene117{4.0 Din-odylphthalat€2064-44 Fluoraothene8&717 Fluorene118-74-1 Hexachlorobenz€n€87$8,3 Hexachlorobutadi€nef7471 Hexachlorocycjopeniadiene6?.72-1 Hexactlloroethane19139,5 Indeno (1,2,3-cd) pyrene
90.12,0 1-Meth!4naphhalen€7a-59-1 lsophorone91-57-6 2-Methylnaphthalene95-48-7 2-Methylphenol
106-39a, 3,4-Melhylphenol106-114{91-2G3 Naphlttalene8a-74-4 2-Nilrcaniline99{+2 }Nitroenitine
BRL1, r40BRL930BRLBRL
BRLBRLBRLBRLBRL
8RLBRLBRLBRLBRLBRLBRL1,370BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL2,990BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARL
BRLBRLARL
!S/kS dry 444
!S/kS dry 484
pg/kg dry 484
f.ig/kg dry 444
Ugftg dry 444
pS/kS dry 444
!S/kS dry 4U
pS/kS dry 44
UdkS dry 4U
pS4g dry 484
!S,4(S dry 484
!g/kg dry 4M
!g/kg dry 484
US/kg dry 484
lgkgdry 444
!g/kg dry 4a4
!S/kS dry 4a4
ldkgdry 4A4
UdkS dry 484
pSftS dry 484
!S/kS dry 444
!Si4<S dry 4M
l.islkg dry 484
Lig/kg dry 4A4
Ug/kg dLt84
udkg dry 441
US/kS dry 4a4
!g/kg dry 444
pdkS dry {44
pg/kg dry 444
!g/kg dry 444
!g/kg dry 4U
!S/kS dry 484
USn(S dry 444
ugkgdry 4upS4$ dry 4A4pgkgdry 444ps/ks dry 484
LrgftS dry 4a4
!g/kg dry 144
!g/kS dry 444
!S/kS dry 4A4
ugkg dry 4E4
Ug/kg dry 4a4pS/kS dry 484pdkS dry 444
!g/kg dry 4a4
US/kS dry 4€4
Ug/kg dry 444
IdkS d.y 444
sw846 8270C5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
26-Mat47 28-Mat41 7031514 M.B
This labomta,! repo.t it noa whd wiahoat an atthodze.l signahne on the catter paEc .
* Reportable Det€ction Limit BRL = B€low ReportinB Lidit Page l l of165
Page 208
Sarnple ld€ntificationMtF-t7 4'-6'
sA5964l {2
Client Proiect #301-88
MatrixSoil
Collectioo Date/Tim€2 I -Mar{7 00:00
Bessivcd22-Mar-07
CAS N^ Anallte(s) Resuk Flog Anib 'RDL Dilatia,r Method nel. Prepored Aaalyzed BdEh AMDst
Semivolstile Orgrnic Compo{nds by CCMS
Semivolatile Oroanic Comoounds bv SW848 8270C
Pr€pa.ed by method SW846 35508
ioo{i€ 4-Nito6nilin€94.95-3 Nihob€nzene€t-7t5 2-Nrtr@henol10Go2-7 +Nitlphenol62-7ts N-Nitdsodimelhylaminem1€4-7 N-Nilio6odi-n-prcpylamine463{!6 N-Nihrsodiphenyhminea7ls5 p€ntacfilorophenol
45.01{ Phenanthr€ne1089$2 Phenoli29{0{, Pyrene
ll0+1 Pyridine1m{z-l |,2,4-Trichlorcb€nzene9Cs+4 2,4,STdchloroph€nole0-0F2 2,4,GTrichlorophenol
Sunogale.ecowdes:321e-a 2-Fluorobiphenyl
?k7-124 z-Fluorophenol
1165-604 Ni'/obenzena45
116162-2 Phenol45
17 18.s1 4 Terphenyl-dl4
11e79-6 l4,6.Tribtodtophenol
Totn Med3 by EPA 60Oy7000 S€ri6 Mea$odt
BRL8RL8RL8RLBRIBRLBRLBRLBRLBRL3.020BRLBRLBRLBRL
6150705168
0 -135
BRL
6.41
46.I
0.569
38.4
7S.8
BRL
WkE dty 1940
Idl(S dry 484
Ugrsdry 444pgrs dry 1940
Ugn(g dry &4
udks dry M
US/kS dry 84
lSftS dry 4€4pdksdry 4a1pdksdry 444
!S/kS dry 464pdkS dry 444pdkg dry &4
ldkS dry &
!S/kS dry 454
30'130 %15.110 %30-130 %1*110%30-130 %15'110%
mg/kg dry 0.0318
ms/kg dry 1.17
mg/kg dry 1.76
mgikgdry 0.586
nE/kg dry 0.293
mgl(g dry 0.586
ttE/kg dry 0.880
m€it(g dry 1.76
N/A
msn 0.0200
lngn 0.0150
mgl 0.0150
n€n 0-0025
nEI 0.0150
nrg/I 0.00040
mdl 0.0150
mSl 0.0150
%
55
55
1 EPA 200_7
1 "
t '
1 "
1 '
28-lvla.-07 28.{!lar{7 7031494
28-l ar{7 7031652
2&Mar47 7031651
SW846 8270C 26.Ma.{7 2&Marfi 7031514 M.B
7439,97{ M€mrry
Toirl M€{rb by EPA 200 S€rtei Methods
?44G224 Silver
7440.3&2 Arsenic
71.1+393 Barium
7t4o-4s9 Cadmium
7440-47-3 Chromium
74i19€2r Lead
7782-4+2 Selenium
SWE46 7471A 26:Mat47 2a].',E,t47 7031495 YP
RM
SPLP Merrb by EPA l3l2 & 600{y7000 serl€s Methodr
SPIP Extra€tbn CorFleled
744$?24 Silvor BRL
Z.()'3sz Anenic BRL
7440393 Badum 0.0440
71-104+9 Cbdmium BRL
74rlo4?-3 Ctrornium BRL
743ss?{ llercury BRL
7439€2-1 Lead 00298
282-19-2 S€tiEnium BRL
CeDedl Chdnistry Prrrm€terg
% Solids 84.0
1 SW84A 1312 28{rer47 26-l €r{7 70315G0
1 SW8461312/60109 2&Mar-07 2&Mar-07 7m1651
1 '
1 "
BD
HB
t '
I s!v8,t6 1312?470A
I SW8,r{i 1312/60't0B '
1 ' ,
HB
1 SM2540 G ifod. 24.lulat47 24.Mar-O7 7m1470 OP
Thit laborurory Epott ls ,tot tdid without an rzlhorizd sigt BtE ott the coeet pqgz.
+ R@ortable D€tection Limit BRL = Below Rcptrting Limit Page 12 of 165
Page 209
Sample IdentificationM8F-18 2'-4'sA5964l-03
Clieot Proiect #J0l-88
Collection Date/Time2l-Maro7 00:00
MahixSoil
Received22-Mar07
CAS No, An tk(s) Resul( FbE 0nits *RDL lllethod ReJ Prepued Aubzzd Batch Antllst
Prepared by m€thod SW846 5O35A Soit (low levet)
76-13.1 1 ,1 ,2_Tichlorotrifl uoroethane (FreotBRL67s-1 Acelone BRL107-13-1 Acrylonitrile BRL714+2 Benzene BRL108-86r Brornobenzene BRL74-97-s Erornochloronrethane BRL75-274 Eromodidtloromethane BRL75-2+2 Erofirofom BRL74{3-9 Bromomethane BRL78-e3-3 2-Butanone (MEK) BRL104-sl-E n-Butylbenzene BRf13+98-8 sec-Butylbenzene BRL98{6{ tert,Butylbenzene BRt7115+ Ca.bondisullide 8Rt56-23-5 Carbon tetrachloride BRL10€-90-7 Chto(obenzene BRL75'00-3 Chloroethane BRL67sc3 Chlorofotrn ARL
14413 Chlorohethane BRL9s-4+8 2-Chlorotoluene BRL106 43-4 4-Chlorotoluene BRL96-12-8 1,2-Dibroryro-3-chtoroprop6ne 8RL124{8-1 Dibromochloromethane BRL10+e3-4 l,2,Dibromoethane(EDB) BRL74-9$3 Dibromomethane BRt
95-5c1 1,2-Dichtorobenzene BRL
541-73-1 1 ,3-Dichtorobenzene BRL106-46-7 1 ,4-Dichtofobenzene BRL71714 Dichtorcdinuoromethane(Freonl2)BRL
75 3+3 l,l-Oichtoroethane ERL
107 06-2 1 ,2-Dichloroethane BRL
75-35-4 1,1-Dicl{oro€th€ne BRL156,59-2 cis-1 ,2-Oichtoroeth€ne BRL15&60-5 trans-1,2-Dichtoro€thene BRL78{7'5 1,2-Dichlo@propane BRL
Volatile Orgrnlc Compounds
VOC ExtractionVolatile Oroanic Compounds
142-28-9 1,3-Dichlorop.opane
59420-7 2,2-Dichloropropane563-58S 1,1-Dichtoroprop€ne10(161-015 cis-1,3-Oichtoropropole1006142€ trans-1,3-Dichloropropene100a14 Ethylbenzenea7{8-3 Hexachloaobutiadiene591 786 2-Hexanone (MBK)
98{2-8 lsopropylbenzene9s{7{ 4-lsopropyltoluene
pS/kS dry 5.7
liSI(S dry 115
lig/kg dry 5.1
!g/kg dry 5.7
!g/kg dry 5.7
!g/kg dry 5.7
!g/kg dry 5.1pg/kg dry 5.7
!g/kg dry 1'1 5
!g/(g dry 51.4
!9/rg dry 5.7jJdkS dry 5.7
uS/kg dry 5.7pdksdry 28.7pdkS dry 5.7
ldks dry 5.7
UdkS dry 11.5
fS/kS dry 5-7
ldkS dry 11.s
Lig/kg dry 57
!S/kS dry 5.7pS/lAdry | 1.5pg/kS dry 5.7
lS/ftS dry 57
!S/kS dry 5.1pg/kg dry 5.7pg/kg dry 5.7
!g/kg dry 5.7
!g/kg dry 11,5pglkg dty 5.7
uS/kS dry 5.7pg/kg dry 5.7pgkS dry 5.7
FdkS dry 5.7pdkS dry s.7
uS4qdry 5.7
lqks dry 5.7
!S^S dry 5.7
ldks dry 5.7
ldts dry 5.7
tg/kg dry 57pdkS dry 5.7pS/kS dry 57.4pS/kS dry 3.7
udks dry 5.7
tSikSdrll 5.7
rd|(g dry s7.4
USn€ dry 57.4
ldkS dry 5-7
26-Ma(41 26-^/lat47 7031584 BD
27-MarO7 27-Mat-O7 7031658 RLJ
Field extr€cted voc
sw 846 82608
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
i63a+a-a ,lethyl (ert-butty' eoher 8RL108-10-1 4-Methyl-2-pentanone(M|BK) BRL75{9-2 Methylene cfilodde BRL
BRL91.2G3 Naphttlalene
Page 13 of 165
Thb labotuory repod k not volu withott! a aathorized siEnztarc o, tAe mvet page
' R€portabl€ DEtection Limit BRL = B€low R€porting Limit
Page 210
Sample IdentificationM8F-18 2,-4'sA5964l-03
Clietrt Proiect #301.86
MatdxSoiL
Collectiotr Date/Time2l-Mar47 00:00
Received22-MEr-07
CAS N^ AaLlrrz(t) R€sllt Fl"E Ania *ftDL Dilutbtl Method neL Prcparcd Analfzet Ba/fh Atrztrsl
Vohtil€ Orgenlc Comporod3
Volatile Orcanic C,ompoundsPrepared by rnelhod SW846 5035A Soit (bw tevel)
75{!Fr T.ichloroffuomrn€tnsne (Freon 1l) BRL
'03{5-1 n_Propylbenz€nel0H2-5 Sorene631)-20-6 t, t t 1,2-Tetrachtoroethane79.345 |,1 .2,2-Tetracl oroethano127n8.4 TetEchloaoeth€ne10&€61'3 TOlUene87616 1,2,+Tridtlorob€nzenerana2n 1,2,4-Tfjdllo.ob€nzene7l-5s |,'l,l-Trichloro€thsne79{D5'1,1.2-Tridrkro€thane?9{1{ Tii,cf oroethens
96-18-4 1,2,+Trichloaopropane95{3€ 1,2,4-Trimethylb€nzene108-67{ l,3,tTdmethylbenzene?5{14 Vinyl cfitoridel$0-m'7 m,p-Xylene95tr74 o-Xylen€10$99-9 TetahtdrofuEn@-2s7 Ethyl eherS4o5{ Tert-amy' m€(.ryl ed1ea637-92-! Edly4 tert-buryl edrert0&2o-3 Dii6opropy'ledEr754S0 l€rt-Butdnol / bultt alcohol12191-1 1,+Dio)@ne
S./t/ogale rccov€nbs,'460{0!1 4.8zomofluorcbenzene
2037-2&5 TohEna4S
lvlaat 474 1,2-Dichloroethane<!4
1 86e-53-t Dibanofl uoro,?ethane
Ertrrc{rble P€i.oleum Hydro$dons
Extradable Total Pelroleum FtudrocarbonsPrepared by m€thod SW846 355088006€r€ crasolhe6847s3G? Fu€t Oil #26&f+31n Fu€l Oil ,r408553{0-4 Fuel Oit f6iao9€000m i/iotof oilJ001m0oo Avialbn Fuel
Unid6nlifiedOtt|e OilTotal Pef olsurh HydaocadonsC+C36 Aliphalic Hydroerbons
Srrnsgl3lo recovbrbs:Atge3l2 | -Ctionodadecane
S€mivol.tile (kgrtrL Comportr& by CCOrqanocfilorine Pegticides SW846 808,1APr€pa.ed by method SW846 35,{5A309{x,-2 Aldrin
BRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRL
BRLBRtBRLBRLBRLBRLBRLBRLBRLBRLgRL
BRLBRL
95
9299
BRLBRLBRLBRLBRLBRL287Calculat€d as247
62
US/l€ drypdkg drypS^g d.y
ugl(g drypdks dry
$Snq diy
|ls/(g dry
udkS dry
uSfig dry
ldxS dry
lSrkg dry
rdkg dry
!Si*g drypgts dry
Udkg dry
ldks drypgag dry
lqxg dry
PdxS dry
ldkg dtypgkS d.y
t Sikg dry
Ugl(g dry
ldlS dry
udks dry
5.7
5.7
5.7
5.7
5.7
5.7
5_7
5.7
5.7
5.7
5.7
5_7
5.7
5_7
5_7
1 1 . 5
57,1
5 7
5.7
57.4
1 1 5
1
1
1
I
I
1
1
1
I
1
1
t
I
I
1
1
I
I
11I
I
1
1
SW 8,$ 82604 27-Mar47 27d.tac-07 7001658 RU
+CTETPH 2a^4sr-07 28-A,lar-07 7031513 DS
7G130%
7G130%
70.130 %
70-1fi %
ntg/kg dry 130r€r'I€ dry 130mg/t(gdry 130ftEftg dry 130mg/kgdry 130mdkS dry 130nrgL/kg dfy 130hgilqdry r30ftE/tg dry 130rvkg dry 13O
4G140%
55
5
5555
}|d@ dry SW846 801llA 26+,lar{7 :E-Mer{7 7031516 TG
Thi6 le&*aory rqod is not wlid pi&rou att or.droriEd signeatre on ttE cow! page.
* Reportabl. D€t€ction Lidir BRL= Below R€portiry Limit Page 14 of 165
Page 211
Sample IdentificationM8F-I8 2'-4isA5964l-01
Client Proiect #301-88
Collection Date/Time2l-Mar-07 00:00
MatrixSoil
Received22-Mar-0'7
C,'IS No, Analyte(s) Result FloS UniE t{e.hod ReL Prcpa.ed Atu|ted Balch Analyst
S€mivolrtil€ Orgrnic Compounds by cC
Oroanochlorine Pesticides SW846 808'tA
Prepared by method SW846 35454
31+845 a-BHC31s-8r7 b-8HC319-€6{ d-8HC58{$9 g-BHC (Lindane)
57-749 Chlordane72-544 4,4,-DDD (p,p')725ts a,4'-DDE (p,p )5G2e3 4,4,-DDT (p,p')
60-57-1 Dieldrin95s98-S Endosulfan I3321a65-9 Endosulfan ll1031{74 Endosulfan Sulfaten-2o4 Endrin7421-934 EndrinAldehyde1644 A Heptachlor7243-5 tvethorychlor1024-57-3 Heptadllof Epoxide8001-35'2 Toxaph€ne5103-71-9 +Chlorclane5s66-34,7 g"Chlodane
5349+70-s Endrin Ketone
Swrcsate rccov€nes:18ae,8+2 4,4-DB-OclafluotobiphEnyl (Sf)
2ost -z+3 DecachltJrobipheny4 (54
Polvchlorinated Biphenvls bv SW846 8082
Prepared by method SW846 35454
12674-11-2 PCB 101611104,2+2 PCB 1221111.41-16 5 PCB 12324n469-21-S PCB 1242'12672-29n
PCB 124811097,69-1 PCB 125411(L9$2.5 PCB 126031321-235 PCB 126211100-144 PCB 1268
Sunogale rccoveies10386-u-2 4,4-D8-Oclafluorobiphent4 (54
2051-2a4 Decachlorobhhenyl (Sr)
S€mivolrtile Org{nic Conpounds by CCMS
Semivolatile Omanic Comoounds bv SW846 8270CPrepared by method SW846 35508
€3n2-9 Acenaphthene:0&963 Acenaphthytene62-593 Aniline12G12-7 Anlhracene1912-24-9 Atazin€10+33+ Azobenzene/Diphenyldiazine
9247-5 Benzidinef'G5+3 Benzo (a) enthracene
svr'846 B0€rA
SW846 8082 26-Mat47 2g-Ma(O7 7031515 S[/l
SW846 8270C 26-Mar-07 28-MaF07 7031514 M.a
8RL8RLBRLBRLBRLBRLBRLBRLERLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRL
107
BRLBRLBRLBRLBRLBRL484BRLBRL
5080
BRLBRLBRLBRLBRLBRL
BRLBRL
ldkS dry 6.25
l4/kS dry 6.25
ldkg dry 6.25yg/kS dry 6.25
!g/kg dry 31.3pS/kS dry 6.25pS/kS dry 6.25pg4(S dry 6.25
!g/kg dry 6.25
!g/kg dry 6.25
!g/kg dry 6.25pS/kS dry 6.25
!S/kg dry 6.25
t g/kg dry 6.25pg/kg dry 6.25
uS/kg dry 6 25pdkS dry € 25pS/kS dry 3'1.3pg/kg dry 6.25
!g/kg dry 6.25
!g/kg dry 6.25
30-150 %30-150 %
Ug/kg dry 126
UdrS d.y 12.6pg/fq dry 12.6pdkg dry 12.6
Ug/kg dry 12.6
!S/kg dry 12.6
uS/kg dry 12.6
!g/kg dry 12.6
lgikg dry 12.6
3G150 %30150 0.4
I
1
1
I
1
1
1
1
1
1
1
l
1
I
1
1
1
I
t
1
FqkS dry 4O2
!g/kg dry 4Oz
fg/kS dry 402pS/kS dry 4O2pdkS dry 4n2pg/kg dry 4O2
!S/kS dry 4O2
Fg/kg dry 402
5
5
5
5
5
5
5
5
This labontory feporr h no. vatid withoul zrr snthofized Eigntturc on the eover poge_
' R€portable Detection Limit BRL = Below Reporring Limit Page 15 of 165
Page 212
Samole IdentificatiooM8F-18 2'-{,sA5964l-03
Client Proiect #30t-88
MatrixSoil
Collection Date/Time21-Mar-07 0O:00
Receiv€d22.M^t4'l
CAS No. Adab'ta(s) Fldg *nDL Dilution Methad Retr Prepued Analwd Ear$ AnaW
ScrEivol il€ O.g.nlc Conpodtrd! by C,CMS
Semivolalile Oroanic Comoounds bv SW846 8270CPrepared by mabod SW846 3550850-32{ Benzo (s) pyrone20+99-2 B€nzo (b) fuoranhene1er.24,2 Benzo (g,h,i) p€rylenem7-l)a-9 Benzo (k) fluoranthene6'AE-O B€nzoic acid1(10-51.6 B€nzylalcotvol1114r-1 Bis{2dllorcefiory)mothanei11-.4-4 Bis(2drtoro€{iyl)ehe.396ire32-e Bis(2-d [email protected] )€tf,er1r74i-7 Bis(2-ehythexyl)phthatate1OL5+3 +Buiophenyl phenyt elher85-6&7 BuM b€nzyt phthatateF71l-8 Cabezole5+5G7 +Chloro-3.m€thytphenol106-47€ +Cl{om6niline91.5&7 2-Chtomnaphthalene9s{7,8 2-Chlompt|€nolzx)5-72-3 +Chtoropheny' ph€nyl ether218-01-9 Chrysene53.7G3 Dibenzo(a,h)anthfacene132{4-9 Dib€nzofij.an!,6-5n-1 1,2-Oido.obenzene541-73-1 1.3-Dichtorcbenzene106-4G7'1.+DichloroberEene91€41 3,3'-Ok$lorobenziline120412 2,4-Didloroo€nol84€F2 Diehy,tphthatater31-i1.3 Dmetiytphhalater0tr74 2,4-oimettlytPhef|olU-7+2 Di.n-buMphtElste53+52-1 4,6loinito-2-methytphenol5l-285 2,+Dinitroph€nol12t-14.2 2,4-Oinitrtol!€n€60c2ll2 2,6-Dinihrtolu€ne1r7{4{ Di_fl-octylphhalat€alfl+o Flud.anthene0&717 Fluoa€nei1g7+1 Hex€chbrobonzene87€ll3 tb)(adtlooh,Utadienen4f1 Hexadorocydopentadiene61-72-1 Hoxad o.mthane19&3e.5 trd€no (1.2,3-cd) Pyrcnesr"12{ t_M€thytnaphthal€ne78{!}1 lsoptrorone!)id7{ 2-tlkthytnaphhaten€!r5.{&7 2-MefiylptEnd10&394, 3,4-Mebylphenol10G44-5gl-293 tlaphthaisneu.7+4 2-Nitranitin€s{s2 }.Nitoanlltne
SW84{i 8270C 26-[,lar-O7 2SJvlar{7 7031514 M.BBRLBRL
BRL8RTBRTBRLBRL
BRLBRLBRLBRLBRLBRLSRLSRLBRL
BRTBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLARLBRLBRLBRI-BRL
BRLgRL
BRL
pSftS dry 42pdks dry 402
USftS dry 42pgkSdry 4oz
ldksdry Q2
rc/(S dry 402pSl(S dry Q2
Fg^g dry &2pSlkS d.y 4O2
usfts dry 4o2pdksdry 42pgrs dry Q2
IgtS dry &2
t gftS dry 62
t SI€ dry 4O2
ldkS dry &2pqkS dry 4O2
lrg/kS dry fi2pS/kS dry Q2
lgkS dry &2
rdkSdry &2pdkg dry &2
USftS d.y 42
tdks dry 4O2
!g/kS dry 4O2
!S/kS dry 62
udlls dry &2pdkg dry &2
rcrkS dry &2
Igr(gdry 4O2pdkS dry 4o2
Fdkgdry 1O2
ld}g dry &2
US/kS dry 62
figkS dry &2pdks dry 1O2
ldkg dry 402
lgftgdry 4O2
tdksdry 4o2
ldksdry 4O2
Idkg dry 62
Idkg dry a@.
USikS dry &2
9gkS dry 42
USAS d.y 42pgRg dry N2
Fg/kg dry 4n2
l.'gts dry Q2
ldkS dry 42
@kgdry &2
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
Thir l4botutory .cpod is noa vali.I witiod r ardho.Aed slg,'tatdrc on thz cover page.
i R€portable Dete.tion Limtt BRI = Below Reporting Limit PNge 16 of 165
Page 213
Sample IdentificatiorltfttF.l8 2'-4'sAs964r -01
Ctient Proiect #301-88
MatrixSoil 22-Mar-07
Cotlectiolr Date/Time2l-Mar-07 0t):00
CAS No- Anafute(s) Res/llr FIag Unitt ,RDL Diluion Method ReJ Prcparcd Anslyed Eatch A,uryst
Senivotatile Organic Compo'rnds by GCMS
Semivolatile Oraanic Comoounds bv SW846 8270CPfepared by method SW846 35508
100{15 4-Nitroenilihe98-95-3 Njhobenzene
08-75-5 2-Nitrophenol100{2-7 4-Nitrophenol62-1+9 N-Nitrosodimethytamine621€a-7 N-Nit.o6odi-n-propylamine66-30i N-Nilrosodiphenylamine87J6-s Pentachtoroph€hol8541{ Phenanlhrene10&95-2 Phenol12900{ Pyrene11G€6J Pyddine12l}821 1,2,+Trichlotobenzene95-9.F4 2,4,$Trichtorophenol88{6'2 2,4,&Tdchtorophenol
Sunogele recoveies:
32140-8 2-Fluorcbiphenyl
36/124 2-Fluorophenol
5 SW846 8270C 26-Ma'.o7 28-Mat-O7 7031514
5 "
5 "
5 "
5 "
5 "
5 "
5 "
5 "
5 '
5 '
5 '
5 '
5 "
5 "
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
615 1
lgkS dry 1610
!g/kg dry 62pgftS dry &2pS/kS dry 1610pdts dry &2
ldkS dry &2
!S/kS dry 62
ldl(g dry &2pgikS dry &2
!g/kg dry &2
lgftS dry 4O2
ldkS dry 4O2
tig/kS dry 42
!g/kg dry 62
!g/kg dry 4t)2
30-1W %15-110 %30-130 %1Ul10 %30-130 %15-110 %
mgftg dry 0.0319
mg/kg dry 0.936
mgl(g dry 1.4O
mgfl(g dry 0 468
mgkSdry 023/
mS/kS dry 0.468
n€/kg dry O.7O2
mg/kg dry 1.40
M . B
4165404 Nitobenzene-d5 52416542 2 Pheno!4s 521/1*514 Teryhenyl4l4 72t1A-795 2,4,6-Tibromophenol 55
Tot8l Mctrb by EPA 6000/7000 S€ries M€thoos
7439-97{ Mercury
Totrl Met{ls by EPA 200 Serier Methods
7440-22-4 Silver
7440-38-2 Arsenic
7440-393 Badum
7440419 Cadmium
7440{7 3 Chromium
74394h Lead
7182-192 Selenium
1 SW846 7471A 28-Ma''O7 2A-Ma'.Ot 7031495 YP
1 EPA2007 28-Mar07 28-Mar-07 7031494 Rl\,{
1 "
1 '
1 '
1 '
1 '
' t '
'1 SW84G 1312 26-Mar47 26-Mar-07 7031560 AD
1 SW846131260108 2A-Mat47 2g-Utal-OT 7031651 Ha
1 '' t '
1 "
t "
1 SW8461312'470A " 28-Mar.07 7031652 YP
1 SW846131ly60108 " 28-MaF07 7031651 HB
I '
0 0605
BRL
4.53
30.8
0.674
34.3
44.4
BRL
SPLP M€tsls by f,PA 1312 & 6000/7000 S€ries Methods
SPLP Ext action Comdeted
7440-224 s'ilvet BRL
BRL
0.0850
BRL
0.0312
BRL
0.0190
BRL
92,2
mg/l
msr
mgr
msnrYEn
fiur
rngrt
rng/l
%
0.0200
0.0150
0.0150
0 0025
0.0150
0.00040
0.0150
0_0150
7,t40-3&2 Aisenic
74-40-393 Barium
74!{l-13-9 Cadmium
74lo473 Chromiufit
7439-97-6 MercUry
7439-92-1 Lead
tE2-49-2 Selenium
Cenerrl Chemistry P.rrm€t€ri
SM2540 G ltl,ed. 24-Miat47 24Nar'O7 7031170 AP% Solids
Page 17 of 165
Thit laborulory report it ttot tqlid Nllhoa an alihodzed sigmture on lhe drver p.tge
' Reportabl€ Detection Limit BRL = Below Reporting Limit
Page 214
Sanpl€ ldedtificatiodMEF.19 2'-4,sA5964 t-04
Cliert Proiect #301-88
MatrixSoil
Collection Dat€/Time2l-Mar47 00:00
Received22-Mar47
CAS N^ Anolru(s) n"E UniB "RDL Dilntun M.lrad ReI PrcWen ,4nalwd Botch Atsltst
Vol{lil€ Otg.rlc Compoondf
VOC Extraction N'A
ldkS dry 6.6
udkgdry 132
uEksdry 6.6psftgdry 6_6
iJdkgdry 6.6
ugkgdry 6.6
lgr€ dry 6.6
t SikS dry 6.6
UgftS dry 13.2
!dl(gdry 66.0
ugkgdry 6.6
US/kg dry 6.6
US/kS dry 6.6pCftS dry 33.0
sgtkgdry 6.6
Ugv€dty 6.6
ttgilq dry 13.2ydlgd.y 6.6
ldkgdry 13.2
rs/kg dry 6.6pdkgdry 6.6
usirqdry r3.2psngdry 6.6pdxg dry 6.6
!g/kS dry 6.6
IqkS dry 6.6pdkg dry 6.6pdrs dry 6.6pg,/xg dry 13.2
ldkSdry 6.6pSftSdry 6.6
Udkgd.y 6.6pqkS dry 6.6
ldkS dry 6.6
!g/kS dry 8.6pdks dry 6.6pSftg dry 6-6
lgksdry 6.6
!g/kS dry 6.6pSftgdry 6.6
t S/kS d.y 6.6
USAS d.y 6-6pdksdry 66.0
UdkS dry 6,6
lqkg dry 6,6pSASdry 6-6
Pgkgdry 66.0pdkgdry 68.0
sdkSdry 6.6
2€+ilar-07 26-l'rar-07 ?031584 BDField extraatedVolatile Omanic ComooundsPrepared by method SW8,l6 5035A Sdl (low l6vet)76-1+l l,l,2.Tridtlorofinuqoetfune(FreoFRL674+1 Acebne BRL107n3-l Acrylonitile BRL7143-2 Benzens BRLt0a{6r g@nobenzen€ gRL
7447-s gromodlloaomehane BRI_ftr-274 Bomodidtlorornelhane BRLf*2r2 Bornoform BRL7:l++9 B,omom€than€ BRL7843.3 2€utanone (MEK) SRL10461€ n-gub'lberEene 8RL13+983 sec-Butylbenzene gRL
s8fi€ tert€ulytbenzene BRL7t15-o Carbofidisumde BRL58.23-5 Caabon tebachloalde BRLi0&9(l7 Chlorobenzene BRL75{03 Chlorc€fEne BRL€7€&3 Chlorotorm BRL7447-3 Ct oromefian€ BRL95-aS8 2€hlorotoluene BRL106{3-4 4-Ortorotrduene BRL9{-12€ 1,2-Dibrono-3-chloropfopan€ BRL124-4{r-1 Dibrcmod\lorcm€hane BRL'r(1693-4 1,2-Dlbrornoethan€(EDB) BRL74-9$3 DibKnno.n€thane BRL9$5{rr |,2-Dichlorobenzene BRLsi4r-73n l,3-Didi orcbenzene BRL1(E-a6-7 1,{-Oichlo|.obenz€ne BRL7t71{ Dlcfilorodifluoroftsthsne(Freont2lBRL75-34-3 i.l-Dichtoroethan€ BRL107{e2 l,2.DlcftloroLethane 8RL7t35-4 1, I -t)ic'|loloethene aRL1s6-5+2 ci9-l,2.Oichtoroethene BRL156{0.5 tEir-1,2-Dhhloro€d1ene BRL78{7.s t,2-Dichtoropop€ne BRLt42-284 l,$Diafiloropropane BRL594.e7 z,2$idrlomp[opalte BRL56$5d{ l.lolcltoropropene BRLtoo61{15 cis-1,}DichtoroF}aopen€ BRLiotl61-02$fans-1,$Oidrtoropmpene BRLl0c4i4 Ethyb€nzene BRL87€&3 Hexacfitorobutadien€ BRL5ei-78-6 2-Hexanon€ (MBK) BRL!l€{2{ lsop.opyb€nzene BRL99{7-6 Alsopropyltolugie BRL163411{4 lr€ltlyl terl-butyl ether BRL108-10-l {-Mehyl-21o6n!anone(M|BK) BRL7549'2 Methyl€ne chtoide BRL
SW 846 8il60B 27-|l'at47 nlnar4f 7031658 RLJ
91-2'3 Nsphthalene
Page l8 of t65
Ihit lzbonlorf reporl is aat vali.I Nithotd sn tathor*"i sigrutuE on &a coler pqE.
' ReporEble Deleclion Limir BRf = B€low Reportirg Limit
Page 215
Sample [d€otificationM8F-19 2,-4'
sA59641-M
Client Proiect #301 -E8
MatrixSoil
Receiv€d22 M^r 0'7
Collection Datc/Time2l-Mar-il7 00;00
CAS No. Analtte(s) FloS *RDL Dilutiorl Prcpdrcd Analyzed Bolch Analjsl
Volatile Organic Compounds
Volalilo Oroanic ComDounds
Prepa.ed by method SW846 5O3SA Soit (tow tevel)
103-65-1 n-Prcpylbenzene BRL10042-5 Styrene BRL630-20$ 1,1,1,2-Tetrachlorcl€thane BRL79-34-5 1,1,2,2-Tetrachlorelhane BRL127-18,4 Tetrachlorcethen€ aRL108,88.3 Totuene BRL87.616 1,2,+Trichlorobenzene BRL12C82r 1,2,4-Tdd1lorcb€nzene ERL71-s5 6 I,1 ,t-Ttid'lor.et1€ne BRL79{0-5 i,1,2-Trichloroethane BRL7941-€ Trichloroethene BRL75694 Trichlorofluoromethane (Freon .j1) BRLs6-18 4 l,2,STrichloropropane BRL95 61.6 1,2.4-Trimethylbenzene SRL10€-67-8 1,3,5-Tdmethylbenzene BRL75{1-4 Vinylchtoride1330-20-7 m,p-Xylene95-47-6 o-Xylene10s994 Tetrahydrofuran60-29-7 Ethyteher99r-054 Tert-amyl methyl ether637,S2,3 E ryi ted{utyi ether1ta-Zl-3 Di-isopfopldetherT'6to Tert-Butanol/ butyl alcohol12+91-1 |,4-Dioxene
Suftogat€ rccoveies:460-004 +Bronofluorobenzene
2037-26-s TolLEne4S
| 7o6co7 4 1, zOichloroethane-d4
1868-53-7 Dibromofluorcmethane
Ertractable Petroleum Hydrocarbo||3
Erlraclable Total Pehol€um HvdrocarbonsPrepared by method SW846 3E5OB
8006$1-9 casoiine68476-3r>2 Fu€t oil#268478-31-3 FuetOiln4
68553{0-1 Fuetoil#6rrl98000m Mobr OilJ00100000 Aviation Fuel
Unidentifed
Other Oil
ARLBRLBRLBRLBRLBRLBRLBRLBRLBRL
96921Ul103
lqkg drypdks drypSftS dry
tiS/kg dry
!g/kg dry
LiS/kS drypg/kg dry
t4/kg dry
Fg/kg dry
lqkg drypsn(g dry
Ugr'l(g dry
IJS/kS drypS,[(S drypq/kq dry
udks dry
Ug'kS drypS/kS dry
t g/kg dry
!g/kg dry
USftS d.Y
udkS drypdks drypdkS drypgl(g dry
6.6
6.6
6.6
6.6
6.6
6.6
6,6
6.6
6.6
6.6
6.6
6.6
6.6
6.6
1 3 2
6_6
66.0
6.6
6.6
6.6
6.6
66.0'132
28.428.428.42A.428.42842A.426428.428.4
1
1
1
1
1
1
t
1
1
1
l
1
1
1
l'|
1
1
1
1
1
1
1
1
SW 446 82608 27-Mat47 27-Mat47 7031658 RLJ
7G130%
70-130 %
7G130 %
70-130 %
BRLBRLBRLBRLBRL
BRL3,260Calculated as
mg/kg drymg/kg drymg/kg dryrnS/kg drynrS&S dryn€r'kg d.ymqkg d.ymS/kS drynrgfl(g drymgn(g dry
+CTETPH 26-MarO7 28-Mar-07 7m1513 DS
TotalPetroleumHydrocarbons 3,260CgC36AliphaticHydrocarbons 3,260
Sunogate rccovedes:$a6-33-2 l-Chloroocladecane tS6
Semivolatile Orgrnic Compounds by cCOrqanocfi lo.ine Pesticides SW846 8O8.lAPreparcd by method SW846 354SA$s{0-2 Atdrin BRL
40.140 %
rcI€ dry 6.16 SW846 8081A 26-Mar-07 28-{\rar{7 7031516 TG
ThLi laboratory repod is notyrldfr rou @ ar.thofited sEnatwe on lhe covc! page.
* Reponable D€tection Limit BRL = Below Rcportinc Limit Page l9 of 165
Page 216
Samole ldentificationM8F-I9 2'-4,sA5964144
Clied Proiect #301-88
MatrixSoil
Received22-M^t-07
Collectioo DatelTime2 I .Mar47 00:00
CAS No- Analrte(s) Flog Units 'RDL D atio,, Mahad netr Przparcd Amlyzd Batch A,,zlys.
Semivotrlfle Orgrdc Compoo.dr by cC
Oroanochlorine Pesticides SW846 8081APrepared by method SW846 35454319{a.6 a-BHC319-85.7 b-BHC319{€{ d_BHCsa.8+e g_BHC (Lindane)57-74-9 Chlordane72-s.a 4,4.-ODD (p,p')72.s+e 4,41DD€ (p,C)50-2s-3 4,41DDT (p.p')60.57-r Deldrin9s9-98{ Endosutfan I33213€S Endosutfan ll103r-o7€ EndosltfEn sulfate72-2O-A Endrin7421-934 EnddnAklehyde76-t!l+ tleptachlor724a5 i et|oryC* or1024,57-3 Heptachlor Epoxid€8001.3+2 Toxaphooe5100.71.9 a-chlodane5566,3+7 g_Chlordane53494-70-5 Enckin Kebne
SurDg€te re\cowrtts;1 0386-8+2 4, 4-DBoctafr @rcWhenyt (Stesl-zaa Deca$lonbhhenyt (Sr)Polvchlo.inaied giohenvls bv SW846 8082Pfepared by method SW846 3545A1267+1t-2 PCB 101611tO+28-2 PCB 122111r41n6-5 PCB 123253{6$2ia PCB 124212622-29{ PCB '|248
1rae7{$r rcB 12541r0s€-02,5 rcB 126037U+23-5 PCB tZ62t1r0Gr1.1 PCg 1268
Sanrogale rEcovsnies:1 6&e+2 4,+DB4clduoroblphe, yt (5429s1 -2aa Ogcachlorobiphenyl ( St)
Semlvolrtile Orgrtrl€ ComFounds by CCMS
SWO46 0O8tA -Mat47 284?tr47 7031516 TGBRLBRLBRLBRLBRLsRtBRLBRLBRLBRLBRLBRLBRLBRLaRfBRLBRLBRLBRLBRLBRL
6968
BRLBRLBRLBRLBRLBRL247BRLBRL
1(E
SRLBRLBRLBRL
BRLBRLBRLBRL
lgl€ d.y 6.16pdkSdry 6.16
ldkgdry 6.16
UdkS dry 6.16pCAgdry 30.8
FYkgdry 6-16
ldxS dry 6,16
rgkqdry 6.rG
ldkS dry 6.rG
!S/hS dry 6.16
t'gkg dry 6.16
IS{€dry 6.16
uSASdry 6.16
Wkg dry 8.16pg1(Sdry 6.16
udks dry 6.16
rc/kS dry 6.16
!S/ko dry 3O.8pdkSdry 6.16
t Cdqd.y 6-16ydkS d.y 6.16
m_lf l%3G1ffi%
t'dkS dry 12.3
trgkg d.y 12.3
F3iks d.y 12.3
FSikg dry 12.3
Ug,l(gdry 12.3
udks dry '12.3
pdksdry 12.3
tgtS dry 12.3
FdrS dry r2.3
3G150 %30-150 %
trdks dfy {40
tldl,Sdty 44
|lSn(g dry 440
udksdry 44O
lSftsdry 44
rdks dry 140
lJg,kS dry 44o
|rglkg dry 440
SWSrlt' 6082 2GMar-07 28-tvlar-07 7031515 SM
Semivolatile Oroanic Compounds bv SWB46 B27OCPrepared by meulod SW8,l6 35508tl:t32-9 Ac€naphthene20e9e€ Acenaphthyl€n€62.533 Aniline12G12-7 Anthraceno1912-2+9 Alrazine10$333 Arob€nzene/Diphenytdi6zine92€7{ B€nzidlne56-5t3 Benzo (a) anthaac€n€
SW848E27OC 2&Mer-07 28-lr{-07 70O15145
5
5
5
5
M.B
Thls laborabrf EFoa Is nol valid xtithoa an aalhodzpd sigfiztarc o^ thz c.re.r pa$.
. ReporEble Det€ctioo Limir BRL = Below Reporting Limir Page 20 of 165
Page 217
SampLe IdentiftcationM6F-19 2'-4'sA59641-04
Client Proiect #l 0 l - 88
MatrixSoil
Rcceivedz1-Mar-Ol
CoLlection Date/Timc2l-Mar-07 00:00
CAS No. Analfte(s) Fl"C Unit$ *RDL D aiorl Method Ref, Prcpated Analyzed Btkh A','allst
Semivolrtitr Org|nic Compoonds by GCMS
Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 3550850-32-8 Benzo (a) pyrene205-!Xr-2 Benzo(b)fluoranthene191.24.2 Benzo lg.h,i) pet\y'ene207{8-9 Benzo (k) ffuoEnbene65410 Benzoic acidr0G51€ Benzytatcohol111 91r Bis(2-ctrtoroethoryFnethane111.4aa Bis(2-chtoroethyt)ether39638-32-9 Bis(2-aiitoroisopropyt)ether117€1,7 Bis(2-ehythexr)phthatate101,55'3 +Bromophenyl phenyl ether8568-7 Butytbenzylphthalate86-744 Ca|tazote5S50-7 +Chlorc-3-methylphenol106-474 4_Chloroaniline91-54-7 2-Chtorcnaphthalene9557-8 2_Chlorophenol700s-723 +Chlorcph€nyl phenytether218{1-S Chrysene53-70-3 Oibenzo (a,h) anthrac€ne132-q-9 Oibeflzofuran95-5G1 1,2-Dict{orobenzene541-7+1 1,3-Dichlofobenzene106116-7 1,4-Dichlorobenzene91,94.1 3,3',-Dichtofobenzidine12F8r2 2,4-Diihtoropt|FJnal3466-2 Oi€thylphthatate131-11-3 Oime$ylphhatatel0t67s 2,4-Dim€th),tpfienolu.712 Oi-n.butytphthatetes3+52-1 4,6-Dinitro.2.methyiphenol51-28-s 2,4-Dinitrophenol12r-1+2 2,4-Dinitrotoluene60e2G2 2,G-Dinitrotoluene117-84{ Oi.n-octyl phbalate2OH4{ FluofanhsneW-7+7 Fluorene11&74{ Hexachlorobenzene87{8-3 Hexachlo,robutadienen474 Hexachloroclclopentadi€n€67-f2-1 Tlexachloroethane19+3e-s Indeno (1,2,3{d) pyrcne90-12{ l-Methylnaphthalene76-59-r lsophorone91'576 z-l,letflylnaphthalene954+7 2-Methylph€nol10€-3s-4, 3,+Methylphenol1U6-44-591-20-3 Naphthalene&7+4 2-Nitroenitine99-0+2 $Nitroanitine
BRLBRLBRL
BRLBRLBRLBRLBRL8RL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRL
BRLBRL
BRLBRL
SRL
ldr€ dry 44o
lgftSdry 440
!g/kg dry 44O
Fg/r€dry 440pg/rqdry 44o
lrg/kg dry 440
wkg dry 44o
tg/kg dry 44o
Itgksdry 440pS/kS dry 440pdkg dry 44O
uvkg dry 440
u$rcdry 440
IdkS dry 44OpdkS dry 44OpSrkS dry 44OpdkS dry U0pdkS dry 440
lrSftS dry 440
ldkg dry 44O
lSftS dry 44O
ldkS dry 44O
US/kS dry 44OpS/kS dry 44O
ldkS dry 44OpdxSdry 44Dpdks dry 44Opdks dry 44O
ldkg dry 44O
lrglg dry 440
liS/kS dry 44O
PdkS d.y 440pg'lqdry 44opgkg dry 440pSlkS dry 44O
US/lqdry 440
Fdl(g dry 44O
uSftSdry 44o
udkg dry 44opgkg dry 440
ls/rs dry 440
!g/kg dry 440
tgtkg dry U0pdkS dry U0
udkg dry UOpg/kg dry 440
lSI(g dry 44O
pSIedry 44OpSftgdry 44O
lSftSdry 44o
sw846 8270C5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
This ldoruot! rcpor'a it ,tot wIA v hotlt dn auhotlz.d signoturc on ahe cover Nge.* ReFortable D€t€ction Limit BRL = B€low ReDortins Limit Page 2l ot 155
Page 218
Sample ldentificationM8F-19 2'-4'sA5964l-04
Client Proi€ct #301-EE
MatrixSoil
Coll€ctiop Date/Time2l-Mar-0? 00:00
Received22-MaFO1
C"4S No. A^dlyta(s) RcsaA Fl"S Ur,i6 *RDL lNuio Mdhod Retr PtzpaAd A,rilr"asd B4tch Anafust
S€mivolat e Orgroic Compoutrdr by GCMS
Semivolatile Oroanic Compounds bv SW846 8270C
Prepa.ed by method SW846 35508
10+01{ 4-Nltro6njtine98413 Nitrot enzene88-7t5 2-Nitaoph€nol10GO2.7 +Nitrophonol62.719 il-Mtrosodimethytamine621€4,7 N.Nitrosodj-n+ropylarnin€€6-30$ N-Nibo6odiphenylanxneE7{&5 Pentachlomphenol85-01-8 Phenanthr€n€10&95.2 Pftenol129{OO Pyrene11046-1 pyridine
12GE2r 1,2,4-Trichlo,ro,benzeness€5-4 2,4,tTridltofophenol8{r-06.2 2,4,FTrichlorophenol
Sufioga/E rccovedes:32140.8 2-Fhntuhiphonyl
fiz-r2-4 2-Ffuorophqol
4165404 Nitrcbenzene4s
116r.62-2 Phenol4s
1718s1-o Teehenyl4l4
118-79-6 2,4,&Ttibtoflldlphenol
Totel Metsb try f,PA 6000/7000 Serte$ Me{hod!
7439-97-6 Meroury 0.195
Tol M€trb by f,PA 20O Seri6 M€lbods
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLERLBRLBRLBRLBRL
u60715 1
lSit€ dry 1760
llg/rS dry 440
USn(g dry {40pdkS dry 1760pdkS dry 44o
UdLSdry 44Opdkg dry 44u
lSrtS dry {40pSftgdry 44O
ld*gdry .l{O
udl€ dry 44o
ldkg dry {40
rdksdry 440pSftS dry 44O
lgfkB dry 140
36130%1+110%3L1n%15-110%&130%1U110%
rngr'kg d.y 0.0342
nE4(g dry r.08
mgr'kg dry 1.62
rng/kg dry 0.540
mckodq 0.270
rngftg dry 0.5,10
mCl€ dry 0-810
mg{kgdry 1.62
t{/A
mgn 0.02tX)
mgn 0-0150
mg/l 0.0150
"En O-0O25
ftEn o.o15o
mgn 0.(Xx)40
o'dl 0.0i50
mSI 0.0150
%
55
5
55
55
5
55
SW8,l6 8270C 26-Mar{7 28+!,lar{7 7031514 M.B
7,r4G?2-4 Silvsr
744G3$2 ABenic
7440-3+3 Barium
7440-4+9 Cadmium
714G47-3 Chromium
743992-1 Lead
n824$2 Selenium
SPLP Metrk hy EPA 13 12 & 600M000 Sedes Mctftods
SPLP ExtEctbn
7410-22., glvel
74,{L3&2 Arsenic
74ilo-3+3 Banium
7440.419 Cadmium
7440-17-3 Chromium
7439€73 Mercury
?43942-1 Lead
aa8a4+2 Selenium
Ceneral Cbembtry Prr|meterl
SW8.l{l7471A 2&Mar-O7 2&lvtar-07 7mt495 YP
EPA?OO.7 2A nat47 2g]'L,,ar47 7031494 RM
'l SW84{i 1312 26+.iar-07 26-lelar-07 7031560 BD
1 SW84€ 1312/6010A 2&uar-O7 28.lvrat47 7m1651 Hg
1 "
1 '
'I SW846 131224704 ' 28-t\-l5r{7 7m1652 YP
1 SWA4€ 131zli0l0B ' 2A-Mat47 700165l HB
I '
8RL
5.68
12.7
0-735
56.9
r24BRL
Compl€bd
BRL
8RL
0.0300
ARL
BRL
BRL
0.0167
BRL
SM2540G Mod. 21+'Iid47 2 .d,at47 7031470 OP% Solit s
Page 22 of 165
Ihit lzbordoq rqon is noa rditt t&hotd at aQdrhrizcl sigdattr. o8 ,ha @ear pge.
+ R€ponable Detectiod Limit BRL = Below R€portin8 Limit
Page 219
Samptc IdentificationM8F-20 2'-4'sA5964I-05
Client Proiect #301 -88
MahixSoil
Received22-Mar-07
Collection Date/Time2l-Mar47 00:00
CAS No. Analrte(s) RestA F/"s Unirs *RDL Dilation Method Retr Prcpeat Aaalrzed Barch AMUstVolatil€ Orgrnic Compounds
VOC ExtractionVolatile O.qanic Com!ounds
lgkg dry 7.o
!g/kS dry 139pg/kg dry 7.0pdlg dry 7-0
ttqtKgdry 7_0
Ug/kg dry 7 O
Ug/kg dry 7 O
UdkS dry 7.OpS/kS dry 13 I
lig/kg dry 69 5
ldkg dry 7.opg/kg dry 7-0pg/kg dry 7.0
!g/kg dry 34 8pg/kq dry 7.O
lrdkS dry 1 O
ldkS dry 13.9pdkg dry 7.opS4<S dry 13.9
UdkS dry 7.OpgkS dry 7.Opg/kg dry 13.9
!S/kS dry 7.0
!g/kg dry 7 O
!g/kg dry 7.O
Udks dry 7.opSlkgdry 7.O
Ug/kS dry 7-0
!S/l(gdry 13.9
ldkg dry 7-0pg/kg dry 7 O
t g/kg dry 7.0pS/kg dry 7.O
fdkS dry 7.O
ldkS dry 7.opS/kS dry 7.O
tgkSdry 7.0yCkS dry 7.O
udkS dry 7.0
udkg dry 7.0pgkg dry 7.Opgks dry 7.O
ugks dry 69.5pdkS dry 7.O
lgkS dry 7.o
!g/kS dry 7.O
!g/kS dry 69.5
!g/kS dry 6S-5
fg/kS dry 7-O
Field extracted VOC 26-MaFO7 26-Mat-O7 7031584 BD
Prepared by method SW846 5035A Soit (tow t6vst)
76-141 1,'1,2-Trichlorotrifluorcethane(FreoERL
6764-1 Acetone BRL107r3-l Acrldonltrile BRL714t2 Benzene BRL103€6-1 Bromobenzene BRL71-91-5 Bfomochlorornethene BRL7r2r1 Bromodichloromethane BRL71252 Bromoform BRL7,143-9 Bromomelhane BRL78-93 3 2-Butanone (MEK) BRL104-51{ n_Butylbenzene BRL135,98r s€c_Butytb€nzene gRL
98{+.6 tert_Butytbenzene BRL75 15 0 Carbon disujfide BRL56-21s Cafuon tefachloride BRL10&90.7 Chlorob€nzene BRL7fiG3 Chloro€thane BRL67{G3 Chlomtorm BRL1447-3 Chloromethane BRL95 !r+8 2-Chlorotoluene BRL10,643-4 4_Chtorotoluene BRL96-12-8 1.2_Dibronro-3_cfiloropropafle BRL12448-1 Dibrcmo€hloromehane BRL106-e3-4 1,2_Dibronbethane(EDB) BRL74-9s 3 Dibromomethane BRL9s-5Gl 1,2-Oichlorobenzene 8RL5r1-r3-1 l,1DtrhlorobetEene BRL106-46-7 i,4-Dichlo|ob€nzene BRL75-71-8 Dachlorodifluoromethane (Freonl2)BRL7s-34-3 l,l-Dichloroelhane BRL107{G2 .1,2-Dichloloethane BRL7$35-4 '1,1-Dichloroethene BRLr 56-59 2 cis- 1,2-Oichtoroethen€ BRL15c60,5 t ans-l,2.Dicl,tlotoeth€ne BRL76{7 5 l,2-Dichloropropan€ BRL1.2'2&9 l,3-Dichloroprop€n€ BRL59420 7 2,2-Dichloropropan6 BRL563-fr95 l,1-Dichloroprop€ne ARL10061{1-5cis-1,3-Dichloropopene BRL10061{2{tran9.l,}Dichloropropene BRL10041-4 Ethylbenzene BRL8768-3 Hexachlorobutadaene BRLse1,78{ 2_Hexanone (MBK) 8RL98€2-8 tsopropytbenzene BRL99€76 4-tsopropyltoluene BRL1614.{14-1 Methy{ten+utytether BRL108-10-1 4-Mehy-2-pentanone(M|BK) 8RL7fi*2 Methylenechloride91-2G3 Naphthelene
BRLBRL
1
1
1
1
1
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1
1
1
1
1
1'|
l
1
1
I
I
1
1
1
1
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1
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1
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RLJsw 846 82608
Thb laborulory repod h rrot valid nithou an auahodaed signalure on the coter page.
* Reportrble Detection Lihit BRL = Below Reponing Limir Page 2l of 165
Page 220
Sample IdentificationM8F-20 2'-4'sA5%41-05
Clienr Projeci #301-88
MatrirSoil
Rec€ived22-Mafi7
Collection Datey'Time2l-Mar-0? 0O:00
CASN?. A Jlc(s) Rerak Fl"s 'RDL Dilulion Me.hod REI PnpaEd Anzlfen Bofth AMIyst
Volatil€ Orgrnic Compouodg
Volatile Oroanic CornooundsPrepared by melhod SW846 5S35A Soil (lor{ level}
10!65.1 rFPropylbenz€n€ BRL10G42,5 Strene BRL63lrm{ 1,1 ,1,2 -Tetrachloro€thane BRL79.3+5 1,1,2,2-Tehachloroehane BRL127.184 Tet€chlorootlrcne BRL10&88.3 Toluene BRL87'614 1,2,:FTrichlorobenzene BRLt20{2-1 1.2,4-Tricilorcbenzen€ BRL71-5'5-6 1,1,1-Trichloroethan€ BRL79-oG5 1,1,2-Trichloroethane BRL79-ll1i Trictlloroethene BRL75€9.4 TrichlorDfluorornethans (Freon I 1) BRL
SW €46 8260S 27-Mar{7 27{ar-07 7031658 RLJ
+CT ETPH 27-NIaFOT 8)v',ar47 7G1500 DS
96-1&,1 l,z,3-Trichloropmpan€9s,63'6 1,2,,t-limethylbenzene'ro8{7{ l,3,tTdmethy{benzene75{r-4 Mnylchlo*l€1330-2G7 m,p-Xyl€n€95-475 o.Xylene10999-9 Tebahwaofuran@-2s7 Ethylether99a-05€ Tert-anryl methyl ether637.923 Eu1yl ted-butyi edlerro+mi Dijsopropyleth€r
Te.i€uhanol / butyl alcohol12'91-l l,4oioxane
Sunogate r€cowrias:45o{04 tl-Elrornofiuorobenzene
m37-26-5 Toluene4S1 7 0eO7 4 1,2 -Dichloroethane44
l86a' -7 Abrcnof,uorcmethale
Extr.atrlrL PetrcI€um llydro...bors
Extractabl€ Total P€lioleum Hvdroca6onsPrepared by me$od SW846 355088006-61.9 Gosoline68a7e30-? Fu€loil tt268a7e313 Fuel Oil tr4e6553{0-4 FuelOjt#6M0980m00 Motor OilJ00t0oco0 Aviation Fuel
Unidendf€dOther Oil
BRLBRLBRLBRLBRLBRL8Rl-BRI-BRLBRLBRLBRLBRL
83
a399
BRLBRL
BRL8RLBRLBRL136Calculat€d Es
Fgl(g dry
Ug/kS dry
rc/kS drypg/kS dry
t rytS dry
lSlko dry
Fgkg drypgrg dry
lgkg drt
ldkg dry
ldlqS dry
tgkg dry
ldko dry
t siks dry
trgikS drypdrg drypgl(g dry
us,rs dryudks dryUS/kS drypS/t(g drypgil€ drypg/tg drypS/kg d.y
Fdl(g d.y
7.07.0
7.07.07.07-07.07.07_07.O7.07.0
7-0f.n7.O7.O13.97.0
69.57.07.O7.07_0
t39
70-130 %
70-130 %
7L1fl %
n-1m %
ftE/kg dry
ngikg dry
firg,kE drynE/kg drymgr'kg drymg/kS dryngLfl(g dry
mSftS dry
m9/k9 dryrndkS d.y
26.026.0
26.028.026.026.O28.O28.026.0m.0
ToblPettoleuml-lydrocarbons 136
C$C36 Aliphalic Hydrccatbons 136
Srrzogal,t /€covsnlrs.'$8e3+2 t-Chro.ooa{adec€.r€ 97
S€mivolrtile Org'nic Cornpoln& by cC
Oroanochlorine Peslicires SW846 8081APreparcd by method SW846 3!15A
:09{G2 Al&in BRL
40-110 %
t'EkS dry SW846 8081A z&ldarry 2Stvlsr{)7 7031516 TG
Ilrac laboralory .eport is tufl eaIA w hotd et ltthorizEtt siglotuE on ahe coeer pogc.
+ Re?odrble Detection Limit BRL = Belou Reportitrg Limit Page 24 of 165
Page 221
Sample IdentificationMEF-20 2'-4'sA5964l-05
Cliedt Pmiecr #301_88
MatrixSoil
Received22-M^.-07
Collection Date/Tim€2l-Mar-07 @:00
CAS No. Analftc(s) FIag "RDL Dilution L[e.hod Rel. Prepsred Analyed Batch Anotrst
Semivohtile Orgrnic Compoun& by cC
Oroanochlorine Pesticides SW846 8081APrepared by method SW846 3S45A
319-84{ a-BHC319-a5t b-BHC319-86-8 d_BHC
s84$s g-BHC (Lindane)
51-f4-9 ChlordaneT2-54-B 4,4.-DDD(p,p ' )
72-55'9 4,4.-DDE(p,p')
50-2e,3 4.4.-DOT(p,p')
60,57-1 Dietdrin
959-98S Endosulfan I33213-65-9 Endosutfan ll1031i7,8 Endosulfan sulfate72-20 a Endrin7a21'99 EndrinAtdehyde7644-8 Hieptachtor7243-5 Methoxychbr1024-s7'3 HepiachlorEpoxide8001-312 Toxaphen€s103 71-9 a-Chbrdane556c34-7 g_Chlordane
53494-70-5 Endrin Ketone
Swrcgale Ecoveries:1 038c84-2 1, 4-DB-Octafl uorobiphen yl (S t)2051-24-i Decachlorobiphenyt (Sr)
Polvchlorinated Biohenvls bv SW846 8082
Preparcd by method SW846 35454
12674112 PCB 101611104-24-2 PCB 122111141-16-5 rcB t232s3469-21 I PCB | 24212612 a4 PCB 1248110e7{s-1 rcB 1254110ee8?-s PcB i26037324.23.5 PCB 1262r110G144 PCB 1268
Ssnogaf€ recov€rbsi1 0386-84-2 4,4-DB-Octafluotobiphenyt (Sr)
ms1'2a.3 Decachtorobiphenyl (Sr)
SemivolNtile Orgrnic Compounds by GCMS
Somlvolatile Oroanic ComooLrnds bv SW846 8270CPrepared by method SW846 35508
83€2-9 Acenaphth€ne208-968 Acenaphthylene62{}3 Aniline
120-12-7 Anthracene1912-24-9 Atazine
103-33-3 AzobenzenerrDiphenyldiazine
92-€7-5 Benzidine
56-55-3 Benzo (a) anthracene
SW846 8081A 26-Mar-07 28-Mar-07 7031516 TG
SW846 8082 26-Ma.-O7 28-Mat47 7031515 SM
BRLBRLBRLBRLBRL
8RLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
67105
BRLBRLBRLBRLBRLBRL28.6BRLBRL
12595
BRLBRLBRL475BRLBRL
8RL652
pg/kg dry 6 66
!Sl(S dry 6 66
ldks dry 6 66pdl€ dry 6 66
ldkS dry 33.3
riS/l(gdry 6.66
t/dlq dry 6.66
t'sftS dry 6 66
ldkS dry 6.66
USftS dry 6.66
l.'dks dry 6.66
Ug/kg dry 6.66
t4/kg dry 6.66
!S/kS dry 6.66pSlkS dry 6.66
PSlks dry 6.66
1.|g/k0 dry 6.66
t Sikg dry 33.3
!S/kg dry 6.66pdkS dry 6.66
trdkg dry 6.66
30-150 %30-1s0 %
lrSikg dry 13.3
l.rg/kg dry 13.3
Ug/kg dry 13.3
us/kg dry 13.3
U9/k9 dry 13.3
ugkg dry 13.3pdkS dry 13.3
lsftg dry t3 3
sdks dry 13.3
30-150 %3t\150 %
1
1
1
1
1
1
1
1
1
1
1
I
I
1
1
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1
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!s/ks dry 322FS./kS dry 322
!S4(S dry 322
!S/kS dry 322pgl(g d'y 322
UdkS dry 322
USftS dry 322
US&S dry 322
SW846 8270C 28-Mat47 28-MaFO7 7031514 M.B
This laboralory pporl Lt aol valU witttoa! od au[odzel ignat!rc oa the cover page-
' Reportable Detecrion Limit BRL = Below Reporting Lirnir Page 25 of 165
Page 222
Sample ldetrtincationM8F-20 2,-4'sAs964l-05
Cliept Project #30 r -88
MafixSoil
Collection Date/Time2l-Mar{7 00r00
Received22-M8J-07
CAS No- A.talrk(s) FlIe *RDL Dilution Mc.hod Retr. Prepand Anolyzd Babh Ansbtl
SeDivoletll€ Org.nlc Comporr& by GCMS
Semivolatile Orqanic Comoounds bv SW846 827(rc
Prepared by mehod SW846 355085&32{ BerEo (a) pyrenea)$S.z genzo (b) duorentrene191-21.2 Benzo (g,h,i) p€rytene207.{rE-9 Benzo (k) fuoranthene6s.a+0 Benzoic aodl0G5i€ B€nzyl alcohol11r-9i-1 Bis(2-chloroe$oxy)nEthane111-44-4 Bis(2-chloroouryl)€tler3863&32'9 Bis(2-chtoroisopropytFttEr117-8r.7 Bis(2-€hylheryl)phtlatate10r-55n +&.omophenyl Fhenyl ether85{8-7 Bu!/ benzyl phthalate8G74-€ Carbazole59{}7 +Chloro-3-.nethylphenol106-47{ +Chlorosniline91-5&7 2.Chloron€phthalene95574 24hlofophenol7005-7?.3 rlchloaophenyt phenyl eth€l218.01-9 Chrysene53.703 Dibenzo (a,h) anthracene132-64-9 Dibenzofuian9+50"1 1,2-OiclJorobenzene541-73-1 'l,3-Dichtorobenzene
106-4&7 l,+Dichtorcbenzene91-9+1 3,3'-Dichtorobenzidin€120-83-2 2,4-DichlorcphenolE4-86-2 Diehyl phhalate131-1r'3 Dimehylph(ralate105{74 2,+Dimethylphenolu-7+2 Di-nSutylphthalate$4.52-1 4,GDinitro-2{ethylphenol5!-2&5 2,4oinltrophenoll?l'i4-2 z,4-Dinitotoluenesls2$2 2,6-Dinitroto'lu6ne117{4{ Di-fi-oct},tphhalat€2&4{ FluolEn[lenelF7$7 Fluor€ne11&a-1 Hetachlo.obenzeile87{&3 Hexac}orobutradi€nen474 Hexachtorocyclopentadiefle6r-72.1 tlexachloroethanete+3s-5 Indeno ('1,2,3.cd) pyrenesG12{1-t/ iethylnapht' lalene78-5!Ir lsophoronee1-57.6 2-Mothy{naphthalenoS-{&7 2-M€6ylpienol108-39-4, 3.4-ft sthylph€nol10Frt4.591-2U3 Naphthalene&7+1 2.Nifroenjliness{$z }NiUoonilins
774778353474ARLARLBRLBRLBRLBRLSRL8RL8RLBRLBRLBRLBRLBRL412BRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1,680
BRLBRLARL8RLBRLBRL
BRLBRLBRLBRLBRL
BRLBRLBRL
!S/kS dry 322
lgr'kg dry 322pgi(g d.y 322
ISAS dry U2pgts dry 322
ldkg dry 322ydl€ dry 322pdko dry 322
t gikg dry 322
Udrg dry 322pgkg dry 322
trgtsdry 322pgks dry 322pdkg dry 322
Fgtgd.y 322pgkgdry 322pdks dr, 322
f.'dkS dry 322
lS/kSdry 322pdksdry 322
FC/kS dry 322pdkSdry 322
ldxgdry 322
udkgdry 322
ldkS dry 322pg^Sdry 322
USftSdry 322pgrsdry 322
ldkSdry 322
fjg/ks dry 322
!g/kS dry 322psikgdry 322
rcAS dry 322pdksdry 322
ldkSdry 322
!9/k9 dry X22pdkg dry 322
lrgkg dry 322pCftSdry 322
HglS dry n2
lidlsdry 322
rcfl(S dry 322pdks dry 322
lSikg dry 322
UC/tSdry 322
tidks dry 322
lgkgdry 322
!S/kS d.y 322pS/kg dry 322
US/IS dry 322
SWe46 6270C 26-lrar-t 7 28-{,t€r-07 7031514 tl.B
Thb ltbonlotf Eporl is Eot valld ellhoQ aE outtotlzed slgdsqre or the cover pqe.
' Reportabl€ Detection Unit BRL = Below Repofting Limit Pagc 26 of 165
Page 223
Sample IdentificationM8F-20 2'-4'sA5964t,05
Client Proiect #301_88
MatrixSoil
Received22-Mar-0'7
Collection Date/Time2l-Mar-0? 00:00
CAS No. Analrta(s) Resuh FI"g Unia *RDL tuIetho.l Retr. Pftpued AnotrzPd Bakh Atu'lrst
Semivohlile Organic Compoonds W GCMS
Semivolatile Oroanic Comoounds bv SW846 8270CPfep€red by method SW846 35508
100{1$ 4-N,toaniline98-95 3 Nitrobenzene88-715 2,Nihophenol100{2,7 4-Nitrophenol62-75-9 N-Nitrosodimethylamine
62lg'7 N-Nikosodi,n,prOpytamine8G3D-6 N-Nitrosodiphenylamine€7-€F5 pentachlorophenol
€541{ Phenanthrene
10&93-2 Ph€nol12S404 Pyrene1104€r Pyridine12G82-1 1,2!4-Trichtorobenzene95-95-4 2,4,tTrichtorophenot88{d2 2,4,G1nchbrophenol
Sunogate rccovedes:321-60-0 2-Fluorobiphdnylj6/ 12 4 2-Fluorophenol
416t6o-o Nitrobenzene4s
4165-62 2 Phenol4s
1718-514 Tetphenyf4l4
118-/9-6 2,4,6Tibromophenot
SW846 8270C 26-Mar{7 28-[,1aF07 7031514 M.A
7439-S2-1 Lead
778239-2 Sgtenium
Getrerrl Chemistry PNrrmeters
% Solids
pSi$ dry 12e0pdlg dry 322pdls dry 322
!S4(S dry 1290ps(gdry 322
!g/kg dry 322
!q/kg dry 322
!S/kS dry 322
!g/kg dry 322
ldksdry 322
ldks dry 322pdksdry 322pg/kg dry 322pg/kg dry 322pg/kg dry 322
30-130 %15-110%30-130 %15-110 %3G130 %15-110 %
mg/kg dry 0.0360
mg/kg dry 1.20
mg/kg dry 1.80
mg/kg dry 0.598
mgL/kg dry 0.299
mg/kg dry 0.598
mg'rkg dry 0.898
mg/kg dry 1.80
mg/l 0.0200
mg/l 0.0150
mg/l 0.0150
mg/l 0.0025
mg/l 0.0150
mg/l 0.00040
mg/l 0.0150
mg/l 0.0150
%
BRLBRLBRLBRLBRL
BRL8RLBRL848BRL1,700BRLBRLBRLBRL
624959497562
1
1
1
1
1
1
1
1
1
1
1
1
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'Io{rl Mctals by EPA 6000t000 S€ris Merhods
7439-97€ Mer@ry
Tolrl Melrlr b) EPA 200 Ser;cs Methodr
7440'22r SiMer
744G38 2 AaSeniC
7440-39-3 Barium
7440-43I Cadmium
7440.47,3 Chromaum
7439-92-1 L€ad
7782-49,2 S€t€nium
SPLP M€trls by EPA 13l2 & 6tn0r000 Sedes Merhods
SPLP Extraclion Cotnpleted
7440-!2-4 Silver BRL
7440-38,2 AGenic BRL
74zro-39 3 Barium O.O277
7440-43-S Cadmium BRL
744037-3 Chrcmium BRL
7439-97-6 Mercury BRL
0.641
BRL
10.3
101
1.90
12.3
283
BRL
sw846 74714 28,Mar{7 26-Mar-07 7031495 YP
1 EPA2oo.7 2A-Mat47 2A-MarO7 7O3149d
1 '
1 '
1 '
1 '
1 '
1 '
1 SW8461312 26,Mar{7 2&Ma.-07 7031560 BD
1 SW8461312/60108 28-Mar07 28-t',lar{7 7031651 HB
1 '
1 ' ,
1 "
1 "
1 SW84613'127470A ' 28-lviaF07 7031652 YP
1 SW6461312r'60108 ' 28 tarol 7031651 HB
t '
1 SM2:140 G Mod. 24-MaFO7 24-MaiO7 7031470 0P
RM
0.0182
83.0
Thit lahorulory rcpotl b ,tol ealu nithoul oa suthofuel rigaoturc on the cove. page-
* Reporrable Detection Limit BRL = Below Reporting Limit PaAe 27 of 165
Page 224
Samole ldentificationMEF-2r ?'-4'sA59803-06
CtieotProiect #301-88
MatrixSoil
Cotlection DatelTime26-Mar-07 00l00
Re.€ived21-MaF07
CAS No. Aadlr6(s) RestU nag UnAs *RDL Dila,ba Method Retr. Prcpare.d Aadyzed Bzlch Anelfst
Volstil€ Org.dic Compornds
\€C Exlradion Fdd dlraded
Vdalilg oruanic Comoounds
Propa.ed by mehod SW846 5030 Soit (high tevel)
ttl$1 l,l2.Ttichbrotnfluoroehane(Fnon 8AL67 6+1 AEdOoe BFL101-13,1 Acryldurile BRL71-,13-2 €€rlzeie SRLlC&€&1 &qnob€ozene BRt7147.5 Brcmochbonethane g8L
75.tu Stdmdctftmriehal€ 8fu1VE2 Brunolorm ERL7+&9 g|Dfl|ornedlane gRL
7&e3.3 2.8uhno0e{MEK) 8RL10+513 n.Biytffzene 8nL13+94-8 sec€utyh€nzeE 8ALsnffi bn€{vbenzer€ BFL7t1fi cadon disulfide BRL&ai CattooLfacfibnG 8RLrdl-gG7 O&Obglre{ie 8FL75.0G3 Chtoruehane BnL
2&MarO7 2gMarOT ftts1767 8D
3Hiftr{7 30-frar.07 7(191675 ftr
BFL
BRL
8RL
8tu8RlBFLSRLBFL8RLBRLgnL
8ff1BNL8Rt-BRI,BAIgRL
8fi1BRL8RL8RLBRLB8L8FLBRLBRTBBLBHLB8L8RLBRL8R-
50505050505t)505050505l)505i)505050505)50505050505050505050505050505050505050
505050505050
50505t)505050
tdlq dry S.5
p9rqdty 1670
!S40 dy 83.5
!S/XS dy 85
|lglxS dy 83J
ldb dlv &15
ldXSdry 8i].5
$glgdy 835
ldkS fry 167
ldl€ dfy E35
|.gr€ fry 835
ugrs dy Ei'.5
UgrS dy 8i1.5
!9lS try 117
lgts &y €3-5
|4/rO dy 835
yClS dry t67
|lg/l(! dv {t3.5
!9lg dy 167
|dkg dtv &3.s
Wlr4dfv 83J
|.€/l€ dy 167
wk'ey $5
Wr,S d] 83.5
ljgfto dl a3.5
tgu,gfrt 83-5
pgrq dy 835
pdlq dy 83.5
lgrgdy 167
tiC4q dry E3.s
WkS d)' El.5
lgkS dry 831
Kl4q dry 83.5
uglq dry 83.5
rytS dV 83.5
|JgkS $' 83.5
t4lq dry 83.5
lSlq try SilJ
l4ilq dy 83.5
$kgd] (15
|lg/](g dr m.s
lgrh fy E3.5
tafrS dry 835
|{/rq dy &35
|lglqdy 83.5
|jgD.S dV 83.5
!g4q dy E35
!s/rs diy E€5
t41{tt E35
voc
srr{ 8{6 826{8
67{d3 Chlodofin7{-073 gtbfdnelhane
$.{+8 2ahtorcloluenel6-4iH 4-Crjorotoluenerr'r2.0 lloihomcs+lloropropans12{-r+l D.honochlommefiane10Os-4 1,zobmmo€tlan€(EDB)74-9t3 oibonomehane9650r t2od{orob€nEne5.r-7+1 1,3{tidlor'obenzen6r06-4G7 1,4-{Idoroben2enettTl € DidiorEdfluoromeuBno (Fleon t2)t5-1,1.3 1, t -otddor€thane
1ns.2 t ,2-olailom€ftlane635.1 t,l-[)iahlorodh€ne1se59.2 ciet,zok lom€thenels6-605 tsa$.l2,fidooeth€nei8{?-5 1l-DiddoproFens1e.4.9 1,$0iahloropttsn65&1207 2l.Didrtompropane50!-50-6 t,l{)idiofopropene1006r{1.5 ds.l,}Di* ompfopeft10061-02.6 tar6,lS.oidtolopop€nelqHr-1 Ehylbenzenear{&3 lloEdltorobuladen€s9r-78+ 2+terdo|r€(I,l8K)!B€-8 l!opl!p!|be en€99{7-6 4-lsogopyltoNlg1elE {4,{ ti.l6hy brt+dy{ atjerl0&l0r {-l{odryl.2{€nErcneU|BK)?@2 MehyLrF djodde01.r!.3 NaFhMene
Thb kloraraveport tE nat tal l drhonr o4 autho?izgd signzturu oi ahe aover prge.
. Reportable Detecrion Limit BRI_ = Below Reportiog Limit Fage 2E of | 54
Page 225
Samole ldentificatiooI[8F-212'-4'
sA59803-06
Client Proiect #301 -88
Collection Drte/Time26-Mar-07 00:00
Received
2'7 -Mar-07Makix
Soil
CAs No. Aasble(s) Fl"e Unils 'RDL Dilurion Method ReJ Prcpa.ed Anallzed Bttch Ana|\l
Volatile Organic Compourdi
Volatile Orcanic Comoound$
Prepared by melhod SW846 5030 Soit(high tevet)
103{51 n,Prcpylbenzene 8RL1@ '12.5 StF€fls 8RL630 20 6 1,1,1,2-Tetrachloroethane BRL793,4 5 1,j,22-Tetrdchooethane gRL
121.18.{ TelrachloR|edlene 8RL1m ss.3 Totuene BRLt7t16 1,2p-f idbtdenzene Bft12G82'l 1,2,4-Tdchloroben2el|e BRL7!.55.6 l,1.1-Tichtoroe(hane BFL79{0-s 1,1,2-Trichloroethane BFL7s1r1s Tridtoroelhene sFL?5{e-t Tridllorcftroromehane (Freon i 1) BRL
BNL
OHL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
8Rl
8RL
BRL
99
102
90
94
50
50
50
5{)
50
50
50
50
50
50
50
50
50
50
50
5t)
50
50
50
50
50
50
udkSdry 83.s
!S,?,S dry &3.5
tS,lS dy &3.5
lglq dy 835
!9rS dry 83.5
uS.ftS dry 835
pgths tt 8.15
!94q dry 83.5
pdrs dry 83.5
pdkS dry 83-s
|Jg/kS dry 83.s
US4q dry 83.5
rc,kS dry 8:].5
tdkg dry 83.5
rc/kS dy 83.5
ldkS dry E3.5
pg/kq dy 167
pdq dy 83.5
lgtS dy 835
lgiq f}' 83.5
lglq dy 43.5
!9lg dy &3.5
!g4q dy 83.5
lSlq dry 835
!g/kg dry 1670
7019)%
70130%
70t30%
7019%
mSftS drymg/rq ftymEkg drymqks drynMs drymSAS drymgks dryILkS drymg^q drymqt(S dry
40140%
lgftS dy 34.8
sw 846 82608
+CT ETPH
9G18.4 l,2,3,TrichtonploPane9t6a{ 1_2,4-Trimelhy'benzene
108-67-8 l,3,5,Trimelhlbenzene75-01 4 Vinl chloridel33O2G7 m,p-Xyleoe9547 6 cxylene109 s99 Tethhydroiuran
m-2s 7 Etryteflerlr94{5{ Ten€rrylmelhylelher637 e2-3 Elh/ leftuvt eher103 2G3 Di-isoFopyl elher75t5-0 Tert Bubnol/ bqt),I almhol123-91-1 1,4-oioxane
44|tat 4BvnonuotcheEene
nJ7-265 Toluene4S
n6o4/4 l,2-Dcllorcethane44
I86ts3-7 DbrofiollwtoflEthffie
Extrsctabl€ Petroleum Hydroc{rbons
E{aclable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
S0Oe5l.9 Gasolined4%.30? Fueto *268176.31-3 Fuei oitt46rs534c1 Fu€tOit#€ms000000 Moff oilJ001o0000 Aliation Fuel
Unidenlilieii
Ohsl Oil
Totat Pstrolsum ftdocarbons
C9-C36 Alipfla[c Hydro€dons
?A6332 lcnbdxladecane
Semivotslile Orgatric Compolnds by CC
Orcanod odne Peslicides SW846 8081A
Prepa.ed by melhod SW846 3545A
309-00 2 Atddn
291\,!ar{7 3&Maf 07 7031772735 1
73.5 1
73.5 1
73.5 1
73.5 1
73.5 1
73.5 1
73.5 1
73-5 r
73.5 1
BRL
BNL
BRL
8RL
BRL
BFL
BFL
BNL
BHL
BfrL
8RL stYE46 80EtA 28-f,iar.07 02-Apr{7 7031739 TG
Thk taboruhvepo.t is notwlU withod on ttho zed sig alue on ttu cover page-
* Reportable Detecrion Limit BRL = B€low RepodnC Limir Pa€e 29 of 154
Page 226
Sample IdentificationMAF-2r 2'4'SA59E03-0'5
Cli€ot Proiect #301-88
MatrixSoil
Collection Date/Time26-Ma.47 00:00
Received27-MaJ-07
CAS No. Aaalfk(s) ResaA F14s Uaia *R.DL Dilnioa ttethad Retr. hepared Atu4zed BQLh Anabsl
Semivo|rllk Orgrtric Compounds by cC
Ooanocft lodne Peslidtes SWE46 8081A
Prepared by method SW846 3545A
319.0,16 +BFIC
319'85-? b-BHC
319-€6.0 +EHC
5&8ei SSIE {[h&ne)5t-t1.9 Chtodanen510 4,4{)DD h,p')726$e a,A -DDE (p,p')
5G2e-3 44,-DI]T {p,p)st-1 Di€ldjin
95$S,3 Erdo6ulan I
30213{54 E ldoc|jlan ll1031117{ EndGullanSultale
n-zra Eidin7atg4 Erdrm l$*yde75-4+€ ttoptachtor
a4!5 Melhoxyd o.1utzAs/-X HepiachtorEponde
€0orn52 Tor4helD
[email protected] +Chhfdane556d!+7 g{HordEne
5349+7Ss Enddn Ketone
1M9aa 4UDeafr&tfi4tlcni@)
Mt24.3 Decdlddtplnnfl(Sr)
Polvd oniaabd Eliohswh bv SWg46 8082
Prepared by mehod SW846 3545A
126r!1r-2 PCB1016
11t01-&2 ?Ce,lnl
11111.re5 PC81E2
s34€9-2te frcB124212672?9-6 PCg 1248I'097-6+t PCB 12541 r0e602€ t c8 t2€0
3r!+45 tE8 t2621110G144 PCts 1268
103,6.t11 4,+Deo{'aflwt&phen l (g)
Ntz+3 D€.,dd0lobipltsttyl(3r)
Semlvolelile Orgmic Compo||ndi by GCMS
S.mivolatile 0ro6nic Cofiooun& bv SW846 8270C
Pr€pa.ed by method SW846 35508
8+@{, Aa6rEpfftsne2!8-46.0 A{enaphhyl€ne
6e-5+3 AnIrF
lbrzt Anhten€
192.24{ Atazjn€1@93-3 AzobenzendDipfienytd€zins
e{74 BenzilheE&s$,3 B€nzo (a) hnc€fie
8RL8RL8RLBRIBRLBFLBRLBRLER.BFLBHI.BRLBFLBFLBRLBRL8RL8RL36.339.0BFL
6491
BRLBRLBFLBRI.BRL8RL1048RLBRL
nN
BHLBRLBRLBRLBRLBRL8Ft-8Rt-
!g/f0 dy
Pg}s dv
m/lq dy
|db dv
l4lq drypsrq drypdks dy
!s4q dy
scl.{ dypgls dv
tdlq dry
!9'r€ ry
t8ao dry
|l9r! d)
|,04(g dy
rYls d)'
l4nq dry
FEtq av
l|dlq dv
lls,|q drypdlq dry
*19*1fl
pq4q dry
ugts dv
udrs dw
lgrs dv
!g/ks try
!4ts dy
t4t4 frl
|drs dlvpgre a
wtg%gl1fi%
sw846 mStA
sw846 €082
sw816 8270C
34.8
343
31.8
31.8
171
34J
34.E
34.8
343
31.8
34.8
31A
34J
34.8
34_8
34.8
34.8
3{t
34J
34.8
2g4qr47 m-Aprfl 7(x|1739 TG
?f-M?'47 30'Mar.07 70S173i SM6SG
MG
69.6
6qE
61.6
69.5
63.6
ldlq d.y
jignC dry
$/l0dy
rrgks dy|4lq dvldks rvudk dvdls rv
912
cl2
9l?
9r2
912
912
912
?9. 6r{t m-Aprc7 71101771 ttB
Thb hLorolo4 ,epo.l ls aor ratid xlithoqt ad ctrtonzed sigaalure oa the @wr pzge.
' Reportahle DetE{tion Limit BRL = BeloN Re['orring Limit Page 30 of | 54
Page 227
Sample IdentificatiofiMEF-21 2'-4'
sA59803-06
Client Proielt #301-88
MatrixSoil
Received27 -Ma(01
Collection Date/Time26-Mar-07 00;00
CAS No. Analykls) FIag *RDL Dilution Method Rel, Prcparcd Anruzed Batch Analysl
SrmirolNtile Orgrnic Compounds by cCMS
Ssmivolatile oloanic Compounds bv SWB46 8270C
Prepared by method SW846 35508
50-32 8 B€nzo {alpyrenem5.ee2 B€nzo {b) fluoanhene1912+2 B€nzo(g,h,i)p€rytene
al7]E{ Eenzo (k) tluoranftene66.054 Senzoic add,0ost-6 8en44 at,oholnr.grr gis(2-chlorcelhDry)rnehane
11r-4r-4 8rs(2-chtoroehyt)€lher
39638.324 &s(2{hloroisop{opyDether117+r'7 Brs(2+ththexyl)phlhatare101-5s.3 4Bromophenytpheflyleiher
8s 7 Bulyl benzy,l phhatale
8674.8 Catt)azole5eso.7 4.chlof}Smethylphenol106 47 3 4{hlofooniline
915s7 2{hloronaphhalene9rr 3 2-Chlorophenol7m5 72'3 4{hlorophenyl pheflyteher219.01-9 ftrysene$'70.3 Dibenzo(a,hladhracene132 649 Dibsnzofuran95501 1,2-0idorcbenzene5,U.7&r l,3-Dicilorob€nzene10fi67 1,4{ichloDbenz€ne
91.94r S,3lDichlorobenzidins120$2 2,+Dcl o'Dphenol&1.66? Diethylphthalale131 r1-3 Din€fryl phlhalate
10567.9 2,+tlimettrylphenol
u 71-2 Di-n-butyl phhalate
534.521 4,&DinitrP2-mehylphenol51 23 5 2,+Dnibophend1X1+2 z,4-tlinihototueiemG 202 2,SDnibobluene117414 Di{{dylphfiatate206-444 Fluoranlhong86-73.7 Fluoen€
110'7+l Hexacfroob€m€n€
E/60.3 HexaCNobbutadiene
71414 Hexadiorccyclopsnladieoe97.721 Hexaclrorcslhane193-3$5 Indeno(1,2,3{d)py€ne
sr2{ 1-Methtlnaphthalen€7&591 lsophoone
91.st.6 2-Melh!,haphthdene
es-4&7 2-Methyphend
108-39-4, 3,4.Melhylphsnol
91'20 3 Naohalene
@74-1 2-Nitroarilinoee-0s-2 SNibDanitine
8BL
8RL
BRL
BRL
BRL
BRL
BffL
BRL
BFL
BRL
BRL
BRL
BRL
BRL
8RL
8RL
8RL
8RL
8RL
8RL
8RT
BRI-
8RL
BRL
BRL
8BL
BRL
8FL
8RL
8RL
8BL
BRL
8RL
8RL
8RL
BRL
8HL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
8RL
BRL
BRL
pdkS dry
W/rsdypc4q dy
us4q dy
!S.4q drytNkS dtypgkq dry
lidlq dry
|js/ks dry
|4/ts dy
us,ts dry
|lg/hs dry
t4lS d.ypgkg drv
Pdlq drypdk! drypdkS dry
rdlq dypgks dry
PS'IS dty
udls dry
ps/ks dry
pEt(s dry
pdks dy
|l94q d'l
tigtks dty
!94q dy
lJs4(s dy
pgkg dy
ls/ko dy
lJs,l(s dy
US4(S dy
uglq ry
pS,lS dy
ldks dy
pS4(S dy
tdkS dry
pgks dy
tslq dry
pdkS dry
ldks dry
p94q dry
uS4g dry
pnnq +y
Ps/kg dry
m/k! drypdko dry
pYtg drypVre dry
Udl(S dry
9 1 2
9 1 2
9 1 2
912
912
912
912
912
912
912
912
912
9 t 2
9 1 2
9 1 2g l 2
9 r 2
912
912
912
912
912
9 1 2
9 1 2
s l 2
912
912
912
912
9 1 2
9 1 2
9 1 2gtz
9 1 2
912
s 1 2
s 1 2
912
s ]20 1 2
s12
912
912
912
912
s t 2
912
912
9!2
912
sw846 8270C
This labo4tory repo.l k no, vold withoat oE authoized &ignala.e on lhe cover page .
* Reportable Detection Limit BRL = Below Reporting Limit Page .] I of 154
Page 228
Samole ldeotificatiooM8F-21 2'-l'sA5980l-06
Client Project #301-88
Collection Date/Time26-Mar-07 00:00
MatrixSoil
Receivod27-M 47
CAS Na Anzba(s) Reruh FIag UniB 1RDL Dilulion Method Retr. Prepated Auryzd Botch Anaust
Semivolalll€ Orgrnic ComFour& by GCMS
Semivdatile Oroanic Conoounds bv SW8,t6 8270C
Pr€pared by melhod SW846 35508
1o(Hrr6 4-liitroanitins$45.3 I't'Uob€ilzene
lo.tr5 2-Niuophenoi1tr{I.7 d-iliropnfiol
62,?F9 N_Nit6odmetnybminefq1417 ltNifo6od{flEpytainine861$-6 NNiurlsdph€r|/arir€F, 86s Penbct orqhenol85{1-S Phemndlr$e
l0&lG2 Pn€nd
129{lt{ P}r€ne
lrn{G1 fudnela!02-1 1,2,+Tridlloroben?ff|g
Fsrt 24STd6toqnenol80{e2 a4,STric}torophefiol
P1&4 2-Fwfiiplwyl
67-121 z+\U6@l!6nd
i16!,@4 Niflf€,lwla4'
f 1ffi? Ptl€t,ol4'
171&514 lqplEnyld4
1t&Ei Zl,enhiornqhend
sw846 82ruC
swB46 74714
EPA20'.7
s1r/8.{6 t312t4nu
sll€46 t3t2fl)r0B
8tuBFI-
BRL
8tuBRL
BHLgFL
BFL
BFL
8Rr-8RL8Rr_BfiLBELBNL
ffi
6 l
n6?
15
ldkg fy 3650
dfS dry 912
l4/rs ey 912
E4qdry 3654
ltksdry 9t2
|MS trV 912
rdlS dy gt?
l4rS dry 91?
}clq dy 912
lrg qey ,t2pg&dy 912
MSdy 012
lgft{ fy 912
WrS (Y s12pdb dv 9t2
$-ra%1r1t0%* l N %
trt l0
30.t9)%
trt10.t
mdks fV 0u385
mdbdry 1A
mgqdry r.gs
|Iqfi{ dry 0.6,44
mdrs ry 0P.
mg'lq dfy 0.6,{4
ntSnq fiy 0.$5
mglqdrY lS
n9l 0.0100
fig/l 0_0150
fldl 0.lXE0
'rE4 0.0@5
mgl 0.0125
rn!, 0.q1040
fi94 0.m75
m91 0.01s0
1
I
1
I
1
1
l
I
I
I
1
1
I
Told M€lrb by EPA 6000/7000 Seri6 M€rhodi
71t39976 lrercury
Totrl Metrb by EPA 200 Seri€s Methods
7t1o44 Sifuet
74!J}*2 A/E€nic
?4ro393 &rtrn
1141L9 C€d Um
74eaf-X Chlolnlum
7'r3&94J Lesd
0.0656
8FL
9.91
60.8
0.611
231
68{
02-Apr47 0GApr{7 7031810 YP
r7@4vz S€l€nium 2.80
SPLP Merdr by EPA r3I2 & 6tXXy7000 sertea Mcihods
SPIP Exlradion Csndel€d
14a0e4 Sfs BRL
71los.2 As€nia BFL
741{f3+3 Beriufi 0.0144
7+{!{s9 Cadnium BRL
71!o4i3 ChftrnitFn BFL
7'Il&074 lllstqrry 8RL
7n+94.1 Le3d 00080
77le.1v2 S6td um BFL
G€oerrl Che mislry Psr':rmeters
%Sdids 75.4
SW8461312 28 atn1 28-f'lar{7 7(Xll763 Bo
s:w8.46 1312/60108 3lrrarc7 02.Apr-07 701t1805 tB
@.Apr{7 70318s YP
' ll2-Apr{7 ?G1606 LR
SM254t G llod- :O-ilar.07 m{er.07 m31879 \lll,l
Thb laborulory rcpod ts tut volid Bdthou an aathnriaad signoarc on th. catcr poge-
. Reportable Det€ctioo LiEit BRL= Below RQorring Limit Page l2 of 154
Page 229
SampLe IdentificationM8F-22 2'-4'sA5964r-06
Cliert Proiect #301-88
Collection Date/Time21-Mar-07 00:00
Matrix$oil
Received22-Mar-o'l
CAS No. Anable(s) Resah Fhs Unirs *RDL Diluliott Method ReL Prcpand Anzbzed Batch Analyt
Volrtlle Organic Compounds
VOC ExtractionVolalile Oraanic ComDounds
Fieh extracted
pdkS dry 5.4
pS/ftS dry lOA
pdkS dry 5.4
pdks dry 5.4
!S/kS dry 5.4
pSI(S dry 5.4
pdkS dry 5.4
pSrkS dry 5.4
pdkS dry 10-8
pgkS dry 53-S
pdkS dry 5.4
ldkS dry 5.4
pStxg dry 5.4
pSftS dry 27.O
pSngdry 5.4
vdks dry 5 4
usftg dry 10.8pdkg dry 5.4gsftg dry 10.8
ldks dry 3 4
US/kS dry 5.4pg/kg dry 10.8
!g/kg dry 5.4
!g/kg dry 5.4
ug/kg dry 5.4
wKgdry 54ydkg dry 5.4
ug/kg dry 5 4
!g/kq dry 10 8
lgkg dry 5.4pS/kS dry 5-4
!g/kg dry 5.4pg/kg dry 5.4
irg/kg dry 5.4
ugkS dry 5.4
lqkSdry 5.1
Udkg dry 5.4
US/kS dry 5.4
UdkS dry 5.4
Idkg dry 5.4pdkq dry 5.4pVkS dry 5.4
Udkg dry 53.9
ldxgdry 5.4
ugKg dry 5_4
ugkg dry 5 4ps/ks dry 53.9
!g/kg dry 53,9
FS/(g dry 5.4
2Gt]lar-07 26-Mar-07 7031584 BD
Prepared by method SW846 50354 Soit (tow tevet)76-111 1,1,z-Trichlorotriffuoroethane(FreoERL6144-1 Acetone SRl,107-13-1 Acrylonittite 8RL7143-2 Benzene BRL104{6-1 Bromobenzene 8RL7447-5 Bromochloromethane BRL7u2T4 Bromodichloromethane BRL75-212 Bromoform BRL74€99 Bromomethane BRL7843.3 2-Butanone (MEK) BRL1M-51{ n-Butylbenzene BRL135-98{ sec-Butylbenzene BRL9846{ teft-Burylb zene BRL75rt4 Cabon disulfide BRLS-2t5 Cabon teirachloride BRL108.90.7 Chtoroben:,ene BRI7so0.3 Chtomethane BRL67$6-3 Chloroform BRL74{7.3 C,hloromethane BRL9s-d9-a 2-Chlorotoluene 8RL106:43'1 4-Chlorotoluene BRL96-12{ 1,2-Dibromo-3-chloropropane BRL124-48-1 Oibfomodrloromethane BRL108s34 l,2-DibromoettEne(EDB) BRL74-95-3 Dibromomethane BRLs5-50-1 1,2_Dichlorobenzene BRL54r,731 l,3_Dichtorcbenzene SRL106-46 7 1,4-Dichlolobenzene BRL75 71J Dichlorodifiuoromethane (Freon.12) BRL75,34-3 1,t-Djchjoro€thane ARL107-06-2 1,2-Dichlorcethane 8RL7t35-4 1,1-Dichloroethene 8RL156-s,9-2 cis- l ,2-Dichloroethene BRL156-60-s trans- l,2.Dichtoroehene 8RL78{7-s l,2-Dichloropropan€ BRL142-28.9 l,3-DicNofoprop€n€ BRL5942G7 2,2-Dichlo{oprop€ne BRL5163'545 1,.1-Dichtoroprop€ne BRL10061-01,5Cis-1,3-Dichloroprop€n€ BRL10061-{12€tt?ns-1,3-Dichtoroprop€ne BRLi0n{14 Eh!4benzene BRL876&3 Hexachlombutadiene BRLss1-78€ 2_Hexanone (MBK) BRL98{2-a lsopropylbenzene BRL99+74 4-lsopropyttoluene BRL1634{44 Methyl tert-bug,l ether BRL10810r 4-Methyl-2-pentanone(MlBK) BRL7549.2 i,lethytene chloride BRLs1-2G3 Naphthalene
Page 28 of 165
Thit hboratory rcport is ^ot valid x,irtoaa 6 at lhoiz.d slgnaluH on the cover page.
' Reportable Der€ction Linit BRL = Below Repofting Lini!
Page 231
Sample IdentificationM8F-22 2'-4'sA5964l-06
Client Proiect #l0l -88
MatrixSoil
Collection Date/Time2l-Mar-07 00r00
Rcceived22-MarO7
CAS No. Analrte(s) Result FIaK Unirs *RDL Dilution Method Rel. Prcpcred Andlrzed Bdtch Annlrsl
Vobtile Orgrnlc Compounds
Volatile Oaoaoic ComDoundsPrepared by method SW846 5035A Sdl (low tevet)
BRLBRLBRL
BRLBRLBRLBRLBRL
BRI.BRLBRL
75{9-4 Trichtorofuoromethane {Freon jj) 8RL
10365.1 n-Propylbenz€ne10G42 s Styrene63G20-6 1,1,1,2_T€trachtoroethane79-34-5 1.1,2,2-Tetrachloroethane12718! Tetrachloroethene10&48-3 Tolsene87€1i 1,2,3_T.ichtoroberuene12G82-1 .1,2.+Tdchtorotlenzene
71,554 1,1 ,1-T tichhoethane794+5 1, 1 ,2,Trichtoroethane79414 Trichtoroethene
SW84682608 27-Mat47 2I-Mat47 7031658 RU
+CT ETpH 27.Mat47 29.Ma'.o7 7031590 DS
!,6-18-4 l,2,Slrichtoropropane
9543-6 l,2.4.Trimethylbenzene10&87€ t,3,tlimethytbenzene7s{11-4 Vinyl chloride1330-20 7 m,p-Xylen€95-474 o.Xylene10999-9 TefEhydrofuran
60-2+7 Ethl ether99+45-8 Tert-amyl methyl ether637,92-3 Ethytted-butry'ether10&20 3 Di-isopropyt ether7545-0 Tert-Butanot/butylatcohol123-91r 1,4-oioxane
Surogale rccovedes:
460404 4-Bromonuorcbenzene
203/-265 Tduene4S
17o6a07-0 1,2-Dic.hloroelhane-d4
1A6O-53-l Dihromof, uoromelhane
Ertrscarble Petmleum HydrocNrbons
Extractable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
800ffi1-9 Gasoline
68476-30-2 Fuetoit#2
6S47C31,3 Fuet Oil#4605,53{04 FuelOil#6
M09800000 Moto'r OilJ00100000 Aviation Fuel
Unidentified
Other Oil
Total Peholeum Hydrccarbons
C9{36 Atiphatic Hydroc€rbons
Sunogale reeoveries:
a38633-2 |-Chbftocladecane
Semivolr.ile Orgadc Comporr& hyCC
Orqanochlo.ine Pesticides SW846 8081A
Prepared by melhod SW846 3tl5A
30$0l)-2 Aldrin
BRLBRLBRLBRLBRLBRLBRIBRTBRLBRLBRLBRLBRL
93938599
BRLBRLBRLBRLBRLBRLr64
Calculated as164164
98
!g/KS ijry
!g/kg dry
!g/kg drypg/kg drypg/kg dry
Lig/kg dry
!g/kg dry
!g/Kg drypgxg dry
US/kS drypg/kg dry
lgKg dry
U9/k9 dry
ug/Kg drypg/kg dry
Pg/kg dry
!q/kg drypS/kS drypg/kg dry
ttgkq dtypdks dry
ldks drypdkS dry
!S/kS dry
lqks dry
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.1
5.4
5.4
5.4
5.4
5.4
r0.8
5.4
53.S
5a
5.4
5.4
5.4
5 3 9
108
1
1
1
1
1
1
1
1
1
1
i
l
1
I
I'I
'|I
1
1
1,1
1
1
1
70-130 %70-1W %7G130 %70-130 %
mgi Kg drymgftS drymgu4(g drymgL/Kg drymg/kg drymg/tg drym!r'kg dryndkg dr,lmdks drymgftg dry
,10.1
40.1
40.1
40.I
40.1
40.1
40.1
40.1
40-1
40.1
222
2222222
44-140 %
ugfts dry SW846 8081A 2&Mar-07 28-[,lar47 7031516 TG
Thit hbofstory @port it nol valw *ilhoq an authoizei signaturc ot the coeer page-
I Reportsble Detection Lihit BRL = Below ReportinB Limit Pige 29 of 165
Page 232
Sarnple ldentificatiotrM8F-!2 2'-4'sA59641-06
Client Proiect #301-88
MatrixSoil
Colle€tioo Dat€/Time2 I -Mar-07 00i00
Received22-Mt-o7
CAS Nu Aaslytz(s) Resuk FrtC ,RDL Diluion Method R4 Ptpared Aaalyzel Bstch AMlttt
S€mlvol{tile Orgrnlc Compounds by CC
Oroanod orhe Pesticides SW846 8(E1A
Prepared by method SW846 3545A
319-84{ g-BHC
319-E5-7 b-BHC31$ffi d-BHC
58€$9 gFBHC (Undan€)
57-f+9 Chlordane72-51-s 4,4!DDD (p,C)
72-5+e 4,4'-DOE (p,p.)
so-2$3 4,4.-DOT {p,p.)60-57-l Oeldrin95S-944 Endosulfan I3321165.9 Endosulfan ll1031{74 E tdosllfan Suhhte72-2GE €ndrin742i.9!4 EndrinAldehyde
76-44{ H€ptacilor
72-4?5 Methoxydtlor
1024{7-3 Hoptacldd Epoxide8041-3t2 Toxaphone510!7t-9 a-Chroftlan€5666'34-7 g€hlodan€
5349+70-5 Endrin Keiono
SlnTogafe recovertss:I o38e4+2 4ja&Octdfr uotobiphonyt (Si
m5t-2+j Decachbtobiphenyl (Sr)
Polvchlorinated Biohenvls bv SW846 8082
[email protected] by metM SW846 3545A
1A1+11-2 PCB 10161110+2&2 PCB 12211i141-16{ PcB ,l232
5346r$21-9 PCB 1242126f2-?94 PCB 1248r1c97@l f,rcg t254
1100c€2-5 PCA 1260
3ft2+n 5 PCB 1262rrr0G14-. PcB 1268
Su/'oglefu rEcovrar€srt.Bea-e+2 4, 4-DB-Oddquotubipheny' (St)
msl-21-3 Deeechlombiphenyl (Sr)
S€nivolstilc Org.dc Conrpounds by CCMS
gRL
BRLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRL8RLBRTBRLBRLBRLBRLSRLBRL
69
BRLBRLBRLBRLBRLBRL
BRLBRL
35
BRLBRLBRLBRLBRLBRLBRLBRI-
lgkg dry
lgl(g drypdkS dry
US/kS dry
lrdks dry
ldkg dry
udks dry
ldkS dry
ugkgrtFJ 5.€O
udkg dry 5.80pg/tg dry sao
ldkg dry 5J0
UdkS dry 29.0
udkS dry 5.80pqkS dry 5.80ydko dry 5.80pdkg dry 5.80
ldkg dry 5.80
ldxgdry 5.80
ldlg dry 5.80pSng dry 5.00
Ugikg dry 5-80pgkg dry 5.80
lqrg dry 5-80pw6ry s.80
ldkg dry 29.0pdko dry 5.80
ldks dry 5.80pdkg dry s-80
3G1fi Yotu1 f l%
udkS dry 11.6
ldlS dry '11.6
pS/kS dry 11.6
Ug,fkS dry 11.6pdkg dry 11.6
lrdkS dry t 1.6
udkSdry 11.6pS/rS dry 11.6
ldkSdry 1l-6
30-150 %30-150 %
SWS,ltj 8O81A 2&Marfi 26{{ar{7 7031516 TG
SW846 8082 26-Mar47 2&Mar-07 7031515 SM
SUA46 8270C 26Ma.-07 28.[nar{7 7031514 M-B
S€mivolatile Orqanlc Cornooonds bv SW8,t6 8270CPrepared by nEthod SW846 355088$32-9 AcenaphltEne2G+9e8 Ac€naphttryleneE-5+3 AniIn€12{}12-7 Anthacene1912-2+9 At?in€loi!.9&3 Azobenzoneoiphenytdiazine9247-s B€nzj{tine56-5t3 Bonzo (a) anthrscene
249 5249 5249 5249 5
249 5245 5249 5219 5
Ihk labors&try ftpora ls Eot tolid tiithoU an dt thortzzd signortt e on Uc corer page.
* Repo able Det€ciion Limit BRL= B€low R€Porting Lnnit Page 30 of 165
Page 233
Sample IdcntificationM8F-22 2'-4'sA5964l-06
Client Project #301 -88
Collection Dale/Time2l-Mar-07 00100
MatrixSoil
Received
22-Mar-07
CAS No, Anabte(s) F,oE 'RDL Dilaioh Merhod Retr Prcpared Anal!.e.] Batch Anabst
Scmivolrtile Organic Compounds by CCMS
Semivolatle Oraanic Compounds bv SWg46 BZTOCPropared by method SW846 35508
50-32-8 Benzo (a) pyrene
?0+99-2 Benzo (b) fluoranthene191-24-2 Benzo (g,h,i) p€ryt€ne207-0S€ Benzo(k)fiuoranthene65{5-0 Eenaoic acid10tr514 Eenzylalcohol111-91-1 Bis(2-chloroethoxy)methane111-14-4 Bis(2_chloroethyl)€ther3963+32€ Bis(2-chloroisopropyt)ethef117€1,7 Bis(2-ethythexyl)phthalate101-55'3 4-Brchophenylphenyleth€r8568-7 Bu!/benzylphthalate
€6-748 cabazole59-5G7 4-Chto|o-3-methylphenol106-473 4-ChloDanitine9r-s87 2-Chtoronaphthatenes5-5ru 2-Chtorophenol7005-72-3 4-Chlorophenyl phenyl ether218{14 Chrysenef,3-7G3 Dibenzo (a,h) anthEcener3244-S Dibenzofuran9s-5O-1 1,2-Dichlorobenzen€
!11-73-1 1,3-Dichlorobenzene10€-46-7 1,4-Dichlorobenzene91-94-1 3,3'-Dichtorobenzidine120-83-2 2,4-Dichtorophenolu$+2 Diethyt phthatate
131-11n Damethytphthatate10tr7-9 2,4-Dimethylph€nolu-74-2 Di-n-butylphthalate534-52-1 4,6-Dinitro-2-ineUrylphenol51-2&5 2,4-Dinitrophenol121-14-2 2,4-Dintrototuen€60e20-2 2,o-Dinitrotoluenet17€4{ Di-n-octylphlhatate206r,{{ Fluoranhene
W73-7 Fluorenel1&?4-1 Hexachlorobenzen€87$8-3 Hexachtorobutadiene
n174 Hexacltlotocyc)opentadiene
67-72-1 Hexachloroelhane
1913e-5 Indeno (1,2,3d) pyrene9G12{ t-Methytnaphthalene785$1 lsophorone
91.57$ 2-Methylnaphthalene9538-7 2_Methylphenol
10&394, 3,4-Methytphenol106-.14-59l-2G3 Naphthatene88741 2-Nitmenitine!19-0+2 S.Njtroanitine
ARL8RLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL8RLBRLBRLBRL
BRLBRLBRL
rc/kS dry 249
!S/kS dry 249pdkS dry 245
ldkS dry 249
ldkg dry 249pg/kg dry 249pgts dry 245pdkS dry 249
lgkS dry 249
lgkS dry 249
!g/kS dry 249
trg/kg dry 249
uS/tS dry 249
udkg dry 249yg/kS dry 249pg/kg dry 249pStkgdFt 249pqlkSdry 245
Ig/kq dry 249pS/kg dry 249
Udkgdry 245
USAS dry 249pdkS dry 245pdkSdry 249pg/kg dry 249
lqkSdry 249
lSikg dry 249
ldkS dry 249pdkS dry 249pS/kS dry 249pS/kS dry 249pSI(S dry 249pdkS dry 249
!S/kS dry 249
!S/kS dry 249
Ug/kS dry 249
Fg,kS dry 249pg/kS dry 249
l.idkg dry 249
ug/kg dry 249
Lig/kg dry 249
!g/kg dry 249
!g/kg dry 249
udkg dry 249
ldkg dry 249
ldkgdry 249
!C4(S dry 249
pS/kS dry 249pdkS dry 249pS/kS dry 249
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
Thh laborulory rcpon is not veld wirtoa an a!rtorized sigEature on the cover prye-
' Reportabl€ Detecdon Limit BRL = aebw ReportinC Limit Page 3l of 165
Page 234
Sarnple ldentificationMtF-22 2'-41
sA5964l-06
Ctieot hoiect #30t-88
MatrixSoil
Collection Date/Time2 I -Mar-07 00:00
Received22-Mar41
CAS No. Atautc(s) F L g ateils aRItL Dilaion Method Retr Prcpand AtsQzed Bath Anolfst
SemivoL.lil€ Organic Comporn& by CCMS
Semivolatlle Orqanic Comoosnds bv SWe46 8?70C
Pr€pared by melhod SW846 35508
r !015 4-Mtoanitine98€5-3 Nitrobeflzene
8E-75-5 2-NibophenolIO(!!A-7 4-NitEPhenol62-754 N-Njtrosodimethylamin6621-64,7 N-Nit!5odi-Gpropylamin€BG.3G6 N-Niaosodiphenylaminea7€e5 Pentacfilorophenol85.Oi€ Ph€nanlhrenelO&€5-2 Phenol1294+0 Pyr6n6rlo{Fl f}yridhe12{}€2-1 1,2,4-Tdcf{ofobenzene
95-9+4 2,4,$Trichlo.ophenol8O{G2 2,4.dTdchlorophenol
Suiogate 'atj'\lerias
32140-8 2-Ftuor&iphenyl
367-124 2+fuorophenol
4165404 Nillobenzene4s
4165-62-2 Phqol45
1718.s14 Tephenyl4l4
1 18-79-6 2, 4,o-Ttibton@phenol
Totll MGtrli by EPA 600(y71n0 Series Merhods
SW846 a270C 2GMsrry 28lhr-07 7031514 M.BBRLBRL
BRL8RLBRLBRLBRLBRLARL
BRLBRL8RLBRLBRL
4851
54
0.0614
BRL
4.95
28.8
0.69s
40.9
4t1.9
BRL
Completed
BRL
BRL
0.0682
aRro.0214
BRL
BRL
8RL
90.6
ldkg dry 994
ldrS dry 249
Fgl(S dry 249
ldl(g dry SS4
ldl€ dry 249
ldl€ dry 24s
UgJkSdry 245
l€il€ dry 249
lSASd.y 249
UgtS d.y 249
udkgdry 249pgrs dry 249pdksdry 249
ldkS dry 249
FdkS d.y 249
3O-130 lo1UI10 %30-130 %15-110%3G130 %1+flo%
mglkg dry 0.033,0
drg/kg dry 1.04
mg/kg dry 1.56
mSn€ dry 0.519
mgn(g dry 0.259
drdkS dry 0.519
mgtg dry 0.71A
n€rkgdry 1-56
msl 0.O20o
mg.fl 0.0150
mgl 0.0i5O
rnSI 0.0025
mdr o-o150
rndl 0.00040
mdl 0.0150
mgn 0.0150
%
5
5
5
5
5
5
5
5
5
5
5
7439-S7{ lredrry
Total Mebls by EPA 200 serles Mettodt
7440-224 Silye(
Zt4lts3&2 AE€nic
74ao.393 BAriUm
7+G43-9 Cadnrium
7r.4crt/-3 Chromium
74:99?-1 Lead
7782-492 S€lenium
SPIP Afaclion
71"1G22-{ Siker
7a,|{)ie2 A6enic
Trlrl{)'3+3 Badum
7r.1O.13-9 Csdn{un
74'(F17+ Chromlum
7439-974 Mercqry
7+3s-C2-1 L@d
7?82-49-2 Selanium
Generd Chehbtry Prrsmetels
% Solids
1 Sw846 747fA 2g-n1at47 284a147 ?031495 YP
EPA 200.7 2A-Mar-O? 28-&lar{7 70314S4 RM
SPLP Mctdr by EPA 1312 & 600{y7000 S€rier Me0ods
1 SW8461312 m.Ma.-07 26-&ta.47 70315€0 BD
1 SWE|6 f31:l/60108 23'-Mat47 28.|nar4f 7031651 HB
1 '
1 '
1 SW8,|613127470A ' ?6-MEt47 7031652 YP
I SW8461312/601@ ' 284ar47 7txil651 HB
1 '
1 SM2540 G Mod. 2+Mat47 24]|n9f47 7031470 QP
Thtt lab&tury Epora ls nol eotu wi&ra!! att arthorlzd sigrratara on lhe coye page -
* Reporbble Detectiod Limit BRf = B€low Reporting Limit Page 32 of 165
Page 235
Samole IdentificationM8r,'-2t 2,-4'sA59641-07
Client Proiect #301 -88
MatnxSoil
Received
22-Ma(0'7
Collection DatE/Time21-Mar-07 00:00
CAS Na A"aryte(s) FIag A a *RDL Dilqtbz Merhod Ret Prepa.ed Adalr.ed Barch Analtsl
Volrtile Orgrnic Compounds
VOC ExtractionVolatile Oroanic Comoounds
Field €xtrected
Prepared by method SW846 5035A Soit (tow tevet)
76 13'1 1,1,2-ftidllototinuoroethane (Freo€RL6744-1 Ac€tone ARL
107,13-1 Aor/lonitrit€ BRL
714T2 B€nzgne BRL
108-86'1 Bromobenzene BRL
f4-97-5 Bromochloromelhane BRL
75-274 gromodichtoromethane BRL
75-?12 Bromotorm BRL
7,1+3-9 Bromomethane BRL
78-9+3 2-But6none (MEK) BRL
104-51-6 n-Butylbenzene BRL
13+9€{ sec-Butlbenzene BRL98{6-6 tert_Butytbenzene BRL
75,rt0 cabon disu tde BRL
56'23-5 Cabon tetrachtoride BRL10&90J Chiorob€^z€ne BRL75-00-3 Chloroethane BRL67€S.3 Chlororoarn BRL
74Af-3 Chloromethane BRL
9549{ 2-Chlorotoluene BRL
10643-4 +Chlorotoiuene BRL
96-12{ 1,2-Dibromo,3-chloropmpane BRL
124-48-1 DibromochloaomedMne ERL
10Gs3-4 l,2-Dibromoethane(EDA) BRL
74-95-3 Dibmmomethane BRL
95 50,1 1,2_Dichtorobenzene BRL
54173-1 1,3-Dichlorobenzene BRL106-'16'7 1,4-Dichtorobenzene BRL75-71-A Dichlorodifluoromethane (Freonl2)BRL75-34-3 1,l_Dichloroethane BRL
107{6-2 1,2-Oichlofo€thane7s-35-4 1,1-DachlofoetfEne15+59-2 cis- 1 ,2 -Dichloro€thene1s6{0-s t?ns-1,2-Dichloroelhene78{7-s 1,2-Dichloropropane142-28-9 .1,3-Djcldoropaopane
594-20-7 2,2-Dichlofopropanes61s8{ 1,1-Dichloropropene1 0{,61{1-5 cis-1,3-Dichloropaopene10tr6r{2{ taans-1,3-Didlloropropene10H14 EhylbenzeneA74B-3 Hexachlorob{,ttadiene591-78{ z-He1anone(MBK)98{2-0 lsopopylbenzene9€47{ +lsopropyltoluene1634{4-4 Methytted-butylehef
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
10&10-1 4-Med1yi-2-penranone(MIBK) BRLr5+*2 Metfiytene chtoride 8RL
pqksdry 60
lgftS dry 120
lqkg dry 6 0pqkS dry 60
lgks dry 6 0pgkS dry 60
VdkSd(y 60
lgks dry 6 0
lgks dry 120
ldks dry 59I
PgkS dry 6.0
!S/kS dry 6.0pgftS dry 6.0ggnq dry 30 0
udkg dry 6.0
USiTKS dry 6.0
US/kS dry 12-0pS/kS dry 6.0
!g/kS dry 12.0pgftg dry 6.0
ldkg dry 6.0
W/kg dry 12 0
!g/ks dry 6.0
!g/kg dry 6.0pgkg dry 6 0
!S/kS dry 6.0
ldkS dry 6.0pg/kS dry 6.0
!g/kg dry 12.Opg/kg dry 6.0
ldkg dry 6-0
tig./kg dry 6.0
ldkg dry 6 0
Fdkg dry 6 0pdks dry 6 0
udks dry 6.0
ldkg dry 6.0
ldks dry 6.0
t Sikg dry 6.0
t'dkg dry 6.0pg/kg dry 6.0
ldkg dry 6 0pdkS dry 59.S
ldkS dry 6.0pg/kg dry 6-0
HdkS dry 6.0pS/kS dry 53 IpStkSdty 599
US/kS dry 6.0
26-MaF07 26-[4ar{/ 7031584 BD
91-2G3 Naphthatene
Page ll of 165
This labo4loA ,eporl b ,rol e.tlid wilhou! on authoir?d signatare on the covr paEe-
a Reportable hection Limit BRL = B€low Reporting Limit
Page 236
Samote ldeotificationMtF-23 2'-4.sA5964l-07
Client Pmject #l0t-t8
MatrixSoil
Collection Date/Time2l-Mar-07 00:00
Rec€ived22-M,.r-07
CAS No. tuslru(s) Restll Flos "RDL Dilution Me.hod Retr hepar.d A@lyzen Bahh An4lfsl
Vohtile Orgrnic Compoohds
Volatile Oroanlc CornooundsPrepar€d by ms0|od SW846 5035A Soil (low l€ve{)103{5n GPropy'benzene BRLi00{2-s St}'I€n€ BRL63G2c6 1,'|,1,2-T€{r€cHoroethan6 BRL7s-3+5 1,'|,a2-T€Fachloroethane BRLt27-18-4 TetachloroellEne BRLt0&883 Toiuen€ 8RL87€1{ 1,2.}Tdchlorobonzen€ BRL12o"B2n 1,2,+Tdchlorobenzen6 gRL
7l-55€ 1,1,1-Td, oroetharte BRL79{G5 1.1,2-Trict' oroefhane gRL
79{1{ Trichloroethene BRL?5{9-{ Trichloaonuorcrhethane (Freofl 11 ) BRL9&18-4 t,2,$Trichtoropropane BRL95$3{ 1,2,+Tdmethytbenzene BRL10&674 .l.3.glrimethytb€nzene BRL7Fo1-4 Vinyt chtoride BRL133G20-7 m,ptsXylene BRL9s-47i o-Xylene BRL10999-9 T€trahydrofuran BRLdl"2s7 Ethylether BRLgarcs{ Tort-amylmethy' ether ERL637-s2-3 Ethyt ts -buM eher. BRLl0e?G3 Diisopropyl €ther BRL75€t0 Tert-Butanol/ butyt atcohol1?+9rr l,4-Oio,€ne
S|'rogale reovelies:1@401 +Btofitofluorottenzeie
m1z-26-s Tolucne4g
| 7060474 1,2'ichlorcethane44
186V5?7
SW8468260S 27-Mat47 27-Met47 7031658 RLJ
BRIBRLBRL
BRLBRLBRL
Calculiated as5545$4
123
pqlqdry 6.0pdxgdry 6.0
!S/kS dry 6.0
!SI!S dry 6-0
lqkSdry 6-0pdkSd.y 6.0pg^gdry 6.0
FS/&S dry 6.0
Fgtsdry 6.0pdl(gdry 6.0
!g/tS dry 6.0
ldl(g d.y 6-0
ldkg d.y 6-0
lglq dry 6.0
lrgxS d.y 6.0
lSrqdry 6.0
IC/X9 dry 12-0pdts dry 6.0
ldkS dry 59.9
UdkSd.y 6,0
ldtsdry 6.0pdxs dry 6.0pgtS dry 6.0
!g*9 dry 59.spCftS dry Im
70-130 %70130 %7G130 %70-130 %
nE/kg dry 219mgilqdry 249mgfl(g dry 249mgr'kg d.y 249rndkS dry 249meftgfty 249mdl€ dry 249msr€dry 249nE/tgdry 249nqfgdry 219
40-140 %
+CT EIPH 27-Mat47 29 lat47 7031590 DS
f'ttrft bbh Pcft oleum Hydrocrrbou3
Extractable Tdal Pelroleurh Hvdmc€rbonsPr€pared by method SW846 35508flXlftl-S Gasolinee18.476-30-2 Fuel O[ #2eaa7a31,3 FuslOil r,46855$00{ FuelOiltSM0se0@00 lroto. OllJ0l)100000 Aviation Fuel
UnidefltifedOth€f OilTotal Peboleum MrocgrbonsC9436 Aiphatic Hydr@rbons
Slnrogat€ rBcowriss:3i86-JXZ l-Chtotoocladecane
Sehivoldlc Oryrrtc Compornds by cC
Oroanochlorin€ Pesticides SW846 808'lAProparcd by method SW846 3545A3tr9-q1,2 Aldrin
BRLARL
9292u99
t01010
101 01010t0t0
t0
ygtg dry 6.26 S1418,16 SOEIA 2AMar{7 28{rar{7 7031516 TG
Thit bborulory reIofl E Eot ealld x,ithotu ta aathoiltd slgnalaE ol the caver pz$-
a Reportable Detcctiotr Limit BRL = Belo*' Reporting Limit Pase 34 of 155
Page 237
Saftple ldenfificadon
M8F-23 2,-4,sA5964l-0?
Client Proiect #30t-88
Collection Date/Time2l-Mar-07 00:00
MatnxSoil
Reoeived22-Ma.-07
cAS No. Anab'E(s) FloC UniLs *RDL Dilation Method ReJ Prcpared AnaIWd Batch Anabsl
Semlvoladle Organlc Compounds by CC
Oroanochlorine Pesticides SW846 8081A
Prepared by method SW846 3545A
319-8,{4 a-BHC319-45-7 b-BHC319-86{ d-BHC58€e-e g_BHC (LiMane)
57-7+9 Chlordan€72-s4.4 4,4.-DDD(p,p')72-55-e 4,4-DDE (p,p')
5&2+3 a,4-ODT (p,p')
60-57,1 Di€ldnn
95998-0 Endosulfan I332J3it9 Enotosulbn ll103147-8 Endosulfan Sultate72-204 Endin7421,93-4 EndrinAld€hyd€7644'4 H€ptachtor7243-s Methoxychtor1024-57-3 tleptachlo.Epoxide80013S2 Toxaphene5103-71-9 a-Chlordane5566-34-7 g-Chlordane
53494,70-5 Endrin Ketone
Sunogtale recov€nesi1.;]8fre+2 4,{-Dgocte\uorobiphenyr (s4
m51-2+3 Decachlorobiphenyt (Sr)
Polvchlorinated Biohenvls bv SW846 B082
Pfegared by method SW846 3545A
12671,11-2 PCB 10161110d.28-2 PCB 1221111-41-16.s PC8 12325346+21-e PCB 1242126f2-4n PCB 124811097{9-1 PCB 125411096-82-5 rcB | 260x732+2r' PCB 12621110+144 PCB 1m8
Sunog€ls recow'bs:10386842 4,4-DB-Octatluorobiphenyl (Sr)
2051-243 Decachlombiphenyl (Sr)
Semivoloail. Orgraic Conpounds by CCMS
8Rt_8RL8RLBRLBRLBRL8RLBRLBRLBRLSRLBRLBRL8RLBRLBRLBRLBRLBRLSRL8RL
126
BRLBRLBRLBRLSRLARL109BRLBRL
3585
BRLSRLBRLBRLBRL8RLBRL888
pg/kg dry 6.26
PS{(S dry 6.26pg/kg dry 6.26
!S/tS dry 6.26
ldkg dry 31 3
!g/r(g dry 6.26
!g/(g dry 6 26pS,4(S dry 6.26pS/kS dry 6.26
lSftS dry 6.26
!S&S dry 6.26psftS dry 6.26pSAS dry 6.26pdkSdry 626pdkg dry 6 26
!g/kg dry 6 26
!g/kg dry 6-26
trdkS dry 31.3
!S/kS dry 6.26pg/kg dry 6.26
UdkS dry 6.26
30-150%30-151) %
UdkS dry 12 5
Fg/kg dry 12.5
!g/kg dry 12.5
t'g/kg dry 12.5
Ug/kS dry 12.5
US/kS dry 12.5
!g/kg dry 12.5
!C/kS dry 12.5
rrdks dry 12-5
30-150 %30-150 %
pdkS dry 771
lgftS dry 771
lgftS dry 771pdkS dry 771
ldks dry 771
!S/kS dry 771pS.4€ dry 771
Us/kS dry 771
SW8468081A m-Mar{7 28iL,lar-07 7031516 TG
Sw846 8082 26-Mar 07 28-MaF07 7031515 SM
SW646 8270C 26-l\rar47 26-Mar-07 7031514 M.B
Somivoiatile Oroanic Comooonds bv SW846 8270CPrepared by method SW846 355084332-9 Acenaphthene20es6{ Acenaphthylene62-5+3 Aniline120-12-7 Anthracene1912-24-9 Alrazine10+33-3 Azobenzene/Diphenyldiazine92{7-s Benzidine56.55'3 Eenzo (a) anthracene
5
5
5
5
5
5
5
Thit laborutoty rcltor'l is not uolid withotl.t sulhotized slgn^itre on lhe covr page.
' Reporta.ble Detection Limit BRI = Below Reporting Linit Page 35 of 165
Page 238
Samole ldentificationMEF-23 2'-4'sA5964l-07
Clietrt Proiect #301-88
Collection Datey'Time2 I -Mar{7 00:00
Received22-Mat47
MatrixSoil
C"1S No, Andlrte(s) FIag Adia *RDL Diluion M.lM Ret Prcpzrcd A&olfaad Batch Aralyst
Semivolalile O€rnk Cortrlour& by GCMS
Semivolatile Orqanic Comoounds bv SW846 8270C
Preoared by nethod SW846 35508
50-32{ EerEo (a) pyreneS-S-2 B€nzo (b) fluoran$ene191-24.2 Senzo (9,h,i) perylene20?-(E-q Benzo (k) fluo(anthene85{5-0 Benzoic acid1o,+5r€ B€nz!'lalcoholi11-911 gis{2-chloroethory)rnethane
i1l-444 Bis(2-chtorcethyt)€her39sH2-9 Bis(2{hlooisopropyl)elher117-s1.7 Bis(2_€6ylhexyl)phthatate101-55-3 4_Brofippt€nyl ph€nytether85.68.7 Butylbenrylphthalate8&74-a Cerbazole5g.5tl7 4chlorE-3-flethylphenoli06-.|7{ +Chlomaniline915&7 2-Chloronephthalene95{7{ 2.Chlorophenol700e72-3 +Chloroph€$yt phenyl ether21841s Chrysene53.7G3 Dib€nzo (a,h) anthracene132{44 Oib€nzofuran95-50-i |,z-Oichlorobenz€ne4,41-&1 l,+Oic*orobonzen€10ffi7 l,4-Dichlofobenzenes1€4-1 3.3'.Oid$orobenzidine12Gs+2 2,4-Oichloroph€nol64+s2 Diefly' phtrlalate131-11.3 Dimethyl phthalate10567€ 2+Oirnethytpherctu-74-2 fx-n-buvphthalate534-52-1 4,6-Dlnitrc-2-methylphenol51-2F5 2.4-Dinitrophenol121-14-2 2,4-Onibololuene606-2G2 2.(ioinibotoluene117{44 Dkl.octylphlhatate20G.r4-o pluot€nthene
&7+7 Ffuofen€l1&74-l Hoxachlorobeozene87{S3 Hexachlorobutadienen474 Hexachloroq/dopentadi€fle67-12-1 Hexacfiloroethane19$39-5 tfld€no (1,2,3-cd) pyrenefi.124 1-Methylnaphthatene7E-59-l lsopftorcne9157$ z.tlethynaphhatene9s$? z.Methytphenol1o&x94. 3,4-Mehylphenol106-44-59l-21>3 Naphthal€ne&-744 2-Nitroanitine9O.O+2 $lliuoanitin€
BRL1,370BRL1,180BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL1,G)0BRLBRLBRLBRLBRLBRLBRL8RL8RLBRLBRLBRLBRLgRL
aRlBRL2,090BRLBRL
BRLBRLBRLBRL8RLBRL
BRLBRLBRL
BRLsRtBRL
ldks dry TI1
udks dry n1pgrs dry nr
USrkS dry 7?1
tdl(g dry 771
tdks dry 771
t|g^g dry 771
uS&Sdry Tll
USAgdry 771pSrrS dry 771
UdrS dry 771
Ug/kg dry 7f1
!g/ko dry 771pS/kS dry 771pS/kS dry 771
l,gkgdry 771pdks dry 771
ldlq dry r7r
IS/IS dry 771
lgkg dry 771pSikS dry 771
UC/tg dry 771
uErsdry 711pdrs dry 7lr
lgrkS dry 171
US/kg dry 711
rdkS dry 771
IISA9 dry 771
tdkg dry 711pS/kS dry n1pgl(g dry 771
ldlq dry f1r
Udks dry 771pgi€ dry 771
lgl€ d.y 771pSftS dry 771
IdkS dry 711
udks dry n1pgrs dry 771
ldtS dry nl
Uglq dry 771
lqkSdry Tt'l
Itg/kg dry TI1ys/kg dry 771pg,lq dry n1pglgdry 771
ldkg dry 77r
US/kS dry n1
frgftS dry n1
Ug/kS dry 771
SW846 8270C rc-Mat47 28-l4a..0l 7031514 M.B
Trth lafuorf rqod ls t ol volid w hoa dn at lhorlzd slgnaleQ ott the coeer IraE .
' Reportable lh€crion Limil BRL = Below Reporting Limit Page 36 of165
Page 239
Sample IdeptificationMtF-23 2'4'sA5964147
Client Proiect #301-88
MatrixSoil
ColLectiotr Dato/Time2l-Mar-07 00:00
Received22-Mar-0'l
CAS No. Andr.c(s) Resa,t Fhc Unia *NDL Dilution Method Retr Preparcd Arralyzed Borch AnaQsl
S€mivohtil€ O.ganic Comp0undr by CCMSSemivolatile Oroanic Compounds by SW846 8270CPfepared by method SW846 35508
SW846 8270C 26-Mar47 2g4l,ar07 7031514 M.B
1 SW8467471A 28-MaF07 28-li,lar{7 7031495 YP
Toral Me..ls by EPA 6000/7000 Srries Merhods
7439-976 M€rcury
Total Metab by EPA 200 Sarler M€rhods
74rlct-22-4 Silver
74.rc-3€-2 Arsenic
7444-39-3 Earium
744043-9 Cadmium
7,140-17 3 Chromium
74@-92-1 Leacl
t82-49-2 Selenaum
100-0lS 4-Nitroaniline
96-9+3 Nitrobenzene
8a-7+5 2-Nitrophenol
10G02-7 4.Natrophenol62-7+9 N-Nitrosodimeihylamine621s4-a N-Nitro6odi,n-p.opylamine86-30{ N-Nitrosodiphenylamine87{+5 PentadtlorQphenol
a5-01€ Phenanthrene
108-95-2 Phenol129-00{ Pyrene11G86r q/ridine
r20-82'1 1,2,4-Tricilorob€n2€ne9s95-4 2,4,+Trichlorophenola8{+2 2,4,6-Trichlorophenol
Surrogate .sco!/€ti€s:
32140-8 2-Fluorobiphenyl
36r-124 2-Fluotophenol
416a404 Nil/obenzet e4S
116542 2 Phenol4s
1718,51-o Terphenyl-dl4
1tB n'6 2,4,6-Tibromophonol
trdkS dry 3080
udks dry 171
!s/ks dry 171
W/kS dry 3080
w/kg dry 171
W/kS dry 771
lgkg dry f71
WikS dry 771
lsiks dry 771
ldkS dry Tl1
WftS dry 771
rr9/k9 dry Tl1
!g/kg dry r71
lSftS dry 771
!S/kg dry Tt1
30-130 %1*110 %30-130 %1+110 %30-130 %15-110 %
mg/kg dry 0.0327
ddkg dry 1-02
mgL/kg dry 1 .52
ms/kS dry 0 506
mdlQ dry 0.254
mg/lg dry 0.508
ngkq,try 0.t62
mq,/kg dry 1.52
mg/l 0.0200
mgl 0.0150
mq 0.0150
nrsn 0.m25
mgLI 0.0150
mg|n 0-00040
tndl 0.0150
firg/l 0.0150
BRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL2,210
BRLBRLBRL
6 l
59745 l
0 t93
BRL
6.41
39.2
0.599
29.4
99.7
BRL
5
5
5
5
5
5
5
5
5
5
5
5
5
5
SPLP Met{ls by EPA 1312 & 6000/7000 S€ri€s M€thods
I EPA200.7 28-Mar07 28-[4ar47 7031494' t "
1 '
1 "
I '
t '
1 "
1 SW84613t2 26-Marfi 26{v1aF07 7031560 BD
1 SW84613'f260108 2a-Ma(41 28-Mat-07 7031651 HB
1
1 '
1 ' ,
1 ' ,
1 SW846131274704 ' 2&Mar-07 7031652 YP
1 SW846131260108 ' 28-Mar-07 7031651 HB
1 '
1 SM2540GMod 244tarO7 24-Mat47 7031470 QP
RM
SPLP Enraction
744G22-4 Silver
7440-34-2 Arsenic
7440-3s3 Barium
74a0-419 Csdmium
7440-47 3 Chmmium
7439-97{ Mercury
7439-92-1 Lead
7ra2{92 Selenium
Gercral Chcmirtry Perar€ter!
% Solrds
Completed
BRL
BRL
0.0427
BRL
BRL
BRL
0.0336
BRL
89.9
This lahorutory rcpod is ,ot valid wilhotd a saahori.et sEnarare on thz cot'er pqge .
'Reportable Detection Limit BRL = Below Repoding Limil Page l7 of l6J
Page 240
Sample ldentificationM8F-242'4'sA5964t-08
Client Proiect #30t-88
MatrixSoil
Collectiotr Date/Time2l-Mar47 fr):00
Received22-Mafi7
CAS No- Adat z(s) Rett/lt Flzs A^i6 *RDL Dilatbd Method Rel Pnpand AnaIWd Bakh tut4lfsl
Volatile (kg lc Compoulds
v(,u Exlrafiron Fbld extracted
198
pg/kg d.y 102pqkS dry 2030
ldkS dry 1o2
fjdkS dry 1O2
ldksdry 1o2
lslkg dry 1o2pdkgdry 1o2
ugftsdry 1o2pSfl(g dry 203pdkgdry 1O2OpC4(S dry 1O2
!S/kS d.y 102p€lkgdry 102pdks dry 508
rdxsdry 102pdxs dry r02
ldxs dry m3
ldxS dry 1O2
!dlc! dry 2O3
!g/kg dry 102
t glS dry 1O2
!d*S dry 203
US/tg d.y 1O2pdfq dry 1o2
ldks dry 1O2
ldl(g dry 1o2
lgkS dry 102
t4k9 dry 102
ldkg dry 2O3
us/xg dry 1o2
US/kg d.y 1O2pdks dry 102pg/l(gdry 1o2
USI(S dry 1O2
UgL/kg dry 102
US/kS dry 1O2
udkgdry 1o2
us/rs dry 102pg/l(g dry 1O2
ldkgdry 102
ldko dry 1O2
$srkgdry 1OzpSJkAey 1020
ldkg dry 102
lSftsdry 102
udks d.y r02pdkgdry 1020pdks dry 10m
ugkgdry 1o2
26-Mar-07 26-t\rer{7 7(X]1584 BD
Volatile Orqanic Comoounds R05Prepared by method SW846 5030 Soil (high level)7G1$1 1.1,2-Tddrlorohifluoroethan€(FreoBRL67$+1 Ac€ione BRL107-13-1 Acrylonitrite BRL7143.2 Benzene ARl-100-86-1 Bromobstzene BRL7+97-5 Brcmochlorornethane BRL?'27-4 Brcmodichltrofiethane BRL75-2rz Bromotorm BRL74$3-9 Bomomethane BRL7&9+3 2.Butanone (MEK) BRL10+5i€ rFButylb€nzen€ BRL13t9eA sec.But!'ibenzen€ 8RL98-oe6 tert-BuMbonzen€ BRL75.1s-o Carbon disulnde BRL5&245 Carbon tebachlorid€ BRL10&907 Chlorobenzene BRL7fl1G3 CfiloroetMne BRL6756.3 Chloroform BRL74€7-3 Otlorom€thane BRL95-49{ z-Chloroiduene BRL10fi34 +Chlorotolu€ne BRL9&12{ 1,2€ibomo-3-dtloropropan€ BRL1?1-.1&1 Dibrornoohlorom€thane BRL1os$a 1,2-Dibromoehan6 (EDB) BRL7445.3 Dibromornelhane BRL95r5Gl i,2-Dichlorobenzene BRL541-73r t,3-Dichlorobenzene BRL1()6-45-7 |,4-Dichiorcbenzene BRLfar714 Dichlorodiouoromethane(Freon12)BRL75-34-3 l,l-Dicfiloroethano 8RLt07.06-2 1,2-Oicruo.oethane BRL?5-3+4 1,'t-Dichloroethene BRLi56-ss-2 crs-l:-Dichloroeth€ne BRL15{i€0-5 t?ns-1,2-Dicilorceth€ne BRL78{7'5 i,2-Dichlorcpropone BRL142-20-9 t,+Diailo.op.opade BRLs94-20.7 z,2-Dichloropmpane BRLs63-s8€ l,l{)icHoroprop€n€ BRL10061-01.5 cis-1,3-DichloropiJpene BRLl006142ibans-1,3-Oichtoropropene 8RLi0(}4l4 Ethyib€fEene BRL87{e3 tbxachb(oblt€dGn€ BRL591-7€{ 2-Hexanon€ (tlBK) BRL96-82+ lsopmpylbenzene gRL
S37{ 4-lsopropy'totuene BRL!634{4-1 Msthyl tert-tutyle$er BRLlostG1 +M€thyl-2-pentanon6(M|BK) BRL75{$2 tsl€dryl€no drloide BRL
505050
5050
5050
5050505050505050
50505050
5t)fl)50505050
5050
505050
50
505050505050
50505050
SW 846 S2608 27-[,lar{7 28+rar47 7031642 mer
91-203 i,bphthalene
Page 38 of | 65
Thii taboradq report is ,td volu ',irhotd u atrtodzsl sigt oure oa tk cot r pzge
' Repo.table Dercction Limit BRL = Bolow R€porti[g LiE r
Page 241
Samole IdentificationM8F-24 2'-4,
sA5964l-08
Client Proiect #301_88
MatrixSoil
Received
22-Mar-01Collection Date/Time
2l-Mar-O7 00:00
cAS No. Anahtc(s) Ft4S rRDL Dilarion Metj'od nel( Pryprren Ansbaed Balch Aralt't
Vohtile Orgrnlc Compounds
Volatile Orqanic ComooundsPrepared by melhod SW846 5030 Soit (high tevet)103{5.1 n-Propylb€nzene100-425 Styrcne63(!206 1,1,1,2_T€trachtoroethane79-3{_s 1 , 1 ,2,2-Totrachtoroethane127184 Tetrachloroethene10&84-3 Tolu€ne87515 1,2,3_Trichtorobenzene120'42-1 1,2,+JidtlorcbetEene71554 1 , t,.t _Trichtoroethane
794u5 I,1,2-Trichloroethane7941-6 Trichtofoethene
96,184 1,2,3_Tichtorcpropsne95€3'6 1,2,+TinrlethylLrenzEne10867-8 l,3,tTimethytbenzene75{r+ Vinylchloride133O-2C7 m,p_Xylene95-47S o-Xylene10s-9€-s Tetrahydrofuran@J-29-I Ethylether994{54 Tert-amytmethylether637-92 3 E$ryt tert-butyl ether10&20-3 Di-isopropytether7s-65-0 Te.t-gutanot/butylalcohol123-91-1 .l,4,Dioxane
Sufiogate recovedes:46A00-4 +Btomotluorobenzene
2037-26-s Toluene-da
1 t 060-014 1, 2Oic hlo@ethane-d4
1e6&5i-r Dibrcmofluorcmethane
Eft.rct ble P€troleum Hrdrocrrbons
Extractable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
€006{14 casoline6847e3O-2 Fuetoit#26447G31,3 FuetOit#464s53i04 Fuetoit#6M0980000q Motof oilJ00r00000 Aviatjon Fuel
Unidentified
Other Oil
Totet Pehoteum Hydrocarbons
C9-C36 Aliphatic tldrocarbons
Sdrogale rcco|€les;33eG$-2 l-Chloloocladecane
S€mivol{rik Orgrnic Compound$ by cC
Orqanochlorine Pesticides SW846 8081A
Preparcd by method SW846 3515A
309{G? Atdrin
BRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRL
BRLERLBRLSRLBRLBRLBRL8RLBRLBRLBRLBRLBRL
1021069697
BRL8RLBRL
BRLBRLBRL
Calculated as262262
125
Ig/tS drypdkS drypEr$ dry
Pq(g dry
!g/kg drypq/kg dry
!g/kg dry
)J9tK9 dry
!g/kg dry
lgkg drypdkg drypdkg dry
ugks drypdkg dry
!S/kq dry
us/ks dry
!g/kg dry
tiSi l(9 dry
9dkg dry
rrg/rQ dry
t g/rq d.ypg/kg drypdkg drypg/kg drypg/kg dry
102102102102
102102102102102't02
102102102102
102102203102102010210210210210202030
50
505050
5050505050
5050505030
5050505050505050505050
SW 846 82608 27-MBt47 2A-Mat47 7031642 mal
75€9_4 Trichlorotluoromethane(Freon.ll) BRL
70-130%7U130%70-130 %70-130%
mgL/kg dry
mgL/kg dry
mdkg dry
mdr€ dry
mgks dry
mgL/kg dry
mS/l€ dry
mg/kg dry
mgr'kg dry
mgr'kg dry
50.2
fi.2
f i 2
f i 2
502
fi.2
f i 2
50.2
50.2
50.2
+CT ETPH 27-Mat47 29.MarO7 7031590 DS
1G140 %
BRL pS/kg dry SW846 8081A 26+Iia(47 28-'./|,ar47 7031516 TG
Thit laborutory Epod k na. told wirhotr an authori.ad ignarare oa the cover page
r Reponabl€ Deta:iion Lim|t BRL: Below Reporting Limit Page 39 of 165
Page 242
Sample IdeotificationM6F-24 2,-4'sA5964l-08
ClientProi€ct #30t-88
MatrixSoil
Collection Date/Time2l-Ma.{7 00:00
Received22-MaF07
CAS No. Aaaltta(s) Floc UEIA .RDL Dihlina Method Retr, Prcpaed A^olfzed AoM ABalys,
S€mivolattle Orgrrlc Compornds by CC
Orqanochlorine Pesticides SW846 80814Prepared by mebod SW8,l6 354543i9-e4{ a_BHC319+5-7 b.BHC319-86{ d_BHC584$9 g-BHC (Undane)57-74-9 Chlotdane72-5,r{ 4,4.-DDD (p,C)72-5$e 4,4'-DOE (p,p.)50-2e-3 4,4'-DDT(p,p')60.57,1 Dieldrin95998{ Endocultan I3:121 345-9 Enclosulfan ll1031474 Enalosulfan SutFdte72-2t)i Endrin7421€34 EndrinAldehydet6.44€ HePtachlor724T5 Mettrorychlori024-s7.3 Heptachlof Epo de8001-3+2 Toxaphene510C-71-9 a-Chlo[dane5566-34-7 g-Chbrdane53494.70-5 Endrin Ketone
Sa/togale recovarrrss.'1038Gu-z 4,1-DB-OctatluotDbiphenyl (542051-2+3 Decachlotobiphenyt (St,Polvchlorinaled Biohenvls bv SW846 8082Prepared by method SW8,l6 35454t267+1r-2 PC81016111O1-n-2 PCB 1221r1141-16-5 rcB i232534€9?1-9 rcB t24212672-2e4 PQB 12481i097{e1 PCB .t254
110S82-5 PCB.t2503732+23-5 PCB 12621110Gi4-4 PCB 1268
Suftogale rEco!./€/res:I o3a6-o+z 4, 4O&OcIdfl @tobipheny' (Sr)ms1.2a3 bcechlotobiphenyt (Sr)
Senivolrt e Oigrrlc Cornpounds by CCMS
BRLgRL
SRL
BRLBRLBRLBRLBRLgRL
BRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL
69101
BRLBRIBRLBRLBRLBRLBRLBRfBRT
501n
BRLBRLBRLBRLARLBRLBRLBRL
Udks dry 8.0r
lSikS dry 8.01
lgrg dry 8.01
UC4(S dry 8.01
ldkS dry 40.0pSftg dry 8.01
rdkgdry 8.01pCftS dry 8.01pgrg dry 7.00
!d19 dry 8.01
ldkg dry 8.01pSI(' dry 8.01
ICitq dry 8.01
t dkg d.y 8.01
ldkg dry 8.01
!g/kg dry 8.0'l
tdkgdry 8.01pS/kS dry 40.0
tJg/kg dry E.Ol
FS/kgdrY 8O1
ldkS dry 8o1
3Gt 50 %3&150 %
pgkS dry 16.0pdkgdry t6-0
US/kS dry 16.0pdks dry 16.0
IgkSdry 16.0pqkg dry 16.0pdkS d.y 16.0
lS,lkS dry 16.0
ttglkedry 16.0
3A-150 %30-150 %
SW846 6m1A 26-[rar47 2&Mer47 7mi516 TG
SW84A 8082 26.|,,,a'4? 28\4ar47 7m1515 SM
SW846 8270C 27-l''a(47 27+nar47 7031592 ir.S
Semlvo|atils Oroanic Comoouods bv SW846 8270CPr€pared by method SW846 3545A&32-9 Ac€nsPhthene20+Fa Ac€naphtfil'l€ne€453-3 Adtin€12G12-7 Anth6csn€i912-24-9 Abazine10:l-3$3 AzobeozeneDlphenyldiazines2{7-5 Benzftlin€5O.5t3 Benzo (a) antftracene
pdksdry 374
Fgikg d.y 374pgkS dry 374
ldkgdry 374
udlqdry x74
ldks dry x74
t S/kg dry 374
USnlgdry 374
?hh laboruro,f ftport is naa yalid uAhaul sa atthadtad rlgddu.. od lhe cav6 poge.
'Reportable Detetion Limit BRL = B€low ReponidC Limit Page 40 of l6J
Page 243
Sample ldentificationMtF-24 2,-4'
sA5964l-08
Clielt Proiect #l 0 r -88
MatrixSoil
Collection Dale/Time2l-Mar-07 00:00
Received22-Mar07
CAS No- Analrte(s) FIag rRDL Dilutiort lwethod Rcl Prcpared Analwed Bateh A,alyst
Semivolstile Organic Conpolnds by GCMS
Somivolatile Oroanic Comoounds bv SWB46 8270CPrepar€d by method SW846 35454
50-32-8 Benzo (a) pyrene
20s,99,2 Benzo (b) {luoEnlhene191 2a-2 Benzo (g,h,i)peMene
207,06 9 Benzo (k) fluoranthene6535-0 Benzoic acid10051-0 Benzytetcohol111,91-1 Bis(2_chtoroethory)mebane111-144 Bis{2_chtoro€thyt)eflrer
39638,32,9 Bis(2_chtorotsopropyj)ether117'41'7 Bis(2-ehythexyt)phhatEte101-55-3 4-Bromophenyt phenytether
8548 7 Buty! b€nzyl phthalate86-74-8 C€rbazole5e-50-7 4.Chto.o-3-methytphenol10647,8 +Chloroaniline91-sa7 2-Chloronaphthalene95-s7-8 2.Chlorophenot70os-72-3 4-Chlorophenyl phenyt eth6r218{1-9 Chrysene
53-70-3 Abenzo (a,hl anthlacene132{4€ Dibenzofuran95-5Gl 1,z-Dichlorobenzene
t{r,731 1,}Dichlorobenzene
106.467 1,4-Dichtofobenzene
91-94-1 3,3--Dichlorobenzidine120€3-2 2,4.Dichlofoph€nol845F2 Diehylphthalate131 113 Dimef1yl phthalate
10s7-e 2,4-Oimethytphenolu-r4-2 Din-b'ltylphthalate
534-52-r 4,6-Oinfto-2-methytphenot
sl-28-5 2,4-Dinikophenol
121-14-2 2,4-Dinitrotoluene
60G20-2 2,G-Dinitrotoluene
117-84.0 Di-n-octylphthalale206-444 Fluoranlhene
86-73-7 Fluor€ne
118-741 Hexachlorobenzene
87€8-3 Hexachlorobutadiene
Tr4T4 Hexachlorocyclopentadiene
67-721 Hexachloroelhane
19+3S-5 Indeno (1,2,3-cd) pyrene
90-r2{ 1-Methyl€pha|atene?8-59-1 lsophorone
91-576 2-Methytnaphthat€n€
951+7 2-Methylphenol
10b-j94, 3,4-Me'l.\y'pher)ol105-4{,591-20-3 Naphthalene8a-74-4 2-Nihoanilines9{9-2 }NitrDaniline
SW846 8270C 27-Mat47 27+,/tal.O7 70315S2 M.BBRLBRL
BRL6RLBRL
BRLBRLBRLSRLSRLSRLSRLSRLBRLBRLBRL8RLBRL426BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRL771BRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRL
BRL8RLBRL
!g/kg dry 374
!g/kg dry 374
Ug/kS dry 374pS/kS dry 374
ldkS dry 374
UgkS dry 374
tSftS dry 374
udKg dry 374
!s/ks dry 374psfts dry 374
lgKs dry 374ps/Ks dry 374
usftg dry 374
ldkS dry 374
ldks dry 374
lgftg dry 374
!S/kg dry 374
!g/kg dry 374pS/kS dry 374pdkSdry 374
PdKS dry 374
ldKs dry 374
lSlqdry 374
!S/kg dry 374
!s/ks dry 374
!s/ks dry 374
ldkS dry 374pg/kS dry 374
ldkS dry 374
!S/kS dry 374
tqgdry 374
UdkS dry 374pdkS dry 374pSftg dry 374pSftg dry 374
ljg/rS dry 374
!g/Kg dry 374pSikg dry 374
US/kS dry 374pS/kgdry 374
lgil€dry 374
ug/kg dry 374pgkS dry 374
FykS dry 374
usftS dry 314
LrS/kgdry 374pSLSd,y 374
pS^S dry 374
Udkg dry 374pdks dry 371
Thit litoratury rcporl B t ot ialid wuho4t dn ozlhod?ad signatwe on thc caver Fage.'ReFxtable D€tection Limit BRL = Below Reponing Limit PEg€41 of l6J
Page 244
Sample IdentificatiouM8F-r4 2,-4.sA5964l-{}r
Clietrt Proi€ct #301-88
Mat ixSoil
Received22-Mat47
Coll€ctior DalelTime2l-Mr.47 00:00
CAS No. A"E+12(s) f,cscrt FI4S *RDL Dituion Method Retr. Pftpaed Ar,alyud Bdch Aizllsl
Semivol.lil€ Organlc Compo|rtr& by GCMS
Semivolatile Oroanic Cdnoounds bv SW846 8270CP.epared by merhod SW846 35454100{r€ +Nitroanillne98-!F3 NttrobefEen€86-75-5 2-Njtrophenoltoo42.7 +Nitrophenol62-7t9 N-Nitrosodirn€Etytamine621.6,1-7 N-Niiroscdi-rr-propylamine86.30€ N-Nitrosodiphenylarnin€87{65 Peotad oropt|gnol8s41{ Ph€nanlhEne
108-9s.2 Phenol
12s{0{ BnerE1i0.86-i tfidine120{21 1,2,+Trichlorobenzene
9$95-1 2,4,$Trichlooph€nol
88{€F2 2,4,&Trichlorophenot
S.fiogafe €couenbs.'
321a0a z-Ftudobiphenyl
SW846 4270C 27-Mar47 27.to1ar47 703153? M,BSRLBRLBRLARLBRLBRLBRLBRLBRLBRL705BRL8RL8RLBRL
68
0 .115
BRL
4 . t 1
34.9
0_701
44.9
22.O
BRL
67.0
Ugkgdry 1f,0O
!S/kS dry 374
tg/kg dry 374
!el(S dry 15(mydks dry 374
ldkS dry 374
!c/&s dry 374
ldkSdry 374
udlgdry 374
ldkS dry 374
ldkg dry 374pCikgdrv 374pqtg dry 374
lElgdry 374
!S/kS dry 374
3L130 %15-110 %30-130 %15.r10%
m-1n%1'-nO%
ftig/kg dry 0.043{
mqr'kg dry 1.36
mgr'kg dry 2.M
nE/kS dry 0.680
mdkS dry 0.340
nVkS dry 0.680
n€/tg dry 1O2
mg/kg dry 2.O4
mgI 0.02m
nrdl 0.0150
mgil 0.0150
nE,n 0.m25
n'gn 0.0150
mgl 0.mo1t0
mg/l O,015O
rrgrl 0.0150
%
I EPA 200.7
1 '
1 '
l '
1 '
1 sw8rl6 1312rr470A
1 SW€461312/60108
2A-Matr-O7 n+llat47 7031494 RM
2&Msr{7 7031652 YP
2Stlar{7 7ct166l HB
?67-124 2-Fluoropt6nol 551165404 Nihobenzene4s 63116542 2 Phenolds 561718-514 Tefpllenyldl4 77tte7 z,4,fiTtibft/'tophenol 67
Totrl Meti6 by f,PA 6lXXy7000 S€ries Methodt
74394?.6 Merqlry
Totel M€trb by EPA 200 S€ries Methods
7140-U4 Silvel
742{l-38.2 Arsenic
744S393 Baaium
7{4l).4}9 Cadmium
7,trO.47-3 Clromium
743s-9?.1 Le€d
7?82-4+2 Selenium
SW846 7471A 2&Mar-07 28-tuar{7 70314S5 YP
SPLP Mearlr by EPA t3 l2 & 60fiy?000 sed.s M€tiods
SPLP Exbacton Co,ndetod
z!r.o-2?-1 situer BRL
7!lo-3+2 AFenic BRL
7,t40-3+3 Barium 0.0300
74a04$9 c€dmium BRL
7t140.17-3 Chrcmium SRL
743$97€ Merdrry BRL
74S-92.r Le€d BRL
7782-4+2 Selenium BRL
G€||eid Chembtry P|r.mcter!
I 5r,/\/8161312 2SMEr{? 2GMar-07 7031560 AD
I Sl/V8461312/60108 2&Mrr.07 28-lrer-07 7031651 HB
1 '
1 '
1 "
'1 SM2540 G Mod. 24-l'iar47 24,llne'-07 7031470 OP% Solids
Page 42 of t65
TNlt labonlory rqod * aot valid n'Lhout oE aartodzod signauft od rte aover pago-
* Reponsble D€tectioo Limir BRL = Below Rcporring Limit
Page 245
Sample IdentificationMEF-25 2,-4'sA59641-09
Client Proiect #l 0 l - 88
MatrixSoil
Collection Date/Time2l-Mar-07 00:00
Receivcd22-Mar-07
CAS No- Anallte(s) Units *RDL Dilution Merhod Rel Ptepaftd Aruryzed Botch ,4mlpt
Volatile Organlc Compounds
vOC Extraction
pg/kg dry 6.3
Pgkg dry 127
US/kS dry 6.3
USAS dry 6.3
!g/kg dry 6.3
ldkS dry 6.3
Udkg dry 6.3
tiS^q dry 6.3
lEkS dry 12.1
ldkS dry 63.4
!g/kg dry 6.3ps/kg dry 6 3
liS/kg dry 6.3pgkS dry 31.1pg/kS dry 6.3pg/kg dry 6.3
LrgkS dry 12.1pdkS dry 6.3pg&S dry 12.7
lSftS dry 6.3pqkS dry 6.3
l.rdkg dry 12.7
ldkS dry 6 3pdkS dry 6.3
!g/kg dry 6 3
Lig/kg dry 6 3
ldks dry 6.3
ldks d.y 6.3
ldks dry 12.7
lgkg dry 6.3
UdkS dry 6.3pgkg dry 6.3
Pgkg dry 6.3
lgkS dry 6.3
PdkSdry 6.3
ldkS dry 6.3
lgkS dry 6.3pdkg dry 6.3pqkS dry 6.3
lgks dry 6.3pdlqd.y 6.3
!S&S dry 6.3pg'l(gdry 63.4pdkS dry 6.3pdks dry 6.3pdks dry 6-3pdksdty 634
ldkS dry 63.4
!S/kS dry 6.3
26-Mar-07 m.tlar{7 7031584 BDField extractedVolatile Orqanic Comrounds
Prepared by melhod SW846 5030A Soit (tow tevet)76-13-1 1,1,2-Trichtorotrinuoroethane (Freo€RL6744-1 Acetone aRL107-13,1 Acrylonitdte BRL714+2 Benzene BRL10&€e1 Brodrobenzen€ BRL74-97-5 Bromochloromethane BRL15-274 Bromodichtoromethane BRL75-212 Eromoform BRL7.1€3-9 Bromomethane BRL7s-e!3 2-Butanone (MEK) BRL104-514 n-Bltylbenzene BRL13t98-8 sec-Butytbenzen€ BRL9846+ tert-Butylbenzene BRL75-15-0 Carbon disulfide BRL56-23-5 Carbon tetrachloride BRL108-90-7 Chlorobenzene BRL7540-3 Chtoroethane BRL67$6-3 Chloroform aRL7447-3 Chlororhethane aRL9549-8 2-Chtorototu€ne BRL106-434 +Chtorotdu€ne BRL96-12J 1,2-Dibomo-3_chlorcpropane BRL124-1€-1 Dibromochloromethene BRL106 934 1,2-Dibromoethane (EDB) BRL7,1-9t3 DbromorDethane BRL9s'sG1 I,2-Dichtorobenzene BRL541-73-1 l,3-Dichlorobenzene BRL106-16-7 l,4-Dichtofobenzene BRL75 7 1-e Dichlorodinuoromethane (Freoni2) BRL7s-34 3 l,t-Dichtofoethane BRL107-06.2 l,2.Dichtofoethane BRL7s-35-4 1,1-Oichto.o€thene BRL156-59-2 cis-i,2-Dichloroettiene BRL15ffi0'5 trans-1,2-Dichloroethene BRL70{7-5 1,2-Dichloropropane BRL142-28€ l,lDichloropropane BRf5942G7 2,2-Dichlorcpropan€ BRL56$50{ 1,l-Dichloroprop€n€ BRL100€1{1-s cis.t,3-Dichloropmpene BRL10061{25fans.l,}Dichlorcpropene BRL10c.114 Ethylbenzene BRL07€8-3 Hexachlorobutadiene BRL5e1,70{ z-H€xanone ([,,!BK) BRL9442{ lsopropylbenzene BRL9947€ +lsopropyltoluene BRL163.1{.1-1 Methyllod-buty'ethor SRL1D+t0-1 4-Metllyt-2-pentanon€(M|BK) ARL7S0S2 Methylene chloride BRL
I
1
1
1
1
1
1
1
1
1
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I
1
1
1
1
1
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1
1
1
1
1
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1
1
1
1
1
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SW 846 82600 27-Mat47 2a-Mar07 7031658 RLJ
91-207 Naphthalene
Page 43 of 165
Thi, bbonlory nporl is ^ot vau x,ithou al aatlrodzed signatarc on the cot er page .
{ Reporirble l)etection Limit BRL = Bclow R€poning Limir
Page 246
Sample ldentificationMEF-25 2'-4'sA5964l-09
Clieflt Proiect #l0l-88
MatrixSoil
Colleclion Date/Time2 I -Mar-07 00:00
Received22-Mar-Oj
CAS No- Amlyte(s) FIzg 'RDL Dilutio.' Method Retr. Prcporcd AEaIwn Barh Andllst
Volrtile O.grnic Compoundt
Volatile Oroanic ComgoundsPr€pared by method SW846 50354 Soil (low bvet)
7569-4 Trichloronuoromehane (Fr€on ll) BRL
103-61 n-Prcpylbenzene10tl-42-5 Styrene630-20{ '1, | ,1,2-Totracl toro€thane
79-34-5 1,1,2,2-Totrachloro€lhane
12H8-1 Tehadlloroetlrene
108i83 Toluene
87{1{ 1,2,}Tridllorobenz€ne
12G82-l 1,2,4-Tdd o@benz€ne71{5{ 1,1,l-Trichloro€hane
79{ l }51, I ,2-Tr i* l toroethane
79{1S Tdchlo.o€th€ne
96-18-4 1.2,$Trictllorcpropan6
9gt€3{ ,|,2,4-Tdmethylbenzene
1085/{ 1,3,5-Trimethylbenzen675{r-4 Vinylchlo.ide1330-?07 m,p-Xyiene9547{ +Xylene109.!19-9 Tetahydrcfuran
6G297 Ethyl ethef9s4{s€ Tert-amy'methyletfEr637-12{ Ethy t6rt+utr.t ether108-20'3 Di.isopropyt€ther75{5-0 Tert€obnol/ butyl alcohol123-91 -1 'l
,4.{)ioxan€
Sutugate rccoldrias:46040-4 +B@ntofluotobenzene
m37-26-S Toluene4S
1 7 060474 1,2-Dichlotoethane44
186&5?7 Nbrcmofluoronelhene
Exlrrctrble Peftoleum Hyd.oc$bons
Ext.ac'table Total Petroleum Hvdrocarbons
Pr€pa.ed by method SW846 35508
800661-9 Gasoline6&tF30-2 Fuel Oil #2684743r-3 FuelOitt 4
6e5s90{}a Fud Oil #5M6doo{D0 Moto!. OlJ0O10O00O Aviation Fu€{
Unidentifed
O{h€. Oil
Total P€0oleurn Hydrocadons
C!€36 Aliphatic Hydrocarbons
Sunogts{e a9co!4er*es.'33E633-2 l-Chloroochdecane
Senlvolotil€ Orgulc Compoutrd! by CC
Orqanoctrlo.ine Pesticides SW846 8081A
P.epar€d by rnethod SW846 3545A
3O9-O0-2 Atdrio
SW 8{6 S260S 27-[,tar47 28{r,1a.47 Zm165a RllBRLBRLBRLBRLBRL8RLBRI-BRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLgRL
88
97
BRLBRLBRLBRLCalculat€d asBRL206BRL206206
t0()
USASd,y 63pgr(g d.y 6.3
ldkSdry 63
ldkS dry 6.3
!s/kS dry 6.3pSn(S dry 6.3pSI€dry 6.3
US/tg d.y 6 3pdks dry 6.3pdks dry 6.3
UgI(S dry 6.3
t'Stkgdty 6.3
tlgJksdry 6.3pgrsdry 6.3
ldks dry 6,3prytS dry 6.3
!g/xS dry 12.7
Lrdkg dry 6.3
UgJkAdry 63.4ydkS dry 6.3
$ikg dry 6.3
!S/kS d.y 6-3pdksdry 6.3
ldksdry 63.4
|]g/kS dry 12f
7L130 %7G130 %70-130 %70-130 %
rEL/kg dry 34,4mg/l!gdry 34.4mdkg dry Y.4nE/kq d.y U.4rvlg dry u.4ndkS dry 34.4mdkS dry 34.4mdfQ dry 34.4mg/kg dry 34.4rng/kS dry 34.4
'40-140 %
+cT ETPH 2t4 at47 29+nt47 703159/)
ngtg dry SW8,$ 8m1A 2&lle.O7 28-l!lar47 7031516 TG
Tttit lshoaldrf ,epod is not vU without zi althodu.I slgrratare ol lhc cover pag.-
' RQortabl€ Det€ctiotr Limit BRL = Below Repqiing Limir Page ,14 of | 65
Page 247
Samplo IdentificationMEF-25 2',-4'
sA5964l-09
Clent Proiect #301 -88
MatrixSoil
Received22-Mar-07
Collection Date/Time2l-Mar-07 00:00
CAS No, Anabre$) Resalt Fl"s Units *RDL Dilution Method Retr. Prcparcd Anaryzed Bakh AnaIJst
Semivolrtile Orgatric Compourd3 by CC
Orqanochlorino Peslicides SW846 8081A
Prepared by rn€lhod SW846 3545A
319-84{ a-BHC319{s-7 b-BHC31s6-6 d-BHC5s4+e g-8HC (Lindane)
5J-749 Chlordane72-s-a 4,4'.DDD (p,p')
72-55-e 4,4,.DDE(p,p,)
50-2s-3 4,4,-DDT(p,p.)€0-57-T Dielddn959-96{ Endosulfan I33213-65-9 Endosulfan ll1031{7,8 Endosulfan sulfate72-2O-A Endrin7421-93-4 EndrinAtdehyde76-44.8 Heptachlorr243-E Methorychtor1024-57-3 tleptachlor Epoxide8001-35-2 Toxaphene5103-71-9 a-Chlordane556€-34-7 g.Chlo.dane
53494-70-5 Endfin Ketone
Surogalg rccovedes:1N8Ge+2 4,+DB-Octafl uorobiphenyl (54
N51-2+3 Decachlorobiphenyl (St)
Polvchlorinated Biohenvls bv SW846 8082
Prepared by melhod SW846 3545A
12674 11 2 PCB 10t611to+28-2 PCB 122111141-16-s PCB 12325346s21-s PCB 124212672-?9{' PCB 12481r0s75e-1 PCB 1254110€6{2-5 PCB 126037324-23-5 PCB 12162ir100-14-4 PCB .1268
Sunogale Ecowries:fl 38 e, 84 -2 4, 4 - D &Oc I afl Llo rob i p he n yt ( Si
205 t-2+3 Decachlo.o b ip hen yl (Si
Semlvotalile Organic C0mpounds by CCMS
BRLBRLBRL8RLBRLBRLBRLARLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRL8RL
6876
8RLBRLBRLBRLBRLBRL25.98RLBRL
4570
8RLBRLBRL597BRLBRLBRL946
!g/kg dry 6.65
tig/kg dry 6 65pg/kg dry 6.65
!g/kg dry 6.65
!g/kS dry 33.3
!g/kg dry 6.65
ldkS dry 6.65pg/kS dry 6.65pgftS dry 6.65pdkg dry 6.65pS4<S dry 6.65pSftS dry 6 65
!g|4(g dry 6 65pSftS dry 6.65pS/kS dry 6.65pg/kg dry 6.65pglLg dry 6.65
!g/kg dry 33.3
!g/kg dry 6.65
!g/kg dry 6-65
!q/kg dry 6.65
30-15, %m,t50 %
pg/kg dry 13 3
!g/kg dry 13 3pg/kg dry 13 3
ldkS dry '13 3
!g/kg dry 13-3
!g/kg dry 13 3
!g/kg dry 13 3
ldkS dry 13 3
!q/kg dry l3-3
n-|50 %30-150%
iJdkgdry 4?7
pglgdry 427
pdkS dry 42f
UdkS dry 427
UgkS dry 127
UgkS dry 427
IdkS dry 427
Ug/kS dry 427
1
1'|
i
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1
1
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1
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SW846 8081A 26-MaF07 28{,lar-07 7031516 TG
SW846 8082 2€-Mar47 28jv1ar-07 7031515 SM
Semivolatile Orqanic Comoounds bv SW846 8270CPrepared by method SW846 3545A83-32-9 Acenaphthene20FS€-€ Acenaphthylene62-s3-3 Anitine12e12-7 Anthrac€ne1912.2+9 At?ine103-33'3 Azobenzene/Diphenyldiazine92{7-5 Benzjdjoe56-55-3 B€nuo (a) anthrac€ne
SW846 8270C 274lar17 27+,/ta?07 7031592 M.B
Thk bboratory npoq is not vaIA dfiotl an d..thorizli slgaatarc o^ the cwer pqe .
' Reportable Detection Limit BRL = B€low Reporting Limit Page 45 of 165
Page 248
Sample IdadtificationM8F-25 2'{,s45964149
Clietrt Proje€l #301-88
Collection Date./Time2l-Mar47 00:00
MatrixSoil
Received22-MaF01
CAS Na AM+k(s) Flig *RDL Dltution LLthod Ret Ptepared Anzlraetr Batch Anzfi*
Semlvoletile Org.dc Compounds by CCMS
S€mivolalilo Oaqanic Comlounds bv SW846 8270C
Prepared by rnethod SW846 3tl5A
50-32+ Bonzo (a) pyrene2otss'2 B€nzo (b) fiuorandreoeis1-242 Bcnzo (g,h,D peryle|]e20ru&9 Benzo (k) nuorsnthene65€fi Benzoic acjd10G51{ Benzy'l alcohol111-el-r Bis(2rhlom€thory)methane111-444 Bis(2{hloro€thyt)efier3963S32-s Bis(2dltoroisopfopyl)eheri17{1-7 Bis(2-ehyllr€xyt)phttEtate101-5+3 +Bromophenylphenylefiea85{s7 Auty,l b€nzyl phthatatie86-74{ Csfbazole5950-7 rlchbo-3-methylph€flol1&7{ 4-Chlo|oanilino91i$7 2-Chtoronaphhalen€9t57{ 2-Chlorophenol2005.72-3 +Chlorophenyl D,tletrlyl eiher218-th-9 Chrys€n€53-70-3 Dibenzo (a,h) snthracene1326+9 Dibenzofurei95-5G1 l,z-Dichlorobenzene541-73-1 1,3-Oichlorcbefizene10Sa&7 1,4-Dicidoobenzen€9l€{-1 3,3lDichlorobenzidine12G83'2 2,4-Dichlo1.ophenol84{62 Di€tlyl phttEtater31r1-3 Dimeflryl pht€tate105i7-9 2!4-Dimefiy,tphenolu-74-2 Di-n-butylphthalate$a-52r 4,6-Oinito-2-methylphefiols1 .2$s 2+Oinitrophondt2i-14-2 2,+Oinilro{oluene606.4)-2 2.GDinitrototuene117{4{ Di{.oclylphtnatatea)8-14-O FluorEnt1enefr-7r7 Fluorene1i&74_l Hexadrlorcbenzen€876€_3 Hexac-hlorobutradrenen174 Hexadiorocydopsntadiene67.72-1 HexeChloroefEne193-3$5 Indeno (1.2,3-cd) pyrene9012{ l-ilethy'naphthal€ne7&5$1 lsophoron€91'57{ 2-Metrylnaphoratenee5-4e7 2-trtethylph€nol10&3s-4, 3,4-tet|ylphonol10€-zK'591-zl3 Naphb\Elene
E-7,4 2-Nitroaniline
99{92 }Niuoanilin€
Sw846 0270C 27llt?{47 27-Mat-07 7031592 M.B9829804838mBRLBRLBRLBRLBRL8RLBRLBRLBRLBRL8RLBRL
BRLBRL't, t80BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL2,3fiBRLBRLBRLBRLBRL433BRLBRLBRLBRLBRL
BRLSRLBRL
VglxSdry 427
Pslts d.y 427pEtgdry 427
lg,fl€ dry 427pg4qdry 427
Udl€ dry 427
UgkSdry 427pS/kS dry 427pdks dry 427pS/kSdry 427pS4(S dry 427pdrs dry 427pdrgdry 427pdtsdry 427
UdkS dry 427
uglksdry 427pdks dry 127pdrgdry 12]
lgikSdry 427pdl(lgdry 427pdkg dry 427pdkSdry 427
Ugn(S dry 427
!S/kS dry 427
ttdV,Sdry 427
UdkS dry 127
rrykg dry 41
l4/kS dry 427
u/rSdry 427pdks dry 427pdks dry 427
ldko dry 427
ldkS dry 42r
!S/lq dry 427
US/kS dry 127psfts dry 127
lJg/ks dry 427
ldks dry 427
rdts d.y 427pdko dry 427
ldkgdry 427
!Sn(S dry 427
ldkS dry 427
ISftg dry 127
ldlg dry 127
lgl(g dry 427
Idkgdry 427
ydkg d.y 427pdks dry 427
rdkgdry 427
This ,4.hralory rcpad h not eaIU x,irhoat tE aantoriet dgao&,rc on the cote. pqE-
' Reportable Det€ction Umit 8RI = Below R€porti.g Limit Page 46 of 165
Page 249
Sample ldentificatia.nM8F.2s 2'-4,sA5964 | -09
Client Proiect #301-88
MatrixSoil
Received
22-Mar-01ColLection Date/Time
2l-Mar-07 00:00
CAS No. Arra4te(s) Resun Ftzg Unia +RDL Dilation Merhod Rel. Prcpand Anaqed Batch AMb\t
S€mivolatile Orgsnic Compourds by GCMS
Semivolatile Oroanic Comoounds bv SW846 B27OCPrepared by method SW846 3545A
100-01-6 4-Nilroaniline98-95,3 Nikobenzene
88-75-5 2-Nitrcphenol10G02-7 4-Nitrophenol62-75-9 N-NitrosodiaEthylamine621+-7 N.Nitro6odi-n-propylamine06-30-6 N-Nitrosodiphehylamine07-€G5 Penlachtorophenol8541-8 Phenanlhrene10&9t2 Phenol1?9-00-0 P,rene11G86-1 Pyridine12G€2r 1,2,4-Trichtorobenzene95-95-4 2,4,5-Tdchlorophenol88-06-2 2,4,6-Trichlorophenol
Sunogale rccovedes:3?1'60-o 2-Fluorohiphenyl
36/-124 2-Fluorophenol
SW846 S270C 27-Mat47 27-Mat47 7031592 M.BBRLBRLBRLBRLBRLBRLBRLBRL942
BRL2,360BRLBRLARLARL
6761
o.747
BRL
10.7
1 M
3.47
12.4
247
BRL
lSikS dry 1710
rlglkg dry 427pg/kg dry 427
!S/kS dry 1710pg/kg dry 427
ldks dry 427pdkS dry 427
lSftSdry 427
!g/kg dry 427
!g/kg d.y 427pdxgdry 427pgkg dry 427
lrg/Kg dry 427
USIkS dry 427
ldkS dry 427
30"130%15^110 %30-130 0/o
1U t10 %301m %1u l10 %
mS!4q dry 0-0352
rnS/kS dry 1.04
rnSikg dry 1.56
mg/kg dry 0 518
mg/kg dry 0.259
mdkS dry 0.518
mg/kg dry 0;l7S
mdksdry 1.56
mg,4 0.0200
nen 0.0150
rng/| 0.0150
mgn 0.0025
nEI 0.0150
nun 0.OO04O
mSI 0.0150
mg/l 0.0150
1
1
1
1,1
,1
1,l
1
1
1
1
1
1
1
4165404 Nitrcbenzene4s 64416542-2 Phenol4S 5617ft.514 Teryhenyl4ll ts118-7e.6 2,4,6-Tdbrcmophend 67
Totrl Merrls by EPA 6000/7000 Series M€thods
743+975 Mercury
Toral Metrh by 8PA 200 S€ries Methods
7440-22-4 Silver
74!0-38 2 AJ.SenaC
7440-39-3 Barjum
744043-9 Ce(lmium
74,10-47-3 Chromium
7439-92-1 Lead
?74249-2 selenium
SW846 74714 28-Mar-07 28-t.,laF07 7031495 YP
EPA 200 / 28-Mar-07 28.Ma.0/ /031494 RM
SPLP Mctels by EPA 1312 & 6000/7000 Srri€s Methods
SPLP Extraction completed
7440-22-4 SiMer BRL
7440,3&2 Arsenic 8RL
7.440,3+3 Eadum 0.0362
7440-43-9 Cadmium BRL
74.10-47-3 Chrcmium BRL
7439-974 Metcury BRL
7439-92-1 Lead 0.0230
7782-49-2 Selenium BRL
G€mr|l Chemistry Parlmet€rt
% Sol ids u.2
1 SW8461312 26-Mar47 2SMar{7 7031560
I SW8461312/60108 28-Mer{7 28]\4ar-077031651
t '
1 "
1 '
1 SWU6131Z747OA ' EMaLD7 7031652
1 SW846131260104 ' 2&Mar.07 7031651
1 '
8D
H B
H B
1 SM254O G Mod. 24.Mar47 24-Mer1f 7A31474 QP
This labontory rcporl k not ralid Hilhou sn oalhoi.el signawe on the coyer poge.
a Reportable Detectioo Limit BRJ- = Below Reporting Limir Pige 47 of t65
Page 251
Sample ldentificationM8F.26 2-4'sA595l7-06
Clicnt Proiect #30t -88
MatrixSoil
Received
20-Mar-07Collection Date/Time
l9-Mar-07 00:00
CAS No- Aao+t4s) Floc *RDL Dilation MetAod Retr. Prepted Analyzed Batch Atullsl
Volatile Orgrtric Compounds
VOC Extraction
US/kS dry 7.6
!g/kg dry 152
us/kg dry 7.6pfudry 7.6ps/ks dry 7.6
trs/ks dry 7.6ps/ks dry 7.6
!s/ko dry 7.6
!g/kg dry 15.2
!s/ks dry 74.2
PqxSdry 7-6
!g/kS dry 7-6pgkg dry 7.6
sdkS dry 38.1
US/kS dry 7.6
us/ks dry 7 6
rcAS dry 15.2pg,tkS dry 7.6
UdkS dry 15.2
[dkS dry 7.6
IS/kS dry 7 6
!S/kg dry 15.2
ldkS dry 7.6
FS/kS dry 7 6
ttgtkSdry 7-6
ts/ks dry 7 6
tS/kS dry 7.6
UdkS dry 7.6pg/kg dry 15.2
IS/kg dry 7.6pS/kS dry 7.6
f.rglkg dry 7.6
t4/kg dry 7.6
trg/kg dry 7 6
trg/kg dry 7-6
!g/kg dry 7 6
ldkS dry 7-a
FS/kS dry 7-6
lS/kS dry 7.6
!S/kS dry 7-6
!g/kg dry 1.6
!S/tS dry 1.6
liS/kg dry 16 2
trSlqdry 7.6
ldkS dry 7.6
lgkS dry 7.6pqkS dry 76.2
Fg (g dry 76.2pg4qdry 7.6
21-Ma.-O7 21-MarD7 7031261 8DField extract€dVolalile Oroanic Comoounds
Prepared by method SW846 50354 Soit (tow tevet)
76 111 1,1,z-Trichlorotriiuoroethane (Fr€o8RL674+1 Acetone 8RL107-13,1 Acr-t{onitdle aRLf11r2 Benzene BRL100-86-1 Bromobenzene 8RL74,97-5 Bromochloromethan€ aRLT5-274 Bromodichlorcmethane BRL75-212 Bromoform BRL71419 Bromomethane BRL7e-$,3 2-Buhnone (MEK) BRL10+514 n8utylben?ene 8RL13+98{ seeButylbenzene BRL9A-06,6 tert-Butylbenzene BRL75,15'0 Carbon disulfide BRL56.23,5 Carbon tetrachloride BRL10&90-7 Chtofobenzene BRL75{0-3 Chloroethane BRL67{6"x Ch/orofom BRL74-47-3 Chloromethane BRL95-4!l-8 2-Chlorotoluene SRL10H3-4 4-Chloroioluene BRL9€'12_8 1,2-Dibfomo-3rhloropropane 8RL12qS-1 Dibromochloaomethane BRL106-93-4 1,2-Dibromoethane(EDB) BRL74-913 Dibfomomethane BRL95 so,r 1.Z-Dichlorobenzene BRL541 731 1,3-Dichlorobenzene BRL106,46-7 1,4-Dichtorob€nzene BRL15.71-8 Dichlorodiiuorcmethane(Freon12)BRL75-34 3 l,l-Dichloroethane BRL107-06-2 1,2_Dichloro€thane BRL75-s5-4 l,l.Oichtoroeihene BRL1s+s9 2 cis- 1 ,2_Dichtorcedrene BRLlsffio-s taans-1,2-Dichloroethene BRL7a€7-s 'l,2.Oichto.opropane BRL142-28-9 l,3-Dichlorcpropane BRL594-20-7 2.2-Dichtoroprcp€ne BRLr,615€5 .1,1-Oachtoropiop6ne SRL10061111-5 cis-1.!0rchtoropropene BRL10(}6142€ trans- 1 ,3_Oichtoropropene BRL1{n-41-4 Ethytbehzen€ BRL87{&3 Hexachlorobutradiene BRL5e1.784 z-Hexanone (MBK) BRL9a{2€ lsopropy'benzene BRL99€7{ +lsoprapyholuene 8RL1634{4-4 Melhyltert-butytether 8RL10&10-1 4-Methy'i-2,penlanone(MIBK) BRL75-0s2 Methytene chtodde BRL
SW E46 82608 22-MarOI 23-Ma.-07 7031335 RLJ
91-201 Naphthalene
Prge 27 ofl24
This laborutory repo4 is nol ualii Nllhod aa a ho.lzed s@au!rc on tfu cover ptge.
' R?dta)le Dete{tion Limit BRL = Below Replrrin8 Limir
Page 252
Sa8|Dle IdeltificationMAF-16 24'sA5951746
Clied Proiect #301-88
MafixSoil
Collection Dat€/TimeI 9-Mar{7 00:00
Received2GMar-07
CAS No- Adabte(s) Reast Flog Uai6 *RDL Diladoa Llethod Rcl. PEparcd ,ltulfzci Bqlch Ad4lfsl
Vohaile Orgrnic Compoudr
Volalile Omanic ComooundsPrepared by method SW8il6 50354 Sdl (low level)10+65-l n-Propy'lbenzene BRL1qr-42-5 Styrene BRIdrG20€ '1,t,1,2-T€trachloro€thane BRL7+34.s 1,I ,2,2,Tetrachlorffthane BRL127-18-l T€lrachloroethene BRL10&84€ Toluene BRL07{14 !,2.}Tridrtorobenzen€ BRL12G82n i,2,+Trichlorobonzene BRI7i{5-6 1,1,1-Tri{*llorcethans BRL79{G5 1,1,2-Trichloroethane BRL79-01i Trichloroethene BRL75{9-4 Trichlorofiuoromethane (Freon 11) BRLs+1e-j 1,2,&Tri€hlorooropane BRL95-634 1,2,+Trimethylbenzene BRL108-67{ 1.3,5-Trimeh},lbonzene 8RLf5414 Mnyl cikrider330-2{L7 m,p-Xylen€95-47-0 G.Xylenet0$999 T€hahydrofu€n*29.7 Ed1yt ettler994-oS Tert-€nryl mothy'l elher637s2-3 Edlyltert+ulylefllerr0e20.3 Di-isopfopyleth€r7$6+0 Tert-Butanot / but/l alcoholr2+9u 1,+Dioxene
Su,firogale rEcorrsnes:4tt04o2t 4lkomofluotubenzenee37-2A-5 Toluene4St/o6o474 r,2alchloroelhane441868-$-7 Ahrqnonuorcmethane
Ertrrctrble Petroleflm Hydrocrrbons
Extradabl€ Tolal P€troleum Hvdroca.bonsP'epared bV melhod SW846 354548O0O€1€ Gasolin€68a7+.3tl2 Fu€l Oil #26447+31J Fuel Oil #:4685s+oc{ Fu€l Oil #6rnem$oo Motof OlJoolooooo Aviaton Fuel
Unldenttf€dOttFr Oil
BRLBRL8RLBRLBRLBRLBRIBRLBR!BRL
101118102
Sw 846 82608 n4ht47 &Me(47 7031335 RU
+cT ETPH z.-|,tl€,t-O7 m^tat4I 7031284 DS
usrkg dry 7.6pglkgdry 7.6
ldkS dry 7.6
wlkgdry 7.6
tdkg dry 7.6
rdkg dry 7.a
$dkSdry 7.6
USikg dry 7.6pcrks dry 7.6
Ugkg dry 7.6
USI(S dry 7.6
tNu,S dry 7.6pdkq dry 7.a
lSikS dry 7.6p*s drY 7.6
lqkg dry 7.6
Itgkgdty 15.2
ldkg dry 7.6pdkSdry 76.2
ugkSdry 7.6
ldkg dry 7.6
lgtg dry 7.6
ldkg dry 7.6
!S/kS dry 16.2pSI(S dry 152
70-130%7L130 %7G130 %70-130 %
TotalPebdeumHydrocarbons 404C$C36 Aliphatic Hydro@bons rl()4
BRI-BRLER!BRL
BRLBRL4UCalcllat€d as
nvl€ dry t37n€/kg dry 137mg/kgdry 137nEr'kq dry 137rEngd.y 137mgdfo dry 137mdkSffy 137n€/*g dry 137mgikg dry 137nE/kg dry 137
10-140 %
5
5
sal.'ogatc aEoor€rie&_t3€Ga?-2, -Chlorooctdecarg
Scmlvol{tile Orgrtric Compoun& by cCOroanochlorine Peslicldes SW846 8081APrepared by method SW846 355083Oe-0+2 Atdrin trdks dry 7 .Os SW846 e0€1A ?2-Mato7 27-Met47 7mi275 TG
Thit brororary rcpod ls not eeli.l withos! an aud.o;aed signarw on the colv 4rye.. Reportnbb f,retection Limit BRI- = B€low Reporting Lnnit PryEzA ot 124
Page 253
Sarnple IdentificationM8F-26 24'sAs95l7-06
Client Proiect #301-88
MaEixSoil
Collection Date,Tirnel9-Mar-07 00:00
Received
Z0-Ma(0'7
CAS No. Anabtz(s) Fl"S Unils *RDL Dila.aon Method Ref Prcpored Anauzed Barch AnaUst
Semivolrttle Organic Compoutrds by cC
Oroanochlonhe Pestrbides SW846 SOglAPrepared by merhod SW846 35508
319€a{ a-BHC
31$85-7 b-BHC319{6{ d-BHCs8-€se g!8HC (Undane)
5T-74-9 Chlordanerz-*a 4,4-DDD (p,C)72-5te 4,4-DDE (p,p')50 2+3 4,4-DDT (p,p.)60.s7,1 Oielddn95+98-8 Endosulbn I33213.6s-9 Endosuthfl ll1031-07-8 EndosulfansutfateI2-2O-A Endrin7421-eH EndrinAjdehyde76-44-8 Heptachtor124+5 Methoxychlor10?4-57-3 Heptachlof Epoxide8001-35-2 Toxaphene5103-71,9 a{hlordane5566,34-7 g-Cl o.dane53494-70-5 Endrin Ketone
Sufiogale rccoveies:10i8$8+2 44-DB-Octafluorobiphenyt (St)
2051 -2+i Decachlotubiphenyl (Sr)
Polvchlo.inated Biohenvls bv SW846 BOB2Prepared by method SW846 35508
1267411,2 PCB 101611to+28-2 PCB 1221ir141-1c5 PC8 12325346+21-s PC8 124212672-m4 PCB 124811097{S1 PCB 1254110€tr2'5 PCB 1 2603f32+23-5 PCB 12621110G144 PCB 1268
Suaogale rBcov€n'esj103aea4-2 4,+DB-Octafluorobiphenyt (St)
N51-24-3 Decachlotobiphenyt (St)
S€mlvolrtile Orgsnic Compounds by c{MS
BRL
BRLBRLARLBRLBRLBRLBRLBRL
8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLSRLBRLBRL43153.2BRLBRL
2540
BRLBRLBRLBRLARLBRLBRLBRL
ldkS dry 7.05
ldkg dry 7.05pdkS dry 7.05
ttEkgdry 7.O5
ldkS dry 35.3pEkg ory 7.05
lrgr(g ory 7.05
Fqkg dry 7.05
lEkg dry 7.00
ldkS dry 7.05
lgkg dry 7.05
lg/kg dry 7.05
udks dry 7.os
UgkS dry 7 _05pdkS dry 7.05pgkg dry 7.05pgkS dry 7-05
ldks dry 35.3
ldkS dry 7.05pdf(g dry 7.05
ldkS dry 7,05
30-150 o/L
30-150 %
pdks dry 14.1pdks dry 14.1
ldkg dry 14.1pdks dry 14.1
udkg dry 14.1
ldkS dry 14.1
FgkS dry 14.1
lqkg dry 14-1
lgkgdry 14.1
30-150 %30-150 %
1
1
1
1
1
1
1
I
I
1
I
1
1
1
I
1
1
I
I
I
SW846 8081A 22-Mat47 27-Mar-07 7031275 TG
SW846 8082 22-llkt47 244,lat-07 7031274 MP
SW846 8270C 22-Mar-O7 2A4,eF07 7031279 M.B
Semivolatile OEanic Comoounds bv SW846 8270CPrepa.ed by merhod Sw846 35008
03-32-9 Acenaphthene
200-Sffi Acenaphthylene
62-5+3 Anilino
12e12-7 Anthracene1912-24-9 Atraine103-33-3 AzobenzeneJDiphenyldiazine9247-5 Benzidine56-5i3 B€nzO (a) anthracene
pEks drypgks dry 680
tidkg dry 680
Pgks dry 680pStkS dry
udkS dry 680
udkS dry 6S0
rdkS dry 680
fhit 'storutory rcprt ir not vallil nithottl ot auihori.cll signatwe on the cover page.
' Reponable Detectiod Limit BRL = Below Repftting Limit Pase 29 of l?4
Page 254
Sample ldeotific{tio'pM8F-26 2-t'sA595t7-06
Clietrt Proiect #301 -88
Mahi{Soil
Collection Dare/TimeI 9-Mar47 00i00
R€ceived20-M^r47
CAs No. Atuba4s) FI"e A,ri'l 'nDL Dihttion t{erhod Ael. Prepdtcd Analfud Bdeh Analpt
Semivolrtlle Oryrnic Cohpouds by GCMSSemivolatile Oruanic Compouods bv SW846 8270CP.epared by qeltrod SW846 3550850-32{ B€nzo (a) pyrene20+992 B€nzo (b) lluoranhene19r-24-2 Benzo (g,h,i) peM€ne207{84 Benzo (k) flooranfiene65{5{ BerEoic acid10G51.6 B€rEyl alcohol111-S1-i &s(2-chloroetrory)dlethaner11{a{ Bis(2-chtoro€hy'Ftner394?+32-s 8tq2-chtodsopropytFtherr17{i-7 Bis(2-€tlytherythhtretatel0l-55-3 4BrodroptEnylph€oytethgr8f!€&7 B0tyt b€rEyt phtjatat€86-744 Carbezot€s9-5&7 +Chlrm-]rnehytphenol108-474 +CNoroeniline91,5€-7 2-Chloronephhalonee55/4 2-Chloroph€ool7@s72'3 4-Chlorophenyl phenyl 6fier218-014 Chrysene5$70-3 Dberuo (a.h) anthEcene132{4.9 Dbenzofuran955G1 l.2oicttorob€nz€ne511-711 1.lDichtorobenzen€10&4&7 !,+Dichtorobenzen€914t1 3,3'.Oichtorobenzidin€1m-e2 2,4-Diqhlorophenol€{{e2 Di€[1yt PhttElatet31rrn DimohylphdElatsi05{74 2.il-Diftefiy'ph6no,la+7+2 Di-n-butytphthalat€r,3452-1 4,&Dinitro-2flethytphenolsi-2&5 2,4Oinitopfienolr21n4? Z,+OiniFobtuene606.20.2 2,GDhibotoluen€iiru4{ Di_n-o4/lphthalate206-44{ Fluoran{teoe&f T7 Fluo.enel1&7,1{ H€xaclrlorobenzenea7r6&3 l-bxaclrlombutadiene7t174 HoxachlorocyclopentedieneEr-72-1 Hexachloroethane19!3+5 Indeno (1,2,3d) pyrene9Gi2{,t- lvlethytnaphthal€ne78-5s.i tsopfiorone91{7{ 2-M€{hy'naphthetene954+? 2-t €ryphenol10&3€.r, 3,4+!,tehylphenol1116-,{4-591-2G3 Naphth6l€ne8€-714 2-Niboeniliness{$2 }Nitsodniline
SW846 4270C 224n 47 261\nat47 781279 M.BBRLBRLBRIBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRI-BRLBRLBRLARLBRL8RLBRLARLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLARLBRI-
lg}'sdry 680
lgl€dry 6{mpgxo dry 680
FS/tS dry 660
lo,rsdry 640
Fdxsdry 6a0
|lgL/ks dry 680
t gn(g dry 6E0
lglqd.y 680
FgY€dnt €40
ldxsdry 680
UgkS dry 680
t€I€ dry 6€0
|lg?€dry 680
UgkSdry 680
ItSllgdry 680
ldkS dry 680pgil€dry 660
IC/tgdry 580
udkS dry 640
Fdksdry 680
UgnrS dry €a0pg/kS dry 680
lgtsdry 680
lqkS dry 680
ldxg dry 680
usl€ d.y 680pSAg dry 6a0
IS/kg d.y 680pg/rs dry 880
ldkg dry 680
ldi€ dty 6{10
|,9n€ dry 600
FSlkg dry 6€0
lsilqdry 680
ldkgdry 640
ldkg dry 680
u*q dty 680
r€/kg dry 680
Ugtg dry 680
lgkg dry 880
fldkg dry 680
!S{!S dry 680
trykS dry 6€0pdkg dry 680pdkgdry 680
ug/kg dry 680
lsftgdry 640
rdkSdry 6a0
Pgtg dry 680
I
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117
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Tnb bbontory Epod is nor edld pihoat aa atntodzrd sknafirr. oE tk cow! pcEe.
'Rqoflable Detcction Limit BRL = Betow Reporting Linit Poge 30 of 124
Page 255
Samole Iden tificationMEF-26 24'sA595 t7-06
Clicnt Proiect #301-88
MatrixSoil
Received
20-Mar-07Collection Dare/Time
19-Mar-07 00:00
CAS No. Analyte(t) Resuk Fl"s Unit *RDL Dilaion Method Retr. Pnparcd Anollzed Batch An lst
Semivolatile Org{nic Conpounds by CCMS
Semivolatile Oroanic Comooonds bv SW846 8270CPrepared by rnethod SW846 35508
100{1-6 4-Nitroaniline
98-913 Nilrobenzene8€,755 2-Nitrophenol100{2-7 4_Nitophenol
62-7+9 N-Nitrosodimethylamine
s2t{4-7 N.Nikosodi-n-propylamine
06-3G6 N-Nitrosodipherrylamine07{6-5 Pentachlorophenol
0541-0 Phenanthrene
10&9$2 Phenol
129-00{ Pyrene110-86-1 Pyradine
12042r t,2,4-Tfichlorobenzene9t9t4 2,4,STfichtorophenol8a-06-2 2,4,&Trichtofophenol
Su'rogate recover'esr321-60-8 2-Fluorobiphenyl
367-121 2'Ffuorophenol
4165404 Nitobenzene41
BRLBRLBRLBRLBRLBRLBRLBRLARLBRL876BRLBRLBRLBRL
836575
Compl€ted
BRL
BRL
0_o148
BRL
BRL
BRL
0.0226
BRL
80.7
lglg dry 2720
lgftS dry 680pgftS dry 680
!g/kg dry 2720pdts dry 680
udksdry 680
Ug/kg dry 660
udks dry 680
t4/kS dry 640
US/kg dry 680
!S/kS dry 680
ldkg dry 680
ldkg dry 680
tiS/kS dry 680pgkS dry 680
m-1m o/.
| 5-1tO %3c-130 %15'110 %30-130 %15-1tO %
mgr'kg dry 0 0367
mgL/kg dry 1.14
hg/kS dry 1.72
mgr'kgdry 0.572
mg/kg dry 0.286
tng/kS dry 0.572
thg/kS dry 0.858
hg/kg dry 1.72
mgn 0,0100
mgl 0,0150
mSI 0.0050
mgfl 0.0025
mS/t 0.0O5O
mgl 0-00040
mg/r i.oozsnEI 0.0150
%
1
1
1
1
1
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1
1
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SW846 8270C 22-Me(07 26.4lat47 703'1279 M.A
416162-2 Plhenol45 621/18-514 Terphenyt4t4 110118-79-$ 2,4,6-Ttibtu.Z]]ophenol 78
Total Mct|ls by EP.{ 6000fi000 S€ri€s Mettodr
743$97€ MeroJry
Tot{l M€tals by EPA 20O Seri€s Methods
7440.22 4 Silver
7440n6.2 Arsenic
7440-39-3 Barium
7,140,499 Cadmiuh
7411047-3 Chaomium
f13g-92-1 Lead
r7a2-4+2 S€lenium
St Lt Extractron
7a4G?2-4 Silver
7440-3&2 Arsenic
7440393 Badum
7440499 Cadmium
7440-47-3 Chromiuh
7439-9rc Mercury
7439-92,1 Lead
a/E2'4+2 S6leniun
C€n€rrl Ch€mirtry Psrsmeten
Yo Solids
0 .141
BRL
8.56
58.7
BRL
7 .11
123
BRL
1 SW846 7471A 26-Mat47 27-Marl7 7031322 YP
EPA200.7 26-Mat47 214ttaiJ7 7031321 HB
SPLP M€t|ls by f,PA 1312 & 5000,t7000 S€ries Merhods
1 SW8461312 22-MarA7 2214at47 7031344 BO
1 SW846131260104 29Mar{7 24-tlar-07 7031408 LR' t '
1 '
1 '' t "
1 SW84613127470A " 26-fr,iar-07 7031409 YP
I SW846131260108 " 24.M,aFO7 7031408 LR' t '
1 SM2540 G Mod. 2SMar07 23-Mar{7 7031429 QP
This l ontoty rcpoa is noa talid r|ithoU ad aathorked signalu?e ontlg clrvcr page.
+ Reporbble Det€.tion Limit BRL = Betow Reporting Linit P a g e J L o f l 2 4
Page 256
Sample IdentificationMEF-27 2'-4,sAs964l- l0
Client Pmject #l0l-68
MatrixSoil
Rec€ived22-Mar4'7
Collection Dat€/Ti.ne2 t-Mar{7 00:00
CAS No. Anatya(s) Rcs,'It Fbs 'R"DL Dilution Me,hod Rel Prcpand Analfzcn Bdch AM4EI
Vohtile Or€rnic Conrpounrls
VOC Extraclion Fieh ext'acted
BRL
N/A
lgftSdry 6.6
tSil€dry 132
tSASd.y 6,6pg|(g dry 6.6pslqdry G.6
ldkS dry 6.6
tdkS dry 6.6
ldkSdry 5.6
rcAg dry 13.2
USAS d,y 65.Spdlgdry 6.6
ldlS dry 6.6
Udksdry 6.6pdks dry 32.9psilqdry 6.6pSl(g dry 6.6
Fgrsdry 13.2pgtg dry 6.6
ldkS dry 1X.2
t,gkSdry 6.6
ISftgd.Y 6.6pdkg d.y 13.2
ugr(sdry 66ps,rs dry 6.6
Ug,fkS dry 6.6
!Sn<g dry 6.6
tjL/kS dry 6.6ygn€dry 6-6
vstkedry 13.2
Ug/r<g dry 6.6pgrsdry 6.6
UglS dry 6.6
ldl€ dry 6.6
tjr'kS dry 6.6
ldkgdry 6-6pS/kS d.y 6.6
Ug,r<S dry 6.6pg,lsdry 6.6pgr'l(g dry 6.6
Ugtqdry 6.6pS'lqdry 6.6ySn€d.y 6-6pSftS dry 85.9yqkgdry 6.6
HdkS dry 6.6
lgl€ dry 6.6
lgrg dry 65-9
ugrftS dry 65.9pqkSdry 6-G
26.MarO7 26ind47 7031584 BD
Voiatlle O.qan'rc CompoundsPrepared by mettbd SW846 5035A Soit (tow tev6t)76-13-1 1,1,2-Trid o.ofinuo.oethano(Fr€oDRL67€rL1 Acetono BRL107-rlr Aqyoniu.ile 8RL71.l.T2 Benzone BRL10&€&1 Bromobeflzen€ 8Rf71-97-s Brornod orcrnethane BRL75'214 Brornodidrlorornethane BRL7*2*2 Bomofoam BRL74{}9 Bromomethan€ BRL78-e3.3 2-&bnone (MEK) BRL104-sl{ n-BulylbefEene BRI_r3t98€ s€c€utylbenzene 8RLs€{6{ tert-Butylbenzeoe BRL75-15{ Carbondisutfidb BRL56-23{ Cafuon istrachloride BRL10&90-7 Chlorcb€nz€ne BRL75.00,3 ChlofoedEne SRL676&3 Chlo.o{orm BRL7a{7-3 Chlorgrnethano BRL96-49-A 24hlorotoluene BRL10643.4 +Chlorotoluene BRL9+1 2€ 'l ,2{)ibron}o-3d{orcpropEae BRL1?,r-4€-1 DibromoEhtoromethane BRL10G90-4 l.2oibromoefiane (EOB) BRl-74-953 Dibromomethan€ BRfs+sGl l,2-Dichlorobenzene BRL541-7$1 l,SDichlorobeEeng BRLl0G2!6-7 l,+Dichlorobenzene BRL7t7l{ Oid oddiffuo@nrethene(Freonl2)BRL7t3+3 l.l-Dicldoroethane BRL107{6-2 l.2oichloroethan€ BRL75.35-4 '1
,l Oichloro€thene BRL15€-59-2 cjs-1,2-Dkfloro€thene BRL15€€$s t?ns-1,2-Dichlorcethone BRL7E{7-5 |,2-Oidiloropropane BRL142.28€ 1,3{)ictdorc,prop6na BRL59+20-7 2,2-O[chloroplop6ne BRLr615e€ l,l-DlchloEpropen€ BRLi0061{1-5 cis-1.}Dlcfitoropropene BRL'0061{24bans.l.3_Di.hloopropene BRLroo4r4 Ehybeflz€ne BRL87€63 HeEcfibrobuhdierle BRL59r,70{ 2-Hexanon€ (MBK) BRLs8l2€ lsopropy'b€nzerF BRL9g+7-o +lsopropyttolueab BRfr69a{a{ Metfiyttert-butl ether BRL1081c1 4-Mgtryl-2+entanon€(M|BK) BRL7s.{l$2 tiehyien€ chbrid€ ARL
SW 846 82608 27-Mar-07 28- ar{7 7031650 RLJ
9l-20n Naphthalene
Page 48 of165
TIns bbontory rcpod h nat vatiil irld,ocl on aartoriey' s4naue ofi lhe @v.r page-
r Rcporhble Detectior Limit BRL = Below Reportiq Limit
Page 257
Samole IdentificatigqM8F-27 2',-4's,{59641-10
Clieot Proiect #30 t-88
Collection Date/Time2l-Mar-07 00:00
MatrixSoil
Received22-Mar-07
C"1S No. Analtte(s) ResaL Flog +RDL Dilution Melhod ReJ, Prcparcd Analwd $alch Anaryst
Volatile Orgaric Compourds
Volalile Oroanic ComooundsPrepared by melhod SW846 50354 Soil (tow tevet)
75$9-4 Trichioroffuoromethane (Freon ltl BRL
103{5-1 rFPropylb€nzene100-42-5 Sty.ene630206 'l
, 1 . 1 ,2-T€trachloroelhane79-34,s 1 , 1 ,2,2-T€lrachtoroelhane1?7-18-4 Tetrachloroeth€ne10&Ea-3 Toiu€ne87414 1,2,U'fichtotobenzene120'82.1 1,2,+Trictioiobenzene71-5s I ,1 ,1-Trichloroethane79405 1,1,2_Trichtoroethane79{1$ TricHoroethene
96-18-4 1,2,$Trichloropropane95636 1,2,+Trimethytbenzene10&67-8 t,3,STrimethylbenzene75{1-4 Mnylchloride133o-2G7 m,p-Xyten€95-.17{ cxylene1099s9 Tetrahydrofufan60-297 Ethylether99+05€ Ted-amyl methyl ether63712-3 Ethy{ tert-butyl elher1oF2OJ Di_isopfopyteth€r75-6+0 Ted-Butanol/butylalcohol12!91-1 1,4_Diorane
Surogale recove.ies:46t)404 4-Bromofluorobenzene
2U7-26-s Toluene4S
1 706047 -o 1, 2-D bhloroethane-d4
186a-53-/ Dibrpmofluo@methane
Extiacaable P€trol€um Hydrocrrbons
Extractable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
8006€14 casoline6&47C30-? Fuel Oild26047ts31-3 FuetOit ft46855900-4 FuetOitt6
I'109600000 Motof OilJ00100000 Avialion Fuel
Unidentified
Other Oil
Total Peholeum Hydrocarbons
Cg-C36 Aliphatic Hydrocarbons
Surogale recovedesl33ee3}z 1 -Chlorooc(adecaDe
Semlvolatile Org.nlc Comportrds by GC
O,oanochlorine Pesticides SW846 8081A
Pr@ared by method SW846 3545A
30900-2 Alddn
SW 846 62608 27-MaGO7 28-Mat47 7031658 RLJERLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRL
BRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRL
99958295
BRLBRLBRLBRLSRLBRLBRLBRLBRLBRL
72
vgkSdry 6.6
Udkg dry 6.6
pdkg dry 6.6
t S/kS dry 6.6
pdkg dry 6.6
l.,S/kS dry 6.6
pSlkS dry 8.6
pg/kg dry 6.6
lig/kg dry 6.6
t S/l€ dry 6.6
ldks dry 6.6
!g/kg dry 6.6
tiS/kS dry 6.6
!g/ks dry 6.6
tis/ks dry 6.6
fg/kg dry 6.6
!s/ks dry '132
!q/kq dry 6.6pg/kg dry 65-SpS/kS dry 6.6pg/kg dry 6.6
tig/kg dry 6.6
ttdkgdry 6.6pg/kg dry 65.9
us/ks dry 132
70,130 %7G130 %7G130 %7G130%
T
1
1
1
l
1
1
1
1
I
i
I
I
I
1
I
1
1
1
1
i
I
l
l
mgftg dry 34.0
IrE4(g dry 34.0
nEftg dry 34.0
nEAg dry 34.0
mS/kS dry 34.0
mdkS dry 34.0
ngil€ dry 34.0
mg/ko dry 340
mSftS d.y 34.0
mS&gdry 34.0
40-140 %
Lrg/kg dry 5.85 SW846 8081A 2&Mar.07 28-Mar47 7031516 TG
This labontory relmn is tnt tqlid p hoa an rlahorir?d siEnalure on lhz coter poge
* Reportable D€ta:tion Limit BRL = Below Reporting Limil Pag€ 49 of 165
Page 258
Sample ldentificatiodM8F-27 2,-4'sA59641-10
Client Proiect #301-88
MatrixSoil
Receiv€d22-Mat07
Collection Date/Time2l-Mar47 00100
CAS No, Anelrtz(s) Flog Uni6 .RDL Dil,Itj]o'| Merhod Rel. Prqand Andyzed Batch A@tt5'
Semivohlll€ Orgrtric Compo{nd! by ff
Orqanochlorine Pesticides SW846 8081A
Prepared by method SW846 3545A
319-84{ a€HC31e4n7 bIBHC3i9-86{ d_8HCsa39e gFBHC (Lindane)
s7'71-g Chtordane72.5.1 4,a'-DDD (p,p,)
725s.e 4,4'-DDE (p,p')
s&29.3 4.4 €DT (p,p,)
60$7-1 Oi€ldrin95$98{ En(lcsullan I33213.66.9 Endo6ulfan llro3l{ru Endosultan Sulfate12-204 Endrin?421-93-4 Endrin Aldehyde7644-A Hepiachjor72.43.5 Methoxy(hlor1021-57-3 Heptachlor Epoxide6001.3S2 Toxaphene5103-71,9 E-Chlordane55€6.3+? g-Chlordane
53494-706 Endrin Ketone
Sunogale Eco!€riesi1 woes+z 1, 4-Dgoctafl uoroliphenyl (St,
msr-24.3 Oocachlorobiphenyt (54
Polvcf orinated Biohenvls bv SW846 8082
Prepared by mothod SW846 3545A
t?674r1-2 PC8101611101-24-2 PCE 122111r4nle5 PCB 1232
5346+21€ PCB '1242
12672-2e{ PCB 1248
11097{s.1 PCB 12541r0sc0?-s PcB tmo3732+?3-5 rcB 12621110Gr4-4 PCB 1268
Sunogale /ecotcriesint:t86-8+2 1,+DB.ocffi @tobiphenl (Sr)
2o5t-21-3 Decehlotobbhenyl (54
S€nlvolrtile Orgrnic Compo|rrds by GCMS
sw846 8o81A 2<at47 2a4 ar47 7031516 TGBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRL
79
BRLBRLBRLBRLBRLBRLgRL
BRLBRL
5085
ERL
BRLBRLBRl-BRI-BRLBRL
BRL
pdftS dry 5.85
lg[rsdry 5.85
ldl(sdry 5.85
rdkS dry 5.85
rdksdry 29.2pS/t€ dry 5.85
ldkSdry 5.65
udkSdry 545pdksdry 535pgl(sdry 545
Ug/kS dry 5.85
IgkS dry 5.8s
Fdksdrv 5.8s
ldko dry 5.8spgtgdry 5.8spdrgdry 5.05
Fdtgdry 5-8s
udredry 292rgkSdry 5.8sggikS dry 5.85
tgkSd.y 5.85
w-|ffi %fi-I50%
I'SikS dry 11.7
Udkg d.y 11.7
lSftSdry 11.7pdts dry 1r.7
Ugkgdry 11.7
UgtS dry 11-7
UdkS dry 11.7
!g/kS dry 11.7
FSilg dty 11.7
u-lfl%30-1ffi %
FdkSdry 421
ISA9 dry 421pdrgdry 421
ldks dry 421
!gl(g dry 421
f./dkg dry 421
lgrko rtry 421
frdkS dry 421
SW846 6082 z&Lrlar{7 28{vlar47 7031515 SM
Semivolatfle Oroanic Comoounds bv SW846 8270CPr@ared by me0|od SW846 3545A
03-32-9 AcenaphthenemBsH Ac€naphthylene62-533 Aniline12G12-7 Althaec€ne1912-2+9 Afazin€103-33 Azobeflzeoe/Diphenytdiszine92{7.5 Beeidine5&563 Benzo (a) entfu'acene
SWS46827@ 2?+lar{7 2f.{nar47 703t5g2 t.B
Thit bboalory npod At ttot vobd withoat dn uthadzd slgnlurc on rhz coee, page.
'R€porhblc Det€ction Limit gRL = Below Reporting Limir Page 50 of 165
Page 259
Samole ldenrificationMAF-27 2t4l
sA59641- 10
Client Project #301-88
MatrixSoil
Collertion Dat€/Time21-Mar-07 00:00
Received22-Ma(07
CAS No. Atnute(s) F,oC Unit. *RDL Dittrinn Method Ret Prepand Analy4ed Bdch Anallst
Semivolrtlle Organic Compouods by CCMS
Semivolatile Orqanic Comoounds bv SW846 8270C
Prepar6d by mothod SW846 354SA
50,32 8 Benzo (a) pyrene
20+99-2 8€nzo (b) fluoranthen€1e1 24-2 Benzo (g,h,i) perytene
207{8-9 Benzo(k)fluorandrene6s-as B€nzoic acidlrxr-s1{ Benzylalcohol111-91-1 Bis(2-cl{oroethoxy)mothane111-44-4 Bis(2{htoroethyl)eher
39638-32-9 8is(2d oroisopropyt)other11741-7 Bis(2€fit/hexyDphfEtste101.s5.3 4-Bromophenyl phenyl ether856&7 Butyl benzyl phthalat€
{16-74 I Carbazole59.5G7 4-Chlo.o-3-methylphenol
106-47{ 4-Chlo,roanaline
91{e7 2-Chloronaphthalene95!57-A z-Chlorophenol7m+72,3 4-Chtomphenylphenylether
218n1-9 Chrysene
53-IA3 Oibenzo (a,h) anthEcene1324.1-9 Dibenzofuran95,5L1 l,2,DichloaoberPen€541-73-1 1,3-Dichlorcbenzene10646.7 .1,4-DacNofobenzene
e1-e4,1 3,3-Dichlorobenzidine120{3-2 z,4-Dichlofophenolu4+2 Oiethyt phthalate
13f11-3 Dimethyt phhalale10ft7-9 2,4-Dim€thytphenol
u-74-2 Di-n-butytphthatate
s34,52,1 4,6-Dinito-2-melhytphenol
51,2&5 2,4-Dinitrophenol
121r4-2 2,4_Dinitrctotuen€
606-m-2 2,GDinitrototuen€117444 Di-n-oclyiphthstat€
206-144 Fluorandren€
&73-7 Fluoren€118-74-1 Hexac}rlorcb€nz€ne
875&3 Hexacfilorobutadien€
Tt17-1 Hexaafiloroclclop€ntadiene
67-72-1 HeXaCfOroethane1S3-39-5 hdeno (1,2,3-cd) py.en€
90r24 l.Methtnaphthalen€786+1 lsophoaone
e1674 2-Methylnaphthalenee5-4&7 2.Methytphenol
108€e-a, 3,4-Methylphenol106-..4-591-20-3 lGphlhatene8a-74-4 2-Nitroanitine99{9-2 }Nilroanitine
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
fg/kg dry 421
!g/kg dry 421
!S/kS dry 421ps/kg dry 421pS/kS dry 421pS/kS dry 421
Udl€ dry 421
!s/ks dry 421pS/kS dry 421
ldks dry 421pdkS dry 421pg/kg dry 421pS/kS dry 421pg@dry 421pS/kS dry 421
lgkS dry 121
US/kS dry 421
!s/kg dry 421
!S/kg dry 421
!g/kg dry 421
!S/kS dry 421pdkS dry 421pdkS dry 421pSAS dry 421pdkS dry 421
!S/kS dry 121pdks iiry 421pgkS dry 421
Pqkg dry 421pdkg dry 421
lqkg dry 421pdks dry 421
UdkS dry 421
ldkg dry 421pgkSdry 421pgkSdry 421
iJgtkS dry 421
UdkS dry 421
ldkS dry 421pdkS dry 421pdkg dry 421pdkS dry 421pCftS dry 421
ldkS dry 421
lgks dry 121pgkg dry 421
Udkg dry 421
tlSJkSdty 421
!S/kS dry 421p€/kg dry 421
sw846 8270C 27-Mar-O7 27-MaPO7 7031592 M.B
This labotaloA rcport Lt ,rol taid *irroU an autlloried signst!rc on lhe coeer page.
' Reportsble Detection Limit BRL = Below Reporting Limit Page 5l of 165
Page 260
Sample IdentificationMEFJI 2'4'sA5954l - 10
Client Proi€ct #l0l-88
MatlixSoil
Collection Datey'Time2l-Mar47 00:00
Received22-Mnr-07
CAS No. Anabte(s) Fl4g 'RDL Dilaion M..hod Retr P.epated Analytd Edch Analyst
S€mivolalile OrS.nic Compoundr by cCMS
Semivolatile Orqanic Compounds bv SW846 8270CP.epared by mehod SW846 3545A100416 +Nitroaniline98-9t3 Nibobenzene6E.7t5 2-Nibophenoll0o{2'7 +NitEpheno,l62-75-9 N-NitKrsodimethylamine6?1{4-7 N-Nihos4di-n-propytamioe86-30{ t$Nitrosodiph€nylgmine87{G5 per achlo{ophonda5{1-8 Phenanthrehetoe95.2 Phenolr29-0o{ q/r€ne
tlF€6.1 Pyridinel20{2-1 1.2,+Tddilorobenzen€95-s5-4 2.4,$TrichlorophenolS8{G2 2.4,&Tricilorophenol
Sunog|af€ rEcover'esr32ta68 z-Huotobiphenyl
357-124 2-Fhnrophenol
11654/)4 Nitrobnzene4s
416562,2 Pherbrds
171e51-0 Teeh6nyHl4
t 1e7*6 Z4,Fftibromophenol
SW84682mC 274tat47 274ar4f 7031592 M.BBRLBRLBRLBRL8RLBRL8RLBRLgRL
8RLBRL8RLBRL
BRLBRL
6158
60
ldl€ dry 16q) 1
lrytC dry 421 |
Fgtg dry 421 1
t C/Xg dry t690 |
ldkg dry 42r I
lgkS dry 421 1
UdkS dry 421 1
ugxg dry 421 Iydlqdry 421 |pSftg dry 421 I
ldfq dry 421 1
t9ft.Sdty 421 I
usl(S rtry 421 1
t4/kg dry 421 1psilqdry 421 t
30-tm o/.
11110 %30-1N%1r110%30-130 %15-110%
Totrl Metds by EPA 6m0t000 S.rl$ Methods
743s.974 Merdrry BRL
Totrl Metlk by EPA 200 S€ries Methodt
SW8.l6 7471A 28-Mar-O7 28 4a.47 7031495 YP
EPA20O.7 2&|.ner-o7 za']l'',Erif 7031,194 RM
SWE461312 26Mar{7 26.ltarfi 7031560 BD
SW846 1312r'60'l0B 2&ti,lar-07 28-Mar{7 7031651 HB
7440-2-4 SiVe.
7440n€-2 A6€nic
714G39,3 Earium
144H3-S Cadflrium
7+rc47-3 Chrcmium
7439.92-r Lead
744{F22-4 Slv€r
71.10-3&2 Arsenic
7'!tt',3+3 Badum
?4aoang Cadmium
744O'aZn Chlon um
7439€7$ Mercury
713942-1 Lead
n8a4$2 Setenium
Generrl Chemirlry P.r.meaer!
% Solids
r€/kg dry 0-0345
nrdkS dry 1.05
mg/kg dry 1-58
ntgilg dry O.ml
rngikg dry 0-263
nrgukg dry 0.527
mgr'kg dry 0.790
mgfl(gdry r.58
0.0200
0.0t50
0_0150
0.0025
0.01s0
0,ofix{)
o.ot50
o.o150
sw8{6 t9127470A
Sw846l31z6ol0a
28+!,lar-07 7031652 YF
28+!,lar.07 m31651 HB
BRL
8RL
| 1 .5
BRL
3.97
8 .18
282-4+2 Solenium BRL
SPLP Mer.k by EPA 13 12 & 6tXXy7000 Serier Methods
SPIP Ext Edion CompletEd
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
45.2
mgn
msf
lngn
msr
msrl
rncl
nrgil
mg/l
I SM2540 G l\rod. 24-Mar47 24t {-07 7031470 QP
Thls laboratory Eport ls d tdid pdlhou cn arrtot*Fd sig d!rc on Utt coee, INg.-* R€portable Detection Umir BRI, = Below REporliry Limit Page 52 of 165
Page 261
Sample IdentificationM8F-28 2'-4'.sA,59641-1t
Clietrt Proiect #301-88
Collectiop Date/Time2l-Mar{7 00:00
MatrixSoil
Received22-Mat-01
CIS No. Anaryte(s) Result Flas *RDL Dilution Lletho.l Rel. Prcpared Amltzed Bakh A al$t
Voletile Orgsnic Compounds
VOC ExtractionVolatile Oroanic Comoounds
Field extracted
BR,J-
ps/ks dry 6.2tigikg dry 125tiSikS dry 6.2
tig/kg dry 6.2pdkg dry 6.2
!S/kS dry 6.2
!S/xg dry 6 2
uS/kgdry 62
lSftg dry 12.5
uS/kS dry 623
!g/kg dry 6.2
!g/kg dry 6.2
!g/kg dry 62
Ir$tSdry 3r.2
!S/kS dry 6-2pdks dry 6.2
udksdry 12.5pdkS dry 6-2pSlkSdry 125
ug/kg dry 6.2
!g/kS dry 6 2
Ug/kS dry 12.5pg/kg dry 6-2pSlkSdry 6.2pdkg dry 6.2
ldkS dry 6.2pdkg dry 6.2
lqkS dry a.2
ldkg dry 12.5
udkg dry 6.2
Itdkg dry 6.2
lqkg dry 6.2
ldkSdry 62
ldkgdry 6.2
U94(S dry 6.2pg/kS dry 6 2
ldkgdry 62
ldkS dry 6-2
!S/kg dry 6.2
lSftS dry 6.2
ldkS dry 6.2pgkS dry 6.2
rc/kg dry 62.3
!g/kg dry 6.2pS/kS dry 6.2
IdkS dry A.2
FS/IS dry 82.3pS/kS dry 62.3
ldkS dry 6.2
voc
sw 846 82608
26-Mar{7 26-tvlac07 7031584 BD
Prepared by method SW846 5035A Soit (tow tevet)
76-13-1 1,1,2-Tdchtorohinuoroethane (FreoSRL6764-1 Acelone BRL107-13-1 Acrytonitdl€ BRL7113-2 Benzeno BRL108-86.1 Brornob€nzene BRL74 97-5 gmmochbrornelhane BRL15-?14 Bromodichtoromelhane BRL75-)12 Eromotorm BRL74{}s Ercmomethane BRL78$13 2-Butanone (MEK) BRL104-51J rFBulytbenzene BRL11t98€ sec_Bu!y'beruzene BRL98{6-6 tert-gutylbenzene ARL75-15:l Carbon disutfide ARLt6-23-s Carbon tetrachloide 8RL108-9G7 Chlorobenzene BRL75{0-3 Chloroethane ARL67€6-3 Chloroform BRL1447-x Chtoromethane BRL954s8 2-Chlorototuene BRL106-434 +Chlorobluene BRL96,12-8 .1,2-Dibromo-3_chloropropane BRLrea4a'1 Dibromochto.omethene BRL106.93i l.2D,brornoethane(EDB, BRL74 9t3 Dibromomelhan€ BRL95'5G1 l,2.Dichlorobenzene BRLs41-73-1 l,3-Dichlorobenzene BRL106-,16-7 1,4-Dichlo(obenzene BRL75-l1-€ Dichtorodifluoromelhane (Freon12)BRL75-34-3 l,l-Dichlofoethane BRL107-06-2 l,2-Dichloro€thane BRL75-35-4 t,1-Dichtoroethene BRL
156-59-2 cis- 1 ,z-Dichloroethene SRL
156€G5 tans-1,2_Dichloro€thene BRL
78{7-5 l,z-Dichloropropane BRL
1{2-28{ 1 ,3-Oichloropro'pane BRL
59t20-r 2,2-Dichloropropane BRf563-586 1,l-Dichtoropropene BRL
10061{l-5 cis- 1 ,3-Dichloropropene BRL1ilo6r{2{ trans- 1 ,}Dichloropropene BRL100-414 Ehylbenz€ne BRL
876+3 Hexad orobutadiene BRL
591-784 2-Hexanone (MBK) BRLssa2a tsopropytb€nzene BRL9€47$ +lsopropyltotu€n€ BRL163444-4Metfryltert-butyletf|er 8RL10&1G1 +Methyl-2-pentanone(MIBK) BRL
75492 Methyl€ne chloride 8RL9r-2G3 Naphthalene
Page 5l of 165
Thit labonlor! Eport is not vatid withaut aE zstho.ized sigtutaure on the cover paEe.
* Reportable D€rection Linir BRL: Below Reponing Limit
Page 262
Sample ldentificatodMtF-28 2'-4'sA5964l - I 1
ClieEt Proiect #301.88
Collectiod Date/Time2 I -Mar{7 0o:0o
Rectived22-Mt-07
MatrixSoil
C"1S No. 4narrtc(s) Flog Uti6 'nDL Dllution Method Rel, PEWed Analwd Edtch A&tyst
Vobdle Or€ooic Compot|ndr
Volalile Oroanic ComooundsPrepared by m€f|od SW846 5035A Soil (low tevel)103-6s1 n-Propylbeizone 8RL10G42'5 Styrene 8RL63G20{ I,l,'l,2-Tet€cfiloroethane 8RL7$1,L5 1,1.2,2-Tetracfiloroethane BRL127n04 Tebachloro€ltEne BRL108-8&3 Toluene ARf8761$ 1,2,$Tichlorobenzene 8RL120€21 1,2!+Tridhlorob€nzene BRL715# |,1.l-Tricfiloro6thane BRL79{0-5 1,1,2-Trid ooethane 8RL?941€ Tichloroethene BRL754S4 Trichlofofluoom€thane (Fr€on 11) BRLs.1a4 1 ,2,+Trichtoopropene BRL95-63i 1,2,+Trimethylbenz€ne BRL108-67€ 1,3,5-Trimedlylbenz€ne BRL7s414 Vinylcfiloride BRL1330-20.7 m,p-Xyt€ne BRL95-47{ Gxylen€ BRLlosss Tet.ahldmturan BRL60-2s7 EhyledEr BRLsgt{s{ Tert-amyl methyl ether BRL637€2-3 Ethy' left-butyt €ther BRLl(a-iG3 Di-isopropyl ether BRL7s€5i Tert-Bubnol/ butyt alcohol BRL123.s1-'1 l,+Dioxane BRL
&nrogals €coleresj4@40-4 +Ekoftnfruorcbenzene 86m37-2e5 TohEne4S 90,706G074 l,2iic o@ethane-d4 871868.53-7 Dibtonbf,uoromehane 98
Ertrrctable P€tml€um Hydrocrrbon!
Extractabl€ Total Petroleum HvdrocarbonsP.epared by nethod SW846 35504
BRLBRLBRLBRLBRLBRL932Calculated as
llJg*S dty 8.2
sdrS dry 6.2pg/rg dry 6.2pq*s dry 6 2pdrs dry 6.2
ldksdry 6.2
tlgtg 6ty a.2
lgkg dry 6.2
l.rdkg dry 6.2pS/rS dry 6-2
t SI(9 dry 6.2pdkS dry 62
ldkgdry a.2pdlq dry 6.2
lSftSdry 6.2
lslt(gdry 6.2
ldkS dry 12.5pcrks dry 6.2pdrg dry 62 3pdxg dry 6.2
ldkg dry 6.2
lJgn€ dry 6.2
I'dktd.y 6.2
lS^gdry 62.3
ISrI9 dry 125
70130%70-130 %70-t30 0,6
76130 %
mdkSdry 161
mgkg dry 161
flEn(gdry 161
mgn(g d.y 161
nE/kg dry 161
mg/kg dry 161
mg/t€d.y 161
mgftgdry 16'l
ngftgdry 161
ttlykg drt tG1
41114 %
SW S46 82608 27-Met47 28-Mat47 7031656 RU
8006€1-9 Gaeolin€68a7S30-2 Fuel o{l #26847s31-3 Fu€lOilt4
€€s53-0o.1 Fuel oil #6
MlNsloOoO Motor Oil$0100000 Aviglion Fuel
ljnidentified
OtlEr Oil
2
2
222
2Total P€trol€um Hydrocarbons 932
C943,6 Aliphe6c Hydrc€66n5 932
Surrogats rEcovEriosli38o-33-2 l -Chbr@cladecane 209
Semlvohlilc Org!tric Compounft by CC
Oroadochlorine Pesticides SW84ti 8081APrepared by melhod SW846 3545A3Xl9{,4 Aldrin BRL UqkS dry 6.21 SWB46 8081A 264nar47 2g-nAa.47 703151€ TG
This labrdlory |'Iorl is not valid tithou tn oadatlad slgadfi. on the cow. pate.
+ Reportabk Dete.tion Linit BRL= Below Re?orting Limii P.ge 54 of 165
Page 263
Sample ldenttficarionNtSF-28 2,-4'sA5964l-t I
Client Proiect #30 t -88
MatrixSoil
Collection Date/Time2l-Mar-07 00:00
Received
22-Mar07
cAS No- Anaqtz(s) FbE Unia *RDL Dilutiarl Method ReJ PrEp ed A&bzed Bakh AnaDst
Semivol{tlle Organic Compounds by CC
Orqanochlorine Pesticides SW846 809.1A
Prepared by melhod SW846 3545A
31934$ a-BHC
319-8t7 b-BHC
319-863 d-8HC
5849-9 S-BHC (Lindane)51-f4 9 Chtordane
n54'a 4,4.-DDD (p,p ' )12-s5-e 4,4.-DDE(p,p.)
50-2e,3 4,4.-DDT(p,p')
60-57-1 Dieldrin
95$98{ Endosulfan I3321365-9 Endosulfan ll1031{7{ Endosulfan Sulfale72-2G8 Enddn
7421€+4 EndrinAldehyde76-44-A Heptachtof72-1.3.5 M€thoxychlor1024-5?-3 Hepiachtof Epoxide4001,35,2 Toxaphene5r03'71'!, a-Chlodane5566'34,r glchlordane
s34947G5 Endrin Ketone
Su7rogate Ecovenes:t 03a6.u.2 4,+DEoctafluorobiphenyt (Sr)
2051 -24-3 Decachlorobiphenyl (St)
Polvchlorinated Biphenvls by SW846 8082
Prepared by method SW846 3545A
12674-1r-2 PCB 1016111o4-2a-2 PCB 122111141-16-5 FCB 123253,469-21-9 PCB t 24212672-29$ rcg 124811097-69-1 rcB 1254110sG82-5 PCB 126037324,23,s PCB 12621110c14 4 PCB 1268
Sufloga/€ EcoveiEs:
103868+2 4,4-DB-Octafluotobiphenl Gr)N51-2+3 Decachlorobiphenyl (St)
S€mivolatile Orgrric Compoundr by GCMS
Semivolatile Oroanic Co'.npounG bv SW846 8270CPrepared by method SW846 3545A
83-32-S Ac€naphthene208-96{ AceMphhylene€2-53-3 Aniline12G12-7 AnthEcene1912-2+9 Attazine103-33-3 Azobenzene/Diphenyldiazine92.47-5 Benzidine
56.513 Benzo (a) anthrac6ne
BRLBRLBRL
BRLBRLBRL
SRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRL
3194
BRLBRLBRLBRL8RLBRLBRLBRLBRL
3045
8RLBRLBRLBRLBRLBRLBRL
BRL
Ug/kg dry 6.21
UdkS dry 6-21
ldkS dry 6.21
tgkS dry 6.21
ugtgdry 31.1
UgftS dry 6.21gkS dry 6.21
udkS dry 6.21pgkgdry 6.21
USftS dry 6.21
frg/kg dry 6.21pdtSdry 6.21pdkS dry 6.21
udkS dry 6.21pdkg dry 6.21
lig/tqdry 6.21
!g/kg dry 6.21pS,/kS dry 31.1pS/kS dry 6.21pqks drl 6.21pdks dry 6.21
30-150%30.150 %
!g/kg dry 12.4
!S/kS dry 124
tS/kS dry 12.4
|'s/kg dry 12.4
ldkS dry 12.4
!S/kS dry 12.4pdkg dry '12.4
Lig/kg dry 12.4
UdlS dry 12.1
3G150 %m-|50%
SW8,f6 80alA 26-Mat47 29-Mafi7 7031516 TG
SW846 8082 26-Mar-07 28-MaF07 7031515 SM
Pe/kg dry 3o0
!S/kS dry 3O0
UdkS dry 3O0
UgkS dry 300
!Sl(S dry 3fi)
ldkS dry 300
lgkg dry 300
ldkS dry 300
5
5
5
5
5
5
5
5
SW846 8270C 27-Mar-O7 27-MarO7 70315S2 M.B
Thb laborutory rcpo.t ie dot edd hilhoar an anhoned siEnature on tht co,er page.
* Reportable Detection Ljmit BRL = Below Reporting Limit Page 55 of 165
Page 264
Sample ldentificationM8F-24 2,-4'sA5964l-l r
Clietrt Proiect #301-88
Matrix50r l
Collectioo Date/Tih€2l-Mar-07 00:00
Received22-Mat47
CAS No- At'ctrk(t) FloC .RDL Dilaion Mdhod ReJ, Prcpuen Aaa[zed BaLh Aralw
Semivohtil€ Orgrrlc Comportrdi by GCMS
Somivolatile Oroanic Compounds bv SW846 8270C
Prepared by rnethod sv'r846 3545Aflt42-a g€nzo (a) pyrene20199'2 B€t|zo (b) fluo|anftetrei91-24,2 B€nzo (g,h,i) peryl€ne207.08-9 Benzo(k)fluoranthene65€s) Benzoic acid10Gs16 Bdlzyl alcohol1t1-s1-i Bis(2-chloroethoxylnstrEne111-44-4 Bis{2dloroehyl)eh€i3{'618-12-9 Bis(2d{oroisop.@yt)ether117€1-7 Biq2-€trfheryl)phfi€late101.s5-3 4-EEmoph0nylph€nytether8t6&7 8uM b€nzyl phlhalate86-Z+8 Ca|tazole595G7 4-Chloro-3-rnethylphenol106-4T3 +Chloroaniline915&7 2-Chh.onaphthalene95'57{ 24hbmph€nol7005-?2.3 4-Chlomphenyl phenyt ethea21641.9 Chrysene5il-z().3 Clibor|zo (a,h) anthi*ene13264€ Db€nzofLrranS-5G1 l,2OicHo@benz6n€54t-73-1 l,3-Dichlorcbenzene1HG7 l.+Dichtorobenzen€914+1 3,3',-Oh.htorobenzidine12G€3.2 2,:l-Oichloropi|€nol846rt2 Digtryiphthalate131-i1a Dime[1yiphhalater0fi674 2.4-DimethylphenolU-7+2 Di{-butylpf'tElste5{452-1 4,e>Dinibo-2-methytphenol5l-2&5 2,4-OiniEoph€nol12tn4.2 2,+Dinitgtolu€ne6ql2G2 2,GDinihrtotuene117{a{ Di-n-octylphhalate20e4-{t Fluoiondtene&7+7 Fluorenellg74.1 l-lexachlorcb€nzene87{&3 tbxad{orcblladienon474 Hexadrlo,rocyclopontadiene67-72-1 H€xaaf$orc€lhane1e+396 Indoio (1,2,3-cd) ptrene90-124 t-Methylnaphrnabne7869n lsophorOnesl-57.6 2-Methy'naphhal€n€!r5i.4&7 2-[,lgthylphenol1{I+?€4. 3,4-Methylphenol106.r.r-591-2Gl Naphthet€ne$.7+rl 2-Nitoaniline9s-O€.2 lNifoaniline
BRLBRLBRL
BRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRI.BRLBRLARLBRLBRLBRLBRLBRLSRLBRLBRLBRLARLBRI-BRLBRL
BRLgRL
BRLBRLBRfBRLBRLBRLBRL
BRLBRI-BRL
!g/kg d.y 30O
tldksdty 300
lglsdry 300
udlsdry 30o
Ug/kg dry 300
lSftS dry 300pdksdry 300
lSiks dry 300pSftSdry 3O0
lglg dry 3o0
ldksdry 30o
udks dry 300
udksdry 300
ldkg dry 300pSftS dry 30OpS/kS dry 3o0
ldrg dry 300
wllg dry 30o
Ug/kg dry 300
ISrkgdry 3OOpS/kS d.y 3tX)
IgAg dry I)0pdks dry 3o0
lcrrs drv 300
$gksdrr 30opSI(S dry 3O0
Itg/kg dry 300
W/kg dry 3tX)
llglkS dry 3fi)
[dkg dry 300
Fg/kS dry 30O
rdks dry 30opdkS dry 300
Udkg dry 3o0pgkqdry 3fl)
IS/tgdry frX)pgts dry 300pdks dry 3O0
lglS dry 300
!S/kS dry 30OpdkS dry 300pgks dry 30o
US/kS dry 3O0pqkgdry 3o0
ldkSdry 300
tdkdry 300
lSftS dry 3oo
pdkS dry
lgftsdry 300
Ug*Sdry 300
SW846&170C 27.Ma147 274td47 7031592 M-B
Thir labontarf ,qod is'rattdii p hoa aE or/[torlz.d sbt dqre on tt'E dtEr pagc.
' Reportrble Det€ction Limit BRL = Below Reporting Limie Pagc 56 of 155
Page 265
Sarnple IdondficationM8F-28 2,-4,sA5964l-l I
Client Proiect #t0 l -88
MatrixSoil
Collection Datc/Time2l-Mar47 00:00
Received22-Mat07
CAS No. Anatye(s) Resall Fhs Anits IRDL Method Rel. Prcpand Aaalrzed Batch Analrsl
S€mivolatile Organic Compounds by CCMS
Semivolatile Oroanic Comoounds bv SW846 B27OCPrepared by melhod SW846 3545A
100{1{ 4-Nihoaniline96-9ti Nifobenzen€86-7$5 2-Nitrophenot100-02-7 4-Nitroph€nol62-7Fg N.Nitrosodim€ftrylamine621{4-7 N.Nitosodi_n_propylamine86-30{ t+Nitrosodiphenylamine87-SA5 Penlechlorophenol85{11'€ Phenanlhrene10&95.2 Phenol12+00{ Pyrene110{6-t Pyridine120{2-1 1,2,+Trichto.obenzene9s-9s 2,4,Slrichtorophenol86{e2 2,4,GTdchtorophenol
Sunogate r6covsrbs--321-6da 2-Fluorobiphenyl
36r-12-4 2-Fluorophenol
4165{04 Nilmbenzene45
116542-2 Phenol4s
171g-Sti TeMenyl4t4
118 79-6 2,4,6Tdbromophenot
ps/kg dry 1200
ldkS dry 300
uS/kg dry 300pdkS dry 1200
lr94g dry 300
Lrdkg dry 300
!S/tg dry 300
Lig/kg dry 30O
!g/kg dry 300
UdkS dry 300
lsng dry 3o0
Pg/kg dry 3O0
trg/kg drypS/kS dry 30O
lrglkg dry 300
30-t 30 %15-110 %30-130%15-110 %m-lm %15-tt0 %
rngr'kg dry 0.0329
ms&s dry 0 995
mgiks dry 1-49
mg/kg dry 0.497
mg/kg dry 0.249
ngtkqdry 0.497
mg/kg dry 0.746
mgfl(g dry 1.49
hgn 0.0200
lhgn 0.0150
mg/l 0 0150
mg/l 0.0025
hg/l 0.0150
rng 0-000d0
|ngn 0.0150
rng/l 0 0150
%
BRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
61
4A7057
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
SW846 8270C 27-Mat47 27+l,at47 7031592 M B
7440 22-4 Silver
7440-39-2 ArseniC
7440-39 3 Badum
7440419 Cadmium
71404r-3 Chrcmium
7439-92-1 L6ecl
778?-492 Seleniuft
Tot l Metds by f,PA 6000/7000 S€ries Merhods
7439 9?,6 Mercury 0.0388
To(tl M€trk hy EPA 200Srrics Metnods
1 SW846 7471A 2B.l./,at47 za-Ma4l 7031495 YP
I EP4200.7 28-Mat47 2841,a.47 7031494 RM
l "
1 '
1 '
1 "
1 '
1 SW8461312 26-Mar-07 2Gt4ar-07 7031560 8D
1 5W846131260108 28-Mat47 28+lar47 7031651 HB
1 "
1 '
1 '
1 '
1 SWU6131A747OA ' 28-Mat47 7031652 YP
1 SW8,16131?J60108 " 2&Mat47 7031651 HB
1 "
1 SM25.f0 G l\4od. z+Ma(Ot 24^iat47 7031470 QP
BRL
1.60
1S.3
0.333
7.39
25.3
BRL
SPLP Metdr by EPA 1312 & 6000t000 S€rtes Merhods
SPLP Extraction Compl€ted
7Mo-224 Sitvat gRL
7440-3&2 Arsenic BRL
7,140-393 Barium BRL
744043.9 Cadmium BRL
7440-47-3 Chromium BRL
7439-9?{ Mercury BRL
7439-92-1 L€ad BRL
7782-4$2 Selenium BRL
General Chemlsary Prrsmeters
% Solids 90.8
Thh lahoralory rcport is not valid withoat dn autltorir2d sigt,a,tcrc on thc coter pzge .
i ReponablE D€tection Limit BRL = Betow R€porting Limit Page 57 of 165
Page 266
Sample ldeotificationM8F-29 2',-{'sA5 4l-12
Cliert Project #301-88
MatrixSoil
Recaived22-M^r-O7
Collection Dat€/Tim€2l-Mar-07 00:00
CAS No- Analyaz(s) FlaB Units *EDL Diluion Method Retr, Preporcd AaqlyTsl Batch Anaust
Vobtile Orgrnic Compounds
VOC Erdraction ?s.M3{47 2iltat47 7031 584 BO
pSAS dry 64,3pgrkg dry 1290
!s/kg dfy 64.3
!4kg d.Y 64.3
ldkSdry 64.3
ldkS dry 64.3pdkS dry 64.3pS/kg dry 64-3
rdkS dry 129
IS/kS dry 643pS/kgdry d+.3
lgrsdry 64.3
lglkgdry 64.3
ldts dry 322pdkS dry 64.3
t€/ko dry 64.3
ldtS dry 129pSftSdry &1.3
lqkSdry 129pdxgdry 6,{.3
!g/k€ dry 64.3
USI(S dry 129pS/kS dry 64.3
lSlkS dry 64.3ydXS dry 64 3pdkg dry 6{.3
lCftS d.y 64.3
ldkg dry 64.3
ldkS dry r29
udks dry 64.3
@v,S dt t 64.3p9rk0 dry 6,{.3
ldkg dry 64.3
USA9 dry 64.3
lgl(gdry 64.3
lcrrs dry 64.3pdksdry 64.3
US/kS dty 64.3
lSftSdry 64.3
Fdks dry 64.3
rdkgdry 64.3
tiSikS dry 64.3pgtgdry 643
Ugkg dry 64.3
ldkgdry 64.3
!gI(S dry 64.3
ldl(g dry 643
l|gn(g dry 643
lSn€ dry 6,1.3
Field €idracredVolatile Orqanic Comoounds vocsPrepared by m€tfiod SW846 5030 Soal (high lovel)76-13-1 1,'1,2-Tdct o.otrifuoroethane(Fr€o€RL6l{+1 AEetone BRL107-13-1 Acrylonltrite BRL'114}2
B€nzene BRL1o&o€-1 Bromobenz€ne BRL74-97-5 Bro.no{filororn€thane BRL75'271 Brg.nodichloromthane BRL7s2r2 Blomoforfi BRL74{3-9 Bronomethan€ BRf78.933 2€ubnone (MEK) BRL1045i€ n-Butylbenzene BRL135-984 sec€utylbenzene BRL98-06-€ tdt€'-rtyhenzene BRL7s-ls-0 Carbon disutfide BRLs6.23.5 Carbon tebachloride BRL10es+7 Chlorobenzene BRl-75{0-3 Oilorc€thane gRL
67{e3 Chlomfolm BRL?4{71 Chlo(omethan€ BRL9t4$€ 2-Chlorotolu€n€ BRL10€-ts 4-Chlorotoluene BRL96-124 1,2-Dibromc3-ciloropropane BRL124-44-1 Dibmrhochlorcmefian€ BRL10+e3.{ 1,2-Dib,rornoethane(EDB) BRL74-95-3 Ditxomornethane BRL95-5Gl l,2-DlchloEbenzene BRL5,11-73-1 l,3.Oichlorobenzene BRL106-{6'7 l,4oidNorobenz€ne BRL75-71.6 Dicf orodifluoronretherE (Freonl2)BRL?s+,G3 1,'l-Dict$r.oethane BRLi07{6-2 l,2-Dichloroeth€ne BRL7$35-4 i,1-Dbhloroethen€ BRLi5tr92 cjs.1,2-Dichloroeth€ne SRLl5G6G5 tEns-1.2-Di(hlo.oethene 8RL7a€7,5 t,2-Dic* ofopmpan€ BRL142.24-9 l,3-Dichloroprcpane BRL5S+2c7 2,2-Dichloropropane BRLs6$584 1,|-OioHoropopene BRL1006141.5 cis-1,3-Dichloroprop€ne BRL10u61-o2€hans-1,$Diohlorcpropene BRLl0o4l4 Ethytbanz€n€ BRL8?{&3 Hexadrlombutadiene BRL591-764 2-tt€xanone (MBK) BRL9842{ tsopropylb€nzene BRL99{7{ zl-lsopmpyltoluene BRL163444-4 Modryl bd-butln edier BRL108-1$1 +Methyi-2+entamne([ BK) BRL7fis2 Meftylene chlorid€ BRL
5050505050505050505050505050505050505050505050505050505050505050
50505050
50
50
50
505050
SW 846 82604 23-Mat47 29-Ma.47 7031784 mar
9l-20.3 Nephthlene
Page 58 of 165
Ihb lalontory rcpod h ,et volitl h,lthou sn acrtorized sEnztrlre ott th. @ftr pqe.
' Reportlble Detection Limit BRL = Below RepdtiEg Limit
Page 267
Samole IdentificationMEF-29 2,-{'sAs964l- l2
Client Proiect #301-88
ColLection Date/Time2l-Mar-0? 00:00
MatrixSoil
Reccivcd22'M^.-01
CAS l1o. Analyte(s) Restlt FloC *RDL Di, ia'n PrcpaEd Antbwd Balch Anltlts.
voladle O.ganic Compoundr
Volatile Oroanic ComooundsP.epared by method SW846 5030 Soit (high tevet)
7549-4 Tdchloronuoromethane (Freon .11) BRL
103{5.1 n_Prcpylbenzene100-425 Sty€n€63G20S 1,'1,t,2-TetEchtoroethane79-34-5 1 , 1 ,2,2-Tetrachtoroethane12h8-4 TelEclioroethene109-€43 Toluene87616 1,2,STrichlorobenzene120-821 1,2,4-Trid,rtorobenzene71-5+6 1,1,1-Trichloroethane79{0-5 1 ,1 ,2-Trichtoroethane79414 Trichloroethene
s6-18-4 1,2,+Tric*rto|opropane95$3-6 1,2,4-Tdmethytbenzene108 67J 1,3, tTdmeflrytbenzene75414 Vinytchlonde1330,20-7 m,p-xylene9547-6 o,Xylene10s-98-9 Tetrahydrofuran@2s7 Ethyt ether9944s{ Tert-amylmelhytether637-92-3 Ethy{te(-bu9tether10s,m,3 Di-isopfop!4ether75{5{ T€rt-Butenot/butylatcohol12191-1 1,4-Dioxane
Su/ogate aecovedes:46'4tt4 4-Bromofluor1benzene
N3f -2e5 Toluena4S
I 7o6a07 -0 l, 2 -Dichloroethaoe-d4
186a-53-f Dibromofluoromelhane
f, xtraclrblE Petroleum Hydrocarbons
Extractiable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
6006{r-9 casotine6€47t30-2 Fueloit#z
6€47F31-3 FuetOi l#4
6855$00r Fueloil#6
M09800000 Motor oilJ00100000 AviationFuel
Unidenlified
Other Oil
Total Peholeum Hydroc€rbons
CSC36 Aliphatic Hydrocarbons
Sunogate recoveies:3386-3i-Z l-Chloroocledeczne
Semivol{til€ Orgrnic Compoundi by CC
Oroanochlorine Peslicides SW846 8081A
Prepared by method SW846 3545A
3090G? Aldrin
SW84682604 29-MaA7 29{.1at47 103178/ mal
+CT EIPH 27-MaF07 28-e1ar47 7031589 DS
BRL183ARLARLBRLBRLBRLBRLBRLBRLARL
BRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRL
1011019196
BRLBRLBRLBRLBRLBRL294Calculated as294294
89
!g/kg dry
trglkg drypg/kg dryyg/kg dry
!g/kg dry
!g/kg dry
Ug/kg dry
!S/lg dry
!S/kS dry
Pg/kg dry
tqKg dry
!g/kg dry
!g/kg dry
!q/kq drypS/kS drypg/kS drypg/kg dry
Pg/kg dty
!g/kg dry
UgftS drypdks drypqkg dry
rdkg drypcn(s dryp/ks dry
64.3
64.3
64.3
64.3
64.3
64.3
64.3
64.3
64.3
64.3
64.3
64.3
64.3
€d.3
64.3
u.3129
64.3
643
a+364.3ar364.3
643
1290
505050
505050505050505050
505050505050505050505050fi
fiE/kg drynE/kS drymg/kq dry
mg/kg drymg/kq drymg/kg dry
mgL/kg drymg/kg drymg/kg drymg/kg dry
70-130 %70-130 %70-130 %70-130 %
4U140%
83.683.683.6
0 3 603.603.6
03.683.6
pS/kS dry SW846 80€1A 2&Mar{7 2&MaF07 7031516 TG
fhis labontory repod as nat palu* hoat an aathodted r,jlgnatare oalhe cor psge.
* Reportable Det€clion Lirnit BRL = Below Reporting Limit Page 59 of 165
Page 268
Samule IdeotificationMrF-29 2'-4'sAs964l -12
Client Pro.iect #301 -88
Collection Date./Tim€2 I -Mar-07 00:00
MatrixSoil
Received22-Mar-07
CAS No. Analflc(s) FIaS 'RDL Dilarioa Method Rel Prcpoted Aaalyad Edch Arroltst
Semivobillc Orgrnic Codpounds by cC
Oruanochlorlne Pesticid€s SW84{i 8081A
Prepar€d by method SW846 3545A
31944{ a-BHC
3r9{t7 b-BHC
319{6€ d€HC5€{99 g-BHC (Lindane)
5r-7+9 Chlodane72-5:r€ 4.4 -DDD (p,p')72.5$e 4,4,-DDE (p,p,)
5G2e3 4.4,-ODT (p,p')
60-57-l Dieldrin959-98{ Endosulfian I33213'65-9 Endosulfen tl1031473 Endoeulfan Sufate72-a'Ug Endrin7421.93-rl Erd.inAtd€hyde76.44-8 Heptachlorf243'5 Methorychlor1024-57-3 Heptachlo. Epoxide0O0l-3S2 Toxaphene5103-71-9 a-Chtoddane5566-34-7 g_Chlodane
53a94-7G5 Endrin Ketone
Sunogate rtcoyarbsl1 qsGe+z 4,448-Oc!afl wtobiphenyl (5,)
2951-2+3 Daeachlotobiphenyt (Sr)
Polvchlorinatod Biphenvt5 w SW846 BO82Prepared by method SW846 3545A
12674-r i ,2 PCB 1016111U-U-2 rcB 122111141-1e5 PCB 12325346s-21€ rcB t24212672-2s{ PCB 12481r0e7s-1 PcB t254r10e6!2-5 PCg 12603732+23.5 rcB t262rlr0G14-,. PcB 1268
Su?oga{e a€coMeiesrt 03864+2 4,lO+Ocb,nuorcbidtenyt (Sr)
u51-2+3 De@chlorobiphenyl (Sl
Senivoladlr Olgadc Comporrds by GCMS
BRLBRLBRLBRL8RrBRLBRLBRLARLBRTBRLBRLBRLBRLBRLBRLBRLBRLBRL8RL8RL
4176
BRLBRLBRLBRI-BRLBRLBRLBRLBRL
4570
BRL
BRLBRLBRLBRLBRLBRL
lgftodry 665
ISI(1gdry 6.65pqrs dry 6.65
lgrg dry 6.65
ugkg dry 33.2
t'gfr4 dty 6 6spdkS dry 6.65
Fg/kgdry 6.65
ldtgdry 6.65
ldkgdry 6-65
rgkS dry 6.65
l€@ dry 6.65p{r^gdry 6.65pgkgdry 6.65
Lrdl1g dry 6-65
ldl(g dry 6-65
FSn€ dry 6.65
lg/lsdry 33.2
PgtS dry 6.65
IdlS dry 6.65
Uglkgdry 6.65
30.150 %3o-lf l%
pdkgdry 13.3pdkg dry 13.3
ldkg dry 13.3
ldkg dry 13.3
udkgdry 13-3
rgkgdry 13.3
tdke dry 13.3p{ykS dry 13.3
t/dlg dry '1 3.3
30-150 %30-150 %
rc^g dry 415
udkSd.y 415
Fcr19 dry 415pdlqdry 4t5pgtsdry 4'15
lgl€ dry 415
lrdkS dry 415pglqdry 415
I
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5!\446 e081A 2&ttlat4l 28-lr.,at47 7031516 TG
6W846 8062 26:Mat47 284tat47 7u]15r5 SM
SW8.r6 8270C 27.Ma147 274ta147 7ull592 M.A
Samivolatile Omanic Compounds by SW846 8270CPrepared by melhod SW846 3545483-32-9 Acon6phthenea)e96€ Acenaph$t46ne62-5$3 Anilingt20.12-7 AnttrEc€ne1912-2+9 At€zine103-33-3 Azobcnzene/Diphenyldiszinee{7,5 Benzldin€56.5$3 Benzo (e) anthracen€
2
222
2
Thb latonlary Eporl Is not volid rdthou, an uahoried slgruatr. oa the covz' page -
' Repodabl€ D€tectioE Limit BRL = BElow Reporring Limit Page 60 of 165
Page 269
SampLe IdentiflcationM8F-29 2'-4'sA5964l-12
Clicnt Proiect #30t-88
Colleotion Date/Time2l -Mar-07 00:00
MatrixSoil
Receivcd2?-Mar-07
CAS No. Analru(s) Flag Units *RDL Dilutio^ Methotl Retr. Prcparcd A?uvzed Bstch Analjst
Semivolatile Orgsnic Compounds by CCMS
Semivolati16 Oraanic Comoounds bv SW846 8270CPreparod by meihod SW846 35454
50-32{ Benzo (a) pyrene
20+992 Eenzo (b) nuofanthene191-24-2 Benzo (g,h.i) perylene
207-08-9 Benzo (k) fluofanthene65€60 Eenzoic acid100-514 Ben2ylalcohol111-91-1 Bis(2-chtoroethoxy)methane111-44-4 gis(2-chtorcethyt)efier
3963&32-9 gis(2-chtoroisopropyl)ether
117{1-7 Bis(2€thy{heryt)phthatate101-55-3 +Brornophenyl phenyl ether85{&7 8uM benzyl phthalate86-74-8 Carbazole5s-50-7 4-Chtoro-3-methylphenol106-473 4-Chloroanitine
91-58-7 2-Chloronaphthetene9s-s7-8 2-Chlorophenol700t72-3 4-Chlorophenyt phenyt ether218{1-9 Chrysene53'7G3 Dibenzo (a,h) anhraceng132443 Dibenzofuran
96.50-1 1,2-Dichlorobenzene
5.11'731 1,3-Dichlorobenzene
10s46 7 1 ,4-Dichlorobenzene91-94-1 3,3--Dichtorobenzjdine120€3-2 2,+Dachlorophenol444f'2 Diedryfphthalet€131-11n Dimethylphthatate10tr74 2,+Damefiylphenotu-r4-2 Di-n-buvphthalate534'52-1 4,$Dinitro-2-methylphenol
51-20-5 2,+Dinitrophenoi121,14-2 2,+Dinitrotoluene60G20-2 2!6-Dinikotoluene117-84{ Di-n-octylphthalate
20€44{ Fluoranthene6-7TI Fluorenel1&741 Hexadllorcbenzene
e76A-3 Hexachlorobutadienen474 Hexachloroclclopeotadiene
6l-f?-1 Hexachloroeihane
19+3e-5 lDderb {1,2,3-cd) pFene90,12{ 1-Methytnaphthalene
78-59-1 lsophomne
91-57'6 2-M€thytnaphthatene
9s-4{-7 2-Methytphenol
108-39-4, 3,4-M€thyiphenol106,44-591-20-3 Naphthalene8a-74-4 2-Nitroaniljn€9{H)S2 }Nitroaniline
BRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRL
BRLBRLARLARL8RL8RL8RL8RLBRLBRLBRLBRLSRLSRLARL8RL8RLBRL8RL8RL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLARL
!g/kg dry 415
!g/kg dry 415
!g/kg dry 415
ugfts dry 415
!g/kS dry 415
lSi kS dry 415pSlkg dry 415
lrS/kS dry 415
rrEks dry 415
lSikS dry 415
!9ft9 dry 115
PEkSdry 415
Udks dry 4'15
US&g dry 415ps/ks dry 415pdkS dry 415pS/kS dry 415pS/kS dry 415
!g/kg dry 415
!g/kS dry 415
lSrkg dry 415
!g/ks dry 415
!g/kg dry 415
lS,lkg dry 415pg/kq dry 415ps/ks dry 415pqlkS dry 415
ldkg dry 415
Ug/kg dry 415
!g/kg dry 415
!g/kg dry 415
Ljg/ks dry 415
Pg&S dry 415
!g/kg dry 415
f.ig/kg dry 415pg/kg dry 415
!S/kS dry 415
!g/kg dry 415
ldkS dry 415
rrS/lqdry 415psfl(g dry 415
frg/kg dry 415
!g/kg dry 415
!S/kS dry 415
LigftS dry 415
i.igrkg dry 415pdks dry 415
!g/kg dry 415
ldkS dry 415
ldkg dry 41s
222
2222222222222222222222222222222222222
22222
2
222
SW846 8270C 27-Mat47 27+l,at47 7031592 M B
Thir laborato.y rcpo.t is not velA * holt an aartori.Etl sighafrne o1 the cowr page.
* R€portable Detectio! Limit BRL = Below Reporting Limit Page 6l of l65
Page 270
Sample IdentificationM8F-29 2'4'sA5964l- 12
Ctiepr Pmject #301-88
MatrLYSoil
Collectiofl Dat€/Time2 I -Mar-07 00:00
Received22-Mst4'l
CAS Na Anzlyk(s) FqC Uaia 'RDL Dilatinn Llahod Retr, Prcparul AMIWi Bat h A@lrsl
Semivohtil€ Organlc Conpornd! by CCMSSemivolatile Oroanic Cornoounds bv SW848 8270CPtepared by rnetFd S\tr,846 3t+5Al0{>0l4 +Nitosniline94.9t3 Nilrobenzene8&755 2-Nibophenol1('0.{2-7 +Nitophenol62.7+9 N-Nibosodimethylamine62r-€4-7 N-Nitosodi+popytamineaailo{ N-Nitrosodiphenytaminea7+4.5 Pentadoaophenol€5.{11€ Phenanthtene10e9aF2 Pharol12€{04 Pyr€ns110{6-1 Pyddine120&-1 .1,2,+Ttidllorobenzene
954t'4 2,4,$.TrfttlorophenolE8-0G2 2,4,&T.ichlorophenol
Surogde recarlsries:32150-8 z-Fluotubiphmyl367-124 2-FfuotoFllenol1165-604 Niltobenzone45411842-2 Phenot45t7lwta Toryl1enyl4l411&79-6 2,4,6-Tibtqnnpllenol
tdllg dry 1660 2
IC/tgdry 415 2
PElqdry 415 2
ldkg dry 1660 2
fldko dry 415 2pgkqdry 415 2
€iko dry 415 2pS/kg dry 415 2pdkgdry a15 2
ldks dry 415 2
udksdry 415 2
FdkSitry 415 2
UdkSdry 415 2pdkgdry 415 2psagdry 4t5 2
tu130 0k
15-110 %3tL130 %trfio %30-130 %1+1tO %
SW8468270C 27-Mat47 27iret47 7031502 H.BBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRL
676157
Totsl Metrb by EPA 60001000 Seri6 M€thod3
743+976 M€rcury BRL
Tot l Met.b by EPA 200 Seri€s Merhods
SW846 747f4 2B&la'.Ol 28.Mat47 7031€5 YP
EPA 200.7 28-lt ar{7 2g-[rar{7 7031494 RM
1 SW8461312 26-Msr47 26lrar{7 7031560 SD'1 S14/E46 1312/60108 28-Mar-07 28+vlar-07 7031651 HB
1 "
t '
1 .
1 '
1 SW8.161312'470A ' 28+,lar{7 7031652 YP
1 SW84€ 1312160104 ' 28-lrar0 7031651 HE
fitg/ko dry 0.0333
7.14(!22-4 Silver
7,r40-3S2 Arsonic
7r!0-393 Barium
744043-9 Cadmium
7440-a7-3 Chloftium
?4SS2-1 Lead
nEr'kg dry r.tl 1
org/kg dry 1.66 |
mgagdry 0.554 I
mSI(g dry 0.277 'l
flB4€dry 0.554 1
m€fl(g dry 0-831 1
nr€L/kg dry 1.66 1
BRL
BRL
15.2
BRL
7.06
t6. I
?82-1$? Selenium BRL
SPLP Metd3 by EPA ljl2 & 5000/7t00 Se.ieJ Mertrodi
SPLP ExEaclion
74,10-22-4 Silver
7rt4{t3&2 A6enic
Z.(,-3$3 Baduft
7&U){3-9 cadmium
ll40-473 Chtpnium
743947-€ Msrqrry
7tt3+92.1 Lead
Z8?-4$2 Sebolunl
G€r€ral Cbe irtry Panmeters
% Solids
mgfl 0.0200
ngl 0.0t50
mgn 0_0150
nE/l 0,m25
nEil 0.0150
rftSl 0.m04O
n'Sn 0.0150
msn 0.0150
Cornplebd
BRL
BRL
BRL
8RL
EIKl-
BRL
BRL
BRL
87.4 SM25,f0 G Mod. 24-M6147 24nnsf47 7031470 OP
Thb t,'5ordorf rqort h ,ot vdU xtitttou an oathorizal sigdraue on dr. cover p{/ge .
' R€porEbl€ Dete.tioi Limit BRL = Below R€porting Linir Page 62 of | 65
Page 271
Salnple ldentificatiooM8F.30 2'-4isAs964l- l3
Client Proiect #301-88
MatrixSoil
Collection Date/Time2l-Mar{7 00:0O
Received22-Mar-0'l
cAS No- Anoqte(s) Flag Unil, 'RDL Dilution Method Ref. PEparcd Ana+.ed Batch Analjst
Volstile Organic Compo{nds
VOC ExtraclionVolatil,9 Oroanic Comoounds
Ug/kg dry 5I
!S./kg dry 117
!S/kS dry 5.9pdkSdry 59pg/kg dry 5IpgkSdry 5.9
ldkS dry 5.9
UdkS dry 5.9pS/kS dry 11-7pgks dry 58.6pdkS dry 5.9pdkS dry 5 I
UdkS dry 5-9
Ug/kg dry 29.3
!g/kg dry 5.9pgkg dry 5.9pgikS dry 11.7
lgkg dry 5 9pS/kS dry 11.7pgkSdry 5.9pdkS dry 5.9
lSftS dry 117pdkS dry 5.9pSftS dry 5.S
t gkg dry 5.9pC4<g dry 5.9
udkg dry 5.9pqks dry 5.9pdks dry 11.7pdts dry 5.9
!S/kS dry 5 9
ldkS dry 5-9
ldkS dry 5.9pdksdry 59
ldts dry 5.9
!g/kg dry 5-9pdkg dry 5.S
ldkS d.y 5-S
ldkS dry 5.9
UdkS dry 5-9
Lidks dry 5.9
i/dlqd.y 5.9
!g/kS dry 58.6
Lidks dry 5.9
Ug/kg dry 5 SpdkS dry 5.9
fldl(g dry 54.6
ldkS dry 54.6
UgftS dry 5.9
26.Mar-07 26'Mar-07 7031584 BDFi€ld ertEcted
Prepared by metirod SW846 50354 Soit (tow tevet)
76_111'1,1,2-Tr ichlorotr i f luoro€t fEne(FreoERL
6754 1 Ac€tone BRL10713r Acry loni t i te BRL7143-2 Benzene BRL108-86-1 Brcmobenzene BRL74-97-5 Bromochloromethane BRL75-274 Bromodichloromehane BRL75-25-2 Brcmoform ARL74{3-9 Bromomethane BRL78-93 3 2-Butanone (MEK) BRL104 5, 8 FButylbenzene BRL135 984 sec-Bulytbenzene BRL98{6-6 tert-Butylbenzene BRL7s 1s-0 carbon disutfide BRL56-2$5 Carbon t€trachloride BRL104-90-7 chlofobenz€ne BRL75-00-3 chbro€thane BRL67$6-3 CbJoaoform BRL7447-3 chloromehane BRL9519'8 z-Chlorotoluene BRL10643-4 44hiorototuene BRL96-124 1,2-Dibromo-3-chloropropane BRL124-40-1 Dibromochloromethan€ BRL106'e34 l,2-Dibromoethane(EDB) BRL74.95-3 Dibrffnornethane BRL9s-50-1 1,2-Dictllolobetwene BRLt41-7+1 l,3-Dichlorcb€nzene BRL10G4€-7 .1,4-Dichlorob€n2ene BRL15-7 1'8 Dicitorodilluoromethane (Freonl2)BRL75-34-3 l,l-Dichloroehane BRL107,06-2 i,z-Didlloroeulane aRL75'35-1 t,l-Dichloroethene BRL15e59-2 cis- I ,2-Oachlo.oethene ARL15M0'5 tran91,2-Diclhlo'ro€th€n€ aRL78{75 l,2-Dichloropropane BRL142-26+ t,3-Dichloropropane BRL59+20,7 2,z-Dichloropropane BRL5€$58'6 1,1-Dichlorop.opene BRL1006141,5cis_1,3-Oichloropmpene BRL10061{2-6tEns-1,3-Dichloropropene ARL100-114 Ethtlbenzene BRL874&3 Hexachlorobutadiene 8Rt_5sr-78€ 2-Hexanofle (MBK) BRt98 €2 8 ls(propylbenzene BRL99€7{ +lsopropyltotuene BRL1634{4-4 Methyt ted-butyt ether BRL108-10.r +Methyl-2-pentanone(M|BK) BRL7549-2 Methytene chlonde BRL
1
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SW 846 82608 27.Mat47 2A-MarO7 7031658 RLJ
91.2G3 Naphthatene
Page 63 of 165
This hno4bry rcpod Lt not ralid *,ithout zn z!rtorizeit sigaotwe on ahe cove, page
* Reportable Detecrion Limit BRL = Belo*, Repodng Limir
Page 272
Sarnol€ ldentificationM8F-30 2'-4.sA59641-13
Clielt Proiect #301-88
MatrixSoil
Rec€ived22-Ma.-07
Collection Date/Time2l-Mar-07 00:00
CAS Na Antu@k) Resull FW Ania *RDL Dil.lian Merhod R.tr Preparcd AnatyEd Bdch Anaryst
Vohlil€ Orgsnic Compouods
Volatil€ Oroa$ic Compour\dsPrepared by method SW845 5035A Soit (tow levet)r03{5-r n-ProPytbenzeneIOO-42-5 Styetre63(L20€ .t,1,1,2-Tei|achlorc6thane
79-3+s 1,1,2,2-Tetrachtoro€thane127-18{ T€IEd{oroelhene1offi.3 Tohtene87{1{ |,2,}Tictoaobenzener20-82-r 1,2,+Tridllorobenzene71-s+6 1, |, t -Tri{:hloroethan€79{Gs 1,t.2-Triafitoroethane79{1{ Tdchloroethene
96-1e-4 l,2.lTrichloropropane95{3-6 1,2.+Trimslhytbenzene108$7{ 1,3,s-Trimethytbenzone75-014 Vinyl c.hlorilet3$-?G7 m,pFxy'ene9s-47€ o-Xylene1c|9 99-9 T€lr€hydrofu€n60-297 E0tyt etEr994{5{ Tert_srnyl methyl eth€r637-92-3 Etiyt trsd+uvt etlEri0{120,3 Di_isopropytetfEr75{5.0 Teat-Butanot / buv atcohol123-91-1 '1,+Obxane
Sufrog€le recot€r,€s..4@-004 +B@npfluotobenzaB203/-26s Tduene4SI 706@074 1, z-Dichloroethane44186&5i-7 Abrwrloffuotumelhane
Erhrtsbh Pcfol€rm Hydroqdrons
Extraclable Tolal P€troleum HvdrocarbonsPrepared by melhod SW846 3551)8tilcr6-€1.9 Gesolin€68476-3G2 Fuel oit ,t26&+7431-3 Fuel Oiln46855100-4 Fuel Oit tt6M098o0000 Motor OilJo0100O0O Aviatiofl Fuel
UnidentifiedOther OilTotal Peboleum Hydrocarbor6Cg.C36 AliphEtic Hydrocarbons
Srnogale recoveriss--33E6-33-2 1 -ChbtRoctadecdne
Semivol$ile Orgr.tc Compounrt by cCO.oanocfibrine Pesticides SW846 8081APrepar€d by method SW846 3545A3OS(xr2 Atdrin
BRLBRLBRL
BRLBRLBRLBRLBRfBRLBRLBRL
BRLBRI-SRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRL
a6898899
BRLBRLBRL
BRLBRLBRI-475Calorlaled 6475475
110
IS/tg drypSfto dry
ldkgdryrcl(g dry
ldlg dry
v€rkodryldkg d.y
Pcrtg dry
udkg dry
ldkg dry
udkg drypdks drypolkg d.ypSftS drypgrs drypdkS dty
!S/kS dry
ldks dry
Wksdry9qtS drypg/kS dry
udks dry
UdkS d.y
lSftS dry
IgI€ dry
5.S
5.9
5.9
5_9
5_9
5.9
5.S
5.S
5_9
5.9
5_9
5.9
5.S
5.9
l1.f
58.6
5.9
5.0
5.9
5.9
5E.6
f l7
75.375-375.375.375.375.3
?5.3
75.3
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SrrV 846 82608 274n{47 zs-Mat4? 7031658 RLJ
75€+,1 Trichloronuoromethane (F.eon 1l) BRL
7u1fi%7E1n%70"130 %70-130 %
mgrkg drymgut(g drynE/kg drymg/kg drymgttg drynEI(g dry
nE/ftg dry
mgukg dry
ingr'kg dry
mgr'kg dry
+CT ETPH 27.[,lar47 28+,lar{7 ru1589 DS
BRL
,4-110 %
|ldko dry 6.11 SW846 80E1A 26-t €r{7 20-lrar47 7031518 TG
This labo.dh.f rcpod is lot vdid Nithau da aslho.iazd Jjg.totttre on the caeer IBge_a Reportable Derecrion Liorit BRL = Betow RcpqtiBg Limir P6€€ 6,1 of 155
Page 273
Sample [dentificationMtF-30 2'-4'sA5964 l - t l
Cliept Project #30 t.EIl
MatrixSoil
Received22-Ma(07
Collection Datc/Time2l-Mar-11? 00:00
CAS No, Aazlyte(s) Result FI"E Units *RDL Dilution Method ReL Pftpared Anabzed Balch AtutlJs.
Semivolrtile Organic Compounds by cC
Oroanochlorine Pesticides SW846 8081APrepared by m€thod SW846 3545A
31914€ a-BHC319{S7 b_8HC319€54 d_BHCs€-€$s 9-BHC (Lindane)57-74-9 Chlordane72,5,L8 4,4'_DDD(p,p')72-5*e 4,4'-ODE (p,p')50,2s-3 4,4rO0T (p,p')m-57-1 Dieldrin95+9e€ Endosullan I33?13{5€ Endosuttan ll1031{7-8 Endosullan Sutfatet2-2M Endrin7421.93-4 EnddnAldehyde76-44-€ Heptachlor7243-5 Methoxydllor1024.57,3 Heplachlo.Epoxide8001.3t2 Toxaph€ne5103-71,9 a-Chbrdane€,566-34,7 g-Chlordane
53494-70-5 Endrin Ketone
Sutrogate rccovedes:1038d842 4,4-D&Octafluotobiphenyt (So
205t2+3 Decachbtobiphenyl (Sr)
Polvchlorinated Biohenvls bv SW846 8082Prepared by method SW846 3545A
1267+11-2 PC81016111o+2s-2 PCB 122111141,16-5 PCB 123253449,214 PCB 124212n72-294 PCB 1248110S7-€9-1 PCB 1254i10e6-€2-5 PCB 1260j7324-23-5 PCB 12621110e1{-4 PCB 1268
Sutog6ls 16s6v"ti""'103864+2 4,1-DB-Octafluorobiphenyt (s4
N51-24.3 Decachlotobiphenyl (St)
S€mivotatile Organic Compounds by ffMS
BRLARL8RL8RL8RL8RLBRL
BRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRLBRLBRLBRL
45/0
BRLBRLBRLBRLARLBRLBRLBRLBRL
4575
BRLBRLBRLBRLBRLBRLBRLBRL
lguftS d'y 6.11pdls dry 6.11
lig/kg dry 6-11
US/kS dry 6.11pS/kS dry 30.5pS/kS dry 6.11
ldks dry 6.f ipdks dry 6.11pgkg dry 6.11
LrS,/kS dry 6-11
lgl(s dry 6.11
udkg dry 6.11
UdkS dry 6.11
ljg,rks dry 6.11
US/l(gdry 6.11
!g/kg dry 6.11pg/kS dry 6.1'1
ldtg dry 30.5
UdkS dry 6.11
USftS dry 6.11pdkS dry 6-11
30'150 %3Gt50%
pg/KS dry 12.2
lgftg dry r2_2
rc/ks dry 122
trS/kS dry 12.2pglkg dry 12.2pS,kS dry 12.2
!S/kS dry 12.2
US&S dry 12.2
lSftS dry '12.2
30-150 %30-150 %
1
1
1
1
1
1
I
I
1
1
1
1'I
I
I
1
1
1
I
1
1
TGSW8468O81A 26-Mar-07 28Nar47 7031516
SW846 8082 26-Mat47 28-Mat47 7031515 SM
Semivolatilo Orqanic Comoounds bv SW846 8270CPrepared by mebod SW846 3545A8s-32-9 Ac€naphthene2oE-96{ Ac€naphthylene62-5'3 Anitine120-12-7 Anthracene1912-24S At€zin€103-33,3 Azob€nzene/Diphenyldialne92.€7-s Benzidinesss5-3 Benzo (a) anthEc€ne
pdkS drypdkS dry
!S/kS dry
!g/kg dry
ldks dry
!g/kg dry
LrdkS drypdkS dry
167
6f
467
467
467
467
467
467
5
5
5
5
5
5
SW846 8270C 27-Mar{7 274Jar-07 7031592 MB
This labontory Epotr it not ealld toithott zn authoriaed si|naturc on the eoter ple
' Reporlsble D€i€{tion Limir BRL = Belo* ReDortins Limir Paee 65 of 165
Page 274
Sample ldentificatiorMtF-30 2'-41sA59641-13
Client P.oiect#30 t-88
MatiixSoil
Received22.l[',at47
Collectiop Datey'Time2t-Mar-07 00:00
CAs No. AnaWG) Floe rRDL Dilutiotl Method Retr. Pftpqred Aaaltud BdEh Annbs!
Semivolslile Orgrnic Compoohds by GCMS
Semivolatile Oroanic Comoounds bv SW846 8270C
ftepa.ed by method SW846 3545A50-32{ Eenzo (a} pyrene20199-2 Benzo (b) Ruofanthene191-24-2 Benzo (g,h,i) p€fylene20rc8€ Beruo (k) duoranth€ne65{5-0 Benzoic acid10G51{ BerEyleloohol111-91-1 8s(2-chloro€thory)methane1r1-414 Bis(2-ct{odo€hy)eher39638-324 Bis(2-chhroisopropyl)eh€ri17{1-7 Bis(2-ethtdhexyl)phhatats10155-3 +Bomophenyl pheflyl ethera5$&7 Butyl benzyt phthatate8&?4{ Ca.bazol€59{G7 4.chbao-}m€thytphenol106474 +Chloroaniline9r,5&7 2-ChloronaphthaleneF57{ 2-Chlorophenolruo572-3 +Chlorophenyl phenyt ether218{14 Chrys€ne5+7G3 Dibenzo (a,h) anthrac€ne132€4-9 DlbefEofuran95{+1 .1,2-Dichtorobeflzeoe
541-73-1 |,3-Dicfilarobenzene106-46-7 1,4-Did orDbenzene91-94.1 3,3'-Dichlorob€nzidinerm€:!2 2,4-Dichlo,ophenol04{+2 Dl€thyt phthllate13i-1rn Dimethyl p,hthatate105-67-9 2.+Dimetry'phenolu-7+2 Di-n-butytphhatate$a-s2.1 4,6_Dinitro-2nethytphenols1.2&5 2,4-Dinitlphenol121n4.2 2,4-Dinitrotofuene60620-2 2,6€inihotoluene117€4-0 O-n-oct!4phfialats206-,ta{ Fluoranlhsfle86-73-7 Fluorene1i8-74-1 Hexachlorcbenz€n€87-68-3 Hexachto.obutadiene11474 |lexachlorocydopentadiene67-72-1 Hexachlorcothane193'3+s Inde{ro (t,2,3-cd) prrcne9G12{t l-Me$ytnaphthalen€78-591 lsophoron€9r-57{ 2-M€thylnEphthalene95-4&7 2-M€thytphenol108-39-4, 3,4-Methylphenoli06{rt591?43 Napnhabn€€&74-4 2-Niboanillne9S{S.2 }Nitroanilin€
SW846 8270C 27+,J'€,r47 27-Mar47 703'1592 M.SBRLgRL
BRLBRLERLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRI.BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLaRtBRLBRLBRLBRLBRLBRL8Rt_BRI-BRLBRL
BRLBRLBRL
lglSdry 167
[gkS d.y 467
IdkS dry 467pdkS dry 467
FgkS dry 67pgts dry 67
lgrsdry 467
lgtS dry 467pgks dry 467
ldkS dry 67
IdkS dry 67pgtS dry 67
lgkg dry 467
ldrSdry 87
lgkgdry 447
Ug/l(g dry #7
trgks dry 67
USAS d,y 67
Isftgdry ,167pdkgdry 67pdks dry 467
!S/kS dry 467pdkS dry 467
trSI(g dry 67yqfs dry 67
tigftS dry 67pglSdry 167pdks dry 467pdksdry 467
udks dry 67
lgkg dry 467pSAg dry 67
UgrS d.y 46r
PglSdry &7
ldkS dry 67
rc/kS dry 467
ldkS dry 4G7pSikg dry 67
lgkSdry 61ygrS dry 67
lg1(S dry 67
ldkS dry 467
UdliS dry 4A7
lSitSdry 487
t dkg d.y 67pSifS d,y 67
IgrS d.y 6r
Fg/kg dry 167
fiSl(S dry 67
ldks dry 47
5
55
5
5
55
5
55
5
5
55
55
55
Thk lobomtory Eport B not vrI I wl4totd on ourhorizd sjg&trtt e od thz caeer page.
+ Reportable D€rection Limit BRL = Bdow R@ning Limir Page 66 of 165
Page 275
Sample [dentificationM8F-30 2'-4'sA5964l-13
Client Ptoiect #10, -88
Collection Date,/Time21-Mar07 00:00
MatrixSoil
Rec€ived22-Mar07
CAS No. Anobta(s) Re$uh FtoC Ani6 'RDL Dilation Method ReJ, Preparcd Andbzed Batch Anabst
Semivolalile Orgaric Conpounds by CCMS
Semivolatile Orqanic Cornoounds bv SWB46 B27OCPrepared by method SW846 35454
100-01s 4-Nitrc€niline9a-gt3 Nitrobenzene83-715 2-Nitrophenol100{2-7 4-Nitroph€nol62-7s-9 N-Nitrosodimethylamine621-64-7 N_Nitrosadi_n_ptopylamine86-30-6 N_NilrosodiptEDylamine87{6-5 pentachlomph€nol
85{14 phenenthrene
10&95-2 Phenol129{04 Pyrene110{61 Pyr id ine120-82-1 1,2,4-Trichtorcbenzene95-954 2.4,s_Tdchtorophenol8a-0e2 2,4,GTichlorophenol
Sunogale rccot"edes:32140-8 2-Fluorohiphenyt
36?-121 z-Fluorophenol
416540-0 Nitrobenzene'ds
416542-2 Phenol4s
1718-514 Teryhenyl4l4
118-79-0 2,4,6-Tdbromophenol
Totrl Metals by EPA 6000/7000 Seri€s Me.hods
7439-92-6 Mercury BRL
Totsl Metlls by EPA 200 Series Mcthods
27-MarO7 27 -Ma(47 7031592BRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
655758617159
BRL
BRL
12.2
o.2a4
5 .11
14_5
BRL
lSftS dry 1870pS/kS dry 67
UdkS dry 467psfis dry 1870pS/kS dry 467pEl(s dry 467pgtg dry 467
!q(g dry 461pS/xS dry 167
!S,/kS dry 467pg/kq dry 467pdkS dry 467pdkS dry 467
!g/kg dry 467
US/kS dry 461
30-130 %15-110 %30-130 %16110%30-130 %15-110 %
mg/kg dry 0_0330
mdkS dry 0.997
mgi(g dry 1.50
mg/kq dry 0.49e
mg/kgdry 0.249
mgkgdry 0.499
nStkgdry 0.748
filgi KS dry 1.50
mg/l 0.0200
mg/l 0,0150
tng/l 0.0150
mgn 0,0025
mSfl 0-0150
mg,l 0.00040
mgl 0-0150
ftr€rl OO1fi
yo
5 SW846 8270C
5 '
5 "
5 "
5 "
5 "
5 "
5 '
5 '
5 '
5 '
5 "
5 "
M-A
74t'J 22 4 Sit\tel
7440-38-2 Arsenic
741k)-39-3 Barium
7440{3-9 Cadmium
7440-17-3 Chromium
7439 92-1 Lead
n 824+2 Selenium
SPLP Metsls by EPA lll2 & 6000/7000 Sert€s M.thodi
SPLP Extraction Comp{eted
7440-224 Sitver BRL
7440-3&2 Arsenic BRL
It40-39-3 Badum aRL
74404$9 C€dmium BRL
7.1.4047 3 Chromium BRL
7439-97{ Mercury BRL
7439'92'i L€ad BRL
7824+2 S€lenium BRL
Cenrrrl Chcmistry PNrrmehrs
Y. Solids 90.5
1 SW846 7471A 28-MaF07 28-Mar{7 7031495 YP
1 EPA200.7 28-MaF07 28-l\rar,07 7031494 RM
1 "
1 '
l "
l '
1 SW8461312 2GMar{7 2fi\rar47 7031560 BO
1 SW8.{6 't 31260108 2&MaF07 28-[,laG07 7031651 HB
l "
1 ' ,
1 ' ,
1 SW8461312/7470A ' 28-MarO7 7031652 YP
1 SW846131260108 " 28+.,1ar47 7031651 HE
1 SM2540 G Mod 24-Ma'47 24-Mat47 7031470 OP
Thh lsaorclary rcpott ir nol voIAI wuh0ut an raahoriacd slgnature oa the corer page
* Reportabl€ D€tection Limit BRL = Below Repding Linit Pagc 67 of 165
Page 276
Sample IdetrtificationMtF-312'-41sA5964l-14
Client Proiect #30t+8
MatrixSoil
Collectioll Dat€/Time2 I -Mar47 00:00
Received22-Mat41
C"1S No. A&lyte(s) FloS *RDL Dilatto.t Llcthod Rel Prcparcd llnal$,at Balch Aaalls,
Vohdle Orgrni. Compounds
Volatile Omanic ComooundsPrepa.ed by melhod SW846 5035A Soit (tow tevet)
76-13-1 |,1,2-Trid orotifuoroethane(FreoFRL SW 846 8260S 29+ne47 2g+lar47 7031779 RLJ6-l€+1 Acstone107-13-1 Adytonitite7143-2 EerEene10&€6-1 Baomoh€nzene7rt-97-5 EronrocfrloronEthane71274 Brcmodichlorcmethane712+2 Brcrnolorm74J3-9 Brcmoh€thane76-93-3 2-Butanone(MEK)104-51{ n-Bulylbenzene135.98{ s€c-Butylbenzene9S{6{ tert€utylbenzene7!15r.0 C€rbondlsutfdeg-215 C€rbontefachloride'0&SO-7 OrlorobenzenoTtrxl-3 chtoroethaoe67{+3 Chtd.oform
/dkS dry 7 _o
FsftS dry 139pSAS d.y 7.O
Fgl(g d.y 7.OpC,tSdry 7.OpdlS dry 7.O
UdkS dry 7.o
US/kS d.y 7.O
t,{,/k9 dry 'l3.9
pdkgd.y 69.5pS/kS dry 7.0
ls/ksdry 7.0pdkS dry 7 0
Udks dry 34.8pS/kS d.y 7.0
ldxgdry ropdkg dry 13.9
lg/kgdry 7.o
ldrS dry l3.g
ldkS dry 7.0
l€/kS dry 7.0
!S/kg d.y 13.9pdts dry 7.O
ldrs dry 7.0
ldtSdry 7.0
Igrkg dry 7.0
ldkS d.y 7.0
US/kgdry 7.Opgr(gdry 139
lgrs dry 1.0
ldksdry 70
$dl(g dry 7-0pdro dry 7 o
tqft,gdry 'Lo
tqtuSd(y 7.O
ldkS dry 7.o
UdtS dry 7-0
ldkS d.y 7-0
rrdks dry 7.oyS/kS dry 7.0pdks dry 7.o
fd*S dry 7.0
ldkS dry 69.5
UdlqC dry 7.0
ldkS dry 7.o
IdIg d.y 7.O
us/ks d.y 69-5pdkg dry 69.5
ldkg dry 7.o
UdkS d.y 7.0
BRL8RLBRLBRL
BRLBRLBRLBRLBRLBRLBRLgRL
BRL8RLBRL8RLBRL
1
I
1
I
1
1
1
I
I
1
1
t
1
1
I
1
1
1
I
I
I
I
1'|
1
1
1
1
1
1
1
t
I
I
1
I
I
1
I
1
1
1
I
1
1
1
1
1
1
7t-67-3 Chlommethane BRL95-49{ z-Chlorotoluene BRL106-434 +Chlorotolu€ne BRLS-12€ 1,2oib.omo-3dllorcDroDane BRL124-4ar g[bromod{ofomethane gRL
i06-$-4 1,2oib@mo€thane (EDB| BRL7+!l$3 Dibromomethane BRL95-60-1 l,2-Dichlorobenzene BRL541'73-1 1,3-DichloroberEene BRL10646'7 l,+Dlchlorobenzene BRL7t7l{ Dicf orodiffuoro.nethan€ (Freoflt2)BRl75.343 1,|-OicNoro€thane SRLi07-il6-2 1,2-Oichlo(o€thane BRL7s-35-,r 1,1-Dichlo.oeth€ne BRL15trs2 cis-1,2-Didlloireflrene BRL15640-5 l€ns-|,2-Did rroedl€ne 8RL7A47-5 l,2-Dichloropropane BRL1.2-28-9 l,3loidrloropr.opane BRL59+20-7 2,2-D{d{o.oprcpane BRL563-5e€ 1.1-Dichlo@propene BRL1{x)61{1.5 d+1,3-Diclllorcpropene BRL10061{2€U?ns-1,3-Didlloropropene BRLio0-414 Ebyt€nz€ne BRL8768-3 Hexad orobubdien€ gRL
5s1-78{ 2-Herdlono (MBK) 8RL98-82{ lsopopylbonzene BRL99{7{ +lsopropttotuene BRL163444-4 iredlyl bd-bulyl e$er BRL10e10.1 +Modltl-2fentanone(M|BK) sRL7549-2 tvlethyleie .filoride SRLfi-a}3 Naohth.len€ BRLi03€51 n.Piopylbenzene BRL
Thb lzbofllory .q,od is ,toa tdu wiahaut di ardtorw sigaurzrc on the cowt page .* R€podable D€tection Liftit BRL = B€low Repo{ting Limir Page 68 of 155
Page 277
Sample IdentificationM8F-31 2'-4'sA5961r -14
Client Project #30 t -88
Collection Date/Time2l-Ma.-07 00:00
MatrixSoil
Received22-Mat-07
CAS No. Analrte(s) Resuh FIag Uni,l 'RDL Dilutian Method Ref. Prcparcd Aaatrzed Ralch Andljst
Volrtile Organic Compounds
Volatile Oroanic Comoounds
Prepared by rnethod SW846 5035A Soit (tow tevet)
100-425 Styrene BRL
€n0-iD5 1,1,1,2_Tettachtoroethane BRL
79-34-s |, l,2,2_Tetrachtoroethane BRL
127-18 4 Tetrachlorcethene BRL
108€8,3 Totuene BRL
8761-6 1,2,3_Trichtorobenzene BRL
12H2r 1,2,4_Tdchlorobenzene BRL
71-5s$ l,1 ,1_Tdchtoro€thane BRL
79-oGs 1,1,2_Trichtoro€ttEne BRL
79{14 Trichloro€thene BRL75{9{ Trichlorofluorcmethane (Freon 1t) BRL
96-18-4 1,2,3.Tnchloropropane BRL
9s€$6 1,2,+Trimethytbenzene BRL
ro8{/.8 l,3,5-Trimethytbenzene BRL
7541-4 Vinyt chloride1330,20,7 m,p-Xylene95-47 6 o-Xytene109-99-9 Tetrahydrofuran
60 29,7 Ethyt ethef99,1{5{ Tert-amylmethylether637-92-3 Ethytterl-butytether10€-20 3 Di-isopropyt ether75{5{ Ten-Butanol/ butyt atcohol123-91-1 1,4-Daoxane
Sunogale recowies:4604@4 +Eromofluorobenzene
20ir-26-5 foluene4S
I 7A60 0r 4 1,2-Dichldo€thane-d4
1868-si-7 Dibrcmofluorcmelhane
VOC Extraction
Volatile Orqanic Comoounds
BRLBRLBRLBRLBRLARL
8497107107
Field extractBd
!g/kg dry 7.0
ldkS dry 7.0pdks dry 7.0
us/ks dry 7.0pdks dry 7.0pSl(gdry 7.opdks dry 7.0
lgtS dry 7.0pS/kS dry 7.0pS4(S dry 7 0
!S/kS dry 70pdkS dry 7.0
ldkg dry 7.i
UdkS dry 7.O
lgikg dry 7.O
udkS dry 13.9
ug/lgdry 7.Opg/kg dry 69.5
t4lkg dry 7 Opdkg d.y 10
ldkg dry 7.0pg/kg dry 7 O
UdkS dry 69.5
ldkS dry 139
70-130 %70-130%70-130 %70-130 %
pg/kg dry 740pg/kg dry 1480pdkg dry 74.0pdkg dry 74.o
trdkS dry 74.0
ldkg dry 74.0
ldkg dry 74-o
r€/kq dry 74.0pSftS dry 14ApdkS dry 74O
ldkg dry 74-0pg/kg dry 74.Opsn(s dry 74.0pg/kg dry 37OpdkS dry 74.O
!S/kS dry 74-O
lSftS dry 148pdkS dry 74.O
1'|1
1
1
1
1
1
1
1
1
1
I
1
1
1
1,1
l
l
1
1
1
1
505050505050505050505050505050505050
SW8460260S 2S-Msr47 29-Mar47 703177S RLJ
BRLBRL8RLARL
Prepared by method SW846 5030 Soil (high levet)
76-13-1 1,1,2-Tdchlorotdnuoroethane (Fr€o8RL67$rL1 Acetone BRL
107-13-1 Acrytonjtrile 8RL714l-2 B€nzene 8RL
108-86-1 Bromobenzene 8RL
7447-5 Bromochloromethane BRL75'271 Bmmodichtoromethane 8RL75-212 Bofioform 8RL74{}9 Bromomethane BRL78-9!3 2-Butanone (MEK) BRL104-511 n-Bulldbenzene BRL
13$98{ sec_BuMbenzene BRL
98-06-6 tert_Butytbenzene BRL
75-154 Cafton disutfide BRL
s6-23 5 Carbon tefechtoride BRL
108-90 7 Chlorob€nz€ne BRL
7tu0 3 Chloroethane BRL
67S3 Chloroform SRL
VOC 26.Mar-07 26-l ar-07 7031584
SW8468m0B 214ttar41 2g'l/,al-o7 7031642
BD
Thk labortlory report k not valid *dthoq an a.tdtoritpd sipatarc on lhe cowr prye.
* Reportable D€tccrion Limit BRL = Below ReportinC Limit Page 69 of 165
Page 278
Samole IdentificationMtF-31 2'-4'sA5964t-14
Cliept Proiect #301-88
Collection Date/Time2t-Mar-07 00:00
MahixSoil
Received/2-Mat41
CAS No. Anolru(s) Flog Uni.s 'RDL Dilaion Llethod Retr Preprrcd Analf.ed BaLh A8lfst
Vohlil€ Orgadc Compornds
Volalile Orqanic CommurdsPrepared by malhod SW846 5030 Soil (high levet)14-87-3 Chlorom€thane BRL9541F8 2-Chlomtoluene BRf106-43-4 +Chlorotoluene BRL9e123 1,2-Dibronro-$chloroprcpane BRLl2,Ha-1 Dibromochlorornethane BRLloH3.a i.2-Dibromoehane (EOB) ARL74€t3 Oibromornethen€ BRL95{Gl l,2.Dichlorob€nz€ne BRL54t-73r l,3oidllorob€nzene BRL106-46-7 1,4-Did{orob€nz€ne 8RL75.714 Didllomdinuorcmsthane(Freon12)BRL7+14-3 l,toichhoehane BRLr0ru6-2 1 ,2oichlo{oethan€ BRL7t354 t,t-Dichtoroethen€ BRL156-592 cis-1,2-Diciloroethene BRL15e6O5 trns-1,2-OL*tlome(nefle BRL7a€7-5 1,z-Dichloropfopane BRL142-24.9 i,3-Dichloropropaoe BRL59a-2o-7 z,2-Dichldopropsne ARL563-5€{ 1,'l-DlcHo|'opropene BRLt0061{1-5 Cis-1,}Dichloropropene 8RL10061+{ t€ns-1.}Obhloroprcpene BRL100-4r-r Ehy'b€rEene BRL476+3 Hexschlorobutadien6 BRL5e1-78{ 2-H€x€none(MBK) BRL9a{2€ lsop.opytbenzene BRL99{7{ +lsopmpylloluen€ BRL1634{4-4 l\,lethyl tort-butyl eUrer SRL10€.1Gi +iibthy'-2-p€ntanone(M|BK) BRL75{&2 ttehytene dtlodde BRL91.203 Naplrthslene 19210&6$1 tuPropylbenzeno BRLl0H2€ S0r€n6 BRL63G20€ i,1,1.2-Teb'scfiloroethane BRL79-3,1-s l.l,2,2.Tetrachloro€thane BRL127n84 T€t-achlotro€thene gRL
10€-88-3 Tdu€ne BRIa7€1€ l,2,gTdc$lorobenzen€ BRL120-82.1 .t,2,+Trichlorobenzene BRL71-55-6 1,1, t-Tri.filorcethen€ BRL79,rn!5 1,t,2-Tddtloroethane BRL79{15 Tdchlorc€thene BRL75$9-4 Trid ofoiuoronEthane (Froon 11) BRLs18-4 1,2,&Tri$lomptEp€ne BRL95€3{ 1.2,+Tdm€thylb€nzene BRL10&€7{ l,3.9Tdm€thytberEene BRL7.}071 Vinyl d{odde BRI_l33L2G7 m,p-Xylene BRL95474 o-Xylene BRLi09999 Tot-ahydrofuran BRL
pdks dry 1$
t,qikS dry 74o
ud*gdry 74.opgAS d,y 148pdkg dry 74.O
!S,/kS dry 74.O
lgtS dry 74.0
USI(S dry 74.Opdkg dry 74.O
rdks dry 74.o
lgil(g dry 148
FdkS dry 74.opdlqdry 74.o
ldkS dry 74.o
USI(S dry 74.OpglkS dry 740pgXS dry 74.0
!g/kg d.y 74.0
UdkS dry 74.O
lJgftSdry t4.opcftsdry 74.0
lcrrq dfy 74.O
ldkg dry 74.o
ldkg dry 74.O
lgkSdry 740
rgkS dry 74.0
WkS dry 74.O
Ugxgdry 74.Opyks dry 74OpgtS dry 74Opgkg dry 74.o
lgkg dry 74.0
ltgkgdry f 4.0
rdkg dry 74.0pdkg dry 74.0
lrg/kg dry 74.0
IgkS dry 74 o
lgf€dry 74.opdks dry 74.Opgks dry 71.0
ldrSdry 74.0
rc/kS dry 74.o
!S/kS dry 74.Opgikg dry 14.O
Wl(g dry 74.o
f.rgkg dry 74.O
US{lgdry 74.OpgkS d.y Ua
Lr9/k9 dry 74.O
Fdkgdry 740
50s505050505050505050
5050505050505050505050
505050505050
5050
505050
5t)5t)505050
5t)50
505050
SW 846 82608 27)'llar-O7 20+nat47 7031642 m€r
Thi' Iahonlotf rqort it aoa eaIU x,ithatt an outhoriicil slg',attarc oa rtE cover ptge.
+ R€porhble Detection Limit BRL = B€low Repdting Limir Page 70 of 165
Page 279
Sample ldentificatioflM8F.3t 2i-4'sA5964l-14
Client Proiect #l 0 t - 88
MarrixSoil
Collection Date/Timc21-Mar-07 00:00
Received22-Mar-01
CAS No- Analrtsb) Floq 'RDL Dilalion Method Retr. Pftparcd Analyzed Betch Analysl
Volrlile Oiganic CompoundsVolatile Oraanic ComroundsPrepared by method SW846 5030 Soit (high level)60-2+7 Ethytelher994-05{ Ted-amytmethylether637-92-3 Ethyt tedSutyj ether108-20-3 Di_isopropyiether75-6t0 Teft-Bubnol/ butyl alcohol'123-91n
1,4-Dioxane
Sunogale rccoveies:460404 +BromoflU1robenzene
203/-26-s loluene4S
1 r06co74 1,z-Dichlorcethane44
1 6EE-t+t UrDtomodlmfomethane
Ertrft table Petrol€um Hydrocarbotrs
Extractable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
S006$1-9 Gasotine68476'30-2 Fu€t Oit #26847&31,3 Fusl Oil#46855HO-4 Fuel oil #6M09600o00 Motor OilJ001o0fti0 Aviation Fu6l
Unidenlifi€d
Other Oil
Total Petroleum Hydroc€rbons lU
C9-C36 Aliphafic Hydrocarbons 1U
Sunogate rccoveies:$e6-332 1-Chloroocladecane 110
Semivolrtile Org.nlc Compounds by CC
Oroanochlorine Pesticides SW846 8081A
Prepared by method SW846 3545A
SW 846 82608 27-l\tlzt-O7 28.l.lal-07 7031642 '']'al
+CT ETPH 21-Marol 28:Mal.07 7031583 DS
SW8.46 8081A 26-Ma'-07 2a-Mat-O7 7031516 TG
BRLBRL8RLBRL8RLBRL
t03tu93s4
BRLBRLBRLBRLBRLBRL184Celculated as
lgkg dry 74.0
lgkg dry 74.0
l{r/rc dry 74.o
PgkS dry 74.opgkg dry 74O
Pgkg dry 1480
7G130%70-t30%7L1m%7G130 't
mg/kg dry 1o.2mdks dry 4o.2mg/kg dry 40.2mg/kg dry 4O.2qt/kg dry 4O.2mg/kg dry 4O.2mYkg dry 4O.2mdkS dry 4O-2mgkg dry 4O.2mg/kgdry 4o2
40-140 %
505050505050
3q9{0-2 Alddn319 84$ a-BHC319-85-7 b-BHC319,86S d€HCsa{s-e g_BHC (Lindane)57-7+9 chlordan€72-54-a 4,41DDD (p,p.)7255,e 4,4.-ODE (p,p.)5G2e,3 4,4_DDT (p,p,)60-57-1 Daeldrin9s$98€ Endosultan I33213€s-s EMosut[an tl1031.07-8 Endosuifan sutfat€72-2GA Endfin7421.S3-4 EndrinAldehyde76,4,r€ Heptachlor724+s Methoxychlor1024-57-3 HeptachlorEpoxide8001-3t2 Toxaphene5103-71-9 a-Chlofdane
!g/kq dry 7.12
ps/ks dry 7.12
f.iS/kS dry 7.12
Lig/kS dry 7.12
f.ig/kg dry 7.12
tig/kS dry 356
tig/kg dry 7.12
Ug/kg dry 7.12
tiS/kS dry f .12
t/dks dry 7-00
pdkS dry 7.12
ldkg dry f-12
Fdkg dry 7-12
lrs/ks dry 7-12
!s/kg dry 7.12
ru/kg dry 7 -12
t Sikg dry 7.12
US/kg dry 7-12
!g/kg dry 35.5
t4/kg dry |.12
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLARLARL
Thb labo&lor! reporl it notiolld rrllhou t authodze.l slgnalure on the cover pdge-
* Reportabl€ Det€ction Limit BRL = Below Reponing Limir Page 7l of | 65
Page 280
Samole ldeatificationMtF-31 2'{'sA5964 t- t4
Cli€nt hoiect #301-88
MstrixSoit
Collecrion Dat€y'Time2l-Mar-o? 00:00
Received22-Mat-07
CAS N^ Analfta(s) FW 'RDL Dtl"tion Mdhod Rel, Prcpued AE IWI Batch AnalrA
Semivol.dle Organic Compornds by CC
Oroanocfilorins Pesticides SW846 8081A
Prepared by mgthod SW846 3545A
556e3+7 g-C.h&fden€
53494-70-5 Erdrin lGtofl e
S!,rogeie rEcol€ri,gs-1 03a6a+2 4,+Dgoctafl @@Nphenyt ( 542051-2+t Cl€cachbrobipt€fl1 (Sr,
Potucfrbrinated Biohenvls bv SW846 8082Prepared by rnehod SW846 3545412674-11-2 PCB 101611tO+2&2 PCB 1n11rr{1-16{ PCB 12325346+2r-9 PCB 1242126?2,2s{ rcB 1248110974Sr PCB 125411096-82.5 PCB i26037321-?3.s PCB 12621110G14.1 PCB 1268
Sunogate recovorrbsr| 038f.8+2 4, 4-D&Octaf, uombipheflyt (So2061-2a,3 Decad otobiphonyt (Si
Semtvol.railc OiErnic Col|rporEds by GCMSSemivolatil€ Oroanic Compounds bv SW8,l6 8270CPrepared by rnelhod SW846 3545AE3-32€ Acenaphth€ne20&9e€ Acenaphtht4€ne62-53-3 Anitine12G12-7 Anthrac€nei912-24.9 Al?zjne10$33-3 AzobenzendDiphenydi6zine92{7-5 Benzidine56-513 Benzo(a)enlhrscene50-324 Benzo (a) pyr€ne2os€9-2 genzo (b) fuoranlhene1e1-242 Benzo (g,h,i) p€Mene20t{84 B€flzo (k) fluorantiene65{5{t B€nzoic acid10G51{ Eenzylalcoholr11.91.1 Bis(2.dhloroefliory)mehane11t41.4 Bis{2d o.o€thyt)ehor3963&32-9 Bis(2-chlof Disoprotrryl)ether117€1-7 Bis(2-ethylhexythhtnabte101-5$3 +BrofiDoph€nylphenylether8s6s7 Buq/ benzy phthatate&?4{ Carbazole59-5G7,{-Chbto-}methylphenoll0€.{7{ 4-Chlom,adline01{tl7 2-Chtoronaphthalenegtr?a 2-Chlorophenol7m+72'3 +Chloropheny4 phenyt ehef2181X$ Chryseno
BRTBRL
611U
SRLBRLERLBRLBRLBRL17.rBRLBRL
6080
BRLBRLBRL9298RLBRLBRL81412001,O20
1 ,160BRLBRLSRLBRLSRL
BRLBRLBRLBRI-BRI-BRLBRLBRLBRL1.390
pdks dry 7.12pgikgdry 712
30-150 %30-150 %
tgksdry 14.2
US/kS dry 14.2pdrgdry 14.2
ldks dry 14 2pgkgdry 11.2pdk0 dry r4.2
lrgts dry 14.2pdkS dry 14.2pgrS dry 14.2
361ff i%30-1il./.
SW845 8081A 26-Mar47 26-1ra..07 703'1516 TG
ldkS dry .199
Fdksdry 499p9ik0 dry 499pSn(g dry 4SgpEkg d.y 499
lgrg dry 499
FS/kS dry 499pS/kS dry 499
IdkS dry 499
tdl€dry 499
l,gAS dry 499pgkg dry 4Sg
trdks dry 40SpSn(S dry 499
tl€/ks dry 499pgikS dry 499psrts dry 499pqkgdry 499pdxg dry 4ss
!9rS dry 49€pqkg dry 499pS/l€dry 49SpS&gdry 49s
lqkgdry 499pgkgdry 499
rdkSdry 4ss
ldkg dry 499
I
I
1
1
I
I
1
I
1
I
I
I
I
I
1
1
1
I
1
I
1
I
I
I
1
I
1
SW8,l6 8270C 27-M3,t47 27.tulat47 7031592 M.B
Thls bboratt,l ..port is aal valid ttlthoat on outhodzed tignatare on lhe cots We .
i Reportable Det€cri Limit BRI- = Belour ReportiEg Limir Pag€ ?2 of 165
Page 281
Sample [dentificationM8F-tr 2'-4'sA59641-14
Client Proiect #l 0 l - 88
Collcctior Datc/Time21-Mar-07 00:00
MatrixSoil
Received22-Mar-07
CAS No. Anaute(s) Floq *RDL Dilution Method Rel, Prcpued Anrbzed Batch Analyt
Semivolatile Orgenic Compounds by cCNtS
Semivolalile Oroanic Comoounds bv SW846 8270CPropared by method SW846 3545A
53,70-3 Dibenzo (a,h) anthaacene132-€,{-9 Dibenzofuran9tsG1 .t,2-Dichtofobenzene
4,41-73-1 1,3_Dichtofobenzene106-467 .1,+Dichtorobenzene
91-S4-1 3,3-Oichtofobenzidane12083-2 2,zlDichlorophenol64{+2 Diethylphthatate131-11-3 Dmethyl phttialate
105-67,9 2,4-Dimelhylphenolu-7+2 Oin-butytphthalate534-52-1 4,6-Dinitro-2-nethytphenol
51-2V5 2,4-Dinihophenol121-1a-2 2,4-Dinitrotilluene006,?0-2 2,6.Dinit'otolqene117{44 Di-n-octylphhatate206-44{ Fluoranthene86-73-7 Fluorene114-74-1 Hexachlorobenzene87{83 H€xachlorobutadiene7r4T4 Hexachlorocyctopentadiene67-72-1 Hexachloroethane19il-39-5 Indeno (t,2.!cd) pyrene9{!12{ l-Methylnaphthatene78-5S1 lsophorcne91-57$ 2-Methylnaphthatenee5-48-7 z-tltethy'phenol
10+39-1, 3,4-Methylphenol106-44-591-20-3 Naphthelene8€-74{ 2-Nitroanitine99{!'-2 3-Nitroanitiner00{r1{ 4-Nitoanitin€
9€-95-3 Nifobenzene6&75-5 2-Nitrophenol100{2-7 4-Nitrophenol62-7S9 N-Nitaosodim€thytamine621S-7 l,lNitrosodi-n-propylamine86J0-6 N-NitrGodiphenylamine87€6-5 Pentachlorophenola9O1{ Phonanthrcne10&95-2 Phenol129-004 pyrene
110,86,1 Pyridine12G82-1 1,2,4-Trichlofobenzene9t95-4 2,4,$Trichlorophenol€a-0S2 2,4,elricfilorophenol
Surrogale recover'esj
i2140-l 2-Huorobiphenyl
367-124 2-Fluorophonol
41As-6o4 Nilrobenzene4s
BRLBRLBRLBRLBRLBRL8RLARLBRLBRLBRLBRLBRLBRLARLBRL3,090BRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL
BRLBRLBRI8RLBRL8RLBRTBRLBRLBRLBRL1,890BRL2,970BRLBRLBRLBRL
67
60
pg/kg dry 499
ldkS dry 499
US/kS dry 499pdkg dry 499pdks dry 499
!g/kg dry 499
!S/kS dry 499
US/kS dry 499pS/kS dry 499
Ug/kg dry 499
!g/kg dry 499
!g/kg dry 4ggpdks dry 499pdkg dry 499pqkS dry 499
!g/kg dry 499
USftS dry 499
ldkS dry 499
UdkS dry 499
US/kS dry 499pS/kS dry 499
ldkS dry 499pg/kg dry 499pg.4<S dry 49SpSftS dry 499pgkg dry 49S
ldkS d.y 499po/kS dry 499
pgiks dry 4SS
!g/kg dry 4SS
USlkSdry 499
UdkS dry 2000
!g/kg dry 499
udkS dry 499pg/kg dry 2000
lSftS dry 499ydkg dry 499
t g/kg dry 499
rrg/kg dry 499
!g/kg dry 499
!g/kg dry 499
!g/kg dry 499
!g/kg dry 499
ldkS dry 499
UdkS dry 499
UdkS dry 499
30-1s0 %15-110%30-130%
swE46 8270C 27-MarO7 27-Marn7 7031592 M.A
Thi! labotutoty rE ort h wt valid a'ithou an authorized ignatue on ths coter page
* Reporhble Detection Limit BRL = Below Reporting Limit Page 7l of 165
Page 282
Samole ldentificationM8F-312',-4'sA5964l-14
Cli€nt Proiect #301-88
Collection Date/Time2l-Mar-o7 00:00
MahixSoil
Received22-Mar-07
CAS N^ A alr,e(s) nesaU n^g UEia ,RDL DiIt4ita Method Rctr Prepared Amlyzed Batch Anaqst
Semivolrtile Orgr|rk Compounds by CCMS
Semivolatile Orqanic Compounds bv SW846 8270CPreparcd by mehod SW8il6 3545A
4166-62-2 Phenoldi 541718-514 Terphenyl4l4 75118-79-o 2,4,6-Tribmmophenol 66
Total Metrli by EPA 60fiy7000 S€rt€s Method!
7439-974 Mercury 0.753
Total M€lrb by f,PA 200 Sedes Metbodi
74,{r.224 Silver
7440'3&2 Arse'lic
74-4+3+3 gadum
7440-43-9 Cadmium
7,H047.3 Chromium
7113942-1 Lead
7782-4+2 Selenium
SPLP Exbaclion
7.40-224 Salver
74.4-3&2 AFenic
74,4G3+3 Earium
?440-4a9 Cadmium
74i[]47.3 Chromium
743$97{ Meac!ry
7439€21 Leed
202-,r+2 seleoium
G€n€ral Chemislry Prr{met€rs
% Solids
trf lo%30,130 %t1110Yn
mgL/kg dry 0.0(,69
fiigl€dry 1.m
mSikS d.y 1.E0
nEftg dry 0.599
nvl(g dry 0-299
'rB/kg dry 0.599
rE/kg dry 0.8S8
mg/kgdry 1,80
ll€n 0.O2O0
mgl 0.0'l5t)
mg,t 0.0150
rEn 0.0025
ndl 0 0150
mSI 0-fi1O4O
mSiI 0.0150
mg/t 0.0150
%
SW846 E270C Z7-Met47 27-lIiet47 7031592 M,B
SPLP Mead6 by EPA lf 12 & 600{y7000 sede3 Methods
1 SW846 7471A 26-MarO7 28-Mat47 7031495 YP
1 EPA 200,7 2A4td-O7 28-Mat47 7031494 RM
1 "
1 '
1 '
t '
I '
1 SW846l3t2 2flUaF07 26-Mer{7 7031560 6D
1 SW8461312/60108 2A:Mat47 28-[rsr{7 7031651 HB
1 '
1 "
1 '
1 '
1 SW84613'12t470A ' 2g4 d-07 7031652 YP
I Sw8,|ti 1312r'ffi108 ' 28-t a.-07 7031651 HB
1 "
1 SM254 G Mod. 24+rar-07 2+MarO7 m31470 OP
BRL
9.77
134'1.88
12.O
BRL
Comd€led
BRL
BRL
o.0242
BRL
BRL
BRL
0.025.1
BRL
80.7
Thi| lrbotuory nporl b dot tdU w holt an .uhodz.l slgadwe on thc corer page.
'R€portabl€ D€tection Lioit BRL = B€low Repoding Limit Page ?4 of 165
Page 283
Sample [dentificationM8F-32 2-4,sA595l7-07
Client Proiect #301 -88
MahixSoil
Rec€ived
20-Mac07
Collection Date/Timel9-Mar-07 00:00
C,4S fib. Ana|!te(s) FI0C 0ii6 *RDL DiTuio,' Method ftetr Prcparc[ Analt'zed Balch Analtsl
Voladle Organic Compourds
VOC ExtraclonVolalile Oroanic Compounds
pgtkg dry 6.2
udks dry 124
US/kS dry 6.2pSI(S dry 6.2ps/kg dry 6.2
udkS dry 6.2pglkg dty 6.2
UEkg dry 6.2
!Er(g dry 124
!g/kg dry 61 8pg/kg dry 6 zug/kg dry 6.2peksdry 6.2
US/kS dry 30.9
PdKg dry 6.2
tfg/KS dry 6.2
Ug/Kg dry 12.4pg/kg dry 6.2
@kg ctry 12.4pS./kS dry 62
!g/rg dry 6.2
WkS dry 12.4
lSftS dry 6.2pS/kS dry 6.2
r.|g/kS dry 6.2
!g/KS dry 6.2
!g/kg dry 6.2
lgrrkg dry 6.2pgkg dry 12.4
!g/kg dry 6.2
tlS/RSdry 6.2
!S./kS dry 6.2
!g/kg dry 6.2pS./kS dry 6.2
!g/kq dry 6.2pg/kg dry 6.2
tlStkgdry 6.2
t g/kg dry 6.2pg/kg dry 62pg/kg dry 6.2pS/kS dry 6.2pdkS dry 6.2pg/Kg dry 61.4
lrg/kg dry 6.2pg/k0 dry 6.2pS/kg dry 6.2
t4/k9dry 61.8pg/kS dry 61.8yg/Kg dry 6.2
21.Mat47 214J1,at4t 7031261 aDField extracted
Prepared by method SW846 fO35A Soit (tow tevet)
761T1 1,1,2-Ttichtorotdhuorcelhane (FreoERL674+1 Acetone BRL107-13-1 Acrylonitrite BRL
B€nzene BRL104-86-1 Bromobenz€ne BRL74-97,5 Bromochtorom€thane BRL75-27-4 grornodichloromethdne aRL75-25-2 Bromofom BRL74{3-9 Brornomelhane BRL78.93 3 2-Butanon€ (MEK) BRL104 s1€ n-<ylb€nzene BRL13s-98€ sec-Butylbenzene BRL9A{6{ tert-EuMbenz€ne BRL7s-1H Carbon disulfide BRL56-23-5 carbon tetrachloride aRL10&so-7 chlorobenzene 8RL754G3 chloroethane 8RL67.{j6-3 chtoroform BRL71-J7,J Ch/oromethane BRLs5.19-8 2-Chtorotduene BRL106-434 4_Chtorotduene BRLr,6-i2,8 1,2-Dibromo_3drtoropropane BRL124'.ia'1 DabrcmochlorcmedrEne BRL106-s34 1,2_Dibromoethan6(EDB) BRL74-95-3 Oabroolomethane ARL95-5G1 l,2-Dichlorobenzene BRL5'41-73-1 1,3-Dichlofobenzene BRL106-a6'7 l,4-Dichlorcbenzene BRL15-114 Dichtorodifluoromethane(Freon12)BRL75-X4-X l,l-Dichloroethane BRL107-06-2 |,2_Bichtorcethane BRL7s-35-4 1,.1-Dichlom€thene BRL15859'2 cis-t,2-Dichtoroethere BRL1s6-60.5 t?ns_t,2_Didrtorcehene BRL78{7-5 l,2-Dichtoropropane BRL142-28-9 l,lDichtoropropane BRL594:D-7 z,2_Oichloropropane ERL563-58€ 1,1-Dichlo|.oplopene BRL1006141-5 cis_.1,3_Dichtoroprcpene BRL10061-0?6 t?ns-t,3-Didllorcpropene BRL10(!-41.1 EUtyjbenz€ne BRL87{8-l Hexachlorcbutadiene BRLs9r-76€ 2_Hexanone (MgK) BRL98{2{ lsopopylbenzene BRL99{75 4-lsopropyttotuene 8RL1634{44 Methyltert-butyteth6r BRLr0s10-1 4-Methyl-2-pentanone(M|BK) ARL75-09-2 Methylen€ chtorid€ sRL
SW 846 82608 22.Mar47 23+4ar47 7031335 RLJ
BRL91-&3 Naphthalene
Page 12 of 124
This lthorolory rcpod B not tatid *ithoul li a.!rtofiaed signatarc on the corer page .
' Reportable Det€ction Libit BRL = Below Reporting Limit
Page 285
Sample ldetrtificatiooM8F-3! 2-4'sAJ9517.07
Clielt Proiect #301-88
MatrixSoil
Received20-Mar-o7
Collection Date/Timel9-Mar-07 00:00
CAS No. Anabte\) FI"S 'RDL Ditation Method RpJ Prepured Aulyzed Bat!:h At tstVolatile Orgrnic Compounds
Volalile Orqanic Compounds
Prepared by m€thod SW846 5035A Soit (tow levet)
10+6+1 n-Prcpylbenzene BRL'10(F42 5 Styrone BRL63G205 1,1,1,2-Tetrachloroethane BRt79-34-5 1,1,2,2-Tetrachloroehane BRL'127J8-4
Tetrachtoroethene 8RL10&€43 Toluene BRL87{15 1,2,}Trichtorobenzene BRL120€21 1,2,4-Trichlorobenzene BRL71-55-6 1,1, t_Trichloroethane BRL79{o 5 I,1,2-Trichloroethane BRL7941{ Tric oroethene BRL7549-4 Trichtorofluoromethane (F.eon 11) BRL96'14-4 l,2,3-Trichloropropane 8RL95€3-6 1,2,+Trimethylbe0zene BRL108-67{ 1,3,5-Trimed1ylbenzene BRL75{1'4 Vinyj chtoride BRL133G2tr7 m,p_xylene9547{ o-Xytene109-99-9 Tetrahydrofuran60,?9-7 Ethli ether99.-05€ Tert_amylmethytether637-92 3 Elhyttert-butyl elher108.20-3 DisopropytetfE.7s354 T€rt-Bubnol / butytalcohol123-s1.1 1,4-Diorane
Surcgate rccoveries:46040-4 +Bomofluoro,benzene
2037-26-5 Toluene4S
1 706e07 0 1,2-D bhloroelha ne.d41866-5J / Dibromofluoromethane
Ertrrctable Pettoleum Hydrorrrbons
Eidractable Total Petroleum Hvdroca rbonsPrepared by method SW846 3545A
8006-61-g Gasoline68.{76-30,? Fuet oil #26847e31,3 Fu€t Oil #468553{01 Fuet Oil #6M09800000 Motor OilJ00100000 Aviation Fuel
Unidentified
Other Oil
BRLBRLBRLARLBRL8RLBRLBRLBRL
1041061 1 5105
BRL8RLBRLBRLBRLBRL450Calculat€d as
pdkS dry 6.2pdks dry 6.2pg/kg dry 6 2pg/kg dry 6.2
ldkS dry 6.2
ldkS dry 6.2pSl(S dry 6.2pdks dry 6 2pdks dry 6 2
ISAS dry 6.2
!S/kS dry 6.2
irS/kS dry 6.2
!S/kS dry 6.2
!g/kg dry 6.2
Ug/kg dry 6.2
t/9/k9 dry 6-2pdks dry 12.4
ugksdry 62
tS,kg dry 61.8pdkSdry 6.2pg/kg dry 6.2pgikS dry 6.2
ldkS dry 6.2
!S/kS dry 61.8
lgkSdry 124
70-130 %70-130 %70'130%70-130%
nrg/kS dry 147
nlgftS dry 147
nrgr'kg dry 147
nBrk0 dry 147
frg/kg dry 187
B€/kg dry 147
mgtS dry 147
mdkS dry 147
mg/kg dry 147
wlks dry 187
44-140 %
1
1
1
1
1
1
l
1
1
I
1
1
1
1
l
1
1
1
1
1'|1
I,l
1
SW84682604 22-MarO7 23 Mar47 7031335 RLJ
+CTETPH 22-Mat47 26-Ma(47 7031284 DS
TotalPeboleumHydrocarbons 450C9-C36 Aliphattc Hyd.ocarbons 450
Sunogale ecorledes:i3eG$-2 1-Chloroocladecane 147
S€mivol.til€ Orgrnlc Compounds by CCOrcanochlorine Pesticides SW846 EoB1APrepared by method SW846 35508309{0-2 Atdrin BRL udrs dry 6-62 SW846 8081A 22-MaFO7 27-Met47 7031275 TG
Thi! Iabofatory rcpod is not valid tellhorlt 4n 4urtoriud slgnatarc oa the cotet page .
' Reporta5le D€tedion Lirnn BRL = Below Reporting Limit Pase 33 of 124
Page 286
Samole ldeotifica.tionM8F-32 2-a'sA595l7-07
Client Project #30 t-8t
Matrixsoll
Collectioo Dater'Timel9-Mar47 00:00
Rqceiv€d20-Mat4'l
CAS No. Analrb(s) Raak FI'g 'nDL Dilutinn Method Retr Pnpuen A&abzzd Barch AnalFt
Scmivol.lile Orgrdlc Comportrds by GCOrqanochlorine Pestrcidcs SW846 808.1APrspared by rnethod SW846 3550831+€a{ e-8HC319{$7 b-Bl{c319.€6-8 d€Hcsa{se g-BHC (Undane)t-1+s C-hlordane?2-54-8 4,4-DDO (p,p')72-s+e 4.4ODE (p,p')5[2e3 4,4DDT (p,p,]60{7-l DlsHnn95+98{ Endosrrlfsn I!3?13€5-9 Endo6ulfan ll103'l4T-8 Endosllfansulfate7?.20-8 Endrin7421.9!4 Endrin Mehyde78.11.8 Heptachlor72-13-5 ilbtho)rychlor1024-573 Heptact{of Epoxide80or-3s2 Toxaphene5103-71.9 e-Chlofdane5,5:6C34-7 g_Cihlofdane53a9+7G5 Endrin Ketone
Suroga{o recovsridsrt o3a6atz 4,4418-Octafl @robiphenyl (SlN51-2+3 &cachlotobiphenyt (SiPolvchlorinated Bbhenvls bv SW846 8082Prepared by method sw846 355081267+1r-2 rcB 101611104-28-2 PCB 1221r114i-t6-5 PCB 12325346921€ PCB | 24212872-?34 PCB 1248i10€7€91 PC8 12541109&e-5 PCB 12603732+n-5 PCB 1262rilq}la.l pCB 1268
St aro$le r€coyelt6$.'10i864+2 4,4-D&Odaauotobiphonyt (SiN5t-2+3 Deca&brobbhenyt (Sr)
Semlvol.r|b Orgrtrtc Compound! by GCMS
8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI.BRL8RLBRLBRL
30
BRLBRLBRLBRLBRL39.0
BRLARL
3055
BRLBRLBRL
BRl-BRLBRLARLBRL
rdxgdry 6.62pdrq dry 6.62
uqkS dry 6.62pg^gdry 6.52pqrs dry iX,.1
rdkg dry 6 62
t dlq dry 6.62
WkS dry 6.62yg^g d.y 6.62p4kg dry 6.62
ldrgdry 6.62
udkS dry 6.62
ldkS dry 6.62
tglksdry 6.62
udkgd,y 6.62
udks dry 6.62
IdkS dry 6_62pdkS dry 33,1pglkSdry 6.62
Fgtgdry 6.62
Fdkg dry 6.62
*150%3G150 %
ldlgdry 132
rdxs dry 13 2pS4€dry 13.2
ugxgdry r32pgfgd.y 13.2
ldl€dry 13.2
ldkgdry 13.2
vdkSdty 13.2pg4!g dry r3.2
so-150 %yrt50 %
pS/kS d.y 527
ldkgdry s27
uen(gdry g27
pdkS d.y 927
rcn€ dry 927
tglkgdry 927pdl€dry 927
Fgrgdry 927
1
1
1
I
I
I
1
I
I
I'|
1
1
1
I
1
I
1
I
SW846 80814 22-l{at47 27n d47 7(]61275 TG
SW846 8062 2-1tur47 24l.i/.3tr47 7031274 MP
Semivolatil€ Omadc Compounds bv SW84€ 8270CPreparsd by moolod SW846 35508a3{2.9 Ac€naphthenez)&se€ Acenaphtlrylene6-2693 Aniline12Gi2.7 Atthlacens1912-2+9 Atazh€10133-3 Azob€nzene/Diphenyldiazine92{7's Bemijine56{+3 Eenzo (e) anthracen€
SW846 8270C ?}Mat{7 2$rar-07 7031371 M.g
22
Thb btoratory rcpo is noa ealitt uAhoal a sulhottat! signatue .m thz coeer page.
'Reportsbl€ DerectioD Limit BRL:Below Repnting Limit Prge 34 of 124
Page 287
Sample IderltificationM8F-32 2il'sA595l7-07
Client Proied #301 -88
Mat.ixSoil
Collection Dare/Timel9-Mar-07 00:00
Received20-Mar-o7
CAS No, Analrte(s) Flag *RDL Dilutbn Method Rej. Pnparcd AnzllEed Batch Analyt
S€miyolrtil€ Organlc Conpounds by cCMS
Semivolafile Oroanic Comoounds bv SWB46 8270CPrepared by method SW846 35508
&-32-a Benzo (a) pyrene
205-992 Eenzo (b) nuoranlhene191-2+2 Eenzo (g,h,i) perytene
m7{8-9 Benzo(k)fluoranthene65 65-0 Benzoic acid10051€ BenzylalcDhol111-91-1 Bjs(2-chloro€thoxyrnethare111-4.4 8is(2-chtoroethyl)ether3963s32-9 Bis(2-ohloroisopropyt)ether117'81-7 Bis(2-€thythexyt)phthatate101-55-3 +grcmophenyt phenyl ether456&7 Butyl benzyl phthalate86-7,L8 Cabazole595e7 +Chloro_lmethytphenol106-47-8 +Chloro€nitine9l-s&7 2-Chloronaphthatene9s-57-a 2-Chlorophenol7005-72-3 zl-Chlo.ophenyl phenyt eher218-01-9 chrysene53-7a3 Dibenzo (a,h) anthracene132{+9 Dibenzofuran95-5G1 1.2-Dichlorobenzenes41-73-1 .t,3-Dichtorobenzene
10S46,7 1,4-Dichlorobenzene91-94-1 3.3'-Dichtorobenzidine't2oat2
2,4-DichJorophgn1t8446.2 Diethylphthatate131-11-3 Dimethylphthalete105{7-S 2,4_Dimethylph€nolu-74-2 Di-n-butytphthatate53.L52r 4,6-Dinitro-2-methylphenol51-28-5 2,4-Dinitrophenol121 1,12 2,+Dinitrololuene606-20-2 2,o-Dinitrotoluene117-84{ Di-n-ocMphthalate206-44-0 Fluoranthene86.73-7 Fluorene11&74-1 Hexachlorobenzene8748-3 Hexachlorobutadiene't74r4
Hexachlorocyclopentadiene67-72-1 Hexachloroethane1s3-3e-5 Indeno (1,2,3{d) pyrene90-12{ 1-Methytnaphthalene76-59-l lsophorcne91-57{ 2-},tbthylnephthalene9548-7 2-Metrylphenol
l0&39-4, 3,4-M€thylphenol10G44-591-20-3 Naphthalene84,7{-4 2,Nitroanitines9-o+2 }Nitroenitane
BRLBRL1 , 3 1 0BRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLERLBRLBRLBRLBRLBRLBRL8RL8RLARLBRLBRLARLBRLBRLSRLBRL8RLBRL
BRL8RLBRLr,520BRLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRL
BRLBRLBRL
22?2222
2222222222222?2222??22
22222?
222222
22
222
!g/kg dry 927pdkgdry 927
lgxSdry 927pgn(g dry 927
PgkS dry 927pgks dry y27
pslksdty 927pdkgdry 927pg/kS dry 927
!g/kg dry 927
fig/kg dry 927
ridkS dry 927
frg/r(g dry 927ggks dry 927
f.igkS dry 927
Ug/kg dry 927ygks dry 927pg/kg dry 527
l4/Kg dry 927pg/&s dry 927
!g/kg dry 927
t dkg dry 927
!g/kg dry 927pdkS dry 927
ldkSdry 927
ldkgdry 927
!g/kg dry 927pdks dry 927
ug/&dry 927
!g/(g dry 927
lgkSdry 927
ldkS dry 927
uqkgdry 921
lqkg dry 927
uqkgdry 927
lJg^S dry 927
uqkgdry 921
ug(S dry 927
lqkSdry 927
!g/XS dry 927
lqkgdry 927
!g/kg dry 927
ldkS dry 927
ldkg dry 927
ldkg dry 927
Igftgdry 927
Idkg dry 927
UVkS dry 927
lgikS dry 927
lvkg dry 927
SW84E A27OC 23-Mat47 25-Mafi7 713fin M.A
Th labotutot] repod b not ealid hthhoul an aulhortzed sbnslate on the oeer Fage.r Reponable Det€ction Lnnft BRL = Below Reporting Limir Page 35 of l?4
Page 288
Sample IdeotificationM8F-32 2-{'sA595l7-07
Client Project #301-88
MarrixSoil
Received2GMa.47
Collestioo DardTime1lMar47 00:00
CAS NtL A,.abE(s) nesuh F,Ag +RDL Dilution Method Retr Prcparai ,4aalyzctt Datch Analfsl
S€divohtil€ Orgarlc Collportrds by GCMS
Somivolaiilo Oroanic Co.n@unds bv SWE46 8270C
fteparcd by merhod SW846 355081(){141 $ +Nito€niline984+3 NiboberEene84.7+5 2-Nibophenol
10G02-7 +Nitophenol62-7*9 N-Nibcodimethylarnine
62t44-7 N-NitcodirFpropyt€mine86-3t{ N-Nibosodiphenylamirc
87{G5 P€nladllofopheml
8s-01.8 PhenanthEne
r0eF99!2 Pheiol
t2s0{}.{) P},rene
11c86-i Pfidine
12GS2-1 1,2,{-Td{$lo.obenz€n€
2,4,$Trid orophenol8€{e2 2,4,6.Tdchlorophonol
S@rogale rccoveies:
3214c.8 2+hJorobipheny'
6H2a z+ludopllenol
1165-il4 Nilrobanzene4s
416s-62-2 Phenol4s
1718514 Terphe44t4
118-79-6 2,4,6Tdbronophend
Tord Mearb by EPA 6tt00/7000 seri6 Methods
7439-974 Mercury 0.0S85
Tolrl Mctrk by EFA 20O Seri€! Methods
2 SWA46 a27QC 2SMar-07 25-Ma.{7 70iI1371 M.g2 '
2 .2 '2 '
2 .
2 '2 .2 "2 '
1 SrrV846 74714 2&Mer47 27][tat47 7O3r322 YP
'| EPA?OO.I 2aMaf47 2f'dnat47 7031321 HB
1 "
1 '
1 '
1 SW6461312 22+nar.of 22itar47 70313,14 Bt)
1 SW8A6!312/6OI0B 2&tja(-07 24-Mar47 7O314OB LR
1 '
1 '
1 '
1 SWA.451312?470A ' 26.t{ar-.07 7m1409 YP
1 SW8,l6 1312€{tl0B ' 24.'.''iar47 7ml4m LR
1 '
Garerd Ch€mirtry P|]rtdetetr
% Solids
rrgkS dry 3710
rg,lg dry 921pgAgdry 927pS4gdry X710
ldkgdry 927
ldkS dry 927pdkS dry w1ygtks d.y 921pdks dry 927
ldkS d.y 927
lgrgdry 927
udkgdry {2rpg/kg dry s21
!S^0 d.y 527ps*gdry 927
n-rw%1i-fiO %36130 %18110 %30.130 %1&110 %
mg/kg dry 0.033i'
nrdkg dry 1 .0S
ntgrl€ dry 1.63
nrgikg dry 0.544
nE/ks dry 0272
n\gnqdry 0-544
mglt(g dry 0 El6
rtg/f,g dry 1.63
mg/l 0.0100
ngr 0.0150
ttrgl 0.0050
mSI 0.0025
mgur o.0o5o
flgI 0-00040
nrgl 0.m75
mgl 0.0150
%
BRLARLBRLBRL8RrBRLBRLBRLBRLBRL2,570BRLBRLBRLBRL
1A86
88
74a0,22-.t Silver
7/1403&2 Atsenic
7t40-3g3 Eadum
74-{OJ}9 C€dmium
74a0_!7-3 Ch&miun
7.1t992.1 Lead
7782-1$2 S€lenium
1 . 1 8
8_03
55.4
0.931
7,01
177
BRL
SPLP M€trk by EPA 1312 & 6000/7000 Scrt€r Metbods
SPLP Exbaction Completed
7l!l+?24 Silv€r BRL7{1{}-3&2 Arsenic BRL
7r!rG3e3 Badum 0.0126
7+r'(}4ils cadmium BRL7+{}rl7-3 Chrcmlum BRL
74N€7-6 l$€i.{llr/ BR!7:|l1942r Lead 0.0179
n82'492 S€l€niuin BRL
88.3 SM254O G Mod. 24-Mad7 24+rar-07 70314€3 OP
Ihb labodoty npoA ts nof valid x,itho4 an et hoiud stgrrdlare od ahe covrx pagc.
. Reporebl€ Derection Limit BRL = B€low Repo.ting Limit Page36 ot 124
Page 289
SampLe IdentificationM8F-33 2'-4'sAs964l-15
Client Proiect #301 -88
MatrixSoil
Received22-Mat-01
Collection Date/Time2l-Mar-07 00:00
CAS No. Anrlye(s) Flag *RDL DiIAian t{ethod Retr. Pnpoted Adoltzed Batch A4a4st
Vohtile Orgrnic Compoundl
VOC Extraction Field extfacted
t g/kg dry 55
!g/kg dry 109
!g/kg dry 5.5pgkS dry 5.5pS/kg dry 5.5
!g'lq dry 5.5pdkg dry 5 5pg/kg dry 5 5
ldl€ dry 10I
ldkS dry 54.5pSftS dry 5 5pS/g dry 5.5
Mkgdry 5.5
!g/kg dry 27-3
lgftg dry 5.5pdl(g dry 5-5pS/kS dry '10.S
lEtS dry 5.5
!gI(S dry 10.9pdks dry 5 5pS/kg dry 5.5pg/kg dry 10.9
ldkS dry 5.5
i./dkg dry 5-5
UdkS dry 5-5
ldkS dry 5.spS/kS dry 5.5
udkg dry 5.5
ug/kg dry 10.9pg/kg dry 5.5
Udxgnry 5.5
!S/kS dry 5.5
tig/kg dry 5.5
t/g/kg dry 5.5
ldkS dry s.5
ldkS dry 5.5
IdkS dry 5.5
Ug/kg dry 5.5
uERgdry 5.5pqkg dry 5.5pg'l$ dry 5.5pgkS dry 5-5pdks dry 54-5
tigl(g dry 5-5
lgkS dry s.5pgks dry 5.5
lCeS dry 54.5
ldkS dry 54.s
FgASdry 5.5
Volalile Oraanic ComDounds
Prepared by method SW846 50354 Soit (tow tevet)
761!1 1,1,2-Trichlorotriffuomelhane(FreoERL
67541 Acetone BRL107-13-1 Acrylonitrile BRL7145-2 Etenzene BRL104-86-1 Bromobenzene BRL71-97-5 Bromochloromethane BRL75,274 Bromodicttoromethene BRL15-25 2 Bromoform BRL74-33-9 Bromomethane ERL78-93-3 2-Buranone (MEK) BRL10!-51€ n-Eutylbenzen€ BRL13t93€ sec€utylbenzene BRL98-{}64 tefi_gutylbenzene aRL7s,1s-0 cefton disullide BRLs6,23,5 Ca6on tefachtoride BRL1O8-9O-7 Chlorcbenzene BRL75-OG3 Chloroehane BRL6746-3 Chlo.oform BRL7447-3 Chlorcmethane BRL954$8 2-Chlorotoluene BRL106-43-.1 4-Chlorotoluene BRLs6-12'8 1,2-Dib'romG3-chloropropane BRL124-!€ 1 Dibrcmochlorcmethan€ BRL108,33-4 1,2-Dibromo€hane(EDB) BRL74-95-3 Dibrcmomethane BRL9+5G1 1,2-Dichtorobenzene BRL5'{1-731 l,3-Dichtorobenzene BRL10€F467 l,4_Dichtorobenzene BRLr5'71'a Dichlorodafluoromethane(Freon12)BRL75-3+3 l,l-Dichloroethane BRL10LlG2 l,z-oichloroethane BRL75314 l,1-Dichloroethen€ BRLj5e59-2 cis-1,2_Dichloro€thene BRLr5e60-5 kans-1,2-Dicfllorcethene BRL78€7,s |,2-Dichloropropane BRL142,28-9 l,3-Dichlorcpropane BRL5S4?0r 2,2-Dichloropropane BRL563'58{ l,l-Dichloroprop€ne BRL1m61-01-5cis-1,3-Dichloropropene BRL10061{2{trans-1,3-Dichloropropene BRL10G.{1-4 Ethylbenzene BRL87{&3 Hexachtorobutadiene BRL591-78$ 2-Hexanone (MBK) BRLsa€2-6 tsopropylbenzene BRL99{7{ +lsopropyltoluene BRL163{{4-1 Methyt tert-butyl eher BRL10&10-1 +Methlt-2-pentanon€(M|BK) BRL754$2 M€thylene chlorire BRL
26-Ma(O7 26-Ma.-O7 7031584 BD
27-Mat47 28-+'la67 7D31658 RLJ
voc
sw &16 82608
8RL91.263 Naphthatene
Page 75 of 165
Thh hborulory rcpod is noa wlid t4'ithod an aalhoriz,ed slgndurc on the cowr page
' Reponabl€ Dete.tion Limit BRL = Below Reporting Limit
Page 290
Sample IdentificationMtF-33 2'-4'sA5964l-15
Client Proiect #301-88
MatrixSoil
Collcction DardTime2l-Mar47 00:00
Recrived22-Mar07
CAS Na Analfla(s) Retuu Fag *nItL Dilaion Mdhod Retr. Prcparcd Analyzcl Balch At&lfd
vokiile Org.oic Compounds
Volatile Orqanic ComooundsPreparsd by m€hod SW846 5035A Soil (lo!v tevet)
BRLBRL8RL8RLBRL8RLBRLBRLBRLBRLBRL
75-6a-4 TaichloroffuororEthane (Freon 11) 8RL
10965n n-Propylb€nzene10Oa2.5 Styren€6iXF2o5 1.1,1,2-Telrachloroethane79-3'r-5 1,1,2,2-t6trachloroethane127n84 Telrachlorc€thene108-8Ai Tolu€ns87{l{ '1,2,}Trichlorobenzene12+82-l l,2.4Triohlorobenzene7t-55-6 1.1.1-TdcfiloroettEne79{es 1.1,2-Tdd oroethsne79.01{ Trichloroethene
SW84682608 27+,lar47 28+,lEr47 7031658
BRLBRLBRLBRLBRLBRLBRLBRL8RL8RfBRLBRLBRL
97
9098
BRL
BRLBRLBRLBRLBRI-BRLSRL
'
BRLBRL
84
pdks dryldks dryudks dryUdtS dryldks dry!sn(S dryrdks dryFdkg dryrdks dry!S/kS dry
pdks drypdks dryUdkS dryUgts dry!g/kS dry
ldkg dry
l4ikS drypgikS dry
Fg/kg drypgrg drypdks dry
lisfl(g dry
rdks dry
|lg/kS dryygts d.y
5.5
5.5
t0.9
5-5
54.5
5.5
5,1.5
109
I
I
I'|
1
1
1
I
I
1
I
I
'|
1
1
1
I'|
1
I
t
1
i
1
RLJ
9€-i8-.{ 1,2.}.Tdchlofopropane95{3{ 1,2,+Tdmethylb€nzene10&67a l,3,tTrimeht'lb€nz€ne75{t-4 Vinyl cHofido133G2G7 m,pFxyleno9+47{ o-Xyler|e10$9S9 T€t-ahydrofuran@-z+7 Etty' eth€r99ffi€ T€d-amyl m€lhyl ethet637€2J Edryl teft-buhy' e{]eri00-2G3 Diisopropyl€th€r75€to TertButianol/brrtytstcoholi219r-t 1,4-Oioxane
Suoogate Ecoveries:46040.1 [email protected] Tduene-al8t7 0604t4 l,zaichloaoethane44t86€53-I Olbrornof iJoroDglhane
Ertractrble Petlohum Hydrocarboos
Eftadable Total Petroleum Hvd.oc€rbonsPr€pa.ed by m€thod SW846 355088006.61.9 Ga.6lin668a76312 FuelOl#26eaze3l-3 Fuel cll #46€6534H Fud Oil #6ir09U00000 Motor OilJ0O100mO Avialion Fuel
Unld€ntnedOO|€tr OilTotal P€troleurn HydaocarbonsC9436 Aliphatic tlydmcarbons
Srfiogsfe recul/9ttts.'?tsaeS+2 l.CttbrlJoctadecatl€
Semivoldile Orgrric Con[ouods by cC
Orqanocfilorine P€aticid€s SW846 8081APrepared by rnethod SW846 3tl5A3os.m-2 Aftlrin
TCTETPH zf-Mat4f 29.|./'a,-O7 7031590 DS
7G130 %701m%7G1fi%70-tN %
|rgftg dryntg'Xg dryntgL/kg dryndkS d.ymgl€ dryn1gk9 drymdkg dwfirgn(lg drymdks drymgl€ dry
22.1
22.122.1n.1n . l22122.1
22.1
40-11$ %
ydts d.y SW846 80614 2&t Er{7 28-tylar47 7m15t6 TG
Thit lahrratory npod it,ra, wld witho .E ardtortzd sipaAre on lhe covcr pzge.
* Reportable Deiec.ion Limit BRL = B€low R€portirrs Limit Page 76 of | 65
Page 291
Sample IdentificationM8F-33 2'-4'sA5964l- l5
Clieot Proiect #301-8tt
MatrixSoil
Received
22-Mat-Ol
Collection Date/Time2l-Mar-07 00:00
CAS No, Awtrt (s) FloC *RDI Dilutian PEltaten Aflalfred Darch A zllst
Semivohtlle Orgrnic Comporods by cC
Orqanochlorine Pesticides SW846 8081A
Preparod by method SW846 3545A
31+845 a-8HC31+8s-7 b-BHC319,86{ d-8Hc
58{+9 g-BHC (Lindane)
57-14'9 Chlodane
72-u-a a,4.-DDD (p,p')72-5rs 4,41DDE (p,p,)
50-2s_3 4,4!DDT (p,p')60-57-1 Dietdrins5+94€ Endosulfun I33213-65,9 Endosulran tl1031{74 Endosulfun Sulfate72-1O-A Endrin7421-93-4 EndrinAtdehyde1644-8 H€ptachtor7243-5 Methorychtol1024-57-3 HeptachlorEpoxide8001-35-2 Toxaphene5103-71-9 a-Chlordane5s66-34-7 g-Chlordane
s31F,+70-5 Endrin Ketone
Surrogals r€cor,erssr10386-e/ 2 4,4-D8-Octafl@rodphent4 64m -2aa Decechlorobiphenyl (54
Polvc$lo.inaled Biphenvls bv SW846 8082
Prepared by melhod SW846 3g5A
126?4,11-2 PC8 101611104-24-2 PCB 1221r1141-10-5 PCB 123253469-21-9 PCB 124212672-294 PCB 1248110e7-6e-1 PCB 1254110ec82-s PCB 126037324-23.s PCB 12621110G14-4 PCB . l268
Surrogaf€ r€covofl€s.'
1038&812 4,4-DB-OctalluotDbiphenyl (Si
20i1-2aa Decachtorobiphenyl (Sr)
Semivolrtile OrgsEic Compo|rtrd! by ffMS
92i7-5
5G5t3
BRLBRLARLARLBRL
8RLBRL8RLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
73
BRLBRLBRLBRLBRLBRLBRLBRLBRL
75120
BRLBRL8RLBRLBRLBRLBRL8RL
t g/l€ dry
tigks dry
!g/kg dry
!g/ks dry
t/g/kS dry
!g/kg dry
!g/kS drypdkq dty
tidks dry 5.32
ldkS dry 5.32
US/kS dry 5.32
tStkgdry 5.32pgks dry 26.6
!g/kg dry 5.32
lSrkS dry 5.32
tig/kg dry 5.32
lqkS dry 5.32
Ug/kg dry 5.32
rd*s dry s.32
USikg dry 5.32
!g/kg dry 5.32
UdkS dry 5.32
Ug/kg dry 5.32pdkgdry 532pg4(g dry 5.32pdkS dry 26.6pS/kS dry 5.32pg/tg dry 532pg/kg dry 532
30-t 50 %3A-150 %
pdkS dry 33.6pgkS dry 33.6pgkg dry 33.6
Pg/kS dry 33.6
US/kg dry 33.6
rc/kg dry 33.6
rc/kg dry 33.8
t g/kg dry 33.6
!S/kO dry 33.6
i0'15O %30-150 %
1'|
l
1
I
l
I
I
I
I
I
1
I
1
I
1
l
1
1
1
SW8468081A 26-Mar-07 28-l,lar-07 7031516 TG
SW846 6082 27-MarO7 27-Mat47 7031591 SM
S€mivolalile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35454
83-32-9 Ac€naphthanez'o+9t13 Acenaphthytene62-53-3 Anilin€12G12-7 Anthmcene
1912-24.9 Atrazine103-33-3 Azobenzene/Diphenyldiazin€
SW846 8270C 27-Mar0t 28-Mar47 7031592 M.B5,r9 1
5,r9 |
549 1
549 1
54S 1
54S 1
549 1
549 1
BenzidineEenzo (a) antfracefle
Thb labotulory rcpo.t h ,toa valil wilhoal ot authorized sigt tlure on ahe Eover psge
' R€portable D€tection Limit BRL = Below Reporting Limit Page 77 of 165
Page 292
Sample ldefltificationM6F-33 2'-4'
sA5964l-15
Client Project #301-88
MatdxSoil
Collection Date/Time2l-Mar{7 00:00
Rec.eivd22-Mt -07
CAS No. Arnlft (s) Fbc UEi^ 'RDL Dila.iorr Method REI, Przporcd Arnlfzett Bdch At alysl
Semlvol.lile Organic Compounds by GCMS
Semivolatlo Oroanic Compounds bv SW846 8270C
Prepared by mehod SW8,{6 3545A
5G32.8 Benzo (a) pyrenezlrr549-2 B€nzo (b) fluoranthen€191-2+2 Benzo (g,h,i) perylene2orua-s Benzo(k)fluoranhene65{5{ Bedoic acid10G51€ Benzyl alcohol11i-9i-1 Bis(2rhlorcethory)mehan€11t4a4 Bis(2-chloroe{hyl)oher39638'32-9 Bis(2ahloroisopropyl)ether1t7$1-7 Bis(2-ehtth€xytlphdrahte101'5t3 4-Brofibpll€nyl pheny' ether85$&7 Butylbenzylphthalate86.?4S C€rbazoles9-5+7 4-Chlo.o-3-m€thylphenol106-474 4-Clrlorcanilin€91-5&7 Z_Chloronaphthet€ne9s-574 2-Chlorophenol700+72-3 +Chloophenyl phenyl ether218{i4 Chrys€ne53-7G3 Dibeizo (a,h) anthracen€132€4-9 Dibenzofuran955&1 1,2-Dicilo.ob€nzene54r.73r 1,3-Didrloobenzene106-46-7 t,4-Didrlorobenzene9r-94-r 3,3:Didtlorobenzijine'rz\l{}2 23-D-rchlorophenotu&2 Dehyl ph$|slatei31-11-3 Dinrethytphthatatet0s7-s 2,+Dimethylphenolu-74-2 Di-n+utytphlhdates34.52r 4,6-Dinito-2-m€thytphenol5r-2&5 2,4{)initrophenol121-14-2 2,+Dinih.otolu€ne60G20-2 2.6aoinit'Etoluene117-84.0 Di-o-octylphthatate20G44{ Fluoranthene86-7$7 Fluolene11&Zl-1 tbxachlorobenzene67$&3 Hexachbrcbutadienen474 Her6chlorocydop€ntadieneAl-72-1 H€xeafito@ethane19!395 |rde.b (1,2,+<d) pyrcno90-12{ l-trt€thytnaphthalene70-59-t lsophorcne9157{ 2-Methy'n6phthalene95-4+7 2.iiethytphenol1o&3s4, 3,4-Metiylph€nol106-4459t-2G3 Naphthslene8€.74.4 2_Nitoanflines,l)$2 +Nitroailine
SRLERLBRLBRLBRLBRL
8RLBRLBRLBRLBRL8RLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRI8RLBRLBRLBRLBRLBRLBRT8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRL
BRLBRLBRL
fdlq dry 549
tgis dry 549
ldkg d.y 549
tS/t€dry 549ydts dry 549ygtsdry 54Spdkg dry 54SpglSdry 549
ldkS d.y 549
Idkg dry s49pdkgd.y tlgpsikodry t19ygtgdry 549pdrgdry tlgpdkS dry 549pdkS d.y 549
!Sn(S ey 549pdks dry 549
tdkS dry 549
lg/kS dry S49ggrrg dry 549pdl€ dry 54s
tdkg dry 549
dkg dry 549
ldkS dfy 549
UdkSd.y 549
ljgikS dry 549pdkg dry 549perlg dry 54S
lJdkSdry 54S
ldkS dry 549
US/kS dry 549
lSrkS dry 549
ldks d.y 549
WXg dry 549ySlrg dry 549pgkgdry 549pdkSdry 549
ldkS dry 54S
UdkS dry 549
tldksdty 549
tdks d.y 549
Wftg dry 549
lSftSdry S{9pdksdry 549
ldlq dry 549
Fdlq dry 549
lgftS dry 549pgkSdry s49
wtg dry 549
SW846 8270C 27-Met47 2a{ngtr-Ol 7031592 M.B
Thk labontorf npo.l ls tst vald wdlhdu alt duihorizcd iEitaue on iha @wt gqe.
I Reporbble Dct€ctioo Limit BRL = B€low Reporring Limit Plge 78 of 165
Page 293
Sample ldentificationM8F.33 2'-4'sA5964 t- l5
Client Ptoiect #30 , -88
Coll€ction Date/Time2l-Mat4100:M
Received
22-Mar47
MatrixSoil
CAS No. A,nlyz(s) ResaIl Fl"C Ualts 'RDL Dllutbn Method Retr Pnpared Analtzed Batch AnoDst
Sehivolatile Orgaric Compounds by CCMS
S6mivolatile Oroanic Compounds bv SW846 8270CPrepared by melhod SW846 35454
100-01€ 4-Natro€niline98-95-3 Nitrob€nzene88-7t5 2-Niuophenotr00 02-7 4-Nitrophenoi62-75-9 N_Nitrosodimethylamine
621-€a-7 N-Nitr6od-n-propylamine0€-304 N-Nitrosodiphenylanine07{6-5 pentacilorophenol
05{1{ Phenanthrene
10&ss-2 Phenol14.@ PyrenellGe,6-1 Pyridine12G82r 1,2,4-Trjchlorobenzene9195-.1 2,4,$TrichlorophenolaB-o6,2 2,4,6-Trjchtorophenol
Sunogale recoveries:32140-0 2-Fluorobiphenyl
361-121 2-Fluofophenol
1165604 Nitobenzene4'
116si2-2 Phenol45
1718s14 Teryhetryl-dl4
1 1 a-/t4 2,1,6-fibromophenol
1 SW846 8270C 274J,al-o7 za-Ma..0t 7031592 M E
1 '
1 '
1 '
1 "' I '
1 '
1 "
1 '
1 '
l "
BRLBRLBRLBRLBRf
BRL8RL8RL8RLBRLBRLBRLBRLBRLBRL
665563577465
BRL
BRL
1 1 . 3
BRL
3.86
8.r6
BRL
!S/kS dry 2190
LiS/kS dry 54S
Udkg dry 549
lS,ftS dry 21S0
ldkg dry Sl9pSn(S dry 549pgkqdry 549
!g/kg dry 549pg/kg dry 549
US/kS dry 549pg/kg dry 549
!g/kg dry 549
Ig/kg dry 549
USfl(S dry 549
lSftS dry 549
30-1m %I 5-110 %30-1m %15-110 %30-1m%15'110 %
mgr'kq dry 0.0316
mg/kg dry 0.324
mg/kg dry 139
mSI(S dry 0.462
mS/Kg dry 0.231
nE/kg dry 0.62
nE/kg dry 0.693
mSik0 dry 1-39
mg/l 0.0200
mg/l 0 0150
mg/l 0-0150
mg/l 0.0025
mgn 0.01{)
mgrl 0.0(X)40
mg,1 0.0150
mg/l 0.015t)
%
Total M€tals by EPA 6000/7000 Seites M€thods
7439,97€ Mercury BRL
Totrl Metals by EPA 200 Seri€s M€lhods
1 SW846 7471A 28-Ma(47 284llacl7 70314S5 YP
1 EPA200.7 28-MarO7 28$iar07 7031494
1 ''l "
1 '
t "
l '
7440-221 Silver
7,t40-3&2 Aasenic
7440-3S3 Barium
7440-4!9 Cadmium
7c.4o47-3 Chromium
1439-921 Load
77€2-4+2 Selenium
SPLP M€trk by EPA l3l2 & 6000/7000 Seriei M€ahods
SPLP Extraction Complet€d
7440-22-4 Silver 8RL
74-{o-J€-2 Arsenic BRL
71.40-39-3 Bedum ARL
74,{0.43 9 Cadmium BRL
714047,3 Chromium ERL
7'!39-974 Merc!ry BRL
7439-92-1 Lead BRL
77824+2 Setenium SRL
Gcnerd Chemhtry Prr.|t|eiers
% Sohds 94.3
1 SW84613'12 26-Mal-O7 2U'Aar07 7031560 AD
1 SW8461312/60t08 2A-Mar07 2A-Mat47 703'1651 Ha
1 "
1 '' t "
I '
I SW84613127470A ' 28-|!lar{7 70316V YP
1 SW846131260108 . 28-Mar{7 7031651 HB
1 "
1 SM25.l0 G Mod z4-Mar0i 24{i/tat47 7031470 OP
Rt\4
This labotutory Hport is not vaIU wirhorlt an aatlioized sig aturc on the cowr prye.
* Repodable Detection Umit BRL: Below Reporting Limit Page 79 of 165
Page 294
Samole IdentificarionMtF-34 4'-6'sA59ri4l - l6
Clieot Pmiect #301-88
Collection Date/Time2l-Mar47 00:00
Received22-Mar-07
MafrixSoil
CAS No- Anolyte(s) FloC A,,As ,RDL Diltdioa Lldhod ReI Prcpond Andyzztl Batch Ad4lfsl
Voktile Orgsnlc Compoonds
VOC ErlEctionVolatile Omadc ComgoundsPrepared by method SW846 5035A Soil (low l€vel)
76-1+1 1,1,2-Trid orotainuom€hane(Fteo€RLBRL
BRLBRLBRL
BRLBRLBRLSRL
70-9+3 2-Eutanone (MEK) BRL10.-51{ n-But},b€nz€ne BRL13f!98-8 sec-Buttdbenz€ne BRL9846s tert-Butylbenzene BRL75-154 Carbon disulfide aRL56-2&5 C€rbon tetehtoride BRL108.90.7 Chloroberuene BRL75oo3 Chloroethane 8RL67{&3 Chlootorm BRL7447'3 Chlofomethane BRL95-49-0 2-Chlorototuene BRL106-13-4 4-Chlomtotu€ne BRL9&123 1,2-Diblomo-3drbropropan€ BRL
Field ext-act€d
pgltq dry 5.4
FgASdly 1O7
lSftS dry 5.4pdkgdry 5.4
ldks dry 5.4
|lgn(S dry 5 4
ldks dry 5,4
$r'kg dry 5 4pgn(gdry 10.7
Fdts dry 53.6pdkg dry 5.4
ldk€ dry 5.4pdkS dry 5.4
udkgdry 26.8pgikg dry 5.4
rg/tgdry 5.4
ugl€dry 10.7pdrgdry s.4
ldkSdry 10.7
tdks dry 5.4
ldkS dry s.4pg^gd'y 10.7ygiks dry 5.4psilq dry 5.4pdrgdry s.4pdksdry 5.4
IS/kS dry 5.4
udkg dry 5.4pdlq dry 10.7
lS/|€ dry 5.4pSAg dry 5.4pdlgdry 5.4pdks dry 5.4
dkg dry 5.4
udkSdry 5!pg/kg dry 5.4pS/tS dry 5.4pdks dry 5.4
ldkgdry 5.4
[d|(10 drv 5.4
sdkS dry 5-4
!€ftS d.y 5.4
tdkg dry 53.6pS/ksdry 5.4
!S/kS dry 5.4pdkSdry 5.4pslxgdry 53.6
IdxS dry 53.6
lCl€ dry 5.4
1
1'|
I
I
I
t
1
1
I
I
1
1
1
1
1
I
I
I
1
1
1
I
I
1
1
1
1
1
E.Mat47 2 ',,,at47 7031 584 9D
674+1 Acston€
107-13n Acry,tonitrile
71432 B€nzene
10&€S1 Bromobenzene74-97-5 Bromochlorom€lhane
75-2t4 BronEdichloromethane712+2 EromoformZIJ+g Brcmolrlolhane
1244€r Oibro.nochloromethane10eF934 1,2-Dib@moehane(EDB)7{-9t3 Dibrornomethane95-50-1 l,2-Dichlorobenzene54i-73-1 1,3-Oichlorobenzene10se7 l,+Dichlofobenzene
15ffi05 trans-l,2-Dichloroeth€ne7a-67-5 1,2-Dichtoropropane142-2&9 1,3-oichloaopropane
594.20-7 2,2-Dichlonrp|.opane
56+s86 1 , | -Oiddq.optopene
10061{t-5 cis- 1 ,3-Okl{oropmpene
75-343 |,1-Dichloaoethene BRL107.06.2 I,2-Oid{oroethene BRL7s-3s4 1,1-Di.*Jtro€tfEne BRLt5F59-2 cjs-1,2-Dichlorcethen€ BRL
BRLBRL8RLBRLBRLBRL
(Freon12)BRL
BRI-aRtBRLBRLBRLBRL
10061{26tra1s-l,3.Dic.hloropropene BRfi0o4i-1 Edryibe{zehe sRL07{8-3 Hsxacilorobuuad'ene BRL591-784 2.lfe)€none {MBK) BRL98€2€ lsopmpylb€rEene BRLs€7.6 +ls@ropyltotueno BRL1634-0s Methyt bd+utytether 8RL10&10-1 4-Methyl-2-penranon€(M|BK) BRL75{9.2 Methylene cfiloride BRL9l-20.3 N€phthalgne
Page 80 of 165
Thb labodory ftpo.t X not vau N hoar zn.a&torlzed dgaaurc od dte cowr Inge.+ Reportable Detection Limir BRL = Below Reportiflg Limir
Page 295
Sample [dentificationMtF-34 4'-6'sA59641-16
Client Proiect #301-88
MatrixSoil
Received22-MaA1
Collection Date/Time21-Mar-07 00:00
CAS No. Arurlte(s) FlaE 0nits *RDL DiIAio Method Retr. Prepared AnabEed B ch Analyst
Vohtilc Orgrnic ComFornds
Volatile Omanic CompoundsPrepared by method SW846 5035A Soit (low l€wt)
BRL6RLBRLBRLBRLBRLBRLBRLBRLBRLBRL
75s9-4 Tdchloronuoromethane (Freon 1.1) BRL
103{51 n-Propylbenzene100-42-5 St]/rene630'209 1 , I , 1 ,2-Tetrachtoroethane79-34.5 1 , 1 ,2,2-Tetrachloroelhane127-18-a TeFechloro€lhene108-08,3 TotueneB7$1-6 1.2,3-Trichlorobenzene120-8?-i 1,?,4-TrichlorDbenzene71'5!F6 1,1,1-Trichloroethane79.00-5 1,1,2-Tridrtoroethane7341-6 Tdchloro€thene
SW84682608 28-Mat47 28-MarO7 7031693 RLJ
+CTETPH 274J,at47 29-Mar07 7031590 OS
9618-4 1,2,3-Tric*rloropropane95$35 1,2,4-Ttifiethytber'zerle108-67{ 1,3,s-Tim€thylb€nzene7s{1 4 Vinylchloride133c2c7 m.pFxylene9s47-6 o-Xylene109-99-9 Tetrahydrofuran60-29-7 Ethylethets94-05{ Tert-amytmethylether637-92-3 Ethyt tert-butyl ether10€-20-3 Di-jsopfopylether75-65-0 Tert_Butanot/butylalcohol123 91-1 1,4-Dioxane
Sucogate .ecovelies,46Mo1 +Bromofluorohenzene
2037-26-s Toluene-dg
1 7o6uo7 -o 1,z-DichlqcEthane -d4
ft6a-83-7 Dibmmolluoromelhane
Erttsctabl€ Fettoleum Hydrocarbotrs
Extractable Total Petroleum Hvdrocsrbons
Prepared by method SW846 35508
800691-9 casoline68476'3G2 Fuel Oil#z6€47S-31-3 Fuel Oil#46€553{0r Fuet Oit#6nl0960cDol Moior oilJ00100000 Avialion Fuel
Unid€ntified
Other Oil
Total PebDleum Hydrocarbons
CSC36 Aliphalic Hydroc€rbons
Surogata /ecoyei€s:
336-33-? 1-Chloroocladecene
Semivolrtilc Organic Compoudds by GC
Orqanochlorine Pesticides SW846 8081A
Prepared by method SW846 3545A
30$00-2 Aldrin
BRLARLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL
891021141U
BRLBRLBRLBRLBRLBRLBRL
BRLBRLARL
udks drypdks dry
ldks dry
!g/kg dry
UdllS dry
t4/l€ dry
ldkS dry
UgkS dty
!S/kS drypdkg drypdkS dry
ldks drypgks dry
Pstkg dty
t S/kS drypdks dry
ugks dry
ldkg drypdks dry
lldrS dry
ldks dry
IdkS dry
udkS dry
ldkS dry
udks dry
5-4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5 4
5.4
5.4
10.7
5 4
53.6
5.4
5.4
5.4
5.4
53.6
107
70-130%
7&130%
7G130 %
7G130%
mgkS dryftrgkS dryFrglkg drynsfts drymgkS drymgrxg dryhgkg drymgr'kg drymglqC drymg/kg dry
15.0
15.0'15_0
15.0
15_0
15.0
15.0
15.0
15.0't5.0
40-140 %
BRL !S/kS dry SW846 8081A 26-uat47 28 4a147 7031516 TG
That ltboratory Eport b not vaIU xtithalt aE aurhoized sigfiola/-e on the cover page.
' Reportable D€tection Limit BRL = Below R€porting Limit Page 8l of 165
Page 296
Sample ldentificatiorM8F-34 4'{,sA5964l- r6
Clieot Proiect #301-88
MatrixSoil
Collection Date/Tirr1€2 I -Mar-07 00:00
Received22-Mar47
CAS NlL A,tolyte(s) Respk UnjaFlog *RDL D utlon Mdhod Retr Prepated ArBIyel Balch 'lna$sl
S.mlvolsiile Orgatric Compoutrds by CC
Orqanocfi lorine Pesticides SW846 E081APreparad by n€lhod SW846 3545A
319€4€ a-BHC3198s-? b-Blrc319€6€ d€HCs,B{e-e g€HC (Lindane)57-7+9 Chlordanef2-54-a 4,4'-DDD(p,p')z5+e 4,4'-DDE (p,C)50-2+.3 a,a-DDT (p,C)6tr57-i Dioldrin95S98{ Endosulbn I33219€5€ EMosulran tl1031{ru EndosulnanSulfate
7{2r-S3{ Endrin Alrtehyde7411-A Heptachlor724$5 Methorychlo.1021-57.3 Heptachlor Epoxide800135.2 ToxaptEneslo:l-71-9 +Chlordane56G63+? g_Chlordane53494-705 Endrin Kebne
Sunogale @coved6s:t03a6a+2 4,+D&Octefi@robiphenyt (Sr)2051.?+3 Deca&brcbhhenyl (Sd
PolvchlorirEted Biohenvls by SW846 8082Prepared by rnethod SW8,l5 3545A12674n1-2 PCB 10161110+28-2 PCB 1211t141-164 PCB 17325346*214 PC8 1242126n-N4 PCB 1248r1097$9t PCB 1254110s€-02-5 PCB 126037324.23-5 PCB 12621110Gr4-. rcB t268
Swmgete rccowles:103864+2 4,+D+Ociafl@rcbiphenyl (Sr)zostzaa Dacachlototiphenyl (St)
Semivolrtlle Orgrnlc Compo[nds by GCMS
S\i846 80814 26-fi,lar{7 28-l ar{7 7031516 TG8RLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLSRLBRLBRI-BRLBRLBRLBRLBRLBRL
79
8RL8RLBRLBRLBRLBRLBRLBRLBRL
70115
BRL
BRLBRLSRL8RfBRLBRLBRL
IS^gdry 5.22
udkS dry 5.22
!df(g dry 5.72
ldkS dry s.22
ls/t(gdry 26.1ps4€dry 5.22
U€ifgdry 5.22
uS/kg dry 5.22
ldkg dry 5.D
!C4(S dry 5.72
USI(S dry 5.22
lsftgdry 5.22pglk0dry 522
!S/kS dry 5.22pdt.gdty 5.U
ldko dty 5.22
lgkg dry s.22
lqko dry 26.1
Fdtgd.y 5.22
ligftg dry 3.22pgkgdry 522
3G150 %3$1tu %
pS/kSdry 32-8pdkg dry 32.9
ldkg dry 32.8
lSftSdry 32.ApSI(g dry 32.ApSftS dry 32,8pglqdry 32.8
ldkS dry 32.8psA(S dfy 32.a
3G150 %30-150 %
udks dry 371pgkSdry 371
lSftS dry 371
FdkSdry 371pdks dry X71
ldkS dry 371
ldkS dry 371
Idkg d.y 371
SW846 8042 21-Mat47 27-Md47 7031591 SM
SW8,r8 8270c 27-t\'€,t47 '8-ltat47 703'1592 M.B
S€mivdalilo Oroanlc Cornpounds bv SW846 8270CPrepared by meflod SW846 354SA
E332-g Aaenaphthene20+9GS Acenaphthylene6253-3 Anilinot2Gl2-7 Anlhracene1912-24.9 AtBzin€i0$33n Azobenz€ne/Diphenyldiazineg2€7-s Eenzidine$-55>3 genzo (a) anthec€ne
Thh laboturory rcpora it nol &lid idroa cn aut'odzed tiga ue on rle cover page.
* Rpportable Dcrecaion Li6ir BRL = Below Reporti[g Limia Pege 82 of 165
Page 297
Sample ldenfilicationM8F-34 4'-6,sA5964r-16
Client P.oiect #301-88
MatrixSoil
CoLlection Dat€/Time2l-Mar.07 00:00
Received22-Mar-07
CASNo, Analyte(s.) Flos Utia 'RDL Dila.ion Method Rel. Prcpared Anaryzcd Bdtch Anallst
S€mivolatll€ Organic Compound! by CCMS
Semivolatile Oroanic Comoounds bv SW8rt6 8270C
Prepared by mehod SW846 3545A
50-32-8 Benzo(a)pyrene20s-99-2 Benzo(b)fluoranthene1e1 2,4 2 Eenzo (g,h,i) perylene
20748,9 Benzo (k) lluoranlhene65{5{ Benzoic acid100-514 Benzyl elcohot111,S1-1 Bis(2-chtoroethoxy)methane111-41-4 Bis(2-chloro€thyt)ether3gfi eF32-9 Bis(2_chloroisopropyt)ethe,117-81-7 Bis(2-€thythexyt)phthatate101 55-3 4-Bmmophenyl phenyl ether85{8-7 Butytbenzytphthatate86-74-A Cadazoles9'507 4"Chloro-3-methylphenot10s7{ 4-Chloroaniline91's8-7 2-Chloronaphthalene9s'57{ 2.Chlorophenol7005-72-3 4.Chlorophenylphenylether
?16-01-9 C+lrysene51.7G3 Dibenzo (a,h) anthracene132-64-9 Db€nzofuran
9!50-1 1,2-Dichlorobenzene
5.11-73-1 1,3-Dichlorobenzene10646-7 1,4-Dichtofobenzenes1-94-1 3.3loichlorobenzidine12e831 2,4,Dichlorophenol84€6-2 Diehylphthalate131-11 3 Dimethyl phthalate
10s7's 2,4-Dimefl1ylphenolu-r4-2 Di-n-butylphthalae
534-52.1 4,6-Dinitro,2-methylphenol
51-28-5 2,4-Oinitrophenol121r4-2 2,4-Oinibotoluene606-20-2 2,6-Dinitrotoluene
117-644 Di-n-oc\dDhfiatate206-444 Ftuoranlhene
86-717 Fluorene118-741 Hexachlorobenzene
87$8'3 Hexachlorobutadiene
7f4f4 Hexachlorocyatlopentadiene
61-72-1 Hexachlooethane
1e!3+5 lndeno (t,2,3-cd) pyrcne
90'12-0 1-M€thylnaphthatene
78-59r lsophomn€
91-576 2-Melhylnaphthalene
95-4&7 2-Methylph€nol
108,391 3,+Methlphenol106-44-591-20.3 Naphthalene88-744 2-Nitroanilinees{s2 }Niroaniline
BRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLaRtBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRL8RL
BRLBRLBRL
ldkS d.y
!g/kg dry
!9ks dry
Pg/kS dry
tig/ks dry
Pgkg dry
UgeS dry
ldkg drypgkg dry
lgkS dry
lS/kS dry
lgks drypgks dry
LrEKg dry
Lrdkg dry
udkg dry
ldkg drypdks dry
Pdks dry
UdkS dry
irgks dry
!g/kg dry
!g/kg dry
!E(g dry
!S/kS dry
!S{(S drypdkg dry
!S4(S dry
ldkS dry
Pgks dry
PS/kS drypS/kg dry
!g/kS dry
lEkS dry
lSi kg drypS/kg dry
t g/kg drypdks dry
!g/kg dry
Idkg dry
lsfts dry
ug/kg dry
lgkg dry
!4ks dry
!S/kS dry
lqks dry
Wlkgdry
pSftS dry
USftS dry
lgkg dry
371 1
371 1
371 1
311 1
371 1
371 1
371 1
371 1
371 1
371 1
371 '1
371 1
371 1
371 1
371 1
371 1
371 1
371 1
371 1
371 1
371 1
371 1
371 1
371 1
311 1
311 1
371 1
371 1
371 1
371 1
371 r
371 |
371 |
311 1
37r 'l
371 1
371 1
371 1
371 I
371 1
371 1
371 1
371 1
371 1
371 I
371 1
371 1
371 1
371 1
371 1
Thit ldtoratoyeport ie aol valu ''ilhoat on authorized signdue ot1 ,fu colter p4ge.
i Reportal'le Def€ction Limif BRL : Below R€portiflg Linit PaseS) ot 165
Page 298
Samnle ldeotihcationM8F-34 4,{.sA5964l-16
Clieqt Proiect #301-88
Matrix Receiv€dU-MarO1
Coll€rtiori Date/Time2l-Ma.-07 00:00
CAS No- Aaalftz(s) Resell nq A'tur 'RDL Dilaio,, Mzthott Rcl Prcpated Analyed Batxh A^aN
SemivoL.ltle Orgrtric Compoundr by CCMS
S€mivolatile Oroanic Comoounds bv SW846 8270CPr€pa.ed by mehod SW846 3545A
lo(}ol4 zl-Nihtaniline9E€rF3 NitrDb€nz€ne€&7+5 2-Nitophenol1{Xrc2"7 +Nitophenol62-7ts N-Nihosodimethylamine621-64,7 N-Nit'osodi-Fpropylamine&3|).6 N-Nilrosodiphenyl€mine87+Gs Pentacl omphenol85{i{ Phenanthr€nel0&9t2 Phenol129{lo-o Pyreneill}€6-1 Pyririn€r20{2-l i,2,4Tridito@benzene95€5-4 2,4,$Ttichlorophenol88-oFz 2,4,GTaichlorophenol
Sunogale rccowdes:32140.8 2+luor&iphenyl367424 2+luotophenol418frilA Nillobanzene4s416542-2 Phend4s171c-514 Telphenyl4l41 l8-79-O 2,4dTtib@nnphenol
7140-4!9 C€dmium
744@7-3 Ch,omium
7439-97-6 Mef@ry
7439-92-r L€ad
7782-a92 Selenium
Gene.d Cbemirary Prr|meters
% Solils
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
6282597749
lrgrkg dry 1490
!C/tS dry 371pdkS dry 371
us/kS dry 1490
|rSn(S dry 371pgftS dry 371pslqdry 371pdks dry 371
US/IS dry 311
UdtS dry 371
USftgdry 371psrxs dry 371
ldkS dry 37r
ldkS dry 371
ldkS dry 371
30.130 %t+110%3L130 %ls t l 0 %30-130 %tE f i o%
rYrgl(g dry 0.0325
mdkSdry 0 S32
mdks dy 1.40
rnS/kg dry 0.466
ms/kg dry 0.233
(E/kg dry 0.4m
ru/kg dry 0.69S
mgrlqdry 1.40
mg/l 0-0200
mgl 0-0150
r€I 0.0150
msn 0.0025
orSI 0.0150
mgn 0.0fi)40
tngl 0.0150
rEn 0.0150
%
sw846 8270C 27-|,1l€/-47 2a.l,,ar47 7031592 M-A
Tot{l Mctrb by EPA 6000t000 S€.ies Meatodt
7tl:|€l€7i MetEUry
Toral Mearb by EPA 200 Series Methods
7440-?2-4 Silver
7,t4+3&2 Arsenic
7r,qL3S3 Badum
744{4r,9 Cadmium
744G47'3 Chromium
743O.92n Le€d
ZA2-192 Selenium
BRL
BRL
BRL
t0,4
BRL
4.41
3.65
BRL
SW846 747fA ?3-Mat47 294ar47 7031495 YP
EPA 200.7 2&Mar{7 2E-Mar-07 7031494 RM
SPLP Metdi by EPA l3l2 & 600{y7000 Scricr M€thodr
sPtP Extraclion CorfiPleted
lK+22-. Silver gRL
74rloa&2 Ansenic BRL
zaG3*3 Earium BRL
BRL
BRL
BRL
BRL
BRL
91.9
1 SW8461312 26-lrsr{7 26lvl6r47 7031560 BD
1 SW8461e1Z60l0B 2&Ma.-0? 2e-[,ta(42 7031651 HB
1 '
l '
1 SW841i 13f2//470A ' 284at47 7031652 YP
1 SW8,l{i 13'1260108 ' 26-firar-07 7ffi1651 HB
SM2540 G Mod. 24-ttaq9l 2+Mafi? 7031470 QP
Thls tabo.dlorf Epod ls nol vobd wilht.d an authot:hd tlgndarc od the eeer pagE-
+ Reportabl€ Detection Limit BRL = Below R€porting Lhnit P.ge 84 of l6J
Page 299
Sample IdentificationMEF-3s 2'-4'sA5980l-07
Client Proiect #301 -88
Collection Date/Time16-Mar-07 00:00
MatrixSoil
Received27 -Mar-l'l
CAS No. Analyte(s) Result FloC Unib "RDL Dilutioa Method RzI. Pnpand Amlycd Bot.h Analrsl
Volrtile Orginlc Compounds
yOC €xlcction
Volabl€ Oqanic Compounds
Field enracled
!s4q dry
lCftS dry
!s.4q dry
lEkS fiY
!e4q dry
lsfts dryps,4(sdry
lsnq dry
ttdks drpsn(sdry
lsnq drypsn(sdiy
uC4q dry
l,gkc dvp$4{g dlyptkg dy
PS/rq dy
uces dy
tidks dy
fdks dry
fore dryp940 d.y
|'jdks d,y
l4ikS d,ypglq dry
!S/rs dtYydkS dry
!S,4(S dry
ls,4(s dry
!04s dry
lCftS dry
!S4q dry
uSi$ drypsas fy
MceyuS,lg drypS/kS dry
la4q dry
t€,lq dry
l4lq dry
tj$/is dry
tldrs dry
l{As drypEKg ory
t,dks dry
}4fts(yus/rsdy!9'lq dry
udrs dy
voc
sw 846 82608
28{ar.07 2b+1a'{1 1031761 B0
@'AVAI 02-Apt.07 7M1017 mar
Prepared by method SW846 5030 Soil (high lev€l)
t613.1 1,1,2-Trichtorotifluoroelhane(fleon oBL
675,{-l Acetone oRL
107191 A.qy'onitdle 8RL/14x2 Benzene SRt
1o€.0e1 &omobsuene 8RL74.97 5 Bomochlorom€thane 8RL
75-27 4 Bmrnodidlloromelhane 8RL
15-2sz Bomolofln BRL/4.83 9 Eaornomefiane o8l
n.$.3 2-Eulalone {MEK} BRL
104.s1.8 n-EuMbanzqe BRt
r3s.98.8 sec-Sulylbnzene BRL
9€{6 6 ten€uvlbnzene BRL
7+15.0 Carbor di$rllide BFL
5623.5 Ca6on letrachtoride BFL
106'!,0-7 Chlorobenzefle BFL
7rrr0.3 chtooethane BFL
67€6.3 Chlorojom BFLt4 413 Chtosn€lhan€ BFL9549{ 2{hlo{ok{Uene BRL
1m4H 4.Chtootatuene BnL
9612_8 l,2-oibrorno3 chlorotnTane BRL
r21-46.i Dibomochlonynethane BRL10G93-4 1,2{ibrofioethane (EDB) BRL
74 qe1 DblomometuF BHL
s 501 1,2-Dichlombenzene BRL
s41-711 1,3-Dic+iorobenzene BRL106-1+7 1,4-0ichtorcbenzene 8RL
7571s Didlolodinuo{trnethane (Fleon 12) 8RL
701
t(]0
701
701
701
70_t
70-1
70.r
140
701
701
70.I
70.1
351
7 0 1
70.1
110
7 0 1
14!
70.1
74.1
1.40
70.1
70.1
70.r
70,1
70. r
70. r
14rl
70. I
70.1
70_1
70.1
7 0 1
701
7 0 1
fl1.1
70.1
70.1
70.1
70.1
70.1
701
70.1
701
70.1
701
701
70_l
50
50
50
50
50
50
50
50
50
5l)
5D
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
5{)
5t)
5t)
50
50
75.3,43 1,1-Dchloro6than€107{6 2 l2-Dd oroelhane1135! 1,1-Didloroelhene156.s92 ais.1,z-orchloroeh€ne156t0-5 lra1s.l,2-0ioiloroethene7&87-5 1,?'Didtoropop6ne
142-2ss 1,3.Oichlo(opropane
59+20.7 2,2-OichloOpropane
509s€6 1,1-Dicloopopene
10061{1.s cjs.1,}Difloropropene1cd61424 lens-13.DichwoptDrye10041-4 Etrylberuene87{8.3 flexehloobutadienes91-786 2-Hexanon€(M8X)
98-82.0 bopropylb€nzene
9S-87.6 4lsoptDpyiloiuene
1634{4-1 Me$yl ten-bltyl ether10810.1 4-lirethyl-2-pentanonelMlBK)
E@2 Methyiene chlodre9r-2G3 Nsphhalene
8RLBRLBRLBBLBRLBRLBFLBRLBNL8RLBRI8RrBRLBRLBRLBFLBFLBfrLBFLBHL
Thic laborurory kpon it noteali.l h,ttfuat an autho zed sig^atwe oa the coee, page.
+ R€porlable Detection Limit BRL = Below Reponing Limit Page lJ of | 54
Page 300
Sample ldentificationMtF-3s 2'-4'sA5980l-07
Client Project #301-88
Collectioo DatdTime25-Mar-07 0O:00
MaarixSoil
Rec€ived27-Mat47
CAS N^ Analrb(s) Resu! Fl"S 'RDL Dilatun Llertod ReJ. Prepated Anzltzel BoEh AMW
Voldile Org.dc Compoundt
Vohne Oroanic Cofitoourds
Prepared by method SW846 50A0 Soit (high levet)
lcg4tl nfmpyb€nzeng 8FLlm-42'5 Slyr€ie SRL63eAi-o 1,1,1,2-T€t-edtoaedEn€ 8RI793+5 t,l2,2.Tdrad oroeham BAL127.1s4 Tetadlkrc€$€ne BFL108Sn Tdue{le 8FL87-616 i2,+TncHoohenz€ne 8BL12O82r 1,2,+Tddhlrb€r|za1e 8FL71-566 l.l,tTricfiloroqhane BnL791tr5 1,1,2-Tridllotodlare BFL791115 Trd oroehs|g 8RL75i$'r friclllorolbolwn€bano {Freon j1) BHLsjs.4 1,2,3_Tdd oEpropsne BFLe5.63.6 I B,+Tftnerybsnzene BAL10€{/_s l,3,tTdmehylb€nzene BFL75{l-4 Vinyldrtonde BBLl330'2G7 m,Fxy'ene BFLe547{ oxykn€ BnL1@9+s T€lrahydduran BFL&'.297 Efiyt efrer BFLs€{i6.0 Tert{my fi€hyi eher 8RL637-e2-3 Efi!4 tsd{r4i €her BRIl(c2o3 oi-isoproplt etllel BeL7s5{ T€n-Bulanol/ bulyt atcohol 8FL
mnq dy 70.1
Wrq dy 70.1
|lg/lq fiy 70.1
l4lq dy 70.1
lgxS dy 70.1
ljgfrs try 70.1
!9rS ry 70.1
AE dy 70.1
|€&sdry 70.1
tlg,rs dv 70.1
lryt0 frt 70.1
!s4€ fiy 70.1
wrady 70.1
rg,lqdy 701
rgrgry 70.1
wrg fiy 7!.1
|lg/s dy 140
ldb dly 70.1rddliqty ru1
tdko trv ml
N*qd.y 70.1
|4|rC dy 7Ot
l4trgdy 70.1
lS/tSfl 701
wrs d] l{xr
7V130 %7G130%70-13, %70-1fi%
sw 846 82608 @-Apr{7 IX00175l)50505050505050505050505050505050505i)5050505{)5050
@-49t47
12+911 1,4-Doxan6
1&404 +Br'n]onrhrob€'l?c,tlle
&1.2fr TolEno4S
t7060474 l,LDicllooellane44
t8dl-5?Z oibrOmoift$(ErneEtBne
ErOrcaNble Petroleuh Hydrocarbotrs
Eitaclable Tohl Petrohum l|]ldrocadons
Prepa.ed by method SW846 35508
&B-61.9 Gssolhosa7s3c2 Fueloilt2
6817e31.3 Fueloit#4
d86s?00.1 Fu€t 0l +61096!0o0 Moh(OtJ00l0qF0 Ariation Fuel
unklsnif€d
of|er oil
Told PetrdaJm tlydrc&rhons
Cf C36 Atipl|atic l-lydrMftoru
Semlvol.tlle Org.dc Coroportrdi by GC
OEarbd orine Posticid€6 SlV848 8081A
Pfepared by me0pd SWSil(i 3545A
309@2 Alddn
8RL
97
tu94
111
BRLBRLBRt
BALBFLBRI.2,,4{0Calculated as
a,{Eo2,480
192
nvro dry 711
dMg dry r11
n'gnqdry 741
mglqdry 741
|rdrg dy 711
mE*gdry 741
mdhdy r4l
nC4qdy 741
m$4q dty 141
ndlg fy 741
4+144 %
HI€ dY
n arc7 3GUar{? nF1Z2|cT ETPH
S1VB/|6 $8lA 28lt€f47 (|z.Aprfl 7031739
Ihk labonlory Eport t$ rrorvtlid tolthou on otrthoriud sigturure od th2 dtee! pa#.
' Repo.tabl€ Detection Limit BR! = Below Reponing Limit P€e 34 of 154
Page 301
Sample IdentificationNI8F.35 2'-4'sA5980l-07
Client Proiect #30 | -88
MatrixSoiL
Received2'7 -Ma(O'7
Collectioo Date/Time26-Mar47 00:00
CAS No, At'abte(s) Result Flog Unils +RDI Dilu,ioi Method Rel. PEparcd Aruuzed Balch Ahallst
Semivohtil€ Organlc Compo{nds by CCOroanochlodne Pesbcides SW846 8081APrepafed by method SW846 3S45A319{4€ a-BHC3r9 S5-7 b_BHC3re-86-8 eat&5&3s s g_BHC ltindane)t'7+9 Chlofdane2,5,r_! {,4'.000 (p.p }72 5ts 4,-4LD0E (p,C)
5G2*3 a,4LDoT (p,p )6GtJ oieldnn95990'0 End6ulfan I3"13.654 Endosufan tlr@1{7-€ Endosullansultaten2as Endin71tr.934 EndrinAtdehyde7e444 Heptachlor7?135 Methoxychlor102157'3 H€ptachlorEpoxide3001-35'2 Toxaphenes103 /1 9 a{hlordane556&3f7 g.Chiordane
t3194?0 5 Endin K€tone
t0M-81, 4j-Dg&hn@djphenyl(Sl
45t.2+3 Def€$lotobiplgnyl(Si
Potuchlorinated Biohenvh bv SW846 m82
Prepared by method SW846 35454
12674 I|2 PCB 1016]lr04 2&2 pCB 122111r1rr6.5 PCB i2328t169.214 PCB t24212672'2s-6 PCB 124€110e76s 1 FCB 12541r0$82.5 PCB 12603132+tr5 FCg 129211r0cr44 PC81268
t886a+2 4,4 DB CYqnuotdiplp1l't (g )20512+3 Dec&tloafulgDyl(St)
Srmivolstil€ Orylnic Compounds by GCMS
Semivolalile oryanic ComoounG bv SWB46 8270CPrepared by rnethod SW846 35508
&L3? I AceGphhene20S-96€ Acsnephh!4ene62 53 3 Adln61n.12.7 ff{hrec€ne1912.21-9 Atrazine1@3'3 fuobedeneniphenytdiaTine9.87.t Bazllinessst3 Benzo(a)anhracen€
BFL
BRL
8FL
8RL
BRL
BRI.
BRL
BRL
BRL
BRL
BFL
BHL
BHL
BFL
BFL
BFL
BFL
B8L
BRL
BRL
67
102
BBL
BRL
BRL
BBL
BRL
8Rt
194
ERL
8RL
ffi
95
3it4
33.4
3r.,133.4
167
33.4
334
334
B 4
33,1
33,1
33.4
33_4
33.4
33_4
33.4
33.4
167
33.4
3:r.4
33.4
pg/ksdry
|'}g*S dry
wlg ey
tiS/r(g drypgks dly
!s/kq dypS,tS dy
tS4(e dy
$4q dry
!s4q dry
lsnq dry
lgftS dry
tigts dy
Ps*s dry
!SI(S dry
!s/rS dryps,ks dry
|]drs dry
lEtq dly
/9t9 dry
lrg/lq dry
w150 %
3Gtfr r.
!S/kg dy
fdkg dry
yg/rq dy
!04q dy
ys/rc (lly
lslq dy
!g/l€ dry
!s/rq dry
ldfs dry
30-1fl %
&150 %
sw846 80ErA
I
I
I
I
1
1
1
1
1
1
1
I
I
1
I
l
I
!
2E-Ma,{7 02-!Or-07 rc61739 TG
BRT
1,lffi
BRL
3,120
BRL
BRL
8RL
28,000
ldlq dy
udlq dry
!S4q dry
ldlq dly
lglq dry
ldre d'ywke &y!S4q dry
sw8.46 8$2
sw846 827m
66.8 1
66.8 |
66.8 1
66.8 |
66.8 1
516.8 1
66.8 1
66.8 r
66.E 1
919
9 1 9
9 1 9
9 1 9
9 1 9
9 1 9
9t9
s19
28{1 07 3+Mar-07 703173E SM
29{rar47 0GAprr)7 703124 M.B
thk labotulory repod is not rdlid withou! er au,horized sigt'sturc on the .orer page.
* Reportable D€iection Limit BRL = Below Reporting Linir Page J5 of 154
Page 302
Sample IdefltificationM8F-35 2'-4'sA5980347
Client Prciect #301-88
Matri{Soil
Collection Date/Time26-Mar-o7 00:00
Received27.Mar07
CAS No. Anolyk(s) FI4S Unia *RDL Dit,tlion MelM ReJ, PEpand Arralrz"n Babh Aaalyst
Sfmivoktile Orgstric Compounds by CCMS
S€n*volalile oroar c Com!@nds bv SW846 8270C
Ptepared by msthod SW846 35508
sc3?.8 Benzo (a)pyen€20t90.2 Senzo(b)nuoanfEne1s1.2+2 &nzo(g,h,ilp€Mene207{8 9 EaEo {k)fluo€nhene6s-€6{ B€Qoicacidlql5r-6 Eenzy ajmhol111.9r-r B6{2d1lorc6hory)nehaner11.4r.1 8is(2dtoroetryl)dErwa Eias(2{tordsoprEpyl}e$er11?{t? E}is{2€t'ytr€xy')Fthehte10n553 +&omopfienylpftff/eher85{&7 suv bd[y' phtEhte
8&7,1-8 carb€zol€5S.5G7 +cHofo-9melhylpfi*tol16-.47-8 +Ctoioaniline9r-5&7 2{htoronadlhalene9'57-8 2{fitoroph€rd700$72.3 44 orophenyj phefiyleth€r
2lS!r.9 dvlsene53703 Db€ru0(a.h)antlrac€na13e{.tg Ub€nzoluanF50r t2-Dic]{orobenzene!11-7!1 l,$oidOrd€il?€ie106-{6-7 l,lH}cnloaob€nz€n€9t9r-r 3S.Ddorobeoidnerzo.slz z,4.DchtoroFh€noi3/r5G2 Dia v phhatate
131n13 Un€dM phflateh
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S,RLBRL
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Tkle laborcbry repfi is not volid d!ho.!t ad acthorkd slgndur. oE rte coeer page.
I Reportable Dct€ction Limir BRL = B€low Reporting Limit Psge l5 of 154
Page 303
Salnple JdentificationM8F-3s 2'-4'sA59803,07
Client Proicci #301_88
Collection Date/Time26-Mar-07 00:00
MatrixSoiL
Received27 -Mar-0'7
CAS No, Andyte(s) Flag Units *RDL Dilution Method Retr Pnparcd Analyzed Botch Antll.st
S€mivolatll€ Orgrnic Compourds by CCMS
Semivolalilo oruaric Compoun6 by SW846 8270CPtepared by method SW846 35508
100.01-6 4-Nitroanitine!E-95 3 N'trob€nzene0&?5 5 2-Nitropt€[email protected] / 4-Nirrophenol6?_759 N,Nitrosodimetiylamine621.6+/ N-Nilros€di-n-propylamine8630{ N-Nilrosodiphenylamine
tr/lFs Pentadlorophend
E54r'8 Phe0anfrenelod 9.t2 Phenol129,00-0 ryrene1rGB6r ryridine12G02-1 1,2,4-Tiohlorobenzene95€s-4 2,4,5-Tnchlorophenol33{62 2,4,FTrichlorophenol
Pt-@4 2-FhJotobi*]€nyl
367-12.4 2-FhJolophenol
1165601) l&frObenzene4s
1tou62-2 PlErol4s
1/1e51-0 l6rpl6nyl-d4
lte44 2,4,6-Itb@n]opheflol
ERL
BRL
8RL
8RL
BRL
BRL
BRL
BNL
2,90n
8ff1
56,500
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BFL
B8L
BFL
55
66
75
65
41)
sw8!6 6270C 29-M3r47|]g/lq dry 3670
ldkS dry 919
lsnq dry 919
fdk! dry 3670
pSAS dry 919
Irsas dry 9r9
|alls dy 919
|aAS dy 919
llg,ts dy 919
MCet 919
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la4(sfry 919
l,qn(Sd] 9rg
uq/l(Sdry 9rg
*13,%
15-110 %
3tJ-19 %
11110%
w130%
1 1 1 1 0 %
mgaofiy 0 0366
mgkg dly 122
'ngle dry 1.83
mS4(S dry 0.610
mgrs dry 0.30s
'ng/|(S dry 0.610
mSfiS dry 0.91s
mglg dry 1.83
rngl 0.0100
mg, 0.0150
mgn 0.0060
no,l 0 00e5
mgl 0.0125
mg4 0.00041
mgl 0.@75
mgl 00150
09Apr{7 7031774 M.8
Totrl $letals by EPA 6000/7000 Sertes Merhods
Total Metal! by f,PA 20O Seri€s Methods
7440-e.4 Silrcr
744G3F,3 Barium
7140rA3 Cadmium
711447-3 Ciromium
7€9-@r Lead
rl821r2 Seledum
03'AF'{7 7031810 YP
02-Apr{7 7031809 HS
2&Mar-07 7031763 BD
02-Apr{7 7031805 LA
02-Apt{7 7031806 YP
02-tg{7 n31N5 tR
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SPLP Exlrachon Compl€led
14!+n-1 Silver BRL
744$?&2 Acenic 8RL
74|l).393 B€rium 0.0126
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74,|0-17.3 Chrc.niurn BRL
743s97$ M€rc!ry 8RL
74N42.1 tead 0 0300
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Cenetrl Chemistry Parrmeiers
% Solids 81.3
sw8{513t2t47M
srt846 13.12/ffi106
Sll2tl0 G Mod. 30+,la147
Th labo.atory repo.l is noa vdd flilhoat aft aulhoized sigadute on the cover page
* Reporlable Detection Limit BRL = Below Reporting Limit Pege 37 of | 54
Page 304
Sample ldentificationM8F-36 4'{'sA59803-08
Cli€nt Proiect #30t-88
Collection Date/Time26-Mar47 00r00
Received27-Mat-07
MalrixSoil
CAs No. Aaalr'te(s) Reszlt FloS Uails 'RDL Inuion Med.od Rel, Prcporcd Anatyzed Eokh A^aIFt
Volal s oroanic Conbolnds
Prepared by method SW8,l6 5030 Soii (high tevet)
78131 t,12-Tidtlomtrifluoroehane(Fr€on BRL
@5+1 AaetoG BRL
ro7-13,j A('yloiitrile BRL71w2 Benzu€ gFL
1@€61 Bonobglz*ts BRL
7+97-5 Eomoahlom|nelhane BFL7rzr4 Eomodkfilorollletturle BRL
E&2 Eomolorn BRL7{{3€ &mdnohale 8H!
?&s-3 2-Buhnon6 (MEK) 8Rt1or-51.9 n-Butylbenlens gFL
1ffi8 s€eBulylbnzen€ BfiLsc{G-6 tert-Bulyibnzene BFL7s150 Carhsr dEllfrde BRLsn-2o5 Cadon tdraclto do 8Rt-
10&9G7 ChlotEh€nzene BFtt5+3 Chtoro€lfiare BRL
57-66-3 Ctbrotonn BRL7447-x chlotun€tl*ne BFL9549'8 2tl{orDtoluene BFL106'13-4 4-Cl*rotdu€n€ ARI
9c123 1,2-0ib.Cfilo-Jdltooprogane BRL12'1.4&l Dib.unod ololnehanB 8RL0e9+4 lz$bronoelhane (€DBl 8RL7+9+3 obrcnun€lhane BfrL96JG' 1,2-Dicl orcbenzene BFL
5/rl t+l l,C.Drcl orob€nzene BFL106',167 l,l-Did{oobenz€n€ BRL
Volstile Org{dc Compound!
VoC Ext-adion
?5.71-8 Dchtorodiffloroftetiane(Fem12)
75-3,r.j l,1-Dciboetune
1n&2 12-Did doghane?+354 1,l_ttichlflo€ltlene150{92 cis.l,2{)idoro€henor56-6Gs tans-1,2€ichloros$€n€1t41.s lp-DicfloroFopan€
1.2-?44 l,3.0id{ofop.ogane
s+a}? zl{icftloropropans5G358{ l,l-Oido@popen€
m61{r.5 cis-1,3.0idhropnDslslF€l€{ tra1s.1,3-0ichtooproFemro0-.1J EhyoeizBn€O€&3 lt€td*rDbutadenes1.74€ z+to|rldts (MBK)
S-€2-8 lsoprlDrlben!€ne9s{45 4kopropyibfusot6a4-0t-. ohy'toii.butyl€tEr1{€ro1 4-f'lettryl-2{enbndl9{MIBK)754&2 Mdtyl€ne d oidegtltt-s llepht|ql€ne
284sfA7 28-lrar{7 7m1767 BD
C2$rfl 02-Apr{7 40017 oLr
Frdd exlra.led
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ltlqdy AEo
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tdkCdy r04
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ldh a r04
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pd*S dry t04
t.qh d'y 208
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!C,lq*y 1(X
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!S49 dry 10{
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$nqdry to4
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|lgrg d! 104
vclc
sw 8,46 82608
SRL8RL8FLBRLBfiLBFLBRLBRLBRI.BRL8RLBNLBfrLBFL
BRL
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g
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fr5i)
50505050505050fr
5050505050505050505050505050505o50
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This hbodo.y rcport ts not vtIU *itltot( z^ zathorizd stgt ficre oa thc cover pqe.
'R€portable Detectioo Limi. BRL = Below ReportinC Limit Page 38 ofl54
Page 305
Sample [dentificationM8F-36 4,{,
sA5980348
Client Proiect #301-88
Collection Date/Time26-Mar 07 00:00
MatrixSoil
Reccived27-MaPl1
CAS No. Analyte(s) FloC Unix +RDL Dilatioa Melhod ReJ PrcpoEd Atebized Balch Analrs.
Volrtile Orgrnic Compounds
Volatile Orcanic Comoounds
Prepared by method SW846 5030 Soit (high tevet)
r016t1 n-Prcpylbenzene BRL100-42-s Styrcne BFL83020{ j,i,j,2_Tetrachlorcehane BFL79.345 1,1,2,2-Telrachlooethan€ BRL12718-1 Tetrachloroehene 8RL103{3 3 Toluene BRL07{1{ l,2,3,Trichlorcjbenzen€ BRL12ss?-1 1,2,+Tridlootcnzene BFL7r-5s-6 1,1,1_Trichtoroethane BRL7s{0 5 1,1,2,Tri$loroelhale BRL79-01-6 T.idrtoroeti1ene BFL7s{+,r Tdc}torofluoromelhane (F€ofl 11) BFL96r+,r jl,3-Tdchloropropane BFL95-63-6 12,4-Timeltrytb€nzene BBL108-67.0 j,3,S,Trimelhybenzene 8BL75.0r-4 Vinytdtoride 8RL'300.207 m,Fxyt€ne BRt95-47{ oxyi€ne 8RL10s99.9 Telohydroturan BRL60 !e.7 Ettryt eher BRLs94.n5r Tenn|lrytmeiiyi elher BFLa7-e-3 Ehyl lerl-butyi eber BFL108-2G3 Ojsopfop/ elhe. BFLtus{ T€rt€ubnot/ buM ajcoitoi gFL
12&e1.1 l,-4,Dioxane BBL
16-sI1 4-Bononurmbenzene
Nt-265 Totuer,edB 1001tw474 | 2aichloroetharc44 94t36+53-/ Dihmnofluo@nehane 1'14
f, rlrrctrble Petroleum Hydrorarbon!
Exkadable Total Pelroleum Hydrocarbom
Prepared by method SW846 35508
3ao6-619 Gasoline BHL6e47 02 Fuet Oittz BRL6B47E3rn Fuet Oitt4 BRL
Er55s-00'1 Fuelol*6 BHLms€ldtoo Mo|o{Ot BRLJ0010{000 Aviafon Fuel BFL
Unid€nlified BFL
Olhero BFL
Tolal Petrdarm Flydro..adons BFL
C$C36 Aliphatc ftdocaftons BFL
ttl6-3?2 l-ClloifrE&cme It7
Semivolrtil€ Orgrnic Compouods by CC
oroanochlorine Peslicjdes SW846 8tr81A
P.epared by method SW846 35,{5A
30e{0.2 Atddn BRL
lgrlg dry 111,1
ldks dry 104
|-€AS dry 104
lElg dry r04
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lylqd] ltx
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pSrkS dry 104
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ldrq dry 10.{
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ISAS dy 104
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tidr(S dry 10,1
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7Flin %
7+130 %
/0-130%
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sw 846 8260A
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50
50
50
50
50
50
50
50
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50
50
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50
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50
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Thb labonto4t rcpotr is not edld {ithotd on authorized sipta.urc on the cnwr page.
' Reportable Detection Limit BRL = Below R€porting Limit Ps€e Jq of 154
Page 306
Sample ldeotificationM8F-36 4'-6'sA59E0l-08
Client Proiect #301-88
MalrixSoil
Rec€ived27 -Matr41
Colle€tioo Date/Time26-Msr47 00:00
CAS No. A"rlyte(s) Resatl Flag Unitt *RDL Dil ttion Method n4 Prcpared Analyzed Batch Anzlfdt
S$rivolatile Orgrntc Compoundr by CC
Ordanodllodne P€stcii€d SW846 808rAPrepared by method SW846 3545A31!IC4-6 a€ltosr$or7 b€rcsre€6.E +BHC5&se.s $BHC (Lindane)5t.7L9 O o|lhaE
72-5,r€ 4,4,-0tt0 (p,p )72-sf,e {,4'-DDE(p,p')
5G293 4,{.-DDT(p,p)60.5?n Dielddnss9{l-8 fudcufisn I3!p13.664 Edo€ulfal lltm1{7{ EndGulhnsulfaten.?!4 Endrin71214-1 Endrin adehyd€7!{,Hr H€phd{otz{3-5 tt4ethoryd orr@'Lt-3 Heghd o( E0oide8m1{9? Toraph€$e
5103,7r-9 a{ldoadale556e317 g{hla.dane
534947G5 Endnn K€tone
twe12 1l-DBMtunrdithst4(St)
,'61-21,. oed,bobifunrlBt)
Pdvd odnaled Bi*envb bv 5W8,4{i 8082
Preparcd by method SW846 35454
r26r+x4 rcB 101611104?C-2 PCE 1221111{1-16.5 rcB 1E2s346+21-9 PC812{212t72.294 PC8124811(s7-€s1 PCB 125{r1o9€€-5 PC81250Te+es Pc€IZgzr11fi!r1.,1 PCB 1266
54ro98l, /eco€rt rit@644-, 4Ae&htthr&iptenf(s4Mtas Def€f,llotoLw(*l
Semivolstile Orgaolc Compoutrdr by @M
S€mivoladle Ooadc CdnmunG bv SWt46 8270C
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2t. al{7 02{pr{7 7m1739 TGBRLBRL8Ft8RL881B8LBFL
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67105
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td)
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lth dv!g/rq ryU91q dry
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ldh dv
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43.343.34334332164i1.3
€.3431€ 34]3€ 343.3
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* Reponable Detection Limit BRL = Bcbw Reporting Limh Page,(} of 154
Page 307
Sample IdentificationM8F-36 4'-6'
sA59803-08Cliept Proiect #
30 l -EEMatrir
Soi lReceived
27-Mat 07Collection Date/Time
26-Mar-07 00:00
C4S No. Analyte(s) F,oe Ani6 *RDL Dilutioh Method ReL Prepatert Ahulyled Batch An.tlfst
Semivohtile Organic Compounds by cCDtS
S€mivolalile Orcanic Compounds bv SW846 O27OCPrepared by method SW846 35508
s0-32-6 8€nro (a)pyf€nemtes 2 8€nzo (b)nuoranthenelel-21-2 &nzo(g.h,i)p€ryI€fle207{€-9 Benzo(k)lluoranhene55-€€4 &nzoic acidr0cs1.6 Benzyl alcohotr r r .91-t Bis(2{hlobehoxy)nEthaner11-4,t-4 Bis(zdo{o€lht)elher39c38-32-9 Bis(2+htororsopropyl)elher117.017 8bl2+htheryDphlhatale1fi-55n 4-Brcmophenyl ph6i/ €her0s{&7 &rtyt benzyl phthatate86 t r.8 Cabazole59507 4{hloro-}fistnytphend106-17{ 4-Chloroanitine91-5&7 2,Chloromphthalenssasrr z_Chtorophenol7w-12 3 +Chtorophenyt pheny' €th€r2r3{r.9 Chrysene53143 oibeflzo(a,hianftraceoe132.6,1.9 Dibffzofuran95-501 1,2-Dictoobenzenes41.?31 t,3.Ddttolobenz€net6-4+7 1,4-Ckhlorob€nzene9144.1 3,3',0ichtorob€nzidtnet1r89.2 z,1-Dtltuotgnd8466.2 Delhytphthatater31.r1.3 Dimebytphdlalate105 67e 2 4-tlmelhylpheoolw1q.2 Di_n_butylphhatale$452.1 4G0inilrG2-melhy,lphenol5r-2s.5 2,4-tlnitrophenol121-t+2 2,4-Oinitolol0ene606.2G2 2,6_0iritrotoluene117444 D_n_ftl/ph$alate2c6.14-0 Fluodnthefte
11&7+1 ll€xadotobenzene07{€.3 Hexsdorobutadienen47.4 ltexadtloncydopefilad€nett12-1 }l€xadkriE€liane1s3 3e5 Indeno (1 ,2,3{d) pyrenes12-o l-Methylnapfihateje78-591 hophomnee1-5z6 Z.irethytnaphhalene95-4&7 2-Mslttytph€nol
10s.3s4, 3,4-Meh',iphend
9!'lo-3 Naphthaleneo&7,r4 2-Nitroanitine991rsz $Nitroaniline
gRL
BFLBFLB8LBRL8RL8RL
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MLBFLBFLBFLBFL8RLBRLbFLBNLBRLBBLBBLBRLBRLBRLBBL8BL
BRL8RL8RL8RL6RLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRL
8RL8RLBRL
l4kg d'y
t'SkS dy
lqkg dry
ldkS dry
lyks dy
PtrS dy
x9lq dy
rc4q fry
rgrc dry
lgtg dty
194(s dry
wkq dry
wrsdv|rs^s drvlrq/l(S dry
rcag dry
ldlq dry
uglq dry
UgfrS dry
@WevrctS dry
runq dv
!s,4q dypgks d'y
Psiq dy
trol'tq dypErq dy
tsas dypgag dq'
Ug/rg *y
I'dlq ty
ldko fy
ldks ry|lyl(s rv
!c4q dy
!S4{0 try
rcnq dry
rdkg ffy
fSIq dry
ugAS dry
lsiks dry
usas dry
!S.4q dry
tg.4q dry
fS4{ dry
!94q dry
!g4q dry
ldkg dry
ldkS drY
tdk0 dry
609 1
609 1
609 1
609 I
609 1
609 1
609 l
60s r609 l
609 1
609 1
609 1
609 1
609 1
609 1
609 1
6 m r
609 I
6ffr 1
6C9 I
609 I
609 |
60s I
609 1qts I
@ 9 r
609 |
609 I
m9 1
609 l
603 1
609 |
609 1
m g 1
m9 1
@ s 1
@9 1
€09 1
609 1
m9 1
@9 1
@9 1
m9 1
@9 1
609 1
609 1
@9 1
609 1
609 1
60s 1
slt/8{6 8270C 29Mar{7 03-AO.{7 7931T4 M.8
Thie laboralory rcpo is not vstid without aB zalhofiad sigaat re on ahe cover pge.
+ Reportable Derection Limit BRL = Below Reponing Limit Page 4l of 154
Page 308
Sarnple ldentificationM8F-36 4'{'sA59803-08
Cliedt Proiect #301 -8 I
MatrixSoil
Receiv€dZ7-MaFo'l
Collechotr Dat€y'Time2GMar{7 00:00
CAS No. AnatytA(s) ft.salt Flag Ania rnDL Dilullaa Method Ret Prepared AMIWi Bateh Adzbsl
Scmivohdle Orgmlc Conpordds by GCMS
Senivolade Oqartc Cornoofids bv SW846 8270C
Pr€pared by method SW846 35508
100{13 4ltto€d[ne
s 953 Nitrobdu4fle
88 r55 2-NitroplEnol
{b{e.7 [llitroplrenol
82-754 N-Nifoooditiehylamin€@1n+1 [+Itorodi4{ropytarnine
ftiJircsodplErytanin€87llO-5 Ps\tad'lorcFh€f,d
85{1{ Phenarhrene10&9s-2 Pn€rdr29{on h/rmell0-8s1 PWin€ro-02t ',z,+Tftlorohenzene
Fls-. a{,5-Tft$brophenol8!(F2 2,a,ST'idttorophe.lol
e14-a z-nuodlnffiri
s/.121 2hn@E(d
1t65aa lliffig'zene4'
11f6{2e Pt!€tdi6
tTta-i14 ferpw44
tt'.:9-6 24,+Td4atagh*A
2949/47 tFApr{7 7O3i?4 M.8gRL
8eLBFLBRL8RL8RLBRLBgLB8L8FL8RtBFLBRIBRLBflL
4!)
n17
|l9l|(gdy 2,1.{1)
tEkSd] 6A9
|lgftS dr 6oe
tqlS dry 2U
r4h dy 609
lglqdy 609
ugtsdy 600
E/to tI m9
!!yh fI 609
lglS dry 609
la/l€ fi} 60e
Uglqdfy 609
pgdqdy mS
l{/l(g dy 603
!ELS dy 609
*130%
trfio%
&1E)%
1*110%
w130%
t5.110%
sw846 8270C1
I
1
1
i
I
I
I
1
1
I
I
7,F0{7{ ltrs|ulry
Tot.l M€ads by EPA 200 Se.ies M€thods
240.224 Silver
71,{}3*2 ArEenic
zt{oost garfutn
7'|{l4gg CedriLn
71101r'3 ohro(nfum
7,lig92-1 Lsad
zle{? Sd€nium
Totrl Mctrls by EPA 6tn0/7000 Series M€tnod3
Bfu
BflL
.1
64.5
0.m7
3.65
212
2.30
SPLP Metals by EPA 1312 & 5000/7fi)O S€ri6 Metftodr
SPIP E$Ection Comd€led
11,0-?2-. Srlver 8H-
744!3&2 An€na BRL
7{41-39-t Bariun Om59
7{0<-9 Cadnirfi BnL
7@4-s Chsniun BFL
7'r@47t ttlerdxy BRL
ftBc2-1 LOd 8RL
na2+2 S€l€nilrn BRt
Cenc..l Ch€mirEy P.rl]Del€r!
% solds 65.5
n'grgdry 0.0452
ndlsdy i.ls
n'gftg dry 2.17
ndrs dry 0.723
"Elq dry 0.36r
mdlq dy 0.7n
'nghdy 1.0€
mgt0 d'y 2.17
mq/l 0.0100
ms4 00150
nE4 0J050
mgt o@5
mgi 0.012s
me, 0.0m40
mS4 0.qt5
'tlg/l 0i150
swB46 7471A
EPA 200.7
g2-4fI47 m-Apl{7 7031810 YP
sw84613t2 28.lrar{7 2&t49f.ll7 703176:} 8D
Sw846131260109 3!ttar47 (B-AF-07 70i11805 LR
sw!16131274704
SW8461312,&109
0e-Apr{7 TlxI$6 YP
02.AF47 T(]3lmS H
$tir2t40c$od. xlMsrfi 3rH,tur{? 7031879 YM
Thb hno.alorl EFotl is not rqli.I wi out ad iathoized sigaaure on lhe corerpoge.
r Reporbble Detection Limit BRL = Below Reportiog Limit Psge 42 of l5{
Page 309
Sample [deotificationM8F-37 2'-4'
sA59803,09
Client Pmiect #301_88
Collcctioo Date/Time26-Mar-07 00:00
MatrixSoil
Rcceived27-Mar0'7
CAS No. Anauk(s) Resalt F'lag L-nirr 1RDL Dik tion Itethod ReJ Prepared Analyzed Bctt:h AnarystVolalile Orgsnic Compounds
VoC Efraction
!g,tg dry 73.0
t4lrg fiy 1'!m
UgkS d'y 73.0
WkS 4 7X.0
tigtg dy 73.0
ldkS dry 710
u94g dry 73.0
Udr(S dry 73.0
!g4q dry 146
pg/|(s dry 730
J]g/is dy 73.0
pgiq dy 7t.0
lgrq dy 73.0
!C/rS dv 365
rrg4q dy 730
lgkS fy n0
!s/ks dry 146
lS.ftS dry 73.0
!S,4( dry 1€
llg4(S fy 73.0
ldkS dry 73.0
!S.4q dry 146
US/kS dry 73.0
!S.(g dry 73.0
N,4(S dry 73.0
lgftS dry nn
!q4q dy 73.0
!S4q dry 73.0
ug/kS dry 146
ugkS dry 73.0
udrs dry 73.0
|lg/kS dry 73.0
ug/l(S dry 73 0
UdrS dry 730
pdrs dy 730
Udlq dry 730
lElq dry 730
pgrs dry 733
lgrS my ft.o
lVkS dy 73.0
lglqdy l3o
!9rS dy 23.0
lgrS d!' 730
udkg dy 730
ldhdy 730
lCiq dD' 73.0
lyko dy T$
pO{ dry 730
pCAg *y 73.0
Volat-le Oroanic ComooundsPrepared by mothod SW846 5030 Soit (high tevet)76191 1,1,2-Trichlootdflrjoro€lfianelFreon BFL67611'1 ACelOne BFL107.13.1 Adytonitile BFL7r4r2 Ser'zene BBI108.861 Bonoberuen€ BRL7497-5 g|!{nodtiolo|n€lhane oRL75274 Bomadi$lolomeihane 8RL75212 Bmmoform 8RL7443-9 Brcmomehane BRL73.e'3 2.Butanone (MEK) BRL1M.s1r n-Butlt}lruere BFt135-s3€ sec-Butytbenzene BRL
led-Butylb€nzene BRL75.rs Cabon disumde BRL56235 Caoon tetmchlorjde BRL10S91'7 Chloroben2ene 8HL75-{03 Ctiorcelhane gRL
r-6F3 Chtorotom BRL7t'913 ChlorometEne BRL$-4+8 2{htorohJuene 8RL10643-4 +ChtorEtduene BRLe612{ 1,2,Dibrcmo-3drtorc9rcpane BRL1241+1 DibrodEdllo|l}mehane BRL10640-1 l,2,Dibomo€lhane (EDBI BFL71-9t3 oikofilornothane BRL95.scr l2-Drchloobenzene BRL541-7+1 1,$Dic{lorobenzene BRL10e4&7 1,4-Dichlorobenzene BRL15714 Dichloodillooromethane (Frcoil2) 8RL75343 1,l-Diciloroelhane 8RL1tr&z l,2-oichlooelhane SRL75-354 l,l-Dicitooethene 8RL15&58.2 cie1,2-0id ooefEne BRL1ffi5 trdrs-1,2-Dicilorcethene 8RL7r.87-5 l,2_Dichtoropopan€ 8RL142n.s l,$Dichtoopopane BRLwh1 22'Drchloopopane BFLs6$58.6 l,1-Drcfloropopene BRLr006r-01-s cis-1,+oid oopopene BRL10061'0?.6 ttars-1,3-Didrlooprop€ne BRLr004r-4 Ehylbenzene BRL8763-3 HdachlorEbutadene BRL
541JS.6 2+€xenone (MBK) BHL$-@_8 lsoprcfylb€nz€ne BRL99-87{ +lsopoDyfio{uene 8RL1631.04-4 [,]€$ylt€n buly erher BRL10slo.1 4.tvtethyl-Z-p€nlanone (tyfgtq 8RL75492 Me$ylene dbrile BFL
Field extaded voc
SW E46 826!8
2EMar01 26-M3r{7 7031767
@-apr-07 02-Apr-07 1140017
BHL
50
50
50
50
50
50
50
50
50
5t)
50
50
50
50
50
5!
5{
50
50
50
50
50
50
50
5{
50
50
50
5t)
50
50
50
50
50
50
50
50
50
50
50
5091-2G3 Naphhal&e
Page 43 of 154
Thit labo4tory rcpo.t is t ol vcud piihou an tuthorized signature on the corer page.
* R€portabl€ Detection Limit BRI = Below Reponing Limit
Page 310
Sample [dentilicatiorM8F-37 2'-4'sA59803-09
Clieot hoiect #301-88
MatrixSoil
Received27-Mar07
Collectiop Date/Time26-Mar-07 00:00
CAS No. AnzbE(s) Flag UalA 'RDL Dil$io6 L{etho.l Retr. Prepaied Anslwd Eatch An4ltst
Volstil€ Orgenic Compouods
Volalils oroaic CornooundsPrepa.ed by m€ltEd SW846 5030 Soil (high l€v€l)l0s.65r t}Pl[pylt€ru€.|e100-42.5 Styr€no630.205 1,I,12-To$adlloro€han€7!!3,15 t,|,22-Tdrachhroethan€127.184 Tdrddoa€fpne1088t{ Tdter\€87{1-6 1,2,gTdJ{oobg1zale12082.1 12,1-Tridorcae'uens?1-556 1,1,1_Tido|etiarcB{G5 t,1,2-Tridllofehane79O16 Tri:l ooefreng75.6s_4 Tticldo€nuoorc$ane (Frsn l l)sr8-4 12,lTridooPropanesG3-6 l2,4,TdmetrytbefPenerr,837{ l,s,lTdmsqy'ben2ene75{1-4 Vaylc.l o*t€r@e07 m,Fxyl€ns9447{ [email protected] Tetrdltdrolu6n
@-297 EryeherS1-05-s Ted€myj me0v eher87-92.1 Ery tert-hltyl eher1rF2G3 Dii6oFoBt drer753s4 Ten€lbfiC / blltyj atcohol12991-1 1,+DiOxarB
1@404 48tutpfrtuobqzene
M7-t6-s Totuene4e
t7@4t4 l,z-Adtfudlw1el4
taf'-597 AfuadofiuxutplItste
Ortr.ct ble Petrcl€{m HydroqrboE!
E*rE{aHe Total Pqtobln ttudtocadons
Prepared by m€thod SW84ti 35508
,d661.1 Gasoline0847s3+2 Fu€tOIt2
6847631j1 Fu6t otr *4
68sslo-1 Fud 0t 15
Wsd(oo ti{obr$l
J@10000 Aviati{ Flj€l
Unii€ntfi6d
on'.r OilTotd Peholdm l|}dllcartqB
C9-C36 AlFh6lh F drocaboG
.trfiolEb rBcotia'ier:
Semlvolrtile Org.nlc Comportr& by cC
oldod oihe P€sti{ii€6 SV{846 80€'lA
Prepared by metpd SW846 3545Aa09{G2 Atdrin
BFL8FLBFLBRLBRIBRI.BAt
BEL8nLBNLBRI.9Ri-BRL
BRI.BflLBALBFLBFL8RL8RL8Fi.BRI,BRLBNLBFL
991UJc4t11
505050505050505115050505050505i)5050505050s05050fl
50
wt{ trvHrq dv
dh dv
udh dv
dlqdvpo/bdty
ugre dv
H/lq dv
ldh trv
!9lr€ dy
dl'! try
drs dv
E/lq dy
UC,tq dry
dlq dv
lgls dv
|Jg/t{ dl
'Jdr€er
us,rs dy|lsnq dy
uglq dv
udl{ dv
|ryrg tl'
lqlq fr)'
lcE dt
70t3014701fi%7Vtfi%7V1n%
nglS dY f14
lr€nq dry 7t 1
rg,lqdry 7l-1
rnplqdry 7t 4
mB4qdy 71.1
mglqdy 7r.4
myxo dy 71.4
.nclq dry 71.4
'r9AS dry 7!.4
'rdE fiy 71.4
4tltlo %
l/g4S Ov
sw 846 826C9
€T E]PI1
73.073073.073.07t073.07X.073.0730
u73,0
73-0
730
73.0
73.0
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t{6
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73.0
73.0
7J.0
73.0
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t{60
@{pf{7 0?-AFfl 790017 nr
291tar'{7 *klnf 781n2 DSBFLBnIBRIBRLBRI.BFLB8LBFLBFLBFL
sT{&6 8m1A 2'l,8147 02-Afl.47 7{X,l73{, TG
This rtldfllory repod h nor t)dM Hithon! at thor*td sEnat ue oB drz cwE p$4
* R€portable Dctccrion Limit BRI- = 8€low Reporting Limir Page 44 of 154
Page 311
Sample IdentificationMEF-3? 2,-4'sA5980t-09
Cliept Proiecr #30 t - 88
Collection Date/Time26-Mar-07 00:00
MatrixSoil
Received27 -Mar-01
CAS No. Ana+tz(s) Resuk FIoC Units 'RDL Di,utioa Method Rel, Prcporcd Anaryud Baich An/tlysl
Samivolatile Organic Compoundr by CCOroanochlorine Peslicides SW8{6 8081APrepared by method SW846 3545431934{ a_BHC319357 tsBHC
319-068 +BHC58.ses g-8rc (lndan€l
57.7+9 Chlodan€z-54r 4,4O0D1p,i)72-!64 4,4{DE (p,p )50.4n 4,4!0Dr(p,C)6t57.r Dieldrin95s.98-8 Endosultan I321355.9 Erdogrllan ll103107.0 EndosullanSulhtenzoa Enddn7421-s3{ E ddn Alddryde76414 H€phdlorn+95 l4ehoxycl or1024s73 HeplachlorEpoods3m1 3$2 Toxapiene5103-7r s *Chlordane5566347 gchtordane
$agl.7Gs Endin K€lone
1@6aa 4l-N.Uafrwffibheit4 (30
,,51-213 oe{aclXotobbhenyl(Sl
Polvdrlorinaled $ohenvts bv Sw846 8082
Prepared by melhod SW846 35454
12671-1 r-2 PCB 1 01 6111M-?3-2 PCB1?2111r11-16,5 PCB 12325346921.9 PCB 124212672-2+6 rcB 124611m7-6$1 PCB 125!1109s8n5 PCB 12603na!23-5 PC812621r1@r1-4 PCB 126€
103a6.84.2 44-Dg4ctafluotobwenyl(s0M1'2Lt ^e@hbrobhlcnyl(s4
Semivolatile Org{lic Compounds by CCMS
S€mivotatile &oanic Cornodjnds bV SW846 8270C
P.epared by mettpd SW846 35504
&-e4 Acenapldlene2084€.0 A.snaphfiyl€ne62.s3-3 Anilne12G12-7 Anhra4€nel9l2-2,1-9 Atrazine103+3-3 AzobenzsraoiptBrMdiazne92-87.5 B€nzidines&5$3 B€@o(a)anhrs{€ne
?3-Mal{7 t2-AN-07 7fi1rc TGBRL
BRI-
BFL
BFL
BFL
BRL
SRL
8Rt-
BRL
BRL
8fl1
8FL
BFL
BffL
BBL
8RL
8RL
8RL
BRL
BRL
BHL
122
8RL
8RL
BRL
BRI
BRL
BHL
BRL
8RL
8RL
u110
8RL
8RL
8RL
8RL
8RL
BRL
BRL
2,470
I9lS d,y
ts,lq dy
lsfro rvlJs&g drvWrsdnt!4rg dry
pglq dry
ldlq dv
pdks dv
us4q dy
pEl(sdrv
l,!As dry
|ls/ksdrv
t]s/ks drv
fvlq dry
trS4q dry
ldlq dry
!S4ts dy
ps/hl d]
!o4q (fy
ldkg dry
30-154 %
30-150 %
!91q dry
p91q dry
ugks dy
pltg dy
pgks dy
!9Xs dy
!SI(g dry
!s4q dry
pgrs dry
30t50 %30-1fr %
tlgts dry
ldks dry
lsh dv
lgng dvpgts dv
l,gftS dYpglsdv
H,lq dV
sw846 €081A
sw846 80E2
s!i18.46 8270C
36.5
365
365
t83
365
36.5
36.5
36.5
35.5
365
36.5
36.5
365
36.5
36.5
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36.5
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Thit lahonlo.! rcporl it ,rol vqlu x,fuhoul on atrtofized signaar/re on the col'er page.
* Repo.lrble Det€ction Limit BRL = Below Repodng Limil Page 45 of 154
Page 312
Samolc [dentificationM8F-37 2.-4'sAs980349
Clieot Prciect #301{8
Mat ixSoil
Received27 -M^t-07
Collection Dal€/Tim€26-Mar-07 00:00
C,4S No. At nlrt k) Resuh Fl4s U,,i,l *ftDL Dilutiorr Method Retr PEFored Analtzed Batch AnalBt
Semivoletilc Org.nic Compounds by GCMS
Semivolatle Olanic Compourds bv SW846 8270C
Prepar€d by method SW846 35508
5G32€ Bsnzo (a) pyrere20t9e.2 Bsuo (b) fluotanfiefle19124.2 8€nft (g,h,i) peryj€ne207{ss B€flo(k)fluo|ant|ei€ffi{ g€nntc ecidl@51{ g€nzyl ahohol11141r Bls(zdorostloxy)nE$an€i11-4,!-,1 tlis(zdrtoro€ftt)dher@Q{ etsedrbftisopqy0etEr117{1.7 Bis{2+f1},{he4r)dfl!atare10r.s:|3 +Somoph€nyl phfiyt eher856&7 Butyj bat4l pnhahb
88.74-8 CodazDlos-5G7 44hlo|'olmettry[figrd10647+ 4.Chloodlitine91-547 2{hloronaphdEhn€96.57-8 24Hofophenol7oo+72,3 +CHoroph€nyt ph€nyl ehei219{1.9 Chry!€ne5970.1 Db€atzo {a,h) anthracene132{,1-9 oibslzofuran!F5Fl 1,2-Dd1otob€nzsn6trr.7$1 l,+Dcliorobenzens1064S7 l,4-oictiombenzffe914,q 3,3--Echloroben2dn€12o€'2 l,&Dicloophenola1t&2 DidnylphfEtate131-11n oimery phhatate1ffi/€ 2,4€imoth!4phdtd*7+2 oi{+dylptrttaht€sl+52-r 4,S0inilo-Z-fi|ethyFtt€nd5r .2es 2,4$nitofi€rd121-1+2 a+Dinitrobl6ed)620.2 2,&Dnihotofu€neri7.E4{ O{1{dylphhahb?18.444 Fl]otarrlisn€8S797 Ffuo€ne11&741 H€xd omberEe{Esft&3 Hsxdlloobotadsn€n{.74 Hexactorocydopontadi€n€6'l'7*1 ftexe*boetfEne1e3.395 lndeno (11,3{dl pyreies12{ 1 -ridvnaphhal€no
78.59t lsopfiordlee.t7.6 2{rsbytmdtst€{,€6Fl&7 z{i.telhyphstol
1(r&3s-.1, 3,+Metjybh€nol106.4t59I.203 thphfdene8&7rr4 z-NitoinilnoS.(+2 $Nltgefine
21ffi
aolo8FL
2170BRL8Rt-BRTBRL8Ri-SFTBflLBRLBRLBflLBfrLBFL8FLBFL3,370BRL8R.8R-BR.BRLBRL8RL8RLBNLBRLBNLBFLBFLBFLBFLBFI
3,940BRT
8RLBRI-BRLBRLgf,L
BHLgRL
BFLB8L
BFL
8RLBRI.
NU ty 886
t.db dy 886
l4b dy 886
lglqdy 886
USIqdy 886
UglSdy 885
pgk0d, 885
t,g/rS d] €86
|,Ets fl 886
|jg}S try 686
tiglo 4y 886
l'ClS fy 886
uglq dy 886
E/rg fiy 886
rlgh dY 8€6
rdb dv 8E6
|'|g/b dy 866
|db dy 886
pSlqdy 885
pdlqd] 886
Udlq dy 886
l,gilq fy 886
tgrq dy E6
!gl0 dy 886
trgh dy 886
ldlq dy E86
ldh dry 8€6
!9*S dy 886
udbdy 886
/$qA 886
Aq dy 886
lYlqdy 886
r{tbd} 886
rurtq dry E65
Igtq d, 886
|dh dl 886
|lgIq dy &6
!g/fq fy 886
tJg](s d)' 88€
tiS,?€ 4y E86
lSrq dy 886
tjglq dy EE6
!S/XS dy 8EE
psftedy 8s
t{/rq dy 866
ldb d'y 886
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$nqdy 886
ug,|qdv €86
l,g qd} €86
SI,Y816 8270C 2S-lr€r{7 o3.Ap.{7 m6174 M.B
Thb laho@lory rcpwl is,.ot vdd x,l toat a!, aa{toriud tigaataw ott thc coter page-
. R€portable Dete.tion Limit ERL = Below Reponing Limit Page 46 of 154
Page 313
SampLe IdentiftcationMEF-37 2'4'sAs9803-09
Client Proiect #301 -88
MatrixSoil
Received
2'l-Mar-07Collectioo Datf/Time
2GMar-07 00:00
CAS No. Analrte(s) Resutt FloC Uni.s *nDL Dilution Me,hod Rel. Prcpand Analyed Bctch Anabtst
Semivolatile Orgrric Compounds by CCMS
Semivolatilo oroanic Compo{nds bv SW846 8270CPrepared by method SW846 3O5OB
1m{1i 4-Nitman ine9€{t3 Nifobenzene08-75 s 2-Nitrophenol100-02-7 z$tilophenol
6e-75-e N-lfirosodimehytamin€@1441 N+lilrosodi-ntropytamine86-30-6 N{,lhmsodiphenytamine37-96.5 penhdlotophenol
9t018 Phenanf[ene10s 95-2 Phenol
110-0d1 Pyddne120-02-1 1:,4-Tricr oroben2ene95.9n 2,4,5-Trichtoropienol8!-0€.2 2,4,6-Tri{*toroph€nol
a1&4 2+l@r@,ent4
36tJ24 z-Flwry,tend,(r6s-60-0 l'lilrobalzaE4s
110562 2 PlEnol4S
171&51-0 ledpnyl4l4
tt&N4 2,4,6-Trkrcnophend
29-l,lar.07 0}Ag'A1 7fA1774 M.BBRLBRLBRLBRLBRL
BRL8RL8RLBFL8RL4,260ERLBRLBRLBFT
6154n
7051
3540836886
3540886
886
8€6
886
886
686
666
686
886
886
886
pyrsdvpslq dry!S4q diypdks d'v
l]s4(s dv
lglq dry
tllliA dt l
|ls^s dry
|a4(S dry
Nkq vugfrs dry
vSllS*ylsas dy
ldkg dry
rcAS dry
30130 %15-fi0%iEli0%t5-110%30-130 %15110%
sw816 8270Cl
I
1
l
l
l
I
I
1
1
I
I
1
Totd M€tab by f,PA 6000/7000 Series Methods
Total Metds by EPA 200 S€ri8 M€lhods
14t+221 Sitver
714139.3 Baiurn
744e39 C3dnium
7n{H7-3 qlunjum
743$91-1 lead
nn249-2 s€l$ium 2.S0
SPLP Mctde by f,PA l3l? & 60001000 Series Mrrhods
SP|P Extiadion Compt€led
741$224 Stver 8RL
74!eM-2 A|s€flic BRL
74.{e3$3 Eadum 0.0126
74{0-43-9 Cadnium BRI
Ta447.3 Chrcmtum BRL
743e,976 l,terc1]ry BRL
zl3$92-1 Lead 0.0542
n821e.2 Sdfiium BRL
G€trerrl Chemistry Prrrmel€rs
% So$ds 82.8
1.m mSAS dry 0.0356
r'S*S dry r.16
rrE/rg dry 1.75
riS/}€ dry 0.582
m{rg dry 0.291
mdlCdry 0.582
mdlqdry 0 871
mSftS dr] 175
mgl 0.0100
mq,l 0.0lel
mq 0.0050
mgl 0.0@5
rill 0.0125
mgl 0.0{X}10
mga 0.0075
mgrl 0.0150
slrt46 7471A
EPA2W7
sw8461312
swE16I312/60108
sw8461312?470A
sw8461312/S108
SM25,l0 G Mod
1
1
l
I
l
1
1
I
1
I
l
l
I
1
I
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1
H8
02-Apr0/ 09Apr{7 7031810 YP
BRL
28.8
64.5
o937
14. i
302
02'&r07
28 Lrar{7 2€- ar{7 7031753 8D
3GMar47 02-Apr07 7031805 LR
' 02-AF{7 /031€06 YP' 02.AF{7 7031805 Lq
30{lar-07 30-lrrl{7 7031879 YM
Thb labotdory rcpod k ntt talid without aa autiorizel sigwtare on ,he cover page_
'Reportable D€t€Etiofl Limir BRL = Below Repodng Limit Page 47 of 154
Page 314
Sampl€ ldentificationM8F-381'-4,sA59803-10
Cli€nt Proiect #301-88
Collectio! Date/rime26-Mar-07 00:00
MahixSoil
Received27 -Mat47
CAS No. Analra(s) R.s|,/lt Flag Uni,$ *RDL Dihttiorl Itahod R?tr. Prcpaled Aulyzed Batch Aaabst
Fdd e{rad6d
Volafle Oqanic ComoounG
Prepared by method SWE46 5O3O Soil (high l€vel)
7$13.1 l,l2.Trichtorclifluo(EtEne(Freon 88167.€+1 Acetone BRL10'-rlt Adylonitrito BILtt.tLt2 Bs|zene BFL10g-061 grofllobenzene BfiL11.911 Bomcitoromethans 8Rl-Enl BDnodchloronefiano BRL1r&2 Brornolorm 8ru-748i19 &undn€thane 8Rl-7843.3 2-Butanmo (MEK) BRL104s1{ G8utytbenzene BnL1l+98€ s€r,Blqdbenzene BnL€0s-6 lsd-hlytbenzene BRL?F15{ cedon dsutfide BRLse23.s caftonleirad{ori& BRL1(6.{l{17 Crhlorcb€nzene 8RL
28{rar-{7 2&Uar{7 1ts1757 BO
t2-1lot47 02-Apr{7 nxlol7 fiar
Volrtile Orgar|ic Compound!
!r'oc Effaclion
lSrq dry n.1
l{lqdy um
|.grq dy 73 4
lglq dy n.4
Ud{q dy n!
|clq dy 73A
ldkS try n.4ydhs dy r31
ldlq dy r47
|jg/h dy 734
l.dlS dry 73 4
Blqdry n.4
Ig/lqd} 73.4ydhtry 367
!g/]q try 73a
E qdy 7i{
B4€dy 147
IErqdI 734
ldlq dy 141
!g/kg dy nA
mlq dv n.1
Ug/rq ry u7
lglq dy n4
t'dkS dy I}4
l4h d'y n.4
|]grS dy ?3.4
|4/lS dy 73.4
Igl{ dy 73.4
|dlq dV 147
|JdkS try 73.4
|j049 dr n4
lgls dy 73.4
r{rq dy f3_4ygrqdl t3.4
|,g4q dry 73.4
lglq dy n.4
|EIq dy 7X.4
Udr0 dy lXA
H/rq dr 73.4
udt{ dy 73a
!9,rS dry ?83
ldre &y n.4
ldbd'y 7u
udr€dy 73.4
Ug,lqdy 73.4
lghdy 7x.4
lStS try 734
ldhdy ru
lClqdy 73A
505l)505050505050505{)5{t5i)50
5050
fl)
50505050505050
5050505050
50
5{)505050505050505050
50
505050
voc
s1,li 846 82608
75{l!3 Cl oroshaneeI{63 Chlorolofln11413 qtbrooellan€
51S3 20rlorotoluene106.13-4 4{l orohluae9e12€ j2-ttibromo3d oropopane124-1&1 Dbrfi|odo.ornethane1qf0}a l2-DbromoedEne(E0B)744F3 DbromomBthene95.5c1 1,2-Ddltoob€nzenes417}l l,&oidlhrob€nu€ne106-a+7 t,4oCldolobenzen€75_71-s Didiloodffrol('ndhanelFreoni2)75.34-3 1,l-Dicito|DeflanelO{Gz 1,2-Did do€thaners"3fi l,l-DicttorodhsrErs6-5$z cisl,2ok*o€ehene156-6Os lrEns-12-oldoro€ft€ne78{7.5 l,2-DdoroFopane14p.44 t,&DicHofopropane*r-tu1 2,2.DcHoropmpanes4950-€ l,toido|DproPene1@61{r5 cb-1+Di,hblop{tp€r1elm61{26 telg-1,3-0id{o.opropen€'q)-41-4 Ehy'b€nz€n€fl.593 H€rd orobutad€ne591.785 z+iexanono(tl8qs.82-8 lsoPropylbenz€i€9+e7€ +lsoproprthbd|€fiar44-4 lr€hyl tediuM €fier10&1r!1 4-tiretfiy1-2{€nhnon€(Mt8K)7S9-2 Meftylene dbdre9r-a!3 Nepnfd€n€
BRL
8FL
BNL
BAL
BFI.
BNL
BRL
BFL
BFL
BFL
BRL
B8L
SFL
BFL
BBL
BRL
BRI.
BRL
BRL
BNL
BRL
BFL
8FL
BRL
8RL
8RI
BRI
8eLBALBFLBFIBRtBRL
Tkb htofllory repott b not vatjy' Nirtoat al du&otlzd lignafitn oE thE cover prg.
. Rcptrtrbl€ Detectioo Limir BRL = Bdow ReForting Limir Page 48 of 154
Page 315
Sample [dentificationMEF-3E 2'-4'sA59803-10
Cliflt Proiect #30 t -88
Collection Date/Time26-Mar47 00:00
MatrixSoil
Received27-Ma(07
CAS No- Anattte(s) Resull FlzC Ani6 *RDL Dil,ltiorl Mahod Rel. PMpared Anallzed Botch Anat$t
VolNtile Organic Coft pornd!
Volalilo orqanic ComooundsPrepa.6d by method SW846 5030 Soit (high tevet)10'6+1 n-Pmpylb€nzene10042.5 Styren€64020.6 1,1,1,2-Tetradlooelhane7s3,lt 1,1,2,2-Tettachloroelhane121-tA4 TetreiloDelhene10S-Sg 3 Toluene
87.61.6 1,2,3-Tdchtorob€n?ene120121 1,2d-Tichlorobenzene7r-55.6 1,11-Triciloroehane79{0.t l,12-Trichloroehane79{16 Trdtloroelhene7*9-4 Tri*torottuoromethane (Fleon I i )96'101 1,2,+Tridto.opopanes5-53-5 12,4_Trimethytbenzen€10€{7+ l,3,5,Trimethytbenzene75{1.4 Virryldtorids133G2G7 m,Pxytene95-47-6 oxyl€rp109-999 lelrahydm{oran&29.7 Etvleher
94{Ef Ten{mylmehyleher87923 Etryt tert-bulyt etter1m-m3 Djsopop/ elher75 65.0 Tert-Eutanot / buty4 atcoholr239r r 1,4-Dioxane
#4404 4-Ercnonwrobenzarc
tu3t'26i Toluen*dB
tiM474 1,2-Dichlotoethane.A
1868-53-7 Dlbroraquorofiekane
Ertrrctrble PEtroleum Hydrocarbons
Exlnc{able Tolal Pelrcleum Mroaafton6
Prepared by method SW846 35508
80661.9 Gaso[ne
60476.3G2 Fud oil {26347F3f3 FUelOil d463s53 00-4 Fuei Oil ,6M093000fi iiolor oilJolm)oo Avjalion Flel
Unidenlified
Ot€r Oil
Total Petroloum Hydrm€rbons
C9{36 Aliphalic Mocarbons
s$3yz l{tlorccrjadecarc
Semivolatil€ Orgrnlc Compou!& by cC
organod orift". Pestidd€s SWM6 8081 A
Prepared by method SW846 3S15A
8RL8RL8RL
BNLBFL106BFLSRLBRTBRL8RL8RL8RLBRL8RrBFL
8HL8RL8RLBHLBRL8RLBRL8RLBFL
1(Ata
s?113
50
50
50
il
50
50
50
50
50
50
50
50
50
50
50
50
5{l
fll
511
50
50
pg4S dy 134
lSeS dry 734
rcfrS dry 734
pSftSdry 73.4
lSftgd] 73.4
UdiS *y 73.4
pg/lg fy 73.4
pg/\s,rv 73.4
pSIq dry 73.4
|lgn(S dry 13-4
lCftS dry 73-4
lgtS dry 734
!9,,rg fy 734
lgrS dry 734
rceS ey n.1ldks dy 73-4
lStS dry 147
lSrlq dry 13.4
pglq dry 734
pS&S fy 73.4
Wtg dy 73.4
Fs4q dy 13.4
pS4qdy 73.4
ldrS d] 7U
ldlq dy 1170
n1&%
?v1& %
70-1U %
7F1U %
dkS d,y
mdrg dy
mgtg dry
mgtS di)
motS dry
mS/xq dl
mSf.g dy
mS/rg d)
mgtq d]
mdlS diy
44.140 %
SW 846 82mB 02-Apd7
+CT ETPH
02-Apr-07 7040017
2g-Marq 3UMaJ{7 7031772 DS69.8 1
69.6 1
63.8 1
69.8 1
69.8 1
69.8 I
6T.8 1
69.8 1
69.8 1
69.8 I
sf,LBFLBRLBFLBFLsffLBFLB8LB8LBRL
8€L VgrStt 37.9 swt46 @Era a-Mu47 l}2-Apr{7 7031739 TG
Thh laborutory nFod is not valiil x,Aou an authorhed signaraE on the cover pqEe-
* Reportable Detection Limit BRL = Below Reporting Limit Page 49 of 154
Page 316
Samol€ IdetrtificationM8F-38 2'-4,
sA59803-10
Clie Proiect #301-88
MatrixSoil
Received21-Mar47
Collection Date/Time26-Mar-07 00:00
CAS No- Analrlc(s) Resdt AnibFbg aRDL Dildion t{ahod Retr. Prcpared Artalyed Bdlch An4lfs!
Semivohrile Organic Compoun& by CC
Orqanocibine Poslicides SW846 eO81 APrepared by method SW8,f6 3545A
319{,r-6 rg{C319.657 b&{CJ1$0&8 dBHC58-8e.e 0-BHC (Undane)5r.7+9 oibrdan€z.s,l-o 4,4.DDO{p,p)z ste 4,4.DDE (p,p')5lt2+3 a,1.D0T (p,p')6115|-l Di€l&in95940-€ Edoculhn I3321$6ts Endos0llan tlr03l{7€ Endosxltansulhten-244 Endnn1Qt.tt34 ErnriiAldehydetua Heptad orn115 lrefioryd or1rl24t{ HeptEd of Egotdedloli$2 ToradHe5jG71.g a-Cl{otdane
566&3+7 g4ltodane
5349+7Gs Endin KetJ|€
,Gn042 1,{DE&a0uot&dEtV(Sr)
ffir2+3 o€caE,lonbilld/rl MPotudlloiEted BioherMs bv SW846 8062
Pr€pared by nethod SW846 3545A
1267+11-2 PC81016trr0+2s2 rcB 1221t1r41n6-5 rcg l23Z
53469.21-n PC81242
B6n-?94 rc8124811ll€7€.r PCB 1254
1l0*€e.s rcB 1260
tp,+23.5 Pc81262111001+4 PCB 1m8
@8.a+2 1,+08-Uan@tdids1yl(g)
,f61"r3 l]€fEdltorcdipttr.tryl (*)
Ssthivolraile Otg.nlc Compornds by crCMS
S€r!'vdane OEanic Co.noolmds S'/YM 8270C
Prepared by method SW846 355088+32.9 Aenagh$e.r6
200-s64 AcdEphthylon€@-53€ AllilE
1&12'1 AnhacBnstg12'2,H, Alrazin€
10+3+3 AzobgnzeneDiphenyldazine
Q{7.s Benzidn€
56-5S3 8€azo (a) anhrEce|]e
8RL
8RL
BFL
8RL
BRL
BNL
BNL
BRL
BFL
BRL
8RL
8RL
88r
8Rr-
BRL
BFL
BFL
BRL
8RL
8RL
SRL
107
BFL
BFL
BRL
8RL
BRL
BRL
BRI.
BRL
8AL
m95
37.9
3 7 9
37.9
Tf.9
189
37.S
n.937J
379
37.9
379
17.9
37.9
37.9
37.9
37_g
n3l8
37.9
320
3 7 9
rdb dvpdlq dv|jgrs d'v$g/rg dVlsrq dvlgrs cy!s/}'s AlS,trS fiy
R01 |lg/tq dy
Ah dv
|ldks drypgkg dv
$rq dv
|,o/l(s dv
ldks try
ldkS dry
lglq eY
l8fr9 frv
l4balslq dly
r9tq dy
&lf l%3+1fl %
t4rs dy
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N$eY|ryb dtypg/lq dry
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IdrS ol]s/}{ 4y
!s4q dY
30tg%#1&%
r91s dygdro dv
ldlq trv
lgls dv
I4r4 6t
!4ls dv
ah dv
t'gb dv
sw846 80814
sa{a$E@
$rY8fi A27C
75-7
75.7
75.7
757
75,7
75.7
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a.|.lai.07 30r1tr{7 lfi}1738 SM
294ai-07 6t l0rl7 VBlnl M.B8RL
8RL
8RL
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845
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' R@rtable Der€dion Limit BRL = Below Reptrrirg Limit Ptge 50 of 154
Page 317
Sample IdentificationMEF-38 2'-4'sA5980l- l0
Client Proiect #30 t - 88
Collection Date/Time26-Mar-07 00:00
MatrixSoil
Received27 -Mar-07
CAS No. ALaltte(s) Re$ah Flog Anib +RDL Dilutinn Mehod Rel. FnpaEd Analrzed Ratch Anallst
Semleolelile Orgaoic ( ompounds by cCMS
Senivdafle ofoanic Comoounds bv SW846 8270C
Prepared by method SW846 35508
so32-8 8en2o {a)pyrer€415-9$2 Ben:o(b)ltuoranlhene1s1-212 Ben:o (9 h,i) p€rytene
m7-08 e Benzo (k) fluo.anhene66-89) Benrcic acjd100-sr.6 Benzyi akohol111-9lr Bs(2rnbroehory)melhaner1r-44-4 Bs(2{hloo€lh}4)elher38638.32-9 Bis(2{htooisopropyl)efier117.81.7 Bis(zahyth€Iyt)phihataler0r.s53 4-Bromoph€nyl phenyl efEr115.60-7 Eutytbenzylphlhatale36 74-8 Caba2ole59.s0.7 4,Chtoro-&mettrytphefld10S47.8 4,Chlotoanilines1s&7 24htoronaphlhal€ne96 57{ 2-Chlorophenol700s,72-3 4_CHorophenylphenyleth6r213{r S Chrys€ne5$70-3 Dibsruo {a,h) anlhracene132t4-9 Ditrenzofuran9+50r j,2-Dchlo{ob€nzene
s4l.73r ],3-oiohlorobenzsne16467 ],4-DDhloiobenzen€sr941 3,3'-0ichlorobenzidine12aa!2 2,4-Dichtoophenol0,146 2 Dielhy,i phhatale
r3rrr3 Dim€fiylphlhataler0567e 2,4-DirEltrylphenola4 74 2 Di-n-bulyt ph$atate
53!-52r 4.&Dnilro-2-mettryloendsr.28-5 2,4-oinihoph€fld121.1+2 2,+Dnikobtuefleme20-2 2,6.Dinilrcbtuene117.8.1{ oi{{dylphtfElate4k444 Fluo€nth€ne
8St97 Fluolenell$74.1 HexaChloDb€izen€
r7{&3 Hexachlorcbtiadenen474 Hexedllorb,.yclopenladiene67 72-1 HexachloD€tErE19339s hdeno (1,2,3{d) pyrefle
9G12{ t-llelhylnaphthat€n€7!-59-1 lsophotone
91.5r-6 2-Methlnaphhatenees-44'7 2-Methyiphenol
10&39-4, 3,4-Melhylphenol
s1r0'3 l\hphhatg'le*:r+4 2-Nitfoanilnee9-09.2 }Nitroani{ne
BFL
BFL
8RL
8RL
BRL
BRT
BRL
BRL
BRL
BFL
BFL
BFL
BRL
8FL
BRL
BRL
BRL
BRL
8RL
BRL
8RL
snLBFL
BFL
BFL
BFL
BFL
BBL
BFL
BRL
8RL
8RL
sRtBRLSRLBRtBRL8RL8RtBRLBRLBRtBRIBHI.BFI.BHL
BRL8nL8nL
ldks dv
!S/iS d.ypgts dv
|lgas dry
lglq dry
lglg dry
ru4q dry
|lg}sd.vlatsdrvydks d'y
tlgft! dYpgks d]pg/rt0 dyps/]{s dv
!S4q dry
!94{ dry
!S,4(S dypdls d}pg/tg dv
|lgilq d,y
|lslrs dry
ta4€ dry
|4r'lq dry
!04q dly
lqE dv
ldlq dvpdks drypsiq dypgls drypYks trv
ugl(gdvu04q dty
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|Jdkg dY
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|]!iks dv
ldrs dty
!c4q dy
!s4q dry
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!S/tS dry
lsas A
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wts *v|a4q dry
865
E65
665
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865
865
865
665
865
865
865
865
865
865
865
865
865
865
865
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Thit lalorotorx rcpon k not BIid w hoar aa authodzrit signolure on ahe cowr page.
* Reportable Deiection Limii BRL = Below R€porting Limir Page 51 af 154
Page 318
Sample IdentificationM8F-38 2'-4'sA59803-10
Client Proi€ct #301-88
MatrixSoil
Collectiod Date/Time2GMar{7 00:00
Receive-d27-Mat0'l
CAS No. Adalyak) Result Flas Unix 'RDL Diletion Method netr Prcpted AnrIWd Balh tusrfsl
Semlvolrlile Orgsnic Compounds by GCMS
Semivolads Orcanic ComoounG bv SWgd6 8270C
P.epared by melhod sw846 35508
10(H116 +Nitoe lne
98{,53 llilrcD€n2g|le8&7+s 2-Nitophsnotlllo-Cp-7 +Mfrophenol
6e-754 ifltt€sodimetrylamine
6er5+7 $lfrttosodi-ntropyldnine36306 tlt{tosodipn€nylarnin€
07-8s5 P$lacttloftAhenol35{1-! Ph€nanlhr*D10Fst2 Phenol129S{ Pyleno110-€d1 PyidrF!m{2.r 1,2,+Tndbrcb€{E€ne95s 2,4,tTdJ ooph€nol8ss-2 2,4.6-Tddtorophenol
eft44 2+hefuiphstyl
#f-121 2+lwtgpl'€nd
1165j04 N|@12ale6
41fia2 PW45
17tsst4 fe(M4a
1t4/96 2,4,6-frtbtunophdtd
2S sri7 0+Alr.O7 7031n4 M-BBBt
BRL
BHT
BHL
BFL
BFL
8RL
BRL
8RL
BHL
BFL
BflL
BFL
BBL
8RL
57
59
60
n75
15
pg*S *y 3460
t'gt! dy 865
a& dv 865
Udlqdy 34€o
l9,lqdy 865
lErS dy 86s
|Jgls fy 865
tdr{ dy 865
pgrS dry 865
tdh dry 865
ldlqdry 865
llgftS dy 866
tghdy 865
!g[q fy 86s
|4/k0 ry 865
30tf l%
tr t l0%
3Etg%
tt l l0%
30F130
1r110'a
mdlqdry 0!B63
rnsilqdry 121
n'gks dl 1.82
mglgdry 0m7
n'g*g dry 0.3{X
nqlqdry 0607
mghdry 0 911
mdrgdry t&
mgl 001m
n$l 0.0150
mg4 0-m50
ngr'l 0.005
ms,,l 0.0125
mg,l 0.{m40
m! 0.0075
mgf 0.0150
sirY8{6 82mC
5!118,16 74714
EPAa]f:I
Tot.l Mctrls by EPA 6001y110{ Seria Merhods
7(l$gr{ lrgdtry
Total Merrl! by EPA 200 Series Method!
7@41 Sjlv€r
7443X.2 AJsenc
?{4SS.l Baium
?44449r Cednium
71!G11-3 Chrdniun
7'B9. t t ad
r|82{!,4 Seleniurn tB
SPLP Mereb by EPA t3l2 & 6000/7000 Sed6 Methods
SPtP8hadion Cornd€r4d7@21 Situ€. 8Rt-74+&z Arsenlc SBL
71,10.3+3 B€rium 0.O1n
7'1441-s Cadniun 8AL74aO-47.3 Olodilm 8AL
713+97-6 M€rqlry mL743892r L4ed OUgzrn24.2 Sder um BRL
G€nerrl Chemi6lry Prrlmetens
% Solids 81.2
0.972 1
I
1
1
1
I
I
l
t
I
I
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1
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m-fur-o7 t)& c{7 7ts18t0 YP
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299
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SW846 i31460108 fl)ilaroT m-Apr{7 7031806 tB
sw846 131274704
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This lanorutury rcporr is not did whhod an atlhodzd signetare oz thz coter Fage .
+ Rcportable D€lection Limit BRL = B€tow RQortidg Limir Page 52 of | 54
Page 319
Sample IdertificationrrtSF-39 2'-4'sA5980 l - l l
Client Proiect #30 l -88
Mat xSoil
Receiv€d
27-MaFOl
Collection Date/Time26-Mar-07 00:00
CAS No. Anolrte(s) ResuA Floc Uni6 *RDL Dil'/non Method ReJ. Peparcd Arnbtzed Barch Anallst
Propared by method SW846 5O3O Soit (high tevet)
76-1x1 1 1,2 Indk rotnltuoro€$ane (Freon BRL67€,11 Acetone eRL10713 1 Acry4onitrite 8RL71.tx2 B€nzene BRLr03 35 1 BEmobenzeoe 8RL74s15 Bmmochlommelhane 8RLtt27-t BmfiEdidlordrehane 8RL75212 Bonotom 8RL7,1'019 Bromomelhane 8RL7!-e13 2-Eutanone (MEK) 8RL104511 n-Butylbeuene 8RLrx5.ss4 !€c,B{n/benzene BRLeds Gn'suvl6€nzene 8817515{ Ca6on disotfid€ BFL56 23 5 Grbon tetrachtoride BFL10&90 7 Chlorob€nzBle BFL75.00-3 chtorcethane BRL67-66-3 Chlorolom 8HL7+87.3 C,hloror€thane 8RL9549-8 24htorotoluene BRL106-43-4 44htorotoluene BFLs612r l,2-Dibronlo-3rhtompropane BFLl2lr-$ I Dibroflpchloomethane BRL106e3-4 j,2,Dibromoeihane (EoBi BFL71-e5'3 Dibroflomeihane 8ff195-m-1 j,2-Dichtorcbenzene BFL5417:1 1 l,$Dichlorobenzene BHL10&,1$7 l,+Dcntorobenzen€ BRL7171-8 Dichloodifluoromsthane (Fleofl12) BnL75-3+3 l,l.Dchtoroelhane 8RL107-{F.2 1,2-Gchtor4thane 8RL7t3t4 l,1-oichloroelhene BFL1scs9.2 cis-l,2.0ichloroethene 8RLrsml's lrans-1,2-Dichtoroelhene BRL7!-07-5 l,2-oidtoropropane BFL14c.284 l,$DichtooproparE 8RL
s4&-t 2,2-0i*,la!aprcpare 8RL
s6$s35 1,l-Dichloopropene BRL1006141-5 cis-1,3Di$hrcpopene BRL
111061{24 trars'l,O-Did{oropopene 8Rt
Volalile Orgsnic Compounds
VoC &lracliodVolalile oroanic Comoofi ds
1@414 Efrylb€nzenegl.6€3 lhxadkJobuladiene591.7&3 z_Heraflone(MBKi98.828 lsopropylbenzenet937-6 +lsoprop!4ioluene16ir4 {r44 l,t€thyl ted-butyl etherr0€.r0.r 4.Metryf2-penianom(M|BK)7s$2 t €lhyt€ne cnlodde9fal3 Naptlhal€ie
lJg4! d'y 98 z
lEfiq dry 1960
lqrS dry 1t8.2
tS4(S dry 118.2
lgrqdry s82
lg,kS dry 98.2
tltJr(! dry 9.2
rye dry 98.2pgegdry 196
yCq dry 982yvk! dry 982
IrS/kg dy 9E.2
pgtg dy g2
pS4$ dy 491
pqkS dy 982
psft! dry s82
!dk0 dy 1SG
|lg/k! dy 982
'lg,ks dy 196yg/l(o dy s2
ps/l(o dy s2
|]gn(! dy 196
pS,lq dry 9E2
Krtq dy 982
pgACdy *2
pgn(0 dv s2
pSI$ dy 98.2
ptk! dy 2ys/r! dy 196
Ps&t dy 9€.2
MS*y 9d.2
!s4(! dy 9€2
!S4q dy 9E.2
ldr! dry 98.2
!S4q &y 9E2
tlglq dry {t€2
W+get 98.2
!g,lq dry s8.2
|€/kS dry tB.2
rcnq dry S82
lgts dry 981
tlg/lq d'y 982
tt9'l,Set 082
psnq fy 082
rS*S fiy 08.2
|lg^S dry 98.2
pS/kg dry 982
liS*! dry 982
MkS dt 982
28-MN47 28-Mat41 7031161vclc
sw 846 6?608 294arc7 3GMar47 703lEN
8RI
BRT
8RL
BRL
BRL
8RL
8RL
BRL
170
50
50
50
50
50
50
50
50
50
50
50
50
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This labontory Hport k nat ,alid *ithout an authorized signatyrc o^ the cover page
a Repoftable Det€ction Limit BRr = Below RQorting LirEir Pag€ 53 of 154
Page 320
SampLe ldentificationMSF-39 2'-f'sA5980l-11
Client Proi€pt #30 t -88
MatrixSoil
Collection Date/Time26-Mar47 00:00
Received27 -Mat47
CAS No. Andlfu(s) Resan Flds Ul',iat "RDL Ditution tc nd ReI- Pnryed Aruryzei Bdkh An4lrst
Vohltle Orgadic Compounds
Vohde Orqarfc CunmrnGPrepared by nehod SW846 5030 Soil (high l6vel)100{51 ftPopyb€nzene10G.12-5 Sty€n66x!204 1,1,1,2-TetEdoroeltEnels3r5 1,1,22,T*Edorcelf€no1n-144 T€llachbro€t|ane108{93 Toluene0761{ 12,3-Triddord€n@neu!62r 12,4.1fi$brob€nzffe71'5!r{ t,j,j.Trichloroehanet9{,G5 1,1i.Tricloo€t€ne7!.015 lddJotlc€hdE7s-694 Tdd{oronuorornetEn€ (Freon I 1)$.1E-4 1,2.+fftfibrcpopane9ffi4 1,2,4Ttimeffylb€nzfll€10s.67{ 1,3,glnne6}ib€n2€n€75{1.r vinyt d orir€133G207 r4FXy1€00!6{7-6 o|Xyi€n€r0ss4 TelEhydrotunn@?*? Ehy eher
sg$s€ Teninylmsfiy'elhe.63? 94'3 Ehryl hrt hilyl etler10&20.3 oHsapogy' €h€r756fi fed.Eulanot / h4,tatc€hol12+El-l l,{{ioxane
41ilJ,4 +gnnoflwnb$Ene
&7-&5 Tduerle{fr
11!60474 1,2-DiC q1ethane44
164-Elt DifuoflpfrJorfilelhane
f, ttrcctrble Petoleum Hydro{r.bont
Enractabl€ Total Petdeum tMroaatods
Prepar€d by method SW846 35508
{Oe61'g Ga$ohe6A|76-3C2 Fu€lc{l#26817F31-3 FUel O1#{68s53-004 Fuet0lt6MF€O0&0 Mobloil.s010o00 Aviation Fuot
t lr*rentified
ohqoil
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CSC36 AlFhalic BydrGrtons
338F3+2 l4hwoMcaB
Semlvolaaile Orgr r Compounds by @
oroapd odne Peslicil€s SWE 16 8$l A
Prepared by method SW846 3545A
s{Gz Atdin
2Sl aF07 gl sr{7 761830 matBRL
BflI.
BflL
EffL
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8RrBRLBRT8R-8RLBNLMLSBLBRL8At88LBRI.SRL
1001&)g
95
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BFLBRLBRL8RL8fi1BfiLBFLBBLBRI.
90
50
50
50
50
50
50
50
50
{1
50
50
50
50
50
50
50
50
50
s05050al5050
Bfgdry g2
uykg dry 2
lgto dy 982
!$S eV 962
ldlS dry (182
pg,l€ dry 9a2
UdlSdy 982
llg,lq dry lxl,
$/rS ey 982
l4A0 dy 982
udl€&V 982
!d*S dty {lE2
l{/lt dY 982
lgr€d.y 982
lg,lqdry 982
tg/tq dy 962
t4l4ty 196
!s,to trl s82
rcnqdlY 982
|db rv 982
lSlqdy 98?
@fqdy q2
tgkg dY 982
ldkS ty W
!dk{ drY llm
7vtfr %76130 %7G130%70-td%
'!€/Iq diy ?82
mdlqdry 332
mglq dry A2
mgtgdry 332
mglSd] 332
n'Snqf} 332
nEl€ dry 3:i2
rEIq dry 3i12
rBlqdry 3t!
mSlqdy 33.2
4+140
rulq dv
sw 846 82ffi
+CT ETPfII
I
' 1
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BNL sw8a€ 80814 ?a41?f47 @.AF{7 mlng IG
?hk laborubr? Epo.t is ,ut vdid *ithod an aslhoizd sigAdare on the catcr poge-
! Rcporbble Detecrion Limit BRL = Below Reptrting Limit Page 54 of | 54
Page 321
Sample ld€ntificationM8r'-39 2'-4'sAs9803-l t
Cliert Proiect #30 t -88
MatrixSoil
Received27 -Mar-07
Collection DatelTime26-Mar47 00:00
CAS No- Analrte(s) Res,tll Flag IJnits *RDL Dilutbn Method Ref. Prcpsrcd Anslyzed Batch AhalJst
Semivolalile Orgrnic Compounds by CC
Ooanochlorine Pesticides SW846 8081 A
Prepared by method SW846 3545A
319-€4 € a.8HC319-85,7 SBIrC
319-86.8 d 8rc5e8e4 g,8HC (Lndan6)
st-74.9 Chbdanens4.s 4,a{00 (p,p')
72-5s.e 4,4r00E (p,C)
sG2e.3 4,a',00T (p,p )6G57.1 DielMn
95$9&8 Edos/fan I3321$65.9 Endosullanll103147-8 EndosulfanS0llale|Z-ZA-8 Endnn7421-s-4 Endnn Aheiyde/64,1-3 l-leplaafilora-€ s Metroxyc$lorr021t 57 3 Hedac+llor Epoide&01-35-2 Toxaphene510371.9 a-Chlordane556e34 7 g4htodane
5n4947G5 Enddn Kslo{l€
tB86aa2 1,4-Dg-0dalwtobiptent4lsr)
N6t2+3 Decachloro ptenyl (3r)
Polvdrlorinated Biphen!,ls bv SW846 80P,2
Prepafed by meihod SW846 35454
12674r r.2 PCB 1016r104?&2 PcB 1221r1r41, !6.5 PCB 1232
5345e-?1 e PCB 12rt2!2672-29.6 PCB 1248r1m7{9.r PCB 1254110e 25 PCB 12603732423 5 PCB 12621110014-4 PCB 1268
1@86a+2 4,4'D8-thafl@tDbiphenyi (St)
2051-21.J Decacllotobphenyl(Sl
Semivohtile Orgaoic Compounds by CCMS
Semivdalih Orcanic Comoounds b{ SW846 8270C
Prepared by method SW846 35508
8su{ Acef€phh€nezu46.8 Ac€mtht'yhne6A-$-3 Anilins1&-12.7 Anh€cens1912.24.9 Altazinelmnsr fuob€nz€n€/Dipheny,ldiazine92-87-5 8€ruidln€5&553 Seozo(a)anhacsn€
28'Mar{7 3qMar{7 703173a SM
211-{l&r{7 Cl}Apr{7 7031774 M B
8RL
BRL
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8RL
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119
91
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478
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47.8
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47.8
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47.E
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pvlq *vldkS dry
lgrs dvlgtg dry
lgkS dry
lgrs dry
ISAS dry
lgftS dry
lsas dry
wKs ory
lgxs ory
ldrs dry
|ls^s dry
lJgr(s drv
ldkg dry
Nag dry
lykg drypgxs ory
lgks 6y
lgks dry
ug,lq dty
30t50%3+150%
lgrs dry
lgks drypyks dry
|Js/l(s dry
udrs drypdls dry
!s.49 dry
rc4(0 dry
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*150 %gr1fl%
sw846 8081A
sw846 8082
sw846 627m
95.6 I
95€ 1
955 1
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|lgr'iq dry
This lzboratory rcpoa is nd wlid withoat aa o!rtoized sigMlurc on the coler ldge
* Reportable Detection Limit BRL = Below Reporting Limit Page 55 of 154
Page 322
Samole ldentificationM8F-19 2!-4'sA5980l-r t
Clieot Ploiect #30 t-E8
MatrixSoil
Rec€ived2'l-Mar-07
Collection Date/Time26-Mar{7 00:00
CAS No. Anzb@g) Rcsn/l FIAC Unia rRDL Dllaian Method ReL Prcpared Analy.ed ktch Aaatfst
Semivolatilc Organlc CorhlroIn& by CCMS
Semivdalf,e Orgonic C,srEounds by SW8,{5 827@Prepared by metllod SW846 35508so.e{ Benzo (alptEne205-992 Beflzo(blf@Entrene191-242 Benzo(g,tti)parylene?!7{&9 Bg]m (k) fluoranhene66'054 Bffzdc€ci,1oc5l.6 Befl4tatcdol11 1.s1 r Eb(2+loroehory)mefiane11l1rr{ Bd2doroetryj)efEr3trs@{ Bi{2dthdsopo9},1)edrer11741.1 es{2+tr'y'trexy0PhtDtate101.553 +BffinoCt€nyt ph€nyt etherss8.7 8tjtyl b€nzt ph$a,ate
&74€ Ca66!ole595r!7 44htdo-3-mqhytpltenol10F47{ rtclrloloanlin€
91.*7 2o{o'maphhal€nes5.57-8 2{|{orcF€ndTmtz'3 +Ctdorcphqylphonyt€her
218{1-9 onys€ne5+70.3 oabenzo(a,h)anhracsb1t2419 DbenzofuEn9S501 1,2-lld't|q'obenze0os11.791 1,3.tkfih.obenzene1116-'{&7 l,,t-Dtdiorobenzene
014+1 3,3',.Dnfibrobenzidiner2G8+2 2,4,0id{(.trphsnotu&2 oierhyl ptddate
13r-110 Dmehylp+ |atale1H74 2,+Dimeihtderd*7+2 On-butyl phhelate
s3+s?r 1,6.Dinitrc-2rndhy'phend5t'2+s a4.Dinihpn€nd'121.1t-2
aa-oinitdotsl€oG2O2 2,+Diritoduene1i7{'rc tt.n-od$ph[,able&444 Fuordittgn€&7I1 Fl O|EIet1&7't.1 Helad oDh€n:E|le6/48i1 tl€xdltorDhlsdenen474 Heradllooqcbp€ntadiene6r-121 lle)@d Oroetune1e+3e5 tndem(1,2,9cd)prBns!o12i l+JrymdhdEne7&5e1 hoptFiErloe!-57J 2-M€h&apitdens95.{&7 2- dry'Dheflol
10&39{, 3,4-lirehtphend106{r!t91413 Nephmaknew71-1 2tliboaniline0s0&2 $Nitrofiif,ne
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Ir.b labo&tory Epo.l it,tottdid wirhou.n aalhorizfd sigEaate od !h2 coter pa* -
r' Rcportrble Dete.tion Limir BRL = Below Reporting Limir Pegc 56 of 154
Page 323
SaErple ldentificationM8F-39 2'-4'sA5980l-r r
Client Proiect #301_88
MatrixSoil
Recoivcd2'7-Mar-07
Collection Date/Time26-MaG07 00r00
CAS Na Anatrte(s) Result Flag Units 'RDL Dilation Merhod ReJ, Peparcd Anqbzed Bakh Analrsl
Semlvolrtll€ Orgrnic Corr|poundr by cCMS
Sernivolalile Ooanic Compound b! SW846 8270CPreparod by method SW846 35508
10041€ +NitDamtine BHt9s€5.3 itmb€nzme BRL
!s'25-5 2.Nitoph€not BRL10042-7 +Ni@Enol [email protected] 9 N,Nifosodinethylarnine 8RL@lt+7 N-Nilrosodi-ntropylamine 8RL
6.30{ N-Nilmsodiphenylami0e BRL
Er{6.5 pentadllorcphend BRL
6rr_8 Phenanhrene 8RL10€452 phenol BRt129{04 ry.ene BRL1lo-oc1 pyrtdine 8RL120.02-t 1Pd-Trichloroben2ene 8RL
95-991 2,4,5-Tridiorophend 8RL6.06.2 2,4,6-Trid orophenol BRL
a1{o4 2-Fhrorofuhenyl 546?-t21 2-Fhlorqvnd 571166@4 Mtt6qzene45 n1166f4-2 PheMl4s 5f17106t4 leqlwyl44 n1t&tc4 Z4,efibtonophgnd 51
Tskl Melrls by EPA 6000/7000 Series Mettodr
0.209
29-Mar{7 o&{p.{l 7031174 M.BtiSlq fiy 3300
fSfrS dry 824
pSfrS dry 824
!g4q dry 3300
p$4q dry 8?4
pdlq dry 824
fS,Tq dry 824
pdkS dry 824
lslq dry 824
!s/rq dry 824
ldlqdry 824
ldlq dry 824
pg4q dry 824
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30.130 %
1r110%
iG130 %
t r 1 t 0 %
&130%
l 6 t l o %
ng/tq dry 0.0455
ms^S dry l.4l
r,g/kS dry 2.12
n'94(g dry 0.705
fidkg dry 0.353
nqls dry 0 705
myrs dry 106
mS,4q dry 212
mS/ 0.0100
mgl 0.0150
mgl 0.0050
mgn 0.0025
mdl 0 0125
ngil 0.0m40
mg/l 0 0075
mq,4 0.0150
sws46 8270C
o2.Apr{i 0}Apr07 7031810 YP71ls975 Merc!ry
Tolrl Metrb by EPA 200 Seri€s Methods
lt4u-al Silver
?lrl$38? AGenic
7,!lll3g3 Badum
741$4+9 cedlnium
t1,d"41,3 Cktrnium
TIEF !lz-1 Lead
[email protected] S€leflium 3.3s
SPLP Melrls by EPA 1312 & 600Ot000 Series Methods
SPIP Extaclron Corndeled
7@-?44 Silvor BRL
t440.3S2 AEenic BFL
71{0n&3 Bariom 0.m98
7440-13{ Cadmium 8RL
7lr$<^t Chomium BRL
?130.gr{ M€rolry BRL
r3ss2-l kad 8RL
782492 S€tenium BRL
Cetercl Chemfu try Parsh€terj
%Sohrh 65.7
1 i . 8
sw8.167471A
EP4200.7
sw84613r2
sw846 r31260108
sw846131274704
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3)Mar-07
HB
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02-Apr-{)7 70{11805 tR
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This labonlory rcFod it not ealid wirhott an authori.ed signara.z oa lhe coter Fage .
I Reportable Detection Limrt 8RL = Below Repoding Limit Page 57 of 154
Page 324
Sample Id€ntificatio11M8F-40 2-4,sA595l7-08
Client Proieot #30t-88
Collection Date/Timelg-Mat47 00:00
MatrixSoil
Rcceived20 Mar-07
CnS No. Ana\te(s) Res l FI"S Units +NDL Dilutbn Method Retr. Prepared AnatJzed Batch Analfst
Volatlle Orgrnic Compounds
VOC Extraction Field exfacted
181
pgftg dry ts1.4pdkgdry 1230
lqkg dry 61.4
UgkS dry 61.4
!g/kq dry 6r.4
!g/kg dry 6'1.4
fdkS dry 61.4
Udkg dry 61.4pdkS dry 123
LiS/kS dry 614pg/kg dry 61,4pdkg dry 61.4pdkS dry 61 4
ldkS dry 30/
IdkS dry 61.4
Ug/kg dry 61-4
rc/kS dry 123pS/kS dry 61.4pS/kg dry 123
US/kS dry 61.4
ug/kg dry 61 4pg/kg dry 123
tgtkgdry 61.4
lrdkS d.y 61 4yg/kg dry 61 4pdkS dry 61 4
US/kS dry 61.4pdkg dry 61.4
l.dkg dry 123
US/lg dry 61.4pg/kg dry 61.4
ug/kg dry 61 4
l4/kg dry 61.4pgtkSdty 61-4
PdkS dry 61 4
tdkg dry 61.4
udkg dry 61.4pSftS dry 6'1 .4
PdkS dry 61.4pdl€ dry 61.4
!S/kS dry 61.4
tSlkgdry 61,4
!S/kS dry 614
ldkS dry 61 4
ldrg dry 61.4
i.idkS dry 61-4
!g/kg dry 614pg/kg dry 614pS/kS dry 61.4
Volatile Oroanic Comoounds vocoPrepared by method SW846 5030 Soit (high tevel)76't+1 1,1,2-fidrlotohnuorcethane(FeoERL676rr_r Acetone BRL107-13F1 Acrylonltrile BRL7143.2 genzen€ BRL108-46-l Brcmob€nzene BRL7+97-5 gromochloromethane BRL71274 Brumodichtoromethane BRLf,2r2 Brcmoform BRL74{}9 Bromomethane BRL7&913 2-Eutanone (MEK) 8RL104-514 n_Bulytbenzene BRL13S984 s€c-Butytbenzene BRL9a{G6 tert-Butytbenzene BRL7r1SO carbon disutftde BRL56-23-s Cabon tebachtoride BRL10e.s0-7 chloobenzene BRL750G3 Chlomelhane BRL67{F3 Chloroform BRLt447-3 Chloromethane BRL95-49{ 2-Chlorotoluene BRL10q3,! +chlorotoluene BRL5124 1,2-Dibromo-3-chtoropropane 8RL124-,€n Dibrornodrtorcmethane BRL10&93-1 1,2-Dibromoethane(EDB) BRL74-9t3 Dibromornethane BRLgs.slj.l l,2-Dichtorobenzene BRL541.73-1 l,3-Dicllorobenz€ne BRL10tu6-7 l,4-Dichtorobenz€n€ BRL75-71-8 Oichlorodifluoromethane (Frcont2)BRL75-31F3 1,.t -Dichloroethane BRL107{6-2 i,2-Dicthloroethane BRL75-3s4 l,l-Dichloroethene BRL15e59-2 cis-t,2-0ichtoro€hene BRL156{0-5 trans.l,2-Dichloroetf€ne 8RL7&47-5 1 ,2-Dichtoropropane BRL142-20-9 I ,3-Dichtorop.opane BRL594-m-? z,2-Dichloropropane BRL50+584 l,l-Dichloropropene BRL10ool-01{cis-1,3-Dichloropropene BRL1m61{2€ kans-1,3-Dichloropropene BRL10S,114 Ethytbenzene BRL674&3 Hexacblorobutadjene BRLs9r.784 2_Hexanone (MBK) BRL98€2-8 tsopropytbenzene BRL99-87{ +lsopropyttotuene BRL163a44a Mehyl teft_butytethef BRL10&10-1 4-Methyl2-pentanone(M|BK) BRL75{9-2 Methytene chtoride BRL
voc
sw846 8m08
21-Ma.-O7 21-l at 07 7031261 BO
27-Mar07 27-Mat 07 7031602 fiar5050505050505050505050505050505050505050505050
505050505050505050505050505050505050505050505050
505091.20.3 Naphthalene
Pss€ 37 of 124
This labotulory report k noa valid arithoat on atthoriaett signoture on ahe corer page
' Reportable Delecrion Limi. BRI- = Belovr Repsting Limit
Page 325
Sample Idetrtific{tionM8F-40 2-4'sA5951748
Client Pioie€t #301-88
MatrixSoil
Collection Date/Timel9-Mar-07 fi):00
Receivedzo"Mtt47
CAS No. Analrle(s) Fl"g U,zi^ 'RDL Dilutiatr n{ettud Rel, P.eprd Analturl Bdlc$ Analtsl
i0$651 n-Propylt€nzene10(82-5 Styr€no63s2o4 1,1,1,z-I€trachloroehane7s3+5 1 ,'1 ,2,2-let-ehlorce$ran€127-18-4 TetrachlO{Oehene108{&3 Tolu€ne87-6i.6 1,2,lTdthl6obenzene12G€2-1 l.2.4lrichlorobenz€ne71-s5-6 1,1,l-frichloroethane79{0-s '|.1,2-Tnc$loroethan€
79{1{ Tficfiloroethene
vohaile Orgrnic Compolndr
Volatile Oroanio CompoundsP,oparod by method SW846 5030 Soil (high level)
BRLBRL
BRLBRLBRl-r58BRL
BRLBRLBRLBRL
75-69-4 Trichloroffuoromethano (Freon 11) BRL96-10-4 l,2,3.Taichlo.opopane ARL9543-6 1,2,4-Tdmethylb€nzene BRLt08$7{ 1,3,5;Trimethytbenzene BRL
BRL1.{}
66.3BRLBRLBRLBRLBRL8RLBRL
1001A
94
BRLBRLBRLBRLBR.LBRT791C€lc{rlated as
vdkgdry 61.4
t/glkgdty 61.4
Fdl€d.y 61.4
rdkS dly 61.4
rcikS d.y 6l.4
UdkS dry 61.4pdkgdry 61.4
ldkS dry 61-4ydkSdry 61.4
rgtgdry 61.4
|,4kg dry 61.4pdkg dry 6f .4
rc/XS d.y 6t.4
USrkS dry 61.4pgftSdry 61.4pdkgdry 614
IdkS dry 123
!S/kS dry 61 4pgrkS dry 614
rdkg dry 61.4ygtsdry 61.4pgts dry 61 4pdksdry 61.4pdxg d'y 614
UdkS dry 1230
76130 %70-130 %70-130 %70-130%
mg/kg dry 17amS/kS dry 174mgn€ d.y 17amgftg dry iAmdkg dry t7a.rE/kg dry 178mgilgdry 17Amgrqdry 17ArE/kgdry 178nglagdry 178
4+140 %
50
5050
50505050505050505050505050
50
SW 846 82608 27-Mat4f zl-MaFO7 70316m mar
+CT ETPH 22-Ltur{}7 26lvlar-07 7031284 DS
7541.1 Mnyt chlo*teit3o.2cr m,p-xylengs+474 o-Xyleoe1O$9S-9 Tetrahydrofuran6{F2s-7 Ethytet}Ef9s4ffi T€ft-arnyldlethylethere37-92-3 E|hyl tan-butyl edEr10e20-3 Ctiisopr@yt€th€r75.65{ Tert-Butanol/ bntyl alcohol12$9r-1 1,+Dio)(ane
Srr,?og€le r€cov€nes:46040{ +Brcfiof,uorcbenzeae
2037-265 foltr€.t€4S
17060474 1,2-Did O@e?hane-d4
1868-gA-7 Dbtondlto@rnethane
f, nctrble Petrolatm llydrocrrbont
Extractable Total Pgtol€um Hvdrocarbons
Prepar€d by mefiod SW846 3545A
AOo€al-9 Gasoline6€{7e3cz FuelOll#26842631-3 FuetOil#466553-00-4 Fuel Ol #6Mos800o00 Moto( OilJOOI()()000 Aviatjon Fud
Unid€ndf€d
of|€r Oil
Total Peboleum Hydrocedons 797
CSC3,€ AliphElic Hydrccarhons 797
Sunog6fo f9cot ends.'$8n332 1-Chlot@ddecarE 158
ScDlvolrtil€ Orgrnlc Compourds by cCOroanochb.ine Pestbides SW846 8081APr@ar€d by method SW846 35508349{e2 Atdrtn BRL LidXS dry 6.16 SW84A 8G1A ?2't|er-Ol 27+ns47 7031275 TG
Thit laboruloq rqort &t ̂ ot uaIU *ilhout aA authotl&d dgralare on dte &rer pcge -
' R@orhbl€ Detedion Limit BRL = B€low Reponing Lirnit Page 38 of 124
Page 326
Sample IdeptificarionMtF-40 24'sA595 | 7-08
Client Proiect #:r01-88
MatrixSoil
Collection Date/Timel9-Mar-07 00:00
&!!siyed20-Mar-07
C,aS No. AMIla(s) ResaIt FI"S Units *RDL Method ReI. Prcpared Analrzed Batch Arutltst
Semivohaile Orgrnic Compounds by CC
Oroanochlodne Pesticides SW846 8081A
Proparod by method SW846 35508
31se4{ a-BHC
319+5-7 brBHC31+86{ d-BHC58{}9 g-BHC (Lindane)57-1+9 Chlordane
72-3+s 4,4-ODD (p,p')725'e 4,4,ODE (p,p')
so-2s-3 4,4-DDT (p,p')
on57-t Dieldrin95948€ Endosulfan I33213{+9 Endosultan ll1031-07{ Endosulfan sutlat€72-204 Endnn7421-934 EndrinAldehyde7641-A Heptachlor7243.5 l,bthorychlor1024.57-3 H€ptaclhtorEpoxidea0O1-35-2 Toxaphene
s1o3.71'9 a.Chlordane5,s{t6.34.7 g-Chlordane
r,3,49+70-s Endrin Keirne
Sudog€ls rscover'gsi1 03863+2 4, 4 -DB-Octaff uorobiphenyt (Sr)
mst-2a-3 Decachlorobiphent4 (St)
Polvctrlorinated Biohenvls bv SW846 8082
Prepared by method SW846 35454
1262L11-2 PCB 1016111u-28-2 PCB jZ21
11141-16-5 PCB 12325346*21-9 PCB 12421fr72.:g-B PCB 124A11rxr7-6s1 pCB 12541 109tr2-5 PCB .1 2603732+23-5 pC8 12621fi0c144 pC8 1268
Sunogale recoyeresr1 03864+2 4,4 -DB-Octan uorobiphenyl (Sr)
2051-213 Oecachlorobiphenyl (54
Semivolrtile Orgstric Compounds by CCMS
BRLBRLBRL8RLBRLBRLARL
8RLBRL
BRLBRLBRLBRLBRLBRL8RLARLBRLBRLBRLBRL
3252
BRLBRLBRLBRLBRLBRL23.4BRLBRL
4090
BRL
BRLBRLBRLBRLBRLBRLBRL
ldkg dry 6.16pdks dry 6.16
lig/kg dry 6.16pdkS dry 6.16
UdkS dry 30.8
udkS dry 6 16
UdrS dry 6.16
IS/kS dry 616pdkS dry 6 16
lgtgdry 616pg/kg dry 6-16
ldkS dry 6-'16
lgrS dry 6-16
ldkS dry 6.16
!Sn$ dry 6.16psil$ dry 6.16
lqkg dry 6 16pS/kS dry 30-8pdkS dry 6.16pgkS dry 6.16
!S,/kS dry 6.16
30-150 %30-150 %
!g/kS dry 12.3
ldkS dry 12 3
tdkSdty 12.3pdkS dry 123pq/kg dry 123
!S/kS dry 12.3pg/kS dry 12.3
!S4<S dry 12.3
!S/kS dry 12.3
30-150 %3G150%
ldkS dry 1770
ldkS dry 1770pgks dry 1T7O
lrdkg dry 1770
udks dry 1770
Uqlgdry 1770pS/kg dry 1770
lSn(g dry 1770
I
I'|I
1
1
1
1
1
1
1
1
I
1
1
1
1
1
1
1
1
SW8.f6 8081A z2-Ma.Ol 27-Mat47 7031275 TG
SW846 8082 22-Mat47 24-Mat47 7031313 l\rP
SW846 8270C 23-Marol 25-M^t47 7031371 M.B
Semivolatile Otuanic Comoounds bv SW846 8270CRepared by method SW846 35508
a&32-9 ACenaphth€ne206'964 Acenaphthyten€
Aniline12G12-7 Andl€Cene1912-24-9 Ataazine10$3$3 AzobeMene/Diphenytdiatne92-€7.5 Benzidine5645-3 Benzo (a) enthracene
22222222
Thie laborularf rcpoft b not vdiil withou an auihorized signatt rc on lhe corer page
* Reportable Del€ctioE Limir BRL = Below Reporting Limit Page 39 of 124
Page 327
Sample ldqntificationMEF-{o 2-t'sA5951748
Client Proiect #30t-88
MatrixSoil
Collection Dat€/Timel9-Mar-07 00:00
Received20-Mat-07
CAS No. Andtrta(s) Resalt Fl"S atb +RDL DUdIfi Mdhod n4, Pry)arul Analyzd Adch Adrtyst
Semlvol.lile Orgrtric Compo(trd3 by CCMS
Semivolatile Orcanic Co.nooonds bv SW846 8270C
Preparcd by method SW846 35glS50-32{ Eenzo (a) pyiEne20tgs-? Benzo (b) nuoraMeie191-24-2 Eenzo (g,h,D perylene207-08+ Eenzo (k) fuofsnthene65-0tO BerEolc acit10+51{ Benz}'l alcohol111,91r Bis(2drlo.oethory)rnecr6ne1i1-,!4-4 8is(2d{om€hyt)etE.3.963+3?-9 Bis(2.cl' cinisopropyl)€th€rr17€r-7 Bis(2-ethyth€ryt)phthdato10155-3 +Brcmoph€nyl phenyl eth6r65{&7 Butyt benzyt phthdtate€&74-€ Carbazotessfl).7 4-Chlorclmethytphenolr06-a7€ rl_chlofoaniline9f5S7 24htoronaphlhalen€F57-A 2chtofophenol700+72-3 4oftlorcplrenyl phenyt elher21&01-9 Chaysen€53,7G3 oib€|lzo (a,h) anthracen€132-64-9 Dibenzofuran95{,G1 |,2-Dafilorobenzenesr1-73-1 1,3-Oiohloaot€nzene106:-16-7 t,+Did{orobenz€ne9r€4-1 3,3',{ichlorobenzidine1aH3-2 2.4oicHorophenol844c2 Di€f|yt phthatatei31.r1-3 Oinethylphthatate10tr7€ 2,4oimethy'ph€no,lu-74-2 Di-n+utylphthalato5'?+52-t 4,6-Dinito-2-methylphenol5l+s5 2,4oinibophonol121-14-2 2,+Dinatobhene€0G2G2 2.8-Dinitrotoluener 1 7.€1-o Di{.octyl p,hfEt€tje20Ga4-0 Fkro€ndr$ew-7T7 Ffuof€nell$Z,l-1 Hexad*lrob€rizen€€7{e3 Hex€alorobutadienen474 l-lexgchlorocydop€itadiene5f-72-1 l-lexac'troethane191395 trdem (1,2,3-cd) pyren€!lo-12{ l-llathylmphtrEtene7E€$1 lsophomn€9l-574 2.Mefirnapfihatene*48-r 2-t{etrytpt eootr0&3e-., 3,4-Methyph€nol105JH-591-20-3 NapMElene8e-74-4 2-Nitlanilines9{92 }Niloanllin€
BRLBRLgRL
BRLBRI-BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRfBRLBRLBRLSRLBRLgRL
BRL
BRLBRLgRL
2.m0BRI-BRL
BRLBRLBRLgRL
BRL
BRTBRLBRL
BRLBRLBRL
ldkS dry 17fOpS/kS dry 1nOpg/kg dry 1770
ldlSdry 1770
Fdks dry 1no
lgftSdry lno
uSn{S drJ '1770
pdks&y 1770pSikS d.y lTlO
IglaS dry 1770pgrs dry lnl
Ugkg dry l77o
UdkS dry 17ro
IrSftS dry 1f?o
Wil€ dry l77OpC/kg dry 1nOpSftg dry 1T7opdke dry 1770
udks dry 1770
ldkg d.y 1770pSI€ dry 1770pdks dry 1770pgrS dry 1no
!g/kS dfy 1770
ldks dry r77o
rcftg d.y 1770
!s/ks dry 1770
ldxSd.y 1Tl0pdkSdry 1770
fdrgdry 1170
ldkS dry 7770
rgrq dry lf?o
!9ft9 dry 1770pdkS d.y 17fo
Ug/kS dry 1T7Opqkgdry 1770
ldrgdry 1770
fldrqdry t?70
rdkS dry 1770pdko d.y 1770
US/tgdry 1Tl0pdks dry 1770
ldksdry 1770
FS/kS dry lrTO
tdfqd.y 17rO
tgftSdry 1770
!g/kS dry 1770
pS&S dry 1770
ldrgdry rno
UgkS dry l77O
22222
2
222
222
2222
2
222222
22222
2
2
2
2
2
SW846 8270C 23.Ma147 2r>^tief47 7031371 M.B
Thlt bboraloq .eporl k ,roa tditl tsithoet a, seho z.d stgdatsrc on ahe cavu pagc.
' R€portable Deie€lion Limit BRI- = B€low ReportinC Limit P.ge 40 of 124
Page 328
Sample [d€ntificationM8F-40 2-4!
sA59517-08
Client Prorect #l 0 r -88
Collection Date/Timel9-Mar-07 00:00
MatrixSoil
Received20-Mac07
CAS No, Anabte(s) Resqll Flog Unia *NDL Dilutian Method ReJ Prcpared Anallzed Rarch Anaryst
S€mivolrtile Organlc Compounds by CCMS
Semivol€lib Oroanic Compounds bv SW846 8270C
Prepared by method SW846 35508
10G01{ 4-Nitroaniline
98-9+3 Nitobenzenea8-7gFs 2-Nitrophenolt0tr02-7 4Ntroph€no,l62-75.9 N-Nitrosodimethytamine62r{4-7 N-Nitrcsodi.n-propytamine86-3G6 N-Nilrcsodiphenytaminel7€GS Pentachlorophenol
85-01€ Phenanlhrene10e95-2 Phenol
i2lHD{ Pyene11G86-1 Fl.idine120-02-1 1,2,4-Trichlorcbenzone
95-95-4 2,4,s.Trichlorophenolg€.{G2 z,4,GTrichlorophenol
Sufogale recoveies:
3214G8 2+luorobiphenyl
7-12-! 2+luorophenol
4r6s-6oo Nitrobonzene4s
416s42-2 Phenol4s
1718-514 Teryhenyl4l4
1I&794 2,4,6-Tibromophenol
Totd Mellls by EPA 6000fl000 Series Methods
743947{ Mercury
Toarl Mctrls by EPA 20O Series Merhods
zr4G22-4 Silver
744036-2 Aisenic
7440.39-3 B€rium
7440-4+9 Cadmium
744Ga7-3 Chmmium
7,13992-1 Lead
z7E2-1+2 S€bnium
SPLP Metrh by EPA 1312 & 6m0/7000 Serier Methods
SPLP Extrection
I{4+22-4 Silver
7,1,|I)-3&2 AEenic
74rg!393 Berium
74()4+9 Cadmium
?.r,{o-.r7,3 chromium
7439€7-€ Merc!ry
2439{2-1 Load
7782-492 Setenium
C,€n€rrl Ch€mistry Panmet€rs
222222222222222
SW846 0270C 23-Mar47 25-MarO7 7031371 M.B
1 SW846 747'lA 26-Mal-07 27-Mar47 7031322 YP
EPA200.7 26-MaFO7 27-Ma?O7 7031321 HB
BRLBRLBRL
BRLBRLBRLBRLBRLBRL
BRL2,090BRLBRLBRLBRL
108809876122106
Completed
ARL
BRL
0.0128
BRL
BRL
BRL
0.0263
BRL
89.9
pg/kg dry 7O7Opg/kg dry 1770
!g/kg dry 1770
tgkS dry 7O7O
IgftS dry 1770
UdkS dry 1770pdks dry 1770
lSftS dry 1710pdkS dry 1770pgtS dry 1770pg/kg dry 1770pdkg dry 1770
!g/kg dry 1770
ldkS dry 1nOpdkg dry 1770
30'130 %1U l10 %30-130 %15-110 %30-130 0k
1&110 %
mg/kg dry 0 0330
fitg/kS dry 1-O7
mS/Xg d.y 150
rnSftS dry 0-535
mgftg dry 0-267
nEftg dry 0-535
rE/kS d.y 0.802
ntSnq dry 1.60
mg!4 0.0100
mg/l 0.0150
mqa 0.0050
mg"4 0.0025
mg./l 0.0050
mg,4 0.00040
mg/l 0.0075
mg/l 0.0150
0 .136
'| .24
10.4
52.1
1 .00
25.0
201
BRL
1 SW8461312 22-Mar47 22-Ma.-0l 7031344 BD
1 SW846131260108 23-Mat4f z+Mer07 7031408 LR
1 "
1 ' ,
1 '
1 "
1 SW8461312t470A " 26-Mar07 7031409 YP
1 SW846131260108 " 24-Mal.O7 7031408 LR
1 ' ,
1 SM2540 G Mod. 24-Mat47 24jv.al.07 7031463 OP% Sol ids
PaBe 4l of 124
This hbodory rcpod is noa wlid arithot ! an suthorked sEnatare on the coeer poge.
I R€ponable D€.ection Limit BRL = Below Reporring Limi(
Page 329
Samole IdentificationM8F41 4-5'sA5951749
Client Proiect #30IJE
MatrixSoil
Received20-M^t47
Coll€ctiop DatdTime| 9-Mar-07 00:00
CAS No, Aaolytz(s) FI4g A a rRDL Dilttlbtt Method Retr Pepared A@lyzed Bat4h Analr$t
Voladl€ Orgstrlc Compounds
VOC Enra€tion MA
ldks drv 6.6
t dks dry 132
lSftS dry 6.6pdks dry 6.6
lgrg dry 6.6
flg](S dry 6.6
Wks dry 6.6
rdks dry 6.6pSftSdry 13.2
Fdks dry 66.2
lg,lqdry 6.6
Uglkgdry 6.6
lgkg dry 6.6pdkg d.y 33.1
lgxgd.y 66
uSASdry 6.6pdrg dry 13.2
ldkgdry 6.6
udkS dry 13_2
Idkg dry 8.6
tdks dry 6.6yCftgdry 13.2
Pdkg dry 6.6
tdkgdry 6.6
fldkS dry 6.6pdkg dry 6.6
tjgiksdry 6_6pSftSdry 6.6pdkg dry 13.2
tgkgdry 6.6pdkSdry 6.6
VdUvJdty 6.6
trdkg dry 6.6pdkg dry 6-6pS/*Sdry 6.6pdrg dry 6.€pdtgdry 6.6pdkg dry 6,6
tdkdry G.8
udkg drv 6.6
!S/rqd.y 6.6
rdts dry 6.6
lcrtgdry 66.2
udkSdry 6-6
ldlq dry 6.6
Igrkg dry 6.6
ldkg d.y 66.2pel{g dry 66.2
Fdrg dry 6.6
21-L.lar.07 21-llar-07 7031261 BOFreld exbacledVolatile Oroanic ComoaundsPrepared by mef|od SW846 5035A Soit (torv bvet)76n11 1,,|,2-T.id orohnuoroothane(FreoERL674+1 Acebne SRL107,13,1 Acrytonitdte BRt_f11t2 B€nzene BRL108-86-1 Bro.nobenz€n€ BRL71-91-5 Bronroafiloron€thrne BRL75-27'4 Brcmodichloronethane BRL7r2r2 BDmototrri gRL7,t{}9 Brcmcmethan€ BRL7&9!3 2-ButanorE (MEK) BRL101-51€ n-Bulylbe@en€ BRLl3tFgE{ s€eBuq/b€nzen€ BRL9€{6.6 tsft€utylbenzere BRL7!v1s4 C€rbon disulfde BRL5€-23{ Ca6on letrachlodde BRL10&$7 Cftlbmb€nzene BRL?5{G3 CHormthane BRI_676e3 Chloroform BRLA-47-3 Chloromelhen€ BRL!15-49{ 2{hlorotolu€ne BRL106-434 +Chlorctoluen€ SRL9G12€ 1,2-ubro{ytc}chtoropromne BRL124-4€.r Dibrcmochloiomediane BRLioCg3.a l,2Obrorno€lhan€ GDBI BRL744+3 Dibrchom€thane BRL96-5G1 l,2.Dichlorobe.Eene BRL54r-?!l |,3-Didrloob€nzene BRL10€-1{}-7 |,4oicfilomb€nzene BRL7s71€ Dichlorodffuoromethane(Freon12)BRL75'34-3 1,1-Oict{oroethane BRL10rc€-2 l.2-Dichtoroethane BRL74.3s l.|-Dichtoroethene BRL156-5e2 cis-'1.2-Dichloroeh€ns BRLt5G@-5 bam-1,2-Dichloroethene BRL7E{7-5 l,z-Dichloropmpsne ARL142-28.9 l,3{iclilorcpopane BRL59+20-7 2,2-Dicl{orcprop€ne BRL563-58€ i,1-DichtorcDroo€n€ BRL10061{r€ cis-1,3-Dichloroprcpene BRLi0061-o2€tEns-1,3-Didtloroprop€ne BRL100-41.1 Ethyft€nz€oe BRI674&3 Hexaailorobutadiene BRL591-786 z-Hel(anon€ (MBK) BRL9O{2{ tsopropylbenz€ne BRLs-87-6 +Lsop.opy'bluene gRL1634{s ilethylt€rt-brtylether BRL108-rct +ilethy'i-21o€i1l&one(MIBK) BRL7s4*2 M€thylene dtlodde BRL
SW 846 82608 e.-Mat47 n+tat{7 7m1335 RLJ
9l-2G3 Naphhaleno
Page 42 ol 124
Thit lzborotor! rqod is noaealld vi pat an ar.thorizey' sigdaturc o, the cora, page.
' Reporhble DotecrtuE Lindt BRL = Betow R€poning Limit
Page 330
Sample IdentificationMEF-4r 4-6is459517-09
CLient Proiect #301 -88
Collection Date/Timel9-Mar47 00;00
MatrixSoil
Received2I-Mat07
CAS NL Ahqlrte(s) FI"S *RDL Dilution Method Retr Prepared Anzltzed Batch Anobst
Volatlle Oryrhic Compoundr
Volalile Oroanic Compounds
Prepared by method SW846 SO3SA Soit (tow tevet)
10365J n-Propylbenzene BRL1fi82-5 Slyene BRL6:1120{ 1,1,1,2-Tetrachtoro€thene BRL?9.34's 't
,1 ,2,2-Tet.achloro€thane BRL127n4-4 T€kachtoroelhene BRL10&€43 Toluene BRL07{1{ 1,2,}Trichtorobenzene BRL1A|82n 1,2,+Trichtombenzene BRL7r{54 1,1,1_Trichloro€thane BRL79{C5 1,t,2_Trichtoroethane BRL79{1{ Trichloroethene BRL75{H Trichloronuoromethane (Freon 11) 8RL96{0-4 l,2,sTrichtoropropane BRL96-63-6 l,2.4.Trimethylbenzene BRLi0&67{ 1,3,5-T.inrethytbenzene BRL7541-4 Vinytchtoride BRL1S0-2G7 n,p_xylen€ 8RL9+47{ o-Xylene BRL10s99-9 Tehahydrofuran BRLdl-2+7 Ethytether BRLBa{5{ T€rt-amyl methyl eher BRL6fl42-3 €thytte,t_bulyt ether BRLt0&2G3 Diisopmpytether BRL7565-0 Tert-B,llanot/ butyl alcohot BRLi2341-1 l,4-Dioxane 8RL
Sanwale Gcove,i€sl4loM 4-Bromofiuorobenzene 92m3f-2e5 Toluane4S 9917060474 l,2Dichlorcethane44 109lAOA-sj.7 Dibronofluorcmathane 1O5
Extrrctrble P€troleum Hydrocrrbom
Extractable Total Petroleum Hvd.ocarbons
Pr€pared by method SW846 354SA
SW84682604 22-Mar47 2rMarOT 7031335 RLJ
+CTETPH 22-Mar47 26-Ma(OI 7031284 DS
lgkS dry
!S/kS drypdks dry
ldks dry
rrS/kS dry
!S/kg dry
l4/kg dry
lig/kg dry
tdlq dry
!g/ks dry
LrdkS dry
t'S./kg drypg/kg dry
l'dkS d.ypqkg dry
!S,kS drypS:ftS dry
LiS/kS dry
!g/kg dry
ldks dry
t4/kg dry
!g/kg dry
!g/kg dry
US/kS drypdks dry
6.6
6.6
6_6
6.6
6.6
6_6
6_6
6.6
6.6
6 6
13_2
6.6
66-2
6_6
6.6
6.6
6.6
66.2
132
I
1
1
1
1
1
1
I
1
1
1
1
1
I
1
I
I
1
1
1
1
I
I
1
1
8,Om{1-9 casdine6€47s3G2 FuetOit#26847s31.3 Fuet Oil #4€€563-{rs4 Fuel oil #6lvtlgso(o(l) Moto, Oiirl010o00o Avialirn Fuel
Unidenlified
Othef Oil
BRLARLBRLBRL
SRLBRL728
Calculsted as
70-130./o70-130 %70-130 %7G1m %
mgr'kg drymg/kg drynE/kS dryn'qkg dry.ndkg drymg/kg drymg/kg drymdkS drymSftS drymS/kg dry
40-140 %
185 1
185 1
185 I
185 1
185 'l
185 1
185 1
185 1
1 8 5 1
165 1
TotalPelroleumHydroceftons 728
C}C36 Aliphatic Hydrocarbons 72A
Sunwafe recouenes_,3?'86312 r -C h I otoo cts d eca n e
Sc]r|holstil€ Organlc Compouds by cCOroanochlorine Pesticides SW846 8081APr€pared by method SW846 355083q9{X}2 Aldrin PSi l(g dry SW84680€14 22-Mar47 27{.nat47 7O312f5 fc
Thb laboralory repo.t k not volid |9ilhoat an ouahorized signaru.e on lhe coeer paEe_
. Repodabte Detedioo Limit BRL = Below Reporting Limit Page 4l of 124
Page 331
Sampl€ IdentificationMtF-41 4-6'sA595l7-09
Clietrt P.ojec! #301-88
Mari{Soil
Collectiotr Date/Timet 9-Mar47 00:00
Received20-lvlar47
CAS No. AaalWG) Fl4e 'RDL Diluioa Me.hod Retr. Ptepated Anaryzd Balch Aaztpt
Semivolsdle Org. c Compounds byCCOrqanocf orin€ Posticides SW846 8081APrepared by melhod SW846 3550831$44{ a-BHC3rs-0+7 b,BHc31s{6{ d-BHC58{99 g-BHC (Lindane)57-7+S Ct ordane72-u-a 4,40DD (p,p,)72.5$s 4,+DDE (p.p,)5o?s3 4,4-DDT (p,p.)6{L57-1 Dieldrin959-98{ Endo6ulfan I36213-65{ Endlosulfan lll03i{74 Enclosultan &rtfet€72-20.4 Endrin7421.93-4 EndrinAtdehyde76-44{ H€ptadtlor72-.3^5 M€froxychlor1024€7r H€ptachlof Epoxide60olns2 Toxaph€ne510$71-9 a-Chlordan€5,566,3,t-7 g-Chbdan€5349|70-5 Endrin Ke{on€
Sdaog€fe r€coysnies.'103866+2 1, +Dei-Oclduotohiphenyl (Sr)m5t-21-3 Decachbrobiphenyt (Sr)Potucfibrinated Biohenvls bv SW846 8082Preparod by mehod SW8,t6 354SA12674-i1-2 PC8 t0t61110+2V2 PCB 121rr1.r-16{ PCB 12325x46$214 PCB 124212672-29+ PCB 12/|81i097$r PC8 t 254rr0e6{.5 PcB 12603732+3"5 rcB 1262r11(rc-r4r PCB 1268
S(,/rlogEle r€co|Eriesr1u#re4+2 4, 4-DSOcbf @rcbhhenyt (Sr)mq.zaa Dacadrbtobiphenyt (Sr)
Semtvolrtile O.grnlc Colr|po!trds by GCII{,S
SW846 8081A 22-Mar-O7 27n,€t47 7031275 TGBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
3589
BRLBRLBRL8RLBRLBRL8RLBRLBRL
30fi
BRLBRLBRLBRLBRLBRTBRL|,, t10
pdlqdry 6.60
ldxgdry 6.60
lS/lqdry 6.60
ldkgdry 6.60gflrg fiy 33.0
WkS d.y 6.60pSlqdry 6.60pglg dry 6.60
trgkg dry 6.60
lSftg dry 6_60
IgftS d.y 6.60
l€ k0 dry 6.60
udl€ d.y 6.60pc/rg d.y 6.60
lgl(gdry 6.60
Udlgdry 6.60
US/kS dry 6_60
ldks dry 3:i.0pdko dry 6.60
IgkS dry 6.60pqtgdry 6.60
tu1 f r%38 f l%
lgftSdry r3.2pgts dry 13.2
lrgkg dry 13.2
lgkS dry 13.2pgkg d('r 13.2
rcn(S dry 13.2gSn(S dry 1X.2
Hfil(od,y 13:
rglSdry 13.2
fr-150 %381fi%
ugkg dry s20
ldkS dry s20
ldkS dry P0pSn(S dry 920
ldkSdry !n0
udkSdry s20
Idfgdry 920
rgks d'y 920
I
1
I
1
i
I
I
I
1'|
11
17
1
I't
1
1
1
1
SW846 8082 ?2-Mat47 24lller07 7031313 MP
SW846 8270C 23-l\,larO7 2g\rar{7 7031371 M.B
Semivolatile Omanlc Cornoounds by SWB,|6 8270CPrepared by metrlod SW8,t{i 35508a3<2.9 Acenaphthene20$96{ Ac€haphthyleoe62{}3 Aniline14n12.7 Andyaoefle1912-2+9 Atrazino103-33.3 Azob€flzen€/Dlph€nytdiazine92{75 B€nzidine56-lt3 Benzo (a) anthrEcene
TLb bbralort EpoA ls not vald withoU an outhorid siF ttnne on tL. col{lr pq. .. Re?brhble DEtection Limir BRL = B.tow R€portitrg Liruit PaAe tA of 124
Page 332
Sample IdentificarionM8F-1t 4-6's,A'595 t?-09
Client Pro.iect #101 -88
MatrixSoiL
Received
20-Mar-07
Collection Date/Timel9-Mar-07 00:00
CAS No, Anolr.e(s) FloE "RDL Diluttun Method Rel PrepaEd Ana+1/d Eatxh A,'absl
Semlvolrdle Orgrnic Compounds by GCMS
Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 35508
50'32{ Benzo (a) pyr€ne
20t99-2 Benzo (b) lluoranlhene191-2+2 Eenzo (g,h,i)perylene
20ru8-9 Benzo (k) fluoEnthene65{5{ Benzoic acidl0c5l{ Benzytalcohollrr-91-1 Bis(2-chtoroeflroxy)mehanelllaa{ Bis(2-diloroetlhyl)etrc.39638-32-s Bis(2-cjtjorojsopropyl)ether1i7i1-7 Bis(2-€hythexyt)phthalate101-5s-3 +Eromophenytphenylether85{s7 Butylbenzylphthalate66-74-A Carbazole59,5G7 4-Chloro-3-methytphenol106-47-8 4-Chloroaniline91-5$7 2-C+lloronaphthal€no95-574 2-Chlorophenol7m6-723 +Chtorophenylphenylether21841-9 Chry,sene5$7G3 Dib€nzo (a,h) arthracene132-64-S Dibenzoluran9+5r|1 1,2-Dicf{orobenzene541-73F1 1,3-Oichtorcbenzene10qG7 1,4-Oichlofobenzene9l-94'r 3,3"Dichlorob€nzidine12033-? 2,2[-DichlorophenolE4{G2 Diethytphthalate131.113 Dirnehytphthatate105€7-s z,4-Dimethytphenolu-7+2 Di-n-butytphthalate534-521 4,6-Dinitro-2-rnethylphenols1-2&5 2,4-Dinilrophenol121-1rL2 2,.{-Dinitrotoluene6oe2G2 2,6-Dinitrotoluenei17-M{ Di-n-octylphlhalatea)G,444 Fluoranthene86-73-7 Fluorenei1&74.1 H€xachlorobenzenea7€&.3 Hexacfilombut€diene7f..7-1 Hexachlorocyciopentiadiene67-72-1 H€xachloroethane1g}.3€-5 Indeno (1.2,3rd) pyrene{rG12-O 1-MethylnEphthalene78-5Sl lsopho.oneg1{7S 2-Mehy{nephthalene9S4&7 2-Methytphenol
10&39-4, 3,4-Methylphenol106-.{4-591-2G3 Naphthalene
&744 2-Nifoanitine99{&2 3-Nitroaniline
| ,2701,670
BRL1,840
BRLBRLBRLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRLSRL2,180BRLBRLARL8RLARLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRL3,1408RLBRL8RLBRLBRLBRLBRLBRLBRL
8RL8RL
BRLBRLBRL
Ig/kg dry S20pS/ko dry 92O
lgikS dry 92Opdks dry 920pdks dry 920pgks dry 920
lS.ftS dry 920
!SI(S dry 9mpg/kg dry 92O
udks dry 920
UgkS dry 920pdks dry 920
t S/kS dry 92O
!S/kg dry S20pdks dry 92OpdrS dry 920
tigkS dry S2Opsn(g dry 92OpgkS dry 920pd,|(s dry 920pdkS dry 920
ldkg dry 920
udks dry 920
US/kS dry 92O
ldkg dry 92Oyglkg dry S20
US/kS dry 920
t'dkg dry 920
ldkS dry 920
ldkS dry 920pSn(S dry 92O
ldks dry 920
Ig/rS dry 920
ldkS dry 920
udks dry 920
UdkS dry 920pdl€ dry 920pgftS dry S20
!g/kg dry S20
!S/kS dry 920
ldks dry 920
!S/kS dry 920
tig/kg dry 920
ldkS dry 920
lgkS dry 920
!S/kS dry 920
ldkS dry 920
ldkg dry 920
!g/&g dry 920
LiS/l€dry 920
SW84€ 0270C 23-Mar0l 25-Mel-07 7031371 M A
This labodorf Eport Ir ,tol valU pithotd an au.honzed signzturc on the cover page.
I ReDortable Det€ction Limit BRL = Below ReDortjns Limir Page 45 of 124
Page 333
Sample IdentificationMEF-41 1-6.sA595l7{g
Cliept Pmiecl #301-tt
MatrixSoil
Collection Dare/Timel9-Mar47 00:00
Receiv€d20-Mar-07
CAS No. Aaalrtz(s) Res,ttl Fl"C U,tj't *RDL Dilution l{dhod Retr Pep$ed Adalyzzd Both A"zlyst
Semlvolaille Otgadc Compotrtrds by GCMSSemivolatile Oroanic Comoounds bv SW846 8270CPropared by rn€thod SW846 35508l0o{1{ 4Nit|oaniline9€-9$3 Nitrobenzen€8a-7+s 2-Nitoph€noll0o{2-7 4-Nitbph€nol62.7s-9 N-NitEsodimetfiylamine62r-Ar-7 N-Mtusodi-rFpfopylamine€+'3GG N-Nitr6odiph€nylamine87{F5 Pentachlor@hsnde5{1-8 Phenanthr€n€10+9t2 Phenol129-00{ Pyrene1101+1 Pyridinel2G€2-1 1,?,+Trichlorobenzene95-95-4 z,4,sTdchtorcphenol0a4&2 2,4,GTridtlorophend
Surogate re.nwies:32140-8 2+luotobiphenyl367-tz-4 2-Fluorophenol4165404 Niiobenzet@-at,116sa2-2 Phonol45171e.514 lerpheny'4l4tte-79-6 2,1,&Tlibtottbphenol
Iot t M€trb by EPA 5000/7000 S€ri6 Mettods
BRLBRLBRLBRLBRLBRLBRL
8Rf8RL3 ,110BRLBRLBRLBRI-
108
88102s21091 1 1
0.307
BRL
9.64
40.4
0.516
9.81
15?
BRL
pgl(g dry 3680
Ug/tgdry 920
UdtS d.y C2Opgftgdry 3640
!4kgdry 920
ItgxSdry 920
ldkg dry 920
lSftS dry 920
FdkS d.y 920
Fdks dry 920
IS/kgd.y 920
lSftS dry 920
lgrsdry 920
[grsdry 920
lgr'kg dry 920
30-130 %1t110%3L130 %15-lto%311130 %t t l t 0%
mg,fkS dry 0.0340
mg/ko dry 1.10
nBikg dly 1-65
mgikg dry 0.549
.r€/kg dry 0.275
mg/kg dry 0.549
m.drg dry 0-824
rrldkS dry 1.65
msn 0.0100
mSn 0.0't 50
mg4 0.m50
mgil 0.0025
lrlsr 0.0050
mgLI 0.m(X0
fiSn 0-0075
msil 0.0150
%
743947{ Mefcury
Tot.l Mearb by EPA 200 S€ries Meahods
744G22{ Sitver
?.?10'!&2 A.senic
74,10-393 garium
74t|1l3a9 Cadmium
71,{0-47-3 Chro,rnium
7(19.92n Lead
282!9.2 seleoium
I SW846 7,f71A m-Mar47 27']l|,,et47 7031322 vP
1 EPA m0-7 ?s.Maro? 27-|nar47 7ml32l HB
1 "
1 '
1 '
t '
I '
t '
1 SW8.{6 f3'f2 2-Itar47 22,,g'47 7031344 BO
1 SW8451312/6O106 ZA-llaFo7 244.147 70ill4o8 LR
1 '
1 '
I '
t '
1 SW8461312'470A ' 2ff!,lar47 7Gl1d0O YP't SWE461312rd0108 ' 24-lrr-07 7031408 LR
1 SM25{O G Mod. 21.1nd47 24nnat47 7O31{X} QP
SPLP M€tds by EPA 13 12 & 6001V7000 Serles Methdr
SPLPExtrEdtun Comdeted714444 sjlvet BRL7't4o.3a.2 Arsenic BRL
71,(13$3 Barium 0.00907440a3.9 C€dmium gRL
744047-3 Chromium BRLzF9{7{ irerdJtY BRL7439€2-1 Lead O.D2522E2.1$2 Seienium BRI_
GEne|'rl ChembF Prrr|||€ters
% Solids 88.2
Thlj labordtarf rcpod it,rat vdupithord att astlrotitl signott r. on E @ver lq..+ RepodablE Det€crion Limit BRL = Below Relorting Limit Page 46 of 124
Page 334
Sample ldentificationMilF42 2'4'sA59803-r2
CLient Proiect #301-88
MatrixSoil
Received2'7-Mar01
Collectiorl Date/Time26-Mar-07 00:00
C"4S No. Anolr'te(s) Resa Flac Unia rRDL Dila.ioa Method netr Prcpared Andtzed Batch Analrsl
Volalile oroanic ComoounG
Prepared by method SW846 5030 Soit(high tevet)
7G1+l 1,12-TfthtorolnjtuoroethanelF@on BRL0744-1 Aceton€ BRL107-l$1 Acrylonihite 8RL71+le B€nzen€ 8RL1G06r BrorDb$zene SRL7+97.5 BEftEchtoornelhane 8RLEnl Bomodciloomethane BRLt 2j.2 BrDrotot|n BRt7'l{3-9 godbm€thane BRL78 93.3 2€uranone (MEK) 8RL10{'51{ n-Butylbenzene BRL1354S+ sec.Buvlb€flzene BRLs1rc6 t€i,Buvbenzene BnL7$1S Cadon disultide BRL5F235 Cadon tdlad orid€ BFL1(lg9o7 Chlonrb€fzene BFL75{03 Chtooethane BFLF7-6e3 Chlorotonn BFL744t-3 Chlordnehane SFL!6-498 2{hlorotoluene BFLlllc/B.1 4thlorotduene BFL96n2€ 1,2-Dbomc3dioropopane BFL124-181 Dibromod oonelhane BRL106s-1 12-DbrDmoefEne (ED8) BffL7+95-3 DibrorbrnefEne BFL96sct 1,2-Dchtorob€n:ene BRL54r-7l.r 1,3-Dicruoobenzen€ BFL1n6-46.7 t,4-Dicttombenzem BFL7$71-8 Ddiorodmuorcmslhane (Freon12) BFL7s3,{-3 1,1-oicltomethan€ BFL107{6.2 1,2-Dcldo.oettEne BFL?5.354 1,1-oicltoroefEne BFL156.50.2 cb-1,2-Drdtlorcelhene BBLls6€G5 bafls-1,2-Dd orodhefe BRL7l.Et{ 1,2-Dkhloo0opane BRLi{z.z&s 1,3-Dddoropopane BFL5ga-d'.7 z,2-Dichloropropane BFL5615lr{ l,1-Oichloroprcpene BRL1006r'016 cis-1,3-0idlloroprlp€ne BRL1006r-025 faE-1,3-0id{oropropcns BFt100-.r-4 Efiytb€nz€ne 123g/{63 HeEdrloobutadlene BFL591-78n 2-H€nanolle {MBK) BnLs6.828 tsopmpylberuene BRLstt{ 4.lsoprop}{toluene BFL183,r.04-,1 lvlsttyl ted-buty1 eher BFL
28-l,rarfl 28-ltl€t4t 1131767 BD
02'N147 02-Apr-07 ru4m17 mal
VoLtile Orgrnic Compounds
VoC Exkaclion
1osrGr +Methy,2renlanGre(MIBK)75{F2 Mehylsne c} orides! 20.3 Naphhdm€
ldtg dy 632
!94<9dry 1260
WkS dry 632
!S&dy 632
lrdko dy 632
ug4(g d] 632
!gA0 dry 63.2
lSrrg dry 602
lElS dry 126
|.lg/rg dry 6&
|lg/rS dry 632
!g/kg dry 53.2
ldlS dry 63.2
lqkS dty 316
|lg,tS dry 632
us,lq dry 63.2
psrts dry 126
tdks dry 53.2
us4€ dry t26
|lg/lq dry 632
ldlq dry 632
pS4qdy 126
ldkS dry 632
tdrq dy f,3.2
tidks diy 63.2
lig4qdy 632
lgre dry 63.2
pdksdry 632
U94q dry 126
tdks dry 632
lql€dy 632
lCl€dy 632
pg4qdy 6il2
E/r€ dy 632
wkg dy 632
fgnq dy 632
lglq dry 632
fdl€*y 632
Mq dy 6il2
pC4q dy 632
pg,lq dy 632
!S4q d.y 632
tdEdy 632
ldrq dry 632
B4qdry 632
ldlq dry 63-2
|.€/lq dy 632
fdE dry 632
pglq dy 632
Field exirad€d voc
sw 846 8260€505050
5050
5050
505050
50
505050505050
50505050
505050
50
50s0
50
BRLSFL155
Thi! laboratory Epora is not salid withoat an oathorial signsttne on rte cover page .
. Reportable Detection Limit BRL = B€low R€porting t.imir Page 58 of 154
Page 336
Sample IdentificationM8F42 2'-4'sA5980l-12
ClientProicct #101 -88
Collection Date/Time26-Mar-07 00:00
MatrixSoil
Received21-MaF07
C4S No, An rte(s) ResuL Fl"g U^i6 1RDL Dilution Method Retr Prepored Awlyzed Bttch Antltsl
Vol.tile Orgrnic Compound3
Volalile oroanic Cor'lolnBPrepared by method SW846 5030 Soil (high tevet)103191 n.Prcpyhehzene1dr,t2-5 Styrene
6SG206 1 ,1 ,1 .2-Telbchloaoettrane7$3,1.5 1,1,2,2-Tetiachloroehane
127n44 Tetraahlooeihene
10&0&3 Toluene
87.61.6 1,2,&Trichlorobenzene
1m-82-r 1,2,4-TrichloDbel1zene7r.!56 1,I,1-Trichlooethane7$0G5 1,1,2-Trichtomehane7S0l-6 Tri{t ooethene7tt9-4 TrijhtorottuoometEne (F€on j 1 )sG1S4 l23-Tichloopropane
95€-6 1,2,{-Tirn€frytbenzene108-67.S 1,3,5-Trimehytben2ene75.01-4 Vinyld oride1@,2{17 m,Pxylene95,176 exyl€nelossss Tetrahydroluan8G2s7 Ethyl ether90445{ Ten{m9 mehy' eher6fl/-Vr 3 Ehy,l lertt0tty1 elherl08.al3 Di-isopropylelher
75.654 Ted€ubnot/ buyt atcohol12'sr 1 l+0ioxane
46n-''J4 4-Btanonlo@hnzene
&37-266 Toluene4S
tTMal4 1,2-Dichbtoethane44
18fl.53-t Abrornonu,rcrEllwe
Oxtrrctehle Petroleum Hydrocrrbons
Edractable Tolal Pelroleum Mrocarbons
Prepa.ed by method SW846 35504
mo$l.g Gasoline
68{7F30-2 Fud Oilt2
a!ftt-31-3 FuolOil t4
6€554|{0-,r Fud 0( t6ti)9000{E() Moloroil
$0100000 Aviation Flel
Unidenulied
ohef oil
Total Pelloteum Hydrocadons
C9{36 Aliphatic Mroalrtons
jB1,6ip2 l4hloe&ladec4rg
Senrjvolrdle Orgroir Compolnds by CC
Or@nod orine P€slicies SW846 PO81A
Prepar€d by merhod SW846 3545A
tl9{}2 Atdrin
8RLBRL
8RL8RLBRL154BRL
BRI-8RL8RL8AL
BRL8RL
8RLBflL26379.7BRLBRLBRL8RL8RL8RL8RL
98t0t99t09
BRLBRI-BRL8RLBRL8RLn6Calorhted asTt6n6
2U
lykS ey $2
ldkS dy 632
tdlq dry 53.2
ldkg dry 53.2
tiS^S dry 632
!g(S fy 632
l1g^S dry 63 2
!S/rS dry &32
lscs dy 632
WkS dy 6:]2
!s,rs dy 632
!S& diy 63.2
F9CS dry 63.2
l€/rs dy 63.2
llg/rs ry ff2
!g/tg dry 632
!s4q dry 126
t€frS dry 612
!s/ks dry 632
|rg/kS dry 632
I'S4s dry 632
tS&g dfy 632
ldrs dy 63.2
llgAs dry 632
ldrS dry 1260
70-130 %
TEtg%
7Vt@o,L
70130%
iWrS dryrhg4g drynsfts drymg/rg drymses drymElS drymg,tS dryfilglq dryxrgltg drymglq &y
4+144%
pdlq drv
sw 816 82608
+CIEIPH
50
50
5050505050
5050
5050
50
s0
50505050l0
02.Apr{7 O2-Apt-07 J040017 n^l
29Maf-07 30-Mar-07 7031773709
709
7m7m7og
709
709
709
7Cr9
709
BFL sw&{5 80814 28-{,lar{7 02.Apr{7 7031739
Thk bbomury repoa is not wlid tlithoct an aurtoisd siF',ature on tha coyer page.
* Reportable Detection Limir BRL = Below Reporring Limit PaBe 59 of 154
Page 337
Sample ldentificationMtF42 2'-4,sA59803-12
Client Proiect #30t-88
Collection Date/Time26-Mar47 00100
Mat.ixSoil
Received27-Mat41
CAS No- Analyte(s) Resuk Fhg A n s *RDL Diluian Method ReJ, Peparcd Atblwd Ealih Analyst
Semivolatile Org.nic Compoo||ds by CC
orqanod{odne P€slicjdes SW846 q}€1A
Prepared by method SW846 35454
3|9-0,r-6 a_Bl-tc
i1986-? b€lr
3198&S d.gHC
s8se g-BflC (tjrdane)
st-1+s Chlordano
n544 41.DDD (p,p,)
z-55s 4,{-D0G (p,p')
ss2$3 4,4-DDT lpr)6Gt-i Oslfin
Etltossualr I
$e19H E rdodjlfrn ll161.07-8 EdGjhnSuttale72.2GB Eddn7€l'g-.1 El|llin Alt€fiyde7614-8 Heptad{or1213.a l,l€ho4d{or102r'r3 l-teptad{orEpoxid€m01.352 Tox4lE06
510971.9 a.Chlordare
$8S34? g{hbdfle
5349+705 Endrin K€0one
1'3fd4+2 4,+Dgadatundiptvt4 (St)
d6te+i Decd otilirlBv (e)
Polvd*riEted Eiohenvis bv SW846 8082
Pfspared by method SW846 3545A
126?+112 PC8101611rO+2&2 PC81221fit,{1-t65 PC81262
5346921,9 rcB 12421262.2$6 PCB [email protected] PCg 1254nc6.02.s Fc8 t260tnz+2cs Pc8l26211r@r4-4 PCB 1268
lwta-z #4v4M@tiliptBnl(SlNt'21-t Mlbnbiptvrlt(Si
S€mho|'dlc Orgrtric Compounds by GCMS
Semivotade Oroanlc Cofipoonds by SW846 eB70C
Pr€pared by method SW846 35508
s+34 9 A.a0aphh6no
2n&960 Aae|taphtrylsr€€a 533 Anihe12G12.7 Andreno
t9r2-2't4 Arra&€
1@393 AzobdEeieDiphenyldarine
s2fi-5 Bsuirine
5&55.3 E€nlo(al?'ltfeie
BfiLBFL8Rr-BRT8RX-BRI.BRLBRLBNLBRLBBLBRLERLBfrLBFLBRL8RL8Ft-8RLBRLBFL
IN
BFLBFLBRLBRLBFI.BRLBFLBFLBNL
7595
69.1
69.1
6S.1
6S.1
69.1
6 9 t
€9.1
69.1
63.1
wlgdryudrc dv!cI{ dv
|lg}S dry
ldks dv
ab dv
|dredYrdrg dvpdkg dv
lgrs dy
ldrg (y
NTq dYpsnq dY
$/tq dy
|Js4(s dv
!S/ko dry
ldt0 drypgrg dv
P9& d'y
usrq cvIEt{ 4}
a>lfr%f i 150%
!s/rq d]
rj94q 4'!g/kg dry
|lsfrs dv
|dh dy
rob d'Y
|Jgrsdvlyts trY
!s4q fft
*tq%gyfi%
swE4{J 8081A34.5 1
34.5 1
34.5 |
3 l r
t n l
34.5 l
34.5 1
34.5 r
34.5 |
341 |
345 |
34.5 l
34.5 r
31.5 1
34.5 |
345 I
34.5 1
t73 1
34.5 I
3,{.5 |
34.5 |
sw816 8082 2&tl'J47 30-ttar'07 7061738 s
zS-l'ls{7 FApr{T ru31?4 M.BBBL
BFL
BFL
BFL
BFL
8RL
8RL
BNL
|dh dv
$llqdIpgrq dY
lqh dv
ldis try
tdtqt'lugnq dy
|ldlqdv
swB45 8r/0C8€0 t
880 1
880 1
880 |
EEO 1
EEO 1
&t0 I
8 & 1
This labotutory rcpo b ^otwlid wAhorn an auttotized siF tzt,lre ott lha corer page.
. REport"ble D€tcction Limit BRL = Below Reportiog Limit Pag€ 60 of 154
Page 338
Samole [dentificationM8F-t2 2'-4'sA.5980l-12
Clielt Proiect #301 -88
Collection Date/Time26-Mar-07 00:00
MatrixSoil
Rcceived27-Mar01
CAS No. Anab,e(s) FloS *RDL Dilutiot, Llethod Rel. Prcpltrul ,lnalyzed Botch Atutttst
Scmivolatile Organjc Compounds by GCMS
Semivohtile Oroa' c Cohpounds by SW846 82i0C
Prepared by melhod SW846 35508
5032{ Benzo {a)pyrcnez0+r13.2 &nzolb)tuoranhene11'1-24.2 Belzo {g,h,i) perylenem1489 Be$zo {t) fluoranifiefle8S05{ 8€nzoic acid1llc51{ Bonzyt atcohol111-91-1 8is(2doroelhory|mehanet11{e 8is(2,€hlooethyl)ether3S63!-324 8isi2-chtoroisoprap!4)elhcrt174t-7 8is(2-ethylheryt)phttEtate10r6s3 4-Eomoph€ny' pheny,i edrerE 6&7 &Iytbenzyl phhatate
F74-! Cadazole5960-7 +Chtoro-3-mehytphenot106-{71 4.chtoroanitine9.58.7 zchloroiaphlhaleoe96.57-6 2{hlorophend700572 3 4-Chtomphenyt phenyi eher2r8{i4 Ch.Fene597G3 Dibenzo(a,h)anthrac$e132+4.9 oibenzofirran!,5sGi t,Z-DicfitorobenlenesilrXll j,3-Dichlorob€nz€ne
lo64tt7 1,4-Ddorobenzene913.4.1 3,3-oicltoobenzidine120++2 2,4-Ddorophenolu{62 Di€ttryl phlhalale13n!1-3 DihBftylphlhalate105-€79 2,4-Ome',h!4phenols-7t-2 Di n,butyl phthatale53,r-s2-1 46_Dinjtro-2-rnethylphenol51-28-5 2,4,Dinirrcphenol121.1+2 z,4-DinitolotuenesF2o2 2,6,Dinitrotoluensr17-&r4 Di-0_octytphtfialat€a,6r4{ F|uoranlfcne
€&737 Fluorenet1&7+r Herad oob€flzeneAr-6&3 Hexacljorobuladi€ne17471 HeracHobcyclop€nladieno
67-72-1 hetaClioro€fEnelt+39-5 InderF(j,2,$cd)pyrene
90.12{ l{,lethy'naphlhat€n€7&59-l ls4phorone01't_6 zlvlelhylnaphthaten€s6r8-7 2{dnylphenol
t@39-r, g,4-M€hlphenol106-{+591-a)n NaphthaleneW74-1 2-Nihoaniline!1941"2 $NitrDanitm
BRL
8RL
8RL
8nL
8RL
8RL
8fr1
BRL
BBL
BBL
8RL
ORL
BRL
BRI
8RL
BHL
BHL
BFL
SFL
SFL
BRL
BRL
BRL
8RL
8RL
BRL
8RL
BRL
BRL
BRL
8RL
8RL
8RL
ERL
BRL
BFL
BFL
BFL
BRL
BFL
BFL
BRL
BFL
BRL
BFL
BHL
BBL
BRL
BNL
BRL
!S/rS dry
l]drS dry
|/dlq fiv
lglg drypdkg dry
uC/rS dy
|rs4(sdyUS4q dry
!S/kS dry
llgl(s drv
lsts diy
LgfrS dry
lgrq dry
lqkg dry
!!t& drvpdkS drypgro d]
|lgrs dvpglq dv
UgtS drypdks dry
rc,tS dry
!91s drypgKq ory
ldks drypg4(S dry
udts dry
udlq drypdq dlypotS drypskg dypg/ks dry
l,94(o dv
|Js4(s dy
l,gksrv!C4e,tyISAS dry
!C4(S dry
!04(S dry
!q4(g dry
!4rs dry
tqwfit!g4q dv
lqrs fiv
$/fS dly
|ls/rsdlyArc ev
rdl€ dy
ldks d.y
A& dv
880 1
880 1
&t0 l
88{ I
880 1
880 r
880 I
880 1
8€0 I
880 |
8€0 1
880 1
880 1
8 m 1
880 1
EEO 1
660 1
E60 1
E€O I
880 |
880 |
880 1
880 1
880 1
880 1
880 1
8EO I
88{r 1
880 1
880 1
880 1
880 |
880 I
880 1
880 1
8E0 1
8Al 1
880 1
880 1
880 I
E80 1
880 1
E€O 1
8€0 1
880 1
EEO 1
880 r
680 I
880 1
880 1
sw845 8270C X+lar-l1 03-&f{7 7031774 M-8
Ihk labontory ?epo Lt not valil withaa an outhorir?A signatarc or the covr pzge.
+ Reponable Detection Limit BRI- = Below Reponing Limit Page 6l of 154
Page 339
Sample ldentificatiotrM8F-42 2'-l'sA59tol-r2
ClientProiect #301-88
MatrixSoil
Collection Date,/Tirne26Mar-o? 00:00
Reoeived21-Mar-07
CAS No, Anrlyte(s) Rdr&t Flag Uni6 *RDL DUBtian Method nej PEpared Analyen Baftl, Analfsa
S€mivolrtile Orgrnic Compounds by CCMS
&nitolaltl€ oroaric Compoonds by SW8,t6 8270C
Prepared by mehod SW846 35508
100{15 {-{ifoenilire90 9r3 lfircbeu€n€0&7s-5 2-flitophenol16{2-7 +Nitrfhsndu-7$9 J\ll{ltlsoditrEhy{anne@lt+7 ltt$lrcsodin{rEpyantne8F30-6 $Nitos(dohengdnirE87{66 Pentacilooph€nd
8601{ Ph€nolhcn€1{,8-95.2 PtEnol129.00{l ry€rle110's5r PFdne1!182-1 12,+Tritoobenzenss!E-4 2,4,$Tdfloophend881162 2,4,STli*boph€nol
plat 2-Fl/lt.,iphenfl
3f,z-121 z-Fhsqlwd
4165504 ^I'tfuEelte4s
1t65@-2 Ffa.nt4s
171&514 l6tpl}3,ntl44
11e794 Zl,eftbwnophend
SwBl6 8270c ?s u{' 0&lpr-07 m81774 M.8
Sw8167471A @.AF€7 GIApr{7 7031810 YP
EPA 2m.7 024pr.07 02-Aprfl 7ulmg HB
S|V84E 1312 2&Uar.07 Ansr]Ir 71131763 B0
SW846 1312m108 30.ilar{7 m.Ag{7 7ml&5 t-H
BFLBRLBRT8RLBRLSBLBALBFLBRLBRT8RL8RLBFI.
BFLBFt
&7363n5t)
lglS dr 3520
!g,iS dy 880
ryb a 880lS,l€dy 3520
twet 880
|,grs dy 880
IEr96y 880
ljg/}S dry 8€0
lS,rc &y 880
tlg/lg dy 880
EYbdry 880
lcngdl 800
Nlqdy 880pgrq dy 880
!g/rg fiy 880
fr.l30%t5-u031}r30%trl t0%&rg)%1rt10%
'tvts dry 0.ffi2
mYrS dry 1.10
mdtgdl l.5s
tidks dry 0 551
mq^g dry 0276
r'01q dry 0-551
ndrS dry 0.&7
mo4qdry 1.65
rng.l 0.01m
nrdl 00150
mg4 0.lxl50
mg]| 0.00e5
'rwr 0.0125
mgl ojflXo
rr$,l 0.0075
rngl O01s0
sw84613r2?170A
sw84li 131260t0€
Tobl Met b by EPA 6mO/7000 Serier M.rhodj
?43!l'97.6 ilerWry
Tot l M€td! by EfA 200 S€rie3 Merhods
+e4 sifuBr
t!l(rg2 ABeric
7'!{G3+3 Bdium
74/(}499 CadDium
r4tfr4J.3 Cltunium
7$F92n bed
nV4U2 S€l€nium
SPLP Metlls by EPA lfl2 & 6000t000 Serter M€thods
SP{-P Ertadlon Compl€N€d
711r'J-?44 Slv€r oFL
tr10-l&2 A6enic BRL
z.rtll,3g-: BaJilh 0.tB&
7,!{)4}9 Cadniwn BRL
74li}.|7-3 Otomilm 8RL
7'139976 lil€Gry 8AL
7'13$92r Lo€d BFL
7t&4-2 Sel€nfum BRL
G€nersl Cbcmtuky P.trmeter'
%Soh(h 88.9
' {P.l{r{7 70S1806 YP
' 02.4F{7 ru3rgl5 tR
BNL
795
l m
0 58.1
11.7
366
1
I
1
I
l
I
I
1
1
I
1
I
1
1
I
1.6€
Sfl2540GMod. g).llar{r7 3&rNar{7 7[01S/9 Ytt
Thit labo.slorf report Lr ,.ot wlU withord an authotlzrl ignsturc on thz cove, page .
' Reportable D€t€.rion Limit BRL = Below Reporring Lioil Page 52 of | 54
Page 340
Sample IdertificationMtF-43 2'-4,
sA59803-13
Client Project #30t -88
CoLlection lJate/Time26-Mar47 00.00
MatrixSoil
Received
21-Mat07
CAS No. Analy.e(s) Resalt FtoC Iinils *RDL Dilutbn Method ReI PrcpoAd Ana4zed Bdch Anabst
Volrtil€ Organic Compounds
VoC Frlraclion
Volalile orcanb Comoolnds
F 6ld exlBd€d
Prepared by method SW846 5030 Soil (high tevet)
7t1+1 1,1 2-Tichlorotnlluoroehan€ (Frcon BFL67-6rr Acetone 8RL1mr31 A.rylmirr e 8RLn 41-2 Benrene 8RL108-86.1 Brcdnobenzene BRL7497.5 Bdnmhloaomelhane 8RL7'214 B{Emodichloomelhane BRL7t 2 Bomolortn BRL7l-83.9 Bromomelhane BRL7843.3 z-BL{anone (MEK) BRL1o,r5l{ n-Bulyibal2ene BFL115-9S4 sec-Butyhenzene SFLsl{6$ Ed-Bulylben?ene BRL75.rfi Cabon dsufiide BRL5S29s Cabon tet€chtorid€ aRLlll&90'7 Chlorobenzeno 8RL
zE-Marfl z&Mar-o7 7031767 80
oz-Aprfl 02 Ap/{7 7040017 mar
BRL
BRL
BRL
BRL
8RL
8RL
8RL
8RL
BRL
BRL
BHL
BFL
BFL
BRL
BFL
SFL
EFL
BFL
BHL
BFL
BFL
BRL
BRL
BRL
BRL
BFL
BHL
BRL
8BL
BBL
BBL
BRL
8RL
61.5
r630
8J.5
81.5
81.5
81.5
81.5
8 1 5
103
Er5
E15
81.5
81.5
40€
81.5
81.5
163
8 1 5
163
8 1 5
81.5
8 t . 5
€1.5
8 1 5
81.5
E1.5
€1.5
r63
6r.5
8 1 1
81.5
81.5
81.5
81.5
81_5
0t.5
815
8 1 5
815
8t i
815
815
815
8 1 5
815
815
8t.5
50
50
5l)
50
5l
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
5l)
5{)
50
50
5l)
5{)
50
50
50
50
50
50
50
50
|Jdrs dvpgfrs dypgxs dvpgrq orv
lgrs dry
ldrg dry
lglS dryps.4s dry
lStS dry
Udlq dry
U$4rS drypStS dry
!g4q dry
uofts dv
U0,1q dry
ldlq dvps/xs fiy
lgh dry
!S4q dry
lVrS dry
!S.4(S dry
uS.4S dry
|Js4(sdr/!S4(S dry
!S,4S drypdkS dry
lgtS drypS/xS d,ypsng dry
$4q dry
w/kS dry
|gk! drv
tErt drypdks dry
ucfrs dry
udks drypS4q dry
UofrS dry
udks dy
lots dy
lsnq dvpdlq dyps,4q dy
uc4(s dy
!dr(s d4'ps4(s dl'
tiSfio dyps49 diy
lls4s flv
voc
sw 846 82608
75{G3 Chlorcethaner-6e3 Chloojofln71nL3 Chloaomelhane95.{9S 2€hlorololuene16{l-4 4{hlootoluene*12{ 1.2-Dbmlna3-dloropropane124.48r Dbrornochloomehane10ssg4 1,2-Obromoelhane(ED8i7,1€+3 Dibromomethane9+5G1 l.2-oichtorobenlene
5{r.?}1 l,}oichloroben2€ne106-467 1,4-oichlorcbenzeno
75.710 Crid orodinuoromethang (Fleofl t2)75.343 11-Dichtoroethane
1O-0e2 l,2-Diclooettlane7+114 l,l-Dichloro€lime156-5!,? os-i2-DtdtloroellEnerso5 l|ans-Il-Didoro€lt^€ne1g-s7s l,2ochtoropropane142.ws l,Soichlooprooane
504207 z,z{ichloopropane56+58$ I,Ioiohloopmpene1006r{r.5 cis-t,3-Di.hloropropene10061{2-6 l€ns.1,3-gdoopropene
1m-4r-4 Ehy'benzer€
8?683 H€xe€ilorobutadienesr1-7e.6 2+t€ranone(MBKIs-82-8 lsopropyb€nzenes-rrJ 4-hopmpyltotuerc1d34{4.4 Methylten-burylethe{10&101 4-n4ethy,t,2-penlanone(MIBK)75492 u€hyieaechtoridesr?o3 ftaphhaten€
Thb hborztory rcpod is not tqIU r,ilhod an sqlhoriz?y' signdurc on lhe coler page.
'Reportable Detection Limit BRL = Below Reporing Limit Page 6l of 154
Page 341
Sample ldentificatiotrM8F-43 2,-l'sA59803-13
Client Proieot #30t-88
MatrixSoil
Rec€ived2"1-M^t-07
Collertion Date/TimezGMaFO'l OO:OO
CAS No. Azaly.e(s) Resljll Fhg UaUs 'RDL Dilution Method Retr Prepared Attalfzed Batch Anausl
Vohlile Orgallc CompoudsVo{a$e Organic Compoundsftepared by method SW846 5030 Soit (high t€vel)r00.6s1 n-Prcfl&enzene B8L10c1t2-s Styrera BFL60020{ l,t,t2.fetlachtoroslhane Bn[79\345 1,13,2-T€trachbrodnan€ BRI-'t21 184 Tetrsd o|ehen€ 8FL108.8+3 Tduene 8Fta/{l-6 l2,}Trirlrlonbenzene 8RLr2o{2 r 1,2,+Triilorat€ru€ne BfiL71.55.6 1,1,i-Triciloroehal1g BRL?94G5 1,1,2-Tlit ooetEns B8L790.6 Trid ofoehene B8L75'6k TddllorDlfuorofEfiane (Fl€on 11) 8FLsro_'l l,2,gTridloropropdle BRL9+6+6 1,2,4-Tirnerybenzene BR-1lIf67.ll l3s.TnrEfrtl/benzene BH_7+014 Vinytdltor*l€ BRL133+2G7 m,pxyt€n€ 8FL9sr74 oxylene 8ff1to9 9s9 Tetrahldmlu€n BFLtu2vr EUMet|el BFL994-05e Tenrnryl metiyl eh€r BRL&t 92,i Etryt t€dtlty eher BRL10&203 Di-isoprqyt etie. 8Rt-75-€s.0 T€n-Butand / hJM aLohol12$91-1 l+Doxen€
4&@Er +Brcnofrtoobenzene2@7-26-5 Tduerc.d€17M$074 l,zaidtdodlane4t186e53-7 DlbatpfllDdnetlane
Extrcclrblc Pdroleum Hydro€{rbons
E(lrachbls Total Polrolsrm l-fudl€aftoisPrepared by mEthod SW8,f6 35508em6.6r'9 &sdine6847+3C2 FFtod 1268r7$31n FlF| oit #tr68s63{0.1 Fuetot t6m€00mo MobrolJ0010{1000 Aiaton Fuel
{hld€rnifi€dOtE OlTolal Potrcleum HydocatcnsC€436 Aiipialtc Hydroca.bons
Senrivolrtile OrBrnic Compounds by cCorcanod{odn€ Pestdi€s SWB46 0081APrepared by method SW846 35454O94G2 Ahdn
B&8RL
971021@1 t 1
8Fr-BFL
BFL
BRL
BffL
BFL
BFL
BRL
BRL
8RL
lvls trvloaq ryldh ey|dh evE/l€ fiV
|4ls dry
tlq dry
Ug,lq dV
ldks dv
$rq trv
uqks ey
arc rvldl€ dvpg|q Ar9l€ dv
lrylg dy
|Jgl{ d}
lgrq dy
!g4s ry
!S/rS dry
$& dv
ljdlq dvpdqA
ll9t9dvt4r€ 4y
7&1fr%7ttil%7Gt30 %701$%
mgaq drymgrS fymdks dyrrM{ drynul€ dry|rBr€ fiymdb d'yngnq d'yr'9,1q dryorS,lq dy
4+140
sw 846 826{E
+Cr EIPIJ
8r.5
81.5
61.5
8 1 5
8 1 5
Et5
Br5
81-5
8r5
€ 1 5
EI.5
8 1 1
811
8 t 5
81.5
r63
8 1 5
8 1 5
81.5
81.5
815
8r5
8r5
t6B0
7 1
7.1
7-1
7_1
7_1
7.1
7.1
5i)5050
50505050505{t5n505050505t)50505050505050505050
m"Aprfi 02d[f47 704m17 mar
29-il€r{7 3l}t{al1)7 m17,ts 0S
BFL |r'cretv sw4| alSta z&ilar{7 02.tur.07 ?t31me
Thtrt labotuory relNt l is Eot vrIU pt&to.d oE cttthadeil s,gnatarc on the corer page .
. R@rtable Detection Limit BRL = Below R€poding Limit Page 64 of 154
Page 342
Sample ldenlificationMtt-4r 2'-4'sA59803- l3
Client Proiecr #301 -88
ColLectio1l Date/Time26-Mar07 00.00
MatrixSail
Received
27-I./:a(07
CAS No. AnaIyuG) Resall Floq anib *RDL Dilktbn Method ReJ Prcprcd Analyed Batch Analyt
Semivolstile Orgrhic Compounds by CC
Oroanociiorine Pes[cides SW8{6 8081 A
Prepared by mettrod SW846 3545A
319-8{-6 a-BFIC3r+85.7 b.8HC
3rs€68 d-8ftc
58-8+e g-8tc (Undane)
7-1rq Chbrdanen543 4,4!0OD (p,p)/25s s 4,4,.00E (p,p')
5q293 4,4'O0T (p,p')qlt 1 oiddnn
s5F96-€ Endac{llan I332i+8tg Endosullan lli031{7+ End6ullanSuttaten-&4 Endin7r12t,93-4 EnddnMehyde76_.4_0 Hep|achto(72-r9s irethorycitor102+57.3 Hepiad or Epondesnor.352 Toxaphene5103719 a-Chlordan€ss663rr-7 gthlodane
534S+7C5 €nddn Xeton€
10f8eu.2 44.08-(Xhllwtobiphenyl(Srl,,61-2+3 Decaclfurcbiphenyl(si
Polvd odnatod Bbh€{vis bv SWP,46 e,082
Prepared by method SW846 3545A
12t74||-2 PCB 1018
1110420 2 PC812211fl.1-r6.5 PC812325316e21-e PCB 124112672.4.6 PC812481r097{s1 PCB 1254110${25 PCB 12603l@l-ri$s Pcg 1262111$14rt PCE 1268
1ts'641.2 4,4-DB-Octafluot&id6nyt(Sl
MtZn oecacflonitliphertyt(St)
Sehivolatil€ Orgaric Compounds by CCMS
Sed lalaltle O.oa|lic Conpol,nds by 5141846 8270C
Prepared by method SW846 35508
m-324 Acsnaphh€nsa{}*8 Ac€naphhyl€n€@-53.3 Anrfin€120-12-1 Anthlacen€1912-2+9 Altazhs1&s.7 A.4ben.f]rctapherytdezirc@.!7-s &nzidinese5+3 8€fzo (a)anhracgn€
BBL
8BL
BRL
BRT
BRL
BRL
BRL
BRL
BRL
SRL
BRL
BAL
BRL
BFL
BFL
8FL
BFL
BFL
BRL
BRL
BRL
u97
8RLBRL8RL8RL8RLBR]-BRL
BRLBRI.
70g)
39.9
399
3 9 9
39.9
199
39.9
3S.9
33.9
39.9
39.9
39.9
399
39.S
39.9
39.9
399
39.9
r99
39.9
3 9 9
399
!S.4(S dry
lsts dy
pSIq dry
$4€ dry
!g4q dry
ldks dry
tdkS dry
tidks dry
Irdlq dy
lgks try
!s4(s dry
!g4q dry
lig/tg dry
lSrtg dry
!9lS dry
lsilS dry
!s4(s dry
lVkS dI]/
ldks dry
trs,ks dry
t44(s d.y
3Et5A %
+t5a%
!S4q dry
ldlq dry
!s/kg dry
lEtq dry
lErq dry
uslq dry
ug4q dry
!S4q dry
tiC4q dty
&150 %
38150 r,
SWE46EOSIA
sw846 80€2
sw846 8270C
l
l
l
l
I
I
I
l
I
i
I
I
I
1
l
I
l
1
1
2t-i,lar{7 @-Apr'07 7031739 TG
28-Mar'07 30.Mar'07 7031738 SM
29.1,1ar.07 03.AVl7 1$1n4 M.B
79.7
79.7
79.1
79.7
79.7
79.7
19.1
19.7
19.7
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
pg/ts dry
Ps4q dry
us4q dry
Psfrs drypdks dry
WkgdPluS4q dty
Ug'k! dry
886
€86
8€5
886
886
d€6
886
886
Thit labontory rcpod is not valid tpitkoul an aartorized signzta.e on the coeu page .
+ Reportable Detection Limit BRI : Below Reporting Limit Page 65 of 154
Page 343
Sample ldentificationM8F-13 2,-4'sA59803-t3
Client Proiect #301,88
MatixSoil
Received27-Mar-07
Collettion Date-/Time26Mar-07 00:00
CAS N^ Analyt (s) Resl,lt FIag rRDL Dilabn Method Rel Prcpared Analfzal Bslch Analfsl
Semivolartle O.gonic Comporrds by CCMS
Semivolalil€ Oroanic Comoolods bv SW846 8270CPreparcd by m€lhod SW846 35508
5o{e-0 Bslao (alpyrens
2o$9e? B€{zo(b)fuoranthene1912+2 Benzo (g,h,t) peryten€
nr.@A Benlo ft) nuonnhen€66-854 EenZOiC add10o5r G 8en4,l alcohol111-9rr &5(2dtroeliory)mehan6't114-a
Bis(2{itu,oehyl)dlEr
396!8-32.9 gs(2dloaoisopr.o0ytle$e.
1lr'81-7 Bis(2€hy'he4)pnhatab101-55n 4-Bomophary'd€nyleh€f
c56&7 Butyl b€nzy' pnthatab
8e7+6 Cab€roles9so'7 4{hlora}meqlphenol
106-47{ +Chloroanlineel'58-7 2{hldonaph$do|e
s57-o zchlo|o0henol7tot72-3 4.ci orcpnenyi phenyteher
213i1.9 ChrFen€53?Gt Dh€mo lAh) anthra.ene13e-6+9 Dib€{Eofuran
9550.1 1.2-DdOobenz€rE
5417?t 1,+Ddtoobenzen6
loc46'7 1,4-0idio@benzene
91-941 3,3-,DicHolohenzijne1m4.'2 2,+0ii* orDpt€ml&{4, Diedvlphthatats13111.3 oiftElhy'pnthalate105.67-9 a+Dmdrypn€iol*1+2 Di+tw phhatats
53.1-52-1 4,&DinftD-2-rnethyiph€iol
51'2&5 2,4oinitEphenol121-t+2 2,4-oinitobluene6oFaE z,&Diititobluenerl?.€4i orn-odylphbatats206-,rrr{ Ffuorfl sn€8e7+7 Rlor€ito11t7+1 H€xidbDbenzene
6/-083 Hexadroobutadione
n44 Horac+{oEcyclopentad€n€
6l-12-1 HoEd orc€lhaners3e.5 Indeno {1,2,3{d) pyrsle
sl2{ l+r€dtylrBphfid€.et859.r lsaphoron€91.5r.5 2+neftltEdffidele
95-1&7 z.lre[ulpidld
100-30-,1, 3,+Mehylphenol184591.2c0 Naphhal€n€0&7r-4 2-Nitroarihe99{s2 }Nitbanifne
B€L
BFL
BFL
BFL
8FL
8FL
8FL
BFL
BBL
BFL
BRL
8RL
8Rr.8Rt-BRLBFLBHL8RLBRL8RLBRI-BRLBRLBFLBRLBFLBRL8RL8RLBRL8FLBRLsRtBR!BRLBRLBRL8FLBRL
8Rt8RLBNLBnIB8LSFLBRLBRL
BNLgaL
BFL
udks d]
!g4rS d)'
!s4s drv
|ldh dv
|a4€ A
uglq dv
|,grs dl
dkg trv
udks dy
ljdiq fiv
|rylq dv
tigr€ dy
lsls dv
wh dr
ldlq dy
wrs dv|lgh 6v
|Jgredlv|lglqdyu$S ny
wro fvlqlq fr|'
!91€ fry
t4b dY
I9tq dy
WYS dY
lgls t)'
lgks mv
lgrc eY
llgb dv
t€/rg dry
rc,!€ dtY
ugr0 dy
|dlq dl
!049 dl
$ng dv
l{/t€ dy
lo4qdv|lglqdvllsit(g dl
rgtg ry
uEtg dy
Wl4drlt4*4trvBS dry
rcIq dv
uglg dv
!$4q rY
|ldto dry
wt{ dv
886 r
886 1
886 1
886 1
886 r
886 1
886 r
885 I
886 1
886 1
8€6 |
886 1
836 r
886 1
886 1
886 1
886 |
886 r
88lt 1
886 I
6t6 1
8€8 1
886 1
886 r
886 r
886 r
8t6 I
EE6 1
8E5 1
8E6 1
8€6 |
8116 r
886 |
885 r
8€6 1
E86 I
E{t6 I
8€6 |
886 I
886 r
885 I
885 i
886 1
886 1
E€6 1
E€6 1
886 i
886 I
886 1
€86 1
sw8.{6 €2?m 2gMBr{7 c+Agr4? ?031774 M.B
This labonJory rqot k aot vali.I Nithoa! a6 althoiac.! tignature on alte cowr Ingc.' Reporrrble Detection Limit BRL = Below Repoding Limit Page 66 of | 54
Page 344
Sample IdentificatiouM8F-43 2'-4'sA5980l-13
Client Proiect #301-88
MatrixSoil
Rcceivcd21-Mar-07
Collcction Date/Timc26-Mar-07 00:00
CAS No. Anab.e(s) Resah FIag Irzr'6 'RDL Dilution Me,hud Rel. Prcparcd Aaalyed Butth AMqsl
Semivolrtil€ Org{nic Conpounds by GCMS
Sanivol€tile Orcanic Comoounds bv SWB(; S27OC
Prepared by method SWB46 35508
1c0{1s +Nitoaniline984+3 Ntlbeozers8&7$5 z-mtropheflol10002r +NjtDphsnol62_?5'9 l{-Nitrosodrnelhlanine0216+7 N-Nitmsrdi-ntroFtamine63!_6 l{-Mlmsodiphenylaninen4&5 Peniachtonphenol&01-8 phenanlhrene
100 9t2 Phenol
fio.srl pyidine
12{182 r 1,2,4-Tricl orobenzene695"r a4,s-Tichiorophenol88.062 e4,6-Tichtorophenol
ar$t ZFhMobbhenl
fi7-t24 2-Huotophenol
t16s644 lkLnhenzene4s
41654t-2 Ptpnol4,
t7t6-51i fepfunyLdl4
t1&84 2,4,6.Tdbtoft)phenol
29Mar{7 0}Apr{7 70317/4 ti.8BHL
BHL
BFL
BFL
BFL
BFL
BFL
BRL
BRL
BFL
BFL
BRL
BBL
BRL
BRL
61
ffi
49
68
49
0 362
51.1
2 U
pS4S dry 3910
lYkg dry 886
!/fS dy 886
trg,&g dry 3540
ldlS dry 886
lgre dry 886
|ldre dry E66
ldlq dry E86
pdlq dry EE6
lgr€ dry 686
N,4(S dry E€6
pdlq dry 886
pdkS dry 886
pS/lq dy 886
Udlq dry 886
tu130 %
15110%
3+13! %
1u110%
3+1& %
15.110%
nglq dry 0.0391
m/kS dry 129
mS4(S dry 1.9,1
n'dkg d,] 0 647
ndrq dry 0.W
mdlq dry 0.6'{7
tlgt<S dy 0-970
ndkg d'y 1.94
mgn 0.0100
tng4' 00150
fi9,1 0.0050
nrg,l 00115
rnS'l 0.0125
mg,l 0.000{0
mg/l 0(D75
fi94 0.0150
sw846 8270C
swe46 747tA
EPA200.7
Total M€trls by EPA 6000/7000 s€ries Methods
Totrl M€tals by EPA 200 Series Methods
144041 S lver
7t{G3t-2 A6enic
74{0.39.3 Barium
7440-419 Cadmfum
7440-'r?,3 Chromium
7419-92-t tEad
7792.1,!2 Sdenium
SPLP Metsls by f,PA l3l2 & 5000/7000 Series M€thods
SPLP Exlraction Comdeted
ll'lnzl4 Siher BflL
z4r3&2 A/senic 8BL
7,14cx93 Ba.ilm 0.0064
71404!.9 Cadmiur BRL
144117-3 Chmmium BRI
7,F&97-6 llercury BFI
743$92-l Lead BRL
n@4*2 Sdenium BRL
Gererrl Chemislry PrrNmetera
%So4i6 750
0.0530 02.Apr.07 0& pr47 781810 YP
BFL
3.9S
53.4
02Apt-07 H8
SW8461312 2&Mar{7
SwE161312/60108 301'rarfi
sw8461312?470A
s1rvE46 r3l26r)10A
2&Mar-07 7031763 ED
q2-ApF07 rc31805 lR
02-Apr{7 7ff1m6 YP
m-Apr-o7 7031805 LR
Sii254o G Mod 30.iraq SHrcr{7 /03i8/9
This labomtory .epod is nol vold x, haA aB aalhoriaed signoture on the cowr page_
* Reportable Detection Limit BRL = Below Reponing Limir Pag€ 67 of 154
Page 345
Sarnole ldentificationM8F-,1.t 2'-4'sA59803-14
Client Proiecl #30r-88
Collection Date/Time26-Mar-0? 00:00
MatrixSoil
Received21-Mar-07
CAS No. Afialru(s) Resatl Fhe *RDL Dil..,ion Method Rel Prcpared Analyzet Batch Analw
Vohde organic ColrDoinds
Prepared by mettlod SW846 5035A Soit (tow tevet)
7&191 1,12-Idchlooffiuoroehane(FGon 8FL67-6+l Aaetone BRL107.r$t A{rybnede BRt7t4-2 BsEen€ 8AL100-8Gl Bromobenz€n€ BFL7t97-5 Bo|rtochlololnetrane BFL1tru B|Dlnodidlto|tlr€tlane BRL7E25.2 &unob{m BFi-74{3'9 Bromdnghan€ BFL7e$.3 2_&ranone (MEK) BRLl{l+51{ n-Buldb€ru€ne 8FL1354s0 s€c€'rlylb€nzone 8Rfs€{e6 bd&tyibenzene 8RL75rsl Cafion d&lfide gfiL
s62+s ceitfi tdEchlonde BEL10&m-7 CHombenzene BFL7s+3 drroro€hane BRLr.66.s Cnloldorm BFt7ir€?.3 Ollorofighai€ BRL6{9-s 2-cl olutoiug16 BRL1116-{3-'l +Cfihotdufie BFLs12_8 1 ,2-Dbroot}3drlorcptEpane 8RLraH+l Diirofiodbomehano BRLro6.sH tl.Dbmmoefiane (EDB) BRL7rt-95.3 DboflDm€trene SnL95.561 1,z{ichtorobffzene BFL511.73.r l,}Dtchlcrob€rEene BRL16n6.7 l,ADbhlorotJ€nzen€ BRL7571.0 Didkodi&rordn€thane (Freon12) BRtE3.r3 1,1.Diddorc€$a1e gnl
107{ez l,roidltorc€fiane BFL7535r l,l1oicildo€tler€ BFL1565&2 os.t,2-Did{oroefiene 8RLl5&6G5 ! s.1,2-Ed om€fieno 8Bt7447-i tz-tldlo{opropa'le BRLrrE-zs{ t,}Oichkro$.oDone B8L5o+zG7 2z.oidnoDpropane BFL5631&6 l,tDafildoFopene 8Rt-l@61{r-5 ds-j,310id{orcFopeno 8Rtl@€14e{ taN-1,3{kflo(opmpg1€ BRL10rH1{ Emlb€rusne B8Lsr.6r.3 H€radtorDbdBdiene BFL5€1-78 n 2+t€xsiorE (M8K) BRLs{2{ lEop|lpy6eiz€rle 8RLssar{ +t$oprop}ltoluen€ BFLl6ll.lrlt4 t ettyl tqt b{r9 st|€r BnL108rc1 a_ etryt_2-p$tanon€ (ti{BK) BRL
m4al{1 28-]lra'{7 7ffi1167 BD
29-lMBr-07 z$Mar{)7 7031790 RU
Volrtlle Orgaoic Compoords
Voc Exfadtor
|lg/ts dl 6.0
llgli! dy 120
!91€ dry 6_0
!s4€ dy 6.0
|Jo/l(s dy 6.0
ldkS df 6.0
|4/kS dy 6.0
|dh dv 6.0
Iglq dy 12.0
udrqdy 59.8
ldkg dy 6.0
t4t,Sty 6.0
gdlq dy 6.0
pdtqdy 299
uSIEdry 60
!dk0 dy 6.0
lll/lq dl' 1?.0
|.gts 6y 6.0
ISlq d) r2.0
|lgl|(gdy E0
!g/rg dy 6.0
|lg/kS trV 12.0
lldl€ dry 6.0
!04qdy 6.0
llg/r0 dy 6.0
!S/to d] 6.0
tig+€ trI 6.0
USIqdrf 6.0
l4llq dy 12n
pg/tqdy 60
ldlq dy 6.0
Wh fy 6.0
|4/rS dl 6.0
!94€ dy 6.0
rcre dry 6_0$h0 dry 6.0
lglg try 6.0
l4rS &y 6.0
tdb rv [opg,lqdy A0
|,gl{s dv 60
!S*S 'tI 6.0
$4S 'ty 59.8
pglq dy 6.0
UdkSdry 6.0
|lE},g dy 6.0
lgrs dv 59.8
Enq dy 59.8
$9ey 6-0
Fleld sarad€d vcrc
sw 846 82608
7F0s2 Me$ytene dlbdter,r.2o3 thptfd€no
BRL6RL
Thb labonror!.epon it Nrt eaIld pihout ott aulhoized siAnatart on the cawr poge.
' Refortable D€t€dion Linit BRL = Belotry R€portiag Limir Page 68 of 154
Page 346
Sample ldentificationM8F-14 2'-4'sA59803- t4
Client Proiect #301-88
CoLlection Date/Time26-Mar-07 00:00
MatrixSoil
Receivcd2'l-Mar-07
CAS No- Anqbte(s) Flos *RDL Dilution Method Rel Prcpared Analrzed Batch A,rallst
Volrtil€ Orgrnlc Compourds
Volalile oqanb Comoounds
Prepared by method SWM6 5035A Soit (tow tevet)
103-6tl n-Propyh€nzene 8RL1110..2.5 Styrene 8RLaG2O.6 1,1.1,2-Telrachloroethane 8RL793,1.5 1,1r,2-TelGchloro€than€ BRLtn-lg4 Tetrachlooeheno BRLt06rt8.3 Toluene BRLsr-€r.6 1,2,3-Trichlorob€rEen€ BFL1ar'82r 1,2,4-Tichtoroben2ene oRL7155,6 1,1,1-Trchlorc€thane BRL79.00.5 l,12-Tidltoroelhane BRL71413 Trbhboehene 8RL75i9-4 TridtorofluoromethenB {Freof t1) BRL!r&18.4 12,$Trichloropropane BqL95€{ j,2,4-Trinehylbenzer€ BFLr061t7-8 1,3,S_Tdmeltrytbenzene BFL7s4r-.t vinyi dttorde BFL1s'G2G7 m,Fxylene BRLs-47€ oxylene BRLr0es-s Tetahydofuran BRL4.2u7 €$ylelher 8RLes!rc5.s Td-amy' methy4 6lh€. 8RL607{2.3 Elfiyl ten-bjtyl ehef BRL1@-2r!3 Di_isopopyteher BffL75.66.0 Ten-Bulanot / botyt atcohol BFL
2gMa.-07 29-1,lar-07 7031790
29-l'rlar{7 30.r'lar-07 7031773
ugrs dv|,vrs drvrtdlq d'y
t'4kg dry
rdl€ drypdks*ypgrs drv
!91$ dry
ISAS dry
Ps/ks d.Y
ars dryudre dryldks dv
|ldfio dy
tiglq dy
!s,4q dry
ISAS drypC4(S drypg^g dw
|a,tS dry
!94!1dyu94q dryps]|,o drypgrq dypg4(s dry
70,tn%70-t30 %7trt30 %/0-130 %
mdkS dry
n'grq dly
mgeg dry
mdq ey
m$4q dry
mSAS dry
mVlq dry
rigfts dry
mqlo fiy
mS/kS d|y
&t4n%
sw 846 826086 0
6.0
6.0
6.0
6.0
6_0
6 0
6_0
6 0
6.0
6.0
6.0
6.0
6_0
6 0
6.0
12.0
6.0
59.8
6.0
6.0
6.0
6.0
59.8
\m12341'1 1,4-Doxam
1&4).4 +Srcnol|Dobapene
,,37-285 ToiEne-dg
t/ffi474 |,2-Dlchloroethane44
t8@3?7 Dibmnonuovnelhane
Ertmctabh Petroleum Hydrocarbons
Extaclablo Tolal Petroleum Hvdocarbons
Prepa.ed by method SW846 35508
8006 61.9 Gasoline@t?6no2 Fletoil f264176-3r '3 Fuel oil *4686s3-00-4 Fueloil{6|,l]98@0 Motor oilJ10100000 Avialbn Fuel
Unidentitied
Otrer oil
Told Petrdeum Hydrcc€rbcns
C9{36 Aliphalic Hydrccaftons
n8-3t+ tohlo[oxtadecane
SemivolNtile Organk Compoutrds by cC
Oqanodllorine Psqj.idss SWe,46 8ffi JA
Prepared by method SW846 3545A
F{0.2 Atdin
BFL
105
1 1 1
115
BfrLSFL
BFL
BFL
BFL
BRL
38€
Calculated as
388
388
315
{T ETPH65.0 r
65.0 I
65.0 r
650 r
65_0 r
65.0 J
65.0 1
65.0 r
650 1
65.0 1
t4tqdv s!1846 80814 2UnaA1 VAVAT 703173ts
Thk lahomlory ,eForl is nol vzld x'ithorlt aA authoi\ed slg&turc on the coeer page
* Repo.table Detection Limit BRI- = Eelow Reporting Limit Pase 69 of 154
Page 347
Sample IdeotificationMtF-{4 2'-4'
sA59803-14
Cliert Proiect #301-88
MatrixSoil
Rec€ived21-Mar07
Collectiop Date/Tim€26-Ma.47 00:00
CAS No. Andyta(s) Ressla FloE Unltl 'RDL Dilation Method Retr. Prerycd AAa4zed Batch Anallst
Semlvolatile Orgrnic Compounds by CC
Oroanodrlodno P€sdcid€s SW846 8081A
Prepared by method SW8,l6 3545A
3l9M{ a€l-|c3198&7 b-BHC3198&S dEHC5&8s{ g-8fc (Undans)
ll-744 Chlordan€72.5+s 44ODO F,p)n15.e 4a ODE (p,p')
5G2$3 d4.0DI lp,p)qltr D€lddnSS.98-8 End6ulan I3lP1+659 Endoou an llr03t{7-0 Endooulansdlat€n-&B cndin7121,93-{ EdrinAldoiyd€76{4-0 Heplaailor72{r.5 irehoryd{or1u2r-5t-3 Hspta*brEpoxjdee0135.2 Toxalhene5103t14 a-chlodane5566-a!7 $& odane5:XS+70-5 Enddn K€ld1s
t@@44-2 4,4-08-6htuhtdiptstyl (Sr)
nsla4.i DeeMeidEwl(St)
Poh&ildinated thrhsrds bv SW846 8082
Prepared by method SW846 3545A
1267+11.2 PCB 10161110+e2 PCg 1n11r14t-tFs PCB 1232534€o"1's PC8124212672.295 PC812481r@7{Sl PCB 125411096{25 PCE t2S03tt 1.2?5 PCB1Z6211t0G1r-4 ru1ft8
[email protected] 4484daflw@En1(54,,5124-3 Dec2dlot&lrtenyt(Si
S€mtvolrtile Org.tri. Compo|rtrd! by ffMS
S€mi/olade oroaric Comodnds by SW846 8270C
Prepared by method SW846 35508
8i-32€ AceiaphtEne
A8€{ Acenedhylsfte62.513 Anjlnot&r2.7 Anthraceae1912.244 Atsazing103ill-3 l"ob6nz€n€,iDilhenyldaznes2474 B€nzidine566s3 B€nzD(a)entmc€ne
2&lrar{7 02.Aprfi rulng TGBBLBRLBRT8RL8RL8RL8RLSRLBRLBffL8FLBFI.8FLORLBRLBHI-BHI.BHLBflLBFLBFL
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sw846 8081A
sw846 8082
34.5 1
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fhb laboralory ,eport is Mrt vslld Eithoul tE zathofize.I sig attft on lhe cowr page.
. Reporlable Det€ction Limit BRL = Below R€porting Linit Page 70 of 154
Page 348
Sample Identifica(ionM8F-44 2,.4'sA59803-14
Client Proiect #301-88
MatrixSoil
Collection Date/Time26-Mar-07 00:00
Receil'ed
27-Mat 07
CAS Na Anatytets) FI"S Units *RDL Dilution Method Reli Prcpared Amlyzed Batch Ahalyst
Semlvol.tile Org|nic Compounds by CCMS
Semivolatil€ Orqanic Compounds bv SW846 9270CPr€pared by method SW846 3O5OB
5lr?-8 B€nzo (a)pyreiealt992 Benzo(b)tluoranlhene1n.^.2 Benzo(g,h,i)pe04ene20?i)8.9 Benzo(k)fluoranlhene05{54 Benzcic acid100,51€ B€nzylatcohdIII9r1 Bis(2dtloroethoxy)ri€hane1lr-{r!r Bls{Zdfuroethy,l)ethsr3stt8 92 e BE2dioroisopropyl)€tEr117-s1.7 Bis{2€h},th€xyt)phtnahb101_5t3 +Bromophenyl pheryi eth€rel5.G8-7 Bdyl ben4,t phlhatate8&74.0 Calbazote5SsG7 +Chtoru,$methylpt|enolr0fi7-8 4-Chtooanitine915&7 A.Chloronaphhatare&57€ 2{hloroph6ndro0tz.l 4Cruorophenyt ph€nyt eher210-01'9 ChryserDs17e3 oibenzo(a,hlanthEcene132.6+9 DibenzofuEng5.5Gr l2-Dichlorobenzene541-?+1 1,3-Didtlorobenzene106-4$7 l,4,Didoobenzene91441 3,3',{ichtomben?idine1203+2 a4-Ddltorophenol
56.4 Detryt phthatate
13r,t1_3 Dmelhylphhatate10&67-s z,4-oimettrylphenol*14-2 U-n-butylphtlalat€
!!+52'r 4,6-0inrto-2fieihytph€nolsr.28.5 2,4{initrophenol1211+2 2,4{inilDlohreneo6.202 2,Foinilrolollene117-84{ Di-n{d}4phtEtateaG{4-0 FluoEnlhene
11&741 H€nchloroben2me87.6&3 FlsachloDbuladienen17.1 HeEclorocyclopenbdiene
61n-1 Helacl oroetlarc193.1$5 Indeno (1,2,3.cd) pyreno
s.12.0 't-M€thylnaphlhalene
71.59.r lsopt|oone91.5r-6 2-MethytnaphthaienelF,ls-7 2.tethytphenol
108-€9-1, 3,4.Mshylphend106'1115g1-al3 Naphhderc0e74-{ z-Nilroanifin€9t{€-2 }Nitroanilin€
BRL
BHL
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8RL
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BRL
BRL
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ORL
BRL
BRL
BRL
8RL
BRL
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BRL
SRL
BRL
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BRL
BRL
8RL
BRL
8RL
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8RL
8RL
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BRL
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lVtS dry
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uc4q dry
pg?.o dty
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!0k! frv
rc/kg dfy
tg\sdrypgl(s ev
]Js/rsdrypS4rS dry
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lEts drypErs dry
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!s.*s dry
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llsrlg drv
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ts4q dry
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!94€ dy
fcrc dv
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801 |
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sw8{6 8?70C 29-Mar.07 03'AF-07 7031774 M.S
Thk laborutory Rport Lt dot t'dd withoat an aartoized signatare on thc cover prye-
I Reportable Detection Lim'i BRL = Below Reporting Limir Pas€ 7l of 154
Page 349
Sample ldentificationMtF44 2'4'sA5980l-r4
Client. Proiect #l0t-88
MatrixSoil
C-olleciion Date/Time26-Mar47 00:00
Rec€ived2?-MaI-07
CAS Na Anzlyu(s) Resuk FI"S Unia *RDL DilBtioft Method Ref, Prepated Ana$zcd Botch Analysl
S€mivolalile Orgrrllc Compornds by GCMS
Semivolalile Oruanic Cqnmuods bv SWer46 8270C
Prepared by method SW846 35508
r@4r{ 4-Ni!od lne
sct3 Nilrdsl?q|e
0a75's 2+lilodt4holrm{2-7 +Nitrcfiend6a-7F9 N_NiuocodkloryanineEr€+7 N-NiEosodi{.progy'arnine86n0-6 N+litosodiptErylanine
ar{6.5 P€flhchbrophenol
85{1-0 PhemnfiEne108 9t2 PlEnol129-00-0 Pyrerc1'0€Gt [email protected] 12,4-Tt*tfuidba1z€!]lee5s54 2,45,Trichtofoph€mls8-(BJ 2,4,6-Tridofophenol
P1&4 2-Fh-nrdphewt
367-12.{ 2+hffdldnd
4t55-@4 llifunene45
1165-62'2 Pheml45
t71e5t4 fqpwd4
t1&N4 24,6-ftiban@ta1d
2$Mar{7 ()+Apr{7 7(X}1774 M IBRL
8RL
BRL
8RL
8flL
8RfgRL
BFL
BNL
8FL
BFL
BFL
B8L
BBL
8RL
57
71
65
d9
0 586
BFL
7.m
16.2
0.461
Lm
1 1 S
3ZD
807
$7
3Al0
w7
807
&7
807
E07ql7
wwlEO7
E07
607
pglq fiv
|lglq dv
usre drylgtS dry
|4,lqdvlgrs dy
ldts dv
!s4q dv
lgrro rv
|jsfts rv
ldfts drypdl€ dv
ljgb dv
|drs ev|ldks dv
*tg%
1Ul10%
w-130%
1+110%
*13t)%
,r110
swE46 8270C
s1v8,45 t47 tA
EPA 200.7
sw84613r2/t{70A
strs46 1312/60108
Totrl Metrk by EPA 6000/70{0 Se e! Methods
713$97+ MerqJry
Iotal Metals by EPA 200 Seri€5 M€thods
f@44 Sav6r
7.Wf39.3 &iun
7rut 139 CaddLrn
71401t:J Cirfrrlium
743+92n Lead
ns24.2 S€l€nium 8RL
SPLP Met.ls by EPA 1312 & 6000fl000 sertes Merhods
SruEftaclio.r comdgl€d
7@24 Sitv€r BnL
7l{+3&2 ,,lssric BRL
71,t0-39,3 Earium Omj4
7,1'l{lr$9 Cadnulm BnL
1145!,1.3 Ch|unium BRL
7a!197-6 tlelclry BRL
7439 P-t Lead ERL
77te.192 S€t€.'i,rn 8RL
Getrara.l Ch€tnirtry ParaDeaer3
% Solds 90.1
nB& dry O0@6
m94q dry 1.lE
mdtsd'y r.59
mg/kgdry 0.530
mgtgdry 0.266
mg/},gdry 0.591
mElg dif 0.796
mgfg dry 159
rigi| 0.0100
ngn 00150
mgr 0.m50
ngl 0.00es
mga 0.0125
r'1dl 0.m040
'r|gl 0.m75
mS]| 0.0i50
MM41 0$Apd7 7031810 YP
H8
' 02-Arr{7 7091806 YP' mrApr4T TllBlSlXt $
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SW8461312 284tur.07 28.t ar.07 7031763 8D
Sl'1846 1312/601G 3Glrar{7 m.Afl-07 7031805 LR
slilzto G Mod StHvtaroT 3l.t&r-07 7001879 yli{
Thit labora,ory rcpod it not volid lfithor.t q, asthoriaed signamrc on the couer poge.
r Repo.tnbl€ D€oection Limit BRL = Below Reponing Limit Pase 72 of 154
Page 350
Sample IdentiftcationM8F-45 4-6'sA595 r7-10
Client Proiect #101-88
MatrixSoil
Received20-Mar-07
Collection Date/Timel9-Mar-07 00:00
CAS No, Anolyte(s) ResuIt Fl"S Units *RDL Dilatian Method ReJ Prcparcd AnoDaed Batch Anoust
Vol.tile Organic Compounds
VOC ExtractionVohtile Oroanic Comoounds
Field €xt|acled
't77
!g/kg dry 95I
!g/kg dry 1920
Ug/kg dry 95 I
|lgkS dry 95.9
us/ks dry 95 IpdkS dry 95.9pdkS dry 95.9
!g/kS dry 95.9
!g/Kq dry 152pg/kg dry 959
!S/kS dry 95 9pg/kg dry ss.s
PgkS dry 95.9
ugr(rg dry 479
Pg/kg dry 95.9ydkS dry 95.9pdkg dry 192
!S,(9 dry 95.9ps,'xs dry 192
UdkS dry 95.9
lgkS dry 95IpgkS dry 192
lgkS dry 95.9pdkg dry 95.9
lSftg dry 95.9p94(S dry 95.9
!94q dry 95.9
ldks dry 9s.9
lSftS dry 192
!g'I(S dry 95.9pgkS dry S5.S
!/kS dry 95.9pgks dry 95.9
trg/kS dry 95.9pg/kg dry 95.SpSn(S dry 95.9pgKg dry 95.9pdkS dry 95.9
PgkS dry 95.SpdkSdry 95.9
Fg/kg dry 95.9ydkg dry 95Ipg/kg dry 959pg/kg d.y 95I
tgkSdry 959
Fg/(g dry 95 Ipg/kg dry 959
lis.ixg dry 959pdks dry 95.s
voc 21-Mat47 21-Mat47 7031261 BD
Prepared by method SW846 5030 Soit (high levet)76-1x-1 1,1,z-Trichlorotrifluoro€thane(FreoBRL SW84682608 27-Mar1l 27-Ma.{7 7031602 mar676.+r Acelone
107-13-1 Ao.ylonit^iler14+Z Benzene
BRLBRLt8a
l0&€C1 Baomobenzene gRL
11-97-s Broft'o(hlo.omethane BRL15-214 Bromodichtoromsthane BRL75-2+2 Erclnofofm BRL74.43.9 Eromomethene BRL7843.3 2-Butanone (MEK) BRL10+51{ n-Butylbenzene BRLi3t98{ sec€utylbenzene BRL9E{€{ tert.Butylbenzene BRL75-114 Carbon disulfide BRL5F2$5 Carbon tetrachloride BRLt00+0-7 chlorobenzene gRL
75{03 Chtorcethane BRL67{&3 Chlorotorm BRL744f-3 Chloromethane BRL9s49-8 z-Chlorotoluene BRL11164:lr +Chlorotoluene BRL!re12-€ 1,2-Dibromo_3_chtoropropane BRL12{-48-l Oibromoohloromethane BRL106-934 l,2-Dibmmoethane(EDB) BRL7445.3 DibromometfEne BRL95.501 l,z-Dichlorobenzene BRL3i1,73-1 I,3-Dichtorobenzene BRL106.46.7 l,4-Dichtorobenzene BRL75-714 Dichlorodifluoromethane (Freonl2)BRL7+U-3 l,l-Dichloro€tf|ane sRL10746,2 1,2-Dichto.o€thene gRL
7135!.4 l,l-Dichloro€t|€ne 8RL1s&59'2 cjs-1,2-Dichloroethene 8RL1sffiG5 t-an91,2-Dichtoroethene BRL7&1t7-5 l,2-Dichioropropans BRL142.2&9 |,3-Dichloropropane BRLs9{-2G7 2,2_Dichloropropans BRL5eF584 |,'l -Dichloopropene BRL10061{1-scis-1,3-Dichlofoprop€n€ BRLt00€t-02€taarls-1,3-Diclhlorop€pene BRLi El-4 Ethylbenzene BRL07€8-3 H€xachlorobutadiene BRL591-7eo 2-Hexanone (MBK) BRL98{2{ lsopropyibenzene BRL99{7{ 4lsopropyltoluene BRLr63a4H Methyl tert$utyl ether BRLl0e1c1 4-Methyl-2-pentanone(MIBK) BRL7$O$2 Methylene chtoride BRL
50505050505050505050505050505050505050505050505050505050505050505050505050505050505050
50505050505091.2G3 Naphthabne
Page 47 of 124
Thb loboralary report It hol wlid f ilhoul a, thoriazd signetwe onthe coeer page
* Reportable D€teclion Limit BRL = Below ReDortine l-imit
Page 351
Samole [dentifrcatiotMEF-45 ,l{'sA595 t7-10
Clieot Proiect #301-88
MafrixSoil
Collection Date/TimeI 9-Msr-07 00:00
Received20-Mar-07
C"4S No- Analytz(s) FloC 'RDL Diluioa Mdhod R.J Prcps.ed Anztyzed Bdtch Anzllst
Vohdle Orgtuic Compoundr
Volotile Oroanic CompoundsP.epa.€d by mettrcd SW846 m30 Soit (high tevet)
75{9-4 Trictrlorof,uoromethane (Freon | 1) BRL
103€+i tuProF,ylbenzene1(10-{2-5 Styr€ne63G20€ 1,1,1,?-Tetsachtoroethane79.3,t-5 I , 1 ,2,2-Tetrachloroethaale12710-4 T€trachloroethenerO€-88-3 Toluene8751-€ 1,2,3-Tridorob€nzene121l€2-1 i.2,+Trid ofobenzene7165"6 I,I,l_Trid oroethan€79{1}5 I,1.2-Tnchbroethan€79{14 Tdchloroethene
sG18-4 l,2,STrtchtoropopanee5€3-€ t,2,+Tdmethytbenzen€'ros67{ 1.3,$Tdmethylberjzen€75{1-4 Vrnyt d{odds13ilG2c7 m,p-xylene95-47€ o-Xyienell)999-9 T€fahydrofuran@-297 Ehyl etiter991-05-0 Tert-emyt methyl €ther637-€12-3 Efiyl ted+ubd ether10&20-3 Di-isopmpy'ether7555rO Tert-&rtanol / butyl alcottol12+S1-r 1,4-Dioxane
sunog,a{a /ecove/lbs.'460404 +EJnmofluorcbenzene2037-26.5 TdrEne4SI 70&47 4 1, 2-Diclldoethane441s6€.63-t Dibrcnofl rbmfiethane
Ertra..Lbl€ P€trolenm Hydrocrrbof, sExbactable Toial Peboleum HvdrocarbonsPrepaEd by method SW846 354546006€1-9 Gasoline6847G3G, Fu€t Oit tt26€47S31-3 FuelOil{t468s6340-1 FuelOit#6[r0!t8oq]00 Motor OilJoolorxDo Aviatjon Fuel
Unidentifi€dOther OilTotral Pototeum Hyd.ocarbonsCSC36 Alphatic Hydroca.bons
surtogab B@vefus:3386.33.2 1-Chlor@dadecane
Semivol.all€ O.grdc Coflpounds by CCO.oanoc{lodne Pesticides SWBi{i EOgIAPrepaf€d by mehod SW846 35508:,09{G2 Alddn
SW 8,f6 82608 27-Mar47 27.{'r'lat47 7001602 marBRL8RLBRLBRLSRL333BRL
BRLBRLBRLBRL
8Rr8RLBRLBRL22499.7BRLBRLBRLBRLBRLBRLBRL
1028992
BRL
BRLBRLBRL8RLBRL203CaldJlated as203203
140
ldkS dry 95.9
$gkgdry s5.9
rcikS dry 95.9pgls dry 95.9
ldkS dry S5.9
|l9ft9 dry 95.9pdkS dry 9s.9
UCftS dry 95.9
ldxg dry 9s.9
!Sn(S dry S5-S
FdkS dry Ss.g
rdks dry 95.9
lcrls dry 95-9
US/kS dry 95.9pdkS d.y 95.9pCrkE dry 95.$pgrsdry 1s2
lrgtS d.y 95,9
t gks dry 959pdtg dry 95.9pdrgdry Ss.g
UdkS dry 95,9
rdtgdry 95.SpSftg dry S59
ldksdry 1920
7d'130 %7G130%lGtfi %76tm %
5050505050505050505050505050
5050
5050m5t)
ngftS dry 46.1
nE/kg dry 4€ 1
mgkg dry {6. I
ntg/rg d.y 46.1
otg (g dry 46-1
rnglsdry 16.1
mg/kg dry /t6.t
nt€/kg dry {6.1
rng^g dry 46j
nElkg dry 46.1
40,140 %
+CT ETPH 22-|hr-O7 26-ttat47 703128,{ DS
BRL lgtg dry 7.74 SWE46 80814 n-M4r47 271iat47 7031275 fc
This latonrorf rcpod is dor wud nAhord arr &rhorizetl slgrulc?c oE thc coeet page.
' Reportable Det ction Limit BRL = B€low R€poftiog Linir Page 48 of 124
Page 352
Sample IdentificationM8F4s 4-6'sA595l7-10
Client Proi€ct #301-88
MatrixSoil
Received20-Mar-07
Colle,{]tion Date/Timel9-Mar-07 00:00
CAS No. Ahalrte(s) Resdt FloC rRDL Dila.ian Method Rel Prcpand Anabzed Bdtch Analyst
Semiyolrtile Org{ric Cohpounds by CC
Omanochlorine Pesticides SW846 8OgiAP.epar€d by method SW846 35508
319{4,6 a-BHC319{5-7 b.BHC319-864 d_BHCs8{9e gFBHC (Lindane)
57-745 Chtordane72-54a 4.4.DOD (p,p')72-5+e 4,4.DDE (p,p.)
50-?+3 a,A-DDT (p,p,)@-57-r Dieldrin95$9€{ Endosulfan I33?1$6S Endosulfan ll1031{7{ EndosulfanSulfate72-?0-€ Endrin7.121-93-{ Endrin Aldehyde7g,r{ Heptachlor724!5 Methoxychlor10445ru Heptachlor Epoxid€E00135.2 Toxaphenesr0$71-9 a_Chlodane55SGl47 glchjordane
s349.1 70.5 Endrin Ketofle
Sunogete |Bco|uEies:
10386412 4,4-DB-Oclafluorobiphenyt (54
20 -2a-3 Decachlorobiphenyl (54
Polvcilorinated Biphonvls bv SWB46 eO82Prepared by method SW846 3545A
1267+11-2 PCB 10.161110+28-2 PCEJ 122111141-165 FCB 12325346+21-s PCB 124212G72-296 PCB 124811497-6€r PCB 1254i109€{2-5 PCB 1260x1n+?6-s Pcg 1262rl lrxr-14{ rcB tm8
Sunogale reotedes:1 @ae8+2 4, logoclef, trc'atiphenyt (Sr)
2t51-2+3 Decachlorobiphenyl (St)
Ssnivoladte orgrntc Cohpounds by CCMS
BRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRL
36
8RLARL8RLBRLBRLBRLBRLBRLBRL
45
UdkS dry 7 t4
Ug/kg dry 7 74
lgkg dry 7.74
lgkg dry 7.14
t S/kS dry 38 7ps/kg dry 7.74
Pqkq dry 7.74
ud*g dry 7.74
Ug/rS dry 7.00
USftS dry 7.74pSftS dry 7.74pdks dry 7.74
!g./kS dry 7.74
Ligt(S dry 7.74
f.ig/kg dry 7.74
P$4(S dry 7.74
UdkS dry 7.74pSAS dry 34.7
Fdkg dry 7.74
PEkg dry 7.74
!s/kg dry 7.74
30-150 %30-150 %
!g/kg dry 15.5
trdkS dry 15.5
Udkg dry 15.5
FS/kS dry 15.5
!g/kg dry 15.5
trEkg dry 15.5
ldkg dry 1s.s
!s/ks dry 15.5ydksdry 15.5
30-150 %30-150 %
FSftS dry 343
!g/kg dry 343
ldkg dry 343
!s/kg dry 343yg/[g dry 343
Fs/kg dry 343
vs/kg dry 343
ldkg dry 343
sw846 8270C
1
1
I
I
1
1
I
I
1
1
1,1
1
1
1
1
1
1
1
1
sw846 8081A 22-Mal-O7 27-Ma?O7 7031275 rc
SW846 8082 22.Mat-O7 24-Ma.-o7 7031313 IVP
Semivolatile Orqanic Camoounds bv SW846 8270CPrepared by method SW846 35508
83.32-9 ,@naphthene20&96-8 Ac€naphthylene62-513 ,{nitin€12{112-7 Anthracene1S12-2+9 Atazinet03-3+3 Azoben2ene/Diphenyldialne92{7.5 B€nzidine56'5t3 Benzo (a) anthracene
23-Mar{7 26,Mar-07 7031371 t\r-ABRLBRLBRLBRLBRLBRLBRLBRL
This laboralory tepotl is ,tol wlw vithoat zn authonTed si4nalurc on thc co|er page .
t Reponable Det€ctiol Limit BRL = Below Reporting Limit Page 49 of l14
Page 353
Samole ldentiflcaaiotrMtF-45 4i'sA595 t7-10
Client P.oiect #301-88
Mat ixSoil
Rec€ived2O-Mar47
Collectioo Date/Timel9-Mar47 00:00
C"1S No. Analt,e(s) RescU Flrg 'RDL Dilation Aefiod Rctr PQpared AMIWd Batch An&qsl
S€mivol.tne Orgrolc Compo{trds by CCMS
Serni',/olatile Omanic Cornpounds bv SW846 8270C
Prepared by me0lod SW846 3550850-32{ Benzo (a) pyrene2019$2 B€fizo (b) nuorantEne1s1-24-2 B€nzo {g,h,i) peryl€ne207{&9 Ebnzo (k) fluoranthene05€5-0 B€nzoic acidr0o-5r€ oenzyl alcohol111-91-1 Bis(2-chtoro€thory)melhan€tll-aa4 Bis(2-chi.xo€thyt)etrEr3963&u4 Bis(2d oroisopropyt)ether117{1.7 Bis(2-ehy,ltExyt)phhalate101-56-3 +Etrornolhenyt pheny' ethera5{&7 gutyl bonzyl phthatate86-74-8 C€rbazole59-50-7 +Chloro-3-rnethyph€flol10G47{ +Chloroaniline91{&7 z-Chloronsphthalen€95-57{ 2-Chlorcphenol7005-72-3 +Chto.ophenyt phenyl sther218{r€ ChryEen€53-703 Dibenzo (a,h) anthracene132€1-9 Oibenzofu.enst5G1 i,zoic{iorcb€nzenes41-73.1 1,3-Dicl{qob€nz€ne1oeF4&7 l,+Dbhloaobenz€ne91.94'r 3,3',-Dict{orob€nzidinei?0€3'2 2,+Dichlo{opheno(€4$e2 tJiefiy phtt|atate13r.rri Dimed1yl phthatate10667€ 2,4-Dirnethylph€nol8,4-7+2 D'-n+r.(ylphthetatE53{-52.1 4,6-Dinito-2-m€thytphenol51-2&s 2,+Dinkophendl2l-1+2 2.4-Oinihotolu€ne60de{F? z,&DlnitEto|ueno117{a{ Di-{r-ocoil phtnalEte2{6-14'0 Fluqanthene8&Zll Fluoione11&7+1 Hexacfrloaob€nzefle87{&3 HExadorobutadi€nen474 Hexadorocyclopentadiene67-72-1 Hexaatdoro€thane19139-5 Indeno (1,2,3-cd) pyrsn€90-12{ l-Mefiylnaphhabn€7E-5+l lsophorcne91.57€ 2-Methylnaphthatene!F4&7 2-Mettylph€nol108-304, 3,4-M€thylph6nol106-{4{g1-2S3 NaphtEleneE8-7+4 2-Nifoahitines,os.2 +Niboanitlne
BRLgRL
BRLBRLBRL
BRLBRLBRLBRL
BRLARLBRLBRLBRL8RLBRLBRLBRL
BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRI-BRLBRLBRL
BRLBRLBRLBRLgRL
BRL
BRL
BRLBRL
lgrg dry 343pdkS dry U3
ldkg dry 343pgr'kg dry 343
Idko dry 343
PdkSdrY 343
lgl(gdry 343
UdkS dry U3
UgkS dry 343
ldkS dry 34i!
ljgIlg dry 343pgrsdry 343
FgtS dry U3
udkSdry 343
rdkS dry 343
lgr'kg dry U3
lgkS dry u3
Udl€ dry 343pdtg d.y 343
liSl(g dry 343
lgkS dry 343
Ugr(S dry 34:|p9/k0 dry 343
ISfl€ dry 343pqks dry 343
!4kgdry 343
!S/kS dry 343
trdkS dry 343pgr'kg dry 343
Igkg dry 343pgkS dry 343
trdtg dry 343
t/dkS dry 343
UdXS dry U3
ldrsdry 343pg/t€ dry 343p9ik9 dty 343pdks dry 343
ldkg dry 343pgkgdry 343
IgkS ttry 343pgkg dry U3
}rdkS dry U3pCn$ dry 343
lgrgdry 343
ugtsdry 343
IS/kS dry 3,13
rcftS dry 3,13
USikg d.y 343
l,dkS dry 33
Thir ltbnbry rqort h noa edd toilhod o eudtottzd si.'l.tatc/re on the coee, pdge.
. Rcporiable Detectioo Limit BRL = Beiow Reoodng Limir Poge 50 of l!4
Page 354
Samplc IdentificationM8F-{5 4-6'sA59517-10
Client Project #301-88
Collection Date/Timel9-Mar47 00:00
MatnxSoil
Received20-Mar-07
CAS No. Ana$a(s) FIas Uttilt *RDL Dilution Method nel Prcpdnd Arnlyzed Botch Adabtsl
S€mivoladle O.garic Compounds by CCMS
Somivolatile Oroanic Comoounds by SW846 8270C
Prepared by melhod SW846 35508
10o-0t{ +Nitroaniline98-95-3 Nitrotr€nzene88-755 2-Nit.ophenol1OO{2-7 4-Nitrcphenol@'7+9 N-Nitrosodimethylamine62144-7 l+Nitrosodi-n-propylamine86-30-6 N-Nitrqsodiphenylamine474€.5 Pentachtorophenol45101{ Ph€nenthrene1O8,9s-2 Ph€nol1294t{ Pyreneri0{6-1 Pyridine
rz0+2r 1,2,4-Trichlorcbenzene95-954 2,4,$Trichlorophenolg8-0G2 2,4,G-Trichlorophenol
S4f'ogale rccoveies32140-8 z-Fluorobiphenyl
367-124 2-Fluorophenol
4165-40-0 Nitrohenz€ne45
416ffi2'2 Phercl4s
1718-514 Teryhenyl4l4
1 SW846 8270C z3'Marlr 26-Mat-o7 7031371 M.B
1 "
1 '
1 "
1 '
l '' t "
1 "
1 "
1 "
1 "
1 '' t "
1 '
1 "
BRLBRL8RLBRLARLBRLARLBRLBRLBRLBRLBRLBRLBRLBRL
106787986123
0.0948
8RL
21.6
59.6
BRL
4_50
65.3
BRL
pg/kg dry 1370
UdkS dry 343
Ug/kg dry 343pdkg dry 13'10pg/kg dry 343
!g/kq dry 343
rgks dry 343pSnq dry 343pg'{$ dry 343pS4(S dry 343
ldkS dry 343pgkg dry 343
US/kS dry 343
t g/kg dry 343pdkS dry 343
30-130 %1Ufi0 %30-t m %15-11O To30-130 %I ul10 %
mg/kg dry 0.0436
mg/kg dry 1.40
mg/kg dry 2_1O
mg/kq dry O.7O2
mg/kg dry 0.351
mq/kg dry 0.702
n'dkS dry l-05
ntS/kg dry 2.1O
mg/l 0-0100
mg/l 0.0150
mg/l 0.0050
ng/l 0-0025
mg/l 0.0050
mgn 0.00040
mg,'l 0-0075
mg/r 0.0150
t8-7*6 2,4,6Tib@mophenol 107
Totrt Merrk by EPA 6000/70{0 series Merhods
74399rc Mercury
Totrl Metsls by EPA 200 Series Methods
744G22-4 Sih/er
744-3+2 Arcenic
7,t40+9-3 Badum
7,140{3-9 C€dmium
744{47-3 Chromium
7439-92n Lead
7782-19-2 Setenium
I SW846 747'lA 264,Aa(O7 27-MarO7 7031322 YP
EPA 200.7 2f-Ma(47 27 -Ma'-o7 7031321 HB
SPLP M€trlr by EPA 1312 & 60O0t000 S€rtes Methods
SPLP Extraction Completed
7440-22-4 Silver BRL
zt40-38-2 Arsenic BRL
7.l,l0-393 Barium 0.0236
7rt4o-43-9 cadnium BRL
7440-47-3 Chrcmium BRL
74!9,97€ Mercury BRL
743$92.1 Lead BRL
t82.4s2 Selenium BRL
G€nerrl Chembtry Prrrmei€rs
68.5
'1 SW8461312 22-MarD7 22-Ma(Ol 7031344 AD
1 SW8461312/60108 23-MaAl 24-Mafi7 7031408 LR
1 '
1 "
1 '
1 '
1 SW8461312'470A ' 26-Mar07 7031409 YP
I SW846131260108 ' 24-l\,lar-07 7031408 LR
1 '
SM2540 G l\rod- 24-Mat47 241ta(47 7031463 OP% Solids
Page 5l ,rf 124
Th laborclouepod is Aot t)alid |9llhot t an authorized signsrwe on rhe cowt pcge.
+ Report ble Detection Limil BRL = Belo* Reporting Limir
Page 355
Sample ldeptificationMEF-16 2{'sA595l7-r l
Client Project #30r-88
Collection Date/Timel9-Mar-07 00100
MatrixSoil
Received20-Mar47
CAS Na A^rlrt(s) Flas 'RDL Dilution Llethod Rzl. Prcporcd Analyzed Batch Ar.dysl
Fi€kt €xtracledVolatile Oruanic ComooundsPr€pa.ed by mehod SW846 5035A Soil (lovi, level)76'1+1 1,1,2-Trichlorolrifluoroethan€(FreoFRL
Volrtile OrB.rl. Compo{Ed3
VOC Extraction
psikgdry 6.7pgr€dry 134pgkg dry 6.7
udxg dry 6.7
irdkS dry 6.7
UdkS dry 6.7
IdkS dry 6.7
udkS dry 6.7pdkg dry 13.4
USd€dry A7.2
IS/rgdry 6.7
lSikS dry 6.7
udksdry 6.7pdksdry 3i'.6pdks dry 6,7
lgkS dry 6.7
lgkS dry |3.4
ugkg dry 6_7pdkodry 13.4
ldkS dry 6-7
USikS d,y 6.7
rc/tS dry '13.4
pdls dry 6,7
Udks dry 6.7
ldkg dry 6.7
ldkS dry 6.7
Lrdl(g dry 6.7
[gkS dry 6.7
US/kS dry 13.4
udkS dry 6.7pdks dry 6.7pdkg dry 6.7
t dkS dry 6.7
IS/kS dry 6.7pdkSdry 6.7
ldksdry 6.7
ldlSdry 6.7
ldkSdry 6.7
vdkqdry 6.7
Fdks drv 6.7
UdkS dry 6.7
udkg dry 6.7
USi*S dry 67.2pgtsdry 6.1
!g^S dry 6.7
ldtg dry 6.7pglgdry 87.2
ldkSdry 87-2
ldkg dry 8.7
1
1
1
1
I
1
I
1
1
1
1
1
1
I
I
I
1
1
1
I
1
1
1
t
t
rI
t
I
1
1
1't
1
1
I
1
I
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t
1
1
I
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1
I
1
I
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1
21-Met47 214nEf47 7031261 BD
SW 846 e2608 2ilat47 23]|lat47 7031335 RLJ67{41 Ac€lone107-13r Acryo,nitrile7143'2 B€nz€nel0a€6-l Bromob€nzene7447-5 Brcmochhaomethane7s-274 Brcmodicfih.omethane75-2*2 BrOmOIOrm74{}9 Bromom€thane78€93 2-Butanon6 (MEK)
1Oa-51{ n-Bulylb€nz€n€135-9€{ sec-Butylbenz€n€98{6{ tertSuiylbenzene75-15{ Caabon disulfide56-?+5 CarbontetaacHorid€l0&9G7 Cl o{obenzeoe75.{lG3 qrbroefhane
67463 Chtoroform7rl{7-3 Chlorom€thanes5-49-€ 2-Chlorototuene10€-43-{ zl-Chlorotolu€ne
BRLBRfaRrBRTARLBRLBRLBRLBRLBRL8RLBRLBRL8Rt_BRI-BRLBRLBRLBRLBRL
9Gl2-8 1,2-Dibromo-3-chloropropane BRLr2q€-r Dbromocl{orcmethan€ BRL10&93-1 |,2-Ob.ornoeE|an€ (EDB) SRL74-95F3 Dibromomethan€ BRLs6-sG 1 l,2-Dichlorob€nzene BRLs1.73'1 l,SDictiorobenzene BRfi05-4c7 l.+Oicfllorob€rEene 8RL75-714 Dic.to.odi0uoromethane(Freon12)BRL75tL3 |,l-Dichloroethane BRL107{6.2 l,?-Dichlolehane BRL7t36-.r |,l-DicHqo€thene BRL15C59.2 cis-1,2-Obhloaoethen€ BRL15e60-s lEn91.2-Di* oroethene BRL7847-5 l,2.Oichtompropane BRLr.2-2e4 l,Soichlomp.opane BRL59+2e7 2,2-DichloroDropane BRLfr63-58{ I ,1 Oichlorcqroene BRL10061-{tr6 ds-1.}Diclrtoropropene BRL10061-02€bans.l,$Dichlorop|npene BRLrm-1i4 Ehy'benzene BRL87{&3 tbxac* orcbuhdiene BRLsol.784 2-H€xanone(MBK) BRLg8-82-E l6ogrbpy'berE€ne BRLss€7€ +lsopropyttoluene BRL1634-o4-a M6dryttsrt+ut!,1ether BRLi08-1e1 4-Mehyl-2-p€ntanone(MIBK) BRL?5{+2 Methylon€ chloride BRL
BRL91-2G3 l{aDhthabno
Paga 52 ot 124
This bbotulory rcport is Ed t@d vlthotd sd outhoriz"t signatn oa the cove, page.
* Reporiable DetectioE Limit BRL = Betow ReDorting Limit
Page 356
Sar[ple IdetrtificationM8F-{6 2-4'sA595l7-r l
Client Proiect #30 | -88
M^EixSoil
Received20-Mar-07
Collecrion DatelTimel9-Mar-0? 00:00
CAS No, A^olrte(s) Result Fl"S Uni4. 'RlrL Dilatioa Method Retr Prcparcd Analtzed Bateh Analtsl
VoLllle Orgrnic Compoundi
Volalile Oioanic ComooundsP.€pared by melhod SW846 50354 Soit (tow tevet)103€5-1 n-Propylbenzene ERLi00.42-s styrene BRLen$:D4 1,1,|,2-Tetrachtoroethano BRL79-3+s 1,1 ,2,2-Tetrachloroethane 8RL127-18F4 Tetrachtoroethene BRL10&€a-3 Tolu€ne BRL87€14 l,2,3-Trichtofobenzene BRL12G32n 1,2,4-Tdchtorobenzene BRL71str 1,1,1-Trichloroethane BRL79{r}s 1,1,2-Tricftloroethane 8RL79{16 Tdchlorcethene BRL756€_4 Tdchlorofluoromethane (Fr€on lt) BRLg.FlA{ 1,2,}Trichloropropane 8RL95{3{ 1,2,+Trimethyjbenzene BRL10e{7{ l,3,tTrim€thytbenzene BRL75414 Vinytchloride BRL1330.2G7 m,p.xylene BRL95-17-6 o-Xylene BRL10+99-9 TelEhydrofuran BRL6G2$7 Ethyt ethef BRLs€,Hrs€ Tert-emylrnethy'edler637-92n Ethytied-butytether10&aF Disopropyteher75{5-0 Tert-Butanot/butylalcotlolt23-s1-l 1,4-Dioxane
Surrogde Ecovenes:460004 4-grcfionuorcbenzene
m37-264 TokEne4S
I 706047 4 l,2-Dichloroethane44
1a68-53-7 Abromofruarcmethano
f,xtraotrble Petroleum Hydrocrrbons
ExtractaHe Total Petrcleum Hvdaoc€rbons
Prepared by method SW846 3tt5A
Amffi1-g Gasoline6447em.2 FoelOit#26{1476-313 FuelOit#468s53.{Xr.4 Fuel Oit #6lvl098o0oo0 Motof oilJ00t00o0o Aviation Fuel
Unidentifed
Oth€r Oil
Total Petroteum Hydrocarbons
Cg-C36 Aliphalic Hydrocarbons
Su?Dg6te €cover'€si33Pd-33'2 l-Chlotooctadecene
Samivolrtile Org|nic Compouods by CC
Orqanocfilodne Pesticides SW846 8081A
Pr€pared by method SW846 35508
slg.oG2 Aldrin
BRLBRLBRLBRL8RL
100102110107
Sw 846 82604 22.MarO7 23-MaFO7 7031335 RLJ
BRLARLBRLARLBRL8RL1 ,150Caldllated ast , 1501 ,150
lSftS dry
ldkS drypq/kg dry
udks dry
udkS drypgftg dry
ldks dryyqkS dry
udkg drypdks drypq/kg dry
ldkg drypdkg dty
US/kS dry
ugks dry
IrS/kS drypdks dry
ldkS drypgnq dry
udkg drypdks drypg/kg dry
!s/kg drypdks dryps/ks dry
70-130 %
7G130 %
7G130 %
70-130%
rndkS drymg/kg dryr€,4(g drymdkS drymdks drymS4(S drymdkS drymg/kg drymg/kg drymg/kg dry
40-140 %
6_7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6_7
6,7
6.7
6 7
6 7
6.7
67.2
6 7
6.7
6 7
6 7
6l.2
134
1
1
1
1
1
1
I
l
I
1
I
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1
1
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1
1
1
1
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1
1
l
i
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187 1
187 1
187 1
1E7 1
r87 1
r87 1
147 1
187 1't87 r
107 1
+CT ETPH 22-Mat47 aaMa(O7 7031284 DS
231
rdks dry Sw846 8081A 22-Mat47 27-llet47 7031275 rG
Thh labofttory rcport is not vlid ttlthoqr aI uthori.et ignatarc on the cover p,age
* Reportable Detection Limir BRL = Below ReportinC Linit Page 33 of 124
Page 357
Sample IdentificatiorM8F-46 24'sA595 17-ll
Client Proiect #301-88
Collection Date/TimeI g-Mar{? 00:00
Received20-Mar07
MahixSoil
CAS No. Anabre(s) Ressh Fl"C 'RDL D ttlort Method ReJ, Prcwrcd Amlyed Bdch A,n4'st
S€mivolNtile Org|oic Conpound! by CCOroanodrhdne Pesticldes SW846 8081APrepared by method SW846 3550a319-84€ s€HC319-8t7 b€HC319t'8 +BHCs6{s.e g.BHC (UMane)57-1+9 Chlordane7z-$-a 4,4.oDO (p.C)72.5$9 4,+ODE (p,p,)50.2e-3 4,+DDT (p,p.)€o-57.r Oietdrin95+98€ Endosulfan I332i3{54 Endosutrbn ll1031-07{ Endosulfun Sulfate72-204 Enddn7421.9!.r Endrin ludehyale76-44-8 Heptachlor7243-5 lethoxychlor10?457-3 tbplachlor Epoxide60ot+5-2 Toxapheno5103-71-9 a-Chlordane5s66J4-7 gchlordan€5349+70-5 Endrin Kebne
Surrogaie,ccoyeai6s-_103864+2 4, g+Octafl uotoupherryt (Sr)m51-24.3 Deca&lorobiphenyl (Sr)
Potuchlorinated Bbhenvls bv SW846 8082Prepa.ed by melhod SW846 35454126f+111 PCB 1016111o4-U-2 PCE 122111141-16-5 PCB 1232s3.6e21-9 PCB t24212672,2e{ FCB t248rrrET-Bsn rc8 1254r1@6-s2{ PCB 12603132+??4 rc8 1262ir10c14-4 PCB 1268
Sunogale /Bcovrabs.'1 03864+2 1,4-OB-Oclafr uotobifreny (St)2ost'2$ Decachlotobipheny (54
ScEdvolslit Orgrnlc Compo{rds by crCMS
BRLBRLBRIBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
3180
BRLBRLBRLBRLBRLBRL2 l . 2BRLBRL
4070
BRL
BRLBRL8RLBRLBRL8RrBRL
pgkSdry 6.63
!SI(gdry 6.63
udksdry 6.63
rdkSdry 6.63
rdkSdry 332
ru/kg d.y 6.6i]
lgrg dry 6.63pgtg dry 6.63pdkg dry 6-63
ldkSdry 6.63
ldkS dry 6.83pdks dry 6.63pSfts dry 6.63
lSftsd.y 6.63p91S dry 6.63
Itglgdry 6.63
trdl€ dry 6.63ygas dry 33.2psftg dry 6.63
U€ftg d.y 6.63
USi€d.y 6.63
3o-tg) %361fi%
9SftS dry 13.3
Fgn(g dry 13.3
lSftS dry 13.3
|lgks dry 't3.3
lcrls dry 13.3
ldrsdry 13.3
t gl(g dry 13.3
ldks dry r3.3
IdkS d.y 13.3
3rL150 %30-tg) %
len(gdry 923
lSn€ d.y 923
llg/tS dry 923pSI(g dry 923
Pgkgdry 923
!df(s dry g23
fldksdry s23
ugftgdry 923
SWB46 8081A 22-l,d,(47 27 at47 7031275 TG
SW8l|6 6OE2 22-Met47 24^llat47 7O3t3'13 MP
Semivolatile Oroanic Comoounds bv SWB46 8270CPropa.ed by me0|od SW846 35508A3-32-9 Ac€oaphthene20&96-8 Ac€nqhthy'ene62€93 A$line12+12.7 Antfrac€ne1912{49 Atrazjne10$333 Azobenzerie/DiptEnyldiazinee€7-5 Benzidine5e5S3 Benzo (a) anhracerE
swt46 8270c 2&Mar{7 28+{larfl 7u}1371 M.B2
2
Thb laborcory Eport h nol vali! withart on althorizd sigQatue oE tlp coser page.
. R€porbble Derection Lidit BRL = B€tow R+ortitrg Lidir Page 54 ofl24
Page 358
Sample ldetrtificationM8F-46 2-{'sA595 l?- l l
Client Proiect #301-88
Collection Date./Timel9-Mar-07 00:00
MatrL(Soil
Received20-Mar-07
CAS N^ An ye(s) nesult Fhs Units 1RDL Dilation Method Re{. Prcparcd Anal)1ed Botch Aulrsl
Scmivolatil€ Orgrnic Compounds by CCMS
Semivolaiile Omadc Comoounds bv SW846 8270C
Prepared by method SW846 35508
5G32€ Benzo (a) py€ne
mtse-z Benzo (b) ltuoranthene191-24-2 Eenzo (g,h,i) perytene
207-08.9 Benzo (k) fluoranlhene65{tu Benzoic acidi0G51€ Benzylalcohol1r1-9rr Bis(2dlloDethory)methane111aaa Bas(2.ohloroethyl)ed1€r39€38-32-e Bis(2-clhloroisopropyl)ether1i7{1-7 Bas(2-€thylhexyl)phfialate101-56-3 4€rcmophenyl phenyt ether65-6+7 Butyl b€nzyt phthatate
86-71-g Carbezole59.5G7 4-Chtoro-3-methytphenol106-a7{ 4-Chloroanitine91697 2-Chloronaphthatene95-57{ 2-Chlorophenol7005-72-3 4-Chlorophenytph€nylether
2i8-01,9 Chrysene53-703 Dibenzo (a,h) anthrac€n€132€4-9 Dib€nzofurang$snr 1,2-Dicfilorcbenzene541-731 1,3-Diclllorcbenzene10e.46-7 1,4-Diohtorobenzene9'l€+1 3,3'.Dichlorobenzidine120€3-2 2,,t-Dichtorophenol84{G2 Diethytphthatelel3i-1l-3 Oimethyl phthatate
105{74 2,4-Dimethylphenolw7+2 Di-n-butylphthatate53,1-5?,1 4,6-Dinito-2-methytphenol
51-286 2,+Dinitophenol121n4-2 2,4-Dinilrotoluene606-20-2 2,6-Dinilrotoluene1i7{4{ Di-n-oc{|/lphthalateam-44{ Fluoranthene&7T7 Fluorene11&74-1 Hexachlorobenzene874&3 ll€xachtorobutadiene
n471 tl€xachlororyclopentadi€ne87-72-1 Hexac.hloroethanet9s95 Indeno (1,2,3-cd) pyrenesonz{ 1_M€thytn€phthaleneTESSn lsophorones1574 2-M€tlylnaphthaleness-a&7 2-tl€thyiphenol
106-3s4, 3,4-Methylphenol106-44,591+G3 Naphhalene&744 2.Niuoanilin€99{sz }Nitroanitin€
8RL8RLBRLBRLBRLBRLBRLBRL8RL8RL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRL8RLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRL1,120BRLBRLBRLBRL
BRLBRLBRL8RLBRLBRLBRL
BRLBRLBRL
!S/kS dry 923pg/kg dry 923pgftSdry 923
!S/tS dry 923
IdkS dry 923pS/kS dry 923
!S/kS dry 923
ldkS dry 923pS/kS dry 923
US/kS dry 923pg/kg dry 923
ldkg dry 923
UdkS dry 923
UdkS dry 923pdks dry 923
rS/kS dry 923
!g/kg dry 923pdks dry 923
ug/kg dry 923
US/kg dry 923
rc/kg dry 923ps/qdry 923
Ug/kg dry 923pYr(S dry 923pgtS dry 923
tiSftS dry S23
!S/kS dry 923
!s/ks dry m3
ldkS dry 923pS/kg dry 923pS/kS dry 923
!s/ks dry 923pdks dry 923
IgkS dry 923pdksdry 923
!S/kS dry 923pdkg dry e23
ldkS dry 523pdks dry 923
rdks dry C23
rcAS dry 923
rc^S dry 923
USftS dry 923
Ugks dry 923
UdkS dry 923
UEkg dry 923
l.'dks dry 923
yS4<9 dry 923
tdkg dry s23
lrS/kS dry 923
sw646 8270C22
222222
22
22222222222222222222
222
22222
222222
22
222
Thit laborolory repon k aot ,alid ta,ilhout an utlhorize.l signatare on thc coyer Nge.' Reportable Det€ction Limit BRL = Below Reponing Limit Page 55 of 124
Page 359
Sample ldentificatiooM8F-46 2-4'
sA595 t7-l l
Cli€trt Proiect #301-88
Collectioo Date/TimeI 9-Mar47 00100
MatrixSoil
Received2GMa[-07
CAS No. Analrk(s) Resull Flos Unia .RDL DiIarLrn MdM Retr, Pnpond Analyzed Batch Analfst
Semivolrlil€ O.g lc Compoundr by CCMS
Semivolatile Oroanic Comooonds bv SW846 8270CPrepared by aFlhod SW846 3550810o{1{ 4-Nibo'enilin€9a€$3 NitEb€nz€n€a&7t5 2-Nitoph6nol100-02.7 +Nit'oph€nol62.75>9 N-Nfuosodimehyiamine621€4-7 N-Nihosodi-rFpropylamine86.3{t6 N-Nitrosodiph€rrylaminea7{ss Penta(fibrophenol85{1€ Pienanlhren€108s5-2 Phenol12900{ Pyrene110{61 Py dine12G82-1 ,|.2,+Tdchlorob€nzene
95€5-4 z,4,5-Trichto|oph€nol8s{G2 2,4.6Trichloro,phenol
Sffogate €coMe/resl3?160-8 z+l@robiphonyl
367-124 2+luorophenol
1165{04 Niltob€nzene4s
416542.2 Phq10H5
1fle5r4 lerphony'44
SPLP Extradion
7"KO+24 Silver7,trgl.3&2 Arserlic
71,{0-393 Badum74-rO-439 C€dmium744G.47.3 Chromium7rB9-97S Mercury
743&92n Leacl
7782-4+2 SeleJlium
G€nerel Cbembtry Psram€ten
% Solids
pcrkg dry 3690pgxgdry 923pgkg dry 923pdkS dry 3690
!g/kS dry 923
lgkS dry 923gg/kS dry 923
IgkS dry 923
ldkgdry 923
ldlqdry s23pSil€ dry 923
t dkg d.y S23
ldts dry 923
rcrkg d.y 923pCrkS dry 923
30-1X) %1 ,nO%3t\130 %1r110z!)-130 %1*110 %
rng/kg dry 0.0336
|rrg^g d.y 1.12
mgilqdry 1.67
rE/|q dry 0-558
nEftg dry 0279
tng/kg dry 0.558
ng/ksdry 0.836
d€/kg dry 1.67
N/A
mgl 0.0100
msil 0.0150
mSI 0.0050
rnSil 0-0025
mdl 0,0050
ntgn 0-00040
mdl 0.0075
mSI 0.0150
%
BRL8RLBRL
BRLBRLBRI-BRI-
BRIBRL
BRL|,ssoBRLBRLBRLBRL
1686
122
0.363
BRL
19_7
69.0
0.457
7.42
136
BRL
2
222
2
222
SW846 8270C 23-irar47 2frt ar{7 7031371 M.B
11&794 2,l,6-Ttibrcnophenol 1Og
Total Metab by EPA 6000/7(Al S€rl€s Method!
7439-97€ MercUry
Total Metrlr by EPA 2t0 S€rte! Methods
74/o-U1 Sivel
74arH+2 A6enic
7440-3+3 Badum
7440{}9 C€dmium
71140-47-3 Chromium
7439€2n L€aCl
262-ag2 Selenium
SW6{6 7471A 2A at47 27-N|E,r47 703132. yP
EPA 200.7 -Mar47 274atr47 7031321 HB
SPLF Merab by EPA l3t 2 & 6tXW7000 S.rt$ Merhodl
Comd€bd
BRL
8RL
0.0t 30
BRL
BRI
BRL
0.0 t.t6
BRL
87.4
I SW84613f2 22 1€f47 21nEr47 761344
t SW8461312@104 €.Ma.{7 24-Ma..07 703140€
t '
t "
t '
1 '
1 SW8r1613127470A " 26.t!,lar47 7031409't SW8461312/60108 ' 24-f'rar-07 7031408
1 '
ED
LR
1 Sn425,f0 G Mod. 24411a'47 241nat47 7m146:] QP
Thit labotuory d{o.l is ^ot vslid u,ithou ta oartod@d signihE oE the coter pag. .
. Reporrrble Detection Limi. BRL = B€low Repodilg Limit Page 56 of 124
Page 360
Samole ldenrihcationM8F-17 2-4,
sA595l7-12
Client Pfoject #101-88
Collection Date/Timel9-Mar-0? 00:00
MatrixSoil
Received20-Mar-07
CAS No. Anabte(s) FloS *RDL Dilution lvethod nel Prcparcd A,'dIWd Batch Anobst
Volalile OrSanlc Compo|rtrds
VOC ExtractionVolatile Oroanic Compounds
pSftg dry 61.Spdkg dry 1240
ldkS dry 61.9
Pgn(g dry 61.9
!9ft9 dry 61.S
!g/kg dry 61 9
Ug/kS dry 61 9
rdkS dry 61.9pdkS dry 124pg/kS dry 619
!g/kg dry 6i.9
!s/ks dry 61.9pdkg dry 61.9pS/kS d.y 310pgkg dry 6l Ipg/kg dry 61 IpdkS dry 124
!S/kS dry 61.9pSftSdry 124pS/kS dry 61 9
t gkg dry 6'l .9ygkS dry 124pdkS dry 61.3
FqkS dry 61.9pdkg dry 61.9pS/kS dry 6l-9pdls dry 6r.9
!S/kS dry 61.9
Ud](Sdry 124pgrs dry 61 I
ldkS dry 61.9
UdkS dry 61.s
ldkS dry 61.9pg/kg dry 61 Ipg/kS dry 61 9
PdkS dry 6'l .9
t gkg dry 61.9
t dks dry 61.9
usnq dry 61.9
Udkg dry 61.9
lSn€ dry 61.9pSnq dry 61.9pElq dry 819
lgkS dry 61.9pqkS dry 61.9
lgftS dry 61-9
fdkg dry 619
!g/kg dry 619pdkS dry 61.9
Prepared by method SW846 5030 Soit (high tev€t)7s13-1 1,1,2-Trichlorotrifiuo.oetrane (FreoBRL47441 Acetone BRL107-13-1 Acryjonihle BRLt14t-z Benzene 72.5108-€61 Bromobenzene BRL71-97-5 Brcmociloomethane BRL15-274 Bromodicl oromethane BRf75-25-2 Bromoform BRLzl{3.9 Bromomethan€ BRL7&9!3 2-B'ltanone (MEK) BRL10+51{ n-Butylbenzene BRL135-9€€ s€c.Butylbenzene BRL98.06-0 tsrl€utylbenzene BRL75ts1s.O Carbon disultide BRL5€-23-s Carbon tetrachloride BRL10&s0"7 chlorob€nzefle BRL75{eJ Chloroetrrane BRL67€+3 Chlomform BRL7147< Chloromethane 8RL9149-€ 2-Chlorotoluene BRL106-43-4 4-Chlorotoluene BRLS12.8 1,2-Dibromo-3-chtoropropane BRLu4-4€-1 Dibromochlo(omefrane BRL10€43-1 1,2_Dibrcmoethan€(EDA) BRL74.9+3 Dbromomethane BRLgs-sr].1 l,2-Dichtorcbenzene BRL541-7$1 |,3-Dichlorcbenzene 8RLr0G46-7 ,1,4_Dichlorobenzene BRL7$71-s Oichlorodifluoromethane(Freont2)BRL7$3+3 |,l-Dichloroethane BRL107{6-2 l,z-Dichloroethane BRL75Jt4 l,|-Dichloro€th€ne BRL1S50-2 cis- 1 ,2.Dichloro€fhene BRL15ffi tfans-1 ,2-Dichtcro€then€ 8RL78-07{ 1,2-Oichloropropane ARL'142-28€ .1,3-Ochtoropropane BRL59420-7 2,2-Oichtoropropane BRL5615€{ 1,1-Dichloroprop€ne BRL10061.01-5 cis.1,3-Didlloropropene BRL10061-02{bans-1,3-Diciloropropene BRL100-4i-4 Ehyibenzene BRL87{&3 }bxachlorobutadien€ BRL591-76{ 2-l{eranone (MBK) BRL9€{2{ lsopropylbenzene BRL!19-876 4lsopropyltoluene BRIi63r.04-4 Methyl tert-butyl etfier BRLr0&1Gr 4-Methyl.2-pentanon€(M|BK) BRL7t{)9-2 Methylene chtonde BRL
VOC 21-Mat47 21-Mat47 7031261 BO
Sw84682604 27-MaA7 27-Ma(07 7031602 mar
Field extracted
505050505050505050505050505t)5t)5050505050505050505050505050505050
5050505050505050505050505t)5050505091-2S3 NaphtlElene
Pag€ 57 of I24
Thit laborutory Epod it aot tdid t tithout aE suthori,Fd rignatarc on the cover page .
* Reportabie Det€crion Limir BRI- = Below R€porting Limit
Page 361
Sa.rnple IdentificationMtF-47 2-4'
sA595l7-12
Clietrt Proiect #30t-88
Collectiod Date/Timetg-Mar{? 00:00
MatrixSoil
Received20-Marry
CAS No. Analtta(s) R".rull FW rRDL Dilaion Method nei PnpaQd Arnllzed Beth Anrbst
Vohltl€ Org|nic Cofi pouds
Volatile Oroanic ComooundsPrepared by mothod SW846 5030 Soil (hlgh lewl)t09651 n-Propylb€nz€n€ BRL101X2-5 Styrene BRLS0.20"6 1,1..1,2-Tetrachtorcethane BRL7+34-5 1,1,2,2-T€t'echtoroethan€ BRL127-18-4 Tet?chloro€th€ne 8RL10&84.3 Toiuene 2M87{1{ 1,2,3-T,ichto|obenzene BRL120{2-1 1,2.+Trichlorob€nzene BRL71-5+6 1,'1,1-Trichlofo€thane BRL79{0-5 1,1,2-Trichloroetfune BRL7941-6 Trichloro€thene BRL7569-4 Trjchlorolluoomethan€ (Freon 1l) BRL96-18-4 .1,2,$Tddtloropopen€ BRL9563-6 1,2,+T.inethy'benzen€ BRL10&67$ 1,3,5-Trimethylbenzen€ BRL75{1-4 vinylcf oride BRL13aX!20-7 m,p_xytene 16595-47-6 o-.Xyierie 80.5l0+9S-9 T€trahlidrofursn BRL60-2$7 Ethyt sth€r BRL
Ug/kS dry
rdkS drypgkg dry
ldkg dry
lSI€ dry
lSrkg drypgts d.ypgrs dry
ldks dry
lgkS dry
[dks dry
ugfts dry
lgfts dry
t S/kS dry
tidkg d.y
ugkr drypSAg drypCng d.y
tjc/ks dry
ldks dry
UgtS dry
USn(S dry
ldkS dry
t glq drypS/kS d.y
5 1 . 9
6 1 . 9
61_9
6 1 , 9
61.9
61.9
61.9
6 1 . 9
61.9
6r .961.96 1 . 9
61.9
6 1 _ 9
6 1 . 9
61.S
124
61.S
6 1 9
6 1 . 9
6 t _ 9. 61.9
61.9
6r9t240
5050
505050
50
505050505050505050
5050
Sw 8,46 82608 27-[,lar-0727+rad7 7031602 mar
gs,rcs Tert.amylmetfiylether637-92,3 Edryl lert+utyt €th€ri0&2o3 Di+oprgpylether7s{t0 Tert-Bubnol / buq/ atcohott2+91-1 1,+Dioxane
Sunog€te recoy€res..tiGoo4 +Eitomonuorobenzenem37-2cs Toluone4St 7 0604/4 l,z-Dichlorcethane441868-5X7 Abrononrcromethane
E(Ecrrble Peftoleum HydrocrrbotriExhactable Total Petroleum HvdrocarbonsPrepar€d by method SW846 3115A806{1-9 Gasoline6&+7+30-2 Fuel Oil #26e47fi1'3 Fuel Ol #464s53{0.4 Fuel Oit #6M0980m00 Motor OilJ0ot0@@ Aviaiim Fuel
BRLBRLARLBRLBRL
9910391
BRLBRLBRLBRLARLBRL1.310Calqrlated ds
70-1n %76130 %7G130 %70-130 %
mg/kg dry 350mgr'kg dry 350flig/kg dry 350tn€L/kg dry 350mgr'kg dry 350mgttgdry 350rndkg dry 350nEAg&y 35Omo/kg dry 350nEitg d.y 350
40-140 %
+CT ETPH
unidenlifiedOth€r OilTotllPefoleumHyd@carhons 1,310C+C36 Aliphatic Hydrocadons 1.310
Surrogal€ recovgrios:fia6t.33-2 l-Chlotoocladecene zos
Semlvolirtlle Orgrnic Compounds by GC
Oeanochlorine Pesticides SW846 80BtAPropa.ed by nethod SW846 3550430eoo"2 Ald.in BRL l|g^g d.y SW846 S08tA 2.+ttat47 27,rM6tr47 7031275 IG
This tthoruta! rqort is not volid wlthod an oalhofizd sipoa.re od thz coeer page.
* R€porrable Detection Limit BRL = B€low R€Dorting Linir Page 5E of 124
Page 362
Sample ldentificationM8F{7 24'sA595l7- 12
Clieot Proiect #301-EE
Collection Date/Timel9-Mar-07 00:00
MatnxSoil
Received20-Mar-07
CAS N^ Anattte(s) Result Flag Units IRDL Method ReJ. Prcpand AmDzed Batrh An lst
Semlvol.tile Orguic Conpounds by CCOroanochlorine Peslicides SW846 808tAPrepared by method SW846 355083l+oa€ a-8HC319-05-7 b-BHC319-86{ d_BHC58{$e g-BHC (Lindane)57-74-9 Chtordane72-5,t{ 4,4-DDD (p,p.)72-5+e 4,4-DDE (p,p,)5{F2}3 4,4-DDT (p,P.)60{7-1 oieldrin9599€{ Endosulfan I3321+6&9 Endosulfan ll103r{7-8 €ndosulfian Sutfater2-m4 Endrin7421,93-4 EndrinAldehyde78-444 Heptachlor72.t3-5 M€thorychlor102+57-3 HeptachlorEpoxide€0O1.3+? Toxaphenes10s-71-s a-Chlordane55€6-3+7 g-Chlordenes3aga-nr.s Endrin Kelone
Suflogale 'Etcov€des:
10386842 4,4-DB-Octefluorobiphenyl (54
2051-24-3 Decachlotobiphenyt (Sr)
Polvchlorinabd Biohenvls bv SW846 8082
Prepared by method SW846 3545A
1247+11-2 PCE 1016ltt(]!-24-2 PcB 122111111'185 PCB 1232r,346121-9 PCB 124212672-2S6 PCB .1248
11097{Sr PCB i25411096€2'5 PCB 126031324-2+5 PCg 12621r10G14-4 PC8 1268
Sunogat€ rccoveias:rowa2 4,1-O&Octafl uotobiphenyt (St)
m5t-243 Decachbrobiphenyl (Sr)
Se[rlvolelile Orgrnic Compo([ds by C,CMS
BRLBRLBRLBRLBRLBRL8RLBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL
3356
BRLBRLBRLBRLBRL8RL28.0BRL8RL
5090
BRLBRLBRL
8RLBRLBRLBRLBRL
US/kg dry 6.36pdkg dry 6.36
l./gkg dry 6.36pdkq dry 6.36
ldkS dry 31.8
trytg dry 6.36
UEl$ dry 636pgn(g dry 6.36
ldls dry 6.36
ldkS dry 6.36
Udkg dry 6.36
Lig/Kg dry 6.36
!g/Ig dry 6.36pdkS dry 6.36
ldks dry 6 36pgkS dry 6 36
l,gkS dry 6-36pg/kg dry 31_8
Fq/kg dry 6.36
ldkS d.y 6.36pdkS dry 6.36
30-150 %30-150 %
lqkg dry 12.7
!S/kS dry 12.7
udkg dry 12.7
ldkg dry 12.7
trS/kS dry 12.7pS/kS dry 12.7
!S/kg dry 12.r
ldkg dry r2.7
!g/kS dry 127
30-150 %30-150 %
ldkS dry 1740
FdkS dry 1740
pSrt(g dry 1740
ydkSdry 1740
FgkS dry 1740
pgks dry 1740
ygl(g dry l74O
p94(S dry 1740
t
I
l
1
1
1
1
1
I
l
l
1
1
1
1
I
I
I
I
I
1
SW846 8081A 22-Mat4f 2741a(47 7031275 rc
SW846 8082 22-MarO7 24-Mat47 7031313 l\rP
SW646 8270C 23-[4ar{7 m-[4ar47 7031371 M.B
Semivolalile Oroanic Compounds bv SW846 8270CPrepared by method SW846 3550883-32-9 Acenaphth€ne20e4fr Acenaphthylene62.513 Aniline12G12-7 Anthracene1912-24-9 AtrazineiO$33-3 Azobenzen€/Diphenyldiazine92{7-5 Benzadine5S5+3 Benzo (a) anthiac€ne
2222
22
fhh laboruloq .epott is not valid plthou an salhoied signalarc or lhe colv pagc.
+ Reportabl€ Detection Limit BRL = Below R€porting Limit Page 59 of 124
Page 363
Samole ldentifioatiooMSF-{7 2-4'sA595l7-l?
Client Proiect #30t18
Collection Date/Timet9-Mar47 00:00
MatrixSoil
Received20-Mar47
cAs No- AnaMu(s) F"S l&DL Dilution Melhod ReJ, Prcparud Analyzlr' Bebh Anal$r
Semivoladle Orgatric Conportrd3 by GCMS
Sernivolatile Oroanic Cornoounds bv SW846 8270C
Prepared by mehod SW846 35508
50-32{ Benzo (a) pyr€ne1!+S-2 Benzo (b) nuoranthene191-24-2 Beflzo(g,h,i)p€rylene2OZ{8-9 Benzo (k) fluorenhhene
Benzoic acid10G5r€ Eenzyl alcoho'll1r€r-1 Bis(zrhloro€thory)methane111-4{-4 Bis(2-diorcethyl)€bef35€e324 Bis(2-dhlorolsopropyl)ether117{i-7 Bb(2-efhylhexyl)phfiatate101.563 +BrornoplEnylphefiyl ethel65€&7 Buty' benzyl phhalateE6'ZL8 C€rbazole5s-5G7 4_Chtora.3-methytphenollo€-47{ 4-Chloroaniline91-s+7 2-Chlorunaphthalene9t57-a 2-Chloropf€nol7oo5-72-3 4-Chloropfienyt phenyl ether2t&0i€ Chayseng5l-7G3 Dibenzo (a,h) enthracene132{4-9 Dibenzofuran95-5&1 |,z-DichloDbenzene541.73-t l,lDichlofobenzonerofi6-7 1,+DichloroberEene91-94-1 3.3'-Dichlorobenzidine120{3-2 2,4.Dlchlorophenol84€&2 Died1ytphthalatei3r-11-3 Dimehyl phthalate105-674 2,+Dimegylphenolu-7+2 Di{-butytphthatate534.52-1 4,6-Dioito-2-methylph€nol5l-2s5 2.r|.Dinitropheflol121-1a-2 2,+Oinit'otoluene€oe2G2 2,+Dinitrotoluene117-64{ Oi_n-oct/phthatate206-44{ Ftuo€nthenoa6-717 FluorenetlA-741 HexaChlorobenzene87$&3 Hexachlorobutadiene771f4 l'lexadllorocyclopentadiene67-72-1 tlexadoro9thane193-3+5 Indeno (1,2,}cd) pyrene9Gr2-0 l-Msthylnaphihslene78€Sl ls@horon€91-57{ z-Methynaphthalene95.4&7 2-Methytph6nd106-39.4, 3,4-Methylphenoli06-44-591-20.3 NapfithaleneE8-744 2-Nihoaniline9S.Os-2 $Nitroanitine
SW846 8270C ?3-Mar{7 26-tlar47 7031371 M.BBRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRL
BRLARLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRL2,770BRL8RfBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRI-gRL
BRL
ldkSd.y 1740pgrS dry 1710pgtsdry 1740
ldrg dry 1740
$gv€dcy 1140
ldks dry lf4o
ldkS dry l74O
udkg dry 1740pgr'kg dry 1740
udkg dry 1740
lgkg d.y 1740
FS/kg dry 1740pqls dry 1740pqkS dry 1740pdkgdry 1740
ldkS dry 1740
rdks dry 1740
US/kS dry 1740
tdks dry 1740pdkS dry 1740
tdks dry 1740
lg/kgdry 1740
USftS dry 1740pErq d.y 1740
lgxgdry 1740
ldtsdry t740
ldkS dry r74o
USftS dry lf40
udl(g dry 1740
Pgkg dry 1744
t gr(g dry 1740
ItS/f€ dty l74O
Udkgd,y 1740pSftS dry 1740pqkg dry 1740
Pdkgdry 1740
9d}gdry lf4i
ldks dry l74o
USI(S dry 1l4Opdks dry 1740
rdks dry 1740pdkSd.y 1740
rc/ko dry 17fi
us/ks dry 1740
[dkS dry 1f40
t'dkgdry 1f4opdkg dry t74o
lgkg dry r74O
rgkS dry t74O
IrSftS dry 1740
2
22
2222222
2
2
2222
2
2
2
2
2
2
Thts hbatuorf rcpod is Bot yslid ttitlrord sd a.tthorized signdare oz thz uver page-
. Repodable Detection Limit BRI_ = Betow Reporting Limit P'.Ee fi of 124
Page 364
Samole ldentificationMEF-t7 2-1'sA595l7-12
Cli€nt Proiect #30 t -88
Collection Date/Time19-Mar-07 00:00
MatrixSoil
Received
20-Mar-07
CAS Na An4lyre(s) Resuh F14s Units ,RDL Dilution Method Retr, Prcpored A.ullzed Barch Anallst
Scmlvolrdle Olgroic Compounds by GCMS
Somivolalile Oroanic Comgounds bv SW846 8270CPrepared by method SW846 35508
100-01€ +Nitioaniline
98-9t3 Nltrobenzen€
!t-755 2-Nitroph€nol
10Go?.7 +Nitophenol
i-2-7$9 N-Mtrosodimethylamine
621$a-7 N-Niblsodi-n-propylamine86-30'6 N-Mhosodiphenylamine
074&5 Pentadllorophenolg5{1-S Phenantfirene
10+9+2 Phenol
129-004 Fyrefie
11G641 Flridine
12042.1 1,2,+Tdchtorobenzenegt95-4 2,4.5-Trl$toroph€nol
$-0e2 2,4.&Tricfiloroph€nol
&nro96ta rEcoven€srj2140.8 2-Fluorobipkenyl
36t-12..{' z-Fhtorophenot
4to5j44 Nit Lrbenzentds
416642-2 Phenotr4,
1718-514 Teehenyl4l4
1&7 2,4,6-Ttibrcmophend
BRLBRLBRLBRLARL
BRLBRL
BRLBRLBRL3,260BRLBRLBRLBRL
102919196128101
Totrl Mcl.lt by EPA 60t10/7000 Series M€thods
743&97{ Mercury 0.182
SW846 8270C 23-MaA7 2 Mafi7 7031371 M.B
BRL
10.7
54.7.
0_589
8.64
183
BRL
Comdeted
BRL
BRL
0.0120
BRL
BRL
BRL
0.0261
BRL
s0.9
usn(g dry 6940
usftg '1ry 1140
lrgks dry 1140pSftg dry 6940
lYkS dry 1740pSftS dry 1740
lSftS dry 1740pSftS dry 1740pgilKg dry 1740
lrgftg dry 1740
ISftg dry 1740
lsilg dry 1740
!S/Xg dry l14O
ldkg dry '1740
!g/kg dry 1740
30-130%1s- l 10%36130 %15-110 %30-130 %15-110 %
nE/kg dry 0.0324
mg/kg dry 1.O7
mgr'kg dry 1-61
mgr'kg dry 0.535
m€/kg dry 0-268
nrg!4(g dry 0-535
mgL/kg dry 0.803
rngkS dry 1 61
ntg4 0 0100
mg/l 0 0t 50
mg4 0.m50
ng/t 0,0025
mgl 0.0050
mSI 0.00040
mg/t 0.0075
mg0 0.0150
v.
sw6461312/7470A
sw846131,y60108
222222222222222
SPLP Merrk by EPA l3l2 & 6000/7m0 S€ries Methods
Totll Mearls by EPA 200 Series Mertods
7{40.22.1 Sitv€r
7a4+3&2 AFenic
r44G3$3 Barium
?4.10-13.9 Cedmjum
7440{7.3 Chaornium
143942-1 Lead
882.1&2 Selonium
SPLP ExFacton
744G22-{ Silver
?4403&2 ArEenic
zl40-3s-3 Baaium
7440-4+9 Cadmiuh
744H7-3 c}lromium
743+97{ Mercury
743€-92-1 Le€d
ng21r2 SelBn;Dm
C€tr€rd Ctemlstry PNram€t€rs
% Solids
SW846 74714 26-Ma.-07 27iAa(O7 rO31322 YP
EPA2cn.l 26-Mar07 27-ttar47 7031321 HB
SW846 1312 2-Mar47 221.4a(07 7031344 80
SW84€ 131 0108 23-Mat47 24+lar07 7031408 LR
1
1
I
1
1
1
1
I
'|
1
1
1
1
1
1
I
1
26{raF07 70314m YP
24.lt4ar-O7 7031408 LR
SM2540 G irod. 2+Mat47 24]'4at47 7031463 OP
Thi. laboraaory report it aot volid *irhou dn altthori?pd sigrrzlure ot the coper page.
* Reportable Detection Limit BRL = Below R€porting Limit PaBe 5l of 124
Page 366
Sample IdentificationMtF-4t 2'-4'sA5980l-t5
Client Proiect #301,88
MatrixSoil
Collection Date/Time26-Mar{7 00:00
Received2?-Mar-07
C"4S No, Analyre(s) Result Flas Uaias aRDL Dilabn Method Rel. Prepared Anolyed Batch Anaust
Volrtile Orgaric Compornds
voo Extrlclion 2E1!!ar47 z&Mar{7 7031767 Bo
29{ar{7 29Mal{7 7031790 FU
VohRe Orcanic CornooundsPrepared by method SW846 50354 Soil (low level)i6:13-r l,tl-TricntorotriiuorcethaflelFrcon BFL
BqL
BFL
BFL
BFL
BRL
BHL
BHL
BRL
BRL
BRL
8RL
8RL
BRL
8RL
8RL
8RL
BRL
BAI
BFL
BFL
snLBFL
BRL
anL8RLBRLBRLBRL
BRLBBI.BFLBFLBFLBRLBHL8BL8RLBRL8RLBFLBFLBFLBfrLBRL8RL8RLBRL8RL
107Jll Adylfiitrle71{3'2 Beozenei08-8El ED|IEienzene7+874 Bmoloahlorom€lhaneEn4 BmnFdichloomfEneE2r2 Bro(r)ofoam7|-€3{ Bormmehane?!493 2-outsnone (MEK)
l0+5r{ FE!rylb€nzeoe
135S-8 3€c-Butylbenzeflect{ffi t€rt fuMbenzenet5.r5.0 fulbdl disrltfide
56.23.s Cabont€{rachloid€16407 Otlorobenzsne75{G3 Chlo{o€lhan€5t{&3 Cl orolonn714?.3 CftbDmefiane9$4!18 24 oohluene1643-4 44lioobluene9S12{ l3-Drbomo3{htompropaneIBI-4SI Okqnehloromehanerm-sH j,2-0ibtq'n@thane(EDB)
tLEs Dh.olnor€UlaneE5-5Ol l,2-Dichlorob€nz€ne5,r1-7+r l,Soiciloob€nzene
106{G7 l,4oichlorobenzeneE.71-8 Ddhrudiffuoomethane(Freoni2)7$3,r-3 l,l.Ddooothane107.06.2 l2$Monethane750$4 i,l.Did omethene1566s2 dsl,z-olchloroehene156{lF5 trdt5-l,2-oichloroelhene?&876 1,2-0icto.opropane1{2-2lA l,$Oid oropmpane5s+2G? a2{ichtoropopane$$s8€ t,l,DichiootrolerE10061{1-5 cis-l,}Dhhloropropene1006!{e-€ rans.l,}Dichloropropene101H1-4 Ahibenz€neEr€&3 Hg)caChlorobutadene501-71-t 2-H€!anon€(MBK}s-€e{ boprq}dbeuene1F876 +tsopopyltotu€n€
lEr44+. M€hy'ted-butyledrer
1lFlsl 4- dhy'-2,pentrnone(MtBn7Hrs2 Met|}4€n€ chloide9l-2G3 |hphtt3len€
F€ld exlracted
ljdks dry
pdks dry
!s,4q dry
!4kg diy
vs/q dryvqE dry!0&S dry
tS4(S dry
!s4q dry
|lgnq dry
!S/rS dry
ISAS dry
|Jg4s dry
UglS dry
pVrS dry
!g4q dry
pSeS dry
ldrs dy
tglgt y
pgro &ypS4(S dryldtS dry
pdkS dry
pdlq&v
w)sbl
llqs dry
lgkS dry
9s/}s drv
lEhS dry
!g4q dry
!g/fg d}y
ti9kS dy
ldlrS dy
ldlq dry
!9lS dry
trSfrS dry
psl€ ey
ls^s dry
lYlS dry
pglq dry
!9h ey
lJs4(s dv
pqts dvldlq dq
udlq dvp9t9 dry
lgks dy
r94€ dlvpg4€ dry
voc
sw 846 826086.3
126
6.3
6.3
6.3
6.3
6.3
6.3
r2.6
53_1
6_3
6_3
31.5
6 3
6.3
12.6
6.3
12.6
6-3
6.3
12.6
6.3
6.3
6.3
6.3
6 3
6 3
I ? 6
6 3
6.3
6.3
6.3
6.3
6.3
6.3
6.3
6 3
6.3
63.1
6.3
6.3
6.3
63.t
63.r
6.3
Thk lohorotory rcporl is nol,wlU u,ilhost aa aalho zed signtrue on the coret page.
I R€portabl€ DelEction Limit BRL = Below Reporting Limit Page 73 of 154
Page 367
Sample ldentific.tionM8F-18 2'-4,sA59803-15
Client P.oject #30r -88
Matlix Received27-Mar-O?
Collection DattTime2GMar{? 00:00
CAS No- Analrtz(s) Resuh FloC Anilj *RDL Dilatioa Method ReJ PrepzrcC Anolyzed Bdtch Atutbsl
VoLtilc OrBanic Compo||trds
Vohtle Orqanic Codbounds
Prepar€d by melhod SW846 5035A Soit (tow tevet)
l0+nt1 |}Prcpyt6'uone 8RL100.126 slyreno Bfudrc2r}6 j,t,t,2-T€lrad{o.o€thar€ gRL
79346 1,1,2,2_T€trad{oro€tt6ne BfiLt2f-184 Tdrad olo€hen€ BFL10e€8.3 Toluene BRLl)761-6 12,&Trit orobena€h€ 8RLrz0-€?r 1,2,+Tid orob4nzen€ 8fu715s 1,1,1-TridJorootllane 8RL?r-o'-5 l,l,2.Trid oro€dwE BRL
|4t{ dV
|lgrs tr}'pgts dry
Elq dy
ug,lq dy
uSIq dy
|lgrsf}
tr9*0 &yu€n4d/|l
uCts dy
abdyligkg dy
l|gls try
are dy|4/l€ dy
|'glqdy
ldks ry
lgrq fvpdrs dy
l&tqdv|Etqdrylglq dy
!S/rq fy
t€^g dy
lElq dy
7Ut3074130%TGIN%70.1il %
mdkg dwn'g4q drytrqr€ dryngnq dryflVfg dwn'qtS dyrngh 6yngnq d'y
lrqlq dry
.'19frq dry
&.144 %
st/'l8{6 &b(8
€T ETPH
6.3
6.3
6l
6 3
6.3
6.3
6_3
6l
6 3
6.3
6.3
6-3
6.3
6.3
12.6
6.3
63.1
6.3
6.3
6.3
6.5
63.1
1 X
I
I
1
1
I
1
1
1
1
I
1
1
1
1
1
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1
!
I
I
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1
1
29{,tar{7 29-tlar{7 7031790 RU
?94r{ rddtbrc€tEfla7t69-l Tftfttomfiuoromohane (F€on I i)9610-{ 13,}Tdfbopropane
503.6 12+Ttime$ylbenzeneros5./-o l,3sTrimeryt€naene75{l-4 Vinyl dllolilj€1SG2G7 |rtFxylorp95-47-6 o.xyl€ap10s!qs Tdr*ldr0|u|an
crz+7 Etd stter9s44+0 Tedffryl mehyi ether63r{2,3 Ery bn.h(nyt olterr00-m.3 D-ijoproprt dt€r6{5-0 Tei€utaml/ buly{ alcohol123.91-1 l,4{ioxan€
@-oo-1 4-Bronor(]oobonzere
ag7'?6 5 ldueft$
1/u6oat4 1?.Dktiddt1Ere44
le6e-5r7 DMbtonekae
Ertnctable Petroleum Hydrocarboos
Extaclabie Totd Petd€um tMrccadons
Prepared by method SW84.6 35508
mo€-c1€ Geii|e6r4763tr2 Fud Oa $268476.31.3 Fuol C{ #46055340-{ Fuel0llt6
[{E&looo MoWOI,x10100m0 Atiatim Fu€t
t d€itlied
Otl€r Oil
Told P€trdelm Hy(kaartms
Ca{sE lldlaitc l{.rdisattons
Su/rqgare Ealroibis&*2 lctddl@bcdE
Semlyohdl€ Orgrllc Compounr|l by GC
Organod otin€ Pedtcijes SW8,46 8081 A
Prepared by method SW846 3545A
ff{r,'z Aldin
BFL8Rr-8BLBRIBALBRL8nLBRL8ni-881BRLBHL8Rr-8RtsFt-
1011t2117tw
8RL
Bfu
BRL
B8L
BFL
BRI.
BRI.
BRL
BNL
BAL
7.0
7 0
7.0
7.0
7.0
7 0
7_0
1 0
7 0
7.0
2g{,1€r,07 3OMar-07 781/t3 DS
|dlq dv sw8$ SmtA 28-r&r.07 @.4pr.07 7t61739 IG
This laborotorf Epo.a ls ,rol vdjd *lrhou sn surtoriz.d slgtutla.e oa the cover page .i Repo@ble Deterrioo Limit BRL = B€tow ReDortins Limit Page 74 of 154
Page 368
Sample ldentificationM8F-48 2'{'sA5980l-15
Client Proiect #301-88
MatrixSoil
Received
2'l -Mar-01Collection Date/Time
26'Mar{7 00:00
CAS No. Anrqte(s) FIag *RDL Dilutioh Mertod ReJ. PrcparcJ Analyed Buth A tltst
Scmlvolrtile Org ic Compounds by cC
ooanodhrins Pesticites SW846 8O81 A
P.€paEd by m€thod SW846 3545A
3r$846 +8t63r$857 b-BHC3190&6 dBuc58-s+e g_BHc (undanel
t7+9 Chtodane12.51-8 4,a-O00 @,p')7266.s d{'-DDE (p,p,)
sc?$s a,{,OoT h,p,)m'5-f'r Dleldins50-€€-8 Endogllfan I3s213ffi Endosulfan lli(B1-07{ EndcdlanSllfate72-20.0 Endin?121_93-1 EndinAHehyde?6.44_0 H€fltadtlort2,4C5 Mefidyd or10r+r3 Hsdedltor EFoidestD1.352 Toxaph€ns51@?1€ act{odflls566&347 94 orda6s14{.7o5 €ndrh (6lone
r@t1-2 44-DE-&Efruorcbiphenyl(SlM1.2ai De'tsEhlotobiplEnyl(So
Pqlvcr{ofiated Biohenlh bv SW846 8082
Prepared by method SW846 3545A
!267+11.2 PCB 10161110420.2 PCB 1221nrrt-tos PcB 1232!,r@2r'9 PCg 124212612.2$6 PC8124811097{S1 PCB 1254110€68e.5 FCB 1260rteL&s PCg 1m21110G14.4 PCB l26E
1@t6aa2 4,1D&Odatuorobipheny'(3t)
ffi114.3 b@dlot6phsjyl(64
S.ftlvolclile Orgrnic Compounds by GCMS
S€mivoladlo Ooaic Compound6 bv SWP,46 8270C
P.epa.ed by m€Olod SW846 35508
8332.9 Aconaphhone?0&*{ Acoiaphbyl€n€6e$.! Anihn€12L12-7 ,4afiaecsn€1912.24€ Alrazjne1q!$-3 AzobenzeneDiphenyldiazinesiET{ &nuidns56-ss3 &nzo (a) aa$.acene
p.4 Ip,4 Ip a 1
:2,r 1
162 1
24 1p A 1
p1 1p_4 1p.4 1gzl Ip 4 1p t 1
p a l
p.4 r
32.4 {p.4 |
162 I
9..4 1
32.4 l
e.4 |
8FL
BFL
BFL
BFL
BFL
BFL
BFL
BFL
BFL
BNL
BRL
BFL
BFL
BFL
BFL
BffL
BRL
8RL
BFL
8RL
8fl1
NkSdrlpS4€ dry
wtqoy
lEtq dry
|,s4(s drytS.l(g dry
|dksdrv
usks dry
|JgkS dry
pgkg dry
tgtS dry
|Jgfrg dry
llg4s dry
l,s,ks dry
!s'lq dry
@k9dryp4rs &y
pgKg ory
pgks dry
us,4(sdry
Ms&y
tu150 %
3,150 %
tlgks ray
!S,kg dry
[S,lq dry
p(ylq ory
pq'q qry
pdk4 dry
!94q dry
psh dry
ldtS dry
3+150 %
il.l5t %
swe,16 808tA
sw846 8082
sw846 8270C
2&Ma47 tz-Aptlt /0i179 IG
28-|'/,ar07 3Gilar{7 7031738 Sl',
29-Mar47 09Apr-07 7m1774 M.B
51
76
55
60
64.9 1
64.9 I
54.9 1
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64.9 1
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643 1
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BRL
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874
874
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8r4
871
874
874
674
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ORL
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8RL
BRL
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lsnq dy
!S/rS drypglq drypdks drypg/lg dry
fS4€ dry
us,ls ory
tigtS dry
Thb lahoratory rcpofl b not wlid withou! an aathorized signalsrc oa tht .oeer page.
+ R€ponable Detection Lirnit BRL = Below Reporting Linrr Page 75 of 154
Page 369
Sample ldedtihca tiotrMEF48 2'-4'sA59803-15
Client Proiect #30 t t 8
Collectioo Date/Time26-Mar47 00:00
MafixSoil
Received21-Mar-07
CAS Na Aialyte(s) Fl4S *R.DL Dil ttion Method Rel, Pnpored Analfzen Ba,ch An4lfsa
Semivolatile Org.nic ComFounds by CCMS
S€mivolatle Oroanic Comoounds W SW846 8270C
Prepa.ed by method SW8,l6 35508
5one{ B€nzo (a)py€n€205-93.2 Benzo(b)fl|,anfi€ne1s1-2+2 Benzo(O,h.i)p€rytene207{8-9 B€nlo E) nuoEflhene6S850 oenZoiC acid10G5r.6 BsW atcohol111.!r1r Bis(2-chbroelhoxylrnetEne1114-1 gs(2dtofoefiyi)sttFr
3S€e324 EI5(2dOolsoFEpytle{|e'1t7.81.7 Bis{2{ht{h.dy0phlhatabr01-5s.3 4€rqnoph*vphffytetEf85,6&7 Buty h€rr4i phthahblF74{ Caft€rol€s9{}7 .t-cflo|'o-3-|nellrytdrdtol
10F47-B 4ctdoros linesr,ss7 zcllduBphfialene9$t{ 2$bophenol70572-3 lChbophffyj phenyt sh€r21&01.9 Cnays€n€s$1I3 ofr€fuo (Ah) anhEc€ne132-6,t4 DibenzoluEn$-so1 l,2{idh.abenrenB5.11-7+1 l,3[IdorobeEene16{+7 l,4Dd robei?ene91a41 g,3..Dchhrobenzidne
1Al-€+2 2,4.Didorophend8166 2 Diettrylphhdat€131.113 Dmelhylpnhalab105.67.!1 2,4{ilr|€q&h€nol*7+2 D-n-butyl phhahte534.52r l,SDinitD2fl€fltlphend5r{&5 2,4.Dnihophenol121.1+2 2,4-Unikdotr€nqoGrD2 2,6.0idtrolotu€rE117{.4 D+odyl phtEtate206-4411 Fuor3ntEnesSXt-7 Ffuo|En€1M+1 HexadilorDbqrzeneo{€a? Hexaciloohbdeno.r{r_4 Hexadoocydopeitadi€n€6r-T2-1 H€rad ooetmmrs!-9si lndem(1,4d)py@nost2{ !_f dnyl6ph$Etsne7l{$1 lsapho|ono91{7-6 2.lrohytmphdElelroe6-{&7 z{etrylphsd
108.!$4, 3,4+rdhtphoidr06r!L591203 ilapht|atqlew1+1 2.Nibofltinesos2 SNitoanilne
BRL
BAL
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8fi1
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8HL
8RL
8RL
8nLBNLBFLBFL8RLBRISRLBNLBFLBRL8RL8FLBRIBRLBFLBRL8RL8Rr8RLBntARLBnIBBL
9fll-
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8RL8RLBRIBNLBRLBBLBRLsfl.
8RLBnt8FL
I
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lglqdy 871
wlg try 874
pd*s ev fi4
db dv 871
US,lqdy 871
$ctgdry 814
ldhtrV a74
l4kg dry a74
|dt! try tt{
lrytS dy 871
gglqdy 871
dtg dy a74
dE fy a71
l4k! fy a74
l4ts dy 874
!9lqdy 874
wrg dy 874
ldrq fy a74
ldrg dy 87,1
t446v a
dh dv E71
lg4qdy 874
tdLSdy 874
!S'kS try a74
t4ilS fy a
Wlq fy a74
dlq dy 871
Igflqdy 514
pdks dy 874
tMg dV 871
sS*S dy 874
pgtS dy 874
ldb 6y 874
$,{q dy 874
ldks dy 874
lSitS tr)' 874
!S^S dry 874
wlgdry a74
!S4€dy 871
ugfqdy 874
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tryxs d) €74
!g/ig dy O4
pdl€fiy 871
lgnqdry 874
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lcrs fty 814
wl.gd''t a74
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swB4€ &270c A.Illtar.07 o&AF{i 7llB1 z4 til.B
Thit laboratory Eporl it nd wlid wirhou aa ruhorded s,gnolar. oB thz cover psge.
+ Reporbble Deteqion Limit BRL = Bdow Repoding Lirnir Pag€ 76 of | 54
Page 370
Semole ldentificationM8F-48 2'-4'sA59803-15
Client Proiect #l0l-88
MatrixSoil
Receivcd2'7 -Mar-07
Collection Date/Time26-Mar-07 00:00
CAS No. Atslyte(s) Resull n"s Unils *RDL Dilation Method Rel: PrcF.el Anauzed Batch AtuIjtt
Sehlvolrtlle Ory.nlc Compounds by CCMS
Semivoktile Orqanic Coooounds bv SW846 8270C
Prepa.ed by method SW846 35508
t00{1{ +t{itroanjhsl$gl3 i|ilrcb€flzeno8&7rs 2-tlitoph{El100&-7 +Nifophflol6e7$9 fl.Nitrosodmethylarnine@14-7 &Mtoso&n-propylaffie8+30j N.Nitosodphenylamine8?.t&5 pendiorophenol
8541{ Phendlhrene10&9t2 Ph€nol1?3{04 PyEn€110-861 q/ndne
1!182-1 li,+Tichlorobenzenes54i-,t z,4,tTditomphend8&os2 aa,FTrKfilobphenol
,r?1{0{ zawebhalyl
fi7-124 z-fr-bqlard
1t65{'4 llifrofu1zflN4s
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t7t85t4 TerptEnyl-dl4
118-194 Z4,FTtbtonophenol
s!1i84€ 8270C
sw846 74714 02-4U47
2gl,lar 07 0&ApF07 ?031774BFL
BFL
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BNL
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8RL
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BRL
8RL
57
72
62
76
lgeS dry 35m
|SAS dry 874
l4ks dry 871
$eS dry 3500
!s^s'1ry E74
UdkSdty 874
lgftS dry E74
!S.4$ ty 874
!0AS dry 874
IS,4q lly 874
,r9ftS dy 874
lglq cty 874
pdkS diy 674
!Sr1q ory 814
pdrs (ty 874
i&134 %
11110%
3+130%
15,t10%
3+|fr %
t 1 1 t 0 %
mg4(S dry 0.0:33
mg/kQ dry 1.11
mC.4q dry 166
mgks dry 0.555
nS/kS dt! 0.277
mdE dry 0.555
rdrg dry 0.832
mg/kg dry 1.66
mg4 o.o1o0
rngn 0.0150
mg,l 0 0050
mM 0.002s
mgl 0.0125
mgil 0.00014
mql 0.0075
rng,l 0.0150
M 8
Totsl Metrh by EPA 600{l/7000 Serl6 Methods
SPLP M.rds by EPA Il12 & 6000t000 Serler Mefiod!
7139.9?4 lt€tulry
Totrt M€tsls by EPA 200 Series M€thods
7140P4 $lvel
14&&2 AFeflc
7140-39-3 Batiun
7140..C9 Ca&dtjn
7!r{!t7,3 Clhffinium
7439.t4.1 Lead
nP2.4sz Sds !m
SPLP Eftastion
741021 glv€r
74,$138-2 AFenc
7il4&S3 BariLm
7a,4049 cadni|Jn
741l|{13 Chromium
7<q974 tilomry
74$92n [.eed
7tQ1s2 Sd€nium
Gcn€trl Ctcmlstry Pr.&m€t€rs
8RL
BFL
3.43
393
0.871
10.4
28
BFL
EPA2M.7 02-&r{7
Compleled
BRL
BRL
0.0150
8RL
sw846 1312 28-l'lar{7 2&Maf{7 7031763 8D
sw846 t3rz6010B 30-MaL07 02-!{rrl7 7031805 LB
Sl{846131a7470A ' @ Aprc7 7031806 YP
SW846131260108 02-Apr{7 7031805 tt
BFL
BffL
o0210
BHL
% Solds SM2540Gitod. 30-{lar{7 3&Marfl 7031879
This labamlory .epod ie nol wlu niahout an aurtorized signature on the cow, p{ge .
r Reportable Detection Limit BRL = Below Reporting Limir PaEe l'7 of 154
Page 371
Sample lde ificationM8F-{9 ?'-l'sA59464-06
Cliept Proiect #301-88
MatrixSoil
Coll€ctiotr D6te/TimeI 5-Mar47 00:00
Receiv€d19-Mat07
CAS No. Arralrtz(s) Resdt Fl4e ani6 'RDL Diluio,' Mdhod Rq tueparcd laalyen Bdch Atatl'st
Voladl€ Or$$k ComDo$ndt
VOC Enraction Field extraded
uS/kgdry 4-5pgkSdry S0.9
ugkg dry 4.5pClgdry 4.5
lSfiS dry 4.5
rdkS dry 4,5
rdkSdry 4.5
ugr0 dry 4.5pdkgdry 9.1
Ugn(gdry 45-4
Usn(g dry 4.5pS/kSdry 4.5
lCASd.y 4.5pdrsdry 22.7
US/kS dry 4.5
ldkS dry 4.5
ttgtlxsdry 9.1
rqlgdry 4.5
Pdkg dry 9.1
!dl(g dry 4.5
!Sn(S dry 4-5
rcnrg dry s-1pS/kS dry 4.5pdks dry 4.5
ldkS dry 4.5
Igl€ dry 4.5
ldkS dry 45pSilq d.y 4.5
uglg d.y I I
ldkS dry 4.5
!S/kS dry 4.5
ldkg dry 4.5
WkSdry 4.5ySAS dry 4.5pdkg dry 4.5pc4Qdry 4.5
lgkSdry 4.5pdkS dry 4.5pgksdry 4.s
t S,/kS dry 4.5
udkS dry 4.5
ldkS d.y 4.5
t g|!g d.y 45.4pgtgdry 4.5pdkgdry 4.s
ldkS dry 4.s
ldkg dry 45.4
lgkg dry 45.4ps/ks d.y 4-5
m.Maf{7 m-i[x07 7 031156 ADVolatile Orqanic ComooundsPrepa.ed by method SW846 5O35A Soil (low levet)76-13-1 1,1,2-Tddorotrifluorcetftane(Fr€oFRL674+1 Acelono BRL107-13-r Acrl'lonitile 8RL71'112 Benzen€ BRL108-05r Baoinob€nzene BRL14'w'5 Brctrmahloromelhane BRL75-271 Bromodicfiloromethane BRL7+24ts2 Bromofo.m BRL7r€99 Bromornelhane BRL78-e'3 2-Butanone (MEK) BRL104-s1{ FButylbenzen€ BRL13s€8{ sec€utylbenzGn€ BRL98{t6{ tBrl€utylbenzene BRL7t15-o Ceftondisulfde BRL56-?$s Cafuon tefachlonde BRLt0E-90-7 ChloDbenzefle BRL75{G3 Chlooethane BRL676G3 Chtorobrm BRL74€71 Chlorom€thsne BRf9s-49{ 24hlorctoluene BRL1ftr-43-4 +Chlorotoluen€ BRL9G12-a 1,2-Dib{ome3-chtoropropans BRL12{-44.1 Dibrornochlofodn€tEne BRL1c6-s3-4 1,2-Oibrono€tharF(E08) BRL7+913 Oibromomethane BRL9s-5,01 |,2_Oichlorobenzene BRLs{1-7}1 l,3-OiclronoLbenzene BRL10&6-7 l,r|.Dichlomb€rEene BRL7r71-A Dichlorcdifuoromethane(Freonl2)BRL75-34-3 |,l-Dichlorcethane BRL107{6-2 l,2-Dichlorcothan€ BRLz5<)5-4 1,l-uichtoroethene BRLr5s5g2 cis-1.2-Dichtorcethen€ BRLt5eq)-5 tEns-l.2oichtoroethene BRL7a{7-s t,2.Oichlo.opropane BRL142-28.9 l,Soichloropfirpane BRL50+20'7 2,2-Oichlo.opropene BRL56!5s€ l,l-Dchtoroplopene BRL1006r{1€ cjs- l,}Dichloropmpene BRL10061{2{ trans-1,3-OichloropoFene BRL10041-4 Edlylbenzene BRL07{6+ Hsxad orcbutadiene BRL5s1-7e{ 2-l-loxanone (MBK) BRLsa{2{ lsopropylb€nzene BRLss-€74 +lsopropyltoluene BRL1634{4-4 Mettt'l tert-b{tyt ethe. BRL'10s10-1 +Methy-2-pentanonelMlBK) BRL7s{92 Methyten€ .htodde BRL
SW 846 S?60S 21{nar-O7 22-Srar-O7 7031233 TR
9l-2()-3 l,laphthalene
Page 2E of 152
th& latotuloq r4,s'l b uot r'y'i l uitttotl, on strto;zcd sigfista.e on thz cov.r. page-
* RQortabl€ Det€ction Linit BRL = Below Reponing Limit
Page 372
Samole IdeutificationM8F-49 2'-4'sA594&t-06
Client Project #301 -88
MatrixSoil
Collection Date/Timel5-Mar-07 00:00
Received19-Mar-07
CASND. Analfu(s) Flag Unils *RDL Diltltion Llethod R.I. PrcFa.ed tumllzed Ba!4h AnoDst
Voldle Orgrnic Compounds
Vohlil€ Oroanic ComooundsPrepared by method S!V846 50354 Soit (low tevet)'t03stl rFPropylbenzene BRLi0G42-5 Styrene ARL630-20{ 1,1,1.2.Tetrachloro€than€ BRL793{-5 1,t,2,2-Tetrachloroethan€ BRLrz7-rs-a TetEdilotoediene BRLl0S€0-3 Toluene BRL87{r{ 1,2,}Tridtlorobenzene BRL120{2-1 1,2,+Trid{orcben2ene BRL71-55{ 1,1 ,.1-Trichloroethane BRL79411.5 1,1,2-T.ict o@elhane BRL79{1{ Tdciloroethene BRL75{s-4 TridtlQrofluorornelhane (Freon 11) BRL9Gr8-4 l.2,}Trichloropropane BRL95{xf6 1,2,+Trimethylbenzene BRL10e67{ 1,3,5-Trimethytbenzene BRL75{14 Vinyl cfiloride133G20? m,p-Xylene9547-€ o"Xyl€nelo$Sq4 T€trahyd.ofurdn
@-2S7 Ethyl 6h€rs€,l{s4 Ten-ahyl m€lhyt etl€r€,3?-s?-3 Ehyltert-butytether10e20'3 Diisopr0pylether75-65{ Tert-Butanol / butyl alcohol12+91-1 l,+Dioxane
Su'rogats rBcowrtss:460-ao4 +BrcnofluorotEnzene
N3/-26-s foluene4g
t 106.0474 1,2-Dichlorcethan6-d4
186A-53-7 Abronofluarcmethane
E{reclrbl€ Peiroleum Hydrocaft ons
Extraclable Total Pet.oleum Hvdrocarbons
Prepared by method SW846 35508
800661€ Gasoline68476-30-2 Fuel Oil #268a7B3i-3 Fuel Oil #46&55$0G4 Fuel Oil #6Mm{Doo{I} Motof OilJOoloOooO Aviation Fuel
Unld6nliti€d
Orher Oil
Total Petroleum Hydroc€rbons
C9-C36 Aliphatjc Hydrocerbons
s{rrogsf'g rEc9Msniesr
$a6-33? 1-Chlooocladecane
SemlvoLlllc Orgs|lic Compo{nds by CC
Orqano€f orine Pesticides SW846 8081A
Preparcd by mehod SW846 355083090G2 Alddn
BRLBRLBRLBRLBRLBRLBRLBRL8RLBRL
9610110898
8RLBRL8RLBRLBRLBRLBRLBRLBRLBRL
u
pg/kg dry 4.5
wKg dry 4.5
tiSftSdry 4.5
pS./kg dry 4.5pgkS dry 4.5
trg/kg dry 4.5pg/kg dry 4_5
tis/ks dry 4_5
us.ixg dry 4_5
t4Jxgdry 4_5
t4iKg dry 4_5pg/kg dry 4 5
lrg/kg dry 4 5
!g/kg dry 4 5pdkS dry 4.5
t€/(S dry 15
tdkS dry I 1
FSikg dry 4.5
WkS dry 45.4
pSikS dry 4.5
t S l € d r y 4 5
PdkS dry 4.5
pq/kq dry 4.5
pg/kg dry 45 4
pg/kq dry 90 9
7G130%
70-130 %
70-130 0.1
/0-1n %
mg/kg dry 17_2mgn(g dry 17.2mryig dry 17.2mg/kg dry 17.2mgLikg dry 11.2mdkS dry 17.2m9k9 dry 17.2ftq*.S dty 17.2mg/kg dry 17.2fl|gftS dry 17.2
40-140%
I
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SW 846 82608 2t.Ma'.07 22nna47 7031233 TR
+CTETPH 21-MarO7 21-M^t41 7031167 DS
t dkg dry 5.14 SW846 8081A 2O-Ma(41 25 at47 1031068 TG
Thit laborcory repod ir noa wlu w hout an suthorhel signatun on the cowr page.
* Reportable Detection Limit BRL: Below R€po.ring Limir Pase 19 of 152
Page 373
Sample ldeEtificationMtF{9 2'-4'sAs9,t&L06
Clieot Proicct #301-88
MatrixSoil
Collecrioo Dater'TimeI 5-Mar47 00:fi)
Receivedl9-Mar-t)?
CAS No. l,raws) Retall FI4g A l l , s *RIrL Dllalian HaItod Retr, Prepor.4 ,lrslfud Barch ,lnawSemivoladle Orgaric Compounds by CC
O.oanochlorine Pesticitres SWB46 go8tA
Prepared by liethod SW846 3550831e{46 s-Bl{C31e{57 b_BHC3r9&r€ d.BHCs6{$9 g,BHC (Lindane)5/.74-9 Ct{qdan€7244s 4,+DDD (p,p,)?2€5-e 4,4-DDE (p,p)50-2+3 a,4ODr (p,p')6t -s7.1 Dieldrins5s9o€ Endosulfan I33213r-€$9 Eodosulian ll'103r-07{ Erdosulfan Sutfate72 -2Ga En&in742r{$a Endrin Ahehyde16,{44 H€ptschlorf24rs tir€horycflor1021-57-3 H€ptaclrtq, Epoxide800135-2 Toxaphene5103.7',1-9 a-Orlodane55663+7 +Chlordane*r4!r4705 En&in K€t no
Szr'og6le aecovsriies,'1 $8ea+2 4, 4OB4detutorodphenyt ( Soz05r-21.3 De@diorobiphenyt (SdPolvchlorinated Bioh€nvls by SWB46 8082Prepsred by mehod SW8rt6 355081267+11_2 PCB 10t6111044.2 PCB 122111141n6-5 PcB 1232s346+21€ PCB 124212672-294 PCB 124811097{91 PCB 12541100€-82a5 rcB t26O3f12+2+5 PCg 12621110{}14-4 PCB 126a
S|,TEgaia rgcor/a'tesr1 tEF*a+2 4,tto&Adaf, mrobiphenyt (s4ms1-243 De@c'l,tombiphenyt (Sr)
SeEivokaile Orgritc Codportrdr by GCMS
BRLBRLBRLBRLBRLBRLBRLBRL
6RLSRLBRIBRLBRLBRL8RLBRLBRLBRLaRtBRLBRL
407/
BRLBRLBRL8RL
BRLBRLBRLBRL
40
ldkS dry 5.14 1
tdkg dry 5. 14 1
pdkg dry 5.14 1
ldkS dry 5.14 I
ISftg dry 2s.7 I
l|gikg dry 5.14 1
pglgdry 5.14 1
ldkS dry 5j4 I
IdkS dry 5.1,1 1
Igikg d.y 5.14 1
lgfg dry 5.14 I
ldkSdry 5.14 t
$S/kS dr, 5.14 'l
Fg/|(g dry 5.14 1
pdxg dry 5.14 1
ldkS dry 5.14 t
tgkSdry 5.14 1pgifqd'y 25.J 1
PqXg dry 5.14 1
!rytS dty 5j4 I
ldkg dry 5 14 1
3L150 %
3L150 %
SW846 8081A 20-Mar{7 z5-lrar{}7 7m1068 TG
SW846 8082 22J,,,a147 244 at47 7031274 Mpt gl€ dry 10.3
Lrcl€ dry 10 3ydkSdry 10.3
udrS dry l0 3pgtS dry 10.3
US/kS dry 10 3
|lg4€ dry l0 3pSftSdry 10.3
Pdkg dry 10.3
30'150 %30-150%
Semivolatile Orqanic Compounds bv SW846 8270CPrepared by mehod SW846 35SOB63.32{ Aoenaphthene208-gG8 Aconehtrylen€62{}3 Anitino12G12-7 A|rU1|ECAn€1912-2+S AEai,trF10&313 Azob€rizenoy'Diphenyldiazinev47-5 B€nzldin€56-5t3 Benzo (a) anthracen€
aRrBRLBRLBRLBRLBRI-BRLBRL
pdlq dry
ldkg dry
ldq drypS4€ d.y
FgkS dry
rdks dry
ldlg drypdlq dry
427 1
427 I
427 1
427 I
427 |
427 'l
427 I
427 1
sw846 8270C 22-ltat47 2+Ma(47 7001278 M.B
This bnodoe rapad i| Eor vslitt fr ho( on aartorized signaure o^ tlE cov.r page.r R€ponable Detectio0 Limh BRI = Below R€ptrting Limit Pag€ 30 of 152
Page 374
Sarnple ldentificationM8F.19 2'-4'sA59464-06
Client Proiect #301-88
MatrixSoil
Received19-Mar-07
Collection Date/Timel5-Mar-07 00:00
CAS No. Arlalfu(s) F|AS *RDL Dilatioa Method Rztr Pnpared Analfied Batth AnalDt
Semivolriile Orgsnic Compornds by GCMS
Sgmivolalile Oroanic Comoounds bv SW846 82ZOCPr€par€d by method SW846 3SS0a50-32{ Benzo (a) pyrene20tgq.2 B6nzo (b) fluoranthene191.2+2 Benzo (g,h,i) perytene207{8.9 Eenzo (k} fiUoranthene6545-0 Benzoic acid10G51{ Benzyl alcohollt1-91.i Bis(2-chtoroethoxy)methane1llaaa BiB(2<hloroethyl)ether3S63&324 Bir(2-chloroisopropyl)ether117S1.7 8is(2-€urylhexyt)phthalate10155-3 +BrornoFhenylphenyief|ero6{s7 Buq/| benzyl phttlalate86-7,1{ Carbszote5s5G7 +ChtorD-$methytphenolt08-47€ 4-Chtoroaniline91.5&7 2-Chtoronaphthalene95-57{ 2-Chtoophenol700$72'3 +Chtorophenyt phenyl ether21eO1€ Chaysen€53-7G3 DiberEo (a,h) anthracener 32444 Djbfizofurarl95-5Gl 1,2-Dichlorobenzenel'41-I$1 1,3-Dichlorobenzene10s€-7 1,+Dichlorobenzene91.9+i 3,3_-DichtofoberEidine121!832 2,+Dichtorophenol844&2 Disthytphthatate131-11-3 Dinr€thy'phflratate10S74 2,+Dimettrytphenolu-7+2 Di{-butytphthalete$4-s2n 4.6-Dinito-2-m€thytphenol51.2+s 2,4-Dinkoph€noli2t-14+ z,4-Dinitotoluene60F2G2 2,6:Dnib|ololueflei17{4-o Di{r4ctylphhatatemH4-0 Fluoranhene&f+f Fluoronel1&7+1 Hexachlorobenzene87{+3 ilexadtlorobutadiene71414 He)(adtlorocyclopentadiene67-72-1 Hexadoroethan€i93-39'5 In<leoo (1.2,}cd) pyr€ne90-12.0 1-Methytoaphthalene7E-5gl lsophorone91-57{ z-llethylnaphthatene96-4&7 2-Methylphenolt0&39-r, 3.+te{fiy'pfienol10€-4469-2G3 NaphthaterE
6-744 2-Nilroanitine
SNiboaniline
BRLBRLBRLBRLARLARLBRLBRLBRL8RLBRL8RL8RL8RL
BRL8RLARLBRLERLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRL447BRLBRL8RL8RLBRLBRLBRLBRLBRL
BRLARL
SRLBRLBRL
lS/kg dry 427
tg/kg dry 427
!g/kg dry 427
tdkSdty 427
Ug/kS dry 427
US/KS dry 427
!s/kg dry 427
!9/k9 dry 427
ldkg dry 427
!g/kg dry 427
trs/ks dry 427
!S/kg dry 427
lSftS dry 427
lgftgdry 427
rcrkS dry 427
Ugikg dry 427
US/kg dry 427
lSftS dry 427
lSftS dry 427
ldkS dry 427pglkgdty 427
IdkS dry 427
[qkg dry 427
UOkS dry 127
USrkS dry 427
usrks dry 127
UdkS dry 427
USAS dry 127
UdkS dry 427
lgkS dry 127
Ugkg dry 427
IgkS dry 427
Ugr(g dry 127pqxSdry 427
!g'kS dry 427
Ug'kS dry 427
u94q dry 127
ug{q dry 427
UgkSdry 127
lCl(gdry 427
!S/kS dry 427
lgrkS dry 427
USI(g dry 427
us/ks dry 427
ldkS dry 427
rc/kg dry 421
lgksdry 427
ldkS dry 427
FS/IS dry 427pS/kS dry 427
1
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SW846 8270C 22-Mat47 244tta(Ol 7031278 M B
This l4boratory rcpon is ^ot vald rgllhoat ad aldroized sEnaure oh thc coyer page .
+ R€portabl€ Detedion Limit BRL = Below Reporting Limjt Pase 3l of 152
Page 375
Sa-rnple ldeotiflc.atiotrM8F-49 2,-4'sA59464-06
Cliaot Pmieci#301-r8
MatixSotl
Colleciioq Date/Tirpel5-Mar-O? 00:00
Receiv€d19-Mu-07
CAS No. thralyte(s) F"g 'R.DL Ditaion Mdhod ReJ Preparcd ANIWd Botch Anallst
Semlmlcaile Oryrnlc Compourds by GCMSSemivolatile Oroanic Comoounds bv SW846 B27(rcPrepared by ntetEd SW846 35508100{1.€ 4-Nit'od line98-9+3 Nibobenzene0+75'5 z-Nitrophenol10G02-7 4Nitropheoo62-7+9 N-Nihdsodirnethytamine6C1{+7 ll-Mtosodi.n-propytamine8630{ N-Nitrosodiphenylamine87€0{ PefltrachlorophenolE5-01{ Phemnthrenel0g-95-2 menol12900{ Pr€nE110{6r Pyrilin€120-82-i .1,2.+Trichloro6enz€ne
95-95-4 2,4,$Tricfitorophenolaa,o€-z 2,4,6-Tridttorophenol
SsnDgate aecow r€s.'321404 24uor6iphd1yl367-12{' 2+luorophenol416r{p4 Nitobenzerc451t6542-2 Phend4s171&614 Terytwvl-dt411a-794 24,6-Trib@nnphenol
lgkS dry 17rO
udkSdry 427
US/kSdry 427
ldkg dry 1710
udkS dry 427
WkS dry 427
uSAgdry 427pdrgdry 427
tgt<gdty 427pgftg dry 427pdks dry 427pgkgdry 427
FdkS dry 427pdl€ d.y 427
lEftS d.y 427
30.130 %1U110 %30'130 %l r t l 0%3Gtn%1r110 %
r€ikg dry 0.0310
nrgL/kg dry 1.0'l
n'gkS dry 1.52
ftEftg dry 0.506
mgr'kg dry 0.253
n{l/kg dry 0_506
nrgkS dry 1.01
||lgts d.y 1.52
nEil O-010O
mgd 0,0150
mgr 0.0050
mgl 0.0025
n€rl 0.0050
mgn 0.00040
ngn 0.0075
r€rl 0.0150
%
BRLBRLBRLBRLBRLBRLBRLSRLBRLBRL4€6
BRLBRLBRL8RL
7764
6387
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SW846 8270C 22nnat47 214tar47 703127A M.B
Totrl M€trb by EPA 6000/?000 sffie! Meahod!
743997s M€rEUry
Totd MetrtB by EPA 200 S€rie! Meahods
?41S22-r Silver
21.44.3€-2 Ars€nic
74itr!39-3 Barium
744G:t+9 Cadmium
z!():u-3 chromium
743+92-1 L66d
262{9-2 Selenium
SPLP Met ls by EPA ISrl & 6000fl)00 S€ri€r Merhods
SPLP E'tredion
71,{G22-1 Silv€f
744G3&2 AEenic
744q393 Barium
744O4$S Cadmium
7a,1r)-47-3 Ch(omium
2(|947€ i/krcury
7431)€2n Lsad
?624S2 Seldnium
C€reral Ch.tnfutrjr P|tame 1er3
% Solids
sw8,t6 7471A 234d-O7 8.t!tdt47 7031306 yp
EPA 200.7 2$Mar{7 24-fr,l{-07 7031305 HB
24-Nlef47 ' LR
24-t\.t r-07 ' HS
SW8,f61312 21*lz(47 21-ttat47 7031229 BD
SW846 13fZ60l0B 22+.,.tt47 23.Nlato7 7m1323 tR
0.0683
BRL
1_64
2t.a
BRL
4.29
23.6
BRl-
Compl€led
SRL
BRL
0.0r 8€BRL
BRL
BRL
0.0497
BRL
s4.5
swB46 r3ra7470A
sw8,t6131?J6010823.&!ar{7 7031324 yp
2 vbr-O7 7031323 LR
SM2540 G [rod- ?2-Mat47 22+J{47 7031302 YM
Ihit labtuorf Eport is natedilt'ithoat oaaudtoi4cd sigrrtan od rhe cow, page,* Report ble Detectioo Limir BRL = B€low Rsporting Limit PsAe 32 ot 152
Page 376
Samole ldentificationM8F-50 2'-t,sA59,t5447
Cli€nt Project #301_88
MatrixSoil
Receivedl9-Mar-O7
Collection Date/Timel5-Mar-07 00:00
CAS No, .4aaly.e(s) FI"C 'RDL Dilation lr{ethod R"l. Prepared Analfred Bdlch Anal!$t
Votraile Orgmic Compounds
VOC Extracton
9t-2G3 tGphthalene
pstksdry 4.opgks dry 7S.4pgks dry 4.0pSftS dry 4.0
!C&S dry 4-0
lgrkS dry 4.0pgtxgdry 4.D
!S4<S dry 4.0
!g/kg dry 7.spg/kg dry 39.7
!g/kg dry 4-0
!g/kS dry 4.Opgr<gdry 4.0
Ug/kg dry 19.8pg/kg dry 4.0
Lig/Kg dry 4.0
!g/kg dry 7 I
ldkS dry 4.0pgJkSdry 79pdkS dry 4-0
!g/kg dry 4.0
!g/kg dry 7.9
!g/kg dry 4.0
!g/kg dry 4.0pdkS dty 4.O
ldkg dry 4 0
!g/(g dry 4.0
FS/kg dry 4.0
ldks dry 7.9
US/tS dry 4.0pdkg dty t.opdrs dry 4.0pdks dry 4.0
UdkS dry 4.0
Udkgdry 4.0
!g/,1(0 dry 4.0
MkS dry 4.O
!gl(g dry 4.0
ldkg dry 4.0pdkg dry 4.0pdkS dry 4.0pdkg dry {.0pdfq dry 39.7
!S/ko dry 4.0y9/k9 dry 4,0
udK$ dry 4,0
ugKs dry 39.7
lgKS dry 39.7
,.ISlkgdry 10
20-Mar'07 m.Mar{7 7031156 BOF€ld extracled
Volatile Oroanic Compoundshepared by method SWE46 5035A Soit (tow tevet)7G1}l 1,1,2-Ttichlorotiftuoroe,i-Ene (FreoERL67€+1 Aoetone SRL107n3-r AdYlonfit€ BRL714Y2 B€nz€ne BRL106-86-1 Brcmob€nz€ne BRL74-97-5 Bromo{fitoromethane BRL71274 Brofi€dj€*tlorom€lhane SRL7+2U2 Brcmofom BRL74{3-9 B&momelhane BRL7E-S.3 2-Butanone (MEK) BRLl(X-51{ n-Butylb€(uene BRL135-98-8 s€c-Butylb€nzene BRLs-06€ tdt-BtrMbenzene BRL7+15-0 Cafbon disutfide BRL56.2$.5 Cafbon btrachtoride BRL1o+!D-7 Chlorcbenzene BRL75-Oo-3 Chloaoethane BRL67{G3 ct o.oform BRL14+7-3 Chlo.ornethane ARL95.$-e z-Chtorotolume BRL10G4il4 +Chtorototuene BRLsr2{ 1,2_Dib|brno-.3_chtoropropane BRLr24a8.1 Dibromochtoromethane BRL10e93-a i,2-Dibmlno€r,ane(EDB) BRL74-953 Dibloftofiethene BRL95-5F1 1.2-Dichlorobenzene BRLf,41-aJn 1,3_0{chlofobenzene BRL1O€F46.7 1,4-Did{Orcbenzen€ BRL7t7t{ oichlorodinuorornethane(Fr€ont2)BRL7+3+3 l,loict{o.oethane BRL107-6-2 |,2-Oiclllorcethane BRL7+35-4 l,|-Dichlofoethene BRL15e592 cis- 1 .2-Oichtoroethene BRL15d60-5 trms-i,2oichtoro€thene BRL78{7{ |,2-Didtkfopropane BRL142-26-9 l,3_Dichlorcpropane BRL5gGacz 2,2-Oidrloop.opane ARL56!58{ t,l-Dichtoropropene BRLt00€l{l{cis-1,3oict{ofopropene 8RLt00€r{2$tEns-1,3-Dichlorcpropene 8RLi0(F4i.1 Ethybenzene 8RL87{+3 lbxad orobutadiene BRL591-78{ 2-t-iexanone (MBK) SRL
lsopr@ylbenzene BRL99€76 +lsopropyttoluene BRLl€34-&-4 Meftyt ted-butytether BRL10&1G1 +Met.|yt-Z-pentanone(M|BK) BRL?5{+2 Methytene chtoride BRL
Thk lahorotory ppod is ttot volid Eirhoa an authoized siEaoture on the cover page
r Reportable Detection Limit BRL = Below Reporting Limit Page 33 of 152
Page 377
Samole ldentifrcstionM8F-50 2'4'SA5946,1-07
Clieot Prcject #301J8
MatrixSoil
Received19-lilar-07
Collection Date/Timel5-Mar-0? 00:00
CAs No. Aaabt4i FIag *RDL Dibtrion Mdhod Ref,. Prcparcd ,lMlJEd Bokh Anal}f,a
Volrtile Org'l||tc Co|npouf, dsVolatile Oroanic ComooundsPrepared by m€hod SW846 5035A Soit (tow tevet)
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
75{9-a Triclrl6oiuoromethsne (Freon 1t) BRL
i0$6tl n-Propy'ltr€rEene1{x}42-5 sgrene€3(!zt6 .l,l.l.z-Totrachloroethan€
7$34-5 J,l,z2.TeFachloroefiane127-1e4 TetadrlorcodBneio&aa-3 Toluene€7-61-€ 1,2,+TnchloroberEefle12G82n 1,2,4-Tridllorcbenzone715$6 1,1,1-Tddtloro€thsne7g{Gs 1,1,2-Trichloro€han€79{1i Trichloroeth€n€
SW 846 8260S zl-ltsf4f 22-Mat47 700123 TR
+CT ETPH 21-Mat47 21'll a147 7031167 DS
96{84 1,2,}Tfidlloropropan€95+16 1,2,+Trinethylb€nzene108{7{ L3,gTrimelhylb€nzene75{1-4 Vlnyl cfiloride133O.2L7 m,p-Xyl€n€9547S oFxy,l€|l€10999.9 Tetahtdmfuran6G2+7 Ethye$erse4{s{ Tert-smyl methy' etherfa7-92n EUlyt tert-buty' €[1er10€-20-3 Di-isoproptieth€r7a'€fl) T6rt-Bubnol / butyt stcotrol12!91-1 l.+oioxane
Srnroga{€ EcolerJbs,4&40.| 4-arcmofluorcbenzenem37-26-5 Toluene<ft)1 706047 4 l,z-Dbhtooethane4l186&$-7 Abtumonuorcnolhane
D,rtnctrble P€troleum HydrocarbontExtradabls Total Potroleum FMroca6onsPrepsr€d by method SW846 35508800631.9 casoline6847sE!2 Fue{ Oil #26847s31*! Fuel Oil ,t468ss!-{E-1 Fuol Oil #6rr098om0o Motof OilJ001@0oo A!,lalion Fuel
UnldenIifi€dOtler Ol
Total Pefoleum Hydroca.bo sC9-C36 Ajiphatic Hydrocabons
SafrolEtfo fEcot€nbsr&186-332 l4hlotoodedecarc
Scrnhohdle Orgroic Compo!trds by cCOraanochlorin€ Pesticides SW846 StAlAPrep€red by mehod SW846 35504300{0-2 Aldrin
BRLSRLBRLBRLBRLBRLBRLBRLBRLBRLsRrsRtBRL
99105113106
pdkS dry 4.0
lS^gdry 4.0ggtgdry 40
ldxg dry 4.0
ug[Qdry 4.0
lgrtS d.y 4.0
ISikg dry 4_0pgkg dry 4.0
lgLSdry 4.0
rdr€ dry 4.0pgfg dry 4.0
UCAg d.y 4.0pgkodry 4.o
udkg dry 4.O
ldl(gd.y 4.0
t{d4s dry 4.o
Ig/lgdry 7.9pdlqdry 4-0
lgkg dry 39-7
|,9,1q dry 4.0
|'/tgdry 4.Opgtg dry 4.0
tigl(g dry 4.0
t,Sftg dry 39.7
trg/fq dry 79.4
7&1U %76130 %70-130 %7G130 %
1
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BRL
BRLBRLBRLBRLBRLBRL8RLBRI-BRL
n4Lkg dry 19.1
dtCkg dry l9.l
rr€/ks drv 19.1
mgftgdry 19.1
rEftgdry 19.1
r€rtgdry 19.1
mgikg dry lS.l
nqhgdry 19-1
ng/kgdry 1S.1
nrgr'kg dry 19.1
44-14) %
pgl(gdry 5-5t SWE46 808fA m-Ma[47 X1tat47 7Gr1068 TG
fhis lzbratoq Eporr Is ,ot vsld tthort on outhottal sknd/|'t- on ahe uw. page.
i Reponable DetectioE Limit BRL =B€low ReDortiaa Limit Pag€ 34 of 152
Page 378
Sample ldgrtificationMrF-50 2,-t'sA59,1at-07
Client Proi€ct #301 88
MahixSoil
Collcction Date/Timel5-Mar-07 00:00
Receivedt9-Mar-07
C,lS No. A,rolrle(s) Ft"S Uhia aRDL Dilutind Method ReJ Preparel Arrab'zed Bltch Analrsl
Sebivolrtile Orgatric Cornpo{rds by cCO.oanoc*rlodne Pesticides SW846 8O8tAPrepared by method SW846 355083190a6 +BHC319-0+7 b"BHC319-66{ d_BHC58-8$9 g'BHC (Lindane)57-7+9 Chlordane72+44 a,a-ODD (p,p')I2{+e 4,4.DDE (p.p.)5G2e.3 4,4-DOT (p,p)€o5t-l Dielddns5s€8€ Endosulbn I3321$65€ Endosulfan tl1031fi{ Endosulfan Sulfaten-m-a Endrin7421414 ErddnAldehyde76444 l-leptachlor724}5 tirethorychlorl02a-57J l-leptachlor Epoxide8001.352 Toxaph€Nre5103.71.9 a-C+ ordane55€€-3+7 gS ordane53491-705 E ldrin Kebne
Surrogale aecorcr'esrft3e 2 4,4D4-Odanuorobiphenyt (Sr)zo -2aa &cad orobiphenyl (Sr)Polvd odnated Biohenvls bv SW846 8082Prepared by method SW846 355081267+1r-2 PCB 10161110+ZE2 PCB 12211r141-16-5 PCB 123253169:21€ PCB 124212672-29€ PCB 124811007€91 PCB 12541100€{25 PCB 12603732+23-5 PCB 1262r1r0e1+4 Pc8 1268
Sunoga,' (@vedes:1 0iwc+2 1, 44 B-O ch n u orcb i p he n y' (S 02A&-2+3 Docz&lorobiphenyt (Sr)
Se dvoladle Orgr c Compounds by CCMS
ARLARLBRLARLBRLARLBRL
BRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
50a4
BRLBRLBRL
BRLBRLBRLBRLBRLBRL
5075
BRLBRLBRLBRLBRLBRL
BRLBRL
!S4(S dry 5.51
!S/kS dry 5-51
fdkS dry 5.51
!g/kg dry 5.51
Ug/kg dry 27.5
pdksdry 55l
Ug/kg dry 5.5'l
UdkS dry 5 51
IgkS dry 5.51
US/kS dry 5.51
pg/kS dry 5.51
ugkS dry s.s1tSlkg dry 5.51
t SikS dry 5.51pg/kg dry 5.51
ItgtKgdry 5.51
!S/kS dry 5.51
!g/kg dry 27.5
ug/kg dry 5.51
ISAS dry 5.51
!g/kg dry 5.51
30-150%30-150%
tiglkg dry 11.0
ldkS dry 'l1 0pqkS dry r r.0
!g/kg dry r r.0
Pg/l(g dry 11.0
!g/kg dry I l.o
lgftSdry 11.0
ldkg dry 11.0
Ug/kg dry l l0
30-150 %30-150 %
ldks dry 475
!g/ks dry 475pdkS dry 475
Lidkgdry 475
LidkS dry 175
ISAS dry 475
ISAS dry 475
ldkS dry 475
SW846 8081A 2O-MarO7 25-Mat-O7 7031068 TG
SW846 8082 22-Mat47 24-Mar47 7031274 MP
SW846 8270C 22-Mar07 24-MaGO7 7031278 M-g
Semivdalile Oroanic Comoounds bv SW846 8270CPr€pared by method SW846 355084332-9 Acensphth€ne,O&9$ ArerEphthylene€A-533 Aniline12&12-7 Anthaac€ne1912-219 Atzzjfie10$333 Azob€nz€'re/Oiphenytdi€zineg247-5 Benzidin€56{+3 B€nzo (a} anthracene
Thit labonto.! report is ,tot volid ,'Uho..t an aulhorize.I slprature on tho cover ptge .
' R€portable D€tectioo Limit BRL = Below Reporting Limit Page 35 of 152
Page 379
Sample ldeltificationM8F-50 2,-{'s459464-0?
Client Proi€ct #301-88
MatrixSoil
R9c€iv€dl9-Ma.-07
Collectioo Date/Timel5-Mar{7 00:00
CAS No- ABalW6) Resull Flag Uaix 'ML Dilalion ,Iakad netr, Prepond lnztyzpl Eatch Atubtsl
Semiyolstil€ Orgrolc Conpo|rnrls by GCMSSemivolatile Orqanic Comoounds bv SWBit6 E270CPrepared by method SW846 35508so-32€ BgfEO {a) pyrehe20$s-2 gerEo (b) fuoranthene191-24.2 BerEo (g,h.0 psylene207.0€-9 EerEo (k) nuorenthene65J54 8€nzoic aodloe51€ 8€nzylalcohol11141-1 Bis(2-chb.oodExylnetEnei1144-4 8is(2dioroeftyt)edrer39638-32€ Bi6(2dttodsopropyt)eo|e.1r7'81.7 Bis(2€drthoxyl)phthatate101-56-3 4Bmmopheny' phonyt ether05-€€-7 &ttylb€nzylphthalate8G74{ Calbszde59-5G7 +Cfiloro-3-mehylph€nol106-47{ +Chloroaniline91-5&7 2-ChbfonaPhthalene9557{ 2.Chlomph€nol7005-72-3 4-Chloaoph€nyt phenyeth€r218-ol-9 Chrysene597i1-3 DiberEo(a,h)anthrgceno132e.9 Db€rEofuran9'5G1'l ,2Sict{orobenzen€tl l-zJ-t ' .3-Dildorobenzen€106-46-7 1,4-Dichtorobenzene91€4-1 3,3'OichtoroberEidiner2G83,2 ?,4-Oict{orophenol€466-2 DiethytphfEtale131-11-3 Di.nehy phtlEtate10tr7-9 2,+Onnedrylphenolu.7+2 Dl-n-butytphthalate53452-1 4,&Otnitro_2_flethy'ph6lrol51-2s5 2,+Dinltopfienol12t-14-2 z,4-Olnltmtotuene60c2s2 2,6roiniftobiuene1r?{4.0 Di{-octytphhalate206-44{ Fluoh'rhene8&7+7 Fluoron€11&741 tbxechlorob€nzene87{&3 H€xadorobutadi€ne77474 Hexacfilorocydop€ntadiene87.12-1 ilexadrloro€thane1s33s-5 trdb.|o (l,2,3acd) ptrcne9(}i2-o l-lrlethy'naphfialene7B{9i l6ophorones157{ 2-libtlytnaphfElenes$4&7 2-Methylphenol1063€-4, 3,+Medry{phenolt06-1,1-591.203 NaphthaloneU-714 z.t*tr@nilin€99{9.2 }Nitoanilin€
BRLBRLBRLBRL8Rf8RLBRLBRLBRLBRTBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBBLBRLBRLBRLBRLBRL8RrBRLBRLBRLBRLBRL
BRLBRL
BRLSRLBRLBRLBRT
BRLBRLBRL
BRLBRLBRL
t 9rlg dry 475ydtsd.y 4tspgrg dry 475
ldlg dry 475gdkS dry 475
ldkS dry 475
WkS dr, 475
IS&gdry 475pdtg dry 475
FgrS dry 475
Igkg dry 475
lgkS dry 4rspgilq dry 475
US/IS d.y 475pqxg dry 475
ldlS dry 475
rdk€ dry 475
l|g/kg dry 475
Udl€dry 475
$I(g dry 475
trgl€ dry 475
|./, gdry 475
Idkg dry 175
IS/kg dry 475pdrSdry 475
ldks dry 475
ldkS dry 475ydkg dry 415pdkSdry 475
udkg d.y 475
udkldry 175pdr€dry 475
ldkodry 47spgkS dry 475
UCI€ dry 475pgts d.y 475pdrg dry 175
ldkg dry 175
ugkSdty 475pgkg dry 475pdkSdry 475
Pg*gdry 47spdkgdry 47s
Fdkodry 475
US/kS dry 475
lgkg dry 475
pSAod.y 475pgkgdry a1s
ld*odry a7s
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SW8468270C 22.1td47 24.1t6t47 7031278 M.B
l7'le lafuary rqorl is "ot
tldid pbho& s" aahodlzd sig/l{/'nre oE thc corer pqe.
+ Reportabl€ D€le{tion Limit BRL = Below ReportiBg Limit PBg€ 36 of 152
Page 380
Sample IdentificationM8F-50 2'-4'
sA5946t-07
Client Proiect #301-8$
MatrixSoil
Receivedl9-Mar-07
Collection Date/Timel5-Mar-07 00:00
CAS No. Anab'te(s) Rest/U FIag Unia lRDL Dilktbn Method Retr. Peparcd AnzlJzed 8o1ch Aulrst
Semi\ol.tile Orgmlc Compoutrdr by GCMS
Semivolatile Orqanic Comoounds bv SW846 8270C
Prepared by melhod SW846 35504rcrcot{ 4-Nitro€niline98€t3 Nifobenzene8F75-5 2-Nitroohonolt0o{?-7 +Nitophenol62-754 N+{ikosodirnelhylarnne62t{4-7 N-Nitlsodi-n-propy'amine86-30{ N-Nitrosodiphenylaminea7-46-5 Pedachlorophenolas-01€ Phenanihrene1@9s-2 Phenol129-{X)4 P},renelloei F/ridine1A)€2-1 1,2,4-Tridllorcbenzeness5-4 2,4,$Tric-hlorophenol08{€-2 2,4,GTricilorcphenol
S{]tmgElo fgcovorbs:?21.60{, 2-Fluotohiphenyt36r-t21 2+luoropheno!1t65-6p4 Nilnrb6nzene45416542-? monol4s1716-s1e Teryhenyt4l41 l0-m4 z,4,6-TihtotnoplFJnol
Totd Mctrb by EPA 6000n000 S€ries Mctftods
sw846 8270C 22-Mat47 24^!tal{7 1031278 M.BBRLBRL8RLBRLBRL8RL8RLBRLBRLARLBRLBRLBRLBRLBRL
79
63755090
o.0344
BRL
1_98
23.5
BRL
5 .12
9.99
BRL
udkg dry 1900
ldkg dry 475
UgkS dry 475
t|g'/kg dry 1900pSlkSdry 475
ttgKS dry 475pgKs dry 475pdks dry 475pg/kg dry 475
]rgkg dry 4f5
Ug/kg dry 475pEkg dry 4r5
t g/kg dry 475pSI(g dry 475pg/kS dry 475
30-130 %19110 %30-130 %11110 %3G130 %1U110 %
mg/kg dry 0.0326
mg/kg dry 0 963
dg/kg dry 147
mgfl(g dry 0 491
m$4(g dry 0.246
mdkgdry 0.49r
mgks dry 0.983
mSI(g dry 1-47
mg/l 0 0100
nEI 0-0150
mg/t 0.0050
@4 0.M25
mgl 0.0050
mg/l 0.00040
mSfl 0-0075
mg/l 0.0150
%
1
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7439976 M€rcury
Totll M€trb by 8PA 20O S€ris Meahods
74,u}22r4 Sifuer
7a{-3&2 A6€itiC
zt4$3+3 Badun
744(Hgg Cadmium
71.4G1t7-3 ChroLmium
743992-l Lead
f702-49? selenium
1 SW846 7471A 23-Mat47 26-Mat.ot 7031306 YP
EPA 200.7 23-MarO7 24-Ma.-O7 7031305 HB
24-Ma.-O7 ' LR
24-Mar0t ' HB
SPLP Meaals by DPA lJ12 & 6000,q00O Seri$ M.rhods
SPLPExtEction Completed
7.!r&22-i Sllver BRL
71K+3&2 AFenic BRL
7rt40-393 Barium 0.0146
7.140-{}9 Cadmium 8RL
7rt4{H7-l Chrcmlum 8RL7t3S.97{ M€rdrry BRL
7€942.1 Lead 8RL
7782{$2 Sele.nium BRL
Gcierrl Ch.mktrJ Porcm€ters
% sdids 8s.5
I SW8461312 21-Mat47 21-Mat47 703122S AD
1 SW846131260104 22-MarO7 23-Mar-O7 7031323 LR
1 '
1 '
I
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1 SW8461312/60108 " 23-|\,1a.-07 7031323 LR
1 '
'1 SM25.40 G Mod. 22-Ma(47 2241at47 7031307 YM
fhit lstotutory repo"l k ,ral tslU wuhaat an aarhodzed signdare oa tha cover page .
r RQortsbl€ lxtection Limit BRL = Below Reporting Linrt Page 37 of 152
Page 381
Saropte tdentifrcationM8F-51 2'-l'sA5946,+{8
Client Ploj€ct #301-88
MatrixSoil
Collection Ddte/Timet5-Mar47 00:00
Rec€ivedl9-Mar{7
CAS No. Addytc(s) nq aRDL lHdiorl Mdhod Rel Prapated Arulyzen Bdch Adelftl
Vohtil€ O.grnlc Compounds
VOC Extraction Field ext-acted
BRL
pgls dry 3.5
WkS d.y 7o.7
rdkgd.y 3.5
lgftg dry 3.5
lglSdry 3.5
rslksdry 3.5
USI(S dry 3.5
ISI(gdry 3.5
lSftS dry 7.1pdks dry 3s.3
flgfts dry 3-s
Idks d.y 3.s
l,gftg dry 3.5ggkS dry 17.7
FdkS dry 3-5
r|dkg dry 3.5
lrgkg dry 7.1
Pgtg dry 3.5pdksdry ?-1
UgI(g dry 3.5
UdkS d.y 3.5pgftg dry 7.1pgks dry 3.5
Pgn(S dry 3,5
IgkS dry 3.5
lSikS d,y 3.5
lSftS dry 3.5pgrs dry 3.5
ldks dry 7-'l
lsfts dry 3.5
ldks dry 3.5
Iqtgdry 3.5
udrq (lry 3.5
flgksdry 3.5
tdksd(y 3.5pSikS dry 3.5
ldlsdry 3.5
UdkS dry 3.5
sdkS dry 3.5
t€ikg dry 3.5
lqtgdry 3.5
Pdkodry 3.5
lgkgdry 35.3
tt*g dry 3.5
$ikS d.y 3.5pdtsdry 3.5
$gksdry 35.3
!Si(S dry 35.3
IdkSd,y 3.5
zGt,lar{7 20{r€r47 7031156 BOVolatile Omanic CompoundsPrepared by melhod SW846 5035A Soil (|ow bvet)76_1$1 1,'1,2-TdcttlorotrifLroroethane (FreoDRL6754-1 Ac€tone BRL107-13-1 Acrylonihile BRL714T2 B€nzene BRI_108-86-i Bomobenzene BRL1..gt-s Bromochlororn€thane 8RL75-214 Bron|odichlorcm€thane BRL1r2r2 Bmrnoform BRL7,143€ Bornomelhane BRL78.e13 2€stanone(MEK) BRL10r|.5l4 n-Butylbenzene BRLr3t98-o sec4utylbenzene BRL90{6€ te{t-BuMbenzene BRL75-1t0 Caabon disutfide BRL56.23-5 Carbon tetrechtoride BRL108-SO-7 Chlorobenz€ne BRL75{10-3 Chloroethan€ BRL67{63 Chlo.ofoam BRL7447-3 Chtorom€than€ BRL95-498 2-ChlorDtoluene BRL106-43-4 4-Chlorototuene BRLs6-12{ 1,2-Dibromo-Sdlloropropan€ 8RL124-4€.1 Oibromochloromethane BRL106s3{ 1,2{ibrornootrEne(EDB) BRL74-95.3 Dibromomethane BRL9150-1 lJ-Dichlorobenzene BRL5,11-73-1 l,lDichlorobenzene BRL106-4G7 l,4oichtorobenzene BRL75-71-8 Didllorodinuoromethene (Freonl2)BRL75t1.3 1,l-Dichtoroethane BRL107-06.2 .1,2-Dichlorc€{fiane BRL753s..1 |,1-Didtlam6thene 8RL15€'5s-2 cjs- 1,2-Diohbro€thene BRL15e@5 tEns-1,2-Dichloroeh€ne BRL78{7.5 1.2-Dichtorop@p6ne BRf1€.29-9 l,lDic+tbropropan€ gRf
5!M-20,7 2,2-Dichtoropropane BRL56$s83 1, I Oichlorcpropene BRL10061-01'5 cis-1,3-0idilodpropene BRL100€r{25trars-1,3-Didiloropropene SRI-10{F114 Edrylbenz€no BRLfl48'3 Hexachloobutadiene BRLs91.784 2-Hexanon€ (MBK) BRL9e{2{ lsopropylb€nz€ne BRL99{7€ +lsoproDyltoluene BRf1634{.1-4 Methyt t€n-butyl ether BRLt0&10.i +MeditG2-penta one (MIBK) BRL7s49-2 Methytone .fttodde BRL
I
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S1^/ 846 02608 2l+det47 2]['/€t47 7031233 TR' ;
9t.iG3 Naphthelene
Page 38 of 152
Thb bbrdo4 ,epod it Aol reli.l wiahou an oathoriztd signztare a.t ake .owr gage.
' R€portable Detection Limit BRL = Below Reponing Limit
Page 382
Sample IdentificationM8F-51 2'-4'sA59464-08
Client Proiect #30t _88
MatrixSoil
Receivedl9-Mar-07
Collection Date/Timel5-Mar-ll? 00:00
CAS Na A^abt4s) Flae Ufiits 'RDL Ditution Method Rel, tuepale.d Analped Botch Analysl
YokliLe l)tgr'i. Compounds
Volatle Omanic ComooundsPrepar€d by m€thod SW846 5035A Soit (tow tev€t)
BRL8RL8RLBRLBRLBRL
BRLBRL8RL8RL8RL
75-69-4 Trichtorofluoromethane (Freon 1l) BRL
103{6-l n-Propytbenzene10r!r2-5 Styr€ne630.206 1,1,.1,2-Tetfachtotlethane7+3rL5 .l,1,2,2_Tetrachtoroethane
127.i€i fefechlorDelhene10844{ TOlUen€87{ i4 ' l ,2,STr ichlorobenzene
120-82-1 1,2,+Trichlorobenzene71-554 1,1,1-Ttid oroethane7940-5 l,l,2-Trid oroethane794t6 fricl oroethene
SW 846 62604 21.Ma.-07 22'MaA7 7031233 TR
+CT ETpH 21-MaF07 21-[rlac07 7031167 OS
96.i84 l,2,S.Trichtofopropane95.63$ 1,2,+Triftethytb€nzene10&6/€ l,3,STrimethytbenzene75.,01-4 Mnylchlo.idel3cl-zG7 m,p-Xt4en€95{7{ Gxylene10940-9 Totrahydrofuran
.6G2+7 Eftyletler90.1{5-€ Tert-amyl meth!{ ether63742J E!]yttert-hrtyteher10&21L3 Di-isoprDpylether7545-0 Tgrt-Butanol / butjyi alcohol12+9i-1 1,4_Dioxane
Sr/'rog€te a€coyGrlesj410{04 4l-Btononuorchenzene
U37-26-5 foluene4S1 7@Do7-o 1, 2-Dbhlorcelhane-d4tffi€.53-7 Abtumofluoromethane
Ertncarble Petroleum Hydrocrrbons
Efadable Total Petroleum Hvdroca.bonsPrepared by method SW846 355088006{1-9 Gasotine6847&fi-2 Fuet Oit #26847&31-3 Fu€to tf4€455100-{ Fuel Oil t oM06800000 Mo,tof oil
"00100000 Aviation FuelUnidentifiodOtre. oilTotal Peboleum HydrocarbonsC9436 Aliphatic Hydrocatons
Srnrogale ,fooyedBsj33116.33-2 l-Chlorooctadecane
SeBtvolrtile Orgmtc Comportrds by cCOroanocfi lorine P€sticides SW846 8081APrepared by mehod SW846 3550830+{h-2 Aldrin
BRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRL
1001001 1 199
BRLBRLBRLBRLBRL8RLBRL
BRLBRL
88
!S/kS d.y
!g/kg dry
lSn(g drypEtQ drypqkg dry
lgkg dry
lgkg dry
lSftg dry
IIEXq dry
lqis dry
trS/kS dry
!s/kg dry
vdks dryps/kg drypdkS drypdkg dry
lgks dry
ldks dry
ldks dryyS/Kg dryyg/lQ dry
!g/kg dry
US/kS dry
usfts dry
t/dks dfy
3.53.53.53.53.53.53.5
3.53.53.53 5
7 1
35.33.53,53,5
35.370.7
t 7 017.0r7.0
1 7 017.017.017.0
17.0r7.017.0
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70,130%70-130%7G130%70-130 %
mqks drymS/kS drymdkg drymqks drymdks dryrng/kg drymgrq dryngn(g drynE/(g drynEnq dry
BRL
40-140 %
lgkg dry 5.41 SWOtl6 8001A 20-Mar-07 25-lvlar{7 7031068 TG
Thit hbotutory rcporl is Eol vald ,,ithout zn aafioizcn sipaturc on the cover page
+ Reporlable D€tection Limit BRL = Below Reporting Limit Page 39 of | 5.2
Page 383
Sampl€ [dentificationMtF-sr 2'-4'sA5946+08
Client Proiect #l 0 l+8
MatlixSoil
Collectioo Date/TirEeI 5-Mar47 00:00
Receivedl9-Mar-07
C,lS No. Ana$E(s) Resc/l Flzc 'RDL Diluion ntdhod nel Prcpared Arslfud Bdch Aao4st
S€mivol.tile Org.tric Colnpordr by CC
Orcanochlorine Pesticides SW846 8081A
Prepared by merhod sw846 35508
319-845 a-BHC31e{S7 baBHC31$86€ d_BHC5E{99 gFBHC (Lindane)
s7-7+g Chlordane72-/4 4,4-DDD (p.C)
n.s+e 4,4-DDE (p,p.)
50-2e-3 4,4-DDT (p,p')
60.57-1 Dieldrins5$9€$ Ehdosulfan I33213€5.9 Enclosuffan ll1031-074 Endosulfan Sulfatls72-m4 Enftin7421 -934 Endrin Aldel|},de7G.14{ Heptec*{orf24r' Methoxychlor1024-67-3 Heffacl or Epoxideglol.3F2 Toxaph€n€51()3.71-9 s-Chlodane5506-3+7 gchlordane
53494-70.5 Endrin Ketone
Sunogate ecoveies:t 03868+2 4, {-o&Octaf, uorobiphenyl ( Sr)
2051.21-3 Deczchtorobiphenyl (Sr)
Polvchlorinat€d Biohenvls bv SW846 8082
Prepared by method SW846 35508
12671.11-2 PCB 1016111o+A-2 PcB 122111141-16-5 PCB t232$46+2r-s PcB 124212672-294 PCB 124811097{9-1 pCB 12aJ41r0s6-E2-5 PCB 12603712+?l-5 PCB 1V621110ci4r PCB t258
SdTogale aecolf€fres.'1 03a6.8+2 4,+DB-OcIafl tmrcbiphenyt (5.)
N5t-2+3 Decachlonhiphenyl (So
S€E volatile Orgrnlc Compo|rtrd! by GCMS
BRLBRLBRL
BRLARLBRLBRLBRLBRLBRLBRj-8RLBRLBRLBRLBRLBRLBRI.BRLBRLBRL
44
BRLARLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
BRLBRLBRLBRL8RL
lgkg dry 5.41
rdksdry 5.41pdks dry 5 41
lrg/kg dry 5.41pdkdry 27.D
ldks dry 5.41
Udks dry 5.41
ldkS dry 5.41
t gil(g dry 5 41pS^S dry 5 41pdks dry 5 41
ldkS dry 5.41
9gkg dry 5.41
trdkgd.y 541pgrkg dry S,41pgftS dry 5 41pdtS dry 5.41
udkg dry 27.O
USftg dry 5.41
$lkg dry 5-41
lgftSdry 5.41
N-150%30-150 %
Igkgdry 10.8pdlqdry 10.8
!Sn(S dry 10.8
$gkSdry 10.4pdkgd.y 10.8
ISikS dry 10I
Frylgdry 10.8
ldlg dry 10.8
UdkS dry 10.8
30-150 %3o-t& %
$ftg dry 423
ugrS dry 423
UCASdry 423pgAS dry 423
ldkS dry 423
ldkS dty 423
t dkSd.y 423pSftgdry 423
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Semivolai e Orqanic Compounds by SW846 8270CPrepa.ed by melhod SW846 35508E3-32-9 Acgnaphth€ne20&s&S Acenaphthylene6?.513 Anilino12Ot2-? Anttus1912-2+9 Ntainet0!33-3 Azobenzener'Diphenytdiazine9247-5 Bqnzidine5'6.55:3 B€nzo (a) anlhracene
SUA}46 8082 22-Ma(47 24+ler47 7cB1274 kP
SW046 8270C 22-lla(47 25 tar47 7@1278 M.B
Thh ,ano.alory rcpod ie t ot wlid withou sn aath ized rq,alarc oB tlrc dawr psge.
' Repofiflble Det€ction Limit BRL = B€low R@orting Lirnit Pase 40 of 152
Page 384
Samole tdentificationMtF-sr 2'-4'sA59464-08
Client Proiect #301_88
Collection Dare/Timel5-Mar-07 0O:00
MatrixSoil
Receivedl9-Mar-07
CAS No. Anaba(s) Flog 'RDL Dilutirn Method ReI- Prcparcd Anaq@d Botch Anabst
Scmirolrtilc Organic Componrdr by GCMS
S€mivolaue Oroanic Comoounds bv SW846 8270CPr€pared by method Sw846 35508
s4l-32-8 Benzo (a) pyrene
Al$*).2 B6lEo (b) fluoranthene191-24-2 Benzo (g,h,i) perytene
al7,m.9 Benzo (k) fluorantEne66-45-0 Eenzdic acicl10{i-5r6 B€nz}4alcohol111.s1-1 Bis(2d{o.o€thory)methane111-44.4 Bis{2-cl.{orcethyt)etrer3s6:l+324 Bis{2-chtoroisopropyl)ether1174r-7 8ls(2-ehylh€xyt)phthatate101-5t€ 4Bromophenyt phenyt ethera5+17 BuVbenzylphthalat€€G7.t{ Catbazole5e-5G7 4-C;ttloro-3-rnethylphenol106-47{ +Chloroanitine91$6-7 2-Chloronaphthalene9557{ 2-ChloroPhenol70{872.3 4-Chtorcphenyl pheny' ether21&014 Chrys€rEs3-703 Dib€nro (a,h) anthracenei32-€4-9 Dib€nzofuran95,5Gr i,2-Dichlorobenzenea,4l-73-1 1,3-DichlorobenzenelGa6-7 i,+Dichlorobenzene
91{4-t 3,3lDichlorobenzidinerll€3-2 2,+Dichlorophenol846&2 Diethytphthatate131-11-3 oimetht{ phthalater05167€ 2,4-Dim€thytphenol
81-7+2 Di-n-butylphlhatate
534521 4,GDinilro-2-melhylphenol
51-2+5 2,4-Dihhrophenol121-1,L2 2,4_Dinilrctotuene
@8iry2 2,6-Dinitltrtotuefle117€4{ D{-n-octytphtratateztlGl4-O Fluolandrene86.7+7 Fluorcn€11&7+1 Hexachlorobenzen€475&3 Hexadtlorobutadienen 474 llsy€Chlorocyclopentadieoefl7.72.1 ller€d oroelhans1e&3es Indeno (1,2,3-cd) pyren€
9lt-12-0 l.ldetty'naphdlalene78-5$1 lsophorone915/6 2-Mehylnaphthal€nes5-4&7 2-ttt€hylph€nol
10&3s-a, 3,4-Methylphenoll0€.!1'591-2[3 Naph$alene
8Ii-7'!-,1' z-Nitroaniline
SS4$2 3-Nihoaniline
BRLBRLBRL
ERLARLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRL
BRLBRLBRLBRLBRL
BRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
ARLBRL
BRL
Pdks dry 423
l.t{t/kS dry 423
PS/kS dry 423pS/kS dry 423
Pdksdry 423
Pdks dry 423
!g/kg dry 423
ldks dry 42Xpg/kg dry 423
udks dry 423
Lidks dry 423
f.ig/l(g dry 423pdkS dry 423
PdkS dry 423pg/kg dry 423
ldKg dry 423
USftS dry 423
Ug/kq dry 423
Udkg dry 423
rc/kg dry 423
USnq dry 423
ug/kg dry 423
Fdkg dry 423pg/kg dry 423
ISngdry 423
rc/kq dry 423
US/kS dry 423
f./S/kS dry 423
ug/kg dry 423
udkS dry 423
Ug/kg dry 423pg/kg dry 423pSn(S dry 423pslkgdry 423
ISAS dry 423
lsftsdry 423
lgftS dry 423
lSftS dry 423
PdkS dry 423
PdkS dry 423
Irdkgdry 423
ldkg dry 423
FdkS dry 423
PdkS dry 423
F94(S dry 423
tg/kg dry 423
Hdkg dry 423
ldkSdry 423pSftS dry 42X
udks dry 423
SW846 8270C ?z-Ma'-OI 25-Ma(47 7031278 M B
Thit labontor! Eport ]a tor vqld wLhod an authorizctr sfuatue on the cover pagc_
' R€Fortable Det€ction Limit BRL = Below R€porting Limit Page 4l of 152
Page 385
SantDle [d€otificariooM8F-5r 2'4'sA59464-0r
Client Proiect #301-8s
MarixSoil
Colle!tiou Date./Ti!flet 5-Mar{7 00:00
Received19-Ma.47
CAS No. Anatre(s) Res t Fl4g A l s .RDL DiTAio,I Mdhod Rel. PEpar.d Analfied Bdch Atzlysl
Semlvohaile Orgsllc Conportrds by GCMS
Semivolalile Oroanic Comoounds bv SW846 827(rc
PreparEd by method SW846 35508
100"0i€ 4-Nitroor line9&913 Ntrobonzene
88-7t5 2-Nitroph€nol
100-02-7 +Nitr@heol@-7rg N-Nitrosodirnethylamine62t€a-7 N-Nitrosodi-Gpropylamine
€F3o-6 i+Nitrosodipheny'amine
€7{F5 Pentachlorophenol
85{l-8 Ph€Mnthrene10s95-2 Ph€nolr294O{ Pyrd€ilc86-1 hrridine1?O€-1 1,2.4-Tfidllorcbenzene95-95-4 2,4,STrichlorophenol€84+2 2,4.GTrichto{ophenol
Sutogale rgcowdes:
321aoa 2-Ftuor$bhenyl
367-124 z-FlLwopl6not
416s-@4 Niltubenzone4S
416fi2-2 Phenolds
,ne-514 Terphenyl4q
ltSlCO 2,4,6-Ttibrofitophenol
Toad Metrb by EPA 6000/7000 Seri€s Mettods
7439-9ru M6rcury
Totrl Metrb by EPA 200 Serie! M€thods
744n'224 Silver
Zt40-3&2 AF€nic
74,10-3+3 Barium
741O49S Cedmium
71-4047-3 Chrondum
7iK!942n Lead
282-4+2 Selenium
1 SW846 827OC 22-Mat47 25+trat47 7SUZ7A M.Bl '
' I '
1 .
1 "
1 '
1 '
1 "
t "
1 '
1 '
1 '
BRLBRL8RL
SRLBRLBRLBRLBRLBRLSRLBRLBRLBRL8RLBRL
81678069a9
lgr'Xg dry 1690
udksdry 423pdxs dry 423
US/kS dry 1690pdlsdry 423
ldxsdry 423
udks dry 423pS/t€ dry 423
rdkgdry 423pdrg dry 423
ldl(g dry 423
lgl€ dry 123pglqdry 423pSikSd.y 423pdrg dry 423
30-130 %18110%3G130 %,5-110%30-130 %tFllo %
mg/kg dry 0.03m
mgr'kg dry r.02
nrgr'kg dry 1.53
mgr'tg dry 0.500
mgiko dry O_2U
nrS/tg dry 0.509
nCftO dry 1.O2
mg/kg dry 1.53
mg/l 0.0100
nEA 0.01fl)
rngl 0.0050
IrE l 0.m25
mgn 0-0050
mgl 0.00040
"Elt 0.0075
msil 0.01m
%
BRL
BRL
1.96
25.6
BRI
6.60
BRL
1 SWE46 7471A 23-Mat47 m4et47 7031306 YP
EPA 200.7 23li.i,at47 24-Mat47 7031305 HB
' 24+'4et47 ' LR' 24-ltd47 ' HB
SPLf Met l. by EPA l3l2 & 600O/?000 Series Meihods
SPLP ExtEclbn7440-22-4 Slver
74rt0-3s2 AEenic
7{40.3+3 Barium
7a40-4i|9 Cadmiurn2440,,t7.3 Chrorruum7139-976 Merdty
?43942-1 L6ad
r|@-492 S€lenium
C€dertl Cl€milfry Prromelers
% Solids
1 SW8461312 21.N|,j.o7 21][n 47 7031??9 eD
1 SWB/61312/60106 22+,lar47 24.llat47 7m1323 LR
1 '
Complebd
BRL
BRL
0.0064
BRT
BRL
BRL
BRL
BRL
1 '
t '
t sw84613tZ/470A
1 Siv8461312rm108
1 '
23-Mat47 7031324 W
24+Jls47 7031323 LR
1 SM25,O G Mod. 22'|.',.a'4f n$iat47 7001307 YM
ThZs lstorolory epo b nolvolid Nlthoat sd aaaho.hcd signttut on dte @e.?poge.
* Repo.table Dele*ion Litrit BRL = B€lo* Rcporting Limit P€e 42 of | 52
Page 386
Samolo ldentificationM8F-52 2'-t'sA59803-16
Client Proiect #101-88
MatrixSoil
Collectiod frab/Time26-Mar-07 00:00
Received2'7-MaL07
CAS No, AEdyteG) Result FI"g Units *RDL Dilutioa Me.hod Rcf Prcpand Anaqzed Batch A rlysl
Volalile Oeanic Conuounds
Prepared by method SW846 50354 Soit (tow levet)
7r l19l '1,1,2-Tr ichlootr i t luoroethane(Freon BFL67+l-l A.etone SFL1lt-13r fu4ionitdto BFL71-13-2 BgEene BFL108-861 &Omob€nzene BFLr+srn Eomocilorcmehane BFLEn4 &omoddrloomelhane BHLE&2 Bomotonill BRL7l-8+9 Bonomehane BRL7Eql3 z.Eutanoie (MEK) BRL104-51.8 n-ButytbsEene BRL135.{18'8 sec-Bulyli4nzene BRL
9€{6-G ted-Butylb€mzene BRL
615-0 cadofl disufide 8BI
562+5 C€don tetBchtonde BRtr@got orlorobenzene gRL
75{G3 O ometfiane BRL
67s3 O orctom BRL1147.X 0{orcm€t|ane BBLsir+8 2{ibro{otuene BBL1ft-43{ 44 orctotuene BRLsel2-€ l,2obfom+3<filorcprcpano BRL124-4s1 Sbonod oomelhane BRL'@93-r 1,zloihunoehane (EoB) BRL740s3 [lbnnruneiharE ARL9+5G1 l.2.oichtoobenzene BRL
5,ll-73.t l,3{ichlorobenzene BRLr6-1s7 1,4-Dichtorobenzene BBL671.8 Dcftorodfluosnethane (Freont2) BRL1U*3 1.1-oicldorodhrn€ BFL1n7{G2 l,2-Uclioro€hane BRL15.35-4 l.l.oicliorcqhene BFLls6-5&2 ci91,2,olcilormthsn€ BffL
156{l}5 ra$-1,2-0hhloroethene BFL78c/'5 tz.Sdibopopane BffLta44 i,+Udiomprooane s8L
5s+a!7 22-Didltoopropane SFL
56950{ i,l-Djdlbopopene BFLlrxFr-01-5 cin1,3-oiciloroprcpone BFt10(E1-@{ tfi$-l,3oicliooprop€n€ 8FL100{1-4 EryDenzene 8BLt/-6s3 Herad{srobulad;a.a BRL
sl-78i 2+lelanone (t!,i8K) oRL
28Ma@7 A'Ma47 7U1761 8D
2g4lar07 29-Mar'07 7031790 8Ll
Voladle Orgrnlc Compounds
VOCExtadtot
jrS^S dry 6 6
ISAS dry 133
!S.4(S dry 5.6
lSilq dry 6.6
lVlS dry 5.6
lStS dy 6.6
lglq d'y 66
lvkg dry 66
lqkS dy 13.3
!S,tS dry 66.4pg,*g dy 6.6
PS/rg dry 6.6
!S4€ dry 6.6
]rgrS dty fi.z
ISAS dry 6.6
!g4q dy 6.6
!S,kq dry 13.3
!S/k! dry 6.6
lS,lqdry 13.3
!St{ dry 6.6
uS4q dry 6.6
Pgb d'y 13.3
!S4q dry 6-6
lglq dry 6.6
@tg,!y 6.6
jrdkd'y 6.6
!S/kS dry 6.5
us/ks dry 6.6
pgtS dry 13.3
pS/kS dry 6.6
lSifg dry 6.6
llgrS dry 6.6
llEls dry 6.6
ISAS ey 6.6
lglq dy 6.6
!$4S dry 6.6
!C4S dry 66
|4/l(S dry 6.6
l]gilS dry 6 6
lJg4(s dry 6.6
rtkis dry 66
$Iq fy 6-6
|lg,,l(S dry 66.1
UEk! dy a6
pg*S fy 6.6
peftS dy 6.6
Udrg d)' €6-4
ldkS dy 66-rl
!g4q dy 66
Field etuadd vcf,
sw84682 AI
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SF€ AbopoDyitduene
163,q,4-,r ehy,lterl+utyl€her100ncr +lirethyi-2{€nknone(Ml8K)
69 2 ff€$yi€ne dloride9l{lr3 Naph$etone
BRL
BRL
BHL
8FL
BRL
8Rf,
mb bboralorJt repo.t i' t ot vtIU vlthost an salttorizd sigftuure on the cover paEe .
' Repodable Detection Limit BRL = Below Reporring Limrt Page 78 of 154
Page 388
Sarple ldentificaJionMtF-52 2'-4'sA59803-16
Client Proiect #301-r8
MatrixSoil
Received27 MaP'l
Collection DatelTime26-Mar-07 00:00
CAS No, Adalf,c(s) Fk'g Unix 'RDL Dilutinn Method RcI, Preparcd Analfzed Bateh Analtsl
VohaihOrg ic Compoonds
Volaule Og6nb ComooundsPrepared by method SW846 5O35A Soil (low tevel)103{$t Fprop}t€nzem100-1!.5 Styr€ne000.20.6 1,I,l,2.Tetradorcelhane1\|"3,1.5 1,12,2-Tetradooethane1r.14"4 TskaElJooetlefl€108.883 TCIU€fis87414 jz,gTdcldorobenzene
120.€en j,2,+Ti{tombenzene
7_5ft 1,1,l.llicnbro€hanen00.5 1,1,2.f'i/.dttuD€d.68?901S Tddttor€fiene75{$4 Tndtlomttuoorn€lhane (Freon I 1 )s184 i2,&TricnbEp0pane
12,l.Trhelhylbenzenel@{r-€ l3,tTdmethytbenzen€tH1.4 Vinyldlonder$clc7 m,Fxylene9s.,r7€ oxylenero949-s l€tr*ydfd ran60.r$7 Eryshsr9to$8 T€rl{llMnElhyi€hera7-a{ Errytbnhrtyielherfla{0.3 Dtjsopropytether75so Ted-Buhrbl / brJtyl alcoholrzfgt,l 1,4{iorane
@404 4-E@noflwrcbenEne
2@1.&5 fduene4S
1tu6n474 1,2-Dil otod.fq''e44
11'6&9,7 Dblonafurovnelhane
Ellttctbl. PerrolcEm Hydrocrrbons
&tnalable Tobl Pdroleum Hrdrccarbons
Prepared by mothod SW846 35508qXEf14 GasOlme6€47S3C2 F$loI +2d847s3l's Fod 0l 14d06530ca FUelOi t8rr0!00m Moffoil.m10m0 Aviatbn Rlel
Unidentfi€d
of|ol oil
Total Peldeum Hldro..a6ons
Cg-c36 Alipllatic Hydreartons
38ff3? latfuadab@le
Senllolrtile Org.tric Compomds by cC
Omanodlodne Pss|itjdss SW846 8$1A
Pr€pared by moflod SW846 3545A
1F0tl2 Atddn
B8L
BFL
BRL
BRL
BRL
8RL
8RL
BRL
BRL
BBL
BRL
BRL
BRL
BRL
8RL
8RL
BRL
BRL
BRL
BFL
BFL
BFL
BFL
BFL
BRL
1U
1(n1231 1 1
lg]l(g ftv
!s4g dry
!c4q drypdks drypgls dry
lgxs di'pgt! dypsn(! drvpgts rv
!g/ks dry
UgrS drypgks dry
ugrs dry
rc.4(s dry
Psts drypEks dry
lqtS dr/
ldrs d'yyS/kSdy
lls^s fivpS4(S dry
lls/rs dry
Ktxs orypS/kS dry
!s/ks dry
7G1i0 %7V130 %7ll'130 %
7G130 %
ntS/kS dry
mgrkg dry
nAtS dry
n€ltg dry
rE/rs dryiE/rs drynVrS dryfldlq drym94s drlmS/rS dry
40,140%
sw 845 [email protected] 1
6 .6 r
6-6 r
6 6 r
6.6 I
6 6 r
6 6 1
6 6 1
6.6 1
6.6 1
6.6 1
6.6 r
6_6 1
6.6 I
6.6 l
6 6 1
1 3 3 1
66..1 1
6.6 |
6.6 I
6.6 |
66.4 1
133 I
29r,lar-07 2FMar,07 7031790 FtJ
2!!Mar{7 3Gl\rlar{7 70317736.5 1
6.5 1
6.5 1
6 5 1
6.5 1
6.5 1
6.5 1
6.5 1
6.5 l
6 5 r
BFLBFL8FL8RLBRLBRLBRLBRLBRLBRL
+CT ETPH
1 1 8
tErs dry slirB46 8061A 28-t'lart GAprOT 70:11739
This labonlory reFort is not dA *ihout a,t authodzed sigttatan on ahe covcr ptge
'RePortable Detection Limit BRL = Below ReporringLimit Page 19 of lS4
Page 389
Sample ldedtificationMtF-52 2'4'sAs980l-16
Client Proje€l #301-88
MatrixSoil
Collection Daje/Time26Mar47 00100
Received27-Mar41
CAS No, Analrk(s) Resalt Flag Uni,5 'RDL Diluio,. Me,hod ReJ. PrcpaQd Analfzed Bath An4lpt
S€mivolrtll€ Orgrnic Compounds by CC
@ganodlhrirF Peslicid€s SW8{6 8081 A
Prepared by m€thod SW846 3545A
319-8rt-6 +Bt|c
919-8F7 b+8C319.S&8 d€HC58.49.e +8[C (Ltndens)
lt7+s Chlordam7254-8 4,4,-DD0 (p,p,l
72.5rs 44'-0DE h,p)5G2e3 1,4'.00T {p,C}q!57-J oidddne5998{ Endosdtan I332rtt6rg E rlosjlat tl1{Bl-07-8 ErdGuffal SU al€
7421-934 Endin rJdelde
7lH4J tbdad{or72495 lretbryddorl@4-t'3 HepbdiorEpojdellDr.352 Totaph€isS1g3-rrg aSlodare5566-347 g-Ctilddane
$491m{ Erdfi (eloie
to36611.2 4,+DeMMdit hed 6t)Nt-21-3 MthtuhlEnyl(St)
Pqlvchlorinat€d giph€nvls by SW84{i 8082
Ptepared by method SW846 3545A
1267+1r-2 PC8 tot6
11101.28-2 PCBtl?l111r1-r&5 PCB 1232s0/6e"14 PCB 124212872.296 PCB 12411flc07{91 PC8.t25l{11@6-@-5 PC8126[sr-J2+29s PC8 t262r11ll$14-1 PCB t268
ttffi412 4,+D84cMM6ip@(St)
Mt-2q DecdMFlEtyl (Stl
S€mivolatite Organic Compounds by GCMS
S€mivolalile Ooaric Co.npounds by SW0,t6 8270C
P.epar€d by m€lhod SW846 35508Anq.g loonaotdld€ae+e* Aenapt'drylanee5$3 Aniir€1m.12-I Antra€ne1912-a+9 AlEzin€{}933.j Azobenzene/Diph€nyldazine92{7-5 g€nzidin€
56F3 8€nzo (a) anhr*erc
8BLBRTBRLBRLBALBFLBRLBRL8RL8tu8ft-
8qL
B8L
BNL
BnI
BRL
BRL
BHL
BFL
BRL
B8L
d5
t19
gRL
B8L
88L
BFT
8FL
BRL
BRL
BAt
BRL
105
BRLBALBRLBFLBRL8tusRtBHL
34J
34_9
u.s34.9
n4
34.9
34.9
343
u334.9
3 4 9
34.0
31.9
34.9
34.9
34!
34-9
174
t4.9
34.9
34.0
lCbdv!c{g dy
lldlqd,lsrq dy
wh fv
lqls try
ttgtlgtyrgts dy
$aaylslq dy
utlq dv
!9h fy
ldls dv
udk{ ry
Ah fiv
tdts dy
ugnq dy
|ldko d,
sgts dy
rEks dv
l4AS dY
Ttf i%EItfl%
pEls ay
USI{S dy
|lg/rS dy
|dts dvpC4q drypdb drv
udh dv
!9rg dypElq dy
30-1fi %*150%
srw845 &81A
sw8,46 8082
sw848827tC
I
I
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I
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1
I
I
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69.7
6t.7
63.7
63.7
a?
89.7
637
69.7
6S.7
28.1V€r{7 30-lrar47 m31738 5M
!9,k0 fy
Brq dv
rdlq dry
lclq dv
@aevl4redvudlq dl
$& dv
€07
807gl7
807
w7
$7
607
wf
2$MarJt 0+AorO7 ml?4 MA
Thb lahordory tepod h ,tot eaIU tcithout an aalhodzed sigaplure oa rte cover pzEe .
* Reporlable Dckctiod Limit BRL = Below Reporting Linit Page E0 of | 54
Page 390
Sample ldcntificationM8F-52 2'-4'sA5980l-16
Client Proiect #301 -88
CoLlcction Date/Time26-Mar-07 00:00
MatrixSoil
Received27 -Mar-07
CAS N^ Aftalrtz(s) FtoC 'RDL Dilulian Method Ret Prepared Analrzed Bctch Autrst
S€mivolafile Orgartc Compourds by CCMS
S€mivElalile organic Comoounds by SW846 pp70c
P.epared by method SW846 35508
5G@-8 Benzo (a)pyrene
205494 &nro (b) llloranlhonetst2+2 B€nzo (g,h,i) psrytene
207{!4 Eenro(k)fluonnlhene6t€5.0 EsEdc acjd10061{ Benzyl abohol1 ,91.1 Bis(2dtlofoedroxy)m€hane1lt-4,1-4 Bis(2doroetiy')ethet
39Fee4 8is(2dtlorrisopropyl)elher117-017 Bjs(2€fryhexyi)phlharate101'5'5'3 +Bomophenylpheiytstl€r
6-€s7 Eulyl b€nzyl phihaht€
8&7r€ Corba?ole
5&507 44htorc}.nethytpiend
1116{7ll tl,Chlorodliline
91.5&7 2{ttoromphliglene5t€ 2{Hofopn€nol?1F67!3 +Cflo.optEnyl phenti e$er218{l-! ftrys€ns537SJ Dibenzo (e,h) anhrscene132{,14 oib€fiZoluan
s65&l i,z-Uchbob€nzene
5.1'x!1 t,3-tXdltoob€nzeneql4s7 1,+Ddlklo&nzene
9r€+r 3,3',-0i6lJorobonzidine12043.2 a+Ddilorophenol04.€6.2 Didt\4 pl halater31.i1.3 Dm€ltytdfElate1ffi7€ Z+fimdtrytptt€nol*f+2 D-n{uty phhatate
$4{n1 46.Dnilrc2-lnethyiph€nolsr-2&5 Z+DnitrEphsnol121-1+2 a4-Uritrdotuen€6Ce202 a6{iailrlto{uen€117{4{ D.ft{clylphhalal€ffi:t+ Fluoanhene
F7$7 FluorerD1rS?+l ll€xadtxrbquene
trr€ss tl€radoobutadienen471 Hexdorccydop€rnadi€nefl-n-1 Hexd Om€lhanelsl3s5 Inddlo(1,2,3-cd)pyrcne!l{f124 l.ti,lebihapnhdene
46$1 loophomfie
9r5r-€ 2-Mohihephhdene
9q$7 2{ileryphenol
106.19{. q4-frefiylphe{'oli0G!+591.203 |\lethtlal€oel&7+1 2-l{itrroanilre
99.0$2 SMftanilrE
8FL
BFL
BFL
BFL
BRL
BRL
8RL
8RL
8RL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
B8L
8FL
SFL
BFL
BFL
BBL
BFL
BRL
BBL
BRL
BRL
ERT
BRL
BBL
BRL
BRL
BHL
8RL
8RL
8RL
BRL
8RL
8RL
8RL
BRL
BRL
BRL
8RL
8RL
8RL
8RL
8RL
8RL
BRL
WtS dry
ISAS dry
!S.4(S dry
pS4(S dry
pgks dry
pErq ory
tjg',q dry
lSfrS dry
u9k9 dry
pg4q dry
pdks dry
pgrs dry
lglq dry
!S4q d'Y
lgks dy
lsrq dy
lSrkS dy
!g/kg dry
tiglQ dry
!gt(S dry
lykg dry
!S4S dry
!94s dry
t{yKs ory
fgks dry
pdks dry
|ls/l(s dry
$rya $l
p4rs fiv
p4rs dry
|rs/rs drvpS4rS dry
Lryks dry
|rs/ks drv
lglq dry
l€&s drv
|Js/ks drvps/rs dry
ugis drypgxg dry
ugks dry
!s4q dy
!94(S dry
llses dry
t94q dry
!g,xg dl]
!g,kS dry
|Js/rs dry
|ls/rs dry
|JEls dlv
N7
&7@7
w7807
w7807
807
807
807
807
407
807
807
80/
807
80/
807
807
@7
ffi1
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n1807
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ED7
807
807
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m7807
807
807
w807
N7
m7m7
807
807
807
swe{6 8270c 2g.Ilar{7 09AF{7 7031774 M.8
This labotuaory nporl is nol ealid fl,ilhout sn zartoriaEd signttwe o^ lhe couer page.
+ Reponable D€tection Limir BRL = Below Repoding Limi! Page El of 154
Page 391
Sarnple ldeotificationM6F-52 2'-4'sA59803-16
Clieni Proiect #301-88
MahixSoil
Collectioo Dace/Time2GMar-07 0On0
R€ceiv€d27-M^r4?
CAS No. Aaalfta(s) nesur Fl"s Ual6 +RDL Dilztion Mdhad Ret Prcparud AnaIWd Bauh Analyst
Sehivolalile Orgrnic Compounds b!, CCMS
Semivolalih Omanic Comoourds b{i SW8.46 0270C
P.epared by method SW846 35508
10on1-6 +Niboflilne
S1193 l{ffi€nz6n6
8&7F5 2-t'litbphenol100@-7 +ifttDph€not
6&7ts l.&Ntosodlnehyjflnine
6214+7 NmhDSodi-rFpoptla,nine
8e30{ tlNitcodph€ny'amine
EI-81t5 PflhcHoloftl€nol
H1{ Ph€nenhrBne1O&S52 Pt|6nol129{D{ Pylem
110-€61 Pynding
r2o{2r l,a4.Tdchtoobenzene95-54 2,4s-TrchtorcptlerEl0&06.2 a4,6.Tddttoopttnol
st&4 z+l@tewentl
$r-t2.4 z.HMM
at65{0r ttlihtrbsuened5
1t6si22 Pl1fltr/-(E
171'nt4 Tqp@-d1
t1&?sn Z4FTfironrf,pherKlt
29-luad7 II}AF-'7 7wtn4 l'n8BCt
B8L
BNL
BRI.
BRT
BRl.
BRL
BfrL
BNL
BNL
BRI.
BRL
8Rt-
BHL
8fi1
55
74
u
Mh d|/
!gr{g fypdks dry
|'|g'lq trv
!g&s dv
|dlqdv|dh dv
|44q trv
udks rva*s evrdhdvrcnq dvudrg dy
tidtS fy
|Jgko d]
rtfr%t5-t t0 %&13J%
1U|tO16
&lf i%
1Ut10
'rdb dry 0.m42
d$|ttd) 1.10
mdks dy 1.65
mS/ks dry 0-549
'rE/kg dry 0.214
rn94€ dw 0.549
rngtq dry 0.84
mg4q dry i.€,5
mgl 0-01m
mgn 0.0150
mS, 0.m50
'Ilg,/| 0.(D25
rng/| 0.0125
ng,l 0000,10
ng 0 m75
m0/l 0.0150
sw846 827m
sw€rt6 74714
EPA 2M,7
3230607u73e30m7
807m7u7
€r07807w7wn7807
807
Totsl Metrb by EPA 60007000 Sedca Methods
7'F+97{ lr€rory
Tot l Metrls by EPA 200 seri6 Merhods
14!,'22! S{ver
l+(t3&2 fuSenic
7,1,rd 393 B€num
7't40{}1t cadnim
71,44f.1 CfiOfliUm
743+921 l_sed
2.87 I
I
I
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1
1
I
1
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1
1
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t
02-AF{7 @+pr{7 7lB18l0 YP
1.82
3.94
95.3
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102
320nv4+2 Selenium 1.82
SPLP Mclds by EPA 1312 & 6000l'000 Se rie! Methods
SPIP E{radbn
t44q'?24 sllver
7@&2 Arsenic
7,1,1t1.393 9aaium
Comdeted
BFL
0.0110
S1V8461312 &bbtJt 2&llar{)T 7031763 BD
SW8{61312/m108 3SMar{7 02.Apr47 781805 tR
?,1r0.{ss Cadn{lm 8RL
7@114 Chromium BRI
743+ct5 MeGtry BBL
7'(FPl |t{l 00138
71le.1s2 Sds um BFL
Gerct'l Ciemistry Paremeter$
% Soldr 06.6
sw€46 t3t2t7470
sw8lf 13r2lm108
' 02.Apr{7 781806 YP
. (P-ap.{7 n81805 |.n
$,@(| G Mod. gl+4ar.07 3cMar{7 7031879 YM
This kbonrory rqn t it nut valld rcllhoaa an zuthofized stgnOtun on thc corer paEc.
' Reportable Detection Limit BRL = Below Repoding Limit Page E2 of 154
Page 392
Sample Identi6cationMEF-53 2'-4's459803- l7
Client Proi€ct #301 -88
Collection Date/Time26-Mar-07 00:00
MatrixSoil
Received27-MEr-07
CAS No. Anauto(s) Flog Unils *RDL Dilution Merhod Rel. P,eparcd AnalJ)zei Bakh Analrsl
Volalile Oroanh Comoolnds
Prepared by method SW846 5O35A Soil (low leyel)
7t'r$1 1, i p-Tidilo|l]tdfluorc€ban€ (Frcon 8FL
6tt+t ,cehne 8RL1|,7.1sr Adyonitde 8RL7l{3? 8€nzer€ BFL
$ad6'r Eromobenzene 8RLt 95 Bomochbrooelhane BFL
75Zt4 Eomodiciloomethane SFL75€t2 Boinolom BFL7.134 BomofiEhane BRL7&e3 2+ulanone (MEK) BRL1ot-5r{ FBuvbenzene BBL135{€-8 ss€uvlbenzene BRLson6.6 t€n€uMbenzene BRL791i4 Carbon dhutfide BRL5e23.5 Cadon t€had oide BRtlo$gG7 Chlorob€i|z€n€ 8RLTrrocs ChloroetEn€ 8RL
r/iss ftloolorm BRL71a71 Orloro.nelhane 8RL
95.4+€ 2{h+orolduene 8RL16-43{ 44hlorotCuene 8RL96128 i,2-Ebonc3dlto@propane 8RL
12'!l&1 Dibornod oomelhane 8RL10643.. 1,2_ObromoefEne (EDB) BRL74.!lt3 Dbmmom€ttEne BRLgs-silr l,2-Ochtorcbenzene BRL
54r-7$1 l,$Dd orobenzene 8RL
i0e{e7 t,+Dcfilorotr€nzBne BRL7E7r.0 Dichtorodifluorcmethans (Fleff12) 8RL7!3+3 i,1-Dchbroqtane 8RL107.0+2 l2-Dd ooeihane 8RL
1,1-Ddllorcodr€n6 8RLrsess? cisn,2ok*lloro€th€n€ BRL
i${o-s [En91,2-0iahlo(oethene BRL7!{/5 '12-Dic oropopane SRL
Volrtile Orgrnic Compounds
r{s,zFs i'3-DicntoropropaneS+zG, 22-Didtloopropane5e5€-0 |,l-Didoopopene1S€1{15 cisl,s{iciloroprop€fielm01@5 trutsl,S{|id oroorolenelGilt-l Efiyjbenz€{po4n Hexad or$Lnadene501-78{ 2+t6ranone(MBx)98{e{ bopopy'b€nuene9S{|€ 4-tsoproMdu€nerdl4-o/r{ tlr€ftyl ten_bulyl elherro&rGr 4{r6t'y'-2fenbnone(Mlg,Kl?5-(192 fi€ttye|edltoride9r.20.! Naphftakne
28{lar{7 28{ar07 7031767 B0
2S-M^t47 29{!br{7 7031790 ffUllg/ks dv
!s/ks dry
lqks dry
!91q dry
tclq drypdkr drypdlq dvpdks d]
Igks dv
!91q drypOks dy
lElo dy
lyts dv
!s4q dv
lglS dry
uS4q dry
lgftS,trylgro dry
lgrs dry
lgrs dry
r{yKg ory
lCqS dry
lSeS drypgrs dry
ugfts dry
lgftS drypS&S dry
!g/kg dry
K,tS dry
|Jg&S dry
!s^s dry
!S4q dry
tEks fry
ldks dy
Ionq dv
loikS dypsn(s dy
|}El(s drv
IS/IS dly
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ldrS dry
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voc
sw 846 8260At51 1 1
5.5
5 5
5 5
5.5
5 5
5.5
1 1 1
55.3
5 5
5 5
5.5
27.7
5.5
5.5
1 1 . 1
5.5
] ] l
5.5
5.5
1 t l
5.5
5.5
5.5
5.5
5.5
5.5
1 1 . 1
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
55.3
5.5
5.5
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55J
5t3
5.5
SRL
BRI
BRL
BRt
BRL
BRL
BNL
BFL
BRL
BFL
BFL
BFL
BFL
BFL
This labonlot! Epo ir ,tot tlalill teithoaa an adhorized signaturc on the cowr page
* Reportable Detection Limit BRL = Below R€porting Limit Page 83 of 154
Page 393
Sampl€ [dentificationM8F-53 2,-4'sA59803-17
Client Proiect #301-88
MatrixSoil
Collection Dal,e/Time26-Mar47 00:00
Rec€ived21-MaFO1
CAS No- Analyz(t) Ftzg 'RDL Dil'lian Method Rel, Prcpzad Aazbzen Bztch A4alyst
Vol.tile Org.nic Compoutrds
Volalile Oro& c Commun&
Pr€parcd by method SW846 5035A Soil (low lovel)
103451 tufupyhHrzene BRL
100-42-5 StyHls 8RL
6s'.20.6 1,1,12-Tetrachlo.oetrhane BRt
7!|"0,1-5 1,1,22-Ie0adrlo.oelhane BRt
127-t8-4 Te{nd orcefi€ne 8FLros-€6.3 Tobene gfiL
67{1{ 1,2,}rrichtoob€flzene BRL
12OS2t l,2.+Trid oobenzen€ BRL
71-5s.€ l,1,l.Tdchlor@fiane BFL
I,l2.td$hft€hare BFL
E{1{ Tnct om€tlqle BRL
75.6s_{ Tict onlluororneha'le (Fr€on 1 l ) 8RL
sl8-a lr,STricnbrcpropane SRL
ffit6 1,2,1-Tdnefrylb€nzsne 8Rf
100-r/{ 1,A,tTdn€hylbenzsrE BRL
75414 Vinyl.tlodto BflL
$3q?G7 |l\o-Xytelle BRL
95..75 cxyjene BFL10$9+9 Tetrahdofuran BRL
80.2+7 Efiyt etrer BnL
99t{5.0 Ten-dnyl m€dryl eiher BRL
a7+2-3 Etty' bdtut{ etler BRL
29 ar{7 29-lrar.07 703179 FUldh dy 5.s
$'lq dy 5.5
|lg,tq dy 5.5
ilg/lg dV 5.5
p9l0 dy 5.5
!g/fg dy 5.5
ldlq fy 5.s
lgftg try 5.5
!g4q try 55
pglq fV 5.5
$/lq dry 5 5
|l9h dry 5.s
|.dlq dy s.s
Udl{ d} 5.s
UgkS dl 5.s
pgkg fy 5.s
ttgh fy 11.1
|Jqh dy s.5
lsAg dy 55.3
WrS dry t5
uErqdy 55
|,Ehdy 55
Iryfu dy 5.5pglqdy 55.3
l,C4g dy l1l
701f l%
7&1W%
TUtU%
70130 %
ms,qdry 55mg,l0dry 5.5mglqdy 5.5mdkS 4y s.stttdkS fy S.5ftdkdry 5.sn'dlq dry 5.5mdlqdry 55nvlqdry i5'tvb dry 5.5
4,t40%
!o& dv
sw 816 826{S
l@2G3 Disoprogyt et|er
7s5-o Ist-Buland / htyl al€ohd1zlt1-r t,4.CIO(ale
@@4 4.Eronofiwabenzerre
M7.&5 Tdt-Btl€49
17ffi414 1,2-DdlotcdlhaB44
186+&7 Di&MbA@OneUBne
Erlrrctable P€t.oleum Hydrocarbo||J
Erhaalable Tolsl Pelroleum tMrdaftons
P.epared by method SW846 35508
9006-614 Gasdine60r6i102 F€t Otj26s7e3'-3 F|l€t 0it*4685510(H Fueloll 16r,!0900000 t&toroilJ@104000 Aviation fuel
U\i!(,lffi€d
0dr6r Ol
Told Petderm Hydbcarbons
Cg{36 lfiphalic |}}drocatbolls
3nfi,*2 l-Clio/officene
S€rEivohaile Orgsilc CotbpoMds by GC
OEandlod0e Peslicides St48a6 8081 A
Prepared by mettEd SW846 3545A
3F{O2 Aktin
8RL8RLBRI
91
107
t22
t14
BRL
BRL
8RL
8Rt
8FL
BFL
BRL
8FL
BfuBFL
+CT ETPII n4luty 30.1&r{7 70elz3 DS
sw846 8001A 28-lilar{7 09lor{7 7ll3izJg TG
Thit la.torubry ,eport h ,tot volid flIhotd aa aaahoriaed Eigrrzlare oE thz cots Fage.a Reportable D€tection Limit 8RL = Below Reponing Limit Page 84 of 154
Page 394
Sample IdeotificationM8F-53 2'-4'st\5980l-17
Client Proiect #301 -88
Collectioo Date/Tirne26-Mar-07 00:00
MatrixSoil
Received2l -MaI.01
CAS No, Anallte(s) Resuh FloE Unias +RDL Dilution Method Ref. Prcpared Anaryud Batth Analysl
Semlvolrdle Orgrnic Compoun& by CC
oroanod ofte Peslicides SW846 6081 A
Prepared by m€thod SW846 3545A
3r$84+ a-BHC3rsB 7 tsBHC319-8e8 GBHC584s4 9BHC (Lhdane)t-74.9 chbdan€7}54{ 4,4.00D(p,p')71.55e a,a.DoE (p,C)ll2e3 a,a-D0T(p.p')dH7-1 o€ldin9699&3 €ndosuffan It021345 e Endosutfan tl1031{78 €fibsrjffansutfaie72-2G8 En&in74211F{ Endin Aldehyde76-4r{ Heotadlorn4s5 lilehorydlorrn2457-3 HoflacnlorEponde0oorn5'2 Toxaphene5log-714 +Ct ordane556t3{.7 g_Chlordane
s31047C5 tuddn K€tone
t0a{€'l-2 4,4oB4claflwrchjplBnl(Sl
2'6'1-2L1 [email protected]
Potucl orhslod tlioh€nvis b! sw846 8082
Prepa.ed by method SW846 3545A
l?67+11-2 ['Cg t016rr10+2&2 Pc8122111r4r-1e5 ft8123250169.21-9 PC81242ft72-296 PCg 1248rr00?{9.1 PC81254!1000€26 PC81260
a34tt5 PC31292111OOr4-r t[B t26€
Sr,|ogElp rwvrdestwa+z 4,4t8&Bnw6iphenyl(6t)
eL2+3 DefEchhnhiphenyl(Sl
S€mir,olalile Orgstrlc Compo[nds by CCMS
S€mivdetilo Oroadc Comoounds by SV'/848 8270C
PrepaEd by mehod SW846 35508
4.3?€ Aaenaphd*nerDs.966 Acq€fifrytenee.533 Anilifle124.12.f Anh|ac€fle1912.2,r-9 AtazirE100-313 A.zob€nzene/Diphenldanne4.67-5 B€nzijine!i-55-3 Beruo (a) anhnE€ne
BRL
BFL
8fl1
BRI
BRL
BRL
BHL
BFL
BFL
BFL
BFL
BRL
BFL
BFL
BFL
BRL
BFL
BffL
B8L
BFL
BFL
64
96
BFL
BRL
BRL
881
BFL
BRL
BFL
BRL
BNL
n110
lCfrS dry
14.4S dry
ug*s dy
!c4q dry
|ls/ks drv
l4/ts drv
$4q dry
t4vrq ory
udrs drypS4q dry
lSfrS dry
udlq drypg4q dry
lgfts dv
IEKS dypgts dy
!0ts dypg/kq dypgkq dypdks dv
$/kS dy
&150 %&150 %
us,ls ctyp94q dy
lls'(s dvpgxsdv
!g,tg dvpgJiq dy
ps/rs dy!g4q dv
pglq dv
iG150 %
30150 0,6
sw8.468081A320
32.0
32.0
32.0
r60
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
3 2 0
32.0
32.0
?.0
160
32.0
32.0
32.0
28{,lar-07 03'&107 7031739 IG
64.1
64.1
64.1
4 .1
fl.1
64.1
64.1
fl.1
64.1
sv/846 8082
SW8,l6 8270C
2S Mar07 30'Mar.07 703173E SM
2g-l'rar{7 0&Apr{7 7031774 M.BBRL
8RL
BRL
BRL
BRL
BNL
BRL
BRL
ugiiS dry
t$\Sdty
rdlq dry
FVIS dry
$4€ ftv
8,4(S dV
!S4!S dy
ysts dry
686 1
686 I
6S6 1
586 1
686 1
686 1
686 1
686 1
Thb Isboratod tepod is not wlid tdlhout an qathorizd slgr'otwe on the corpr paEe-
'Reportable Det€ction Limit BRL= Below ReportinC Limit Page E5 of 154
Page 395
Samote [deo tificationM8F-53 2'-4,
sA59803- t7
Client Prciect #l0t-88
MarrixSoil
Receiv€d27-Mu-O'7
Collection Dal€/Time2GMar-07 00:00
CAS No, Analyte(s) Result FI"S a b 'RDI Dihaiaa M?rtod RrJ tuepared Aatlfud Batch ,Amlpt
Semivolrtile Org.Eic Compounds by GCMS
Semivohne Onanic Compdrnds bv 5$/846 8270C
Prepared by mettod SW846 35508
5&32-8 Be,Eo (r)py€o€
?0$99-2 Selro 0) nuoandrene191-24'- Seizo(g,h,i)peryisE207{S9 Es|zo (k)fiuord tEno66+5{ EaflzDic acid1@{1-6 B€n4lakDM111-91-1 Bis(2dttorehory)meftano11r-4.t-.1 8is(2d\ho€trytle$\e{sS3&349 8b(2dofiisoprogyt)oherfit{r'7 Bi5{2+ttthsyt)phhatatel0l{t3 {-S|lnoptt€iyt pheoy' edlers5.6&t Butylb$zy1phhatate&71-s Carbszole59.s07 4-chloroF}mehylph€nol106-17.8 {{hloroqiline91'5e1 2-fttoromphfiat€nes+574 24htb@Pheiol7!05-72 3 4ctiorodlellyl lhent st\er218{1-9 ChryE€net97rl3 obBfto{ah}anhn(en613?-649 Dibenzofuran5{&1 l,2€ldlkob€n:€n€511-&1 1,$oidoaob€nz€n€m6.,|a7 1,+DtfoobenzerE91.9+i 3,3-oiddorobenzidnsl20rll!.2 2,4.Dido{ophenols+€e2 obtM phhatate13' 11! Direthyld\hat b105{74 2,aoiiFsrylphejolw1+2 D.nt0lylpHnahb534s2'r 4,S0nit$2-nEhylpnenol$'24.5 2,+hitrophend1211+2 a4-DniFqtoluono6G2rF2 z,6.llnitrctduener17t4{ O+odytphfiatate206-..{ FfuoGdh€n€&7J.t Ruoene11&71.1 thxachhrobqtz€ne6/.€93 Hexadoot{r'tadenen474 Ho(adorocldope.ntadioie
-n-1 Hdaddo@offune19{9-5 H€no (12,$cd) pyrenecf12.0 l-fretrytnaphtlalene785+1 hophorffeer-'|{ 2{iethy'naphttalefles&7 2{vteirylpl|gl€l
r00-r0-4, 3,+[,teh/pnndtH+5gr-2c3 Nadbdqi€0s.74.,r 2-Mroan|lneF+2 3-MtDaniur|e
BFL
BFL
BRL
BRL
BRI
BRL
BflL
BRL
BFL
8Rr8RL8RLBRLBRL8FLBFL
BFLSRLBRTB8LBflLBHLBFL8BL8ALBRI,BRLBflLBHLBFLBRL8RL8RLBRI-BRLBRLBFLBRL8Rt-BFI
8RLB8LBFLBRLBRL8RL8FI.
BBLgRL
BFL
l4lq d,
wh rvlgrg dl
lldlq dy
Wt'r!g4q dry
ljg4q dv
lry}0dy|Jqlg trv
lgfts dry
v4*s &y
E/rq fiy
f94q 4y
ilsrq dv
lsrq dfpdrq dv
|lsas &y
Nrq fv
|lgnq dv
lgkg dy
dlq dry
!g/kg trI
!s4q fy
Wks fiy
r{yh dvpdb drv
uC,lq dry
!S,rS dy
usrq dy
lgks ey
rrgcS dI
ldre dy
!s& d]
ugllq dry
B/lq dry
tgh dv
lgrs ry14is s't|lg/tg dry
|ryqs dyu9,lc dyrErg dylgrg d!
wh dvrid*S dry
Ars dy|4k ev
Udlq dry
|,grs dv!g]q dv
685
686
686
686
686
666
686
686
686
6€6
686
686
686
s6686
686
666
6€6
686
686
666
686
886
6E6
6€6
€€6
686
t€6
€E6
6€6
€ffi
686
666
6€6
686
6€6
686
6€6
686
6€6
sw846 U/0C 2glfarfl wAy TBtn4 M I
This ltbo&tory Eport it noa valil without a aathoriact! si-g'ralare on the cotet page.
. R@rtabl€ DerqrtioE Limit BRI- = Below Repdting Limit PaBe 86 of 154
Page 396
Sample IdentificationM8F-53 2'-4'sA59803- l7
Client Proiect #301 -88
Collection l)ate/Time26-Mar-07 00:00
MatrixSoil
Received27-Mar-0?
CAS No. Alotrte(s) Flog Units *RDL Dilution Pnryred Analrzed Batch lnallsl
Semivolrtile Orgrnic Connounds by CCMS
Semivolail€ o(anic Cornpflnds bv SWB46 82?0C
Pr€pared by method SW846 35508
100.{1€ 4-Nitmanitine
$.9S3 Nitrobenzene
6&7$s 2-t'titrophenol100@-7 4-Nifopi€nol
e75€ N-Nilrosodimefiylamine
@1&1 il-Nitiosodi-n-popylamin€
0s30-6 il.Nilrosodiphonytamineg/.€+5 PenlachloEphenol&t-8 Phenanliaene106-9$2 Pheml129.!04 Pyrener 10.06-1 Pyridine140.€2.1 1,2,+Trjchlorobenzene
9545.{ 2,4,tTdcnbrophenol8-05'2 2,4,ATridbophenot
ic1-604 2-H@riltplEnyl
s7-t21 2'f:hhtqlend
4165.co4 Nivobenenells
11ffi2 Ptgnol4s
1718514 teeleryH4
11&7 2,4,6ftibtonoph61ol
29Mar-07 03-Apr-07 70317i4 M.88RL
SRL
BRL
BRL
BFL
BRL
BRL
BFL
BFL
BFL
BHT
8Bt
8RL
BRL
8RL
59
6t
80
51
68
133
1.81
Compleled
BRL
8RL
0.aM
BRL
8RL
BRL
0.011i
Vdr,gdry 2140
pgXS dry 686
l4^(S dy 686
lglq dy 2740
pS,lq dry 686
pdlq dry 6EG
pdlS dry 6E6
!dt(S dry 6E6
|jg,4(S dry 686
pS4rS dry 686
|lgkS dry 686
UgkS dry 685
Udksdry 686
pdkS dry 685
pS/rS dy 606
3+130 %
15110%g-1u%
1 r t 1 0 %
3Gt30 %
1 r 1 1 0 %
nrgAg dry 0 0355
nS4q d'y 1.I8
mdkS dry 1.78
mdksdry 0.s92
mglq dry 0.2s6
mdlqdry 0 592
mdrgdry 0-888
mCtS dry 1.78
mE 0.0100
nrs/ 0 0150
ngn o@50
mgl 0.0025
ngil 0n125
mgl O0{D40
rhgl 0.0075
mg4 00150
3lrl/846 8270C
Total Metlls b!, EPA 6000/7000 Sert€i M€lhods
7,ll+97-6 Mercury
Totrl Metlli by EPA ?00 Series Methods
114t22.{ Silver
7440-3/}2 A6enic
7{rl0'3$3 Baiun
7rr4!t+9 Cadnium
7!'4,J-47-3 Chtomium
743$@-r Lead
f',]2.4g2 S€l€nium
SPtP Exlaclion
114d?24 Sifuer
7,!10.3&2 Arsenic
7.r,ro3s3 Eadm
74aG€€ Cadniun
7140{n qrronfum
7'F997{ Meretry
7,$9.92'l Lead
1
I
1
1
1
1
1
l
1
I
I
I
I
I
1
st/lJE46 7471 A
EPA200.7
sw8,46 r312
SW8461312,60108
SW8,|61312'?4704
sw8461312/0108
$l/trt|o G Mod-
a2-ap1-o7 03-Apr-07 7031810 YP
BRL
4.42
98.3
0.521
02-Apr-07 HB
SPLP Melrls by EPA lll2 & 6000/7000 Serie3 Methods
7n2{$2 Sdelium 8RL
C.DGr.l Chemhtry Palameters
% Solids €4 4
2&Mar{7 28-Mar{7 70317€3 BD
30 ar0 m'Ap.{7 7031805 LF
" 02-Apr{7 7031806 YP
" (}2-Apr.o7 7031805 L8
30-Marfl 3S-MaF0/ 7031879 YM
This bboralory rcpo it not vrlid tiithout u aatho zed slgnalarc oa the cover page.
* Reportable Detection Limit BRL = Below Reporting Limit Page R? of 154
Page 397
APPENDIX DBallast Sample
Laboratory Reports
Page 398
Samplc lde[tificationMSFETsA5946+09
Client Proi€ct #l0l-88
Collccdon Date/Timcl5-Mar-07 00:00
MatrixBaLlast
Reccivedl9-Mar-07
CAS No. Anabte(s) Resall FI"C Uzirs *RDL Dilurian Method ReJ PEpr.ed Ans4red B ch AMryE|
Vobdlc Orgsnic Compo|rnds
Volalile Orqanic ComooundsPrepared by method SW846 5035A Soit (tow levet)76-t3-1 1,1,2-TdchloroHnuoroethane (FreoERL6744-.1 Acetone BRL107-t3^1 AcMonitrih BRL71-432 B€nzene BRL1o€&n Eromobenzene BRL74€7-5 BaornochlorometEne BRL75.274 Bmmodicfiloromethane BRL75-2U? Brornofom BRL744!9 Bronbmethane BRL76-913 2-Butanone (MEK) BRL1{M.s1€ n-Butylb€nzene BRL13s8€ sec-Burytb€nzene BRL98{€-6 tert-Butylb€nzeno BRL75-1fi Carbon dis,_tlfide BRL56-2+5 Carbon tetrachlorde BRL10840-7 Chlorobenzene BRL75{0-3 Chloroethane ARL67{8.X Chlorcform BRL7447-3 Chlorometfiane ARL9549{ 2-Chlorotoluene BRLi0G434 +Chlorotoluene BRL9612-8'1,2-Dibromo-3-chloropropane BRL124-43,i Dibrofibchtoromethane BRL1{rss3.. i,2-Dibromo€thane(EDA) BRL74-9t3 DibrcmoiEthane BRL95{G1 t,z.Oichtorobenzen€ BRL5+1-73t l,3.Oichlorobenzene BRL106-4G7 1!4-Dichlorobenzene BRL7s71-8 Dichlorodifluoromethane (Freon12)BRL75.34-3 1,1-Dichtoroethane BRL107-06.2 1,Z-Dichtoroethane BRL75-35-4 1,l-Dichtoroethene BRL15&59.2 cis-1 ,z-Dichtoroethene BRL15e60-5 trans-1,2-Dichloroettlene BRL7&€7-5 1,2-Dichloropropane BRL142-28€ 1,lDichloroprop€ne BRLS!t-20-7 2,2-Dichloropropane BRLs6$5E{ 1,1_DichloroproF,ene BRL1ar0€1.01.5 cis_1,3_Dic*llorcpropene BRL1(|061{2St-ans-.1,}Diciloropropene BRLi0H1.1 Ethylb€nzene BRL67€al H€xachtorobutadien€ BRL591.78€ 2-H6xanone (l\rBK) BRL96{?$ Jsopropy,,benzene BRL9!1.E7-B +lsoptopyftoluene BRL1eg4!1 M€hytted-buty{ eher BRL1o&i0.i 4-Methyl_Z_pentsmne(M|BK) BRL7s.{r$2 Methylenschtoridesl-zG3 Naphthalsne103{6n n-PropylbefEene
BRLBRLBRL
Ug/kg wet 5.1
Irglhgwel 1O2
pgrkg wel 5.1
pgy'kq lvet 5.1
pgy'kg wel 5.1
lgukg wet 5 1
U94(g wet 5 1
fg/kg wet 5 1
pg/kg wet 1O.2
!g/kg !!€t 50.9
!g/kg wet 5.1
rc/kq wet 5-1
|lgftS wet 5 1
pg/kg wel 25.5
pg/kg weI 5.1
!g/kg wel 5.1
!g/kg wet 1O.2
ug/kg wet 5.1
pgr'kg wet 10-2
yg/kg wet 5.1
rc/kg wel 5.1
pgr'kg wel 1O2
lqn(gwol 5-1
pg/kg wel 5.1
pgL/kg wet 5-1
pgr'kg wel 5.1
lgr'kg w€t 5-1
lgukg w€t 5-1
lgr'kg wet 10-2
!g!kg wet 5.1
!g/kg wet 5.1
!q/kg wet 5.1
lgr'kg wet 5.1
lgr'kg wel 5.1
!g/kg wet 5 1
pg(g wer 5.1
Fqkg wer 5-1
!q(9 wer 5-1
lgy'kg wet 5.1
lgyr(g wet 5 1
lqy'kg wet 5.1
u4kg lv€t 5 1
trg/tg wet 50.9
!9y'k9 wet 5.1
!g/kg wet 5.1
!gA9 wet 5.1
!g/kg wel 50.9
lgr't(g wet 50-9
lCftSwel 5-1
pgks rvel 5-1
sw 846 826091
I
I
1
1
1
1
1
I
1
1
I
7
1
1
1
1
I
1
I
1
1
1
1
1
1
I
1
1
1
1
1
1
1,1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Thit labo.alory epsrl h ,to, w:lu xtitkott sr. zzthoried iignature on thc co,eF pzge.
+ Reportable Detection Limit BRl- = Below Reporring Linit Pag€ 43 of l5?
Page 399
Sampl€ ldeptificationM8FFl
sA5%81-09
CliEnt P$iect #301-88
MattixBallast
Collection Dat€y'Tirpel5-Mar47 00:00
Receavedl9-M6147
CASNq. A^o+k(s) ncsub Flq UnlE *RDL Diluiotl Itdhod Rif, Prepsrctl Andwd B,drh A^4lfst
10(H2-5 Sryr€ne63G2OS 1,.1,1,2-TetEchloaoehene7934-s 1,1,2,2-TetrEciloroethane127-18-4 T€trachbro€thene108-a€-3 Tolu€ne876i6 1,2,9-Trichlo.obenzen€120{2-1 1,2,+Tdchlorobenz6trte71-55-6 I ,1 ,1.Ti{*toroethane79{tr5 '|.1,2-Triahloroethane
79{1{ Trichlorosthene
Vohtll€ Orgrhlc Compounds
Volatile Oroanic ComooundsPr@ar€d by method SW846 5035A Soit (low levet)
BRLBRL
BRLBRLBRL8RLBRLBRLBRLBRL
?5{9-4 TrichlorDfluoromethane (Freon 11) BRI-96-18-4 i.2,3lTrhhtoroprop€ne95-636 ,|,2,+Tdrnethytbenzene
108-67s l,3,tTimehylbenzene75414 vinyldllodde1330.20-7 m,p_Xylenes5-17{ o-Xt€ne10$e€-9 Tebah!'drofuran6{f2$7 EtVle&Er994{5{ led-amytmehyledr€f637{2-3 Edrti tert-butyt etherto&20-3 D-isopmpytether7565{ T6rt Bulaflol / butyt alcohol12191.1 1,4-Dioxane
sunDgala rEcoyer?€sr?160401 +BtufioEuorcbenzene2037-26.5 fofuene4g11otuot-o 1,2-Dichlo@elhEne441e6+$,7 Abrcfiofluo@methane
VOC Exhaction
Ertrrctrbl€ P€trolerm Hydrocarbo13
Exhadable Total Petrobum HvdmcarbonsPrepar€d by metltod SW8.l6 35508800tr1 -9 Gasoline$476.3G2 Fuel Ol f268a7e3r-3 Fu€l oal #4685s3-dla Fu€t Oit #6t1098o00o0 Motor olJ00100000 Aviation Fuel
unidenlifiedOlEr OnTotal Pddeum Hydroca6onsCSC36 Alipfialic Hydrocarhons
Suarog'at€ r9co€rbs.3306.3}2 1-Chlot@ctadeqrne
Samlvolra e Orgrdc Co|nporld! by GCOroanochlodne Peslicides SW846 80BtAPrepared by mothod SW846 355083xr40.2 Atdrin
VOC 20-Mar-O7 20-Mar47 7031156 BO
BRLBRI-BRI
BRLBRLBRLBRTBRIBRLBRLBRLBRLBRL
105107116t6
Field €xhacted
$ftS wet 5.1
$^g wet 5-1
lSrtSwel 5.1
|rgrv€wet 5.1
pg/kg w€l 5.'l
Ug/kg w€t 5.1
|lgr'ftg w€t 5.1
pg/kg wet 5,1
$/kg vrel 5.1
lg^gwet 5.1
lgr'kg wet 5.1
!g/I(S rv€t 5.1
UdkS rct 5.'l
ldkSwet 51
IdkSwel 5.1
pgftgw€t 10.2
pgr'kg wel 5.1
!9/k9l€t 50.9
$E/kgwet 5-1
gglkg $/et 5.1
pg/kg wet 5-1
rc/kg wet 5.1
lgtswel 5O.9
ldkg$€l 102
7G1iO %
70-130%
70-130%
70-t30
mg,l(g n.2mS/kS 30.2fiEI(S 30.2mg/kS 30.2n€/t€ 30.2mgn(g f i .2|rrSftS 3O.2rrrg/kS n,2mgr,xg 30.2n'gftg 3O.2
tltttlo %
1
1
I
I
1
1
1
I
1
I
1
1
1
1
1
I
I
1
1
1
I
I
I
BRLBRLBRL8RL8RLBRLBRLBRLBRLBRL
114
wn(s SV\r446 8081A 2143f47 25-Mat47 7U,1'171 TG
Ihb laborator! rqod k nd vdd *irtort a, aqdroriad dgdofrtE oa tlE cowr pagc.
' Reportrblc Dete4iod Lidit BRL - Below Rcporting Linir Page 44 of 152
Page 400
Sample IdentificationMSFB-IsA5946449
Client Proiect #301-88
Collection Dat€/Timel5-Mar-07 00:00
MatrixBallast
Receive.d
l9-Mar-07
CAS No, Anatrte(s) Result FIsg Units *RDL Method Rrl Prcparcd AnalJ,aed Bdtth Ada4sl
Semlvol|tile Orgrnic Compoundr by CC
Orqanodrlodne Pe$ticides SW846 8081A
Prepared by method SW846 35508
319-84€ a_BHC31$asF7 b-BHC319{6-€ d-8HC58{9-9 g-BHC (Lindane)
5l-7+S Chlordane72-54-a 4,4-DDO (p,C)
72{ts 4,4-DDE (p,p')
5{F2s3 4,4-DDT (p,p.)
6{157-1 Dielddn95+9€{ Endosulfan I33213{+9 Endosulfan Ilr03r-o7-8 Endosulfan sulfate12 -m+ Endrin74Zl-93{ End.inAldehyde76-,14-{l Heptachlorn43-5 MetlErychlori021-57.3 Heptachtor EpoxideE{D1-3$2 roxaphene5103-71-g a-Chlodane5,s66-34.7 gFchlordane
53494-7Gs Endrin K€lone
S{ttwata racov€r'€sl1038f.8+2 4,1-D&Oclafluorobipheny! (54
m5t-2a3 Decachlorobiphenyl (Sr)
Polvchb.inated Biphenvls bv SW846 8082
Prepared by method SW846 35508
12G7.-r1-2 PCB 101611104-23.2 PCB 122111141-rC5 PCE 1232
$.46921 I PCB 124212872-2p4 PCE 1248i1097{9-1 PCB 125,4i1@€-82-5 PCB 126(}3732+2T5 PCB 1262i11(xrl4.4 PCB 126€
SartogEle rgcoMenesjto38c6+z 4,+DB4cbnuorcbiphenyl (Sr)
m51-2+3 Decachlorobiphentt (5.)
Senivotrtile Org.nic Compoutrdr by GCMS
SW8468081A 21-Mat47 25-Mat47 7031171 rG8RLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
BRLBRLBRLERLBRLBRLARLARLBRLBRLBRL
74130
BRLBRLBRLARLBRLBRL8RLBRLBRL
80115
8RLBRL8RT8RLBRL8RLSRLBRf
!gftSpgftg
ug/Kgpg/Kg
UEKS
lrg/K9
!grkspok9ps&9
!s/ks!s/ks!g/ks!gftgpqlks
!sftsrc/kstrs/KslJs/ts!gag!gr'(g!g/ks
14_2
14_2
14.2
71.O
14.2
14.2
7.00
14.2
14.2
14_2
14_2
11.2
1 4 2
71.O
14-2
14.2
14.2
I
I
1
1
1
1
1
1
1
1
1
1
1
1
1
1'1
1
1
I
1
30,150 %30-150 %
psr(s!sr(s!g/ksps/ts
!g/ksusftgugftg!g/Kg
trg/ks
pgfts
rrg/(gusftg
usftgug/kgPgftgpsfts
!9/kg
24.4
28.4
24.4
24.4
24.4
24.4
24.4
24.4
24.4
30-150 %30-1fi %
Somivolatile Oroanic Compounds bv SW846 g?70C
Prepared by method SW846 3550863-32€ Acenaphth€nea)a.96-8 Acenaphthylene62€93 Anitin€1AI,l2-7 Anlhracene1912.2'l-9 Atralne10333-3 lzobenzene/Diphenyidiazin€
92{7-5 B€nzidine56-5+3 8€nzo (a) anth.acene
SW846 8270C 22-Ma(O7 2UMat47 7O312A2 M.B745
749
749
749
749
749
749
749
Thh laboNtory repo.t k nol jolid toithoar an aathoriTrl signattE ol the cover page-
. R€portable Detection Limit BRL = Below Reporting Limit Pase 45 of lJ2
Page 401
Sahple ldetrtihc{tionMEFB.lsA59,16,|-09
Cliept Project #301-68
MatixBallast
Receivedl9-Mar-07
Cotlection Datc/TimeI 5-Mar47 00:00
CAS No. Ahalye(s) Flag ania 'RDL Diluiod Method Rel. Preparcd Awltr,ed Bolch Analfsl
Semivohtile Orgmic Compo{nds by GCMS
Semivolatile Oroanic Co,npounds bv SW846 8270C
Prepared by method SW846 35508
50-32{ Benzo (a) pyrene205-99-2 Benzo (b) fuoranthene191-24-2 Benzo (g,h,i) perylene207{€-9 Benzo (k) f,uo€nthene
BerEoic acid1CD-51{ B€ftzylalcoholll1€r-1 Bis(2rhloro€thory)methaner1laa{ Bis(2-chloroelhyl)etE.3efie32{ Bis(2-ohloroi6opropyl)ether117{1-7 Bis(2-edrylhexyt)phthaiate101.55'3 4€romophenytphenylelher454&7 Buty' b€nzyl fithetate86-744 Cathazole5S50.7 +Chloro-3-metrrylph€nolro6-1ru +Chloroaniline91{8-7 2-Chloron6phthalenessz{ 2-CNorDphenol7005-72-3 +Chlodopheny' phenyl €ther2i8{1-9 Chrysene53-?G3 Oabenzo (a,h) anthracene132{4-9 Dibenzofuran95.:41 l,zoichlorob€nzenes4i-7}1 .l,3oichlorcb€nz€ne
ttrF4eT 1,4-Dichlorobenzen€91-34,1 3,3--Dichlorobenzidin€12(]"83-2 2.+Dichtofophenols,!46.2 Oiedryt phhatate131-r1-3 Darnethyl phthatate105{7-9 2,4-Dimethylph€mlB1-74-Z Di-n-butylphthalatsss4-52-1 4,6FDinjtro-2fiethylphenol51-28-5 2,4{)initrophenol12r-14.2 2,Goinitrcbluene60cat-2 2,&Dinitrotoluene117-6.1{ Di-n{atylphthatetea}6-444 FkJoranthene46.732 Fluo(enei16-74.1 Hexad Oaobenz€nea7{{l-3 l-l€xachtorobutadiene77474 Hexaafilorocydopentadi€ne67-72-1 Hexactoroethane193-3ss Indono (1,2.$cd) pyrene90{2-0 i-l,l€S1g$aph(1alene7S5{}l lsophorone91-57{ 2.iletfrylnaphtfialene95-4&7 2-Mgdtylph€nolro&394, 3,4-fttethylphenol106-,t4,5sl-20-3 Naphthalene&741 2-Nitroanilane99-092 +Nitroaniline
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRfBRLBRLBRLERLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLERLBRLBRLSRL8RrBRLERLBRLSRLBRL
BRLBRLBRLBRL
BRLBRLBRL
!s/ks!gftSrsikgt gftg
ti0/t9
FqkSPg/k9!sr(sLrsftslgks|€T€us^sus/ksus/kgpElq
$srksuslks!s/kspsiks
WftsFgk9p9&9pgks
!sr(srcfts!sftsrcn(s!9ft9
usrkspcftsp4ks
!sftsusftsrcftgt s/tg!s/k9ys/kspdkgpdks
usr(s|lsfts
!sftg
Et,ksl|grkgpgl(s
I,rd*9pg/kg
|lgI(Sugftg1€ikS
749
7{9
749
749
749
749
749
749
749
749
74S
749
749
749
749
749
749
745
749
749
749
749
749
749
749
749
749
749
749
749
749
749
749
749
745
749
749
749
749
7,19
749
z,t9749
749
749
749
749
749
719
74S
SW846 8270C 22-Met47 254t,,et47 703128i1 M.8
Ihlt l4borehrf Eprt 16,tot eali.l pirhout an a hodz.d tignauE on tht qt , page.
'Reportabl€ D€tection LiEir BRL = Betow Reponing Limit Page 46 of | 52
Page 402
Sarflple ldentificationMSFB-1
s459464-09
Client Proicct #301 -88
Collection Date/Timel5-Mar47 00:00
Matrl{Ballast
Received
l9-Mar-07
CAS N.L Anaut4s) Flry Ani6 *RDL Diltttion Method Retr. PnpEd AnaIWl Bot h Antllst
S€dvotatil€ Organic Conpounds by GCMS
S€mivolatile Orcanic Comoounds bv SW84ti 8270CPrepared by method SW846 3550810G0t{ +Nitro€niline98€+3 Nitrobenzen€{lll-75{ 2-Nitioph€nol10G@-7 +Nitoph€nol62-7ts N-Natmsodimef,rytamine6219-7 N-Natrcsodi-n-propytamine8e3o{ N.Nitrosodiphenytamin€07{6-5 Pentachloroph€nolC5{1{ Phenanthren€10+95-2 Phenol'l2gOO{ Pyaene11046-1 Pyridane12G€2r |,2,4-Taichlorobenzene96-954 2,4,$Trichlorophenol88{Fz 2,4,GTrichtoroph€nol
S.Jarogate recover'€s:32150-8 2-Fluorobiphenylfi7-121 2-Fluorophenol4165604 Nitr,benzene4141r,!rt2-2 Phenol4st71e5t4 Ierphenyl-d!4118-7 44,&Tibrcmophenol
Totrl Metab by f,PA 6000/7000 Scri€s Methods
7439{7€ Mercury BRL
Total Metlls by f,PA 200 Series Methodr
BRL
BRL
10.8
0.626'1.97
5.08
BRL
1 SW846 8270C 22-Mat47 2sMaFOT 7O312A2 M.B
1 '
1 "
1 "
1 '
1 '
1 "
1 '
1 ' ,
1 '
1 '
1 '
1 "
1 "
1 '
BRLBRLBRL
BRLBRLBRLBRLBRLBRL
8RLBRLBRLBRLBRLARL
392633284427
PSI(S 3000
pgftS 749
!S/kg 749
Ug/kg 3000
Ug/kg 749
l.iSftS 749
lgftg 749
!g/kg 749
lgftg 749
!g/kg 749
tS/kS 745
!g/kg 749
pg/l(g 749
lsftg 749
pS/kS 749
30-tu %
t u t 1 0 %
m-130 %
t r l t o %
30'1n %
11110 %
ftg/kg 0.0295
mg/kg 0.920
nE/kS 1.38
mg,kg 0_450
mg/kg 0 230
mg/kg 0.460
mSftS 0.690
mS/kS 1.38
mg/l 0.0100
mg/ 0.0150
rngl 0.0050
mg/t 0.0025
nE4 0.0O5O
mg/l 0 m0+o
mgl 0.0075
rhg/l 0.0150
?.4G22-4 Silver
74rr&3&2 Arsenic
I44G3&3 Sadum
744043-9 Cadmium
7rt4o-47.3 Chromium
7439-92-1 Lead
Z€?492 Se|enium
SPLP Mctrk by EPA 1312 & 6000/7000 S€ri6 Merhodt
SPLP Extraction Cornple{ed
7440-2-4 Silver BRL
71.10'3&2 Arsenic 8RL
71-40-39.3 Badum 0_0066
7rt4H$9 Cadmium BRL
71-1047-3 Chrcmium BRL
7439.97.6 M€rcury BRL
743S92-i Lead BRL
1'782-t92 Selenium BRL
1 SW846 7471A 26-Mar-07 26-Mal'07 7031311 YP
1 EPA200.7 26-Mar-07 26-MaF07 7031263 LR
1 "
1 ' ,
1 '
I '
t SW8461312 21-Ma(47 21+,/tat47 7031229 BO
1 SW846l31Z6O10a 22-Mat47 z4-Mat-Ol 7031323 LR
1 '
1 "
1 '
1 SW8,f6 131217470A " 23-Me.47 7031324 yp
1 SW846131260108 " 24-Mat47 703'1323 LR
Thh lab.elory rcpod is not valid ts hoa an authorized slgnalare on the cover page.
' Reporhble Detecdon Limit BRL = Below R€portinC Limit Page 4? of 152
Page 403
Sarrple ldentific{tioflMSFB-2sA59464-r0
Clieut Proiect #301-88
MatrixBallast
Collectiotr Dat€/TiEeI 5-Mar-07 00:00
Receivedl9-Mar47
CAS Na Anebt4s) Fl"8 Unili *ADL Dltalian Mahod nej Prcpered Analfred Bdlch Analtsl
Vohlile O.gaf, ic Coupotrnds
Volatile Orqanic CompoundsPrepared by method SWa46 5035A Sdl (tow levet)76_131 t,1,z-Tndlbrctdfluoroethane(FreoBRL6744-1 Acetooe BRLt07r91 Ad.ttonitile BRI71112 BerEene BRL1o8-8s1 Brcrnobenzene BRL74.97.5 Bfomod oromefiane BRLf5-274 Brffnodidtloromethane BRL-15-25-2
Bfomoform ARL74{3-9 Bro|r|omelhane BRL78-e3-3 2€ubnone (l!lEK) BRL1lM-sl{ nlButylbonzene BRL13+96{ sec-Bu!y'b€nzene BRL9A{6-€ teft-ButytbefEene BRL75-1s{ Carbon disutfide SRL5d23-5 Carbon tsbachtoride BRL10&9e7 Ct odobeEene 8RL75-{)0.3 ChiorD€lfEne BRL67{&3 Chlorcfonh BRL74-9t.3 Chloromethane BRL!'$4+6 2-Chlorotoluene BRL10€-43.1 +Chlo{obluene BRL116-i2-a 1,2-Dabrorno-3-chloropropane 8RLt24-4-1 Dibomochlorcmehane BRL10Ge3-4 1.2-Dib6moefian€ (EDB) BRL7{{$3 Ditromo.nethane ERL95.50"1 l,2oichlorob€tEene BRL:,41-73-1 1,3-Oichlofobenz6ne 8RL106-46.7 l,+Dichlorobenzene BRL7+71-a Dichlorodifluorcmethane (Freon12)BRL75-3.{-3 |.1-Dichtoroethane BRL10746-2 |,2-Dichloroethane BRL7t35-4 |,1-Oicfiloo€thene BRL15&5e2 cis-j,l-Dichloroethene BRL156€0-5 tans.1.2-OiafitoroettEne BRL7817-5 l,2.OichlotEpropane BRL142-28€ l,3-Dichloropfop€ne BRL594-2{l.7 2.2-DichtoroF.opane BRL56358{ l, l-Dlchloropropene gRL
10061{1-sciel,3oicfgoNopropene BRL10061€{trans-l,3.DichbIopropen€ BRLioGal-4 Efiylt€nz€ne BRL876&3 Herecfilorobutadie{e BRL5e1-78-6 2-Hexanone (MBK) BRf98{2{ tsopropylbenzene BRLs&47{ +troprqyltoluene BRL1634.044 M€0iytted-buD4 eth€r BRL10&r0'r +M€thyl.2-p€ntianone(MIBK) BRL75{s2 Methybnecfilodds BRL91-m-3 Naphthalene BRLt0l€+1 n-PropylbffEeoe BRL
SW 646 8260S 22-MIFO7 22tJls47 7031291 RLJtEftg wel 5.2
pg/kgwet 104
!g|/l(gw6r 5.2
ldkg lv€l 5.2
lgL/kg w€t 5-2
pgr'kg wet 5-2
l8rkg wel 5.2
!g/kg wet 5.2
Ug&g wel 10.4
pdkS vret 51.S
f.ig/(g trst 5-2
lgr€ Yret 5-2
pgn(g wet 5.2
rdkgwet 259pg/ftg wet 5.2pdkg wel 5.2
ld lSw€l t04
ldkg Yv€t 5.2
lgtkg wet '10.4
yg/kgwet 5.2
Ig/tqs,et 5.2
lgtgwel 10-4
pgrkg wel 5.2
ldkSw€t 5.2
lgl(g r,'/et 52pS4(S Yrst 5.2
t g/kg wet 5-2
psrkgwet 5.2
pg'kgwel 10-4
!g/kg wel 5.2
ldkS !ve! 5.2
lgL/kg w€t 5.2
lgkS rY€t 5.2
lrS/kgwst 5.2
Pg*Ow€t s.2pgkg wel 5.2
!g/kS wel 5.2
Igr'kg w€t 5.2pdkSwet 5.2pdkS rYet 5.2
!g/kg v{et 5.2pgl(g rcl 5.2
lgkg w6t 51.S
!g/kg wet A2
Ugk€ v/ot 5-2
ldkS vret 5l
trtgr'kg vr6t 5t,9ySikS wel 5l.S
Fg,kg w6t 5.2
!g'kg wel 5.2
Thb labontory Eporl ie .tol vzlitl *lthout M zttdrottzd slgnalarc od ,hz {,,ver' page.
'Rcporiable Detectior Limit BRL = Bctow p.€pofting Linit Pa€e 48 of | 52
Page 404
Samole ldentificationM8FB.2SA5946jl-10
Client Proiect #30 t -88
Collection Date/Timel5-Mar-07 00r00
MatrixBallast
Received19-Mar-07
CAS No- A^alrte(s) Result FloC Ani,l IRDL Dilation Method ReJ PEpaRd A,nuied Balch Aiabxt
Volttile Organic Conpoonds
Volatih Oroanic ComooundsPrspared by method SW846 50354 Soit (tow tevet)100-42-5 Styrene6:10-20{ 1,t,1,2-Tetrachloroethane79-34-5 1 , 1 ,2,z-Tetmchloroethane127.184 Telr€chloroethene108{83 Toluen€
87i16 1,2,3-Trichlorobenzene12(182-1 1,2,4-Trichlorobenzene7t-sfF6 |,1 , t -Trichtoroethane
794Gs 1,1_2-Tichtorcethane
BRLBRLBRLBRLSRLBRLBRLBRL8RL
BRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
1091M105100
Field extracted
BRLBRLBRLBRLBRL
BRL8RLBRLBRLBRL
122
BRL
!g/kg wet 5.2
!g/kg wet 5.2
Ug/kgwel 5.2
pg/kg wet 5_2
pC'kg wet 5 2
pgykg wet 5.2
!S/kS wet 5.2
!g/kg w€t 5-2
pdkgwet 5.2
lig/kg wel 5.2
pg/kg wet 5.2
!g/kg wel 5.2
!g.eg wel 5.2
pgr'kg w€r 5.2
pg/kg w€t 5.2
!g/kg w€t 1n.4
Ug/kg w€t 5.2
!g/kg w€t 51.9
jJg/kg wet 52
pS/kS wet 5 2
uS/kS Yrel 52
Ug/kg wel 5.2
trg/kg wet 51-9
!g/kg wel 104
70-130 %
70-130 %
70-1m%
70-tm %
nE/tg 25.4
mSI(g 25.8
mSn(S 25.8
mg/kg 25.A
rngftS 25.8
mg/kg 25.4
mS/tS 25.8
mgftS 25.8
mg/kg 25.8
mSI(S 25.8
44-140 %
pS/tg 13.8
l
1'|
I
1
I
I
1
1
1
1
1
I
I
1'|1
I
I
1
1
1
1
1
SW846 82608 22-MaF07 22-Ma?01 7031291 RU
79{16 Trichtoro€thene BRL7s{9-{ Trichtorofluoromethane (Freon t1) 8RL96-14-4 .1,2,lTrichtoropropane
95-6ire 1,2,+Trimethylb€{zene108{7{ 1,3,s-Trimethytbenzene75-0i.4 Vinyl chlodde'1330-2G7
m,p"Xylene96-47{ G.Xylene10$€$€ TetrahydrofuEn60-2$7 Ethyiether994-09F8 Tert-amyl methyt ether637-92-3 Ethy ten-butyl etheri0&2G3 Di-isopfopytether7s€r,.{) T€d_Butanol/butylalcohol12$9in 1,4-Dioxane
Surrogale r€cou€niesi460404 A4.cmofluorcbenzene
m3r-2c|5 Toluene-dB
tr0644/4 l,2aichtorcethane-d4
1ffi8-5i-/ Abromoffuorcmelhane
VOC Extraction
Extractrble P€trolcum Hydrocarbofi s
Extrectable Total Petroleum Hvdrocadons
Preparsd by melhod SW846 35508
800ffi1-s Gasoline6€47d3o-2 FuelOil#26847+31-3 FuelOi l t4€€55+o0-a Fuel Oil l(5M09m00(xl Motor OilJA100O0O Aviation Fuel
ljnldenlified
Oth€r Oil
Total Petroleum Hydrocarbons
Cg-C36 AliphEtic Hydroc€rbons
St rTogele rEcov€riesi?3a6-33.2 1-Chlorooctadecane
Setnivohlil€ Orgrnic Conpouhds by CC
Orqanochlorine Peslicides SW846 8O8lA
Propa.ed by melhod SW846 35508
30s0G2 Aldrin
VOC 20-Mar47 20{1ar47 7031156
+CTETPH 224lla(47 26nna'{7 70312A3 DS
SW846 8081A 21-Mar47 2&Mar-07 7031171 TG
Thit labototory rcpod is aot edid taithozt an au&odzed signature on the corer page .
* Reporlable Detecrion Limir BRL = B€low Reoo{tine Limit Page 49 of 152
Page 405
Samole ldeotificationM6FF2sA594*10
Clie P.oi€ct #l0r-88
Collectiou Date/fimet 5-Mar-0? 00:00
MarrixBallasi
Receivcdl9-Mar-07
CAS No. Analyu(s) nesu! Fhs 'RDL Dilztioa Irlcthod Rctr Prepued AnolyzTn Bdch Arultaa
Semivolatll€ (kg.ric Compolrds by GC
O.oanochlorine Posticides SW846 8081A
Prepared by .nelhod SW846 35508
3l$416 a-BHC
319{5.7 b.BHC
319{6€ d-BHC
5€{+e 9-BHC (Lirdane)
57-74-9 Chlodane
7?-544 4,4-DDD (p,p,)
72{5€ 4,4-DDE (p,p')
50-2s3 4,4-DDT (p,C)
60-57-i Dl€lddn95+98{ Endosulfan I
332i$65-9 Endosulfan lli031-07€ Endosulfan Sulfate72-204 Endrin7421-93{ EndrinAjd€hyde79'114 Heptactrlo(7243-5 Methorydrlor102rL57-3 Heptachlof Epoxid€800i.3S2 Toxaphene5103.719 a-Chlodane5566-34-7 g-Chtodane
53{9+70.s Endrin Ketcne
&rTogal€ rBcaveres-,1oia68+2 4.4o&Octaf,rcmbiphenyt (54
n51-24-s Decachlotobiphenyt (Sr)
Polvchlorinated Biohenvls bv SW846 808iPrepared by rnethod SW8,'G 35508
1267+11-2 PC8 10161t1O+28-2 PCB In11r14i-16-5 PCB 12325346921-9 PCB | 24212612-E$ PCE] 1248ilo97s$r PcB 12541 r0s6-82€ PCB I m03132+*5 PCB 12621110S14{ PCB 1268
Su''ogafe rEcovdrbs.'lNse8+2 4,U)+OataflrMtobiph6nyt (54
m51-24i Decachlotobiphenyt (Sq
Semircladle Ory. c Comportrdr by CCMS
Semivolalile Orqanic Comoounds bv SW846 827(rcPrepared by method SW846 35508€g.324 Acen@hth€ne4&96-8 Aconaphthyt€ne62.s+3 Aniling1a).12-7 Anhrgcen€19i2-24-9 A!.azjne103.3?3 ArobenzendDlph€nytdiazin€9247.5 Benzidlne5ssta Benzo (a) a.lhlac€ne
BRLBRLERLBRLBRLBRLBRLgRL
8RrBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRL
76109
BRLBRLgRL
BRLBRLBRLBRLBRL
BRL
801 1 5
BRLBRLBRLBRLBRLBRLBRLBRL
Fs/k9usftst€fts!g/ksug/ksPsn(s|rsftspsfts
!s/ksPgl(s!glksyg/ks
Psftspsfto
lrsAstiS/k9pg/k9psr(9
usr(gpsrkspdrs
13.813.E1 3 81 3 868.9r 3 8r3.813.87.0013.8'13.8
1 3 I13.8t3.8r3.813_813.068.913.8r3.8r3.8
27.5
27.5
27.5
2f .5
27.5
27.5
3G150 %& l f i%
sw8.r6 80814
sw846 6082
1
1
I
I
I
I
1
1
1
I
I
I
I
1
1
I
t
1
I
1
1
21-Ma(07 2&Ma(41 7031171
FSftg
Fs/tg
Fgikg
Fs/ksPgr(strsastrgftsps./kspsft9
us/ksvcr(gPryKSps/rs!s/ksugftg|,9nlgusits
214t|a147 2d.Matr47 7031170 SM
30-150 %3Gtfl %
841
641
641
641
u1u1641
641
sw846 8270C 22+,,lar$ 25+rs{7 7031282 M.B
Thb laLodory report it @t valid t{Uhoat aa atthorizd stgnarnre on the cov.r pqe.
' Rcportable Detection Limit BRL = Below Repo.rine Limit Fage 50 of | 52
Page 406
Sample IdentificatiorM8FB.2sA59464-r0
Client Proiect #30 t -88
Collection Date/Timel5-Mar{7 00:00
MatrixBallast
Receivedl9-Mar-07
CAS No, Anatrta(s) Resall FIag A n s *RDL Dilurian Method ReL Prcpued Anabzed Bdtch Atlalyst
Semfuol.dle Org.nic Comlounds by CCMS
Semivolalile Oroanic Compounds bv SW846 8270CPrepared by method SW846 35508
lO-32{ Benzo (a) pyrene
2os9+2 Benzo (b) ffuoranthenei91-24-2 Eenzo (g,h,i) perytenem7{8-9 Benzo (k) fuoranthene65-05{ Benzoic acid10G51{ Benzyt alcohol111-91-1 Bis(2-chloro€thory)methane111-44-4 Bis(2-d oro€thytFther3e€s32-9 Bis(2.chloroisopropyt)€therri7-e1-7 8is(2-ehytheryt)phthalatet0r-55-3 +Bronrcphenytphenylether85{&7 Butyl benzyl phthalate
E6-7+€ carbazole59-5G7 4-Chloro-3_melhylphenol106{7-8 4_Chlofoanilane91.5+7 2-Chtoronaphthatenes.s74 2-Chtorophenol700$72-3 +Chtisrlrphenyl phenyl ether2l&{11-g Chrysene53-70-3 Dibenzo (a,h) anthracene132€4-9 Dibenzofuran95-6G1 1,2-Dichlorobenzene
541-Zlr 1,3-Dichtorobenzene'106'tG7
1,4-Dichlo(obenzene91.9,r1 3,3'-Dichlorobenzidine12()'83-2 2,4-Oichlorophenolu46.2 Diethyt phthalate
13t-1tr Dirn€lhyjphthatate105,67.9 2,+Dinethytphenola4-74.2 Di-n-buvphthalate534-s2-1 4,6-Dinitrc-2-methylphenol5r{8-5 2,4-Dinitrophenol121-14-2 2,4-Dinitrototuene60+m-2 2,6-Dinitrotoluene'll7+4{
Di-n-octy,tphdrslate20fr4{ Fluo@nthene
0G7$7 Fluofene11S74-1 Hexachlorobenzene87$€-3 Hexachlorobutadienen474 Hexachlorocyctopentadiene67-72-1 HexachloroethaneiS3-39{ Indeno (1,2,3-cd) pyrene90-12-0 1-Methylnaphhatene765+1 lsophorone9157$ 2-Methylnaphthatene95rl&7 2-Methytphenol
10€-3€-4, 3,4-Methylphenolltxi-44-591-2G3 Naphthatene4l}714 2-Nitrosniline90-0!!2 lNitroaniline
BRL8RLARLBRLBRLBRLBRLBRLARLARLBRL8RLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL
BRLBRL
BRLBRL
BRLBRLBRL
!s/ksLjsftgtls/k9!s/kgrc/kspeyK9ps/ks
!g/Kgpsfts
rcftsps/ks
tjgft9
ugks!s/ks!g/ks!g/Kg
Lig/Kg
!g/Ks
ug/kslrq/Kg
LiS'"(S
us,ksugts!s/kspg/ksps/kg
Li9/Kg
Ljsftgpgfts
!sftg
|lg/r(g
!s/ks!s/rs!sr(sugksudksps,4(gpsr(s
!s/tsLiS/kgugftsLis/xs
!gftspsfts
|lglkgpg/ks
!gftg
lsik9
!s/ksus/t(s
641
a+1641
641
64'l
641
641
641
a+1a+1641
u lu1641
641
64r
&11
&t1
641
641
641
641
641
641
u 164'l
641
&t1
&{1
641
641
641
641
641
641
641
641
641
641
an1
641
641
Bl1
641
u1641
u1
641
64'l
641
SW846 8270C 22-Ma(O7 25-MarO7 7031282 M.A
Thb lsborutory rcpod ir ttol valhl withoa att aalhoriZed slgaalurc ott ihe corer psge
* Reportabl€ Detection Limil BRL = Below ReDortins Ljmit Paee 5l of 152
Page 407
Sarnple IdcntificationMtFB.2sA5946L l0
Cliert Pioiect #30 t18
Collection Date/Timel5-Mar47 00:00
MatrixBatlast
Received| 9-Mar-07
CAS No. Andltu(s) ResuL Flae UniB 'RDL Dllutlan Lrahod Retr Prcpond Analyzcd Balch Arultsl
Semlvokdle Organic Compound! by CCMS
Semivolatile Oroanic Comoounds bv SW846 8270C
Preparod by m601od SW846 35508100{1{ +Nitoaniline98-9+3 Nifobenzene{18-75-s 2.Niuophenol10(}02-7 +Mlrophenol62-754 l,l-Nifo6odim€thytamine621€{-7 N-Nitosodi-fi-propylamine86-30{ N-Nitrosodiphenylaminee7{6-5 Pentiaciloroph€nol854i-0 Phonanthrene10&95-2 Phenol129-00{ F}r€ne110-8€-1 q/ridin€120€2-1 1,2,+Tridlorobenzen€96-95-,1 2,4,5-Tfichlorophenolaa{6-2 2,4,GTrichlorophenol
Sarzogrle a€corrgresl3214G8 2-Fluorobiphenyl367-124 2+luotwhend4165,@4 Nitobenzene4s416+s2-2 Phenol4st71A-514 Terphenyl4l4t 1 8-79-0 2,4,6Tl'}tumophenol
Torrl Metr|! by EPA 6{Xxrflt00 scries M€thodi
BRLBRLBRLBRLBRI-BRLBRIBRLBRLBRLBRLBRLBRLBRLBRL
4024303043
ISitS 2570pg/tg U1
FSftg 641pCftS 2570pgks 641pS/kS d{l
ldkS 641
Ug/kg 641
!g/kS U1
tSftS 641
tgftg 641
US/kg U1
pS,}€ 641pSrl€ 641
n-130 %l5-110 %30-1n %ttf io%36tm%15.110%
mglkg 0.0295
mS/kg 0.991
mgikg 1.49
mS/rg 0.49{t
ngts 0.248
mgkg 0.496
mg/kS 0.743
mS/kg 1.49
mgn 0.0100
rngl 0.0150
n€n 0-0050
ntSil 0.0025
mgn 0.q)50
mdr 0.m040
mS/l 0.0075
nE|4 0O15O
2 .{ar47 7@1 324 yp
23-Mar{7 7m1323 LR
SW8/68270C 22rylar{7 2grr€r-07 70:}1282 M.B
7439-97{ l\rercury
Totd Metsb by EPA 200 Serles Methods
744F.224 Silvqr
74,4G3+2 AF€nic
7440-393 Badum
zr40-4+9 Qsdmium
74.t&47-3 Chromium
744942-1 Lead
z82.rr9? S€t€nium
I SW846 7471A 26llar{7 26+ra.47 7031311 YP
1 EPAAn-7 26-|i{a.-07 26- ari7 7031263 LR
1 '
t "
1 "
1 ' .
1 '
1 '
1 SW8461312 21-tlar47 21tur47 7031229 BD
1 SW8.161312/6O108 22+'rd{7 2 vbr{7 7fi}1323 LR
I '
t '
1 '
1 '
I Sr/Ve46 131,y74704
1 SW8,16131?J€010S
BRL
BRL
BRL
0.506
3.22
BRL
SPLP M€bl! by EPA l3l2 & 6000/t00O Serte3 Meahodt
SPIP Extraction Compleied
74{n-22-1 Situ€. BRL
74-1rl3$2 Arsenic BRL
7r4O-3$3 g€rium 0.0092
744(H&9 Cadmiun SRL
7r4O-473 Chrcmium BRI
743997{ M€roury BRI_
7439€2-1 Lead BRL
z€a492 S€l€naum BRL
This labontory nwxt ls not valirl withord o eulhorledslgnatarc on tha cop.r psge.
! R€portable Detection Limit BRL = BeloF ReportiDB Limit Page 52 of lS2
Page 408
Sample IdetrtificationM8FB.3
sA59464-l I
Cliert Projecr #l 0 l - 88
Collection Datci/Timel5-Mar-07 00:00
Mat.ixBatlast
Received
19 -Mat-Oj
CAS Na Analtte(s) Resah Floq U,riB aRDL Dilutiofi Mc.hod Retr. Prcpond Amlyel Batch Anallst
Vohtil€ Orgrnlc Compo|rnds
VOC Exlraction
75{&2 Methylenechloride91-2+3 l{aphthalen€
lSikg 52.2
tS/kg 1040
LiS/kg 52.2
f.iSftg 52.2
yS/kg 52.2
I'Silq 52.2
trS/kS 52.2
pSrkS 52.2
FS/kS 104
!g/kS 522
!S/kS 52.2
!g/kg 52.2
Ug/kg 52.2
lSftS 261
pg/kq 52.2
lg/ftg 52.2
pdks 1O4
pS/kS 522
pS/kg 104
pg/kg 522
!g/kS 52.2
f.iglkS 1O4
pS/kg 52.2
rcfto 52.2
US/kS 52.2
pg/kS 32.2
pg/kS 522
lgn(g 322
!SA9 1O4
US/t(g 52-2
udkS 52.2
pS,4(S 52.2
!g/kg 52.2
!S/kg 52.2
!g/kg 52.2
pdkS 522
lSlkg 52.2
pgftg 52.2
lSftg 52.2
!Sn(S 52.2
pgftg 52.2
lSftg 52.2
USftg 522
ldks 52.2
W/kS 522
l,g/ks 52.2
!g/kS 522
lgftS 522
pgks 52.2
Field extracted voc 20-Mar-07 20-Mar-07 7031156 BDVolatile Oroanic Compounds Ro5Prepar€d by nethod SW846 5030 Soit (high tevet)
78'111 1,1,2_lrichlorotinuoro€ttane(FreoERL67-@,1 Acetone BRL107n3r Acrytonitrile BRL714Y2 Benzene BRL104-86-l Bromobenzene BRL74.97-5 Bromochloromethane BRL75-274 Bromodichloromethene BRL7$2$2 Bromoform BRL74{}9 Brortomelhane BRL7443.3 z-Butanone (MEK) BRL104-51{ n-Butytbenzene BRL135F98i sec-Bu{ylbenzene BRLsa{16.6 tert_Bulytbenzene BRL7s-1s"{r cabon disulfide BRL56-2+5 Carbofl tefachlorjde BRLl0&S0-7 Chlorobenz€ne BRL75{G3 Chloro€thane BRL67{43 Chtofoform BRL7147-3 Chlorornehane BRL95-494 2-Chlorotoluene BRLroG4+4 4-Chtorotoluene BRL9+12€ 1,2-Dibromo-3rhtoroprcpane BRL1zr|.{a-r Dibromochloromethane BRL106-e3-4 1,2-Dibtomoefiane(ED8) ARL744+3 Dibromomethane 8RL95-51F1 l,2-Dichtorobenzene gRL
5{1-7}1 l,}Dichtorobenzene BRL106-46-7 '1.4-0achloroten2ene BRL75.7i4 Dichlorodilluoromethane(Freoni2)BRL7+343 1,l-Oichtoroethane BRLt07-62 '1,2-Dichloroethan€ BRL753514 1,l-Dichloroeth€n€ BRLi5€-59-2 cis-1,2-Dichloroethen€ BRL15G60-5 b6ns-1,2-0ichtoroethsne BRL7E€7-5 ',2-Dichloroprop€ne BRL142-28-9 l,lDichloropropane BRL5,94-20-7 2,2_Dichloroptopane BRLs6,a58€ l,1-Dichlorcpropene BRL1006101-5cis-l,}Dichlorcprop€n€ BRL10061.02€trans-I,3-Dichloropropene BRL1rlc,-414 Etht{benzene BRL87-6&3 Hexachtorobutadiene BRLs91.786 2-Hexanane (MBK) BRLg8-€a€ lsopropytbenzene BRLs37'6 4lsopropyltoluene BRLr634-04-a Metht4 ted-buhy' ether BRLroFrGi 4-Meth!'l-2-p€ntanone(MIBK) BRL
BRLBRL
505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050505t)5050
SW 846 82608 21-Ma(47 22-Mat47 7031189 jro
Thit ldtoratory npod it not vzlitl h'ithoa! an aathorized signatu.e or ahe cowr page.
' Reportabl€ Detection Limit BRL = Below Reporting Limit Page 5l of 152
Page 409
Sarnole [dentificatiooM8FF3s459464-t I
Ctiept Proiect #l0l-88
Collection Date/Timel5-Ma 7 00:00
MatrixBallast
Receivedl9-Mar-07
CAS No. Antlru(s) Result Fhc rRDL Dilution Method Ref. PrcWed Aaztlzed Bach Aazlyst
Voletile Organic Compounds
Volade Oroanic ComooundsPrepared by method SW8,l6 5030 Soil (high levet)
7t69-4 Trichlorofllororn€thane (Freon 11) BRL
1fi65n n-Propylb€d€ne100-42-5 Styl€n€63Gm6 1,1,1,2-T€t€cftloroethane793rr-s 1,t,2,2-Tetrschloroehane12h8-4 Tet€dhloro€fEne108{all Totu€n€87{1{ 1,2,}TnchbrobenzeDe120{2-1 1,2,+Tdchlorcbenzene71-str |,I , i -Tridlloro€thane79{Gs 1,1.2-Tricftloroethane79{1{ Trichloroeth€n€
96-1S4 1,2,$T.ichloropfopane95-6!6 1,2,r1-Trimgthylben2s6s108574 l,3,tTrimethytb€nzene75{r-1 vinyl chloaide133O2G7 m,p"Xy4en€95-47{ o-Xyt€ne1099&9 Te{rahydofuran6+28-7 Ethyl eth6r99{ff Tort-amy' methy' ether637-9?-3 Ethy ten-botyt eth€r10&2G3 Di-isopropyleth€r75-85-0 Tert8utanol / buq/ atcohol12+91.1 1,4-Dbx€ne
Sunogate rccovg'les:tW41 +Bmmofluotubenzene
2o37-26n Toluene4€l
I f 06r|074 1,[email protected] 4186esH Dibromoquoaonethane
Ertrlctsbl€ P€t.oleum Hydrocrrbo$
Extraclable Total Peholeum Hvdrcca.bons
PrepaEd by method SW846 35508
€lXl6€1-g Gasolin€60476-3G2 Fuet Oit #26847G3r-3 Fuet Oit #46855+OOa FuelOil *tGlat)9&0000 Mortor OilJ()()igAOo0 Aviatiofl Fuel
Unid€nliied
Otl|e. oil
ToLal P€lroleum Hydrccalbff s
C9.C36 Aliphatic Hyd.ocarbons
Sl,to€|a{e rDcolenecr338&33-2 1 -Chlotoocdecane
Semivolrtile Org|rL Corbpord! by GC
Oroanocfihrine Pe€ftides SW846 8081A
Preparod by m€thod SW846 35508
3o+oG2 ALldn
BRLBRLBRfBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRL
1 1 21tn110102
!sftspsn(susftgus/ksps/ksru^9lrsAsrgrs!dkspdksps/ks
!g/kSug/kstrg/kgps/kspsft9
l€/ksrryk9pqr9
udks!s/ksps/ks
lsftslrgkg9Sikg
52.252.252.252.252.2
52.2
52.252.252.252.2
52.252.2t0452.252252.252.2
52.2
5221040
505050505050
5050505050
50505050
5050
SW 846 82608 21^tiat47 22 4d47 7031189 ho
rCT ETPH 22-tilar-07 26-t ar-07 7031283 OS
70-1m%70-130 %7&130%70-lw%
BRL8RLBRLBRLBRLBRL
BRLBRLBRLARL
117
nEl(Smgn(gndkomgftsmg/r(gmsfts||'rsftsrwlsor9r(gmdks
25,6
25.625.6
25.625.6
10-140 yo
BRL llslkg SW8.f6 8O8lA 21-Ms,r47 26,.,'atr47 7031i71 TG
Thb labralory rcpod is not voud rrlthout on adhorizd siEnature on the covc. Ird$ .
'R€port blc Detectiofl Limit BRL= Bclow Reponine Lirnit Page 54 of 152
Page 410
Sample ldentiftcationMEFB.3sA59464-l I
Client Proiect #30t-88
Collection Date/Timel5-Mar-07 00:00
MatrixBallast
Receivedt9-Mar-07
CAS No' Analfte(s) Result Flag *RDL Dihl.bn Method Retr. Prcparcd AMItzed Bakh Ahalfst
Sehivohtile Organlc Compornds by GCOeanochlorine Pesticides SW846 80814Prepared by method SW846 3550831944€ a"BHC319€5-7 b-BHC319{6€ d_BHCsa€+e gFBHC (Lindane)5/-7+9 Chtord€ne72r5rl-€ a.4-DDD(p,p,)72-5te 4,+DDE (p,p,)s{l-?+3 4,+DOT (p,p')6O-57J Dietdrin95$98{ Endosut{En I33213{54 Endosulfun ll1031{7{ Endo,sulfanSulfate72.2O-A Endrin7t21.9H Enddn Atdehyde7F.r4{ Heptachtor724Ts Methorychtor102457-3 Heptachlor Epoxide600t++2 Toxap,llene5t0!714 €-Chlordane5586-3L7 g4htordane53494-70-5 Endrin (etone
Sarrrogale /ecolcr'esi,03ec+2 4,4-DB4ctafruorobiphenfl (54msL2+3 Decechlorobiphent4 (SoPolvc*rlorinated Biohenvls bv SW846 808?Pr6pa.ed by method SW846 3550812674-11-2 PCB 1016rri04-2F2 PCB t22l1ri41-16-5 PCB .1232
53.*21-9 PCa 124212672-29{ rcB 124811097{91 PCB t2:}411096€-5 PCB 12603732+?3-5 PCB 12621i1(x}r,{_4 PCB i268
Suarogal€ r€cor€r'esrI 03 B€, 8 +2 4, tl- D 84ct a fl uo ro b i ph en yl ( S 4m51-2+J Decochbrobiphenyt (Sr)
Semlvolrrib Org.ric Compounds by GCMS
21-Mat47 24'Mat47 703'1170 SLl
BRLBRLBRLBRLBRLBRLBRLBRL
BRLBRL
BRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRL
76127
BRL8RLBRLBRLBRLBRLBRLBRLARL
110
,.i9/Kg
Ljgftspslkg
Lrg/Kg
!gikg
USrt(S
['Ek9pg/kg
!g/kspg/Kg
pgfts
ug/(g
ug/kgpg/(g
tjgKspEks
psfts
t S/'(st'g/ks!si(g!g/Kg
1 3 . 5
13.5
r3.5
13.5
13.5
13.5
13.5
7.00
1 3 . 5
13.5
13.5
1 3 . 5
13.5
13.5
13.5
1 3 5
67.7
13.5
1 3 . 5
13,5
27.1
27.1
27.1
27.1
27_1
27_1
27_1
27_1
27.1
30'150 %30-150 %
sw846 0081A
sw846 8082
sw846 8270C
I
1
1
1
1
1
1
1
1
1
1
1
I
1
1
t
1
1
1
1
1
trg/Ks|Js/ksug/(g!9ir(gug(g!sftsps/kgpsfts
!Eks
m-l50 %m-t 50 %
S€mivdatile Orqanic Comoouods bv SW846 8270CPfepared by method SW846 3550883-32-9 AcenaphtBne20e€6{ Acenaphthyten€62513 A,r ,ine12G12-7 Anthracene1912-2+9 Afazine10+33+ Azobenzene/Diphenytdiazine9242-5 B€nzidinefl6{ti B€nzo (a) anthracene
22-Mat4f 264nar47 7031282 M ABRLBRLBRLBRLBRLBRL
BRLBRL
!sftsLj9fts!9ftg|l9/kS!€ftgpsl(g
us/kgpsftg
635
635
635
635
635
635
635
635
This lahorolory nport lr nol wlrl vithout on onahofited signaturc on the corer page.
r Reportable Detection Limit BRL = Below Reporting Limit Page 55 of 152
Page 411
Sample IdeotificatiooMTFB.3sA59464-11
Clieot Proiect #301-88
MatrixBallast
Collection Datey'Tim€I 5-Mar-07 00:00
Recoived19-Mar-07
CAS No. Anavlc(s) Rcs'/A FIas 'RI,L Dildion Mtthod Retr. Pnpdran ArraIWd Bach An4lfsl
S€mivoblile Orgadc Compoutrds by GCMS
Semivolatile Omanic Comoounds bv SW846 8270C
Prepared by metlrod SW8,l6 35508
Benzo (a) pyrene20+99-2 B€nzo(b)f,uorsnthene191-2a-2 B€nzo (g,h,i) perylene20rc8-s Benzo (k) fuorantheneffiso Benzoic acld101>51{ 8€nzy'l alcoholr11-si-r Bis(2_Ehtoroethory)methan€11r-444 Bis(2{htoroethyt)ether3963&32.9 Bis(2<hloroisop.opyl)eth€r1r7{1-7 Bis(2-€h!'lhexyl)phttEtate101'55'3 zl-Blornophenytphenyleher85!6&7 BuV benzyl phthatatje8&74-0 Carbazole5A-5G7 4-Chlooj-methylphenol16-47+ +Chlorcaniline91-5&7 2_Chlo.ooaphhalene9s-s7{ z_Chlorcphenol70ut72-3 +ChlqoFhenyl phonyl ether218-ol-9 Chrysene53-7G3 Dib€rEo (a,h) anthracene132{+9 Dib€nzoduran9t5+t l,2-Dicilorobenzene54i-73r l,3oidhlorob€nzene106-46,7 l,4-Dichtorob€rE€neel-9,r1 3,3 -Did ombenzidine120-83-2 2,+Dichlo.ophenol0.15+2 Diebytphthalate131-11n Oimeth/ phthalate105{7a ?,+Dimethylphenot€/.7+2 Di.n-butylphthalate534.E?-1 4,6-Dinitrob2-melhylphenol51-2G5 2,4-Dinftrophenoll21r{.2 2t4-Oinitrotoluen€60620-2 2,6;Dinihotolueoer 1 ru4{ Dln-octy' pHhat€te208-1.4-0 Fluoranth€n€88.747 Fluor€n€11&74-1 HeXachlorcbenzene87SF3 Herachtorobutadiene7t.1.74 Hexachlorocyclopentadien€6:t.72-1 Hexsdttorosthan€ls3-3e-s Ind€no (t,2,&od) p,fenew12e I _Mehyin@hhat€n€78-59-t lgophoame91-57€ 2-Metryhaphttlal€n€9914&7 2-M€thylphenol10c3€-4, 3,4+redhylphenol1{16-{11.59i.2G3 Naphthalenoe4-7+4 2.Niboanitine994o-2 $HiLoanllin€
BRLBRLBRL
BRLBRLBRLSRLBRI-BRI-BRI-BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRTBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL
BRLBRL
UdkS 635
lSitq 635
t S/tS 635
|4AS G35
|ryl(g 63spdkS 635ps/ks 635
!g/ks 635
!g/kS 635
t€,kg 63s
l€/tS 635
trC^g 635
FC,IS 635pS&g 635pgftS 605
lSftS 6il5
lgkS 635
IS/kg 835
IS/19 635
US,IS 635pS/kS 635
lgks 6il5
!SI(S 635
lSftg 535pgn(g 635
llg/r(g 635
IgrS 635
FgrS ffispg/kS 635
!g/kS 63s
l,rgkS (i15
lSftS 63s
lrSftg 635pS^S 635
USfts 635pdkg 635
[r94(S 635
!g/kg 635
rgftS 635
ugftg 63s
t€,ag 635
rs/ks 635pgkS G35
ldks 635
LrSftS 6:|5
USftS 635
lglkS 635
rSikS 635psfts 635
lrgkS 635
Ihir hh*alotf .qorl b @t voltd tothost on aathotlzd stgnatarc or lhe cover pdge.
. R€portable Detection Limit BRL = B€low ReDortios Limit Page 56 of | 52
Page 412
Sample [d€otificationMTFFS
sA59464-11
Client Proiect #l0l-88
Collection Date/Timel5-Mar{7 00:00
MatrixBallast
Receivedl9-Mar-07
CAS No. Analrta(s) ResuL FIag Units *RDL Dilution Mcthod Rel. P4pared Anab.td Eotch Atullrl
S rivololile Organic Compo{nds by CCMS
Semivolatile Oroanic Comoounds bv SW846 B27OCPr€pared by hethod SW846 35508
lrxr-ol6 +Nitrcenitine9&9t3 Nitmbenzene8a-7t5 2-Nihophenol100{2.7 4-Nilrophenol
@-759 N-Nitrosodimethylamine
64144.7 N-Nitrcsodi_n_propylamine86-306 N-Nitrosodiphenylamin€a7{6-5 Pentachlorophenol8s:013 Ph€nanthrene10&95-2 Phenol
129-00{ Pyfene11&86.1 Fyridine120{2.1 1,2.4-Trichlorcbenzene95-9t4 2,4,STrichlorophenol8l]-0&2 2,4,GTrichlorophenol
Sl'rogate r€co!€n€s--
32t-60-8 z-Fluofobiphenyl
fi7-121 z-Fluorophenol
SW846 8270C 22-MerO7 26-Ma.'o7 7031282 MBBRLARLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
1 7
Completed
BRL
8RL
0.0090
BRL
BRL
BRL
BRL
BRL
lSftS 2540
tiSftS 635
pSftS 635
fiS/kg 2540
pS4{S 635
ps/kS 635
pS/kS 635
UEIS 635
pg/kS 635
pSI(S 635
pS/kg 635
lSftS 635
lSftg 635
pSftS 635
Ug/kS 635
30-130 %
1U110 %
30'130%
15-110 %
30-130 %
1nl10 %
1
I
1
1
1
1
I
I
1
I
I
1
1
1
1t654co Nitobenzene4s 33416542-2 ,thenol45 29171&514 Terphenyl4l4 461t8-7 2.4dTtibftmophenol U
Tor.l Metb by EPA 6000/7000 Series M€thods
71139-97{ Mercury BRL
Tot.l Mdrb by EPA 200 Serie Merhods
ARL
BRL
13.4
0.731
2 1 2
4.70
BRL
SPLP M.tdr by EPA 1312 & 6000/7000 S€ri€s Methods
SPLP Extraction
71,{0.224 Silver
7440.3&2 Ars€nic
744G3!t 3 Barium
7t40-4+9 Cadmium
Zl40{7-3 Chromium
7€9-97,6 Mercury
7439-92r Lead
262.4+? S€l€nium
1 SW646 74714 26-Mar47 26-MarO7 7031311 YP
EPA 200 7 2GMaF07 26+4ar07 7031263 LR
mg/kS 0.029s
74sr-22-4 gtver
7j!t+382 Asenic
7,r4G3+3 Barium
7i!rs4$9 Cadmium
7,uO-47-3 Chromium
713€-52-1 Lead
?824$2 Selenium
mSI(S 0-0S'1
mg/kg 1.u
fiEI(S 0.445
mg/kg 0223
mS/kS 0.445
rng/kg 0-668
mgfts 1.34
msI 0.0100
mg/l 0.0150
mg/r 0.0050
mg/l 0.0025
n€I 0.0050
rYE/| 0.000c0
nEI 0-0075
mgit 0_0150
1 SWE461312 21-Mafi7 21-Ma'.O7 1031229
1 SW8461312/60108 22-Mar07 2X-Ma..07 7031323
1 '
1 '
1 '
1 "
1 SW8461312'470A ' 231ttar07 7oX1324
1 SW8461312r'60108 " 23{,,lar{7 7031323
1 '
BD
LR
yp
LR
Thit labo.alory rcpo.t k not yolid withoat an autho.ized sign ture od ahe dteer page
' Reporhble D€tection Limit BRL = Below Reporting Limit P^Ee 57 of 152
Page 413
Sample Identifr€tiooMtFB4
sA59,t6t t2
Clietrt Proiect #30t-88
Collection Date/fimels-Mar{? 00:00
MatixBallast
Receivedl9-Mar-07
CAS No. Analyta(s) Rcsalt Flzs U,,ia 'R.DL Dilnion Merlrod Ref, P|Epared A&lyzrr' Barch Anslysa
Vohdle Organic Conpouadr
Volatile Omanac ComooundsPrepar€d by method SW846 5035A Soll (low levet)76n3-l 1,1,2-Trichtorolriiuoroethane (FreoSRL67{4.1 Acoton€ BRLi07n3-1 Adylonitil€ BRL714+2 B€nzene BRL10&€6-1 Bmnbb€nz€n€ BRL7447-5 Bromorfttorcmethane BRL7?214 Blomodidtloromethsne BRL7+212 Bronbform BRL74{3-9 Brornomethafie BRL78+$3 z-Butanone {MEK) BRL10451{ n-Eutytbenz6|1€ BRI_13198{ sec.BuMb€nz€ne BRL98{6{ t€rt-ButylberEens BRL7t15{ Carbon disulfide BRL56.215 carbofl telrachloride BRL108-90-7 Chlo@benzene BRL7s{)G3 Chtoroethsne BRL67563 Chbroform BRL74-47-3 Chloiomethane 8RL9'49{ 2-Ctrlorctoluene BRL10S.4+.4 44hlolotolusle BRL96-12{ 1,2-Dibrcnoj-chtcropropano BRL12,H€-1 Dibromochlorornehane BRIr0A93{ |,2-Dibrcrnoetham (EDB} BRI-74.9t3 Dibromofiethane BRL95-s(ll 1,2{ic* o.obenzene BRL541-73-1 l.3oichtoob€nzene BRL106-4+7 1.+Eticldorot€nzene BRL7U714 Oidllotodinuordnehar|e(Freonl2)BRL753+3 l,l-Obhloroethane BRLr07-0f'2 l.2-Oichloro€thane BRL7535-,{ l,l-Dict otoothene BRL15s59-2 ci6-1,2-DkSloroefEne BRL1sE a0-5 tens- | Joichloroe$ene BRL78{7-5 |,2-Oichloroprop€ne BRL142.28.9 1,+Dicfilo{oprop6ne BRLs9+i8.7 2,2-Didrlooptop€n6 BRL56+50{ l,'l.Didiorop{op€ne BRL10061.01-5 cj6-1,3-flichlorcprop€ne BRL1061.024trar+1,3-DichloroproDene BRLioo4i.1 Efty'benzefle BRL67€&3 HexadturDbLdadien€ BRt_591-78€ ?-Hem|}ono(MBK) BRL98{2-6 lsopoptlborBene BRLg9{?{ +lsoprgplitohrene BRL1634{4-. Medtyl bt-bltyt ehef BRLloelGl +Medrt l-2+€ntanone (MIBK) BRL75s.2 ilethyl6n6 chhride ARLs1.2s3 Naphthalene BRL10316+l rtsPrcp!4bonz€ne BRL
lg/t(gw€t 4.3
ldkgw€t S7.0
Ig/kgw€t 4.3
ldkgYY€l 4.3
ldkgw€l 4.3
FdkS rv€t 4.3
lrgl(g rY€t 4.3
ldkg vret 4.3
pg/ko vY€t 8.fggil€ wet 43.5
pgrtgwst 4-3
pg/kg w€t 4-3
!g/r(g w6r 4.3
ldtg w€l 21.7
Lrdxgwet 4.3
ldkg v,,€t 4.3
lgLfl(g w€l 8.7
IgkS Yret 4.3
pSI(g N/et 8.7
|lg4q sret 4.3
pSftg u/et 4.3
pgr'kg wei 8.7pgkgwe{ 4-3
ldkS w€l 4.3
lgll(g wel 4.3
ugy'xg wet 4.3
USn(S wel 4.3
Ug/kS Yr€t 4.3
pdkg w€t 8.7
trdkS rv€t 4-3
Ug./kg w€t 4.3
IqkS vret 4.3
Ug/Xg v{et 4.3
Ug/kg wet 4.3
pdkswel 4.3
ldkswel 4,3
pgy'kg wet 1.3
lglSwet 4.3
Idlgrvel 4.3
rcl(g u/€t 4.3
|lgl(g rr€l 4.3
ldkSwol {.3
tg/i(Sbst 43.5
pg^gwet 4.3
Fdkgwet 4.3
lSftSwet 4.3
FSrkS wet 43.5
pdkSwe{ 43.5
lcjkgwot 4,3
lgrS*€t 4.3
t
1
1
1
1
1
I
1
1
I
1
t
1
1
1
1'I
1
I
I
I
I
1
1
1
1
1
1
1'I
I
1
1
I
I
I
I
t,|
1
I
I
I
1
I
I
1
I
I'|
SW 846 g2608 z4lliaroT 22l^4a[47 7031291 RU
fhis labotuloty ,eport ls ,tot valid *llhod od dnhodzzd sfunatue aa thz cowt page-
+ Repodable Detection Linir BRL = Below Reponing LiEir Pege 58 oI 152
Page 414
Sample IdentificationMSFB-4sA59464-12
Clienl Proi€ct #301-88
Collection Date/Timel5-Mar-07 00:00
MatnxBallast
Receivcdl9-Mar-07
CrrS No. AnsWG) Fhs Unie *RDL Dilution Llahod ReI. Prcparcd Anrbzed Bakh Anaust
Volatlle Orgrnic Compounds
Volatile Oroanic ComooundsPrepared by method SW846 5035A Soit (tow tevet)1m-42-s Styren€ BRL6ilca){ 1,.1,.t,2-Tetrachtoro€th€ne BRL7$34-5 1,t,2,2-tekacNoro€thene BRL127-184 Tetradlloroethene BRL10&{63 Totuene BRL87€1-6 1,2,3.Trichlorob€nzene BRLi2$€2r 1,2,+Tdchlorobenzene BRL71-5sG |,'l,l-T.ichloroethene BRL7!rcc5 l,l ,2-TriChlo(o€thane BRL79{1{ Trichloroethene 8RL7s6$4 Trichlofonuoromethane (Freon 1l) BRL96-14-4 1.2,3-Trichloropropane BRL9553{ 1,2,4-Tdmethylbenzsne BRL108{7-8 1,3,5-Trirnethylbenzene75414 Vinylchtoridet330-2G7 m,p-Xyl€ne9t47{ Gxylene10+90'9 Tetrahydrofuran80-29-f Ethyt etherS4-OS Tefl-amytmelhyteher637-92-3 Ethyl tert-butyt €ther10&?0-3 Diisopropylether7fifr-o T€rt-Butanol / butyl atcohol129911 1,4_Dioxane
SW8!682608 22-Mat47 224l,al-07 7031291 RLJ
VOC 20-Mar-07 m-Mar-o7 7031156 BD
+grclnofluorchenzeneToiuene4S1 ,2-Dichlotuethane-d4
BRLBRLSRLBRL8RLBRL8RL8RLBRLBRLBRL
1041D4105103
Field extracted
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
114
f.ig/kg w€t 4.3
ug/kg wst 4 3
ug/kg wet 43
lg/kgwet 4.3
pg/kg wet 4.3
pgkg wel 4.3
!g/kg wet 4-3
f.ig/kg wet 4.3
Ug/kg,ret 4.3
!g,,kg wet 4.3
pg/kg wel 4-3
rrg/kg wet 4 3
lgr'kg w€t 4.3
trg/kg wet 4.3
!94(9wet 4-3
Ugr'kg wet A-7
pg/kg wet 4.3
t/gL/Kg wet 43 5
pgr'kg wet 4-3
pg/kg wel 4.3
Wkg wel 4 3
!g/kg wel 4.3
Ugr'kg wet 43-5
Ugukgwet 87.0
7L130%
70-130%
70-130 %
70-130 %
,l
1
1
1
l
I
I
1
1
1,1
1
1
1
1
1
l
1
1
1
I
1
1
1
s|rnryars2t60-404
2037-26'5
l7wo474
1868.5X7
VOC Exlraction
Etalsclcble Petmleum Hydrocarbons
Extraclable Total Petroleom Hvdrocarbons
PEpa.ed by method SW846 35508
80lE6l-9 Gasoline68476.30-2 FuelOit#26847e*1.3 Fu6l Oit #46855300'4 Fuel Oil f6im98000ql Motor oil$or(xxloo Aviatiofi Fuel
Unidentified
Other Oil
Total Petrole{]m Hydrocarbons
C9-C38 Aliphatic Hydroca.bons
SsnDgEle recoyanbs;
3386-3+2 l-Chlorooctadocane
SeDivokdle Orgenlc Compouods by cC
Oroenochlorine Pesticides SW846 8081A
Pr€pa.€d by method SW846 35508
30!xrc2 Alddn
ft€n(g
mgfts
mq/fS
mS/kS
mS/kS
nrSlkS
m!/Kg
msftg
rng/kS
mg/(g
27.O
27_O
27_O
27.0
27 _0
27.i
27.O
27.0
27.0
27.O
+CT ETPH 22-Ma(O7 26-MarO7 fO312A3 DS
BRL
10-140%
ug/ks SW846 80a1A 21-Met47 26]lnar07 7031171 TG
Thit laborutory relgd h not vzbd NAhoat aa eulho zen ngnat re oE ahe cover poge.
r Reportable Detection Limit BRL = Below Reponing Limit Page 59 of 152
Page 415
Sampl€ ldentificrtiooMtFB.4sA'59464-t2
Clieot Prciect #l0rt8
Collectiotr Dat€/Timel5-Mar47 00:00
MacixBallast
Received19-Mar47
CAA No. Arzlye(s) Fhg A a *RDL Dilatioa L{ahod Retr. Prepared Aaallzzd Bdth Aa4lfsl
S€mivolatile OrSrnk Compoundr hy GC
Oroanochlo,ine Pesticides SW846 6081APrepared by mehod SW846 355083rgs4{ 8-BHC319-e5-7 b-BHC319-06-€ d-BHC58-89-9 gF.BHC(Lindan€)57-r+9 Chlordarls1'2 '54{ 4,4.oDD (p,p,)72-5re 4,4ODE (p,p')50.2+3 a,a{DT (p,pl60-57.1 Dieldrin9599&A En(bsulbn I3321$68F9 Endosulbn ll1031{7{ EndosulbnSulfate72-2oi Endrin742r-93-4 Endrin Atdehyde764+A H€ptacftlor724U5 ti,l€tloxyrfilor1024€7-! Heptacldof Epoxide80Ol++2 ToGphone5103-71-9 a-Chlo(dane556G3+7 g_Chb.dane5,3491-7Os Endrin Kebno
Srrroga(e /Bcown€sj103ts64+2 4,fieod^fluorobkhenyl (Sr)m5L2+3 Decechbtubiphenbt(Sr)Pohrdtlorlnaled Biohenvls bv SW846 8082Preparod by metfbd SW846 355081267+11-2 PCB 10'61110+n-2 PCB 122111141-16-s PCB ' |232
53{n9-21.s PcB t24212672-294 PCB t24811@7€e-1 PCB.t254r10s6{2.5 PC8 12603f32+zt-5 PCg 12621fl0{}14-4 PC8 1268
Suzwab recosngsjI W64+2 41484ctafl uorobiphenyt ( 34mst-21-3 tu@chlotobi@ (Sr)
Serrlvolrtile Orgrrlc Compo{n& by GCMS
21-M3r{7 26-fvlr{7 7031171 TGBRLBRLBRL
BRLBRLBRLBRL8RLBRL
BRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
118
BRL8RLBRLBRLBRLBRLBRLBRLBRL
75115
BRLBRLBRLBRLARLBRLBRLBRL
pc/t9
t'gt9pry*spsrl9
!gr(9FgftSflgftSlgftspsn€l,siksE/TII
usagpsftspgtk9pdkg
rsn(gU€ftS!s/ksFs,kst gikg
us^g
t3.3t3.313.3
66.7
13.37,006.9013.313.3t3.3
13.3
13.3
13 .3r 3.313.3
ugrs!gftspgfts
wikspslks
l€/k9us/ksusftsPgrs
2A-7
m.726.7
26.7
sltt& %w150 %
sw846 mStA
S111A46 6062 21-Mat47 z4.ll,.el.Ol 7 031 1 70 SM
30-1fl %
3Gtffi %
Semit/olatile Orqanic Comoounds by SW846 g27OC
Prepared by me0Dd SW846 35508
4332-9 Acen6phtlEne20&96{ Acenaphthyl€ne62'5}3 Anllh€14112.7 Anthtec€n€1912'24-9 At?zine10+3:1.3 Azobeoz€noDiphenyldiazineq{7-5 B€fizidine56'5+3 B€nzo (a) anthraoer€
22{tr,147 25-Mat47 7031 282 M.Brsil(gusftspsftsps/kspdksps,/ks
IgksugJks
670670670670670670670
sw846 8270C
Ihis lahnhrf npoft ls aot wlid firthotd an atltorhd stg,B,t E o,r tfu @v.r page.
' Reportable DetectioE Limh BRL = Betow Reporting LirEir Page 60 of 152
Page 416
Sample IdentificatiopII,{EFB.4sAs9464-12
Client Proiect #l 0 l - 88
Collection Date/Time15-Mar-07 00:00
MakixBallast
Receivedl9-Mar-ll7
CAS No. At'!'bta(s) Result FI"C Unit *RDL Dilaiott M4hod nctr Prcpred Anaryzc'| Balch Analrrt
Senivolstile Orgrric Compounds by CCMS
Semivolatile Orqanic Compounds bv SW846 8270C
Prepared by method SW846 35508
5032-8 Benzo (a) pyrene
i'ot$-2 Benzo (b) lluoranUrene191.24-2 Benzo (9,h,i) peryt€ne
a)7{8.9 Benzo (k) fuoranth€ne6545-0 B€rEoic acidl0o-51€ Benzylalcohol111-91r Bis(2-chlorcethory)m€thane11r-14.1 Bis(2-chloroethyl)ed1€r4963&32.9 Bis(z-chloroisopropyl)€lher11741-7 Bis{2-ethylhexyt)phthatate
101.54F3 4-Bromophenylphenytether
65-68-7 But/benrylphthatate8e7,L8 Catbazole5!F5G7 4-Chloro.3-methylph€notlrxi-47{ 4-Chtofoaniline91-5&7 2-Chloronaphthalene9+s7-B 2-Chtofophenol70osF72-3 44hlorophenyt phenyl ether210{14 Chrysene5!7G3 Dibenzo (a,h) anthracene13244-9 Dibenzofuran!F{e1 t,Z-Dichlorobenzene541-73.1 1,3-Dichlorobenzene1rxl..1€-7 1,4-Dichlorobenzene914+1 3,3--Dichlorotenzidine120-E3-2 2,4-Dichlorophenol84-66.2 Di€thytPhthalate131-i1-3 Dimethytphthataler0f|67{ 2,4.Dimeth},lphenolw7+2 Di-n-butylphlhatale53+52-1 4,6-Oinitro-2-methylphenol
51-28-5 2,4-Dinitroph€noli21-14+ 2,+Dinitrotoluene606-20{ z,$Dinitotolu€ne11744{ O-n{ctylph0ratate206-4-0 Fluoranthene
8&7+7 Fluorene
11&74-1 Hexachlofob€nzene
87{&3 H€xadtlorobutadiene77474 Hexachlorocfclopentadiene
67-12-1 Hexadlloroethene19139-5 lrdeno (1.2,3-cd) pyEne
9Sr2{ t-Methytnaphthalene78.5$1 lsophorone91.574 2-Methytnaphthalene95-1+? 2+llethylphenol
10&394, 3,4-Methylphenol10d44-591-413 Naphthatene&144 2-Nihoaniline
99-11+2 3-Niroaniline
BRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLSRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI.BRL
BRLBRLBRLARLARLBRLBRLBRLBRLBRLSRL
BRLBRLBRLBRL
BRLBRLBRL
tig/kS 670
lSftS 670
USI<S 670
liS/kg 670
!g/tS 670
!g/kg 670
pS/kS 670
Pg/kg 670
pgrkg 670
!g/.KS 670
lsftg 670
trS/kS 670
UgftS 670
Hg/kg 670
pgftS B7O
pSftg 670
rcftS 670
US/kS 670
pg/kS 670
lgr'kg 670
uSrkS 670
pS/kg 670
Ugn(S 670
!gI(S 670
!S/kg 670
pgftg 670
pg/tS 670
!S/kS 670
UgkS 670
lgftS 670
!g/kg 670
pgeS 670
UgftS 670
ISAS 670
pSnq 670
ySn<g 670
lqkg 670
!SI(9 670
pg/xS 670
tiS/kS 670
pg/kS 670
!g/kS 670
lsftg 670
!g/kg 670
pSftg 670
USftS 670
lSftS 670
ugftg
!sftsrc/ks
670670670
SW846 8270C 22-Mal-O7 25-MaF07 7031282 M.g
I
1
1
This hbotutory Epo.. iyut valid vithout a.t asthoriad s,g$aturc on the cover paEe
' R€portable Detection Umit BRt- = Below Reporting Limit Page 6l of 152
Page 417
Sample ldrptificationM8FB.4sAs94o+"12
Ctieot Prciect #301-E8
Coll€ction Date/Timel5-Mar-07 00100
Matrl(Ballast
R€ceived19-Mar-O7
CAS No. Ana+t4s) FI4g Ania *RDL Dilaion Meahod Retr. Preryred Aaalwd Bdtch fuulfst
SemhDhdle Olgrtric Compoundr by ftMS
Semivolatile Ofqanic Comoounds bv SW846 8270C
Prepared by Elsthod SW846 35508
10G01{ +Nitoaniline9E{+3 Nitaobenzene88-7+5 2.Nitophenol10G02-7 4-Nilrcphenol62-T+9 N-l$trosodin€thyiamine@1{4-7 N-Mtro$odi-n-propylamine€6-30{ N-Nitosodiphenylemine87{G5 Pentachbophenole5{1{ Phenanthen€10S45-2 Phenol129{0{ Pyrene11G86-1 Pyridinei2{}€e-l 1,2,+Trictlorobenzen€95e5-4 2,4,$Tri:torophenol8a{e2 2,4,Gldchlorophenol
Srr.rDgatg /eaoveabs;32le-g 2-Huorobiphenyl367-12.{' z-Fluorophenol416ssa4 Mrcbnzends416542-2 Phenol4s,7 | e-514 ferphettyl-dl4| | 8.794 2,4,6Ttibronophenol
1 Sw846 6270c 724'/.3r47 ?s.l,a'{7 7031282 M.S
1 '
I '
1 '
I '
l '
I '
t "
I '
1 '
1 '
1 ''1 '
1 "
1 '
BRLBRLBRLBRLgRL
BRI-BRLBRLBRLBRLBRLBRLBRLBRLBRL
3!t
31a4221
BRL
BRL
11.4
o.775
5.95
BRL
BRL
BRL
BRL
BRL
lrgrtS 2660
t4/k9 670
Ig,tg 670
FS/tg 2680pCftS 670plt/kg 670
PgAg 670
!g/Xg 670
!9/t9 670
!S/kS 670
lSftS 670pgftS 670
trgftS 670
lsftS 670
!S/kS 670
s0-130 %t &110 %30-130 %15.110%30-130 %15.110 %
Totrl Metrb by EPA 6lXXy7000 S€.ier Mclhods
743+97{ Mercury BRL
Ioral Metrb by 8PA 200 S€ries M€tlodr
mS/k9 1 SWe,$ 7471A 26-MatA7 26-Mar47 700l3ll YP
74{0-223 Silv€r
zr.r0-3&2 Arcenic
11403+3 Baaium
7440-419 Cadmium
7440.17.3 Chromium
7439€2-1 Lead
2824+2 Selenium
SPLP Metib by f,PA l3l2 & 600M000 Serl6 Mcthod!
SPLP Extractim Completed
74r{t 22.1 Situ€r BRL
7a40-3&2 AF€nic 8RL
714G3+3 Badum 0.0072
7440-4$9 Cadmium BRL
Z!1047.3 Chromium
7'89.97€ M€rcUry
7€S92-1 Lead
77€2-{S2 Selenlum
nE/kS 0.969
mS/kS 1.45
mgikg 0.4€,r
mSftg 0242
ntSlt(S 0.4€4
ndkS 0.726
nE/tg 1.45
mdl 0.0100
mdr 0.0150
n€n 0.0050
nEn 0.m25
mgn 0.m50
msI 0.00040
me,l 0.0015
mdt 0_0150
EPA 200.7 2&Mer47 2dvlar.07 7031263 LR
1 SW846'f312 21-Mat47 21-$ar47 703122S BO
1 SW8.16 f312l60108 2-Met47 2}uat47 7031323 LR' l '
' I '
1 '
t '
1 SvrrS,ftt 1312J7470A ' 234e147 7(n1324 W
1 SV\446 1312r'80104 " 23-Merry 7061323 LR' t '
Thie labtulorf EForl b ,ut eaad withod tn aulhodzed signaturc o8 dta corer pqge ,
* Re?trtable Detectioo Limi! BRL = Betow Reporring Linir Page 62 of 152
Page 418
Sample ldentificationM8FB.5sA5946,t- l3
Client Proiect #l0l-88
I\,IatrixBallait
Rcceivedl9-Mar-07
Collectiop Date/Timel5-Mar-07 00:00
CAS No, Analfte(s) Flog Uni6 *RDL Dilutiarl Method Re/. Prcpared Analf.ed Bqlch Analj-st
Vohtile Orgrnic Cohpounds
Voladle Oroanic ComooundsP.epared by metlDd SW846 50354 Soit (tow tevet)7e-111 1,1,z-Trichlorohiffuoroethan€ (FreoERLa7$+1 Ac€tone SRL107.13-1 Acrylonitdte BRL7143-2 Benzene BRL106-86-1 Brornobenzen€ 8RL74-97-5 Bronrca$loromethane BRL75-274 Bromodichtoromehane gRL
7r2r2 Brcmoform 8RL74-€&9 BroRomethafie BRL7&93-3 2-Butanone (MEK) BRL10a.51{ rFButylbenzene BRLt35-98€ s€c-Butylbenzene BRLs€{6-6 tiert€utytb€nzene BRL75-t5-0 C€rbon disulfido BRL56.23-5 Carbon tetachloride BRL10&9$7 Chlorobenzene BRL75{0-3 chlooelhane BRL67{6.3 Chloroform BRL74{7-3 Chloromethane BRL95-49{ 2_Chlorototuene BRLi0€-43-1 4-Chlorotoluene 8RL96.t23 1,2-Dibromo-3-chloropropane ARL12,14+1 Dibromo€hloromethane BRL1693-1 t,2-Dibmmoetnne (EDB) BRL74-9'-3 Dibromomethane BRL9s-5G1 l,2-Dichloaobenzene BRLEt41.73-1 1,3_Dichlofobenzene BRLlofi-r6-7 1,+Dichtorobenzen€ BRL7+7l.8 Dichtofodiiuoromethan€ (Freonl2)BRL7t3.4-3 1,l-Dichloroethane BRLroruc2 l.2-Drchtoroethane BRL75-35-4 l.1-Drchtorcethene BRL15e592 cis-1,2-Drchtoroethene BRL15G€0-5 taans.1,2-Djchtorcethene BRL7847-s l,2oichloropropane BRL142-28-9 l,3.Dichtoropropane BRL59420-7 2,2-Dichtoropropane BRL563{€t 'l,1-Dchlo.oprcpene BRL10001{1-5 cis-1,3-Dichlorogopene BRL10061.02{trans-1,3-Dichloropropen€ ARLrqo-{r-a Ethylbenzene aRL87€+3 Hexachlo.obutadieoe BRL5€1-70{ z-Hexanon€ (MBK) BRL9842{ lsopaopylbenzene BRL9947{ +lsopmpyltolu€ne BRL16o4{q Methyllert-buv etler BRL10&10.1 +Methyt.2-pentranone{M|BK) BRL75{$2 Methytene chlodde BRL9r.20'3 Naphthalen€ BRL103{5-l rFPropyhenz€n€ BR.L
SW 846 82608 22-Mat47 22-Maro7 7031291 RLJ!g/kg w€t 4.4
lgr'kg wet 8€.8
!g/kg wet 4.4
l4/kg wet 4-4
pgr'kg wel 4.4
lgr'kg wet 4.4
pg/kg lv€t 4A
IgL/kg wet 4.4
rc/kg wet 8-S
lg/kgwel 44.4
ljg/kg wel 4.4
pgn(g wel 1.4
Pgftg wet 4.4
pg/kg \Net 22_2
pg/Kg wet 4 4
pg/kg wel 4.4
lgr'kg wet 8.9
t gL/kg wel 4.4
ligrkg w€t 8.9
!g/tg w€t 4.4
!g/kg wet 4.4
tigL/kg wet 8.9
rc/kg wet 4-4
pg/kg wel 4.4
p€y'kq wer 4.4
pg/kg wel 44ggL/kg wel 4.4
ggrkgwet 4.4
lgfl(gw€t 8-9
!g/kg w€t 4.4
!g/kg \dct 4 4
pg/kg wet 4-4
t4lkg wet 4.4
!g/kg wet 4.4
Fg/kg wet 4-4
tjgikg wel 4.4
Pg/kg wel 4.4
lJg (g wet 4.4
FdkSwet 4.4
!g/kg lv€t 4.4
!g/kg Yret 4.4
!S/kS wet 4-1
Ig/kg wet 44 4
pg/kg $/el 4_4
lSlgwel 44
lig/kg wel 4.4
lg/kgwet 44.4
lgL/kg wet 44.4
p!y'kg wel 4.4
lgr'kg wet 4.4
Thh tabonlory Epotl is ^ol vlu vifioat a^ attltorlze.l sigttattre oa the coyer page.
i Reporbble D€tection Limit BRL = B€low ReForting Limi( Page 63 of 152
Page 419
Sample ld.ntificatiotrM8FF5
sA5%64-13
Clieqt Proiect #301 - t8
MatrixBallast
R€ceivedt9-Mar-07
Collectioo Date/Tim€I 5-Mar{7 00:00
CAS No. A,.alrta(s) FI4C U/'i6 *RDL Dil"tion MdMRef, tuaparcd Analwn Edch ArElFt
rc'oa2-s styr€ne63S20-6 1,1,t,z-Tetachloroethane79-u-5 1,1,2,2-Tetractloroethane127-18-4 Tet€chloroefrcno10&8&3 Toluen€87€1S t,z,}Tridorobenz€ne12O-82-l t ,2 ,+f idhtorobergone7l-5:"6 1,1,l-Trichtoroethane79{0-5 1,1,2-Tfichtoroethane79{l{ Trichloro€thene
Volatite Orgrdc Compoutrr|s
Volatile Omanic ComooundsPrepa.ed by melhod SW845 5035A Solt (tow tevet)
BRI-BRL8RLBRLBRLBRLBRLBRLBRLBRL
75-691 Tricflo.ofruoromettrane (Freon 1l) BRL96,14-4 1,2.&Trichto.oprop€ne9563-6 1,2,+Trimethylb€nzene10€.67{ |,3,s-Trimethylb€nzene75{1-4 Vin, chhtrid€133(}2F7 m,p-Xylen€9547{ exylefis10999-9 Tetrahyalrofuaan60-29-7 Ethyl ether9o4jt€ Tert-amyl medly' ether637.923 Ehyltert+utylethor10&m-3 Diisopropylether75{5}0 Tert-Butanot / butyt alcohol12+91-1 1,+Dioxan€
Sl//rDgale rBcown€s:460404 +E*omofluofotEnzenem37-26.5 fdluene4S1 7 0@-o/ 4 1, 2-Dlchlo@ethene-d4ftta-s,7 Dbrcnofluorcnethane
VOC Exlraction
E tlrclsble PeEoleum Ilydrocirbons
Exuaclable Total Petroleun FMrocaftonsP.epared by rnelhod SW846 355088{xt6{1-9 Gasoline6847e3G2 Fuel Oil #26847S3r-3 Fuet oil #46S55!004 Fu€l Oil #6[rq]800000 Motof oilJoolaxxloo Aviation Fuel
UnidentifiedOth€r OilTotial P€hs m HydrocarbonsC€-C36 Atiphalic Hydrocarbons
Ssnpgat€ recoyelrbs:33aa)il2 1 -Chloroodad€cene
Scmivoleaile Orgrtric Compounds by CCOroaoochlorin€ P€s cktes SW846 BOAIAPrsparEd by mehod SW846 3550830$oG2 Aldrin
Sw 8,f6 8460s 22-Mar47 22-ltar47 7m1291 RLJ
voc 2GMar{7 20jl,!ar-{7 7031156 BO
+CTETPH 22-$al-O7 4n3tr4f 7031283 DS
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI
106105110102
Field ext-acted
pg&gw€l 4.4
pgn(gwet 4.4
l.|grl€ wel 4.4
pgrkg wel 4.4
irgr'kg wet 4.4
ldkgw€l 4.4
lgtkg wel 4.4
lgr'kg R€t 1.4
ldkgwet 4.4
ldkg rv€t 4.4
ldlSw€t 4.4
ldkg rv6t 4.4
us^gYJet 4.4
ug/kq rv€t 4.4
udkgY€t 4.1
US/kS wet 89
!S/kS wet 4.4
IdkSwet 44.4
f.rdkS w€t 4.4
pdkSwst 4-4
|,g/kg vret 4.4
l4lk9 w€lt 4.4
Igilqwd 44.4
rcikg wel 88.8
7G130%
70-130 %
70-tu %
70-tm %
mgtg 25.6
n€/kg 25.6
no/kg 25.6
rfig/ks 25.6
nE/kS 25.6
dtS/kS 25.6
mdkg 25.6
mS/tS 25.6
mS/kS 25.6
mSftS 25.6
40-1'lO %
1I
1
1
I
I
I
I
I
I
I
I
1
1
1
1
1
1
I,|
1
1,]
1
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
1 1 1
|lsfts Sw845 8O81A 21-Mat47 -Mat47 7ul117l TG
Thb labodort .eport is aal eolu waltoul zd ruthoiei Eigdstarc on tfu ct ver psge .
' R€porbble Det€ction Limit BRL = Below Reportine Limir Page 64 of 152
Page 420
SarEple ldentificationMSFB-5s459464,13
Client Proiect #301-88
CoLlection Date/Timel5'Mar'07 00:00
MatrixBallast
Receivedl9-Mar-o7
CrlS No. Analtu(s) Fl"s *RDL Dilaiod Method Rel. Prcpued Anabzed Balch Anabst
SemivoLdle Orgsnic Colnpornds by cCOroanochlorine Pesticides SW846 8081APrepared by method SW846 3550831s&16 a-8HC31s8t7 b-BHC3te{6{ d-BHCsa{se g-BHC (Lindane)5/-7rr-9 Chlordane72-s44 4,4-DDD (p,p.)72-5+e 4,+DDE (p,p.)50-2s3 4,4DDT (p,p)EGt-1 Dleldrins5+s8{ Endosulfian I332i3-65.9 Endosulbn tlt03r.o7{ Endosullan sutfate
tsndnn7a2143-a EndrinAldehyde76444 Heptachlor7243-5 Metfrxychlori02+57-3 Heptachlor Epoxicle6001-3+2 Tou€phene5103J1-9 +Chlordane5566-34-7 g_Chlordane5s491L70-5 Endrin lGlone
sl/rogtate rBcoveaes:t 038€.8+2 1, 4ag-Oebnuorcbipt@nyl (Som5r-2a,3 Decachbrcbiphenyt (54Polvchb.inated Biohenvts bv SW846 8082Prepared by rhelhod SW846 3550812€7+11.2 PC8 10i61110+m-2 PCB 12211r141-ra€ PCB 12325X46+21-9 PCB 124212An-E$ PCg 1249r1097.6e.1 PCB 12541109€-82.5 PCB 1260T32+n5 PCg 1262111OGr44 PCB l?68
Sunogate r€cor€resr1 038d.8+ 2 4, I -D goc t a fl uoto b iphe nyl ( S t)e54a4 Decachbtobiphenyt (Sr)
Smrivoladle Or8rntc Compounds by GCMS
BRLBRL8RLBRL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLSRLBRLBRL8RL
69137
BRLBRLBRLBRLBRLBRLBRL8RLBRL
75110
BRLBRLBRL8RLBRL8RLBRLBRL
!g/kS
!S/',(S
!g/kg
Ljsfts
ug/ksus/Ks|'|sflqtlsfts
wikgug/r(g!g/tsusrkslr9/lglrgfts!siks!s/kg!g/kgtJg/l(g
Ljsftg
!sfts
|lg/ks
13.9
13.9
13.9
1 3 I
69.7
13.9
13_S
r3.s
7.00' t3.9
13.9
13.9
13.9
13.9
13.S
13.9
13.9
6 9 7
1 3 9
1 3 I
13_S
3t>150 %
30-150./.
sw846 8081A
sw846 8082
I
I
1
I
1
1
1
1
1
1
I
I
1
1
I
I
I
1
1
1
1
21 -Mat41 26-MaFO7 703117 1
psilspglxg
!sikspgKgpEks
!g',xs
Psn(sus/kspsftg
2 7 9
2 7 9
27.9
27.9
27.9
27.9
27.9
27.9
27.9
21-Ma(47 24-Mat4r 7031170 SM
30-150 %30-150 %
Semi\,/olatle Oroanic Communds bv SW846 8270CPrcpared by method SW846 35bOB
83.32-9 Acenaphthene20&9G8 Acensphthylene{12'5}3 Aniline
12012.7 Anthrdcene191?-249 Alrazine103-333 Azob€nzene/Diphenyidi€zthe92{7€ Benzidinesa5s3 BerEo(a)anthracene
22-Mal-07 25^nat47 7031282 M.Bps/ksps/ks
ug/ksl'|sftgti9/kS
Fg4(g
FSikg
lig/kS
635 1
635 1
txls 'l
635 1
635 r
635 1
635 I
635 1
sw846 8270C
This bboralory Epod is ^ot rolkl x'ithoaa en.uthoized sigratarc od lhe cowr page
' Reportable Detection Limit BRL = Below Reporting Limit Page 65 of 152
Page 421
Samole IdetrtificationMtFB.5SA59il6l-ll
Client Proiect #301-88
MatrixBallast
Coll€ctiop Dal€/Timel5-Mar47 00:00
Rec€ivedl9-Nla.-07
CAS No. Analtte(s) FIq UniE IRDL Diluiot' Method RrJ, Prcpared Aaalyzen Bdch Atttltsl
Seorlvol ih Orguic Compourds by GCMS
Semivolalile Orqanic Compoonds bv SW846 8270CPreparod by method SWS]{6 355085{l"32-a B€nzo (a) pyrone20S+2 B€nzo (b) ffuora.drd€19r-24-2 Benzo (g,h,i)peryleoe207{8-9 8€fEo (k) fuorandlen€
Eenzoic acid10G51-6 Eonzylalcohol111-91r Bis(2-drloncebory)medEne111-44-4 Bis(2drtolitetryt)eher39€?&32-9 Bis(2-ct{ooisopropyl)eher117€1-7 Bis{2+hylheryl)phthalatel0l-55-3 +grcnrophenyl phenyl oher0$€&7 Butylb€nrylphthalate8d7rt{ Ca6azol65q5&7 +Chloo-3-m€thy'phenol106-47{ +Chloroaniline9i.5&7 2-Chloronaphthalene9$574 2-C.hbrophenol7005.72'3 +Chbrophenyl phenyt ether21&01-9 Chrysene517&3 Oib€nzo (e,h) anhracene1 32d{ OibenzoJuran95-5G1 1,2-flichtomberEene541-F1 1,3-OlcHomb€nzene106...6-7 1,4-Obl]ldob€nz€ne91-94-1 3,3'Oict{oaobenzidine120€3-2 2,+Dichloropheioli446-2 Diethylphthatate13111-3 Dimethyl phfl1alate105$7,9 2,4.Djmelhytphenolu-7+2 Di-n-buty'phthetaE$4-5ar 4,6-Dinit'q2-m€thylphenol51.2a.5 2,4-Dinibophonol'r2r-1+2 2,+Dir.litotoluefle60e2G2 2,6-Dinitotoluenei17€4{ D-n-odylphdrahte20H4{' Ffuorenhene86?!7 Fluoren€11&74-i HexsOhlororrelp€n€876a.3 H€xadorobutadienen474 Hexacfilorocydopentradiene67.72.1 Hex€dtloroethanols939r5 Indeno (1.2,3-cd) pyeoe*124 l-Lle0tyln€phtf|alene7849-1 lsophorwt€91-574 2.MetrytiaFht\aler€9s-1&7 2.Methylptl€nol10e39-a, 3.4-MethMphenolt06'44-591-2G3 t{aphthal€ne8€-71-a z-Nitroanllln€
$ttiho€nilino
BRLBRLBRL
BRLBRLBRLBRL8RLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRL
BRL
BRLBRLBRL
ugftsIrsftst CikS
!gr(sttgul(gpsiksps/r9
!9aSggftsp9lts
t g/ks
t c/ks!gkspdks
!gftgtrdtsrdkspsrqtpg4(g
rg/t(spdkspgks
!dks|lgn(ST€]KS|rsfl(gusrks
rcrkspgrkg
lrS/kS!g/Kg|lsftslsftsps/ks
rurk9t4/ks!g/kspg/ks
tlgr|(guofto
ugfts
9S*9||s*st sftstt$rkspdks
t g/kS
flgr(s|,9r(Sps,ks
635
635
635
635
635
635
635
635
635
635
835
635
635
635
635
635
635
635
635
435
6it5
635
635
635
635
635
635
(i)5
635
635
6i15
SwE46 8270c 22+'!,.at47 25 nar47 7031282 M.B
ThIj l4borsb.y tepora is nd val l x,ithozr sn oaahoried sigrrauE on the awr page.
' R€Dart$tc Det€ction Limir BRL: Below Reponing Limh Fage 65 of 152
Page 422
Sample IdentificationMtFB-5
sA594g-13
Client Proi€ct #301 .68
Collection Date/Timel5-Mar-07 00:00
MatrixBallast
Received
l9-Mar-07
CAS No. Andlta(s) ResuIl FluS Anits TRDL Itethod Ref,, Prcpued Ana,.ed Bolch AMIjst
Semivolrdle Orgrnic Compounrls by CCMS
Sernivolatile Orqanic Comoounds bv SW846 8270C
Prepared by method SW846 35508100{1$ 4-Nitroaniline9S-9+3 Nitrobenz€ne8&7+5 2-Nitrophenolic+02-7 4-Nitrophenol02-7tg N-Nitrosodimethylamine621{4-7 N-Nitrosodi-n-propytamine6&3G6 N-Nitrosodiphenytamine87{G5 Pentad orophenolas{l+ Phenanthrene10&9+2 Phenol129{0{ Pyrenet1016-1 Pyridine12G€2r 1,2,+Trichlorobenzene9&95-.1 2,4.+Trichlorophenol8846.2 2,4,STrichlorophenol
Sunog8[e r*ovedes:32140-8 2-Fluorobiphenyl36r-t21 2-Fluorophenol41e5{44 Nittobenzene45416!,62-2 Phenol4sl7le5t4 Teryhenyf4l4ll8-79-O 2,1,6-Tib.omophond
Toarl M€trb by EPA 60{0/7000 S€ries M€thods
BRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
421 936
4527
8RL
BRL
8RL
1 2 . 7
0.565
3 1 0
3 8 9
BRL
Coftpleted
BRL
BRL
0.0073
BRL
BRL
BRL
BRL
BRL
!g/kg 2540
!g/kg 635
LiSftg 635
Uglkg. 2540
!g/kg 635
u9/k9 635
pgkS 635
lSrt(g 635
pg/kg 635
pS/kS 635
pS/kS 635
!S/kg 635
ugftg 635
LiS/kg 635
pSftS 635
n-130%
15-110 %
30-130 %
1Ul10 0A
30-130 %
15- l10 %
mS/kg 0.02SG
mg/kS 0-958
mS/kS 1-U
mg/kg 0479
mSftS 0.240
nEftS 0.479
mg/kg 0 719
mS/kS 1.44
mg/l 0 0100
mg/l 0 0150
mg/l 0.0050
mg/r 0.0025
rngl 0.0050
mgl 0.00040
n€/l 0.0075
mgn 0.0150
1 SW8467471A 26-Mari7 26-lvlar{7 7031311
EPA 200 7 m-Mar-o7 26-Mar-07 7031263
SW846 8270C 22-Mar07 25-Mat Ol 7031282 l\1 B
BD
LR
743S€7€ Mercury
Toarl Met8k by f,PA 200 Seri€s Methods
74,1+22-4 Sifuer
7'|?{}-36-? Ar€€nic
74@3e3 garium
7140419 Cadmium
ziul.47-3 Chromiuft
3S-m-1 Lead
zec49-2 selenium
LR
SPLP Mctd3 by EPA l3l2 & 6000t000 Serie! M€thods
SPLP Extraction
7,t40-22-4 Sifuer
7440-3&2 ArEenic
Zl40-39-3 Barium
7r!40-4$9 Cadmium
71t{o-a7,3 Chrcmium
213997€ Mercury
7,l:|9-g2-1 Lead
77824$? S€leniurn
1 SW8461312 21-Mar{7 21-Mar47 7031223
I SW8461312/6O108 22-MaA7 23-Mat47 7031323
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vpLR
Thb kborstory nporl k rol volil wilhout on Quthodzed sigfltarc on the are? page.
' ReFortabl€ Dctection Limit BRL = Below Reporting Linit Page 57 of I52
Page 423
Sample IdentificatiopMSFB{SA59?t6l- l4
Client Proiect #301-88
Mat.ixBallast
Coll€ction Date/Tim€I 5-Ma.-,07 m:00
Receivedl9-Mar-07
CAS No. Anutfie(s) Resulr Fl4S U,,i6 .nDL Dilaion Mahnd Rctr. P,tptEd A'u4aed Bdch Aaalyst
Volraile Oryr c Compoundt
Volatile Oroanic ComooundsP.epared by m€thod SW846 5O35A Soil (tow tevet)76-111 1,1,2-Trid orotrifluorcethan€ (FreoBRL8744t Acelme BRL107-13'1 Acrylonibile BRL7143-2 Benz€ne BRL108{&.1 gromobenzene BRL74-97.5 BronodllorometfEne BRL75-274 Brornodid oromethane ARL75-212 grornotorm BRL74€3-9 Bromomothane BRL7a€13 2-&rtanone (MEK) BRL1lM-513 n-Bulybenzene 8RL13+s{ sec-Butylb€nzene BRL98{6€ tert-Butylb€flzene BRL75-15-0 Carbon disutfd€ BRLf!e2+5 Carbon tofachtoride BRL10&90-7 Chlotobenzene BRL?:.{G3 Chloro€thane BRL6766-3 Chtoroform BRl-74€7-3 Chloronethane BRL95-49€ 2-Chloroduene BRL106-434 +Chlorotduene BRL9sl2{ 1,2-Dibromo-}dtloropropan€ BRLi2a-4€n Dibrormchloromethane BRLr0+$r t,2.DibfEmo€h6ne (EDB) BRL74-95-3 DibrcmonEthane BRL95'5Gl i,z-Dichbrobenzene BRL541-73-1 l,$Dichlorobenzene BRL10846-7 l,4-Dichlorobenzene BRL7s-71-a Dichlorodinuoromefiane(Fl€onl2)BRf75-3+3 |,1-Dldrloroeihane BRL107{6-2 |,2-Dichloroehane 8RL7fis-4 Ll-Dichloro€{hene 8RLi5e5o-2 ois-1,2-Olchloro€thene BRL156-60-5 t€ns-t,2.Oichloro€thene BRL7a+7€ 1,2-DichlorEpropane BRL11?-28.9 1,lDbHorcprcpene BRLss+20-7 2,2-Dhhlo{Dprop6ne BRL56}584 l,l-Dicf oroprop€ne BRLi00€1{l'5 cis-'1,3-Dichloropropene BRL1006r{2€t"ns.l,3.Dlcfiloropopene BRL1m-41-{ EgylberEene BRL€7$&3 Hexad orobutadiene 8RL59t7+6 2-Hexamn€ (MBK) 8Rf90{2{ lsopmpylbonzene BRL
4-lsopropylblueno BRL163.{4-a M€thylta.t-bug'lethe. BRLt0s10r +Methyl2+entanone(M|BK) BRL75.0$2 Mehyten€ chtoride BRL91.20-3 Nephthalenet03-65.1 n-Propyltreflzene
Idkgw€l 42
tdkg lr€l E4.6
!S/kg vr6t 4.2
t S/kS vret 4.2pgftS t€t 4.2
Ug/qwet 4.2
Fg/kg wet 4.2pCASwel 4.2pdkg rrsl 6.5pgy'kg wet 42.3
lgrkg wel 4 2
Ugl(S lr€l 4.2
USI(Swet 4.2
ldkS wet 21.2pg/kg Y/€t 4.2
t dko w€t 4.2
Idko wet 8.sygyto wet 42pdtgwel S-5
ldkgwer 4.2
lgy'tg wel 4.2
Ugkgwel 8.5
USI(9 Yrel 4.2
US/kS wet 4.2
FdrS Yret 4.2pg/kg wet 4.2
Ig/kg wet 4.2
Igkg u/et 4.2
ugy'kg wet 8-5pgxgwel 4_2
Udlgwer 4_2pgn€ w6l 1-2
Ugftgwet 4.2
lgxgw€l 42
lg/kgw€l 4.2
frgul(g wet 4.2
Fgr'kg w€t 4.2
UqkS Yret 4.2pg,/rs s.,€t 4.2pgflqwst 4.2
FC/kS wet 1_2pgftgwel 4.2pdkgwel 42.3
ldkgwel 1-2
Igkgw€l 42
!g/l(g w€t 4-2
f.,guftg wet 42-3
t gks Y/€t 42-3
t gkg wet 4.2pr/kS rvet 4.2
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BRLBRL
Thit taborQbry eporl is aot volid wirtord sd zafhoizel si.f.'ra$tr. oa the covs page_
. Rc?ortable Derectioo Limir BRL = Betow Repoding Limit Page 68 of 152
Page 424
Sample IdentificationMtFB.6
sA59464-14
Client Project #301 -88
Collectiofl Datc/Timel5-Mar-07 00:00
MatrixBallast
Received19-Mar-07
CAS N^ Analytets) Resull FloS Uni6 *RDL Merhod ReJ, Prcpa.ed ,hulyze.t Buch ,ladyt
Volotile Orgrnic Compounds
Volatile Orcanic ComooundsPrepsred by method SW846 5035A Soil (lo' , level)10Oa2-5 Styrone${Fa}€ .1,1,1,2-Tetrachtoroethane
7+34-5 l,'1,2,2-Tetrachto.oethane127-18.1 Tetrachloroethene10&e0{ Toluene87€1{ 1,2,}Trichlorobenzene120{?,i 1,2,+Trichlorcbenzonell{5-6 1,'l,1-Tridtloroelhane794G5 1,1,2-Tachlomethane79{1{ Trichloroet}Ene
pgftqwel 4.2
yqy'kg wel 42
Ug/kg wel 4.2
pgL/kg wel 4.2
pg/t(g wet 4.2
lgikgwet 4.2
pg/kg wet 4.2
!g/kg wet 4.2
pg/kg wet 4.2
UgL/kg w€t 4-2
!g/kg wet 42
Ug/kg w€t 4.2
Ug/kg wet 4.2
!g/kg wet 4.2
pg/kg wet 4.2
lrg/kg $ret 8-5
pg/kg wet 4.2
Fg/kg wel 42.3
!g/kg wel 4-2
pg/kq wel 4.2
Ig/kg wel 4 2
!g/kg wel 42
t4/kg wet 42.3
lgr'kg wel 84-6
70-130 %
70-130 %
70-130 %
70-130 %
rYE/.kS 25.4
rnsftg 25_4
'rVkS 25-4
ftrSrkS 25.4
'iSftS 25.4
mSikS 25.4
nE/kS 25.4
nVkS 25.4
nE,kS 25.4
rnSrkg 25.4
40-14] %
BRLBRLBRLBRLARLARLSRLSRLBRLBRL
BRLSRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
103t06112104
Field extractod
BRLBRLBRLBRLBRLBRLBRLBRLBRL8RL
t 1 1
I
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SW 846 82604 22-MaiO7 22-Ma(47 7031291 RLJ
75{9-4 Trichlorofluororn€thane (Freon 11} BRL5-r8-4 1,2,3-Tichloropropane95-63{'1,2,4-Trimethylb€nz€ne10e67{ 1,3,s-Trimethytbenz€nef5414 Vinyldlloride1330-207 rn,p_xylene5476 o-Xylene109-99€ T€fahydrofuran60.297 Ethyteth€r!l9tt-o5!8 Tert-amyt methyt ethef637.s23 Ehylt€rt-bslyjelher108-20'3 Di-isopmpyleth€l7t65{ Tert-Butanol/ butyl elmhol12+91-l l ,4.Dioxane
S0nogala /Bcovsr'es:44o-tn4 +Brcmofluolobenzene2037+G5 Toluene4S1706+074 1,2-Dbhlorcethane-d4t868-SU Dibtomofruaronelhane
VOC Extraclion
Exlirct ble P€lrolerm HydrocarboN
Extractable Total Petrol€um HvdaocarbonsPrepared by method SW846 35508
8006{1-9 casoline6e47Ho+ Fuel oil #26ea7e31-3 Fuet Oil #46e5${G4 Fuel Oil#6M0980000o Motor Oil.re010(x|0o Aviation Fuel
UnidentifedOlher OilTotal PetroGum HydrocatuonsCgC36 Aliphalic HydrocErbons
SunDgafe Ecovenbs:$e6-12- 2 I -Ch btooc Ia de ca ne
Semivobdle Orgtic Compoonds by cC
Oroanochlorine Pesticidos SWE46 8081APrepa.ed by merhod SW846 355083o+olr2 Aldrin
VOC 20-Ma.-07 20-Mar{7 7031156 B D
+CTETPH 22-Mar-o7 26-Mar477O31283os
BRL !ciks 13.7 SW846 E081A 21-Mar47 26Mar07 7031171 TG
Ih.J labororory epod Is nol eolid n ithout an arltho.ized signatare ot the cover page
+ Reporbble D€iection Limit BRL = Below Reporting Limit PaBe 59 of 152
Page 425
Samole ldeatificationMSFB{s459464-t 4
Client Proiect #30t-88
Matrl(Ballast
Collectiotr Dat€/TimeI 5-Mar-07 00:00
Receivedl9-Mar-07
CAS No- Analrte(s) Resalt Flag ania *RDL Dilatun Method Rel, Prcptred Ansbaei Bdch AMU'I
Sedivoldile Orgrtrtc Compo{nd! by CC
Omanocfi lorine Pesticides SW846 8(E1APrepared by rnethod SW846 35508319€4€ a-BHC31F€s-7 b-BHC3'l$86€ dSHCs8€ee g-AHC Gindane)57-74-s Chlordan€72-544 4,+DDD (p,p')72-5re 4,4-DDE (p,p)s0-2e.3 4.4-DDT (p,p.)6Gs7-1 D€lddn95998€ Endosjlan I332136$9 Endosulfan ll1031-07{ Endocullan Sullate7?-?0-8 Endaln7421-93-a EndrinAldehyd€76-{.1-€ Heptachlor72'a.3-5 L{etprychlor1024-57.3 Heptachlor Epoxidea0o1-3t2 loxaphene5103-7i-9 a-Chlordane566€F34-7 g-Chlordane53494.70-5 Endrin l(ebne
Su'rogate a€co@rtes;fi386a+2 44-DB4clanuo@biphenyl (Sdms1.24 Decadbtubiphenyl (Sr)Polvd orinated BipfEnvls bv SW846 8082Prepafed by mettEd SW846 3550812674.11.2 PCB 1Ot6r11o4.n-2 PCg 1221r1141-16$ PCB 1232s34€+214 PCB | 24212672-29{ rcB 124811097{S1 PCB 125411096{2{ PCB 12603732+23-s PCB 12t21l1m-14.1 PCB 1268
SlrtDgab rEcor,ct€sr1 $8e8+ 2 4,4-OB-o('anuorofipheny' (Sr)w5t-243 Decachlotobiplonyl (Sr)
Semivohtile Orgarlc Compoutrds by CCMS
21-|tb(47 26]l.natr47 703117t TGBRLBRLBRLBRLBRLBRLgRL
BRLBRLBRLBRL8RLBRLBRLBRI-BRLBRLBRLBRLBRLSRL
70128
BRL
BRLBRLBRLBRLBRL8RLBRIBRL
751m
BRLBRLBRL
BRL
BRLBRLBRL
u9/k9l.rca9Fdlq
fdkg
t,S/kg
r9ftg
ugfts
lgftst SikgtiSikSpsrkspgrr(9
rjgkg!gtsusl(s$slkspdks
t dksr{'tglgk9pcrkg
13.7
13.7
13_7
13.7
68.7
13.7
13_7
13.7
7.ffi
13.7
13.7
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13.7
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sw846 8081A
sw646 8062
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30-150 %30-1fi%
Semivolatil€ Oroanic Compounds bv SW846 82 rcPrepared by me iod Swgil6 3550883-32-9 Aoenaph0€dea|&964 Acenaphtirylen€@-5$3 Aniline12G12-7 An{iracaEr912-2L9 Alrazina10933-3 Azobenzen€y'Oiphenyldiatne9247.5 B€nzktine56-5+3 Eenzo (a) anthracene
2.-Met47 2*lat47 7031 282 M.BpgJks
!9/ksusftslsftspgfts
t€/K9rc/rgTSAg
629mg629
629
629
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629
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ThjJ lab.alory Eport ir Eat wIU withoa za aythotizd slgaaat . oa rte @wr Fage .
I Repo.table D€tection Limit BRL = Bdow R€podiog Limit PaEe 70 ol 152
Page 426
SarEple IdentificationM$FB{sA59464-14
Client Proiect #301 -88
MatrixBallast
Receivedl9'Mar-07
Collertion Datc/Timel5-Mar-07 00:00
CAS No. Ar'alru(s) Fhc iRDL Dilatinn Dlethod Retr Prcpared Anallzed Bo!.h Analfsl
Semtvolrlile Org€ric Compounds by CCMS
Semivdatile Omanic Comgounds bv SW846 B27OCPr€pa.ed by method SW8,l6 35508
s0-32{ Benzo (a) pyrene
205t99,2 genzo (b) fluoranhene191-2a-2 B€nzo (g,h,i) perytene
20748-9 Benzo (k) fluoranthene0t65{ B€nzoic acid10G515 Benzylelcohol1 r 1 .91 r Bis(2-ctrtoroethoxy)anethanefi1-44-4 8is(2-chtoroethyl)efier3e63E.32-9 Bis(2-chtoroisopropyl)ether117{1-7 Bis(2-ehythexyl)phthatater0t-55J 4€rornophenyt phenyl elhera5{&7 Buttbenzytphthalate86.7,t3 Cerhazoles9-5{].7 4-Chloro-3-rnethylphenol10647€ +Chlorcanitine91-5€-7 2-Chloronaphthatene9+s7{ 2-Chlomphenol700+72-3 +Chlorophenytph€nytether21&014 chrysene5$7S3 Dibeflzo (a,h) anthracene132+a.9 Dibenzofuran9t5O-1 l,2-Dichtorobenzene5,41.73n l,3-Dichlorcbenzene106-46-7 l,4roichtorcbenzene91-94-1 3,3'-DichtofobeMidine1AF3-2 2,4-Dichtorophenol84-6F2 Diethylphthatatg131'r1 i Dimethylphthalate10567'9 2,4-Dimethylphenolu-f+2 Di-n-butytphthatate534-5C-i 4,6-Dinilro-2-methylphenol
51-2&5 2,4-Dinitrophenol121-r.-2 2,4-Dinitotoluenee,oe20-2 2,o-Diniliotoluene11744.0 oi-n-octylphlhalate206-44,0 Fluorenthene86-737 Fluor€ne1i&74-l H€XEchlorDbenzene
67€&3 Hexrchlorobutadiene77474 Hexachlorocyclopentadiene4772'1 H€xachloroethane19.3'3&s Indeno (1,2,3-cd) pyrcne
{,G12{ 1-Methylnaphthalene70-591 lsophorone9i5l€ 2-Methylnaphthalene95-4&7 2-Methylphenol
loe-3s-{, 3,+Methylphenol106-{4.591-2G3 ll€phthalene
88-74-4 z-NitroanilineE9{92 }Nitroaniline
ARLBRLBRLBRLBRL8RLBRLBRLBRLBRLARL8RL8RLBRLARLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRL
BRLBRLBRLBRLBRLBRL
BRLSRLARLBRL
BRLBRLBRL
!s/ts!s/Ksugr(9ugkspgfts
lrs/ks!s/xs!dks!9lksus/ks|ls?Ks
ugfts
|lg/tg
lrg/Kg
rcr(gllg/Kg
FS/kg
!dks
!sfts
!sn(spsfts
!grk9Ps/kspqksps/kspgikg
ps./kspsaspdksps/kspgikspgn(9
!sikglrs,4qpsfts
!s/ksps/kspdks
Ps/ks!siksps/kspdks
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629 1
62S I
62S 1
625 'l
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Thh tahorulory rcpo,1 is .toa roIU t+itho,tt an atthorized sEntturc on the cover psAe .
+ ReDorbble Detection Limit BRL = Betow R€Dortine Limit Pa.ge'7 | of 152
Page 427
Sample ldepdficationMtF8.6
s45946+ t4
Clieut Proiect #301-88
MahixBallast
Received19-Mar41
Collection Datr,/Timel5-Mar47 00:00
CAS No. Analfta(s) Resut ruS Urtus +RDL Diluion Method Rqf, hepared Adalfud Bckh A4lyst
S€mivol.tile Orgrdc CoBpo!trds by CCMS
Semivolatil6 Omanic Compoonds bv SW846 8270CPrepa.ed by method SW846 35508
100{r€ +Nltoaniline98-!'$3 Nitrot€nz€n€0F7+5 2-Nitropheml10G02-7 .l-Nltroph€nol
62-7tg N-Nibocodirn€thytamine62161-7 l&Nibo6odi-n-propylamine8€-30{ N-Nibosodiph€nytamine87€F5 Peota{:foroph€nol
8+O1{ Phehanth.enet0e95-2 Ph€nol12900{ Flfef1e110€&1 Pyridine120{2-1 .1,2,+Tridtlorcbenzen€
ss€s-4 23,+Trid{ofopienol8446.2 2,4,GTrichlorophenol
Surogate recoyerigsr32140-8 2-Fluotobiphenyl
3$7-12a z-Ffuarcphenol
4165-604 Mtobenzene4s
1t6042-2 Phenol45
17tes14 Teffienyl4l4
1 1E-79-6 2,1,&Tnb@fllopl'F.not
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I '
t '
l '
1 '
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1 "
BRLBRL8RLBRLBRLBRLBRLBRLBRL8RtBRLBRLBRLBRLBRL
48193S284928
US/I(S 2520
lsftS 629
rc/kg 629pgAS 2520
tqlkS 629
ugl(s 629psftS 629pdks 629
!S/(9 629
lSftS 629pdks 629
WlkS 629pS/kS 629
W!l(g 629pdkS 629
&-130tsf io %36tm %1U110 %3d-130 %15-110 %
6€/k9 O.9{3
nE/kS 1.41
msfts 0.472
ntgrkg 0236
fiSl*S 0.472
org,rg O.7O7
mS/kg 1.41
ng/l 0-0100
(€n 0.0150
mg/l O.0O5O
n€I 0.0025
mSrl 0.0050
mdl O-(x}o{o
mdl 0.0075
mg/l 0.0150
EPA MO,774{G22-4 Sifuor
74-4S3&2 Arsenic
744G3$3 Eadum
7440-rgg Cadmium
7440-{7.3 Cfuomium
743992-l Lead
-/824+2 S€l€nium
Tord Met b by EPA 6000/7000 sede! M€thod!
7439€75 l,lerqjry BRL
Totd Metrk by EPA 200 S€ri€s Methodf
aRr8RL
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SPLP Exhaction Comdet€d7lKG224 Silv€r BRI_
744{F3+2 Asenic BRL
7440-393 Barium 0.0050744r}{3-9 C€dmium ERL74q!473 Chromium BRL743047€ l\r€rcury BRL7130{2-1 Lead BRL
7|&4$2 S€lenium 8Rf
mglkg 0.029] 1 SW846 74714 &lii€r47 2641,a'47 7031311 YP
1 SW84613'f2 214ta'47 21.lrlat47 7031229 SD
1 SW8461312/6O108 2-Mat47 nl{8t47 7031323 LR
1 "
1 '
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I SW8461312/60104 ' 23{16r{7 7fr11323 LR
Thh hbodo4 reporl ls not vstirl w hoa an oadtodaed siFtt4jare on the cov.. pqc.
'Reportable Detection Limit BRL = Below Rcpding Limit Ptge 72 of 152
Page 428
TASK 210.SUBSURFACE SITE INVESTIGATION
New Haven RailYardTemporary M-8 Acceptance Facility
New Haven, Gonnecticut
Volume 3
ConnDOT Assignment No- 202-3464ConnDOT Project No. 301-88
Prepared for: Prepared by:
m_99:.
State of ConnecticutDepartment of TransportationNewington. Connecticut 061 31
Maguire Group lnc,One Court StreelNew Britain, Connecticut 06051
Apnl24,2OO7
Page 429
APPENDIX ERailroad Tie SampleLaboratory Reports
Page 430
Sample IdentificationM8FT.Is,459464- t 5
Client Proiect #3 0t -88
MatrixWood
Collection Date/Timel5-Mat01 00:00
Received
19 Mar-07
CAS No. Anc+4(s) nesqlt Flag Unlb rRDL Ditution Mertod Ref. Prepdred Anauzed Bztch Atu UstYoladl€ Orga|Iic Compouhds
VOC Extr3clion Lab extracted
6,020
yS/kS 387
pg/kS 7730
lgftS 3a7
lgrkS 387
pg/kg &7
FS/kS 387
pSAs 387
!S/kS 387
rcn(S 773
ttSkS 3870
!S/kS 387
!S/kS 387
!g (g 387
ySn(g 1930
USrkg 387
rrSftg 387
uqkg 773
!gn(S 3a7
FSrkS 773
trg^S 3aI
US/IS 387
pSi<S 713
lgkS 387
lg/kg 347
!g/kg B7
ug/kS 387
WtkS 3El
trSAS 387pg/kS 773
pg/kg 347
w(g 387
US/kS 387
t gkS 387
!S/kg 3a7
Ig/kg 87
US/kS 387
pgtkg 387
pSftS 387
pSftS 387
pS/kS 387
pSftS 3A7
!SI(S 387
€/rg 3870
pS,kS 3a7
pgAS 387
pg/'(S 387
lSftS 3870
UdkS 3870
ISftS 3a7
1
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505050
5050505050505050505050505050505050505050505050505{)
505050505050505050505050505050
voc 20-Mar-07 20-Li1ar07 7031156 BDVolalil€ Oroanic ComgoundsP.epared by method SW846 5030 Soil (high levet)76.13-1 |,'l,2-Tdchtorotrifluoroethane (FreoERL67€4-1 Aceton€ BRL107-11-1 Adldonitnte BRL114l-2 Benzene BRL10&€6.1 Bromobenzene BRI_7197.5 B.omochtoromethane BRL15-2f4 Bfornodichloromethane ARL15a5-2 Brenoform BRL74a19 Brchomethane BRL
2-Blbflone (MEK) aRL10+51{ n-Butylbenzene BRLi3198{ sec-Butylbenzene BRL98.06{ t€rt-Butytbenzene BRL7!F1:F0 Ca.bon disu tde BRL5&2$5 Carbon tetrachloride ARL10&90-7 Chlorcbenzene BRL7fiGs Chloroethane ARL67€s3 Chtoroform BRL744f-3 Chlolqmgt!46s BRL95,{9{ 2-CblorotoJuene BRL106-43-4 4-Chlorotoluene BRL96^12{ 1,2-Dibromo.3{.hloropropane BRL12{-{t-1 Dibromochloromethane BRLi0s93-4 l,2-Oibrornoethane(EOB) ARL749s1 Dbromornethane ARL95S0-1 l,2-Oichtorobenzene ARL54t-7J-r l,3-Ocruofobenzene 8RLl{An6'7 1.4-Dichl€fo,benz6n€ BRL75.714 Dichlorodanuoromethene (Freonl2)BRL75-3it-3 1 , i Oichloroethane BRLloru6-2 1,2-Dichto.oethane BRf75\3s-4 l,l-Dichloroethene BRLi56-€s2 cis-1,2-Oichtoroehene BRL156.6{16 trans-.1,2-Dichloro€thene BRL78i7-s |,2-Dichloropropane BRL'14?-2&€ t,3-Dichlompropane BRLs+tu1 2,2-Didllorc,propahe BRLs6lse6 i,1-Dichloropropene BRL10061{1-5ci9l,3-Dichloroprcpene BRL10061{2-€ lrans.l,3-0ichlorcpropene BRLlo0r14 Ethytb€nzene BRL67$&3 l-l,exachlorobutadiene BRL591-70€ 2-tbxanone (MBK) BRL9&824 tsopropytbenzene BRL9{l{7-6 +lsopropyltoluene BRL16r'4{€ Mebyl te(-butyl ether BRL1o+rGl +Methy'-2-pentanone(M|BK) BRL7tO9? Methy!€ne cfilodde BRL
SW&+682608 21-Ma(47 22-Ll,a?0r ru1r89 jro
91-2G3 Naphth€tene
PaBe 7l of 152
Thk bboratory repod is,tot rdid wirhoar an aurtoizpt sig',eture on ttu coeet page
'Reportable Det€.ction Limit BRL= B€tow ReDorting Limit
Page 431
Sampl€ IdetrtificationMEFT-1sA59,r6t- 15
Client Proiect #l0t-8E
Matrixwood
Collection Date/TimeI 5-Mar47 00:00
R€ceivedl9-Mar47
CAS Na. Anzly.(s) Reszb Flzg .RDL Imuion Method Rctr Peparcd Aazlycd Bdkh Analtst
Voladle Orgrnic Compounds
Volatil€ Orqaoic ComooundsP.epared by rEthod SW846 5030 Soit (high tevet)103{5-1 n-Pmpytbenzene BRLroo-4z-E Sgr€ne BRL630'20{ 1,'l,1,2-Tetrachloro€tr|ane BRL79.3.1-5 1,1,2,2-Tetracl oroethane BRt127-tB-4 Tetracfitoroethene BRL108-8€-3 Toluen€ BRL87{1{ 1,2,3.Trichlo.ob€nzene BRL12G02-i |,2,{_Trid o(ob€flzene ARL71-55€ 1,1,j-Trichloroethene BRL794G5 1,1,2-Trid oroelhane BRL79{1 6 Trichlor€thene BRL?s€94 Trichto.ofruoromethane (Freon .11) BRL96-1&4 .1,2,$.lrichtoropropane BRLs633-6 1,2,+Tdmehytbenzen€ BRLio&€74 1,3,5-Trim€fiLlb€nzen€ BRL75.o1ir Mry' chloride 8RL1330.2c7 m,p"Xylene BRL95-475 o-Xylene BRLt0$9s-9 T€bahydrofuran BRL6{rzs7 Ethyt ethe. BRL99.4-05{ Tert-amyl methy' elher BRL637-92-3 Ethyt tsrt-butytelh€r BRLt0&20-3 Oj-isopropyt ether BRL7s€si Tert-&rtanot / buv alcohol BRL12+91-1 '1,4-Oioxan6
su,rogale rccovades:450401 +Bromof,uorobenzene2037-2Gs Tduene-de| 70@07 4 1,2-Dbhloroethano441868-s77 Dibtdnofluotomethane
Eitrrchble Pet|.oleum llydrocrrbons
Extractable Total P€lroleum Hvdroca,bonsPrepar6d by m€thod SW846 355088OCOS1-9 Gasoline68a7B3ez Fuel Ot #l6847e31.3 Fu€l Olt #4685s3.04-{ Fuel Oit #6M0€q)000{) Motor OilJ001oo0o0 AYiation Fuel
UnidentifiedOS|er OilTolal P€0doum Flydmcarbons@436 Aliphattc Hydocarbons
sunwab fecoveries:3386-33-2 l-Chlotwtdocene
S€mirolrtile Orgrrlc Compou||ds by ffOroanochlodne Pesticiles SW846 8081APrepared by method SW846 3550830+oG2 Atddn
SW846 82608 21-tiar47 224a-o7 7031189p949pgfts
ugksrs^9usfts!sn(9rgftgpo/k9ygrspgkg
|lsftsr8/kstryrcpgkg
rcrksrslkst oftsgslksggtspsfts
FSrkSpdr9
usftslsiksllgr(s
387
30?
307
387
382
87
387
387
3a7
A7
387
387
387
387
347
3E70
347
387
387
3t]7
3470
7730
5050505u50505050505050
50
50
50
505050
1 1 1102109103
70.130 %
7G130 %
7G13O %
70-130 %
BRL8RL8RLBRLBRLBRL1 t.600C€lc1llat€d E6| 1,6001'|.600
rcT ETPHnrSAS
mg/kS
rEftg
nsn(0'nS^9
lnglg
fiigl(g
mS/kS
o€r*g
mc^s
99.2
99.2
99.2
99.2
99-2
992
93.2
9S.2
99.2
2-Mar47 H.,',ar47 703128:l DS
4114) %
trsas SW84A 8081A 2l-Ma!-07 zs{lsr{7 7031171 TG
Thit labnloty r.tori b ,rot lolU '{'ttho,.t aE outorizd signztur. on thz co''a page.
. Rep(rtttrlc Detect'ton Limit BRL = B€low R€portinC Limia Pdge 74 of 152
Page 432
Sample IdentificationMEFT-IsAs%64- l5
Client Proiect #301-88
Collection DatdTim€l5-Mar-07 00:00
Mat ixWood
Rec€ivedl9-Mar-07
CAS No. Anelruts) F,oC Urirr +RDL Dilt'tion Method ReJ Prepued Atullzed Balch Ahaust
SedivolrliLe Or$ric Compoundr by CC
O.qaflochlorine Peslicides SW8,+6 8081APr@ared by method SW846 35508319{4-€ a-BHC31e€s7 b-BHC31S{fi d-BHCs€{s-s g-BHC (Lindane)57-74-9 Chlofdane12-54{ 4,4-DDD (p,p,)n-s+s 4,4.OD€ (p,p,)s0-2+3 4,4-DDT (p,p.)m-57-1 Dietdrin95948-8 Endosulfan I332t36ts Endosulfan ll1031ry{ EndosulfunSulfatell2-?o-A Endnn742r-9il-4 EndrinAJdehyde76-44-0 Heptachlor7243-5 uethorychjor1024-57n Heptachlor Epoxide€Ooi-352 Toxaphene51o}7i.9 a-Chlordane55ffi4-7 g-chtordane53494-rc-5 Endrin Ketrne
Su|rDgsf€ r€cor€niesr10386-812 4,4-D8-Odanuorcbiphenyt (Sr)m5t-2a3 Decachlorobiphenyl (St)Polvcfibrinared Biohenvls bv SW846 8082Preparod by melhod SW846 35508126?+11-2 PCB 10161110+25-2 Pc.B lZ2111141-16-5 PcB 12325346921,9 rcB 124212672,235 rcB 124811W7{&r PCB 1254r i096{2-5 PCB 1 m03f32+2T5 PCB 1262i1t0G11,1 PCB 1268
Srr/togats aecover'esr
SW846 8081A 21-Mat41 26-Ma(07 70311f18RLBRLBRL
BRLBRLBRLBRLBRLBRL
8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRL
843
BRLBRLBRLBRLBRL168t648RLBRL
t siksllsftsps/ksps/}s
tlg/(g
Lrg,r(9
wKg
!s/kgpgrkg
ps/kspsrqpgag
Lrg/xg!sft€pg&s
tlsiftst 9/(9pg/kspg/ng
|lsftspsfts
44.2
40.240.240.2
20140.240.2
6.210.2
6.240.240.240.240.240.240.244.220140.2
44.240.2
1
I
1
1
1
1
1
1
1
I
I
I
1
1
1
I
l
1
1
1
1
u9/tgusftg!9ft9
!9/Kg
!9/1rSps/kstrS/kSusr(suEks
3G150 %
30-150 %
sw846 8082
swE46 8270C
80.380380_38038 0 38 0 38 0 380_380_3
21-MatO7 244Jlarl7 7031170 SM
fi3e04+2 4,+DB4cbnuarchiphenyl(Sr) 65
m51-2+3 Decachlotobiphenl (S!) 95
Se.dvolalilc O.ptric Compounds by GCMS
Semivolatile Oroanic Csnoounds bv SW846 8270C
Prepared by method SW846 35508
a3{2.9 Ac€nEphthene
A)&96{ Acenaphthylene62-5!3 Aniline12012-? Atrlhrac€ne1912-21-9 Nrzzjne103333 Azobenzene/Diph€nyldiazine92€7-5 8€nzidjn€
5&5S3 B€nzo (a) anFracene
30-150 %3t)-150 %
29.00016,900BRL282.000BRLBRLBRL227.60
rc/tspsfts
!snrs!sr(s!sr(spg&spgr(s
ugts
246024602460246024AO2$O
24602460
22-Nl€t47 64 at47 7O312A2 M.B
Thls laborrlo.y Eporl ls nol valu dlhod an adhotlzctt signature on rte cowr page-
' Reportabte Detelrion Limit BRL = B€low R€porting Limn Page 75 of | 52
Page 433
Samole ldentificationMSFT-IsA5946L l5
Client P.oiect #l0t-88
MahixWood
Collection Date/TimeI 5-Mar4? 00:00
Receivedl9-Mar-0?
CAj N^ AMIlte(s) Resah Flig Ania 'RDL Diluttah Malad Rel PrcWed Analyzen Bach Anelyst
S€mivolalile OrScnic Compoundr by GCMS
S€n1iwlatile Oroaric Compounds bv SW846 8270C
Prepared by method SW846 35508s0-324 BerEo (a) py.eneatrFgs.z Benzo (b) fluoranthenets1-?a-? Benzo (g.h,i) perytene207-cro4 Benzo (k) nuorandnene6s€5{ Benzoic acid1oo5l{ Be62yl €laph6{1t1.e1n Bis(zddorc€thoxy)methaner1 l-aa{ Bis(2-ohloroethyt)€trer3s€r1,8-32-9 Bis{2dtloroisopf opyt)ether117-81-7 gis(2-ehylheryt)phthatate
10r-s5-3 4_BEmopheny' phenyl ethers5€8-? Butyt benzyl phtlalate86-74{ Celbazole50,50-7 4-Chloro-3-rnethylph€nol106-47{ +Chlorosnilin€9r.5€-7 2_Chlo.onaphthalenest57j 2-Clrbrophenol700$72-3 4-Chloroph€nyl phenyl eth€r216-{11.9 Chrysene53-70-3 Oibenzo(a,h)anfnracene132-€4,9 DiberEofuran95'5O-i l,z-Dichlorobenzene541-73-1 l.+Dichlorobenzen€106-,!S7 1,4_Di.fdorobenzen€91-9,1-l 3,3'-Dichhroberudine1203!-2 2,4-Oichlorophenol44s6.2 Diehyiphthatete131-113 Dirnethy' phthatete1H7-e 2.+Dim€thy'phenol8r-7+2 O-n-bu!/phthalate534.521 4,6-Dinitro-2{ethy'ph€nol51-2&5 2,4-Dinltrophenol12t-1,1-2 2,4.Dinibolotuene606-202 ?,GDinibotoluene117-844 Di-n-octylphhelate206-i|{{ Fluo€nthene&-73.7 FlUOren€llBT/t-l Heracfilorobeflzene67{&3 Hexadtlorobutadieneru74 He)@chlorocyclop€niadiene67-f2-1 HexadrlorDethane193-3$5 tndeno (.1,2.3.cd) pyr€neg0-12'o l-Methylnaphthelefle70-5+1 lsoptrorone9i57{ 2-Meby'naphdEt€ne95-,re7 2-Msfty'plronol108-3s.1. 3,4-Mefiyhhenol106-44-591-2G3 Naphhat€ne8a-71.4 2-Nitroar line99{9-2 +Nitroanillne
99,300| 60,00,034,200187,m0BRLBRLBRLBRLBRL
BRLBRL152,0(X)BRLBRLBRLBRLBRL358,000r0,90026,900
BRLBRLBRLBRLtJKL
BRL8RL8RLBRI-BRLBRLBRL876.fi1042,700BRI-
BRL
SRL40,4003,700BRLBRL
BRLBRL
BRLBRI8RL
ps/ks
!s/ko$s/kstrSikSlgftg
Fgl(spgks
!s/ksusftspg/ks
t gukg
!gftSpdks
Fs/ksu9ft9
€4qus/k9pg/rs
!sr(gusftsrc/kgps/ks
!c/ksudkslsrkglsfts|ls/kgFSAgpg/kg
ps/k9!s/tst/gfts
r$/kgt€ltg!s/ksfgks!g/ks|lgftS
u9ftgt4/tgFS/kgpdkspsn(g
wftsrslksrsrtspclks
!s/ks|lgftS
lsrts
2460
2460346024602&r)24602140246024602460246024602460246024602'4fO24ffi2{60246024602460246024602460246024$0246024602,1602460246024602#O24602415024602460246021€o
2{6024602&O246024602460
2M2,160
246024602{li0
SW846 8270C 22Jld47 m.+,,et47 7031262 M.B
n&r ldhrabry report ls aot volid t{rthobr zd 4uthoitzd dgnsafie on rtc co',a page.I R€Dortsble Detecaion Linit BRL = Betow Repfring Limit FaaE 76 of 152
Page 434
Samole tdenlificati'rnMSFT-I
sA59464- r 5
Clienf Proicct #301 -88
Collectiop Drte,/Tirnel5-Mar-07 00r00
MattixWood
Receivedl9-Ma.-07
CAS No. Analtte(s) Resuk Flag Ani6 ,RDL Dilation lrlethod ReJ Preparcd AruUud Bat& AnalrslSemivolrdle OrgrDlc Compouods by CCMS
Semivdatile Oraanic Comoounds bv SWB46 8270CP.epared by method SW846 35508
i0o.{r1{ 4-Nitrcaniline98-9+3 Nitrobenzene8A-75.s 2.Nitmphenol100.{t2-7 4,Nitophenol62-75-9 N-Nitrosodimethtamine621{a-7 N-Nitosodi-n-pfopylamine86-30$ l+Nitrosodiphenylamine87{85 Pentachtorophenol8fl11€ Phenanthreno104.95,2 Phenol129{r{ Pyrene1to€6-1 ryndine12G82-1 .1,2,+Tichlorobenzen€
95-95-4 2,4,STnchlorophenol88{+2 2,4,&Tnchlorophenol
Srlrmgate Bcoveias.n140-B z-Fluorobiphenyl
367-124 2-Fluorophenol
41A5404 Nivobenzene4s
116fi2.2 Phenot45
171&514 Terphenyl4l4
118-7 2.4,6-Tibromophend
Totrl Mctrls by EPA 60001000 Series M€thod$
7439474 Merc!ry 0.(x25
Totil Melrls by EPA 200 Series Mcthodt
BRL
BRL
13.9
o.714
2.96
2 1 8
BRL
TCLP ExlEction
74rulz2-4 Silve.
7440-3&! Arsenic
71.()-393 Barium
744+4+9 Cadmium
7421047.3 Ch.omiom
7a39476 lirefcury
743S€2-1 Lead
?e2-4S2 selenium
1 SW846 8270C 22,Mar47 26.Mat47 70y2A2 M.A
1 '
1 "
1 '
l -
1 "' t '
1 '
1 '
1 '
1 '
1 '
BRLBRLBRLBRLBR.L
BRI.ARLBRL4m,m0BRL640,000BRLBRLERLBRL
492639345548
Completed
BRL
BRL
o.0761
0.0050
BRL
BRL
0.0244
BRL
!S/kg 9850
!gn$ 2$0
tg/kg 2M
USftS 9850
US/kS 24ffi
rc/kS 2460
WkS 2460
!S/kS 2460pg/tg 2460
!S/kg 2460pg/kg 2460pSilg 2460pgr'kg 2460
rc/tg 2460pSAS 2460
30-130 %15-110 %30-130%15-110 0A
30-130 %15-110 %
msftg 0 0291 1 SW846 7471A 26-Mar-07 26{v1ar-07 7031311 YP
EFA200.7 26-Mar{7 26{4a.07 7031263 lR71140-22-4 silver
74,40-3&2 A6enic
7440-3+3 Earium
74404+0 Cadmium
,44147-3 Chrcmium
7439.92.1 Lead
7782-492 Selenium
mSftS 0.904
mS/kg 1-36
mg/'l(S O 452
mS/kS 02m
mS/kS 0.452
mSftg 0.678
mS/kS 1.36
N/A
mSI 0.0100
m94 0.0150
mg/l 0.0050
mg{ 0.0025
mgn 0.0050
n SA O.N04O
nEil 0.0075
mg/l 0.0t5t)
TCLP Metals by EPA l3ll & 5000/7000 Seri€s Methods
1 SW8461311 21-l.lat47 21^ta(O7 7031227 AO
1 SW8461311/6010A 23-lrar-07 24-{4ar-07 7031325 HB
1 '
1 '
t "
t '
1 SW846 131 1/747M ' 2!Mar-O7 70;1326 Yp'f sw846 1311/60108 " 24-Mal.I)7 7031325 HB
1 '
Thk laboratory rcpoa k aot valid roithoar a^ attlhori..d tignotare on lhe cover page .
' R€porbble Det€ction Lihit BRL = Below R€porting Limir Page 77 of 152
Page 435
Samole ldentificationMSFT-2sA,594U-t6
Client Pro.iect #301-88
Colleclior Dat€r'Timet 5-Mar-07 00i00
MatrixWood
Receivcdl9-Mar-07
CAS No. Anatk(s) ResuL F'lag Aai6 4RDL Dilation Meahod R4 tueparc.t ,4idlwd Boeh Aaalf;a
Vohlile Orgrtric Compouod3
VOC Exbaction t',t/A
pdks 204pSAg 4090
!g/kg 2U
ugftg 204
USftS 2M
usrtg 204
Ug/lq 7)4
!gn(g 2O4pgrks 409
f.rSftS 2040
FSrkg m4
!S/tg 2O4
]JSI(g 2O4
ttgikg 1O2O
Ig,kS 204pS/kS m4gg/kg 40€
FSftS 2O4
ttgikg 409pgftS 2O4pS/kg m4
lsftS 409
tE*S 2MpgJkS 204pS/kS m4
!g/kS 204
trSftS 2O4
teikS 204
USftg 409pSI(g m4pSn(S 2O4
t gikg 204
FgrS 2Updks n4pSn(g 2M
l4/kS m4
t€/kg 204pg/kg m4
l/g/ks 2u
|rgftS 204
t4lkg 204
ISftS 2A
!gI(S 2(XO
!9I(S m4pSftS 2u
uSfiS 2O4
UCftS 2040
!g/kS 2040
!g/kS 204
LS extracted
5,690
20-Mar47 20.l}l/'447 7031156 BDVolatile Omanic ComooundsPrepaGd by method SW846 5030 Soit (high tevel)7F13.1 1,1,2-T.id orctrifr./oroethan€(FreoERL67{+1 Ac€tono gRL
t07-i3n Acrylonitrile BRL7143.2 B€nzene BRL10F€€-i Bromobenzone BRL7rl€7-5 Bromochlorcmethane BRL?5-?7{ Btonlodid ,olomellane SRL7125-2 Baomoform BRL74{}9 EromomethaDe BRL78-9+3 2-Birtanone (idEK) BRL104'51{ GButtilbenzene BRL13$9€-8 sec-Butytbenzene BRL9€{64 ted€utylbenzene BRL75-i5-0 Carbon disutfide BRL56-2$5 Calbon t€bachloride ARf10&90-7 Chlorobenzen€ BRL75-OG3 Chtorcethane BRL67{+3 Chtoroform BRL14-Af-3 Cibronethan€ BRL95-49{ 2-Chlorotoluone BRL106-43{ 4_Cf orDbluene BRL96-12.9 1,2.Dbmrno-3-cilorcpropane BRL124-a€-1 Dbrcmochto,romef€ne BRL1oe$-a l,2olbromoethane (EDB) BRL74.9t3 DibronrornefEne 8Rf9+5Gl l,z-CxoHorobenzene BRL541-7+1 l.3-Oichlorobenz€ne SRL106-16-7 l,4-Dicfilorobenzen€ BRL15-714 Dichlorcdinuorome$an€ (Freont2)BRL7$34-3 1, I OicHoroehane BRL107-uG? 1,2-Dichloro€ttune BRL7tn5-4 1,1-Diafiloro6thene BRL15€-50-2 cis-1,2-Oichloro€th€ne BRI-156€0-5 trans-1,2-Dichloaoethene BRL7E{7.5 |.2-DicHoroproDano BRL142-2e€ l,3-Dichtoroplopane BRL594-to_? 2.2-DichloroDrcD,an€r BRL56$584 l,l Oichloroprogend BRLl(106l{1.5cis-1,}OicNoroprog€ne BRL10061{26tens-1,3-Dicilbropropene BRL1oc4l-a Ehldb€nzeoe BRLA7{83 H€xad orcbutadien€ BRL59r-78-6 2-Hexanoi6 (MBK) BRL9e{2.8 lsopropldtonz€ne BRLSg47{ ,l-lsopropttoluen€ ARL16!t44-4 Mehylt€rt-bu$d edr€r BRL1oE'lGt +Metli!'f2+eotanon€(M|BK) BRL75492 Methy'ene d oride BRL
SW 8,f6 82608 21+llat47 224a(47 7031189 iro50505t)5050
50
5050505050
50505050505050505050
5050505050
50
50g)
5050505t)50
50
50505u50
5091-2G3 Naphthalene
Page 78 of 152
Thh ltfurdloty r.pod at nat tdid plthot t a asthodaed sigEttttE on th. cor.t pgL
+ Reportlbl€ Det€.tiotr Limir BRl- = Bdow Reporting Limit
Page 436
Sample [dentificationMSFT-!sA59464-r 6
Ctient Proiect #30 t -88
MatrixWood
Reccived19 Mar-07
Collcction Datc/TimeI5-Mar-07 00:00
CAS No, ,lnalrte(s) F,oS A n s *RDL Dilution Mahod ReJ. Preparcd Analyzed Barch AMltst
Voletile Orgrnic Colrlpounds
Voladl€ Omanic CornooundsPrepa.ed by melhod SW846 5O3O Soit (high levet)
7549-4 Tichtorofluoromethane (Freon j 1) BRL
l096tl n-Propytb€nzene1{t0{2-5 Styrcne63Gm$ 1,1 , |,2-Tetrachloroethane79_34-5 1 , 1 ,2,2-Tetrachloroethane127.18-1 TetrachloroetfEne108-8€-3 Toluene8741€ 1,2,$Trichtorobenzene120-82,1 1,2,.4-Trichlofobenzene71-55-6 I ,1 ,l _Tricfiloroethane
794G5 1,1,2_Trichloroethane7901.6 Trjchloroethene
SW 8{6 82608 21-Mat47 22.11,a.-07 7031189 jro
+CT ETPH 22-Mat47 26-Mat47 7031283 DS
BRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRL
BRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRL
110102106101
BRLBRLBRLBRLCalc lated asBRL33,600BRL33,60033,600
70-130 %
70-130 %
7G130%
70-130%
!sn(spSn(S
us.4(sps/k9
!s/kgpg/r(g
!g/kg
!g/ks!9ft9!g/Kgtstks!sfts
!s/ts!gfts
usnlgr/sast'sftgus/kgtrg/kg
trg/kgpg/kg
pg/re,
psiks
w/ksw/x9
204
204204
2442042042012M2M2042042042042042042A4092012040m4204m420420404090
50
505050
5050
50505050505050505050505t)50505050505050
$.ta-4 1,2,3-Tdchloropropanes5{34 1,2,4_Trimothytbenzene108{7.8 l,3,tTimothytbenzenefs414 Mnyt chtorider33G2[!7 m,pFxylene95-47{ o-Xylene109{9€ Tetahydrofuranfi-zs-7 Ehy' eher9gFO5{ Tert-amylftethyletheren732-3 Ethyt tert-butyl ether10&20€ Di-isopropylethef75{$o Tert-Butanot/ butyl alcohol1299't-1 1,4.Dioxane
Surogate recovedes:160401 +EJtomofluorobenzene
2037-26-s Toluene4S
1 70.@47-0 1, 2 -Dichloroethane-d4
,86&5+7 Dibrcmofluommelhane
Erthctable Petroleum Hydrocarbons
Extradable Total Petroleum Hvdrocarbons
Prepared by method SW846 35508
8069t-9 Gasoline6447+30-2 Fuel Oil#26&176-31-3 Fuet Oit#468553{0-1 Fu€loil#6i.,109800000 Motor OilJ001m000 AviatioD Fuel
Unidentified
Ot|erOil
Total Petroleum Hydrocabons
CSC36 Aliphatic Hydrocarbons
Suno€,ale rccovedes:338tF 3 3 -2 1 -C hto rooct ad e cane
Seoivohtile Organlc Compound$ by CC
Orqanocfibrine Pesticides SW846 8081A
Ptefared by method SW846 35508
30+00-2 Aldrin
mS/tS
mg/kg
ms/'l(g
rnsfl(g
mg/kg
n,gJkg
mg/kg
mg/Kg
mg/tS
fig/kg
09.0
8S.0
89.0
89.0
89_0
89.0
89.0
89.0
83.0
83.0
4G140 %
ps/tg SW8.|n E081A 21-Ma'{7 -tittat4T 7031171 TG
Thls lsbo.aloA rcpo.l is nol wlid witho4 an salhorized sEnalur. oa the cor,c, page
r Repon ble Detectjon Limj! BRL = Betow Reprxrirtg ttnjt Page 79 of l5:
Page 437
Samgle ldentificationMSFT-2sA5946+ l6
Ctieot Project #301-88
Mati{Wood
Collection DatellimeI 5-Mar-07 00;00
Rec€ivedl9-Mar-07
CAS No. AErlrE(s) Resdl Flag U'J^ *RDL Dilaion Ll.nod Rel P4parcd AMIyzd Beteh A"alyst
Sc$dvolriile Orgsdr CompouDdi by cC
O.oanochlo.ine P€sticides SW846 808'lAPr€pared by method SW846 35508
3194+{ a-BHC31S8r7 b-BHC31946-0 GBHC5849-9 $8HC (Undane)
57-74-9 Chlordane72-544 a,4-DDD (p,C)72d+s 4,+DDE {p,C)5lr2s3 4,4-DOT (p,p')
6{1.5/-1 Dieldrine5s-984 Endo6ul6n I33213{5€ Endosulfan ll1031-07-0 €ndosulbnSutfate72-2O-A Endrin7121-93.1 EndrinAldehyde
7&{.A Heptachlor
1243-s irlethoryd{or
102a-s7-3 H€plAchloa Epoxrd€80013+2 Toxaphene51091€ a-Chlodene566&34-7 g-Chlordane
s3494-705 Enlhin Keton€
Sunog€/e recowies:| 038634-2 4, 4D8-Adfiuotohiphent4 ( Sdm51.2+3 Deca&lorobtphenyt (54
Poh/chlorinated Bioh€nvls bv SW846 8OB2Prepared by rnetlod SW846 35508
1267+1i-2 PC8-l0t611104-28-2 PCB 122111111-16-5 PCB, 1232s31n9'21-9 PcB 124212672-2e€ PCB 124811097{$1 PC8 1254rr0g6-82,s rcB 126037321-235 PCB 1262i110G14-4 PCB 1268
Srn/ogate /f,cow'resifi286a+z 4, +DB-Octaf, uotot.iphenyt (54
m -2+3 Decachlorobipheryt (Sr)
Semivolatile Orgrtric Compounds by CCMS
BRLBRLBRLBRLBRLBRLBRLBRL
BRI-BRLBRLBRLBRI.BRL
BRLBRLBRLBRL8RLBRLBRL
73
3?o3
BRL8RLBRLBRLBRL402
BRLBRL
601N
trS/kSuqikgpg/ks
Fgts!g/kspsfts
rulks!dkstqr<s!s/rs!g/tgpsag
l4/k9pg/tg
t,9I(Slrltftgusrt9pdkggs,/ks
|rgftspsikg
41.1
4 1 _ l
4 t . l
4 r . l
205
41. ' !
4 1 . 1
4 t . l
41.1
41.1
41.1
41.1
41.1
4 1 1
4 1 1
4 1 1
41.1
11.1
41_1
SW846 8ollfA 21-Mar47 261nat47 7031171 TG
fr.lfi %30-t50%
|lcfts!s/'kgug[(spsfts
t4^9usaspdkg
t4/kspsrg
42.1
42.1
E2_1
82.1
82.1
42.1
82.1
82.1
82.1
SW846 8082 21-Mat47 24]li,a147 7031170 SM
SW846 8270C 22t at47 ?s1]llzt47 7lJ612a2 M.B
wt f l%m-tf i%
Semivdatile Oroanic Compounds bv SW846 8270CP.€pared by mslhod SW846 355086-32-9 Acenaphttrene208++€ Acenaphtlrylene62633 Anitin€120-12-7 AnthEcene1912-24.s AtEzine10133-3 Azob€nzene/Diphonytdiszine9231-5 B€nzidinss6.5$3 Benzo (a) anthrEcene
r5,30010,400BRL
250,000BRLBRLBRL| 37,000
!9/kg|Jsn€|lsftsusit9us/kglsiks!s/ks!g/ks
221022102210
22102210221022102210
Ihis ltborubry Npod is,tot ralU withou arla?rhart?glslg!.4la€a t,a.ouer IdIg.-* Repoftblc Deteation Limir BRL= Below ReDo{tins Limit Prge 80 of 152
Page 438
Sample [denlificationM8FT.2
sA59464 16
Client Proicct #l 0 t -88
MatrixWood
Collection Date/Timel5-Mar-O? 00:00
Receivedl9-Mar-o?
CAS No. Anabte(s) Resull Flog Ani s 'RDL Dilutian Method ReJ. tuepate.l AndIWd Bafth Anabfl
Semivol.dls O.ganic CompouEds by CCMS
Semivolatile Orqanic Comoounds bv SW846 B27OCPrepa.ed by method SW846 35508
50-32-8 Benzo (a) pyren€
20lFs$2 Eenzo (b) fluo.anth€ner9t-2+2 Benzo (g,h,i) peryt€ne
207{&s Benzo (k) fluoranilr€ne6s-8f,{ Benzoic acid10G51.6 Benz/ alcohol11i'91n Bis(2-ciltoro€thoxylntethane11r44-4 Bis(2<htoroethyt)ehel3sE3&32'9 Bis(2d\loroisopropyt)etfi er117-81-7 Bis(2-ehyth€xyt)phthatate10i.55-3 q-Bromophenyt phenytether
A5{&7 Butybsnzytphthatate86-74-€ calbazol€5S-5t!7 +Chloro-3_meth/ph€nd1116473 +Chloroanitine91{+7 z-Chloronaphthalenegs{z{ 2-Chlorophenol7005-72-3 +Chlorophenylphenylether210{1-9 chrysene53-7G3 Dl,ber':o (a,h) [email protected] Diben2ofuran9s-5+1 l,2_Dichtorobenzene54r-79r l,3-Dichtorob€nzene106-46-7 1,4_Dichtorob€nzene91€4-1 3,3',-Dicttorobenzidin€12o-en-2 2,4-Dichlorophenolu$62 Dielhyl phlhalate
13r-11-3 Difnethyt phthalate
105-67-9 2,4-Dimethylphenolu.1+2 Di-n-butytphthatate5,34-52-1 4!6-Dinitro-2-methylphenol51?&5 2,+Dinitrcphenoli2l-1+2 2,4-Dinitrototuene(X)&20-2 2,6-Dinitrototuenei17-84{ D-n-oOVlph0ralate2OE-4,1-0 Ftloranuren€8-717 Ftuor€ne11&74-1 H€xechlorcb€nzene87€&3 HoxEchlorcbutadienen471 H€xachlorocydopentadiene67-72-1 H€xachloroethene1s339.5 Ind€no (1,2,3-cd) pyrene
Crlz{ 1-Methytnaphthet€ne74.5&l lsophoaone9r5t6 2-Melhylnaphthalenee+.4&7 2-Methy'phenol
r06-3s4, 3,4-Methylphenol106-1.r-59l-21>3 Naphthalene&f44 2-Nitfoanilineg9{}2 }Nitroaniline
54,300144.00021,100143,000BRLARLARLBRLaR[ARLBRLBRL199,000BRLARLBRLARLBRL44S,0006,38019,300BRLBRLARLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL369,00026,600BRLBRLBRLBRL24,4005,000BRL4,460BRLBRL
BRLBRLBRL
!s/ksLjsftgr.isftg
Lig/Kg
!g/kg
ug/kg
!s/ksU9/kSWst g/Kg
t 9ft9
!sftg
Pg/r(9
trg/kg
fg/(gpg/Kg
pg/xg
pg/Kg
t S/kg
!9ft9
llg/r(gpg/k9
lrgftspg/kg
ug/t(g
ug/r(gusftsus/ts|Jg/xg
!g/K9
trg/Kgpg/kg
!9ft9
!g/kg
!g/kg
!s/kg
ttS/kS
!gr(s!sagp9,4q
ugft9pqr9
udksusftstiS/kS
tiS/kS
Ps/kg
l.rglKg
Ps/ksrslkg
221022102210
22102210221022102210221022102210221022 tO221022tO221022102210221022 tO22 tO221022102210221022102210221022 tO22102210221022102210
2210221022102210221022102210221022102210221022102210
221022102210
SW846 8270C 22-Mar-O7 -Mat-O7 7031282 M.B
Thb laboratorJ repod k zot talid withod an zathoized signature on the cover page.
'Reportable Det€ction Limit BRI, = Below Reporting Limit Page El of 152
Page 439
Ssmpl€ [detrtificationM8FI.2
sA5946+ l5
Client hoiect #301-88
MatrixWood
Collection Dat€/Timel5-Mar-07 00:00
ReceivedIg-Mat4'l
CAS N^ Aazbtz(t) Resah FILC Unis .R.DL Dildion Llethod Retr, Prcpned Ano$zcd Batch Anabst
Se mivolrtik O.g lc CoEpound! by @MS
Semivolatile Oiqanic Comoounds bv SW846 8270C
Preparad by msthod SW846 35508r0o-o1€ 4-Nit'oaniline9F.95.3 Nilrcb€nzene8&7t5 2-Nitrophenol1OGtr2-7 +Nibophenol62_7t9 N-MitrGodimethylamirE6?1{4-7 N-Nitlsodi{-propylamine86-30{ N-Nitrosodiphenylamine87-46-5 Pentadbrophenol85.{ti€ Ph€nanthrene10+95.2 Ph€nol129{0{ h/r€n€r10-06-1 Pyridin€i2G€2-1 1.2,4-Trichlorobenzeie9t95-{ 2,4,$Tdtrlorophenol8S{&2 z,4dTrichtofophenol
Sunogate rwtei$:32ta)-e z-Fhrorobiphenylx7-124 z+fuotophenolll6a,noi Nitrohenzene454t6ar62-2 menol4stl1e514 Terphenyl4l41te7+6 2,4,6Ttbrcmophenot
Sw846 8270C 22-Mat47 2€-Mat47 7031242 M-BBRLBRLARLBRIBRLBRLBRLBRLt51.000BRL30t,000BRLBRLBRLBRL
54374439
51
Complebd
BRL
SRL
0.t05
0.0040
BRL
BRL
0-0r35
BRL
pSAS 6830
lJSl(g 2210
!g/tS 2210
lgftS 8930
$glkg 2210
l€/tg 2210pEkS 2210
!S/tg 2210
fjSftS U1Ogglkg 2210
l€/tg 2210
t€I(g 2210
Ug/kg 2210pSI(S 2210
USftS 2210
3G130 "/61+110%3Gt30 %|Gfi0 %30-130 %1t110 %
1II
1
1I
1'|
1
1
1
I
1
t
Toarl M€.rb by EPA 6m0rl000 Seri.i M€thods
7430-97s Mddlry BRL
Tot l Mctrb by EPA 200 Series Method!
2GMar{7 26{vler-07 703131 1
26-Mar-07 26-Ila.-07 7m12637440-22-4 Sitver
t4(13e2 A6enic
744{1393 B€dum
74rt0.13-9 Cadnrium
7440-47-3 Chrcotium
7€9o2n L€ad
7782-492 Selenium
rrrdkS 0 E67
m9ft9 1.33
ftrdkS 0A44
n\g/kg 0.222
mdkg 0.444
mg/kg 0.665
rn€tkg 1.33
mgil 0.0100
nS,/l 0.0150
m€I 0.0050
ntdl 0-0025
n4/l 0.0050
nEn 0.00040
n'S/ 0.m75
mSn 0-0150
I SW845 7471A
1 EPA2m.7
1 "
1 '
msag 0-0300
SRL
BRL
5.08
BRL
8,40
BRL
TCLP Metrb by EPA l3ll & 6m(y?000 Sed€! Merbods
TCLP Exlraclion
7{4G22-4 Slh,,er
7440-3&2 AEenic
7a40!393 Barium
74404!9 Cadmium
7,t40-47-3 Olmmiun
7(}$97{ ireacury743W2-1 Lead
?02-4+2 S€l€nium
1 SW8461311 21:M?'-o7 21-Mar4f 7OXln1 BD
I SW846 t311l60f 0S 234€f47 21.+d6t47 761325 HB
1 '
I '
1 '
I Sw8461311174704 ' 2+Mar-07 70Si326 YP
I SW€,f6 1311160 f08 ' 21J.,d47 7031325 HB
LR
fhis tabarctoq repoa b aot salr! witbsr ad c'rlha;azd sigt true ot thc cave ptg..
' R@orhblc Detectiol| Limir BRL - B.low R€porting Limit Page 82 of 152
Page 440
APPENDIX FGroundwater SampleLaboratory Reports
Page 442
Sarnple IdentificationMEF.l,t cwsA595l7-13
Client Proicct #30 t -88
MarixGround Water
Collection Date/Tim€t9-Mar-07 00r00
Reccived20-Mar-07
CAS No. At alXte(s) Flag Ania 'RDL Ditatiott Method ReI Prepated Analyzed Bt ch ,Anal]'sl
VoLtil€ Org{tic Compounds
Volatile Orqanic Compounds bv SW046 82608Prepared by method SW846 5O3O Water MS
7&1!1 1,1,2-Trichlorotrifluoroelhane(FreoBRL67$rL1 Acetone BRL10713-1 Acrylonihile BRLZt4?2 Benzene BRLl0&8G1 Eromobenzene BRL74-97-5 Bromochloromethane BRL75-214 Bromodachlo{omelhane BRL75-242 Brcmoform BRL74{3€ Brcmomethane BRL78€13 2-Butanone (l\rEK) BRL10a,514 n-Butylbenzene BRL13F98+ sec-Butylbenzene BRL9&0s tert-Butylbenzene BRL7!1$0 Carbon disulfde BRL56-2$5 Carbon teirachloride BRL10&90.7 Chlorcbenzene gRL
75{0.3 Chlsro6lhane BRL67-643 Chtoroform gRL
f,147.3 Chtoromethane BRL96-4S8 2.Chtorototuene BRL106-434 4-Chloroto{uen€ BRL9Gl2-0 1,2-Dibomo-3-ciloropropane BRLi2rt48-1 Dibromodllorcmebane BRL10G93-4 |,2-Dibromoef|ane (EDB) BRL74-9s3 Dibromomethane BRL955G1 I,2-Dichlorobenzene BRL54t.73.1 I,3-Dichloobenzene BRL1061|{}.7 l,4-Dichloobenzene BRL71714 Dichlorodifluoromethane (Freonl2)BRL7t343 l,t,Dichtoroethane BRL107.06'2 't,2,Dichtofoethane aRL7535i1 1.l-Dichtoroethene BRL15Gs9-2 cjs.l,2-Dichloroethene BRL15G@s trans-1,2-Dichtoroeihene SRL78-87-5 1,2-Dichloropropane BRL142-2€-9 l,3.Dichloropropane BRL59+20-7 2,2,Dichtoropfopane BRL56+5€{ l,l.Dichlorcpropene BRL1006r{1-5 cis-1,3-Dichlorcpropene BRL10061{2-6trans-1.3-Dicitoropropene BRL100-41-4 Eth),jbenzal6 BRLE/6&3 Hexachlorobut€diene BRL591-78-€ 2-Hexanone (MBK) BRL90-82{ lsopropylbenzene BRLs{7{ +lsopropyltoluene BRL163tog Methyl teft-butyl ehsr BRL10sr0-t 4-Methy'-2tentanon€(M|BK) BRL75{92 Methytene chloride BRL91.2G3 N€Dhthatene BRL1036$1 rFFropylb€nzene BRL
!g/l
psrpsnus4lig/l
tjs4uglplyl
uEl!Er
wl!gntrg/l!gl
psnpsnpgrpsn
!srfg l
pgtl
lJ9/l
Lrgl
!El
ps4
us/lps/lpg/l
wnpgn
vgltis/lvgtl!s/ps/l
l.,silWnuElus4ItEl
ldlpdl
pdl
psrpdlpsrpdlpsn
!c4!94
1 .020.o0_51.O1.0't .o
0.51 .02.O1 0 0
1 .01 01 05.01 .01_O2.O1 02.O1 .01 .0
2.O0.50.5't .0
r 0r 0
l 02 01 .01 .01,01 .01 01 .01 .0'1.0'1.0
0.50.51 00 510.0' 1 0
1.01 010.05.0't.0
1.0
1
1
l
1
1
1
1
1
1
1
1
1
1
1
l
l
1
I
1
1
1
1
1
1
1'I
I
I'|
1
1
1
I
I
I
I
I
1
I
I
'|
I
1
1
1
1
1
1
1
SW846 82608 22-Mat47 22-Mafi7 7031296 ek
This la.toralot! repo.l is nat uotid withou att aun odzett ignaturc on tlE cover p.tge
a Reportabl€ D€tection Limit BRL: Belotr Reporting Limit PaEe 62 of 124
Page 444
Samplc ldentificatiotrM8F-14 cwsA59517-13
Client Proiect #301-88
Mal xCround Wat€r
Collection Date/Timelg-Mar 07 00r00
Received20 Mar-07
CAS No. Atuttu(s) Fl"E *RDL Dilatbn .\Iethod ReI. PMparcd Anahaed Batch Anzlpl
Vobtilc Orgrnic Compounds
Voiatile &oanic Comoounds bv SW846 82608
Pr€parcd by method SW846 5030 Water MS
10rl-12-5 Styrene BRL63oe2l)-6 1.1,1,2-Tetrachloroethane BRL79{r4.s 1,j,2,2-Tetl.achloroethane BRL127-18r Tet?chloro€thene 8RL1lr8-88.3 Toluene BRL€7-61{ .1,2,3-Trichlorob€nzene BRL12l)€2-r l,2,4,Tdchtorobenzene BRL
7t{5€ 1,1,1_Tdchtd.oefhane SRL
7945 | ,1 .2-f tichlfoethane gRL
79{1{ T.ichloroeth€ne BRL
75.€9-4 T.ichlomfluorcmethane (Freon 1.t) BRL
96-1&4 l,2,lTrichtoroprcpane BRL95€96 1,2,+Trimethylbenzen€ BRL111847{ 1,3,5-Tfimethylbenz€n€ BRL75.o1-'r Vinylchloride1330'zl-7 m,p-Xylene95'474 o-Xylen€10+9$9 Tetrahydrofuranfl-2*7 Ethylether99+05{ Te -amyi methyl etier637-S?'3 Ethyttert-butytether10&zl1.3 D-isopropylelher754s Tert-Bulanol/ butyt alcohol12191.1 1,4-Diorane
S!fiogate rccovedes:4EYn4 4-Etomofluotobenzenem37.26-s Toluene4S17060a7 -o 1, 2-Dbhloroetha ne-d 4
BRLBRLBRLBRLBRLBRLBRLBRLBRLSRL
100101931001A6A-53-7
us4 1.0pS4 1.0
pg/l 0.5
ldr 1.0
ldr 1.0
!9/ l 1.0
!g/ l 1.0
fd l 1.0
pdt 1.o
!S/l 1.0
Ug/ l 1.0
pSl l 1.0
fdr 1.0
US/ l r .0
Lig/l L0
frdl 2 O
tJSll 1-0
pS/l 10-0
USfl 1.0
IiSll 1.0
LiS/l 1.0
Lig/l 1.0
!S/ l 100
rdt 20.0
70-t n Yo70-130 %70-t 30 %70-1m %
mg/l 0.1
lng/l 0.1
mg/l 0-1
mg/l 0 1
mg/l 0.1
mgn 0.1
mg/l 0.'!
mg/l 0.1
nW1 01
mg/l 0.1
4rr140 %
Fgr'| 0.0121
Fdr 0.0121
SW846 82608 22-Marol 22-Mal-07 7031296 ek
Ertrctable Petroleum Hydro.arbons
Extractable Total Petroleum HvdrocarbonsPrepared by method SW846 3510C
000+61-9 Gasoline6BrG3o-2 Firel Oil #26047+31-3 Flel Oil tl46055100-{ FiJel Oil tl6lr0g0o000o Motor oilJ0Ol00m0 Aviation Fuel
Unidentilied
Other OilTotal Peholeum HlrCrcca.bonsCgC36 Aliphatic l-lydrocarbons
Sunogale recoverbsi3,efr'a3-z l-ChhtoocladecEne
ScDivolrtlle Orgrric Compounds by GCOroanochh'.ioe Pesticides SW846 80814Pr€pared by merhod SW846 3510C
3O€{G2 Aldrin31+8+€ a-BHC
BRLBRLBRLBRLBRLBRL
BRLBRLBRLBRL
93
BRLBRL
+CTETPH 21-Mat47 22-Mat47 7031160 DS
SW846 8081A 22-Mar47 224'iaro7 7O3127O 7c
Thit lata.tury rcpod is ,tot eclid n ithot on a,tthoriz"l ig.tztxre o.t the cover pzge.
r R€portrble Detedion Limit BRL = Below Reporring Limit Page 6l of 124
Page 445
Sarole ldeotificationM8F-l4 cWsA595t?-ll
Client P.oiect #30t-88
MatrixCroutrd Wat€.
Coll€ctiotr Date/Timet9-Mar{7 00:@
Received20-M8't-01
CAs No. AtuUuG) Fl4C 'RDL D ula,, Merhod ReJ Preryed Aaalwd Botch *talyst
Semivo|'lilc Orgrdc Compoutrds by cC
Oroanochlorine Pesticides SW846 8081APrepar€d by rnetEd SW846 3510C3i9S7 b-Bl{C319€C8 d-BHC5€{+e g-BHC (Lindane)57'74'9 Chbrdane72444 4,4-ODO (p,p)72-5+s 4,4-DDE (p,p')$-2g3 4,4-DDI(p,p')60-57-1 Dleldrin95998+ Endosullan I33213{5+ Endosultan l11031.0ru Eldosutfan sulfate72-mi Endinz2l€3-4 EndrlnAldehyde76-44{ Hoptachlor72415 M€thoxycilor1024-57-3 Heptachlor Epoxid€dx)r,392 Toxaphene51U:r-7r-9 a-Chlodan€5566-34-7 g_Cftbrdane5349+706 Endrin K€tone
Surogate Gcoveries:t t|3t'68a2 4,H)&Octduorobiptlenyj (54N51-2+3 Decachforobiphenyl(Sr)Polvcfilorinated Bioheflvis W SW846 8082Proparcd by merhod SW846 3510C1?674.11-2 Pcg 1016111o+tu2 Pcig l22l11i41-i€-s PCg 1232F,3168.214 PCg 12421m72-?9s PCB 12481r097€9r PCB 12541r09c826 PC8 126037324-2&5 PC8 tt62r1r0G14-1 PCB .t268
S{fiogrs[€ lgcov€rt€si1 0386-8+2 4,4o&Octaf, uorowony' (54e51-21-3 Dec5d otobipl7d.nf, (Si
SehivoLdle Oqrric Co|trDotrtrd, by CCMS
22-l.,€,r47 22-Mat47 ]a1270 rG8RLBRL8RLBRLBRLBRLgRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRI-BRLERLBRL
107
BRLBRLBRIBRLBRLBRLBRLBRLBRL
60100
0.0r210.0't21o.01210.0606o.o1?10.0121o.0121o.00240.01210,0121
0.01210.0121o_01210.01210.0121o.o1210.{m060.0121o.01210.0121
r.'dlItsAps/|
!dl$sllpdl
rglp{
!dlgsfl
pdl
wpdl
uglggnpclpcr
flgl
us/|u€n
30-1fr %3+1fi%
Sw8,l6 80alA
sw846 8082
1
1
1
1
1
1
1
t
1
l
1
1
1
I
1
1
I
I
1
!snjJgl
trdlrgltlsilps/|pdl
t d lI'94
Fdl
tsr|tdlIrgrygl
t d lIrdlt d ludl
30-150 %3O-1fr%
[email protected]
r.000.4o01.00t.m|.001.00't.00
1.000:m
22]ln 47 23 4a(07 70/J1271
Se.nivolatile Oroanic Cdnpoonds bv SW846 OAZoCftepared by method S1w846 ?,510CA3i2-9 Acansphtbene2O&9+€ Aaer6phltryleneeo-12{ t-Meth/naphthalene62{33 Andine12D12.7 AnUrA€etre1912+4-9 AtEdfl€10133-3 Azobenzefl€/Diph€rryldieztuEm47-5 Beozidine56-553 B€nzo (a) aothrac€ne
z-MEt4l 224,.147 7031272 M.BSRLBRLBRLARLBRLBRL
BRLBRLBRL
sw846 8270C
ftb lab.@ry Epo.l b ,et valld withod o oa&arizd stgnattE oa t e cowr We_I R€ptrtable hection LiEit BRL = Below R€porting Linit Page 64 of 124
Page 446
Samole IdentificationllISF-14 cwsA59-517-ll
Client Proiect #30r -88
MatrixCround Water
Collection Date/Tim€l9-Mar-0? 00:00
Received?0-Mar-07
CAS N^ Aftaute(s) Fhs |RDL Dilution Method Retr. Prepared Analyzzd Ba.ch A tllstS€mivolafile Orgroic Compornds by GCMS
Semivolatile O.oanic Comoounds bv SWe46 8270CPrepared by method SW846 3510C
5OJ2{ Benzo (a) pyrene20+99-2 Eenzo (b) fluoranthene191-24-2 Benzo (g.h,i) perytenea7@ Benzo(k)fllorenthene65{5{ Benzoic acid100!51{ Benzylalmhol11i'9il Bis(2-dlloroethoxy)rnetharte11taa Bis(2-chloroethyl)et er3963&u-9 Bis(2-chloroisopropyt)etherr17{1-7 Bis(2€dlylhexyl)phthalareto1-55-3 +Bromophonyt pheny' ef|er85-6&7 BuVbenzytphthatate86.74-A C€rbazole59-50.7 4-Chtoro-3-rhethylph€nol1rl&47{ 4_Chtoroanilines1.5&7 2-Chtoronaphthalene9s-s7-€ 2_Chlorophenol700972'3 +Chlorophenyl phenyl ether218{1-9 Chrys€net3-70+ oibenzo (a,h) anthracenet32€4-9 Dibenzofuran95-5Gl 1,z-Dichlorobenzene54t73-1 1,3-Oachlorob€nz€ne106-a+7 1,4-Dicthlorob€rizene91€41 3,3'-Dichlorobenzidine12G&3.2 2,4-Dichlorophenola4€e2 oiethyiphthatate131.11-3 Dameth!4phhalate10s7-9 2,4-Dimethytphenolw-74-2 oi-n-butylphthatate53Fs2-i 4,GDinrto-z-methyjphenol51-4s 2,4.Dinfophenolr2'r-14-2 2,4-Dinatototuene60€-2G2 2,GDinitrololuene117{4-0 Di-n{ctylphtialate2014{ FluorantheneE+717 Ffuor€n€11&7+1 HexaclrlorobenzeneE7€&3 Hexachlorobutadienen474 Hexachlorocfctopentadiene67-f2-1 Hexachloro€thene19139-5 Indeno (1,2,3-cd) Py.ene78-59--1 lsophoaone91€7{ 2-Methylnaphthat€ne9s-4{-7 2-ilethytphenol
10839"{, 3,4-Meth}lphenol106-{4{91-20-3 Mphth€lene@-714 Z-Nitroaniline9S{$2 }Nitroaniline1OrL0r4 +Nilroaniline
BRLBRL8RLBRLBRLBRLBRLBRLBRL
8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLgRL
BRLBRLBRLBRL8RLBRLBRL8RLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRL
BRLBRLSRL
ttgl 0 200
!9r 0.200
US/l 1.(10
!S/l 0.300
pdl 1.00
lSn 1.00
pdl 1.00
pg/l 1.00
Ug/l I 00
ug/l 1.00
pg/l 1.00
!g/ l 1.00
ld l 100
lSn 1.00
lid! 1.0O
ldl 1.00
!g/r 1.00
pgt 1.(m
lgn 100
IS/l 0-200
W.il L00
ldl 1.00
[gl 1-00
pSn 1.00
LISI 1.00
liSI 1.00
!g/l 1.00
p d r 1 0 0
!S/l 1.00
tiS/l 1.00
rc/l 1.00
pg/ l 100
pS/l 1.00
ld l 1-00
pS[ 1.00
ld l 1.00
Ugl 1.00
ps/| 1.00
pSI 0.600
!9n 1-00
!9,f1 1.0O
!S/l 0.200
|JS{ ton
Ug/l 1.0O
lgn 1.00
tgn 10.0
Ugll 1.00
Itgtt LoO
t g l ' l . to
pdl 1.00
1
1
1
1
1
1
I
1
1
1
1
1
1
1
1
1
1
1
1
1
I
1
I
I
1
1
1
1,1
,1
1'|I
1
I
I
1
1
1
1
1
1
I
1
1
1
1
1'|
This labofalory rcpod k nol wlid tlithod an atdro.taed signaturc on tha cover page .
' Reporlable Detection Limit BRL = Below ReDorrine Limit Page 65 of 124
Page 447
Sample IdetrtificationM8F-14 GWsA595l7-13
Client Proiect #301-88
MatrixGrotrod Water
Cotleotioo Date/Timel9-Mar47 00:fi)
Reo€ived20-Mar47
CAS No- AEzly.a(s) Ft"s *nDL Diluioa Method Retr. Prcpared Anzlwd Botrh Aaalpz
Semilolrdle Orgrnic Compoutrds by GCMSSemivdalile Orqanic Comoounds bv SW846 B27OCPrepa.ed by method SW846 3510Cs&9s-3 Nitrobenzene8a-7t5 2-Nibophenol100-02-7 +Nitophenol62-7s9 N-Nitrosodirnethyamine621-€4-7 t+Nitr6odin-propylamine€6-30{ N-Mtrloodiph€nytsmine87€6-5 Pentachloroph€nol8541{ Phenanthren€loerSs-2 Plienol129-110{ Pyrene110{6-1 Pyrltine1&u-1 1,2,+Trichlorgbenzene9545-4 2,4,tTddorcphcnol8a+2 23,6-Tddtloophonol
Suftogale ,Bcovotles:321a0a 2+tuorobhhqf367-124 z+luuophenol11C,a,e4 Nit ofuftene4jar65-62.2 Flt€noks1718-514 lerphenyl4!411e-m-6 2,4,6TthronophendSVOCS bv SW846 8270C SIMPreparod by method SW846 3510C8c32-9 Acsmphfi€n€
2084e8 Acenaphthylen€9G12{ l-l\t€thytnsphthalene120n2'7 Anthiaceness55-3 BerEo (a) anthracene5G32,a B€nzo (a) pyfone20+99.2 Beruo (b) f uora{l€ne1e1.24-2 gerEo (g,h,i) perytene207fi-9 B€nzo (k) nuoi-anttEn€21S-01{ Ckys€nes3.7G3 Dib€auo (a,h) anlhaaoene20fF44-o Fludanthene&717 F|uorene193.3s-5 hdeno (1.2,3-cd) pyrenee1-s7{ 2-Melhylnaphihatene91-a!3 Naphthaldne85{1{ Phefianthrene129{0{ PyrorE
Surmgsfu rEcowatasl32tes 2+hlotobiphanyl17t8-5tQ Terphenyl44
Tord Metsls by EPA 6m0/r000 S€der Method!
BRL
BRLBRLBRL
BRI-BRLBRLBRLBRLBRLBRLBRLBRLBRL
70
8060u
BRL
BRLBRLBRL0.425BRLo.7620.7380.6500.500ARL0.9t2BRL0,600BRLARL0-3500.850
BRL
0_(X)70
0.0096
Wl l.oo
USi t.oopdl 1.00pgn 1-00
t 94 1-00pSI 1.00pCI 1.00
Fdl t.00
ugt 1_00
FCI 1.00
FSd 1.00
FS/l ',1.00
Vdt 1.0o
tdl 1-oo
30-130 %1+110%3tr1f i%tun, %30-130.t1&1 tO %
USn 0.050
ldl o.o5o
Fdr 0.050
uil 0.050
Wt o.o5o
F94 0.050
Psil o.o5ogn 0.050
tgll 0-050pSi O.O5O
ttgJt 0.050pgt 0.050
ldl 0.050
ldl 0.050pgn O-05O
lsn o.o5opdr 0.050
30-130 %30-130 %
fltSrl 0.0050
"lq,l' 0.m40
n'Sn 0.0050
SW8468270C 22-ttat47 ?I2-*lat47 rOXl272 M.g
1lgil zflr,lar-07
1
1'|t
t
1
1
I
1
I
l
1
I'|
1
1
7lt ().22-4 Sitver
Z4{}382 Arcenic
7140393 Badum
I
1
1
SW846 60108 264af4f 2auat47 t13t413 LR
Thit bbordory .eprr is tnt ealil Nithou afi outLoriz.d sagrrotu. or. th. coyer page .'R€podable Det€ction LiEil BRL = Bclow Reporting Limia Page ffi ot 124
Page 448
Sample ldenrificatiorM8F-r4 cwsA595 t7- l3
Client Proiect #l 0 l - 88
MatrixGround Water
Colledion Datc/Timel9-Mar47 00:00
Received20-Mar-07
CAS No. Aaab@k) Resdl Flag Unla "RDL D anon I4ethod ReJ Prepued Awlyed Batch Analrst
Totrl M€tits by EPA 6000/?000 Series Methods
74.4u-43-9 Cadmium
7ll40{7-3 Chromium
7439'92-! Lead
282-4$2 Selenium
Totd Merrls by EPA 200 seri€s Methods
7a3+976 MErcury
2&Mat-07 26-Mat47 7031413 LR
26-Mar{7 27-t!,laF07 7031414 YP
0.0048
15.7
BRL
BRL
0.00026
mgn
nEI
mgn
mdl
mgn
0.0025
0.0050
0.0075
0.0150
0.m020
sw846 60108
EP4,245.1t7 4704
This ttborarory Eport h dat volid wilttot/l an aUhodaeil signarure od thz cover prge-
r Reponable Detection Limit BRL = Below Reportine Limit PaZe 67 of 124
Page 450
Samplc IdentificationM$F-24 GWsA5964l- 17
Client Project #301 -88
MatrixCround Water
Collection Date/Time?l -Mar-07 00:00
Received2?-Mar-0'l
C"'tS Na An yt(s) Result Flag Unia 'RDL Diluttun Method Rel. Prepare.d Analyted Batch Adallsl
Volrdle Otglnic Compounds
Volatile Orqanic Comoounds bv SW846 82608
Prepa,ed by m€thod SW846 5030 Water MS
76-i11 1,1,2-Tdchtorotdfuoroethane(FreoERL
67{+1 Acetone BRL
107-13-1 Ao.ylonitrilo BRL
7143.2 B€nzene BRL
10&8S1 Bromobenzene BRL
7+97.5 Brornochtorcmethane BRL
7s-274 Brormdichtoromelhane BRL
l+2+2 Bromoform BRL7,t{}9 BrooEmethane ARL
78-913 2-Butianone (MEK) BRf
104-5r{ n-Bulylbenzene ERL
135-9€€ sec-gutylbenzen€ BRL
9€{)6-6 tert,Butylbenzene BRL
TaFi+o carbon disutfide BRL
&2X5 Carbon tefachloride BRL10&90.r chtofobenzene BRL7540-3 Chloroethane BRL6746-3 Chloroform BRL744r-3 Chtoromethane BRL9s"49-8 2-Chlorototuene BRL
1OH3-4 +Chtomtolu€ne BRL
96-12{,1,2-Oibromo.3_chlorcpropane BRL
124-€-1 Dibrcmochlorom€hene BRL
10c93-{ 1,2-Oibromoethane (EDB) BRL
74€t3 Dibromomethane ARL
95.5}1 1,2-Oichlorobenzene 8RL
541-731 1,3-Dichlorobenzene BRL
10ffi.7 1,+Dichlofobenzene BRL
75-714 Dichlorodiffuoromehane(Freon12)BRL75-343 l.l-Dichlorcethane BRL1074G? l,2-Dichloro€thane BRL793tt l,l_Dichtorceth€rne BRL
1a)sss.2 cjs-1,2-Dichloroethene BRL
15G60.5 tans-1,2-Dichloro€lhene BRL
78{7-5 l,2-Dichloropropane BRL
142-28.9 i,3-Dichlompropane BRL
594-2C7 2,2-oichlorcpropane ARL
56+58{ l,j-oichloroprop€ne BRL
1006i{1-5 cis- l,3oichloroprcp€ne BRL
10061-02{trans-1,3-Dichloropropene BRL
10{F414 Ehylbenzene BRL
876&3 tl,exachlorobutadiene BRL
$1-7&6 2-Hexanone (MBK) BRL
98{2{ lsopropylbenzsne ARL
99{7{ +lsopropyltoluen€ BRL
1634+1-4 Methyl tert-butytether BRL
10+10-1 +Methyt-2-pentanone(MtBK) BRL
75{92 i etfrylene chloride ARL
BRL8RL
|lglpgl
vgtl
ug,ItEl
trdl
lrEl
rEl!9rpql
pgl
r./!yl
!s/l
v9p9ntrglpg/l
ttstl
usn!g/l
ugrus,4usnpsn
us4psn
!91
!s/1
!sl
!91
!gnpq/l
pgn
Lis/l
!jsnpgl
Ljgl
!s/l
us/lt /g l
Ljgl
!sruglugl!sn!s{utyl!gltr9lLtEl
1 .0
20.o0.51.01 .01 .0
0.51 .02.Q.t 0_0t_01_01 .05.01.01.02.O1 02.O1 .0't .0
2.O0.50.51 .01 .01 .01 .02.O1 .0t . ot . 01_01 .0t . 0' t .0
1_01 .00.50.51_0
0.510.01 .01.01 .010.05.01 01 .0
SW846 82608 27-Mat47 27^1,3'47 7031617 RLJ
9r-2G3 Naphthalene10!65-1 n+ropylbenzene
This labo4tnry repod is na, volU withost M aathodzed sigalarc ofi tha covcr page .
' Reportable Detection l-imit BRL = B€low ReportinC Limit Page 85 of 165
Page 451
Sahple IdentificationMtF-24 GWsAs964l - l7
Ciiedt Proiect #301-88
MatrixGround Water
Collectioo Date/Time2l-Mar-07 00:00
Received22-MarO7
CAS No. Anabu(s) ncs/,L FI"C 'RDL Dih tion Llethid netr, Prcponl Aaalyzd Bdch Anal8
Voladl€ OrgAnic CoorpoundJ
Voiatile Orqanic Comoounds bv SW846 82608Prepared by metiod SW846 5030 Water MS
BRLBRLBRLBRLBRLBRLBRL8RLBRLBRL
15€9,4 Trictiorolluoromethane {Freon tl) BRL
10l}'ll2-S StyBne63c20{ 1.1.1,2-Tetrachloroethane79.3tr-5 | , 1 ,2,2-Tetrachloroethane127-1€-4 TetrachlofO'€thene108{a-3 Toluenee7{r{ 1,2.3-fiichlorobenzenerZG€2-1 1.2,4-Trichlorobenzen€71-sfi 1,|,1-Tdchtom€rhane79{0-5 1,I,2-Tddlloro€hane79-01{ Triahloroethen€
t,(yl
uslygl
psnttgl
usnusrudl!dl
rcn|l9/l
9gl
ps4
rcnustpdl
!c4!gltglttgll
tdl$npsnpdl
t . 0t.00_5't.0
1.01.0'1.0
1 .0t . 0t . 0
1 .01 .0
1_0'1.0
1.02.01.010_0t_01.01.01 .010.0
20.o
0.0' 4oo l r4
1
1
1
1
I
I
I
t,l
1
1
1
1
I
I
I
I
1
I
1
I
1
I
I
9O-1e-4 1,2,3-Tddtloropropane95-63{ |,2,4Taim€thytbenzene10€-67{ l,3,tTaimethytb€nzene75{r-4 vinytchhride1330-20.7 m,pxylen€964?6 o-Xylene10s99€ Tsfahydrofuran60-2+7 Ethyl einer994{5+ Tert-amyt nreth}'l ehea637-92-3 Ethyt tert-butyl ether10&20'3 O--isoprop/ etf|€r756!0 Tert-Butanol/ bu!y' alcDhol13-91n 1,4-Dio(ane
Srrtrtugate ftcoveties:1160-004 +Bmnoauorobenzenefi37-26-S fdueneiS1 70at0-o74 t, 2-Dbl lotuethane44186&59? DibrorDofuororne{hane
Exlrrctsble PeFoleoh llydrocadors
Extractable Total Pet oleum HvdrocarbonsPrepaed by rnothod SW846 3510C€006-6t-g Gasolin€6€47+30-2 Fuel Oil #26E47+31-3 Fuel Oil tt468553{0-4 Fuel Oil #6m980m00 Motor Oil,()0100000 Aviation Fuel
unidenlifiedOtlEr OilTotal P€foleum Hydro€rbonsC€{36 Aliphatic Hydrocarbons
Sunogata rccovedas:31863x2 l-Chlomocladecat:€
SemivobalL Oryatric Compourds by cC
O.oaoochlorlne Pesticides SW846 8081APrepar€d by mehod SW846 3510C
[email protected] Aldrin319€46 a-BHC
+CT ETPH 26-Mar-07 20{lar{7 7031505 DS
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
94102106105
BRLBRLBRLBRL
SRL8RL1.0Calculated as1 .0
1 .0
BRLBRL
|llgil 0.1
ftqA 0.1
mSn 0.1
ordl 0_1
mg/l 0.1
mgl 0,1
mgr'I 0.1
mgl 0.1
mSn 0.1
msr 0.1
40-140 %
|'|gn|ls4
7O-tW%70,1fr %TGtn %7G130 %
SW846 80814 26l,,,d47 26-Met47 7031497 TG
Thit labonlory reporlls Fol rsu w hoA aa ouhod.ry' sisttz!,tE oE lhe cow. pagc.
' Reporbblc Ddecrion Linir BRL = Belos, Repodng Limit PagE 86 of 165
Page 452
Sampl€ ldentificationM8F-24 GwsA59641- 17
Client Proiect #l0l-88
MatrixG.ound Wafef
Collection Date/Time2l-MaF07 00:n
Received22-lr(ar-I7
CAS Na. A,'alru(s) Resuh Floq Ania *RDL Dilution Prcpored AntlFed Batch AnalystSemivolrdle Orgahic Compornds by cC
Omanochlorine Pesticides SW846 8O8lAPrepa.ed by method SW846 3510C
319{5-7 bts8Ho319r6J d.BHcs€{ss 0-BHC (Lindane)
5f-7+9 Chlordane72-s44 4,4'.ODD (p,p.)72{+s 4,4.-DDE (p,p.)5o-2s3 4,41DDT (p,p')60{7-1 DieldrinS5998{ Endosutfun I33213-65-9 Endosutfan fi1031{7.8 Endosu|lanSulfatef2-?ca Endrin7421+$.4 EndrinAldehyde76-44-€ Heptachlor124+5 Methoxyd.tlor10245r-3 Heptachto. Epoxid€[email protected] $2 Toxaphene
5103.71.9 a-chlodane55€€.34-7 g_Chlordane
s3494-7$5 Endrin Ketone
Suarogate recor€r-es:
10386842 4lD$Ocbnuorcbiphenyt (Si2o51-2a3 DecAchlotobiphenyl (Sr)
Polvchlorinated Biphenvls bv SW84ti 8082Propared by method SW846 351 OC
1267+11-2 PCB 10161110+28-2 PCB 12211114r-rc5 PCB 12325346s21,e PcB 124212672-84 PCB 12491r09749.i PCB 125411006-826 PCB 12603741-ZI5 PCB 126j211100.144 PCB 1268
Sr.rnogale a€covereslto38&8+2 4,+Dgoctaftuoroblphenyt (Sr)
mst.2L3 Decachtotohiphenyt l$r)
Semlvolaiile Orgrnic Compound6 by CCMS
8RLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLSRLBRLBRL
5699
BRLBRLBRLARLSRLBRLSRLBRLARL
6090
BRLBRLBRLBRLBRLBRLBRLBRLBRL
!s/lpgn
ug/lp!yl
ll91psyl
!gn!gnusnusnu9ntrs,'lLig/lLj9lp9I
tr(yl
us/tpg/l
pg/l
lig/l
30-150 %30-150 %
3G150 %
30-150 %
0 0 1 1 4 1
0-0114 1
0.0114 1
0.0571 1
0-0114 1
0.0114 1
0_0114 I
0.0023 |
0 0 1 1 4 I
0.0114 1
0_0114 1
0.0114 I
0.0114 1
0.0114 1
o.o114 1
0.0114 1
0.0571 1
0.0114 I
0 . 0 1 1 4 1
0 . 0 1 1 4 1
oo229 1o.o229 I0.0229 10-0229 100229 10.0225 10.022s 10.022s 1o.o229 1
't.00 10.400 11.00 11.00 11.00 11.00 11.00 11.00 1
0.200 1
SW8468081A 26-tlar{7 26,Mar{7 7031497 TG
Sw846 8082 26-MaF07 26-Mar-07 7031496 SM!g/l
!s4pg.4
plyl
pg/l
pgrl
pg/l
Lj{yl
ugal
Semivolalile Oroanic Comoounds bv SWg46 8270CPrepared by method SW846 3510C
63-32.9 Acenaphthene2oe96€ Acenaphthylene
cF12{ l-irethytnaphthalene
@-533 Anilinel2O-12-7 AntliEcene1912-2+9 Alrazine103333 Azobenzene/Diphenyldiazines2{7.s Benzidine56-5+ii Benzo(6)enthracene
rc4u9n!94pglpg4
ug/ltrsflpEtpgn
SW846 8270C 2f,-Mat47 29.ir'tat47 7031499 M.B
Thb labotuloq rcpod is ,rna vrlid wiatour aa tshorlzed slgnttttrc ott the are? page.
' Reportable D€t€ction Limit BRL = Betow Reponing Limit Page 87 of 165
Page 453
Sample IdefltifrcationM8F-24 cWsA5964l - 17
Cliedt Proiect #301-8E
MatrixCrouDd Watea
Callectioo Date/Time2 I -Mar-07 00:00
Received22-Mar47
CAS No. Aaalylz(s) Fhs *RDL Dilation lnefiod Rel. Prcparcd Analyzed Borch Analyst
Semlvolrtll€ Orgrnlc Compourdr by CCMS
Semavolatile Oroanic Comoounds bv SW846 8270CPrepar€d by method SW846 3510C5{}s2{ A€nzo (a)pyren€m5s2 Benzo (b) fluorenthene1ei-24-2 B€rEo (g,h,D p€rytenea)7-08-9 genzo (k) fuoran{hene65-85,0 Benzoic acid10Gs1€ Benzy{ alcoholi1r41n EIs(2-ohlorcethoxy)methane11laaa Bis(2-d{o.oehyl)€trer3S63e324 Bis(2dtloroisopmpyl)ether11731-7 Bis(2-ehylheryl)ph&atate101'55-3 +Bornophenylphenylether956€-7 BuV b€|1ryl phthalat€86-7,1{ Carbezole59-5+7 4chlom_$rnethylph€nol10H7+ 4chtorcanitine91'5&7 2-Chloronaphthalene0557-8 2-Chlorophenol7005-72-3 +chloophenyt phenyl ethef218-01-9 Chrys€neS3-70-3 Dibenzo (a,h) anthracone13?{,r-9 Oib€nzofuran95-5G1 l,z-Dichtorobenzene541-73-1 1,3-Oichtofobenzen€106-4{i-7 1,.1-Dh.htorobenzens9r-9+1 3,3loichtorobenzijine120-83-2 2,4-Didilorophenolu&2 Di€thyi phth2late131-11n Dim€fltphthatate10s-67-e 2,+Dimethytph€nolu-7+2 O-n{ut)y'phthalato$4-52n 4,6-Dlnitrc-2-methytph€nots1-2+5 z,4oinitrophenol121n4-2 2,+Dinitotoluene60e20-2 2,6-Dinibotoluener | 744.0 Di-n-odyl phthatate206-44-{' Fluoranthene86-73-7 Fluofene11&7+1 Hexacfllorobenzene€7-6E-3 l-bxadtlorobltadiene17471 HexachloocyclopentiadieneA7-72-1 Hexachtoroethane1ess5 Indeno (t,2,3d) pyfen€78.69-t lsophorone9l{7{ 2-Methylnaphthal€ne95-48-7 2-Mehy'phonol10e.39.4. 3,+Methy,bhenol106-{4691-2G3 Naphth6tene&f 44 2-Nitroanitine9!rc92 3-NitrDanitineroo-ih€ +Nikoanl n€
SW8468270C 26-Mar.07 2+Mar-07 7081499 M-BBRLBRLBRL
BRLBRLARLBRLBRL8RLBRLBRL8RfBRLBRLBRL8RL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLERLARLBRLBRL
BRLBRLBRLBRL
vgllsnp{n
us4!srt/grt'dlt g/l
!st!dlt /g l
psn!snpdt
!dlugnpdl!sitpcn
!dlrglpdl
psil
pdl
!dl
uEl
1lql
trlyl
uc4!dl
!tyl
!dl
wlp{rnu4lugluglls/lpc4
udluglgr
ps4
us4udlwn
1lgl
t,gll
Fdl
PSA
0.2000:001.00
0.3001.O01.001 .m1.00
1.00'1.00
1.001.(f01.00
1.001.001.001.001_001_00
0.2m1.(X)
1.00r.001.001.00r.001.001.001.001.001.001.00r_001.001.001.00|.001.00
0.600'1,00
1.0002001.001.001.OO10.0
|.00't.ff)
1.001.00
':hls lefurorarf plfi it not valld toithost an au[tori?A tigttant e on tha caee? pg.
' Repodrble Det€ction Limit BRL = Below R€portinS Linit Pagc 8E of 155
Page 454
Sample ldentificationMEF.24 GWs4596,{ I - I7
Cliert Proiecr #301 -88
MatrixCround Water
Collcction Date/Time2l-Mar 07 00:00
Received22-Mar01
CAS No. Anolye(r) Resan Fhc "RDL Dilutian Mahod Retr, Preparcd Anabzed B ch Analpt
S€mtvolrtil€ Orgsntc Compoun& b!, CCMS
Sernivolatile Orqanic Comoounds bv SW846 8270CPrepared by melhod SW846 3510C
98-9t3 Nilrobenzene88,7t5 2-Nitrophenol100{2.7 +Nilrophenol
@.7$9 N-Nitrosodimethylamine
62164-7 it-Nttrosodi_n_propylamine
86-30$ N-Nitrosodiphenylamine87{65 Pentachlorophenol
s5-014 Phenanthrenei0&95-? Phenol
12940{ Pyrene
ri046-1 Pyridine12G62-l 1,2,4-Trichlorobenz€ne9+95,1 2,4,$Trichlorophenol8O{e2 z,4,GTrichlorophenot
Suzogate recoue4es.
32140-E 2-Fluorobiphenyt
367.124 2-Fluorcphenol
416&604 Mlrobenzene4'
416+62-2 Phenol4'
t7t&5t4 Terphenyl4l4
118-79-6 2,4,ETibmmophenol
SVOCS bv SW8a6 8270C StM
Prepared by method SW846 3510C
83.32-9 Acenaphthene
20&96{ Acenaphthylene90-r24 1-lilethylnaphthaten€l2Gr2-7 Anlhracene
56.5!3 EerEo (a) anth.acer€5G324 Benzo (a) py.ene
205-99? BerEo (b) fluoranthene191-?4-? B€nzo (g,h,i) perytenem7.084 Eenzo (k) fluoranthene218.O1-S Chrys€n€53-7G3 Dibenb (a,h) anthraceneA16-44-{l Fluoranthene8,J'73.7 Fluoaene19s.395 Indeno (1,2,3_cd) pyrene91.574 2-Mgthylnaphthatene91.20"3 Naphthelene85-014 Phenanthr€ne129{0{ Pyaen€
Sunogate rccovedes:321.tu8 2-Fluorobiphenyl
r719'5t4 Tetphonyl4l4
Tot l Metrls by EPA 60o0t000 Series Merhods
26-Mar47 29-MaF07 703149S M.BBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
747568679360
BRL
BRLSRLBRLBRLBRLBRLBRLBRLBRLBRLo.271BRLBRLARLARLBRL0.400
8292
pS/l 1.00
pg/l 1.00
pdl 1.0o
!S/l '1.00
lSn 1.00
US/l 1.00
pS/l 1-00
pg/ l 100
!S/ l 100
rc/l 1-00
US,4 1.00
USn 1-00pSn 1.00pS4 1.00
m- lm%1&flOot30-tm%| 5-110 %3G130 %| 5-110 %
!S/l 0.050
trS/l 0 050
US/l 0.050pdl 0.0s0pg/l 0.050pSn 0.050
trS/l 0.05t)pdr 0.050pg/r 0.050pglt o.o5opg/l 0.050pgll 0.050pg/r 0.050pgtt 0.050pglt 0.050pg/l o.o5opg/l 0.050pdl 0.050
30'130 %30-1n%
n1p,4 0.0300
mS4 0.fiX0
m9/ 0.0O5O
1 SW846 8270C
t "' t '
1 '
1 '' t "
1 "
1 "
1 "'1 '
1 '
1 '
I sw846 8270C/EPA625 S \4
2a-Ma?Ol
l44O-224 Silver
7ll4G38-2 Arsenic
74{}3$3 Barium
ARL
BRL
o.276
SW8.t6 60108 28)1afi7 2*tefi7 7O316n HB
This hbonlory rcpofl ls rrot valtd toltho,/r' on authodrzd sigtatarc on E cote. page
1 Reportable Deleclion Limit BRL = Below Reportjng Limi( Page E9 of | 65
Page 455
Sarpple ldentificationM8F-24 GWsA59641. r7
Cli€nt Proiect #t0l-88
MatrixGroudd Water
Collection Date/fime2 I -Mar-o? 00:00
Recaived22-Mar-07
CAS No. An&lyk(s) Resalt Flag Ani6 *RDL D ctlarl tte.hod Rel. PEFarul Analtz.d Bdch At 4lfst
Totrl M€trls by EPA 6m0/7000 S€rle! Meahods
7440-4+9 C€dmium gRL
Taao-a7-3 Chromium 0.0079
743+92-1 Lead 8RL
282.4s2 S€lenium BRL
Total Mclrb by EPA 2m Srri€s Methods
7€947.6 Mercury O.O0221
SW846 60108 28-l ar.07 28-lrlar-07 7031677 HB.rr9[
nrgn
.run
flI4n
fitdt
0.0025
0.0050
0.0075
0.0150
0 00020
1
I
1
I
EPA245.|T/47OA 28-Ma(41 ?f'-lttat47 7m167S YP
7W l4bdoq npoa ls naa vzlid xfrtou aa asrtariaed signztare on th. @!e. pqe -
* Reporrable Der€ctioD Limit BRL = B€loq, Reponing Limit Page 90 of | 55
Page 456
Samole ldentiftcationM8F-42 GwsA59803-18
Client Proiect #l0 r-88
MatrixGround Water
Collection Date/Time26-Mar-07 00:00
Received2'7 -Mar-07
CAS N^ Analrte(s) Resuk Fl"S Unia *RDL Dilutiort Method Rel. Prepoted Ahary.ed Batch Analyst
Vol.tile Ory{!ic Compounds
Volalilo Oroanic Cornoourds bv SW846 82608
Prepared by method SW846 5030 Water MS
76.rsn 1,12-TrichlootriflLrroe&anslFr€on 8RL6r.6,t1 Acelone BRL107 M Ady'orx1r'te BRLnrt$2 Benzene BRt108'86-1 Emmob€nzene gRL
74-97-5 Bromod oromelhane 8RL15.271 BEmodichtorometharE BRL15.212 Brcmoform BFL7l€€ Bro,nomehane gRL
78.$n 2-Buranffe (MEK) BRL10+st.0 ft<yhenzene BFL135-9&0 se.-Butylbenzene BFL90{66 En-Butyibenzene BFL7$154 Carbon disrlfide BffL*&5 Cafton t€trachloride BRL10s!ro-7 chloobenz€ne BBL7540.3 Chloioeftane BRLrfiG3 Chlorolom BRL7447-3 Chlo,o.tethane gRL
95-4!10 2-chtoolotrjene BRL106.43-4 4{hlootoluene 8RL96r2.s t,2-Djbromo-3dtDropropane gRL
12441 Dibrornodtorornelhane 8RL106'93-4 1,2-fibfomoelhane (EoB) 8RL74453 Dibrornomeihane 8RL550.1 1,2-Dd orob€nzene 8RL511-7?1 1,3.O{drlsrobenzene 8FL1m-467 1,4-Uchlorob€nzene BRL871 8 Ddlorodi(uord'nethane (Fr€on1z) BRLE*3 |,l-Dchloroethane 8fu107{rG2 1 2,oichloroethane 8RLi53H 1,1-Ociloroethene BRL156'5s2 cls-t,2-Dkt o{oelhene BRL156 6G5 tans-1,2-0ichlo(oelhene 8RLn'87.5 1,2-0id o{upopane 8fu14229s 1+CId oroflopane Bfus94,2(}7 2,2.0i$loropropane BRLs6+s84 I 1-Ochtoropropene 8RL1q)614r.5 cis-1,3-DidltorcFropene 8RL10061{2{ ta1s-1,3-0hhlooprop€ie 8RL100.11{ Eht6enzene 8RLEr6s3 ftexachloobutadiene 8RL
pg/l
u94pcn
!snp9l
lr],1!!/l
!91
!94
!s4p
Wn!snrqlsnwPEtvlpsl
P9lp94
tlSll
!srl
!s4
tjs4
!s4psl
u94
u94
ust!c4!olp9!
u9lult!91psn
!c4p91
!94f9l!s.4t41!s4!s4!slfs4!s4!snw
1.0
20.0
0.5
1.0
1 . 0
1 . 0
0.5
1 . 0
2.0
1 0 0' t0
1.0
t 0
5 0
t 0
1.0
2.0
l_0
2.0
l 0
1 0
2.0
0 5
0 5
t 0
t 0
LD
t.0
2.0
t .0
1 . 0
t 0
1 . 0
1 0
1.0
t . 0
1.0
1 . 0
0.5
0 5
r.00 5
1 0 0
1.0
r 0l 0
100
5.0
l 0
t 0
sw846 82608 29lrarO7 *Ma'41 7031197 n!
59t 78-6 z-Hexanone (M8KJ
F{Z-o h{popylbenzene99S?t 0tsopropy,itoluene1604-0/14 Metrylle(-butylelher10€ rG1 +Methyl-2tenlanone (M8075n9.2 Metrytsnechtoride91.2$3 tkphhdale
lqt651 FPopylbenzene
8Rt8RLSRLBRLBRL
BRL8RL
€RL
Thh lahoftttory rcpod it nol wlU wAhout zn oulhofized signalare on the covct IMge .
+ Reportable Dereclion Limit BRL = B€low R€poiing Limit Pas€ 88 of 154
Page 458
Sample IdentificationMEF.42 GWsA5980l- 18
Client Proiect #l0l-88
MatrixGround Water
CoLlection Date/Time26-Mar-07 00:00
Reccivcd2'7-MaL01
CAS No. Andyte(s) nesuk Flog Uni$ 'RDL Dilation Merhod Re[. Prepa.ed AaalyTel Batch Aruryst
Volatil€ Org!ric Compounds
Vo{afle orqanic Comoounds bv SW846 82608PrepaEd by method SW846 5030 Water MS
100-{2.5 Styrene BFLdlG203 1,1,!2-Tellactlooethane BRL793{'s 1,1,2,2-Telrachloroethan€ 8RL1271M Tela*ioroefrene SRL100{s-! Tdlene 8RL3?61{ 1,2,}Trichloob€n2ene 8RL12!,82-1 1,2,4-Tri:hloroben2ene 8RL7t,55.6 1,1,1-Tdchtoroedrane 8RL79.{lG5 l,12-Triciloro€hane Sfu7!{ls Tri:hlorDelhene 8Rt75t94 Tdrhtorotluoromethane (FGon 1l) eRL96.18-4 1,2,3-TriEilomprcpane BRL
5605 1,2,4-Tdme$Vibenzene BRL108574 1,3,5-Trifl'€frylben?ene BRL?5{l-4 Vin},l chtoride BRLrd0.2o7 m,Pxy'€n€ BRL
547{ cxytene BRLl@9+S Tetr"ahydmluan
sG2l-7 Elhy' sher994{F0 Ted-amyl melhyl ehers37,gz 3 E$/ ten_hltyl elherl@2s3 Dijsopropyiether?5€54 T€rt-But not / bulyt alcoholra41n l,{-Doxane
LA@4 48tonbflwnJhenzene
2@7-?6-5 lduen*d8
tiwnl4 |,z'D6lorcetharc44
1@5+7 Dibrutolluorcmethane
Erf .ctsble Pelroleum Hydiocrrbons
Exllaclable Total Pefoleum fudrocabons
Prepared by method SW846 351 0C
Bm6-61-9 Gasoline
6E4763G2 Fueioilt2
6&l763rt FuelOit t46855+00"{ FudOB6
u0(|0e@0 Motoroil
J001O0C]0 A\ialion FUel
tlnideni{ed
Olher Ol
Total Petrolelm Hydrccarbons
C$C36 Aliphalic hydrcabons
W3?2 l4hlotoula&c e
Semivolslile Organic Componnds by cC
OEanodliodne Pesticid€s SW846 Prft1A
Prepared by melhod SW846 3510C
S9.00-2 Aldrin
39e!6 a-BHC
!g/l 1.0
lgn 1.0
!94 0.5
!E 1.0
!s.4 t_0
lSn 1.0
pE 1.0
ps/ L0
psn 1-0
fgn 10
ps4 1.0
ps4 r0
!S4 1.0
!s4 1.0
!S4 !-0
tSl 2.0
t)SA 1.0
Ugl 100
pgl 1.0
VSI l0
ps/l 1 0
t d I o
pSI 10.0
!s/l m0
70130 %
70t30 %
TGtg%
m1fi%
O I
0 . 1
0.1
0.1
0.1
o 1
0.1
0.r
O I
0.1
swE46 E26081
I
1
I
1
I
I
I
1
I
I
l
I
l
I
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1
I
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1
1
1
29-[far{7 ?gl{a]4l 7A31797 RU
101
108
1U
BRL
BRL
BRL
BRL
BFL
BflL
BfrL
SRL8RLBRLBRLBRLBRL8RL8BL8RLBRL
mqn
mg,l
mE
mgn
m94
mgn
mqn
mg,4
mq4
m94
4+1$%
+CT ErPH
sw8468081A
2giiaAi 30tta47 1031772
2$Mar{7 zg"Mar-{)7 7031768
9t)
BRLBRL
$4
M0.0130
0313t)
Thb bborutory rcport is not veld wilhout aE outhoized sig'natare oa the caver page.
* Reponable Derection Limir BRL = Below Reporting Limir Pase 89 of 154
Page 459
SamplE Ide ificationM8F-42 GWsA59E0l-18
Client Proiect #301-EE
MatrixGround Water
Collection DatdTime26-Mar-07 00:00
Received2'l-MarO7
CAS No. At slru6) Fl4g UaAs rRDL Dil4llotr Mettod R.l: Pepored Aaqlgen $alch Adaltsl
Semivohtit€ Orgink Comporr& by CC
Oroanodllodne Peslicid€s SW846 eO81 A
Prepared by m€thod SW046 3510C
319{5-7 b€HC11!!06-0 +Bflc58.€e e gBrE (Lindar€)
t.?{ s ftbrbnen-$.6 44-000 (p"0,)
z.5re a,4-DD€ (p,p)
502s3 4,4OOT(p,p')6s5r,r Dieldin95$q€ 8 End6ulfan I3}213-664 Erddrllan ll10t107.8 Erdosuknsu(ate12?ljg Enddn7{21{3-r EndrinAhehyde7644 H€plact or724r-s Mghox}d{or1@4t3 Heplad or Eponde8001-3+2 TOxe{hsE5l0tl{ a-Chloftldls5655.91-7 g4htorde€53/|e47S5 Endin Keton€
1@&4+2 4,LDEMnwrMplHlyl(Sr)
n61.24!t Decm uobiplrEnyl(Si
Poh/.t odnated Eiohenvh bv Sw846 8082
Prepared by mebod SW8,l6 3510C
r?6/+11-2 PrCE 101611r04?s2 ICB 122.111r11- l6s t ,c8123250r692r-s PCB 1242126r2-2M PCB 12481109?69.1 PCB 1254
r10€e82-5 PCB 12m
r/!e+295 Pc81262rltoGt{-4 rcB 126{l
t@s+2 4,4.D8det@Miptpnl64
8ta+3 D€cedl ojilrrP{lyl (*)
S€mivolitil. Oryanlc Comportrd3 by GCMS
Semilola leorgd c Comoounds bv SW846 8270C
Prepa.ed by method SW846 351 0C
03-324 A.snapllflrgr€206.tt6-0 Arenaph$yleie9G12{ l.rrsrytnapitBlen€6e.5$3 fuilinot&12-f Anhrffin€t9\2-2+4 Al€:jn6ts-3+3 A:oh€nzeno/Dipn€nyttazine12-87.5 B€nzidines55F5 BeEo(a)anhrdcene
BNLBALBRLBFLBRLBF|-8RL8RLBALBFLBRLBRL8Fr-8RLB8tBFLBFLBRt8R_BRT
ljr!l
rylTE]lsn|lg4
!91
ts,l!g,l
tj91
Wlj$i
la4
t44
lsl
1,9r
|Jg/r
Mwldlps,l
*| fr%&tg
&150%
b-l50%
0u1300-013)0.01s0.06490.0t300_0t30031300_0026o0131)0.0i3)0.01300.0130001300 01300.01300.01300.06490.0130001300.0130
sw816 8081A
sua46 E082
sw846 €270C
Z{-Mar])7 29-llar{7 ?IB1768 IG
54
$'lpd
|jg4
Mts4wtlg4
!s4lgl
8Rr_8AL
BFL
BFL
BFL
8RrsR-BRL8RL
|4/l{grts4wltstNlttdltg4!s,
0.0260
o@60
0.86i)
0.860
0.0260
0.0260
0 0260
0.0260
om60
2g-llad? 2$Mar-07 703u69 SM
6090
8fl1BFLBRLBR-BntBRL
BAL8818nL
tgl
0.41D
1.00
1.mLm1tntI]0
1.m0.200
28-ilarc7 31.lraf{7 7C115$ M.S
fhls lab.alary zForl is aot ialid x'ithoat an.!.tho.iz?y' sigrafue on tc cowr pag..
+ RQoflablc Det€ctiod Limit BRL = B€tow Reportirg Lini. Paee 90 of 154
Page 460
Sample ldentificationM8F-f 2 GWsA59803-18
Client Proiect #301 -88
MatrixCround Water
Collection Date/Tipre26'Mar-07 00:00
Receive.d2'l -Mar-07
CAS No- Aaalye(s) FloC Unis +RDL Dilution Ptepared ArEUzed Batch Anslyrt
S€mivolatil€ Orgatric Compounds b) cCMS
Serhivolatt Ooanic Comoounds bv SW846 8270C
Prepared by method SW846 3510C
50-3?-8 oenzo(a)pyrene
26ss-2 Benzo(b)lluo|enhene191-2+2 &nzo (g,h,i) p€rytene
207{84 Banzo {k) ffuoanthene
B€nzaic acidu!51t B€nzyt atcohol11r-!r1-1 Ek(2{ito@thoxy)rne$ane111-.1.1-{ Bis(2dttoro€fv}elher39638.3p-9 Bis(2dttorcisopropyl)efEr11741-7 Bis(2-ehyhoxyl)phrhataE101-s53 +Bromophenylphenytelh€r
64 7 Bdl benzyl phhalale
8ri7'r-8 C€bazoles1l5c7 4-Chtorc3-melhlphe'1ot106{/3 4{hbromiline
s1.50-7 2{hloricmphthatenestr-8 2{hlorophenotftoS72'3 {{hlorophenyi phenyl ehet2r3{r€ Chrysene50'70.3 Dibenzo(a,h)anthrac€ne132-644 Dib€nzoluran9&501 l,2.Dichtorcb€nrene541.7+1 1,$oichlorobenEn€10e46-7 l,4-oichlorobsnzene9-9+1 3,3lDcitorobenzidn€120+a-2 2,+Dichtorophend8+6Gz oie$ylphlhalate131-1r-3 Dimlhylphlhatater0sr4 2,+Dine$ytphenolu.t+2 Di-n-butytphlhatale
l3+52'l 4,SDinito-2-n€lhytphffol
51.28.5 2,+Onitroph€not12t-1+2 2,4{iflitmhtu€ne
dG2G2 2"&Dmjtrototuse11t-&t0 Di{{dylphhataE2ll6-.!m Fuo€nlhen€t6.lJ.7 Buor€n€11EJ+1 Hexacltoob€nzen€87-Gt.3 HexachloDbuladj€nen't74 Hexacf{oocyclopentadi€nefl.n1 H€)acl{oost|ene1!F395 Indeno (1 ,2,3-rdJ pyrene,4.59n kophoones1.t.6 2-Methy,inafithaten€s-4!-7 z.llelhytph$ol
10s39-,1, ol.li,lffiylphenol106!i.591.2O3 I'laphbalen€
@74-l 2-Nitroaniline
F{F-z }Nitoanitiner0n{13 +l{lroanitine
BFL
BFL
BBL
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8RL
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8RL
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8Bt
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8RL
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8RL
BRL
BRL
BRL
BHL
BFL
BRL
8RL
BFL
8RL
8RL
BflL
BRL
BflL
BRL
BHL
BRL
BRL
8RL
BRL
BHL
BRL
BRL
8RL
8RL
BHL
8RL
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BRL
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8RL
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sw846 8270C 28 Mar{7 31 Mar{7 70316€0 M.B
This lfuorutory repon is not uolid withoat on aurtorized signaure on the corer page
* Reportable D€tectior Limir BRL = Below R€porting Limit Pas€ 9l of 154
Page 461
Sample ldenti ficationM8F-42 GwsA59803-lE
Client Proj€ct #301-88
MatrixCrcund Water
Collection Dat€/Time26Mar-07 00:00
Received2'7-MarO1
CAS No. Analy@(s) Resuk FIag Aaib *RDL Dilution Mzthod Retr, heptzd A aqzed Balch Aulfst
Semivol.tll€ Orgrnic Comporn& by ffMS
S€mivolalio Ooanic ClrnoounG bv SWP,46 eB70C
Prepared by method SW846 3510C
!6-!153 Nibob€nz€ne
€E-?$5 2{,litoph$ol100{2.7 +Nitrcphenol
82-75-!r Ni,lhrocodlme$ylemine
621t47 |lMrosodi.n-pfopytemine
s.1n6 itNfosodiptErryhmine
87{6.5 Penhdbrophenol
ll5{114 Pi€na$rf€{le
l0&S+2 Phenoll2goiH PyrBne
llG€+1 h/ridne1aH2-l 1,2,4-TritoroDen2eie!6.9!1 2,4,5-Tddoopienol
0€{G2 2j,CT'ic$ofo$e0ol
e1@4 ?nwdnph$l
fi7r2r 2+luo@hstd
.J66j,4 ili6slzse4,
1166.6?-2 Pllp,tul4s
1rt&514 Terpnenyl.d4
1t&/ 2,4.6-Itbrdwttend
SVOCS bv SW846 8270C SIM
Prepared by method SW84.6 3510C
s32-9 Acomphhene
a,ssfi A.enaphbylone!s12-o t-M#ytnadtfiatenat@-127 Arliracen€5865.3 B€nlo(a)antnreerE5+32-S B€r'!o (aloyene
205s9? 8ffuo(b)fluor|1f|eng1s1-24-l 8€nzo(g,h,i)p€den€2074ss B€n:o(k)fiuoranhene2r0-r)r,9 chrys€n€53.?G3 oibenao (a,h) anhracdeaE.4,t{ HuoEnlhene
8t.797 Fluo|Erc
!B-3&5 trdeno(1,2,3-cd)py€ne
91-t.6 2.]Ueft'y'naphhetenes'-20'3 ihphthalene
F)1-8 PlEnanhem1290{ Pf6n€
S!1qSab ruvai:r
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1nc.514 Te$rllf,nyld4
BRTBNLBFLBRL8RL8RL8RLBqLBRLBRLBRLBRL8RLBNL
e759654
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sw846 8270C
sw846 6ZI0C/EFA625 Sl[,
1
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Totd M€trb by EPA 6fr007000 S€rtes M€thods
Wil 0.05i0
tsl o.ll5l)
|8,r 0.050
wr oo5ovs| 0.060gS4 0.050
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Thit labonbrf reporl B not wUtI *tithost tA u.drorkd sE.eture on the cowr pzg..
i Reportable Detection Limit BRL = B€low R€porting Limit Pagegz of 154
Page 462
Sample IdentificationM8F42 GWsA5980l- 18
Client Proiect #301 -88
MatrixCround Watcr
Collection Date/Time26-Mar-07 00:00
Received27 -Mar-07
CAS No, Anal]te(s) Result Flat UniB 'NDL Dilutian Pnpand AruIrzed Ba.tch ldrlrst
Totrt Merrli by EpA 6000/7000 Series Methods
74ro-,r3-9 cadmium BRL
74rr0{7il chomium BFL
7'f39.92-r Led 0.0132
z&.432 S€ky[{D BRL
Tot l Mebls by EPA 200 S€ries Methods
743+97.6 M€rflry BRL EPA245-1114704 30-0,lar{7
m91
mg,l
mgr
mgn
0_0025
0.0050
0.0075
0.0150
0 00020
SWE4660108 30+lar-07 02-Apr{7 7031823 LR
ms4 02-A9rAt 7431424
Thir laboratory rcprl k ,tot rald plthou an sartoized sigazture on the cover ps|e-
' Reportable D€t€€tion Limit BRL = Below Reponing Limit Page 93 of 154
Page 464
Sanple IdentificationM8F-50GWs459,r64- l9
Clieot Proiect #30r-88
MatrixGround Water
Collection Date/Timel5-Mar47 00:00
Received
19-Mar-07
CAS No- Andr.e(s) Resuh Flag UniA *RDL Dilution Method ReJ Prepaied AntlfiEd Batch Atuttsl
Yohtile Orgrnic Compornds
Volatile Orqanic Compounds bv SW846 82608Prepared by method SW846 5030 Water MS76-111 1,1,2-Tricilorotrifluoroethan€(FreoERL674+l Acetone BRL107-13-1 Ao.ylonitrite BRLf11r2 Benzene BRL10&.861 Brornobenzene BRL74-97-5 Bromochloromethane BRL75-n4 Brornodichloromethane BRL7r2r2 grornoform 8RL7143-9 BrornorDethane BRL7&943 2-Butanone (irEK) BRL10+514 n-Butylbenzme BRL13f.98€ sec+utylbehzene BRLs€{€-6 tert-BrJtylbenzene BRL75.154 Carbon disutfide BRLs6.23.s Carbon tetachtodde BRLi0e9o.7 Chlorobenzene BRL75{0-3 Chloroehane BRL67{G3 Chlorofo.m BRL7{{7-3 Chloromethane BRL95-49-s 2-Chlorotoluene ARL106-43-4 4-Chlorotoluene BRL9&12-8 1,2-Dibromo-3-chloroprop€ne BRL12,88.1 Dibromochlofome$ane BRL10G93-4 l,2-Dibromoethane(EDB) BRL7445-3 Dibromonrelhane BRL9tre1 l,2_Dichtorobenzene BRLsi41.7+1 l,3-Dichlorobenzene BRL10646-7 1 ,4-Dl,c!\lotctbetuene BRL7t7r{ DichlorodiflUoromethane(Freon12)BRL7t3,F3 'l,l-Dichloro€thane BRL107-06-2 1.2-Dichlo(oethane BRL7t35-. l,|-Dichloroeth€ne BRL15e59'2 cis-'l ,2.Dichlo.oethene BRL15'6$05 h?ns-l,2.Oichloroethene BRL78€7-5 l,2-Dichlofopropane 8RL1112-2&9 l,3-Dichloropropane BRL59+m-7 2,2-Dichloropropane 8RL56!5+6 l,l-Dichlofopropene 8RL10061{l-5 cis- 1 ,3-Dichloropropene 6RLtoo6r{2$lrans-1,3-Dichloropropene BRL100414 Ethylbenzene BRL87€83 Hexachlorobutadiene BRL591.784 2-Hexanone (MBK) BRL98€2-8 lsopropylbenzene ARL99€7{ +lsopropyllotuene SRLt63141-4 Methyl teri-b{rb/ efter BRLi0&1(}r +Medryl-2-pentanone(M|BK) 8RL75{9-? Methylene chloride BRL
SW846 82604 21-Mat47 21-Maro7 7031185 ek
BRLBRL
uglusnpdlp94
!g,rl!91!91
!gnli9/l
Pg/lp9l
tr!yl
u(ylp!yl
ps/r
vgaugrt g l
t g l
ug/lpsn
!snvgtlrrgilttgllpsll
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lrg/l
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t g/l
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wl!g'l
t g l
t E l
llgl
wl
|ls,lpgl
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' t .o
20.00.51 .01 .01 .0o.51 .02.O10.01.01.01 05.01,01-02.91_02.O1.01.02 00 50 51_O1 0! o1.02.O1 01.01.01 0' 1 0
1 .01 01.01 00.50.51 .00.510.0
1 .01-01-010.05.0
1 01 .0
91?G3 Naphlhalenel03J-6$l n-Prcp!'lb€hzene
Thb l4boralory repod is ,tot vaIU fiilhou an sathorized ignatarc oa lhe colcr page .
' R€Fortable Detection Limir BRL = Below Reponing Limit Page 9l of 152
Page 465
Samol€ Id€ntificationM8F-50GWsA5%61-19
Clietrr Prciect #301-88
MarrixCround Wate.
Collection Date/Time| 5-Mar47 00:fi)
Rec€ivedl9-Mar-O7
CAS No- Aaalye(s) Fbs 'RDL Dilariot Mrlhot ReL Prcpored Analyvn Bztch Anab,sl
volrlile Orysdc Comportrds
Volatile O.oanic Comoounds bv SW846 82609Prepared by method SW846 5030 Wate. MS100-42-5 Sty€ne
63@2OG '|,1,1,2-T€tr€chloroefiane
79-34-5 i,1,2,2-T€bachtoroethahe127-184 Tetrachlo@€tlEne
10&68n Toluene
07{r-6 l,2,}Tridorohenzone
1?0J2-r 1,2,+Tdctltorobenzone71-55.6 1,.1,1-TriEfloroettEne79{G5 '|.1,2-Tricfiloroethane
79{1{ Tridior6th€$e
9618-4 |,2,lTrichloropropaneet63-6 1,2,+Trimethytb€nzene108-67{ l,3,tTrimedrytbenzene7541"1' Vinyl chtodde'33@2G7 m,p-Xyle.le96.17{ o-Xylenet0&9!|-9 T€[email protected] Efiyl ethergga-Oe€ Tert-aftyl methyl ehereB7-sz-l Efr/ ted+utyl etherr0e2()-3 oi+opropylether75$il T€rt-Butanol / buv alcolrcl12191n l,+oioxane
S{raog8(e /gcoverbsr160.004 /lBronEnuo@benzene
m37-2&5 TOhEne4Str060474 1, z-Diclioroethene-d4I8685i-7 Dibtontofluotunethene
Ertdc{rbl€ P€troleom Hf drocrrbms
Extractable Total Petrol€um HvdrgcadonsPrepared by method SW846 3510C800661-9 Gasoline6847+30-2 FuelOil #26647+31-3 FuetOlt #4f€5,5340-r FuelOil #6M0s800000 riob. oll,rc010(rc00 Aviatiofi Fudl
UnidentifedOtlEr Oillotal Pelroloum HydrocarbonsC+C36 Aliphdic Hyd.ocgrtons
SurlogtE g tgcor,glbs]g#&2 l-Chloroo{jpd€Eane
S€Dtvohdle Orgatrlc Codpound! by CCOrqanoc*rlo,rine Pesticld€s SW8,f6 8081APrepsrad by me0|od SW8il6 3510C3U9{X}2 Aldrin31s€a€ a€FlC
BRL
BRLBRLBRI-BRLBRL
BRLSRLBRLBRL
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1U)10295103
t .0
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1 01.0r . 01_01.02-01.010.01.01 .0't .0
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t c lliC/lpdl
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75{9-4 T.id{dofluoromethane (Faeon jl) BRI_
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BRLsRt-BRl-BRI,
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94
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SW846 808fA m-Mat4? 22411a,47 7031064 TG
This lahorototy .qort is ,tat ,aIU Fitlao an atthorlzcd sigmt*e on the coter page.
' Repo.toble D€rection Umit BRL = Betow [email protected] Liarir Page92 of 152
Page 466
Samrle lder!ificationMtF-s{lGWsA59464-t9
Client Prciect #t0l -88
IUatrixCround Water
Collection Date/Timel5-Mar-07 00i00
Receivedl9-Mar-0?
CAS No, Aaa+te(s) Result FloC *RDL Dilation Method netr. Pnpated .lrulfzed Bdth AnalJrst
S€mivohtile Orgrnlc Comporrds by CCOfoanochlorine Pesticides SW846 808'tAP.epared by method SW846 35iOC319_817 FBHC3198€_8 d-BHC58$ss g-BHC (Lindane)57-f4-g Chlordane72-54-a 4,4-ODD (p,p )7z-s+e 4,4-ODE (p,p.)5G2$3 4,4-DDJ lp,p')S57-1 Dieldrin95$98{ Enalosulfan I33213{+9 Endosulfan lll03i{7+ Endosulaan Sulfate72-20-A Endrin742r_e3_4 EndrinAtdehyde76-4{-e Heptachlor72-4+5 Methorychlot1024'57,3 HeptachlorEpoxade@0i-3t2 Toxaphene51037i.9 a€htodane56863,1-7 g-Chtordane53494-706 Endrin Kelone
Sil'rogate Ecoveies:103e8+2 4,+D&Octafl@rcbiphenri (Sr)2o5r-213 Decachloabiphenyl (3r)Polvchlo.inated Biohenvls bv SW846 8082Prepared by method SW846 3510Cr?s7+11-2 PCB 10t611t0+2s2 PcB 1221r11.t-r66 PCB 12325146921€ PCB 124212672.2e€ PcB 1249110€7S9-1 PCB 1254| 1i)96-€2-5 PCB .t26O
373a+235 PCB 126211100-14-1 PCB 1268
StrK]€ale aecowlias:I 0:)O6-&+ 2 4, 4 - D B-O c I efr uorf,hi phe n t4 ( S iu51.213 Decachlorobiphenyt (Sr)
S€nivoklil€ Orgsnic Co.npadrds by CCMS
8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLARL8RLBRL8RLBRLBRLBRLBRLSRL
9493
ARLBRL
BRLBRLBRLBRLBRI-BRLBRL
75105
BRLBRLERLBRL
BRLBRLBRLBRLBRL
30-150 %m-150 %
0.01430_01430_0143
0,07140-01430-01430-01430,002s0-014:l0.01430.014:]0.014:]0.01,$0 01430.01,$0.01430 07140.01430.0143o.o143
o.o2a6
0.02860.02860.02860.02860.02860_02860.02860.0286
1.000.4001.00t.00t.001.001.00Lm
0200
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tlSJl
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ps/
sw846 8081A m'Ma(47 22-Mar-0t /031064 rG
Semivolatile Orqanic Compounds bv SW846 8270Cftepared by method SW846 3510C
&-32-9 Acenaphthene4&96€ Ac€naphthyteheS,124 1-Mehytnaphthalene@\513 Anilmei2G12.7 Anthrac€ne1912-2{-9 Atrezine103-33-3 Azobsnzene/Diphenytdiazine@€7-5 B€nzidine56.5S3 B€nzo (a) enthrac€n€
SWa468O82 20-nnx-07 29MaG077031o63
sw846 8270C 20-Mat47 23-Ma(47 7031070 M.B
30-150 %30-150 %
!9!
fg/lpg/l
us/l!9/lpg/l
pc4
!94
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I'El
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ItEl
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psntlgJl
t d l!sr
This lahorulory epod B ,tol ,alld wilhour ar. rulhoriu.t signsla.e on ahe corjr page-' Reportabl€ Detei:tion Limit BRL: Below R€po.ting Limit Paae 93 of 152
Page 467
Samole ldeotificationM8F-50GWsA59464- t9
Cliept Proiect #301-88
MahixGround Water
Collection Dat€/Tim€I 5-Mar-,07 00:00
Rec€ivedl9-Mar-07
CAS No- At alyt2(s) Rast/A Fl"c tRDL Dttuloa Method R.l PEWen Analfzcn Bdch Aaabtt
Semlvohlilc Orgrdc Compoun& by GCMS
Semivolatil€ Orqanic ComDoonds bv SW8,l6 8270C
Pr€parcd by rnethod SW846 35't0C$-32{ 8€rEo (a)pyaene2o5"s9-2 B€nzo (b) nuoranh€ne1el.24-2 B€nzo (g,h,i) perytene207{8.s B€nzo(k)fluoranthen€65:€tu Benzoic acjd10G515 B€nzyl alcohol1t1-91-t Bis{2<hloroeboxy)metn€ne111-444 Bis(2{filoroetM)ehe.3e6e-32€ Bis(2-dhlooisopropyl)€ttEr117-8r-7 Bis(2-€drythexyt)phthalatet0l€5-3 4-gornophenyl phenyl €fler85-6&7 BuMb€nzylphthalate86-74{ Cadezole5$50-? +CHoro-lrnehylphenolt0&47{ 4€hloroanitines1-5&7 z4hloronaphthatene9s{7-8 2+hlorophend700s-72'3 4-gtbrophenyl phenyl ethea2i8.01-9 Chryseneti-7G3 Oib€(lzo (a,h) anthra€sfle132+9 Db€rizofuran95-5G1 l,2-DichbroberEooe51ti-73-l 1.3-Oichlorobenzene1064G2 l,4oidoobenzene9l-94'1 S,3.Didllorobenzidine12033? 2,4oictrloNphenol84.66-2 Dieftylphthalate131-11-3 DidEthyt phnhahte105€7-9 2.+Dlm€6ytphenolu-7+2 Oi-n-buMphhatates31-5,2-l 4,6-Dinltro-2-rnethylphenol51-2&5 z,4oinitroohenotl2t-14-2 2,+Dhihodolu€n€f,trczs2 2,eDinitrololuenet17{4{ Di-n-oclylphthalateal€-4a{ FfuoEnthene86-717 FfuOaene11+7+1 Hexechlorobenzene476&3 He'0aarrlorobulsdieno71174 Hexrchlooc.ydopenhdiene67-12-1 Hexadoroethene1sg3ss lrdeno (1.2,3{d} pyreoe?t-591 lsophoam€e15/{ z-Molhyhaphthabne95-4&7 2-Me0vphend1o&3o.a, 3.+M66ytpheool106-44-59l-2G3 Naphthatenell8-zt4 2-Nit@nilines€{x!2 }Nitlgnilinetoo+r€ +Nitoanitine
SW8,16 8270C zGI ar-07 23-ttiar{7 7031070 M-BBRLBRLBRIBRIBRL
BRLBRLBRLgRL
BRLBRLBRLBRLBRL8Rr_BRLBRLBRL8RLBRLBRLBRLARLSRLBRLSRL8RLBRLBRLBRLBRLSRLBRI8RLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRTBRTBRL
BRL
BRL
BRL
ugtl|ldlvstl
wlus/lpdl
Wnp9nFgrlpsnrslpdl
udlpsrl
psn
usrpdI
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rsnpdl
rrg,l
vsnps/|pdl
|ldl
$dl
wl
!glpcl
tjgl!gtsdltldtgllpdl
pdl
rdlusnrs4psil
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02m02001.00
0imt.00Lm1.00to01.00|.00
Lm1.001.00't.oo
1.00t.00|.001.001.00
o.2m1.00t.00t.001.00'1.00
1_001.001.00t.001.00t_001-001.00r.fi)r.00't.00
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0-€00r.fi)1,00
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r.00
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This lab.cory .qod b Eot s&d withod at asrtodztj sigu'tur. on de @ra page .
I R4ortable D€tection Lidir BRL = Below Rcporting Limit PEge 94 of 152
Page 468
Samole IdentificaLionM8F.50GWs459.+e{- l9
Client Proiecr #101 -88
MatnxGround Water
Collection Date/Timel5-Mar47 00:00
Received
l9-Mar-07
CAS No. Anarytz(s) Resall Flog A n s *RDL Dilution Method Rel. Prcpued Anabzed Boteh Anabst
SeDivolrtilc Orgaric Compohds by cC${S
Semivolatile Oroanic Compounds bv SW846 B27OCPreparcd by methad SW846 35t0C98€$3 Nitroben4ene84.75-5 z-Nit ophenol10G02-7 +Nitophenol62-7+9 N-Nitrosodimethytamine621+a-7 N.Ni[osodi-n-propylamine863}5 l$NilrosodiphenytamineItSs Pentachlorophenol85{1-8 Phenanthrene10&9t2 Phenol1?9{XF Pyrone110-€6-1 Pyrfujine120{2-1 l,2,4.Trichlorobenzene9+9+a 2,4,STrichlomphenol€€4e2 2,4,GTriqhtorophenol
Srrzogatg recovenbsl321504 2+luorobiphenyl367-t24 2+htorophetml1165.6,4 Nilrcbenzene4S116542.2 Phenol4sth$sr4 Teryhent44l411e79.6 44,+TnbromophenolSVOCS bv SW846 8270C SIMftepar€d by melhod SW846 351 0Ca3{2.9 Acenaphhene
a)ss€;8 Acenaphthytene90-12{ 1-l/ethyhaphthal€ne12G12-7 Anthracene5G5t3 Benzo (a) anthracene50-32{ Benzo (a) pyrene4+99-2 Benzo (b) flloranthene191-2+2 Benzo (g,h,i) perylene207{€-9 Benzo (k) ffuoranth€ne21M1€ Chrysene53.7G3 Dibenzo (a,h) anthracenea)6-44{ Fluorantheneffi-7T7 Fluorene193.395 Ind€no (1,2.3-cd) pyrene9r-57€ 2-M€thylnaphthalene91-&3 NephthaleneC5{1{ Phenanthrene129{0{ Pyrene
Sunogktl€ aaooyeries:32t&4 2-FluofobiphenyltrteiQ Tefphenyl44
Toarl M€tak by EPA 6000/70010 Series Methoa!
SWE46 6270C 2o-t!4ar07 23-Mar47 7031070 M IBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
595367657444
BRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRL
BRL
5066
pSJt l.o0
Udl 1.00pgl 1.00
ldl 1.00pg/l 1.00
lig/l 1.00
ug/r 1 00
ugr 100
ldl 1.00
ldl 1.00
Ug/l 'l.00
pS/l 'l.00
ttSJl 1.00
ldl 1.00
30-130 %1L110 %30-130 %15-110 %30-130 %15-110 %
pS/l 0.050pS/l 0-050
ldl 0.050
Lidl 0.050ydl 0.050
!g/l 0.050
US/l 0-050
liS/l 0.050
uS/l 0.050
udr 0.050
lisn 0050pdl 0 050
!s/r 0.050
ldl 0.050
udl 0.050yg/l 0.050
tqll 0-050
30-130 %30-130%
n?gn 0.0050
rng/l 0.0040
mg/l 0.0050
!dl 25-rlla..oT
7!ue44 Silvet
744O'3F2 Aserlic
Zg0-3+3 gadum
8RL
0.0m2
0.0322
SW846 6010S z3"Ma'.Ol 24+.4aro7 7031315 LR
Thb tabontory rcpora ie not ealid xtlthottt sn aalhoited signaturc on the cowr page .
+ Repodallle Delection Limit BRL = Below Ref'orting Limit Pase 95 of 152
Page 469
Sample ldeotificationMtF-50GWsAs9464-19
Clielt Proiect #l0t-88
MatrixGround Water
Collectioo Date/Timel5-Mar47 00:ff)
Releived| 9-Mar-07
C.AS No, Anaqtz(s) Fhs A n s 'RDL Diluiarr Method R4 Prcpaed Antlfzrn Dahh Arutlfsl
Torrl Metlb by EPA 50O0,1U)0 Series Methods
71.4043.9 Csdmium
744G{7-3 Chrcmfum
7€9-92-l L€ad
r|S2-4+2 Selenlum
Tolrl Metal$ by EPA 200 S.rie6 Mcthods
7439.975 Mer ry
SWa46 60108 23-Mar4f 24ji1d47 7031315 LR
EPA245.In47OA 2$M€r{? 23-ti,la.47 781316 RM
BRL
BRL
o.0120
BRL
BRL
firgn
mgr
nB/t
rtSI
0-0025
0-m50
0.m75
0.0150
0.mo20mg/I
This lahodor! tzpotl it not wlld nithou an aathoi?rl EiE tttare ot lhz coeer p!{re.
+ Reponabl€ Detection Limir BRI- = B€low R€podng Limit Paee 96 of 152
Page 470
APPENDIX GQA/QC Sample
Laboratory Reports
Page 472
Sample IdentificationFB.I
s459464-17
Client Project #l 0 l - 88
MatrixBlank water
Collection Date/Timel5-Mar-07 00:00
Received
l9-Mar-07
CAs No. Analrte(s) Result FloE Unlts 'RDL Dilution lve.hod Rel. Prcpdred Antryzed Batch AMIlst
Vohdl€ Organic Compoundr
Volalile O.oaoic Comoounds bv SW846 82608Prepared by melhod SW846 5030 Waler MS7F1$1 1,1,2-Trichtorolriffuoroethane(FreoSRL67€+1 Acetone BRL107-13-1 Aciylonitrile BRLf14T2 Eenzene 8RL104-€6-1 Bromobenzene BRL7+91-5 Bromochloromethane BRL75-274 Bromodichloromethane 8RL75-2+2 Bromofoam BRL74{}9 Bromomelhane BRL7843-3 2-Buianone (MEK) BRL1(X-51-8 rFButylbenzene BRL13$98$ s€c-Butylbenzene BRL98{€4 te(-Butylb€nz€ne BRL75.1s4 c€rbon disulftd€ BRL56-23-5 Carbon tefachloride ARLi0&9{r7 chtofDbenzene BRL7$OD3 Chtoroethane BRL
BRLBRLBRLBRL
us/| 1.0f94 2O.O
ldl 0.5
!g/r 1.0
!s/l 1.0
rs4 'l -0
tstt 0 5
tlSJt 1.0
USn 2.O
!S.4 10.0
Ug/ l 1.0
|'jS/l r.0
pdl L0
pdl 5.0
p d l 1 0
p g t 1 0
l.dl 2.o
ust 1 .0!S/l 2.O
tgt 1.0
ldr 1.0
ps/l 2.op d l 0 5
I S n 0 5
pdl 1.0
p S n 1 0
!s4 1.0
lg l 1.0
!g/l 2.O
pSll 1.0
t91t 1.0
trdr 'r _0psr 1.0
N t 1 0
USn 1.0
lSn 1.0pSn 10pSn 1.0pSn 0.5pdl 0.5
!g/l 1.0
US/l 0.5
US/l 10.0
IS/l 'l.0
pdl 1.0pdr 1.0pg/l 10.0
vgl 5,0
vs,tt 1.0ydr 1.0
1
1
1
1
1
1
1
1
1
I
I
1
1
1
1
I
1
t
I
1
1
I
1'|
1
I
I
I
1
1
1,1
'|'|
1
I
I
I
I
I
1
1
1
1
1
I
1
1
1
SW846 82608 21-Mat47 21-Mat47 7031185 ek
67S3 Chloroform74{7-3 Chlofomethane95.49-8 2.Chlorotoluene10H3-4 4-Chlorototuene
-124 1,2-0ibromo_3doropropane BRL121-4&1 Dibromochloromehane BRL10e93-4 l,2-Dibrornoetr|Ene(EDB) BRL74.9$3 Dibronromethane BRL955Gr l,2.Dichtorob€nzene BRL4,41-73J l,3-Dichlorobenzane BRL10646-7 1 ,4-Dichtofobenzene BRL7+7t€ Dicfiloodiiuoromehane(Fr€onl2)BRL75-34-3 1,l-Dichtoroethane BRL107{6-2 1,2-Dichtorcethane BRL
l,1-Dichloroethene BRLt5e59-2 cis.1,2-Dichtoro€thene BRL15ffi{ trans- 1 ,2-Dichioroethene 8RL7847-5 i,2-Dichlo.opropane 8RL142-28-9 |,3-Dichtoropropane BRL59+20-7 2,2-Dicf oioprop€ne gRL
56'5+6 t,1-Dichtoropropene BRL10061{1-s cis-1,3-Dichloropropene BRL10061{24trans-1,}Didrtoropropene BRL1oq1-4 Ethylbenzsne BRL87{&3 Hexachlo.obubdiene BRLi91-78{ Z-l-texanone (MBK) BRL9832{ lsopropylbenz€ne ARLgs{7$ 4-lsopropyltolu€n€ BRL163.4{a4 Mettryttert-buhy' other BRLi0€.1e1 +Methyt.2-pentanone(IflBK) BRL75{92 MetMene chtodde BRL91-2G3 Naphth€lene BRLt09A$1 n-Propy'benzen€ BRL
This taborcoty rcport is ^ot volkl n' hou an outhofizei sig,/,aturc on the colL€r ptgc.
+ Reponable Detection Limit BRL= Below R€podng Limit Pag€ E3 of 152
Page 473
Sample IdetrtificatioaFB.I
sA59.t6r- l7
Client Proiect #301-88
MatrixBlaok Water
Collection Date/TimeI 5.Mar47 00:00
Rec€ivedl9-Mar-07
CAS Na Adqlf,e(s) ResaU FI"S Unia .R.DL Dilatioa MEthod Rel, PEpsred Anzlwd Bach Anzlyst
Vohtile Orgrlic Compornds
Volatil€ Orqanic Comoounds bv SW846 82608Pr€par€d by method SW846 5030 Waler MS
BRLBRLBRL8RLBRLBRLBRLBRL8RrBRL
7559-4 Tri€*{oroffUoomethane (Freon 1l) 8Rl-
tolx2-s St)rcn€63G2O€ 1,.1,.1,2-T€hcl or€thane79-34-5 1,.1,2,2-TetracNoroethane127n8-4 TotladrloloeUlenelom.3 TOlUen€87-61{ 1.2,}Tridltorobenzene12oi2n ,l.2,4-T.ichloobenzene
71.55€ |,1, t -Trichloroelhane
79.0[!.5 |,1,2-Trichtorcethane79Oi5 Trichloro€thene
SW846 82604 2l-Mar47 21+larO7 7031185 ek
BRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRL8RLBRL
9910296101
BRIBRLBRLBRLBRL
BRLBRLBRLBRLARL
88
BRLBRL
tstusn|lsnt'$t4t'dl$nrsfl|lsnpdl
!dlusnuglsdlusflt g/l
l€/l
pc4
|'|s4pqlpglpdl
!dlpdl
t . 0
1 .00.51.01 .01.01.0
1.0r . 0t . 0t . 01 .0r_01.01_02.n1.0't0.0
1.01 .0t . 0t . 010.020.0
o.01210_o121
I
1
I
I
1
I
I
I
I
1
l
1
1
1
I
7
I
1
I
I
1
1
I
1
96-14-4 1.2,9Tri:tlloropropane9163{ 1,2,+Tdmethylbenzenel0o{7€ 1,3,s-Trimethy'benz€ne7501-4 Vinyl chtoride133G2G7 m,p"Xylene95-.17$ o_Xyiene10+99-9 TdEhydrofuran60-2$7 Ehyl dher994-05{ T€rt-amyl methyl elher637€2-3 Ethytsft_butyleherto&mn Di-isopropytefll€r755to Tert€utanol/ buty' alcohol1?3€r-1 I,41Dio)6ne
Surogale recoveries:16oJn4 lt4honofluorobenzene
437-2e5 ToltAne4S17 06047 4 1, zaichloroethene-d41868-sv7 Abrcmofluorcmelhane
Ertrrctrble Petmleum Hydroclrbols
Ext-actable Totral Peboleuin Hvd.gc€rbonsPrepared by method SW846 3510C00064i-9 Gasolino68117&30.2 Fuet oit #26847e31-3 Fuel Oil #468553{0{ Fu€| Oil #6i,10980flm Motof Oil.()01m{P0 Aviation Fuel
UnidenlifedOther OilTotal Petroleum HydrocarbonsC!9-C36 Aliphatic Hydr6arbons
Sr/'rDgata €cot€d,es j3{je643-2 1 4hlorooctdecane
Semlvolrtil€ Org.ric Coopo|rndr by CCOroanoct orine Peslicides SW846 SOBIAPrepared by rnethod SW846 3510C3rls-oGz Aldrin3ls8a€ 6-BHC
+cT ETPH 2l-Mat47 Uia47 7031160 DS
7G130 %
70-130 %
7G130 %
7G130 %
rndl 0.ImCn 0.1mgl 0.1mSil 0.1fiigl 0.1
msn 0-1drsn 0.1mSn 0.1mg/l 0.1mg/| 0.t
4llt'to %
1'snItgl
SW€46 m81A 204.,.?d47 t.+tato? 7031064 TG
Thit laboralory .epott it no, valid tdthotd ott oizd signattte on the cavc!pag..
+ R€portable D€t€ctioo Umit BRL = B€low R€poiting Linit P.ge 84 of | 52
Page 474
Sample IdentificationFBIsA594er- l7
Client Paoiecr #301_88
MatrixBlank Watcr
CoLlection Datc/Timel5-Mar.07 00:00
Received19 Mar-07
CAS N^ Analrte(s) Resull Fl4C Ani6 *R.DL Dilutian Melhod Ref, Preparcd Amlyzed Bqlch A"alyst
Semivolrtih Orgrnic Compounds by cC
Oroanochlorine Pesticides SW846 8081A
Prcpared by m€thod SW846 3510C
3r+8+7 b-BHC31S{64 d-BHCsa4$e g-BHC (Lindene)
5/-74.9 Chtoadane72-544 4,+DDD (p,p')
72,55.9 a,4_DOE (p,p.)
50-2+3 a.4-DOT (p,p')
60-57-l Dieldrin95s98€ Endosutfan I3321+65'9 Endosuffan ll1031-073 Endosutfen Suttate72-204 Endrin7421.93-4 €ndranAldehyde76444 Heptachlor72-43s fttethoxychlor1024-s7-3 Heptachtor Epoxide€001-3+2 Toxaphene
5103-71-9 a-Chlordanef,a,6€,3+7 gchlordane
5349+7Gs Endfin Ketone
Su/rogate rec?ver'es:1 0386++2 1, 4 -DB-OeIafl uorobiphenyl (Sr)
mst'21'3 Decachlorobiphenyt (St)
Polycfilodnated Blohenvts bv SW846 B0B2
Prepar€d by melhod SW846 3510C
126f+11.2 PCB 101611t04-28.2 PCB 12211r14r-16.5 PCB 1232534692r-e PCB 1242126?2-29{ PCB 124811097691 PCB 125411006-82,5 PCB 1260
c7c21.23.6 PCg 1V62
111&144 PCB 12€8
Suftogaie Bcovedes:103864+2 l,4Dgoclafluorobiphenyl (50
m51-243 Decechlorobiphenyl (Sr)
Semivolrtile OrSrnlc Compounds by CCMS
2GMaF07 23.Mar{7 7031063
BRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
9781
BRLBRLBRLBRL8RLBRLBRLBRLBRL
I t
95
BRLBRLBRLBRL
BRLBRLBRLBRLBRL
!El
ljEl
!sI
FEI
FSn
us4ps4
!s{!gn
!g/l
!s/l
!gn
uEl
ug/l
!g/l
ut/l
ugl
|rg/lpgn
|rg/l
!gl
!gn
!gn
ug/l
!s/l
!gnpg/l
rsnpg/l
o.01210.01210.0121
0.06060.01210-012ro.0121o 00240.0'1210.0121
0.0121o.o121o.o121o.0121o.o121o.01210.0606o_o1210.01210_0121
30-150 %3G150 %
sw846 8081A
sw846 8082
sw846 827(rc
1
1
l
l
I
I
1
1
1
1
1
1
1
1
1
1
1'|'|'|
o.02420_0242o_02120 02420.02420.02420.0242o.02420 0242
1
1
1
1
1
I
1
1
1
3F1SO %
30150 %
Semivolatile Oroanic Comoounds bv SW846 8270CPrepared by method SW846 3510C
A3{2-9 Acenaphthene20e96{ Acenaphthylene90.12{ l-Methylnaphthalene
@-5!3 Anitine12&12.7 Aihrac€ne'1912-249
At-azine10$33.3 Azobenzene/Diphenyldiazine
9?{7-5 B€nzidine5&593 B€nzo (a) anthr€cene
2O-Mat47 2344erll 7031070 M.ApEl
Fgn
lgr'l
llEl
FgI
l|sntrgl
ll(/l
rdl
1.000 4001.001.00r.001.001.001.00
0.200
This laboratory npoa is not vafid wirtoat an ra,horized sigttzturc on the cover page .
' Reportable Detection Limit BRL = B€low ReFo(ing Limir Page 85 of 152
Page 475
SarnDle ldentificationFB-IsA59454-t7
Client Proiect #30 | -88
MatrixBlank Water
Collection Date/TimeI 5-Mar{7 00:00
Receivedl9-Mar{7
CAS Na AnaIrE(s) Fl"s Anb *RDL Dilutbn Mdhod netr. Prcpated Analfzrd Adch An&lyfl
Sealvolraile Org.ni. Compo||||ds by GCMS
Semiwlade Oroanic Comoounds bv SW846 8270C
Prepared by method SW846 351 OC50324 Benzo (a) pyr€ne2O$9e,2 B€nzo (b) fr'Jo,rEflth€ne191-2a-2 B€fEo (g,h,i) perylene207{6-9 Benzo (k) nuorantfiene65{S0 genzoic acidl0G5l-6 B€nzylalcoftol111-9r-1 Bis.(2{hhfoEthory)mehane111-aaa Bis(2-ohlo.o€thyl)eflrer38€38-32.9 Bis(2dttoroisopropyl)ether117{1-7 Etis(2€hy,thexyl)phthatatoi0t-553 +Bromophenyi phenyl eher8s6&7 Butyibenzylphth6tEte8G743 Cgrbazole!€-50-z +cftloro-3-mehyiphenol106-47{ +Chloroaniline91-50-7 2-Chloronaphthalene95-57-8 2-Chlompheflol7005-72-3 il-Chlo.ophenyj phenyl ether218{t-9 Chrysenes3-7G3 Dibenzo(a,h)antkacene132{.t€ Dibenzofuaan9&sG1 l,2-Dichlorcbenzone541-73-1 i.3-Dichlorobenzene10c46-7 1,4-Dichloobenzeoe9i++1 3,3-Dichlorobenzijine120-€3-2 23-tlichloro0henol84{&2 Diehyt phthatate131-113 Dimethyl phth€tetetotr7€ 2til-Dimohytph€fiolu-7+2 Di-i+uMplthalat€53+s2-1 4,6-Diniko-2{nediylphenol51-2&5 2,+Dinitrophenolt2r.r,1-2 2.4olnibototuene60G2GZ 2,SoanitbIotuene117{,{.0 Okl{{t/phthshto20G44{ FluoEn$tene&-1rf Fluorenel1e74n Hexachlorobenzene87€+3 Hexachtorobutadiene71474 l-lexachlooctdopentadiene67-7?-1 Hexechloroethaoe1943s-t Indono (13,34d) pyene7€-59-1 lsophorone9l-57$ z-Merhrnaphhatenes54+7 2-Methylphenol1o€.3s-1, 3,+Methytphenol1o€-it{-5et-al3 Naphthalene8€-7.Lrt z-Nitroenitine99:0+2 $Niboaniline10O{t€ +Nitoaniline
BRLBRLBRLARf,ARLSRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL8RLBRLBRLARL8RLBRLBRLBRL
BRL
BRLBRLBRL
wlysn
FSnPdlPS/|FSrltt$wpgl
tlsAyglps4
wItdlpdl
ugl
ug/lt,qtlvgtlp$4
!dlrcnttdrpgrlpglpdl
u g l|'lsnt'q[w!s/l!94uslltlS|l
ItEl
vgtltJslpsA
ugtl|,9/lItgJl
ttgl!dl!dl|lg/l
psn
FS4psr!dlu{l
0,2000200r.00
0.3001.001.00|.0,0
L001.001.O01,001.001.001.00
1.001.001.001.001_00
o.mo1_O01.001.(m
L001.001.001.001.001.00r .m1.001.001 001_(X)r.00
1.001.001 0 00.6001 0 0
|.00
0.zx)1.001.001.0010.0
t.00
1.001-001.00
SW846 8270C 2O-Mat47 23.1t,er'7 7031070 M.A
Thh lzborotoq npo.t ls Eot eold ,rithoa att aalhot zpl ttgadare on thc covr ltzg. .
. R€portable Detection Limia BRL = B€low Reporting Linit Pagp E6 of | 52
Page 476
Sample ldertificationFB-1sA59464- r7
Clierlt Proiect #l 0 t -88
MatrixBlank Water
Collection Date/Timels-Mar{7 00r00
Receivedl9-Mar-07
C4S No, Analyte(s) Resttll Fl"S Ani,s *RDL Diluiotr Method netr Prcpued Anauzed Batch Analyst
Semlvolrtile Orgrnic Compo||nds by GCMS
Semivolalile Orqanic Comoounds bv SW846 8270CPr€pa.ed by meihod SW846 35t0C
sB9t3 Nitrobenzene88-79F5 2_Nitrophenoli0Go2-7 +Nitrophenol62.719 N-Nitrosodamethylamine621€4-7 N-Nitfosoda_n-pfopylaminem.3G6 N-Nitrosodiph€nytamine47J6.5 pentachloroph€nol
854r{ PheMnthrene106-95-2 Pheno{12s00{ h/rene1lc€8r F'Jridiner2o-42-1 1,2,+Tdctitorobenzene9+95-4 2,4,$Trichlorophenol{18{€F2 2,4,GTncfrtofophenol
Sffrogate re€o!€ries-3214c-a 2-Fluorobiphentl
357-124 z-Fluorophenol
1165-604 Nihobenzene-ds
416162-2 Phenol4s
17tAS14 Teryhenyl4l4
118-794 2,4,GTtibtofllopheool
SVOCS bv SW846 8270C SIM
Prepared by method SW846 3510C
8332.9 Acenaphthene
2rl&964 Acenaothylene9O.12{ 1-Methylnaphlhalene120"12-7 AnthEcene56-5+3 Benzo(a)anthmcene50-32-8 Benzo (a) pyrene
?05-99-2 Benzo (b) fluoranthenelgl-24-2 Benzo (g.h,i) peryl€ne
20rc&g Benzo (k) fluoranthene?1F014 Chrysene53-7G3 Oibenzo (a,h) anthracene2{E-1,.-0 Fluo(anthene06-717 Fluorene19$39$ Indeno (1,2,3-cd) pyrene9i-57€ 2-Methylnaph0ratene9l-2G3 Naphthatene854r-g Phenanthrene129-00{ Pyrene
Surrqale reco.y€ies:321-6Go z-Fluothiphenyt
171e-514 ferphenyl4l4
Tobl Metab by f,PA 6000/?000 Serier M€thods
8RLBRLBRL8RL8RL8RLBRLBRL8RLBRLBRLBRLBRLBRL
697083638552
BRL
BRLBRLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
6176
trdr 1.00pdl 1-oo
vq 1.00
U94 1.00
!q/r 1.00
lsr 1.00
lgr ' t .00
llg/l 1.00
t)glt 1.0O
ug4 1.00pS4 1-00pdl 1.00
US/l 1.0Opdl 1.00
3G130 %15-110 %30-130 %15-110 %m- tn%15'110 %
pgn 2$Mar-07
1
1
1
I
1
I
I
I
1
1
1
I
I
I
1 SW846 8270C/EPA625 SIM
7440.224 Silver
7l4O-38'2 Arsenic
7,{403+3 Badum
rsn 0.050pgn 0 05O
l.dl 0-050
FSI 0-050
Ug/l 0.050pg/l 0-050
lgn 0.050
sdl 0.050
liS/l 0.050
tsA 0.050
$slt o.o5o
lsn 0.050
liS4 0.050
ug|/| 0.050pdl o.o5o
fdl 0o5o
US4 0.050
30-130 %3G130 %
mg/l 0-0O5O
mg/l 0.0040
lng/l 0.0050
sw846 60108BRL
BRL
8RL
23-Met47 24+/tat47 7031315 LR' 26.1,{ar{7' 24-Mat47
Ihk laboftaory repod is nor wud rslthoa oE aul'ortatd siFn,/t,,,.? on thz corer pagc
' R€podable D€teation Limit BRL = Below Reponing Limit Page 87 of 152
Page 477
Sample IdetrtificatiooFB-Is45946+ t7
Cli€nt Proiect #30t -88
MatrixBla-ok Water
Collectiol Date/Timel5-Ma.-07 00:00
Receivedl9-Mar-07
c-as N^ ANtrE(s) Resslt FI4g Anib *R.DL uhtu'n Method ReJ. Prepued Amly,en Buctt Aazlpt
Tobl Metab by EPA 6000/7m0 S€rlci Metrorb
74.10-,13.9 Cadmium BRL
7440-47-3 Chmlitium BRL
7439-92r Lead BRL
282-4+2 Selonium BRL
Totd Mettb by EPA 200 Serlts M€thodt
743997€ t\iercury BRL
mgn
ntg/l
mql
mgr
fitsl
0.0025
o.0050
0.0075
0.0150
0.00020
SW84660108 21Mar47 2+[,lar{7 7031315 T-R
EPA245.1n4l0A 23 tafi7 Z3Jtrlar{7 7031316 RM
':hb bbontory Eport It n4t vzlil iirtoar an auttort4d slgn4urc on lh. co|9. page .' R@drble D€t€ction Limit BRL = Bdow R€porting Linit Prge 8E of 152
Page 478
Sample ldentificationTLT5A59464- I8
Client Proiect #30 | _88
MatrixBlank Water
CoLlection Date/Timel5-Mar-07 00:00
Receivedl9-Mar-07
CAS Na An ytc(s) Res!k UnitsFlag *RIIL Dilurio" Method Ret:, Prupan.l Anabgd Barch AnalystVohail€ Orgrnic CompoundsVola$le Orqanic Compounds bv SWB46 82608Prepared by method SW846 5030 Water MS76-111 1,1,2-Trichlorohfuoroothane(FreogRL67€1L1 Acetone BRL1rr3-1 r'€rybnitdle BRL7143^2 Benzene BRLt0&E6-1 Bromobenzene BRL74'97'5 Bromochtoromethane BRL71271 Bromodichtoromethane BRL75-2*2 Baornofom BRL7'l{3-9 Bmmomethane BRL78-933 2-Butzr}c,re (MEKI BRL101L51+ n_Butytbenzene BRL13t90{ sec.Butytbenzene BRL98_0&6 lert-Eutylbenzene BRL75'15'0 Carbon disutfide BRLs6'295 Carbon tetrachioride BRLlosscz Chlorobenzene BRL7s-{ro.3 Chloroethane BRL67{fi Chtoroform BRL744r-3 ChlorDmethane BRL95.498 2-Chbrotoluene BRLloHg zlchlorotoluene BRL96-12{ 1,2-Dibromo-3+htoroprcpane BRL12'/H{l-1 Dbromocitoromelhane BRL16W l,2-Dibromoethane (EDB) BRL7+913 Dibromomethane BRL9l5Gi l,2.Oichtorobenzene BRL541-73-1 1,3_Dichlorobenzene BRLloe&7 l,+Dichlorobenzene BRL73'714 Dchtorodilluoromethane(Faeonl2)ARL75-3+3 l,1_Dichtoroethane BRL107+2 l,2-Dichioroethane BRL75-3F4 l.|_Oichtofoetfrene BRL156-5S-2 cis-1,2-Dichtoroeth6ne BRL'15ffi0-s
tlans-l,z-Dichloroethene BRL78{7-5 i,2-Dichloropropan€ ARL'42-2v9 1,3-Dichtorop@pan€ BRL59+20'7 2,2-Dichtoropropane BRL563-58{ I,l-Dichtoropropene BRL1o061{l-s cis-1.3-Dichtoropropene BRL1006i{?{fans-1,}Dichloroprop€ne BRL10q41-a Ethylbenzene BRL87{s3 Hexachlorobutadaene BRL591-78{ 2-t-lexanone ([/BK) BRL98€2'8 lgopopylb€nzene BRL9+87$ +bopropyltoluene BRL1634{e Methyt tert-but}i ether BRL106-10-1 +Melhyt-2-pentanone(M|BK) BRL7549'2 lrethylen€ chtoride BRL91'2G3 Naphthaten€ BRL10$6$1 rFPropylbenz€ne BRL
r9n 1.0psn 20 0pSI 0.5
pg/l 1 0
ttgtt 1-0
!9/l 1.0
pEl 0.5
lSn 1.0
!g/ l 20
@t tD.o
ttgtt 1.0
pgJl 1.0
psn 1.0
ps/r 5.0lgn 1.0pgn 1.0
rsn 2.o
trgr 1.0
!94 2.0
l g r 1 0p g t 1 0
ttgtl 20pg/r 0.5
t sfl 0.5
l.rs/l 1.0ps4 1.0
! s / l 10
Ug/l 1.0
ug/r 2.0
tsn 1.0pSn 1.0pSn 1.0
!S/l 1_0
!g/r 1_0ps / r 10
Mt 1.0
t)glt 'l.0
t/g/l 1.0pgl 0.5p!,n 0-5
!g/l 1-0
lgr 0-5
|l9r 10.0pg/l 1.0
vgt r.0psfl 1.0
!s4 10.0pc4 5,0
ldl 1,0
l d l 1 0
1
1
1
l
l
1
1
1
1
1
1
1
1
1
1
1
1
1
I
1
I
1,1
1
1
1
I
1
1
1
1
1
1
I
1
1
1
1'|
1
1
1
1
1
1
1
I
1
I
1
Sw846 82608 21-Mat47 21-Ma,-ot 7031185 ek
Thb ItboratoA rcport it ,tol tdljd wdhoat dd aaihorir4d signusre on tlc covq pager Reporrrbte Detectioo Limit BRL = Betow Rwrting Linir Page 89 of 152
Page 479
Sample ldetrtificationTB-IsA59464-18
Client Project #l0r-88
ManixBlank Warer
Coll€ction Date/Timel5-Ma.{7 00r00
Receivedl9-Mar-07
CAS Na Anabtt6) nas 'RDL Dilut& ' Merhod R.l Preparcd ADaltz,.t fulch Anott$l
Vohaile Olgrnic Compounds
Volatile Orqanic Comoounds bv SW846 82608P.epar€d by method SW84ti 5030 Water MS100.a2-s Sttrcn€ BRL63G204 1,1,1,2-Tetrachloroeihane BRL7$34{ 1,1.22-T€trachlo{oethane BRL127-18-4 Tatacfitoroeflrene BRL108{€-3 Toluen€ BRL87Si{ 1,2,+Trict orobenzene SRLl2o{2.1 1,2,+Tricfilorobenzen€ BRL71-5s Ll.l-Tridlloroethane BRL79{0-s 1,1,2-Trichl6oethane BRL79{1{ Tdchloro€lhene BRL75{94 Tdchlorofluo.omethaoe (Freon 11} BRL9G104 |,2,lTddtloropropane BRL
1,2.+Tdm€thylbenzeoe BRLt06$7{ 1,3.5-Trimethytbenz€ne BRf75414 Mrryi chlo{ide BRLr33o-2c7 m,p-Xy'ene BRL9$.17{ o-Xytone BRLlosss-g let-ahyclrofilran BRLao-2+7 Ethyt ethef BRL9ea{5{ T€rt-dnyl methytetr€r BRL637-e2n Ethy tert-but/ ether BRLi0&203 Di-lsopropyl ether BRL75$$o Tert€utanol/ butty' alcohot BRL123.9i-r l,4oioxane BRL
|ldl
lrg/l
us/lFdlpdl
!s4|ldl
|rsnpdl
ItgltsIIJqI
!dluElu$vglsrlvglpgilpdl
udlrcnt s4psit
t . 0t . 0
0.51 0
1 .0'1.0
1.0t . 01.0't .0
1_O1 .01.01.01 .02.O1 .010.01,01 .01.0
1 .010_020-0
I
t
I
1
1
1
I
I
1
t
1
1
1
1
I
1
1
1
1
I
I
1
t
SW846 82608 21{nar-O7 21-tnar-07 7031185 ek
Surogate recoveies:1tu404 +B@nofluotobenzene,n37-26.5 Tduene4B
10010295102
7G130 %70-1n %76130 %70rN%
I 706047 4 1,2Obhlo(oelhane44
fiaest7
Thk bhftlarf ,cpott is not eaIU silhort an atdodzd dgnt ,re o8 th. cowr pqe .
' Reporiable D€tEcri,on Limit BRL = B€low R€porti[g Limit Pag€ 90 of 152
Page 480
Volrtile Organic Compourds - Quality Cortrot
Anslyqsl Resutt I lag
Source %REC
Resulr %REC LimitsUnits rRDLSpike
tevel RPDRPD
Limu
Batd 7031185 - SW8{6 5030 Waier MS
Blank fl031t85€LK1l
P.epared & AnEllzed: 21-Mar.O7
1,'l ,2-Tridrlorotdfluoroethane (Freon I l3)
genzene
Bromobenzene
Brornochlorornethane
8{omodicitororneltEfl e
B.onrolom
2€utahone (MEK)
nAutylb€nzene
s€c-BiJtylbenzene
te|l€utylbenz€n€
Ctrbon disulfde
Carhon tet achloride
Chlorobenzene
Chloroelhane
ChloIototm
Chlorom€thane
24hlorololuen€
4-Chlorololuene
l,2.Dibrorno-3-chlo.opropan€
Dibromochloromethan€
1,2{ibrDno€thane (EDB)
Dibrornomelhane
1,2-Diclllorooenzsne
| ,!Didrlorobenzene1,4{ichlorobenzene
ARL
BRL
BRL
BRL
BRL
BRL
BRI.
BRL
BRL
ARL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
ARL
8RLgRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRI.
BRL
BRL
BRL
BRL
BRL
ARL
ARL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
SRL
BRL
BRL
BRL
!gl
trdlpgl
!sn!dlLjs/|!snps/l
|lgl
Lrgl
t (yl
pgn
W/rltgtl
ugrugl!snp$4
ps4
!91
ugl
!g/l
us/ludlllgl
|ls/lpg/l
pg/r
psn
tsrl
trg4
us^yryl
u(yluglusilg€|/l
uElpEr
ugrus4uglpsnuglpdlpsn!Euql!sn!dl
!dl
tsA
' | .o
20.o0.51 .01 .01 00.51 .02.O1 0 01.01 .01 .05.01 .01 .02.01 .02 01 01 .02-00_50.51 .01 .01 01.02 01 .01 .01 .01 .01 .01 .01 .01 .0LO
0.50-5l 00.510.0't _01 .01 -010.05.01_01.01 .01_0
{Freonl2)| , | -Oiciloro€thane
I 2-Dichloroeti'ane1 , | -Dichlorelhene
cis-i,z-Di.* oro€thene
tranE-1,2{)ic* oroef\ene1 ,2.Dichloropropaie
| ,3-Dichloropropan€2,2{)ij|loropmpan€
| ,I .Oidrloropropene
cis-1,lDichloropropene
lrans-1,3-Dinbrcprop€n€
Ethytbenz€ne
Hexehbrob!tadiene
2+lexanone (MBK)
{-lssropyllolu€ne
Meoryl brt-butyl slh€r
+lrsthy]2+€ntanone ([llBK)
Methylene chloride
Naphthalene
Styrene
1 ,1 ,1 ,2-TetEchloroelfiane
Thit llbo.olory rcpod it ,toa vslrl u,ilhour an at!rtorized ngnatarc on tfu cover pzge
' ReDotuble Detection Limil BRL = B€low R€Donins Lmit Page 97 of lJ2
Page 481
Volatile Organlc Compoutrds - Ql|ality Control
Anallrds) R€sult Flag UnrrsSource %REC
Result %REC Limits.RDLSpikel,ev€1
RPD
LiftitRPD
Brtch ru 1l$ . SW846 5030 Wrt€r MS
Bl.nk a?o3 l 185€LKl I
Prepercd & Analyzedr 21+rar{7
1,1,2,2-Tellachlorethane
TekEdrbroethen€
Toluen€'1 2,lTrid orobenz€ne
I P,+TrlcSlorobenz€ns1,1,1-T.idrlorE€thane
1 , | ,2-Tri€filoro€hanel.iibloeth€ne
Tri.fi bronuorom€han€ (F.eon 1 1 )1,2,}Td.nbrwropane
1,2,+Trimethytb€nzerE
1 ,3,STrimethy'b€nzeneViny' cf dlde
m,p-Xy'ene
o-Xylen€
Telrahydofu.an
Etrryl €{her
Tert-dnyl rnethyl ether
Elhyl ten+uryl eti€r
Di-lsopopy{ eh€r
Ted-Eutanol / butyl €lcohol
l,rmioxanQ
Sunogate : 4-Bmnpfl uo@benzeneSu''oga|€] lduene4gSunogste : l,zokhfotuetane44Sunogate : Dlt*onofluorcmethane
LCS aZ031165€5ll
Preparod & AnalFed: 2l -Mar-O7'1 ,1 ,2-Tdd$rokinuoroethane (Freon 1 '1 3)
Adllonilrib
Benzen€
8mlnob€rEen€grotnocibrun6than€
Brcfirodicl{oromelhane
Bsnotoam
BrqrFfir€lfian6
2€ula0on6 (MEK)
n€r|lylb€nz€ne
s€c-ButyG€nz€ne
lert€uty6onz6ne
Carbon di$dfide
Carbon btsd oride
Chlomb€riz€ne
Chloro€$m€
Chlomfofin
ChlotDmohane
2-chb.otoluen€
4thlo{oioluem
1,2{)bronb-Sc$bropropsrF
Diho|ttod orom€then€
1,2-Dbromo€lt|ane (EDS)
BRI.BRLBRL8RLBRLBRLBRLBRLBRLBRI8RLBRLBRL8RL8RtBRLBRLgRL
BRTBRLSRLBRL19.59.844.850.8
21.921.517 .621.122.020.520_521.020.4l7.o20.4n.s22.A16.623-O2't-5r9.520.0m,121.521-517.621.620.6
pclldlpsnpdlpdl
!dl!snusnt8Arc,TEIpcn!gl
tst|lsnusnt'91ps4!Elpglpdl
!dlugl|ldlpsnpsn
!dl!dlrstIrdl|lglpg/l
lrs/l
rs4pdlpdl
tsrugrr9npdl
tjs/|!snpsnpdl
tts/|!dluglttsf,t grl
wl
0.51.01.01 .0t . 01 .01 .01.01-01.01.0t . 01 .02.O1 .010.01_01 .01.01.0t0.020.0
50.050.050.050.o
20_020.020.0m.0m.020.020.020.o20.020.o20.0m.0m.0m.020.020_020.020,020.0m.0m.om.o20.o20.0
99 7&130102 70-1309{t 70-1Wto2 7013t)
110 70.130108 41.1-1178a 7G130106 7&'130110 7G130102 7G130102 70J30105 7G130102 57J,',15185 48.9134102 7G130114 7G130114 7G130s3 7Gr30115 7G130108 70-1309A 56.$ 1,15r00 7G130100 70-1?0108 701301@ 70.13088 70-130108 61-5-142103 7G130
Thi6 bbo.dloty r.port ls ,roa vdld |4ithd.z, .n dud,oriuat slga&A,e on the cova 1ngE.i Reporlabl€ D€tection Limia BRL = Belov Relorting Limir Pag€ 98 of 152
Page 482
Volatile Organic Compounds - Quality Control
Spike
L€v€l
Source
Result
R}DLimit
%REC%REC LimitsAnalyr(s,
Bdch 7031185 - SW846 5010 Wrrer MS
LCS 17031165€S.t)
Prepared & Anallzed: 21 -Mar-07
Dibrowrodl€thane
I ,2{)idrlorobeozene
l,3OiciloroberEene
1 ,4-Dichlorobenzene
Dichlorodifuoromethane (Freont 2)| ,1 .DiJ\loroethane
I ,2-Dichloroeu|aneI ,1-Oichloroelhen€
cis-1 z-Did{oroethmelrans-1,2-Dichloroethen€
l,2Oichloropropane
1,3-Dichloropmpane
22-Dirhbropropane
I .1 Oichloropropene
cas.1,3Di{:hloropropone
t'ans-l,3oichloropropene
Etrylbeozen€
Hexachlorobutadiene
2+€xa.looe (MBK)
lsopropylbenzene
iiethtl lert-butyl ether
4Jt ethyr2.pentafl on€ (MIB()
Melhylene chbride
Naphttulene
StFgne
1 .1 ,1 ,2-Tstachloroethane1.1,2,2'T€trachloroethane
T€u'achloroeth€ne
1 ,2,+Tncfibrobenzen€I ,2,+Tdchbrob€nzene| ,l , l-Triciloroethane
|,1,2-Trichloroethane
Tdc*ioroetn€n€
TrichlorEf @romethane (Fteon I 1 )1,2,$Tnchbropropan€'1,2,+Trimethy'beruene
'l,3,tTrimehylbenzene
Mny' chbnde
m,pXylene
o-Xylene
Tebahydrcturan
Erhy' elher
Ted-€myl rrehyl ethsr
EflVl ted+uv dher
Di+opropyi eth€r
T€rt€utanol / butyl alclhol'l,4.t)ioxan€
S wrog aE : 1 -B.o mo nu o ro be nzaneSunogate: Toluene4gSunogal€i 1,2.Dk'ilorcelh ana41
19.4
20.5
2 2 4
19.8
21.3
20.6
15.2
18.6
21_7
20.o
20.9
19,9
2 1 . 4
1 9 . 1
21.7
23_2
1S.0
21.1
2 1 . 3
19.5't 8.4
1 9 . 1
17.9
2 1 . 3
21.9
2 4 5
20.1
2 t 6
20,5
16_0
2 1 2
2 1 1
20.2
20.5
20.4
22.1
22.7
22.6
2 2 4
44_4
22.7
14.2
18.2
2 1 . 5
2 1 . 6
20.7
162
r93
53.549.415.8
20.020.o20.020.020.020020.o20.020.020.020_020.020.020_020.020.020.o20.020.020.o20_020.020.020.o2 0 020.020.020.020.020.o20020.o2 0 020_020.020_o2 0 020.o20.020020.040.020.o20.020_020.020.02 0 020020050.050.0500
us/ltrgl
!s/lpgl
!El
l.rg/l
!gn
!s/lpgn
!!t l
uglpsn
QC1 lSn
!s{pg/l
Lrs./lpgl
t g/l
ps/l
udlps4!9/l
iiS/lps/l
us/lu9/lps/l
lig/l
ljg,l
t/gl
tjEl
psnpsnp9l
!gnps,4
usllpgl
!s/l
}l91pg/l
!El
lig/l
!glps/l
lr9l
!cnIE!dlpdl
!91!!y1!91
97 70-130102 70,130112 70-13099 70-130106 36.6-187103 70-1309€ 70-13()s3 70-130108 70-130100 70-1301M 70-130100 70-130136 70.130103 70130107 70-13096 70n30'to8 70-130116 8.7-142s5 56.3-131106 70-130106 7013098 70-13092 55.2.12996 70-13090 70-130106 70-130110 70-130'122 70-130lfi) 70-13o108 70-130102 70-13080 70-130106 70-130106 70-130101 70-130102 70-130102 68.148110 70-130114 70-'130113 7G.130112 7G.130111 7G130114 70-13091 70-13091 57 6-132108 70-130108 7Gr30104 70-13081 70-130
45.2-132107 70-13499 7t)E13492 7G134
Ihk labontory pFod h nol wlil wilhod an at thoriaeit slgnaturc on the.awr poge
'Reportable Det€ction Li&i! BRL= B€low Reporting Limir Page 99 of 152
Page 483
Vol.dle Organic Compounds - Qurllty Control
Batch 7031185 - Sw846 50J0 Water MS
LCS a703t185AS
Pr€parcd & Amlyzed: 2l -rdar{?
Su nngab : Afuonofu roront€fhane
LCS Duo ?03llE gsoll
P.epared & Analf2ed: 2l-Mar-OI
1,1,2-Trichlorotriflt oroathane (Frsn 1 13)
Ac.ybnitile
B€nzene
Bomobenzen€
Brornochlorornelhane
&omodi$brornehane
Brcftrolorm
Brornomelhano
2€t/hnon€ (MEK)
n€utytb€flzene
s€c-Buvbenzene
t6t-8!tylttenzene
Carbm disulfide
Carbm btracfibdde
Cldorohonzene
Chltoethene
Chlonrbrm
ChlorDrnelhane
24hlorotolu€ne
4Chlorotolu€ne
1,2€bmft o-3{hloropropan€
Dlbromochlorofir€thEn€
1 zoibrornoetnan€ (EDB)
Dibrcrnom€6lan€
1 2-Di{$lombenzene'l ,3-Dichlorobenzen€
| .4-Oichbrobenz€n€Did{,orodifl uorometrtar€ (Freon12)
| ,1-Di{$lorcetllane1,2-Oidhro€lhane'|
,1-Okl$oro€th€nsci+1,2{)id oroettEne
trans.l,2oichlom€thon€
1,z-Oichbrcpropane
1 ,3oichbmpropane2.2OiEnbmpropan€
I , I Oichloropropere
ci9l,3-Dichloroprop€ne
t-ans-1,3oicf o.op.opone
Elhylb€lEene
tlo€chlorobutadisns
2+l€xEnon€ (MBK)
lsopropylb€.Eene
4-lsopropyttolu€n€
Molhyl brl+utyl eth€r
4-lrethyL2f onranon€ (Ml8K)
li4elhylen€ .*rlorid€
l,lsphthal€ne
fi.o
19.3
r8_2
17.3
19.6
20.6
19.4
19.7
20.2
19.5
15.3
19_7
21.9
22.O
16-0
19.9
r g . 1
1E.6
20.o
20.2
17.6
20.3
10.0
19.6
21_O
18.4
r9.1
19.5
r8.8
17.r
N.2
14.2
19_9
19.6
2 4 6
18.3
20.3
18.4
19-9
20.7
t8.6
1S.6
z).g19.1ts.114.2
16.5
psn
rslt d l!dlttslugtlugrtrdlpdl
$/lFg/lvdlug/lpcnpdl
vslysll
Xyl|tdlrgltrdlpdl
rctp9lpdlpdlpdl
!dlIs/l!gruglt d l|ldludlrgl!sn!s4udlpdlpdl
vsludl!dl
|lgl
ljgl
udl|,gnlr3/lFSnllgl
50.0
20.020.020.020_o20.020020.om.020.020.020.020.020.020.020.o20_0m.020.0m.o20.o20.020.o20.020.020.o20.020.020.020_o20.0m.0m.0m.o20.020.020.020.o20.o20.020.0m.020.020.o20.0m.020.o20.020.020.0
100 7G13t)
s6 70.130 1491 41.1-147 l7m 70-130 29a 7G130 I103 7Gr30 797 7Gr30 598 7{)'130 4101 70-130 498 57-7-151 476 48.9-134 11s8 70n30 4110 70-130 4fio 70-130 4m 70-130 15102 70-130 12100 7Gr30 886 56.9-145 1396 70-t30 Is4 70-130 6100 70-130 0101 70-'t30 788 70-130 0106 61.5-142 2102 70-130 194 70.'130 39A 7G130 4r05 7G130 692 7G130 796 36.&187 1098 7{t130 5s4 7G130 286 70-130 I101 7G130 791 70-130 9100 70ns 49a 70-130 2123 70-1n t0s2 70'130 t1r02 7G130 592 70.130 4100 7Gr30 8104 8.7-142 1193 56-3-131 298 7G130 I'1& 7G130 296 7S.130 2s0 55.2-129 29t 70-130 5a2 70-13/J I
2550252525
25
5050252525
25502525
25
50252525
255025
2525252525252525
5025
255025
Thb bbonlory ftpon k not edid Niahout ad a4thortzcd tlgnatur. on th. @re. Fgc.. ReF6rtable D€tection Limit BRL = B€low Repoding Limit Pa€€ 100 of 152
Page 484
Volatile Orgar c Compouads - Qualitj,Controt
Spike SourccAnalyl€(s) Resulr Ftag UDirs *RDL Lcvcl Result %REC Limjts Rpu Limrr
Brtch 70l l lEs - sw846 5010 water Ms
%REC RPD
LCS Duo (703118$BSD1l
Preparsd & Anatyzedr 21 +tar{7
tFPropylb€nzene
Styrene
1 , l ,1 ,2-Tetrachlorcethane1,1,2.2-T€trachloroethane
Tetrachloroethen€
1,2,3-Trjchlorobenzen€
1,2,+Tridrlorobenzene
I, |,1-Tdchloroehene
1 ,1 ,2-Tricnbroethane
Trlchloronuoromethane (Freon 1 I )1 .2,3-Tdchbrcpropane12,+Trim€lhyibenzene
l,3,tTrimethylbenzene
vinyl chlodde
m,p-xylen€
o-Xylene
Tetsahydrofuran
ElIy' etrcr
T€rt-€nM melhyl ether
Ethyl ted.buty eth€r
Oiisopropyl ether
T€rt€utanot / butyt alcotrct'l
,4-Oioxane
S utqale : 4 8m mofr uorcbe nte n eSqrcgate: TokEne4SS tnogate : 1, 2 - D i ch loro et h a ne 4 4SuEogEIe : Dib toltio fl uoone lha n e
iletrix Soike (7031 1 85.USl I
PtEpa.ed & Analyzed: 21-MaF07
Benzene
Chlorobenzene
l!l.Dlchloroethene
T.iJ orc€tlEne
Swwate: + Bro zmfl @ mb e n ze n aSltarogale: Tohtene4SS u rraga le : l, 2 - Dktl lo roel h a ne4 4S u nqa te : D ibrc m o n u otu m eth a ne
20.0
20.3
22.2
19.5
19.2
19.0
14.7
20.1
19.1
19.7
14.7
1 8 0
21.1
21.9
21.2
19.8
41.4
21.6
17.S
1 4 1
2 0 8
21_2
20.1
162
179
52.149.945.949.7
Sourc€: SA59.l70{l
23.324.82't .523.522349.750_44 7 4495
ps/lpsn
ugrudl!91
ugn!g l
ps/l
!94
trg/r!s/lt9lltrglusn!g l
!dt!g/1!s/lLj(yl
pg/l
tgtl
v9ulylpsntsllu9luglusnwll
20.020.020.020_020.020.020.020.020.020.020.020.02002 0 02 0 020.040.020.0?0-020.020.020.020.0200200so.o50.o50.0500
20.020.020.020.020.050.050.050.050.0
?0.020.020.020.0?0.050_050.050.050.0
r00 70-130 6 25
102 70-130 8 25
111 70-130 I 25
98 70-130 2 25
96 70-130 12 25
95 70-130 1 25
74 f0-130 6 25
100 70-130 6 25
96 70-130 10 2596 70.130 3 25
94 70-130 8 25
s0 68-148 12 50106 70,130 4 25
110 70-130 4 25
106 70-130 6 25
99 70-130 12 25104 70-130 7 25
108 70-130 5 25
90 7G130 1 25
90 57.6-132 1 50ro4 70-130 4 25
106 70-130 2 25
100 70-130 4 25
a1 70-130 0 25
w 45.2-132 6 25
to4 70'130lM 70-13092 70-13099 70-130
aRL 1' t6 70-130
aRL 124 70-130
aRL 108 70-1 30
BRL 118 70-130
aRL 112 70.130
99 7G1m101 70-13095 7013099 7G130
BRL 114 70-13D 2 30
BRL 124 70-130 0 30
aRL 108 70,130 0 30
BRL 119 70-130 0 30
BRL 112 70-130 0 30
98 7Gl3t)101 70-1U95 70-tU101 70-tg
t{atlx Solk€ Ouo fl031'185-Irl$}l) Source: SA59,tZ0.0.lPrepared & Anatyzed: 21-Marfl
B€nz€ne
Chlorob€aEene
1 , l €ichb.o€th€ne
Toluene
Taldlloro€tn€n€
S/ntwate : 4 - Brono nrc robe n zeneSuiqate: TohEne4SsJrno ga E : 1, 2 -D i dl Io rceth a ne 4 4S unogate : Dib rc mon rcroneth a n e
Brtd 7m1l$- SW846 s030 Soit (high levet)
23f
24.7
2 1 . 7
23.5
22.3
49.250.747_450.5
p9l
pgn
!q/l
!9/lpgl
!Elrg/luglps/r
!gl
ps,l
!g/ltlgJl
!g l
rcl!g/l
!s,4!sn
Thk lal0rotary rcport is nol wld wilhaar ai a!rtodast signtdtrc oa the coter Fge .
a Reportable D€tection Limit BRL = B€low Reporting Limit Pase l0 l of 152
Page 485
Volatile Orgrnic Compounds - Quality Control
Br.ch 7031ttlt - sw8,t6 5030 soil (high level)Blen* 17031180€LKl)
Pr€pared & Analfred: 21 -llar47
1 ,1 ,2-Tnd{oroffiuoroethane (Freon 1 1 3)
Acrylonilrfle
Benzen€
Bromochbromethane
Bromodid oro,nethane
BrorElorm
Bromon€han€
2€utanorc (MEK)
rFBulylbenzene
sec-gutylb€nzen€
t€rt-Bu\lbenzene
C€rbon dlsutfid€
C€rbon tehad|bride
Chlomhenzene
Chbro€thane
Chlo|obrm
Chlorornelhane
2{hlorotolo€neil-Chlo.oto|uen€
l,2.Dibiomoj-drlorcpropan€
Dilbrornodbmdetlran€'1,2-Oibromoehan€ (EDB)
Dlkomomethane
1 Joichlorobenzene1 ,3-Dichbrobenz€ne1 ,4.oichlorobd|z€neDicf*omdiffuorornofi ane (Freonl2)
I,I-Di{r oroe[tane
I ,2-DiibroetEn€1,1€ichbrc[Ene
cis-l,2.Dichloroetherle
transl,2oichloroeth€n€
| ,2-Okhlo.op.opan€|,loit oropropEne
2,2Oi* oropropane
1 ,1 Oichbrwropene
.js-1 ,+Dichlo|lpmp€n€
lrans.l,3oichb.opropene
Ethy&enzens
Heiacl{orobulsdiene
2+ler€non€ (MBK)
lsopropyb€nzene
4-lsopropytbluene
lil€thY lert-butyl 6ther
4{relhyf z{€otanon€ (MIBK)
lrethylen€ drloiir€
Naphthal€n€
n+aopylbsEs|e
SVr€ne
1,1, 1,2-Tehechlormthan€
1,1,2,2-T€fudtoroothan€
BRL
BRL
SRL
BRI
8Rt
BRL
ARL
SRL
ARL
BRL
8RL
BRL
BRL
SRL
BRL
BRI
BRL
BRL
BRL
ARL
BRL
8RL
BRL
BRL
BRL
sRtBRf
BRL
BRL
BRL
ARL
BRL
8Rt-
BRL
BRL
BRL
SRL
SRL
BRL
BRL
BRT
BRL
ERL
BRL
BRL
8RL
BRL
8RL
SRL
BRL
BR,L
BRL
pdks
!dksfldksrcftsrrs^o!sftspdksudr9usn(s!g/kg@ksrgksPdkgudksps/kslsiks!sftspdlg
!drsrdkswr(gpErlspdkspdts
1 .020.01.01-O1_01.0t . 01 .02.O10.01.01.0t . 05.01.01 .02.O1 .02.01.01.02.01.01.0
ldr€ L0
udl€ 'l.0
IdfiS 1_0ps/€ 1.0
lgxg 2.0
tglq r.0
ldks |.o
ldr€ 1.0
lgr(g 1.0
rrdks 1,0psikg 1.0
UqtS 1.0
ldxs 1.0
ttgks 1.0
FSftS 1-0psrlq 1.0
tdtg 1.0
lrgftg |.0
ldkg 10.0ggrq 1.0
ldks 1-o
rdkg 1.0
FdkS 10.0pC4(9 10.0pgl€ |.0
Itglks 1.0pdkS 1-o
lrgikg
Pdllg
1.0t.o
Thb labraloo Eport ls ttd tditt utthoU on aadtorizd stgaagE ofi ahz crver Fge.+ [email protected] Derecriofl Limit BRL = B€tow R€porting Limit Page 102 of152
Page 486
Volatile Organic Compounds - Qualiay Coltrol
Arlalyte(s) Resuh Flag Units
%REC%REC Limits. RDL
Spike
l,ev€l RcsultRPDLi'nitRPTJ
Bahh ?031189 - 5118{6 50J0 Soi l (h igh teveu
Slank {7031t0!I.BLK1l
Prepared & Anatyzed: 21-Mar{7
Tehaciloroeth€ne
Toluens
1,2,$Irichlorob€nzene
1,2,+Trichlorobenzene'1 .1 ,1 -Ttichklro€than€
1,1,2-T.ichloro€thane
Trichloroethene
Trichlorolluoromeft ane (Freon 1 1)1,2,lTrichlorupropane
1,2J-Trinethylbenzene
1 ,3,$Tdmetnylb€nzeneVinyl cnlorid€
m,tsXylene
Tetr$ydrofuran
Ef'yl ether
Ten-amyl ncthyl ether
Elhyl tertnuv elhe.
Di.isopropyl efier
T€rt-Butanol / butyl alcohol'1,4-Dioxane
Chlorobenzene{5
1,4-Oichlorobenz€ne-d4
S utrog ale : 4 -*o mofl uo tobe n zeneSuftogate: Toluene-d8Sutog ate : 1, 2 -D i c h lo roetha ne 4 4Suft og ale : D ib mmo ll u oro m e th a ne
LCs f'031-t89€S
Prepared & Anal)rz€d: 21 -Mar{7
| ,'l ,z-Tricilororrinloroethane (Freon I 1 3)
Actylonitflle
Benzene
Bronoafilororhstnane
Blolnodidrloror.flehane
Bromoform
Saornomethane
2€ubnone (MEK)
n€ulyhenzen€
s€c-Butylbenzene
tert-B0tylbenzen€
Calbon disulftde
CElbon telracfibnde
Chloaotlenzene
Chloro€'1ene
Chlomform
Chloromelhane
2€trloroiolu€n€
44rlorcloluene
l.z.l)blomo3drloropropan€
BRL
8RL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
ARL
BRL
ARL
ARL
BRL
30_o
3 0 0
3 0 0
32.230.232.8$_4
20.7
2 1 6
23.1
18.8
2 1 . 6
20.2
20.8
2 3 0
19,1
20.6
1 9 3
1S.7
20.3
20.8
1 9 . 1
20.8
19.9
20.s19.920.320.42 t . o
!s/xsgEKg
ugKsFgIKg
!q(9psrKs
p94(s
LiS/kg
LjgKs
ug/Kg
t g/kg
ugxsp9Kg
!9/r(gLis/Ksp!yKgpg/kg
rjgxsuEksUEKg!gr(gps/kspg/KgpE(g
!s,Kg!gl(sugftspgks
ugKsudkspg/ks
LIEKSt/g/x9psft9
Pgkspdks
!9Kgpg/|(9
!!yKgpsfts
t gKg
t S/kg!gKgFS&Spqk9
!sftsg/ks
!s/ks!gKsygKg
l 01-O'1 01.01 .01 .01 .01 0'1.0
1.01.01 .02.O1 .01 0 01.01 .01 .01.010.020.0
30-03 0 030.030.030.0300300
20_o20.o20.020.o20.020.020.020.020.020.020.020020.020.020.020.020.020020.02 0 020.0200
u.1 50-200
76.5 50-200
85 50-200
107 70-130101 70-130109 7G130101 70-130
104 7G130
108 3 31-159
116 70-130
s4 70-130
108 70-130
101 70-130
104 70-130
115 70-130
96 50-140
103 47.7-127
96 70-130
98 70-130
102 70-130
104 70-130
96 70-130
104 70-130
100 55.9-135
1M 70-130
100 70-130
102 70130
102 70-130
105 7Gr30
Thit hboralorr repod is trot ytlid vithoat on adhonzed slgnda,e oa the .atet page
I Reporlable D€tection Limit BRL= Below R€poning Linit Page 103 of152
Page 487
Vol'ailc Organic CompouDds - Qurlity Cooarol
Anslyt{s) Result Flag
SPike*RnL lrvel
SorEce y.REC
Result %REC Lin bUnits RPD
RPD
Limit
B.rcl 703118' - SW846 5030 Soit (high tevel)
t9s_tr93!L9935.!lPr€Fred A Anal}.z€d: 21-[,!ar-07
Dibrom€hbrom€lhane
l,2oibronoethane (EDB)
Oabromoin€lhane
I ,2oidrlorobenzene| .3-Dldrlorcbenzene| ,+Dii* orob€nz€ns
m.521.5
2r.220.420.520.120.214.?20.917.620.018-419.919.917.3r8.62 0 120.1m.,rm.3
19.220.322.319.619.019.019.221.7
19.01E-5
20_219.321.8rg .1ts.325.1N.720.41S . t40. I2 r , 123.E20.92'O2r.921.12@
rgr(gpdlqgpsfts
lgkstl/l€ps'xg
!gxs!gt€
usiksps/ksps/Bst'dts!gts!crks!gkg!dxsudkst,9Kg
|lgKs
uslksrgftsugftslrBftspExgvsikgusiks!sftsps/xgpsag
Fdkspgrspgftg
Fdkgps/ks
Fdkg
!dl(g
!g/kS
!gn(S
udts[9K9
ugftsrs/ks!s/kgpgn(sudksldkspsnq
wr€!cftsrdks!dkspgl(9
20.020.o20.02().020.o20,o20.020.o20.020.020.020.o20.020.020.o20.020.0m.020.0m.020.0m.020.020.0z).020.o?0.020.020-020.020-020.oz).020.0m.o20.020.020.020.om.0m.020.020.o40.020.020.020.020_o20.020.o2U)2m
72-12570-1307Gr307G13()7G13070-'t30
102t08r06102102100
I ,1-Didrloroethane1,2-Di$broethane'1,1-Olchloroethene
cis-1.2{)icfi loro€th€n€
t€ns-l,2oidloroethane
1,2-Dichbropmpane
1 ,3-Oidbmpropans2,2{)ichlorop|opsne
1 ,1 Oichbrop.op€ne
cis-1.3-Dichloroptopsn€
tlans-1,3oichloroprwene
Ethylbenzene
Hoxachloroduladiene
z+lexenon€ (MBK)
lsopropylbenzene
4lsoplopy4td|Ene
UetM !6n-buvl €ttl€r
4-M€f ryl2{€ntanone (MIBK)
Metlry'ene ailodde
Naphhalene
stren€
1,'1,'1,2-Tetrad oroehane
1,1,2,2-Tetrad orcethane
Tet"achloroelh5i€
1,z,}Tridrt .lbenleite
1 .2,+Tdd$robenz€ne1,1,1-Trichloroethane
1,1,2-Tichbroehane
Trichloaoehen€
Trichlorofluolome$an€ (F.eon 1 I )l,2,STrichlo.opropdn€
1 ,2,+T{ime$ylbenzefe
1 ,3,$T.im€|f|Ybel|2en€Vlnyl drlodde
m,Fxylene
o-Xylen€
Tet"ahydFfuren
Etlryl ether
Tert-aftyl rlothy' €tt*r
E{V te(-hnyl other
Oi-isoprooyl ad€r
Te.t€utand / bdyt atcohol
1,+Dioxane
(Freon12) '101 42.3-19094 70-r3o104 70-1308B 7Gr30100 7G130s2 7G130100 70-.130100 ro-1986 70-130q) 7s.130rQo 7G130100 7G130100 7u130102 7G1X7108 7G13096 7G130102 7Gt3o112 7G130s8 ,t8_5-127
95 70-13095 70-13)96 70-130108 7G130113 70-130112 70-13095 70.13002 7G.130r12 70.130101 7G'130!6 7G130r09 7G13096 7Gr 3096 66.5-1441m 7Gt3()104 7G.t30102 7Gt309G 70-130100 ?G130106 7G130118 70-130104 64.$.123110 70-130110 70.130106 7G130r00 70-130l0O ,1G134
ThB lttatuloty rqo.l,s aot ezltl Nihoa a, a.tlerid,tignetu.c on ih2 cor,t poge.
. Reporhblc Det€ction Limit BRL = Below R@orting LiEir Poge l(Xof 152
Page 488
Volatile Organic Compounds - Quality Control
%R-ECAnaltle{s) Resuk Flag Units *RDL L€vet Resutt %REC Limirs RpD l_imu
B.act 7031189 - SWA46 5030 Soit (ftigh tevet)
Spike SoDrce
LCS ff031189€S
Pre9a€d & Anal]rred: 21 -Mar{7
Fluorobenzene
ChbrotEnzene-d5
1,4-Okft lorob€nzen6.d4
Su nogale : 4 4rc mon u orc b e n ze neSurogale: Toluene4SSutlog€le: 1, 2aichloroethane44S mog ale: D i b ro no fl u o ro m e t h an e
LCS Oup ?03llag-BSOI)
Pr6parEd & Anal].zed: 21-Mar-07
1 ,1 ,2-Tdchbrotrinuo.o€thane (Freon 1 1 3)
Acrylonfie
Benzene
Bromochlorohletlane
Brotudichloaomelhan€
Brooroforrn
EronEmo[1ane
2€uhno{e (MEK)
n€u@eizene
sec-Bull/lberEme
terl€uty'benzene
Carbon disulfids
Carbon tetsc* oride
Chlorobe$zene
Chloroetian€
Cl oroform
Chloromethane
24hlorolol0€ne
44hlorololuene
l,2.t)btomo-3drloropropane
Dibiomochlorom€tf|ane
1,2-DbtornoetwE (EDBI
Dlbromornehane'l:-DiJ|lorcb€nz€rc
I ,:|-Dicuorob€nzene1,4-Oict$oobenzene
Did orodifl uorom€thane (Freonl 2)t , t Oicttoroettlane
|,2-DicHoroehane
1,l-Did oroethefle
d91 .2oichloroelhene
hEls-1.2{idtloroefhene
1,2-Dlc oropropane
1 ,Soiddoroprcpane22Jirtlloropmpane
1 , I -Didrloroprop€ne
d+1 ,$Dichloropropen€trans-1,3{ichloropropene
Ethylb€nrene
tlexac{ orobutedien€
2+lex8tEne (MBK)
30.0
30.0
30.0
32.229.631.630.6
1S.6
19.5
2 1 . 6
1 4 2
20.0
1 9 . 1
20.2
22.5
19.4
16.8
17.9
14.7
19.4
1 8 . 1
19.0
18.9
19.7
1 9 . 1
18.4
19.8
20.6'19.8
20.9
20.4
r8.7
1 9 . 7
1S.0
1 8 5
18.3
1S.S
17.4
19.0
r7.9
19.1
18.6
16.3
1 6 . 3
19.2
1 9 . 7
19_2
19.6
!s/ksps/ksJ.igK9
!9KStl(!KgtjgKss/ks
tls/ko
l.rgKs
!g/Kg
ug/K9
Lrs/Kspgt,<g
!g/rq
wxsvg/Kgug/rq!s,Kststxsl.,g/K9wl(gt s,xspgKq
lrs/Kgwxsps/ks
ug/KgtrgK9t g/Kgpg/x9pgtK9
!dksIS/KSps/K9
ug/rcr.igKs
wKs
!gKg
Ll9Kgpg/Kg
udksps?Ks
trS/kSg/K9
!gKgus/kg!qkgps/ks
FdkSpgks
30.030.030_0m_0m 0300m.0
20020_020.020.020_020D20.020020.020.02 0 02 D O20.02002002002 0 0m.o20020020.o20020_o20.020.o20.020.020020_020.D2 0 02 0 020.020.020.020.020.o20_o20.020.020.om.020.0
98
s8108
91
100
96'lo1
112
97
u90
94
97'r01
90
95
94
98
96
92
99'103
99
104
102
94
98
95
92
92
100
a7
95
90
96
93
82
92
96
98
96
98't06
r05 5G200s9.6 50-20098_3 50-200107 70-13099 70-130105 70-1fi102 70-130
70-130 6 253.31-159 10 5070-130 7 2570-130 3 2570-130 A 2570-J30 5 2570.130 3 2570,130 3 2550-140 1 50
47 7-121 20 5t)70-130 6 2570-1N 4 2570-130 5 2570-130 3 2570-130 6 257G130 9 25
55.S135 6 5070-130 E 2570-130 4 2570-130 10 2570-130 3 2570.130 2 2572-125 3 5070,13D 4 2570-130 4 2570,130 A 2570-130 4 2570-130 s 25
42.3-190 I 50t0-130 2 2570-130 4 2570-130 1 2570-130 5 2570-130 2 2570130 4 2570-130 7 257G130 5 2570-130 1 2570-130 4 2570-'f30 2 2570-130 470-137 4 n70-130 2
Thb labotuotf Eport ir not valid wirhotd an otrtodzed signattare ott lhe cover page.
a Report ble Detection Limit BRL = Below Reporting Lirnit Pas€ 105 of 152
Page 489
Volatile Organic Compounds - Qodity Cotrtrol
Spike
Bahb ?031189 - SW846 s030 Soil (high t€vet)
LCS DUD ?0!1189-BSD1l
Prepa.ed & Amtf.6d: 21 +rar47
lsop.opylb€rEene
+lsoprEpyhol!9n€
ftrethyl tert.butyl €trler
4-tvlethyl-2+€ntafl on€ (MIBK)
tirethyl€ne d\lortd€
Naphtfialene
n-Propylb€rEene
Styrene
1 ,1 ,1 .2.Totrdchlclrelhane1 , | ,2,2-TshachloroetheneTelEchlo(€then€
Toluene
1,2,3-Trid orobenzenei 2,+Triaillo,rob€ruene1 ,1 ,1-Triciloroehane1,1,2-TrichloroothanB
Trichloroethe{F
Trichkrofuoromefhano (Freon I 1 )12,}Tridlloroprlpane
1,2,4-Trim€hytbenz€ne
t,3,ST,ime'|ylb€nzene
Vinyl ct{orid€
m,p-Xy'sne
o-Xybne
T€trahydrcturan
Etiyt ether
Ten-amyl nt€hy' etrer
Elhyl te.t+ury' stherDi-isopropy' eth€rTert-Butand ./ buv atcohol
l,+Dbxane
Chlorobenzeneds
1,4-Dicfllorohen2ro€d4
S urcg ate : +gdnofl uoraf en ze neSu''-oEal€: fotuane4SSu nlj4atd 1,2 D b h I o rcet h a ne4 4S unogab : Abdrc fl uorc m eth me
B.rch t031233 - SW846 5035A Soit (low tevel)
g|enr aTo3lru€LKl)
Prgpar€d & Ansl].ied: 2l-M€r-t)7
1.1,2-Trichlortiiuom€th€ne (Fr€on 113)
Asyh{reib
Benz€'re
Bronob€nz€fle
Broftrdrlounefiane
Aromodidrlo(om6tn€ne
Aroanofofln
Brcmornelhfl|o
2€ubnon€ (MEK)
n.8ulyllbsnzene
s2 70-130 496 7G130 6105 7Gi30 696 44.5-t27 290 70-130 588 7G130 I96 7G130 0105 70-130 3tfti 70-130 6r08 70-1gt 492 76130 3go 7Gt3t) 2104 70-130 705 70-130 69t 7G130 5107 7G130 294 7G130 296 66.5n,|4 0122 7U1T 399 7G130 599 70-130 3u 70-1m 13ss 7Gr30 1r01 7G130 5'fi8 7G130 098 6r.$.123 6105 70-13/J 5iM 70-130 6100 7G130 696 7G130 4114 4$.134 13103 5&200101 5G200r05 5G200106 7o.BAtol 70-1tutos 7G1301m f+lfr
18.3
19.3
2 l . o
19.2
16,0
l f .5
1 9 . 1
21.0
2 1 . 3
21_6
t8.4
1 7 . 9
20.8
19_0
18.2
21.4
1$.e
19.1
24_3
19.8
rs.8'16.8
39.7
e3.6ts.62r.o20.820.019122930.030.030,031.830.23r.630.6
20.0m.020.020.o20.020-0m.020.020.020.0z)-0m.020.020.020_0m.0m.020.om_020-0mo20.040.020.020.0z).020.o20.020_02m20034.030.030-0fi.o30.ofi.030.0
rdksldksvdksPe/kgpdks
!gl€|ldksugtqugrgudrsLjgkg|Islksrdkg9gtSpdks
udks!clq
lrgt(g
!Et(gpcaguqksps/kspdks!dxsPglq
t/dlslrsftst ckoFs/kspgl(srdl(suglkgt srxs|ls^9!dl(gpdkg|ldkstrsfi(g
lrdkgv{et 5.0
rcAgwet 100pgtg $,et 5.0
lgtS trel 5.0
US/kS Yret 50
rur'kg 'ret t0
Igko{et 5.0
trSftSw€l 5.0
!glkg$/€l 10.0
Igl(g Niet 50-0ISftS N/st 5.0
x25255025252525
2525
252525
25
2525252525g)
25
252525
BRLBRLBRLARL8Rr-gRL
ARLBRIBRLBRLBRL
This lsbrttory eport is t ot r'llitt withou at osdtodtj signart c o,. thz coter page .
t R€portrble D€t€ction Lidit BRL = Below R.porring LiEit Page 106 of 152
Page 490
Volatile Organic Compounds - Quality Control
Spike
L€vel
Source
Resull
RPDLimit
%REC
%REC LimitsAnalyte(s)
Batch 70f,1:3J - SW846 5015A So[ {hw lrvcl)
Blank 17031233€LKl)
ftepared & Analyzed: 21-J\,4ar{7
sec€uMb€nzene
{ert€ulylbenzene
Carbon disulfide
Carbon bnachbdde
Chlorokenzene
Chlorc€thane
Chloroform
Chloromelhane
2Chlo.otoluenetl-Chlorotoluene'1,2-Obmmo3-chloropropane
Dibromochlorornethane
l2oibrodoethan€ (EDB)
Dlbrornomsthane
1.2-Dichlorobenzene
t ,SDicnbrobenzene1,4-Drcnbrcb€nzene
Dichlorodif uorometharie (Freon12)
l,lOichlorcehan€
l,2oichloro€thane
1 .1 Oichloroelhen€
cis-l,2.Dichloro€th€ne
tfan+1,2.Dichloro€thene
l,2.Dicfiloropmpane
1 ,3-Did oropropane
2,2.Did orcpropan€
1 ,'l Olthloropropene
cis-1,3-Dichloroprop€ne
tr ans'1,3-Dichlotgpropene
Ethylbenz€ne
Hexachloroburadiene
2+exanone (MBK)
lsopropylbenz€neiHsopropylloluene
Lielhyt led-b'rtyl €th€r
4-lelehyl-2{€ntanorE (MIBK)
M€thy'me dbnde
Naph0Elone
n-Propylb€nzene
SVrene
1,1.'1,2-f et-dchloroe$ane
1,1,2,2-T€trEchloroethane
TetEchlorc€thene
Toluen6
1 2,lTrichlorobenzen€'1,2,4-Tdchlorob€nzene
| ,l ,1-Trichloroehane|.|,2-Tricr oroohane
Tri*{oroetlEne
Trichb.onuommelhane (Freon I 1 )t 2,STrfuhloropopan€1 ,2,+Trtnethy'b€nzene
BRL
BRf
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRI.
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
ARL
BRL
BRL
BRL
ARL
BRL
BRL
ARL
BRL
8RL
ARL
ARL
BRL
8RL
8RL
BRL
BRL
BRL
BRf
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
SRL
SRL
BRL
BRL
iig/(g wet 5.0
!g/kg wet 5-0
lgr'kg wet 25.0
!g/kg wet 5.0pgrkg wet 5.0pg/kg wet 10.0
!S/kS Yvet 5-0
!g/kg rvet 10.0
ug/kg wet 5,0pg/kg wet 5-0
!g/kg wel 10 0
Ugfig wel 5.0
!g/kg wet 5.0
!g/kg vret 5.0pS,4(S,.vet 5.0
!g/kg wet 5-0
ugL/kg wet 5.0
fg/kg wet 10.0
Ug/kg wet 5.0pgr'kg wer 5.0pg/kg wet 5.0pgr'kg wel 5.0
lgikg w€t 5-0
tS/tS rvet 5.0
t/g/kg wet 5,0
ttgL/kg wet 5.0
Ug/kg wel 5.0
tig/kg wet 5.0
!g/kg wet 5.0pg/kg w€l 5.0
pgks ',vet 5.0pgr'kg wet 5O.0
!gI(9 wet 5.0pg,rkg wet 5 0pg/kg wet 5.0
UgL/l(g wet 50.0pg/kg wet 50 0
!g/kq wet 5.0
lgrkgw€i 5.0
Ig/kg wel 5.0
tjg/kg wet 5.0pS/kS rv€l 5.0pgkgwel 5.0
lrgftgw€t 5-0
ldkswet 5_0
Pg/kg',et 5.0
Ug/tg wet 5.0pgr'kg wet 5.0
!g/kg wet 5.0
Pg/kg w€t 5.0
lglqwet 5.0
Ig/Xg wel 5.0
Thh lalotulary repon is not valid withoaa an a./hottzd s,ignalure od tht .ove! page.
* Reportable Detection Limit BRL = Betow Repoding Limit Page 107 of 152
Page 491
Volatile Orgrric Compoutrds - Qudlty Control
AnalyteG) Result .RDLSpike
lllte)
R-PDLimitFlag RPDUnits
Sowre yoREC
R€8Uh %REC Limits
Batch 703123f - SW846 5035A So (tow levet)
glank 1703123€LKtl
Pre9ared & Analfr€d: 21 -Mar{7'l,3,$lrimethF€nz€n€
Vinyl drlodde
m.Fxylene
Tetrahydrofuran
Ethyl ether
Tsrl-emyl m€thyl ether
Ethyl ,e4.buM ether
Di-isopropyl etn€r
T€rt-Butanol / butyl alcohol
l,4oloxane
S u nqate : 44to nnfl uo rcbe n zaneSurogale: Tohtene4SS u nagale : 1, 2. D ich lo tueth ane 4 4S ulw ale : O i b rcmofi uo tomet harc
LCS t7031233€{ )
Preparcd & Analfzed: 21-Mar-07'1,1,2-Trichloroffiuoroethane (Freon 113)
Acrylonirile
8€nzene
Bromob€nz€ne
Bomochlorom€harF
Bromodichlorcoethane
Bromofom
BrofrEmeihane
2€utanone (M€K)
nSutybenzen€
s€c4uty'benzene
tsrt-Butylbenzene
C€rbon disulnd€
csrbon tet-adbdd€
Chlorob€nzen€
Chloroethane
Cldorofofm
Chlomm€flans
24rh,rotolu€n€
44hbmioluene
1,2-Oibromo-3dforopropan€
Dibfomochbrom€than€
1,2-oihromoolhan€ (EDB)
Dibrornorn€than€
1 ,2.t)idlbrob€nzen€1 ,3-Didbmb€nzene'l,iloicnbrob€rE€ne
Did orcdlffuorom€ttun€ (Fr€ont 2)1 ,1{)ichloroethdtel,2oiahloroethen€
1 ,1Oic*lloro€thenecis-'1,2-Didrlo.oeth€ne
rans. l,2oichloaoethene
1 ,2.Dlcfilo|opropene
8RL
BRL
8RL
BRL
BRL
BRL
BRL
ERL
BRL
BRL
BRL
52.052.756.052.0
12.9
18.0
19_1
18.3
1 6 . 5
19.9
20.o
1t -g
15.6
r9.019.4
20.0
17.2
16.0
19.3
r8.318.018.1
18.5
10_3
17.2
18.3
20.3'19-3
19-2't 8-2't8.2
t4.E19.2t7.s17.O,t9.0
r8.5t9.2
pdkS r€l 5.0
Fdkg rsl 5.0
t gts wst 10.0
lgr'kg v/et 5.0
lgkS w8t 5O.0
Ugllg x,et 5.O
Ig/kg egl 5.oygr'kg w€t 5.O
Ugdtg wet 5.0
lgr'kgw€t 5O.0
pg/t€wel 100
yg4€ wetpgr'kg wel
!g/kg wet
lgftg uret
H4kg x,et
!g'l(9 w€t
ldlS i€t
pdkS {€t
!g/kg wet
ldl(g $'st
ldkg wet
UgftS vr.t
Ugr'kg w€t
ugr'kg wEt
lgr'kg wetpqkS wet
t gftg w€l
Wikgwet
Ig/kg wel
[gl!g wel
liS/kS rst
IE?€ w€lpSrlq r4lpS/kg wel
9gkg rv€lpgltg w€l
lrgftg est
ldkS rEt
ldl€ r'/et
ldkS rvot
tgLllg wet
ugLnlg wet
|lgr'lq v',Bt
Hgr'kg wst
|lgl€ wsl
Igt'i€ vret
!gl!g w€t
Ug/t(g wet
|l€/kg w€t
101 70-130IOS 70"13t)1t2 70-1n1U 70-130
r08 70.13064 3.31-15990 7Gr 3096 70-13092 7G13082 7G130100 70-130100 7Gr30g) 5G140fB 47.7-12795 7G130s7 7G130100 7G13086 7G130s0 70-13096 70-13092 55.S13s90 7G13090 70.13092 70-13096 70-13086 7Gr3092 72-125102 70.130s6 70-t30s6 70-130s't 7G13t)91 70-13074 42.3-19096 7G130I 70-130&5 7G13095 70-130g2 70-1?096 7G130
fi_ofi.0
50.0
20,020-020.o$.02t).020.0a).020.020.o20.o20.020.020.020.020.020_o20.020.o20_020.o20_020.020.o20.020.0m.020.020.0m.020.020.020.o20.020.020.o
Thk lab.obry epoA h not salid )rlthour on osdroftd slgEatuE oz thz er.r Fsge.' Reporlnble D€r€ction Limit BRL = Below Repo{ting Limit Page 108 ofl52
Page 492
Volatile Orgsnic Compounds - QuNlity Control
Sprke Sourc€ %REC
70.1303.31-15970-13070-13070.13070n 3070-13n
RPDA-uab'te(s) Result FlaB Unirs |R_DL Level Resulr o/"REC l-imirs Rpfr Limit
B{tch 70312$ - SW846 5035A Soil (low t€vel)
LCs f7031233€S
Pr€parsd E Analfzed: 21-Mar{7
1 ,3-Dichlorapmpane
2,2.Dichloropropane
| ,1 Oachloropropen€
cis-1,3.{)1*loropropene
trangl,3-Oichloropropen€
Et\/b€nz€ne
Hexachlorobuladiene
2-H6)€nooe (MAK)
4-lsopropyftoluene
Lrolhy' brt$utyl elhet
4-lrethyl-z-pentanone (MtBK)
Lr€tryl€ne cibdde
Naphlhelene
Styrena
1 ,1 , |,2-T€tachloro€tnane
1 . t ,2,2.Tetachloroethaneletradiorceth€ne
| ,2,}Td$brobe|Eene1,2,+Trichlorobenzene
1,'l,1-T.idllorcelfEne
| , 1,2-Trij{oroethane
Trichloroethon6
TdJ oiofluororn€hane (Frcon 1 I )| ,2,}Trid$ropropane1,2,+Trimethytbenzene
1 ,3,STrimeftylbenz€neViny' cfioride
m,p-Xylene
o-Xyl€ne
Tetrahydrcfuran
Ethyl ether
Terl.dhyl n€hy' ether
Ehyl hrt+utyl eher
Dl-isogopyletle.
Tort€utanol / butyl €lcohol
1,4-Oioxan€
Su noga f e : #Jro n ofr u orc be nzen eSwrogde: fduen648S,J/'og ate : 1,2 D i ch I oro eth a ne 44Sfi ogate : D lb rcmofl u o @ nelh an e
Lcs Duo ?031233.8so11
Prepared I Analf2€d: 21-t ar-07
1,1,z-Tdcnbroffiuoro€thane (Freon 113)
Aclylonitrile
Benzehe
Erooobeoz€ne
Bncmocilodorn€thsne
B{oanodichlorornethane
19_3
1 7 6
1 9 3
20.4
20.r1S.3
14.6
14.7
1 7 . 7
19.6
14.6
1 6 I'17 2
2 0 3
19.6
18.7
19_7
17.6
21_O'16.7
20.0
1 8 . 8
17.6
20.4
2 1 . 2
19.2
20.5't9.3
19.3
20.1
37.7
18.8
16.5
1S.6
21.O
20.6
18.3
150
189
49.651.849.440.8
20.4
13_2'18.8
19.4
19.2
1E.0
1S.0
lgr'kg w€t
ug/kq wel
Fg/kq wel
ug/to wetpg/kg wet
!g/kg wel
Ug/kg w€t
ugLikg wer
!g/kg wet
UgI(g wet
uS/kS wel
Ug/Kg wstpg/kg wetpg/kg wet
trgL/kg wet
Ug./kg wst
!g/Kg wet
lgftg wet
ug/kg welpg/kg wel
t g/kg wet
!g/ko w€t
ldkg wet
l./g/kg w€t
ugikg wet
!g/kg wel
Ugy'tg wel
ug/kg wel
lgr'kg w€l
ug/kg wel
Pg/kg wet
UgL/kg w€l
ugL/kg wel
Ugy'kg wet
psn(g Yv€t
Ugy'kg wel
ug/kg wet
Ug!4q w€l
Ugy'kg wet
!g/t(g w€t
lidkg v{€tpg&g wetpg!4(g wet
pgkS Yv€t
usrkg lvet
pgy'kg wet
Pgrkg lvet
pgUl(g wet
lSI(g w€l
pgrkg wet
20_020.02 0 020.020.020.020.020.020.020.020.o20.020.020.020.020.o20.020.020.02 0 020020.02 0 02 0 020,020-020.020.020.02 0 040_020.020_020.020.020.0m.020020050.050.050.o50.o
20.020020.020.020020.020.0
96 70-130
8a 70,130
96 7G130
102 70-130
r00 7G.130
96 70-130
93 70-137
74 70-130
88 70-130
98 7G130
93 70.130
u 4a.5-127
86 70-130
102 70-130
98 70.130
94 70-130
98 70-130
68 70-130
105 70-130
94 7G130
r00 7G130
94 70-r 30
88 70-130
104 70-130
106 70,130
96 66.5-144
102 70-130
96 70,'t 30
96 70-130
100 70-130
94 70-130
94 70-130
82 70-130
98 64_9-123
105 70-1f i
103 70-130
92 70-130
75 70-130
94 40-134
99 70-130to4 7G13099 70-13098 70-130
104
66
94
97
96
90
s5
3
1
9
5
50
2525
25
Thb laborutory Epod tr nal vsIU withoa, an aalhorized rtglnuure oa tha covet page* Reprtable Det€ction Limit BRL = Below ReportinB Limit Pase t09of 152
Page 493
Volatlle Organic Comporrds - Quslity Control
Ai|8lytdd Result Flag Uoits 'RDLSource %RECResu.lt %REc Limits
Spikel.evel
RPDLimitRPD
Bract 703t233 - sw846 50!5A soit (tow tcvc0
LCS Dso (70312$-ASD'|l
Prepared & Anel]/z€d: 21-ird-07
Bromotoarh
Eromom€lhane
2€ubnone (MEK)
n-Butylb€nz€fle
sec€uVboruene
terl-Butylberueng
Calbon disllfide
C€rbon tebad oride
Chiolobenz6n€
Chlolo€fl€n€
CHoruform
Ct{oroneth €
24trlorotol$€rle
44hlorototu€ne'1,2-Oibon|o-3d ompropan€
Dlbmmftibmmdhane
1,2-Dibroneth6de (EDA)
Dibromonted1sne
1,2-Oi:hbmbenzene
1 ,3oichbobenzene'l ,4-Oichlorsb€rE€neDhhlnodifrrorcrnetrEne (Fr€on'12)
I,l-Did|brethane,|,2-Dblrloro6thane
1,l-DaC oroeth€ne
d$1,2-Di{* oroethene
Fans-1 ,2Oichbr@then€1 2-Oic*rloro9rooane| ,}Did orcorcpEne
2,2-Di$bmpmpane
1,l-Did otolmpene
cjs-'1,3-Ok$bopr@ene
rans-'l,3oid|bropf opene
Ethylb€nz€no
H€xachhobutadiens
2+exanono (MBK)
lsopropylb€nuone
4lsopropyibluen€
[4€Aryl tedtrty' ether4+ul6{hyl.2t€ntanone (MIBK)
MethMene chbrile
Naphlhelen€
n+roDybel\zorre
Slyrene
1,1, 1,2.Tohac5loro€than€
1,1,2,2-T€treehloro€thane
TetracilorEth€ne
1 ,2.lTridrhroO€nzen6
1,2,4-Trichbrob€nzene
1,1.1-Trichlorg€fiane
1 ,1 ,2.ldchloro€E|sne
r9.6r0.514.8
18.9
20.1
m.817.5
18.1
19_6
17.5
18.5
17.S
1S:
20.4
18.1
18.7
19-0
18.7
ls. l
19.7
14.2
20.0
19.1
18.0
16.S
14.2
1 f . 9
1 9 7
21-1
17.3
r9.5
21.O
19.7
20.3
18,4
14.9
ts.419.519.S
18.0
16.9
19.8
t9.s
m. l19.8
19.3
19-0
tE.8
19.0
18.2
21.8
20-020.0m.om.020.020.020.020.om.o20.020.020.020-020.o20.020.020.o20.020-o20.020,020.020.o20-020.om.om.o20.020.020-o20.020.0m.o20.020020.020-om.om.o20.o20.o20-020.020.020.020.020-020.020-020.020.020.0
513
4
42
07o30
0I
't0
2
326I010
77
2
1s102
13
!g/kg w€l
lgAg wetyg/tg w€l
|lg/l9 Y/et
!q/kg Yret
!d(g vret
lgutg rv€l
Ig/kg rcl
UgI(g r€l
Fgkg w€tpgfl(s wet
UdkS wet
UgLfllg w€ipg/t€ wel
lgAg w€tpgtg wetpdrs wet
lgr'kg wet
tgtkg w€t
Ug/tq wetpgltg welpdkg w€t
tdks wet
ldkg'r/etrcUkg wet
Ug/t€ wel
!g/kg wel
Idrs rvet
FdXS rvet
ldkS wst
rc/kS @l
lgr'tg lr€l
!g||(g w€lpdkg r€tpdks rvetpdkg vret
!g/kg w€t
lglkg welpdtlg rvet
Ug/19 welpdkS wet
ldkg wet
!g/,kg wet
lgll€ wel
t gag w€t
Igltg w€lpgdq wet
FSXS f,,et
|lgL/kg welggltgw€t
ru/t(g w6l
PgAg r€l
9A 7G130
92 5o-r&74 47.1-12r9t 70-130100 70130t04 7G13088 70-13094 7G.13098 70-13088 55.9-135g2 70-130so 70.1m98 70-130102 70-i30s0 70-130g 72-12595 7{t13094 7G13096 70-13098 7St3691 70-130100 42.3-19096 70-13090 7G130€4 7G13091 70-13t)s0 7G13098 70.130106 70-13086 7G13098 70-13010s 70-13098 7G130102 70-130s2 ?0-13774 70-13097 7Gt3t)98 7G130100 70-130s 4€.512764 7G',t3099 7G130100 7G130100 7Gi3099 7G13096 70-13095 7G13096 70.130s4 7G130s5 ?0-130
91 7G130f09 70-13J
5050
25
2550252525
25502525
2525
2525
252525
b
255025
25
502525252525252525
25
25
This l4bo.etuf npod it aot tofrd xt&hotd zn d,adlorkad signdt e or thz @rzr page,
* Reptrbble Detection Limit BRL = B€tow R€portins Lirnit Page I l0 of | 52
Page 494
Volaail€ Orgalic Compounds - Quality Cootrot
Brrch 703t213 - S\r8{6 50t5a S0[ (to!v levet)
LCS Duo fl031233-ASD'|l
Prepsred & Anal}.zedt 21-Mar{7
Triiloroethene
Tdchbronuorom€thane (Freon 1 1 )1,2,3-Trichloropropane
1,2,4-Trinethylb€nzem
1,3,s-Trim€thylbenzene
m,p-xylene
<}Xyl€ne
lotrahydrofuran
Ehy' €thsr
Tert-amyl mehyl ether
Ethyl terl.butyl ether
Di-isopropyl ether
Te{t€utanol / butyl alcohol
1,+Dbxan€
S u nqa t e : 4 - B ronofl u o tobe n z e neSutmgate: Toluene4SS u oog a Ie : 1, 2 -D ich lo rceth a n e 4 4S u toga I e I D ib ro m ofl u orc m eth a ne
Bdtch 70.31291 - SW8{6 50f5A So oow level)
Blant 17031291€LK1l
Pr€par€d & Anal].zed: 22-[iar{7
1,1,2-Trichlomtriff loroethane (Freon 1 j3)
Acrylonitrile
Benzefle
Bro.nobenzene
Erc{nochbronrelhane
Bromodichloromethane
Eromoform
Bromon€lhane
2-Bubnone (MEK)
n-8lllylb€nzene
soc-Butjb€nzene
lert.Butylbenzene
Carbon disulfide
Cerbor lstracnbide
Chloobenzene
ChlorE€thane
Chloroform
Chlorom€f|Ene
24hhrotoluen€lrchbrololuene
l,2Oibromo-3-c}|bmpmpane
Dibromod orom€thane
I "zolbromoethane (EDB)
Dibrqnomethane
1 .2{ictrlo{obenzene1 ,3-Dichlorobenzene| ,4Oichlorob€nzeneI)id orodifl uoromethane (Freont 2)1 , | -Oi:hloroethen€
2 1 . O
1 8 I
23.7
20.2
20.2
21.8
40.3
20.4
18.3
14.7
1 9 1
2 1 . 2
19.1
169
212
52.051.849.149.8
Spikc
20.o20.020.02 0 020.020.040.020.020.020.020.020.020.020020050_050.050.050.0
25502525
25252525502525
2525
p!/kg wel
pg/kg wet
Ug/kg wet
LrgL/kg wer
|lgkg wel
!g/Kg wel
!g/kg w€l
!g/(g wel
Fg/kg wet
lgkg wet
pdkg rYet
PdkS Yret
pg/kg wet
!g/kg wet
lgkg wet
pg/kg we1
Ugr'kg wet
lgKg wslpg/kg wel
!g/kg wet 5.0
!g/kg wel 100
lgkS vr€t 5.0
!g/kg wet 5_0pg/kg wet 5.0
t gr,kg wet 5 0
ldkS Y€t 5.0
!S,xg Yvet 5.0
!S4(g Yrel 10.0
ldkS wet 50.0
riqr'kg wet 5.0
!g/kg wst 5-0
!g/kg wet 5-0
!g/kg wet 25.0
ldkg u,61 5.0
!g/kg wet 5 0
Ug/kg w6t 10.0
pSfl(g v{et 5-0yg/kg wet 10-0
pg/kg wet 5 0
udl(| vret 5.0
!91/kg wet 10.0
!g/kg wet 5.0
t|gLitg wet 5.0
l4r'kg wet 5.0
rcr'kg wel 5.0
Ug/kg wel 5.0
lgr'kg wel 5.0
rgr'kg w€t 10.0
Ygr'kgwel 5.0
t05 70-130 0.9
s4 66.5144 2
118 70t3o 15
101 70-130 5
101 7G.t30 5
109 ?0-130 I
101 70-130 7
102 70-130 I
92 ?0-130 11
94 64 S123 4
96 70-130 I'106 70-130 3
96 70,130 4
84 70-130 11
106 10-134 12
104 70-t3t)104 70-13098 70-130100 f0-130
ARL
BRL
BRL
BRI
ARL
ARL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
ARL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Thb lzbontory EFort ls aat lalu wdhotd on z!flto;zct sig,,ara,? on the cover pale.
' Rep'ortable D€t€ctEn Li6ir BRL = B€low ReDortine Limir Page ItI ot 152
Page 495
Volrtilc Org|nic Compounds - Qurlity Cootrol
Analyte(s) Result Ftag UnitsSpike
LevEl
Source
R€s t %PfC
%RECLimils RPD
RPD
Limil
Batch 7031291 - SW646 5035A Soil oow level)
Abnk ln)s11'l1€LK'll
Ptepated & futaly?€.d: 2-Mu47
1,2{ichloro€than6
1 ,1 -Dicibro€lhe.E
cisl,2-Dict oto€tlEne
lrans-1,2Oichloro€thene'l,2-Diibropropane
I,}{)ic orcpropan€
2,2-Dichbrop,opa|€
1 ,1 Oichbrop.opene
cis-l,3olchloroprop€ne
trans-l,3JichbroFopen€
Ethylbenzen€
Hexehlorcbutadiene
2-H6xenon€ (firgK)
lsopmpylbenzene
4-lsopropy'loluen€
Mehy' tertndyl ethet
4-Melhyl2-pentanone (M|8K)
Methylene chlorid€
N+hlhalen€
Styrene
1 ,1 ,1 ,.T€t-echloroethano1,1,2,2-Tstrachloroelhan6
Tetacftloro€tltone
1,2,$Tri{fibobenzen€
l,z,+Trid orobenzene
1 ,1 ,1 -Tricfibrcathane
1 ,I 2-Tdc*rb.o€than€T.idloro€then€
Trftt orofuorcmsthan€ (Fr€on l 1 )| ,2,lT.ichlotopropane1,2,4-TrimehyDenzsn€
1 .3,STrim€thylbetEenoVirM cf oride
m,FFxyle@
o-Xylsn€
lebahydroturan
Ew sther
T€rtdrryl mehyl €th€r
Etryl isd+uty' €th€r
Di-isoFopyl efte,
Ten-Butand / buv Elcohol
1,+Dioxan€
Sunogai€: l-AmneauonbenzaneSunogalg: Toh@'€48Su''ogale: l, 2ltichb@elhan644S u nogale : Dib MEfl rn @meth a ne
LCS a7rt9l29t€5r)
Prepar€d & Analfzed: 22-Mar{7
| ,1 ,2-Trichlorotdffuoro€thsne (Feon 1 13)
SRL
BRL
BRL
BRL
BRL
BRL
BRL
BRf
BRL
ARL
BRLgRL
BRL
SRL
ARL
ARL
BRL
ARL
BRL
BRL
BRL
aRf
BRL
BRL
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ERL
BRL
BRL
BR|-
BRL
52.757.O51.9
22.3
12.0
!g/tg wel
$fl(g w€t
lgy'kg v/et
UdkS w€t
Fg/t€ wet
$/k0 wet
pdrS w€t
lgr'kg r{!el
Ug/tg w€t
!91(S $/et
pdrq wet
Ig/kg wet
udts lv€l
pglq w€l
lgflqg w€i
|lgL/kS wet
ygrkg wet
pgi l€ wet
lgy'kg $,el
pglq,,tet
ldkS w€l
usn(s Y/etldkS wetrcn€ wetIg/kg wet
ug&g welpdkg wet
tdtg \r€t
lgr'kg w€tpdkg wetpd@ wetpgikg w€tpdkg welpdkg v!,el
!9&g w€r
Io'kg wet
lgLlkg wet
Fgrtg wet
ug/rg wet
Pg,lg wetpgts tvet
ldkg w€t
rdb w€tpgikg wet
!€/kg wetIS/1S welugftg well.rs/xs wol
Pg/kg wst
rcI€ wet
5.05.05.0
5.05.0
5.0
5_05.05 050-0
5.05.050.050.05.05.O5.05.05.0
5.05.05.05.0
5.05-05.05.05.0
10.05.050.05.05 05.0
50.0100
50.o50.o50.050.0
1O5 761mt05 70.130,14 70-1$1(U 70-130
112 7Gt3080 3.31-159
m.020.0
TIth l^borztory rato.l is not voM h'ith46 an o4lho.hd sigr'rtt&re or ahe cowr pag..
r Reportable DeEcrion Li6it BRL= Betow R€gcding Limit P.ge l12 of 152
Page 496
Volatile Organic Compounds - Quallty Control
pg/kg wet
lgL/kg u/et
!g/kg wet
lgL/Kg wet
plyr(g wet
ug/kg wet
ugkg wel
!g/kg wet
LilyKg wet
Pg'kg wet
pgrkg wel
Igtkg wel
Pqfts wel
Ug/kg wel
pg/kg wet
ug/r(g welplyKg wel
!g/kg wsl
LiEKg wel
Lig/kg wel
ugr'kg wel
pgir(g wel
ugikg wet
Uglkg w€t
pgdkg wet
Pq/kg wet
lJgrKg wet
pg/kg wet
Pg/kq ',et
!g/kg wet
!g/kg w€t
pdks wet
Llg(g wet
pdkg wet
pqkS \ /et
pgkg wet
Ig/kg w€t
ldks w€t
ug{xg wel
lEKg wel
pdkg wel
Pg/kg w€t
!g/kg wer
|rgr(9 wel
|lgi kg w€t
tr(ykg w6t
plyKg wsl
Lig/kg w€l
ldkS wet
lgr'kg wEt
pdks wet
ldkS','/et
%REC
Limits
98 70-130'r01 7G13090 70-13094 70-130104 70-1309€ 70-130101 50-14070 47.7-127104 70-13t)s8 70-130101 7{1130106 70-130100 70-130104 70-13099 559-135104 70-130s6 70-13097 70-130103 70-13084 70-13098 72-125109 70-1n93 70-'t30101 70-13096 70-13096 70-13t)112 42 3-190108 70-13094 70,13095 70-130s9 70-130106 70-130105 70.130102 70-13096 7G.130106 70-130104 70-130'r 14 7S130102 7Gt30103 70-13779 70-r 3097 70-130106 7Gt3010t 7G130s6 4a.t12794 70.130108 70-130't01 7G130102 7G130100 70-130e8 70-130112 70.130
SpikeL€veL
i
Brlch 70lI29l - SWE{6 5015a Soit tton teveu
LCS 17031Ar1€.till
Pr€par€d & Analfzed: 22-Mar-07
Acrylonitile
BerEene
Bromob€nzene
Arorho{hlommelhane
Brornodidnloromeu'lane
Brcinobrm
Eronrornelhane
2-Bulemn6 (MEK)
n€utylbenzene
sec-Buty'lb€nz€n€
tert+utylb€nzene
Ca.tton dis'rmde
Carbon t€lEchlorid€
Cl orob€nzene
Chlorcehane
Chbrofofin
Chloromethane
24hbIotoluene
44hlorotoluene
1,2{ibro,mo-3drlompropane
Dibaomochlorom€than€
1 ,2-Dibromo€Ulane (EOB)
Dibromomethar€
I ,2.oiilorobenzenel,3.0ichlorob€nzene
1 ,4-Dichlorob€nzen€Dichhrodftioromelhane (Freont 2)| , | -0ichloroethane
1 2-Dichloro€thane'l ,l -Di€hloroethene
ci9l ,2-Dlflooethenefans-1,z0ichloro€thene
l lOichloropropane
1,3Oicfiloroprcp€ne
2tOicnloropropane
1 ,1 Oichlompropene
cis-l.3.Dichloroprop€fl st-sns-l,}Dichlompropene
Elhylbenzene
H€xachlorobutadi€fle
2+lexanone (MBK)
lsoprogylb€nzene
4-lsopropyholuen€
Mehyl tert-butyl elher
4-l,lethyl-2-pentanone (M tBK)lr€tryl€ne d odde
Naphhalen€
nPropylb€nzen€
Strene'1,1, 1,2-Tetrachloroethane
t , t ,2,2-Tetacfilorc€tnansTebacfiloroelh€ne
1 9 7
202
18.0
1A.E
20.9
1 9 . 1
20_2
14.O
20.9'lg 7
2 0 2
21_2't s_s
20.7
19.8
20.f
1 9 . 3
1 9 4
20_6
16.9
19_7
2 1 . 8
19.8
2 0 2
19.3
1 9 . 3
22.4
21_6
1 8 I'19 0
1 9 8
21.1
21.0
20_5
19.2
2 1 3
20_7
22.9
20.4
20.6
15.8
19.4
2 1 . 2
20.7
19.2
1 8 7
21.6
20.2
2 0 5
20.0
17-6
22.5
20020_020.o20.020020_o20.o20.020.020.020.020-02 0 02 0 020.02 0 020.020.020.02 0 020.020020.02 0 020.020.020.o20.020.o20.020.020.o20.020.020.020.020.020.020.020.o20.020020.c20.020.020-020.020_020.020.020.020.0
Thit laborulory rcpofl k noa vald wirhod oa suthorized signature on the owr pa$e.
* Reporhble Detection Limit BRL: Below R€porting Limit Page l l3 of 152
Page 497
Volatlle Organic Compounds - Qlality Cotrtrol
Analyte(s) R€sult +RDLSpikeL€vel
%RECLimits RPD
RPDLimitFlag Units
Source
Result %REC
Bstch 7031291 - Sw846 5035A Soil (low levcl)
LGS 47001291€S1)
Pr€Fred & Anatyzed: 22-li4ar-07
Tolu€ne
1,2,&Tli;lrkfob€nzene
1.2,4-Tn_d omb€nzene
I ,1 ,1 .Trt(filo.o€thane
I , | ,2-TrichlorD€dEneTri$loroeheno
Tdchtoronuorcmehan€ (F.6on 1 1 )1,2,&Tdchbropmpan€
12,4-TdfiEthylb€nz€ne
1.3,s-Taim€trylbenzene
Vinyl drlodd€
m,p-Xylene
o-Xylen€
Tetrehydrcfuran
Ethylefi€r
Tert-amyl rnethyl €ther
Ethyl bd-butyl e(tl€r
Diisopropyl 6lher
Terl-Butanol / buv atcohol
l,4oioxane
Su Eogate : 4 Bro rpfl u orcbe n zeneSurrDgElej Tolu€no-d8S u fiog a le : t, 2 -DkhloroEtha rc4 4S u fiog ele: Ditno nofl uodn ath ane
LGS Ouo?03t291+SOll
Prepared & AndFed: 22-ltlar-07
|,|,2-Trichlorotriflloroethane (Freon 113)
Acrylo. iril€
Benz€no
ErEmod{Oromehane
Brornodichlorom€thane
Bronofomgrcmomehan€
2Auhnone (MEK)
ftAdy|b€ru€ne
seo8utylbonz€ne
terl-Buvh€nz€ne
Cerbon disumde
C€fton tet'ad odde
Chloroh€nzefl€
Chlo|oetiene
Chloroloam
Chlorcn€thBne
2Chbmioluene
44hbrololuen€
1,2-DibrDmo-3d{cmpropan6
Dibromodrloron€than€
I 2-Dbrornoethane (EDg)
DlbmmoflEthane
| 2-Didlo.obenzen€
19.420.8
19.3
24-721.621.220_020.821 .738.819.417.420.1
22.4m.4r6214147.25t.a5 t . 152.0
21.412.614.620.317.817.420.419.2'ts_ I13.720_720.120.3't8.0'18.8
19.6r7.419.719.419.'l19.921.7r9.t20.318.921.0
20.020.om.020.020020,0m.020.020.020.020.040.0m.020.020.o20.020.020.020020050.o50.o50.o50.0
m.020.o20.020.020_0m.om.020.o20.020.020.020.020.020.020.020.0m.020.020.020.0m.020.020.020,020.o20.0
529I1620
302I
16
6
r 3
2t
25
7
Fdkg v'/et
ug^g wet
ldkg wsl
!g/kg w€t
!g/t(g rrel
trg/kg wet
l.,g/kg wet
lgrkg wel
|Jdko w6l
rcr'kg r€t
Fgr'kg w€t
US4(S YJ€t
ldkg "velldkS rct
!g/lq n€tpgkS 'r/et
lgtkg wst
Pdkg vJel
ldkS $/61
IgL/i(g n€l
t gkg wst
UdkS wetpSlkg wel
lgkg wel
Ig/kg wet
Pgukg w€tqR2
!g/kg wet
Idks v,€l
lrSrkg lv€t
Pg/tg wst
pg/kg wet
lrgkg w6l
Lrgy'kg wot
lgL/kg rret
pSn€ wet
pg/kg $'et
pg&g wel
ugr'kg R€t
pg/kg wet
Pgkg sret
pg/kg wstpgftg wel
ldlS wel
t gr'kg lr€t
lrg/kg wet
ygilq w€tpgts vret
lgr'kg wel
udkS w€lpgdkg w€t
97 7G130'104 70-13J110 70-13096 7G130113 7G130124 70-130108 66.S1{4106 TG13()1(X 70-130104 7Gt30108 7o-t3097 70-13097 70-13087 7G130f 00 u.g-r23t16 70-130'n4 70-130'lo2 7&13081 7G13070 .t{tt34
94 7+1m104 70-1fi102 7G1fr101 70-1u
107 70-13063 3.31-15973 70-130
102 7Gt3t)69 70-13087 7Gt30102 70-13096 7G130s6 50"1406a 47.7-127104 70-130100 70-130102 70-1fis0 7G13(194 70-13098 7G13087 55.913598 7G13098 7Gr3096 7&i30100 7G130108 70.130
72-125102 7G.t309a 7G130105 7G130
50
25252525
50
25
25
258E
g)
25
This r4borabf Epotl h ,rot vaUd withoa an aalhotirij sig darc ott the coyer page,
* Rcporrable Det€ction Limit BRI- = Below Repoltidg Limit Pige I 14 of 152
Page 498
Volatile Organic Compounds - Quality Control
Anrlt'tds) Resuft RPDUoitsFlae . RDLSfrike
L€vel
Sourc€
Result %RtrC%REC
Linits
RPDLimit
Brtch 703t29r - Sw846 50t5A Soil (lo$ t€yeD
LCS Ouo 17031291-a.SD'l)
PreDarcd & Amlfzedr 22-Mar-07
t .s-DichbrobeDzene1,+0d omb€nzene
Dlchlorcdin!oromethan€ (Freonl 2)'l,l-OiJ oroelhane
1,2-DiJ oruethans
1 ,'l 'Dinbroethene
cis-1,2-Dichlo.oelhene
trans-l,2Oichloroethene
12€kt oropropane
l,SDid oropropane
2,2-Didtbr@ropane
|.r-Di{* oroprop€ne
cis-'1,3-Dichloropropene
trans-1,3-Oichloropropene
Ethylbenzsn€
Hexact orobutadiene
2-He)6none (MBK)
lsopropylbenzene
4-lsopropyltoluene
lll,ethyt bn-butyl ether
4{vlelhyl-2-p€nlaoone (MtBK)
Methylene drlorile
Naphthalene
n+mpldberEene
Styrene
1 ,1 ,'l ,2-Telrachlo.oethan€1,1,2,2-Telrachloroelhane
l,2,STdcnbrobenzene
1,2,+Tri{:trlorcbsnz€ne
I.1, l-T.ichloroethane
1 , | ,2-Trichloroehane
Trkiloroff uoromehane (Freon 1 I )| 2,&Tricitoropropane12,+Trimetlylbenzeoe
l,3,5-Tdhethylbenzene
\rrM d 6id€
m.D-xylene
o-Xylene
T€hahydroturan
EUrt 6the,
T€rt-€myi methyl elher
EthY t€n-buv €ttPr
DLboprosy' elher
fert-But€flol / butyl alcohol
t,4-Dioxsn€
I u fi Egale : +&o n1o fl u orcb e n zen eSunWa'P.: Toluene4SSunWaE : 1,2 -Dichloroethane44
Sunwa b : A b rcrnon uo a n elh e rc
207
204
2 2 4
20.1
1 8 0
1 9 9
18.6
2 1 3
20-4
19_8
18-1
1S_5
21.4
?0.9
20.5
20.2
14.0
19.2
2 1 A
i9.a
1 8 . 9
18.4
20.5
20_2
1S_7
20.9
19.0
20.4
1 9 3
2 0 9
21.1
1 8 . 6
2 t . 4
22_9
20.1
21.2
20.4
r9.9
18.4
3S_6
1 8 . 9
17.3
20.0'18 5
2 1 . 5
15.2
175
202
19.852.048.549.8
pg4(g wsl
pq(g wet
lsftg wet
Pgrkg wet
pS'kS t^rt
trgkg wet
Pg'ikg wet
l]Erq wet
pg/kg wet
!s&g wet
ldkg wet
uEr(g wet
!g/kg wet
us.4€ wet
!g/rq w€t
!q/kq wet
!g/kg wel
lgikg w€l
!g/kq wet
lgr'kg wel
pgi kg wel
lEkg wet
lgkg wel
ugftg wel
irg/kg wel
!g/kg wet
!g/kg wet
pglkg wet
Pg/kg wet
!g{(S \^/et
pgn(g wet
Lig/r(g wet
tig/kg wet
pg/kg wet
pg/kg wet
lgyrlg wel
ugr'kg wet
pgl(g wel
Fg/tg wet
!g/kg wet
!Er(g u/et
!g{(g '4et
pSI(S w€t
pgkg w€t
ug/Kg wet
!g/kg w€t
!g/kg wet
pgkg wet
UgL/kg wel
!g/Kg wel
!g,'kg wetpg,rkg wet
1D4 70-130102 70-130112 42.3-190100 70-13090 70-130100 70-13093 70-130106 70-130102 70-130s9 70-13090 7G13098 70.130r07 70-130104 7G't30102 70-130101 7G13770 70-13096 70-130109 70-1309e 70-13094 48 U12792 tO-130102 70-130101 70-13098 70-130104 70-13095 70-130102 70r 3096 70-1301o4 70-130106 70-'t 3093 70-13t)107 70-130'r14 7G130100 66.t144106 7G130102 70-130100 70.13092 70-13099 70.130s4 70-13086 70-19)'r00 64.912392 70-130108 70-13096 70-13088 7&130'101 4G134100 70-130104 7o-1N97 70"19)100 70-19
2D.O20.020020.020.020.o20.o20.020.020.o20.020.o20.020.020.020.o20.020_o20.020.020.020.020_02 0 02 0 020.o20_020.020.o20.020.020.020.o20020.020.020.020_o20.040.020.024.020.020.020.020.020020050_o50_o50.0ffio
8
6
0
I
5
6
0
3
3
8
3
I
0
2
1 2
1
3
5
2
2
6
0
4
I
I
I
0
3
5
6
I
0
2
'16
2
3
I
0
5
6
I
36
25255025252525252525252525
25502525252550252525
25252525252525255025252525252525502525252525
Thk taboraory rcport b ,tol vdU tellho.,l an auhoirztt signzture on lhe cotpr page.
* Reportable Detection Limit BRL = Below Repodng Limit Psge I 15 of 152
Page 499
Extrrctable Petroleum Hydrocarbons - Qudity Cobtrol
Analyte(s) Resuit .RDLSpikeIavel
SouaceResult
%R-ECLimits RPD
RPDLimiaFlag n/,wcUnits
B.rct 7031160 - SWM6 3510C
A|ank 17031ler€LKll
Pr€pared: 21 -01a.{7 Analyzedi 22-Mer47
Gasolin€
Fuel Oil f?
Fuel Oil *4
Fu€lOi l#6
Moto. Oal
unidenlifcd
Ohe. Oil
Total Pet oleum Hydrocarbms
C9436 Aliphalic Hydrocarbons
Sunogale: t -Chlot@dedecane
LCS f7031160€S1)
Prepared: 21 -l\rd-07 ArElyzed: n-Met4l
CgC36 Afi phalic Hydroc€bons
SufiWate: | -Chlotooctactecl,ne
Brtch ?03116? - Swa46 3SS0B
Ahnk (7031167€LK1r
P.6pared I Analyzed: 2t-lvlar{7
Gasoline
FuelOi l#2
FuslOi l#4
FuelOi l#6
Motor oil
Unidej$ned
OtherOil
Total Petrolsum Hydrocarbons
C!,.C36 Aliphatic Hydrocerbons
Su.'ogate : 1 -Chlotoocladecane
LC€ 1706fl67€{t1}
Pr€pared & Analyzed: 21-Mar-07
CgC36 AliphBlic Hydro€rbofl 6
S u nrpate : I 4 hl otooctadecan e
Dublicat€ 470:li I dl-OUPI )
Pr€pa€d & Analfzsd: 2t -Mar{7
Gasofn€
Fu€l Oil flz
FuelOi l#{
Fuel oll #6
Mobr O{
Unld€r if€d
Oh€r Ofl
Tolal Petoleum Hydrtredons
CgC36 Allph€ltc ttydroc{bons
Sr/'rogate l{'h,j}rEd.adecane
lretrlx $rlt. {7031167{|ll)
Pr€pared & Analfzed: 21-MErry
C9436 Aliphalic Hydroca.bons
BRL
BRL
BRL
ARL
BRL
BRI.
BRL
BRL
BRL
BRL
0.04i0
1 . 4
0.0520
BRL
BRI
ARL
BRL
BRL
BRL
SRL
ARL
BRI.gRL
2.fi
84.6
3.74
Sau.ce: 5459464.07
BRL
ERL
sRt_sRr_gRL
BRL
BRL
BRL
BRL
2.08
Sourcs: 3459484{l
mgl 0.05mg 0.05rngl 0.05mSI 0.05mdl 0.0sntg/l 0.05rngl 0-05mgn 0.05.9n 0.05nEn 0.05ordl
ngl O.05t|u
mgftg wE[ l3-3(€lkgwet 13.3
fl€lkgwel 13.3
rngltgw€t 13-3
ttlSllg Yrst 13.3
r€/kg wEt 13.3
mgrkgwst 13-3
nE/kg we( 13.3
mgr'kg w€l 13.3
mgikgw€i 13.3
rngl(g sr€t
.trgftow€l t3.3
mgrkg rN€l
nSftS dry 18_9
.nSftS 6y to.S
d€tkS dry 18.9
lr€rkg dry 18.9
mgl(gdry 1&9
rEr'kg dry 18.9
nS/kS dry 18.9
nEftSdry 18-9
rtg/kg dry 18.9
nSftgdry 18.9
nEukg dry
mSftodry 14,6
o.oflo
|.40o.tR00
4+140
60.120&)-tm
86
r00104
93.33.et
40.141)
60-12060-1m
91
fi2
BRLBRLARLBRLBRLBRLBRLasu_BRLBRL
505050
50505050
79.6
,ll)-ln
5G15078BRLlo2
This tabordaucpul is twt volid sAhoat at oathotized sig,'Flfrtre ad ahe ca,!e, page.
* Repdbbl€ D€t€ction Limit BRL = Below ReponioC Limir Psgc l16 of 152
Page 500
Extractable Petroleum Hydrocarbons - Quatiqv Conarol
Analyte(s) Result Flag UDits
%REC%RtrC Limits*RDL
Spike
I-evcl Result
RPD
LimitR}D
Brtch 703116? - SW8{6 35508
'|.rflxspikD17031t67-frsl) Sourcc:5A5946/147
P.epared & Analyzed: 21-Mar{7
Suflogste: I,Chtorooctadecane 3.Sl
i|grrfx Soike Ouo fl031167.MSD11 Sou.cs: 5A59464{7
Prepared & Anatt"edr 21-Mer-07
CgC36 Aliphatic Hydrocarbons
S u ttogale : 1 -C hl oroocl ad e c a ne
B.tdr ?031283 - SW846 3ss0B
glenk tm3t283€jLt<11
Prcpsred: 22{rar.07 Anat}zed: 26-Mar-07
Gasollne
FuelOi l#2
FuelOilrr4
FuelOi l16
Molor Oil
Unidentifted
Olh€r Oil
Tohl Pekolellm Hydrocadons
CSC36 Aliphatic Hydro€bons
Suflngate : 1 -Chloroactadecane
LCtf7031283€S
Preparcd: 22-{vlar-07 Analr.edr 26.l ar-07
CgC36 Atiphatic Hydrocarbons
Sunwele : 1 -Chloroocladecane
Prcpa/€'d 22-Mat47 Anegzed 2&t!1afi7
Ga6olin€
FuelOi l#2
Fuel Oil#4
Fu€l Oilt6
Motor oil
U. d€ntified
Othor Oil
Totd Petroleum Hydrmarbons
CS+36 Aliphatic Hydroc2rbons
S u nggal e : l - Ch lo to oclad ecan e
74.4
3.35
3,65
99_9
3 5 /
mS/kg dry
mg/kg dry 14.2mgl(g dry
96 4A-140
8RL 74 50-1a)94 40-140
115 40-140
90 60-120109 60-120
30
ARL
BRL
BRL
8RL
BRL
BRL
ARL
BRL
BRL
BRL
3.84
84.3
J-64
BRL
BRL
BRL
BRL
ARL
ARL
BRL
BRL
ARL
BRL
7 0 5
mg/kg
msftg
mgftg
mS/kS
mExg
mg/Kg
trEftS
r€/kS
mg/kS
mg/kg
ngftg
13.31 3 313.31 3 313.313.313.313.313.313 .3
r€/kS 13.3mgfts
333
93.33.33
Duoltc.t t70312E3{UptI Source: 5459rl.64-10
mS/kS
mg/xsmSI(S
mg/kg
mSI(g
fta/lr's
mS/kS
mg/kg
r,ig/kg
m9ikg
mg/kg
25.4
25.8
25-8
2 5 E
25.8
25-8
25.4
2 5 8
25.4
25_E
ARL
8RL
BRL
ARL
ARL
ARL
BRL
ARL
BRL
BRL
50505050505050505050
109 10-14n
Thb taborqtory rcpod is nol ealU wilhout oI aurtoiel sig'zztare on lhe cowr page.
* Reportable Detection Limit BRL = B€low R€porting Limit Page l l7 of l52
Page 501
Semlvolrtil€ Orgenlc Compourds by cC - Qurlity Control
Result FhS Unirs
Bstch 7t3 1063 . SW846 3510C
B|ank r/o3loB-ALKI IP.epared: 20-Mar{7 AnalFed; 2z-tula( 47PCe 1016PCB 1221PCS 1232PCB 1242PCB 1248PCB 1254PCB t260PCa 1262rc8 126aSunogalE: alae&anuoabiphenr4 (&)S u n9gete : DeoEch lqob i p he nyl ( S I
LCS n031063€8tI
Preg€r€d: 20-lrar-07 Anal:Fed. 22-Mat47PCS 1016PCg 1260Su'.ogate : 4 t+Dg4cbnuorobiphenyl ( SlSu''ogate: Decehwobiphenyl (Sf)
LCS Duo a7081061€50l lPrepared: 2Glrar-07 Analyzed : 22 -Mat 47rca 1016PCB 1260Su|'€gete : 4lABQdanuor&iplbnyt ( SiSufiogata : DEc€chbrobhkenyt ( St)
Brtch 7031061 - Sw646 3510C
Bhnk t7031064-BLfilIPrepar€d: 2SMai-07 Analyzed 2 l-tAat47
a€HCb€r.rcd€Hcg+HC (Lindan€)Chlodane4,4-DDD (p.C)4,+oDE G,p')a,+IDT (p,p')DieldrinEndosuhbn IEndos{ftan llEndosr fan SultaleEiddnE.ddn AH€hydeH€pbdrlori"lelhoxycfttcrH€ptad or EpoddeToxapftea|€aorbrdansgChlordan€
Endrin KebnoS:unogate: +,+Oeoaanro-uptmny 1S4Sufiogate : Decachlorobiphenyt (Sr)
LCS aZ0!106a€311
8RtBRIARLBRL8RLBRLERLBRTBRL0.1500.1w
2.322.35o.t4t)o.170
2_342.3Xo.1fi0.1fo
ARL
ARL
BRI.
BRL
BRL
BRL
BRL
aRl
8Rr-BRL8RLARLBRT8RL8RLBRLBRLBRLBRL8RLSRLBRL
0.01380.0191
udlpdlusxpqlrglwn!glt'$ttsnpdl!tl4
0.2m0-200o.2000.2000.2000.2000.2m0.2000.200
o.200o.m)
30-tfl30-150
,()-140
40-140tui5030-150
4G.14440-140!)-1fi30-1$
7590
t s4!s4pdlrdl
93s470a5
[email protected]
e4
65
udlpql
t9/lu9n
0.2000.200
0-2000-200
0_0r000.01000,01000,0100oo1000.05000.01000.01000_01m0.01000.o1000.01000.01000.01000,01000.01000.01000.01000.05000.01000.01000.0100
2.50250o.2uo.2m
2020
udlug/l'|ldlpsnugnpsntr9/l
!dl
wli
I,lg/l
lrsitp9n!dl
rlgr
Itdl
run!dlpdl
vgl!91ttilpsnpc4pdl
0.02000.0200
30-1tu30-1fr
6996
Thls lahrarory &port is ,rot vdid wtdna an &t^orized sigragre on the .aver page.
. R€portable Det crion Limit BRL = Beloer Repqting Limit Page I 18 of t52
Page 502
Semivolatile Organic Compounds by GC - euality Coltrol
Spike
Brtch 113 106l - SW846 35 locPaepared: 20.1\Iar{7 Analyzed. 21-MaLO7
Aldrio
a€HC
b-BHC
d.BHC
g-BHC (Lirdane)
4,+DDD (p.p )4,4-DDE (p,p )4,+DDI (p,p')
Dieldrin
Endculbq I
Endcullbo ll
Endosuff?n Suttate
Endrh
Endrh Aldehyde
H€ptadrl,or
Hept,dt|dt Epoxide
a-Chlordaneg4nlordane
Enddn Keton€
S u noga te : 1, 4 -D & O cta lhm ro bi p hent| ( S 4S urog ate : Dec achb ro bt p he ny | ( Srl
LCS Ouo f|03106.!A501 l
P.6par€d: 20irlar-07 Ana\zed: 21-Mar-07
Aldfin
a4HC
b-aHc
d€Hc
9€HC (Lindaoe)
4,4oDD (p,p')
4.4oOE (p,p )4,4-DOT (p,p )Di€ldrin
Erdosulb4 |
Endosulfan tl
EndGulfan Sulfate
Endnn
Enddn f\k ehyde
Hepbchlor
Melhorycllor
Hoptachbr Epoxide
a-Chlordarb
g4hlordane
Enddn lGbne
S wrog a te : 4, 4 - DE-GlEfl w tobh he ny I ( S 4SuTogale : Oeca ch I o ro bj ph e n y I ( S r)
Barch 7031068 - Sw845 35fl8
gbnk 17031o€E€lt(l)
Pr€palEd: 20-Mar{7 AnalF€di 21-Msr,07
Ahdn
a-BHC
b€Hc
d€Hc
0_0160
0.013a
0.0103
0 0089
o 014a
0.0167
0 0137
0.0169
0.0164
0.0171
0.0186
0.0154
0.0173
0.0167
0.0174
0.0r62
0.0169
0.0171
0 . 0 1 5 9
0.0187
o.o105o.0236
0_0154
0.0131
0.0r21
0 0085
0.0142
0 0167
0.0134
0-0156
0 0160
o.0168
0 0171
0.0146
0.0166
0.0158
0.0153
0.0152
0.0164
0.0'tot
0.0160
0.0166
0 0 1 7 7o.o244
l,s^p9l
!gn
!g/l
u9rpEl
trgrpsnpdl
!srIrgJl!sr]l91
fg/l
!91
ug/rvqls/l
ugtlLjgl
tr9/lps/l
|ls/l
|ls/l
|'/s/luEtpg/l
pgl
pgl
|lry1
Lis/l
Irlyl
|l9/l
t /g l
usnp(yl
uglus/lusn|ls/l
irdl
|'jsa
!91!s/l
0.01000 01000.01000_01000 01000 01000.01000.01000.01000.01000.01000.01000 01000.01000.01000.0100o.01000.01000.01000.0100
0.01000_01000.0100o_D10D0_01000.01000.01000.01000 01000.01000.01000_01000.0r000.01000.01000.01000_01000 01000.01000.0't00
0.02000 0200o.02000_02000.02000-02000.02000 02000.02000.0200o.o2D00.02000.02000.02000.02000.0200o.o20a0.02000.02000 02000_0200o 0200
0_02m0.02000.0200D_02000.02000 02000.02000 D2000 02000.ozu)0.02000_02m0.02000.02000.02000.02m0.02m0.02000.02000.02mo.02000.0200
80 40-140
69 40-140
52 40-140
44 40-140
74 40-140
84 10.140
6a 40.1,ro
84 10-140
82 40-140
86 40.140
93 40-140
17 40-140
87 40-140
84 40n40
a7 40-140
81 40.140
u 40-140
86 40-140
80 40.140
94 40-140
92 4G110tlg 40-11n
77 4,-140
66 40-140
60 40-'140
42 40-140
71 40-140
84 40-140
67 40-140
78 40..t40
80 40-140
84 40-140
86 4&140
73 40-140
83 40-1{0
79 40.140
76 40.140
76 40-140
a2 40-140
82 40-140
80 4G140
94 40-140
88 10^140122 40-140
4
5
0
1
7
2
2
8
5
5
6
1 3
6
2
5
o0
2020202n20202020202020202020202020202020
BRL
BRL
BRL
BRL
!g/kg wet 14.3
lgkgw€t 14.3pgr'kg wet 14.3
lgukg wel 14-3
Thk laboratory rcport is not wlid wlthoat a aatlto zeilsEnalure on ilv.ovcr pzge.
' Reportable Detection Limit BRL = Beloy/ Repodio8 Limit Paee l19 o( 152
Page 503
Semivolatile Organic Compounds by GC - Quatlty Cothol
Analyqs) R€suli Fhs UnitsSource ToRECR€iult %REC Limits
SpikeLevel RPD
Brtdr 7031068 - SwEa6 35508
Blank fl031068€Lxll
P(€pdsd: 20+rar47 Analfu€d: 21-irar$lq€HC (Undanol
Chlofttane
4,+Dff) (p,C)
4.4oDE (p,p')
4,4ODT (p,p')
Di6l&in
Endosul{an I
Endoertbn ll
Endcdtan Suliate
Enddn
Enddn AH€tryde
H€ptachbr
Methoxychbr
tleptacfilor Epoxide
a-Chlodaneg4hlordane
Endrin tGton€
Si/,rcgate : 1,4-D&Octanuonbiphenf (54Swqale : Decehlorobiphonyl ( 54
LCS n031068€Stl
Preparecf r 2Glrar-07 Analyzed: 2l -Mat47
Ald.in
a-BHC
b€Hc
d-BHC
g€HC (Undsne)
4JoDD (p,p')
4,4-DDE (p,p )a,+DDT (p,p )Oieldin
Endo€uthn I
Endosuffan ll
Endosulbn Suhble
Enddn
End.in Aldehyde
H€ptad or
Methoxychlor
Hepliachbr Epoxide
a4hlo.dan€
g.Chloden€
Endrh K6bne
2,4,5,CTc-l'l-Xybne (lS)
Sunagate: 4,+DB-Octafl uorobiplE]nyt (Sr)Surwata: D€cer;hlotobblFnti (54
LCS Drro O0:t106&830l )
Frepamd: 20-M€r47 Anavr€d: 21 +Jtaf47
Abrin
e€HC
b-BHC
d€Hc
gFBHC (Llidan€)
BRLBRISRLBRLBRI8RLARLBRLgRL
ARLBRL8RLBRLARLARLBRLBRLBRL19.132.0
23.423.712.623.126,025.623.924.926.9
24.426.825.827.228.5
27.726.529.20.o20tg.930.5
26.622.7
| 1 .724.O
za.a28.6
28.6
2862E.628.628.628.62A.A28.628.628.628.628.6
28.628.628,628.628_6
'r0.0
28.628.6
28.628.628.62A-6
Igr'kgwel 14.3
Ig/tgwet 71.5pgtllgw€l r4.3
lgr'kg rvet 14.3
udkSd 14.3
|Jg qwet 14.3pg/kgwel 14-3
Ugikgw€t 14.3
lcrtgwet 14.3pgr'kg w€t 14.3
Wr'kg s/et 14.3
lg/t€wol 14.3
Ugr/kg w€t 14-3pgr'kgw€l r4.3
ugr'kg wst 71.5
$gkgsret 14.3pg/kgwe{ 14-3
!g/kg wel 14-3pgl(g rv€trcr'kg w€t
!g^g v/et 14.3pdks u,€t 14.3pgn(g wel t4.3
ldkSwd 14.3
Igr'kg wet 14.3pg/kg wel 14.3
lYkg wel 14.3pdkg w€t 14 3
!g/kg wet 14 3
|rglkS wot 14.3yg/kg w€t 14.3
t g/kg wet 14.3
ldlSU€l 14.3pS/kS lret 14.3
ug €s/et 14.3
Idkg wet 14.3
t g/kg wel 14.3
ISikg w6l 14.3pdkgw€l 14.3
ldkS wet 14.3
ldhS v'iet
Ugr'kg wstUgkg w€t
lgrl0wet 14.3pgr'kg wet 14.3pdkgwet 14,3
Ig,tswat 14.3pqfgwel 14.3
6f *iil1 1 2 t u t f i
93 4&14082 &1Q83 4S r,r044 40-l4n82 4G140sl 40-14090 4Gl,lO105 ,(F140
a7 40-14/l94 40-140$ 4.0-14085 40-14094 4{}1,()s0 4G14095 40-140100 4tF14090 40-11097 ,1G1,|()
93 4G140102 .O-t40
39.9 50-2fi)70 1+141)1O7 40-t1O
93 40-14079 4G1,lO78 ,|&140
41 &.11Ou &14
7
3030303030
Thls lc6ordo4 tqorl k not volitl N'i haa e, odltorlul stgnsturc on ,he cosd peg..
' Rqortable Detection Limit BRL = Belorv Repodng Limit Pasc lmof 152
Page 504
Semivolatile Organic Compounds by GC - Quality Control
Analyt<s) FlagResulrSpike
l€vel
%RECLimils
RPIJ
Limit+RDLUniLs
So\rrcE
Result %REC RPD
Brtch 703t068 - sw846 35508
LCS Dup O03l 068€SD1 )
Pre.pared: 20-Mar{7 Analyzed: 21 -Mat47
4,+DOO (p,p')
4,4-DOE (p,p )4,4-DOT (p,p')
Diebnn
Errdc|fian I
Endos{Ifan ll
Endosulhn Sulfat€
Endr|'|
Erdfin Aldetryde
Heptedllor
Heplachlor Epoxide
a{hlordane
g.chlordana
Endrin Kelone
S u rog ata ; 4, + D B4da nb rc bi p he n tt ( S 4S unq ate : Dac ac hb to h i ph e nyl ( 34
29.7
26.6
27.9
25.9
27_D
27.5
265
21.3
28.0
26.9
29.6
26_9
27.2
27.0
3 0 8
ft.832.3
14.3
r4.3
14.3
14.3
14.3't4.3
14.3
r4.3
14.3
14.3
1 4 3
14.3
14.3
14.3
14.3
28.6
28.6
24.6
28.6
28.6
28.6
28.6
28.6
28.6
28.6
286
28.6
28.6
2 8 6
2 8 6
2 8 628.6
303030303030303030303030303030
!9k9 w€t
Ug/kg y/et
lgKg lt€t
lEkg wet
/g/kg rrct
pEKg wet
lJgrlg w€t
lgKg wet
ltyKg wEt
lEkq wet
tig/Kg wet
ptyKg $/Et
ug/kg y/et
ugKg wet
!g/t(g yy€t
UEKgwellgkg wet
tig/kg drypdxg drypg/kg dry
ldkg dry
!S/tS dry
ldks dryJ pqks dry
lgks dry
lEkS dry
Uqtg dry
udkg dry
rdks dry
ttglkg dry
!s/Kg drypdkg drypS/kg drypg/kg dry
Idkg dry
ldkg drypg/Kg drypg/kg dry
fg/kg dry
ldkS drypqkg dry
104 40-140 13
93 40-140 3
98 40-140 7
91 40-140 4
94 40-140 0
96 40-140 3
94 40-144 10
95 40-140 1
98 40-140 I
94 40.140 1
103 40-1,10 3
94 40-140 1
95 40-140 2
94 40-140 1
108 40-140 6
66 40-140113 40-140
317I
73 3t)-150109 30-150
102 $-15088 30-'t50112 30-15044 30-15t)10t 30-15090 30-150183 30.15t)
Duolicate l703 l068nUPll SourEe: SASgL5-32
Pr€par€d: 20-lv,f ar-07 Analyzd. 22-Ma'{7
A.BHC
baHc
d€Hc
g€HC (Undane)
ChlodEns
4,4oDD (p,p )4JOOE (p,p')
4JoDT (p,p')
Dieldrin
Erdosulbn I
Endosulfan ll
Endosdfan Sdtate
Endrin
Endrin Ald€hyd€
Heptadrlor
Metrnxya*iht
Heptad or Epoxid€
ToxapherE
a4hlo{dane
gFChlodane
Endrin Kelone
S ulogate : 4, 1 -D B 4 da n uo rcb i p he n tl (S 4Sunqate: Deoschlorouphenyl (Sl
Pr€ps€d: 20+,f ar{7 Analyzed: 22{'i.at47
AHrln
aSHC
b€ttcd4HC
s€HC (LiMane)
4,4-OOo (p,p')
4,+tDE (p,p )
Hardx Spike fl031t)68{S l I So{rrco: SA5944t32
BRL
BRL
BRL
ARL
BRL
BRL
1 1 . 8
136
49.8
8RLgRL
BRL
8Rf
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
22.633.7
r 5 5
15.5
15.5
15.5
15.5
77.5
1 5 5
15.5
1 5 . 5
1 5 _ 5
15-5
15_5
1 5 5
1 5 5
15.5
15_5
1 5 . 5
15.5
77.5
15.5
1 5 . 5
1 5 . 5
BRL
ARL
BRL
BRL
BRL
BRL
1 1 . 5
1 1 6
4 S 3
BRL
BRL
BRL
BRL
BRL
8RL
8RL
BRL
ERL
8RL
BRL
SRL
ARL
BRL
BRL
BRL
BRL
BRL' 1 1 . 5
r 1 6
30303030303030303030303030303030303030303030
15_6
15-6
15.6
15.6
15.6
15.6
1 5 . 6
3 1 031.0
3 1 . 1
31.1
31.1
3 1 . 1
3 1 . 1
3 1 . r
3 r . 1
31.7 pEkS dry27.3 UdkS dry34.9 pgJkg dry13 8 pgitg dry32.2 pg/kS dry39-6 pSftS dry173 OM4x lgr'kg dry
This laboralory rcpon b nat,vld 'ithod an authoi?d signatzE on thc covet page.
' Report$le D€tection Limit BRL = Below Reporting Liftit Pase 12l of 152
Page 505
Semivolatile Organic Comlrcunds by GC - Q[allty Conarol
Analytds) R€sult Flag +RDLRPDLimitUnits
Spike Source c/oREC
Lclel Result %REC Limits RPD
B.rch 7031068 - SW846 35508
Iabri Solt€ O03l05gt{Sl) Source: SA5!M4$3:|
t r6pared: 2o-lrar{7 Analt'zed. 2+ta/47
4,4.DoT (p.p)
OiElddn
Endosulfan I
Endo6ullan ll
Erio6ullEn Sultale
Eirdrin
Endrin Ald€hyde
H€plEchlor
Methoxydrb.
HepHllor Epoxide
a-Chlord€n6
g.chlordan€
Endrin Kehf|e
2,4,5,&To-*l-Xylene (lS)
Sur/ogat€! 44-DB-Oclaf,uorowhenl (SoSunogate : Decachhtobiphenyl (50
a3-534.732.7u.o35.638_O22.1
46.545.344.o36_434.5
0.02023.636.7
l,laHx Soik€ Duo P03l068.t SOtt So{rc€: SA59rt4S.3l
P.€pared: m-Uar{7 Analyzcd: Z2+tat47
30.0
25.4
43.4
12.5
27.3
40.s
176
82.8
35.8
29-2
41-3
36.9
22.1
30.6
44.5
42.3
42.O
34.8
36_6
BRL
8RL
BRL
BRL
ARL
BRL
SRL
!s/ts dryldkg dry
rdks drytgks drytdko dry}llikg d.ypSftS dry
!C,rs dry
udkS dry
lgkg drypSJkS dryySiko dry
Vgr,S drypdkg dry
rdks dry|,€r'l€ dry
r 5_6r5.615.6
r5.615.615.6
15,6
r5.6
15.6
15.6
15.6
15.6
pdxSdry 15.4ugtSdry ls.4$S/kS dcy 15.4
t S/kg dry 15_4pC/kgdry 15_4pgkgdry 15.4
a[r4x !94€dry 15.4
Udtsdry 15.4
!S&S dry 15.4
tgkgdry 15.4pSAg dry 15 4ggkgdry 15.4
lgrsdry 15.4
rdlSdry 15.4
ldkg dry 15.4
Wfts dry 15.4
IdrS dry 15.4
Ug,l(gdry 15-4
!g/kS dry 15 4
udkg dry 15.4
t 9/k0 drytSi kS dry
Alddna-BHcb-sHcd€Hc
9AHC (Lifldane)a.aooo h,p')4.4-DDE (p.p')4,+DDT (p,C)DieldrinEndosuffan IEndosulfan llEndosul an SdfateEndrinEndnn AldehydeHeptacfilofMe0loxyd'lo.Hopbd or €poxidea4hbdar€g€hlordan€
Endrin K€bn€
Sunog6,l€: 4,4og4&f,uomwhenyt (54Su4.ogete: D9cachbtoblpheny' (54
BrLh 713 I 16l . SW846 3545A
Bl.nkrmStlAa€LKllPr@€red: 21{rlarry Analne,l: ?2-Mafi7PCB t0t6PCS 1?21PCB1?32PCB 1242PCB 1248PCA | 254PCB 1260PCB 12€2
3 l . l3 t . 1x1.131 .131 .131 .131 .13l.131.131-131.131 .137.110.031.131.1
30.830_830.430.830.830.830.830,830_830E30.830.830_830,830.830.830.830.E30_030.830.830.8
49.3BRLgRL
BRLSRLBRL6RLARLBRLSRLSRLBRLBRL
8RL
BRL
BRL
BRL
BRL
t 1-5
1 1 6
493
BRL
BRL
SRL
8RL
ARL
BRI
BRL
BRL
BRL
BRL
8Rr-Bfl-
7237t6
0.9710
m2I
7
1
6
0.9
2
1'10 30-150121 30n 50t05 3Gi 50141 30.150'114 30-t50122 3S.15073 30-150t06 30-150150 3C150146 3G150141 30-150117 30-150111 4t15091.2 50-20078 Wlfi118 3&1fr
97 30-15002 3Glso141 30-15041 30-1508S 3G.1509s 30.'150t95 3G151)109 3G150116 3S.r50s5 3tI150134 1)-150s6 30-150r20 3G15072 30-15099 3(l1 50144 3$t5o137 30-150136 3&150118 30.t501r3 3Gr5073 fi-150fig n-|ffi
3t)3t)3030303030303030303()3030303030
5050
Ig g vret 28.6
Fgn€w€t 28-6
t€rkgx€t 28,6pgrsw€l 28.6
ldkS Yrel 28.6
ldkgwEt 2B.Ayer'kg yr€t 28.6
tg,lqw6t 286
fhir labnbry rapora is ,or volld widtoa an atad',a.izd skn4ta]P' on tle covet page.
r Rcptrtrble Det€ctim Limit BRL= Below Reporting Linia PagE 122 of 152
Page 506
Semivolatile Organic Compounds by GC - euality Control
Spike
l-evel
Source
Result
%RECLimits
RPDAnablqs)
Botch703l164 - swE46 j5,{5A
Bl.nk a?03116,t4LKlI
Prepared: 21-Mar{7 Analyzed-- 22-MarO7
PCB 1268
Suiogate: 4, 4-DB-OdanLhrcbiphs nyl (S r)Surcgate : Decachloabiphenyt (Si
LCS n031164AStl
Prepared: 21-Mar-07 Analyzgd: 22-Mat4f
PCB tot6
PCA 1260
S u nog a E : 4, +DB- Oc tafh@obi phe nyt ( 3 OS nEg eb : Dacac h I o tdbi ph e nyl (Sr )
LC.S Oup fl03ll6.|ASD1l
Prcpaed: 21 -MaA7 A^alyzed: 22.Mar47
PCg 1016
PCB 1260
Sniggate: 4lag-Octafl@rcbipheny' (54Su/rogale: Decachlorobi pha nyl ( St)
PCB to16
PCB i260
S u rrogate : 4, fi & Oc k n u oro hi phe n yl ( S IS u ftogale : D ec ac h I orobi p h e nyl ( S r)
Brht 7031170 - SW846 35508
Bbhk a?0llt70€LK'l)
Pr€pared: 21-Mar.07 Analyzed: 24-Mat47
PC€ 1016
P@ 12.1
PCS 1232
PCB 1242
PCB 124€
PCA 1214
PCB 1260
9ualicrt€ 4703'1 16+OUPI ) Source SA59tt54{1
PrEpared: 21 -ii,lar-o7 Analyzed: 23-Irar47
PCa 1016
PCg 1221
PCB 1232
PCg 1242
PCa 1248
PCB 1254
PCB 1260
PCa 1262
PCB't266
Suqogate: 4, 4 -D&Octathnrobiphent4 (S r)Sulogate : De c ac hlo ro b i ph e n yl ( St)
atrlx Solks fl Gtl lG4-tlS l) Scturce: SA59/t6441Prcp€red: 21-lvlar{7 Analfzed: 23-Mar-07
PCB 1016
FCB 1260
Su,7ogale : 4, 4-Dg-Octafl uorobiph4ny! (3r)S u ft ogEt e : Decac h I o tobi p h e ny' ( 54
124
1 5 r
5.44E.39
.ndx Splke Duo ft03ll64,tlliDll Sourco: 5A59464{1Prepared: 21-llar-o7 Anatyzed: 23-Mar{7
%REC R?D
ARL
2 1 43 0 0
427
430
20_o28.6
4 1 3
459
2 0 031.4
28.628.6
357
28.6
357
357
28.6246
| 1 . 71 1 _ 7
r50
150
12.O12_O
1 4 9
1 4 9
1 1 . 91 1 . 9
Ugr'kg wet 24.6pdkg wetpgftg wet
pglkg \Atet m.6
!g/kg wet 28.6
lgkg wet
lgr'kg w€t
!g/kg wet 24.6
Pgkg wel 28 6
trg/kg wel!g/Kg wel
!g/Kg dry 11.7
llg/kg dry 11.7pdkg dry 11.7pg/kg dry 11.7pS/kS dry 11.7
udxs dry 11.7UdkS dry '11 .7
!S/kS ory 11.7pg/kg dry 117sS/kS drypgi Kg dry
pS/kS dry 12_0pS/KS dry 120
usfts drypgks dry
pS/kS dry 11.9
!g/Kg dry 11.9pg/r(g dry!g/kg dry
75 30-1fr105 n-150
120 40-14t
120 40-140
70 30-150100 30-150
116 40-140
129 40-140
70 3&150110 30-150
55 30-15075 30-1fi
83 4G140
86 40-140
4s 30-15070 30-150
81 40-140
84 40-140
50 30-15075 U-150
3030
BRL
ARL
ARL
BRL
BRL
BRL
292
BRL
BRL
6_428.75
120
147
5.978.95
BRL
BRL
BRLgRL
BRL
BRL
21 9
BRL
BRL
BRL
21 9
BRL
21 I
404040404040404040
29
5050
BRL
BRL
ARL
ARL
8RL
ARL
ARL
!dlsgE|(s
ftdk9udksUs/kg,rgKsus/ks
28.6
28.6
28.6
24.6
28.6
28.6
28.6
Thit hbonlory rcpatl k nal yditl *ithout n oulhotited sEnalurc on the cojer page.
'R€ponable Detection LiDit BRL = Belo* Reporting Limit PaBe 123 of 152
Page 507
S€mivohdle Org|tric Compounds by cC - Quallty Control
Spike
Brtch 7031170 - SW846 35508
Ahnk fl03ll70.BLKi)
Prepar€d: 21 Jrf ar{7 AnelyTf,d: 24.Me147
PCB 1262
PC8 't 268
Sunog|ale: 4, 4-O&Octet/D.oblphenyl (S!)Sunogab: De@chbtobiphdlyl (Sr)
LCS fflXIt70€StI
P.eparedr 2l- Er-07 Ahalyzed: z+ltat4t
PCB 1016
PCS 1260
Surmgate : 1,1484cbfl uotoupllent4 (54Suttoga'€j Dec&hbftbiprwtyl (Sr)
LCS Drd ato:'{ 170€SDi l
PrepEr€d: 21 {rar-07 AnEtyz€{j. 244/€147
PCS 1016
PCB 1260
Sunogate : 4, +DBactafi @rohiphenyt ( SlSu,'ogata : Decacnlot&iFhenyl ( St)
BRL
BRL
21.431.4
421
450
20.031.4
|dkgpcl(sdks
pofts
ugls|rdlisr4yksr{y$
l|sasvgts!grsvgks
Fgllsus/ks||gkgt gikg
ugl(9!grslls/kspdkgugksrgkst/dl(S
24.628.6
357
357
2 8 628.6
357
2 8 628.6
28.62S.6
28.628.6
27.4
27.1
27 _4
27.4
27.4
27.4
27 -4
27.4
27.4
24.6
28.6
42946620.o31.4
75 fi"1fi110 tu1tu
1ia 4&140126 4{tt4o70 fr-150,10 3tt1fr
120 40-140r31 44n4070 30-tg114 30-150
u) 30-150115 W-te)
3030
Dudicate fi03l I mouPt l Sourca: 3A59.16+10
Prepar€d: 21 -l,far47 Analy"€d. 24-ndet{i|
PCB t 0t6
PCA 1?21
PCB 1232
PCB 1?!2
PCS 1244
PC8 1254
PCB 1260
PCB 1262
PCB 't 268
S/,j/rcga/l6: 4,4aS4danuorcbiphenyt ( SoSunogdte: Dec'clbrohipheffll (So
Brtch ?03117r - Sr#845 3ssof,
Abok fl0illl7'lSLK|l
Pr€per€d: 21 -Mar47 AnalFed: 2SM€F07
AHrh
a€HC
b.BHC
d€Hcg€HC (U.rden€)
Chlordane
4,15DD (p,p')
4,4{OE (p,p')
4,4ODr (p,C)
Oieldrin
Endosulfan I
Endosufian ll
E ldosulfan gdfate
Erdrin
Enddn Aldehyd€
Hegtad or
M€thqydrb{
l-lEptadlb. Epoxide
ORLBRLARLBRLBRLARLERL8RLBRL21.931.4
BRL
BRL
SRL
BRL
BRI.
BRL
BRL
sRtARL
BRI-
BRL
SRL
sRr-ERL8RLBRL
BRLARL
BRL8RLARLBRLBRL8RLBRLBRLSRL
.t0
4A40&4040404040
2 7 3
pdts|lgr€ps^spgrspdksg{yr(gpsikspgl(spdkg
flgxs!dhst dkgucrts!grst/g'r(g|lgk€l{ftsvdtoItC}q
14.314.314.314.3t4.371.514.314.314.31 4 3t4_314.3t4.314_311 .314.3t4.314.371.5
Thrs taboralory rqn , k dot edtd nitttord an ald.or*ll 4MlaE on ah. cova pag._
'R@ortabl€ Detection Limit BRI= Below R€porting Limit Pagc 124 of l52
Page 508
Semivolatile Organic Compounds by GC - Qurtity Controt
Spike
Level
%REC
Limits
Source
Result %RECRcsult Units
BRL
BRL
BRL
18.531.4
25.8
23.6
24.1
13.0
23.2
28.1
294
32.9
27.5
30.4
3 1 . 6
30.1
3r-o27.238.029.4
28.6
28.O
329
18.33 7 1
24.8
23.1
23_8
12.3
23.9
26.2
2 6 0
295
25.2
27_O
24.7
30.0
30.2
26.6
32.2
26.7
25.2
25.4
27.O
18.2
pryxgug/Kgps/ks
!g/Kg
!9/Kg
LjEKg
ptyKg
r/dksu(/Kg
!sfts
!gKq
PEKg
t/(yKg
tjlvK9
tr9/Kg
trgr(g
t/s/Ks
vslkspgtxg
!gr(sIJgKg
ugKgs/Ks
!slksfdks!9Kgp9(9
pdks
trSilqpgl(spg(g
tjgn9!dk9!s/kgug/Kgt gKs
!gK9pgKs
|lgKgpgKg
ugKgpdl(s
!grsp9xsFS/kSpgkspgkspcks
14.3
14.3
14.3
RPDLinit
303030303030303030303030303t)303030303030
FlaB RPI)
Betch ?031171 - sw846 35508
Ahnk {703ll71.BLKIl
Pr€pared: 21-lvlar-o7 Anallzed: 25-Mar{7
a1,l,Dt6a/],eg{hlordans
Endin Kebn€
S unog ale : 4, +D B 4 cI a ff uorcA p h e nyl ( S 4S unog ate : De c.ac hl o tobi ph e n yl ( S t)
LCS I7Gltt7l€S
Prepafedr 21.tvlar-O7 Analyzedt 25-Mar-07
Ald.in
a€HC
b4HC
d{Hcg€HC (tjndane)
4,4-DDD (p,p')
{,40DE (p,p')
4,4OOT (p,p')
Dietdkin
Endo8llt'Bn I
Endosulfan ll
Endosulbn Sulfate
Enddn
Enddn Aldehyde
Heptact o{
Hegtachlor Epoxide
a0{odanegFchbdan6
Endrin lGtone
S u nogate : 4, 4 O B -Octa fl @ ro bip hen yI ( S ISu.rggate: Decehlorobiphenyl (54
LCS Dup (?03li7laSDl)
Prapdted: 21{lat47 Nralyzed: 25-Mat4t
Ahdn
a€HC
b€Hc
d-BHC
g-BHC (Ljndane)
4.4-DDD (p,p)
a,a-DDE (p.C)
4,4-DDT (p,p')
Dioldrin
Endcsulfan I
Endo$ullbn 1l
Etdosuif€n Suf'ate
Endrin
Erldrin Atdehyde
HspffiilC)f
Methoxyd{or
H€ptachlor Epoxide
+Chlordane
g€hbdane
Enddn K€trn€
Su'd6la : 1,14B4cbnuo@bipheny! (SO
1 4 . 3
1 1 . 3
1 4 . 3
14_3
1 4 . 3
14.3
1 4 3
1 4 . 3
1 4 . 3
1 4 . 3
14.3
1 1 . 3
14.3
14_3' t4.3
1 4 . 3
14.3
14.3
14.3
14.3
28.628.6
28-6
28.6
28.6
za628_6
24.6
2a_6
28.6
28.6
246
28.6
28_6
28.6
24.6
28.6
28_6
28.6
24.6
28.6
28.6
28.628.6
2 8 6
28.6
28.6
28.6
286
2 8 6
28.6
246
2 8 6
28.6
28.6
28.6
28.6
2a_6
28.6
28.6
28.6
24.6
28.6
24.6
28.6
14.3
14.3
14.3
1 4 3
1 4 3
14.3
1 4 3
14.3
14.3
1 4 . 3
14.3
1 4 _ 3'14_3
14.3
14.3
14.3
14.3
14.3
14.3
14.3
65 30-150110 30-150
90 4.0-140
03 40-140
84 40-140
45 40-140
81 40-140
98 40-140
104 Q-140
115 40-140
!]6 40-140
106 40-140'110 ,$-'140
105 4G140
117 40-140
108 44-140
95 40-140
133 40-140
104 40-140
100 40-140
98 40-140
115 4A-140
64 4t)-140130 14-110
87 40-140
81 40-140
83 40-140
43 40-140
u 40-140
92 40-140
91 40-140
103 40-140
88 40-140
92 40-140
94 40-140
86 40-140
105 40-140
106 40-140
93 40-140' | 13 4G140
93 4G140
88 4G140
69 4t!.140
94 4G140
u 40-141)
3
2
1
5
6
1 1
9
1 4
1 6
20
1 l
2
2
1 6
1 l
1 0
20
Thk hborutoq ftport h aot volid withoft M aurhoriz.a signourc on the cover page
r Reportsble Deteclion Limit BRL = Below Reporting Lirni! Page 125 of 152
Page 509
Semivolatlle Organic Compounds by GC - Qurlity Control
Analyte(s) Result Fhg
Sourc€Resuft o/&,ECUnits *RDL
Spike
Letrel
o/oREC
Limirs
RPDLinutRID
Baich t03ll71 - SW846 3ss0B
LCS Ouo fl03ll7l€SDl)
PmpaI€d: 21-{ta.{7 Analrzed: 25J;,,s'.O7
Sunogate: Decachlorohipheny' (Sl 105 4A-141)
Duollcat (7031171-DIJP1) Sourc€: SA5g.l6a-lO
30.1
SRL
SRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRI.
BRL
BRL
sRrARLaR!8RLBRI.BRLBRLBRL19.435.2
BRL
BRLgRL
BRL
BRL
ARL
ARL
BRL
BRL
20.o
13.7
1 3 7
13.7
13.7't3.7
68.4
1 3 7
13_7
r 3 7
13.1
13.7
13.7
13.7
13.7
13.7
1 3 7
13.7'13.7
68.4
13_7
13.7
13.7
ARL
SRL
SRL
Bftr
BRL
ARL
ARL
BRL
ARL
SRL
BRL
BRL
BRL
BRL
BRL
aRtBRL
BRL
BRL
8RL
ARL
ARL
Lrdks
pgxg
!sftsugK9ugx9rdks|ldkst dkspg/tgysft9
t dks!dksr9?q,|ldkous^glrgt€Fgrs!gkstrgrl€udks!dkspdkg
Fs^9t'dksFdks
Ug/kg w6l
ydkg ',v€i
Pg,ts ret
Udkg vJel
Ugr'kg';yet
lSftS wet
lglt(g w€l
!g/*g wel
lrgrkg wet
pgrs !ret
[dkS wet
Prepared: 21-lrar{)7 Aoallrzed: 25-MEr{7
Aldrin
a€tlC
b€Hc
d€Hc
g€HC (Lindane)
Chlordane
a,a.DOD (p,p')
a,a-OOE (p,C)
{,|-DDT (p,p)
Dielddn
Erdosulfan I
Endosulfan ll
Endosulbn Sulfale
Endrin
Endd4 Ald€hyde
Heptachlor
tl€pbdr|d Epoiide
Toxaphene
aChlofdane
g4hlo.dene
Endrh l(eron€
Sunlgde: 4,44a.AdanuotlDipheny, (Sr)Surogatg: Decacl ombiptuny' (5.)
Brlch 703127C - SW846 35508
Blanl O031274€LKl I
PrepaFd & An€lfzsd: 22.1'?tar{7
PCB tO16
PCB 1221
PCS 1232
PcB 1242
PCB 1248
PCB 1254
PCB 1260
PCB 1262
PCA 1268
Su'Ioga€: 4,4-DBndanrgottphenyl (St)S,;1,logate : Decehba phonyt (St)
LCS flOglz7a€Str
Ptbparod a Anslfzed: 22-lrar47
PCA tO16
PCB 1250
Sul'c{/ate: 4,'l{/B-cE.snLarobiphenyl (54Sunogate: Decachli/ohiplr€i'ryl /sr)
LCS Dup t?O3t?IaASEt)
P.epared & Ans,lyzed| 22-Md47
PCB 1016
3030
303030303030303030303030303030m303030
27.327.3
7l129
30-t5t)31 15t)
28.6
28.6
28.6
28.6
28.6
28.6
24.6
28.6
28.6
3SO
4 t 6
20.o30.0
pgagwel 28.€
Fg^gwsl 286pgr'kg r€lldkg wet
Fg/kgw€t 28.6
70 g-1995 n-lfl
i09 4G140t17 40.14070 30-t5o105 vttg
111 4G140
28.628.6
3573,tt724628.6
357&6
Trtis lsbontoryeporl it ,toa vau xtitled dtt arlthod?d dgnatt t or, the coverpge.
t R€poftable Detlclioo Lidit BRL = Bdow R€porthg Limit P.gB | 26 of | 52
Page 510
Semivolatile Organlc Compounds by GC - Quality Control
Analit4t Resutt Frag IRDLUnits
SpikeLevel
Source
ResDIl %REC
%RECLimits RPD
RPDLimrt
Brlcn 7031274 - SW846 3ss0B
LCS Duo O03l27adSO1lPrepar€d & Analfzed: 22,Mar-07PCB 1260S unogEle : + + D EO cta E uo.obiphen yt ( S 4S Mogale : Dec ach I o ro bi phe n yl (54
PCA 1016
PCB 1221
PCB 1232
PCB 1242
PC8 1248
PCB 1254
PCB 1260
PCB 1262
PCE 1266
Su rog aie : 4, 4O 8- Oc b n uo rcb i p h e nt4 ( Sr )Sumg ate : De c ac h brob i p h e n y I ( S 4
43320.0286
Duplicat.{70312ZOUP1I Sou.c€:SA595,|E-02
Prepared ll Anal!.zed: 22-Mar47
ARL
ARL
BRL
ARL
ARL
BRL
BRL
ARL
ARL
21.g31.3
Source: SA59YA.02
llgr(9 wel 28.6
P94(g w€tlgks vr€t
lgkS dry 31.3
Lidks dry 31.3
!g/kS dry 31.3
lVkS d.y 31.3
Lig/kg dry 31.3
lgkS dry 31 3
!g/kg dry 31.3pdkS dry 31-3pg/kg dry 31 3
!S/kS dryPgkg dry
Ug/kg dry 30.5
Pgkg dry 30.5
!s/ks drypSftS dry
LigftS dry 31-0ps/ks dry 3'r 0
Lig/kS dryPg/kg dry
' t21 40-140/0 30-150100 30-150
70 w150100 m-tfi
106 40-'t40
117 40-140
60 30-tfi95 30-150
111 {0-140
121 40-140
60 30-1fl9s m-1fl
357
28.628.6
31.33 1 . 3
381
381
30.530.5
387
387
31.031.0
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
404040404040404C40
5050
latrtx splko a703l27{-tlsl }
Prsp€rsd & A^alyzed: 22-Msr-07
PCB 1016
PCB 1260
S u nog ate : 4, 44 B- Oc ta fl u orobi p h e ny' ( Sr)S u zog ate: De c ac h lorobi p h e nyl ( S r)
405
446
18.328.9
424
46S
14.629.4
BRL
BRL
BRL
BRL
atrix Solts Duo 4031274- SDil Souice: SA50548{2
Prepared & An€bzsd: 22-MaF07
PC81016
PCB 1260
Sunogate : 4, 4-D B- Octa fl @ rob i p h e nyl ( S 4S urogale : De c ac hb tob i p hen y I (S I
Thb ltboralory rcpo.l it ,tol tdd xrlthor.! an salhofu?t sigutae od thc covet plge.
. R€portable D€t€cdon Limit BRL = Below Reporting Limit Page 12? of 152
Page 511
Semivolatile Orgrnic Compoutrds by ffMS - Quslity Cootrol
Analyte(s) Result FhC Units
Spike
Leeel
Source %RECResult %REC Limits
RPDRPD Limit
Brrch 7031070 - swMS 3510c
Blank f?03t070€LKl)
Preparod & Analfzed: m-irar{7
Acenaphhylene
| €thylnaphthal€ne
f -il€ttryhEphtlElene
Atazln6
Azob€nze{E/Ixphefl yldiazin€
B€nzidirE
Benza (a) anthracene
Benzo (a) anthracene
Benzo (alp cne
Benzo (a) pyrene
Benzo (b) fluotanthone
B€nzo (b) ltroranthen€
Benzo (g,h,l) pery4€n€
Benzo (g,h,i) perylene
a€nzo (k) ftroranhen€
BerEo (k) fl0oranfEne
B€nzoic aclt
BenzY fuhd
Bis(2d oro60roxy)fi €tEne
Bis(2d{orGttyl)ether
Sis(2-chb'roi8oDropyl)etller
Biq2-etrylh€xyl)phlhalats
+Brorbphsnyl phenyl €ther
Butyl berEyt phthalat€
Carbazole
4-Chbm-}fnet'tyiphenol
4-Chloroailllne
2Chto.onephttulene
2.chlompheml
4-Chlorophenyl pnenyl €tner
Chrys€ne
Chrys€ne
Dib€rEo (a,h) anlhrac€ne
Dib€nzo (a,h) snthrac€ne
OlberEofu€n'1,2{bhbmb€rPene
1,lDichltrobmzene
I,4-Dir*rkroberu€n€
3,3--Dic*rffi€nzltine
2,+Did ooph€nol
Oierhyr phth€ al€
Dimethyt phtlslate
2 +Dnnetrylph€nolDi{+utyl ph0|ale{€
4,6-Oinilro-2{€thylphend
2,&Oinnroph€ml
sRtBRL
BRL
BRL
BRL
BRL
SRL
BRI,
BRL
BRL
BRL
BRL
ARL
SRL
SRL
ARL
BRL
ARL
ARL
BRL
BRL
BRL
BRL
SRL
BnlBRI-
BRL
8RL
BRL
ARL
aRI
BRLgRL
BRL
BRL
BRL
8RrBRL
BRL
BRL
BRL
BRI.
BRL
BRL
BRL
ARL
BRL
BRL
8RL
ARL
BRt
8RL
r9l|ldl
|lEl
vallustIJdIps,4l,sn|,dl!s/|usn!(t/l[!yl1ldr$llusnFgl
!dl
usrlt (yl
lrg/l
llgn
IJdI
!dl
|,dl
wFS4pql
!dlpdl
ttg/]'
lr9lpgl
psnFdltjs/|ugrll€rl$rluglFdltgllIrdl|,g/lp0,
|lg4
pdl
!dlIrdludlys4pcrl
0.0501_000_4000.0500.05t)1.001.001-000 0501.001.00t.000.0500.200o.0500.2000.2000.0500.0501.00o.3000.050|.fl)'t_t)0
l-001.001.00t.00t_001.00't.00
1.OO1.001.00|.o01.001_000.050o.0500.200|.00t.00't.00
1.001.00r.001.00t.001.00to0L00|.00
Thh lobonury repod b Eot tead withoat zn aadtotlzd igndre ott rhe coje, pogc.
* Relofbble Detection Limir BRL = Belo{ Reporring Limir PaeE t28 of 152
Page 512
Semivolatile Orgaric Compounds by GCMS - eualify Control
An8lytqs) Result Flag UnitsSource %REC
Resulr %REC Limits
Spike
l-€vel
RPD
Limit
Brtch 7031070, SW8463510C
B|a* {m310?0€LKlt
Prepared & Andyzed: 20-MaF07
2,+Dinitotoluene
2,c-Dinibotoluene
Di-n{ctyl phthalate
Fluorene
flerac-hloroboneene
tlexachlorobuladiene
H€xachlorocyclopentad iene
Hexachloroelhan€
lrdeno (1,2,3<d) pyrene
l.deno (1,2,3-cd) pyrene
lsophomn€
2-l,lethylnaphtnabne
2-llr6tht{naphthatene
2.Metrylph€nol
3,4-trr€thylph€nol
Naphtnalene
Naph|tlalene
2-l.litroanifine
3-l{lt oaniline
4-l{iboaniline
Nilrob€nz€n€
2+litrophenol
4-a{ttropherrcl
t{-l'lilr-Godlnethylarnine
N-l'{ilroGodi-n-pmpytamine
N-l'lilrosodiphenylamine
Ph€mnhlene
Ph€ml
Pynijin€
Heradrlorobenzene
1 ,2,+f.*ttt robenzene
Peniacfiloroph€nol
2,4,s-Trid|hroph€nol
2,4,&Trld oophend
H€xadtlorobutadi€n€
Su n({/ste : 2 + I uo rob t p he n ylS,//rogate: 2+ fu o to U p henylSll,roga,€ : 2+ I tb to ph e n o I€unogelg : N ih{,,he n zen e4 5Sfiogata: Phend4sSunogate: feryhenyl4t4Suftlgab; Teryhentl4l4Sunogab : 2, 4,6. Tt b to ft ap h e nol
LCS ft031070€s1)
Plspared & Analyzed: :t()-Marry
8RL
BRL
8RL
BRL
ARL
BRL
BRL
SRL
BRL
ARL
BRL
ARL
8RL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
aR(
BRL
ARL
BRL
BRL
8RL
90,390.393.910690.o10310371.7
ps/l
l.rg/lps/l
!9n
t(yl
Fgl
lrgpgn
!g/l
!9/l
!srp(vl
pgl
psnpsnpc{pgl
!(/l
tj9l
!s/l!s/l!gnps:4ps/lp9l
!gnusllLiS/l!gnpsn
!gnugnLj9l
!gn
!gnpsrl
!gnps/l
psll
!91ps,4
!g/lpg/l
!s/lpsnps,4f s.4!c4!dlIJ9Ipdt
t 0 01_001 0 01.00o.oil1.000.0501.000 6001.001.000.0500.2001.001.000.050t,oo1 0 00.0501.001.001.001_(101.001.001_001.001.001.001 0 00.0501.001.000.0501.001.001.00r.00r.00t _001.00L000.5m
too1001001001M100100100
9090941069010310372
3o-1m30.13015,1103o-1N15-t 1030-13030-13015-110
Thit labo.alory pport h not wlid tollhouj sn atdro zed signtrlne on the covcr ttoge.r Reportable Det€ction Limit BRL = Below Reporting Limit Page I 29 of I 52
Page 513
S€mivolatile Organic Compoundr by GCMS - Qustify Control
AnalyteG)Sourc€
Result
RPDLimit%REC Limits RPDR€sulr FIag Unitt
Baach ?0J 1070 - SW846 3510C
LCS t?(Bt070€S1l
Pr€psred e Analfz6d: 20-Mar{7
Acenaphthyl€lte
l -Ivlelhylnaphthalene
1 .ftlethylnaphthabn€
Azob€nzene/DiptEnyldiazine
B€nidine
Eenzo (a) entluacene
aeozo (a) anthracene
B€nzo (a) py.ene
Benzo (a) pyr€ne
Benzo (b) fuoranthene
B€nzo (b) furoraotr€d€
Benzo (g,h,a) p€rylene
Benzo (g,h,i) pery'enegenzo (k) nuoraothon€
Benzo (k) ffuofanthene
Benzoic aodgenzyl alcohol
Bis(2-dbroethory)rnethane
Bis(2.chloro€thyl)ethe.
Bis(2drloroisopropyt)ert€r
Bis(2-€try'herylE hthalate
4-Aromophenyl ph€nyl efi er
Butyl benzyl pht'halate
Carbazole
44hk ro-3flethytsh€nol
44hbru6nilin€
24hktrohaphthal€ne
24hlotEphenol
4chlotophenyl phenyl ether
Ghrysene
chrysene
Dih€nao (a,h) afl thracrne
Dlb€nzo (a,h) anhracan€
Dib€nmluran
l,2obhbrobenzone
1 ,3oichlorobenzerE| ,+Di€filo.ob€nz€n€3,3..Dlchh.obenzidine
2,+oichlorophenol
Di€thyl phlhalat€
Dhelhyl phthabb
2,4-Dimelhy'phend
Di-n-butyl phuralete
4,6onitr+2Jn€hylph€nol
2 Soinibophend
E2.882.892. r92.185.785.71 1 39r.691 .61U106
83.583.592-0s2.882.682_669.169,110510565.884-692.3
6r.8t0184-010112988.243.287.072.582.949.I89.186-786.7a7.777_O6S.479 .194.9m.090.9E6.€79.390.972.784.6
|lsnt|94!snpcl
!dl!dllrgl!c4pdl
!snrdll€4
pdlpsr!Elpdlps,lpgnpdl
udlItg!l
tjc4pdl
!9n
udlt'$tsllpdl
!sntts/l'@lvgtlpql
!snrs4|lsnItgllp9/l
!dl
Fdlpsnus4pdl
!dl
!dl
us4lrdll)glt'dl!drttglt s {
1-O0o.0500.4000.050't_00
0.050r.00t.000.050't-00
1-001.000.0500.2000.0500.2000.0500.2000.(m1-000.0500.3{x)1.00r . t o1,001.001.001.001.001,OO1.00L001.001-001-001.(X)r.fil0.0500.2000.0501.00r .m1.001_00'1.(x)
r.00r.001.mt-001.001-{X)r.00
r00100r001 m100t00100'tm1 m100t00100100100100r0010016100tmt00r00100100r00r00'tclo
100100r001001001001001001fi)1m'100
100r001001m1001001001001m100'r(x)r001001m
83 .r0-r40&, 40-1109:l 4&1.$92 4Sr4086 40-14086 4{11{0113 40-14092 4&1,1092 4G1401U G200106 40-140126 ,lO-14O
04 40-t,tt)84 40-14093 40-14093 40-1.10&l 40'1{08:t 40-14069 40-14069 40-140tos 40.140105 ,10-140
86 30J3085 40-14092 4S.'14095 ,lG1.l0
62 4Gt40101 40-14084 40-110101 4G1,10r29 ,|{).'140
88 3St3003 .$-140
a7 40-1d672 30-13003 4o.1,r089 4G14069 40-14087 4G140a7 &11088 {G1407f 40-14069 40-14079 40-14095 1S14060 3$.13091 40-14.087 1o-14I79 3G13091 ,lG14O
73 3{!rr085 3G130
This bbralo.y Eltort k ,tot tatfut $ holt ar authorfud sig',&tre oa th. cnter pqe.+ Rcporr.ble DelEcrion Umit BRL = Bclow R€Foriing Limit PaAe 13O of 152
Page 514
Semiyolatile Organic Compounds by GCMS - Quality Control
AnalyteG) Resu,l .RDLSpike
Level
TOREC
Lirni(s RPDRPDLimitFJug Units
Source
Result %REC
B{rch 70J1070 - sw846lst0c
LCS f703t070-ASrl
Pr€pared & Analyzed: 20-Mari7
2,4-Diflilrotoluene
2,GOinitrotoluene
Di-Goctyl phlhalate
H€xachlorob€nzen€
H€xschlorobutadiene
Hexadllorocychpentadien€
Indeno (1,2,3-cd) pyrene
Ind€no (1,2,3,cd) pyEne
lsophorone
z+r€thylnaphlhalene
24rethylnaphlhalen€
2{'lethylphsnol
3,4-M€th)4phenol
Naphthabne
Naphthalen€
2-Nilroaniline
3-ilitoaniltne
4+.litroEnilln€
2+li8opfi€nol
4-Nitrophenol
N-NitrosodimethYamine
N-l,lilrosodi-n-propyramine
N-Nltrosodiphenylamine
PFidin€
Hexachlorobenzene
Hexachloro€lhane
I ,2,+Tri$lorobenzene
2,4,5Trid oroph€nol
Penbchlorophenol
Hexad&aobuiadiene
2,4,&TrftJtlorophenol
S unogate : 2 + hJo n N phe nylS u nogab : 2 + I u o to bi p h e ny ISuftoga|]e.:2+l@tophenolSwrogale : N ihoben ze n e4 5Sl/froga/€: menol4sSunogata: Teryhenl4l4S u nogate : Te,p he nyl 41 4S uiog ate : 2, 1, 6 - f n brcn o ph end
Brtch 703 (278 - SW846 f5508
ehnk 1703'127E€LKIl
95.6
94.3
1 1 8
8 3 0
83-0
8.r.5
8 4 5
80.5
19.4
7 1 . 6
7s.0
59.7
55.7
s 3 8
E9_3
89.3
74.8
84.8
84.8
90.9
8S.6
1 t 5
102
80.7
5S.0
423
4 1 5
1 0 1
7 4 0
8 0 4
80.4
42.5
86.8
86.8
85.9
80.5
75.0
41.2
92.1
74.0
I9A
68.5
91.891.871.71 1 075.597.297.283.5
1_001 0 01 0 01_0000500.0501.00r.000.6001.00r_000 0500.2001.001.000.0501 0 010.00.0501_00't.00'1 00'1 001,001_001 0 01 0 01.O01.00r.001.000.050r.000.0501.001.001_001 0 01,001-001.000.5001.00
100
r00100r00100100100'100
100'tff)
100100I Cro100100100100100'| 001001001001001001001 m1 m1001001001001001001mr001001001(1t)1001001001001001M1001N1001001001(n100
!gn
us.4ugl
!91
!g/l
!s/l
!El
rc/|trg/l
!9r
ItElpsn!c4p9l
u(ylug/lrs/l|lsnvgrllig/l
uElpdlpglps,4
!gn!gn!g l
!g/l
tr9/l
us/lItgtl
lr(yr!91
us/l!g l
lrg,WnpsnpsnpsnpdlFEI!s,4ps/lLjgl
!sn!snpgl
!dlu9/lpg/l
96 ,rO-140
94 40-140
118 40-140
83 40-140
8:t 10-140
84 40-140
84 4G140
80 40-140
79 40-140
72 40-140
15 40-144
60 40,140
60 40-140
94 40-140
89 40-140
89 40-140
75 40-140
75 40,130
85 40-140
85 40-140
91 40-140
90 40,140
115 {S140
102 40.140
81 30-130
59 30-130
a2 40-140
42 40-140
r01 40-140
74 30-130
80 40-140
80 40-140
82 30-130
87 40.140
87 40-1,$
86 40-140
80 40-140
75 40-140
84 4G140
92 3G.130
74 30-130
7S 4G140
68 30-1311
92 #13092 3G13072 t5-110110 fr-13076 15-11097 3L13097 30-1mu 15-110
Thb labontu4t Epotl it ,tot vzlu i'ilhoat tE o!rtoized signainre on the cowr pge
' Ret'orirble D€t€ction Limit BRL = Below R€podng Limir Pase 131 ot 152
Page 515
Semivolatile Orgatric Compounds by GCMS - Qurlity Control
Anflbtds) R€sulr Flae Units .RDLSpike
Level
%RECLimits RPD
RPDLimit
Sour,rResult '/oREC
Brrch 7031278- SWE{6 35508Prepa.6d: 22-MarO7 Analyz€d: 23-Mar-07
AnilinE
Ahazine
Azobenzene/Diphenyldiazanegenzidine
A€nzo (s) snthracerE
Benzo (a) pyrerEgenzo (b) iuoranhsfl€
B€nzo (g,h.i) perylene
B€nzo (k) nuoranlhene
Benzoic acid
B€nzyl alcol|ol
Bb(2drloroelhoxy)m€lhan€
Ai.s(2d oro€trY)€ber
Bis(2d oro{sopropyl)elher
Bis(2-€thylhexyl)phthalats
4€romoph€ny' phenyl ether
Butyl benzyl phtElate
Caabazole
rchb,ro-3-m6thylpheml,{-Chlo'roanilne
24hloronaphfielene
2.chlorophenol
4chlo.@henY ph€nyl elhet
ChryEene
Oibenzo (a,h) anthracene
Dlb€nzofuran'l,2Oichlorob€nzsn€
I .3oichlorobenzene'1 .+Oic+ ofobenzene
3,3'-Oidbrob€flzidin€
2 JOichloroph€nolDietryi phthalats
Dinethyl phtrialab
2,4-Oirn€thylphenol
Oi-nSuryl prtihsbt€
4,$Oinirc2.m€lhylphenol
2,lEinilrophonol
2,+Dinitololu€fl€
2,H)inihotolu€ne
Di+octyl phfialate
FluoEnlhen€
Fluoren€
H€xachlorob€nz€ne
H€xechlombutadisn€
H6xachlofi ccyclop€ntadien€
H€xschldoofn€n€
Indeflo (1 ,2,3-cd) pyren€
1 -fvlelhylnaphlhalene
lsophorde
2-t lethy'naphthsl€ns
2-M€l,hylptFnol
ARL
BRI-
8RL
BRL
8RL
8RL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
ARL
BRL
sRr-ARL
BRL
BRL
BRL
8RL
BRL
BRL
8RL
SRL
BRL
8RL
BRL
ARL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
SRL
BRT
SRL
BRL
BRf
ldkgwet 30
US/kS {v€l ix}opgy'kg v/et 330
rcL/kg vY€t 3:)0
!S/kS Y,/et 330pSr'kS wet 330
!g/kg wet 330
lrg/kg wet 330
lgikgw€l 330
rc/*g n€l 330
lg^g wet 330
!g/kS w€l 330pgftg wel 330
Pgr'kg w€l 330
ldtS lYel 330
ldrgYiel 330
ldkg Yr€l 33t)
!S,4(S rret 330!S/kg wet :}i,,0pdkS wet 330
lgL/kg {,et 30
tidkS vret 3l]0
lgr'kg wet 3il0
lgrl€ wet 330p€/t€wet 330lg/kgwet 330
Ig/kgw€t 33O
|lgr'tgwer 33oIg/?€ $/el 330
tigRg wel 330pgikgw€t 330pdkg wel 330pqkS wet 33O
!g'kg w€l :I:}0
lS&Sn€t 33O
lidks wel 330lgn(g wel :I10
IgL/kg w€t S0
Udkgvvet ai!0!S/kS vret 310lgr'kg wet 3:10
lgr'kg w€t 33Opg/kg wet 33Opg/kgwet 330
l€n€wet 330ug/kg wet 330yg/kgwet 330pgtlg w€l 330pgtg$€t 330pgrkgw€t 33t)pgftgYr€t 330
lSftgrY€l 33O
ldkgw€l 330
rcfxg wsl 330
Thb taborulorf Eporl it nat wIU uUhosr cd .uthori@d sig',,rtare on ahe coee page-
r Repntablc Dett€ion Liqrit BRL = Bclow Reporting Lioit Page l32ofl52
Page 516
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s) Result Flag Units .RDLSpike
t€vel
%RrcLimits
RPI)
I - imi tResult %REC R P D
Betch 70Jt278 - SW84615508
Blank 17031278-BLKll
Preparcd: 22-i,la.{7 Anatfred: 23{,laF07
3,4+vlelhylphenol
NEphthalene
2+lit o€oiline
SNitroaniline
4+{ikosnilin€
Ntrobenzene
2+likophenol
4+liroph€nol
N-NitrGodi.r€lhylamine
N-NibGodi-n+ropylamine
N-Nibosodiphenylemine
P€ntachlorophenol
Ph€ml
Pyridine
1 2,4-T.ichlorobenzen€2,4,$Tdcnbr@henol
2.4,eTdchlomphenol
S u rogale : 2-F I uorob i p h e n ylS u ffo9at6 : 2-F ro rophe no IS u rogate : N ltobe n ze ne - d 5Sutrogate: Phenol46Suroggl€: Te9henyl4l4S u tnualE : 2, 4, 6 -T n b Mno ph en ol
LCS t7031278€5
Prepared: 22-Mar{7 Analyzed: 23-lvlar{7
Aniline
Azobenzen€/Diphenyldiazine
Benzilin€
Aenzo (a) aothracene
Bsnzo (a) pyr€ne
Benzo (b) ffuoEnthene
Benzo (g,h,l) perylene
S€nzo (k) nuoranth€ne
Bmzoic acid
8enzy' alcohol
Bb(2-d oroethoxy)methane
Bi.s(2{hloroehY FtherBE2d'lomisoprop)4Fther
Bb(2-ethylheryi)phthalate
+B@floph€nyl ptienyl etler
BUV b€nzyl phthalal€
Cabazdett4hlom-3fi ethylphenol
{-Chloroanilin€
2-Chlo.onaphthalene
2Chlo.ophenol
4€hlo.oplEnyl phenyl eher
BRL
BRL
BRL
BRL
ARL
BRL
ERL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
532052606490514062903900
5350
5910
66S0
5970
7500
6850
BRL
5'160
5700
5 1 1 0
4550
6 1 1 0
5480
5280
5780
6170
5110
6360
5170
6'r90786055205040$9045305490
667066706670667066706670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
pS./kS wet 330
lgkS Yvet :]i]0
lgr'kg wet 330
Lig/kg wet 3il0
lig/kg wet 1320pg/kg wet 330pgkswet 33O
lgL/kg wet 1320
!g/kg wet 330
Ug/kg wet 330
lgL/kg wet 330
trg/kg wet 330
Ugr'Kg wet 330pgr'kg wel 330pgn(g wel 330
Ugr'kg wet 330pg/kg wel 330
Ug/kg wel 330pgftg wet 330
!g/kg wet
|lg,/kg wet
!g/kg wetug/Kg welUgkg welpgr(g wet
ug/kg wet 330
PgL/kg ',el 330
!g/kg wet 330
Ug/kg wet 330
Ug/kg wet 330
!g/kg wet 330
!g/kg wet 330
Ug/kg wst 330pS/kg Y/et 330
!g/kg Y/et 330
ldkS wet 3il0pdkg rret :l3O
!94q Yr€t 3{}0
ldkS\det 330
ligkswet 3l]0
Ugftgw€t 330pg/kg w€l 330pg/kg wet 3i,0
l4/kg w€t :l:],0
Ug/kg wet 330
Ugltrgwel 330
lgr'kg wet 330
Ug/kgwet 330
Pg/kg we( 330pdkswet :t:|0
t'dkg wet 330
80 m-13079 1U110s7 3G13077 1U11094 30-13058 16110
80 40-13089 40"130100 40-13090 40-130112 4&130103 40-130
0-13077 4o-13o85 4G13077 10-13068 40-13092 40-13082 0-13079 40,13087 40-130s3 40-13078 40-13095 40-13078 40-13{)93 40-130118 40-13083 40-13t)76 40-13082 40n3068 40-13t)82 4.G130
Ihit bhoralary ..po.t is ,un valid vitho4 an c{&oriaed signalw on tre cot E prye -
. Reportabl€ Deteciion Lirnir BRL = Below R€poning Limit Pase t33 of 152
Page 517
Semlyolatile OrgNnic Compounds by GCMS - Qudity Control
Anflbae(s) Result Fhs Uniis RPD*RDLSpikel"evel
RTDLimit
Sourcq %WcResult %REC Lir ts
Brtch 70312?8 - SWE46 35508
LCS r703t270€: I
P.epared: 22{rar-07 AnElyzed: n.l|,€f 47
Chrys€Ile
Dib€ruo (a,h) entnrEoene
Dibenzofuran
1,z-Diihrob€nzen€
I,3.Dicl orob€nzene
1 ,4Oichbrobenzene3.3'nlcilorobenziline
2,4Oidrlorophenol
Di6fi!,1 pht|alele
DinreEtyl phthalab
2,4oimeb/pft€nol
Di{-buM phtl|a|et€
4,6-Dhitro-2{helhylphenol
2,+Dinitrophenol
2.rtDinitrotoluen€
2,6oinlUotoluen€
Di.n-*tylph8lahte
Ft orarttErE
Hexachlombsnz€ne
ilexaclrlsobutadlene
H€xschlorocydop€nlEdiene
HexacrdoroelhEne
Indeno (1,2,3d) pyrene
lsophorone
1 {rethyLtaphthal€ne
2-Melhyhephtrsbne
2-f ethylph€nol
3,+M€lhylpherol
N6phthalen€
2{.litsoanilin€
3-llilrcaniline
4+lihoaniline
Nibot€nzene
2+.litophenol
4{'{itrophenol
N-l.lito$odtn€lhylamioe
N-Nibosodi-n+rogylamin€
N+,lilrosodiphenylahine
PenLdrlorophenol
Phenol
Pyridine
1,2,+Tid*orob€rEene
2 r, tTrichbroptEnol
2.4,STric*rlo.oplEml
Sffilp,ate:2+IwmblphenylSu nogato : 2 +l @toph en otSuftogala: Nfuolj€.nzene4sSunogala: PhenoI4SSurYoga(e: Ierp|t€flydl4S uttogab : 2, 1, 6f tibtonl€ptl€nd
550052705610448042m51505&X)49505690535044105810441050705470
f5205040554050005020,1520
50r046S0s89054'70
4730487D552056,|057E0752063iX)497037605r503@O6470454050505210va04020522058404rtu56rO4"8)6560154)565048fi
6670667066706670
6670667066706670
6tt706670667064706670
667t)6670667066706{t706670667066706670
66706670
66706670667066706670
66706670667066706670
667066706670€670
467086m6470667066706670
!dl!S wet :|:}0
!q/19 wet 330
Ugikgwel 330
Udkg w€l 330
!g/kS Yr€l 330
!g/kg wet 3:10
lS/lqwst 330
Fgfkg wel 330
|Jgtg w€l 330
!9r'k9 rsi 330
Idl(S','/el :l:10pg/!g wst 330
Ugftg w€t 330pSI(Svr€t 330
ldxg vJ€l 330
ldl(g wet 3i'0
FBfkg wel 33O
Ugr'kg w€t 330
t gl(S v{el 330
UdXS wet :l:}0
lgL/xg wet :x)0
t g/|(o w€t 33O
lgkgw€l 330pg/kg wel 330
rcrxg w€i 330lgr'kg wetWftgwet 30
Ig/kg wet 330
lrqrc w€l 330tgfl(g w€l 330
lgL/kg v/et i]:10
ldkg wet 330
wrtg w€t 1320pqkgwel lio
lgftgn€l :]:j0
lgfq Y{€t 1320pg/tqwel 33Opgrl(g w6t 330pglkg Yt€t 330pgr'kg wet 330
lgks w€t 330
Fgftg wet 33O
l€/kg w€t 330
Fgrkg wet 330
$SlkSY{ct 33O
lBkg $/et 330lrgilgwet 330
tis/kg wett€/|(g wetpqto w€tUdkg vJ€ludko wetugr'kg wet
84 40-'t3079 40-13084 40-13073 4G13t)63 {0-130f7 4O-1m87 40-13074 40-13085 4Gt 3080 40-13072 40-1n87 40-13066 4G13076 4Gt3085 .tG130
s0 .40-130
r 13 {G13076 4t)-1&&3 40-13075 ,$n 3075 40-13068 40-13075 4G13070 .tGt30
88 4$r 30s2 4G14084 40.13071 4G't3073 4{}-13083 40-13085 40n 3087 40-130t13 4G130s5 4G13075 4D-13056 4{-13)77 40-13045 1r()-130
97 40"t306a 4{t13d76 40n 3078 4/l-13/l8:l 1{!,r 3060 ,r0-t3t)
78 4S1308E 4.0-13062 40.131184 3lLtfl67 tS1t09A tu19)68 15-11085 g-ln72 1U110
Ihis latorarorf rcpod it nol telitl,tithotd onz. hodztd stgnatuI:. oE tte canet pagc.
. Re.portable D€rection Limit BRL = B€tow Re-portirC Lirhit Page I 14 of | 52
Page 518
SemivolNtile Orgrnic Compounds by GCMS - Quality Control
Spikc
E2t h m307a - sw8t6 35508Duollcatel703l27E{UPll Source:SA59S48{2P.epared: 22-{\,{ar{7 Analyzedr 23-MaF07
Alrarne
Azobenzene/Diphenyldiazine
Beozidine
Senzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fuoranlhme
B€rEo (g,h,l)perytenegenzo (k) lluoranlhsne
Benzoac acid
B€nzyl alcohol
Bb(zd oroetroxy)rn€thane
Bis(2d{orueihyl)ether
Bis(2+hloroi6opropyl )€therBir(z-ethylh€xyl)phthalate
4€romophenyt phenyl elher
8uM b€nzyl phthalate
Carbazole
4-Chloro.3-rhelhylphenolrt4hloroaniline
24hlorooaphlhalene
2-Ct orophenol
44hloroph€nyl phenyl ether
Chrysen€
Dibenzo (a,h) anthracen€
Dibonzofu€n
| ,2-Dichlorcb€nzene1 ,!Dichlorob€nzene'|
,4-Dknlorobenzene3,3
--0i,chlo|ob€n?idine
2,+Didlbrophenol
Dlethyr ph{hahb
Oimelhyl phlhalate
2,aoimef\ylphenol
Di-n-butyl phtt€late
4,60iniho-2fl elhylph€nol
2,4oinrtophenol
2,+Din rctoluene
2,6-Dinitolotuene
Dl-n{cM phtt'Elate
Ruorene
Hexad orobenzene
H€xad orobuladiene
Hexadrlttocyclicpsntadiene
Ind€flo (1,2,3-cd) pyrene
lsophorone
I -l,l€thylnaphtllalene
2#ethyhephtnalen€
BRL
BRL
BRL
BRL
ARL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
ARL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
8RL
ARL
BRL
BRL
ARL
BRL
BRL
8Rt-
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
ARL
ARL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
ldkS dry 231pdkS dry 231
lqkg dry 231
US/kS dry 231
!g/kg dry 231
!g/kg dry 231
!g/kg dry 231pS/kg dry 231
!g/kq dry 231!S/kS d.y n1
liS/kS dry 231
lqkS dry 231pS/kS dry 231pg/kg dry 231pg/kg dry ?31
US/kS dry 231
US4(S d.y 231
!S/kg dry 231
!g/kg dry 231lqkg dry 231pdkS dry 231pdkS dry 231pdks dry 231pg/kg dry 231
LidkS dry 231
!S/kS dry 231
!g/kg dry 231us/kg dry 231pdkS dry 231
!g/kq dry 231
lgkg dry 231pdkS dry 231pdks dty 231
ldkS dry 231pgks dry 231
ldkg dry 231
ldkS dry 231
!SI(S dry 231pg/kg dry 231pg/tg dry 231pdkS dry 231
!g/kg dry 231
!S/kS dry 231
ldkSdry 231pS/lg dry 231pdks dry 231pgks dry 231pS/kS dry 231pg/kg dry 231pg/kg dry 231
lgkg dry 231
ls/ksdry 231
ldts dry 2i1
BRL
BRL
BRL
ARL
BRI.
BRL
BRL
BRL
BRL
BRL
ARL
BRL
ARL
8RL
BRL
ARL
BRL
8RL
BRL
8RL
BRL
BRL
BRL
SRL
ARL
8RL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
ARL
BRL
BRL
BRL
BRL
BRI.
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
50505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050ff)
Thb lIbon1ory rcpoA is not laliil without za oaihoized sigrurwe on th4 cover page_
* Reportsbl€ Detection Limit BRL = Below Reponing Limit Page 135 of 152
Page 519
Semivolatile Orgrnic Compounds by GCMS - Quality Cortrol
Analytds) Flag UnirsSpikeLevel
Br.ct 703127t. SW846 3ss0B
Ouplicater703l27&DUPI) Sourcs:SA5O5a84t
Pr€pe.€d: 22-filar4TAnalFed: 23-Msr{7
2-lr€trrylpherrcl
3,4-lrethty'phenol
Naphthslene
2-Nitroanl ne
3-Nitroanilin€
4-l.lilrosniline
Nitrobenzene
2-Nltophenol
+Nibophenol
N.Nlbosodarnenhy'anin€
N-Nitrosodi-n+ropylamine
$Nitrosodiphenylamine
Pentacibrophenol
'1,2,+Trid crobGnzene
2,4,$Tridtbmph€nol
2,4,ETndrbroph€nol
S u nogaE : 2 +tuoft bip he n ylSunogate: 2+hn@phenolSuflggate: Niffienzeoe45Suftqate: Pheno!4sSunogale: ferphenyl4l4S u zog ate : 2, 4 6-ft i bmrnop henol
l|atir Soko (7o:tl 278{Sil
Prepared: 22+vlar{7 Anal).zed: 2}Mar-07
4€hbro-kh€th/lphenol
2-Chloroph€nol
1 ,+Di{$loroh€nzen€2,+Oinilrolol!€nerH{fuophenol
N-Nilrosodi-fl -propylamin€
PentaEhbaophenol
t,2,+Trichlorobenzene
Su/rogate: z-Fhnnbiphen ytSu'rcgate: z-Fh.toft pherolSunqate:Niffinzene4'Swmgate: Phenol4,Sunogal€: Tefienyl4!4Sur'ogale : 2, 1,A- Td b ft noph et'o/
gRL
SRL
SRL
8RL
sRrBRL
BRL
BRL
ARL
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
1480154t)1800t6@19fit2g)
Sourc.: 3A59548{2
32r059005530293J312037403260,1430
$7035S027103r90263037502491)37n26fr
IeHx Splko OtE fl031274- SDl) SoutE i SAsgstg-O2
Pr€pared: 22-lIaF07 Analyzedt 2?-Nlar 07
pgl€dry 231pS/kgdry 231
ldkg dry 231
ldksdry 231Idlq dry 231
t dl(s dry 923t|g4!S dry n1psnq dry ZJ1
Igr(S dry 9?3pCAgdry 231
!g\gd.y 231
Udl(g dry 231
rc/kS dry 231
ld].4dry 231
FdkS dry n1
trg,ll€ d.y nl
ldrg dry 2J1pgksd.y 231pdkg dry 231rdkS dry 231
ldks dryugt{gdtypdkg drytdkS dry!S/P€ d.ypdks dry
USnqdry 231lgkS dry 231pg/kg dry 231
t SI(S dry 231lJg/kS dry 231pdkg d.y 923pdks dry 231!S,/kS d.y 231UgrS dry 231UdkS dry 231
ldkSdry 231
Idks dryldlg dryrc/kS drypdks dryfgtg d.ypdks dry
m/kg dry 233t|gr'kg dry 83lg^gdry 233
FdkS dry 233
t4fts dry 23,:]ldkgdry qli
64 30-13066 15-11077 3G1m72 15-110u 30-13053 15-110
69 40-14t)63 3o-'t3o5S 3&13063 40.14067 {114040 3G.13070 4&t404a 30-13061 3G'r30t7 4o-14o58 {0.14068 n-131)58 11110a) n-19)53 tSlto&) g)-1tu56 1S-1rO
75 4&1,O74 30'13)64 3{tt3t)65 40.t4074 4[-14t)42 3Gt30
2330B:N?33{)nn23fr23m
4660
s32093204660
4660
9320
4660
9320
9320
4660
4660
16ffi16@16@4664166046ffi
470/)
94t0
9410
4700
4700
94t0
SRL
BRL
BRL
BRL
BRL
SRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
8Rr-BRL
SRL
SRL
BRL
ARL
BRL
BRL
BRL
8RL
BRLBRL6RLBRLBRLBRLgRt
BRLBRL8RLBRL
505050505050505u505050505050505050505050
44hloro-3-|nefi ylptleml
24hlorcphenol
1 ,4-Oi* orob€nzene
2,4-Dhitrotoluene
4+.litrophenoi
35206&106010305034603040
6310
30303)3030
Thb labdory Eporl B not efllid Nithou an authadad tlgndue oa ahe covet We.* Reportablc Det€ctiotr Limit BRL = Below Reportilg Limit Page 136 of I 52
Page 520
Semivolatile Organic Compounds by GCMS - euality Control
Anab,te{$ ResultSpike
Level
RPD
I- imi tFlag Units
Sour€e %REC
Resuli %REC Limirs
Brict 703127E - SW846 35508
t ardx Soike Ouo l7031278.trlsD Source: SAs9548{2Prepared: 22-{vlar.07 Anattzed: 23-MacO7
N.Nllrosodi{-propytamine
Pentad$rcpheml
| ,2,+Trinbrobenzene
Su nog ale : 2 +l tDto bi p he ny1S urog a te | 2 - F I u oto ph e notSunogate : N i t to be n ze ̂ e45Sunogate: Pheftt4sSunogale: Teehentt4l4S unogaE : 2, 4, 6 -Tn b ro nop h e rlol
Batch 70312t2 - SW846 35508
Bbnk 170312E2€LKi)
Pr€pared: 22.Mar-07 Anatyzat Z5,-M1.O7
Acenapht|€ne
Ac€nsphtfiylene
Aniline
Azoberaene/Diph€nyld jazine
8en/dlne
Eenzo (a) anthracene
B€nzo (a) pyrene
Benzo (b) f,uoranthene
8€nzo (g,h.i)perylene
B€nzo (k) fluo.anthen€
Benzoic acid
Ben2yt atcohol
Bis(2-chbroethoxy)rnethan€
Bis(2-chloroothyt )eh€rBis(2<ila{oisopropyt)erher
Bis(2-€thylheryl)phthatatezt8ornophenyt ph€nyt ether
Butyl b€avyl phthahte
C€tbazole
44hbro-3-methylphenol
44hb.oaniline
2{hloronaphthat6n€
2.Chh'roph€nol
4chlorophenyl phenyt ethe.Chrysene
Dlbsnzo (a,h) anrhrene
Dib€nzohrran
I JOlchhrob€nz€neI ,3OichbroberEene| .4-Didrlorobenzene3,3lDichlorobenzbine
2,4-Dkhlomphenol
Diethyl phthatate
Dlmethyl phth3ble
2,4-Dimethylpfi6nol
Di-n-bu!y' phhatat€
40305270641042702470347028203E502840445n2980
pS/kS dry
!g/kg dry
vsftg drypg/kg dry
Idkg dryydks d.y!g/kS drypg/kg dryldkg dry!g/kg drypdkS dry
4700941094tO47004700470047ffi4700470047m4700
40n4030-13030-13040-r4010-14030-13015-11030-13015-110u-t301Ul10
233
233233
BRL
8RL
BRL
BRL
BRL
1 5
1 1
1 7
5
3030303030
86
56
68
91
6 1
74m82609563
BRL
ARL
8RL
BRL
BRL
BRL
BRL
BRL
ARL
8RL
BRL
BRL
BRL
BRL
aRf
ARL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
us/KsUgJKg
!s/ksp9KSpg/(g
!gKsug/KgvgKsug/KgvgRgpgKsps/ks
Ljg(9
ugKgugKst g/Kg
!g/KgudksUEK9rjdkspslks
!g/KSut/KgpgKg
trg/xg!9xsgEr(9
lrdkspdks
fs/r(gl.r9/Kg!gKgugKgps/Ks
!g/r(9ugKspdkspsr(g
330330330303303303303303303303303303303303303303303303303303303303303303303303303303fi)3:}0330330330330330330330330
Thir labotuo,! r.potl it not ,otid xttrhaal an aalhorizpd sigaatarc on the caeu plage .'Reprtabl€ Derecrioo Limir BRL = Betow Reporriog Limir Pase 137 of 152
Page 521
Semlvolatile Orgaric Compounds by cCNIS - Quality Contlol
Analyiqs) Result Fl"S UnitsSource %REC
Result %REC Limits
Spike
Irvel
RPDLimit
Betch 7031282. SW846 35508
B|ank (7O31282€LKtt
P€pargd 22-lrar.07 Anavzed: z5-Mar-O74,6{)inibo-2fl etnyiphenol2.4Ohtropheool2,4-Dinibotolu€n€2.6-DinitrotolueneOa-n-oclyl ph[\abb
FluorgneHexaEfilorob€flzene
H€xachlorohJiadiene
Hgracnrorocydop€nbdiene
Hexachloro€lhan€
Indeno (1,2,3d) pyrene
1 {Iotryhaphthel€ne
2{ilelhyhaphlhalene
z-[{elhylphenol
3,+Me$rylphonol
Naphthalene
2+lfiroaniline
$Niboenflin€
4-l,,litoanihe
Nilrob€naene
2{,{ifophenol
4-tlilrophenol
N-Nibosodim6hylamhe
N-Nfi rosadi-nf ropylefi ine
N-Nibosodiph€nylamin€
Phenol
1,2,+Trichlorob€nzen€
2,4,FTdchbmph€nol
2,4.&Trichlorophend
S u 'rogata : 2- F I uotobip he nylS/uLircgale: 2-HuotophanotSufiWate: Nihobenzene45Sunoga/€] metp145Sunc€at€j Teryhenyt4l4S u nogale : 2, I,ETd Mo ipph a n ol
LCS O03'|242€Sll
Pr€par€d: 22-Mar-07 AnalFed: 2$tl€r{7
Ac€mphthene
Ac€naphthylene
Ardllne
Azobenzene/Dlph€nyldiazin€
Benldlne
B€nzo (a) anthracene
E€nzo (a) PyaeneB€nzo (b) nuolantr€rle
8RrARLBRL8RLBRL
BRL8RLBRLBRLBRLBRLBRI8RL8RLBRLBRLBRLBRLBRLBRLBRLaRt-8RL8RLARLBRLBRLBRLBRLBRL8RLBRLBRLBRtxM)71907890723098307591)
59205260B,RL63r053905490BRL430058504470
3:t0330330t30330330303303]03303,0330330330330330330303:]0
132033033013m3303303i'033030330330:l:]03:n330330
!dftsudkg|lgxs
PEK9
Itdkopsks
rgkgugl(sFdkS!dls!gl(s!gr€llgKg
udr€p€/t!9
pe/kg
FSikS
ugltsFgr(sudkgpdks
!dks|lgts|lgn(S!s4!srdksFdkstdkgps/ks
tldkgudkspdkspdks
udtsudks|ldks|lsftg!dkspsrkspdkst g/kg
pc,rsudks
m? ldkg|Jdkssdks!sftspdksggn€psftspelkg
30-13015-110wl3nt5-fi0m-tfr1EltO
{0-1fi)40-'t30{o-1304{} 1304G130,rG130
0-'t304o-r 3040-r304$ 130
330330330330330lxl0330330
frr0
13gn13W)13fi013fr0t&rot33N
66706€706G70
6670
66706670
5459547457
95
81
82
8079
6488
fhjj lahalorf r.pod b Ao, vaIU withont ., authodd stgaota'" orr thz covcr pge.
+ R@rtable D.t€dion Limi. BRI = Bdow Rcpoftine Limit Fag€ 138 of 152
Page 522
Semivolstile Organic Compounds by GCMS - Quatity Conarol
Analytd$) Resutt Ftaq UnitsSpike
Level Limi(sResult %REC
Brtch 7031242 -,SW846 J5fl)B
LCS r7clr282.BS1l
Pr€pated: 22-Mar{7 Analyzed: 25-MarO7
Benzo (g,h.i)p€ryI€ne
Be.uo (k) ffuoranthene
Benzoic add
Beoryl elcohol
Bis(2{hloro€thoxy)methane
Bis(2<hloroethyl)enher
Bis(2-cfi lo.oisopropylFlher
Bh(z-et'rylhexy)phthelate
4€tomophenyl phenyl eher
Bulyl benzyl phthalate
C€rbazde
4€hlo.e3{ethylphenol
44hloroaritine
24hloron+hlhalefle
2€ltoroph€noj
44hloroph€nyl ph€ny ether
Chrysene
Oibenzo (a,h) anttrracene
Dibenzoturin
1 2Oichlorobenzene1,3oid?b.obenzene
1 ,4-Othlofobeflzene
3,3 Oichbrobenzdine
2,4Oichlorophenol
Diethyl phlhalate
Ditrr€thyl phthalate
2,a€me(rylplrcnol
Di-n-butyl phthalale
4,6-{)iniho-2fl ethylphenol
2,4$inltophenol
2,4-Din botoluene
2,GDinitroioluen€
Oi+octyl phthal€te
Fluoranthsne
Hexaat$orobenzene
He)(d{ombutiadiene
Herachlorocyclopentadi€ne
Hexacirloroelhane
lndeno (1,?,3{d) pyren€
f -i,lethylnaphthalene
lsophorff\e
2-MelhylnapHh€lene
2{ilethy'pfEnol
3,:Aibrhylpr€nol
flEphthalene
2+{llrodniline
3-llilmaniline
4J,litroaniline
Nitrobenzene
2-ilitroph6nol
4{ifoph€hol
4660730038901380339054103730563055905550549050302820549041206500633040906030713032107070571043r051605020393055103690564051905710625C5790570068107410267063304090613055504410334045505810512028906010360040505050
330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330330
33033033033033033033033033033033013203301101320
6670
6670
6670
6670
6670
6670
6670
6€70
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
ffi70
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
!g/Kg
!gKs
!s/kgoc2 !g/kg
!g/Kg
tis,Ks
!s/Kg
!s/kspE(9
!dkslig/Kspsr(s
tigr(s!g/kspgr(s
!g/tsugKslis/Ks!dks!s/KswKs!s/Kslrg/Kg!9/K9vg/kgrc/kswRg!9/KSt/9/Kg!g/ksugKsirs/Ks!s/ks!g/|(gpsiks
!dksug/ksudkspgr(sp(/r(spgxg
lis/Ksw(sfg/Kg
w/I€
|ls/K9
utl/KsUI/Kg
!(vKgp9/Kg
ps/tspg/r€
70 40-130
109 40-130
58 0-130
21 40-130
51 40-130
87 44-130
56 40-'130
64 40.130
84 40-130
83 40-130
82 40-130
75 40-130
42 40-130
62 40-130
62 40-130
97 40-130
95 40-130
61 4G130
90 4G.130
107 40130
4a 40-130
106 4G130
86 40-130
65 4G130
77 40-130
75 4G.130
59 40130
83 40-130
55 40-130
85 40-130
78 40.130
86 40,130
94 40-1
87 40-130
85 40-130
102 40-130
l r l 40-130
40 40.130
95 40-130
61 40-130
92 40-14r)
83 40-130
72 4O-13r)
50 40-130
68 40-130
87 40-130
77 40-130
43 40.130
90 ,|(1130
54 40-130
61 40.130
76 4G130
Thb labodory Epor, is not volitt tritho4 tn a@hoized signatare on tlE cover pzge
* Repodable Detection Limit BRL = Below Reporting Limit Page 139 of 152
Page 523
Semivolatile Organic Compoun& by GCMS - Qoslity Cotrarol
Andyte(s) Resutt Ftas Unirr *RDLSpikelrvel
RPD
Limit
Source '/.REC
R€sult %REc Limi6
Brtch ?03 12t2 - Sw846 35508
LCS t7cll2€2€St I
PreDared: z+lsr{7 Anavlee 2s-Mar{7
N+lilro€odinFryamine
N-Nittosodi-n+ropylsmine
N.Nitrosod'pttentamine
Penta€$brophenol
Pyddine
1 2,+Trichlorobenzsn€
2,4,5-TrichlompherDl
2,4,&Trid orophoml
S u trogale : 2 +hn otE)h e ny'S utrogdle : 2+ fu o Eph en o ISu nogate : I'litroben nne4 5Sutr9gate: PheNl4SSunogatu: ferphonyld4Suftogale : 2, 4, 6 -f rib tu n o ph e n ol
Dupllcats oo3l282oUP1l
52503{5060903690337044tO61706't90641057303250696045e,393046706670628t)
Source: SA5945il-10
pdkg
!gkspsfts
l4^9Fg/kgpdks
Ltgt€t dl€ru/kovs/tspcftgpgkqttgksrcftspdk9tts1l(.spdkg
!dkgugl(srdksps/ks
ugkst dksTSAgpdks
!gks|ldksPs*s!grxgFS&Stdkspdks
|rsftgt€iks!sftspgks
!dtsrgkslrs/l€!dxgpdks
udks|ldkslryksTgKS
usrrcFdlSpdksp91€pdt€pgrs
6670667066706670667066706670667066706670667066706670667066706670
40.1304G1304$.13040-13t)4$.13040-1304G13{4Gr3040-t3040-r3040-130&tNt5tt0#14)15-110fr-ln15-110
79
gl
606793{xl9686491046959701(nM
3303303i]0330330330330330330330:}:10
Preparodt 22-fvlsr47 AnalFed: 2'Mar-07
Atrazine
Azoti€nzene/Diphenyldiazin€
B€nidin€
B6n2o (a) antlxacen€
B€nzo (a) pyren€
B€nzo (b) lluoranf|eneAenzo (g,h,i) p€rylene
Aenzo (k) ftDranthene
Benzoic 6cld
B€nzy' alcohol
Elis(2<hlorEtrcry)olethane
Ais(2drloro€tly')€tter
Bis(2d oroisoFopy')et|er
Ais(24tny$'6xyl)phfi alate,Sronrcph€rryl ph€fl yl erh6rButyl benzyl phtfrabte
Ca|bazole
4-Chloro-lm€t rylphenolrrchbmarilin€
24hhrcnaf*rBBbn€
2{hloropheml
44hlor@heny' phe.M eth€rChrys€ne
Drbenzo (a,h) anthraceneDlbenzofrrran
1 ,z-Di{$lorcbenzone
l.3oiJrbrob€nzene
I ,4oichlorob€nzeoe3,3'Oicrrlorob€nzldine
2,4oi('|loroph€nol
SRL
BRL
ARL
ARL
BRf
BRL
BRL
BRL
aR[
ARL
SRLgRL
BRL
BRL
8RL
BR|-
aRl
BRL
BRT
BRI-
BRL
BRL
SRL
BRL
SRL
BRL
BRI.
SRL
BRL
BRL
BRL
BRL
BRL
BRL
639
63S
639
63S
639
639
639
63S
639
639
639
639
639
639
63S
63S
639
639
639
639
639
639
639
63S
639
{r,9
63S639639639
BRL
8RL
SRL
BRf
BRL
ARL
ARL
BRI.
BRL
BRL
BRL
8RL
BRL
SRL
BRL
BRL
ARL
BRL
BRI
8RL
BRL
ARL
ORL
BRL
BRL
BRL
SRL
BRL
BR(
8RL
ARL
SRL
ARL
BRL
5050
50505050505t)5050505050505050
50
5050505050v)50
50
5050
50
Thb ,.bo.otarl' rzped ls aoa y.li.t at host on a horhd signer!rc or, ahe cover page.
r Repdtflble Dete{tion Lirnit BRI- = Betow Reporting Limit Page l40of 152
Page 524
Semivolati le Organic Compounds by cCMS - Quality Control
Source
Brrch 7031282 - SW84515508
Duolicate lm31282OUPlt SourEel 5A59464-10
Pr€pared: 22-[,f aF07 Analyzed. 25-Mat47
Oiethyl phtrlalate
Dimethyl phthalate
2,4-DirYEthylphenol
Oi-n-butyl phthalale
4,6-{)inibo-2nethylphenot
2,4.oi.|it ophenol
2,4-Dinilrctoluene
2,&Oinitrololuene
Oi{-octyl phdlalate
Hex&hlorobePene
Hsx{-hhobutadiene
Hexachlorocyclop€nhdi€ne
Indeno (1,2,3-cd) pyrene
1-{\rethyhaphlhalene
z+vlethylnaphthalene
2+,tethylphenol
3,+Methylphenol
Naphlhal€ne
2-l'lilro€niline
3-l.litroanilne
4-llitoaniline
Nitob€nzene
2+litophenol
4.f'libophenol
N-Nikosodimethyiamin€
N+liLosodi-n-propylamine
N-Nilrosodiph€nylamine
Phenanlhene
Pyddine
1 2,+Tichlorobenzene2,4,$Trichlorophenol
2,4,6-Tdchlo.ophenol
Su trog Ete : 2-F I uoro h i ph e n yl8u rogate : 2-F | @roph e rc ISuttogale : NifiDben za ne-d 5Sufiogals: Phercl4sSumogale: Teryhenyl4l4S utogate : 2, 4,&Tn bo no p h en ot
BRL
BRL
BRL
BRL
ARL
BRL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
8RL
BRL
BRL
8RL
BRL
8RL
8RL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
s310t03043203850574n3270
PEKg
l.rglKs
tg/Kg
!s/Ksrdkspgr(gpdks!E|<Spdks
pdks
!9Kgpgrls
pg/i(l
ps,K9
!gitqpgxs
uEk9
t gKg
pgxs
!9K9
!g/Kg
us/Ks!dksLr(yK9
|lg/Kg
us/Kspgfts
t gKops/ks
!s/kgps/ks
ugrspgts
l'|dksudksp(y(gpdrs!s/ks!s/kg!dks!9Kg!g/KgugK9ugKg!9/Kg
63S
639
639
633
639
639
639
639
639
639
639
639
639
639
639
639
639
63S
639
439
639
639
639
639
2560
639
639
2560
639
639
639
639
639
639
639
639
63S
639
639
BRL
BRL
ARL
BRL
ARL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
ARL
BRL
ARL
ERL
8RL
8RL
BRL
BRL
BRL
BRL
505050505050505050505050505050505050505050505050505050505050505050505050505050
129001290012fi0129001290012900
34-1m15-11030-13015-1103o-13015-110
3330
25
This lobo.slory Epo is not velid *llhout ar, caahofiazd signaaure oa the clrver page
* R€portable D€t€.tion Limit BRL = Below Repding Limir Page l4l of 152
Page 525
Totrl Metals by EPA 6fi)0/7000 Series Methods - Qua[ty Cotrtrol
Anab,l{s) R€suh FIag RPDUnits IRDLSpike
L€vel
Sourc€
Re3ull %REC%p.EcLimits
RPD
Limit
Brach 703 1306 - EPA2{XySW70{0 Serica
B|8nk O031306-ALKll
P.eparcd: 23diaF07 AnalFed: 26{,tar{7
t uolicels (7031305-DUPI) Sourca: SAlsgLil{z
0-604
1_00
Sourc.: 3A5946440
BRI
Sou.ce: 3A5046+10
mSlkS rvel
OR5 mdkg dry
mg'kS dry
|rE]fg wel
89 75-125
8a 65.S132.6
8Rt
0.350
0.463
1 . 1 3
0.0292
o.033:]
0.0300
0.107
0.190
Prep€red: 23-lrar-07 Analyzed: 2&I|,tar{7
20370_0345
lratlx Solke ft03l106{31) Souicei SA5946a4
Prepored: 23-[,tar-07 AnalFed: 26-Mar-07
Mercury
Rsf..€nc. rTqll306-SRHi IPrepared: Z3-l ar{7 Anal]rred: 26-irar47
Brlch 70ll3rl - EPA200/SW70m Eeri€s
glank 17031111€LKII
Pr€pared & Analfz€d: mjvl{{)T
Duollc.t r03l3l1{ruPPrepa€d & Analyzed: m-Ma|{7
Marnx Sdk. r0313ll.ilsll
Prepared & Analyzed 2AMar-O7
Renaftnc. O031311€Rirll
Prepared & AndFed: 26-Mar-07
Bstch ?03 1315 - SW846 300sA
abnk l703r 3t s€LKt )
BRL ndks o_0292
fi€n(g
rng/kg
BRL 20
0.4440.4700.,tEso.4720.5230.4350.496
0.449o.442
mc4nE/lmg/ntsnmgilftsnmgr
r€nms,l
0.01500.00750.00250.00500.00,r00.00500.0050
o.00750,01500.m50o.00400.00s00.00500.0025
0.00750.0150
0.4t4
0,5000.5000.5000.5000.sfi)0,5000.500
0.5000.50()
SRL0,029E
0.0300
a5 71125
1't 1 65 9-132.6
P.dpar€d: 23-lrariT Analyzed 24+ii.at47SeleniumLeadCadmiumChromium
BsriumSilver
LCS fim€i5€St)
Prepared: 23{itd{7 An€lyzei 2+Mat 47LetdSekfliumChromium
BaaiumSilv€rCdmium
LCS Osp ftml3l$ASDIl
Prep€redr 23-Mar-07 Analyzed: 24-lrar{7LeadSe[,tntum
124 |rElfts
BRL msn
SRL mgL/l
BRI mgl
8RL mgl
BRL mdt
BRI .ng/l
BRL mSrI
s7 a5-11594 8911597 8911594 85115t05 8s11587 85-115100 E$115
s8 8$.115sG 85-1t5
mm
Ihb lzbororory .qort ls not valid w hru an at $orlzz.t signatar. od the cover INg... Report&ble Det€clion Limit BRL = Below Reporting Limir P.ge 142 ot lS2
Page 526
Total M€tNls by EPA 6000i?0{0 Series Methods - Qualit} Control
SpikeL€v€l
%RECLimits
RPDLimit
Sourcc
Result %RECAnab4{t RPD
Brtch 7031315 - SW846 10054
LCS Duo O031115€SDl)
Prepared: Z3-l\r€d7 Anal:Fed: 24-Mar01
Chaomium
SilYer
Barium
Cadmium
Pr€psred: 23-[{ar{7 Analyzet 21-Ma(O7
Lead
Sel€nium
Silv€r
Earium
Cadmium
Chromiuft
Prepa.edi 23-irar-O7 Analyzed: 24-Ma(47
Leed
Solsnium
Cadmitlln
Situ€r
Barium
Chroini{rfh
Selenium
ChromlumSilv€rC€dmiumgadum
Post so[(g f7(x]t 31 s+st I
0.4910.4390.4900.5830.515
ARL
ARL
BRL
0.0060
0 068a
ARL
ARL
0..{48
0.440
0.497
0.440
o.572
0.446
0.490
mg/l
mg/l
mg/I
QC3 mg/l
mgn
0.00500.00500.00400.00500.0025
0.00750.01500.00500.00400.00500.00250.0050
0.00750.01500.00250.00500.00500.00100.0050
0.0'1500.00750.00500 00500 00250_00500.0040
0.00750.01500.oo500.00400.00500.00500.0025
0.5000_5000-5000,5000.500
98 85t15 I
88 E5-115 0.9
98 85-115 4
111 85-115 11
103 85-1 15 3
6
0.4
75-125
96 75-125
99 7s-125
86 75-125
104 75-125
96 75-125
98 75125
96 75-125 0.2
96 75,125 0.8
s8 7t125 0.2
a6 75-125 0.5
99 75-125 0.4
103 75-125 0.7
11125 0
2020m2020
Duollcato lm3l3l5-DUPll Source: 5459424.01
mg4
msrmsrmg/rmg/lmgnms/l
mgnmsnms/rmg/l
msl
msfl
mgn
mg/l
ng,'l
msl
msn
msrms,4mg
mEl
nEI
r'gnfi1gI
rng/l
rngn
rngn
0.5000.5000.5000 5000 5000_5000_500
0.5000-5000.5000.5000.5000.5000.500
0.5000.50uo 5000.5000_5000.5000-500
0.00230.0otr0.0M60 00650.0892BRLBRL
0.0064ARL
0.00r60.0076o 05220 0M0ARL
BRL0 0064BRL
0.00760.00160.05220.00+0
m202020202020
t{arfi x Splk. n03r315.MSt I Source: SA5930O{I5
ll.tix gEike Duo |1031315{SO1) Sourc.: SA5{ty)0{5
Prepared: 23-t\,lar-07 Analyzed: 2+MaF07
0 481
0.4€4
0.489
0-438
0.499
0.568
0_486
Source: SA59300.O5
2020m20202020
Pr€pErcd: 23-Mar-07 Analyzed: 24{ra.-07
Lead
S6lenium
Baiium
Silv€r
Chromism
Cadmium
0.0064 102 80.120BRL 116 8G120
o.o522 111 N-1200 0040 107 80.1200.0076 88 80-120BRL 105 80-120
0.0016 108 80.120
0.5140.542o.6480.5380.4460.5240 542
Thh labodory Epnd is nor |slin w hod an aurtodzed signzlare on the .oee, page.
'R€port ble Detection Limit BRL= Below Repodng Limit Page l4l of 152
Page 527
Total M€trls by EPA 2fi) Series Methods - Quslity Cotrtrol
A""lyt.{0 Result Flag Unils .RDLSo rce %REC
Result o/oR-EC Linits
Spikekvel RPD
RPD
Limit
B{tch 1}31263 - f,PA 200 Ser{et
Bl.nk rT0ll2dtALKllPrepared & Analyled: 2AMar-07SsleniumCadnium
ChroarturhBarlJmSilv€rL€ad
Duotlcat {70312GHruP11Prepared & An€lyzed: 26-Mar-07Sel€nium
AariumCedmiumSituerChromium
Malrix Splk6 fl031263{ilsl IPrepared & AnalF€d: 26-Mad7Sel€niumC€dmlum
BdiumLeadClrromiumSll'rer
t{atlx Solk 4031269{52)PrEpared & Anal)/"2sd: 2GMar{7Sd€niumBariumC€dmiumSilverChmmium
Lead
Po3r S.tro ?03126+PSl)Prepared & Anelfzsd: 26-rrar-07S€l€r umBaaiumCedfltiumSlr€{Ctrro|nfun
Reb.t||c. O03126&,sRt{l)Prepar€d & AnBlyzod: t8+tlar{7S€l€nlun
gartum
ChromiumL€6d
Cadrdum
BRLBRLARLBRLBRLBRLaRl
SourE : S450464-lE
BRL0.stx10.2
0.5€8BRL1.S84.75
Sosrc€: SA50,l€+10
mdxgntgl(grYtSn(gmg/kgrrEJI9mcl(grgls
rngIq,nigrkgmsasmS/k9dr€n(gmSlkSmsas
lr€/kS
$tgrkg
m€rkgnlg/kgn€ftsmgt(9rEItS
mSI(S
ngrkg
firS*0
mgfts
ntSftS
mg/kg
ntg*g
msasmgasm94(gfirg^SmSrkS
1-1801,161.400.4920.4s20.9850_734
r.401.,t00.{670.2330.934o4670.700
1.40o.2341.400.4680.701o-4640-935
1.430.4760.2380.953o.1761.430.715
1.400.468o.2u0.935
0.468.t_40
1.50
1.50
0.500
0-500
0.750
o.250
BRL0,502r0.6
0.626BRL1.S75.08
0.s47o.5060_sso13.23.78
ARL
0_55346.8t . 9 lSRL9_311.242r0
o.u713.2
0.506BRL
0.590
o.465
o.57
35
3535
a5
10f
97-S
100
t 1 9
97.4
t02
1(b
Sourcs: 5A59569{i
1 t s
r60
t 1 0
1 1 0
1 1 8' 1 1 1
386
Sourr.: SA59,164-'10
nS'l(]g
mqx9mS/k9rEn(omgftsmS/kS
oM4X frE^o
100 7o-1?o95 7G13091 7G13t)92 70-13091 7G13092 70-13o148 70-130
93 81115!0 85-ll585 8t1t592 85-11565 8t1158ll 8$r 15
100 77.+12268S 80.&r',19.4N 82.7-117.305 78,$.120.566 81.&118.193 82,1-117.9
117
117
117
117
117
117
1 1 9
1 r 9
l t s
1 1 9
1' t9
1 1 S
1 1 9
117
11f
117
117
117
117
N.2
46.0
41
50.7
46.0
32.6
70-r 3070-13070-1307G13070-13)70-13070130
91E3
so80u90
't to11899.8108't03
r03
80.441.1zx)43.339.630-3
Thb hbo.obry tqor, is nat wlil flirha4 an acthori?d sk u!u. on ahe coEr pq. -
+ Reportibl. Der€ction Limit BRL = B€low fupoding Limit Page 1,14 of 152
Page 528
Total Meaals by EPA 200 Series Methods - euality Cootrol
Spike Sourc€
B{tch 7031263 - EPA 200 Series
Rei.r.nce 1703l263-sRMl I
Pteparod & Analyzed: 26-Mar-07
Silver
Brtct 7frllJ05 - EPA 200 S€ri€s
gl.nk 170:11305-aLK1l
Preparedi 23{vlar{7 Anatyzed: 24-MaF07
42_240.2 m9/kg 95 66.3-133.6
Prepared: 23-l\,{ad7 Anatyzed. 24-Mar-07
SiverSeleniumLea0
CadmiumChrofti(nnBanum
Dqellcaas t7031305nUP1)
S€l€nium
Silver
L€€d
Cadmium
Chrcmium
Bariuh
l|.dr Spik 17031305{51)
Sdenium
Sllve.
Chromi(m
Cadmium
Esrium
ilatir Soik€ (703130tMS2t
Sel€t um
Silv€r
Lead
Cadmium
Cttromium
Badum
Fosl $plke fl031 305-PS1 |
BRL
BRL
8RL
BRL
BRL
BRL
ARL
Sou.c€: sA59442.{2
128
1 1 8
138
446.t4E
1 3 1
197
Sourc€: SA5950ru1
125
1 1 1
120
1 1 7
124
122
153
Sourc€: SA5946d-02
mg/kg wel
mg/kg wel
mgeg w€r
mgukg wet
ftE kg w€t
mg/kg 'fl€t
0.936
1 4 0
0 936'1.40
o.234
0.468
0.468
1.54
1.05
1.58
1_05
0.263
0.526
0.526
1.62
1.OE
1.62
1_08
0.539
0 269
0.539
1_48
0_989
0-742
o_247
0.495
1.48
0.495
1 _ t 2
1.69
0.562
1.69
0.281
1 . 1 2
0.562
135'135
135
135
135
135
135
124
124
124
124
124
124
121
141
141
141
141
141
141
141
BRL
1 . 3 7
13.1
28f
1 1 8
21.6
266
BRL
SRL
1 4 4
I
25.O
1 6 8
53.6
BRL
8RL
6.37
o o5r29 2 8
4.69
28-8
aRL ftg/kg dry0.856 J,OR4 mg/kg dry6-74 QR1 mg,fkg dry160 aRs nrg/kg dry
0.510 QRi mdks dry
18,5 mg/kg dry106 OR5 nsrkg dry
Source: 3A59116+02
46
64
57
79
1 5
86
35353535353535
P€par€d: 23-lrsr{7 Anallrzed: 24-Mar{7
Prepared: 23-l\iEr47 Anatvzed. 24-Mat47
mg/XS drymgl(g drymg/kg dry
o,v8 ng/kg drymg/kg drymS/kg dryng/kg dry
95 70{3087 70-13092 70-130132 70-13091 70-13096 70-130106 70-130
101 70-13090 70-13092 70-1A)s4 70-13093 70-r 3095 70-130100 70-130
Pre9ared: 23-llar-07 Analyzed:. 24-Mat47Sit/€rS€lertumCtuomium
CadmlumL€edBaaium
R€fe.ones {70t1305-5RilllPr€par€d: 23-fr.tar{7 Anslfzed: 24-Mar47
123
145
154
146
136
422
199
mgftg drymg./kg dryr(]g,l,(g drymgftg drymgftg drymg/kg drymgl(g dry
rng/kg dryngRS drymgl(g drynEftg drymg/kg drymSftg drymg/kg dry
aRL 87 8$115
BRL r03 85115
25.0 91 85-115
14_4 93 85-115
1.64 95 65-115
26A 10S 85-115
53.6 103 65-115
This lahorator, rcport ls nol oalu fiithoat zn zurtoi@d signztare on lha.wet page.
i Reportable Detection Limit BRL = Below Reporting Lrmit Page 145 of l \2
Page 529
Totrl Mearls by EPA 200 Series Methods - Qtrality Cotrarol
Analyds) Result UnitsFlag Result %g.Fc Limirs RPD
B.tcb 703t305 - EPA 200 Serica
R€turence f703lm5.sRilllPrepared: 23-{\rar-O7 Analyzet 214ta(47SilverSeleniumL€ad
Chromium
Cadmlum
Barium
Bat h 7031316 - EPA200/SW7000 S€rie!
Bhnk {m3l3l6€LKt}
PrBpar€d E Anelyted: 23-lvlar{7
LCS O03l3l6331l
Pr€pared & Aialfzed: 23-ilar47
Ouolicsie r0:1131&DUPI I
Prepared & Anayzed: 23-M€r-07
t{strlx Soiko OGll3lGHSll
Prepared & AnElfi€d: 23-l{ar-07
atrtx Solke Duo fl03l3lG*lS01l
Pr€pared & Anarfz€d: 2!Mar{}7
Llercury
Posl Solke ft03l316€5l I
Prugsrcd & A^alfzed: 23-M€r47
34.574.O34.339.0
26.Srgo
fiig (gwet 1.00
nEikgwel |.50
nEril(g w6l 0.750
dElkgwet 1-50
mgfigw€t 0-500
rig/kg w€t 0.250
mgftSe/st 0.5fi)
66 &133.6l7_+1?2.481.&1r8.180.8-119.478.9120.582,1-r17.9a2_7-117.3
11_2
78.3
44.9
44-S
49.5
31.8
216
0.00250
8S1t5
64
a5877684EA
0.00265
Sourc€: SASg,lS+17
8RL
Source 345945+19
o.00266
SourE€: SA59,16+19
0.00279
So{rc€: 5459464-19
8Rr-
0.00267
0-00005
0.00005
75-125
73-125
4t115
fngn 0.00020
ITE/I 0.00020 o.00250
flr4,4 0.00020
rE/l 0.00020 o.@250 0.00005
0.00020 0.0025nm9/l 1 1 0
lr'sl o_0m20
Thb loborstory rqort h rral ecli.I tuElaat on otrtofiEd s,gntat on ttg @vd page.
'ReporEbl€ Detectioo Lini! BRL = B€low R€porting Limir PtgE ta6 of 152
Page 530
TCLP Metals by EPA l3l | & 6000t000 S€ries Methods - Quatiay Conarot
Analyte(s) Result Ftog Units *RDLSource %REC
Resuk %REC Limits
Spike
Level
RPDLimitRPD
Bricr 70313?5 - SW8{6 30r0A
Blank n03132$ALK1)Plepar€d: 23-{rraF07 Analyzed. 24-Ma.47Selenium
ChromiumCadmiumSilv€rAarium
LCS 17031325€SPrep€|gd: 23+,,lar-07 Analyzed: 24-Ma'{ 7SeleniumL€ad
Sllver
Hmium
Cfuomium
Barium
l-CS Dup f'03132$Bsol)
Prepared: 23-{\,,lar-07 Anal)r2ed: 24-Mar-07
Lead
S€lenium
Sih€r
Cllfomium
CadiYumgadtj{n
BRL
BRL
BRL
BRL
BRL
ARL
8RL
1.33
1 . 1 3
1 . 1 3
1 . 3 1' | .25
1 . 2 1
1 . 2 1
1.08' | .27
1.07
1.20
1 r 5
1 . 2 5
1 . 1 4
0.0140BRL
0.0034BRLBRL8RL0.100
mg/l
rEnr!)9fl
m94
mg/l
mg/l
mg/l
mg/l
mgn
mg/l
nEx
mg/l
nEI
MEI
mg/l
mgn
nEn
mg/l
m9/l
mg/l
mgn
mgn
rhg/l
mg/l
mgn
rngn
mg/l
mg/l
r€nng,'l
mg/l
rng/l
ng/l
mq/l
ft9.i1
rng/l
rhgl
mgI
nE,4
rngn
0.01500_00750.0r500.00500 00250 01000.0050
0.01500.00750 01000 00250-01500-00500.0050
0.00750 01500.0't000 01500.00500.00250 0050
0_00750.01500.00250.01500.00500.01000.0050
0.00750.01500.01500 00500.01000 00250.0050
0.00750.01500_01500.00500.0r00
1_25
1 . 2 5
1 . 2 5
1 . 2 5
1 . 2 5
1 . 2 5
1.25
1 . 2 5
1 . 2 5
1 . 2 5
1 . 2 5
1 . 2 5
1 . 2 5
1 . 2 5
106 77.1-123
90 73.6-107
90 55 1-124
105 &3.4-111
100 75.+11S
97 N.7-110
97 86-117
86 73.G107'to2 77.1-123
a6 55.1-124
96 75.9-119
92 80.7-110
100 83.4-111
9 1 8 6 - 1 1 7
5
5
5
5
5
5
20202020202020
OuplicaL fi03l325nuPl I Sourc€: 345946+i6
f atrix Soik6 17031325.Ms11 SourEei SA5!146+15
Preparedi 23-Mar.07 tul€lyzei: 24-Marjt
Le€d
Sds um
Cadmium
Chrofiiufir
Sdver
B€rium
Prepared: 23.Mar-07 Analyzed' 24 -Mat 47
Selsnium
Chromiom
Sllver
C€dnium
furium
L€Ad
S€l€nium
Aasenlc
Chromium
Silv€r
t .tslr Solte Duo ft03l3z5{SDll Sourc€: 5A5946+15
Pr€pd€d: 23-Mar{7 Analyzed: 24 -Mat 47
1 . 1 2
1.27
1.20
1 . 1 6
1 . 1 0
1,25
1.25
L09
1.24
1 . 1 9
1 . 1 5
1.()9
1.25
1.25
125
1_25
1_25
1.25
1 2 5
1 . 2 5
1.25
1 . 2 5
1.25
r.25
0 0 1 3 5
BRL
0.0040
8RL
BRL
aRr0.105
o.02440.0063ARLBRLARL
o.00500.0761
4.02440.0063BRLBRLBRL
88 70.1109
101 78_8-120
96 81.4-114
94 767-115
88 59.6-115
100 a17-107
94 84 5-116
85 70_1-109
99 76.0.120
95 61.4,114
92 76.7-115
87 59.+115
32
0.83
0.9
2020202C20m20
2020202020
Thk hboratory repod it nor vdil withad on eurtoired signrtu,e od the covgr page .
' Reportable Detecrion Limit BRL = Belov ReI'odDg Limit Page 147 of 152
Page 531
TCLP Metals by EPA 131I & 5000/7m0 Scries Methods - Quality Control
Analyte(s) Result Flag Unr|l +R-DLSplke
L€v€l
Solllce
Result ./.RICo/.REC
Limils RPDRPDLimit
Bsrch 703r32s - SW846 3010A
tlatix Solk6 Ouo ?0313i15-t{Sol} Sou.ce: 5A!1016+15Pr€paredr 23-Md.07 Analyzed: 24-ltal{7
C€dmium
Barium0.0050 s7 It.7-1070.0761 92 84.5116
0.0063 102 79-5-122o.o241 88 75.5-102sRL S6 8'1.8-10SBRL 98 65.d-114BRr- 98 823-115
0.0050 100 81.9-t100.0761 96 M.7-fi7
122123
|r1S{
msn
flgn
mdl
ndl
nsnmsnn€,
rndl
0.002s0.m50
001500.0075o.0(500.01000.ot500.00250.0050
1-25125
1.251.251-251251.25|.251.25
2020
Posr SoH€ 47031325+St) SourE€: SAlll!l6a-15
Preparedl 2$Mar{7 Anatyzed: 24.tAet 47
Selenium
Leeo
Chromaum
Silver
Cadmium
Bsnum
Brrch ?03 1326 - EPA200/SW7000 Se.k's
Blank l?031326€LKl)
Prepared & Andyz€d: 23-Mar-07
LCS 17031326€S
Prepared & Aneiyzed: 23-Mar-O7
Dupllcate rtrutt3?6{ttPlI
Prepared I AnatFed: 23-Mar-07
matrlx Soik€ ?O3l32SllS1l
PreFred & fuiall.2ed: 23-Mar-07
[atrix Splke Duo ftoll326-f,SDll Source: SA.l9a6a-t5
nEI 0_00uo
nEn
mdl
msrl
o.0oor'o 0.00250
o.o{txo
0.00(xo 0.002so BRL t09
rftdl 0.0m40 0 00250 8RL 104
nE,l' 0.00(x0 o00250 BRL 112
0.m257
Source: SAsg,[a+lC
BRL
Sosrc€: SA5g4S{-15
r281 . 1 3
1.19
1_23
1 2 2
126
1.27
gRL
o.00273
r03 63.$124
Prepar€d & Analyzed: 23-Mar47
PGt Soike l-fl):ll 326PSl I
PreFred & Anall.zed: 23-Mar47
0.00265
Sou.c.: S4!19{6+15
53.'t-126
53-1-126
85115
m
o.oo27s
fhh ltb.otory rcport Is trot edld *irtonr tn adhoriltl sigt aitE oE th. coeq We.+ Repo.table De{.dion Lidit BRL = Below R€portirg Limit P.ge 148 of I 52
Page 532
SPLP Metals by EPA l!12 & 600011000 Se €s Methods - Quality CoDtro.
Spike
Lev€l
%REC
Limits
RPDLimit
SourceResult %RECResul( Flas Units RTD
Bstch ?031123 - SW846 3010A
Bhnk fl03t323{LKtlPrepar€d: 22-Mar{7 Analyzed: 23-Mar-O?SelenlumLeadCado umSilver
CiromiumBadum
LCS f70313zlast I
LOa6
SelsriumCdmiumChtomlum
Situ€lgarlum
LCS Oup ft031313-BSOI )Prepared 22-tr,f ar-07 Analyzed 234,iar0zSeleniumLead
ChromiumCa(mfumSdv€rBarium
ARL
BRL
BRL
BRL
sRt-BRL
BRL
1.20' l -14
' t .15
o_771
1.25
1_09
1 1 6
1.08
1 . 1 4
1 2 l
0.900
1 _ 1 8
ntsnmqnmg/|mgnm9/lmsrmgn
mg/lmsflmg/1mg/tmsflmsnmg/l
ng/lmg/rmgrnE/lnE/llng/lmg,l
mgn
mg/l
mgr
mg/l
rngn
mgrmsil
mg,1
lngr
mg/l
mg/l
mgn
mg/l
mg/l
msrmg/lmgnmgnmgn
0_01500.00750_00250.01000.01500.00500.0050
o.00750.01500.00250 00500.01500.01000 0050
0.01500.00750.01500.00500.00250.01000.0050
0.0r500.00750_01000.01500.00500_00250.0050
0.00750_01500.00250.01000.00500.01500.0050
0.00750.01500.00500.01500.0100
1.25
1 . 2 5
1.25'| 25
1 . 2 5
1.25
1 2 5
1 . 2 5
1.25
1.25
1.25
1 . 2 5
1.25
1.25
96
91
9t)
92
91
62
100
87
93
E6
9 1
s77294
82.3-108
79.106
87.9-110
76.2-114
77.4-109
55 5-115
8 5 . 1 - 1 1 9
79-108 4
82.3-108 3
f7_4-109 5
76.2,118 0 9
87_S-110 2
55.5,115 15
8 5 . 1 - 1 r 9 6
81.&10580-4-10586.+10863_6-10981 5 -11179.2-10688.9-114
81.0-105 280,+105 281 .5 -111 279.2.106 263_6-109 0.8
OuCicaie 1703l323OUPl) Sourc€: SA59,l6a-02
20202020202020
20202020202020
flabir Sprko ft00t323-tI3t] Solrce: SA59,t6.l-o,
Prepared: 22-l,,f ar{7 Analyzed. 24 -MaFO7
Selenfum
Lead
Slver
Ghaomium
CEdr*um
Barium
Prepared: 22-ll,f a.-07 Analyzed: 23-Mat47
Lead
S€l€nium
cadmium
Silv€r
Chro|rfum
Bsrium
L€adS€l€niumChromiumArlenlcglwr
ARL
0.0512
BRL
BRL
0.0109
ARL
0.0168
1231 1 6127
0 9521.20r .16126
IaHr Solke DtE 4f031323-t{sD sourcsr sass.t6{41Prepar6d: 22-t ari7 Analyzed: 234nat47
1.21
1 . 1 4
1 . 1 6
1 . 1 4
0-9,14
1.25
1.25
125
1_25
1 . 2 5
1.25' | .25
BRL0.0507ARLARL
0 0105BRL
0_0170
o o21t8Rr
o.0004ARL
o.0122BRL
0.0120
0_0217ARL
o.0122ARLBRL
97
93
102
95
s3100
95
91
93
91
76
2020202020
Thit |tborotor! fqon is Eot vrtd h'ithou an t,tlho?ized signzlan on lhe cover page .
r Reportable Detectior Limit BRL = Below Reporting Limit Page 149 of I52
Page 533
SPLP Metals by EPA f3f2 & 6000t000 Series Methods - Qmlity Conarol
An ytqt RPDResuh Flag UnitsSpike
trvel
So{rce
Result
RPDLimit./oREC Limits
B.tcl t03l32f - SWE45 3010A
litrdx Srlke Duo 17031323- SOt) Source: SA5!X6,!lllPreparcd: 2241er47 AndFedr 23-MarfiCadmiumBa um
m20
'100
98
Po.l Soike 170:rl 3:llPsl! Sourc6: Srt5g464{l
1.25
1.24
1 . 1 3
1.20
1 . 1 7
0.9m
124
1 1 3
1.23
msrmgn
m9/lfiEnmgnmsnnEntlEilmgn
0.00250 0050
0_01500.00750.00500.01000-00250.01500.00s0
1.251.25
1251251.251.251.251251.25
0.00010.0120
BRLo.Dzl7o.01nBRI.
0.oflxBRL
0.0120
66.+108
88.9114
77.7-108
80.3-108
78.1-ll4
61_7-107
86-9109
79.3-107
86.8-118
Prepared: 22-frar-07An€lyzed: 23-Mar.O7SeleniumLeadChromiumSikerCadmium
BEdum
B.hh 7fi11324 - EPA2|XySW7000 Se.ies
Ahnk rm3l324€LKl)Prepared: 22-llaF07 Analf!6d: 23-MaF07
909493t8sg90s7
8RL ng{ 0.000{0
nvn 0.00040 0.m250 109 86.&117
108
LCS r703t324-A5t)Prepared: 22-MaF07 Anal}.zed: 23-Mar{7Mercurt 0.00273
P@parcd: 22{-f€r{7 Analyzed: 23-Mat 47
Ouollr5t 17031324-DUPI ) So'rrc€: 5A5046.1-02
nrdl 0.00040 ARL
l|.tsix sotks fl03132+us1l SourE€: 5A50461.{ll
Prepared: 22-llar{7 Analyzed : 23 -lfiatrA7
ti4€rorry O_0/J272
Matrlx Soike Duo t?03l32il-llsoll Sourc€: SA59a64{t
Preparedi 22.1!lar4TAnsl].zed: 23-Mar{7
Mercury 0.00270
mg/l 0 00040 o.00250
General Cbemisary Parameaers - Qurlity Cotrtrol
76,1-111
76.t -111nE,ll 0.0@lO 0.00250 8RL o_7
Analyte(s) Reslllt
SourceResult
R.PDLi(rritFIac Units ./"wc Limits
B{tcb 7031317 - CeDeral Prep.rrtloD
Duolharel7oSlloTOUPl) Source:SA59,l5,l.OlPreptred & Anal}l.zed: 22-Mar-07% Sorids 89-1 % 87.7 2 m
Ihir lobontury Epoll ii ,,ot vzlid wirhoat an a$thoriaed ttF rzftln on thc @ru pge.
'Rcptrbble Det€ctioo Limit BRL = Below Reponing Limit Page l50of l52
Page 534
Notes rnd Deflnitions
*TPH Calculated as
Coop Completed
FP Field Preserved
QCI Adalyte out ofacccprance fange.
QC2 Analyte out ofarceptance ratrge in QC spike but Do reportable corcentration present in sample.
QC3 The spike recovery is outside acceptable limits for the LCS. The batch was accepted bascd upon the MS and/or MSDmeeting the LCS limits cliteria.
QM4X The spike recovery was outside ofQC acceptance limits for the MS, MSD and/or PS due to anal]4e concenfiaLion a14times or gr€ater the spike concentration. The QC batch was acc€pted based on LCS and,/or LCSD recoveries wiihtn theacceptance limits.
QM8 The spike recovery exceeded the QC control Limits for the MS and./or MSD- The batch was accepted based uponacceptable PS and/or LCS recovery.
QRI Analyses arc not controlled on RPD values fiom sarnple concentrations less than l0 tim€s the reporting timit. QC batchaccepted based on LCS and/or LCSD QC r€sults.
QR2 The RPD result €f,ceeded the QC control limits; howevet, both petcent recoveries were acceptable. Sample .€sults for ihe
QC batch were accepted based on perceDt recovedes and completeness ofQC data.
QR4 ABalyses ate dot controlled on RPD values from sample conceltratioos less !ha$ thc reponing limit. QC batch acceptedbased on LCS and,/or LCSD QC results
QR5 RPD ou! ofacceptance rangc.
R03 The Reporting Limit for this amlyte has been raised to account for interference from coeluting organic compoundspaesent in the sample.
Elevatcd Reponing Limits dw io the presence ofbigh levels ofDoFtarget analytes.
The sunogate recovery for this sample cannot be accurately quantified due to interference ftom coeluting organiccompounds pr€scatt h the sample exract.
vexl Lab extracted
veto Field extracted
BRL Below Reporting Limit - Analyte NOT DETECTED at or above the reporting limit
dry Sample results reported oD a dry weight basis
NR Not Reported
RPD Relative Percent Difference
A plus sign (+) in the Method Reference columl indicarcs the method is not accredited by NELAC.
R05
s02
Thk lsbonlory rcporl k Eot volitl t ithou al authodzed signaturc on thz covet page.
' ReDortsble Deterlion Limit BRt = Below ReDortins Limit Page l5 l of 152
Page 535
Interprctation of Total Petroleum Hvdrocr.bon Report
Petloleum ideatihcation is detetmined by cornpa.ing the CC frtrgeryrint obtained ftom the samgle with a libEry ofGC fingerprintsobtained from analyses ofvarious petrolgum products. Possible match categories are as follows:
Gasolide - inclLdes rcgular, udle{de4 premium, etc.Fuel Oil #? - includes home hearing oil, #2 tuel oil, and dieselFuel Oit #4 - itrcludes #4 fuel oilFuel Oil #6 - itrcludes #6 fuel oil and bunker "C', oilMotor Oil - itrcludes virgin atrd waste automobile oilLigoir - iocludes minerdl spirits, petroleum nE htha, vm&p naphthaAviation Fuel - includes keroseDe, Jet A and Jp-4Other Oil - includes lubricating atrd cuttitg oil, and silicon oil
At times, 6e uoidentified petroleum product is quaotified using a calibratioo that most closcly approxiEates Se distribution ofcompourds i.D tie sample. Wheo this occurs, the re$lt is qualifred as 'TpH (Calculated as).
Laboratorv Control SamDle (I-CS): A known matrix spiked with cohpouDd(s) r€prcs€otative of the targer aoalJ.tes, which is used todocument laboratory perfonnance-
Mahix DuDlicate: An intr4-laboratory split sample which is used to document the precision ofa method in a given sample matsix.
Matrix Soike: Ao aliquot ofa sarnple spiked with a known concentmtion of biget analyte(s). The spiking occurs prio. to safilpreprepa-.ation and aoalysis- A matrix spike is used to document r.he bias of a method in a givetr sample ltraEix.
Method Blaok: An anallte_free mabix to \r{tich all reagents are added in the same volumes or pmportions as used in mmploprocessin8 The method blank should be carried through the cotnplete sample pre!fiation and aoalytical procedure- The methodblank is us€d ro documeot contamination resulting from the anal)rtical process.
Method Detection Limit aMDLI: The minirBum concentralion ofa substance that calr be measued and reported witb 99oloconfid€nce that the analyte colc€otsation is grcat€r than zero and is determined ftom aoalysis ofa sample in a givetr mahix typ€cootaining th€ affilyte.
Reportabl€ Detection Limit (RDLI: Thc lo\€st codc€m.4tion that cao be reliably achieved wi$h sp€cified limib ofprecisioo arrdaccu.acy duriqg routine laboratory opemting conditions. For many analytes thc RDL aoallte conc€ntmtion is sel€cted as tho lowestDon-zero staodald h the calibration curve. While the RDL is approximately 5 to l0 tides the MDL, the RDL for each sample tak€6into account the sample volume/weight, extsact/digestate volume, cleanup procedures and, ifappticable. dry weigbt can€ction-Sample RDLs are highly matrix{ependenr.
Sunoeate: An orgaDic compound which is similar to the target alulyre(s) in chemicel compositiod and b€havior in the adalyticalprccess, but which is not Dormally found in etrvironmetrtal samples. These compounds are spiked into all blanks, staodards, andsatnples prior to analysis. Percent tecoveries arc calculatcd for each surroeate.
Validahd by;Hanibal C. Tayeb. Ph.D.Cluistopher Hall
This labo hrf ppo.l it ,tol valid l'lhoa aE aartodzd swnalara on rte cover psge
r RcptrrEble Det4€l-roE Limit BRL = B€low R+ding Limit Pw 152 ot 152
Page 536
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Page 539
Samole ldeotificationFB.2sA595l7-14
Clieot Proiect 430t-88
MatdxBlank Water
Collection Date/Timel9-Mar47 00:00
Received2GMar.01
CAS No. Aulyte(s) Resall Fl"C A/''iJs *RDL Diluiatt Me od Retr. Preparcd Analfud Bdc, Anat$t
VolrdL OrgrEic Compoundr
Volatile Oroanic Comoounds bv SW8,l6 82608Prepared by metl|od SW846 5030 Water MS76-1+t 1,1,2-TrichldohifuoroetfEne (F/6oBRL67€+1 Aceton€ BRL107-l3n Ad'ylonitil€ BRL7143-2 Eenzene BRL10&8Ei grcqnq!6626ne 8RLr+57-S Itomochlorcm€thane BRL7+274 Bromodicftlorom€thane BRLE2+2 Bromofo.m BRL7rl{}9 Bronbdlethene BRL76€+3 2-Eubnone (MEK| BRLt0+5t4 n-Butylb€nzene BRL13t9&O sec-Butttlsnzene BRL98-06{ tert-Butytbenzene BRL75150 Carbofldisumde BRL8-2TS Ca.bon tefacfiloride 8RL1o&so-7 Ctdorohenzone BRL7E{X}{ Chlorcett|an€ BRf6166-3 Chlorobrm BRLu-47-3 Chlorom€tlEne BRL95-.19{ 2.Chlorototuen€ BRL1064+.4 +Chlorctoluen€ 8RL96-12-S l,2.Oibrom+3.chloropropane 8RL121-,1€r Dibromod{oad.tr€lfiene BRL106-93-{ l,2-DibfomoetEne(EDB) BRL74-95F3 Dibromorn€thane BRLs6-5o-r '1,2_Dichlorobenzene BRL541-73F1 l.SDichjorcb€.Eene BRL1064.6-7 l,+Dichlombenzene BRL71714 Oid r.odlfluddnehane (Freooi2) BRf7s-34-3 .1 , 1 Oichlorcethan€ BRI_107{6-2 l,2{Ichtoroot}|ane BRL75.3S4 1, I Oichlo.oeth€ne SRLl5$5s-2 cis-l,2-Did oroetheno BRLlscd'-s tans-'1,2-Oidtrlofoethene BRL7€-07-5 l,2.OichloroFopane BRLlrr2-284 l,3-DichloropttDano BRL5ea-2G7 2,2-Oichlorop.opan6 BRL5635q€ i,l-Didrlotoprcpen€ BRL100614iScjs-1,3-Dicl{omprope|le BRL1006t4{t?ns-1,3-Dichlo.oprEpene BRL100-41{ E{rytbenzene BRL87{s3 Hexecfitoroh,rtadief€ BRL5€1-7eG 2-Hexanc|re (irgK) BRL9€{2{ lso@pylbenzene BRLs{7{ +lsopropyltoluene BRL1634.014 M€h),i t6d-tut)4 ettrcr SRL1o&rGr 4.ireh''l-21o€rltanone(Ml8K) 6RL75-092 Methylene chtorid€ BRLgr.aH NaphtElene BRL103-6$i rFPropylb€Gene BRf
rdlpsn
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SWa46 82608 224ar47 2+tar47 7031296 ek
This kbrslory .qod ls 6at wlid vithou att quthoi?ed signohlre oE ttE coyer pq..
' Reponable D€rection Limit BRL = Below Reporting Limia Prge 58 of 124
Page 540
Sample IdeptificationeE-2sA595 r7-14
Client Proiect #301-88
MatrixBlank Water
Collection Date,rTimel9-Mar-07 00:00
Received20-Mar-O?
CASN0. Analytc(s) Rest/ll FloC Uni6 *RDL Dilution L[ethod Ref P,epared Anal)zed Batch Amlrsl
vohdle Org.nic Compound!
Volatils Orcanic Comoounds bv SW846 82608P.epared by rnethod SW846 5030 Waler MS
1549-4 Trichloroffuoromethane (Freon 1l) BRL
10G2-5 Sbrene63C201 1,|,1,2-Tetrachlorcethane79-3+5 1,t,2,2-Tetrachtoroethane127-19 Tebadloroethene1O8J+3 Toluene07{1{ 1,2,}Tddllorobenzene12S42-t 1,2,4-Tdchlorcbenzene7t€ffi '1, t , 1-Tddtloroehane79{0-5 1 ,I ,2-Tdcttloroethane79{14 Trichloroethene
96n84 1,2,3-Tridoropropane95435 1,2,4-rrimethylbenzene108{7{ l,3,gTrimelhytbenzene25.01-4 Viny' dtlorid€r$G2Gz m,p-Xylene95-475 o-xyleneto+se€ Tetrahtdrofu r'anqfFT Ethyl etlerS$1-o54 Tort-amylmedtylether037-9?-3 Ethyltert-butyleherro&?0-3 DiisopropyletfEr75-65-0 T€rt-Bulanol/butytatcohol12$91-1 1,+Dioxane
slnrogale rccot/€ries:160404 +B&molluorohenzenew37.66 Toluene4S1 roeoT 4 1,2-Oicliotoethane-d41ffi&5J7 Abrcmofluoromethane
Ertretrble Petroleum Hydrocrrbons
Exhactabb Total Petrpleum HvdrocafuonsPrepared by melfiod SW846 3510C€O0G€l-9 Gasoline68azciG2 FuelOil#20047e31-3 Fuel Oil #468553-{XX Fuel Oil #5[{BEoI]()Oo Motor OilJ00100000 AvjalirD Fuel
Unidenffied
Other OilTotal Peholeum Hydrocarbonsc$.C36 Aliphatic ttydmcarbons
$nwde rc./^,etus:i3€6-A?2 | -Chlorcoctadecarc
Sernlvol.dle Org.nlc CompouDdr by cC
Oroanochlodne Pesticides SW846 8081APrepared by rnethod SW846 351 0C
3o+{F2 Adrin3l+a{€ +BHC
SW846 82604 22-MarO7 22-MaGO7 7031296 ek8RLBRLBRL8RL8RLBRLBRLBRLBRLBRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
10110094100
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95
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This labotuloq ftporl ls noa vdid wilhaul an.ulhodzed sbnofirc on the cover poge
' Reponable Detection Limit BRL = Below Reporting Limit Pase 69 of 124
Page 541
Sah!,le Id€ntificationFB-2sA595l7-r4
Clieor Pmiecl#301-88
MatrixBlenk Water
Collection Date/Tim€I 9-Mar-,07 0O:O0
Received20-Mar-07
CAS No, AnabE(s) n"E 'RDL Dilution Mertod R.f, P.epann Antlwd Botth Afl8lyst
S€mivohtlle (kgrnic CoEpo{dd! by CC
Orqanocldodne P€stickies SW846 8081A
Prepared by rnethod SW846 3510C
3rea5-7 bFBHC31s-E€{ d-BHCsE{+g grSHC (Lindahe)
57.74-9 cl o{daoe72-54-a a,a-DDO (p,p)
.2-5s 4,4-0DE (p,p,)
50-2s3 a,+oDT (p,p')m'sr.l Dieldin96&{,&€ Endosulbn I3321$6s-9 Endosulfan ll10i11,07.8 Endoeulfan Sulfate72-244 Endrin7421€3-r Endrin Atdehyde76-44{ tbptachlorZ2-43-5 Mohorychlori02a-57-3 Heptachlor Epoxide6001-3+2 Toxaph€ne510}71-9 a4hlofdan€556&347 g,Chlo.dan€534S+7G5 Endrin Ketone
Surogde rc@veies:1 NP,64+2 1,tl-Dg-Octafl uorobFkenyt (S t)?351.2q Daca&lorobiphenyl (Sr)Polvd o.imted Biohenvls bv SW846 8082Prepared by ftethod SW846 3510C1267+11-2 PC8 t0161110/.2e-2 PCB 12211ti11-16-5 PCB 1232s3{6$2i-9 PC8 124212672-zin Pc]B 124811097{s-i PCB t254r 109d82-s PC8 12603732+23{ PCB 12621r10c14-4 PCB '|268
SunEga'e t*ayedes:, 03868+2 1,4o$Uafl@mhiphenyt (Sr)?'51-2+3 bca&lotob;Fhenyl (Sr)
Semlvolrdk Orgrtrt. Compo{ndr by GCMS
U-lht-Ol 22-lli847 7031270 fGBRLBRLBRTBRTBRL
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sw8.r6 80914
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56-ss-3 B€nzo (a) anthaac€ne
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Thb knotuory r.porl ls aot tdd *ithod an aufiotized sigtr<Qe on rhe crver pag..
. Repodrbl€ Detectiod Limit BRL = Below Reporliog Limit Pag€ 70 of 124
Page 542
Sample IdentificarionFWZsAs95l7-14
Client Proiect #l0l -88
MatrixBlank Water
Collection Dat€/Timel9-Mar-0? 00:00
Received20-Mar-07
CAS No, AMlytc(s) FloC Ani$ *RDL Dilutian Method Ret Preparcd Analrzed Batch Ano4lst
S€rdvolNtile Org.nlc Compounds by GCMS
Semivolatle Orqanic Comoounds bv SWB46 8270CPrepqred by mebod SW846 35 | 0C5032-8 genzo (a) pyrene205-992 Benzo(blduofandEne1911+2 Benzo (g,h,i) peryteno207-084 Benzo (k) fluoranthene65{5-4 Benzoic acid10G5r4 Beozyl alcohol1rl'9i-i Bis(2drloroethoxy)methane1tl.4 Bis(2<hloroethyl)ether39fi&r2-9 Bis(2{hloroisopropyt)ether1i7-81-7 Etis{z€trylhexyl)phlhajele101.5t3 +BromophenytphenyleherA5{&7 Butytbenzytphthalate8S74-8 Cerbezole5!r-5r|7 +chloo_3_methylphenol106-47.€ +chto{Daniline$.54-7 2-Chkrmnaphtfialene{16-57-a 24hlo.opfi€nol7ool72.3 4-Chloaophenyl phenyl ether218{1-S Chrysene5+7G3 Dibenzo (a,h) anthracene132€4-9 Dibenzofuran956Gr 1,2-Dichlorcbenzene51ti-7!1 t,3-Didrlorobenzene106-46.7 t,4-Didilorobenzene9l€+i 3,3',-Dichtorobenzidine1UlA3.? 2,+Dichtorophenol8a{j'2 Oi€thyl phthalate13i.1r.3 Oimethyt phthatate1os7{ 2,4-Dtn|ethl'tphenolt+7+2 oi-n-buty'phffralate534-52-1 4,6-Dinitrc-2-m€thytphenol51{8{ 2,+Dinitrophenol121-142 a4-Dinitroiolueng60G20-2 2,GDinihotoluene117-844 Difl-oci/ phhatate20€-44{ Fluormhene8&7!7 Fluorene1i&74.1 Hexachlorobenzene674&3 Hexachlorobutadienen4t4 HexadorccydopentadieneA7-72-l Hexad{orcethane19&3&5 Indeno (.t ,2,3_cd ) pyreneZ8-5$1 tsophorone9i-574 2-Metrytnaphthalene95-1$7 2+rethytPhonol10&3s{, 3,+Me{hyiphenol1o€-i!r,ssi-2r.3 NaphthalenePla-744 2-Nifoanilines-o+2 3-Nifoanilinel|x}{)r.€ +Mtoaniline
SW846 8270C z2-MarOI 23-MarO7 7031272 MBBRLARLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLSRLBRLBRLBRLBRLBRLBRLBRLARLBRLBRL8RL8RLBRL8RLBRLBRLBRL8RL8RL
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ugt 0.200pS/l 1.00
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ldl 1.00
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ldl 1.00
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!S,4 1-0OpS{ 100pSI 1.00
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!S/l 1.00
!g/r 100
!g/l 1 00pS/l 1.00
liS/l 1 00
ldl 100
Udl 1.00
tidl 1 (X)
!S/l 1.00pSI 1.00
lSn 1.00
US/l 1.00
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pg/l 0.600pg/l 1.0Opdl 1.00
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+ Reportable D€tedion Limit BRL = Below Reporting Limit P a g e ? l o f l 2 4
Page 543
Sarnplc [deotificatiotrFB-2sA595l7-t4
Client Proi€ct #301-88
MatrixBla[k Water
Coll€ctiod Datellimel9-Mar{? 00:00
Rec€ived20-MaF07
CAS No. Aaebtqs) Resutt FlLS rRDL Duadon Mdho.l R4 Pdpa.cd lnabzd Detch A|alfst
S€Elvolstllc Oryrtrh Comporn& by CCMSSemlvolatile Orcanic Comoounds bv SW846 8270CPrepaGd by method SW846 3510C90€+3 Nibobenzene80-7t5 2-NitroPhenollOO{}2-7 +NihcFheool6?-7+9 N-Nitosodimehylamtne62t{4-7 N-Nitdsodi-ft p.opylamine8e30{ N-Niblsodiph€nylamine87{e5 Pentacfiloopheflol85{1{ Phenanthr€n€10&95-2 ph€nolr29.{n{ Fryren€110-€6-1 Flridtns12042-1 1.2.+Tri.htofob€rE6ness€t{ 2.4,tTddrtomphenol88{&2 2,4,GTddtlotopheflol
Sr,ttDgal€ /ffir€nias.'32t&A 2+luorobiphenyl$7-124 z+tuuqhenolal6aiah0 Nifunzena4s4te5€?'2 Phenordstr1es14 TqFhenyl4l4t1e"7s4 24,6-nibronaph€/rotSV@s bv S!'V846 8270C SIMPrepared by method SW846 3510ClIF324 AcenapMen€
2{E-96-0 Aaenaphthyjene9n"12{ l-M€hylnephbEton€12G12.7 . Anthaaceno5&553 Bonzo (a) anthracene50-32{ B€nzo (a} py€ne206-99-2 genzo O) nuoEndrene1s1.2r-2 Benzo (g,h,l) p€rytene207{€{ B€nlO (k} flUoaand,lene21C{1€ Chry'6€rF5+7G3 Oib€nzo (a,h) anhdcene206-44-0 Fluot€tr{En€&ll7 Fluor€no1s3-s{ Indem (1,2.}cd) pyr€nes15t€ 2-MedrylnaphhEb#9?G3 Napht|al€|1€8541{ Phonanfftreno129-q1.0 Pyr€ne
Sa7lwa{6 r€coyeriggi321-604 2-Fluo!6lphenyt17tE-514 Terphqlyl4l4
Totrl Mearl, by EPA 6mU7000 Sert ! Methodr
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1
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sw846 827oCGPA625 StM
7a'ao-?2{ Silvof
7:l4o-3e2 A6€nic
z1(L3$3 BA.ium
3o-130 %30-130 %
msrl 0.m5O
mgl 0-0O,$
.r]gA O.0O50
SW84U 60108 2A+rtrfl 2c+vler47 7031413 LR
Thit lobratory rcpod is ^ot vditt withotd oE.Qthotlttd dgazarc oa rte cota 1ngc.' R@orteble Delection Limit BRL = Bclow Rcpoftiog Limit P^Ec 72 of 124
Page 544
Samole IdetrtihcatiooFB-2sA595l?-14
Client Proiect #301-88
MatrixBlank Water
Collection Date/Timel9-Mar-07 00:00
Received20-Mar-07
CAS No. Ana+w(s) Resall Flag UniB *RDL Dilutaon L{ethod Retr. PnF ed Aruryzed Batch AnatlstToad Melrls by EPA 6{XXy?000 Series Methodi
zr4o{}9 Cadmlumz!qx7-3 Ctromium213942-1 Lead
?02-{$2 Selenium
Totrl Met l. by EPA 200 Serte! Methods
743047.6 Mercury
26-Mar-07 26-MaF07 7031413 LR
26-Mat-O7 27-MaFO7 7031414 YP
BRL
BRL
BRL
BRL
BRL
mg/l
mg,4
ngn
nEn
lrrSl
0.0025
0.0050
0.0075
o.0150
0_00020
1
1
1
1
sw8,46 60108
EPA 245.117470A
Thh laboretory rcpoa ir not yalid wirtoa an atrtorizc.l signataru oa the coter IBge' ReDoriable Detecrion Limit BRL = B€low Repodng Limit PaEe73 oI 114
Page 545
Saople ld€ntificationTB.2sA595l7-15
Clietrt Proiect #301-88
MaEix.Blaok Water
Collection Date/Tirp€I 9-Mar-07 0O:00
Received20-Mar-07
CAS No. Adolfle(s) Floe *RDL Diluiotr Merhod netr. Pftpor.d Anabagi Batch ,lnolN
676.-1 Acetone107.1!1 Aq!'lonitnb7113"2 Beaueno10&46-l Bromob€nzenet4-91-5 Bmflochtoromethane7+274 Bromodicfiloromethan€712+2 BmnEfonn74{}9 Baomom€thane78-93-3 2-Butanons(MEK)104-51{ n-But}'lbenz€ne13+98€ sec-Bu9lbenzenes€{)G6 tert€utylbsnzene7s-14{ C€Ibon disulfdes6-2$s carbontetrachtoride108-90.7 Chloaobenzene75{G3 Chloroethane67.€S3 Chhaoform
Vohtile Orgrtrlc Comporndf
Volalile O.oanic Compounds bv SW846 82608Prepared by method SW846 5030 Water MS76-13-t ,|.1,2-Tdcfitorotifluoroethane(FreoERl- SW845 E26OB 22-l,4€d)7 ?2-|4at47 7031296 ek
BRLBRLBRLBRL
BRLBRLBRLBRLBRLSRLBRI-ERLBRLBRLBRLBRLBRL
t(!l
ldl
wPdl
vsAlElltqllvgtlFqlPollt!94ugllgrlvglpgl
udlusnt!{!glps,l
!dlNnu{lys4
udlpsn
!s,uglpEr
Isrpdl
rslugtl|lgl
ldlItgtlpsil
!dlpgn
|tdlFSnucn.tjdl
!gl
|ldlp$
ugrlp9l
t d l!91
1.O20.o0.51 n1 .01 .0
1 .02.010.0t . 0l_ot_05.O1.01 .02_O't _02.D1 .0't ,0
2.O0.50.51-O1.01 .01 .0
2.01.0
1 .01.01 .01 .01,01 .0
1.0't .0
0.50.51_00.5r0.01_01.01 .010.0
5.0t . 0r . 0
7447-3 Chloronethane BRL9t{g-8 ?-chtoroioauene BRL10+434 il-Chloroiotuene ARL$12-€ 1.2-Oibrofto-3-dioropropene ARL124-48-1 Dibromochlofornethane BRIl0ce3.4 i,2-Dibfonro€Blane(EDB) gRL
74-9s-3 DbroanonpfEn€ BRLS{}1 |,2-Oicl orobenz€ne BRL5,{1-73-1 l,3oichlorobenzene BRL106-4G7 l!-OicHo.obenzene BRL75-714 Did orodifuorornethane(Freonl2)BRL7534-3 l,1-Dichloro€thane BRLt07-cr6-2 |,2-oichlororettEne BRL71354 |,l-Dichloroethene BRL15Cs$2 ci9.1 ,2oiclrloro€hene BRL15S60-s hans-1,2-Oic* oao€lh€ne BRL7837.5 l,2-Olchtompropane BRI_142-?trg 1,3-D'ichloropropane BRL5 2G7 2,2.Dlchtoropropane BRL56+586 l,ioichloropfopene BRL10061{t.5cis-1,3-Dichloropropene BRL10061{2at?ns-1,3-Oiohloropropene BRL100-41-4 EthYlb€flzene gRL
07€&3 tt€xad orobutadi€ne BRL591.764 2-Hexanone(MBK) BRL9A€2r tsopropy'b€nz€ne BRLs37€ +lsopropyltoluen€ BRL163a{4.4 Methyt teft-hrty{ eth6r BRLlc'&1c1 4-MethyL2-F€fltanone(M|BK) BRL7549.2 t{ehyleno d o,ride BRL91-2G3 Naphhal€ne BRL1016+l n-Propyheruene BRL
Thh Lhuolary rqod ls aot vditt lfihotd zd adfndzad slgns//are orr thz towr page .
' Reponable D€tectioo Lilnia BRL: B€low Reporting LiEit Page 74 of 124
Page 546
Sampl€ Id€ntificationTB.2sA595l7-15
Clielt Proiect #30 t -88
MatrixBlank Water
Collection Date/Timel9-Mar-{17 00;00
Received
20-Mar-07
CAS No. Analyte(s) Resalt Floq Unia XRDL Dilution lnethod Retr, Prcparcd Analyzed Batch AnalJst
Vobtile Orgllic Compoudds
Volatile Omanic Compounds bv SWE46 82608Prepared by rnethod SW846 5030 Water MS1ql4?-5 Styrene BRL63&a}{ '1,1
,1 ,2-Tetrachloroethan€ BRL7!|.34-5 1,1,2,2-Tetrachloroethane BRL127n6{ T€tEchtoroethene ARLt06{6-3 To{uene BRL4731-€ 1,2,+Trichlorobenz6ne BRL120{2-1 1,2,+Trichlo.obenzen€ BRL7r-55{ 1,1,1-Trichloroethan€ BRL79{01 1,1,2-Trichloroethane BRL79414 Trictloroethen€ BRL75{9r Trichloronuorornethane (Freon 11) BRL96-18-11 1.2,&Trichloropropane BRL9543-6 1,2,+T.imethylbenzene BRLlo€{7€ l,3,STrimethylb€nzene BRL75-01-4 Vinylcfloride BRLi33}.al.7 m,p-XyterE BRL95-47a o-Xylene ARLiogg}-e Teb.ahydrofuran BRL60-2+7 Ethylelher BRLggiros{ Teft-amyl methyt ethef BRL637- -3 Eth!4 tert-butyt €lhel10&e3 Di-isoE ropyl ether75€5-0 Tert-Butand / buty' alcohol12!91.1 1,+Dioxane
Sunogale /ecov€n€s:tl604rJt 4-BtofiofluorobenzeneU37.26-S Tduene-dg1 10@47 4 1,2'Dichlomelhane-d4
ft64-*L7
!sntsllljgnpEl
Itgtl
Lrg/l
lrEl
usnugn!91
f9l
!g/l
rr!yl
ItEl
!gn
tsll
ItEl
usnpsr!slp9l
p9/l
Ljsfl
r.iS/l
1 .0l_00.51 .01 .01.01 .01.O1_01_Ot -01 .01 .01 .0'1 02 0't .0
10.01 .01_01_0l_010_020.o
t
l
1
1
1
1
1
1
1
l
1
1
1
I
1
I
1
1
1
1
1
1
SW846 82608 22'Mat47 22-Ma.{7 7031296
BRLBRLBRLBRL
98102s3100
70-130%70-130 %70-130 %70'130 %
Thls labonlary 7sps11 ;t not val I tuittout ai outhoi.ed sigaatwe on the covet page.
' Reportabl€ Det€ction Limit BRL = Below ReportinB Limit Page 75 of 124
Page 547
Voladle Organic CompouDds - Qrdity Control
Bstch 7031296 - SW846 3130 Wrt€r MS
Blank 17031296€LKll
Prepared & Anal}.z€d: 22-lv1ar-07
1,1,2'Trichlolotriiuoroethan€ (Fr€on 1 13)
Acrylonildl€
Benzen€
Brofiob€nz€n€
Bromochloromehane
Bromodid{orom€ih€ne
Bromoformgromomolhdre
2€uhnon€ {MEK)n€uVb€nz€ne
sec-Butylbenzene
tert€utylberEsn€
C'arbd| dislrlfide
Carbon l€trachlodde
Chlorobenz6n€
Chk!roethane
Chbroform
Chbrornethan€
2chlorotoluene
4{hlorotoluene
I J-Dibromo-3drbropropaneOibrornfthlorDrneft5n€
1,2-Dibrornethane (EDB)
Oibromomelhafie
t ,2-Olchloroo€nzs.r€1 ,lDinbrub€nzene1 ,+DichlombenzeneDid orodifluoromothane (Freonl2)
l,lOichbroethan€
l,2oichloro€than€
1 ,1 Oichloroethene
ds-l ,z.c,[email protected] ,2-Dichbro€thene
1 2-Dic*rloropropane1 ,$Dicfiloroptop€ne2,2okt oroprcpane
1,1-Oinbrcprop€r|e
cis- 1,3-Oichloop.opene
ttEns-1,$Dichloopropene
Elhylbenz€ne
itexachlorobuladi€ne
2+l€xanone (MB()
lsop|opylbenz€n€
4lsopropyltot €neMethyl bd-bug/ eherl-lrothyl-2.!€nlanone U|8K)i,lolhylerc ('lbrid€
Naplrthalen€
n-Propy'tr€nzene
Styr6n€
I,l, !,2-Telrachloro€o€n€
BRL
ARL
BRL
BRL
BRL
BRL
BRI
8RrBRL8RLBRLSRLARLSRLBRLBRLBRI.ARI-BRLBRI.BRLBRLBRLsRr-BRL
sRr-ARL
8RrBRL
BRL
ARL
BRL
BRL
BRI
ARL
8Rr-aR|-BALgRL
BRLBRLBRLBRL8RrARL8Rt8RL8RLBRLBRLBRLARL
tc4!dl
rgll
usnugrlps4t gtl
ugnpdl|ldl
fl41
!gl
tJ9t4
tql
||g/lpsnygl
!dl
ItSll
!dl
udlusnttgfl
t's/ltollusnusrpql
!dl
!dl
trdl
u9nItgAggil
wusnItsnpcn!dlgsfl
usnugA!dlwlt,€ll
llsil
|ldl
udlpdludludludl
1_020.00.51,01.01 .00.51.02.0t0.0t_01 .01_0
1.01.02.0t . 02_Ot.01.02_00-50.51.01.01 .0r . 02_O1.01.01.01 .01.O1.01.01 .0t.00.50.5't_0
o_510.01.01.01 .010.05.0t . 0t.01.01_0
nhit labdorf Eporl b Eot vditt i'Ehau sn aathortztl tur@lE oE the corer page.
. Rcporable Detectiou Limit BRL = Below Reporting Limit PaEe16 ot 124
Page 548
Volatile Organic Compounds - Quality Control
Brlcb 7031296 - SW846 5030 Wsrer MS
Blant a?031296€LKl l
Pr€Fred & Analfzod: 22-Mar-07
|,I,2,2-Tetrachloro€than€
Telrachloroeth€ns
1,2,$Tricilorob€nzene
1z,+Tridbrobenzene
1.1,l-Trid or€taan€1 ,'l ,2-Trirfibroef|aneTriciloroetl€ne
Tddrlo(ofluorcm€tharc (Freon 1 t)1,2,}Tri:hloropropane
1 l,4.Trlmehy'b€nzene
1 ,3,&Tdm€hylbenzeneVlnyl d oride
m,p-Xy'ene
crxyl€ne
Tehahydroturan
Ethy' ether
Terl-€myt m€thy' €ther
Ehyl t6rt.b|t/ efi€rf,liisopropyl etherTert€utanot / butyt atcohol1,+Oioxen€
S ,,''ogaa6 : + Btotnofl uo mh e n ze neS|,'ogate: Totuene4gSuftgete : 1,z-Dichlorcethane44S urrcgate : Di b rononrcrc melh a ne
LCS a7qtl29€4st )Pr€pared & Analrled: 22-Mar4Z
1,1,2-Trid oromuoro€ttnane (Freon.t.t3)
A.fy'ofiit it€
B€nz€n€
BromoberEene
Bronoc||brdnethane
Brofircdidlloaoflt€[lane
Brwnotoarn
Broo|on|ethane
2-Aubnon6 (MEK)
n€otylbenzen€
s€cdu!y'b€rEene
isrr€uttbgnzene
Carbon disrltfide
Catbon tetad{onde
Chlorobs\2ene
Chb|Dehane
Ct{orDf\crm
Chloaomoflane
24hbrobtue.|e
44hlorotoftrene
l,2Olbromondrbropropane
oibfomodtlo.ome0rane
t 2-OibtDmoeu€n€ (EDB)
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRI.
aRl
BRL
BRL
8RL
BRL
BRL
BRL
BRI-
BRL
BRL
ARL
8RL
50.350.746.650.2
21.9
19.9
1 4 7
21.2
21.7
20.6
20.7
21.8
20.2' t9.1
20.5
23.0
16.9
22.8
1 9 3
20.1
2 1 0
22.2
2 1 . 2
19.2
22_1
21.1
!snLi9/l
Ljglpg/l
lr9lpsnpdlpdl
u9lpsnpsll
tj9l
ugl
!91
!gn
usnu(ylttgrllrg/luglt'|dlpg/lpElps/luglugi
psrusnpgn
!s?1!s/l!snus/lltg/tt g/lpg/l
usnusnusn!s4Lj9l
!sn!sntlg/l
rg/lp(yl
!g l
!9,usr!gl
0.51 01 .01_01 01 .0t . 01 .01 .01,01 .O1 .01 .02.O1_010.01_01 01.01 .01 0 020.0
50.050.o50.o500
20.020020.o20.020.o20.020.020.o20_020.020.020.020_o20.0m.020.o20.o20.o20.o20020.020.020-020-0
101 70-130101 70-1U93 70-130100 70-tu
110 70-130'f 00 41_1-14794 70-130106 70-130108 70,130r03 7G130104 70-130109 7Ga130101 62-.t3€96 53.9-133102 70-130115 70-1 30113 70-.t3094 70-130114 70.130108 70-13096 62.&132100 70-130105 7G130111 70-130106 70-13096 70-130110 70-143106 70-130
This labordoty .epod 8 nol wljd Hithaat on atdroriad signalarc on the eover page+ Reponabl€ D€rection Limit BRL = B€tow R€porring Limit F a E e l l o t 1 2 4
Page 549
Volatile Organir Compounds - Quallty Control
SpikeL€vel
%RECLimits
RPDLinit
Source
Result %RECResult Flag Unit! RPD
Brtct 7031296 - SW845 5030 Wrl€r MS
LCS r'031296-AS| )
Prepared & Analyred: 22-Mar-07
Dibromomethan€
l,2.oichbrob€nzen€
1 ,3-Dichbrob€nzene
I ,4-Dlifibrob€nz€neDicl{orcdiff uoromolharE (Fr€onl 2)
t ,l Olchloro€than€'l,2-Didrloro€rfiane
1.l-Dicf oroeth€ne
cis-l2.Dichbro€th€ne
Fdns-1,2-Di{* oroelhene
1 2-Dichloroplopd|e
I .SDichloropropane2,2-Dichb|Epropane
1,1-Dbhlo.opropene
cis. 1,3-Drcnbrcprop€ne
kans-1,3-Didtloropropene
Elhylbenzene
HexachloobuHi€n€
2-Hexanone (MSK)
lsopropylbenzene
4-ls@r(tpyltoluene
Methyl bn-buql ether
4-lreihyl-2f entanone (MIBK)
Itlstry'ene dbrtdo
t'laphthaleoe
Styr€ne
| ,l ,1 ,2-Telrachloroelhan€1 , I 2,2-Tetrachtoro€lhane
12,$Tricnbrob€nzene'1,2,+Tdchlorob€rEene
1.1,1-Trichloroethane
I , | ,2-TridloroethaneTricl{or€thene
Tichlorcouommehan€ (Freon 11)
1,2,!TrirJ oropropane
1,2,+TrnnehyltFflzen€
1,3,+Tdmethy'b€nzen€
Vinyl afiloride
m,tsXyl€n€
TelrEhydrofu.an
Etryl elher
TeGamyl m€fiy' €th€r
Etryl t d+utyl €fl€r
OLisopropy' ether
Tert-Butanol / b(tyl alcotlol
I,+Dioxan€
S u nog^le : lLgtonbfl uo rcbe n ze rcSu/rcgata: k @ne48Su/'ogal3: l,24bhlorodhane44
19.720.622.520.122520.719_4r8.321.720.321.520.826.020.521.9t9.321 .423.620.221.121 .3t9.9m.4.t9.7
18.921.222.2
21.522.020.514.62?.420.s
20.s21.28.022.5
44.923.220.519.221.222.121.2r7€207
50.145.5
usnlldt
l|g4
t€/lpcnPgtt/dl|lsnu9ntt$psil
pg4
pcnts/|usnudlt,€Awt'gluqt!dlTS/||lgl
ttg|t g/l
!snpdl
udlLrglIrdlrcnlrg4rgltsrpdl
!sn[gl
ldl
trgrl
tryl
!s4
us4pdl
edlttgfiuqlwl$nuql!dl!dlugl!dl
20.o20.020.020.020.0m.0m.o20.o20.0m.o20.020.Dm.020.020.020.020020_020.020.020.020_o20.o20.o20_020-o20.020.020.020.0m.020_020-o20.020.0m,020.020.020.020_o20.o100m.0m.020.020.o20-020.0200200fl.o50.o50.0
9a 7G130103 7G130112 7Gt30100 70-130112 39.&167104 70-1fi97 70.13092 7G130108 7{rr301d2 70-130104 7G130lft 70-130130 70-130f02 7v1301r0 7G1309€ 70-t3t)107 f0-130110 70n36101 56.3.131f06 70-130106 7G'r30100 70-130102 70-t3094 7G13{)94 70-130r(Xi 7G.130r11 7G130t18 7G1301o8 7Gr30110 70n30lm 7G13074 70-13rc112 70-130104 7G130102 7G130102 7&130'106 7Gr30115 70-t3o112 70-,t30112 70.10106 ?G130t12 7S1301t6 7Gr30102 zGi 30s6 7G130106 70-1301t0 7G130t06 7G130&! 7G130104 70-r3o105 70-IU100 f0-1fi9t 7E 3t)
Ika! laboelary r?pott,s frteond ''i/,,ord tn otdrodzet signat.E ot ttg cwer poge.
+ Repo.nble Dete$ioo Limit BRL= B€low Rep(trtiae LiEir Paee 78 of 124
Page 550
Volatile Orgalic Compounds - euatity Conarot
Aoalyrds) Result Flag UnirsSource
Resulr %REC+RDLSpikeLevel
%RECLimirs
RPDLimilRPD
Brtct 7031296 - SW8{6 S0l0 Water MS
LCS fl031296€51)
Prepared & Anatyzed: 22,Mar-U7
S u ftogale : Di bro fi tofl u om n€th a ne
LCS Dup l703t29iBSO1l
Prepa.ed & Anatyzed: Zz-Mar{7'1,1r-Trichlo,otdf,uoroethane
(Frson 1 t3)
Aciylonihil€
B€nz€ne
Bromobenzsn€
Bao|hodlbromethane
Brornodit odnethane
Sromoform
Brcrnomehane
24ulanone (MEK)
n€utylb€nz€ne
sec€uiy'benzene
tsrt€'rtylbenz6.r€
Ca6on disulfide
CEfton bt'achlcride
Chlorobenzene
Chloroethan€
Chlolobrm
Chlomdre0lane
24hlorotoluene
44hbroioluene
I 2-Dibro.no-3rJltoropropane
Dibromochloromethane
l,2-Dibrcmoetra e (EDB)
Dibfornomethane
l2.orchlorob€nzene
I ,3Oicfilorobenzene1 ,4-Did oobenzene
Did oro<,|fl uotumerhane (Frsonl 2)|,1-Dldb.E€thane
1 ,2{)i* oro€thane
1 ,1 Oldlo.o€trene
ds-t 2{)i$broethen€t'anE- l,2Oichtoroethene
| ,2ol$loropropane1 ,$Di*k ropropane
z2-Dicl o,ropmpene
1 ,1 Oicfiloropropene
.i5-'l ,3oinbrcpropen€tans-1,$Dictloropropene
€@benzene
Hexechlorobutadiens
2+lexanone (MBK)
lsopropy'berEene
4-boproMolu€ne
Melftyl t€n-butyl etr'er4-[r6thyl-2-p€ntanone (MtaK)
MetrMarE chtoride
Na9hf|5l€ne
49.8
19.4
20.1
18.7
19_7
21.3
20.0
19.7
22.2
1 8 6
18.0
20.3
23.2
23.O
15.9
20.6
21.O
1 7 9
1S.0
1 9 4
21.4
20.7
18_0
21.2
2 0 9
18.8
20.5
21.7
19_4
1 9 1
19.6
18.8
r6.6
20.6
18.4
203
20.2
24.3
ra.4
20.7'18.3
2 0 6
2 1 . 7
1 9 4
20.6
2t .7'19.6
19.9
17.6
17 -4
pdl
pdl
!srpgl
ItEl
rcnFEI
!g l
!g/l
tgnpglpsl
tig/l
tgl
!snpgn!91pgl
us/ygtl
uglps4
!gn
vgl
lr9l
ttEl
lj94p9l
pg/l
usnpg/l
rcnpdl
pdl
!!y1
ug/l
Itgrl
IIEIpdl
udl!g/l
vtttlps4
psil
!glpdl
!sr!sl!snug/l
50.0
20_020.o20.020.o2 0 020.o20.020.o20.020.020020.o20_020020.o20.020.020.020-020.o20.0m.020.020.o20_020_020.020.o20.o20.020_020020.020.020.020.020.020.020.020.o20.020.020.o20.020.020.020.020.020.0
99 7L130
97 70n 30
100 41.1-147
94 70-t30
98 70-130
t06 70-t 30
100 70-130
98 70-130
111 70-130
93 62-136
90 53 9-133
102 70-130
116 70.130
115 70-130
60 70-130
103 70-130
105 70-130
90 62.&132
95 70-130
97 70-130
107 70-130
104 70-130
90 70-130
106 70-143
104 70,130
94 70-130
102 /0-130
108 70-130
97 7G130
96 39_3-167
98 70-130
94 70-13t)
83 70-130
103 70-130
92 7G130
102 7G130
101 70-130
122 70-130
s2 70-130
104 7G130
92 7G130
103 70-130
108 70-136
97 56-3131
103 70.130
108 70-130
98 70-t 30100 70-130
68 7{t130
a7 70-13n
13 25
0 5 0
0 2 5
8 2 5
2 2 5
3 2 s
6 2 5
2 2 5
8 s 0
6 5 0
0 2 5
0 9 2 5
2 2 5
16 25
10 25
3 2 5
5 2 5
8 2 5
4 2 5
2 2 5
6 2 5
4 g
2 2 5
4 2 5
1 2 5
4 2 5
3 2 5
l5 50
6 2 5
3 2 5
10 25
10 25
6 2 5
3 2 5
6 2 5
10 25
4 2 5
9 5 0
4 2 5
2 2 5
7 2 5
8 2 5
Thh labordory rcpofi k tot valid witho4t aa rathortz"j sign ture oa the corer ptage.* Repdable Derection Limjt BRt_ = Betow Repoding Limir Page 79 of 124
Page 551
Volatile Organic Compouods - Quality Control
Amlyr€(s) Result Flag Units R€srlt %REC Lrmrls
B.Ntch 7031296 - SWt46 5030 Wrter MS
LCS Ouo (7Gll296€SDl )
Pr€paEd & Analfzed: 22-Mar-07
Styr€n€
1 .1 .1 ,2-T€trachloro€lhaneI , | .2,2-T€tsachloo6lhane
Tebachlorc€thene
Tolu€n€
1,2,lTrichlorob€nzene
1,2,+Tricnbrob€nzefl€
1,1,1-Tri$broelhane'1,1,2-Tridlnoethane
Trichloro€thsr€
Trichlorofl uoromet|ane (Freon 1 1 )1 2,3-Tddrbropropan61,2,+Trim€tnylb€nzene
l,3,'Trirn€drylbenzene
Vinyl chlodde
m,p-xylene
. Tet ahldofuran
Elhy' €h€r
Terl-amyl nEthyl etier
Efhyl te.ttu!y' efter
Oi-isopropy' €tier
Tert-Buianol / buv alcohol
I,4-Dioxsne
S unogate : + Bto nbfllwoh e n ze neS'l'rcgate: f(rl@ne4gS uiog eh : l, 2-Dich f oroetha n e 4 4Sutogalg: Dibmn$fluot@tethat e
Marnx Soft(€ O031 29&MSll
P.epare<t I Anal}.i€d: 22- ar.07
Benzene
Chlorob€nern€
1 , l -Dlchlorc€flens
Toluen€
Su/7ogab : 4-&otrpfl uor&EnzeneSunogote: foL/6.ne4SS.j'|ogate : 1,2OkahlomdhaE443 u tng ale: Dilbanof, uoronelh a ne
20.621.523.121.5't9.9
19.5'13_9
21-415.220.2t8.6r8.722.922.622.418.543.2
20.419.421.021.420.6r7321353_849.845.049.6
Solrrc6: SA59563{l
1{X} 7G130100 70-lm't1E 70-'130108 70.130100 70n3096 7Gr3070 7S.130107 7tt130s6 70-1010t 70n3094 70-13094 70-130114 70-130113 7Gr30112 70.t3092 70-t 3t)lm ?0-130110 7G130102 70-13xn 70-130105 70-130l(x, 7G130t03 7G13086 7&1 30106 7G130108 7G1g)100 7G1g90 70-13099 70-1m
r18 70-13t)128 70-130104 70-i30117 70.130112 7G13099 7G130tN 7G1$91 70-13099 7G1n
lt4 70-130124 70-1301ft} 70-130116 70-130r00 70-130gg 7o-tu101 70-1fig 7&1fi98 70-130
!dlugll!snydl
t s4pg/l
ug4r.'dlpdl
!dlpgr
ugtl!dtFSilugl!94pgl
tsllpdl
uglu$pdl
WIlrgnt4l4!sntd l!41psn
20.020.020.020.020.020.020.o20.020.020020.020.o20.020.020.o20.0,10.0
20.020.020,020.0200m.0zn200fr.o
fi.o50_0
20.020.020.020.020.050.050_o50.050.0
20.020.o20.020.o20.o50.050.050.o50.o
332010
65
1I120.90.9014
50
0.90.9
2525252325252525
25
50
252525
2550
25625
23.425.720.823A22.549.650.145.649.6
lrEl
wl!g/l
vslluc,4pdlpdlu9l|lgn
8RL
BRL
BRL
SRL
8RL
lilatrlx Solk Ote O031206-flSO1t So{rcr: SA5O!6J-01
Prepaed & Anal]/2ed: 22-Mar-07
B€flzene
Ct{orcb€nzen€
1 ,l .oidtlorcenhene
Toluen6
Trbhlorosthen€
Ssfogate: ttglo/noltuoloben,f,,neSu/'ogale: Td@ne4gShogale: 1,2-Dkithrcethane44S u nqate : Dibtunrcfl uotornelh a ne
Brrcb 7031335 - SW846 5035A Soil 0ow lcvct)
22.924.820_623.1
49.550.715.118.8
BRL8RLBRLBRIBRL
lrdlFSnrcn!dlpdl
rdlu9l|lsnIt
331
0.9
30
30
This labtulrq rqn.a is not vald *&hov an ,,r!rtorize.I sign,d.tre on tte cova, psge ,+ R€portable Dete{rion Limit BRL = Below Rcpqriry Limir P€e 80 of 124
Page 552
Volatile Organic Compoutrds - Quality Control
ADalFe(s) Result Flag UnitsSource 7"RECResult %RtrC Limits
Spike
L€vel
RPD
Limi(
Brrch 7031335 - SW846 50J5A Soit {tow ter.et)Blank {70t133!t€LKtl
Preparcd & Analfzed: 22-Mar-07
I,1,2-Trid orolrifluoroethane (Freon t13)
Acrylonibil€
Benz€ne
Brdnob€nzene
Eromodrbmmelhane
Brornodk$loronehane
E.omofom
Bfomorne$ane
2€uranone (MEK)
n€utyD€nz€ne
6€c-Buiylbenzene
tett€utylb€nzen€
Cdbon disifde
Carhon lehacfilodd€
Chlo@benzen€
Chlooethe|e
Chlorofom
Chlorofir€$ane
2-Chbrololusn€
4-Chlorololuene
l,2.Dlb@mo-3-chlompropane
Dib.omo<fibromethane
1,2-Dibmmo€thane (EDa)
Oibfomomehar€'| .2-Dichbrob€nz€ne
1 ,3oicibrobenzeneI ,lLDichloobenzeneOlcft lorodiff utrom€thane (F.eonl 2)| ,1 Oi{rhloroethane'l ,2-Didtloroethanel,l.Dic$lor*then€
ds-1,2-Oic*rbmethene
t_ans-l,2Oldtloroethen€
1,2-Dldrlorcpropane
1,lDichlompropsne
2,2-Dbt{ompropane
J , l Obhbroprop€n€
cis-1 SJidrlsop.opene
ttans-l,3oid oropropene
Ethylbenzene
H€xachlo(brrtadiene
2-Hexanon€ (MBK)
lsoFopylbenzene
+lsoprorMrolu€ne
Motryl bd-buv dr€r
+M€lhytz-pentanone (tlttBK)
Methten€ crrloRte
Napha|abn€
Slyrene
1 ,1 ,1 2-T€trEchbro€haneI,I J,2-Tetrachloro€{hene
BRL
BRI.
BRL
BRL
BRL
BRL
BRL
8RL
BRI.
ARL
BRL
BRL
ARL
BRL
8RL
BRL
BRL
BRL
ARL
8RL
BRL
ARL
BRL
BRL
BRL
ARL
BRL
BRL
ARL
ARL
ARL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI.
BRL
BRL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
!g/kg wet 5.0pglkg wet 100pS/kS tvet 5.0pg/kg wet 5.0
!g/kg wet 5.0
lig/kg wel 5.0pg/kgwel 5.0
lgkg w€t 5.0
Ugy'kg wet 10.0
!949 wet 50-0
lgkg wet 5 0pg/kg wel 5.0pg/kg wet 5.0
lig/kgwel 25.0
!g/kg wel 5.0
P94(9 w€t 5 0pgkS vret 10.0pgr'kg wet 5.0pq/kg wet 10.0
Ligftg wet 5.0
lgkg wet 5.0
ttg/kg wel 10.0
!g/kg w€t 5.0
!g/kg wel 5.0pS/kS wet 5 0
Ugftgvret 5.0
lgukg wet 5,0pgr'kg wet 5.0
Ug/kg wet 10.0
Ug/kg wet 5.0
Ug/tg wel 5.0
Ugr'Kg wet 5.0
lgftgwet 5.0
!g/kg wet 5.0
!s49wel 5.0
!g/kg w€t 5.0
pgks lvet 5.0psrkswet 5-opdkS wet 5.0
!gl(q wel 5.0
!g/kg wet 5-0
lgL/kg wet 5.0
lgr'kg wet 5()-0
Ug/kg wel 5.0
l.rg/kgwel 5.0pgikgwel 5.0
trSikS vJ€l 50.0
!g/kg wel 50.0
Ug/kg wel 5.0
lgn(g w€t 5.0pdkSwet 50pqkS Yr€t 5-0
ldkg YJet 5.0
Thit labonlory rcpotl b not talirl xrithoul q4 aaihorizcd EiFttzturc on the cover pzEe.
* Repo.table Detection Limir BRL = Below Reporting Limit Page 8l of 124
Page 553
Volalile Orguic Compounds - Quality Cortrol
Bdch 7031J35 - SW846 503sA Soil (low levcll
Blant r|031335{LKll
PtepatEd & Analyzed. 22-Ma(O7
Tetrad$oao€h€na
1,2,3-Tric$lorob€nz€n€
1,2,+Trichlorobenzene
1 ,1 ,1 -fncnbroethan€
1 ,1 ,2-Tridrbro€than€Trici or€th€ne
Tricl orofuoromethan€ (FrEon 1 1 )1,2,$Tric*rloropropaoe
t,2,4-Tri.nehytb€nzene
l,3,STrimeftylb€nz€n€
\rmy' c* oride
m.p-XylerE
cXylene
Tetrahydroturan
Etrylether
Tert-amyt methyt €th€r
ErhY ten+utyl strr€r
Di+opropyl ether
Terl€ltanol / butyl alcotrcl
l,40ioxane
Surrcgale: laronldfrnorden zeneSunqatg: Toluen&8Sufltgate : l,2aichloftethane44S/u/tlgate : Dibro.ilo/fltlotonethane
LCS ft03t3:15€Sr I
Prspared & Anat)/red: 22-Mar-07
1 , t.2-Tricfiloro,trifluoroethane (Freon 113)
Benzene
Itomobenzen€grornod ordnethane
Erornodichlorom€hane
Baofitobfin
Brcmomelhane
z€ubnon€ (MEK)
n€utylir€nzene
s€c-Eulylbenz€ne
t€fi.Buty'b€nzon€
C€rbon disumde
C€rtoo bhacnbride
Chforcb€nz€n€
Chbðane
Chlooform
Chlotom€tl€n6
2Chbro{oluene
44hbrololu€n€
1 2-Dibmmo-:|-ct oropropane
Dibmmodrb(xnethane
1,2-Dibromoeharr (EDB)
Dibromonpthane
BRLBRLERLBRLARLBRLBRL8RLBRLBRLBRLBRLARLARLBRLBRLBRLBRLSRLSRLsRr-52.152.355.452.0
2006.5ls.020.417_a1E.020.218.917.914.216.819.719.417_O18.919.619.018.8t9.319.419.521.720.5m-2'| 0-6
50.050.050.050.o
20.020.020.o20.o20.o20.0m.0m.020.020.020.020.o20.020_020.020.o20.020.020.o20.o20.020.020.0m-oz)-o
Fg^gwet 5.0pgAgwet 5.0pdtSw€t 5.0pdkswet 5.0
lgftgw€l 5.0pgr'kg w€t 5.0
ldlqv,et 5.0
!g/kg wet 5-0
Ekgwet 5-0
lrgitqwet 5.0
lgr'kg wet 5.0pCftg w€l 5.0pg/kg w€l l0 0
UdkS wel 5.0
t/dkS Yret 5O.0
Ug/kS wet 5.0pg/kg wet 5,0
l1g/l€ wel 5-0
ldkg w€i 5.0
Fgftgwet 50_0
UC^gw€l 10O
ldkS w€l
!g'kg w€tldl€ wet|lgL{(g wet
!€/l€ wol
ldtS vret
l.'dks wel
pdkS trel
pdkg wet
ugr/kg w€t
tSn(g rYet
|l9fi9 wet
t gil€ wet
ugn€ w€t
lrg/tg wetpgts w€t
Iqkg wet
ldko Y.€l
lgr'kg tvet
!9Ag wet
!SI!S v{etpg/kg wet
rc/kg w€trc/kowetpSAg w6l
t'dkg YY€t
!$4q w€t
ld](S Yret
rc/kg,ret
104 70-t3t)105 7L1fi111 70-13t)104 70-130
100 70-13/)42 1.77-17595 7G130102 7Gr3089 70-r 3090 70-t3t)10t 7$13094 7G13090 55.113671 #.8-14294 7G130s8 7G13097 70-13085 70-13094 70n3096 70-13095 55.!13094 70-13096 7G13097 70-13/]98 70-t3t)lm 70-lm102 64_7-13910r 7G13093 7G130
Thls bbonbry rcpo.a k,rotvdidw hoa an auttoriud rigazute oa the covet pge.. R€Frtabi€ Detcdioo Limit BRL = B€low RcErrins Lirnit P^ge82 ot 124
Page 554
Volatile Organic Compourds - Quality Cootrol
Analyt€(s) Result *RDLSpike
L€vel
SourceResulr
RTDLimitUnitsFlag
%REC%REC Limi6 RPD
B|ach 7031335 - Sw846 503sA Soil (tow tev€t)
LCS {7031335€3l I
Prepared & Anal!.zed: 22-ItaF07
I ,2-Dichbrob€nz€ne
1 .3oichlorob€nz€ne
1 JJid orobenzene
Dichlorodi0uoromotrhane (Freont 2)1 ,1 .I)bhlorc€than6
1 ,{i6lo.@thane
I . | -Dbnb.oef.n6n€
ci6-l,2-Di$broethene
lrans-l,2.0lc{l toroetr€n€1 ,z-Did orcpropane
| ,SDirJ ororropane
2,2okfiloropropan€
1,1-Did oroprop$e
cis-l,SOichlo.opopene
lran6-l,3 Oicnbrcprop€ne
Ethylb€rE€ne
l-lexachlorobutadiene
2+{exd|one (MBK)
lsoptopy'b€nzen€
4-lsopropyltoluene
rn€thyl lert-butyt ethe.
4+vtethyl2?€ntsnone (MIBK)
M€lhylsfle chlorde
Naphihalene
n.Propy'berE6n€
SVr€ne
1,1,t,2-TeHtloroethane
1,f ,z.z-Tet"ad oro€thane
Toluene
1 ,z,$T.ict orcbenzen€
1,2,+Trichlorob€nzene
I, I, l-T.tctrlorcethane
1,1,2-T.ihloro€thane
Tri:ib.oethen€
Tddbrofluoron€hane (Freon 1 .t )1,2,}Tri<t oropropane
1,2,+TrinlethylberEene
1,3,$lrirhethytbenzene
\rmylchlodde
m^0-Xylen€
oXylene
Tet-alryd$fu€n
Etll|rl et|er
T€nqnyl ftFthyl ether
Etlyl isrl+uM etler
Dl-lsogrepY "h",Ted-8{tanol / b(ltyl elcohol
1J-Dixar'€
S ui(va/e : 4-Bmmoll u orcb e n z e n€Slnrcg'/e: Toluene-daS,J/'rogde: l,2Olchloro€lhane44s/mt,gate: D/D,onld.fl uotomelha rn
18.8
1 8 . 1
1S_3
2 1 3
2 1 . 0' t9.0
17.9
1 8 9
1 8 8
20.4
205
17.9
1 9 . 8
19.8
19_4
1E.5
1 2 6
1 9 . 1
19-8
20.5
19.6
18.5
20.5
19..1
20.0
1 9 . 9
1 9 . 1
1 8 . 8
19.9
1 9 . 9
1 9 . 5
1 9 . 1
20.6
22..1
1 9 , 1
19.8
19.0
21.2
39.0
19,9
1 7 . S
19.2
22.0
22.8
19.4
174
177
48,551.s47.450.1
20.02 0 020020.020.020020.0m 020.020.o20.020_o20.o20.020.020.020.020020.020_020.020.o20.o200?0.020.o20.020.020.020.o20.o20.020.o20.020.o20.020.020.o20.020.040.020_020.o20.020.020.020_020020050.ofl.0fi.0ffi.0
US/kg wet
Fgtg wslpEt(g r^€t
!E(g wet
trdks wetpqhg wet
pyKg wet
Ugr'Kg wetpEkg wetpg/Kg wet
trg/kg wetpg/(g welyg/ko welpEr(g wel
Ug/kg w€lpgkS w€tpgkS vret
oc2 !g/kg wet
lEkg wet
!g/kg wetp9t(g \ /et
Irg/kg wet
tig/Kg wet
yg/tg wet
trgkg wet
ug/kg $/etpgi/kg wel
UEkg wer
Pg/kg wet
lrg/t(g wet
ug/t(g wel
Irg/l(g wet
!g/kg wet
t Et€ wel
uEr(g wet
rrg(9 w€t
!g/tq wel
ug/kg wet
Ug/kg wet
!g/kg wel
UgAg w€t
!g/kg wet
[g/kg wet
FS/kg wet
lglkg wet
uE|(g 'n€l
ygl$ w€t
ugy'kg wet
Ug/kg,,!et
!g/(g w€tt gftg w€lygftg w€lygftg w€l
94 70-130
90 70-130
92 70.130
106 U.+t67
105 70-130
95 70-130
90 70-130
94 7G't 30
94 70-130
102 70-130
102 70.130
90 70-130
99 70-130
99 70-130
r08 70-130
97 70-130
92 60.1-140
63 70-130
96 70-130
9S 70-130
102 70.130
98 46.1,145
92 7G130
102 70-1 30
96 70-130
100 70-130
100 70-130
96 70-130
94 70-130
f00 70-130
100 70-130
98 70-130
96 70-130
103 70-130'110 70-130
96 56_8-140
126 70-130
99 70-130
95 70-130
106 70-130
98 70-130
100 70-13t)
90 70-130
96 65.3-130
110 7G130
114 70-130
97 70-130
87 7G130
88 3+155
97 76130103 70-13095 7)-130100 70.130
This labodary rcport Ir ,tot valid ''tthoat zd outhoirpd siF rararc oE thz cover page .
* R€porrlbte Dereciion Limir BRI = Bclow R@nirg Ljmjr Page 83 of 124
Page 555
Volatile Organic Compounds - Quality Control
AnaMe(s) Resuh Fteg UnitJ
Spik€Level
RPD
LimitRPD!RDLSourc€ oZREC
Result %REC Limits
B.rch 701 1335 - SW846 5035A Soil (tow levet)LCS Duo r70gl33SSDil
Pepared A Ansl}rzed: 22-rvlar-07
|,1,2-Trichlorotmuoro€thane (Freon 1 13)
Acrylonitdle
Benze{|€gromoben:€ne
Bromochbromet,rane
B.oflbdichlorom€thane
Brornoform
Brcrnomelhane
2€uta.lcne (MEX)
n€utybenz€ne
s€c-Butylbenzens
tert-Buqdb€nz€ne
Carbon disulfid€
Cerbon btracnbdd€
Chlorobenzen€
ChloF€thane
Chlorofffm
CNoromettra|€
2chlomblu€ne
44hlorololuen€
1 JOibrofi b-3ddorcpropane
Oltrornociloromelhan€
1,2{ibrorno€lhane (EDB)
Dib|Emomethane
1 ,2-oichloroberEen6l,3oid irobenzen€
| ,4-DirfilorabenzeneDid orodif uoromethsne (F.eonl2)
1,1 -Obhlorc€thane
l,2obhloro€thsne
| , I Oi{$loroeth€ne
cjs-l 2-DirJ oroethene
t-ans-1,2-Dkilor@thene'|
,2-t i(,|bropropz€
1,lDicl oopropan€
22olcfrloroprop€ne
l.l -Dlcfiloropmp€ne
cis-l,3oichloropr@ene
lran9l,SDi.hbropaopen€
Ethylbenzene
Hexachlorobutadi€n€
2-tf€x8non€ (tvtBK)
lsopropylbenze'r€
4-lsopropyltoluem
lllethy' brt+uv 6lher
4-l,lethyl2t€ntanon€ (MlgK)
iretnrybne cfibril€
Nephthalen€
Sty.6ne
!, |,l,2-T€trachlorcethane
I,1,2,2-Tst'achloroethan€
21.39-818.720.318.217_421.O14.71S.912.019-719.420.518.219.5
17.319.220.119,319.31 f . 418.9
21.820.5r6.419.121-120.2r9.514.620.5'19.7
20_o20.017.120.521.321.820.019.9t3_618.620.1a).817.O18.2r9.819.4r9.8m.218.1
20.0m.020.o20.020020.020.020.o20.o20.0m.020.o20.020.020_om.0m.020.o20.020.om.020.020.020.020_020.0m.020.020.o20,0m.020.020.020.020,020.020.020.020.020_om.020.020.o20.020.020.020.020.o20-020.0m.020.020.0
Ugiko wet
lrg/Xg wel
t gks u/€l
Lrdkg Yv€l
lgr'kg {,et
pgr'kg wet
PgtS vJet
lgtS w€l
lgy'kg wet
Ug/kg wet
pg/*g wet
pg/tg w€l
Fgr'kg w€l
ugl/l(g lYel
t gtilg wst
lrgilg Yret
pgy'lq we{
!g,kg w€l
lgkS w€t
$/t(g wet
Ug/kg w6t
Pdkg $€l
UdkS v'^el
t g/kg rv€t
l,g/ko sst
Fgftg u/el
ldkS vr€l
ldkg Yrel
rc/kg vYst
|lg/kg wet
pg/kg wel
udkg vret
Lrg,fkg r€l
ldkS w€t
rc/ko wetygag wel
Fgrkg wel
rur'kg w€tlgL/kg rvet
!S/(9 wetpg/kg wet
lgkg wetQCz !g4qg vr€t
pgr'kg n et
lrg/t€ wet
Pgr'Xg wetpgukg w€l
IdkS $et
lrdlls wet
t€/ko u/et
Pg/fg welpdkg ',vel
UdtS wel
106 70-13049 1.77-115s4 70-130102 7Gt3091 70-130a7 70n3)105 7G13094 7Gr30100 55.3-13660 38.8-'t4298 70-13097 7G130102 7Gr309t 70-13098 70-13096 70.13086 55.3-130s6 70-130100 70-13096 7G.1309{t 7G13087 70-r 3094 64-7-139106 70-r 30109 70n 30102 7Gt3092 7Gt 3096 70130107 y_4-167
101 70n 3098 7G13093 70-?30102 70-13098 70-130100 7G130100 7G13087 7Gr 3{)102 70-130106 7G130109 70-130100 7Gr30100 60.7-14068 70-13093 70n 30100 7&130104 70-13085 46.1n4591 7S.r3099 7G13097 70-13099 70-130rol 70-13090 70-13n
t5 501 2 50 2 52 2 53 2 54 2 50 2 511 5017 504 2 51 2 55 2 57 2 54 2 5
10 502 2 54 2 51 2 5
2 2 58 5 05 2 5t6 25
2 X4 2 5
0.9 504 2 53 2 53 2 58 2 54 2 52 2 52 2 53 2 53 2 57 2 5
0.9 253 2 58 5 04 2 5
1 2 52 2 514 501 2 53 2 51 2 5t 2 51 2 5
Thb ,abodory ra?n.t is nol edld flithoA a4 Mthorlael [email protected] o,t the rover poge .
' Reporlablc Detectioo Limit BRL = B€l,ow Repoding Limir Psg€ 84 of 124
Page 556
Volatile Organic Compounds - Quality Control
Baach ?031335- SW846 5035A Soit (low lcverr
LCS Duo (703133tASDil
PreFred I Analfzed: 22-[/ar-07
Te{rachloro€thene 20.6Toluerle 19.9l,2,lTricfilorobenzene 20 91,2,+Tridrlorotcnzene 19.9I,l,l-T.i$bro€lh€ne 19.6I,l,2.Tdchbroetiane 20 9Tdchloroe[heoe 2Z.aTridrlo.ofluomrn€thane (Freon 11) 2O.2l,2,3Tridrlo.oprcpane 21.51,2,+T.inehytb€nzene 2O.O1,3,$Tdm€f|ylb€nuene 20.1Vinyl d oride 22 7m,p-Xylene 38.8o-XYlen€ 19.0T€hahydrofu.an 18.0EtMether 21.1Tert-emyl medlyteth€r 20.6Ethyl ied$ui/t ettEr 224Di-isopropyl 6t'rer 19.6Tefl-Butanol/ butyl alcohot 1591 ,4-Diox€ne e3Su/'pgate: +BtDt pqtto@benzene 4B.gSu,togate: ToltAne4S 53.0Sunoga'€j 1,2-Dichtorcethane44 49,5Suiogab: Olbtono{Iuorcmethane 50.6
Brrch 70.3 1602 - sw846 s0l0 sott (high t€vel)
tigfl(g wet
Ug/kg wet
!S/kg w€t
lgr'kg wet
lgkg wet
lig/kg wet
pg/kg wel
lgt/kg wet
ligr'kg Y/et
pg/kg wet
t g/xg wel
Igftg wet
plyt(g wet
Ligr/Kg wet
!g/kg wet
Fdkg wet
!g/Kg werpgftg wel
pg,4(g wet
!g/kg wetQc1 pg/kg wet
ggftg wet
Pg'rg wel
!g/kg wetpg/kg wel
103 70-130 9100 70-130 0r04 70-130 4100 70-130 29E 70t30 2104 70-130 1't14 7Gr30 4r01 56.8-140 5108 70-130 15100 70-130 1100 70-130 5114 70-130 797 70-130 195 70-130 590 70.130 0106 65.3130 10103 70-130 7112 70-130 2s8 70-r3U 180 70-130 I62 34-155 3598 70-13n106 70-13099 70-t 30101 70-130
20.020.020.om.020.020020.020.o20.o20.020_02004 0 020.o20.020_o2002 0 020.0zDO20054050.050.050.0
252525
255025
25
2525
5025252525
Blant {7031602€LKl I
Prepared & Analli?ed: 27-Mar07
1,1,z-Tridrbrofiffuoroethane (Freon 1 13)
Acrylor trile
BonzenegromoberEene
BronEdrloMn€thane
Brcrnodicfiloromehane
Bmmoform
Brornomehan€
2€utarEr'€ (MEK)
n€urybenzen€
s€c-guvb€nzene
lsrl-ButylborEene
C€rbd| disifide
Cadon bbachlodde
Cl{orobenzone
ChloD€than€
Chlorobrm
Chloromehane
24hlorctolu€ne
4-ChbrobluerE
1.2-Dibrcrm€d oopropane
Dib.onochbrornethane
1 "z{]ibromo€thane (EDB)
BRL
8RL
BRL
BRL
ARL
BRL
8RL
ARL
BRL
8RL
BRL
BRLgRL
8RL
8RL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
8RL
1 02001 .01 .01_01_01_01_02.O10_01 .01 . Q
1 05_01_01.02.O1 .02.O1 .01-02.01 .01.0
!g/kg wet
!g/kg wet
pg/kg welpgr'kg wet
Ug/kg wet
pg/kq wet
pgr'kg wetpgKg wel
wkg wel
ug/kg wel
pg.4g r4€l
pg/kg wet
!g/kg wet
pg/kg wet
lgkg wel
t g/Kg wel
Fgy'kg welpqkS w€l
lrgkg r €lpEr(g wet
!gl(g w€t
Ug/kg v/st
Ig,/kg wet
t g/kg wel
Thb labarulory Hpon h noa wld withottr an aatho.iae.! siEnatuR o1 the cover page .' Reportable D€rection Limit BRL = Below ReDortins Limit Page 85 of l14
Page 557
Volrtile Orgaric Compounds - Quality Control
Anallte(s) Flag .R-DLSpike
Level
SourceRe$rlt %REC
%RECLimits
RPD
LimitRPD
Batch 7(Lr 1502 - SW846 5030 Soil (bign kv€l)
Bl.nk r76l6O2€LK1l
PrepaEd & An€AEed: 27-ti,tar.07
Dibromornethane
1,2-Oid orcb€izene
1,3-D-hlorob€oz6n€'l ,4-Did|hrob€rEene
Dichlo.odifl uo.om€than€ (Fr€onl2)
1 ,1 Oichbro€thane
1 ,Oichloro€thaneI ,1 Oichlorc€th€n€
ci6-1,2-Did oroellteno
tans- 1 ,2.olafibrc€th€n€| z-Dichloropropsne
t,3-Dhhbroprcpane
2,2-Ditrlorogmpane
1,1{Hrbropropene
cis-1,3Jichloroprcpeoe
tr8ns,1,3-Dihloropop€fl €
Elhylbenzene
H€x€chlo.obutadiene
2,tlexar|one (MBK)
lsopopylbenzene
4Jsopmpyltolu€ne
Methyl ted-buty' €uler
+ld€hyl-2+€nlanons (M|aK)
M€thylens d|iornle
Naphth€len€
Slyrene
1,1, 1,2-Tstrdchloroethane
l. 1,2,2-T€trachloroethane
Tetrachlcao€th€ne
Toli,,ene
1,2,+Trichbrobenzene
I,2,4-T.id orobenzsE
1 ,I ,l -T,ichbroehane
1,1.z-TtiJtlorethane
Trichloroollsle
Trk] orolluo|om€U|an€ (Freon 1 'l )'1 :3Td$brop|open€
1,2.,r-Tdmothylb€.E€ne
l,3,STrinEthylbenzene
Vlnyl.filo|Uo
m.Fxyl€ne
o-Xybtro
Tedlydrofuran
EthM elh€t
T€rt-a||y' m€hyl ether
Ethyl lo.l+utyl etl|er
Dl-lsog.opyl €t'€r
Terl-But4rol / butyl alcohol
1,+Dlxan€
Smr{iab : 4-AtonmfluotolFJnzeneSwrogale: TohEne4SSurroga63: l,zOichloto€han€4 4
BRL
SRL
BRL
8RL
BRL
BRI.
SRL
BRL
ARL
BRI-
BRL
BRL
BRLgRL
BRL
BRL
BRL
BRI.
BRL
ARL
BRL
BRL
BRL
BRI
8RL
BRL
BRL
BRL
BRL
ARL
BRT
BRL
8FL
BRL
BRL
SRL
BRL
BRL
BRL
ARL
aRf
8RL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
ARL
30.129.528.4
30.030.030.o
70-1&70-1n70-130
pdkS v{et 1.0pgkswet 1,0
t gI€ w€t 1.0p€/kg w€l 1.0
Ug/kgw€l 2.0
Ug/tqw€l 1.0
Pg/kg wel 1.0
lgrSYr€l 1.0
ldkg vJ€t 1.0
lgkg rY€t 1-0
!S/kS s/et 1-0
U€r'kg wet 1.0
!g/kg wet 1.0
Fg/kg wet 1_0
!q/l€|t,€t 1.0yg/kg w€l 1.0
!g/kg wet 1.0pdkg tv€t 1.0
Pg,kgw€l 10.0
ldkgw€r 1.0
!Sr(g Yret 1.0
tdkg w€t t.O
|rg qwet 10.0
tdkS wel 10.0
1,g1,k9 wet 1.0
Fgftg w€l 10
ldkgwel 1.0pSrkS ly€t 1.0pgftgw€l 1.0pdkg vi€l 1.0
Ug,/kS rvel 1.0pdkg Y,/el L0
!S/Fg rvet 1.0
IgL/kg wet 1.0
lgr'kg f,'et '1.0
Udkg vret 1-0pg/t€wet 1.0pg/kgwel 1.0pgfl(gwer 1.0
lgukg u/el 1.0pgkg*€t 1.0
ldkS t€t 2.Opg/tg \r€t 1.0
PgL/kg w€r 10.0
UdkSwet 1.0
lgLitg vrel 1.0
Ugi@w€t 1.0
l|grkg wet 1.0
Ig/kg wet '10.0
pg/|(rg wet m.0
Ugl(g ',r,€l
ldkg w€r
Hgr'kg w€l
1@9896
fhis latoraloA Epotl it Ed rclitl ,ritlrou aa aathorized tig&4utft otr lhe cover page.
' Repo.table Dekction Li.nit BRL = Below Rcpdiry Linit Page 86 of 124
Page 558
Volatile Organic Compounds - Qualiay Control
%RECAnalyr(s) Resuir Flag Uni6 *RDL Lcvel Resutt %RLC Limi(s RpD Limir
Batch ?031602 - SwE46 5030 Soll (high tev€t)
Spike Source RPD
Bl.nk 17fi!1602€LKlr
PleparEd & Anallrz€d: 27-Mar47
Su ttogde : Oilb ronbfl u orom elh ane
LCS {?0: 602€sl l
Pr€pa.6d & Analfzed: 27-Mar-07
1 ,1 ,2-Tric$lorolrifuoroethane {Freon t J 3)
Benzene
Bronrb€nz€n€gromochlorometrane
Eaomodicibrom€Slan€
Bromoform
Ercmomehane
2Autanon€ (MEK)
n€uvbenzene
sec-gulylbenzene
iert4utylb€nzen€
C€.bon disulfide
Carbon blrachbdde
Chlorob€nzen€
Chloro€thEne
Chlo.ofom
Chlomlfiethane
24hlorololuen€
4Chbrotoluene
1,2-[rlbromo.3<l orcpropane
Dibrornodbrornethane
I 2-Dibro.noelhane (EDB)
Dibrsnomehane
l.2Jidlorobenz€ne
l,3oiahlotrobenzeno
1 ,4oichloroberEeneDid orodifl uoron€thane (Fr€on1 2)
I ,l Oichlo.oethane'l,zolchhoelhane
1 .1 Oichloro€thsn€
cis-l ,-Di$loroodt6ne
t"ans-l,2oichbroethene
1 Joichloroprop€ne'1 .3oktlbopropane
2,2oicnhopropan€
1 ,1 .Dbhb@prop€ne
ci+1 ,lDidrldoorop€nelrEns-l,lDidrloroFopene
EthMb€nzene
H€x4hlorobutadiene
z-H€xanon€ (MBK)
fsopr@I4Denz€4e
+lsopropyllolusn€
Methyl iart{uv eiher
4-l €hyl-2-penlrnons (MIBK)
MethMei6 dlbrijo
N+hfral€rE
2 9 0
22.213 .420.423.O
22.123.024.O22.415 .120.121.622.723.119.723.420.021.421.123.422.421 .822_923.421 .S23.823.923.O23.A21.121_420.522.621.122.722.618.922.521.922.422922.31 4 021_722.O21.519,020-022.0
Lig/kg wet
p!|/xg wetpgL/kg f,,et
t/EKg wetpgkg wet
Ug/kg wet
ug/Kg wet
pg/Kg wet
!g/kg wet
Fg/'(g wet
lrg/kg wst
!g/kg wet
fgftg wetpg/kg wetpg/tg wet
!g/kg wet
!g/kg wet
!g/kg w€t
!g/kg wet
lig/kg wet
!g/xg wet
tig/kg wet
!g/kq wel
!g/kg wet
!g/kg wet
!g/kg wet
lrg/Kg wet
!g/kg wet
ttEkg wet
lgr'kg wet
ugirc w€tIg/kg wet
lgLftg wetpgLi kg wet
UEkS,,et
lgL/kg wet
Ugkg wet
pgkg wet
!g/kg wst
l.r9r(9 wet
Lig/kg wer
lgr'kg w€t
lgrkg wet
lEkg wetpg4(g w€l
Fgy'kg wel
trdkg wel
lSftS w€t
Fgftg wet
Pg/tq wet
30.0
2DD20.020_020.020_o20.020.020.o20-02 0 020_020.o2 0 020.020020.o2 0 020.o20020020020.020.020.02 0 02 0 020.020-020.020.D20.o20.02 0 020-020.020.020.020.020-020020.020.020.020.020.020.o20.020.o20.0
97 70-t 30
111 t'-130
67 1. f7 -175
104 70-130
115 70-130
120 70-130
1r0 70-130
1r5 /0-130
120 70-130
114 55.3,136
76 38.8-142
100 70-130
108 70-1K
114 70-130
116 70-130
98 70,130
117 70,130
100 55.3-130
109 70,130
106 70-1gl
111 70-130't'14 70-130
109 70-130
114 64.7-139
117 70-130
110 70-130
119 70-130
120 70-130
115 70-130
119 34 4-167
106 70-130
107 7G130
102 70-130
113 70-130
106 70-130
114 70-130
113 70-130
94 70-130
112 70-130
1r0 70-130
112 70-'130'r 14 70-130
112 G0_7-r40
70 70-130'tD8 7D-13D
110 70-130
108 70-'t 30
95 46.1-145
100 70-130
110 70.'t30
This labonrory rcpod it not valid ruithout an authon "A
fiSnotarc od the co'e, paSe.
+ Reporrable Detection Limit BRL = Belou Reporting Liftn Page Sl of 124
Page 559
Volatile Orgaric Compouods - Qusllty Cooarol
AnalyteG) Resutt Ftas Unrts *RDLSpikeItvel
%RECLimits RPD
RPD
LimitSource
Re6uk %REC
Brtch 7031602 - SW845 5m0 Soil (high level)
LCS t7031602€St I
PrepBred & Analfz€d: 27Jt ar-07
n+opylbenz€n€
Slyrene
1 ,1 ,1 ,2-T€tachldoethane
| , | ,2,2-Tetrachloroeth6n€Tetrad{oroehene
1 ,2,3-Trichbrobenz€n€1 2,4-Tricilorobenzene
1 ,1 ,1-Trid!lorc€han€| . | ,2-Tdchlorelh€neTdchloro€th€ne
Tricilorolluorom€fEne (Freon 1 1)
i l,STnchbIopmpaneI ,2,+Trim€fiyib€.Eenel,3,tTrirnetnyt'b€nzen€
m,p-Xylene
cXYlene
T€bEhydrofuran
€thyt eher
Tert-amyl m€6yi ethe.
Et'ly' ierl-buv eth6r
Di-isoptopyl €th€r
Tert-gutand / butyl alcohol
1,4-Dioxane
Su.rog€l€: al-8rc.r|oduor(6€nzeneSufiogate: Toluene4SS udog ate : 1, 2-DM lo t@lh ane 4 1S unogate : Dib rofi D lfu ordi eth ane
LCS Ouo Oo3l602-A50t)
Prepa(ed & AnalFed: 27-Llar-07
1,'1,2-Tri{:r{orotrifuoroothane (Freon I 13)
Acrylonftrile
BerEerEgrqrrobenzene
Bromochbront€lhan€
Bromodidrbmrnethane
Iroftrclorm
Bronrom€lh€ne
2€'lbFone {MEK)n€utylberE€ne
E6c-&It!4benzen6
red€ltylbonz€ne
C€toar disulfde
Carboh tstEchbdde
Cuoroben:€ne
Chloroethd|e
Chlomform
Chlorcm€lhane
2{hlomtoluen6
4-Chlo'roiolueie
19.325.2
22.520-021.O72.522.520_323-'l
20.625.122.723_521.246.624.120.421.3?0.321.719.9
15730.728.727.828.9
20.511.710.321.221-8m.2
22.522.O14,4r8.115.720.417.618.121.318 .319.9'19.5
20.621_1
20.020.o20.020.020.0m.0m.020.o20.020-020.0m.020.020.020.020.o40.020.020.020.020.0m.o20.02002m30.t30.0m.030.0
20.o20.o20.o20.020.020.020.020.020.020.020.020.020.020.o20.020-020.020.020.020.o20-o
pdkS vrel
ugfl(g wetpg/ko wet
Fg/kg wel
Pqkg rv€t
lrgts vrel
!gl(g 'rv6t
lgr'kg v/st
Ug/kg wel
Yqtg w€lgglkg \rqt
ldkS wet
|,9r'k0 wetp€y'kg w6l
Idkg rvel
Fglkg wei
ldks rYet
!94(g wet
Pg/kg w€I
lgvkg wel
llgtkg wet
!g'l€ "!€t
Ugiko wetpgrtg wet
Yglg rv€lpdks Yrerug/kg w€tlgfllg wetpgr'kg wol
pdkS wet
USftS w€t
Pg/kg Y,€tpgr'kg wel
Yslkg w€l
Pgr'kg r€l
!g/kg $/et
lgLftg wet
Pg/kg '/et
Pglg w€tpdks Yret
lgrkg wet
Ig/kg wetaRs Igkg w6t
pg*g wel
PgAg wel
ldkg rwt
ldkg,r,et$r'kg wet
!g/kg wet
USftg wel
96 70.130126 7G130118 70-130112 70-130100 70-130r05 70-130112 7G.130112 7G1 30102 70-t3t)118 70-130112 70-130103 56.&140126 70-130114 7Gt30t18 70-l3t)to6 70-130tt6 7G.130120 7G130102 70-130rrxi 65.3-130102 70-130lm 70-130100 7G13098 70-13098 34-1 55102 7G13099 7$til93 70-lg96 70-tg)
102 7G.1 30 g
8 1-77-175 11s6 70-130 I106 70-130 It09 70-130 10101 70-130 I108 7G130 6112 70-t30 7110 55_3-136 47:L 8.8-142 590 70-1$ 11sB 7Gt3o 10102 7Gr30 1l88 70-t30 2790 7trtfi) I106 7G.130 t092 55.1130 I100 7Gi30 I98 7t!130 0103 7Gt3o 13106 7G130 f
25502525252525
5050
25
252550252525
Thb bhrrdoty repatt is not ,alid wirtod zn curtorizd slgdalarc oE thz cowr pfuge .
' RePo.tablc D€tection Linit BRL = Bclow Reportiog Limir Poge 88 of | 24
Page 560
Volaaile Orgrnic Compounds - Quality Control
Atrrllt4s) 'RDLUnitsFlagResultSpike
I-evel Result % REC%RECLimns
RPDLimitRPD
B{rch 7031502 - sw846 50J0 sott thigh tfvet)
lcs t uo fictt6it2€sotIPr€parcd & Amtyzed: 27,Mar-071,2-Dibromo3{hlo.opropan€Dibromochlorom€thane'1,2-Dbmmoethan6 (EDB)Oibaomonr€thans1 ,2-Dichlo'robe&eneI ,3-Oi:hfrnobeflzen€1 l-Dlchlorob€nzsh€
(F eonl2)
203
21.5
2 1 . 8
20.4
21.4
21_5
20.8
2 1 . 8
19.4
1 8 . 5
r8.4
20.2
18.7
20.6
2 1 . 3
1 7 2
20.8
20.4
2 0 7
206
1 9 . 8
13.2
19.E
20.0
19.8'17.7
'17 2
1S_8'18.0
225
2 1 . 6
21.6
1 8 . 5
19.6
2 i 1
2 0 1
18.4
2 1 . 6
2 0 6
18.S
20.6
2 t . 2
19.6
42_4
21.5
2 1 . 9
19.7
1 9 4
201
18_4
198
20.o20.020.o20.o20,020-o20.o20020.020.o20.020.020_o20.02 0 020.020_0200i {o20.o20.020.020.o20.o20.020.020.020.020020.o20.020.020-oz).020020020.020020.020.o20.020.020_o20.040.020.o20.o20.020.020020_0200
Lrg/kg wet
lrg/kg wet
Pg/kg wel
lgr'kg wer
!!y'kg wel
Pgftg rv€t
ldks wet
lgr'kg wet
!g/kg wst
rc/kg wet
pg/kg wet
Pg/kg wetygkg wel
!g/kg wetggkg w€lpgr'kg wet
!g't(g wet
lSftS YJ€t
!g/kg wetpg,,kg $/et
lgr'kg wetOcl Ug/kg wet
pg/kg wet
ug/kg wel
tig/k0 wet
ug/kg wel
lJglkg wel
lrg/kg w€lpg/kg wet
lgikg wel
tis/kg w€l
ldks vr€t
lgr'kg wet
!g/kg \ret
Udkg wet
Lig/kg wet
!gL4<g wet
lgr'kg wet
ug/kg wet
Ugr'kg wst
t gu4€ wet
ttg/kg wel
lig/kg wel
!g/kg wel
!g/kg w€l
UgAo wel
rcfig welpgrkg wel
ug!4(g w€l
rcrkg $/el
Fg{(g wel
!g (g w€l
102 70-130108 64.7-139109 7n-130'toz 70.130107 70-130fo8 70-130104 70-130109 34.4-16797 70n3092 70-130s2 70-130'101 70,130
70-130103 70-130106 70-13086 7G1301M 7G130102 70-130104 70-130103 70-13099 60.7-14066 70-13099 70-130100 70-13099 70-13088 46.1-14586 7G130ss 70-13090 70.130112 70-130108 70-130108 70,13092 70-13098 70-130100 70-130100 70-13092 70-130108 70.130103 70.13094 56_e-140120 70.130103 70-130106 70-13098 70-130106 70-130110 7G130110 70-13098 65.3-13097 70-130100 70-13092 70-130s9 70-130
7 2 5
5 5 0
7 2 5
4 2 5
1 1 2 5
1 1 2 51 0 2 5
9 5 0
9 2 5
15 25't0 25
1 1 2 5
12 25
10 25
6 2 5
s 2 5
r 2 5
8 2 5
7 2 5
1D 25
12 50
6 2 5
9 2 5
1 0 2 5g 2 5
E 5 0
15 25
1 1 2 5
6 2 5
1 2 2 5
9 2 5
4 2 5
8 2 5
7 2 5
1 1 2 5
1 1 2 5
10 25
7 2 5
8 2 5
s 5 0
5 2 5
10 25
t 1 2 5
8 2 5
9 2 5
9 2 5
8 2 5
8 5 0
s 2 5
8 2 5
8 2 5
1 2 5
1 ,l -Dichloroethane
| ,2-Oit or*thane
| ,1{)ii$loroeflene
cis. l,2.oichloro€thene
t'ans-1,2,Dicl o,?ethene
I ,2{ichlorop.opane1 ,3Oknbropropene
2,2Oictloropr@ane
I .l Oichloroprop€ne
d91,3-Dicf rloroprop€ne
t'ans-1.lDidrloropropene
Eh]dbsnzere
Hexd orobuladiene
z-Hexanone (MBK)
lsopropylb€nzen€
+bopropyllolugne
Mehyl tert.b'rvl €8ler
+Methyl2+entanone (M|BK)
Meihy'ene chbdde
Naptrthal€ne
n+ropylbenzene
Styrene'l ,1 ,1 .2.TetachloroettEn€1,1.2,2-T€t'€chloroethane
Tshsct oroetiene
Toluen6
1 .2,STricfiloroben?ene| ,2,+T.iilorot€EeneI,|,l-Tricttbro€lflan€
| , | ,2-Tri{filorcEtlraneTdi{oroethgne
Tri*bmnuoronEfune (Freon 1 1 )l,2,aTridftroplopane
1,z,+Trimetay'b€rEene
I ,3,+TdmethylbenzeneVinyl d onde
m.P-Xylene
o-Xyl€ne
T€ffahydrofr&n
Elhyl€ther
T6rl-€myl methyl €lher
Ethyl b.t-bdyl ether
Dlloopropyl ether
T€rl€ubnol / fu tyl alcohol
This lzbontory rcpod is ,at ialid *irtoat z^ aarlrodzed signttttrc on the cavu paEe
' Reportabl€ Detection Limit BRL = Below ReDortine Limir Page 89 of 124
Page 561
Vohtlle Orgrtrlc Compounds - Quality Cotrtrol
Analiqs) Result Flag Units *RDLSpikeLevel
Sourc€
R€sult
RPDLimit
%REC%REC Limi6 RPD
B|ich 7m1502 - SW846 5030 Soil (htgh level)
LCS Duo flft'lm2€SDll
Pr€par€d & Anal!.zod: 27-lrar-o7
1.4{)ioxs|e
S/j7'oga te : 4-Srond@tdenzetES,'toga|€: Tduene4SSlJi'ogate: l,2alchbroethane44Sunoge/€ : Dibtonbfl uotgneth erc
ts6&.3fr.226.928.9
2630.030.o30.o30.o
m.0m.020.020.020.030_o30.030_o30.0
20.020.o20_020.om.030.030.030.ow.o
98
101t0190
106104100'r06
tou1011048893
lgflq w€t
Ugy'tg vretru/kg wet!g € wetpgr'kg w€l
LrgVS dry
ldl(g dry
rdkS dry
t dl€ dry
ldkg dryyqkg drypS/tS dryUglq dryldkS dry
t gllg dry
lryxo dry
lsfts dry
rdrs dry
FdkS dry
udks dryUdlq dryt'dks dryIgkg dry
BRTBRI.BRLBRLARL
BRL
BRL
BRL
SRL
BRL
3+r 5570-13070-13070-13070-1N
7t}-t307Gt307G13070-13070-13070-1fi70-tu7L1nTEtm
70-1307G1307G13070-13070-13070-1U70-19)70-13070-tfi
25
llairlr Soik6 ft03t m2.Msll l
Prcpar€d & Analfzed: 27-Mer47
Senzene
Chlorobenz€ne
1 ,1 €ichbro€thene
Toluen€
Trichloroetlt€ne
Suflogata : ttBtonpfluor$enzoneSutogata: ToltEne4SS','rcgale : 1,2 Oichlotdtane4lS u mgaE : D ib rcmofu rorcneth e rE
P.6par€d & Analfzed: 27-Mar{7
Benzen€
Chlorobenzsn€
I ,l-DichbroetheneTolu€ne
Ttid{oroeth€fi€
Sunogde: 4-ErfilonuotdenzeneS|Jl7ogate: foluene4tSu/ftgete : l,2aichloroethane44Suntga.'!- : DibtoflmfllrE.onelhane
Sdrrc.: SA59O:I9-ll
21.?20.920.1
21.230431.226.127.8
lrrtix Solks Oup t7031m2{#tot} Sou.6: SAS| &St I
19.4t9.317.7rg.419.730.331.426.127.8
s7
8a97
s8,01105a793
8
1 3
I
3030303030
Th& ldbrelarf ,Epotr b t ot fiIU wilhor,t on aulr4fiud sigaaarc ot the cowt ptgc.
* Repo.tablc Dct€ttion Limit BRL= B€low Reporting Linil Page 90 of 124
Page 562
Extractable Petroleum Hydrocarbons - euality Control
SpikeLeveJ
Source
Result
%RTCLi')ils
RPDLi i t
And).teG)
Brtch 703t160 - SWE46 3510C
Elenk O0:ll160-E|LKl I
PrBpared: 2l -t!,lar{7 Anatil.zed: 22,Ma(07
Gasofm
Fuel Oil l?
Fu€lOi l#4
FuelOi l#6
Mqbr Oil
Aliatkrfl Fuel
Unbentfi€d
Othor Oil
Total Petroleom Hydrocabons
CgC36 Alphalic Hyd.oc€rbons
Sr/'|'ogal€j 1.Chloloodadecane
LCS a7clfi60€.st I
Pr€pared: 2 f .lvfar{7 Anatyzed: 22-Mat47
C€-C36 Aliphatic Hydrocarbons
S unqate : l -Ch lotaocl a de c a n €
Brtcn 7031281 - SW846 3ss0B
Bl.nk fl0312€1€LKil
Pt€Eaied: n+Itar47 tu tatyzed: 23-tvlaro7
G6solln€
FuelOi l#2
FuelOl l#4
FuelOi l#6
Molor Oil
Unid€ntitu
ehe. Oil
Total Peuotsrm Hydrcsrbons
ClC36 Allphatic Hydrocarbonsgmogate : 1 -Cht oroo dad e c a ne
LCS ftGI2St +rst I
Prepared: 22-{\,f ar-O7 Anat]fzed: 234tat4i
C€€36 Aliphatjc Hydrocarbons
Su,rogate: | 4hlo@o€tadecane
R}D9/,REC
8RL
BRL
BRL
BRL
BRf
BRL
ARL
BRL
BRL
BRI.
0.04m
1 . 4
0 0520
ARL
ARL
BRL
BRL
BRL
BRL
BRL
aRt
8RL
BRL
2.93
83.3
i .72
BRI
BRL
BRL
BRL
BRL
aRl
aRrARL
ARL
ARL
2.53
Sou.c€: SA595ll{l
91.4
86 40-140
100 60-120
104 60-120
mg/l 0_05msn
hgl(g w€t 13 3tng/kg wet 13-3
hg/kg'.!et 13.3
hg/kg wet 13.3
hg/kg wet 13.3
hg/kg wel 13.3
lngftgw€l 13.3
hglkgwel 13.3
mgri(g wel 13.3
rng/kg wel 13.3
hg/kg wet
nE/kg wel 13.3
tngftg wel
mgftg dry 30.3
mSI(S dry 30 3
mg/kg dry 3O.3
mg/kg dry 30.3
mg&S dry 30 3
ftg,ftg dry 30-3
mdkSdry 30.3
hg/kg dry 30.3
mgl(g dry 30.3
mg/kg dry 30-3
mg/kg dry
mSn(g dry 15.4
mg/l
mg/l
mgr
nE/l
lngd
mgn
mgl
nE4
m9/l
mg/l
mgn
0.050-050050.050_050.050.050.050.050.05
0.0500
1 . 4 0
o.o500
333
93.33.33
88 40-140
69 60-120112 ffi-120
Duollcat l703t28loupit Source: S45O511.01
Pr€pared: 22-t\,{aro7 Anatfzed: 23-Mar{7
Gasolin€
Fu€lOil f2FuelOil#4Fu€lOiltreMobr oil
Unidentifi€dOtt!€r OllTo{al Peht€um Hydroc€ruonsC9-C36 Aliphatc MrocarbonsSun<tgete: t +liotcf,daclecane
mat |I spitr aT0:1t281{st)
ARL
ARL
8RL
BRL
8RL
ARL
BRL
BRL
BRL
BRL
50505050505050505050
3.84 77 4+140
Pr€pared: ?2-lrar47 Analyzed: 23-Mar47C$(::l6 Aliphaltc Hydrocaftons 85BRL1 m
Thk labordory rcporl'B ^or valid without M aaahorizd signoture on the cover page.
* Reporlable Detection Limit BRI- = Below R€portinE Limit Page 9t of 124
Page 563
Extractable Pearoleum Hydrocrrboos - Qurlity Control
Anal't{s) Result Flag UEits RPD*RNLSpikeIrvel
Source
Result o/oREC%RECLimits
RPDLimi(
Brl.h 703l2El - SW846 35508
a$x Spit. OO3t2Ot.ltsll
C€-C36 Aliphatic Hydacatons
Sunogate: 1 -C'rll(,'oodad€cane
Sour€e: SA595ll{l
Prepef€d: 22{tiar-07 Analyzed: ii3-Mat47
Sufiogale : | -Chlomocladecatg 3.92 101
fiatrix Solke Ouo t7031231-lrsoi) SorrE€: SASSSiI{tl
BRL
BRL
BRL
ARL
BRL
aRl.
BRL
ARL
BRL
BRL
3.26
Sourc6: SA5D455{3
86-9
3.14
mdkg dry
ntg*gdry 15-ErngftS dry
mgdqw€t 13-3mg^g w€lt 13-3mg/kgw€t 13.3.ngnqwel 13.3mgr'kgwet 13-3n{rrgw€t 13.3.r'g (gw€t 13.3mSlkS e/et 13.3ft$kgc.€t 13.3oE/kgwel 13.3nE/t(g w€l
mg/tgwet l3-3ntgftg wet
rEr'kgdry 28.5rEn<g d.y 28_5mg/kg dry 28.5rnSftS dry 2A.5nEikg dry 2A.5nrS/kgdry 28.5nE/kg dry 28.5mg/kg dry A.5nEI(S dry 28.5nE/kg dfy 28.5r'g^g dry
mg^Sdry 14.3nE/kg dry
ntgikg dry 14.4firg/t(g dry
41t140
ff)-150
4{J-110
4Ir14I)
m-lm@-1m
1+l4A
5{r15040-tlo
5Gi5o 154Irt4)
89.6
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
SRL
SRL
261
1@.
3.U
3.87
111
3.95
3.3
93.33.33
BRL
Prepared: 22-iiar{7 Analyzed: 2}t-tar-07
C9436 Af phatic Hyd.ocarbons
Suftqate : l -ChloroodEdecane
Brtct 7031!84 - SW816 3545A
Blank aZUll2MAL|(1)
PrepsrBd: 22-lrar{7 An6lrz€d: 26Mar-07
Gasollne
Fud rH #2
Fuel Oil #4
Fu€l Oil #6
Molor Oil
Unbenllfied
Othe. Oil
Tohl Petoleum tiydrocarbqE
C$C3€ Alphetic Hydrocarbons
S unogab: 1 4hloroocTadecene
LCS f703r2t4€Sl )
Preparcd: 22-lrad7 Analyzed: 26-Mar-O7
C$C36 Ailphatic t|ydrocsrbons
s u nog 4e : t 4 hl orc&ade cane
Gasolii€Fu€l Oil#2Fuel Oil {4FuelOll#6Motor Ol
Unidendf,€dOrher OlTotal Petol€um HydaocarbonsC9436 Allphalb MrocarbonsSu/rDgais: t-Cr orooajsdocare
lrrtrlx Sotk t70gt 2&Gfist )
81 3{)
78
10sf i5
Ouollcde l7O3l284rUPl I SdrrE€: SA5gil55{3Ptepdrd: ?2{4ar{7 Analyredr 26-Ms{7
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
SRL
8RL
5050505t)5050505050
3.57
1003.50
1013.61
9 l
Prepar€d: 22-irer47 Anallzedt 26-ttar47
C$'C38 Afphalic Hydrorabons 73.8
Sunoga|jj 14 o/oadadecano 3.06
tlatrlx Solk. Oulr fl0t1284. $)tl Sd|r{s: S459455{t
Prepar€di Z?-lrar-07 Anall|zed: 2&.Mer{7
BRT
SRL
74E5
308694
ThJJ lafuntory tqod ls ,td adld x,ithod on .artodtd sWMt oa the cayer pqa.
+ ReFortsble Det€ction Lisir BRL = Betow R€portine Limit Psge 92 of 124
Page 564
Semiyolatile Organic Compounds by GC - eualiq/ Conarol
Spike
[,erel
Source
R€sul(
%RECLimiLs
RPD
Lirni tAnalyt4s) %RDC
B'.ct 7011270 , SW846 i5l(rc
Blenk 47031270€LKll
Prep€red I Anal}.zed: 22-MaF07
Aldin
a€Flc
b€Hc
dSHC
gAHC (Lindanej
Chlordan€
4,{.DDo (p,p')
4,4-0oE (p,p )4,4{n)T (p,p')
Dielddn
E rdoGulfan I
Erdosullan ll
Endosultan Sutfsie
Endrin
EMdn Aldehydo
Heptedrlor
H€Orachlor Epoxide
Toxapfien€
a4filordsfle
gFchlordane
Endrin Ketrn€
S u ttog8{e : 1, 44 B4tckfl u o to b i p he n yl ( S 4Sutlog'/e: Decachlotobiphenyt ( Sl
LCS Oclt270€a1)
P.6par€d & Anaryzed: 22-Mar-07
Atdtitl
a€HC
baHc
d€Hc
g€HC (Lindens)
4,4{DD (p,p)
4,4-DDE (p.p')
a,+DDT (p.C)Disldrin
Endosufdl I
Endosdfan ll
Erdcdfan Sufble
Endiin
Endfi Ald€Me
Hept dlor
MedDrryd'Jor
Heptadlor Epoxid€
a-Chlodane
g4 odan€
Endrin Kebn€
Surqafe: 1,'11)B4clafl uorobiphenyt (54Sunogate : Dec8f.Jl t oro bi ph e nt l ( S t)
LCS Du! f7031270€SDt l
Pr€psred & Analyzed: 22-Mar{7
Aldrin
a€HC
ARL
BRL
ARL
BRLgRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
8RL
BRL
BRL
0 0 1 7 7o 0190
0 0171
0-0137
0.0126
0.0083
0_0143
0 0 1 4 8
0.0152
0.0187
0 0 1 6 0
0.0154
0.0163
0.0r46
0.0167
0.0192
0.0164
o.0183
0.0166
0.0151
0.0129
0.0168
o_o142o.0163
0.0171
0.0'r32
FEI
u9/lItgll!srpErps4
!s4pdl
lg/lug/l|lEl
!9nljg/l
tstlFSnpEt
tglps4
Lj$4
ps/pg/l
!gn
!EluEl
lgll
!gn
ItElpgn
vgtl
!gr
!sn!s4!srljdl
trglpg/l
lrSll
!gn
ugll
ttgt
tgll
ltsn
9S4
Itgtl
tlg/twl
wlpg4
3G1frwl50
40-140
40-140
40-140
4G.140.{o-140
40.140
40.140
4G140
4G140
40-140
4G140
40-140
40-140
40-140
40-r40
40-140
4G140
40-140
40-14t)
40-r40
40-141)40-14.0
40-140
40-140
0.01000 01000.01000.01000.01000.05000-01000.01000.01000 01000 01000.01000.01000.01000_01000-01000.01000.01000 05000.0't000.01000 0100
o.om00.om0
0.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000_0100 0.02000.0100 0.02000.0100 0.02000_0100 0.02000.0100 0_02000.0100 0.02000.0100 0_02000.0100 0 02000_0100 0.02000 0100 0 02000.0't00 0,02000.0100 0.02000-0100 0.02000.0100 0.02000.0100 0_02000.0100 0.0200
0.omo0.0m0
0.0100 0.02000.0100 0.0200
88
866863427274
948077a2
84s6E292u
64
84
7182
88 2020
Thir laboruory report is ,at valrl tlilhou! sn ^uthodaed sigrau.rc oa th. cover page.
'Reportabie Detection Limit BRL= Betow Reponing Limit Page 93 of 124
Page 565
Semivolatile Orgaric Compounds by GC - Quslity Cotrtrot
Brtch 7031270 - sw846 3510c
LCS Dup ft031?0€SDll
Prepaed & Analfzed: 22-Mar-O7
b€Hc
d€Hc
graHc (Undane)
a,+DOD (p,p')
4.4ODE (p,p')
aJJDr (p,C)
Dieldnn
End6ulhn I
EndosulfEn ll
E dosuLan Suffate
Endrin
Enddn Adehyds
tieptad or
Heptad)lor Epoxide
a4hbdaneg€hlo.dane
Endin Kelon€
SunaC8/e: 4,+D&Mf, uotobtphenyt (StSvmgate: Decact otohipl@nyt (St)
8 cl7031271- SWE46 3510C
Bl.nk r?031271€LKt)
Prepa.€d: 22-l\rar-07 Analyz€d: 23Mar-07
rcB 10.t6
PCB 1?21
PCB1232
PCB 1242
PCB 124€
rcB 1254
PCB 126t)
PCB 1262
PCB 1268
S urog de : 4, +D Boclaf, @ft hiphe nyt ( S 4S mogata : Oarachlo ro hl phe n yl ( SO
LCS t700127t3{trl
Preparedi 22-f!fer{7 Anatyzeat: 2€.Iiy'.ar4l
PCg 1016
PCg 1260
Sqmgate: 4,l-DBof€,fi,0,lotiphenyt (St)Sult]ogate : De.',chlo'ohipl@nl 64
LCS Dup flfti12?1€SDll
Pr€pared: 22-lrar-07 Anal}.zed: zlt ar-07PCB 1016PCB 1260
Sunqate: 4,+OBebtuotobhtEt yt (Sr)Suno8ai€ : De(achhtfiiplEnyl (Sq
Batcb ?03127{ - SW8,t6 3s508
Ehnk lm312ra{Lxt I
Prepared & Anab,zedj 22-lrar47
PCg to16
[email protected] _01650.011€0.01430.0194.0.0t610_o1740-0't640.01,$0.01250.0t650.0152o.0164
BRL
ARL
BRL
BRL
BRI-
BRL
8RL
BRL
BRL
o.1700.21o
2.65
2_76
0.170Q-2tA
2.41
3_O1
0.1700.230
pdl
Itdlus/l!dl|lglpgrl
yg/l
psr!dl!gnt,€/lvgllpdl
rcnt d l
tgtl
l,gIpc4rcnrrdl
[email protected] 01000.01000_0too0.01000 01000.01000.01000.0too
Spikc
kvel
0-02m0.02000.02000.02000.0200o-o2m0.02000.04x)o.02(x)0.0200o,02m0.02000.02m0.m000_02000.02m0.02000.02000.o2(n0.0200
Source RPDLimit
64 40-14042 4G'14069 ,lGl.lt)
76 40-14075 4On,$a2 10-140u 4v14076 40-140a 40-14074 1o-14oE2 {014097 1{tr,r0El ,lt!140
a7 40-140a2 4o-14o71 40-14062 &-1448:l 4G14076 40-14082 40-140
o
1
r45
I
I
2
1
I
I
2
2020m202020m202020mm202020mm20
td lttgllus4pdl
t91lu$psnug4pdl
usn|ldl
02000.2000.2000.2m0-2m0_2000.200o.2000.200
ustlTgIwl$sn
0.200o.2@
udl o-20opsn 0.200F9lpcl
85 3)-150105 tu|fi
fm 4o-14/lll0 rl{!140
M fu | f lr05 tu150
't(x 4G1401m 4$t4085 tulffi115 n-lso
a.m0,2u)
2.502.500-zn02M
2.fi2.500.2000.200
20m
gRL pglkg i€l 28.6
Thb lab?abry ,"ipo.t k '@,tvalu wAhol4 o attahorizd Eig,td,ft o., thc @wr Fg]ge.* Reportable Detecdon Unit BRL = Below RcForting Lirnir Psge 94 of 124
Page 566
Semiyolaaile Orgatric Compounds by GC - euolity Control
Spike
B.tch 703I274 - sw846 35s08
Blank a70it12?4€LK1lPrepored e Analfzed: 22-Mar{7PCB 1221PCE 1232PCB 1?42PCS 12{aPCB 1254PCB 1260PCB 1262PCB t260s@ogab: 4,+Deoctafuo.obiphenyt (sr)Sur/ogab : Cgcechbrobiphenyl (Si
LCs r/0lt27a€s.trPrepared & AnalFed: 22-Mar47PCB 1016PCB 1260S trtoge te : 4, +D B4cta lhht obi p h e nyt (S iSutrwate : Decachlotokipheny' (S 4
LCS Doo 17ut1z7a-ESDi IP.eplred & Analfzed: 22-Mar-07PCB t0.t6rcg t260Suntf,ale: 4,+Dg4ctafluorobiphenyt (SlSu ggate: Decachlonbiphenyl (54
Itupltcar. am3t 27a-Dupl)Prepared & Anab/:ed: 22-Mar{7PCB 1016PCB 1221PCA 1?32PCg 1242PCB t24€PCB 1254FCB 1260PCB.t26?PCB 1268
BRL
BRL
BRL
SRLgRL
BRL
ARL
BRL
2 0 027.1
390
416
2 0 030.0
406
433
2 0 028.6
28.628.6
357
357
2 6 628.6
357
357
28.628.6
ldkS wet 28.6
pS/kS wet 24.6pg/kg wet 28.6pgL/kq wet 28.6
trgL/kg wel 28_6
!g/l€ w€t 28 6
Ug/(g wet 2E 6
!g/kg wel 28.6
Pgr'kg w€t
lSftg vJ€t
lig/kg wet 28_6
!91/kg wet 28.6
|lg/kg wet
lrg/kg wet
!g/(g wel 2E 6
Ug/kg wet 28.6
lrglg w€rpgkg wet
ldkS dry 31-3ps/ks dry 31_3ugtkgdry 31.3
Ug/kg dry 31 3
!S/kS dry 31 3
fdks dry 31.3pS/kS dry 31-3
!g/kg dry 31.3
Wkg dry 31.3pdkS dryldkS dry
udrg dry 30.5
Idkg dry 3O.5
udks dryudks dry
!o/kS dry 31.0
l.'gl€ dry 3t.0
ug/kg drypyl(S dry
70 31115095 m150
109 4G140
117 40-140
70 30-tfr105 njg
114 40-140
12't 40-140
70 30-154100 30-150
3030
Srnrcf,al€: 4,+De41afl @rcbiphenyt (Sr)Smt8,eilg : DaEEchbrohipheny' (St)
Sour.€: 5459548{2
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
ARL
2 1 . 931.3
Sd|.ce: 5A59548-{2
ARL
ARL
ARLgRL
ARL
ARL
ARL
ARL
BRL
BRL
BRL
ARL
BRL
4040404040,lo
404040
Iftlr sdk oo3t27+Ms1)ft€pafied & Anslf.ed: 22-Mar-07PCA 1016PCB 1260
70 30-150100 30-150
106 40-'140
117 40-140
60 30-15095 30-1tu
1 1 1 4 G 1 4 0'121 40-140
60 u15095 30-1fi
Su ftogate : 4, 4- D B;&tafl uo n bi phe n yt ( S r)Sunggahj OecaclfutobidEayl ( Sd
Uatk Solk Duo f/031?.|.llsolt Sorr.c6: SASSs4a.o2Pr€p{ed & Anatl.zed: 22-Mar-07
PCS 1016
PCB 1260
sunwa€: 4,+DBMfluotohiphen l (slSurftgale: Decachblobiphentl (54
Br.ct ?031275 - SW846 35508
gatrk f7031275€lJ(l!
PtEpe€d: 22+rar-07 Anal!.zod: 2$Marry
405
446
1 4 32 8 9
124
469
ft.629_4
31_331.3
341
381
30.5345
387
387
31.O31.O
5050
Thit labotuaory Epor, is ,roa iolld pllhoat an zuihoizt.l slgMture on ahe cover page
+ Reporiable Detecdon Limit BRL = Below Reoonins Linit Page 95 of 124
Page 567
Semivolrtlle Org8nic Compounds by GC - Qr&lity Cotrtrol
AnaMe(s) R€sult Flag Units rR.DLsource %RECResult %REC Limits
Spike
Level RPDRPDLimit
Bra€h 703 1275 - SW8,l6 3ss0B
Blank (703i279ALK1l
Prepared: 22-l\rar{7 Analyzet 25-Mat47
AIddn
a-gHC
bdHc
daHc
g€HC (U6dan6)
Chlodans
4,{-DDD (p,p)
4,aoD€ (p,p')
a,4-DDT (p,p')
Dielddn
Endosulfan I
End€s$Kun ll
Endosullan Sulfiate
Endrin
Endrin Aldehyde
Heptachlor
M€lhoxycilor
Heplachlor Epoxrde
a€t$ordane
g€hlordane
Endrin K€ione
S urog ale : 4, 4-D B4c IE fl uorob i p h e ntt ( S 4Smogata : De c ac h Mhhe n yl ( Si
LCS f7mt27s"Bs1l
Pr€pared: 22-l!lar{7 Anatyzed : 25 -Mat 47
a€Hc
b-aHc
d-BHC
g€HC (Undan€)
4,4.ODD (p,p')
4,4-DDE (p,C)
4,4-DDT (p,p)
Dieldrin
Endosulfan I
Erdosulfrn ll
Endosulhn Suttaie
Endrin
End.in Aldehyde
H€ptad or
Methoqchlor
Hoptachbr Epo{de
aChlordan€
g4t[ordan€
Enddn t(gione
2,4,5,6TC-l/l-Xylene (lS)
Sunogate: 4, +DB4ctafl @@Whed 6lSunogale: Decachlon phenyl (St)
LCS Duo fi0312? 5-BSOll
P.€pa.ed: 22-lr,,lar.07 Anal]/.zed: 25-Mer-07
Aldrin
BRLBRLBRLBRL8RLBRLBRLARLARLSRLBRLEfiI8R!ARLBfiL8RLBRLBRLBRLBRLBRLBRL17.627.1
24.922.621-9| 1.522.622.425.729-926.227-A28.026.329.927.A
31 .9
25.825.628.80.m0t7_729.9
232
28.628.6
28.62S.6
.62&628.628.628.628.628.628.628.628.628.628.628,62A.6n,628.628,628.610.028.628.6
2E.6
pdkS wet 14.3
!g/kg vr€t 14.3
!gn(g 'r,et 14.3
lgikg wel 14.3
!g/kg w6l 14.X
Ugrtg w€t 71.5
p9/k9 wel 14.3
lgfl(g w€t 14.3
!gl(g v/et 14.3
!g/tg 'aet 14 3pglt€wet '14.3
lgJkg wel 14-3
pgtgw€t 14.3pdkgYJet 14.3
!gr(g wet 14.3
ydl€ */gt 14.3
Fg/tqwet '14.3
l|g/t€ wsl 14.3
uc/ts w€t 71 3pgikgw€l 14.3pdks Yr6l t4.3pdXS wet '14.3
UdkS u/st
t g/|€ vJet
pgkgwel 143
!s/kS Y,/et 14.3
ldkSwet 14.3
Igllg $ret 14.3
lgrn(gwet 143
!9,[(g wel 14,3pg/rg w€t 14.3pgkgvr€l 14.3
lgr'kg r€t 14.3
US/kS s/et 14.3
Igr'kg wet 14.3
rcrkg wet 11.3pg/,€wet 14-3
t,gxg w€t 14.3pdxg rel r4.3
ldxg w€t 14.3
USfl(S $ct 14.3
lgikgwet 14.3
rc4tg we{ 1{.3pg/l€wet ll.3
Ig/kg wst
Ugftg w€lpgtlS w€l
F€/kgw6t 14-3
62 30-1fi96 fr-1fi
87 &14079 ,lO-1,10
77 4G14040 40-l:1079 40-14080 40-140so 40-10105 4S1,O92 ,l$1,(}
97 40-1.t0s€ 4{114092 40-140fos 4i-14097 4&1,1093 4&1{)112 ,r0-r40
96 40-140
90 4{114090 40-140tol 40-140r98 50.20082 4L140105 '4+14t)
81 4G1{O 30
T,ts l4bonlory ..pod ls aot vslid totthotl au e,trtorizd sigaaUn on thc covclr page.
' Reporbble Ddecrioo Linir BRL = Bclow REporting Limar Prye of lZ4
Page 568
S€mivolaaile Orgaoic Compouods by GC - euality Control
Spike Source
Brrcl7031275 - SWE46 35508
LCS Duo ft03l275-BSD1t
fu epatd: 22^1etr47 Anal yzed : 2 54at47
a€HC
b-BHC
d€Hc
g€Hc (Lindane)
a,aODD (p,p )4J0DE (p.p')
4,4ODT (p,C)
Dleldrin
End6ulfan I
Endosdfao ll
Endosdlan Sulhte
Enddn
Enddn Aldohyde
ileptacibr
H€ptecl or Epoxide
a.ct{ordane
g4hbrdan€
Endrin Keione
Sunogale: 4, +DEOdafl uorobiplenyf ( SoSunEgate: Oecachlotobiphe nyt (Si
20.s21.4
11.7
21.3
22.9
22_f
25_4
23.4
24.5
24.8
24.1
26_3
29.6
21.4
30-3
24.5
23.4
26.6
1 7 . 127.7
Pg/kgwet 143
!!y'kg wet 14.3
Ugftgw€l 14.3
US.4q vJet 14 3
!ga$ wet 14.3pdkS wet 14.3
!g/kg wet 14.3
!g/kg wet 14.3
IgL/kg wet 14.3
Pg./kg wet 14-3
l,g/kg wet 14.3
Ug/kgwet 14.3
Ug/kg wel 14-3
l4/kg wet 14.3
Pgkgw€t 14.3pSftS$,et 14.3
Pqlg wet 14.3
!9.4(g wet 14.3pg/kg wet 14.3pglkg watUg/kg wel
lrg/kg dry 15.7
l.fg/kg dry 15 7
lgkS dry 15 7
!g/kg dry 15 7
lVkS dry 15.7
uS/kS dry 7A.3
Pg/kS dry 15.7pVkS dry 15 r
l4iks dry 15.7
LrgAg dry 15.7
UgkS dry 15.7
!$'tS dry 15.7
Hg/l(g dry 15.7
lgks dry 15.7pdkg dry 15.7
!g/r(9 dry 15.7gg/kg dry 15.7pg/}q dry 15.7
!gl(S dry 78.3
!g/kS d.y 15.7
!S/kS dry 15.7
lSftg dry 15.7
t'gkg dry
rufts dry
Ugn€ dry 15.6pdkSdry 156|lgr'kS dry 15.6
73 40-140 8
75 40-140 3
41 44-140 2
74 40-140 7
80 40n40 0
79 40,140 13
89 40-140 16
a2 44-110 11
86 ,|tt140 12
a7 40-t40 12
84 40-140 9
92 40-140 13
104 40-140 7
87 40-140 7
106 40-140 6
86 40-140 11
a2 4U140 I
83 40-140 8
93 40-140 8
60 40-t4097 40-141)
28.6
28.6
2 8 6
28.6
28.6
28.6
24.6
28.6
28.6
28.6
20_6
26-6
28.6
28.6
2A.6
28.6
24.6
28.6
28.6
28.62 8 6
30303030303030303030303030303030303030
Duplcato {7031?5O0P1 ) Source: SAs95{a.02
Preparcd: 22-Mar-07 Anatyzed: 2'Ms'-O1
Aldrh BRLaBHC BRLb€HC BRLdAHC BRLgFsHc (Lindan€)
Ct{odan€
4,+DDO (p,p')
4I-DDE (p,p')
{,1OOT (p,p )Oieldrin
EndGUltEn I
Endosullan ll
Endosulfan SuKtste
Endrin
Enddn Aldehyde
tleptachlor
[r€tr|oxydlb.
fiepLdilor Epoxile
Toxsphen€
a4hbrdanegChh{dan€
Endrin Kebne
Swogate: 1,+bBoc6]fllr,robiphenyt (54
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
SRLgRL
BRL
ARL
ARL
BRL
BRL
BRL
BRL
21.5Sunogate: Oecachtotoliphenyt (Si 38.0
tlslrlr Solk. OOlll2T$, Sl) Source: SAs9ga.02
Pr€paBd: 22-ftf ar-07 AhEl,fzed: 25-MaFO7
BRL
ARL
BRL
BRL
BRL
ARL
BRL
8RL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
ARL
BRLBRLaR[
30303030303030303030303030303030303030303030
Aldtnl
a€HC
b€Hc
2S.025.627.3
31.3
31.231:31.2
69 3G150121 3A-150
93 30-15082 30-15087 30,150
Ihh labonto4 Eporl Lt not ialid pilhoul az s$horized sigloturc oa thc cow, page .
+ Reportable D€tection Limit BRL = Below ReportinB Limit Page 97 of 124
Page 569
Semivohtlle Orgroic Compounds by cC - Qurlity Control
Analyt€(t Resr.tlt FlaE Unirs Resulr %REC Limirs RPD
Brtch 7011275 - SW846 35508
tlrt lx Solt. ?03127$ilsll So{.cs: SA5O51N{2
Preoared: 22-llaF07 Anah.led: 25-Mar-07
d€Hc
g€HC (Undd|e)
4,4-DDD (p,p )4,4-DDE (p,p')
4,+DDT (p,p')
Diehdn
Erdosulbn I
Endosufan ll
Endosulfan Sulfab
Endrin
Endrin Aldehyde
H@tacfilor
Hepta.fihr Epoxir€
a4hbrdafl€
gChlordane
Enddn Kebr|e
2,4,5,GTGM-Xyl€r'e (lS)
Suftoga6 : 4.+D84cbnuor&iphenyt (SrlSufiogale : DecachlorobipllF.nyl ( Sr)
13.4
29.633.0u.732.034_832.r30.634. I3 r . 529.43 6 632.5
0,02021.641.5
Iatix Solks Dup l7031275.lrsDll Sosrc.: SA595aA-{2
Prepared: 22-lrar{7 Analrzed: 25-Msr-07
29.726.O27.413.625.931 .33t_434.730.532.134.031.7
24.730_639.030.831.040.0
21.3w.2
BRL
BRL
BRL
BRL
Ald.in
a€HC
BHC
d-BHC
g€HC (Lindane)
4,4-{)DD (p,p')
a,aoDE (p.C)
4,4-DDT (p,p')
Di€Hnn
Erdcultan I
Endosulfian ll
End6uffan Sulfale
Endrin
Endrin Ald€hyde
Hepl,adllor
Heptachlot Epoxido
adrlord€ne
g{hlordan6
Endrin K€ton€
S u nqa te : 4,'nBocb tl uotobi phen yt ( S tSu'7qar! : Decachlombiphanyl (Sr)
al.cb 7031313 - SWt45 35454
g|5nk a703lNl3€LKll
P.6parud: 22-!f ar47 Anal:fr:ed: 24 4d 47
PCB 1016
PCA l?21
PCB 1232
PCB 1242
pgrlqdry 15.6
IS&E d.y 15.6
t gkg dry 15.6
ucrrsdry 15.8
rcn(S dry 15-6
ldkS dry 1s.6
tdkS dry 15-6
Wkg dry 15.6
FdkS dry 15.6pdkgdry rs.6
ldrS dry ls.6
ldks dL15.6
IrdkSdry 15.6
l|dtS dry 15.6
US/kg d.y 15.6
irElg dry 15.6
ldkodry 15.6
Ug/l(s dry
UdI€ drypdkS dry
pgfg dry 15.8pgks dty 15.8
!Sn(S d.y 15.8
Igkg dry 15.8pS/kS dry 15 8
lS/kSdry 15.8
Uglqdry 15.8pdxodry 15.8
!Sn(S dry 15.8
[SI(g dry '15.8
lSftS itry 15.0
ldtg dry 15.8
ldkSd.y 15.6pgtg dry 15.8
liSftgdry 15.8
t/dtg dry 15.8
IdkS dry 15.8
IdkS dry 15.8lrg^gd.y 15.6
FqkS dry 15.Epdl(s dryUS/kS dry
pg/kgwel 286pdkg $€l n.6
lgr'kg rel 8,6
Udl€ w€l 28.6
43 3Gt 50E4 30-15t)103 30n50103 30-150117 3&15095 30-1m106 3G150111 30-150103 30-150112 3{1150103 30-15098 30-150122 30-150101 30-r 5096 30-150124 3S.150104 30n50126 50-20069 g-t 50133 fi,l&
91 30-15083 3G.15087 3G15043 3G15082 3(t-t5t)99 30-150100 3G150'r 10 30-150s7 30.150t02 3G150r08 3G.t 50101 30-t5t)115 3G1509t 3G150s7 3+150r24 3G150s8 3G15098 3Gr50127 30-150107 30-15068 *1fl124 30-150
31.2312312
31.23 t . 231.231.2
31 231.231.23 r .231.231.2
31.210.031.231_2
31.53r.53 t . 531_531.531 .5
31.531.53r.531 .53't .531-531.531.5
31 .531.531-531.53t.5
BRLBRLBRLBRLsRr-aRl
BRL
SRL
BRI
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BRL
SRL
BRL
SRL
8RL
SRL
BRL
BRL
BRL
ARL
8Rr-BRLSRL
BRL
BRL
BRL
SRL
SRL
,1
0
3
2
2
1
2
223
30
30309030303030303030303030303050
50
fhit laloralory Eport ts ,tol rdid v hoat anz horizzd tigrrature oa th. cever pzge.
* Reportrble Dcrectiotr Limit BRL = B€low Reportin8 Limit Page 9E of 124
Page 570
Semivolatile Orgatric Compounds by GC - euality Control
Analyt{s) Resuh Flag Unirs *RDI_ t€vel Result %REC Limits RpD Lirnit
Brtch 7031313 - SW846 3545A
Blenk lTUll313ALKilPrepared: 22-[,lar-07 Anat}rzed: 24-MeF07PCB 1248 BRLPCB 1254 aRLPCB 1260 BRLPCB1262 aRlPCB 126a BRLSunogate:4,4-D&Octafluotobiphenyt(SO 20.0Suftogate: Dqcachlorobiphenyl (Si 27.1
LCS O03t3l3€S1l
Prepared: 22.Mar07 Anatyzed: 2SMar-07
PCB 1016 400PCA 1260 436Surogale.4,44t&OchflMrcbrphanyt(Sl 2O.OSfiogale: Decachlonbiphenyt (Sl 2A6
LCS Duo 1703t313.ESp1]
Prepa.€d: 22-1,,1a..07 Anagzed: 2A-Mat47
PCA 1016 40OPCS 1260 433Surogate:4,44B4cknuombiphenyt(St) 2O.OSurogate: Ddcachlotobiphenyl (Sd j4.3
Duollcro. a7O3 | 3t30upt I So'rrce: 5459576{2
P.6pa.ed: 22-Mar47 Analyzed: 24-Mar47
PCB 1016 BRLPCB121 SRtPCB1232 BRLPCB1242 BRLPCB 1248 sRLPCB 1254 ARLPCB 1260 8.63PCB 1262 BRLPCB 1268 BRL
SunqaE;4,+O&Octall@tobtphenyt(54 22.4SuEEgab: Decachhtouphenyl (Sq 34.5
i'larrlr Soir. 4f031313-tts{ ) Source: SA595Z8{2
Prepered: 22{.iar47 Analyzed 24-MarO7
PCB 1016 419PCB 1260 533Sunogate: 4,+DgockftuotobiphEnyt (St 21 .aS,/'rogate: Decachlotobiphenyl (54 33_7
l{atir Soik€ Dup O03'l313. SOll Sourc€: 5A59578.02
Prepared: 22-l,f ar-07 Anal@d: ?A-Ma.'{l7
PCa 1016 478PCB 1260 552Suflag6l9:4,+D&Oclgflwtobipltenyt(54 20.6Sufiogale: Decaclhrobiphenyl (54 37.a
Spike
P9/kg'.vet 28 6pg/kg wet 28.6
!gA9 wet 28.6|€tkg wet 28.6!g/tg wet 28.6
Ugfl(g welpg.4q wet
!SI(S v'/€l 28.6lgr'kg w€t 28.6
!S/kS wetpg/kg trct
yqKg wet 24.6pdks wet 28.6|lg/r(g wetpg/Kg wet
!S/kS dry 34_6lg/rc dry 34-6
ldkg dry 34-6US/kS dry 34.6
Ugxg dry 34.6
UdtS dry 34-6
udks dry 34.6
USXS dry 34.6
UdkS dry 34 6ps,,tt dryUS/kS dry
ps4$ dry 35.5pglqdry 35-5pgks drypdkg dry
US/kg dry 34.4
lrgkg dry 34-1
UdlS drytidkS d.y
28.628.6
357
357
28.628.6
357
357
28.628.6
ARL
BRL
BRL
BRL
BRL
BRL
6.99
BRL
BRL
34.534.5
444 BRL
444 6.99
35535.s
430 BRL1130 6.9S34.434_4
70 3G1fi95 30-19)
112 40-140122 40-14070 30-150100 30-r 50
112 40-140 0 30121 40-140 0.8 3070 30-150120 3Gtil
404040404040404040
65 tu1AJ100 30-1fl
108 40-140
118 4D-144
60 30-15095 30-1il
110 4G140 2 gJ
127 40-140 7 50
60 30-150110 30-150
Thls laboroloty .eport ir,rot vald withou aA at/ihoitedsigE tan on the eorer ptge.
. Reportable D€tection Limit BRL = Betow Reponing Limit Page 99 of l.)4
Page 571
Semivolatile Organlc Compounds by GCMS - Quatlty Control
Spikekr.el
Source RPD
Limit
Bltch 70312?2 - SW846.3510C
Bbnk {m31272€LKll
Prepar€d & Analt.zed: 22-tdar{7
Acenaphth€n6
1-lr€frylnephthal€ne
I {l€t'.iylnaphthsl€ne
Alrazlne
Azobenzenefi ]|pl.ewldiazine
BenZdlne
Benzo (a) anthEcene
Benzo (a) anhrao€n€
Benzo (a) pyrene
Eenzo (a) pyreno
Benzo (b) fuo€nthene
B€nzo (b) fluot'anthene
Benzo (g,h,i) p€rylene
Benzo (g,h,i) peryene
B€nzo (k) nuoranthsne
Benzo (k) nuorantherc
B6nzob acid
Benzyl alcohol
Bi9€{nbrootrory)methane
Bi9(2d oro€thyl)ether
Sie(zd oroisopropy)€ther
Bb(2-ethylhexyl)phthalale
4€Ermphenyl phenyl ehe.
Buty' benzyt phthatarc
Ca.bazole
4-Chloro-3m€hylph€nol
44hloroaniline
2-Chloronaphthalene
2-Chlor@henol
4.chb|ophenyl pnenyl €ther
Ctrysene
Chrysme
Dibenzo (a,h) e'l|trecene
Dibenzo (a,h) Bnthracene
Dibenzofuren
l2oichlorcb€nz€ne
1 ,$Dichlorobeozen€1 ,4oict{orob€nz€ne
3,3 {)id orob€nzHin€
2,4oichloroph€nol
Die$yl thth€btsOlnetryl phtlalab
2J.DinFtr'y{phedol
Di-n+utyl phhetat€
4,&Dinibo-2{€thylphenol
2,4-Dintrophenol
BRL
ARL
BRL
BRL
BRL
BRL
BRLgRL
BRL
BRL
ARL
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BRI-
SRL
8RL
ARL
BRL
BRL
BRI
BRL
BRI.
BRL
BRL
ARL
BRL
SRLgRL
BRL
BRL
SRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRTgRL
!dl
!dlpdl
lsrpsn!41utyrps4!snt'dl!dl
usll
Fdlpsnpcnpdl
u€tlpgn
ItgJlpsrusfluglpdl
vErpdl
udlu€ttlpgn
!9nFS,Itsrtt(/rtrdlrgltgr!dluglpgrl
lrsrlItsrudlrclpgtlpsnFS4!dl!s,lrgrllrsnpcn
!dludl
0.0501.000.4000.0501.00r_tx)0,0500.0501.00Lm|.001,000.o500.2000.200o_0500.0500.2000.050r.000.G500.3m1.001.m|.001.001.OO
1.001.00|.00r.001.001.001.00r.001.001_000.050o.0500.2001.00r.001.001.00|.001.001_OO1-001.00Lm1.001.00
Thb lzborotot! rcpdrt It not eetid w&hott sn zlthafuar' thr&/ta'u oE tha cova pag..
' R€porEble DEt€ction Limit BRL = Below Reportidg Limil Fsge 100 of 124
Page 572
Semivolrtile Organic Compourds by GCMS - euatity Control
Analytds) RcsulrSpikeLevel
RPDLimitFlrg Unih .RDL
Source %BEC
Result %REC Limirs RPD
B.lcl 7031272 -SW845 3510C
BLnk ?031272€LKtl
tuep*ed & AhdEed: 22-Mafi7
2,+Dlnit ololuene
2,6Jinilrctolu€ne
Di-n+M phthalate
Fluoranthene
Fluoranlhene
H6xachlorcbenzene
H6xachlorobutadiene
Hexachlorocydop€nhiene
Hexachloroelhan€
Ind$o (1.2,3d) pyrene
InderE {l,2,kd) pyrene
lsoplroaooe
2-lvlelhylnaphthal€ne
2Jvlelhyhaphlhal€ne
2+vlslhylphenol
3J-M€thylph€nol
l,laphthalene
Naphthalone
2-lliLoaniline
3+titroaniline
4-llitroaniiine
Nrtobenzen€
2+litroph€nol
4+litophenol
N-NirGodlhethylamine
N-Nitrosodi-r}propylamine
N-Nitosodiphenytamane
P€ntachlorcphenol
Ph€nol
Pyrldin€
H€xachlorobenzene
Hexac{loroei||€n€
I ,2,+Tricibobenz€nsPentad|brcphenol
2,4,tTdcfrlo{ophenol
Hsxef,],lorrbularliene
2,4.GTddilodophend
I u ft ogeb : 2+l@ ro b i ph e nylSu nogate : 2-F ! uoto b i phe n t4Surogai€ : 2.Fluo to ph e notSu[Dgaie. /V/tmb9/Eene{5Sunog/ate: Pherc(4sSunogal€: Teryhanyl4l4Sumgata: Teryhanyl-dl4Su nt''gel€ : 2, 4, 6 -Tti bto ft '€{'he n ol
LCS 17CI2f z€Str
P.€par€d & Anayzed: 22-MEr47
ARL
BRL
8RL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
ARL
8RL
BRL
BRL
ARL
ARL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRLgRL
BRL
BRL
BRL
BRI.
8RL
BRL
88.4u)448.810144.899.799_767.4
1.001 0 01.000.0501.OO0.0501.001.000.6001.001.000.0500,2001.001.000.0501.001 0 00 0501.001.{n1.001.001.00't.00
1.001.001.001.()01.000.0501.001.000.0501.001.00.t 001.001.001.001.000.5001.00
8888891018510010068
to0to0tuto0to0l@t@tu
!s/lygtl
ugl
t E lpgtl
psll
ugr!gl
ugrpsn
rrdl!sn!s/ltj9rpsn
!9/1
!s/lpsrl
ljEl
ugl
vgl
!g l
IS/lyg/l
rsflugtl
Lrgi
t/gl
t (yl
ugr!gl
|Jgl
Ljgl
|ls/l
|'lsnu9nLrgl
PEI
l.r9/lpgl
Ljgl
ttg
!sn!gn|J9/l!gnusluglp9lps,4!g l
3n-1n30'13015-110gtln| 5-t t03t>13030-1301Fl10
Thit lahttulory rcporl it not valit wirtav an autho.iZeA signtfrtre on thz corvr pigc.
. R€portable D€tection Linir BRL = Below Reporting Limit Page l0l of 124
Page 573
Semivolatil€ Organic Compotrnds by GCMS - Qurlity Cortrol
Source
Brach 703122 - SW846 35lm
LCS O(li}l272€St)
Prepared & AnalFed: 22-Mar-07
Ac€mphtheno
Acemphtryler€'l +,1€ttrly'n6phthalone
1.lr€thy'naphlhabne
Anilin€
At'azirE
AzobenzonatDiph€nyldkuine
Eenzirin€genzo (a) aithfacsn€
Eenzo (a) anthrac€ne
B€nzo (E) pyrene
B€nzo {E) pyrone
Benzo (b) fluorar{h€ne
B€ruo (b) nuoranlhenegen2o (g,h,i) p€ryen€
B€nzo (g,h,i) p€rylsE
Benzo (k) Suoranthen€
Benzo (k) fluoranthene
Aenzoh acid
Benzyi alcohol
Bls(z.chloroehory)medtan6
Bis(2-€iloro€tryl)elh€r
Bb(2.chloroisopropyi)€ther
Bis(2+tlrylh6xyl)phlhabr€
4Aomoph€nyl pher\4 ether
auryl b€nzyl phfElate
Cdbazole
4-clrloro.3-methylphenolzl4hktr€niline
z4hbronaphthalen€
24hlorophenol
4-Chbropheny' phsnyt ehet
Chays€n€
Chrys€ne
DiberED (a,h) d|f|rac€r|€
DiberEo (s,h) antlu-acene
Oborlzoturan'l,2{)id$rob€nz€ne
1.3-Oil|llorot€nz€ne
1J-ttdbrob€rEene
3,3 Oichktrobe.Eitine
2,4€ldtloroph€mj
Diedr!y' phthslab
Oime0ryl phtnalab
2.4-Oinr9fiylph€nol
Dl-n{rM phthalel€
4,6-Dinitc2-m€lhylph€nol
2,4-OinihoplEnol
7S.5
78.5
87-8
8 7 8
82.2
&2.2
89_5
89-5
1 1 5
105
r0878.5
78_5
86.1
E6.1
T7.S
77.9
71,0
71.O
Eit.5
80.0
87.6
91.6
56.0
s6.4
79.1
94.5
1 1 8
82_0
80.4
a2. l
68.6
81-2
8 1 . 9
8't.g
8r.4
8t .4
83.3
74_O
64.6
76.4
s0.074.283.379.575.086. I72.2u.7
pg,l
rdl|lglpEl
vsllpsrl!dlpgl
uilItSJI
|ls4
t d l
udludltrgrlFSnpgl
tts/|
usn$gAps^pdlpdlpgl
!dl|ldl
rcIps4!dl
TMpsIt grl
ItsApdl
ItsA|ls4wlrgnpdI
!srutyrwirpgn
!srpgl!gl!glpsnItsrpc/l
t'gltrgl
0 0601.000..t000 0500.050r.001.00o,0501.00|.001.00t.00o.0500 2000.050o.2000.2000.o501_000-o500.3€00.0501.00r.001.001.00't.00
t.00r.00't.00
1.001.001.00t.001.001-001.000.0s00.0500.2m1_001.001.001.00|.001.001.001.001.00Lmi.00t_00
100't00
t00100100100100t00t00't00
1m100100t00100100100100r00100100100100tmr001001001001001(X)r001001m100100t001001m1mr001(X)r00r001001 m100r001001001m100100
78 1{)"r4D7E 40-1408€ 40J4088 ,lo-140
82 a&14002 40-140112 4{t14090 4{r1,{o90 4{t140r 15 G200105 4S.14t)108 4{t1401A 40-14078 40n,$86 4G14086 4$ 140?a &-r4t)78 4G14071 4o-1&71 44-14t)ga {G1{098 .r$.r.to
84 3013080 40-t{o88 4&1109? (t140
56 ,10-lrl0
96 40-14079 40-140s4 40.110118 4&1.10E2 3G.13080 40-140s2 40n4069 3013081 4G.1{O82 4G14082 4{t140E1 4G14081 40-14083 4O-l,O74 &1&65 4Gr4476 ,1014{1
90 40-14074 30-lfl)tx) 4&14080 4Gl,l075 3013086 4.Gr4072 3o1?o85 3&13t)
This labetory q,on is not ealld withord an aun2orized slg&atzre on tte corer lroge.i Rcportable Detection Limia BRL = Betow Repodng Limit Page 102 of 124
Page 574
Semivolatile Organic Compounds by GCMS - Quality Control
Anaye(s) Resull F lag Unns 'RDLSource %RECResult %R-EC Limirs
Spike
L€vel
R?D
LimitRID
ktch 7031272- SW846 3510C
LCS {7031272€5fi
Prepared & Anal]/zed: 22-Mar-07
2,4-Oinifobluene
2,Boinibotduene
Dl-n{ctyl phthatate
Fluoranlfi€ne
Fluoaen€
H€xachldob6nzen€
tl€xEchlorobutadfene
tl€xEchlo.ocvclopenladiene
llexachloretfuns
Indeno ( I,2,3-cd) pyrene
i.deno (1,2,3dipyr€ne
2+vlethylnaphlhalene
2+vlethyln4hthalen€
2-fr,ls{trylprt€nol
3 y'-M6lhylph€nol
Nsptffid€ne
2j,litro6. line
3J{itso ilineiH{itrosriline
NitsoberEene
2.1'lltrophend,l+litrophend
NJrlitosodimethyJarnine
ll-NltlosodFn{ropylamine
ll-Nitosodipft 6nylarnins
Pentachloropheml
Pflenanthrene
PlFnd
Pyridine
Hetachloobenzene
I .2.+Tridbrob€nz€neHexachbrcethane
Pentachlorophenol
2,4,+Tri{$brophenol
HexaafibrobvHiene
2,4,GT&$hr@henol
Swrogale : 2+hmobiFnenylS/J/'oga|€ : 2 + h-atubip,he n y'Sunogab: 2+fuotophenolSunogate: Nibobanzene4'Swtugabj Phercl4sSuiqale; fephenMt4Sunogale: ferpheaYd4Swft gate : 2,1,6Tn b(ono ph en o I
Iatlx SDlk. O031272.f, srl
P.€pded & Analfzedt 22-MaF07
8 4 9
89.0
1 1 6
76.9
76-S
6'1.6
8 1 . 6
76.0
75.9
70.0
7 4 2
73.0
7 3 0
88.8
84.0
84.0
70.2
72.2
8t-7
8 1 7
8 5 2
48.2
1 1 6
9 6 0
76.9
5 6 9
77.1
40.4
98.6
6S.4
76.3
16.3
79.5
a2_7
82.7
83.5
76.0
7 8 9
7 4 2
6S.4
87_0
75.9
62_7
85.945.969.O10270.249.189.176.7
Sourc€: SA5q5634t
85 40-140
89 40-140'116 4o-lulo
77 40-140
77 40-140
62 10-140
82 40-140
76 40-140
76 4+140
70 40-140
7{ 40-140
73 40-140
?3 40'141)
89 40-140
84 40-140
84 40-14{
70 40-140
72 44-130
82 40-140
82 40-14n
85 40"140
8A 40-140
116 40-140
s6 40-t4t)
77 30-130
57 30-130
77 40-140
40 40-14u
99 40-'l4r
69 30-130
76 40-140
76 40-14{l
80 30-13t)
83 40-140
83 4G140
84 40-14{)
76 40-140
79 40-140
74 40-140
69 30-130
87 30-130
76 40-140
63 3G130
86 tu13086 3lr13l)69 15-110t02 30"13070 15-11089 30-13089 3+13077 1L110
!9/lpgn
!9/lpgn
Lj!/l
u!/l
!qi I
u9/l
Lj!/l
!wlp9/l
utylgg/r
pg/l
pg/i
ttg4pg/l
pg/l
y9!l
gg/r
ugnpgnpgnpgn
trS/lpg/l
plyt
us/lug4|lg/l
pgn
pgi I
vglpgtl
!(yl
ugl
!gnps/lptufs/l!9/1pg/l
ugnpsr!s4ts4PEudrpsAuElusn
1.001 0 01.001.000.0500.0501.001.000.600r.001.000.200o.ofi1.001.000.0501.001 0 00.0501_001.001.001.001.001.001.001_OO1.00t.001.000.0501.001.000-0501.001.00.t.00
1.001.00'L00'1.00
0.5001 0 0
100100100'100
1001AOr00100't00
r001001001001001001001001001Ul1001001001001001001001DO1001001tro100'r00
100100100100100't 001001001001001001001001N1001001M1001N
Thit hboturory ftpott is dot yalid withota tn authortrpd signot',re on the coecr poge .
+ Reportl$L€ Detection Limit BRL = B€loq/ R€porting Linit Page l0l of 124
Page 575
S€mivolatile Organic Compoutrdr by CCMS - Quality Conrrol
Spik€
favel%RECLimit!
RPDLimit
SourceR€sult %REC RPD
Brtch 7011272. SW816 JslOC
t{atrir aoks fl031 272.l|slr
Preperad & Anall.2ed: 22-Mar{7
4'Chloro-Smethylphenol
2-Chlo{ophenol
1,4-Olchlorob€nz€ne
2,+OtliLoioluene
4+litrQhenol
tl.t{trssodi"n+ropylarnlne
1 2,+Tdahkrob€nzene
Pe.rtaatdomphend
Suflogah. : i-Fl@nbiphenylS u nEgato : 2 + hMo biphen ylS@ogate:2+lt@tod6nolS!,tr9ga/r€: t'litohenzene4sSuftogate: Phenol4liSnogate: TeryhenYd4Suftogal€: Tephenyl44
Sourcs: SA59553-O4
78.476414113369.,176.691.783.2r0613689.569-5G4.810680.4u.465.781.36',094.894.4
81.7a1.716014359.6a2.7s0.694611415099.099.067.611483.08:t.o69.492.169,3161M74.5
wpdl
!dlggl
|rsnvilwl|lgnpdl
!gl
1|dl
lrsil
!gl
FS,l
!dl|ldl|l(ylp[ylpsnrgl!dl!dl
w!sr
aM7 pg'l
aM? lgl
ug/rygyl
ts,|ysil
FdroM7 p94
rdl|'lg,fl
@lFg/l
Fdltlsfl!dlItgAps?l
IEJIl|gilps4
71 40-14071 4Ga140127 30-130120 30-13063 4G14t)50 40.140$ 30no75 40-140ss 3&130124 30-13t)81 40.14081 40-1{05a 40-140s5 30-13072 tu1fi72 30-13059 1511079 g-1305A 1511085 *130a5 a)-19)63 l | l to
76 4614076 4Gt,O148 30-130132 30-13064 40.14071 40-14084 3G13088 4G.140106 30-i 30139 30-13092 40-1fi92 &166:t 4G140106 3$.130n tu1frn 30-1fr64 15-110a5 g-lm
N 161109a tu13098 30-13069 15-110
0-050'1.00
1.00|.00t.mr.001.001.001.00|.000_050r.001.00'LOO
1 l l
1 1 1
t 1 1
111
111
1 t 1
1 1 1'111
1 1 1' t 11
1 1 1
t i 1
1 r l
1 1 1
l t l1 r l1 1 1l t t1 1 11 1 1f l 11 1 1
108
108
108
108
r08
108
108
104
108
r08
104't08
10s'! 06108t081M1(R10410e108108
BRL
BRL
BRL
BRL
ARL
ARL
SRL
SRL
BR!
BRL
BRL
SRL
BRL
BRL
Sun9gEte: 2,1,6Tnbtunophenol 69.6
ItLlrir Spik€ Duo l703tT/2- SDll Souree SAtS9ti6$04
PreEared & A^alyzed: 2.t(et47
AcerEphthen€
44hbro-3m€fiylphenol
2{hbrophenol
| ,rt{idiorobenzen€
2,4-Dtrritrotoluen€
+Nifoph€nol
N-Niuosodi+propylamin6
Pentaddorophenol
| .2,+Trichbrob€nzenePentad orophenol
Su nW aE : 2+ I uorobi p lE n II u nEgate : 2 -F I uorobiphe nylS/,,/'cgate: 2+luorophendSuftogale : Nitrohe n zene 4 5S!/'rogde: Phenol45Sg'7Ega|i-: TeAh@yl4HSU/'$ge/€: Teryhenyl44Sl'/twete: 2,a,6-Ttib@nophanol
B.td ?01279 - SW8,l6 3ss0B
Ahnk fr0:}1279€LKl I
Prcp€re{t Z.ljar-o7 Analyzed: 23-t Er{7
Acenaphtr€n€
Ac6naphf)yl€ne
Anilino
r_000-0501.001.O01.00't.00
1_001-001.001.000.050|.001.001-00
8RL
BRLgRL
8RLgRL
BRL
ARL
8RL
ERL
BRL
BRL
BRL
ARL
BRL
m20?()mm20fr20
202020m20
77t510
t l11 61 1l 1
t 31381 1
BRL
BRL
BRL
BRL
rc49 wetrc/Xg rr'ettrg/kg r€t!94(g rel
330330330330
This labontorf rqoi ts Eat vdid i' hoa anat lhorizd stgnant}z on thz qte.r page.
'Reportable Detedion Limit BRL = Below Relorting Limir Pag€ I 04 of 124
Page 576
Semivohaile Orgatric Compoutrds by GCMS - eurtir-v Cotruol
Spike
Level
Source
Result
%RECLimits
RPDLnnitAnalFe(s) %REC RPD
Brtch 70312?9 - SW846 J5508
Bl.nk O031279€LKll
Prepared: 22-Mar{7 Anatfzedr 23.MaF07
Azo!€nzene/Diphenyidiazine
B€nzidin€
8€nzo (a) antriraoene
B€nzo (E) pyreneg€nzo (b) iuoran$Ene
B€nzo (g,h,i) p€rylene
B€nzo (k) fuorenthene
Benzolc acU
B€nzyl dcohol
Bb(2-cl oro€hory)methane
Bb(2-cfi loro€tryt)€ther
Bis(2-chloroisopropylFther
ab(2-elhyltl€xyt)phthatale,l€mmoph€nyl phenyl etrer
AUV b€nzy' phthalat€
Ce.bazole
4{hbro-3-fir€thylphenol
4{hlorcan ine
24hlorooaphthalene
24hbrophenol
4-ChbroptEny' phenyl erher
Chrysene
Dlbel€o (a,h) anhracene
Dib€nzoturafl
1 t-DichbroberEeneI ,3-DlciknoberEene
1 ,4-Dictllorob€nz€ne
3J .oic* orcbenziline
2l-Dlchlorophenol
Distryl phthalaie
Dimelhyl pMalata
2l-Dlm€thylphenol
Di-niuM phthalBb
d,ruhiro-2-mebylphenol
2y'-DlnlrophorFl
2,4-Dinihololu€ne
2.G-Dlnitrotolrrene
Di-n{clyl phft.ratab
Fluoren€
H,Ex*nloaot €nz€n€
lbxad o.obutadi€ne
Hexachloiocyclop€nladi€ne
FlEx6chkro€tf|an€
Indeno (1 2,kd) pyrene
rsoptloaon9
1 +r€tryhephtral€ne
2-nl€thyhaphthalene
2-lrethylphonoi
3,4-lrefhylphercl
l,laphthalen6
BRL
ARL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
ARL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
SRL
sRtBRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BFIL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
!g/kg wet 330
trg/kg wet 330
ug/kg wel 330
uglkgwel 330
lg/kgwet 330
!g/kg wot 330
Ug/kg wet 330
Pqr'kg wel 330
lgr'kg w€t 330
lsnq',vel 330
lgkg wer 330
lgikS wel 330
ldkg wet 330
lgr'kg wet 3i]0
!94Q YJ€t 33O
!q/kg w€t 330
!g/kg wet 330
Lig/kg w€t 330pq/kg wet 33O
!g/kg wet 330
!g/kg wet 330
lgr'kg wet 330pg/kg wet 330
Lig/kg wet 330
ligr'kg wet 330
pgftg wet 330pg/kg wet 330
!g/kg wet 330pS/kS wet 330
ug/kg !!et 330
Lig/kg w€t 330
Ug/kg wet 330
!g/kg tlet 330
!g/kg wet 33O
pglkgwet ?30
iJq/kg wet 330
lgr'kg w€t 33O
pg/kg wet 3:)0
!g/kg wet 3:]0
!S/kS vr€t 3:}C
pgr'kg wet 330
!g&g wel 330
ttSlkgwet 330
lgkS rvet 330
UgL/kg w€t 330
Ugr'kg w€t 330
pg&g wel 330
Ug/kg wet 330
pg/kgwel 330
t,g/kg n€l 330
!9,49 w€t 330
Igftgwel 3:)0
This laborolory rcport ls nol wliil wilhoet ar, suthoize.l cigdattue od the col'€r prye.
' Reportable Detection Limit BRL = Below Reporting Limit Page 105 of 124
Page 577
Semivolatile Organic Compounds by GCMS - Quelty CoDtrol
AnaMqs) FlagR€sult Unirs .RDLSpikelavel
RPDLimit
Souce %REC
R€sult %REC Limit! RPD
Brich 7031279 - SW846 35508
B|ank 170312794LKl1
Preoa.€d: 22-l1tar-07 Analyr€d: 23-&1ar47
2+litro6nilirF
3{.lilrDaniline
4-ilitroaniline
Nitrob€rEerE
2-ilitrophenolll+liuophenol
N.NitEsod-rnetrylanine
lgNitrosodi-nf ropylsmine
N-Nibosodiphenylamhe
Phemnh|gn€
Phenol
Pyndhe
1,2,4,Tridrlorobenzene
2,4,gTricilorophenol
2,4,dT.ichlorcphenol
Surcgale: 2+lrcrobid16nylSutroga te : 2 + horophenolSurcgalc: Nlhobenbne4jSrnrogator Pheno,.d5Surogate : Te.phenyl4l4Sufiogab : 2,4,eTdbrontophend
LCS f?03r279€Stl
Prepared: 22-{\rar-07 Analyzad : 23 JJ,a( 4I
Aniline
Azobenz€ne/Oiph€nytdiazine
B€nzldlne
Eenzo (a) anthracene
B€rEo (a) pyrene
Benzo (b) lluor€nthme
B€n:o (9,h,1) p€ryienegenzo (k) nuo€nthenegm2dc acid
Beozyl alcotlol
8is(2d oroe0rcryFnethane
Bis(2d{oroethyl)€6ler
Bis{2drlorolsopropt)elher
Bb(2+lht4hexyl)pht|etale
4SromoplEnyl ph€ny' o[|€r
Buqy' berEyl phhabis
Carbazol€
4-Chlorc3fiethyth€ml
4thloroenlin€
z.Chlolonaphthabn€
24hbmpl|enol,4-Chlorophony' ph€ny' ether
ChryserE
DD€nzo (a,h) anthrec€ns
BRL
BRL
ARL
BRL
8RL
BRL
SRLgRL
ARL
8RL
BRL
BRL
BRL
BRL
sRtgRL
BRL53501050489039m6140s30o
5270i9t03390521053{t043907535 t t 053S05060495058403i,504t30346t)39503520491054404720
36i103620495039805960s55052m
467086706670667066706670
667066706670
667066706670667066706670aa7066706670667066706670667066706670667048706670
w70
6€7066706670
pqkgwel 33O
Ygrlg rcl 330
udkswel l3mpg/kg wet 330
ligl€wel 330
rgrtg wel 13m
lg/kgw€t 330
Ugr'kg rsl 33O
lgAg Y{et 330
Ygtl€s/et 33Opg/rgwet 33o
Fgtgwsl 330pdkSt{€l 3:10
ldkg wet 330
lgr'kg wst 330
tglgwet 330pglkg vrel 330
Pqtg vr€tpdkg welps/ks v/etlgL/kg vretlgr'kg wetl|gilq wet
pgr'ko rrcl 330
USftg$ret 330
!g/to wet 30
Ig^gwet 330pg&g wel 3:10pdkgtvet 3ix)
!4k9 wet 330
lgL/kg wet 330
ugfl(gwst 33Op94!g wet 330pg[]g wot 33o
Fgkgrv€l 330pg1(s lnet 3:t0
Fgr'kg w€t 330
!g/t(g wel 30
l|g^g wet :l:|,0
Ig/kg wel 33O
Fdkgrv€t 33opdkg rcr 3ii0
rcr'kg Y/et 33o
ldkSwet 3i,0
Fg/t€ wBt :|i|0
Fg/kg wel 3i)0pgkg w€t 330
l.rgt/lqw€l 3li0
lgr'kg rvet 330
lgil(gwet 330pg&gurer ii:m
N 30-13061 15-11073 N-1N59 ls-11092 30'130N 11110
73 40-130?4 40-1eO51 40-13078 40-13080 4G13066 40-13011 0-130t7 44-13081 40-t3076 8.1n74 4G13088 40-13050 G13062 40-l$52 40n 3050 40n3053 4113074 4G13082 4G13071 40n30120 40-13054 40-13054 40-13074 40-13060 40-13089 40-130&, 4&13078 40-130
Thls labontory tqort it rd yald Nithod an a,/lt ottzd lngddure oD dE cot.' pagc.
. R€portsble Dele{tion Limir BRL = Below Reportiog Lirnir Page 106ofl24
Page 578
S€mivolatile Org|oic Compoutrds by GCMS - Quality Control
Anal),te(s) Resu!t Flag unitsSpikc
Level
RPDLimit*RDL
Source %REC
Rcsult %REC Limits RPD
Batch 7031t79- Sw846 35$B
LCs a7031279€Sll
Preper€d: 22+4a.{7 AnatyzaX: 231,tar4t
Dib€rEoturan
1 .2oi(t|b.oberEene
1,3oic*rlorobsnz€ne
l,4oidrb.oberEen€
3,3'4{chlorob€ntdine
2,4Jidtb{ophenol
Oietvl phthalate
Dinr€thy' phtlEbl€
2,4-Olrn€0yphenol
Di-$t|nyl phttahb
4,6-Dhirro-2{ethylphenol
2+DlnltTophenol
2.4-Dk roloh/€ne
2,fl)inilrotoluene
Dl.n.octyl phihalate
Fluoranfi€n€
Hexadrlorobenzene
H€xadrlorobutadisn€
Htsxaddoroqr'cbpertadiene
Hexadlbroetlgoe
Indono (1,2,3-cd) pyrene
| +rrsthylnaphthslene
lgophorone
2-Melhylnaphthalene
2-lrr€bylphenol
3,4-lrelhy,iphenol
Naphfia{'ene
2+lit oadlin€
3-l,litroaniline
4-Nitroanllhe
Nilrob€ruen€
2i litroph€nol
4-Nltmpr€nol
N-f .libosodim€thy'amine
N-l.li[osodi-n.p ropylamine
N+lttosodiplrenylamine
Phenanth,en€
Ph€nol
Pyddhe
1 ,2,+Tridrlorcbenzene2,4,STrid o.oph€nol
2r,GTrid oroph€nol
Sunryate : 2-H twofi p h e nylSIJ''c{ate:2+lrcmpheno!Sutugete : N ilro ben ze n e4 5&fiogato: Phenol4sS|J/.ogate: TaAhany'4l4S uft gate : 2, 4, 6 f dbro noph e n ol
$40507036604730656036205 1 1 050,103100526041404470561059605160524051005710474046m43205',l7051903700414038404030381047006430672033703520443040003990555053005010366051603010440049504090525037tu3890350057405670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
8670
6670
6670
6670
6670
6670
6670
6f'70
6670
6670
6670
6670
66706670
667066706670
!g/kg wet 330
Pg/kg wet 330
rc/kg wel 330
!g/kg wet 330
lrg/kg wet 330
Mkg wet 33O
!g/kg wet 330pg/kgwet 330
lig/kg wel 330
lgikg wel 330
!g/kg wet 330
pg/kg wet 330
lglkg w€t 33O
lgr'kg wet 330
lAlkg wel 330
lig/kg wel 330
!g/kg wet 330
!g/kg wel 330
Pg^g wet 330pglkgwet 330
!g/kq wel 330
trg/tg wel 330
Fg/kg wel 330
lig/kg w€t 330
!g/kg wel 330
!g/kg wel 330pglkswet 33O
Pg/kq wel 330
Pg/kg wel 330
Fgikgwet 330
!g/kq wel 1320
!g/kg wel 330
Ug/kg wet iBo
tgRgwet 1320
Fg/kg wel 330pg/kg wet 330
t/g/kg wel 330
Pg,/kg wet 330
!g/kg wet 330
PgL/kg wet 330
Pglkgvet 33Opg/kq wet 330
!g/lg wet 330
!g/kg wst 3i]0
Fg/kg wet 330
Pg/kg w€t
!g/kg v/et!9Ag Y/et
PSI(S wet
Pgks w€t
Ugfts wst
81 40-130
76 40,130
58 40-130
71 40-13)
98 40-130
u 40-13D
77 40-1XO
76 40-130
46 40-130
79 40.130
67 40-130
67 4G130
U 4t1"130
89 40.130
77 40-130
79 40-130
76 40-r 30
86 4{t130
71 40-130
69 40-130
65 40-130
78 40-130
7a 40'14C
55 40-130
62 40-130
58 40-130
60 10'130
57 40-130
70 4G130
96 40-1 30
101 4O-t 30
51 40-130
53 4G130
66 40-r3o
60 4G.130
60 40-130
63 40'130
79 40-130
75 40-130
55 40-130
77 40-130
45 40-130
66 40.130
74 4n-130
61 40,130
79 30-13056 15-11058 30-13052 15-11086 30'131)85 15-110
oudtcar. o0: 2790uPl) Sourcer 3A59497{5
kepared: 22-t d-07 Anat'Jzd: 23.tiat47
Thb tttorrloty rcpotl ir nol r,zld withod c, otthorizad signo!fie on lhe av, pa&e.
i Reporiable Detection Limit BRL = Below Reporting Limit Page l0? of 124
Page 579
Semivolatile Orgatric Compoutrds by GCMS - Quallty Control
Analyte(s) R€,sult RrB Unils Result %REC Linits
Bstch ?031279 - Sw8.l6 35508
Duolicarea703l279{UPl) Sourc€:Sl594S?{5P.€par€d: 22-l\,lar47 Aml}r2ed: 23-Mar{7
Acemphthen€
Acenephhyl€n€
Aniline
Azobenz€ne/Diph€nyldiazine
Bonzidiae
B6nzo (e) anth.acerE
Benzo (a) pyr€neg6nzo (b) fluoraMene
Benzo (gn,i) peryl€n€
Eenzo G) nudantherEgenzoic scid
B€nzy' slcohol
Bis{2dtloro€thdy)nElhane
Bb(2drlorcehyl)ether
Bis(2drlorolsopropy')€the.
Bis(2-€tlrylh€xy')phthalate
4-EromoplEnyl phenyl e0€rgutyl b€nzy' phthahte
Carbazolo
4{hloron{fiehylphenollLcl$or@niline
24hbronaphthal€ne
2-Chloropt€nol
44hloficph€oy' pheoyt eth€r
Chrys€n€
Dibenzo (a.h) anthrac€ne
Dibenzofuian'l 2-Oi..hl].ob€{Eene
I,3-Didtlo.oberEene
1 ,+Dic* orobenzene
3,3'Oichbroben:bine
2,4-Oi$brcpheml
Di€thyl phthdale
Diflr€ihyl phlhalate
2,+Dim€lhy'ph€nol
Di-o-butyl ph{halEte
1,GDfr {1rc-2<nathyhh6nol
2,4ohnroph€nol
2,+Dinitotoluer|e
2,6-Diniboblrerc
Di-n-octyl phth€bts
FluoranttErF
Fluor6ne
H€x8chlo(ob€nz6n€
H€rcd orobutadion€
H€xachlorocydot'€ntadi€n€
Hexachloro€[rane
Indeno (1 ,2.3-cd) pyr€ne
1 -lretrykraphttubne
lsophqofle
BRL
ARL
BRL
BRL
8fiL
BRL
BRL
BRL
BRL
BRI-
BRL
BRL
sRrBRLBRLsRrSRL
BRL
ARL
8RL
ARL
BRI
BRI
BRL
ARL
BRL
ARL
BRL
BRL
BRL
BRL
SRL
BRI
SRL
8RL
BRL
BRL
BRL
ARL
BRI
BRL
8RL
ERL
ARL
SRL
BR|-
8RL
ARL
8RL
BRL
8RL
BRL
pdkgdry E55
Udkgd.y 955
US/kS dry 855
lgko dry 855
rglgd'y 855
ldkS d.y E55pdrg dry S55
ltdkS dty 855
udkqdry 855
r4/ko dry 8s5q (g dry 855
uSftSdry 855
ldkS dry 855
Udksdry &55
ugftgdry &55
PdkS dry 8s5
lIgftS dry 855
lgrgdry 055
FdkS dry 0s5
lgl(g dry 855
|lgI(S dry 455pqkgdry 8ss
IS/kS dry 855pdksdry 855pgrgdry e55
lgkS dry 855ydks dry 855
FdkS dry 855
udks dry S55pdtg dry 855pdks dry 855
udks dry 855
ldkq d.y 855pglkg d.y 855
rdksdry a55pdkSdry 855ps/kS dry 855
LrgtS dry 855
ldkS dry 855pglkgdry 855
rdksdry a55
udrsdry 855
!S4(S dry 855
Uglkgdrr 855
udr€dry 855
udkg d.y 855
Idts dry 855pslk0dty 855
udrsdry 855
ugxgdty 855
tlglks d{y e55
Idkgd.y 855
BRL
BRL
BRI-
ARL
BRI.
8RL
BRL
SRL
BRL
BRI.
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ERL
BRL
BRL
BRL
BRI
BRL
SRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8Ft-
BRL
BRL
SRL
ARL
BRI.
BRI.
BRL
50
50
50
5050
50
5050
505050
50
50
505050505t)505050505050505050505t)5050505050505050505t)
Thb labordory rqo.t b nol vdid Ntlhout crr tttdrarized slgfi4lar. od thz .aje, p.ge.
'R@ortabl€ Detection Lirnit BRI = Below R€porting Limit P€e 108 of 124
Page 580
Semiyolatile Orgenic Compounds by GCMS - euality Control
%REC RfDAnalyte(s) Resuk Flag Units +RDL L€vel Resutr %REC Lirnirs RpD Limit
B.r.h 7031279 - SWt4615508
Duollcab (7031279OUPi1 Source: SA5S497-05
Spike Source
Prepared: 22-lrar-07 Anat\zed: 23-MatO7
2-[,lethylnaphthalene
2-l{€Urylph€ml
3,4-l-lefrr4pfi€nol
Naph[|ai€n6
2-l'lilrcannine
3-|.l loa'|iline
4-f'{itsoaniline
Nitoti€nzene
2+.lifoph€nol
+Ntrophenol
N-N ro€adnn€thyamine
N-Nfoosodin-propylamin€
N{.lilrosod{,h€oyiamine
Pentachlorophenol
Phenantfirene
Phend
ryntifl€1,2,4-TdCfi lo.obsnzsn€
2,4,$Trichlorophenol
2,4,FTrichlorophenol
Su.ftgate : 2+hMobiphetrylSuftcgeto : 2 - FI uaft ph e no IS.J ' rogabjNl funzene4sSuflEggte: Pheno!4sSunogate: Tephenyl4l4S unqala : 2, 4, 6 -nibm m o ph en o I
Matrlx Solk 4031279-MSt) Sourcer 3459497{5
Ijs/kg dry 855
USI(S dry 855pg/kg dry 855
t4ikS dry 855
Ps/ks dry 855pgkS dry 855
udks dry 3/'20lgn€ dry 855pdkS dry 855!S/kS dry 3420
!g/kg dry 855US/kS dry 8s5ldkS dry 855lgkg dry 855
LidkS dry 855prykg dry 855!S&9 dry 855
tig/ks dry 855ldkg dry 855Pdkg dry 855
us/ks dry 855l4/kg dryugks dryUgkS drytidks drylsfts dry!9&S dry
!g/kg dry 418
S/kS dry 418pg/kg dry 418
f.rgkS dry 414
ldlq dry 418
USAS dry 1670
ldkg dry 418
|ls/ks dry 418
f.igkg dry 414
ldls dry 418
lgkS dry 418
ldks d.yldkS dryt/91(9 dryrgl(s dryUStXg dryll91(S dry
t gkg dry 418
ljgkgdry 414lghg dry 418lrglq dry 418pgl(g dry 418
ARL
ARL
ARL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
ARL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
705465
776/
BRL 70
ARL 58
8RL 50
ARL 52
ARL 70
BRL 5f
BRL 47
ARL 66
8RL 44
BRL 74
BRL 72
754866420575
BRL 76
BRL 60
BRL 51
BRL 56
BRL 78
BRL
BRL
8RL
BRL
ARL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
ARL
BRL
ARL
BRL
BRL
BRL
ARL
BRL
ARL
121009350| 13008210134ffi| 1600
5S2097508460442058€0s66039801't 1007400
6070632040205530357071706344
5050505050505050505050
505050
5050505050
Preparsd: 22-l\raF07 Anal\rzed: 23-Mar{7
4.Chloro.3fi €thytphenol
2.ChloroDhenol
1 ,zt{ichlorcbenzene
2,+Ohitttotuen€
4+,libophenol
N+{ilro€odi-n-pop!4amine
PenlachlorcphonEl
Phsnol
1,2,+Trichlorobefl zene
S utogat$ : 2 -F luotob i p h e n ylSunogate : 2. F hloroph en o ISunogate : Nitoben zohe4sSumwal€j Phq,1ol45Su''oga|€: feryheny|4l4Sunwate : 2, 4,Eh bmn'f ph € n ol
173401730017300173001730017300
4440
16900
r6900
8440
8,{40
16900
84!.0
16900
16900
8440
8440
84408441)844n844n84400440
4444
16900
16900
8,t40
u&
wt 3t)15-t103{)-t m15-110n,lm15-110
40-14030-13030-13040-14040-1do30-13040-14030-13030-13040-14040-14434-13015-11030-13015-1103Gt3n15-t 10
40-1403G1303013040-r404Gt40
8 3 03 3 02 3 07 3 011 30
I.rnr So{k Duo 4703127t{SD1l Sou.ce: SA5!X97{5Pr€per€d: 22{tar-07 Analyzed: 23-Mar,07
4€hh{o-3fi6t'rybh€rlol
2€hlorophenol
| ,+Dichlorobonzeie
2,+Oinit otolu€n€
638010?00866047506550
Thit lQbofalary ,epnd is aat vald w hout sa zr/thorirrd siflt zaarc on the Eolvr prye.
' Reportable Detection Limi( BRL = Below Repodng Limi( PaCe 109 of 1 24
Page 581
Semivolatlle Org ic Compounds by GCMS - Quality Control
Analtie(s) Flag Unils Result %REC Limils
Bdch 7031279 - SW846 35508
ilaLh 6oika Duo 12011279-LsDll gonrEc: SA3g4g?i5
PrepEtEd: 22-[16r{7 Analyz€d: z3-ldar{7
+Nilrophenol
N-Nilfosodl-n+ropylamine
Pentact oroph€rrcl
'1,2.+Trichlorotr€nzerE
S urogate : 2 + I tptob ipl?p.n ylS mogate : 2 + I uotopherr0lS unqEE : N itroben zene4 5Suft.gata: Phetul4'Surogate: Teryheny'4l4Sunlgate : 2,a,ehb@nophqnol
Batch ?0313?l - Sw846 35508
B|ank lm3l37l€tfil1
ft€paBd: 23-Mar-07 Analyzed: 24.Mat4l
Acenaphtren€
Aniline
Azob€nzendDiphenyldiazine
Benidlneg€nzo (a) anthrscen€
Benzo (E) pyren€
Benzo (b) fluoradtr€ne
BetEo G,h,il p€rylene
Benzo (k) nuoranthene
Benzic scid
B€nzyl alcohol
Bb(2-chlo.o€ft ory)methan€
Bis(2dtloroelhyl)elher
Bis(2-dtlorcisoprcpyFttEr
Bb(2+ltrylh€xyl)phthalate
4€ro.ioph€nt phenyl ether
BUV bonz/ pffi€lale
Carbaole
44hlolo-3-m€f rylphenol
44hb.oaniline
2{hbronaphthalene
2chlorophenol
44hlorophenyl pfEnyl ethsr
Ghrys€rE
Diber8o (a,h) antrlracoae
Dlbenzoturan
| ,2-Di' orohenzer|e
1,}Di{florc$onzerE
1,4-Old{orcb€nz€ne
3,3'{)icfibrobonzldin€
2,4oidllorcph€nol
Diethyt pftrh€hb
Dimethyl phflalato
2,4{)im€thl$henol
t0c001?2011000785063906220s9m644t)89405680t09009640
1670
4 1 8
4r8418d le418
169008440r6900163008,1408.t{08441)84108440S|UO844084'lI)
SRL
ARL
BRL
BRL
BRL
BRL
Fdkg dty
Pdks d'Y
udkgdrypdks dry
ugks dry
PdkS dry
PS^g d.Ypgrs dryldks dryldkg drypdks dry
clMT pg/kg dry
6a 30.13050 ,10140
65 30-r 3046 30-13076 40-14074 +1&118 3t>tg76 t5-110106 3GrW87 lSl l '129 3G1mfi4 15-110
8
6 3030303t)30
BRL
ARL
ARL
BRI.
BRLgRL
BRL
8RL
BRI-
ARL
BRI
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
aRrBRL
BRL
BRL
BRT
lgrkg wet 330
lg/ksrvet 3:10pgtg wel 330
lgtgw€l 330lgr'kg rrcl 30
FdkS vret 3]0
t€/kg wet 330ygtgw€I 330
fgtgwel 330
Idtg r^,€l 330Uglkgw€l 330pS&S rvet 3i,0pg/kg wet 330
Ug/kg wet 330
ldkgwet 330IgI(g wel 330
!s/ks t/et 30
I|SIIS wet 330tidkg wet 330
Pgr'f,g 1 '€l 330
lgkS tv€l 330lg/kqw€l 330pgdkg vret 33otig/kg wet 33Opgr'&wet :F0
lrgy'kg wer 330pdkg w€l 330
ugr'kg sl 330pg €wet 3i10Ig/kg wet 33Opdrqwet 330
ldkgw€t 330gg/kg i,r€t :Il0
rcr'kg w€l 3|0pdkSwet 3il0
Ugftgwet 33Opdksw€t 3:10
Thb bb.ototr r€pod B not v4litt *irtou da outhoizetr 6ig'Eta,e on the @wf pag...
* Reportable DeteatioD Lirnit BRI = Eetoq/ Reporting Lirnit Pag€ I l0 of 124
Page 582
Semlvolatile Organic Compoutrds by GCMS - euality Control
Spike Source %RFC R-PDAnafyle{t Resutr FtaB Unirr .RDL Level Resutr %REC Ljmjrs RpD Linit
&tch ?031371 - SWE46 3s508
Blank 170313?l€l_Kt)
Pfepa€d: 23-llrar.O7 Analyzed: 24-Ma. 47Di-rFbulyl phlhatate
4,6-Dindl$2-m€thylphenol
2,4-Dinibophenol
2,+Diniuololuene
2,&Ohilrobluene
Di-o-octyl phlhalate
Fluoranlh€n€
Hexachloaob€nzene
fl€xEchkrabutEdbne
tiex€chlorocyclof entadienetlexachlom€thane
Ind€no (t,2,3d) pyrene
t -{\rethylnadrthalene
lsoPhorcne
z+.|€thynsphthalene
2+r€thybheml
3,4-MothMphenol
Napfttnal€ne
2+.{ilr('aniline
3i,iltroonilineit-l,{itroer lihe
Nitobe.Eene
2-r.lnroph€nol
4+litophenol
N-Nihcodimethyhlhine
N+lito€odl-nf ropylamine
N{ibo6odiphenylemine
P€ntachlorophenol
Phenol
hddne1,2.+Trichlorob€nzene
2,4,tTricilo{ophend
2,4,6-Trichlof oph€nol
S mogab : 2-H tloto W h e nylS unogste : 2-F f uoro phe n o IS unogate : N it rcbe n ze n e 4 5Swmga./re: meno145Sunnga|€: letphenyl4l4S!4ft gab : 2, 4, &f n kono ph e n o I
LCS a7c'1371 ASt I
ftopaed: 23-ft-{ar{7 Analyzed: 244nd -O l
Ac€nephf|ene
A€€naphhytene
Anftn€
Atrauln€
Azob€nzei€L/Dirhenyldiazine
Bsnzidine
B€nzo (a) €nth.acsne
B€nzo (E) pyrerE
6670 776670 736670 906670 776670 906670 59
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
ARL
8RL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
ARL
BRL
5110485D6010515059703550
4030
5430
5aso548075606300BRL47005170
667066706670667066706670667066706670
30-13015-11030-13015-11030-1301U110
40-1304S.1304o-1304G13040"13040-130G13040-130.r0-130
pg/kg wet 330gSftS Y,,et 330pg/kg lYet 3l]0
tig/kg wet 330
UgL/kg wet 330
Pg/kg wet 3:10
!g/kg wel 330pg/kg wet 330
pg/kg wet 330
lgy'kg wer 330pg/kg wel 330
pgr'kg wet 330pdks wet 330
lgr'kg w€t 330
!g/kg r,/st 330
lgL/kg wet 330
trgL/kg wel 330
Ugr'kg wet 330
pg/kg wet 330
t,gkg wel 330
!g/ko w€l 330
!g/kg wel 1320
IS{9 lvel 330
l4/k9 wel 330
Ugr'kg wst 1320
pgkS vret 330
!94(g Yvet 3:}0
lgkS wet 330
lgr'kg rYet 330pgr'kg wet 330
Lig/kg,./et 33O
ligfl(g wet 330
!g/kg wet 330
!g/kg wet 330
pg € wet 330
lgL/kg wet 330
Ugr'kg wel
Ugr'kg wstUg/ko wel
ligLi K9 welpg/kg wel!g/kg wel
!g/kg wet 330
pg/kg wet 330pgiko w€l 330
!g/kg wel 330
rcy'kg w€l 330
!9y'k9 wel 330
lgikg w€t 330
usrkg lvel 330
pdkS lv€t :x}0
al88821 1 394
707A
This lanotuory rcpod Lj not w!i.L+l!ho,t! ad 4t [rorized sigrratwe on thz covet pltge .
. IGportable Detection Limit BRL: Below ReDortine Limir Page l l I of 124
Page 583
Scmiyolatile Orgrtric Compoutrds by GCMS - Quelity Control
Anabrds) Result FlaeSpike
I,€vel Limitl
RPD
Limit
Soulce
Result %REC
B.lcb 703rJ7l - Sw846 35glB
LCS ft0313?tAStl
Prepared: ?!Mar-O7 Ana!f2€d: 24-Mar-.07
8e.Eo (b) nuoranth€n€
Eenzo (g,h,i) p€rylerE
Berzo (k) fluoranlhen€
BerEoic acid
8€nz]l alcohol
Bis(2-ciloroehoxytnethane
Bis(2.chloro€tr.lyi)ether
Bb(2{hloroisopr@y')€lher
Bis(2-elhy'hexylhht|slate,l-Brornoph€nyl phonyl eth€lBut/ benzyi phfi€taie
Carbazole
4-Chlom-3{efhMphorrclzt4hloroanftE
2Chblonaphhal€ne
24hlorcphenol
4{hlomph€nyl ph€nyl eorer
Ch.ysene
Dib€nzo (a,h) anth€c€ne
Dib€nzofuran'l ,2-Dbhbrcbenz€n€'l,3oichloroberP€ne
1 ,4-Di*lorohenz€ne3.3'Oicfi lorobenzitin€
2,4oidrlonrph€nol
DiethM phtnahle
Din|€lhyl pht|€ble
2,4oimethylfhenol
Oi-n+uy pht|alsle
4,6-Dinilro-2-methylpfi enol
2,+DiniEoph6nol
2,.1-Dinhrololuene
2,6ohh'rololuen€
Dl+odyl phthda|e
Fluo.anttlea|e
H€xachlorob€nzafl€
Hei€ctrlorobutadi€ate
Hexaclrbmqrcbp€nhdbn€
H€xachloroelhan€
lndeno (1 .2.3-cd) pyrene
lsophorcne
t -M€lhylnehtfisbne
2+.let ylnaphthalene
z-il€trylphenol
3,4-M€tt],lph€nol
NaFrr0ralone
Z+{lhooiline
3-Nilroonlline
4-Nitroanilin€
Nitrob€nz€ne
2-f.libopherlol
42S405063304620487053905sgt)4350sno41XO56007no505043404950.{260
5r60{s7047m5130460039604820509044305?,fi49204510533039SO48t052AO55m66704t00smo,t60o
1750420/J469039?05490a85052304390412052005r8047907*058701720
667066706670
6670667066706€70
66706670
667066706670667066706870G6706670
6670
66706€7046706670667068706670667066706670
6670667066706670667066706670
667066706670667066706670867066706670
ldxSwst 330
ldkg Yret 330pdkg rv€t 330
llg/t(g wet 330yg/kgw€t 330
Igut(gwel 330pg'kg wel 3[|0
Lrdkg vr6l 330
!g/kg wet 3i]0
lrgl€wet 3i]0
lrg/kowet 330pgitgwel 330
lgkg wel 330
rdkgYr€l 330
ldl€ v.el :|l}0pgr'tg $,€t 330
lgftgwet 3:t0
Ug/kgwel 330pdlS w€t 330gglkgw€t 330
ldkg$ct 330
rdkg vret 3:)o
rcrlq wet 330
Ig/kgwel 3:]0pc,19 r.€l 330
ldkgl€t 330tigftgYret 33OpdkS Yret 3lOygr'kg wet 33Opgikg w€t 330
Pglkgwet 330
tidkg wel 330
ldkg Yt€l :t:}0
Ig,kgw€t 33OpdkSwet 33opg^g w€t 330
ugitgwel 330
Pgrkg wel 330
ldkgYr€t 380
USI(S Yi€t 330pdkSwst 300
llg^g wet 3:10
Udkg we{ 330pgrts vr€l 330
trdkg Y{€t 330gdkS Y/et 330
IdkS lvet 330
Irgrkg u,et AIOpg/kgv/el 33O
lqr'kg wet 1320pg/kg w€t 330
flgrlqwel 330
64 4&1m61 4G13)95 40ng)69 G13073 40-1308t 40-13084 a&13065 4Gr 30E7 4{tt3071 40-13084 40-13{)108 40-13076 {013065 ,10-130
74 40-13]64 40-13077 40-1m75 40-13071 4G13077 4,0-13069 40-13053 40-13072 fi-I3om 4G1306S 4&13078 4$.13074 40-1U)68 4(l13o80 40-13060 40-13072 40-13079 40-'t3083 40-130100 40-13070 40-.13078 4G13069 40-13071 4Gr3064 44-13/]70 40n3060 40-13082 ()n 3073 4+1,1078 40-13t)66 4t113006 4{t13078 40-13078 4&13072 10.130'fl4 40-13()8a ,$-13t)
71 {0-130
This ,abo.dor| report b trot rditt vfuhoot qn oailoized tE aurc on the caver page.'Reportable Detection Limit BRL = Below Repoding Limir Page ll2of 124
Page 584
Semivot{tile Organic CorDpourds by GCMS - euality Control
Ansltle(s) Result Flag UnitsSource %RECResult %REC Ltrnirs'RI)L
Spike
I-evelRPDLimitRPT)
Brlct 703ll7r - SW846 3ss0B
LCS {703137t€aPrepared: 23-lrar{7 Anatyzed. 24-Mat.!J74j.litrophenol
N.Nitosodimethytamrne
N+litosodi-n-propytamine
N.Nfrrosodiph€nytamine
P6nbd orophenol
Ph€nantir€n€
Ph€nol
Pyri(fins'l r,&T.ichtorobenzene2.4,$Tnchbmphenol
ZJ,GTn-d orophenol
S u iq ale : 2 - F I uo m hi p he n y !S unog ate : 2 - F I uamFke no IS mogate : N i | rcb e n zen e4 sSutogate: Phend4|Surrcgete: Teryt6nyl-d4S udogate : 2, 4, ETd bro n o p h en ot
Dupllcab 17031371 JUpl)
3320
4470
56t]0
6(H0
4130
4&t0
4850
4940
3660
4930
4640
3520
51m44106200418051504450
Sourc€: 3A59455-08
ARL
ARL
BRL
BRL
ARL
BRL
BRL
ARLgRL
BRL
ARL
ARL
BRL
ARL
BRL
ARL
ARLgRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
ARL
BRL
8RL
BRL
aRt
Lig/kg wet 1320
!g/kg wet 330
t g/kgwel 330
ug/kg wet 330pgr'kg wst 330
!94(S $/et 33O
!g/kg wct 330
pgr'kg wel 330
tlg/kg wel 330
lig/kg wel 330pgkg wel 330pS/kg wet 330
Ug/kg wet
lgKg wet!g/kg welpg/(g wet
!g/*g wel
ug/kg wel
!g/kg dry 749
ldkS dry 749pdkS dry 749
rc/kg dry 749
liglkS dry 749pdkS dry 749pdkS dry 749
USlkSdry 749
ldkS dry 749
pSftSdry 719
t g/kg dry 749
rrg/*S dry 749
Ug/kS dry 749pCn(g dry 745pdks dry 749
udksdty 749
uqtls dry 71spdl(g dry 749
ugkg dry 749pS/kg dry 749
Fg/kg dry 749
rdkS dry 749
udkS dry 74s
pgl(gdry 749pdkS dry 749
lgrSdry 749
UdkS dry 749
uslls dry 749
uS/kg dry 749
pdrs dry 749pgks dry 749
FglkS dry 749
rdks dry 749
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670667066/O667066706670
507388916270
7455147053/7609363//67
4G13040-13040-13040-13040.13040-1304G13040-13040-13040-13040,13040-130il-l3n15-11030-130t 11 t030-13011110
P reparedi ?3-Mst47 AnalFed: 24 -Mar47
Acenaphlhyten€
Aniline
Azobefi zen€/Diphenytdiazine
8€nzidin€
BerEo (e) anftraceneg€nzo (a) pyEn€
B€nzo (b) fluoEnhene
Senzo (g,h,l) peryone
Senzo ft) nutrandlene
B€nzoic aod
BerEyl atcotlol
Bls(2+hlo(o€thory)methane
Sis(2-chb'roethyl)elher
Bis{2d$foisopropyl)ether
Bls(2+thylh€xytFhthatale
4-Brdnophenyt piEny 6fl€rButyl beizyt phthatate
Cefiazol€.rchbrc$mehylphsnol
4.Chloro€nitine
2-Chloronaphdl'lgn€
2-Chlorophenol
4-Chlotropheny' phenyt eherClry€ene
Dibenzo (a,h) anthracene
DlberEofuren
1,2{H orob€nzene
1 ,3obilorobenz€ne
1.41)\.hbrc*nzene
3,3 Olcibob€nzidine
BRL
BRL
ARL
ARL
BRL
BRL
BRL
ARL
BRL
ARL
BRL
BRL
BRL
8Rr-
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
505050505050505050505050505050505050505050505050505050505050505050
Tht laborulory rcpo is fiol r'slid withoz! an dud.orizzl sigutare oa lhe covet pogc_
t R€porr[ble Detection Limit BRL = Below Reoortine Limir Page l l :1 of 124
Page 585
Semivolatilc Org|nic Compou||ds by GCMS - Quality Control
Analytds) Result Flag Units
B.ach 70117 1 - SW846 35508
Duollc.te003l37lDUPl) Sourcs:sas9456ollPreparcd: 2'M€r-O7 Anatyzed: 24-ltat47
2,4.Okl{oroph€ml
Dielhyl phlhab!6
Dimelhy' phftlalab
2,,|-Difiethylphenol
Dh+l tyt phthatate
4.6-Dinitro-2-m€thylphenol
2,4-Dinilrophenol
2,+Dinftforoluen€
2,ooinibotoluen€
Di-n-ocv phthabb
Fluoranlftone
F&roren€
Sourc€: SAll0455-08
LrdkS dry 749
ldkg dry 749
rgkS d.y 749
trdks dry 749
Itglkodry 749
Idks dry 749pdksdry 749
ldXS dry 749
UdkS dry 749lgkSdry 749
t g/kg dry 749
ItgJkgdrf 749pc/ks dry 749
tidl(g dry 719
ldkg dry 749
lgkS dry 74s
w/l€ dry 749
ldkS dry 749pCASdry 749
PdkS dry 749!g/kS dry 749lgftS dry 749pdkg dry 119FgJtSdry 719pdksd.y 749pgksdry 3000!g/kS dry 749
!S/kS dry 749lSAg dry 30d0pgt€ dry 749
Pgrkg dry 719pgrs dry 7,tgldksdry 74s
ldkg dry 749Ug/kS dry 749pgil€dry 719!s/ks dry 749Ugkg dry 749
lgkgdry 149pdkS dry 749
lgks drypdko dry|tgikg dryllgftS d.ypgl(g dryPg/kg dry
ygikS d.y 371
PS4(0 d.y 371
Pdkg dry 371lgftgdry 371fldkSdry 371
BRLBRfBRLBRLBRLSRLARLBRL8RLBRI.8RLBRLBRLBRLaRl8RLBRLBRLBRLBRI-aR!_ARL8Rr_ARLBRLBRLBRLBRIBRLBRLBRLBRLBRLBRLBRL8RLBRLBRLBRLARLilst)515061do538t)5930{030
BRL
BRL
BRL
BRL
BRL
BRI.
BRL
ARL
ARL
sRr_BRL
BRL
BRI-
BRL
8RL
ARL
BRL
BRI
8RL
BRL
BRL
BRL
BRL
BRL
BRT
ARL
BRL
ARL
BRL
BRL
BRI
BRL
BRL
BRL
SRL
8RL
8RL
BRL
BRL
BRL
5050e)5050
5050505u
5050505050
50505050
505050
505050
50
505050505050
Hsxdiorobenzeno
Hex€chiorobutadi€ne
Hexachlorocydopentadlene
Hexachloaoothane
Indono (1,2,3d) pyr€ne
lsodioro(t€
I -{tlsthylnaphtialerE
2-frethyhaphthat€ne
2-lret'l]/l,rhenol
3,4-M€fiylphenol
Naphthalene
2-l'lifoadllne
SNitro8nilifl€,LNibosnilne
NitsDbenzens
2+.lltorftenollslittEphsnd
N-Nlhcdimethy'am'tlle
N-Nilroeodl-ntropylamin€
N{{itrosodFhenylamine
Penh<fllo.ophenol
Ph€nanttu€ne
Phenol
q/ddine'l,2,+Tr*,|bobenzene
z,4,tTrid o.opfienol
z,4,GTdd o{opfEnol
s/rnrjga/F : 2 -FluotobiplnnytSullDgatiei z-Flsoroph€notSu''oga/€: NiffinzeneasSufiWal': Phenol4,SunwaiF: ferytun'N4S udog ab : 2, 4, 6-T i b 'I]n1lgf,hetd
X|trlx Sllke fIO3l3?l{Sl}
75707570f57075m75707570
Prepared: 23-Mar-07 Analyzdt 2+Mat47
Acenaphh€n€,f -Chloro-Sfi ethytph€rEl
24hlorophonol
l,4obhlorob€nz€n€
t/4-Dlnitrotolu€ne
519010200921047305m0
7fiOt5()m1500075007500
ARLBRLSRLBRLBRL
$-tntul to3o-1frtF110gtl3t)1U'10
40-144
30-130
3)-130
4&l/O
4G140
67
8l7l7a
696€61
60
fhjs laborslory ryod lt natrdid tttlho,/ or onhoizrd stgitbue oa tt cowr psge.
+ Reporta6le DriectioE Limit BRL = B€low Rcporting Limit Pagc I 14 of 124
Page 586
Semivolatile Organic Compounds by GCMS - euslity Controt
Analyre(s) Resrlt Flrg Units .RDLSpike
Level
Sourc€Resull %RIC
%RECLimits
RPDLimitRPD
Brtch 703l]?l - swE4615508
flrtix Solk r03l37t-Hslt Sou.cei SA59{:ig)8Prepared: 23-t'ar{)7 Ananlzed: 24-Mar4744,lbophenol
N-Nihosodi-n-propylamine
Pentad orophenol
Ph6nol
12,+Trichlorobenzene
S wogato : 2 - H @tob i phe n ytS unogdle : 2 -F I uorop h en otSurrogate : Nltoben ze ne45Sanrogaie; Plr6oor{5S!/'mga|f: Teehenyt4t4S ffi og ele: 2, 4,ETtibmm o p h e n o I
6't40557073209430587044205150423060204190622043ln
lr.Hr Soik Ouo O03l37l -tilsol) Source: SA594SS{8Pr6paGd: 23{rar{)7 Anatyzed. 2+Mat47
560010600947049505620649059108380991062804630554043906180435064904680
Ug/kS dry 1440ugkS dry 371lrSlkg dry 371tidks dry 37'l
YkS dry 371
uvks dry 371PS/kg dryt!9'l(9 drylqkS drytrgks drylgks dryPg/kg dry
|lgkg dry 368l{/kg dry 368lig/kg dry 368pg/kq dry 368Yg/kS dry 368
Ig/Kg dry 1470
l4/k9 dry 368Ugkg dry 368
PgftS dry 368pSI(g dry 368!g(g dry 368
!s/ks drylgks drygg/(s dryFq/kg drypg/kS dryLig,/kg dry
15000
7500
15000
15000
7500
7500
750075/n7500750/)7500f500
7440
14S00
14900
7444
7440
14900
7440
14900
14900
7440
7410
744074407440744074407440
30"130
40-140
3G130
30-r 3t)
40-140
40-140
30'13015.110&-13015-1103G13015-110
40-140
30-130
30r 30
40-140
40-140
30-130
40-140
30-130
30-1m
40,140
40-140
30-1301111030-13015-t 1030-13015-t 10
8RL 41
BRL 74
ARL 49
BRL 63
BRL 7A
ARL 59
695684568358
BRL 75
BRL 71
BRL 64
ARL 67
BRL 76
ARL 44
BRL 79
BRL 56
BRL 67
ARL 84
8RL 62
7459835887
,l-Chblo-3-mothy'ph€nol
24hb@'€r'ol
1 ,,loichbroberEene
2,+Oinibotoluen€il+.likoplEnd
N+lnmsodlrFpropytEmin€
Pentachloroph€nol
Phenol
1,2,+T.lcft lorob€nzen€
S ufi oge,€ : 2+ | t!o@ b i phe n ylS urryele : 2-F I uoto phen olSunogata: lhltult zE ne45SiJ/tuga/€: PhetE4sSu''ogata: faeheafr4t4&lrrngate : 2, 4, GTthro nop h e no I
8
5
6't0
7
7
6
7
5
3030303030303030303030
This hbo&lory reporl l, nal vald withod an Mthoiud sigtaturc oE the coler pqge .
+ Reportabie Detecrion Limit BRL = Below Reponing Limit P&ge 115 of 124
Page 587
Total Mctds by EPA 6000i7000 Series Methodr - Qrslity Cotrtrol
Analyte(s) Result Flag
Spike Source o/oRfc
'RDL lrvel Rcsuh %REC LimitsUnits RPDRPDLirtrit
Brtch 70!1322 - f,PAr0o/SlV?0m Scrter
ghnk lm3l322€LKl)
Pr€pat€d: 26-Ma.47 Analyzedi 27 -Mar 47ilerc!ry BRL
Dupltcrt 1703132-DUPil sourei SA595l7al
fiigLl(g wet
0.232 ORs |r€ukg dry
rngtl(g dry
otgn(g dry
0.0298
0.0341
0.0333
0.0327
0.0329
0.0300
0.4fr)
0.451
20
Uarnr Soll€ t70('l 122{51 | Sourc!: SA5Sgl7.O2
Preparcd: zaMarfi Analyzer!: 27 -Mar47
Preparsd: 26-[rar47 Ananlzed: 27 -ttd47
Mercury 0.69?
Pr€psfed: 26{,f aro7 Analll?!,di 27 1,tlat47
Mo.cury 0.630
0.340 38
0.222 r03 75n25
0.182 9{t 7St25
o22 66 85,115
Larrir solk. o0313u- s2l Sou|Ee: SAlg517.t2
PoEr solk. 170313iI2+A1) So0tc€: SA595l7{2
Prepat€d: 26.ldar47 Analyzed: 27 -Ma47
RefoEnc. .7031 SZlSRlii l)
Prepar€d: 26{\rari7 Amlyzed: 27 -l.t!€to7
Brtch 7031413 - Swt46 3005A
Ahnk a703l{l3aLKtl
Prepar€d & Anal)rz€d: 26-l\rar{7
Selenium
Lead
Silver
Chrornium
Barium
Cadmium
LCS fr03t,l13€St)
Pr€pared E Anal}rzed: 2&Mar.07
0.522 ocl mS/kg dry
0.53,1 @3 mgng *"t
0.456
1 .12 4A 65.$132.6
Sel€rfum
Chrcmluln
Cadmtum
Btr|um
Sik€r
LCS oup fto:tl{13€SD{l
Prepared & Analfz€d: 26{tar-07
Selenium
Cadmium
Badum
Chromium
Silve.
Duolicaae flftll:|l3{UPl !
Proparcd A AnalFed: 2SMar47
Seleriun
0.466o.62o.4740.4860.4810.'157o.471
Sourcr: SA!iOt2.{X
BFfBRLBRLBRLBRLBFILBRL
0.4500_4530_4460.4620.4700.1480.457
lrrg,l
msrrfro/l
n'Ell
mS/l
ntgil
rrls4
mgnnsnmdl
rE/l
rE/l
ms/r'sfl
rEnrngrrf€/l
nsnngrmdl
mdl
n'SI
0.0t50o.00750.00s00.00s00.00500.0040o0025
0.00750.0t500.00500,00250.00500 0040o.0050
0-o1500.00750.00250.00400,00500.00500-m60
0.0t50
0.500o_5{x)0.5@0-5(X)0.5000.500o-500
0.5fi)0.500o_5000.5000-sfi)0.5000.500
85,115a$11585-r'! 585-11585-1't5a$1158S115
8$1r58S.1158S1158S1168$11585-t ' t585-115
90
9'l
89
s2949091
s3I
sg
9194
3
4
mm20mNm20
BRL ARL 20
ThiJ bbrqtorf rcpor, ie ,tol edlil i'irtou aa &dtoriz.d igruurc oa the cav.r pcge.
+ Reportable Det€ction Limit BRL = Belorv Reporting Lilrir Pae€ l l6 of l24
Page 588
Total Metals by EPA 6000/7000 Series Mcthods - euality Cortrol
Source
B{r.h 7031413 - SwE46 3005A
Duplicab l?031413-truP1)Pr€Dared I Anelyred: 26,t\4ar-07LeadCadmiulh
BatiumSilv€rChromium
ilruix Solk€ a703t.t13- Sl|Pre{ared & Ar|al}.red: 26-Mar.07S€l€niumLeadChromiumC€dmiumSiker
Aarium
Sourco: SASS372{4
0.01340,00060-03900 04070.00328RL
SourE€: 5A59380-01
o.473o.466o.4730.4900.4610.4700,479
Source: SA59380-01
0.469
0.464
0.1a6
0.470
0.466
0.478
0.462
fig/l
fig/l
rngnthg/l
ms4mg
mgnmg/lfignmSL/lfIE,
mgL4
mg/l
mgn
mg,l
mg4
mg/l
fitg/l
msnmgr'l
mgnmgnmg/lmg/lmg4lrE/lang/r
0.0139
0.0006
0.0384
0.0408
0.0030
BRL
ARL
0-0ma
ARL
BRL
0 002s
ARL
BRL
BRL
o.o038
0 0025
BRL
BRL
BRL
BRL
0 0038
BRL
BRL
0 0025
BRL
BRL
BRL
75-125
f5-125
75-125
75-125
75-125
75-125
71125
75-125
75-125
75-125
75-125
75-125
75-125
7U125
80-120
80-120
80-120
80-120
u-f2t80-1208&1m
0 00750.00250.00400.00500.00500 0050
0 0150 0.5000.0075 0.$00.0050 0.5000_0025 0 5000_0050 0.5000 0040 0.5000.0050 0.500
0.0150 0.500o.o075 0 5000.0050 0.5000.0050 0.5000.0050 0.5000.0040 0.5000.00?5 0.500
0 0075 0.5000.0150 0.5000.0050 0_5000.0050 0 5000.00+0 0.5000.0025 0.500o.0o5o 0.5oo
00_50.26
202020202020
0.4s70.4990.4920.5140.5040.4970.514
I.ltdr Soi(c OLp fi031413-MSO1t Source: SAE93BO{1PrepeGd & Arulyzed: 26-MaF07
S€lenium
Lea{,
Sivsr
Barium
Chromiqm
Cadmium
P6l Son(e flUr 4t 3+S1l
PrE!€r€d & Analy4d: 26-Mar.Oz
L€ad
S€lenirm
B€rium
Siver
Cedmium
c'rrornilD
999998J0310099103
95
92
94
98
9?
94
96
5
7
6
5
7
6
7
20202020202020
93s397
94
93
96
This labontor! rcporl is nottalid x,irhou ot zuthoried sigaat nc on.he cove pa*e.
+ Reportable D€t€ction Limil BRL = Betow REDortine Limit Page I l7 of 124
Page 589
Total Metals by EPA 200 Series Methods - Qurlity Cortrol
Analyte(s) Result IRDLSpikeI,€Yel
RPDLimirFlaB UniLs
Source %REC
R€sult %REC Limits RPD
Brlch 703 l32l - EPA 200 Scries
Bl.nk n031321€LKll
P@Pared & Analfred: 26-Mar-07
Sih,er
Seleniirm
Leeo
Cadfiium
Chmmium
Banum
Duolhar6 (703132l{)UPll
Preparod & Analtrred: m-irar-o7
Silver
S€ienium
Chromium
L€ad
Cadmium
B€rium
Iarnx Solke flO3l32l{Sl}
BRLsRrBRLBRLARLgRL
8Rr-
Source: SAsgslrul
m€*g w€tmg^g wetnEag w€lttg/kg welfEr'kg wetnEr'tg w€tnEI(g n€t
0.9051.36't.36
0.6790.2260.4530.453
1.091.630.5440.816o.272|.6ij
o.g4
1.08
r.610.5360.2m0-0061-61
0.538
aRrBRL
1 1 ?
0.3s4
8RL
BRL
44.5
0.490
26S
3.97
u.5
BRIBRL
0.56910.78-6,118354.7
ARLBRT.3-970.490
71 10.54aI
BRL nEAg drySRL |rElkg dry76.8 rE kg dryt3o ms/rs dry
0.3!,2 n€/kS dry6.13 OR1 n€ftg dry40-8 rE/r.g dry
Sosrc€: SA595l7{2
133 nE/kg dryr29 mg/ks dry164 msttrs dry124 nrS^g dryllb oM7 r|g,tg dry121 mg <g dryl8O ng/kg dry
35
Prepared: 26-l{ar-.07 Analyzed: 27 -t ''ts,.{7
Silver
S€lsnium
Chrcmiun
Cadr{um
Le30
Badum
P€pared: 26-l\rar{7 Analyzed: 27 -Mar47
S€l€nluln
S&€r
Cadmium
Ctt.omium
Lead
Beritnn
Pr€par€dr 26{vlar{7 Analtzdi 27 -Mat47
Silv€r
S€l6nium
Cadmium
R€feronc. l?031321€Rt l)
Pr€peedi 26-lr€r.07 Analr/rd: 27 -Met47
Selenlum
Silv€r
Chromium
L€ad
Cdmium
Barium
1341 U1341 yt3.lt34134
r2712f127127
r3513513t;135
78.21124.4,19-4
44.93'1.8214
70-1307Gr3070n3070-13{)7G1307G13)7G13{)
s9s68Sc25092101
matrlr Spike 17031 Il.t{521 SourE : 5A!9517-12
Pod Solks a70cl321+Sl I Sourcai S^st5lru:l
't t9't26
1 1 0r23't1s
335177
125129127119
03.1{4.5a5.051,54r.930-5219
mg/kg dry 1.52nErtS d.y l.O2mg/rg dry O2gmgyl€ dry 1.52rnSttg dry 0.508nEl(gdry 0.762.nSn€ dry 0.508
rElkg dry t-08mgrkgdry 152nrgr'kg dry 1.62rELI(9 dry o.mg
rE^gwel 1.50filglkgwol 1.0OrEukgw€l l-50ng (gw€l 0.500hgikg Y/et 0.750mgrkgwet 0.250.ngrtg vr€{ 0.500
94 7Gt3t)9S 70-13086 70-13088 70-13087 7G.1301m 7tri3006 70n30
tx' 8$t1596 8t11591 8tr1586 8$.115
1M 77,+1n,6108 68.+133.6rm 80.&119_4104 78.&rfts93 81-E-118-1s 92.1- 7.9101 82.7.117.3
Thls labtubry Eport ls Eot vatid d tou sD srrttodz.d d81,',aht oE fhc cow, Fqe .
+ Reportrble Detec-rioo Ljmit BRL = Below Re(ting Linir Page I l8 of 124
Page 590
Total M€tals by EPA 200 S€ries Methods - euality Control
Spike Sourcel*vel Result
RPD%RE{: RPD Limrt
Brtcb ?031414 - f,PA2al0/SW7000 Series
Blank {7031414€LKll
PrEpar€d: 26-[f a.{7 Anati 'd: 27 -Mat.4l
mg,4
LCS fr031414€StlPrepared: m-Mar{7 Anatyzed 2f -Ma(07
M€rdrry O.OO247 85-t 15
ouplicrto at03tat40uPt) Sou.ce: SA59517.13
Prepar6d: 26-fvf ar{7 Anatyzed: 27 -Mar47
M€rcury 0.00026
IatsixSplX.{703141+MS1) Sou.c.:SA59517-1.1Pr€pared: m{rar47 Anatyzed 2j -Ma.-o7
luercury O.0O2b3
,ralrix So*<. Duo (7031a14{SD1t Source: sA595t7-14Prepared: 26-{,f ar-07 Anatwe d : 27 -Met 47
Me.orry 0.00240
mg/l
mgn
' 101m9/l
lrE/l
75-125
75-125
Thls lahrutary repod k not wllil fithou c ouhonzci signaurc on the covet pzge.
' Repo(able D€tection Limit BRL = B€low R€Dorting Lirnir Pase I 19 of 124
Page 591
SPLP Met|ls by EPA 13fZ & 6000/7000 Series Mctbods - Quality Control
Analyre(s) R€sultSpik€
Level
RPDLimitFlag +RDLUnils
Source %RECResult %REC Limits RPD
Brich 703r40E - sw846 3010A
Bhnt r7031408€txl)
Prepared: 2}Mar47 AnElyz9.d. 24 +J,at47
S€lenium
L€ad
C€dmium
silve.
Chlomiufil
Eanum
LCS f7ml400€s1l
Prep€red: 23+{ar47 Anelyzad: .Mat47
Lead
S€lenium
Silvea
Cadmium
Chromium
Batium
LCS Duo f031408-g$)t)
Prepared: 23-lt-l€r{7 Andyzed: 24.1ht47
So0rc.: SA595l7-12
mstltrEnftrgl.r€Imdlmsrlmgr'l
mgnmsn
qca r€iltrB,l.rg,AmdlNET
l|lgI
@lnqlntsltndl
OC3 mg/lmgn
mdlmglmdlmdlmgxmsnmgr
rEImgr'lmgnmgn
OR7 triSl
BRL
BRL
BRL
SRL
BRL
BRL
BRL
L l 8
t . 1 3
0.651
1_23
1 . 1 4
1 . 1 8
1.24
't.05
1.09
1.09
1,05
1 . 1 4
0-590
0.0150o.00750.m250.01000.00500.01500.0050
0.007s0.0't500.0to00,00250.01500_00500.0050
0.0r500.00750.00500.0150o.0025o.01000.0050
0.00750_01500.01500.01000.00250.00500.0050
0-0150o-00750.01500.00500.01000.00250.0050
o.00750.01s00.00250.m500.o100
1.251251.251.251.251.25125
1.251.251_251.251251 .25r.25
88.+10879108
55.+11587.+110f7.[-1097A_2-l1A85.1-' l l9
79-10882.3-t087A2-l1A771-10987T11055.S11585.1-' l lg
Selenium
Lead
Chrdnium
cedmium
Silvergadun
ouptkats n0314@{uPtl
94
s0
0891949S
s0s4s0ln54s698
9l
90q'
9'r
202020n20
n
ua7a784914Ts2
m2020
20
7
8
I
E
1 0
Xatru Solke o031{O8-lts l I SosiEs: 5A59517.{1
Pr€pared: 2+itar47 Anatyr€d. 24-MaF07Lead
Selenium
SilY€r
Cadmium
Chaomium
Earium
Pr€pdred: 23+/ar-07 Anahlzdt 244n€'47SebniumL6ad
Chromium
S{ver
Caddium
Bariu|n
L6ed
S€ledum
Cadn*lm
Chmmium
Silver
0.0280gRL
BRL0.0926BRLsRr
0_0132
r.221 . 1 4
1.24
1_18
1 . 1 4
125t151.251.25r251.251.25
1251.25t.251.251.25
0.0261BRLSRLARL8RLBRL
0.0120
BRI-00319BRL
0.0130BRLBRI
0.0rs8
0.031sBRLBRL
0.0130sRr-
80.4-10581.&10579,2n0681.5-l1163.Fr09864-10a86-9-114
8t.&10580.+10586.4-t0881.5-t | 1€i].&lm
20mmm2020
1,13 mSn1.21 mdl1.13 mg/l1..t6 msn
0.672 qM8 n€/l122 rEI1.24 mCrl
Llrlx Splke Our AOgl{OE{SDlt SourEe: SA595t741
Prepared: g3-Mar{7 Analyz€d': 24 -Met47
0-80-9
52
Thk lzbordoq rya.t it not wlld utilhottt en attfiorfuat slga4ltan oa thl .nvr l4ge .
r Reportable tt€r€cti,on Limit BRL = B€low RAo.tiEgLiEit Page 120 of 124
Page 592
SPLP Metals by EPA l3l2 & 6000/7000 Series Methods - Quatiry Control
Flag Units
mgnm9n
frE/l
tnsnmgr'lmsnmgnmq,4
Spike Source
Level Resuft
%RECR€sult
1 . 1 5
1 . 2 7
1 . 1 4
1.23
0 958
1 . 1 5
1 . 1 S
1 2 4'1.27
0.01500.0050
0 01500.00750.01000.0150o.00500.00250 0050
1 2 5
1 . 2 5
1_25
1 . 2 5
1 . 2 5' | .25
1 . 2 5
1 . 2 5
1.25
BRL
0.0r98
BRL
0.0319
BRL
BRL
0.0130
BRL
0_0198
79.2-106
88.9.114
11.7-108
80.!108
61.7-107
79.3-107
18.1-114
86.5,109
86.6-116
I-imits
66.6-117
%RF-C
Brtch 7031{08 - SW845 30r0A
t efix Splks Oup P031108+ISO1) Source: SA59517{iPr€€ared: 23 €r-O7 Analyz€i: 24-Mat47
gadum92'r00
2020
Post Solt€ 17031 {tt8+Srl Sourc€: SA59517{l
Prepared: 23{ar-07 Analyzed: 2+Mat47
S€lenium
Lead
Slver
Chmmium
ftdmium
Eadum
Brtch 713 l4{9 - EPA200/SW7000 S€ri€s
Elank 17031409€LKll
P.€pe.ed:23-Md47 AnaIWd: -Ma?07
9 l
96
77
92
94
9!)
100
8RL ms/
mg,4
0.00040
mq,4 0.000!0
ms,4 0.000,10
0-00250
8RL
0_00250 BRL 107
Dupl|car€ fl03laogoUPll So{rce: SA595l7-12
LCs f70: 409€51)
Pr€p*€d: 23-lrar-,07 Analfred: 26-Mar-07
M€rcury 0.00255
fteptr€d: 23-lvlar47 Anavzet 26-Mat 47
Pr8p{ed: 23411 'J-07 Analyzed: 264tar -D7
Memrry 0.0$267
Pepared: 23-Mar{7 Anal]rzed: 2AMar47
M€rorry 0 00250
0 00040
l|ebir Splke flqll40g-Ms'l I Source: SA595t7-01
l|atix Splke DLb ft031rog-irsoll Source: SA59517.01
Prep{ed: 23Jutar47 AnatFed: 2&Mar-07
Merc!ry 0.00249 mgn 0.00040 0.00250 BRL
Po3t Sol*o ?031409.PS1 I Source: SA59517{1
7 6 1 - 1 1 1
7 6 . 1 - 1 1 1
66-8-'lr0ng/l 0.00010 0 00250 BRL
100
100
Ge[eral Chemlstry Parameters - Quality Control
Brtch ?031429 - cenerd PteD.r.tion
Dudicst fl031429-ouPt)Pr€par€d & AnElf2ed: 23-Mar{7
% Sollds
OuEllcat. fro3146{t.DUP1)
Prepared & Analyred: 244rar-07Yo Solidg
Brtch 7031{63 - C'e eral Preprrodotl
Source: 545051741
SourE€: SA5945l{h
87.4
% 87.4
87.8
0 1 20
20
This labontory EForl is dot vdid rvuhoA an aUhori|ed sig tature ott the cowr page _
+ Reportable Detection Limit BRl, = Belon' Reporting Lirhit Page 121 of 124
Page 593
Notes and Definitions
*TPH Calculated as
Comp Completed
Field Preserved
QCI Alalyte out ofaccepmnc€ raoge.
QC2 Analyte out ofacceptance raage in QC spike but no rcportable concentr8tion presedt in sampte_
QCa The spike recoyery is outside ac{eptable limih for the LCS. Th€ bakh was accepted bas€d upoq the MS aod/ot MSDme€ting the LCS limih criteria.
QM7 The spike rccovery was ourside acceptance limits for the MS anvor MSD. The barch was accepted based oo acceptableLCS recovery.
QM8 The spike recovery exceed€d the Qc conhol limits for tte Ms aod/o. MSD. The batch wrs accept€d based upooacaeptable PS and./or LCS r€cov€ry.
QRI A.nalys€s ar€ oot co rolled on RID values ftorn sample conceDtmtions less ihan 10 times the r€porting limil QC batabaccepted based on I,cS and/or LCSD QC results.
QR5 R-PD out ofacceptance mnge.
QR7 The RPD exceeded the QC control limits; however precision is demoostrated wift acceptable RPD values for batchduolicate.
R05 Elevated Reporting Limirs due to the p.ese[ce ofhigh levels ofDon_target analytes.
S02 The surrogate recovery for this sample cannot be accurztely quantified due to intedererce ftom coeluting organiccompounds present in the sample exhact.
SGC Surrogate rccovcry outside of cooEol limits. Th€ data was accepted bas€d on valid recovery of the remahing suFoga@.
vex? Field eKFacted
VOC8 Reponiog limits r€flect SW846 5030 extraction tecbnique due to marrix interferetrce usitrg SW846 5035A extraotiontechdiquc.
BRL Below Reporring Limit - Anab/te NOT DETECTED at or above rhe rsportine limit
dry Sample .esults reported on a dry weight basis
NR Not Reported
RPD RelaJive Percent Difference
A plus sigfl (+) in the Method Refereqce colwnn indicates the mcthod is not accaedit€d bv NELAC.
Thb labontoq tqrort ls ,ol valid without an ea6odz.l signaa c od lt e @wr page.
. R€porrable Dctcdion Limir BRL = Below ReFoning Limir Page t22 of 124
Page 594
InterDretation of Total Petoleum Hvdftlcarbon ReDort
Petroleum identilication is detetmin€d by comparing the CC tLogerprint obtained from the sampL€ \\,ith a library ofGC fingerpnntsobtained from analyses ofvarious petroleum products. possible match catesories are as follows:
Gasolioe - itrcludcs regular, unleaded, prernium, etc,Fuel Oil #2 - includes home heating oil, #2 fuel oil, and dieselFuel Oil Il4 - includes #4 firel oilFuel Oil tt6 - includes 116 fuel oil and bunker ,,C" oilMoto. Oil - includes virgin and wast€ automobile oilLigroin - includes mineral spirits, petroleum taphtha, vm&p naphthaAviation Fuel - includes kerosene. Jet A and Jp-4Other Oi[ - includes lubricatirg ard cutting oil, and silicon oil
At tirnes, the unidentified petroleu.rn product is qua ified using a calibration that most closely app.oximates the disrributiotr ofcotnpounds in th€ sample- Wtren this occurs, the result is qualifisl a.jl *TpH (Calculareo as).
Laboralorv Cootrol SamDle fLCS)i A known matrix spiked with compound(s) representative ofthe target analytes, which is used todocument laboratory performa.nce.
Marrix Duolicate: Ad intralaboratory split sample which is ussl to document the precision ofa method in a given sampl€ matrix.
Matrix Soike: An atiquot ofasample spiked witha known conccntmtion of target analyte(s). The spiking occurs prior to samplepreparation atrd analysis. A matrix spikc is used to document the bias ofa method in a given sample matrix.
Method Blank: AD aDalyte-free matrix to which aLl reagcDts are added in the same volumes or proportions as Lrsed in sampleFocessilg. The method bLank should be carried through the complete sample preparation and analydcal procedure. The methodblaok is used to document contamination resulting from the analytical process.
Melhod Det€ctioo Limit (MDL): The minimum conceDtration of a substatrce that can be measured and reported with 99%coofidence that the analyte concentration is greater than zero and is determined ftom aialysis ofa sample il1 a given matrix tt?ecoEtainiag the arElyte.
ReDortable Detection Limit (RDL): The lowest concentration that can be reliably achieved within specified limits ofptecision andaccuracy durilg routinc labolatory operating conditions. For many analytes the RDL analyte conc4nt.ation is s€lected as the lowes!Doo-zero standard in lhe calibmtion curve- White the RDL is approximately 5 to l0 times the MDL, the RDL for each sample takesitrto accouot the sample volume/weight, extract/digestate volume, cleanup procedures and, ifapplicable, dry weight conection.Sarnple RDLS ate highly matrix-dependent
Sunogatel Ar organic compound which is similar to the target anal,,te(s) in chemical composition and behavior in the analyticalplocess, but which is not nolmalLy fould in environmental s|mplcs. These compounds arc spiked into all blanks, staDdards, andsamples prior to analysis. Percent recoveries are calculated for each surosate.
Validated byiHanibal C. Tayeh, Ph.D.Nicole Brown
Thk labonlory rcINrt is ^ot tlzlid ttithout aa sathotjzed slgraaure onlhe coeer poge.
' Reportable Deteciion Limit BRL = Below Reporting Limit Page 123 of 124
Page 595
State Of ConnecticutDeparunent of Enviro nental Protection
I^aboratory Quality Conhol and Quality Assurance Form
r The @mpounds udor.len€nts e?ortd!rc a eccificrllyiEqGsred by he clidt on rhe cl8in ofc{siodyond iD $nre cd€s tuymr hctude rhe tullatral'tc list 33 &6nsr in rh. m.'hod.
Negolive rc4tomes for 4 B ond C orc sd&essed in a cese norrulive on the cowr pqe of this rcport
I, the dndersignel, aaust andcr rte psias and perralria ofpeiary thal bssed u!,on ny penonat inquiry ofthose rcqonsiblelor oblaiaing the hformalio4 the ,,raleriol coafainod in this analyticd iqort is, b rte besr o! my h,towtedge oatt befieJqccurab Qnd con plctc-
nfr#-Hanibal C- Tayeh, Ph.D.Presideot{-aboEtory Director
D e: Y2A20O1
Labomtory Namc Spechum Analytical, Inc. - Agawam, MA Proiect Name aod Number:
Project Location: NHRY M8 Ac{eptanc€ Facility - New tlaveD, CT NHRY M8 Ac{cptarce Facility - Ne,r Haveo, CT/
Tbis Form Provides ceflifications for the following drta set:sA595L?,01 SAs9Jl7-ll
sA595t7,02 SA595r7-12
sA59517-03 S&.9517-ll
sA59517-04 SA59517,14
sAJ95l7-05 SA595l7-t5
SAJ9J | 7-rX
sA595 t 7-il7
sA595l7{6
sAJ95l7{9
s,\595l?-t0
List Sp€cific Anab'ticzl Medrods Used:
+CT ETPH
EPA 2OO.?
EPA 245.t 174704
SM254O C Mod
sw 846 E!608
s w E 1 6 l l t 2
sw8{6 L3r26010B
SWSil6l!127470A
sw845 60loB
sw846 r47lA
SWE,I6EOEIA
swE46 t0t2
swE45 82608
SW8,l6 8270C
sw845 8270(yEPA 6?5 |
voc
Sample Manices:
SoiUSedidmt
Were all samPles receiv€d by the laboiatory iD a condition consisteotwith thar described on the Chain of Custody documedtation for the dataset?
E! Yes E No
BWerc all Q'QC prccedures required for the sF,€cified anatlticalEethod(s) included in this report followed?
El Yes E No
c Were all QC performance standards ard a€commetrdations for th€specifi ed methods achieved?
E Y e s E N o
DWere iesults for all arulytelist compouddvelemeots for the sp€cifiedmethod(6) reportad? B Y e s E l N o .
This labonlorf wporr is aot voIU vdrtant da aslharized sigrentrc oE th. coret pagc .
' Repo.trble Der€ctiofl Limit BRL = Betow Repo.ting Limir Page 124 of 124
Page 596
E
s
5
45?
e-6 '
H@dquart^.11 Alnyer.Dtive & 830 SitvnSrEr. Acsw, MA 0l0ol . 1,800-7E9,9115 .4lt-7t9-90rE . FAx 4l l -7s9-rto?6ll rivirior: 8l E0 wodland C€nter Boulcvsld . T.mps, FL 136t4. l-888-49?-j270 .8r3-t8t-9507. FA.l( 800-48044jJ
www.6pectrum-€naltrtical.com Pege I of2
Page 600
Saoole IdentificationFB-3sA5964 t- l8
Client Proiect #l0l -88
MatrirBlank Water
Collection Date/Time21-Mar-07 00:00
Received22-Marn'l
CAS No. Analla(s) Flag Unib tRDL Dilution Melhod Ref Prepaed Ana\,aed Eatch AnaDst
Yohlil€ Orgrnic Compould3
Volatile Oroanic Comoounds bv SW846 82608Prepared by method SW846 5030 Water MS7&111'1,1,2-Tricf i lorohifuoroethane(Freo€RL674-1 Ac€tone BRL107-13.r Acr},tonitrite BRL7113-2 Benz€ne ERL10E-86-1 BmmobefEene BRLf+97-5 gronrodlloromethane BRLf5-274 grornodichloromethaDe BRLf+2U2 grcmoform BRL74419 Brornonethme BRL7€-9!3 2-Bulsnone (MEK) BRL10+51{ n-Butylbenzene BRL13f,9€J s€c-Butytbenzehe BRL98.064 t€rt€utytbenzene BRL75-l!0 Carbon disutfide BRL56-23-5 Carbon tehachtoride SRL10&90-7 Chto.ob€flzene BRL754rL3 Clrlo{oethen€ ARL6t€83 Cftoroform 8RL1147.3 Cruoaoflehane 8RLss-4e8 2-Chlomioluene BRL10643-4 +Chlo,rotoluene BRL116-12{ 1,2-Oibroarp3-Chloropropane BRL124-4+1 Dibrornoct{oromethane BRL1fi+93-4 |,2oibrornoethane(EOB) BRL7ir€:.3 Dibrornornethane aRL96{G1 'l,2oichlorobenzene BRL54i'73-1 '1,3-Dicl{orobenzen€ BRLllE-{&7 l,4oichlorobenzene BRL7*714 Oicilorodinuoromethene (Freonl2)BRL75-34-3 'l,I Oichloroeth€ne BRLi0ru6-2 |,2-Dichloroethane BRL/5.35-4 |,l-Oid oroefi€ne 8RL1ss5s'2 cjs- 1 ,2-Dichloro€then6 BRLl5s€o5 tans-1.2-Dichlofoeth€ne BRL78i7.s l.2-Diciloropropane BRLr12-2&s 1,0-OichloroproF,ane BRL594-2e7 2,2-oichloropropane BRL563-584 1, t-Dichloropropene BRL10061{1-5 cis-1,3-Dichloropropene BRL10061{2sbans-l,3-Dictloropropene BRL100{1-4 Ehyibe{Eene BRL87{U3 Hexachlorobutadione BRLs91-78{ 2-Hexsnone (MBK) BRL98{2-g lsopropylbenzeoe BRLso{?4 +bopfopyltoluene BRL16344+4 Methyl tert-butytether BRLloercr +Methyl-2-pentanone(MIBK) BRL75{gz Methylene ctlodde BRL9l-203 Naphth6lene ARLl0l6tl n-P@pylberEene BRL
pg/lpgn
!g/l
!g/l
!El
!gn
lJ9./l
!gn
!sn!El
!gn
!91
ttgrl
!g/l
ugn
lr!yl
!dlpEl
!El
tjElpg/t
!El
t,gl
trgl
rr(yr
|lEl
rrtyl
|lEl
FS/l
!!yl
!gn
ugl
!gn
!gn
!sn!dl
!dl
t'Erpgtpgl
!gl
!g/l
!El
u9nugnpgn
u!|/luEl
Fg/l
pg/l
1 .020.o0.51 .01 .01-00.51-02.O't0.0
1 .01 .01 05-0'1-0
1 -02.O'1 02.n1_01_02.00.50.51 01 01 01 0
2.O't _01 .01_01 .01 .01 .01 .0
1 .0't .0
0.50.51 .00.510.01 .0
1 .0'1 010-05.0' | .0
1 .0
SW846 82609 2741ar47 27^tar47 1031617 RLJ
Thit hbo4lory rcpod is ,tol vau ,,ilhaqt on aulhottzcd signaaa'? on the cover psgc
' RePortable Detection Limit BRL = B€low R€poning Limit Page 9l of 165
Page 601
Samole ldentificationFB-3sA5964l- 18
Clieot P.oieat #30 t -88
MatrixBlank Warer
Collectiotr Date/Tim€2l-Mar47 00:00
Received22-MaF07
CAS No- A,rabac(s) R,fnI Fhc 'RDL Dilubl Method ReJ PEpamI Analyed Balch An4lfsl
volrtile Orgrtrlc Conpounds
Volatile O.qanic Compounds bv SW046 82608Prepa.ed by mehod SW846 5030 Water MS100-42-5 Styrene BRL63c2o€ 1,1,1,2-Tehachloroethan€ BRL79-345 1,1,2,2-Tetrad oro€trane BRL127.184 T€hachloroothene BRI_108-8E-3 Toluene BRL87-61-6 1,2,$Tridttorobenzene BRL12o.a2r .1.2.+Tridllorob€nzene BRL71-56.6 1.1,1-Tfidlloroethan€ BRL?g{Gs 1,1,2-Trid oroethane BRL79{1{ Tdcfilo.o€thene BRL75-69-4 Tricilorofluoromethan€ (Freon 11) gRL
96-1&.4 l,2,lTrichloropropan€ BRL95{3€ 1,2,+Trirnethylbenzen€ 8RL10s67{ l,3.5.Tdmeff.|ylbenzene BRL75414 Vinyt citoddet330,&7 m,pFxylene9f!47$ o.Xylene1099€-9 T€trahydofuren60-29-7 Ehyl eher991-05{ Tert-amyl methyl ether617-923 Efiyl left-butyl ethert0&20n Diisoproptether7t65-O Tert-Butanot / butyl alcohol12+91-1 l.+Dio/6ne
&raogats .Ecoveresr46orn4 4&ofltof,uorcbenzene
m37.26-5 Tdluene4S
I to6o474 1,24ic @@thane-d1
BRLBRLBR!BRLBRLBR,LBRLBRLSRLgRL
92101106
t03ta68-53.7
SW846 62808 274nar47 27-Mar47 7031617 RLJ
+Cr ETPH 2&Mar-07 2&l,rar47 7031505 DS
pSn 1.0
ttil '!.0
ldl 0.5
tldt 1.0
ttgfl 1.0',/gtt 1.0
t4 1.0
lgn 1.0
FSn 1.0
VSA 1.0
Vglt 1.0
Udl 1.0pdi t-0
Itgll 1-0
rc 1.0Fgl 2.opdl 1.0
Fdl 10.0
ItdI 1.O
rlglt 1.o
t!{ 1.0
t4 1.0
t'eI 10.0
t'gn 20.0
70,130 %70 tm%7o-130 %70-130 %
lrg/l 0.I
mC/t 0.1
lnSI 0.1
mg/l 0 1
mgn 0.1
mSn 01
fi€I 0.t
'nsil 0.1
m9 0.1
ngll 0.1
4L14O %
sglt(/l
Ertr.ctrble Petrcl€um Hydrocsrbong
Extractable Total Petroleum HvdrocatuonsPtepa.ed by metlod SW846 3510C8tx)6€1.9 casoline6847d-3112 FU€l C)il #26€47631.3 Fu€l Oil ,f46&553-00-1 Fu€t Oil ,t6illlggtoooo Motor Oil$olfiiulo Aviatjon Fu€l
thidentifiedOf|er Oll
Total Petoteum HydroaafionsCgC36 Aliphatic Hydroc€rbons
Sarnogal€ r€coy€nbs:3386-312 1 -Chloro@tadecane
Semivobltl€ Ory.iic Compo trdr by CC
Oroanochlorlne P€sticides SW646 8081APreparcd W mefpd SW846 3510C3094G2 Aldfin319-64{ 6-BHC
BRLBRLBRLBRLBRLARLBRLBRL
BRLBRL
119
BRLBRL
0 . 0 1 1 1
0.011'1
SW8{6 8O01A .^lsr47 &4{47 7031497 lG
Thjs labodor! rqorl is ^oa saM ',/ilho'n s.t tsthorizc.I slgn,',t re oa lhe coie Fsge -
r Repo.tdle Dotection Limit BRL = B€low Repoding Limit Prge 92 of 165
Page 602
Sample JdeotiftcationFB.3sA5964r-r8
Cli€nt Proiect #l 0 t -88
MatrixBlank Water
Collection Date/Time2 t-Mar-07 00:00
Receivcd
22-Mar-07
CAS No, A"alrk(s) FIog Uni'l DiIAiofi Method Retr. Prcpated Analycd Ba.ch Aietyst
Semivolrtlle Otgrnic Compounds by cC
Oroanod odne P€sticides SW846 8081APr€pared by mslhod SW846 3510C3t9-et7 b"BHc3i9-€6{ d-BHC58499 S-BHC (Lindane)57-71-9 chlordane72-5{J 4,4-DOD (p,p')726$e 4,{.-DOE (p,p')50'2s3 4,4.-DOT (p,p,)@-57-1 Dietdrinc5$$4 Endosulfan I3321165-9 Endosufan ll1Ar{7€ Endosulfansultate72-2O-A Endrin7421€3!4 End.inAidehyde76-44.4 Heptachtor7?-435 Mefnorychlor10?4-57-3 Heptachtor Epoxidemo1++2 Toxaph€n€5108-7r-9 a-Chlodane€,566347 gchtordane53tg|70-5 Endrin Ketone
Sa|Iogate €cou.enes:1 0186-8+2 4,+DB4danuorouphenyl (Sr)mg-2+3 Decechlorobiphenyl (Sr)
Polvcfilo.inaled Biohenvls bv SW846 8082P.sparcd by melhod SW846 35i0C12674-11-2 PCB 101611104-?d-2 PCB, 12211114r-1615 PCB 1232s346+21-e PCB 124212672-2s{ PCB i24811007{+1 rcB 12541i0€6{2€ rcB 12603732+ts'5 PcB 1?621 r 1{X}14-4 rcB | 268
Slnro$l€ ,€cov€rfus:ro38e8/-2 4,4O&Octafl uorobiphenyt ( Sr)2o51-21-j Decachbrobiphenyl (Si
S€nivobdl. OrS.nic Compounds by C.CMS
BRLBRLBRLBRLBRLBRLSRLBRLBRL
BRLBRLARLARLBRLBRL
BRLBRLBRLBRLBRL
14077
ERLBRLBRLBRLBRLERLBRLBRLBRL
5085
BRLBRLBRLBRLBRLBRLBRLARLBRL
pgn
tlgllug,
FSnpEl
!9n,J(ylp9l
r91lugtlps/l
pgl
1.,91
u9/l
ugrlrg/lpdt
!g/l!sl!qn
0 0 1 1 1
0.0 '1r1
0 _ 0 1 1 1
0.0556
0 0 1 1 1
0 . 0 1 1 1
o.ot11
0.0022
0 . 0 1 1 1
0 - 0 1 1 1
0 _ 0 1 1 1
0 0 1 1 1
0 _ 0 1 r 1
0 . 0 1 1 1
0 . 0 1 1 1
0 . 0 1 1 1
0.0556
0.01'11
0 . 0 1 1 1
0 . 0 1 1 1
3rr150 %3c-154%
sw846 8081A
sw846 8082
sw846 6270C
1
1
1
I
1
1
1
1,1
1'I
1
I
I
I
I
l
1
1
1
26-Mar{7 26-l.,lar-07 7031437 TG
pg/r
pgn
t)g
l.rEl
!dl
!sflpgl
tlSJl
ugl
Wnp(yl
!g/li.isnp{vl
!g l
Ljgl
!slu94
0_02220 02220_02220 0222i_0222o_0222o_0222o 0222o_0222
2GMar-07 26-lv1aF07 7031496 SM
30-150 %30-150 %
Semivdatle Orcanic Comoo'.lnds bv SW846 8270CPrcpared by m€lhod SW846 35'l0C83-32-9 Acenaphthene2O&9H Acenaphthylen€9Gr24 [email protected] Ar ine12G12-7 Atthracenel9l2-2+9 At?zine1fi13!3 Azobenzen€y'Diphenyldiezine9247.5 Benidine56-513 B€nzo (a) anthracene
26-Ma.47 2g-Ma(O1 7031499 M.A1_000.4001_001.00.t.00
r.001.001.00
0200
Thb labontory rcport Lt ,rol .olU wirho& rE laahoriaed sbfiature on the cover psge .
' Report!5l€ D€tection Limit BRL = Below Repor.ine Limit Page 93 of 165
Page 603
Sample IdedtificationFF3sA5964l-18
Client Pmiect #301-E8
MatrixBlank Watef
Collection Dale/Time2l-Mar47 00:00
R€ceived22-Mat4'l
CAS No- Aaslyu(s) Flag "RDL Dilation Mdhod nel. PEpand Aazlyatd Bdth At olfst
SeEdvol.lile Org ic Compouods by GCMS
S€mivolatile O.oanic Comoounds bv SW846 8270C
Prepared by rnsthod SW846 3510Cs0-324 Bdlzo (s) pfene205-9S-2 86tE0 (b) ffuoranthene191-?+2 B€rEo (g,h,i) Ferylene20ru8.9 Eeruo (k) fluoranthene65{54 g€nzoic acidlCXl51{ Benzyi alcoholr11.91-1 Bis(2-chbro€thoxy)mehane11 l-444 8is(2-cfitoroethyt)ether3so3&32-9 Bis(2rhloroisopropyl)ethe.117-81.7 Bis{2-€hylf€xyl)phhalate101.H +Bornofienyl phenyl et|6a85€&7 Butyl b€nzyl phthalato86-7+8 Carbazol€sg-sll.7 +Chloro-lm€thylphenol106-47{ 4-Cf{orc€niline91-5€-7 2-Chtoronaphhelene95-57+ 2-Chloroptr€nd7005-2-3 4-Chlomphen/ phenyt e0Erle01+ Chrlrs€ne53-703 Dibenzo (a,h) anthrac€ne13?-6,1.9 Dib€.Eofuran9s-5o-1 |,2-Dichlorobenzenos{1.?iln l,}DicNdbb€nzene105-4G7 l,4oichhrobenzene91-9.{-1 3.3-Dlchlorob€nzidine120312 2,+Oichloroph€nol8.16&2 oied.|yl phhalate131-11-3 Dimethylphthalatel0s7-s 2,+Dimethylphenolu.71-2 Di-|}S'nylphthalateS+s2-1 4.GDinitro-2{ethylphenol51-2&5 2,+Dinitrophenol12r-1il2 2,+Oinitrotoluen€60G20-2 2,G.Dinitsoitolueoe117{r{ Oin-od}dphthalaG20€-4,r{ Fhotranthene86-7+7 Fluofene11+74-l Helaclilorob€rrzene87S&3 Hexadtlorobltradi€n€n474 Heoadrlorocyclop€ntadiene6l-72-1 He)€doroethanslc+3s-s Indeno(,|,2,3d)pyrene78{s.i lsophod€9157{ ?-l{€thylnaphhalene954&7 [email protected] , 3,+Melrylph€nol1&11-5si+o-3 Nephthalene8,i-14-4 2-Mbo€ndine
'NiltE€nilineioerx{ +Nltroaniin€
BRLBRLBRLBRI-BRL
sRr_BRLBRLBRIBRL8RLARLBRLBRLBRLBRLBRI-BRLBRLBRLBRLARLBRL8RLBRLBRLBRLARLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRLBRI-BRLBRrBRI.BRLBRLBRLBRL
BRLBRLBRLBRL
FSn!!nus/l|lsnpsn
!41pdl
Itgl|lsnugll|gr'lt4FSnw!dlpdl
!dl
eglusnudl!tylldlpsn
wltstlpsnFSn!Eltgt!dluglpgl
rrdlt c lt grl
wpgnpc4pdl
!dlfldl|ldl|lgt
pgnpdl
l€it
||gn
wEr{pcn
[email protected]
0.3001.00'1.00
1.001-001.001_00L00
1.00|.00r.00r.00r.00
1.001-001-O0
o.2001.00r.00r .@
|.001.00|.00l.oo1_001.001.001.001.001.()0t.mt .m|.00t.001.oo
0-6001.001-00
0.2001.001-001.0010,0
t.m|.00r.001.00
?:hls t4brdory ppora ls ,tot wIU *i hoar tE osrto;Z..|stgnofrtE on tha @E page.
I ReporrEble Dei€ction Li&it BRL= Below Reportine Limit Page 94 of 165
Page 604
SafllDle ldentificationFB-3sA59641-18
Client Proiect #30r-88
MatrirBlank Water
Collection DatdTime2l-Mar-07 00:00
Received22-M^t-07
CAS No, Analru(s) FIsE |RDL Dilutioa Melhod ReL Prcparcd Ana4zed Batth Anabst
Semivolsdl€ Organic Conporndr by cCMSSemivolatile Oroahic Compolnds bv SW846 9270CRepared by method SW846 351 0C
98+s3 Nitrob€nzene88-7t5 2-Nittophenol100{2-7 4-Nitfoph€flol€-7sg N-Nitrosodinethylamine6?1{4-? N.Nltrosodi-n-propylamine86JO{ N-Nitrosodiphenylamine87{+5 Pentachtorophenol85{1{ Phenanthrene10F9r2 Ph€nol129&, ryren€11G€6-1 Pyddine120+2n 1,2,+Tnchtorobenzene95-S5-4 2,4.tTrichtorophenole6{F2 2,4,GTricilorcphenol
S.r,n€at€ recov€flbs:i2t40-o 2-Ftuuobiphenyl36'7-124 2-Fluorophercl1165404 Nitrchenzene-ds110162-2 Phend4'171a-814 Terykenyt4411d-79-5 2,4,6-TrbrcmophenotSVOCS bv SW846 8270C SIMP.eparcd by melhod SW846 3510C83-324 Acenaphthene
208-96.{ Ac€naphdrt4ene9G12{ 1-Methytnaphthatenel2Gl2-7 Aithrac€ngfG55-3 Benzo {a) anthracene$-32{ Benzo (a) pyrene2os-2 BerEo (b) fuoEnthene191-24-2 Benzo (g,h,i) p€rytene2tru8€ Benzo(k)fluorantfEne21&014 Chrys€ne5&70.3 Dibgr]zo (a,hl [email protected] ]Lo Fluoranthene8&73-7 Ffuor€nei9ix9{ Indeno ('|,z,}cd) pyrene9r€74 z-Methy'naphtnalene9l-?0-3 Naphthatene85.01{ Phenanthrene129004 Pyrene
&,'|oga(e fEcov€nbsi321{0-8 2+luotobiphenyl1718-514 Tedlenyl4l4
Told M€rrb by EPA 600M000 Series M€thod3
8RL
BRL
BRL
SW846 8270C 26-Mar-07 29-I,tar47 7031499 M.BBRLBRLARLBRLBRL8RLBRLBRLBRL8RLBRLBRLBRLBRL
737780689250
BRL
BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL
BRLBRLBRL
BRLBRLBRLBRL
8398
pg/l 1-00
!g/l I 00
!S/l 1.00pg/l 1.00pdl 1.00
ldl 1.00
USx 1.00pg l 100pdl 100
Lidl 1.00
!S/l 1.00
ldl '1.00
Ug/l 1.00
l4/l 1.00
30-130 %15-110%3G130 %15-110 %30-130 %1u110 0k
!g/l 0.050
!g/l 0.050yS/l 0.050
Ug/l 0.05t)
trg/l 0.050
!g/l 0.050
!g/l 0.050pg/l 0.050
!g/l 0.050
US/l 0.050
tlglt 0.050pSn 0.050
udl 0.050
lSn 0.050pdl 0.0sopdl 0.0so
!s,4 0 050
!S/l 0 050
3G1m %30-130 %
mg/l 0.0050
mgl 0.0040
ms,4 0.0050
1 sw846 8270C/EPA625 StM
'1 "
1 "
1 '
1 '
1 '
1 "
1 "
1 '
1 "
1 "
1 "
1 "
1 "
1 "
1 "
1 '
1 '
28-MaF07
A4t-22-4 Silv€r
744ft&2 Alsenic
74,()1393 Bsrium
1
l
1
SW84660108 27-Met47 2A-Mat47 7031619 LR
Thit laborsaoq rcpon is not valid *ilhou an sulhotiae.I sigdaluft on the covet page .
' ReDortable D€tection Limit BRI- = Below ReDortins Limit P€e 95 of 165
Page 605
Samole ldentificationFB.3sA5964l-18
Client Proieot #l0tt8
MaffixBlaEk Water
Collection Date/Time21-Mar-07 00:00
Received22-Mat41
CAS No. Analyu(s) FI8C 'RDL Dilattu',| Melhod Rdtr. Prepared Analwl Botth A&lys!
Torrl M€rrl6 by f,PA 6lxxy7000 s€rlfl Merhod!
zl40-43€ C€dmium BRL
7440.47-3 Chromium ERL
7439€2n Lead BRL
7782a+? Selgnium BRL
Tor.l Metrh by EPA 200 S€ricr Metftods
743947-6 Mercury BRL
sw64a 6010s 27-Ma'47 m lar47 7031610 LR
EPA245.tn470A 2t.Mat47 28.tto'47 7031620 YP
ng/l
mgn
msnmg/l
0.0025
0.0050
0 0075
0.0r50
0.00020
t
I
'|
1
mgn
Thjs bborolory repod b Nt eabd wllhot ur audtoriaeil slgn tLr. ot the coaer pag..
'ReporEble Detection Limit BRL= Below R€porting Limit P€e 96 of 155
Page 606
Sample IdentificarionTB.3sA5964 t- l9
Client Proiect #30t-88
MatrixBlarl Water
Collection frate/Time2l-Mar07 qq:t 0
Reccived22-Mar-07
CAS No- Aialy,Ek) Fl"g Units 'RDL Dilation Method Retr. Preryr.ed Aaaltzed Barch Ant lrsl
Volrtil€ Org.rtc Compounds
Volatile Oroanic Compounds bv SW846 82608Prepared by rnebod SW846 5030 Wat€r t\tsu6-l+t 'l,1,2-T.ichtorotriflu6oethane (FreoBRL67{+1 Acetooe 8RLi07-13-1 Aq-ttonitite BRL714}2 Benzene BRLi0F€6-1 Bromob€nzone BRL7+Sf-5 Bromochtoromelhane BRL7+2f4 Bromodichtorornethane BRL712+2 Bromoform BRL74{34 Bromonethane BRL74413 2.<anon6 (MEK) BRL10+51{ n-Butylb€rEene BRL13+€8{ sec-Butylb€nzene BRL
tgrt€ltylb€nzene BRL7+rs-0 carbon disuttide BRL56-2+5 Carbon tetrachtoride €RLr08€G7 ct orobenzene BRL75{&3 chloroefhane sRLa7{&3 Chlorolorm BRL74{7.3 Chloromethane BRLs5.494 2-Chtorototuene BRLio s-4 4-Chlorototuene BRL9612-a 1,2-Dib|omo-3-chtoropropane BRLt2{-4&1 Dibmniocl{oromehan€ BRL1Fs3-4 .1,2-Dibmmo€thane(EDB) BRL7445n OiblomonEthene BRL95{+1 l,2.Dicruofobenzene BRLar4t-73-r l,3-Dichtorobenzen€ BRL106-1G7 l,4-Oichlorobenzene BRL7rf14 Dicfilorcdifluoromehane(Freoni2)BRL75-3+3 1, t-oi{:t oroethane BRL1074G2 1,2-oichlo|oethane BRL7t35>4 1,1-Oii:htoroethene 8RLt5$5€-2 cis-1,?-Dichloroethene BRL1s€-0G5 fars-.1,2-0idtloroetheno BRL7a{7-5 l,2-Dictrloropropane BRL142.2€€ l,}Dichloropropane ERL594-2G7 2,2-Dichloropropane 8Rf563.58€ 1,l-Dhhloropropene BRLlllu61.o1.5 cis-1,3-Dichloropropene 8RL100614{ h?ns-1,3-0idllofopropene BRLtot}.tl-1 Edrylb€nzene aRL87'6&3 H€xechlorobutsdiene BRL5e1-76{ 2{{exEnone ([rBK) BRL98+23 lsopropylbenz€ne BRL9S{76 +lsopr@yltoluene BRL163.44-1 Methyl left-but,,1 eth6r BRLroetGl 4-MedlM-2-pentanone(M|BK) BRLIs0s2 Methylene chlorid€ BRL91-zL3 tlapht|abne BRLl0+€+1 n-Propylb€nzene BRL
UMyg/l
!g/l
pgnpg/l
trg/l
!snlj(/r
!91
!gn
!g/l
!g/l
!91
ug./l
u g lpg/l
pg/l
!gn
!gn
!!,./lp{yl
p(yl
pql
pgl
pgl
plyl
plyl
!sl
!g/l
u9n!9n!dl
!9/l
!g/l
!9n
!gn
Lj9lp9l
tl(yl
uElysll
!Et
Lrg/l
rcnpgl
pgit
uglpg/l
pgl
ygrl
1 .020.00.51 0'1.0
1 .00.51 .02.O10.0't _01 01 05-01_O1 0
2.O1.02.O1 .01 .02.00.50.51 .01 .0l_0't .0
2.O1.01_01_0
1 01 .0
1 01 01 .0'1.0
0.50_51 .00.51 0 0'1.0
1_01 .Dr0.0
5-01 -01 .0
1
1
1
1
1
1
I
1
1
1
1
1
1
1
1
1
1
1
1
I
1
1
1
1
1
1
I
1
1
1
1
1
1
1
1
1
I
I
1
I
1
I
1
1
1
1
1
1
1
SW846 82608 2741,ar01 27.Mar07 703t617 RLJ
This lrborolory repod Is nol patd withou M tcrto ad sigaataru on the cowr page.
+ Reportable D€t€ction Limit BRL = Below ReDortins Limir Page 97 of 165
Page 607
Sample IdentificatiooTE-3sA5954l- 19
Clietrt P.oiect #301-Er
MatrixBlalk Water
Colleotion Date/Time2l-Mar{7 00:00
Receiv€d22-Mar-07
CAS No, Analtre(s) Reselt FIae rnDL Dilutk'n Mahod Retr P.z?orel Ansb\ed Balch A.taryst
100425 styrene
63G20-6 1,'1,1,2-Tetachlorcethane79-3{-5 | , I ,2,2-Tetrachloroethane127-184 Tetfachloroethene108-6aJ Totuene87{t-6 '1.2,}Tddt lorob€nzef le
r20-82r .1,2,+Tdd{orob€nzene
71.5t6 1.1,l-Tfft* oro€thane79{0-5 1,1,2-Tridllofo€thane79.{)1{ Trichlofoettr€ne
Volrtile Org.nlc Compornds
Volatile Oroanic Comoounds bv SW846 82808Prepared by mehod SW846 5030 Water MS
BRLgRt
BRLBRLBRL8RLBRLSRLBRLBRL
75.6s-r Trict o(oilroromethane {F eon 1.1) BRL96-18{ 1,2,3-Tridlloropaopan€ BRL9{,€+6 1,2,4-TrinElhylbenzene 8RL108.671 1,3,5-Tfimethylbenz€ne BRL
USI 1.0
ttgl 1.0
tgl 0-5
rcil 1.0
td l 1 .0
Udl 1-0
ldl 1.0
IrSl 1.O
N t 1 0
tglt 1.0
t dl 1.0pdl 1.0
ldl 1.0
UgA 1.O
w 1 .0
rcn 2.O
Ig/l 1.0
ldl 10.0
ldl r .0
lSn 1.0
t'il 1.0
tdt 1.0
FCn 10.0
ldf 2o.0
7F130 %70-130 %7F130 %70-130 %
SW846 82604 z7-MaFOl 274nat47 7031617 RLJ
7rr{1-4 Vinylchbndel33G2c7 m,p-Xyten€95-47{ Gxylone1C'eS+9 Tehahydrofurans297 Ethyl et|er994{5{ Tert-amylm€bhyletf|ea637-92J Ethyttoft-butyt €theYr0e2G3 Oi-isoFr.opyleth€rTsso Tert-Bubnol / b'lq/ atcot|ol12$91-1 1,40bxane
SunDgaIs rEcoveriesi4F,to4o.4 +Btomofluoabenzene2$7-zes foluene4S1 70*07 4 1, 2-Dichloroethane 441868.$,7 Abrcmofruomnethaae
BRLBRLBRLBRLBRLSRLBRLBRLBRIBRL
90102105102
Thh laborubrf Epor', it ,st volid nt&lrod sn sqthodre.I slgndarc ot ahe cover ptge.
i Rcporbbie Detection Limit BRI- = B€lou' Reporting Linit P6ge 98 of 165
Page 608
Volatile Organic Compounds - Quality Control
Aralytqs) Flrg Units
Source %REC
Result %RtrC Limits
Spike
Levcl
RPI)
Limi t
B.rct 7031517 - sw846 5030 w|ter MS
Bhnl r703161?€LKl)
P.epared & Anal].aed: 27.t\rar{7
1.1,2-Tricfibroffi uoroethane (Freon 1 13)
Acrytonitib
B€rrzen€
Enmobenz€n€
Bto(nod)brolnehanegromodicttloromethane
Sr('nofofm
B(xnonEfhane
2€ubrcne (MEK)
n{{rtyt,€n4.re
E€c-Buvb€nz€n€
tert-BuMbenzen€
C€tbon diermde
C€rbm b['achlodde
Chlorob€rEene
Chlo1o€thEne
Chiomform
Chlorometlane
24hbrctoluene
44hbrotoluen6
1 2.Dibronrc-Schbrcpropan€
Dlbromod{orornethane
1 2oibronDethane (EDB)
DibromorEfl€ne
1 ,zoichlorob€t|z€n€'l,3-Dichbrobenzene
l,4.f)bhlorobenzene
SRL
ARL
BRL
ARL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
8RL
BRL
BRL
BRL
BRL
ARL
ARL
BRL
ARL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
|l9/lpg/l
u9/lpdl
!Elpsl
pgl
trg/l
rr(yl
lJg4
lrs/lpgtl
lls/lps/l
p9/l
psrl
|lg/l
ugl
ut / l
|Js/l
rs/lgrl
us/lus/ltrg/lpsnp9l
Lig/l
9 lpdl
!sn!dl
lJdl
!91
tts4
ugl
!gr
!g/l
!g/lpg/l
pgn
!El
|ls/lp9/l
ugnpsn!s/lp9/l
!s4pdlpqt
1 .020.00.51 01_O1 .D0.51.02 01 0 0' 10
1_O1_O5.01.01 02 01 .02.01 .01_02.O0.50.51 01 .01 .0l 02.0r.D1 .01 .01 .01 .01.01 .01 .01 0
0 50 51_00-510.01 .01 .0'I 010.05_0t_0
1 -01 .0
(Freon12)
l,t-DidrbrDeth8'l€I loihlorcethane1 ,1 .old o.oethen€cis.'|,2-Oichbmethenefa8-i,2-Oi{t oroetherEt Z-Dichbmpmpar'€1 ,3-Dict orogopan€22-DidloropropdE1 ,l -Dlchlo@prop€n€
ds-l ,'Dld oropiopenelrahg1,3{)l.fi lo.opropeneElhy{berEenetlox8chlo.obuladiene2+ler€none (MBK)lsoprJPYS€nzone4-lsop.opytolueneMetht tert-butyl etherGid€fif2+entanone ([rlSK)Mstrylsr€ dbrijeN+ht€len€n.Prcpylbenz€neStFen€
Thh ,abo.abry rcport it no, vzlu tsithoul an aathorized signotu.e on rte cove, pdge.
+ R€ponable Det€ction Limit BRL = Betow ReForting Limir Page 99 ol 165
Page 609
Volrtile Organlc Compouods - Quallty Control
Analyte(s) Result Flag Units *RDLSpike Source o/"R.EC
kvcl Result %REC Limirs RPDRPDLinut
Brtch ?031517 - SW846 5030 Wrter MS
Blar|t (703161?€LKil
Pr€par€d & AnarFed: 27-Mar-07
1,1,1,z-lebad oroelhane
I, 1,2,2-Tetracl{or*thane
l,2,STrichlorobenzene
I ,2,+Tdchloroberuene1 ,1 , 1-T.icfibrGfhane
1 ,1 ,2.Tridlcro€lh€fl€
Tridrloroelhene
Trichlorofl uoror|letlene (Freon I 1 )l.2,STrichloropropane
1 2,+Trinrelhylbenzene1,3,STrid€thYb€nzeno
o-xylen€
Tetrahyd'oturan
EdIy' elher
Tert-ffrry| methyl 6th€r
Ethyl iert-butyl efler
Di-lsopropyl sth€r
Tert-Buianol / buvl alcohol
1.4-DioxEne
S u nwal€ : 4-B rono fl u oto b on zenoS',Iogate: foluene4SS unogate : 1, 2 D i ch lo rcel h arc4 4Suntga.'F- : D i h rono fl u orc n elh ane
LCS r7ftit6t7€S1r
Prepared & AnalFed: 27-Mar-07
1 ,1 ,2-T(i$k)rotifluoroethan€ (Fr€oo 1 13)
8€nzen€
Broanob€nz6n€
Bromoct oaomethane
Bromodichlorcfielhane
Brornoform
Eromo$et|an€
z-Bubnone (MEK)
n-Butylb€nz€ne
s6c-gu!/b€nzene
torl-8utylb€nz€ne
Carbon disulfide
Carbon tetaac oftt6
Chlorob€ruene
Chlor@than€
Chlorobm
Chlo(ometlan€
24hlorotolu6ne
4{hlorololuene
1,2-DibrsnGH*rrop{opan€
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
SRL
8RL
BRL
BRI,
BRL
BRL
BRL
BRL
BRI-
BRL
BRL
8RL
BRL
aRl-
ARL
45.649.951.251.4
'17.5
13-9
20.2
r 9 s19.4'ts.8
19.6r9.620.4
19.0'17.6
17.7
lt.o19.5r8.8r 9-7
20.820.422.7
t'$psnydl
IJdIttsnudlus4psx
tt$!dl|ldlt 9 ll€n!s4pdlgEl
u(yl]|gil!dlPdl!dludlItgtl
psrl!cnlldlIJCI
pslpsn
!s4!Ert,gltlgi!s4pdl
!sn|r9n1lg4l8/lpgl
F91!g/l
!dlIrg/ll!g/l
Pgltrdlfldllsn
1.00.51 .01 .01 .01-01.0t . 01 .01 .01 .01 01 .01 .02.0'1.0
10-01 .0t . 01 .0r 010-0m-o
50_o50.050.o50.0
20-020.0m.020.0m.020.020.020.020.0m.020.o20-0z).020.020.020.020.020.o20.0m.020.020_o
91 70-1n1M 70.1mlm 70-lm103 70-tg)
88 7G13070 11.r-147101 70-130
100 70-13t)
97 7Gl3t)g9 7G130s6 70-130sa 7G130102 62-13666 53.+133s5 7G13088 70-',t30
88 70-13086 7(}.13005 7Gr3098 7$t3094 62.0-t3it
98 70-130
r11 70.130104 7Gt301U 70-130114 m-130
Ihb hbordory reped h nor vdu Nlth*r cE aulhod,td sagnoure on lhe cow, pq. .'R€portable Detc(ti@ Lioii BRL = Below Reportiog Limit P{ge 100 of 165
Page 610
Volatile Organic Compounds - Quality Control
Spike
Level
RPD
Lirnit
B.ach 7031617 - SWE{6 5030 Wrter DtS
LCS t7031617€S1l
Prepsred & AnelFed: 27-Mar{7
Dlbrbmoc'|brdn€thane
1,2€lbrorm€thane (EDA)
Dlbomomeihane
1 JSlchb.ob€nzene
1,3-Dlchlorob€nzene
1 ,4-Dici orobenzene
Did$rodif !,ofom€thane (Freonl 2)
| ,l -Di$loro€thane
1 ,2-Ornbm€thane
1,1.Dichlorc€lh€ne
ds- l 2Oicnloro€tttsne
tans, l,2oichlo(o€thene'I .2Oichlo.opropane
l Soichloropropane
2 2-Oidrloropropane
I , | -Dichlompropene
cis,l,3-Oic+ oropropene
tlans-'l,3oicnbroFropen€
Elh/b€nzene
Hexachloncbutadiene
2-Hexanone (MBK)
lsDpmpylbenzene
+l€opropyltEluetP
Ilothyl brt-buv ether
4+.relhyl2rentanone (MISK)
ftr€thybne cfilodde
Nephihabne
of.opylb€nzene
Styrene
1,1, 1,z-Tetrachloro€thane
1.1,2,2-TeUEchbroehan€
Tellacfiloroelhen6
Tolu€n6
1 ,2,&Tri'lbmb€rE€ne
| ,2,+TrtchlomberE€ne
1 , 1 ,1-Tricibroehan€
I ,l ,2-Trbhloro€tfiane
Trichloroefnene
TftJ oronuoroflEthane (Freon 11)
l2.STrichloroproDane
1,2.+Tdm€bylbenzene
1,3,$Tdm€lhy'berEene
Vtr\4 cnlorue
m,FX9€ne
o-Xybo€
Telaahydroturao
Elhyle0€.
T€d€rny' methyl €f|€r
Ehyl b.t{utyl eth€r
Diisopropy ether
T€d-gutend / butyl alcohol
1 9 . 8
20_0
19.3
21.3
20.5
19.4
20.4
19_4
19.8
17.1
2 0 7
14.7
20.4
202
18.6
18.4
21.1
22.5
202
1 9 I
1 3 . 5
18.2
1 9 2
20.7
18.4
18.5
19.8
14.2
18.8
19_5
20.s17.6
1 8 . 7
2 0 8
1S_g
17.7
rE.2
17.3
?2.6'| 9.2
18.7
22.1
39.2
19.9
20.5
20.2
19.4
2 1 . 8
20.8
205
ps/l
|lgl
psn
t/s/lusnpdl
!dlpsrljgn
rglpgl
ljg,l
!s/l
vs,4pgl
psn
!91
Ljgl
!g/l
t /g l
ps/l
IJEI
tlEl
!s/lpsnljglpgl
!snpdl
!si4rdlps,4
r.i!yl|llyl
!gl
pEl
p9/lps/r
!s,!glpgl
rs/lpg/l
wApsnpsn
tsllFSnjrdl
psn
!c4
20_o20.o20,020.o20020.o20.020.o20.020.020020.020.020.o20.020.020.020.020.020020.020.020.02 0 020020.020.02 0 020.020.o20.020_o20.02 0 02 0 020.o20.o20.o2 0 020.o20.o20020.040.020.0m.020.02i.o20_o20.0200
99 70- 143100 70.130s6 70-130106 70-130102 70-13097 70-130102 39.3-16797 70-13099 70-13086 70-130r(x 70-13094 70,r 30104 70- t 30101 70-13093 70-13092 70-130106 70-1301t2 70-130101 70-130100 70-1366a 56.3-131s1 70-13096 70-130104 70-13092 70-13092 70-13099 7G13091 70-13094. 70-13098 70-130104 70-13088 70-13094 70.130104 70-130100 70-13088 70-130106 70-13091 70-130E6 70,130113 70.130
96 70t3094 70-130110 7G13098 7G.130r00 70-130102 7G.130101 7G130s7 7G130109 70-130104 70n30102 70-130
Thh latonlary rqorl it not valid Nithout att sathoritett signat,.e on lhe cover page
r Reportable Detection Limit BRL = Below Reporting Limit P^ge l0l of 165
Page 611
Volatile Organic Compounds - Quality Control
Anallt€(s) R€€ull Units .RDLSpik€Level
RPDLimitFlag
Source %RECResBft '/IREC Limib RPD
Bahh 70Jr5l? - SW846 5030 Wrter MS
LCS f70318t7.Bstl
Pr€parod & Anslyzed: 27-Ma.-07
1,4-Oio€ne
S u ftogate : 4 €,lonon uotd en n neSunoqal?-: Tohtene4SSunogata: l, zaid tbftetha'€44S u rogate : Dih ro nafl uo@n atha ne
LCS Duo (703161?.BSOil
Prepared & Ana\zed: 27.Mar{7
1 ,1 ,2-Trichlorobinuoto€thane (Freon 1 13)
AE ylonirile
B€nz€ne
gmmoct|lorornethane
Bronbdichbrornehane
Sromoforn
2€ubnon€ (MEK)
n€utylbenzon€
9€oBuMbe.Eene
isrt€utylbenzeo€
Carbon disulfde
Carbon letrachbdde
Chlorob€nzen€
ChlorEethane
Chloroform
Chlofomethane
2-Chlorclotuene
4{hloroioluene
1,2.Dibtomo3-chloropropane
Obromo{hlorom€than€
1,2-Dibromoethane (EOB)
Dibromomethane
1 ,2-Dichlorobsnz€ne1,'Oldrlorobenzen€'t ,+Di*rlorohenzen6
Didrlo.odiff uoromethane (Freonl 2)
1 ,1 Oichloroe$Ene
l,2Oichloro€tl|ane
1 ,1 Oichloroeth,ene
cis, 1,2-Dichlorcethene
trans-1,2Oichlor€th€ne
| ,2-Dl* oroprcpan€
f ,3oichlorop{opan€2,2olchhopropane
1,1-Diehloropropene
cis-l,3-ttknbroprop€fl e
lrans-l,30lat orop.op€n€
EthylblEeo€
Hexachlorcbutadiene
2+io(anone (MBK)
2m50.5
49.819.7
16-0
13_7
r9.8
rB.7
18.4
18.8
r8.6
19.0
18.2
13.6
17.3
16,6
16.2
15.6
18.4
17.7
16.8
20.7
1S.6
19.3
22.O
19.0
19.1
1 6 9
19.9
19_4
rE.4
18.6
18.3
r9.4
r5.8
19.6
17.4
19.6
19.5
17.4
16,9
21.9
19.1
17.3
t2.st 7 . l
Fgr
!dl
!dl
|lgl
|ldl
|tdl
w/lI,lEl
tsnpcnpgl
!dl
!dl
!dl
udluqlygrl
|,dlpsn
ug/lrc/lusnpqlpdl
!dluc4!dlWn|lgl
t d lFSntjEl
rglusnp9/l
tjdllrdlljdl!dlsgludl!dl|ldlpsn
20050.o50.050.050.o
20-om.o20.0m 020.020.020.o20.020.020.o20.020.020.o20.0m.020.020.020.020.020.020.o20.020020_020_020.020.0m.020.020.o20,020.020.020.0
20.020.020-020.om,0m.020.0m.o20.020.0
100
101101100
t,(yl
lldlpsil
rsrlllgn
7G13070"1Uf&13070-t 307G130
70-1fr) 10
41.1-147 3
7G130 2
7G130 6
7G130 5
7G130 57Gi30 570-130 362-t36 11
53-9.133 4
7G130 10
70-130 770-13/J 6
70-130 6
7G130 I7G130 6
62.&132 770-130 4
70-130 770-130 670-130 6
70-130 47G143 170-130 170-130 27G13) 67G130 57Gi30 5
39.1t67 S
70-130 57St30 27G130 I7G1a) 670-130 I
70-130 A
7G130 3
7G130 77G1 30 S7{}-130 4
7Gr3o 2
70-t3o 5
70-138 15
56.3-131 I7G130 6
25502525252525
5050
2525252525
25252525255025252525
50
2525
252525
25E65025
8068sg94gz
94
95916986
838178c28ll9{10498961109596s4tfl)9792gt
v9779988798s8784r02fl096
€486
Thl! labntotf Eport Is not rdu frdhoaa ad aafrorbcd stgt arta o,r lh. @ve page.
i Repotuble Detectio[ Limit BRL = Below R€poding Limil Pag€ 102 of 165
Page 612
Volatile Organic Compounds - Qualify Control
Analytqs) Resuh Flag Unjts + R D LSpike
Level
R P D
I-inrit
Souroe %REC
Result %REC Limns RPD
Bercb 7031617 - sw8,t6 5030 wrter Ms
LCS Ouo t703l6t7ASD1l
Prepa.6d & Anal}.zed: 27,Mar-O7
4lsopropyltoluene
Melhyl terttuv ether
4-fvlethyl-2-pentanone (MtBK)
M€trlyl€ne chloride
Naphthalene
Slyrene
1 ,1 ,1 ,z-Tetrachloroethane
1,1,2,2-Tetrachbrostfrane
Tatrechbro€lhene
1 ,2,3-Tdchbmb€nzene
1,2,4-Tdchlorob€nzene
l ,l ,l .Trichloroethane
1,1,2-Trichlo.oethane
Trfttrloro€tl|€ne
Trld{orcfl uoomethane (Ffeon 1 I )1,2, $Trichloropropane
| 2,+Td.nehylbenzen€
| ,3,tTrimehylt€nzene
Vinyl dd,oride
m.p-xylene
o-Xylene
T€hshydrofurEn
Etryl stfi€r
Tert-amyl rn€bryl elher
Ethyl tert{ui/ ether
Dii8opropyl ether
TsrtBubtlol / butyl alcohol
1r{ioxen€g/llggefu : /l+l to nofl uorob e n ze neSuftcgate: Tohlene4gS u fi pga/€ : 1, 2-D ich lo rcet ha rc 4 4S unqab : Di btu mof lu oro metha ne
tlatrlx Spik 17031017-{rlslI
Pr€pared & Analfzed: 27-Mar-07g6n2en€
Chlolob€nz€n€
1 ,1-Dichloroeth€ne
Toluone
Trict{oroehene
Swntgate : llStomonuor&enzene
Surcgate: Toluene-daS ulroga|€. 1, 2 -D lch h.roel h a ne 4 4S u fl og ab : Ahrcnofl uorc mel h e ne
17.7
20.5
1 8 1
17.4
18.4
1 7 2
1 8 2
18.3
20.2
16.4
1 7 . 7
1 9 4
18.3
16.4
20.7
1 6 8
1 6 . 1
1 8 . 1
r7.3
20.3
36_4
18.9
20.4
20_2
1 8 6
21_2
1 9 9
204
214
5 0 55 0 549.149.6
SourE.: 5A59642.01
!g/l
!gnp9/l
ltgtl
trs/l
ljgl
!9npdl
!snugnpgl
!snp9nItgtl
psnps/l
!sn!(yl
I.t94psn
!g/l
!g/l
!dl
ugl
Lis/l
u9/l
Itgllpg/l
pgl
PSI/l
!grpsnpsnPE
2 0 020.020.020.o20.0m.020.020.020.020.o2 0 02 0 02 0 020.020.o20.o20.020.o20.o20.020040.020_020.o20_020020.o200200200500aa.o50.050.o
20.o20.020_020.020.050_050050.050.0
20.020.020.020-0
25255025252525252525252525252525502525252525
255025252525
88 70-13t1
102 70-130
90 70,130
87 70-130
92 70-130
86 70-130
91 70-130
92 7G130
101 70-130
82 70-130
88 70-130
97 70-130
92 70-130
a2 70.130
104 70-130
84 70,130
60 7G130
113 70-130
90 7G't30
86 70-t30
102 70-130
91 70,130
94 70-130
104 70-130
101 70-130
93 70-130
106 7D-13o
100 70-130
102 70-'130
107 70.130
101 70-130101 7G1n98 70-13099 70-1m
70-13t)70-13070-13070-13070-t 3070-13070-13070'13070-1m
70.13070-13070-1307G130
I
2
2
6
7
6
3
6
3
7
7
7
8
7
2
8
7
0
6
9
8
7
6
2
0
3
4
0
7
1 9 2
1 9 . 7
21.1
19.3
19.0
46.550.751.650_4
!s/l
Fgn
!s/l
Fgn
l.i9/l
!s/lpsll
t /g l|lgl
8RL
BRL
ARL
BRL
ARL
96
9a
106
96
95
93101103101
tlat ix Solks Ouo 1703161?.|its0lt Sourc€: SA5t682jl
Pr€par€d & Analyzed: 27-MaF07
Benzene
Chloobenzene
1 ,1 Oidrloroethene
18.519.220.319_1
BRL8Rt-BRLBRL
9296r0296
30303030
rg4rglpsrlpsn
42
o
This lahorarorf reryd is not edid withoet oa attrtoized signaturc on the covet page .
' Reportable Deleclion Limit BRL = B€low Reporring Limir Ple€ 103 of 165
Page 613
Volrtile Orgrnic Compoutrds - Qurlity Cotrtrol
Spike
B.tct 7031617 - SW8,l6 50J0 Wrtel MS
Matrix Solk6 Dup fl03l617.ltsol) So{rco: 5A50682{1Peparcd & Analfied: 27-i.laf-O7
Tdchbrosth€ne
S ufl W ele : tt8lomon uoroben ze neSfimge|€: TohEne4SS uiogtu : 1,2 -D k:h Io rEth arc 4 ISunog e : Dlbrc nofl uomm dh a ne
BNtch ?031642 - SW846 5030 Soir (hrgh tevetl
Blank 17031€4il€LKl)
Pr€pared & Anabzed: 27-Mar47
|,|,2.Tnchlorotrifluoro€tharNe (Freon 1 13)
Acrylonitnb
B€nzs|€
Brcmob€nzsn€
Bromochbromethane
Eaomodid orofirethanegrornofom
Brornornelhan€
2€utamn€ (MEK)
n€ulylb€nzgne
s€c-Bulylbenzene
tert-Butylbenzene
Carbon disulfide
c€rboi btradlbnd€
Chbrob€nzen€
Chloro€thane
Ct{oloform
Cruo@melhane
2-chlorotoluene
44hlorotolu€n€
1,2-D0rcmo-3rhbmpropsne
Dibromo€hlorom€thane
l,2obornoethane (EOg)
Dibronlomsflan€
12-Dlchlorcbenzens
1 ,3-Dk$lorobenzene
1 ,+Ok*rlo.ob€r|z€ne
Did{orcdfl luoromethane (Freonl 2)
I,lOhhioro€lhane
l,2.Dldiloroehane
1,l{]bhbroeth€ne
ds-12oid$icrDsth€ne
lrans-l,2olciloroethen€
1 ,2ol*loropmpan6
1,3{)ir$bmpropan€
2,2-DlJ oropropang
1 .1 -Oichbropropen€
cis-1,3-Dlchloropropen€
tlan+l,lDicf oroprcpene
Ethylb€nz€ne
HexactlorobutEdi€ne
2+lex€non€ (MgK)
'18.6
46.350-651,650.4
ARL
SRL
8RL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
SRL
BRL
SRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
SRL
BRL
BRL
BRI
ARL
BRL
BRI.
aRl
EFL
BRL
BRL
BRL
SRL
BRL
ARL
SRL
8RL
8Rt_
ARL
20.0il.ofr.ofr.o50_o
BRL 70-13070-13070-13r')70-1n7G1g)
ugilpglpqlpdlpdl
sl9!l101103101
lgrkg wet 1-0
ruLrkg wet 20.0
rcI(g wet 1-0
pgllg wel 1.0
Wl(rgw€l 1.0
pg/kg wet 1.0
!g/kg wel 1.0
pC/}g tv€l 1.0
pdks wel ?.O
pdkgw€l t0.0
lg/kg\rel 1.0
!g/kg vJet 'l.0
lg/tS vJet 1.0
ldkS wst 5-0
lgr'kg wEt 1-0
lgL/kg 'r,et 1,0
pgn(g wet 2.O
pglkg wet 1-0
Ugr'kg wet 2.O
ugagwet 1.0
lgr'kg w€l 1.0
Ug/kgw€t 2.O
Fgl(g tv€l 1.0
Ugr'kg wel 1.0
PSrrS Yrel |.0
lglgtYet 1.0
pSftS w€t 1.0
UdkS wet 1.0
llgftS v{at 2.0
tdkSwEt 1-0
lgr'kg w€t 1-0
!g/kg wel 1.0
Fgikg weI 1.0
t€/kg wet 1.0
tg/ lq wol 10
rc/kg $/ol 1.0
rg/kg w€t 1.0
Pg/kg '/61 '1.0
pgkg rY€t 1.0
pS/kgr€l 1.0
pdkg Yret 1.0
ldlS Y/€t 1.0
Ugr'kg wet 10.0
Irtb laborolaty r.Ior1 b nd valid tdthottt.a altthoria.l sig,@!*re on the cover ptF -
+ Rep.rtable Detection Limh BRL = Below R@orting Limit P.ge lo4 of 165
Page 614
Volatile Orgrnic Compounds - Quality Control
Analytds) Result Flag Units %REClRDLSpikeLevel
SourceResult
%RBCLimits RPD
RIt)
Limit
Brtch 7031642 - SW846 5010 Soil (high level)
Abd( {7031642.8LK1 |
Propared & Anal).zed: 27-Mar-07
4lsopropyltoluene
Mothyl t€rl-butyl €th€r
4-rvlethyl-z{entanone (MIBK)
Methyl€ne chloride
t{aphlhar,rne
Styren€
1 ,1 ,1 ,2-Tetsachloroethane
t . t ,2,2-TefachloroettEne
Tolu€ne
l,2,3'Talclrlorobenzene
| ,2,+T.kfilorob€nzene
| ,1 , l-Tri{$bro€thane
| , t ,2-Ttid orc€flane
Trichkroelhene
TdnbroRuorom€tlane (Freon 1 1 )I 2,lTricfibropropane
l,2,GTrimethyltrenzene
| ,3,$TrilnetrYb€nz€ne
Vinyl cf*oride
m,p.Xy'eno
TeHrtdroturdn
Ethyl ether
Te.t-arryl melfyl ether
Ethy' tert+ut/ etner
Di-lsopmpyl €ther
Tett€utanol / buvl alcohol
1,+Oioxane
Su/fog ale : 48 m monuo nb en ze neSwtu'a;le: fohene4Ss uif ogale : 1, 2 -Dich larcet h an e4 4Su/roga/€ : A brc rofl ttoruh elh a ne
LCS ft031AU€SI)
Prepa@d & Anal!.zed: 27-Mar-07
1,1,2-Trlchlorotrif,uoroethan€ (Fr€on 1 13)
Aqylonihlegenzene
BroanoberEene
Brornodrbmrn€than€
Bmnodichbrorfi€fEne
Brorhofoam
BroNnonrolhsne
2€ubnone (MEK)
nAdy|b€r'z€ne
s€c-Eulylb€ru€n€
l,erl€ut)4b€nzen€
Crlbon disutfide
BRL
BRL
BRL
BRL
ARLgRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
8RL
8RL
BRL
30.729.928.929_3
1 7 5
1 6 _ 1
20.4
16.5
21_2
21.5
20.2
21.O
20.6
16.0
16.6
18.3
19.3
18.O
30.o30.o30.030.o
20.020.0x.oz).020.020.020.0200z).020.020.020.020.020.0
1021009698
pS,4<S r €l 10
!g/kg w€t 1-0
pg/kg w€t 1-0
pgL4q wot 10.0
Udkg wet 10.0
pgxgwel 1-0
Lrgftg wet '1 0
!g/kg wet 1 0
lgr/kg wet 1.0
pq/kg wet 1.0
pg/kg wet 'l.0
pg/kg wel 1.0
!q!4(g wel 1.0
pg/kg wet 1.0
pg/kg wel 'l.0
!g/kg wet 1.0
!g/kg we{ 1.0
Uq/kqwet 1.0
t/g/kg wel 1.0
Ug/kg wet 1.0
Ug/kg wet 1.0
!g/kg wel i.0
!g/kq wel 2.O
!g/kg wet 1.0
Ug/kg wel 10.0
t/g/kg wel 1.0
pg/kg wel 1.0
!g/kg wet L0
pg/kg wet 1.0
Ug/kg wet 10 0
Ug/kg wel 20.0
Ugr'kg wel
ug/ko wet
!g/kg wel
LigLi kg wet
pg/kg wel
Ug/kg wet
pg/kg wel
!g/kg wet
U!r'kg wst
Ug/kg wet
lgr'kg wet
!g/kg wet
pg/kg {,et
Pg/Kg wst
lgr,l(9 wet
!g/kg v/et
FqkS Y,/et
Ugut(g w€t
88
80
to2
a2
106
108
101
105
103
80
83
92
96
90
70-1307813070.13070-130
70-130ln-17570-1n70-13070-13070-13070-1307G130
55.3-13638.8-'r427Gt307G1307G13070-130
This laborotorf Epon it ltot ealill wuhot l ar. u.horlud sigmtap on the cover page-
+ R€portable Detedion Limi! BRI = Below Reporrins Limit Prge 105 of 165
Page 615
Volatile Orgstric CompotrDdr - Qurlity Cortrol
Analyt{t Resuh .RDLSpike
tevel
RPDLioitFlag RTDUnits
Soufce "/il<EL
Result %REC Limits
Br.ch 70316,12 - Sw846 3t30 soit (higb kveu
LCS {70316,{2€S
Preparcd & Anely:ed: 27-Marfl
Ca6on ietachlodde
Chlorob€ozene
Chloro€lhan€
Chloroform
Chlorom€lhens
2.Chlo.otolueil€
44hlo€toluene
1,2-obrDmo-S\lo.opro[€ne
Oibromochlorcanethane
1 ,2-Oblomostrane (EDB)
Dlbromom€hane
l,2oichloobenzen€
1 ,S Dichbrob€nzene
| ,+DichlorEbenzen€
(Fr€on12)
15.420.419_719.620.7
20.019.620.921_420.6
20-sm.3N.2r9.719.61g_120.519 .120-421 .1?5.317.219.419.619.E18.1't4.5
18-6t E 9
18.818.920.817.0
20.1
lt .718.0m_219.617.121-A20-s16-823619.720.3'r9.8
20.020.020.020.020.om.020.020.020.020.020.0m.o20.020.020.020.020-0m.0m.020.020_o20.020.o20.020-020.020.020.020.o20.020.020.020.o20.om.0m.o20.020.020.0
20.020.020.o20.020.om.020.020.020.020-020.o20.0
70-1307G130
55.3-13070-r 3070-'t 3070-13()70-13070-130
64.7-1397G13070-r3{)7G13070-r 3070-130
UgL/kg w€t
|,g/kg wst
yg/kg wet
!g/fg wel
pCAg wel
ldkg',t€l
ldkS wet
lgr'kg w€t
Udkg rv€l
t g/kg vyet
pgkg wet
U9k9 wet
pd*S wet
ldkS w€t
!g/XS Y{€t
!g/tg YJet
lgr'kg wet
pE k9 wd
!g/kg w€t
pg/tg wet
Ugrlg wol
ldkS wel
lgftg r€l
lgr'kg w€r
!94(g w€t
Wr'kg wet
Ug/kg w€t
Ugkg wet
ug/kg wel
t/dlS w€t
lgr/kg \r€t
lgr'kg wet
ldkg Yret
t dks s/etpg/tg wst
!g/kg wetydkg w6l
lrgrlq w6t
!dl(S $€l
u94(g welggltg wetpgr'kg wetpg/kg vret
Ig/t(g wet
Pg/kg wetpdkg rv€r
lgftg w€t
Ugrkg r€l
UgLtkg yrst
tlgn(g s/et
t g/kg vrst
t01 34.4-1679a 70-13098 7Gr3090 7Gr30102 70-13096 70-130102 70-130t06 70n 3076 7Gt3om 7G13097 7Gr 3098 7&130s9 70-130sx] gl,7-140
72 70-130s3 70-13094 70-130103 7G13094 46.1-145s4 7Gr30'l0{ 70-13085 70-130110 70-130t00 70-13099 70-130EE 7G13094 7G130101 70.130s8 70-13086 70n30109 70-130102 70-130a4 56,&140118 7G1309E 70-t30102 70-t3osg TGlg)
102
9898104101to098104101103'103
102102
1 ,1-Dkfilor€f|ane1 ,2-DiJrloro€han€
1.1 -DichbroouFn€
cis-1 2Oidrlo.oethen€
trans-l,2-Diciloroethene
1 ,2-Didlloropr@ane
1 ,3-Didlloropropane
2,2'Dichloropropan6
1,1Oicl oropop€ne
cis-1,3-Oinbrcprop€n€
lrans-1,3{)idlblopropene
Ethy'benz€ne
l-lexachlorobuladl€n€
2+exanone (MBK)
lsop.opylb€rE€ne
4.lsopropyltdu€ne
Methyl ed{utyl ether
4-t\46tryl-2f €ntanorE (MIBK)
Me{hyl6€ d{orlde
NaPhthalen€
Styrene'l,1. l.2.Tehachkrelhane'1,1,2,2-Tolradtk,roelhene
Tetachlofoefrlen€
Toluene
l S.STridbroben:ene
1 ,2,+Td{$brob€nz€ne'1 ,1 ,l -Tridbro€fEne
1 ,1 ,2-Tricnbro€Urano
Tri:trldo€lhen€
Triilorofluoomelhan€ (F €on 1 1)
l,2,3.TncnbrbpEpone
l2d.Trimehyb6nz€n€
1,3.:>Tdrn€thyb€nz6ne
This bLonroq .eport b nol wIU ,sithout oa c&rtodsi tignra4 oa aha covc. prg..'R€poriable Detectior Limjt BRL -Below Reporriry Limit Plge 106 of 165
Page 616
Volatile Organic Compounds - Qurlity Control
Spike
Btub 7011642 - Sll'846 sox' Soit (tigft tev.l)
LCS ft03t642€31l
Prepar€d E Anal}i"zed: 27-Mar{7
rn,Fxyl€n€
o-Xylene
Telahydrofuran
Elhyl ethor
Tert-amyl methyt ether
Ethyl brttutyl ether
Di-bopropyl ether
Tert-Buland / bulyt atcohol
1,4-Orbxane
Sunllgate : ltB ro nrcfl uofi ft e n ze neSurogate: Toluarc4gS urqete : 1, 2 -D bh lo rce I h a n e 4 4S unqeta : D ibm nofr u o lDmel h E ne
LCS Du3 at031642.ASD1l
Prepared & Analyz€d: 27-Mar47
l.|,2-Trichloroffiuoroethane (Freon 1 13)
Acrybnihile
Bonzene
Brornobenzeoe
Brorno.filoromethane
Brornodicibrorn€tnane
Srcrnofofin
Brcanomefiane
2€ubnone (MEK)
niulylbshzEne
seeguMberEene
tert€uMb€nzene
C€rbm didnde
C€rbon tehachlodde
Chlorob€nzsn€
Chloroelhane
Chloroform
Chloroamhene
2-Chbrotoluene
4Chbrololuene
1 .2Oibttho-3-chlompropane
Dibrdnodllomm€f|ene
l,2olbohoefiane (EDB)
Dib.omon€hano
l,2obhhrobenz€ne
1 ,3oichhrobeozene
t.4-DichhrDb€nz€ne
(Fr€on12)
udks wet
9&g wet
!S/kS wel
!g/tg wet
pq/kg wet
!g/kg wet
Pg/hg wet
!gl(g wet
!g/hg vret
ugL/hg wetlgL/kg wstpgn(g wetPg/kg wet
yg/kg wet
Ug/Kg wei
!g/Kg wet
LiEr(g wer
|lg/kg wet
Ug/kg wet
ugr'kg wet
uqr(q wet
Lig/hg w€t
Ug/kg wetpglkg wet
lgy'kg wet
Lig/hg wet
Ug/Kg wst
Pg/kg wet
p(y(g wet
Pgr'hg wet
Pg/hg w€t
]ld\S wet
!94q wet
!g,kg wet
ldkg vret
pE(g wet
Ug/hg w€t
Pgilg wel
!g/kg wet
Pg/kg wet
lstitg wel
Pg/kg wet
Igi k9 wet
trg/(g wst
pg/kg wet
Ug/kg wet
UgL4(g wel
Ug/kg wet
USI(S v{et
34_4.16770-13070-13070-13070n 3070-t3070-1307G130
4 0 2
20.9't9 7
20.9
19.8
20.9
19.2
1 U
1 5 1
30.730.52E.129.1
16.3
15.6
1 8 7
19_7
20.3
20,0
20.1
20.2
20.5
15.2
15.9
17.4'18.7
1 6 . 1
r 4 5
1 9 9
17.4
18.9
18.6
19.9
1 9 . 1'r9_4
20.1
20.0't 9.5
2 0 4
1 9 7
1 9 8
17.7
18.3
18.4
1 6 4
19.8
14.2
19.7
20.1
40.020.o20.o20.020.020.020.02620030.03n_03003n.0
20.02 0 020020.020.02 0 020_020-020_020.020020.020_020.020.020.o20.020.o20.020.020020.020.020.020.020.020.020-020.020.020.020.020_024.020.020.0
50
5050
50
?5?5?5
50
2525
50
2525
25
100 70,130
104 70.130
98 70130
104 65.3-130
93 7G130
104 70-130
96 70.10
92 70-130
76 U-155
102 70-t 30102 7G13094 rG13097 70-1m
82 7O-13O 7
7a 1.77-175 3
94 70-130 8
98 70-130 18
1O2 70.130 4
100 70-130 8
100 70-130 1
101 7G130 4
102 55.3.136 1
76 38.8-142 5
80 70-130 4
67 70-13) 6
94 7G130 2
00 7G.130 12
72 70-t34 7'f 00 70-130 2
87 55.3-130 12
94 7G130 4
93 70-130 11
100 7G130 1
96 70-130 4
97 70-130 1
100 64.7-i39 4
100 70-130 7
98 70-1$ 5
102 70-130 1
98 70-130 4
99 70-130 3
'l,1Olt{oroenhane
l,zoicfilaroethane1 ,l {)lchloroetfteneci8-i,2-Dichloroethenet€rls-1,2-0ichloro€thene| ,2-Oit oropropans'l ,Sohhloro0rcpane
88
s29282999198100
't4
6
6
3
5
6
Thit labo.atiry rcport is ttot ralu x'ith4t 4n aurhorlzel signarsn on the coeer psge
'Reportable D€tection Limit BRl-: Below ReFor.ing Limir Pzee 107 of 165
Page 617
Volatile Organlc Compounds - Quality Control
Anaba4s) Result Ftag Unir.s +RDLSpike sourc€ '/"REC
kve I Result '/"REC Linits RPD
RPD
Limit
Brrcl7011642. SW8,t6 50J0 So (hign kvet)
LCS Dup lIXll6a2€SD1 |
Prepar€d & Anav:€d: 27+rar{7
2,2-OictUorcproFdt€
1 ,1 {)ichlorcprop€ng
cis-1,3-Dk$lorof mpene
bans- 1,3{icib@prop€n€
Etrylb€nzene
Hexachlorob|Jbdien€
2+lexanon€ (MBK)
lsopropy'tcnzsn€
4-lsopropyltoluei6
M€lM brtbut'4 elh€r
4{r.l€ttryl-zf €nrsnono (M|aK)
MethMene d oride
Naphthalefle
n+mpylbenzene
Styr€ne
1 ,1 ,1 ,2-T€tlachldo€lhaneI , I ,2,2-Tet'achloroetheneTel,€dftroethen€
l,2,STrichlorobenzene
1.2.4-'Idcilorobenzene
1 ,1 , 1-Td.filoro€trane
1 , I ,2-Trichbro€han€
Trichlofir€thene
Trictioronuoromethene (Freon .l 1 )12,$TdchbrcFltspsrte
1,2,+Trimehylbeozene
1 ,3,tT.im€f|y'b€{rzene
m,p-Xyl€ne
o-Xyl€ne
Elhyl6ther
T€rt-€rnyl m€thyl €th€r
Ethyl ted+u[,] €ther
Diisoptopyt ether
Terr-Bl,tanol / hnyl €lcohol
1,4-Dbxane
Sutrogeb : 4 -*o nofl uor6e nzen eSu'o9ate: Toluene4SSunogale: l,2-Dicl orcelhane44S u trogde : D ibronDfl uo rcmeth ane
IahixSolke flCllA|2{S1l
Ptcpafed A Ansl]r:ed 27-[4ad7
Benz6n€
Ct{orobeaz€n€
1,1-Did{oroethene
Toluen€
Trichloro€her|e
I u nWaE : 4- Btc,rof, uotobe nze neSufiWate: Td@n048
13_9
182
18.0
17.9
18,8
13-5
17.8
14.2
19.6
16.9
17.?
19.2
15.7
2 1 . 5
19.4
19.7
16-4
17.9
19.4
18.7
15.8
20_4
19..1
r4.8
22.5
19.2
19.6
15_9
38-8
20-4
1 8 . 1
19.3
19.3
19-9
18.3
108
183
30.729.727.928.8
Sour6: SAsgli4St)2
22.a23-4
23.230.131.9
Igr'kg wEt
lrg/kg wet
lgts wel
ldkS wsl
Ugfrg Yr€l
IdkS vr€iOCI pg/kg wet
USikg vr€lpgrkg welggtkg w€t
Ugkg rvet
trgrlq w€t
trg^g wet
|lgag wel
lrg'l(g urel
lJgkg YY€l
lgr'kg rv€t
lrgikg wet
rcrrkg yr€t
pgts wel
ldrg w€l
tdkS wet
lgdkg wet
lrgrkg wet
lgr'xo w€lpdkg si€t
ldks wel
Pg/kg w€tpdkg wet
rc4(g wet
Fglkg w€(pgks w€l
Pdkg vr€tyg4(g rvetygr'kg wet
Lrg/ko w€l
Pgukg wol
ldtg wel
lgl(g rrett dkS w€tPgr''llg ''stLrdkg wet
ldks dry
YSftS dry
tlg/kg dry
uS/kS dry
Ug/tg d.ypdkg dryudks dry
70 70-130
9't 70-130
90 70-130
90 70-t30
94 70-t3)
88 60.7.14068 70-130
89 7013091 7Gr309E 70-130
u 46.1-14588 70-13096 7G1307A 70-130108 70-1309t 70-13n9B 70-13082 7G1n90 7G.r 30s7 70n3094 7G13079 70-130ro2 70-13096 7G13074 56.&140112 7G130s6 7G1309a 70-13080 7G13097 7G130102 70-13090 70-13096 65.113096 m.130100 7613092 7{rr3t)94 7G13092 34-155102 70-1349S 70-13093 TUlg96 7Gt30
774 70.130tl7 70-1xo110 71t130116 7{ll3t)116 70-130101 7G130106 70-1fi
20.020.020.o20.020.020.o20.020.020.020.o20_020.om.020.020.o20.o20,0m.020.o20.020.0200m.0m.o20.o20.020.020.o20_o40.020.020.020.o20.0z).0m.0200200fr,o30.o30.o30.o
20.020-o20.020.020.030.030.0
BRL
BRL
BRI
BRL
BRL
8
7
s52
1 1
7
8
23I
7
8
7
6
1 3
5
2
21
3
2
I
3
2
1 9
25
25252550252525
5025252525252525252525252525502525252525252550252525
This btordorf rqofl ls Dot ealld wilhoar an aulrotizpd sig,tot . on tfu .otct pege.
' R€portable Detcdion Limit BRL = Betow Reporting Limit Page 108 of 165
Page 618
Volatile Organic Compounds - Quality Conarol
B{tch 7031642 - sw846 s0l0 soil (trigh level}
llaHx Solk 17031642.frslI Sourcs: SA5S54tu2Prepared & Anal]/2€d: 27-Mar-07
swrcgate: 1,2Dlchlorceth ane44S urcg ate: Dlhrc n ofl u o rc m et h a n e
28.029.0
2 3 022.822422.622.930.131 .227.529.1
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
ARL
ARL
ARL
aRt
ARL
BRL
BRL
BRL
BRL
SRL
BRL
BRL
8RL
BRL
BRL
ARL
BRL
ARL
pg/kg drypdkg dry
!g/kg dryyg/kg dry
ug/kg dry
udks dfyps/}g drypg/kg dryug/kg dryudkg dryUS/Kg dry
30.030_o
20.020_020_020.020_030.030030.0300
BRL
BRL
BRL
BRL
BRL
0.93232
3030303030
93 70-13097 70-130
115 7G1 30
114 70-130'112 70-130
113 70- r 30
114 70-12t
100 7/qi13o104 704m92 7n4m97 70-tn
Iabix Spiks Duo ft031642+aSOl) Sou.ce: 3A59545-02
Prep€red I Anatyted: 27-t\,tar-O7
B6nz€ne
ChloaoberEeno
1 ,1 Oichloroelhene
Toluene
Suftcgato : I -B ronollu o ro b e n zen eSufrcgate: Toluene-d8S urcg ate : 1, 2- Dldt I orc eth a ne 4 4Sulog a|E: A b twno fl u orom e th ane
Brtch 1l3l55E - SW846 5015A Soll (low level)
Blrnk 17031658€LKl I
Preparod e Analfzed: 27-l\4ar.07
1 .1 ,2-Trichlorotriffuoroethane (Freon .l 1 3 )
Acrylonltril€
Benzene
Blomod*rroft€han€
Bromodichbrom€thane
Baomotorm
*o''oflr€thg'l€
2€utanon€ (ltlEK)
n€utylberEene
secguty'benzene
lert€uvbenu€ne
Carbon disuttde
Carbon lehachbrii€
Chlorob€nzene
Chlo@etiane
Chlorofodm
Chlolornehane
24hlorobluefle
4-Chbroblusn€
1 2Oibrcnrc-3rhloropropan€
Dibrottodrloromethane
l,2olbromo€than€ GDA)Dibroflronelhane
1 ,2-Didbrob€nz€ne
1 .St)icnbrob€nz€n€
1 ,+Oitrbrotlenzene
Dld orodnuddiet'hane (Freonl 2)
I , l -Did*rroetlEne
I ,2-Oi{Storoeth6ne
I,l-Dic* oroettEne
cis-l,2-Dicihruethen€
ban$l.2Oichlof o€thene
IrgL/kg wet 5.0
lgL/kg wpt 100
pgr'kg wet 5.0
!g/kg w€t 5-0
lqr'kg wet 5-0
pS/kS Yret 5.0
!g/kg wet 5.0
!g/kg 'ret 5.0
tgr'kg $et 10 0
pgr'kg wet 50.0
lgr'kg w€l 5.0
!g/kg wel s.0
lgy'kg wer 5.0
lgr'kg wet 25.O
!g/kg wet 5.0
pg/kg wet 5.0
!g/rg wel l0-0
pg/kg wel 5 0
pg/kg wer 10.0
aJglkg wet 5-0
pg/kg wet 5-0
!g/rg wet 10.0
pgrlq wet 5 0
pg/kg wet 5 0
pg/kg wet 5 0
!S/kS wet 5-0
!g/k€ wst 5.0
lgr'kg wet 5.0
pg/kS \,Yel 10.0
fg/kq vrer 5.0
Pqrkgwel 5.0
!g4q lvet 5.0
pgr'kg w€t 5.0
pg^g wel 5.0
Th'J lzbotuoFr Eport k not volid withour s!. suthori<ed signa/aft on the cover page .
r Reportable D€t€ction Limit BRL = B€low Reporting Lhrit Page 109 of 165
Page 619
Volrtile Orgrnlc Compourds - Quality Cootrol
Analytds) RBult Flug RPD*RDLSpik€L€vel
Sourc€Result
%RECLimits
RPDLirrut
Bstch 7031658 - SW846 5035A Soit oow tevet)
Blank 1703lcfA€L(ll
P.epar€d & AndFed: 27-lrar{7
I ,2-Dichbropropan6
1,'Olchloropropan€
2,2-Didrloropropane
1 ,1 Oichbroprop€ne
cis-1,3-DichloroFropsn€
trans-1 ,3oicuorcplopofle
Et'ry'b€rEene
Hexachlombuladiene
2+leEnon€ (MBK)
Iropropylb€nzsfl€
illsopropytEtlue{€
Methyl isrr-bu!/| €ther
4-!rehyl2f enlanone (M|BK)
tirethy'en€ .fitor*le
Naphlhalene
Styren€
1, 1,1,2-T6H o.oelharNe
1,1,2,2-Te{rad oroethane
Tehachloao€lhon€
1,2,$Tri*rlorobenzene
1,2,4-Tdcnbrub€nzene
1,1,1-Trid oroet'€ne
| , | ,z-Trichlorogthane
Trid oro€th€ne
Trichkrrofuoiom€thane (Freon I 't )1 ,2,lTn.filorcprcpan€I ,2,4-Tdmefr/benzane'1.3,$Trimethylb€nz6ne
Vinyl d odde
m,p-Xyi€ne
Tefdrydroturan
Elnyl€ther
Tert-anyl msthyl ether
Ethyl terl-buy €ther
Di+opropyl €th€r
T€rt-Butand / tuty' abofrcl
l,4oitxEn€
S uft ogale : 4+}.c monrcrcbe n E n eSunqate: fohJ€ne4oSu/'og E te : l, 2 -Dkhl ofoelh a N4 4S u fl ogate : Dlho nofl uoron eth dE
LCS 170:lt6s8€St)
Pr€{'arbd & AnatEedl 27-Mar{7
1,1.2-Td$bro fuoroet'ran€ (Freon t 13)
ActYonifl€
Benzene
8RL
BRL
BRL
BRI.
BRL
BRL
SRL
BRL
8Rt
BRL
BRL
ARL
BRL
ARL
BRL
BRL
BRL
BRT
8Rt-
BRL
BRL
BRL
BRI
8Rt
BRLgRL
BRL
BRI
BRL
BRL
BRL
8RL
BRL
ARL
BRI.
BRL
SRL
BRIgRL
BRL
49_249049.750.8
15.6
10.4
21.4
17.1
1g-7
t g/t€ wetpgtg wetpgr'kg w€tpdtg ret
Igkg uret
!g/kg v,/ol
t SftS ',v€t
ldkS rrer
trdkg d
!94!g w€t
Ugr'kg w€tpdkg w€t
ldtS w€tpgL/kg wet
lrdkg w€lpgl(g w6lpdkg welgL/ts vJet
pgl€ wet
!g/kg welpdks lv€t
ugts Yrel
UdkS v.,et
t g/kg we{
ugAg welpg[ts wcl
usas wet
lglq wet
w/t!g wel
Wr'kg wel
lgkg Yr€l
Lr€/kg re€t
!dl(g v,/et
Fdks wer
tigts w€l
lgtS Yrelpgkg wet
Ugfl€ wEt
Idkg w€l
Ugy'kg wet
ligts YJ6lIdkS wetpg/l(g wetIgr(1g w€t
lgL/kg w€tpgl(g wet
lgkS w€t
lgkg w€l
lgrkg w€t
70-1fr70'13070-13070-130
70.130
1.77-1757G13070-13070-130
5.0
5.0
5.05.05.050.0
5.050.050.05.0
5.05_05.0
5.05_05.0
5.05.0
5.0
r0.05.050.o5.05.05.05_0500.t00
50_o50.050.050.o
m,020.020.020.020.0
9899102
7A
109
869a
Thk labnh,r Epod is ,tot valid *ithour aE aat*orizd funaote on the covu page .+ Reporrable D€teation Limit Bht = Below Reporting Limir hge I l0 of 165
Page 620
Volatile Orgenic Compounds - Quality Conlrol
Spike
Level
Source
R€sult
RPDLiflit
%RIC
%REC LinritsAnalytqs)
Btach 7031658 - SW846 50lSA Soil (to\r l€!e,,
LCS f/0fi658€S
Prepared & Analyzed: 27-Mar{7
Eromoct{oro(l|e[|ane
Brdnodi€hloronethane
Srornofofm
Bromornelhane
2€utanon€ {MEK)n€uVb6nzene
sac+utylb€nzen€
bd-Butylbenzen€
Cerbon dtsulfid€
Carbon btschloride
Chloob€nz€ne
Chlo.oelhan€
Chlomform
Chlorom€th€ne
2€hlorotoluen€
4.Chbrotoluon€
| 2-Dibrom+3.chloroprcpane
Dikomochlo,o.nef|ane
l,zobmmoelhane (EDB)
Dlbromorr€t|sne
l r.oic+ o.oberusne
I ,+Dichlorobenzen€
| ,+Dichlorobenzene
(Frcon12)
20.6
14.2
23.3
21.3
14.5
14.7
16.6
17.3
1 5 3't4.6
19.2
1 8 0
1 8 . 1
16_6
17.6
1 7 6'19.6
2 0 1
20.4
1 9 . 7
1a.a
19.5
1 7 . 5
16.0
17.0
r 7 . E
1 5 2
19.0
r7.0
14.4
1 9 . 1
1 4 . 1
15_2
1 6 8
16_9
1 7 _ 4
15.2
13.7
16.2
16.3
19.2'18.3
17.0
20.0
16,4
19.2'r 9.5
20.8
1 5 8
17.0
20.1
20.020_020.o20.o20.020.o20020-o20.o20.020.o20.020020-02 0 020.020.020.020.020.020020.020.020020.020.020.o20.o20.o20.020.020020.o20.o20.020.o20.020.020.020.020_020.020020.0m.o20.020.o20.020.020.020.o
tig/kg wel
Ug/kg wet
lgr'kg /€t
!gL/r(g wet
Ug/Kg wet
lrg,kg wet
!g/kg wel
Ug/kg wel
Pg'kg wet
!g/kg Y/et
Ugr'kg rvet
pg:/kg wel
!€y'kq wet
!g/kg wel
pSAS wet
lEkg rvet
!q/kg wet
pg/kg wet
pg/kg wer
t4/kg wet
!q/(g wel
Ug&g wel
psrtq r€t
!9,&g w€t
!S.t(g wet
Ligkg wer
!g/kg wet
pg/Kg wel
pg/kg wel
pq/kg wel
Ug4(g wet
pgkg wet
pgr'kg wet
!g/kg wet
Ugy'kg wet
!!/kq wet
!g/kg wet
Oc2 Ug/kg wet
l,g/kg w6l
!g/kg wet
Ug/kg wel
l4/k9 wel
pgks vr€t
!S/rg Yv€t
!q/kg wet
!g/kg wet
Lilt/kg wet
t/gL/kg wet
rcr'kg wel
!g/kg wet
tlg./kg wet
103 70-130
91 70-130
tt6 70-130
106 55.3.136
12 3A.A-142
74 70-13n
83 7G130
86 70-130
76 70-130
73 70130
96 70-130
90 55 3-130
90 70-130
83 70.130
88 70-130
88 70-130
98 70-130
100 64.7,139
102 70-130
98 70-130
94 70-130
98 70,130
88 70-130
80 34 4.167
85 70-130
a9 70-130
76 70-130
95 70-130
85 70-'t 30
92 70-130
96 70-130
70 70-130
76 70-130
94 70-130
94 70.130
87 70-130
76 607-140
6a 70-130
81 70-130
E2 70-130
96 70-130
92 46.1-145
85 70-i30
100 70-130
82 70.130
96 70-130
98 7G130
104 70.130
79 70-130
65 7G130
100 7G130
1 ,l Olchlorc€thane
I ,2{ichloroet'rans
1 ,1-Dichloroethene
ds-12-Dichltroethene
lr3ns-1,2oichloro€lheoe
l,2oichlo.opropane
1 ,3-Dicfilo.opmpans
22-Dichloropropane
|,|.Dii:l oropropene
d9'l,$Oi:hbmpropene
ttans-l,3.Did oropropene
EtMbenzene
Hexachlorobutadi€n€
2-He)6none (MAK)
hopropylb€rEene
4{sopmpyltoluerE
lroihyl ted-butyl efr\€.
4+vlethyl-2{€ntamne (M|aK)
liefiylene cfilorit€
Naphtrabne
n€ropyfio6nzefle
Stfen€
I,1,t.2-TelracfilotDethane
l,'1,2,2'l6Factrloo€thane
Tet'achlorcethen€
Toluene
l,2.ST.ichlorobenzene
Thit lohorulory rcpor1 is noa valid without an aathoiaed signelare on ahc cover page .
* Reporlabl€ Ihection Limit BRL = B€low Reporting Limit P a g € l l l o f 1 6 5
Page 621
Voladle Organic Compounds - Qurlity Control
Brtch 70315s6 - SwM6 5035A Soil (low t€vet)
LCS 1703165r€Stl
Preparcd & Analyzsd: 27-Mar.07
1,2,4-Trx$lorob€nzene
1 ,1 ,1-Trid{ormtiane
1,1,2-Tridrloroethane
Tichloro€then€
Td€ilorofl uorofi*fEn€ (Freon 1 1 )1,2,3-Triciloropropan€
12,&Trifiehtbenz€ne'l,3,5.Trime$lylbenzene
Vinyl chlorid€
m,Fxyl€fle
Terahydlofurm
Ethyl elher
T€rt-€rnyl rnehf emer
Ethyl bri+uv ether
Dl+opropyl elh€r
Ted.Butanol / buv Elc.hol
1,4{ioxane
S u rDga/€ : 4 -Eto iafurc ro b en ze rcSurqate: Toh.Eno4|SufirBatg : l,2aichbroethane44Su''ogale : Dibro'''ofr u o Mn e I h ane
LCS Duo fio:ll65t€SD1l
Prepared & Aoalfied: 27-ttar-.07
1 ,1,2.Trid*rrc,ffiuoroeftme (Fleon | 13)
Ber|zen€
Eromocl oromOtiane
Brornodichloromethanegromoform
Erornofirethene
2€utamne (MEK)
n€uVlt)€nz€ne
sec.Butybenzen€
brl-Butylbenzene
Carbon disunde
CErbon tetad odd€
Chlo,obenzon€
Chloroelhan€
Chloroform
Cl ororn€thane
2Chlorotoluene
44hlorsbluen€
1,2€ibrcmGldtuopropane
Dibromocfi toaorhe(rane
1 z.Dib'omo€trlane (EOB)
Dlblonom€tran€
1 2-Dichlorob€nz€ne
1 ,3-Dichlorob€nz€fls
1E,315.2m.o16_6
14.0
22.O
14.2
17.6
17.3
19.0
20_o
20,9
16.0
18.6
17.6
14S
0.0
49_54 9 146.949.6
't 5.9
10.1
19.7
17.4
20.2
19.4'16.3
22.O
1 8 I
13.2
r 5 3
17.2
t8.0
15.7
11.7
19.6
17.7
18.2
16.6
18,1
16.1
r8.0
19.7
1S.8
18.8
18.3'19.6
20-020.0m.o20.020.020.o20.020.020-040_020.o20.020.020.020.020.02002650.050.050.o50.o
20.020.020.020.020.020,020.020.020.020.020.020.020.020.020-020.o20.0m.0m.020.020.o20.020.020_o20.020.o20.o
pdkg wel
pdkg Yr€t
ldkS y/et
UgkS {,et
Igl(g vYet
|rg € wet
lqkg w6t
l4y'kg wel
Ugkg wel
IS/kS ri,€l
pg/kg w€t
pg4(S w€t
!dl(g rvet
Lidl(g wet
IdkS wet
lgftg wet
pg/kg w€iclc2 !g/kg w6l
|lg^g welISrkg tvel
ldkS rrerpdrg vret
Ug[tS v,,et
IgkS vJet
lgr't€ we{
Ug/tg wet
pgikg wet
!g/kg rr€t
uSftg wel
Uqkg yiet
pdts yret
ldkS wet
ldkg vret
!gL[(g w€t
lgr'kg vJet
pgil€ w6l
Ig/kg w€t
pg/kg wel
lCftS YY€l
lqrg Yiet
Pgr'Ig w€t
Pg/kg wet
Fgtkg wet
pdkS v{et
#gfilg wet
Ugr'kg wel
Ugr'kg wel
Ig/kg wot
pdks w€l
92 70-13076 70-130100 70-13083 7G13070 5{t.E-140110 7Gr30
91 70-13088 70-13086 70-130
8S 70-13095 7G130100 70.130104 6s.113090 7G13093 70-13088 70-13t)74 70-130
34-15599 7G130
7G1N94 tF1fr99 70'131)
80 70-130 3fi 1.77-175 498 70-130 1187 70-130 1f01 70-13D 397 7G130 692 70-130 1fio 7G130 594 55.1136 1266 3a_&142 I76 7G13t) 386 7G't 30 4s0 70-130 57A 70-130 374 70-130 198 70'l3O 288 55.3-130 291 70-t30 |83 7Gr30 090 70n30 290 70-130 2so 70-130 Is 64.7-'139 299 70n30 394 7G130 492 TGi30 298 7Gr30 0
255t)25252525252550502525252525255025252525
50
Thb lzbodory ftpod ls ^o, eolU wiLhar/r tn dathotizrl slgnatarc on rte cover page .
. Reporreble D€rection Limit BRL = Below Reporring Limit Pagp I 12 of 165
Page 622
Volati le Organic Compounds - Quality Control
Spike
Level
SourceResult
%RF-C
Limits
RPD
LimitAnalytqs)
Birct 7031658 - SWE{6 5015A Soit (tow level)
LCS D(o f/O3l65€-BSOt I
Peparcd & AnaDzed: 27-MaF07
l,+Di{ibrobenzsne 18.0
(Freon12)
17.2
17.5
15.3
19.0
17.2
1 E . 6
16.4
1 4 4
15.4
18.5
1A_2
1 8 . 1
1 5 1'12.1
16.8
1 6 9
1 9 . 1
1 7 2
17.9
1 7 8
16.9
1 9 6
l 9 2
2C.O
1 6 2
1 1 1
18.4
17.7
1 5 6'19.2
1 6 8
14.3
21.9
1 8 3
r 8 0rE.236.5
1 9 3
17.9
19.5
1 7 1
18.6
l7.8
127
0.0
49.749.144.7496
1,1-Di.fibroerhane
l.2Oichbro€than€
l,lOicnbro€thsn€
cis.1 ,2-Dlchlor€tt€n€
trans-l,2olchloroethsn€
1 ,2oichloroprcpane,',3ol*|broprcpane
2,2.Didbropropane
l,lOidloropropene
cis-l ,!IH orcpropene
bans-1,3-Dichlo,ropropene
Ethylb€nzefi€
llexacHorobt Ladiene
2+€x8none (MBK)
4-lsof{otryltoluen€
t erhyl led+uty' ether
4-Methyl.2+enr,anorle (MtAK)
l.kry€n€ d{oride
Naphtrlalene
nPropy'b€nzene
StFene
1 ,1 , t.2-TeE&hlorcethane
1,1,2,2-Teir,(j*.rcethene
Tetrad oro€thene
Tolu€ne
I 2.STndrlorob€nz€ne
1 ,2,+Trid oroberEene
|,1,l-Tridrloro€thane
1 ,l ,2.Tnchbroetrane
T.ld{oroethefle
Tridrloro{uo$m€hane (Freon 1 1 )1 2.ST.id oropropan€
1 2,4-Trifir€thy'b€nzene
I,3,'Tnnr€ftyb€nzene
Vinyl ct{oride
m,Fxylene
o-Xylan€
Tetrahydrcfuran
Efryletr€r
T€d-erv m€Ury' €lfi€r
E6ry' bd.buty' €r'€r
DHsopropyl ether
Ted-Buranol / butyl alcohol
l,r$ioxEne
S,J'logate: 4&onpfutarobenzeneS|jl7wate: Toluene4SS|j'7ogate : 1,2 -Dichl oroo I h an e4 4S{//Iageta: Dibrutnfluorcfiethane
%RTC RPD
lig/kg w€l
lg(g w€l
IgAg wetpgftg wer
F94q wer
!gl(g vi,et
pdkS yJet
pS/kS yr€t
!g/Kg wst
lig/kg wet
lEkg wet
!Et($ wet
!g/t(g wet
Ug/kg wet
psrlkg wet
OC2 pgr'kg wet
ugkg wet
lgr'kg w€t
Ug/t(g wel
!g/t(g wel
[g/t!g wel
lgi kg wel
!g/kg wst
Fg/Xg wel
ugt(g wet
gglkg wel
trg/kg wet
lrg/kg wet
ug/kg wel
ug/xg wer
pg/kg wet
ug/Kg wel
pg/kg wel
ugfto wel
IEt(]g wel
lgkg w€l
Ugt€ wel
trg./Kg wel
lrg/tq wet
tgkg wel
|l(yKg wel
|l!r/kg wet
Ugi/Xo wel
pgdK$ welpgLi kg wet
clcl FgLnlg wet
oc2 !g/kg wet
LigL/kg n et
Lidtg rvet
ugL/kg wet
lgxg wet
90 70-13083 34.4-167 4
86 70-130 1
88 70-130 1
76 70.130 0
95 70-130 0
86 7G130 '1
93 7G130 1
92 70-130 4
72 70-130 3
77 fO-130 1
s2 70-130 2
91 70-130 3
90 70,130 3
76 60.7-140 0
60 70-130 12
84 70-130 4
84 70-130 2
96 70-130 0
86 46_t-145 7
90 7G130 6
89 70-130 12
84 70-130 2
98 70-130 2
s6 70-130 2
100 70-1K 4
61 70-130 2
86 70-130 1
92 70,130 E
68 70-130 4
78 70-130 3
96 70-130 4
84 70-130 1
72 56.8-140 3
1' t0 70-130 0
92 70n3O 1
90 70.130 2
91 70-130 6
91 70-130 2
s6 70-130 1
90 70-'130 11
98 65_3-130 6
86 70-130 5
93 70-130 0
89 70-130 1
64 70-130 14
34-155
99 7113098 70-13089 70-13099 70-130
20.020.020.020,o20.02 0 020020.020.o20.020.020.020.020.020.020.020-020.o20.020.020_020.o20.020.020.020.020.020.020-020_020.020.020.02 0 020.020.020.020.040.020.020.020.o20.020.020.020020050.o50.050.o50.o
255025
252525252525252525255025252525502525
252525252525252525
502525252525
2550
2525
25
Ihb ldton/ory repod it fiat vdlid wirtau! oE sattoriz.d sigttstzrc n rte cos.r page.
' Reportable D€tection Limit BRL = Below Rqnaing Limit Page I L3 of 165
Page 623
Volatile Orgauic Compoutrds - Qurlity Control
Analyte(s) Result .RNLSprkeI*vel
RPD
LimitFlaBSource %RECResuft o/oREC Limits RPD
Barch 70f1693 - SWE{6 50JSA SoI (low tevel,
Bl.nk O031693€LKl)
Preparod & AnalFed: 2&L,lar47
t,|,2-T.idlorotifluoroethane (Freon 113)
B€trz€ne
B@mob€nzene
Bromocfilommethane
Bromodichlororn€trune
Brornoaom
Bromom€hane
2€uianoo6 (nrEK)
n-Eutylbenzene
sec€utylh€rEene
lerl€ulYbenzen€
Cerbon dF{lfde
Carbofl tretachloiide
Chlorobenzene
Chloro€than€
CHo@foan
Chklrornethane
24hbrobfuene
4-Chbrololu€ne
1 2-Dlbromo-3d$ropropan€
Dibromd$orom€thane
1,2-Dibromo€lhan€ (EDB)
Ditnomorn€ihsne
1 .z.{)itrlorcb€flz€ne
1 ,3Ol* orobenzene
1,4.Dk$loroberEene
(Frcon12)
BRL
BRL
BRL
8RL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
aR[
BRL
BRL
ARL
ARL
BRL
ea|.BRL
BRLARLSRLBRLBRLBRLBRL
ARLBRL8RLBRL
8Rr-8Rr_gRL
BRLARLBRL
pg/kg wel 5.0pgr'kg wel 100pg/kg rrel 5.0
ldkSw€t 5-0pgl€wet 5.0
Ig/kg rvel 5.0pC&g v/el 5.0
lgr'Xg rcl 5.0
lgr'kg v/et 10.0pgr'kg wet 5O.0pg/kgwet 5 0
lgr'kg wst 5.0pdtgn€l 5.0
|lg^g Yret 25.0pgL/kg w€t 5-0
t grkg wet 5.0
Fgr'kg vr€t t0-0pqrg$,el 5.0
!g/kg $€t 10_0
trdkS rvet 5.0pg/kgwet 5-0
Ug/|!gw€t 10.0pdkg wet 5.0
UdtS rrel 5.0
u€/kg wet 5.0
lgkgwet 5.0
FS/kg r{el 5.0
lig/tS wet 5.0pdl(gw€t 10.0
ISAS vrel 5.0
lgrkgwe't 5.0
t glkg wet 50pgtgw€l 5.0pc/kg lr€t 5.0pgftgw€l 5.0pdkS lvet 5.0
lgr'kg wet 5,0
tEAg wet 5.0
UdkS wel 5.0pgls r€l 5.0ggr'kg ri€t 5.0
lgL/kg wet 5-0
!g/t€ $/et 50.0
Fg/kgwel 5.0pgtgwel 5.0
lgr'*g wet 5.0
tgn(g w€t 5O.0pgr'kg wet 5O.0
ldkgwel 5.0
Pglkg ' €t 5.0
Fg (gw€l 5.0
| ,1oid{orc€thane|,2-Di.trloroettBne1 ,1 -oid oroethenecis-1,2.I)ktrloro€lhenetans-l,2Oichbroelhen€| ,2-Di{tioropropane1,$Otd{orog(opane2,2.t)it* oropropane1 ,1 .Dicilorop(opsn€
cts-|,$Di{t oroDrop€nelrans-1.3-Dldrlof opropen€Etryll}qnz€n€H€xacttorobltadien€2+lexanon€ (MBK)lsop.opylb€nz€ne4-lsoproFyltolugneMe$yl t6 +uV efi€r{-r,a€tnY.2-penhnone (M|aK)Mol,hy'€rE chbrueNephdral€nen-PropylbenzeneStyrene
TLt labratory rqorl it rot vdht wilhou an authorizty' lnt''dla'? oa 6a cavct pagz -
. Reportlble D€tcction Limit BRL = Below Repoding Limit Page I l4of 165
Page 624
Volatile Orga[ic Compounds - Quality Control
Spjke Sou.ce %REC RpDAnab't{s) Resulr Ftag Units +RDL Levet Resutr %REC Limirs RpD Linit
Edch 7031693 - SW846 5035A Soil (lo$ t€veu
Bh* 1703t€93€LXll
Pr€p€r€d & Analf.ed: 28-Mar-O7'1 ,1 ,1 ,2-Tetrachloro€lhane1 , 1 ,2,2-Tebachloro€lhaneTetlacftloloett€n€
1,2,lTricilorobenzen€
1,2,4-Tricfi lorobenzene
t ,1 ,l -Triciloro€rhane
I.|,2-Trid oroetEne
Trichloroetheoe
Trichloroff uoromehene (Freon 1 1 )1 ,2,STrid oropropan€
1,2.+T.imsflyltenzene
1,3,+T,imetnylbenzene
m,p-Xylene
GXYI€n€
T6hahydroturan
Elhyl etnel
T€.|-€myl methyt €ther
Ellhyl t€d{utt ett'€r
Di-isoproPyl elher
Tert-gulafiol / buv atcohot
1.4{ior€ne
Su fl og ate : 1 -Btoolofl u o ro b enze n eSulroga/€: Toluene4ASutr9gat9: |,z-Dichloroeth ane44Sunccale: Dibtotnffuoroneth ane
LCS r781693€S.tt
Pr€parod & Analt/.zedi 28,Mar{7
1,1 ,2-Tric*{ootrifluoroethane (Freon 1 1 3 )
Ac|yionible
Benzeie
Ercrnobenzene
BEmochloaorhelhan€
&olr|odichbromethane
Brcrmform
Bradrom€trsne
2€utanon€ (MEK)
n€ailylbenz€ne
3ec€uMbenz€n€
brt€urybenzen€Cetbon disumde
Caabon tgtrachloalde
Chlorobenz€ne
Chldgehan6
C.t ooform
Cl orom€lrrane
2.Chlo,robluerE
+4hb.obluefle
1 2-Oft mmo-kfi lo$propane
ORL
BRL
BRL
SRL
BRL
6RL
BRL
BRL
BRL
ARL
ARL
ARL
BRL
BRL
BRL
BRL
ARL
8RL
BRL
BRL
ARL
ARL
ARL
49.65 5 953.2
21.O
1 4 2
19.8
1 9 3
20.9
1 9 . 8
207
21.3
2 0 9
15. '1
19.2
19.7
19.9
20.2
18.8
20.a
18.5'19.6
21.8
20.a
20.3
20.3
50.050.o50.o50.0
2n.om.o20.020.o2 0 020.020.020020.020.020.020.020.02 0 02002002i.o20.o20.020020.020.0
lgr'kg w€l 5.0
PEkg wet 5-0
Ugr'kg wet 5-0
!g/kg wet 5.0pg/kg wer 5 0
!g/kg w€t 5.0
lqkS w€l 5-0
pqr'(g wet 5.0
LigL/kg wet 5.0
t,gkg wet 5 0
!g/kg wel 5.0
pSn(gw€t 5.0
!g/kg wet 5 0pg/kg wet 5-0
Lrgkg wer 10.0
lrgl(g wet 5.0
lgr'kg w€l 50 0
ligL/(gwet 5.0
pg4(g wet 5.0
Lig/kg wet 5 0
Ug/l(g wel 5.0
!g/kg we( 50.0
pg/kg wet 100
lrs/ts wet
!S/kS wet
!gl(g wetLig/kg wet
pg/kg wel
Pg/kg w€t
!g/kg w€t
!g/kg wet
pEKg wer
trg/kg wet
t g/ko wet
!g/kg w€t
ljEr€ wet
lgr'kg lvet
!g/kg wet
lgr'kg wet
UgL/kg wel
pg/kg wet
lgr'kg wel
ug/kg wel
ps/ks wet
!g/kg Y/st
!g/kg wet
!g/kg wet
!g/kg wet
pq/kg wet
89 70-13099 70-130112 70-tm106 70-130
105 70-13071 1.77-17599 70-130s6 70-130104 70-13099 70-1:'0104 70-130106 70-130104 55 3-13676 38 a-14296 7G13098 70-130100 70-130101 70-13094 70-130104 70-13092 55.313098 70-13010s 70-r 301M 70-130102 70-130102 70-130
Thh laborarory Epad it dot vatial *tlhoq! on aathofiaed signafuE on the cover page_
+ Reportable D€cction Limit BRL = B€low Reoortins Limit Page I l5 of 165
Page 625
Volatile Organic Compounds - Qurllty Cotrtrol
4I4f,"(") Result Flas unirsSpike
lrvelSoulce
Result %EEC Limits RPD
Brtch 703169J - SW846 5035A Soit oow levet)
LCS r703t6g3Astl
Prepercd & Anslyzed: 28-Mar-07
Dibromochboriethane
|,2{ibromoefiane (EDg)
DibEmorn€lhan€
I,2-DiJ orobenzene'l,3{)i.hbrDb€nz€ne
l,4Olchb.obsnz€n€
Dic.itlorodinuo.om€then€ (Freonl 2)1,l-Dichloro€thane
1 2Oichloro€thane
1 .l-Dbhloro€thene
cis-l,z-Did oroetheno
trans-1,2-Dicfi lorBthene
I,2.{)ichlorcpropai€
1 ,SDli oroF opan€
2"z-Dbhloropropane
1 ,1 OichloroproFene
cls.l,3.Dic'|loroprop€ne
fr€n9-t,3oia* oroprop€n€
Elhylbenzene
Hexachlorobutadiene
2-l'l€xanon€ (MBK)
lsopaopylberEon€
+lsopropyllolueoe
M€thyl brt+uM ether
a-iretttyl2+s$anone ( tBK)MerhyteGe dtbride
${6phthal€ne
StyYeng
1 ,1 ,1 ,2-T€tachbroet||ane'1,1,2,2-T€trachloro€thane
Tetrd orcethen€
ToluerF
1,2,!Trld or$Gnzene
1 ,2,+Trichbrob€nz6fle1 ,1 ,1 -TddrbE€than€
1 ,1 ,2-Tri6bro€hanc
Tdchhf€th€De
Tridrlorofuorornelhane (F.eon 't 1 )I ,2,&TdchlorDpropaneI ,2,+Tdmetrytb€nzEne1,3,tTlifiEthytbenz€ne
Vhtl dr|o.ide
m,trXy'eneo-XyloneTeLEhyd|!'ftrrdnE*|yl €therT€ri-€my' nethyt €herEhyl brt.butyl gtrtsr
Di-isopropyl ethsrT6.t-ButErd / buty atcotrol
21.6
2 r .620.221.220.319.825_419,019.7tE.4
18.220.420_717 .118-8'r9.6
20.2m.818.017.A19.620.o19.91 9 518.020.3r9.2m.721.620.820.119.720.119.4't s-021.3r9.5r9.8
23.019.819.823.341.1
21 .418.4r9.8la.720.3ts.4tm
!g/rg wet
Ug/kg w€t
|lgl(s v,/etpg/tg wet
rclkg s,etydkS v/st
F9ft9 w€tpglg wet
!g/kg wel
ldkS wel
lgL/kg n€l
!S/kS rv€tpg,tg w€tpgn€ wet
lrg/l€ wet
Ig/kg wetpdts wel
!94q w€t
!S/kg wel
USI(g vr€t
Idrrs rvet
lgrS wet
trykS vet
lrg/lq wetpglkg wetpg^g w€tpgrl(g wetpgkg wel
!S/kS Y{€lgg/kS wet
lgr'kg net
!gn(g wet
tdks wet
Irg/kg wetyg/kg wet
Pgit{g w€l
FdkS wet
ldkg u/el
lgl€ v"€t
lgr'kg w€t
!Sn(S Y€tpSlkS wd
$/kg welpgr€ wet
Igftg wet
lgrkg w€t
Pg'kg welpdkg vr€l
US/kS wel
US/kS w€l
sdkg Yret
20.020.020.o20020-020.o20.0z).0m.0m.o20.020.020.020_020.D20.om.0m.020.020.020.o20.020.020.0m.020.0zJ.020.020.020.020.0z0_020.020.020.o20.0m.0m.o20.om.o20.020.o20-040,0m.om.o20.0m.020.020,02fi
108 64_7-139108 70-130101 70-130'106 70-130102 70-13xs0 70.130127 y.+167
95 7G.13098 70-13092 70-13098 70-13091 70-1I)102 70.130104 70-13086 7G130s4 70-1 3098 7Gt30101 70-130104 70-13090 60.7-14083 70-13098 7G130100 7G130r00 7G130sa 46.1-14590 70"130102 70-13096 70-130104 7G130108 70.130rM 7G130100 70-13098 70-130100 7G.t3097 70-13095 70-t 3t)106 70-130s8 70-1309g 56.8-140115 70.1mso 70-13090 70.130116 7G130103 7Gt3ot07 70-130
92 7{rt3o99 65-913t)94 70n 30102 m-130s7 7G13090 7G130
This lonatuory ..put k not did ,ti hoct on orfrorLd dgr',ohre oE tle cor* Fege.' Repntable k€clior Umit BRI = Bdow R@orting Limit Ptee l l5 of 165
Page 626
Volatile Organic Compouqds - Quality Control
Spike Sourcc %REC RIDAnalyt{s) Rcsult Flag Unirs .RIL L€vel R€sult %REC Limirs RpD Limit
Br|cb 7031693 - SW846 503sA Soit (low levet)
LCS flUltGStAS
Prepared & Ana\zed: 28-Mar-07
|,4-Dioxane
S urqgte : +arc n'0fl u orob e n ze n eS'']'ro,gate: Tolu@e-doS u mgale : 1, 2D bh loroe tt a n e 4 4Su rrogete : Dittn fl nfl u orcm eth a ne
LCS D{o l7(B|693€SiDt)
Pr6pe€d & Analyzed: 28-irar-07
1,1,2-Trid{otofffuoro€lhan€ (Fr€on 113)
Benzene
Bromobenzene
Bromod omm€thane
Brcmodiit*yomet.|ans
Baomofom
BrDmomelhmo
2€uhnone ([rE()
n€utylb€nzene
s€c-gu!y'benzerte
tert-ButylberEene
CE bon disulfide
Csrbon bbachlorxle
Chloobenz€ne
Chlo.oethane
Chlo.obrm
Chlommelhane
24hlorotolu€n€
4-Chlorotoluon€
1,2-Dibrom}3+ o.opropan€
Dibromod oomethane't,2-DibromosthEre (EDB)
Oitromomelhane
t ,2-Dlchlorot€nzene
1,$Okfilorcbenuene
1.+Didrlorobenzene
Did 6odif uorohethane (Freoni 2)
1,1-Di{filord€thane
1,2-Dk hloroethane
1 ,l Oicnbrc€lh€ne
cls-1P-Oid{orceth€ne
lrans-1,2Olctloro€thene
l2olchlo.opronano
I .S{)idrlo.oproFane
2,2-Dic*rktopropan€
| ,l .Dlchktroprop€ne
cls-1,3.Dldioroprcpene
trafl s- l,3-oicibropropene
Ethylbenz€ne
H€xachlorobuladi€ns
2-Hexanone (MBK)
lsopropybenzene
2M
47.250.551.350.3
15.7
19.2
14.7
20.2'19-3
19.6
19.4
21.O
15.3
21.6
19.9
20.6
19.0
202
15.2
18.9
2 2 5
20.4
20_7
20.1
20.0
19.9
20.0
20.6
21.1
19.8
27.O
18.6
1 9 . 5
18.6
19.6
14.4
19.8
19.4
17.1' t9.0
1S.0
19.3
2 0 2
1 9 9
16_0
19.4
Ig/kg wet
pgy'kg wetpg/rq wetpEKg welpExg wel
pgr(g wet
ps'kg v/et
pSkg wet
lgr'kg wet
pg/kg w€t
lgks w€t
tlg/kg wet
!g/kg wet
!Er(g wet
pg/kg wet
!g/kg wet
!g/kg wet
pg/kg wet
Lig/kg wet
pg/kg wet
!g/kg wet
pg/kg wet
trg/kg wet
!g/r(g wer
l.lg/kg wet
!g/kg wet
pg/kg wet
pg4(g wet
pS,4(S wel
pEr(g wet
pg/kg wet
pdks wet
pdks yvet
Fg{kg \,,/et
pdkg wet
pg/l(g \4,et
pqL/kg wet
pgkS wer
lg/kS wer
Ig/kg w€t
pgL/kg welpErq w€l
!g/kg wel
Ug/kg w€l
Ugftg wel
pgftg wel
pq/kg wet
t g/kq wel
lrg/Kg wet
20050.050_050050,0
20.020.020.020.020020.o20.020020020.020.o20.o20.020.o20.o20.o20020.o20020.020.02 0 020.o20D20020.020.o20.02 0 020.020.020_020.020.020.o20.02 0 020.020_020020.020-020.020.0
1O2 1415594 70-1fr101 78130103 70-130lDl 70-130
116 70-130 1078 1.77-175 Is 70-130 394 70-130 2101 70,130 396 70-130 398 70-130 697 70-130 I105 55.3-136 176 34.6-142 0'f 06 70-130 12't03 70-130 5100 70-130 0103 70-130 295 70-130 I101 7G130 396 55.3-130 494 70-130 4112 /0-130 3't04 70-130 0104 70-130 2100 70-130 2100 &.7-139 I,00 7u13D I100 70-130 1103 70-130 3106 70-130 499 70-130 0135 U.4-167 693 7G130 298 70-130 093 70-130 1
98 70-130 092 7O-13O 199 70-130 397 70,130 786 70-130 095 70-130 I95 70-130 396 70-130 5101 70,130 3100 60_7-140 11
80 70-130 11
97 70-130 1
255025
25
25
50502525
25
255025252525255025
25
5025252525
25252525252525502525
Thb leborutotr ftpo.t k ttoa volid wilhout aa aathoized sigtarure on the cover Fage.* Reportable Detection Limir BRL = Below Reporting Limit Page I l7 of 165
Page 627
Volrtile Organic Compounds - Qurllty Control
Analyte(s) Result Flag
Soulre %RECResult %REC Limits RPDUnits *RDL
Spikekvcl
RPDLimit
Brtch 7031693 - SWE{6 5mSA Soil (low l€vel)
LCS Dup fio:tl693"gSDl I
Prepar€d & Analfzed: 28-Mar.07
41g@ropyltLolu€ne
Methyl tert.buty' e0|€r
4-lr€fryf2-p€r,anoru (MIBK)
M€lhyl€ne c,hlorile
Naphthalene
Styrene'1
,1 ,1 ,2-TeFa.filorethane
1,1,2,2-Telract om€then€
T€trachloro€lhene
1,2,}Tri{:hlorobenzene
1,2,4-Trkt ora6€nzeoe
1,1,1-Tricnb.o€ttEne
1 ,1 ,2-Trichbmethane
Tricf orofiuommethane (Frcdr 1 1 )1 ,2,3Tdcnbropmp€ne
I,2,+TrioEth@nzsn€
1,3,s-Trimethy'b€nzen€
m,p.Xylene
o-Xylene
Etiyl ethef
Ted-amyl m€hyi ether
Elhyl tert-butyl ef|er
Oi-lsopropy' €t|er
Terl-Bulanol I bulyl alcohol
1,41)ioxane
S u1o g Ete : 4-Btonafl @roh e n zeneSunogale: Toluene4SS ufiOga te : 1, 2O ich b methane4 4Sunogate : D i h tDnE fl u oronelhane
B|tch 7031779 - SW&46 5035A Soil oow l.vet)
Bhnk 1ru31779€LXll
P.eptr€d & An€'fzed: 29{lar{7
1,1,?-Tricnbrot tffuo.odhsn€ (F.eon 1i3)
Acr/oniblb
Benzene
Erornobonzene
Srorflod oron$lhan€
Bronrodid*)ronlethane
BronElonn
8turnofit€liane
2€ubnone (MEK)
n€utylbenzen€
s€c'BuVb€rE6ne
tefl-AuvberEene
C€rbon disulfdo
20.818.816,2
19.220.020.419.819.620.519.719.920.418_920.6m.020.222.720.820.3
{0.820.418.419.6t8_119.6r9.0r7020944.850.4
50.1
BRLSRLBRLBRLBRLgRL
sRr-BRI
BRL
BRL
BRLgRL
BRL
sRt
Ugikg wet
t8/kg wel
pytS wet
PdkS Yr€r
UgkS rv€t
$grkg {ret
yg^g urel
!g/kg wel
pdkg w€t
!S/kS ret
ldkS wet
!9r'k0 wet
Ig/kg w6t
rc/kg l/t€l
lgtS wet
udkS wst
Ig/tg wst
||gitS,re{
!g/kg wel
pgkS $,el
lg/tg w€t
Ugr'kg wet
pgrkg wet
Ig/kg wet
pglq w€t
ldkg vr€t
UdtS Yret
trg/kg wet
lgr'kg wet
Fgr'kg wel
Ug/kg n6l
t g'l(g lvel
lgrkg w€tIdkg w6t
20-020.020.020.o20_020.020.020.020.o20.020-0m.0m.020.o20.020_om.om.020.020.020_o40.020.020.020_020.020.020.o200200fl.o50.o50_o50.o
10{ 70-130
94 7G130
91 46.'l-145
86 70-130
96 70n30t00 70-130102 70-130s9 7G.130s8 7G130
102 70-t30
98 70-130100 70-13)102 7G13094 7(}.t 30103 7G130r00 70-130r01 56.&140't14 7G1301ft 70-'t 30102 70-130118 70-13t)102 70.130r(x 7G13092 70-'130
98 65.3-13090 70-130s8 70.130
95 7G13085 70-130104 3+155
. 9a 7&1mt01 7L1fr101 70-130101 70-130
6756
2
6
0051322
0.9532130'I
2
2
252550
25
25
25
25252525
5025252525E25
E25
25
!S/kS wet 5.0
ldkSwd 100pgr'@wst 5.0ydkgw€l 50ygkgw€t 5.0
lgtkg wel 5.0
ldrSw€t 5.0
ldkg wet 5.0
t g4!g w€t 10.0
USASwel 50-0
trC/tSwdt 5.0
lgtg y/et 5.0gg/kg rv€t 5.0
lgr'kg wet 25.0
Thl$ latodory rqotl is not erlld nithornt n rnahor*pd sigtrsture o^ drc coee. page.
' Reportable Detection Limit BRL = Below Repodng Lioit Page lt8 of165
Page 628
Volatile Orga c Compounds - Qrality Control
Spike
Brtch 7031779 - Sw846 50JSA Soil (tow tcvet)
Elank flUllz79€LK1)
PEpar€d & An€l!.zed: 2g,t4ar47
C€6on tetachbrid€
Cl orob€{Eene
Chlo.o€than€
Chlo.olom
Chloomohane
2€hlorotoluene
44hlorotoluene
| zoib.oftlo-34dpnr'opane
Dlbrqnod{oroan€than€
l2olbromoethane (EDB)
Dibrcrnolrbthane
l,zoidrbobenzene'l ,3oi*lorobenzene
1 ,4Diclllitobslt:p/?€
(Frcon12)'1,1 -Oidrloroethane
1J-Olchloro€hane't ,1 Oidlo'roethenecjs-l2-Did oro€fn€netrans. t,?-Dichlr.oethen€1 .2-Dicfibloprooane1 .SDichloropropsne22Oi$loropropene1 .1 Oicihwropened9l ,&Dlchloropropen€t-rns- t,go,chlo.opropen€Elhtbenz€n€H€xachlorcbutadi€ne2-He,€none (MBK)lsopropylbenzene+lsopropyftolueneMstlf, brl$tltyl enr€l,grr€try!2+€rtanons (MIBK)irs0tlene chbrkieNaphfialeoen€rosrybenzeneStrenel.t . t J-TetracfdorDethan€I,1.z.2-Telract oo€than€Totr&ldoroethen€Toluene| ,z,STdflorobenzeneI 2,+Tri6brob€nzeneI .l ,l-rti.*t|f,.tlx.f'€ne| ,l ,2.TriilorsfieneTftlrloro€theneTridrlorof uorcmehane (Freon 1 1 )I,2,$T.ichloroprcpane1,2,4.Trirnehylbenzenel ,3,STrjrn€by'berEen€V|rry| cfilorid€
8RL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
8RL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
ARL
BRL
8RL
BRL
BRL
ARL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRT
BRL
BRL
BRL
BRL
8RL
BRI,
ARL
BRL
BRL
BRL
8RL
8RL
BRL
BRL
BRL
BRL
8Rr-8RLBRL
!g&g Yv€t 5.0
Pgtgilet 5.0
lgr'kg Yret 10 0
!g/kg wet 5.0
lgr'kg wet 10 0pg/kg wet 5 0
Ugr'kg wet 5.0
Pgkgwet 1O.O
pgkg we{ 5 0
ug/kg wel 5.0
lgkq wel 5.0
rc^g wet 5.0
Ug/kg wet 5.0
fdkSwet 5.O
$r'kg wel 10.0
Ig/kg wel 5.0
!g/kg wel 5.0
pg/kg wel 5.0
pg/kg wel 5.0
Wkg wet 5.O
ugkgwet 5.0
!g/kg wet 5.0
Pg/kg wet 5.0
Pg/kg wel 5.0
Ig/tg wet 5.0
pSlkgw€l 5.O
Pg/kg wel 5.0
mr'kg wel 5.0
lg.itg wel 500
lgLlkg wel 5.0
Pg/kg wet 5.0
Pg&gwet 50
!g/lq wel 50,0
pgr'kg wet 5O.0
LigL/kg $/€t 5.0
lgkg r,/et 5.0
Pdkg wet 5.0
Pglkgwet t0
Fq^g wet 5.0
pgr'kg wet 5-0
Fgtkg w€t 5.0
pdks wet 5-0
pS&gwet 5.0
P9'l(9$€t 5.0
Ig4(gwet 50
Ugn(gw€t 5.0
USt(gw€t 5.0
lgAgwet 5.0
Yg,/kg wet 5.0
llgl/tg wel 5.0
pgr'kg w€t 5.0
Thk hbontory rcpotl is not vtlid uithout tn ztthori.d sigr.arure on the cover paEe .
* Reportable Detection Limit BRL = Below Reporting Limit Page I 19 of l6J
Page 629
Volatile Organic Compounds - Qurlity Control
Analyte{t Result FlaC Units Result %REC Limils
RPD
Limit
Bsrch 7031?79 - sw845 5035A soit Cow levet)
Blank {703l7t9.BLK'll
Prepared & Anavzed: 29.Mar-07
m.p-Xylene
Tetrahydroturan
Elhyl ethe.
Ted-amyl mehyl elher
Ethyl tsrtiutyl elher
Di-isopropyl etfler
Tert-Bubnol / butyl alcohol
1,+Dicxan€
S u nogale : 4 -B mnoff uo tube n ze n eSunogale: Toluene4Ssuftogaae: 1,z-Dichlorcethane44Su ECEate : D tb rcmon M Mn dh a ne
LCS Ooiltzgast I
Prepared & AnalFsd: 29-Mar{7
1,1,2-Trichlorolriff uoroetharE (Freon I 13)
Ben:sn€
Ersnob€nzene
Brornodrbrorll€thane
Brornodlt [email protected] €
Bromolorm
Eromo[€than€
2€utanone (MEK)
n-Butylbenaene
sec€utylbenzene
terl-Eutylbenz€ne
Ca6on disrJlfide
Caftofl btacnlodde
Chlo.obenzene
Chloroethane
Ct{oroform
Chkrmm€fhsne
2-Chlomtduerl€
44hlorotolu€ne
1 2-0lbromo-3drlo,ropropane
Dibro.nodrlorodnef tan€
1,z-DibronF€than€ (EDB)
Dibfomoanethan€'l
,z-Dichlorobenzene'1,3-Dichlorcbenzene
I ,4oichbrobenzeno
(Freon12)
BRLBRLBRLBRLSRL8Rt-BRLSRLARL.t&950.557.153.2
r7.410.s19.219.5
21-121.0
18.715.918.018-8't9.9
15.418.2
21.617.720_619.721.O20.319.9
20.620120.421.320.520.319.518.920.716.7m.81 9 . 1
rs.919.8
fi.0
50.050.0
20.020.020-0z).0m.020.020.0m-020.0m.02t.020.020.020.020.om.020.0m.o20.o20.020.020.0m.020.020.0m_020-020.om.om.020.o20.020_o20.o20.o20.0
34_4-167
7G130
70-130
7G.130
7Gl30
70-130
70-t 30
7G',|30
pqlgrv€t 10.0
ldkg Y/et 5-0
ugr'kg u/et 50.0
USftgwet 5.Opgr'ko wet 5.0
Fg/kgw€l 5.0
trg/kg w€t 5.0
!4kS w€l 50.0
Ug|/Xg s/et 1m
!g/kg M,elpgL/kg w6tpg/kg rv€lrc/kg w€l
|lgLnq wet
Igrkg w6tpg/tg wet
Pgtg w€l
lqlg vJ€t
!g/kg wet
lgr'kg wetpgr'ko wel
t€4(]9 w€l
USAg r€l
lgltS w€t
IdrS wet
rcr'kg wet
Igr'kg wet
l€/kg w€t
Ue^g rl€tpS/kg wel
lgrs wet
lgkS wet
lgr'kg wetpg/t€ wet
rcftg w€l
trgftg w€l
Lrgfl€ w€t
Ugr(g wet
!91fl!g wet
UdkS sret
lrg*g ' €t
Pg/tq rct
!94(g rvel
Lrglg ir€t
rcttg wet
trgr'lq.rJ€tugAg w6l
lqtg w€t
!9r'k0 w€t
9E 70-1fi101 7E1g114 7G130106 7G1m
87 70-13054 |.n-17596 70-13098 7G130112 70-r 30106 70-130t05 7{F1301oo 70-13094 55.313680 3A.&142s0 z)-r3094 70-130r00 70-13077 7c-13091 70-130108 7013t)s8 55.3-130103 7Gr30g8 70-'t30105 70.130102 70,1m100 7&130103 64.7-139t04 70.130lo2 70'13)106 7&130102 70-1301O2 7{1'l3o
I .l -Dldllo.o€thane
1,z-Di{t oroethane
1,1-DiJ orethene
cis-1 2oi$loroethefletrans-l,z{)id or€fh€og
1 ,2-Dichloroprop.ane1 ,${)lchlo{opropsne
94
104
64
104
96
100
99
Thb bbonlorf rqort b fiotr/d l ttiittout aa c$horitl sigrraure on the @wr pqe.
4 R€Fntabl€ D€t4ction Lidrit BRL = Below Rcporring Limit Pag€ 120 of 155
Page 630
Volatile Organic Compoulds - Qoality Conarol
Spike
LCSt703t7t9€st)
Preparod & AnElFed: 29-[4ar-07
2,2oichbropropan€
1 ,1 OL+ oropropene
cis.1 ,}Di{* orQropene
trans-1,&Dicitoropropene
Efirb€nz€n€
Hexachlorobutadiene
2+lexanone (MBK)
koprofMbenzene
4{sopropyt\bluene
ldelhyl brl+Uty' ether
4.li4ethyl-29€ntanone (MtBK)
MethMene cfitodde
Naphttr€le{r€
Styrone
I ,l ,1 ,2.T€lrachloro€thane
1 , | .2,2-Tetacftloro€tfEne
Tehad oroetlien€
Toluens
1.2,'Tdcnbmbenz€ne
I ,2,4Tnct orcb€nz€ne
1 ,1 ,1-Tricibro€thane'1,1,2-Trichloroethane
Trid{oroeth€ne
Trid{orcnuomm€flane (Freon 1 1 )| ,2,STrid oropmpane
1,2,+Trimethylbenzene
| ,3,tldm€frylb€nzeneVhyl ctloride
m,p-Xylene
o-Xylene
Tetralrydtofurao
Ethylef|€r
Te.l-amyl m€thyl ether
Elhyl ied{utl eth€r
Di-i6opropyl elh€.
Tert€ulsnol / hrtyl atccfiol
1,4-Dioxane
Su''r8sle : + Brornfl u orche n E neSufioCate: Tolr6n648Sudogate : 1,2&tlorcethaoe44Suoogate : Dihrurcfluotomethar@
LCS Duo lTCll77g€SDl)
Prepar€d & Analyzod: 29.Mar47
|,|,2-Tlidiolotriff uoroedrsne (Freon 1 13)
AE ylonitil€
Benzene
Bromob€rEene
Brcnndrloro.rEtlafle
ArorFdicttboo€ttene
17.1
1 8 3
19.1
20.1
21.1'18.8
1 6 1
19.4
1 9 5
2 1 . 3
18.4
17.6
21.1
18.8
21_4
20.5
18.0
20.2
19.8
21.2
201
1 9 0
21.8
20.7
1 6 0
21.4
15.7
20.0
1 7 7
41.5
2 1 3
18.4
20.3
19.2
21.1
19_3
169
203
48.549.650.451.6
18_1
1 1 . 6
1A_7
18.6
20.0
20_4
m.3
lgrkg wet
trg/kg wet
Lrgkg wet
pg/kg wel
ug/kg wet
UgkS wet
lgkS Yv€t
!g/kg wet
pg/llg wet
!g/kg wet
ugkg w€t
ugn<g wet
pgrkg wet
pg/kg wet
Ug/Kg wst
lgL/kg wet
!g/kg wet
Ugftg wel
pg/kg wel
ldks wet
!g/kg wet
Ig/kg wet
pSI(S wet
l4/kg wet
!g/kg w€t
ug/kg wet
pg/kg wel
Ug&S wet
pg/kS lvet
Lrg/kg wet
Ult/kg wet
,lgkg wel
!g/rq wet
ugikg w€t
Ug/kg wel
Pg/kg wet
ldkS wet
lgrkg wet
ugKg wet
Pgr'kg wet
!g/Kg wetyg/kg wet
ugikg wet
pgks vret
!g,'kg wet
pg/kg wet
!g/kg wet
lgr'kg wet
ug,kg u,e(
20.o20020.020_020.020020020.020.o20.020_020_020.020.o20.o20020.020.o20.020.020.020-020_020020.o20020.o2 0 020.040.02 0 020.020.020020020.o20020050.o50050050.0
20.020.0m.020.0m.020_020_o
86 70-13092 70-13098 70-130100 70-130106 70-13094 60.7,14080 70.130s7 70-13098 7G.t30106 70-13092 461-14588 70-130106 70-13094 m-1301O7 70,130102 70-13{)s0 70-130101 70-13099 70-130106 70 130102 7G13095 70-1301m 70-130104 70-13080 56_8-140107 70-13098 70,130100 7G13088 70-'t30104 70-130'106 70-13092 70-130102 65.3,13096 70-130106 70-13096 70.13084 7G130102 3+1559/ 70-13099 7G130101 711301O3 70'130
90 70.130 35A 1.77-175 794 70-130 293 70-130 5100 70-130 11'102 70-'t30 4102 70-130 3
2550
2525
25
Brrch 70317?9 -Sw646 50JSA Soit (to$ te!e,,
This lobonro.f rcFon is zot volitl u,thout ed ddhoriztd si|Eatwe on the cowr page.
* Reportablc Det€ction Limit BRL = Below Reporhng Limit Pag€ l2l of 165
Page 631
Volatile Orgaric Compounds - Quality Cootrol
SpikeLevel
%RECLimitr
RPD
Limit
Source
R€sult %RECResult Flag Units RPD
Batch 7031779 - SW846 5035A Soil (low lev€l)
LCS Ouo fl03177$aSDl)
Prepar€d & Analyzed: 29-Mar47
Baomolom
Bao|mmelhane
2€utanon€ (MEK)
nSul!,henzen€
sec-BuVbenzene
tert-gutylberEen€
Ca.bon disulfide
Carbon tet'adrtodde
Chbroti€nzeoe
Chloruethane
Chlorotorm
Chlorom€thane
24hlorotoluen€
44htorotok €ne
1 2Oibronlo-3-afi bropropane
Dibrumoc* oofirehane
1,2-Dibton'o€tha'le (EOB)
Oibrcmometlane
I ,2-Oicnbrobenzene
| ,3-Didrlorobenzene
I .+Oinlorcb€nzen€
Oicilorodinuoromethan€ (Fteont 2)
1 , 1 Oibhloroethane
1 ,OichbroefEne
1 ,1 .Dichlom€thsn€
cis-1.2-Olchloroethen€
fans-l,2oichloroethene
| ,2-Dichloropropane
l,SDldrloropmpEne
2,2-Dichlor@ropane'l,1-t)id orerop€ne
ci$1,3-Dichbropropefl e
lrans-1,$Oichloroprop€ne
Elhylb€nzene
Hexadrldobutsdiene
2-Hexanone (MAK)
lsoFopylbenzene
4-l60propyltofuerE
MetV brl+utyl eft€r
. +Mslhyf2tentanone(M|BK)
Melhylene c'|lorid€
NEphthalene
n+mptb€nzen€
Styrene
I .'l .1 ,z-Tebachloroethane1,1,2,2-Tetracnloro€[lane
TsiEchloaoeihene
l,2,}Ttichlorob€nzene
1,2,lLT,l,chlorobenzefl €
1.1.l-Trid oro€hane
20_7
17.7
14.6
1 6 3
17.5
ra.7t8.018.3
19.4
17.0
19.9
1a_7
19-0
18_6
20.0
21.0
21.0
m.019.7
19.0
10.5
20-4
16.4
20.2
r6.6
m.2
14.2
t 9 . l
19.6
16.9
17.A
19.6'19-0
17.3
15.2
17.4
l8. l
20.7
18.0
16.9
20.6
17.0
19.4
21.3
18.3
19.0
16.6
21.r
19.6
18.8
lgr'kg wet
t giko wetpg/kg $,€t
ug/rlg wel
Pslkg welpgl(s vr€l
tgl(g w€t
Fgftg rvet
lgrtg vret
ugul€ wet
Ig/l€ welpgftg wet
Ignlg wet
Fgr'kg w€t
trgikg wet
ldtS wet
ldkg wet
!g/kg wst
IgftS wet
!g/kg wetpg/kg wel
llgl(g w€t
9g/tg w€l
|lgkg wetpdks wet
ldlS rct
trgL/kg rv€tpgr'kg wet
lgr'kg wet
rc4lg w€t
Ug4!g w€l
Ig/kg wel
rgfkg welpgks w€lpdkg vret
t/dlg w€t
!g/kg w6t
IS/kS vlbtpdl.€ v{et
lroftS $€tpg/kg wel
!g/l€ vret
Ug/kg w€l
wkg tr€lpdkS welpdks Y{et
lgr'Ig wet
lgffg v/et
Itgl(s v{gt
trg € wet
lgrl(g w€r
20.o20.020.020.020_o20.0m.020.020.020.020.020.0?0.020.020.020.020.020.020.o20.020.o20.020.0m.02t).0m.020.020.o20.020.o20.020-o20.o20.0m.om.020.020.0
20.020-o20_0t0.020.0a).oa).0m.020.020.o20.020_o20-o
104 7G130 188 55.$.136 f73 38.8-142 I82 70n30 S88 70-130 794 7G130 6s 70-130 1692 70.130 r
97 70-130 1185 55.3-130 3tm 70-130 3s4 7L130 4s5 7G130 1093 70-'r3o I100 70-130 0105 64.7-139 2t05 70-130 I100 7G130 298 7Gr30 I95 70-t30 7s2 70-130 't0
102 34-+167 492 70-130 2101 70-130 38i) 7Gt30 It01 7G't30 391 70"130 5s6 70130 49a 7Gt30 164 70-130 283 70-130 396 70-130 298 70-130 295 7G130 1186 60.7-140 976 7G1 30 5E7 70-130 tl90 70-t30 I104 7Gt3o 290 46,1-t45 284 7G130 5103 70-13I) 385 7G130 1097 70-130 10f06 7G130 492 70'130 295 7G130 693 70-t30 6106 70-130 098 70-1$ 4s4 70-t3. l
25505025252525252550
252525
5{)
25
2525502525
2525252525
25
2550252525
5025E
x
2525
25
Ihis latotutory rqod tt ..ot eal I rr,fuut o,r z,ttholid sigaa&tre on the olw pgc.
. Reportable D€tEction Limit BRL = Bdow RQorting Limit Pag€ 122 of 165
Page 632
Volatile Orgrnic Compoundr - Quality Control
Analyte(s) F!ag Units rRNLResult
Spikc
Level
Source
Result
RPDLimit
%REC%REC Limus RPD
Behh ?e31779 - SW846 S0l5A Soil ilow levet,
LCS Oue (7031no.aso1)
Pr€par€d E Anal\ried: 29-Mar-07
I .l ,2-Trkfilo(oetnan€Tridrloroeth€ne
TRt oroffuoromethane (Freon 1 1 )1,2,STrid oroprop6ne
1,2,+Trimehylb€nzene
1,3,tTdr€fiylbenz€ne
m,p-Xyl€$€
Tolrshydrofuran
Elhyl €th€r
Ted-6myl methyl ether
Ethyl tert-buM eth€r
Oii€apropyl ether
Te.t-Eulanol / bulyl alcotrol
1,+Dioxane
Su/'ogeto : 4 B m molfu o rc b e n zeneSunoga/€: fotuene4aSu.ro$te: t, 2oichloroethane 4 4S u noga E : Dibtono fl uorcn et h a ne
Brlcb 70317E4 - SW846 5030 Soil (high level.
Blank tt03l78,l€LKl I
P.6pared & AnalF€d: 2g-Mar-07
1 ,I J-Tridbrotrif,rroroethane (Fr€on 113)
Acayionluile
B€nzenegromob€nzefl€
Brcrnoc'lborn€thsne
Bromodicfilorom€ihane
Bromofom
Bromomelhano
2€utanon€ (MEK)
n€uvb€nzen€
6€+Buty't€nz€ne
ted.Bu!y'b6n2€n€
C€6on dislrlfde
C€6on tefachlodde
Chlombenzene
Chloloothan€
Chlomtorm
Chlorcm€han€
2-Chlorololuene
44hbrololuene
1 r-Dibrorne3d oropropane
Dibmmod ordnethane
| 2-Oibmmo€thsrc (EOA)
Obrcmornettune
|,2-Dld o.obenzen€
| ,3-Did orob€ruene
| ,4oidllorob€nzene
20.4
1 9 . 1
16.4
21.5
18.8
18.7
18_0
37.5
1 9 4
1 7 5
1 9 . 7
18.7
20.6
18.9
r65
205
4 8 950.250_451.6
BRL
BRI.
BRL
ARL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
sRr_BRI.
BRI.
BRL
SRL
ARL
pgag wet
Ugr'(g wet
!g/kg w€t
u9xg wet
rc/kg wet
!g/kg wet
Pg/kg wet
pg/kg wel
ugy'kg wel
Pg/kg wel
lgr,kg wel
pS/kS vJet
!g/kg wet
pg/kg wet
!g/kg Yi,et
!g/kg wet
r.rglkg wet
!g/kg wet!g/kg wel
lgftg wel
lgl€ wet I 0
pg/kg w€t 20.0
pg/kg wet 'l.0
!g/kg wet 1.0
pg/kg w€t 1.0
Ugftg wet 1.0
pg/lgwet 1.0
t g/kg wet 1.0
pg/kg wet 2.O
!g/kg wel 10-0
lgikg w€l 1.0
Ugr'ko wet 1.0
lgr,kg wel 1 .0
yqy'kg wel 5 0
Ug/kg wel 1.0
Ug&gwet l0
lrSftS ',Y€l 2.O
pdkSwel 1.0
ldkg Yllet 2.O
!4fS w€t t.0
pdkS v.€l 1.0
f.iS/kS vJ€l 2.O
!g/kg w€l 1.0
fgr'kg w€t 1.0
!g/kg wet 1.0
!q/kg w€t L0
!g/kg w€t 1.0
tSn(S Yr€t '1.0
102 70-130
96 70-130
82 56.8-140
108 70-130
94 70-130
94 7G130
90 70-130
94 70-130
97 70-130
88 70-130
98 65,3,130
94 70-130
103 70-130
94 70-130
a2 70-130
102 34-155
98 70-130100 70-130101 7L130103 70-130
20.020.o20.020.020.o20_020.040.020020.o2 0 020.020.o20.o20020050050.050.050_o
7
8
2
0 9
6
2
1 0
I
4
2
3
2
2
0
5025252525252525502525252525
This toborutary rcpott k nol tulU without an etthoized si?nztan on thc cover paEe.
+ Repoftabl€ Detection Lirnit BRL = Below R€porting Limit Page 123 of 165
Page 633
Volatile Organic Compounds - Quality Conlrol
Analytds) Result Flag Units +RDLSpikekvel
SouaceRes!ll %REC
%RECLimits RPD
RPDLirnrt
Brach 7031784 - SWa46 5030 Soil {high hvert
Blank (70317&a-gLKl I
Prepared I Ahdyzed: 29-Ma{7
1 ,1 -Di:hlor€thane
1,2-Did or€tt|sne
1 , 1 -DiJ$ro€thsns
cis-1,2-Dichloroethens
trarls-l,z-Dichloro€thene
1 ,2oidbropropane
1 ,3-Di* oropropane
2,2.Dichlorcpropane
1 ,1 .Oicnb{oprop€n€
cis-1,3.Dlcliorot|lEp€n€
hans-'l,3Oichloroproperc
E8rylb€rEene
Hexachbrubutadiene
2+lexanofl€ (n BK)
isopropylberueno
4{sopropyholuene
Msthyl bn+utyl dher
4-[,]€thyl-2-pentanone (MlBl()
Mehyleoe chloride
Naphthabne
Styren€
1 ,1 ,1 ,z-Tet.achlor*hEne1,1,22-Tefadtlorctfi ane
T€irtrhloroethen€
Toluen€'1,2.+Trichbrob€nzene
1,2,4-Trichbrobenzene
1,1,l.T.idrbro€ttEne
1,'1,2-Tridrloro€than€
Tdchbrocthen€
Trichloroff uoomethane (Freon t 1 )1,2,$Tri$broprcpane
1,2,+Tdrnehylbenzen€
1,3,tTrin€lhylbenz€rF
Vin, chloride
m,Fxyl€il€
Tet'ahydrofulEn
E[|. drr€l
T€tl-aftryl melhyl €ther
Ethyl bniut!,1 €bl€.
Dl-lsop.opyl strer
Ted-Butanol / buM alcot|ol
l,4{)ioxans
S u tqate : )tB m noff &rIJben ze neSuftqate: Tdu€ne4aSunoga|P-: 1,2 -Dichbr@thane44
S/J/twaae: OilDtonafknronqthane
LCS f7fill78,t€St)
(Freonl2) BRL
BRL
BRL
BRL
BRL
BRL
BRL
8Rt-
8RL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRI
BRL
BRL
SRL
BRL
ERL
BRL
BRL
aRI
aRl
BRI.
8RL
BRL
BRL
BRL
BRL
SRL
SRL
aRl
ARL
BRL
ARL
BRL
BRL
BRL
BRL
SRL
31.13 1 . 730.630.5
rc/l(g wel 2.OpgI€wel 1.0
lgftgwel 1.0pg/tgw€t |.0pdksw€l t.0
Fg4gw€t 1.0
ldtg vret 1.0
UgI(g wet 1.0
ldkS v{et 1.0
|,glfl€ wst 1.0
l4kg wet 1.0
lg/kgw€t 1.0
Ug4€wel 1.0
ug/l(g r{el t.0
lrgrtsYrel 10.0
ldxSw€t 1.0
lgkg rvet 1.0
rcn(g $/et 1-0
€ikg wet 1O.0pgrkg wet 10.0
lg/kgwBt 1.0
Ug^gwel 1.0
Ig/tgvrol 1.0pg/l(Su,€l 1.0
Pgr'kg rv€t i.0
t/dkSrYet 1.0
ldkg Y/et 1.0
t g/kg wst 1-0
t gl(g wet 1-0
rcfl(g wel 1.0
I€Agwet 1.0
lgrkgwet 1.0
lg/kgwet t.0
USASw€l 1.0
l.dkS w€t 1.0
!C4(g vr€t 1.0
!S/kg wet 1-0
USn(g wet 2_0
FS/IS v',et 1.0
|lgkg wet 10.0
Itgftg'rJel 1.O
lrg/kgwol 1.0
tgAgw€t 1.0
usrks rv€l 1.0pdkgw€r 10.0
iJdkg wet 2O.O
ug/kg wetmr'kg wetUgLn(g wetlgr'tg wet
30.o30.ou.om.o
70-1307G1@70-1N70-130
104106102102
T h laborulory rcpan is not valu frithod zn oa&odtd signatrt on the covet poge-
' Reporrable D€tectioo Limit BRL = B€low R€porting Limit PaBe l2,l of 165
Page 634
Volatile Organic Compounds - Qurlity Control
Spike
lrvel
%RECLimits
Source
Result %RECFlag UonsRPDLimrt
Betcb ?031781- SW8{6 5010 Soil (high level)Prcpared & Analyzed: 29-Mar47
1,1,2-Trichlo.otriRuofoethane (Freon 1 j3)
Acry'onitrils
Benzene
Brombenzene
Brdnochloromethane
Bo.nodid o,om€6anegrdnoforo
Eromomelhane
2€ubnone (MEK)
n-Buglb€rE€n€
secA'rty$€nzen€
tert€utylbenzen€
Carbod drs.rlfide
Carbon tetrachlodde
Chlorob€nzene
Cl{,oroelhans
Cttoroforn
Chloromellrane
2{hlo.otoluefle
1,2{ibrorno-3-chloropropane
Dbaomo(trlorome{hane
1,2-Dibromo€thane (E0B)
Dibromornelhane
1 ,2-Did|lorobenzene
1,$Dictlkrobenzsn€
| ,4-Dk rloroDenzeoe
Did$mdifl uoromethane (Frconl 2)
t,t-Didrloro€thane
I ,2oktior*thane
| ,l .Oichlor€lh€ne
cis-1 2-Dlctrloroeth€ne
trans-l,2Oichloroothen€
t.2-Djchjoropr@EDe
| ,SDichloropropsne
22Oicnbropr@an€
| , | -Dicnb.opropen€
ds.l,SDldiloroplopene
trans-'1,3{ichbroD.opene
Ethylbe.Een€
H€xachjorobutsdiene
2+€xanone (MBK)
lsopaopylb€nzen€
4-lsopropyltolu€ne
Metvl ta.t-hnyl elhet
4+retryl-2f entanone (MI8K)
M€thylon€ c*rbrid€
Nephthsiene
n+ropylbenzene
Styreng
1 ,1 ,1 ,2-Tet'acl*croethane
Result
16.8
13.2
18.6
20.2
20.4
1 9 4
2 1 . 4
20.1
14.6
16.9
1 8 E
19.7
1 6 0
15-6
20.1
1 f . 4
r8.8
1 8 . 5
19_1
19.5
19.2
20.5
21.1
19.8
20.5
20.6
19.3
18.5
18_3
1 8 . 0
r6.5
19.2
17.8
2 D 3
20.5
r4.6
1 8 I
1 S 0
1S-4
19.3
14.8
13.0
18.1
1 S . 1'19.8
1 6 4
16.3
19.5
17.4
21.6
20.5
!94q wet
lgr'kg wet
!g/kg wet
!g{kg rv€t
!g/kg wet
lgftg wet
tigkg wel
trgkg wet
pgkg wel
ugL/kg wel
ugkg wet
Pg/kq wet
pg/kg w€t
lSf(g eret
lgkg wel
Pg/kg wel
!g/*g w€l
t/g/kg wet
!q/kg wel
t,g/(g w€t
l./g/kg !"€t
!g/Kg wel
$g/tg wel
lqy'kg wet
!g/kg wet
tig/kg w€t
trg/kg wel
US|kS wel
Pg/kg w€t
lg^g wel
!g/kg wet
!g/kg wet
!g/xg wel
W*g wet
pg!ftg w€l
lrg/kg wel
tg/kgwet
tgr'kg wel
Fq/kg wel
Ugt(g wel
rcr'kg we(
pg'l.,€wel
ac1 Ugkg wel
trgkg wel
Ugkg wet
ugL/kg wel
tl!!4(g Yv€t
!g/kg wet
!g/kg wet
!g/kg wel
tigftg "el!g/kg wet
84 70-130
66 177-175
s3 70-130
101 70-130
102 70-130
97 70-130
103 7G134
107 70-130
100 55.3-136
73 38.8-142
84 7G130
94 70-130
98 70-130
8A 70-1n
7A 70-130
100 70-130
6/ 55.3-130
94 70-130
92 70-130
s6 7G.130
9A 70-1fr
96 70.130
102 64.7-139
106 7G130
99 70-130
to2 70-130
r03 70-130
70-130
92 U.4-167
92 70-130
90 70130
a2 70-130
96 70-130
69 70-130'to2 70.130
102 70-130
73 70-130
94 70-130
95 70-130
97 70-130
96 70.130
94 60.7-140
65 70-130
90 70,130
96 70-130
99 70.130
92 46.1-145
a2 70-13[
98 70-130
a7 70-130't06 70-130
102 70-130
20.020.020.020_020.020020020.020.o20.o20_020.o20.om o20.020.020.020.020.020020.o20.020.020020.020.o20.o20.o20.020.020020.020.o20.020.D20020.020.0m 020.020.020020.020_o20.020.020.020.020.020020.020_0
Thit hbo@ory rcpor1 is Eol vot t witho|d aE rnlhoriutt sigt alaE oa thc coeet page.
+ R€Foriable D€iection Limir BRL = Below ReDortins Limir Pag€ 125 of 165
Page 635
Volatlle Organic Compoutrds - Quslity Control
Anatf,te(s) R€sult Flag Units Resulr %REC Lhnirs
Brach 703 U84 - SW846 5030 Soll (high levrt)
LCS f703t7E4asi )
Prepared E Analfzed: 29-MaF07
I , I ,2,2-TeFarhlorsthsne
Tetrachloroethene
1,2.&Trichlorobenzene
1 J,+Trichlorobeozene
1 .1 ,l.Trichloreflsne
l,1,2.Trichloro€lhane
Trilhloronuoromethan€ (Freon 1 | )'1,2,3-Tricl oaopropan€
1,2,+Trim€thyibenzene
l,3,STrilneflylb€nzene
Vinyl drlodde
m,p-Xylone
Tel€hydrEturan
Ethyl eth6r
Ted.amyl mothyl €lher
Ethyl b.t{dyl ether
Oi-isaprooyl n$er
Te.t-But nol / buM alcohol
1,+Dbxane
S u iog ate : +gronbff uo rDb e n zeneSu/'ogate: Tol@ne48Sunogate: l,2Dlchbtodhane44Su rrcgetg : Di fuomonuo@melh a rc
LCS Duo aTo3l?tt l-BSDll
Prepared & Analfr€d: 2$Mar-O7
1,1,2-Trid oroffiuoroethane (F|eon 113)
Acrylonitril€
Benzerlegrornob€nzene
gro.nochbrch€thane
Bmmodii:hloromethan€
Baomofom
Bromoftelhan€
2€ubno.|e (MEK)
n8urylbenzene
sec-gutdb€nzene
krt€utylb€nz€n€
Cshon disulfoe
C€rbon btraanbdd€
Chbrcf,grEefie
Chlo{oethane
Chlooform
Chlorcrnethane
24hlorouuene
44hbrotoluene
12oDromo-3-ct otoproperF
Oibroflod ordnethan€
20.1
17.2
18.2
19.6
19.3
16.8
21.o
r9.7
16.1
23.2'19.3
't 9.8
t6-9
39.4
20.4
24.4
19.3
18.8
214
17-0
192
30.329.827.331.5
18.8
1 l . o
2 l . t
21.2
21-9
21.9
23.3
24.4
16.5
18.4
20.1
21.6
l8-2
16.8
21.6
19.2
20.6
20.3
20.7
2 1 . 0
21.6
n.3
pgr'kg wet
pg/kg wet
Ug/Xg v.,el
uc/kg',v€l
ldkS vret
|/S/XS wet
ldkS wet
t g4!0 w€l
Idkg wet
lgixg wel
ldkS lv€l
ldls rst
ug/l(s Yret
!94{g $ret
t g/kg wel
!g/rg wel
tid*S lr€l
lgl€ Y{€t
lgr'tg w€t
pdl€ w6t
Pgifi(g 'r,et
pg/l€ wel
pgftg wetpdkg welpgl/kg u,et
!C&g vret
pg/kg w€t
pgftS {,el
lgtg w€l
ldkg w€t
ldkg Yret
pgL/kg $/et
pgL/kg wel
pg/kg wol
!g/kg wet
lidkg r€l
ldkg Y{€l
|lgl,kg vet
ldkg rvet
pg/ko vret
tig/kg w€l
t4ftg s/€t
pg/tg w€l
Idkg vret
Ugr'kg wst
t!r'kg wet
pg/kS vret
Lrglkg w6t
rs/kg w6l
m.020.020.020.o20.oal.020.020.020.020_020-020.om.040.020.020.020.o20.om.0m.0200200m.030.030.030.o
20.020.020.020.020.020.020.020.0?0.020_020.o20.020.020.0m.020.020.o20-0m.o20.020.o20.020.0
100 70-'t308A 70-13091 7G13098 70-13t)s6 7Gr3084 70-130105 7G13098 7G130ao 56.&140t16 7G13096 7o"l3t)99 70-'t3084 70-'t30s8 70-lo102 70-130122 70-13096 65.3-t3093 70-130107 7G13085 7G130106 70-13096 3+155101 70-19)ss 70-1fr91 7F1fi105 7G130
94 7G130 11
85 1.77-175 25108 70-130 151Q6 70-130 5113 7G130 10110 70-130 13| 10 7G130 7t16 7G130 I122 55.!136 2082 3a.&142 1292 70-130 9100 70-130 6t08 7G.130 10
91 7Gt30 13
84 70"130 7
108 70-130 096 553130 10to3 7G130 I102 70-130 10r(M 7G130 If05 7G.t3o 7106 70.130 12f f6 u]-139 13
502525
25
25
Ex2550
E252550
Thk lsb.olary reFod It Aol tolU p haa an aufroriz.d signzttre o, dE qe., poge.
' Repodebl€ D€t€ctioo Lirnit BRL = Below Reporting Limit Ptgc 126 of 165
Page 636
Volatile Organic Compounds - Quality Control
Spike Source %REC RpDAnalyk(s) Result Flag Units .RDL kvel Resulr %REC Limits RpD Limit
Bstcl 703 1784 - SW846 y)30 Soit (high tev€r,
LCS Duo a70el 78,1€SDt I
Prep8|ed & Anatfzed: 2g-Mar{7
1,z-Dibtumo€than€ (EDA)
Dibaomorn€tlan€
1 ,2oichlorob€nz€ne
1 ,$Oid orobenzen€
1 ,4-Dichlorobenzene
Dichbrodifluorornemane (Frcon1 2)| ,l-Dichbro€th8ne
| ,2-Dicfibro€[|sne
1,1-Dit oro€ltBn€
cis-1,2-0i4fi loro€lh€ne
lrEns-1,z-Dichbroeh€ne'l.2oichlorop.opane
l,3Oichbropropane
2 2-Dicfiloropropanet,1-Dichloroprcpene
cis-|,3{iJ icropropene
trans-1,3-Dichlorl0ropene
Eq/benzen€
Hsxachlorobutadi€ne
2-Hexamn€ (MBK)
4-lsopropyltoluene
Metlryl brt.butyl ether
4+vlethyl-2-pentanone (MtBK)
M€thybne dlbfije
Naphthdene
Slyrene
1.1, 1,2-Tetehloroettlane
1,1,2,2-Tetad croethane
Telrehloroethene
1,2,'Trichlorob€{rz€ne
1,2.4-Trici orobenzens'1,'1.1-Trichloro€thane
1 ,1 J-Tricl oroetEne
Trlchloro€lhene
Tdchlorofl letom€thane (Freon I 1 )l2,STrichloroprop€ne
I J,&TrlmelhylberEene
| ,3,$Trim€hylbenzene
Vinylchbnde
m,P-Xyl€n€
o-XylEn€
Tetrahydrofuran
Ethy| ether
T*t-drM mehyl ether
EfiM brt+utyl €tn€r
oii.sopmpyl athe.
Ted€utanol / hrtyi alcohol
I,4-Oloxdle
245
2 1 8
2 1 . 8
2 1 8
21.O
2 1 . O
20.1
20_5
19.0
2 1 0
19_6
22_O
23.0
1 6 . 3
1 7 . A
2 1 _ 3
22_3
20.8
20-4
1 6 . 5
19.8
2 0 3
21.6
20.8
1 9 . 3
24.2
18.6
23.2
22.3
2 1 4
1 9 3
20.5
2 1 . 9
21.5
17.8
2 3 8
2 2 . 1
1 7 . 8
25.8
21.5
2' t .7
18.5
42.3
22_O
21.4
20.5
19.7
2 1 1
1 9 3
241
261
20.020020.020.020.020.020020_o20_020.020020.o20.020.020_o20020.020.020.020.o20020.020.020_o2002 0 020.02 0 020.020020.o20.020.020.020.020.020.020.020.02 0 020020.040.02D_020.020020.o20.ox.o200200
pgn(g wet
lgL/kg wet
!g/kg wet
Lig/kg wel
pgr'Kg wer
pg/kg w€l
pg/kg wel
Ug/kg wet
Ugr'kg wet
pg/kg wet
Lig/kg wet
!g/Kg wet
pg/kg wel
Ug/kg wel
!g/kg wet
Ug/kg w€l
ligkg wel
ps.fts wetpg/kg wet
pg/kg wet
!g/kg wet
pgL/kg wet
Ugkg wet
Ig/kg wet
!g/kg w€l
!g/Kg wet
pgftg wet
pgftS wer
Pgr'kg wet
lgr'kg wet
Pq/kg wet
pg/kg wet
!g/kg wet
!g/Kg wet
Li9Kg wel
Ugr'kg wet
!g/kg wel
!g/kg wet
t g/kg wel
lig/kg w€r
tiglkg w€t
pgr'kg wet
Udkg wet
Ugfrg wet
!g/t(S wet
!g'kg $/et
lgr'kg wet
Hqftg wet
v4@wel
lgftg wet
aRs !g/kg wet
122 70-'t30109 70.'130109 70-130109 70-130105 7G130105 34.4-167100 70-130'to2 70-13095 70-130105 70,13098 70-130110 7G130115 7G13082 70-t3089 70-130106 70-130'112 70,1301U 70-130102 60 7-14082 70-13099 70-130102 70-'130108 70-130104 46.1-14596 70-130'l2l 70-130g3 70-130116 70-130112 70,130107 70-13096 7G 130102 7G130110 70-13010E 70-13089 70-130119 70n30110 70-13089 56-0-140129 70-130108 70-130108 70-13092 70-130't06 7G130110 70-130r07 70-130102 65.+13098 7G.r 30106 7G13096 7&130120 70-130130 34-155
14 25
10 25
7 2 5
6 2 5
9 2 5
13 50
8 2 5
1 2 2 5
15 25
9 2 5
10 25
4 2 5
12 25
12 25
5 2 5
1 1 2 5
14 25
6 2 5
8 5 0
23 25
10 25
6 2 5
9 2 5
12 50
16 25
21 25
7 2 5
1 2 5
9 2 5
1 2 5
1 1 2 5'11 25
1 2 2 5
12 25
6 2 5
1 2 2 5
1 2 2 5
t1 50
1 1 2 5
12 25
9 2 5
9 2 5
8 2 5
8 2 5
1 3 2 5
6 5 0
5 2 5
0.9 25
12 25
12 25
30 25
This lahoralory repo.t k not valid Nithoat an ouihodzed signatare on thc cewr page
' ReFortable Derecrion Limit BRL = Betow Reporring Limir Page I 17 of 165
Page 637
Volatile Orgatrlc Compoutrds - Qurlity Cotrtrol
Spike Source %REC RPD
R€suh Flsg Units 'RDL t-€v€l R€sult %REC Limirs RPD LimirA"a$dt
Brrct 7031784 - sw846 5010 So (high level,
LCS Dup 17031 7g,t€Soi I
PreFred & Analyzed: 29+rarJ7
S u fi ogele : .lB romo n uotd en z e neSufiogab: Toluene4SS u dog ale : 1, 2 t bh b roet h ene4 4S uno g ele : Dfuo n ofl w ro melha rc
m.731.0
293
Pg/kg Yrel
lgtS Yr€l
lgn(g w€!
lgtS wet
102103
98
30.030.030.030.o
70-13070-13070-1307G130
Ihk l4bofttuy ryNtt is t'ot tdu nithout oz authotisd signrnt". oA tlE covc, page .
+ R@ortrble Det€ction Limit BRL= Bdow R€porting Limir Pse€ 128 of 165
Page 638
Extractable Petroleum Hydrocarbons - Quality Control
Analyle(s) Result Flag I RDLUnits
Spike
Level
Source
Resuh "/oREC
%REC
Limits
RPDLimrtRPT)
Brtch 7031505 - Swt4615loc
Bl.nk {7031505€LX
Prepared: 26-nler-07 Analyzed: 28-l\,tar-07
Gasolin€
FuelOi l#2
FuelOi l#4
FuelOi l#6
Motor oil
UnldendRed
Other Oil
Tobl Pelroleum Hydrocarbons
C9436 Afiphatc Hydroc?to.rs
Sunogate: 1 4hlotoodade cane
LCS 1703t505-BS0
Pr€pd€d: 2GMar{7 Anal]rzed: 28-Mar-07
CgC36 Aliphatic Hydrocabons
S u iqa te : 1 - C h I otoo da de c an a
Bdcb 7m1513 - SW846 35508
Blank o0r1513€LK
Prepared: 28-Mar-O7 Analyzed: 27 -Mar07
Gasolile
Fuetoi t* r2
FuelOl l#4
FuelOi l16
ti4ator Oil
Ur*tentifed
OtlErOil
Total Pefoleum Hydrocarbons
CllC36 Aliph€lic Hydrocarbons
S u tugale : I I hl oroocl a de c an e
LCg fto315r3€s
PGpared: 26-lrrar-07 Analyzed 27 -Ma.-O7
C$C36 Aliphatlc Hydroc€dons
S urcga te : l -C hl o@od a d e can e
Batcfr 703 1589 - Sw846 35508
ghnk r?O3l5ltg€LKll
P.€p6red: 27-Mar47 Anal}rzed: 28-Ma.{7
Gaso{lne
FuelOi ld2
FuelOi l i . l
Fu€lOi l t6
Mottr Oil
Uniden{6€d
OtEr Oil
TolBl Petrdeum Hydrocadons
C9436 Aliph6tic Hydrccarbons
Suro{,ala: 1 -Chlotwcladecane
LCS O03tsEgAStI
mgtt(g wel 13.3
mg./kg wet 13.3
mg (g wet 13 3
mgl(g w€t 13 3
mg/kg wet 13 3
mg/kgwet '13.3
mgl(g wet 13.3
ng/kg wet 13-3
mg/kg \N€t 13-3
mg/kg w€t 'l3-3
mgl(g w€t
mg/kg \a€t 13.3
mgl(g $/et
3.33
93.3333
mg/kg !rct 13 3
mg/kg lvet 13.3
mg/kg rrct 13 3
mgfl(g w€t 'l3.3
mg/kg lv€t 13.3
mg/kg $€t ?3.3
mg/kg wet 13.3
mg/kg \r€t 'l3-3
mg/kg w€t 13-3
mg/kgwet '13.3
mg/kgwet 3.33
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
ARL
0_0585
o 0573
BRL
BRL
BRL
BRL
BRL
8RL
BRL
8RL
BRL
BRL
2.56
7 5 8
2.83
BRL
BRL
BRL
BRL
ARL
ARL
BRL
BRL
8RL
BRL
2.24
rngl
ms.4
mg/l
mg/l
mg/l
mgrm9/l
mgn
mg/ l
mg]l
mg/l
0.050.050.050 0 50.050.050.050.050.05o.05
rng/l 0.05msn
0.0500
1 . 4 0
o 0500
40-140
60-12060-120
100115
8 1
85
40-140
60-12060-120
67 46140
Paee l29of 165
This labodo.f rcporl ir Eot ralid.,airto& ci a!rtorizcd tigaalure oa rhe coperpoge
r R€porteble Detedion Limir BRL = Below Reporting Limit
Page 639
Exiractrble Petroleum Hydrocarbons - Quality Control
Anab,teG) FlasResult Units *R-DLSpik€l€vel
Sourc€
Result %REC%RECLimits
RPDLimitRPD
Brrch 703 1589 - SWE46 35508Pr€pared: 27-Mar-07 An€lyz€'d 2A-Mat47
C9-C36 Alipharic Hydro.erbons
Sunogate: 1 -Chlo,ooctadecane7413.3
ouollclto 1703t s8gtrtlPlI Sour[€: SA59ZI,|-03
6E.9
2_'lt)
BRLBRLARLBRLBRLBRLARLBRLBRIBRL3.(E
75.0
242
78.4
2.59
93.3
1023.63
t02
3.63
60-1ma0-120
mgftg wetn€^9 w€l
nEn(g dryrngrkg dryrngn€ dryriS/ko dryflEikg dryrERg d.yrElkg drynEtkq drymgL/ts drymgftS dryF€n(g dry
mdks dryfiig/t(g dry
mSilq d.ynE*g dry
Prepared: 27-lrar-07 Analfledr 28-Mar{7
Gagoline
Fuel Oil #2
Fu6l Oil ,r4
Fuel Oil iS
ftiolo. Oil
Avi€lion Fuel
Unirentned
Otf|er Oil
Toral Ps{rcleum Hydrocaftons
C9C36 Aliphatc Hydocarbons
Suncgate: I 4hlo,oocta.lecane
Msrdx Splke 17031589-ISll
28.92E.928.92 8 928.928.924.928.S28.924.9
ARL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
50505050505050505050
Sou.c€: SA5O724{3
8RLBRLBRLBRLARLBRLARLBRLBRLBRL2.24
70.7
8RL8RLBRLaR[ARL8RLBRL
13_313.313.313.313.313.313.313.313.313.3
BRI
BRf
BRL
ARL
BRL
SRL
BRL
ARL
4+114
50-1504L144
5G15040-14n
411144
60-12060-120
Prepa.ed: 27-Mar47 Analf2edr 26-Mar{7
CgC36 Aliphatic Hydrocarb€rE
Sufiogale : | 4hfdgocladecaneBRLt4.5 74
67
at ix Spik€ DuoOO3l589. SOll Sou.Eo: SAsgzit{t3
P teparcd: 27 4[ar47 A^alFed: 28-Mar{7
C$C36 Aliphatic Hydrccarbons
Suft''ga.'P-: 1 -Chlqoda&cane
Brlch 703l5m - SW846 35508
Blank a7031590€LKll
PreFrEd: 27-Mar{7 Analyzed: ?s-Mat47
GEsoline
FuelOi l#2
Fu6l O tA
Fuot Oat *6
Molo{ Oil
Unidonlifi€d
Other Oil
Total Petoleum Hydrocartrns
C9436 Aliphat& trydmcadons
S Mogate : I 4 h I o/ood adecan e
LCS f?03t590€slt
Prepaed: 27-lrEr47 Analfzed: 29-Mar47
CgC36 Aliphatic Hydrocarbons
S unogato : l -Chlotooc./€,deca no
30
71
14.5
rng/Kg w€tmglkg r'retmgl(g wetrnSftS welmgftg w€lrBkg welmgr'kg welmgr(g weln€L/kg w€tmgl(g welmg,t€ v{et
mglkg w€tttE/tS wst
mSn(0 d.y.rE^o dryrno,tg dryo$rkg drymg/kg drynSftS dryfiglkg dry
93.3 76
82
r3.3
Dupllcstu ft031sq)JlUPI) S'ou.€€r SA596al-16Pr€pa|€d: 2TJlrar-OTAnalt.z€d: 2g-Marry
Gasollne
Fuel Oil f2
Fuel Oil f4
Fu€l Oil #6
Motor Oil
Unid€ntifi€d
14.9
14.9
14,S
14.S
14.9
14.9'14.9
50505050505050
Thb bbo"otu ! rcpod b not jslu wllhod an aathotizd sigaatarc oa tfu ovr page.
* Reportrbl€ D€te{tion Limit BRL = Below Reptrting Limit P|ge 130 of l6J
Page 640
Eraractable Petroleum Hydrocarbons - euality Control
Spike Source %REC RpDAnalvte{s) Rcsutr Ftag Uoits *RDL Lelet Resuit o,tREC Limns fi?r, Limir
Brtch ?0l l5q) - SW846 35508
Duolicrtl7031590Ollpil So!.cs:SAS96ai-16Preparcd: 27-lrar{7 Anat}zed: 29-t!tar-O7
Odrer Oil
Total Petroteum Hydrocarbons
ClC36 Aliphauc Hydroca.bons
S unogatd : 1 -Ch toroo ct ad e c a n e
alrir Solk€ 17031 590-MSl )
1 4 9
14.9
1 4 . 9
1.87
1 4 4 1 0 1
3.60
14.4 101 8RL
ARL
BRL
BRL
65 40-140
BRL 6a 50-150
76 44-140
Sou.ce: 5A596,lt-16
rnSI(S drymS/kS drymg/kg drymgftg dry
mdkS drynlg/kg dry
mg^S drymgl(g dry
SRL
ARL
BRL
t . 2 1
68.22 7 3
74.7
2.78
505050
Prepared: 27{\Iar{7 Anatyzed: 2g-Mat.O7
C9436 Aliphdic Hydro€ft onsS Mqete : I 4 h I o too clade c ane
rldx Splko Duo fl031590-MSDIt Source: SAS96,ri_10Prepared: 27-{rar07 An€trzed: 29.[rar-07
C$.C36 Aliphatic Hydroc€rbons
S unogate : 1 -Ch I on octade c a n e7E 50-150 14 30
77 4tr140
This labontory ft?od h floa rali.tt tritttod sn aalhoized siEnature on the cover page+ Repodable Det€ction Limit BRI = Below R€porting Limit Page l l l of 165
Page 641
Semivol.til€ Orgstric CoDpourds by GC - Quality Cotrtrol
Spik€Ifvel
Betch 70r1496 - SW84{ 3s l{rc
Bbnk r7mi496€LKt)
Pftpared & Anal}/red: 26-lrer-07
PCB 1016
PCB 121
PCB 1232
PCS 1242
PCB 1248
PCA 1254
PCA t260
PCg 1262
PCA 1268
S u rog ate : 1, 4-O B -Oabtuloroh i p hen yl ( Sr )Sffiogate: Dacacnbrohiphenyl (54
LCS 47031496€31 |
ft€pared & Anal].zed: 26-Mar-07
PCB 1016
PCB 1280
Surrog€t€r 4,+DB{ctafuorobhheny, (Sr)Suno€ale : Oe c ach I oto biphe n yl ( S 4
LCS Dup ftmia96.BSDtl
Prepared & Analfzed: 26-n ar-07
PCB't016
PCB 1m0
S nogato : 1, 4 D & Oc bfl uoto biphe n yl ( Sr)SunDaae : D€cachkfobiphefl yl (St)
afl-BRLBRLBRLBRL8RL8RLBRLERL0.2000.?10
2_672.96o t30o.210
2 .713-l ro.130o.2m
ilatrirsplkoft0:11/*96{sfl source:sAst}d{$fi
Pr€parcd & And!.2ed: 2 {ar-07
llg4
rsxIStlpdl
!dl
!dlpgll
u(yl
udlpdlll€/l
0.2000.2000.2000,2000.2000.2m0_2000_2000,200
0.2000.2m
0.2000.?00
0.2350.235
o.22.o.222
!glpdlpsrludl
rgru9/llsnIrs/|
0.2u)o.2u)
2.502.50o.2uo.2f f i
2-s0250o.2000.200
2.942.940.2350.235
o.2220.222
too 3+t50tos #15{)
107 40.140118 40-140
65 30-150105 3G150
108 ,$-140
124 4{1140
65 30'150110 3G150
106 4{!1{0113 40-t40ffi 30'1fita1 3c150
t12 40-140113 40-140ffi g-150110 30-150
0.95
PCB 1016
PCB 12603. r33.72
m20
ItsA!s4pdlpdl
50pqljr4l
!91Ltg?l
BRL
0.411
BRL0.411
Su.togale:4+D&octatuorcbhhenfi64 O.t41Sutugale: Decachlorobiphenyl (Sr) 0.247
Xatdx Solke Dup 17031496{SD1} Source: SA!O659j l
Pr€pared: 26-f,1f a.-07 Analyzed: 27.Mat47
3_103-54o.133o.244
PCB 1016
PCB 12A0
Surqate : l,+OBochn uorobiphonyt ( SiSffiogaiF : Oecadlorobiqenyt (St)
Bctch 7031d9? - SW846 3510C
Blank 17031497€LKll
Prcpared & AnalFed: 26-Mar-O7
a€HC
h€Hc
dSHC
g€HC (u.dane)
Chlodarle
4,4 €oo (p.C)4,4,OOE (r,D')a{{)Dr (p,p')Di€ldrin
Endo€ufEn I
BRI.BRLBRLBRLARLARL
BRLBRLARLBRL
0.01000.01000.01000.01000.0r00o.05000-01m0.o1000.01000.01000.0100
!snusn|lgnps,l
!dl
!dl
t/(yl
|lsn
ldl
t,€llpsrl
This tzhonrory Eport h,rd eald wirharlt aa o ho.ltd tig',da.c ot rtz coverpq.-
+ Reportabl€ lkection Liruit BRL = B€low R@rting Lidit Page ll2 of 165
Page 642
Semivolatile Organic Compounds by cC - euality Cortrol
0-0120 ug/l0.0102 tidl0.010S IlS/l0 0046 z.z pg/l0 0113 pg/l0.0153 ttgtl0.0127 us40.0144 us/l0 0129 pdl0 0130 Fdlo.o153 psn0.0115 pgn0.0138 ldl0.0148 !S40.0131 pg/l0.0141 !S/l0.0132 pgll0.0128 ljs/l0.0144 ldl0-0150 pgn0.0146 !940.0196 pg/l
0 01180.01040 01090.00500_01110.01360.01250.0139o.01240.01260.01400.0120
|l94
ug/lps4
z-2 t S4!dlpgL,l
ljEl
pgl
!s.4uElwrl
Spike
Levcl
0.01000 01000_01000_01000.01000.01000.01000.05000.01000_01000.0100
o 0200o.0200
0_0100 0.02000.0100 0_02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000.0100 0.02000_0100 0_02000.0100 0.02000 0100 0 02000-0100 0 02000.0100 0_02000,0100 0.02000.0't00 0,02m0.0100 0 0?000 0100 0.02000.0100 0_02000.0100 0.0200
0.omoo.omo
0.01000.01000.0r000.01000.01000.01000.01000.01000.01000.01000.0r000.0100
0.02000.02000 02000.02000.02000.02000.02000.02000.02000.02000.02000.0200
62 30-tffi76 m-t 50
60 40'140
51 40-140
54 40-140
23 40,140
s6 40-140
76 4A-140
64 40-140
72 40-140
64 (r'r40
65 40-'t40
76 40-140
5A 40-140
69 40,14{)
74 40-140
66 .t0-140
7t 4n-u4
66 4D-14D
6,1 40-140
72 40-144
75 40-140
73 4!-14t)98 44-140
Source RPDLimit
Brtch 703t497 - SW846lsl0C
Blank fto3ta$TAlKt I
PreparBd & AnatF€d: 26-MaF07
EMosultan tl
Endosulfan Sulfat€
Endrin
Endrin Aldehyd€
H€plachlor
MeftExychlo't
Hsptad or Epo(ftte
To*aph6ne
aChlor(hn6
gChlordaoe
Enddn Ketone
Suttoga te : 1, 4. D Aid a f I uo tou p he n y I (S oSu'rogeta : Decachlotobipheny! ( 54
LCS ft031497€stl
Pr€pared & Anatfred: 26-MaF07
e.6HC
b€Hc
d-BHC
gFSHC (tindere)
4,4'ooD {p,C){,4-OOE (p,p.)
{J'{DT (p,p )Dielddn
E.dosultan I
Erdosullan tl
Eftbsulfan Suftate
Endrirl
Er|drin Aldstrydg
Hephchtor
t lolhoxychbr
Heptac$lor Epoxide
s4hlddane
g{hlodane
End|in K€bn€
Sufi E{,ele : 4, +DB-Odsf I u o rob i p he n yr F 4Sufiogele: tbtachlotobtphenyt (SO
LCS Dup r7031497-BSDll
Prcparcd & Analrzed: 26-Mar-07
Ahdn
a€HC
b€Hc
d.EHC
gEHC (LiMan€)
4,4.ODD (p,p,)
4,4,{)DE (p,p')
{,4{)DT (p,p')
Diqtdrin
Endcullan I
Endo6u an ll
Endosuffan Suff€te
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
SRL
BRL
BRL
0.o1250.0152
pgl
!gl
!g/l
!91psll
pg/r
lrlvlpg!
tig/lpdl
psnpdl
!9./l
595254255668627062631060
40-140
40140
40-140
4G140,10-140
40-140
4G140
40-140
40-140
40-140
40-140
40-140
2208011333383
202020202020202020202020
Thk leboturary Epod it not valii! wllhoU an osdto.iaci! signalurc oa the coter prge .
+ Reportable Detectioo Limit BRL = Below Reporting Linit Paee l l l of 165
Page 643
Semivolatile Organic Cotrlpounds by GC - Quality Cotrtrol
Anal''t{s) Flag Units *RDLSpikeL€vel
RPD
LimitSource o/oWC
Resuft VIFSC Limits
Batch ?031497 - SWE46 3510C
LCS Dup {703149?.4{ ll
PreP8 ed & Anal)..€d: 2&Mar-07
Endrin
End.in Aldehyde
tleptachlor
Heptad{or Epoxito
a4hlordane
g{hlordan€
Eltdrin Kebr|e
SunDgEl€: 4,+O84c|aa{ro.otrlottenl (Sr,Sunqate : DeeeHotobipheny' (50
Brrch ?031515 - SW846 3545A
ahnk fi031315€LKll
Prepared & Analyr€d: 26{vlar-07
PCB 1016
PCB 1221
PCB 1232
PCB 1242
PCS 124a
PCB 1254
PCB t260
PCa 1262
PCg 1268
Sunogd6: 4i4g4danuorcbiph€nj4 (Sr)S ur@gate : Dacechlotobiphenyl (St)
LCS O0B15t5€{ltt
Prepared & Analyzod: 2GMar.07
PCB r0't6
PCB 1260
2,4,5.€FTC+|-Xybn€ (tS)
S u nog tu : 1, 40 &OcW uotobhhe n yl (54SunDgEte: D€cachlorottphany, fS,,
LCS Ouo fioil15l$ASDI)
Prepatod: 26-Mar{7 Analyz4d: 27 -Mal{7
PCB 1016
PC8 | 260g//togata : 4,u)B&fl@rcbiptenyl (S4Su7og,ale: Docachlorotiphenyl (Sl
o.01220.0152o.01270.0r37o.0r2ao.0124o_o1420,014so.o1140.0200
BRL
ARL
BRI.
BRL
BRL
BRL
BRL
BRL
ARL
20.o32.9
401
45!3
0.0m021.435.7
476,t66
21.4
8RLBRLBRI
BRLBRLSRLsRr.BRL
3r.636.3
ugtlpdl
t,snItslps{pdl
[r9/lrdlulylItsA
0 01000.01000.0'1000.01000.01000.01000.01000-01q)
0.02000.02000.02000.02000.moo0.02000.02000.0200o0?000.0200
28.6
35710.028.628.6
35735728.628.6
31.631.6
BRI-BRI.BRLsRtBRLARLBRLBRLsRt-
61 .t{r140
76 ,10-l4t)
u 40_14068 40-14064 40-14062 {/l-1{671 &l&74 10-14072 4*^144tu) 40-14t)
1 2
3
1
1
2020mm20202020
pgkgY{€l 28.6
!S/kS rYel 28.6
ldkg rct 28.8pgko wst 28.6
t€rlg yJ€t 28-6
trgikg w€t 28-6
Ug&g wel 28.6pdtSwel 28.6
!g/Ig w€l 28.6
UdkS n€trcr'kg v/€t
Ig/kg wot 28-6
Ugkg wet 28.6pgr'kg w€l
ldkg Yret!gr*g rct
pglkgwel 28,6pg^gw€l 28.6
lrgJtg w€tpg/kg w€l
pdks dry 31.6p€ikS dry 31-6pg/kgdry 31.6
Ugl€d,y 31-6pdks d.y 31.6
lgkg dry 3'1.6
ridks dry 31.6
Igrkgdry 31.6pdhs dry 3'1.6pelg d.ylsao dry
70 *lfi115 #151)
112 4S140
127 4G140
11.6 5G200
75 &-|fl125 30-1s0
r33 4-110
131 4G140
75 *|fi1 2 5 t u l f l
30173
Dupllcet! azo315lS{uPt} SonrE€: 5450629-10
Prepared: 26'Mar-07 Analy?F,d: 27 -Mat47
PCB 10r6PCB 121PCB t232PCE 1242PCB t24ePCB 1254PC81260PCB 1262PCB 1260
sunogate : 1}o84c1fr t0mbipl'6,nyl (Slsunogate: Decachlorouphenyl (Si
6&4040444040{o
100115
Tt503o-tN
fhis lzbonlor! r.port ls ',et vaud t{'tltotd slt a!rtoded ipauft on the @vd pase-
'RrtorEble Detection Limi. BRL = Bclow ReFrting Limit Page l34of 165
Page 644
Semivolatile Organic Compounds by GC - Quality Control
Analyte(s) Result Flag IRDLuni(sSpike
Level
Source
Result % R E C
%REC
Limit5
R.PD
t-inrit
B.rch ?031515 - swE46 3545A
Hattr Solko fl03151tMS | | Source: 5A59629-1 0
Pr6par€d: 2&Mar{7 Anarfled: 27-i{ar-07PCB 1016PCB 12602,4.5,STC-ir-Xyl6ne (lS)
S wwab : 4, 4 4B4c tafl u otob i p he n yl ( S t)S u nogala : Dec ac h lo,o,li' p h e nyt ( Sr )
aAix SFil6 O|ro i70315ts{USDI) Source: SAig629-10
Prepared: 2&Mar-07 Anatyzed: 27 -Mat-O7
426511
0.0200
2 3 /45.8
37038224.130.6
39439410.031.631 6
402402
32.232.2
BRL
BRL
BRL
BRL
pSftS dry 31.6
lgkg dry 31.6
tgks dry
tiEkS drylgks dry
gdkS dry 32 2
!S/kS dry 32 2
US/kS drypS/rS dry
Ug/kg wel 5.00
ug/kg wet 5.00
!g/tq wel 5.00
!g/kg wel 5.00
pglkgwgt 5.O0
!g/kg wel 25 0yg/kg wel 5.00
lgr'kg wet 5.00
!g/kg w€t 5.0O
!g/kg wel 5.00
!g./kg wel 5.00
Ug/kg wel 5 00
tig/kg w€l 5.00
!g/kg wel 5.00
!g/kg wel 5.00
!g/kg wel 5.00
pg/kg wet 5.00
!g/kg x,€t 5.00
!g/kg w€t 25.0
tg/kg wel 5.00
trg/kg wel 5.00
!g/kg w€t 5.00
tig/kg wetpg/kg wel
rgkgwel 5.O0
9gr'kg wet 5.00
t'|g,/kg wet 5.00
lgL/lq wet 5.00
pglkgwet 5.M
!g/kg wet 5.00
tig/kg wet 5-00pg/kg wet 5,00
pq/kg wet 5.00
!S/kS Yret 5,00
108 40-140
130 40,140
76.5 50-200
75 m-lfr145 30-1fl
92 40-140 16
95 40-140 31
75 30-15095 30-150
PCA 1016
PCa 1260
S wDga le : 4, +De!}ck]f I uotoh i p h e n y r ( S lSunogab: DecacnbnfiplEntl (54
B.hh ?031516 - SW846 l54sA
B|ank r703lSl6€Ll(1)
Prepared: 26-l!1ar.07 Anatl.zedt 28-Mar,07
Aldrin
a€HC
b4ltc
d€Hc
g!8rc Gifldar'€)Chlodane
4,4ODD (p,p )a,{'OOE (p,p')
4.4 {)DT (p,C)
Dietdrin
Endosulfan I
Endosulfan ll
Endosulbn Sufste
Enddn
Enddn Abehyde
Heptadllol
Methoryciloi
HepHrhr Epoxide
a-Chlorclen€
o4hlodaneEndrin Kebn€
Sunog,ale : 4, 4 D g-Man uarc b i ph e ntI ( S 4Sunogate : hcachlorobiphetryt 6l
LCS (70:11516€31l
Pteparedr 26-Mar-0TAnallrzed: 2&MaF07
Add4
e€HC
b-aHcdaHc9FBHC {Urdere)a,a'{)OD (p,C)4,4'-DDE (p,C)
4,4'ooT (p.p')Oelddn
Endostf& |
ARL
BRL
SRL
BRL
ARL
BRL
SRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
6.241 1 . 2
1 0 2
9 3 8
10.9
4.70
9.61
I8 '1
1 0 . 5
1 1 3
10_9't 1-0
to.010.o
'10.0
1 0 010_010.01D,D'10.0
10.010_010.010.0
62 3G150112 N-150
1O2 4O-1,1O
94 40-140
109 40-140
47 4i-140
96 40-140
98 40,140
105 40.'140
113 4n-144
r09 40.140'f10 40-14n
this laboratory rcpoA is ,tol vall.l x'ilhatl or. zkthorizcd signatare on the cover page-
* Reportable Detection Limit BRL: Below Reporting Limit Psge lls of 165
Page 645
Semivolatile Organic Compounds by GC - Qralily Cotrtml
An&lyt(s) R€sult Flag Units *RDLSpiket.evet
o/oR_EC
Limirs
RPDLimit
SourceResult o/oREC RPD
Brtch 70J1515. SW8{6 ls4sA
LCS a703t5t6€S
Prepared: 26-fr,lar{7 A^alfued: 2&Mar{7
E rdosuffan ll
Erdosullan SuNfate
End n
Endrifl Aldehyde
Heptachlor
Heptact or Epoxirs
a4hhrdane
g4hlordane
E drin Keton€
Sunwate: 4,4-Og4danrodnpheoyt (SlSuftogate : Deead@ouplrcnl (Sr)
LCS Duo fl0gl 516€SDl I
Prepard: 2GMar.O? Analy.ed: 28-Msr-07
Alddn
a-AHC
b€Hc
d€Hc
g€HC (Li^dane)
4,4'sDD (p,y')
4,4{)DE (p,C)
4,4-OOT (p,p')
Diddnrr
Endoslllbn I
Endo6ulbn ll
Endosu(an Su$ate
End.in
Endrin Aldehyde
Heptac,lld
Hepta.t or Epoxftte
a4hlordane
g4hlodan€
Endrln KobrF
S u ncgate : 1, +D BQehfl $ nhiphen f, (Sr )Sunogeb: Dacact o.ow@nyl (Sd
11.2
10.0
9.71
10.7
10.6
10.1
10.6
10.5
13.2
11-7
6.209.27
10.3
s-31
1 1 - 0
4.69
11.2
10.7
11.2
10.9
1 1 . O
t 1.o
112
9 4 9
9.03
10.s' t t .0
10.7
10.7
10.5
13.5
1 1 . E
6.149.15
!g/kg wet 5.00
||gn€ wet 5.00pgftgwel 5.00
Igftgwel 5.00pdtSw€t 5.00
!{rg\r€t 5-00
|Jg!ftg n€l 5.0O
lgrkgwet 50O
lgn(gwet 5,0O
Fgnqwet 5OO
Wftg w€rpC^g u/€t
ldks wet 5.0o
rcL/kg wet 5.0O
Fgr'kg wet 5.0O
lrg/kgwet 5.0Opg/kgwel 5.0O
IS/kg lv€l 5.mpdrgYr€l 5.00
lgkgv.€t 500
|l€r'kg wet 5-00
ugr'kg wet 5.mpgr'kgwet 500
l€/ko wst 5.0opgy'kg we( 5.00
Udkg v,/et 5.0Opgilgw€l 500
lgtl(g w€t 5-00
rcr'kg wet t00
lgftgwet 500pg/kg wet s.fi)pg/kgw€t 5.00
ISAS vrelpdkS w€l
'112 40.140100 40n1o97 40-'144107 40-140t0€ 4G' 40101 40-140106 40-110105 40-140132 40-140117 4c-14o62 40-14093 4.0-141)
103 4n-14[93 40-140110 40-14047 40-1&102 ,lG14O
107 ,r0-t4t)
112 40-t40109 40-140110 40-140110 {0-140112 40.11035 40Lt:lO96 4G.140lff 40-110110 40-144107 40-140107 40-140105 40.140r35 40-14/J1t0 {GlrO62 4Ir1,U)94 40-141)
10,010.010,010.010.o10.010.010-o't0.0
to.010.o10.o
r0.0't0.o
t 0.0'10.0
10.010.010_0r0.0t0.oto.010.010.0'10.0
10_010.o10.010.010.010.010.0lo.olo.o
1
I
0.9
0
6
I
4
0.9
0
0
5
1
2
6
0.s02
0.9
30
303030303t)30m3030303030303030303030
Dudkd. o03l5l6aUPll SourEa: SA59€38{1
Preoaredl 26+r€r.07 Analyzed: 2eMsr{7Aldrin BRL udt(g dry 9.03a€FlC BRL pdkg d.y 9.S3b-BHC BRL $r€ d.y 9.83d.efrc BRL yg?€dry 9.83g€Hc(Urdan€) sRl ucfts dry s.t}:'Chlordan€ BRL pdksdry 4S. I4,4-DDD(p,p') BRL pd*Sdry 9.834,4'ODE (p,C) BRL ldkS dry 9.834,a'.DOT (p,p') BRL lgkS dry 9.83Dietdrin BRL ydks dry 9.93Endosulhn I BRL pSAS d.y 9.83Erdsu$an ll BRL lgftS dry g.B3Endosillbn Sulfat€ ARL pC/tS dry 0.83
BRL
ARL
ARL
BRL
SRL
BRT
8Rt
BRL
BRL
BRL
BRL
sRtARL
303030303030303030303030c)
fhb lalo$lory EFort is aottolil Nithau da allhodrpl sagn ture oE th. cowr p4ge-
J Reporlable D€t€ction LiEit BRL =Below R€poding Limit Pa€e tl6 of | 65
Page 646
Semivolatile Orgflnic Compounds by cC - euality Control
Prepared: 2Gt aF07 Anatyzed: Z&Mar{7
E drtn
Etutdn Ald€hyde
Hepladltor
Heptachlor Epoxil€
Toxehene
aS ordane
g4hlordane
Eftdtin Keione
S/'l'wete : 1, + D & Oc laff rE rob p he n y t (S 4S/u/r9gete : Oeca.hlorobiphenyt (Sr)
tlatrtx Sbtks l'f 031stGMslt Sourc.: SA5953a4l
Brtch 703r516 - Sw8,t6 t545A
Ouolicalo O0315l6OUPl ) Sourc€: 5A59638-01
ARL
8RL
ARL
BRL
BRL
BRL
BRI
BRL
ARL
10.719.0
PreEErcd: 2AMar{7 Anatyzed: 28-Mar-07
Aldrin
6€HC
b€HC
d€Hc
g€HC (tjrdane)
4,4'{)m (p,p')
4,4-ff)E (p,p')
4,4 -OOT (p,p')
Dieldnn
Endcuffan I
Endo€uffan ll
Erdo6ulhn Sdfate
E.rdrtn
Erdrin Alliehyde
H€ptachlq
ld,6rloxydrbl
l'leplachlor Epoxide
a.chlordane
g4hbdane
Endrin Ket)n€
S unga lo : 4, +DBoctafl uo rob i phe n ta $ iS unWaE : Deca ch k,rob i ph e n yl ( 34
18.2
16.4
19.4
4.62'].2
22.4
21.1
23.4
2 l I
22.4
14.2
205
1S.6
1 8 0
1 9 . 9
2 0 3
22.8
20.5
1 1 . 420.2
X.Hx Soike Duo fo315tfitso fi Source: SA5!'€3E{1REpsred: 26-L,la.{7 Analrzed: 26-Mar-07
pdkS d,y 9.a3
PSftg dry 9.83
UqkS dry 9.83pSI(g dry I83pS/kS dry 9.83
UdkS dry 49-1pg/kg dry 9.83pdlg dry 9.83
Fdks dry S.83pdks dryldks dry
Ug/kS dry S 87
USn(g dry 9.87
!S/kS dry 9.87
ldkS dry 9.87pdks dry LAI
!g/kS dry LA7
!g/kg dry 9-87
!g/kg dry 9.87
ridkg dry 9.87
lgkgdry 9A7pS/kg dry 9.87pS/kS dry 9.87
t/s/ks dry 9.87pdrs dry 9.87pS:4(S dry 9 87
ldkg dry 9.87
!g/(g dry 9,87
!g/kg dry I87
udkS dry S.87
US/kS dry S 87
ldks dryUS/kg dry
55 34-15097 30-150
92 30-15083 30-1509a 30-15044 3G15087 30-150114 30-150'tol 30-150119 30,1501O7 30.150105 30-150'116 30-1506a 30-15092 3G150104 30-1 5099 30-15091 30-150101 30,150103 30-150116 30-150104 30,15058 ni 50to3 30-150
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
303030303030303030
Abdna€tlcb€Hcd€Hcg+HC (Llldan€)4,4'OCto (p,C)4,4'OoE (p,p )4,4{)oT (p,p')DielddnEndosutfan IEndcutFan llEnd6ufian Sulfsle
udks drypdks drypdks drypSftS dry
lgfts dry
!S/kg drypdks dry
!g/kg dry
rdks dryyg/kS drypg/kg drypgkg drypdks dryEidfi
Endrh
22.O
18_1
24.1
9.64
19.7
24.4
24.0
27.1
22.5
23.9
25.2
17.0
r8.8
20.1
r 0 . 1
1 0 . 1
10.1
1 0 . 1
1 0 . 1
1 0 - 1
1 0 . 1
10.1
1 0 1't0_1
10.1
10.1
to.1
10. ' l
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
ARL
ARL
BRL
BRL
8RL
BRL
109
90
1 1 9
4A
98
121
1 1 9
137
1 1 1
1 1 6
125
84
93
100
30-15030-t 5030-15030-15030-15030-15030-15030,15030,15030-15030.1503G1503G1503Gr 50
19.619.6
1 9 7
1 9 7
19.7
19.7
15.7
19.7
19.7
1 9 7
19_7
19.7
1 9 . 7
1 9 . 7
19.7
19.7'19.7
1 9 7'19.7
19.7
1 9 . 7
1 9 . 7
1 9 /19.7
m.220.220.220.220220220220220.220220.220_220220.2
BRL
BRL
BRL
BRL
BRL
BRL
BRL
SRL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
ARL
BRL
ARL
ARL
8RL
1 7
8
l 9
I
1 2
6
1 l
1 4
1 2
7
5
1
3030303030303030303030303030
Ikb laSonlor! ,zpotr ir not valtuI w[!hou! an oathodzed signztarc on the cover pale.
+ Reporlable Delection Limit BRL = Betow Reponing Lirnit Page 137 of 165
Page 647
S€mlvolatil€ Org{nic Compounds by GC - Qurllty Cotrtrol
Analytqs) Result Ftug Utrits .RDLSource o/'frFc
Resulr YoREC LimirsSpikeL,er'el RPD
RPDLimit
Brrch 7031516 - SWE46 1545A
iratrix Solk Ouo OO3l5l&{ilSOl) SorrEs: 5A596:1841Prepared: 26,1\rar-07 Anall.zedt 28-Mar-O7
Heplachlor
Methoxy.filor
Heptachlor Epoxide
a-Chlordane
g-Chlordane
EMdn Keton€
S u fiog ate : 1, 1-D & Ocb fl uotob i phenyt ( S t)S u iog de : Oec ac h lotob i phe n yI ( S t)
B.lch 7B 1591 - SW846 3:4sA
Blrnt 17031:r!tl €LKl I
P.epared & Analyzed: 27-Mar-07
PCB 1016
PCB 1221
PCB 1232
PCB 1242
PCB 124a
PCB 1254
PCB 1260
PCB 1282
PCB r 268
S u,rogate : 4, 40 &Oclafl &n b ip hG nyl ( S 4S u nog ah : De cach Mi phe nyl ( Sr)
LCS {70:lt 591ASl }
Prepar€d & Anabrzed: 27-ttar-07
PCB t016
PCB 1260
2,a,s,&rGM-Xyl€n€ (lS)
Su ogate: 4j-DeocbnwrcNpfunyt (S4S u Eqale : Oe@c h kltl],b i phe n yl ( S t)
LCS DuoOo3lsol€sol)
P.€par€d & Anavzedr 27-Mar{7
PCB 10t6
PCB t260
Sunqale: 4, 4.Da4cki:lombidEnyl (SdSunt8,e'€': Decachbtobiplnny4 (Sr)
22.4l7.a23.022.422.621_412.321.1
BRL
8RL
BRL
BRL
SRL
8Rl-
BRL
BRL
BRL
20.030.0
396
427
0.0200
m_o30.0
394
426
18.630.0
20.228220.220.2
20.220.2N.2
28.620.6
35735710.028-6286
35735728.628.6
BRL
ARL
ARL
SRL
BRf
BRL
FdrSdry l0.l
rdl€ dry 10.1
ldkg dry 10.1pglkg dry 10.1
lgtrg d.y 10-1
Ug?€dry 10.1pS/kS dryldks dry
Ig(g lvet 28,6pdksYrel 286
[g/kS wer 28.6
Igr'kg vret n.6
!€n!g wet 2A.6
ruI€ wet 28.6
Igikg wel 2E,6pdrs vY€l 28.6pgfkg w€t 28.6
ldXS Yretugnq ',/et
yg/tg w€l 28.6
Iga,gw€l 26.6pgrs w€l
!9&g w€tFdkS rvet
pgrkgwet 28.6
Ig[(g wet 28-6pgtg welpdkg Y/el
ldkS dry 33.1
tdkg d.y 33.1
lSfiS dry 33-1
UdkS d.y 3:1.1pdxsdry 33.1
Fdl€ dry :}:}.1
uS/kS dry 31.1
lgkS dry iI!,lpdkgd.y 3:'.1pgr€ dryFdrg dry
t ' t3 3G150 13
88 30-150 3114 30-150 12
tl1 30-150 7
112 3G150 4
106 3G.150 2
6t tulillU 30.150
303030505050
Sourc.: SA5!r€:ll-16
BRL
BRL
BRL
BRI
ARL
BRI-
BRL
BRI-
8RL
t4.g21_5
70 31]'150105 3ttlffi
111 40-140120 40n40102 50-20070 30-150105 3t-1fl
1r0 4+144 0.911S 40-140 0.865 n-150105 3111il
15 n-Ifl65 30.1fr
3030
Ouolhat .z03t59lOUP|lP.epded & Analzsd: 27-Mar.07PCB 1016PCg 121PCB 1232PCE 1242PCB r24aPCB 1254PCB 1260PCB 1262PCB 1268
8RtBRLBRLBRLBRLARLBRTBRLBRL
64040
40404440{040
Su,/'agale : 4,+DBocbf,uotdiptgnyt ( 54Sunogdte : Decach lo towhen yl (Sr)
33.1
Sowcs: SAsgG4l.tAX.kir 5o (. O03l5e1{8tl
Pag€ 138 of 165
Thit lebonbt! eporl is Eot talU l*hau sd arlhorizd iig&atte od drc cowr pqe .
* Repo.table DetEction Limit BRI = Below Reporting Limit
Page 648
Semivolatile Orgaric Compourds by CC - euality Control
B.ach 70f1s9t - sw846 354sAPrepared & Analyz€d: 27-Mar,07PCB tO16PC8 t2602,4,5,&TGM-Xybne (tS)S 6aga e : 4, 4 -D& Octaf t uo roh ip h e nyt ( S 4g-r7oga t e : De cach I o to bi phe n yt ( Sr)
tlatrlx soit. Duo fi03159t.ftsD souTc€: sA59f4.t-16Prepaed & Aflav:ed: 27+rar-07
PCB t016
PCB 1260
SuTogate: 41O& twanuotpbiphenyt (Sr)Smogate : Oocachtorobi phe nyl (SO
449
490
0.0200
24.540.8
451
490
22.8
404
408
10.0
32.632.6
407
407
32.6
BRL
BRL
ldkg d.y 32.7pS,kS dry 32.7pg/kg drypglkS drypg/kg dry
Pdkg dry 32.6
Pdkg dry 32.6
!S/!9 dry!Sn(S dry
110 40,140
12O 4l-14o
91.9 50-200
75 m-t50125 3O-15O
111 40-140
120 40-140
7D m-1fi115 m-150
0_9
oBRLBRL
5050
Thh lzbontory repo.l h ,toil edid xtdhoLt an authoized sigaature od tke cave, poge_* Reportable hactioE Limit BRI_ = B€tow Reportin8 Limir Pas€ 139 of 165
Page 649
Semivolatile Organic Compounds by GCMS - Qurllty Cotrarol
Analyte(s) Result FlaC UnitsSpike
Lvel
RPDLimit
Sourc€ ./.REC
Result %R.EC Limirs
Botch ?031499 - sw846 35||tC
Blank (70314${LKll
Prepared I Analyzed: 26-Mar{7
Ardllne
1 .lilelhylnaphthabne
Azobenz€ne/Diphenyldiazine
Ber\zrdirle
Benzo (a) ar hrec€ne
Benzo (a) anthrac€ne
Benzo (s) pyrene
Eenzo (a) pyrene
Benzo (b) nuorEnthene
Benzo (b) fuolanth€ne
Benzo (9,h,i) pe.y€ne
Benzo (g,h,i) perylens
Benzo (k) ffuoranthene
B€nzo (k) fluofdnther*
B€dzoic acid
Benzyl alcohol
Bis(2d{oro€thory}nelhan€
Bis(z-chbro€thyl)ether
Ais(2dtloroisoprQyl)ether
Ais(2+thylhexylhhhalale
44romoph€nyl phenyl eth€r
BUV b€nzyl phthalate
Ca.bazole
4-Chloro-3-methylphenol
4-Chloroanilin€
2-Chloronaphthat€ns
24hlorcphenol
44hbrophenl phenyl elher
Chrysene
chrysene
Oib€nzo (a,h) anhracene
Dib€nzo (a,h) anhracene
Dibenzofu€n
1 ,2-Dichlorob€nzen€
I ,3-Dicilorobenzene
1 ,4-Dichlorobenz€ne
3,3'-Dhnbrobenzldtte
2,{-Oichb'roptFnol
Diethyl phlhal€b
Dimdt\yl phthsl€b
2,4.Dim€lhylph$ol
Oi-n-brrtyl phthalate
4,6-Dhnro-z-mef ryhhonol
2Joinibophdrol
BRL
SRL
BRL
BRL
BRL
BRI.
BRL
BRL
SRL
BRL
BRL
aRf
BRL
BRL
BRL
BRL
sRrBRLBRLARLgRL
sRrBRL
BRL
BRL
BRL
BRT
sRr8RL
8RL
BRL
BRL
ARL
8RL
ARL
BRL
aR[BRLBRIgRL
8RLBRLARLBRLARL8RLBRLBRLBRLBRL
|'!g/rP9npdl
uglps/i
l4rlttdlt d lttgll|lglrcnFSnpc/t
tdlugllrc4rdlFSrlt d lLig/l
uglpdlpg/l
udlpdl
!dlttgll
||gr'lpsnt4lil
Fdl
!dl
tgl
lsn$s{usnpdl
FdlItsA|rBn!snpsn!dl!gluglI4llttsxpgl
rdl!dludl
1 .Oo2000.2000.4001.001.(n
0.200r.001 0 0't.00
1.000.2000.2000 2000.2000.2000.2 )1 .m0.200_2000.3001 0 01 .mr.00t_00't 001 0 01.00'|.00
|.001_001.001.001.00t.00|.000.2m0.2000.2001.001.001.001.001_(X)1-001.00|.001.001.00't-00
1.00
Irit labotulory rcpod it aot wlid u, ttoat a, a.trtodrd sqnala.e oa thE covet page.
+ Rrpmtable Detectioq Limi. BRL = B€low Reporring Li$ir P€e I4O of 165
Page 650
Analyt4s)
Semivolatll€ Orgatric Compounds by GCMS - euality Control
FlrA Unitssource %REC
Rcsult %REC Limits
Berch 7031499 - Sw84635t0C
Blsnk 17031499€LKll
A€pa.ed & Anat!.2ed: 26-Mar{7
2,4-Dinikol,oluene
2.6-Dinikotoluen€
Oi-n-octyt phthatab
Fluo|antfiefle
FluoGnlhone
H€xachlorobenzene
Hexechlorobutadiene
ll€xachlortryclopentadiene
l'iex"?ctloro€then€
lrdeno (l,2,3.cd) pyrene
Ind€no (1,2,3-cd) py.ene
2-{llethylnaphthal€fl e
2-Meltrylph6nol
3,{-Ll€thylphenol
Naphfhsl€ne
2-ilitroaniline
3{.1lroanlllne,l-$lilrod line
Nirobeizefle
2{'liboph€nol
4-llifophenol
N-Nit osodlmetf tybmine
N-Nibcodi-n{ropytamine
N-llibos.di,Dhenlar.nine
P€ntachlorophenol
PherEnthrene
Phemrnhrene
Pyddine
Hexachlcob€nzene
1 ,2.{-Trid orob€nzene
z.4,tTrid oropherbl
P6ntedlloroph€nol
2r,&Tn.fibrophenol
HoxacNo.obutadisn€
Sun1&ate : 2-FluotobiphenytSl./rrogate : z-FlwohiphentlSmt8,ate: z+luo.ophenolSuEWb. Nilobenzene4sSmt:gete: Phenol4,Suftogale: Tefienyl4l4s/.lno€ak]Tefuenyl4l4gr nEgate : 2, 4, &f d bm nop he nof
LCS 17U31499€St )
P.eparcd & Analyzed: 2&MaF07
BRL
8RL
BRL
BRL
BRL
BRL
SRL
ARL
SRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRLgRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8Rl
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
ARL
8RL
BRL
BRL
87.787.79 3 510684410810869_8
81.2
81.2
ttgtl
tgtl
!sr!s/lpg/l
r91lp9/lpgl
lig/rps4p9l
!snpglpsn
Ljgn
!9nug/lps/
lig/l
rgtlugnuglpgl
!sn!s4psn
ugtl!9n|l9/l
pgn
t/gl
tgtl
trs/l
Itg
ttgl
t g l
!gn
ll(rl
v9pEl
trElvgllI'Sllwll.'dluglpsnp94
pcn!9/l
1.001_001-000.2001.000.2001.001.000.6001_00't _000.2000-2001 0 01.001.001 0 01.OO
1_001.001 0 01.0r01 0 01.001.001 .001.001.001 0 00.200'r.00
0.2001.001 .m1.001.001.(JO1_001.000.200
1.000.200
1001001(n1m1AO1001001n
100100
30'13030-1m1 1 1 1 0301JO15-11030-13030-13015-110
40-140
4G140
8888941068810810870
81
8 1
Thb labodoq rcpo.r k noa valid alithoU aa aathotlltd slgt tttre on the cover page.
* Reportable D€tocijon Limit BRL: Below ReDonins Limit P a B e 1 4 l o f L 6 s
Page 651
Semlvolatil€ Orgatric Compoun& by CCMS - Quality Control
Analyte(s) Result Flag
souce %RECResult %P.F,C Limits.R DLUniis
SpikeL€vel
RPDLimitRPD
Batch 7031499 - Sw8{6 3510C
LCS aro a99€S
Prepared & Anslyzed: 26-Mar-07
AcenaphthYen€
I -Melhylnaphthalene
Aniline
Azob€nzene/Diphenyldiazine
Benzidine
Benzo (a) anftrecenegenzo (a) anthracene
Benzo (a) pyr€n€
Benzo (a) pyr€ne
Benzo (b) fl@rdnlhene
B€nzo (b) fuo.anlhene
Benzo (g,h,i) peryiene
B€nzo (g,h,i) p€ryene
8€nzo (k) iuoranhon€
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
Bis(zd oroethoxy)m€fhane
Bis(2d oroeoyl)€ther
Bis(2-cnbrcisopropyl)ether
Bis(z-etry{h€xyl,phlhalate
4Sromophenf ph€nyl ether
BUV benryl phhalale
Carbazole
44hloro-3rnelhylphenol
44hloroaniline
2 4hlorunaphthdlene
24hlorophenol
44hbrophenyl phsnyl ether
Chrysene
Chrysene
Dibenzo (a,h) anth.acene
Dib€nzo (a,h) anutracene
Dib€nzofuran
1,2-DiJ orob€nzene
1 ,3-O*Ibrobenzene
13-Dichlorobenzene
3,3 --Didrbrob€nzidins
2,4-Dlchlompheiol
Di€ftryl phthalab
Dintethyl ptrthabts
2,4-Di.n6hylphef|ol
Di-n-buy phthalaie
4,&Oinito-2-rn€thylphenol
2,4-Dnitoph€nol
2,4Ohitrotolu€n6
2,6oinitroiotuerle
90_090-0ao_211694.294.2't79
10519780.6
90.090.0al2a1.262.462.89e.698.682.479.1$9.095.155.910279.098.41 1 984_377.7E1_76 9 683.786.1a6.l63.069.08{_074.66 4 877.1E5-176.S86.082.O74.768.275.582.48{i.290-5
0.2I]00.4001.001.OOl_0002001.001.00L000.2000.2000.2000.2000.2000.2001.000.2000.3000.200t.001.001.001.001.001.O01.001.001.00|.00r.001.001.001.001-000-2000.2000.2m1.001.(m|.001.001.001_00
1.001.0{)1.001.001.00|.00|.00r.(,rc
100100100100t00t00100'tfi)
1m100100100100100r00r001001m100100100100r00100100100t00100100'100
100100100t00r001001001001001001oo100t00100100100100100
100ro0't00
psntdl!dl$s,lt!{,tsrlldlt4
Ac2 ljgnt'dlp4lpdl
!dlugnudlp€rl
wltdl|lg/l
pqlpsll
udltttylttgl'ldlIdltt9,r'|us/|llgt
Pdl
!dl
!gl
r{l
|tdl
llg,l
trS/l
mnlsrlpc4
!dl
!dl
lt9rl
Irdl
ldl
wt sxpcnpsr!dlfdl|'lsn
90 4G140
90 ,lO-'1{O
80 4S140116 4.&140
€r4 4Gt40
94 ,t0-140
179 S.200t05 40-'140
197 40-140
81 ,r&14O
81 40-1{0
so 4$140
90 40-140
81 40-140
81 4tlt40
63 40-14063 40-140
99 40-140
9S 4G1{O
82 3G13079 4Gr40
89 40-14095 40-140
56 40-140102 40-14079 4O-14{J
98 4G140119 1Gl,lO
84 3G13078 .1G140
82 4{1140
70 30-13084 40-14086 40-14O86 40-'14069 4O-14O
69 {0-140
84 40140
75 4G140
65 4{rr40
n 4!-144
85 4S140
n 30.13,j
06 40-140a2 4$-14075 3&1308a 4G140
76 3G130
82 3()-130
86 4{)-l,l090 40-140
Thit lnhotuory rclorl h Eor dld N,UhoU oE axrtoized $gttttare oi the cowr prye.
'It€portable Detection Limit BRL = Below Repoftitrg Limit Pa€e 142 of 165
Page 652
Semivolatile Organic Compounds by GCMS - euality Control
Spike Souce %REC RPDAtrElytqs) Resuh Ftag Units +RDL L€vet Resutt %REC Limits RpD Limit
Batch 701149{ - Sw845 3510C
LC8 1703t499€S.t )Prepared E Ansh.zed: 26-irar-07Di-n-octyl phtheleb
Fluorantlene
Fluorantllene
Fluoren€
H€xaafilomberE€n€
H€xadrloftbutadi€ne
Hexacilof ocyclop€ntadi€ne
Hexact orcethane
l.deno (1,2,3-cd) pyrene
lrdeno (1,2,3-cd) pyrene
lsophorone
2-MethylnEphthal€ne
2-M€thylpheml
3J-Medl&tlenol
Naphthalene
2-l lilroanilne
+Nilrosnilin€
4-l{ilroani{n€
Nitobenzene
2-t{iLophe{ol
4+libophenol
NJ.lib6odir|l€ihylamin€
N+titGodi-fi $opylamineN-Ntltcodlphqny'arme
Pentachbrophenoi
Phenol
Pyridn€
H€xedrlorob€nz€n€
1,2,+Triafi lorobenzene
Penla.'|broph€nol
2,4s-Tridllorophenol
2,4,GTrichlo{ophenol
Hexachk robulEdiene
Su/'o8ate: z-FhwobiptEnr4Swogate: z+tuonbiphenylSurog ale : 2+luor'o phe nolSuft g ele : N ittoben ze n e4 5S@ogale: fhe@l4sSurogale: Ta6enrt4l4S urggate : To tp l|€nyl 41 4S l/,,'€ate : 2, 4, 6 - f tibrc nop h 6 n o I
lratrlx Solko alcilaog-trls | )
Prcpar€d & Ar@lyed: 26-trar47
Acenaph0lene
Acamphh€n6
44hloro3.rn€6ylphenol
24hbrophenol
1 3 1
7 8 8
78.8
85.5
85,5
76.6
fa.4
60.4
73.9
64.2
u_293.4
85.5
71_0
86_5
85.6
8 3 7
8 8 9
114
s6.7
74.4
59.2
7 9 0
67_0
97.2
6 8 5
r7_5
77.5
7S.0
aa284.2
78.5
76_6
80.9
68.5
75.O
62.8
7 8 4
83.283.267.110067.88 9 88 9 873.6
Sou.cc: Sl5t€€9-11
73_1
73.1
143
123
pgn
trdl!s/lvglllis/l$g1luEl!ErItgtl
vs/lpsn
!gl
psn
vs]l'vsAusnpglpsA
uqrttgtlpgl
!9r
!snrgl!g/lg9l
FSn
vaJl
!El
trg4
wtl
Itg
|lg/l
ltgl
u9nPEI
!g/l
!9/lp9l
!s/lF9lpsn
!9r!9/lpsr!s/|
!grvgtl
oM7 lgnllsn
131 40-140
79 40-140
79 40-140
86 40-140
a6 40-140
71 40-140
7A 40-140
60 40-140
74 40-140
64 40-140
64 40-140
93 40-140
86 40-140
71 40-140
86 40-130
86 40-140
84 40-1l|()
89 40,140'r14 40.140
97 4O.14O
78 30-130
59 30n 30
79 40-140
67 40-140
97 40-140
6a 30-130
78 40,140
78 40-140
79 30-130
8a 40-140
88 40-140
7E 40-140
77 4O-14O
81 40-140
68 30-130
75 30-130
63 30-130
78 40-140
83 3G1m83 3F1fr67 | S1l0100 30'1m68 1U11090 3G13090 3c1fi74 15-110
7373143123
40-14040-14030-13030- 130
r.001.000.2001 0 00.2001,00
0 6001.001.00
0 2000-2001.001.00'1.00
10.o1-OO
1.00'1.00
1.001-001.001.001 0 01_001.001.001 0 00.2001.00r.00
0.2001.001.001.001.00r.001.000.200
0_2001,001.001.00
100100100'100
100'100
100100100100100100100100100100100100100100100100100100100100100100100100100100100100100'100
1001001M1001ffi100100100100100
100100100't 00
BRL
BRL
BRL
BRL
Thit labo.Qlory repo.t is aot wlu withorlr an authoiral sigttdltne on the cover Nge' R€portable Detection Limit BRL = Below Reportiog Limi( Paee l4l of 165
Page 653
Semivolatil€ Orgsnic Compounds by GCMS - Qurlity Control
Analyte(s) Resulr Flag *RDLSource %REC
Result %REc LimitsUEits
Spik€I.tvel
RPD
LimitRPD
Bitch 7031499 - SW846 3510C
Matdx Spits {7ml{g$irsll
Prepared A Andlz6d, 26-Mar{7
1,+oiJrhobenzen€
2,4-I)initrotoluene
4{,litophenol
N-Nibosodi-n-propylamin€
1 ,2,+Trid orob€nzen€
Pentachloropilanol
Sutrogate : 2-FhMofiphenylSutrog ale : 2 - F I @robi phen ylS u nog ale : 2 -F I uoro phe nolS u@gate : N iltobe n E rre4 5Sudogate: Phenol4sSufiqate: feryfuny'4l4Sutogat€j Teryhenyl-d4Sufiogale : 2,4,6 f ttbtumophenol
Sosrco: 5A5166S11
42.4
74.2
u.485.0114
121
s0.'l
90.1
58.3
1 1 4
74.574.56 t . l83.461.31U)10064.0
Hatrb( golkc Ouo r703la99{SDt} Sowc€: SA59669.ii
Prepared & AnEl).zed: 26-Mar47
74.8
7 4 A'146
129
64.8
77_5
86-7
E8.4
112
133
s3.1
93.1
57.4
112
7+074.0aLo79.761.798.098.063.6
BRI.ARL8RLBRIARLBRLaRt
Ac€naphfl€n€
4.chloro-3{€trrybhenol
24hlorophenol
1 ,+Dichlorobenzeri€
23-Dinibotoluen€
4+lilropienol
N-Nitrcodi-n-9lopyl€mine
Penlachloropheml
Ph€nol
1,2,4-Trichlorob€nz€ne
Pentachlo.oph€nol
S u nog ale : 2 -F I wto bi phe n ytSMogaIe:2+h$towhenylSu|'egate: z+luoropherglS uftogale : N itto be nza fi e4 5Sunogate: Pheipl4sSu''ogate: Teryh6nyl44Su.'ogate: feql6ntl4lS uiog ale : 2, 4, 6 f tibmnwh @ ol
B.tch 7F1514 - SW846 15508
Blank f7031514€lxl )
Prepared: 26-t'/ar-07 Analyzed: 27-Msr{7
,@naphh€ne
A.€naphtry'en€
Ar{lne
Azotenzens/Diphenyldiazin€
B€nzdine
pstpdl
Idl!dlps4
vElpcnpdl
rcnvd!94Fdr!dlWn|ls4pdl!glpsn
rdl!gl
qM7 pgt
!dl
vg/]'rdl!snu94ucn
aM7 pgt
tt(yi
t'ilt'dlpdl
!dlg(yl
rc4t4ltlrsxFdl!dlrdl
62 40n4074 40-14084 3G13086 40-140114 3{1130
127 3&.130
$ {G14090 4G14050 4Gr40114 30-13074 N-13074 30-13061 15-110E:J fuI3O61 t| l to1g) 30-13t)t@ 30-13064 1+110
75 4i-14075 40-14146 30-r 30ln 3Gr3065 40-140z8 40-14087 30-13088 ,l()'l{o
t12 3G130133 30-130s3 4S140
93 40-140
57 {G140r't2 3&r3r)74 3&1974 n-196' tEl10@ 3Gt3062 1&11098 fi-1fu98 n-1@64 lF1lA
1.m1.001.001.001.001.000_2001.001.001.00
1.000.200r_001.00
1.001.001.001.001.001.001 0 00.200Lm1.00
100r00'r00
rfi)100100100100r00100
1001@,N1Cl)IN1M1(ntm
't00
1001(X)1mt001m100'100
100r001001001001001001001M,an1001001001(n
BRL
BRL
BRL
BRL
SRL
BRL
BRL
ARL
BRL
BRL
6RL
BRL
BRL
BRL
BRL
BRL
BRL
BRI-
BRL
BRL
BRI.
ARL
BRL
BRL
mmmm
2020202020202020m
32
5
25
3
tidks u/€t
ldkg vrsl
$/t(g c/€l
l€ftg wet
UgkS wel
Pg/kg,.€tldkS vret
3:103303303303303ilo330
This l&torqtarf epatl ls not vdid tltdhotd s 4ttdrorhd sig,,tzture on &a coe6 N4' R€portabh kectioo LiEJt BRL = B€low R€F.ting Limit Pige l,l,l of I55
Page 654
Semivolatile Organlc Compounds by GCMS - eurlify Conarol
Spike
l-€vel
SourcrResult
%RECLimits RPD
RPDLimit9/OREC
B.tch 70Jl514 - Sw84d 35S0B
Alenk fl tlSl,tALKl)
Pr€p€redr 26-Mar-07 Anatyzet 27 _Ma.-O7
Benzo (a) antfiracene
Benzo (a) pyrene
Eenzo (b) fluo€nthene
Benzo (g,h,i) perylen€
B€nzo (k) fluorani\ene
Benzoic acid
Benzyl alcoholgis(2drloroerhoxy)msthane
Bls(2-chlorc€6hyl)ether
8i$(2-dloroisopropyt)ethergis(2-olhylhery')phthatare
{€romoph€nyl phenyt ethertuVl benzyl phthatate
Cetbade
4{hloro-3fi ethytphenol
4€hlo.o3nilin€
2-Chloronephthatene
24hlorophenol
4-ChlorodEny' phenyt ether
Chrysen€
Dibenzo (a,h) anthracene
Dib€rEofurao
| ,2-Did orobenzene
1,3-Oichbmbenzene
1,+Oichbrob€nz€ne
3,3'-Dichbrob6nzidine
2j-oichkrcphenot
Diethyl phth5late
Oirn€thyl phthatale
2,4-Oimethylphenol
Di-n-butyt phlhetale
4,6-Dinilro-2{eflytphenol
2,+Dinihophenol
2,+Dhihotoluene
2,o€lnibo[oluene
Di-n-oclyt phthalate
Fluorsntl|ene
H€xachlorobenzene
H€xed oobucadiene
Hexad{orccydopentadi€ne
Indeno ( 1,2,3-cd) pyrene
1-lrefrylrlaphthabn€
2-l4othylnaph$atene
2Jr4ethylphenol
3,4-Methylph€flol
Naptthalene
2-Nilrosnilin6
$Nihoani&|o
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
8RL
BRL
ARL
ARL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRI.
BRL
BRL
8RL
8RL
BRL
BRL
BRL
BRI.
BRL
8RL
BRI.
!g/r(g wet 330
ps'kg wet 330
pg/kg wel 330
pgr'kg net 33o
!g/kg wet 330
t gitg wet 330
!!r'kg w€l 330
pgllgwet 330
pqy'kg wet 330
pg/kg wet 330
!g/kg wet 330
pgkgwel 330
lgikg w€i 330
pg/kS vret 330
!gL/(g rN€t 33O
pg/kg wet 330
pdkS wet 330
Ug/kg wel 330
r4/I9 wel 330
!g/kg wet 330
Fqkg w€t 33Opdkg wet 330
fgr'kg wet 330
pg/kg wet 330
Ug/kg wel 330
!g/kg wst 330
!g/kg wet 330
lg/rc wel 3:]0
pg/kg wet 330pgks vJet 330
lgr'kg wst 330
!g/kg wet 330
Lig/r€wel 330
lgL/kg wer 330
pgkgwet 330
!g/kg r,t€t 330
!9ft9 wel 3il0
!q/kg wet 330
pdkg wet 330
pdkg wet 330
pg/kg wet 330
!g/kg wet 33O
Lig !g wet 330
Ugkg vret 330
pg^g wel 330
pg/kg wet 330
!g/lq wel 330
ugr'kg w€r 330pg'l(g wet 33O
lgy'xg wot 330
ldtS rvet 33O
This latamlory repo.t k ,nl talid drhot t oi zslhori@d sipnture on th. cover We. Reportable D€t€ction Limit BRL = Below ReDortins Limir Pag€ 145 of 165
Page 655
Scmivolatile Organlc Compoutrds b' GCMS - Quality Control
Analyte{s) Result Flag
Sourc€
R€sult %RECUnitsSpikeLevel
%REC
Limitj
RPD
LimitRPDrRDL
Ellch ?mr514 - SW846 3ss0B
Blank t70315l{€LKt}
Prepa.ed: 26-ldar.07 Anglyzad: 2l -nnat47
4-Nitrodiline
Nilrob€uen€
2.Nllrophenol
4-Nitrophenol
N-Nitsosodim€lhy'amine
N-Nitrosodi-n{'ropylamine
t&NitroEodFhenYamine
Phenanlhren€
Pheml
Pyriline
1 2.+Trichla,roben2ene
2,4,s-Trichbmpheml
2,4,ATnchbroph€nol
Surogale: z+heobiphenfS unogafu : 2+ luotoph en o ISu/|icgat3: NillobnzenedsSuftrga/€: Phercl4sSu''ogaig: Teryhenyt4ltSuiogale: 2,4,6-Ttibrcnrcph o|
LCS a?03t51{-AS1l
Pr€p{€d: 26JL{ar-07 Anavzed| 27 4,na'.07
Acenaphtlyl€n€
Azobenzen€/Diphenyldiazine
Benziditle
B€nzo (e) snthracene
Benzo (a) pyren€
B€nzo (b) fooraothene
S€n2o (g,h,i) perybne
Benzo (k) frroranth€ne
Benzolc acid
Benzyl alcahol
Bis(2drloroet\ory)m€dlane
Bb(2dtloro€f tyl)€ther
Ais(2-dlbrcrsopropyFt[t€r
B s(2-€thyltt€xyl)ph$alale
4-gromoph€ny' phenyl 6uler
Butyl b€nzyl phthalate
Caftdzde,l4hlorclm€thylph€nol
4Chbr@niline
24hk ronaphthaler€
2€hlorcph€nol
4€hktroptEnyl ph€nyl etlr€r
Chrys€ne
Dit€rEo (a,h) anfiEc€ne
BRL
ARL
SRL
BRL
BRL
BRL
SRL
ARL
BRL
ARL
8Rt
BRL
BRL
BRL
BRL
ffig59m6660a2m6741)42m
57706380788064m96907260BRL54306090514051806al0
50306190636035406't605160611081105810sSgO5730&205S905E:1057fi
13203in3301320330330330330:It03it0330330gt0
33030
!g'xg r"et
lgr'kg $'el
rcn(g wet
Fg/t(g w€t
t gn(g wst
Fgrtg w€t
pdfg vr€t
lgxS wel
pgy'Ig wet
lglkg wet
pgtkg wet
$I€ wet
lrg/tg w€t
pqrg $el
pdlg wel
Ugr'kg $/et
rc/kg Yret
!g/t€ wet
IrgJkg w€tpg/kg wel
Ugtg w€l
ligkS Y{et
lgr'l(g wet
lgrkg wet
w'kswetqc2 !g/kg wet
udkg rv€l
pdkg v'€l
ldkg Yr€t
ldkS wet
lgLr'kg wet
pglq wet
pgiko wst
Igrkg wel
pgutg w€l
ldkg vrel
!g/kg w€t
!S/kg Y{et
lgr'kg wet
pdkS wet
pgftg wel
IdtS t!'€t
pqkg w€l
pdkg YJel
UdkS wet
ldko vret
!g/ko rYst
lrglq wet
pg/kg wet
90 30-t 30N 11110100 30-13093 1*1101O1 30'1306:J 1U110
€7 40-'t30s6 40-130118 40-13096 40-130't48 40-130109 40-13)
0n 3081 40-13091 40-13077 4r)-13078 40-130102 40-13076 0-13t)
75 4G130
93 40-13005 40-13053 40-130qz 44-1n
f7 4+1n
92 {1130122 4Gr3087 40-130
90 {1130
8€ 40n3063 {-130so 40-130
87 $-13/J86 4G130
3'0$o
3303303303303303303:10330330
330:I}03303303(i0330330330330:l:r0330330330
330330
667066706670667066706670
66706670667066706670667066706670667066706470ffi706670
667066706670667066706670667066706670€67066706670867066706670
Thit bbodoryeport ls not volid ,ithoA an aurtofiaal sFnzfiln on the coea l,age.' R€portsble Detection Limit BRL = Below Reporting Limit Frge 146of 165
Page 656
Semivolaail€ Orgatric Compounds by GCMS - Quality Control
Ana!,te(s) F-lsgResult UnitrSpike
Level
RPI)
LimitRPDIRDT-Source "/"RICResult %REC Limits
Batcb 7031514 - SW846 3s508
LCS {703t514€S
Prepared: 2SMar{7 Analyzed:27 -l a(41
Dibenzofurdn
l,2Oichloobenzerc
l.3ObJ orobenzerNe'I,4olaf orobenzene
3,S Oichlorobenzlline
2,4Oichlorophenol
Di€tfiyl phlhslab
Dim€thyl phth€lab
2,+Dim6thy'pt'€nol
Di-nautyl phthelate
4,6-Ohi!to-2.methylphenol
2,4-Dinihopherbl
2,4-Dinihotoluene
2,6-Dinihotoluene
Di{-fttyl lhthalatsFftroranthene
Fluoaeno
ilexachlorob€nzene
H€xachlorobutadaene
H€xechlorsydop€ntadiene
hdeno (1,2,3-cd) py€ne
1 +vtsthylnaphthalene
2-tvlethylnaphthalene
2{vlelhylphonol
3,C-n/bthylpfEnol
Nephthal€ne
2-l{ilroanitine
3{,lltroshlllne
4.$litrmhilin6
Nitrotenzene
2{.litophenol
4+tibopfi€nol
N-Nftro6odinehylamin€
N-l,litrosodi-n-propytamine
N+,{itrosodrph€nylamine
P€ntachlorophenol
Pyidin6
I ,z,+Tdd oobenzene
2,4,$Trichloroph€nol
2,4,GTridrlorophenol
S urogate : 2-F hnro b i p ha n ylSmogaae: 2-FluonphenolSunqate: Nitofunzene4sSunogete: Phenol4'Suftogale: Tephonyl4l4S wogab : 2, 1, 6-T ti b @ ft 10 p he nol
593049804270517058505260583055605 1 r 058803900479054405760710054306240509055r048005050503061006460610047905630613055S06250772066105 1 1 0359054903150671046705300530057704050562052404250643048207430191062905280
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6€70
6670
6670
6670
6670
6670
6670
6670
667066706670667066706670
!g/kg wel 330
pg/kg w€l 30
!g/kg r€l 33O
!g/kq wel 330
pg/kg wet 330
!g/kg wst 330
!g/kg r /et 33O
Ug/kg wet 33O
Ug/kg wet 330
!g/kg w€t 330
USftS vJet 330
ug/kgw€t 33O
lgr'kg wet 330
Fgkgwet 33O
lgr'kg 'Net 330
pg/kg \a/et 330
Ug,4€ wet 30
pgr'kg wet 330
tgftSwet 330
pgr'kg ret 330
pg,4(g wet 330
pg!49 wet 33O
pS/qYret 330
ISAS wet 330
pg,4qw€t 330
UgrS wet 33O
lgkg wet 33O
!g/kg wet 330
ldkS wet 330
!g/kg w€t 330
!g/kg wel 1320
rrg/ko wet 330
t/g/kg wel 330
lg/ftg wel 1320
rc/kg w€l 3n]
Ugr'kg wet 30
ug/kg wel 330
pg/kg wel 330
pg/kg wst 330
pg/kg wet 330
|Jq,,kg wel 330
!g/kg wel 330
gglgwet 330
!9r'k9 wet 330
lgr'kg wet 330
ldkg v,/et
Ug/tg wetpgfl(g wetpgks YJeipSIq vJetpdkg Y{et
89 40-130
75 4G130
64 40-130
78 40-130
Ea 10-130
79 4G130
a7 40-130
83 40-130
77 40-130
88 40"130
5a 40-130
72 40-130
82 40-130
86 40-130
106 40-130
El 40-130
94 40-131
76 4{t130
a3 40-1m
72 40-130
76 40-130
75 40-130
9l 40-140
97 40-'t30
91 40-130
72 40-130
u 10-1311
92 40-rm
84 40-130
94 40-130
116 40-130
99 4G130
]t 15130
54 4G't 30
82 411130
47 40.130
101 4G130
70 40-130
73 40.130
79 40-130
e7 40-130
61 40-130
a 40-130
79 40-130
64 40-130
96 30-13072 15-110
111 30-1m74 1511094 30-13079 15-110
Thit lnborutory ftpo.t it iat wlid dlhout 6t oaiho.ized sEnatzre o.t thz co'er Fge.
* R€ponnble Detedion Limit BRL = Below Repo.ting Limit Pase 147 of 165
Page 657
Semlvolatile Orgrric Compounds by GCMS - Quality Contlol
Analyte(s)Spike Souri;e
Flag Units Result %REC Limits
B"lch 70lrsr4 - Sw846 35glBDuollcatafl031514-ItuPll Sourca:sA5oG'71-18Prepa€dl 2&l\rar{7 Analyzed: 27 .{MaFO7
Acenephihyiene
Azobenzone/Dipheny'diazne
Bervidinegenzo (a) antlracene
Benzo (a) pyr€ne
a€nzo (b) nuoranhene
B€nzo (gll,i) p€rylene
Benzo (k) ffuorantfEne
Bsnzoic acid
Benzyl slcohol
ais(2-chbroethory)melhane
Ais(24hbro€$yl)e.tr|er
Bb(2-.*rlorcisopropyllether
Bis(2-ehyihexy')$rlelat€
4€romophenyl pheny' eut€l
BUV benzyl phlhalate
C€bazole
4-Chhro-3{6lhybhend
44hloroanilne
2-Chlo.onaphffElene
2-Cl olophenol
44hloroph€nyl pheny' etqel
Chrys€ns
txbenzo (a,h) anhr@ne
DibenzofiJaan
| ,2-DidrlorobenzerE
1,&Dicl orob€nzene
l,4orchlorobenzene
3,3'-t)id rrob€nzidin€
2,4-Dichlorophenol
Olehyl phhehte
Dinretryl pfiu|alal€
2,+Dim€tnylphenol
Di-n+utyl phtlhalab
4,6-Onilro-2<nethylph€nol
2,4Oi.nitrophenol
2,4.oinifotoluene
2,G-Dinibotoluene
DLn-octyl Atlt€labFluorantherle
Hexachbroberuene
Hexachltrobutadiene
Hexachlorocyclogentadlene
HexachloroehEne
Indeno (1,2,3d) pyr€ne
lsophorfi€
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
SRL
SRL
BRI.
8Rt
BRL
BRL
ARL
SRL
BRL
BRI.
BRL
SRL
BRL
BRL
BRL
BRL
8RL
SRL
BRL
BRL
BRL
BRL
BRI
8RL
BRI
BRI
BRL
BRL
ARL
BRL
BRL
8RL
BRT
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
ARL
l,gikg dry 699
lgtgdry 699pC,19 dry 699
lgtg dry 699
dkS dry 6s9pSn(S dry mgpdks d.y 6S9
tdks dry 69€pCikSdry 699pC,tg dry 699pdkg dry G99gdkS dry 6sg
USI(S dry 6eg
tdksdry 699
ldks dry 699
UCI(S dry 699
t'dlg d.y 699pdkg dry 6sg
UdkS dry
lgrSdry 699
lgkgdry 69s
Udkg d.y 6S3
ldks dry 699
Fdks dry 699
ldkgdry 6S9
ltglkSdrJ 6S9
udksdry 609
UdkS dry 699
t gftg dry 699
rdtsdry 699pdks dry 69spdl(g dry 699
ldxgdry 699
ldtS dry 699
udrsdry 699
lgkS dry 699ptS/kS dry 699pdkS dry 699pdkg dry 699pdksdry Gge
tdkS dry 699gdkS dry 699
|€iks dry 60e
Igrkg d.y 699pSftS d,y 699
ItSlkSdry 699pdkgdry 699
ldksdry 6sg
lSkSdry 699
ldkS dry 6sspS/kg d.y 699
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRT
BRL
BRL
BRL
ARLgRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
SRL
8RL
BRL
BRL
BRL
505050505050505050505050
50505050505050
5050505050
50505050505050505050505050
50505050
50
5050
Ihlt talro.atuy .qod is Aot rlau wit,,ord on aathodztd signattue o" dte towr pg..
I Repoftble Dct€ction Limit BRJ- = Betow Reporting Limir P.ge 148 of 165
Page 658
Semivolati le Organic Compounds by cCMS - euality Control
An.lyre(s) *R.DLFlag UDrNResultSpikefr:veJ RPD
RPD
I-imit
Sdurce %REC
Resuli %R€C Limirj
B.hh 703151{ - SW846 35508
. Duollcatd 11031 514-OUP1 | Sourc€: SASE6Tl-18
Propded: 26-t!,f ar07 Analirzed: 27 -Mat-O7
1+rehMr|aphthalene
z-avlethylnaphthal€ne
2{vlethylph€nol
3r-lvl€lhylphenol
Nspl{hal€n6
2J,lltrcaniline
3.tllhtanlhne
4J.li['o€oiline
l,lilot'enzene
2+.lit bphenolr|'|{boph€not
N+lih6odknethylamine
N-Nitrosodi-n-pmpy'amine
t[Nibosodipft enylatn'n€
Phenol
Pyridine
J J,il-Tricf rlorobenzeoe
2,4,STridrloroph€nol
2,4,&Trichloroph€nol
S urioga E : 2 -F luor&i p he n y ISuftogate : 2-Htlotodlenolsu'rosEta- /vlLoD€nzgre{sS|l'|'cf,al€: Phenol4sSlJllogate: Teryhenyt4l4S ut og ate : 2, 4, 6-hbron o p h e n ot
Pr€Fr6d: 26-lvlar{7 Analyzed: 27 -Mat 47
4-Chloro-3{€thf phenol
z{|llorcgh€nol
1 ,+Olcf[orobenzene
2,+Dhltsotolue{|e
4{ibopheml
N+.litro€odi-n{mpylamine
Ph€irol
Py.ene
1 ,2,+Tricl orcbenzene
Sutogate : 2 -Fluorobiphenyl
S/]'togrl€: z-FhJomphenolSuflogak:Nftrc&nzene4'Sunqate: Phercl4,Suno8,ete: Teryhenyl4l4S ffi qal3 : 2, 4,&T nbm n o p h €not
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
6750538063705490726043en
4940907082S043104310573051707300850055403970
uu)445058604ioo6230458o
]|rt ir Aolk. Dip a703l514-MSDi I Source: 5A596?1-18
Pr€par€d: 2Gt ariT Analyzed: 27 -Mat47
507092008430
Acenaphfieoe
C{hloro-3{ehylphenol
24hloroph€nol
pg/kg dry 699
US/ftS dry 6S9
Lig/kg dry 699
ug/kg dry 699
trg/kg dry 699
t/g/kg dry 699
trS/kg dry 699pg/kg dry 2800pdks dry 699pdkg dry 6S9pdkSdry 2800
ldkg dry 699pq/kg dry 699
!g/kg dry 6S9
ldkg dry 699
ldkS dry 699
t/g/kg dry 699
!s/ks dry 699
!g/kg dry 699
t/g/kg dry 699
!S/kS dry 699pg/kg dry 699pdks dryLig/kg dryug/kg dryugl(S dryldks drypg/kg dry
!S/kg dry
!9&S drypqks dry
S4(g dry
ldks dry
lgkS dry
ldks drypS/kS dryps/tg dry
udks dry
US/kS dry
tiS/kS drypg/kg dry!g/kg dryrcftg dryug/kg dryudkg dty
!S/kS dry
!g/kg dry
!s/kg dry
3533533533533531410353353
353353
70707070707070/o70707070
7120142001420071207120142007120142001420071207120712071207120712071m7120
707014rAO't 4100
BRL
SRL
BRL
3tLt u15-11030-1301Ul1030-13t)15-110
40,14030-13030-13040-140{o-14030-13040-'14030-13030-13040-14040-14030-130t r l t o3G1mt5tt03t]'13015-110
40-r403&1303G130
BRL
ARL
ARL
BRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
ARL
BRL
BRL
BRL
ARL
8RI
ARL
BRL
BRL
BRL
ARL
505C505050505050
5050505050505050505050505050
95/69078t0362
Iafix Soite fl03151+$Sl) Source: SA5967'l-18
350350350
ma+5861
407351607A56
6282ffi8864
72
6023
30
n30
Thb laborabry Epott ls not ealid h,ithoat an authorlztd signatu. on thz covr page_
* Reportable Dekction Limit BRL = Bclow Reponing Limil Page 149 of 165
Page 659
Semivoladle Organic Compouod$ by GCMS - Quslity Control
Anabte(s) Result Flag Units Result %REC Limits RPD
Brtch 7031514 - SW846 3ss0B
Matrtu Sotks Ouo ft0315t,t itso Sourte SA5967t-t8Prepar€d: 2&l\rar{7 Analyzed: 2l -Mat47
438t)144057305200783085705350,O7o
563011fi61304410666046@
BRL
SRL
BRL
BRL
BRL
BRI.
BRL
BRL
BRL
BRL
BRL
ARL
aR|-
BRL
BRL
BRL
BRL
BRL
BRI
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
8RL
ARL
aRl
ARL
8RL
l,4Oi(,|lorob€nz€n€
2,4Oini0otoluefi€
4-llitrofhenol
N+llho€cdi+proOrylamins
PenLacilorophet|oi
1 ,2,4-Tndbrcb€rEefle
Su fl ogate : 2 + I uon tiphen ylS u nEgate : 2+ luo toph enolSutogate: Nitobenzene4 5Suftogate: Phetd45Surogale: fetphenyld4S u ftog ele : 2, 4, 6-f dh @nophdtol
Brrch 113 1592 - SwE{5 3S45A
Blank 1703150?€LKl I
Pr€par€d: 27+rar47 Analyzed. 2B+td 47
Acenapht|€n€
Azobenzene/Diph€ny'diazin€
B€nzidine
Eenzo (a) antkacene
Benzo (a) pyrsi€
Eenzo (b) fuordnhene
BerEo (g,h,i) p€rylenegenzo G) nudanllEne
Eenzoic acid
Esnzyt alc hol
Bis(2-chloroethoxy)melhane
Bis(2-chlo.oehyl)€ttler
Ais(2-chlorolsopropyl)€lh€r
Bls(23trhylfi exyi)phthalate
4{romoph€nyl phenyl et1e.
BUM benzyl phthslale
Carbazole
4€hloro-3fl €Ihylph€nol
44hlor€nilin€
24hloronaphthakn€
2{hlotrophenol
44hb.ophenyl phenyi ef|€.
Ch.yEen€
Dit€nzo (a,h) anthracene
Dibenzofuran
1 2-Dichbmberuene
1 ,3-Did orobenzene
| ,4-Di{:hlorobenzene
3,3'.Didrlo'rob€nzidin€
2,,|-t)i.* oroph€rc|
tlg/ks dry 350pdl(g dry 350
ldkgdry 1400
lgkS dry 350
t dl€ dry 35Opdks dry 350pSfts dry 350pgtS dry 350
sdkS dryldkg dtYrdkg dryrdks drypdkS dryrdkg dry
62 4+14063 4G'4041 30-13075 44-14l)56 3&13061 3&13084 40-1,1058 4trr408A &-13o63 1r1to87 30-13062 15-11094 g-13066 16110
70707070141007070t4100t410070707070747070707070707070707070
BRL
BRL
SRL
BRL
SRL
ARL
BRI
BRL
2323
7
3030303030303030
lgr'kg wet 165
Ig4€wet 165
Fglkgwst 165
pdts vrel 165
Fgr'kgwel 165
t g/Xg w€l 165
trglq wet 165
$4(g wet 165
pgllg wet 165
pgikgwet 165
UgkSwel 165
lcrtswel 165
Ugr'kg wer 165
Ugfkg er€t 165
pg/kg wet 165
l4/kg wel 165
pgrn€ w€t 165
pdkgwet 165
Udkg Yr€t 165
pgL/kg v/et 165
Ugr'kg wet 165
Ug/!g wet 165
Ugil€vr€t 165
!g/kg wel '165
lg/kgwol 185
ldkSw€l 165
IdkS v,/€t 165
t|.Jr'kg 'r,et 165
Fgnqw€t 165
ggitgw€t 165
pdkgwet 165
tgr'kgw€t 165
UdkS$€l 165
!S/kS w€t 165
This laboratory rqod ls noa tsud wilhou an atdtodsy' sigrraare on the caw pqe .
' R€portoble Detectiod Limit BRL = B€low R€portine Linjr Page | 50 of 165
Page 660
Semivolatile Organic Compounds by GCMS - euality Controt
Source
Brtch 1131592 - SW846 3545A
A|a.rk t703t59a.BLKt t
Prepar€d: 27+vla.47 Anal].zedt 2&MaF07
Diethy' phtharate
Dknelhyl phtheLate
2,4-Dirnethylphenol
Di-fiSrtyl phthalate
4,&Dinilro-2-methylphenol
2,4-Dinitrophenol
2,+Dinihoblu€n€
2,6-Dinibololu€ns
Oi-n-oclyl phtlnitat€
Fluo€nthene
Flrorene
Hexachlorobenzene
H€Edrlorobutldiene
H€r€cHoreyclop€ntadiene
Hexacfiloa€than6
Indeno (1,2,3cd) pyrene
lsophorone
1-lrelhylnapht\alene
2-lvl€thylnaphthal€n€
2+,lehylphenol
3,4-Melhylph€nol
NEphthel€ne
2{,litroenilins
3-llilroeniline
4{[loanlllne
NiSobenzene
2+{ilrophenol,l{'liboph€nol
N-llllrosodimethyhmine
N-Nhrosodi-n-propytamine
lJ-Niro€odiphenylanine
P€ntedlloroph€nol
Phenantfu€ne
Plrenol
Pyren€
Bdtine'l,2,+Trthbrobenzene
2,4,tTri{nbrophenol
a4,&Tnd oroDh€nol
S u fi ogele : 2+lvomb i phe n ytSunogele: z+lwtuphenolSunogab : Nibo66nzeden5Swtog6l6t Phanol-dsSurrogale: f erphsnyt-dl4S./''ogate : 2, 4,eTd fuo n o p h e n ol
LCS fl0ilt5g2gs
Prepared: 27-l,lar47 Analyzed. 2A -MarO7
Aconaphhen€
Acenapht\yien€
Andlne
Anlhracene
BRL
BRL
BRL
BRL
BRL
SRL
BRL
ARL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
ARL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
6RL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
280026703250273031302180
2400
2 6 1 0
3550
2570
3330nmgm333033303330
3330333033303330
u849882
65
7278'101
77
!g/kg wet 165
!g/kg \Net i65
pg/kg re€t 165
pgltgwet 165
lgr'kg wet 165
!g/rg wet 165
pgr'Kg t'/et 165
Ug/Kg ',vet 1 65
Ugkg wet 165
Ug/kg wet 165
ygr'kg wet 165
Ugi/kg wet 165
Ugirg wet 165
Ug/Kg wet 165
lgftg wet 16s
Ug/kg wet 165
!g/kg wet 165
pgi kg wet 165
trg/kg wet 165
pgkgwet 165
UgAg wet 165
lrg/Kg wet 165
UEkg wet 165
UqL/kg wet 165
UgL/kg wet 660
ug/kg w€t 165
Ugr'Kg wet 165
Ug/kq wet 660
pg/kg wet 165
!g/kg wet 165
lgr'Kg wet 165
!g/kg rlet 660
!g/kg wet 165
!g/kg lYet 165
pgr'kg w€t 165
!91!gw€t 165
lgL/kg wel 165
tgftg wel 165
pq!4q wet 165
uEkg wetUgftg wel
Ug/kg wei
!g^g w€l!g/kg w€lUg/r€ wel
Ugr'kg wet 165
!g/kg wet 165
lgL/kg wet 165
Yg/Kg wet 165
30,1m| 5-110SGIN15-1101I1m15-110
4G130
4o-130
4o-130
40n 30
Thit hborutory rcporl b tua velid wirhout an strtorized signatue on the cover page.
* Reportabl€ lxtection Limit BRL = Below Repodng Limit Page lJ l of 165
Page 661
Semivolatile Organic Compounds by GCMS - Quality Cortlol
Source
B{tch 7031592 - SW846 3545A
LCS f7(Bt592€:t1)
Prepared: 27jvlar47 Anal]/"zedt 28]tlar47
Afalne
Azobenzene/Dqrhonytdiazine
B€nzidine
Benzo (a) anthracene
B€nzo (a) pyrene
B€nzo (b) fluor€nthene
Benzo (g,h,i) p€rylene
Aenzo (k) nuorar||hefle
Benzoic acid
B€nzyi alcohol
B6(z-chb{oed\oxy}nethane
Bis(2-€nbro€trnyi)ether
Bis(2d oKisopmpyl)ether
Ais(2-€thylh€xyl)phtralat€
4€ornopheny' [ft enyl ether
B0ty' benzyl phthalate
C€rbazoie
,{-Chloro-3{rEhylphenol
44hloroanilne
2-Chloronapfitl|alen€
2-Chloroph€nol
44hloroph€nyJ phenyl eher
Chry6ene
Dlbenzo (a.h) antn.ac€ne
Diben:ofuran
1 ,2Oicnlorol,€nz€ne
| ,3-Dichlofobenzen€1,4-Dlchlorob€nzene
3,3'-Dichk robenzidine
2,4-Di:hbroph€nol
Dlehyl phthabte
Oimethyl phthalate
2,4-Dlmethylphenol
Di-+butyl phlhalate
4,6oiniko-2-met\t$'heml
2.4-DiniboDhenol
2,+Dinilrotolu€ne
2,&Dinitsotoluen€
Dl-n-oclyl phthalale
Hexad orobenzene
He)(act{o.obubdion€
Hexacfi lorccydopenHi€.E
Hexachldoslhane
Indeno (1,2,3d) pyrene
1 +,tetMnepttfulene
2+ ethytEph{halene
2-tlrelhylpnenol
3,4-Molhylphenol
515029401430243026tX)2'/0
235026802!60254028002f5027AO22$'027lO3420250025802$0213{J239024602690249022702020zno28602244244025002120252024m2920282028102360214024602m02200217021202790269023tO244022302620
3{t303330333033303330333033303330333033303330333033303:X)033303l}l]033:1033303330333033i1033:'0ix)303:,303:raro3330333033303330333033:]033:103330333033iX)333033:)0333033303330333033303330
3:}:X)3330333033303:[t0:t330:Ii30
Oc2 lgn(g w€t 165
Irdkgd 165
yg^gwet 165
Ug/tg vr€t 165
!dkg',v€l 165
Ugtkgwei 165
lgr'kg u,et 165
Ig/kgwet 165
tdkgw€l 165
!gr/k9w6t 165
Ug/kg e/et 165
pg/kg $el 165
pgr'kg wel 165
pgr'kgr,€l 165
Igr'kg wet 165
lgkS !^ret 165
Fg/kgra€t 165
pdls$rel t65
Ugrlg rst 165
rdl1g t d 165
Fg/kg wet 165
Igftg wel 165pdkgw€l t65
lgrkg i,€t 165
US/kSwet 165
tgl(gwet 165pgtg wel 165
!gr'kg$,16r t65
lgkS r€t 165
$gkgwet 165
Wkg w€l 165
lgn(g wet 165
pgftow€t t65
ugkS Yr€t 165
rctkg wel 165
Ig/|(gwet 165
pgkgw€l 165
lgfl(]g rret 165
!gr!S,,{et 165
pg/kg wet 165
ygr'ko wel 165pgkgw€t 165
ldkg n€t t65
Udkgwot 165pgikgw€t 165
lgL/tg w€l 165
ldkgw€l 165
Ug/kg wet 165
UdkSwet 165
pSrlSr,r€t 165
pgr'kg wel 165
155 40-1308a 40-t30
4i, G13073 40-13078 4G.13077 40-130
n 40-1g]71 44-1n80 0-13074 4G130
76 .t{t130
84 40-13083 40.13083 40-13068 4{tr 308r 4G13t)103 40-13075 ,O-t3o
77 4613072 40-13064 40-13072 &-13074 40-13081 ,m-130
75 40-1m68 40n 3061 ,lO-l3O
69 4G13086 40n30
67 40-13073 40-13075 4G130
64 40-13076 40-13072 4A-13o88 {G13085 4G13)04 ,10-130
89 4G13073 40-13074 ,rS130
66 4$.r3o66 4+.13065 40n3064 r()-13O
84 4t)-1300r ,(rr306S 4&14073 4&13067 rl&130
79 .t{t't 30
Thb labo.olaq rcptl ls notvslitt *|t!toc! oE aatlodzd tlgn./,.E oE fie.,w. pagc.
a Reportable D€tecdon Limit BRL = B€low R€portiag Linir Page 152 of 165
Page 662
Semivolatile Organic Compounds by GCMS - euality Control
Brrch 7031592 - SW8{6 3s4sA
LCS t70fi592€31l
Ptepared: 27-[rar{7 An3lyzed: 2A-Mat4f
Nsphbalene
2+liboanilinegNihosniline
4-Nilrcaniline
Nitrobenzene
2+liuoph€nol
4+{irrspfienol
N-Nibosodimethylathane
N-Nitosodi-n+r@ytaman€
N-ffi trosodiphenylahine
Pllenol
Py.idine
I 2,+Trichlorobenzefle
2,4,tTrichloroph€nol
l,4.eTdctiorophenot
S u nogdle : 2 -F I uotobi ph e n y ISunwate : 2 -F I uotoph e nolS urqate : N itto tten z e ne 4 5Sunpgate: Phenol4,S/u/rngel6: Tepheni4l4Sunrgah. : 2, 4 a-f n bmnn p henol
Ouottc.te {7031592{up1 | Sourc€: SASE6ll-16
24102620301037402410230018002410240027AO22502330213022701800232021301S30258021308D2250263023m
BRL
BRL
BRL
BRL
BRL
BRL
SRL
BRL
BRL
ARL
BRL
ARL
ARL
BRL
BRL
BRL
BRL
ARL
SRL
BRL
BRL
BRL
ARL
BRL
8RL
3330333033303330333033303330333033303330333033303330333033303330333033303330333033303330$n3330
!g/kg wet 165
!g/kq wet 165
Ug/kg Y/et 165
!g/kg wet 660
lgr'kg wet 165
lgr'Kg wet 165
!g/kg wet 660
!g/kg wet 165
!g/kg wet 165
t g/kg wet 165
pg/kg wel 660
lgkg w€t 165
lrg/Kg wet 165
!g/kg wet 165
!g/kg wet 165
pg/kg wet 165
Ug/kg w€t 165pg/kg wet 165
FEr(g welUg/kg wet
uEXg welpg/kg w€tt g/kg wetPgr'kg wel
pgkS dry 370
UgftS dry 370pg,'ks dry 370
pdkS dry 370
pgxS dry 370
[gKg dry 370
pdkS dry 370
!S/rS dry 370
UdkS dry 370
pS/kS dry 37O
pg/kg dry 37O
!s/ks dry 370!Si*S dry 370
Pg/kg dry 370
!S/kS dry 370
rdks dry 370yS/xS dry 370
udks dry 370
!g/kg dry 370
t g/kg dry 370pS/kS dry 370pdkg d.y 370
t4/k9 dry 370
Pdks dry 370
trg/lq dry 370
72 40-130
79 40-130
90 40-130
112 40-130
84 40-130
69 40-130
54 40-130
12 40-130
72 40.1fi
83 40-130
6a 40-130
70 40,130
64 40,130
68 40.130
54 40-130
70 40-130
64 40-130
58 40-'t 30
// 30-t3066 15-11092 U-t 3068 15-11079 34-19lo 15110
fuepared: 27-Mat47 Analyzed: 28&laG07
Azob€nz€n€/Diphehyldiazine
Benzidine
BerEo (a) anthrac€ne
Eenzo (a) pfene
Senzo (b) fluoranthene
B€nzo (g,h,i) peryene
B€nzo (k) fluoranfEne
B€ruoic acid
BerEyl alcohol
Bta(zdrlooethory)rnelhane
Bis(2d$roehyl)eUEr
Eis(z-€f doroisopropyl )elherBis(2-€fi Mh€xyl)phthalate4Sromoph€ny' ph€nyl ether
Butyl benzyl phth€late
C€lb@ol€
44hbro-3{etlrylphenol
44hbroaniline
2Chlorcnehthal€ne
24hbrcptEnol
ARL
BRL
ARL
ARL
ARL
ARL
BRL
8RL
ARL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
5050505050505050505050505050505050505050505050
50
Th/J laboratort 4pora is Aot dU xlthout an rulhortze.t signarae ott the .over page_
+ Rqlortable Det€ction Limit BRL = Bctow R€porting Limit Page 153 of165
Page 663
Semivolatile Orgrtric Compoutrdi bv GCMS - Quality Controt
Analyte(s) Result FluC Units Result %REC Limirs
Batch 7031592 - SwE453545A
DuollcaterTfi'lsgz{)UPll Sourca:SA59C4t.t€Prepar€d: 27-Mar{7 Anal}rzed: 28-Mat47
{-Chbropheny' phenyl ef'rer
Chrysene
Dibenzo (a.h) anhrac€ne
Dib€flzofuran
| ,2-Dichlorotr€nzenet ,3-Dicilorob€nzeno
l,4oichlorsb€nzer€
3,3'-k orut €nzidine
2,4Oichlorophenol
Di€lhyl phlhalate
Dimethyl pfilholale
2,+Difi€thylph€rlol
Di-n-butyl phth€bte
4,6-Dininci-2-fi ethylphenol
2,4-Dinihopherbl
2,+Oinitrololuene
2,6-Danitrotoluene
Di-fl-octyl phthalab
Hexachlorobenzeoe
Hexachlorobutadiene
Hexachlorocydop€ntadiere
lndeno (1 ,2,3-cd) py.ene
1 -t{€f'ryidaphthal€ne
2-1!|€thylnephthalene
2+rethybhenol
3,4{,1e$rylDharbl
Naphthel€ne
2-l'lltroanilin€
!Niboanifin€
4{'lihoanilin€
Nitobenzene
2-f'lltrop|lenc,,k{ihophenol
N-t!ikosodimethylamine
N-Nilrosodi-n-propytamine
N-Nitrosodipltenylamine
Ph€nEnihren€
Pfienol
Pyridine
1 .2,+Trl.hlorobedene
2,4,STddibropherrcl
2,4,ATddbr@h€nol
Sufiogate: 2+luoabiphenylSwrcgate: 2+hrorcphenolS u nogate : N inob€ n za ne-<t 5
BRL
BRL
BRL
8RL
8RL
BRL
BRL
8Rt-
BRI.
BRL
BRL
BRLgRL
BRI
BRL
SRL
ARLgRL
BRL
BRL
8RL
sRt_BRI.
BRL
8RL
ARL
BRL
aR[ARL
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
sRt_SRL8RLBRLBRIgRL
BRI.BRL8RLARL8Rt2'a023103060
t€/kg dry 370pS/rSdry 370pdkgdry 370
ugkS dry 37O
Ugr'kS dry 370
lrg/tS dry 370pdks dry 37O
irdlgdry 370
ldkS dry 370
frdl€d.y 37o
Ugikg d.y 370pdksdry 37o
ldkS dry 370
ugkgdrr 37o
rcftS dry 370pgikg d.y 370pgur(gdry 370
trglS dry 370
frgts dry 37O
IrgA9 d.y 370
lSftS dry 370
ldlq dry 370
lqkS dry 370
rgko dry 370
$S/kS d.y 370
t44(g dry 37O
ldkg dry 370
UdkS dry 370
lgftSdry 37O
tgkg dry 37OpSftSdry 370
ldksdry 37o
flgl(g dry 370
UdkSdry 1480
t dkS dry 370
FSftS dry 370
Fdkgdry l4a0
udkSdry 37o
US/kSdry 370pgngdry 370
tg}gdry 1480
lgkgdry 370
USlftS dry 370
tdksdry 370
WlWdry 370
ldkgdry 370
ldksdry 370
udkSdry 370pdkS drytnlks dtyFSikg dry
sRtERIBRLBRLARLBRLSRLBRLBRLSRLBRLARL8RLBRLSRLSRLBRLBRLBRLaR-BRLBRLSRLSRLBRLgRL
BRLBRLBRLBRL8RrBRLARL
BRLBRLBRL8RLBRLSRL
BRLBRIERLBRLBRI.BRLBRI.BRLgRL
505050
5050505050505u50
505050505050505t)5050505t)
505050505050505050505050505t)5050505050
5050
3741)37103?10
3G1fi15-11030-130
58
82
Ihb letorob,y r.porr is not ealid w hoa an onlhoizc.I sigrr&tare on ahe cowr page.
* Reportdbl€ Det ction Limit BRL = B€low Reponing Lirnit P.ge 154 of 165
Page 664
Semivolatile Organic Compounds by GCMS - Quality Control
Spike SoLrrce
Brrch 703 1592 - SW845 ls45A
Duolicat rT03lsg2{)UPil SourEer5A59641-16
iiatrlr Soike fl0115!t2-t St) Source: 5A5964l-16
nep6[ed: 271\tat47 Ar',at\rzed: 28]\,tar{7
Sunogate: PhermI4SS@WaE: faryhenyt4t4SUl'lgate : 2, 4,&Ttibrcn o p h e not
220n29101680
2610263022tO25402650184015002090259026602460282021903340238029602420
iratsh soikc Ouo fl03t592-t{sD Source: sA59641-.t6Prepared: 27{rar47 Analrred: 28-Mar-07
27502?702400266027701920163022AO27aO28102600m0024103550250031102550
Ptepa(d: 27j{,et47 Analyzed: 28-Mar -O7
Acenaphlh€ne
44hbro-3{ethytphenol
24hlorophsnol
| ,4-Di.t orob€nz€ne
2+Lriaitrololusn€
4.Nitophenol
N+{ilro6odi-n.propyl6min€
Pentadllo'rophenol
Ph€nol
13.+TriJrlorob€nz€ne
S u ftog ale : 2 + I w rfi i phe n JtS u trog de : 2+ luotoph e n o ISufio€ale : Nltobenzene4 5SuEogate: Phenol4'Sutogale: Te@enyl44S u nog ele : 2, 4, ET i bmmo ph en ol
44 oro- 3.'nethyl pte nol
z{filorophenol
1 ,+Dlchlorobenzene
2,+Oinhrotolueno
4-l'tibophenol
N{,litrssodi-ntmpyiarn jne
Penlachlorophenol
Pheml
1,2,4-Trichhrclbenzene
S,/'rogae : 2+l uo tob ip he ny'S,//rogate: 2+luorophenolSunogete : Nittoh nz€ n e4 5Sufiogel€: Ph€nol4'Surl.c8ele: Teryhe/'444Su,tugate : Z 4,&Tnhnnophqnl
IS/ig dry!g/kg dryFS/kg dry
ldkS dry 184
UdkS dry 184
US/}S dry 154pg/Kg dry 1M
vgKgdry lu
uS/KS dry 735pg/kS dry 1M
t'dks dry 735
!S/kS dry 1U
PqlNS dry lUpdxgdry 1u
rc/kS drypg/kg dry!S/kS drypdks drytlglxS drypdks dry
pgikS dry 185
Pg4q dry 185pg/kg dry 185
Ug/kg dry 1e5pgfl(g dry 185yg/Kg dry 741
Itglkgdry 185
ug/(g dry 741
ldkS dry 185ydKg dry 185
!g/kS dry 185
!9K9 dry!9kg dryr9ll,g dryldkg dry!s/kg dry!S,4(S dry
59 1111078 30-1n45 15,110
70 44-140
71 30,130
61 30-130
66 40-140
71 40-144
50 30-130
40 40-140
56 30-130
70 30-130
72 40-140
66 40-140
/6 30-tu59 15-11090 30-t 3064 15-11080 30t3065 15-110
74 40-140
74 30-130
64 30.130
7'1 40-140
74 40,140
sl 30-130
44 40-140
6'1 30-130
74 30-130
75 40-140
70 40-140
80 3t)-13064 1$11095 3013467 15-11083 30-t 3068 15-110
374037403741)
37103710371037103710371037103710371037103710371037103710371037103710
374037403740374037403740374037403740374037403740374037403/4437403744
BRL
BRL
BRL
ARL
8RrBRL
BRL
8RL
BRL
ARL
8RL
ARL
8Rl,
ARL
ARL
8RL
BRL
BRI
BRL
BRL
ARL
BRL
6
5
4
2
l o
I
6
4
6
3030303030303030303030
Thit Mo.atotl rcpod Lt aol wIA tu hou an ourhori4d signatarc on tha cover pege.
i Reponable D€t€ction Limit BRI- = B€low Repodng Limir Page 155 of l6s
Page 665
Total Metals by EPA 6000/7000 Series Methods - Quallty Control
An&lyt€G) FiagResult Unirs 'RDLSpikel,evel
o/.REC
Limits
RPD
Limil3ourc€Rcsult %REC RPD
B{tch ?031495 - EPA200/SW7000 Se.ie*
Blrnk l7O3l49sALl(ll
Prepared A AnalFedt 2&M6r{7
Mersl(y ERI_
Duollcate a70314954UPl)
Prgpared & Anelyzed: 28-Mar{7
fdtt Solt fl031.19$Ist I
Prep€red & Anal}rr€d: 204rar.O7
r.ff x Spiko fl 0gl,€5.||S2)
Proper€d & AndFed: 2&Mar-07
Rcferunco A0ltagSSR[l)
P.spar€d A Anallaed: 2&Mar{7
Sourc.: 5A596A0{2
o_0327
Sourcs: SASgO{l{?
0.566
Sourca: SA50A|1-16
ngtkg wet
mS4(S dry
nE/kg dry
rlglkg dry
mS/kS we{
0.0299
0.0334
n.0327
0.0289
0.1s(}
BRL
20l2
820.454
0.451
1 .33
aRtBRLBRLBRTBRLBRL8RL
0.4710.4920.5210-4450.5100.{€40,471
0.0320
0.0300
0 445
1 -13
101 75-125
118 65.9132.6
Brrch 70316t9. swEl6 r005A
Abnk 1703l6l9.BLX1)
Prcparedr 27-lrar-07 Analyzp,d: 2A-Ma..07
Lead
Selenium
Sflver
Chroflfum
Barium
Ca(tmium
LCS fl031619€S
Prepa6d: 27-1 a.47 Analyzed: 28-tuler-'7
Seleniuft
Lead
B€num
Sik€r
Cadmium
Chromium
.ngImsnlns,r€rmgnms4msr
mgrtnEnmgutnBnmgnrDdlrlcrl
NETotSIdtS/l
n€nn€nms,lmcil
firgn
olgrl
Insl
lngn
0.00750-0r500.tx)500.00,$0.00500.0050o-fi)z5
0.01500.00750.00500.00500.00250.00500.0040
o0.t500.00750_0060o.00500.00250-0050o.0(X0
0.0075o.0t500-00500.0025
0.5000,5000.5000.5000.5000_5000.500
o.5000.500
0.5000.5000.5&0.5&)0.500
Barium
Silvgr
Cadmium
Chomium
Duplica|. (m3t5l9.Dt Pl)
0.517o.1140.5060.4780.467
Souir.i SASS508{1
9t 8S115
9A 85-115
t04 81115
89 85-115
1tr2 8$115
97 8!fi5
94 8$1t5
94 85-115
9€ 85-'t t5
t03 85-115
89 85115
101 8t'-t15
96 85-1t5
ltil 8s115
LCS Oup ft03l61*'BSDIt
Prepared: 27]r,1a.47 Analyzed: 2e-Mar-O7
Sebnlum 0.46SLead 0.4s9
0.60.60.8
0.81
mm202020m20
m20m20
Prepar€d: 27.1!sr-07 Analyzfd: 28-l,rl€I47
S€lenium
Si$st
Cadrlium
8RL8RL
0.00248RL
BRIBRL
o.0c27aRf
Thlt lobnbry repaa is ,rd rolil wirhoa atr audtorizd stgnaar. oi tte @je. pdge_
* Report blc k€ction LiEit BRL = Betow R€porting Limit Pag€ 156 of 165
Page 666
Total Metals by EPA 6000/70 ) Series Methods - euality Control
Analyte(s) Rcsult Flag
Source %REC
Result %REC LimitsUnits *Rl)LSpike
Levcl
RPI)
Limi tRPD
Bshh 7031619 - SW846 3005A
Ouolhat€lm3l619OUP1l Sourc€:SAsgsos.ol
Pr€pare.d: 27-lelar47 Anatvzed: 28-Mat -O7
Chrooium8€rium
frt|ir soile t703l6le+$t)
BRL
8RL
BRL
So.r.oe; SA596{l-18
0 4630.4650 .5140_464o_4370.500o 418
rng/l
rng/l
lng/l
ms/lngr'l
mgmsrmg/l
mg/l
mg/l
mg/l
mg/l
mgn
tngn
mg/l
mg/t
mgn
mgn
mgn
mg/l
rng/l
thgn
rhgn
rngn
rhgn
nE,,l
lhgn
rhg/l
lng/l
rngn
rhg/l
rhg/l
lng/l
mgn
mg
rhg/l
lngr
0.00400.00500.0050
0 01500_00750_00500.00+00.00500 00250.0050
0.00750.01500.00500.00500.00250.00500.0040
0.01500.00750.00400.00500.00500.00500.0025
0.5000.5000.5000.5000.5000.5000.500
0.5000.5000-5000_5000 5000.5000.500
0 5000.5000-5000.5000 500o-5000.500
BRL
8RL
BRL
ARL
BRL
0_001.1
BRL
ARL
ARL
BRL
8RL
BRL
BRL
0.0014
BRL
BRL
202020
Pnepar€d: 27+1€r{7 Analfled j 28,MaF07SelenlumL€Ad
Baium
Silv€rCadmiumCtuomlum
L€ed
Sel€nium
Slvea
Badum
Cadmium
Chromium
Po.t Splte O03t6t$PSl)
t{5trlr so{(€ Ooo fl031619-filsol} Sourc6: sAS964t-ta
Propared: 27-llar.07 Analyzed: 2A-Mat-07
s3 75-125
97 75-125
103 75-125
93 75.125
a7 71125
lo0 71125
95 75-125
9A 75-125 'l
75-125 1
88 75-125 0.5
103 75-125 0.4
101 75-125 1
96 75-125 0.4
94 71125 1
0.491
0.468
0.439
0.516
0.505
0.440
0.470
Sou.co: SA5964t.tE
20202020202020
P.6par€d: 27-t!lar{7 Analf?ed: 28-Mal{7Selenirm
ChromaumBariumSilverC€dmium
Brtch 113 1677 - SW846 3005A
Ahnl( O03l677ALKll
PGp€r€d & Anabzed: 28-Mar-07LeadSeleniumBariumSawrChromium
Cadmiom
LCS a?O3t€Tf .8st lPlepar€d & AndFed 28-Mar47Le€d
S6l€nium
Barium
Sft,er
Chronium
0 4760.5000.4780.445o.522o_4350.51' l
BRLBRLBRLBRL8RL8RLBRL
0.490o.4730.4450.451o.4760.48e
0.00750.01500.00s00.03000.0050o00t00.0025
0.00750.01500.0050o.03000.00400.0050
0_5000.5000.5000 5000-5000-500
BRL 95 80,120
BRL 100 80-120
BRL 96 80-120
aRL 97 80,120
0.0014 104 ao-120
BRL A7 AO-1m
BRL 1n2 80-120
98 85-115
95 85-115g7 a5i15
a5-115
95 85-115
98 81115
ThLt labontory rcFod is noa eali.l wilhoat an aulhotized sigaalure on rte cover page .
* Reportable Detection Linit BRL = Below Reporting Limit Page 157 of 165
Page 667
Total, Metlk by EPA 60([l?fi10 Series Method! - Qurlity Control
Analyte(s) ResultSpike
Lev€lRPDLiflitFlag Units *RDL
Source %WC
R€sult o/rR-Ec Linits RPD
OuElic.lsl703157OUPll SourESA5964t-t7
Pl€9ar€d & Anal}rzed: 28-Iler-0?
Brrct 70316?? - swEd6 30054
LCA 17031677€3ll
PrBpared & AnalyzEd: 2&Mar{7
Cdmium
LCS Duo f/03187ASDi)
Pr€parcd & Anatyz6d: 2&Mar{7
S€l6oium
L€ad
Bari|lm
Silver
Ch.omium
Cadmium
Selenirm
Cadmium
ClYoniumB€riumSl\,sr
l||tdrspn r7o:11677-flSl)Pr€paEd & Analfzed: 28-M€r-07LeedSel€oiumBEritffn
SnvorChrqniumCadmfum
L€€d
Sel€nium
Chrooium
B ium
Hmium
Silv€r
Pod Adke ft03-l577.Ps
P|epa€d & Ana\zed: 28-liler{7
S€l'snium
Slh/€.
Cadmium
0_500 mgn
0.464 otS/|0.,$4 ftSn0.472 nEn0,467 ms{0-43s mdlO.4f 7 mCI0.490 ndl
BRL fiS/t
0.973 qRG m97|
0-0026 -gI
0.0734 nE.Il
0.103 AR6 mg/t
0.608 aRd mSI
0.0206 J,ORa nE,t
Sourc€: SAlto532.01
O.{aO CSIT mS1|
O.47A nE/
0.760 OMz nrgrl
0.4€4 ntS,
0-447 nlg4
0.496 mgl
c.472 NI
0.492 aM7 nrgll0.4€9 mdl0.512 mCI0.79'l aM7 mg,/l0.448 '|'eA
0.5|0 rE/l0.502 mS4
So!rc.: SAsgSll?-Oi
0 0025
0.01500-0o750.00500.00400.03000.00500.0025
0.01500.00750.00250.00400.00s00 00500.0300
o.00750.0't500.00500.00400.03000.00500.0025
0,o07s0.01500.00500_00500-00250.03000.0040
o.01500.03000.0dI5
0.500
0_5000.5000.5000.5000.5000.5000.500
85-115
&1115
8$115
8S115
85.115
65-r15
85-1t5
85-115
75-125
75-125
75-r25
75-125
7U125
7$125
75-125
75-125
7*1
75-125
75-125
75-125
75-125
tu125
60-120SGlA)80-120
100
9397s4s3a79590
2I
,t
2
2
172
26
22
5
197
2020mm202020
2020202020m20
[.lrlr Solke Oop fl03167f{SDl) Source: SA59532-0i
Pregercd & Analfled: 28-lrar{7
BRLo.oo72ARL8RL
0.0079o.2760.0268
0-5{D 1.020.500 BRL0.5tn 0-6040.500 0.07560.500 0.02120.500 0.1060-500 0.0032
o.sco 1.o20.5m aRL0-500 0.1060.5m 0_6040,500 0.00320.500 0.02120.500 0_0758
0,5{x}0.5(X)0.500
BRL
o.m12o.0032
NR
3182937A94
NR9881
97s8
202020mmm20
0.4580.5410.{51
trg,lrE/lmg/l
104
Thls, ttto'{lort ,t$tt b ,tot a{f,d flirho|,, on aathodzed sig/'gd*e oE te @'er pq.-
' R€portable D€tedion Limit BRL = Below Reportiog Limir Prge 158 of 165
Page 668
Total M€tals by EPA 200 Series Methods - Quality Control
Bctch 7011494 - f,PA 200 S€ri€s
gl.nk fi031,194€LKl)Prcpared & AnalF€d: 28-li1,,lar-07
Silv€rS€lenium
Chrornium
CadmiumBarlum
Ouolicate ft03ll9{.I)UPI IPrspa€d & AnalFed: 28-[.,tar-07
SllveaSelenium
ChromiumHmiumBarium
alrix SDll. t703149+lirsr IPFpared & Andyzed: 28-Mar,07Sik€rS6leniumCfi.omlumLe€d
fumiumBadum
reHr Srtr. n03149+MS2l
Prepared & Analf:€d: 28-Mar{7
Sel€niumSitu€r
ChlomiumLeadC€dmiumasium
BRL
BRL
BRL
BRL
ARL
8RL
ARL
Sou.E€: 5A59620.02
nE/kg wel 0.938mg/kg w€l 1.41mgukq wet 0.704mgukg wet 0 469mgukg w€t 1-41mgukg w€t 0.235mg/kgw€t 0.469
mg/kg dry 1.11mg/kg dry 1.67mS4(g dry 0.43sndkgdry 1.67ng/kg dry 0.557mgfl(g dry 0-278mg/kg dry 0.557
mS/kS dry L04mg/kg dry 1.56mg/kg dry 0.522mgftgdry O 742mg/kg dry 1.56mg/kgdry 0 261mSftS dry 0.522
mgftg dry 'l -54ng/kg dry r_03mgftgdry I -:,4mgftgdry 0.515mg/kg dry 0.772nEftSdry 0-257nSftSdry 0.515
mgftgdry 1.65rhg/kg dry 1-10mg/kg dry 0.549mSI(g dry O.2f4fiE/kSdry 1.65mo/kg dry 0.549
ARL
BRL
33.9
2.90'15.2
0.368
52.9
Source: 5A5364l{7
121
132
1 5 3
218
131
120
168
Sourc€: 5A59641-16
130
130
130
130
130'130
'130
129
129
129'129
129
129
129
137'137
137
137
137
137
78.0
41.1
44.7
49.3
3 1 . 7
BRL
ARL
38.7
2.47
16.2
0.502
56.5
BRL
BRL
29.4
99.7
6 4 1
0.599
39.2
BRL
8RL
1 . 1 5
4 4 1
3.65
0 . 1 1 7
10.4
BRL
BRL
29.4
0.599
6.41
39.2
1 66317
35
3535353535
130
114
1 2 3
125
121't23
1 3 8
mgr'kg wetm9n(9 wetmgukg w€tmgtkg w€tmgukg wst
93 70-130
102 70-130
95 70-130
91 70-130
96 70n30
92 7C-130
99 70-130
101 70-130
88 70-130
70-130
93 70-130
91 70-130
95 70-130
99 70-130
101 85-115
91 E5-115
109 85-115
92 85-115
98 85-115
108 85-115
114 77 +122.6
108 66.3n$-6
101 81.8-118.1
s7 78.$120,5
101 42.1-117 _9
PoEr Sdko t703l4x+Sl I Source: SA596,H {7Propded & AnatF6dt 28-Mar-07
1 3 9
125
t 7 9
127
141'| E7
8 8 6
44.3
45.0
47.8
32.0
Sel6niumSlverChromiumCadmlum
Barium
Rrf6|E|lco O031494-SRttllPrgpaGd t Analyzedt 2B-tdar-O7S€l€niums|lverL€adChro|txumC€ddum
1.501.000.7500.500o.250
Ihis laborutoty repod is Foa vs&t Hirtotu aa aathotked signaare on the coter paEe.
' Reportable Deta:tion Limir BRL: Below Repo.ling Limit Psge ls9 of 165
Page 669
Total Metals by EPA 200 S€ries Methods - Qrality Coqtrol
AIlaryte(s) FlsgSpike Sourcc
L€vel R€sult
%RECLimifs
RPDLimit
B{tch 113 1494 - EPA 200 Series
Reter€nca ff031404-SRil I I
Pr€pared & Analfzed: 28-t ar-O7
Bsrium
ktch 70J 1620 - EPA200/SW700 S€ries
Blank (t03164€LKil
P.spared: 2 ar47 AnalFed: 28-Mar-07
46.1
219
m€rl€wet 1.50mS/kow€t 0.500
80-8-119-4
azz-177 -3
44.7
2 1 5
1(X102
LCS (?0r1620€Si\
Peparcd: 27 l!lat47 Aaatyz€d: 2g-Ma(47Mercury o.m2€s
LCS fi031679€31)
Pr6per6d & Anal).zed: z&Marfi
Dupllc'b lm3167g{UPll
Prepared & Analfz€d: 28-t1ad7
Xrt lr Soite flfi11679{S1l
Prep€€d I AnatFed: 2&Ltar-.07
srdr SolI. Duo flO316'tg*ls0lr
Prepared & AnalFed: 2&Mar-07
Po3t Sdk. O0:l1670fsir
Pr€pared & Anal}.!6d: 28-Md{7
0.m245
So{rrc.: SAsgGal-17
0.@?26
SourE.: EA596a{-17
0.00479
SourE€l SA5964l-l?
o.0048:,
Sou.E€: SAlt96al'17
nEn
nEJl
irSn 0.fin20
msn
tr'sA
msn
mgr
n€n
rngl
rvl
Duotlcate 1703tGi:m-DUP1l Source SAli965&O l
0$r'15
8 S 1 1 5
Prepared: z7-Mar{}TAnalFed: 28-Mar47
U.tix Splke l703l62G S1l SouEs: SA5O6.t1-t6
Pr€pared: 27-l'rar47 Anavzed: 284{ie47
atdr Soik€ Ouo l7031clo.t{5tr)t} Source SA5064t.18Pr6pared: 27{v,1tr47 Analyzet 2&.{l'/.at 47
Me.crry 0.m284
Port Soike {?0ll6;10+S1l So(rce: SA596al.lE
114
75-125
75-125
8&115
Pr€pared: 27-&lar-07 Anal:r2eil 2B.|i,at47Mercury o-m267
Brtch ?031679 - EPA2{XySW7000 Series
Abnk {70316794Ll(l IPr€pared & Anaifzed: 28-Mar-07
msn
r|En 0.000m
0.00221
o.(n221
0.00221
o.0022r
75.125
75-125
45115t15
This L6orco4 .qorl ls aot vztitt blrhod eE sulhorizd tlgnata?c on rtz cotet pg..
. R€portable Detection Lidit BRL = Beto$,Reporting Limit Page 160 of 165
Page 670
SPLP Metals by EPA 1312 & 6000/7000 Series Methods - eualie Control
Spike Sourc€
B.rch 7031651 - sw8453010A
Blank 47031651 €LK1 )
Prcpared & Andyzed: 2A-Ma"{7
L€ed
Selentum
S0ve.
C€dmlum
Chromiom
Barium
LCS O03165t€Slr
P.epaed & An€l}.zed: 28-Mar{7
Lead
Selsnium
Chomium
Cdmium
Silv€r
B€dum
LCS Ouo ft03l65lSSDrl
Pr€psrEd & AnalFed: 28-MaF07
S€16nfum
Lead
Siiv6r
Cedmaum
Chrorium
Berium
ARL
BRL
BRL
BRL
8RL
BRL
8RL
1 . 1 8
1 . 1 4
1 . r 6
1 . 1 4
1 . 2 2
1.06
1.26
1 1 3
1 1 8
1 . 1 3
0.866
1 . 2 1
1 . ! 5
1.27
Ouolicatefl03l65lJuPlt Sourco:SAi96ai-is
Prep€rod E Analyled: 28-Mar-07
Leift
S€lenium
Sfver
Chromium
cadmium
Badum
I.trlx Solt ff 031oitl{tS
Prepared E Analfz€d: 28-[,lar-07
S€l€nium
Silver
Chrmhrm
Cadmium
Barium
0.0025
BRL
BRL
BRL
BRL
BRL
0.0r18
Source: SAS96a1-16
94 82.3-108
91 79-108
93 76.2-118
91 77 4-109
s8 87.9-110
85 55.5-115
1 0 1 8 5 1 , r 1 9
90 7S-108 0.9
94 82.3,108 0
90 77.4-103 0.9
69 55 $1r5 20
97 87.9-110 0.8
92 76.2-114 0I
102 85 1-119 0 8
96 0r .8-105
94 80_4-105
7S 63.6-109
94 79.2-106
94 81.5-r ' t 1
99 06.4-108
102 88.9-114
93 80.1-105 0I
95 81.8-105 0 8
94 81.5-111 0
98 86.4-108 0.8
mg/l
mg/l
mEl
mg/l
mg/l
mg/l
msr
ms4
mgr'l
mqil
mg
mg/l
mg/l
mg/l
m!
mg/l
mg/l
mg/r
mg/l
mgn
mg/l
msrmgnmg/l
mg/t
rng/l
lnsn
mg/l
mg,1
mg/l
rE/l
msi
fi€/l
filgn
mgn
mg/l
mgrm94TTE,
0.01500.01500.02000.01500.00250.0r500 0150
0_01500.01500 01500.01500.00250.02000.0150
0.01500.01500.01500.02000.00250.01500.0150
0_01500.01500.0m0o_01500.01500_00250.0150
0 01500_01500.02000.01500.01500.00250.0150
0.0t500.01500_01500.0025
1 2 5
1.25
1_25
1_25
1.25
1.25
1.25
1.25
1.25
1.25
1 . 2 5
1 . 2 5
1.25
1.25
202020202D2020
1.20
1 . 1 7
0.989
1 _ 1 7
1 . r 8
1.24
1.28
1 . 2 5
1 . 2 5
| . 2 5'| _25
1.25
1 . 2 5
1 . 2 5
1 . 2 5
1.25
1.25
1.25
0.0030
BRL
BRL
BRL
BRL
BRL
0.0098
BRL
BRL
BRL
ARL
ARL
ARL
0_0052
ARL
BRLgRL
8Rt-
1 9
20202020202020
mm2020
f,Etdx Solk. Ouo t703l651.ltsol) Source SASg6.t1-16
Prepdr€d E Analfzed: 28-Mtr{7
1 . 1 6
1 _ 1 9
1 1 8
123
Sel€niumuta0Chrc(r{rr lftdmiun
Thb laboralory ftpod h not valU withoa aA aathoirzd signalure on the cover page
* Refortable Detection Lirnit BRL = Below Reponing Limit Page l6 l of 165
Page 671
SPLP Metsls by EPA 1312 & 6{100/7000 Serles M€thods - QuNlity Cooarol
Analyte(s) Resulr Utrit3R.PD
RPD LimitFluS
Spike Source '/"REC+RDL fwd Resuil %REC Limitr
Batch 7031651 - SWE{5 3010A
Ialrir Soiko Duo c7031651-tilSD'l I Souic€: 5A5964l-16
Pr€pared A Analyzed: 28-Msr{7
1.fi)
1 . 1 6
1.28
Sourc€: SA59G41-16
Silver
Bsrium
P€t So|te fl031G519S1)
Prepared & Anall.re.dt 28-Mar-07
Selenium
Lead
Cadmium
Situer
ChtDmium
Barium
LCS {7fi 6i2€slI
Prepared & Analyledi 28-Mar{7
Ouolic€le t703165:lOUPtl
Preptred & Anel]/"zed: 28-Mar{7
alrir Spik€ l7031652.irsll
Prepared A Analyzed: 28{vlar{7
1 . 1 7
121
1-19
1.25
t . t l
1 . 1 9
1.29
SRL
nrs/|r€/1mgn
mg/lrEnnElms/|ftrSImglmgil
mgn
fttsn
0 02000.01500.0150
0.01500.01500.01500.m250.02000.01500 01s0
1.25
125
t.25
125
r.25|.251.25
1-25
125
1.25
ARLBRL
0.0052
BRLBRLBRLBRLBRLBRL
0.m52
2020m
100-90
8793102
63.6-10979.2-1(X88.9-1'14
n.7-10a80.110E79.$t0786.5{0961.7 -107
78.1-11486.&118
94.9794100809l;103
Bstct 70f159 - EPA200,6W7000 S€ri€s
glank (7O3i652€LK1l
Prepa.ed I AnElfi€d: 2&Mar.O7
0.00244
Sou.ce: 3A59€41-15
BRL rngl 0.00040 BRt
Sou.ce: 5A39641-tG
0.00251 nrdl
0.00010
0.00040 0.00250
0.0@ro 0.00250 8RL 100
BRf 99
99
66_6-117
20
lraHx Spike Ouo 4r031652{SDl| Sourc€: 5A50641.16
76.1-111
76.1-111
E6.&110
Pr€pared & Analyzed: 2&t ar.07
Posr Soik6 O031652-PSl I
Prepared {l fu|elf2ed: 28-Mar{7
O.tn247 mgl 0.000.10 0.m25O
Sour€e: SA595al.l6
20
0.002/|a |rSI 0.mO4O 0.00250 BRL
G€oerrl Cbemistry Pammeters - Qsallty Control
Bstcb ?0ll,u0 - Ceo€rrl keper.aloo
Duollcare aTu tT0ouPt IPrepar€d & Analraed: 2+Msr{7% Solicls
So(rc€: SA59619{1
% 97.9 m
Thtt hbraro.y r.port b wt ts6d uidro!, oa oartoried tl8/,.ata!. or, rtz cover poge.+ Reportable Detection Linit BRL = Below Repodrg Limit Page 162 of 165
Page 672
Notec and Definitions
'TPH Calculared as
Comp Completed
FP Field Preserved
QCI
QC2
QM?
QR4
QFJ
QR6
R05
s02
vela
Analle out of acccptance tange.
Analyte out ofacc€ptance ra-oge in eC spike but no reportable conceotmtion present in sample.
The spike recovery was outside accepiance limits fot the MS and,/o. MSD. Th€ batch was acc€oted based on acceotableLCS recovery.
AMlyses are not controlled otr RPD values ftom sample conceDfatioos less tha[ the reportiog limit. QC batch acceptedbased on LCS andlor LCSD QC resutts
RPD out of acceptance |ange.
The RPD exceeded the QC control limits; however precision is demonstrated with acceptable RpD values for MSA{SD.
Elevated Reporting Limits due to thc presence ofhigh levels ofnon-target analyres-
Tbe surrogate recovery for this sample cannot be accurately quantified due to interference ftom coeluting organiccompounds present in the sample extract.
Field extracted
VOCS ReponiDg limits reflect SW846 5030 extraction technique due to matrix inrerlerence using SW846 5035A extractiontechnique,
Z-2 The recovery ofd-BHC wes outside ofthe acceptatrcc range due to a breakdown ofd-BHC within the spike mixrure.The CCC is withi[ acceptable limits which demonshates that thc problem lies with the mixture, not rhe instrumentarion-
BRL Below Reporting Limit - Analyte NOT DETECTED at or above rhe reporting limir
dry Sample resulrs reportcd on a dry weight basis
NR Not Reported
R.PD Relative Percent Dilfcrence
J Deteoted but below the Reportiog Limiq therefore, result is an estimated concetrtration (CLp J-Flag).
A plus sign (+) in the Method Reference column indicates the method is not accredited by NELAC.
Iot€rpretatiod of Total Peholeum Hvdrocarboo ReDort
Peroleulrt identification is determined by comparing the GC fingery.int obtained fiom the sampte with a library ofGC fingerprintsobtrined from analys€s ofvarious pekoleum products_ possible match categories are as follows:
Gasoline - includes regular, unleaded, premium, etc.Fuel Oil #2 - includes home heating oil, #Z fuel oil, and dieselFuel Oil ll4 - includes ll4 tuel oilFuel Oil 116 - includes l/6 fi.rcl oil aod bunker "C,, oilMotor Oil - includes virgin and waste automobile oilLigroitr - iEcludes mineral spirits, pekoleum naphtha, \,ln&p oaphthaAviation Fuel - includes kerosene, Jet A and JP 4Other Oil - includes lubdcating and cutting oil, and silicon oil
At times, the unidentified petroleum ploduct is quatrtified using a calibriation that most closely approxinates the disfibution ofcompomds in the sample. Who! this occurs, the result is qualified as *TpH (Calculated as).
Thk laboraary repod is nal vol t wirhout an aurtoi4cd tripatttrc ot lhe cover pge.
* Repdlable Detection Limir BRL = Below R€podng Limir PaBe 163 of 165
Page 673
hboratorv Cotrtrol Sample (LCS)t A knowr mafix spiked with compound(s) r€prcs€nhtive ofthe targ€t a(atytes, which is used todocument laboratory perfonnance-
Matrix Duplicate: An intra-laboraiory split sarnple which is used to document tbe p.ecision of a method in a given samplo matrix.
Matix Soike: An aliquot of a sample spiked with a knowu concentratiotr of targEt aoalyte(s). The spiking occus pdor to samplepreparatiotr and analJrsis. Amahix spike is used ro docum€nt lhe bias ofa rnethod itra given sampl€ inahix.
Method Blaok: Atr adal)'te-fte€ nat ix to which all reageots are added in the same volumes or propo.tion$ as us€d in sampleprccessi[g The metbod blank should be canied through the complet€ sample pnqnration atrd aoal]tical procedure. Tho Eethodblaok is used to document cootamination resulting from tbe a[alyticll process.
Method D€tection Limit (MDL): The minimum concentiation ofa substance that ca! be measut€d and Eported with 99%confidence that the arullte concentration is greator thatr zero ldd is determined ftom aoalysis ofa $ample in a giveo matrix q?econtaining 6e analyte-
Reportable Dotection Lirnit (RDL): The lowest conceobation that catr be r€liabty achieved withil specilred tihits ofprecision andaccuracy duidg routine laboratory operating cooditions. For Eany analytes the RI)L analyle cotrccobation is selected as the lowestnon-zero standard itr lhe calibration curve. while the RDL is app.oximarely 5 to l0 tim€s the MDL, th€ RDL for each saGple takesinto accoutrt the sample volume/weight, exlract/digestate volume, cleanup pr<rcedures atd, ifapplicable, dry weight con€ction.Sample RDLS are highly matri[-dependent.
Surroeate: An organic compound which is similar to the targ€t analyt{s) io chemical composition and behavior in the aaalyticalprocess, but which is lot normally found in environmeDtal samples. Ttese compouods are spiked into atl blatk, stand.ards, andsamples pnor to adalysis. Perceot recoveries aae calculated for each sufiomle.
Validat€d byiHanibal C. Tayeh, Ph.D.Christopher HaltNicole Bro$1r
Thit l&boturory rqorl b nol vaful r,ltlro.t! an aythorlzed sb''{/tuE on ale coe.r poge_+ R€portable Detection Limir BRL = Beloq, Reponiog Limit Page 164 of l6J
Page 674
State Of ConnecticutDepartmcnt of Environmental protection
Laboratory Quality Control and euality Assurance Form
I-aboratory Name: Sp€ctrum Anal'.tical, Inc - Agawam, MA
Project lncation: NHRY M8 Acccprance Facility _ New Haven CT NHRY ME Acceptance Facilify - New Haven, CT,/Tl s Form Provides ce(iljcations fof the followlng data ser:
sa5964l-01 sA5964l_t IsA5964t{2 5A59641,t2sA5964l-0t sA596{r- l lsA5964t-04 sA596.u 14SA596{t-05 sA5964 L_ 15sAJ964t-06 SA5964t_16sA5g64t{7 5A5964I,17sAJ9641,08 SA59&t lEsA5954t 09 sA5964l_19sA596{l l0
List Sp€cific AnalyticaL Merhods Used:+(jT ETPH
EpA 200 7EPA 245.1/7470A
SM?540 C Mod.sw 8,t6 8260A
sw846 Bl?
sw8.r6l l t2/60108
swE46l3t3/7470A
sw846 50 t0BswE46 74?tA
sw846 EOEIA
sw845 80E2
sw846 8?60A
sw8468270C
sw845 82?0C/EPA 625 |voc
Werc all samples received by the laboratory itr a condition consistentwrth that described on the Chain ofcustody documentation lior the dataset? El Yes E No
Were all QA/QC procedures required for rhe spocilied anah,ricalmclhodts) included in this repod followed? El Yes E No
W€rc all QC perfonnarce standaads and recommendations for thespecified methods achieved? E Y e s E N o
Were results for all analyteJist compounds/elernents for the sDecifiedmethod(s) reported? E Ycs El No *
The mmpou(h andd €lenenl! rcPfrr.d ar€ as sPecifi@llv r€quesled bv h€ ctieflt on rhe chain ofcustody ant in $me @s6 may no( inctude rhc aulrnalyr. lis a! defin€d,n rhe m€dod.
Negqlive rcsponses lor A, R arrd C ore td.lrdsed in a case nanst re on the cover ptge ol this rcporl
I' the andenigned, anev under rhe pains .tnd penorlics olpedsry that, based tpon my percondr inquir! ol lhose ftsponsibteror oblaiaing rhe info 'ration' lhe dalerizl conrained in thb an;Irficdt r"port it,u *e best o\my kaonledge and berieJaEok rale s.rd contplela
nftd-tlaaibal C. Tayeh, Ph-D,President/LaborEtory Director
Datr: 3/29Dffi7
This taborurory rcFat h not valid Nithaat oE zy.honzad slgaa/sre on tha cove! paEe.i R€portabte D€rection Limit BRL = Below Reoortine Limit PaBe 165 of 165
Page 676
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Page 678
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2 i ' -
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Page 679
Sample ldentificatiooFB.4sA59t0l- l9
Client PFiect #301-88
MafixBlank waier
Collection Date/time26-Mar47 00:00
Received27-MaFO1
CAs No. Anab.z(s) Res r FIag UfiE 'RDL Dihltiot' Mahod Retr. PEparcd AnalJztd Barch Anolyst
VolEtile Orgrnic Compounds
Volalil€ organic Comoo.hds bv SW846 82608
Prepared by me$od SW846 5030 Waler MS
?6111 1,12-Tidh6tifiuor€hane(Freon 8HI6r&t Acetoi,e BnL107.1$1 Adyionitr{e BFL714!2 B6?en€ BFL108-86t Erctrjotenz€oe 8Rl7+9/-s BlollEcl{orcnethane BRL'itru
Eromodbhlooln€tlane BRLEh.2 Bornolorm BRL74+r-9 B|D|ftrnsdane B8L7818.3 2-Eulandte (MEK) BBL10451{ +Butyt€fzene 8RL13srl s€c€utylbenzene BRL90{6{ teGgr$r{tenrene BRLE1fl Cerbon dierlfide BnLs6-2+s Cafton telracdonde BFL10!-907 Chbrobenzene BFL?5{lG3 Chtorcefl'|e 8RLsl-te3 Chtonforrn BRL74.47s clioFn€hene BRLss8 24hlootdu€ns BaL1Od'13.. 4{hlorotdueo€ 8fl1F12_8 l,2{ikomo3drlorcpropane 8FLl2,l-{&l Dibrofibcl Oon€hans Bful0em-4 l,2-Diborno€hane (EDB) 8RL7+953 DibronEmethane 8RL9+5et 12-Dchtombenzene BnL511.7!1 l,O.Dichlolob€flzene BRL106.16.7 1,+oichtorob€nzene BRL75-71.8 oidtorcdiuorcrne$ane (Freffl2l BFL75-3+3 l,lSiciloroettlano BRL10146.2 l2-Dichto.o€ Ene 8Rt7t!64 j,l.Dcflomefiene BFLr5&5s z dsl.2-Did orcetlene BffLrfs-6c5 rangl2.Dicnbro€tpie BFL
BFL
BFL
8BL
BNL
BRL
B8L
BFL
8RL
8RL
BRL
BRL
BfrLBFI.
8RL
8RL
BRT
pdl
1j44!04!s4
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Itc4
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t 0
20.0
1 . 0
1.0
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0.5
1 0
a0
t0.0
1.0
1 0
1_0
i0
1.0
1.0
z0
1.0
zot 01.0
?.0
05
0-5
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t_0
1 0
1.0
2.0
1.0
t 0
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0.5
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0.5
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sw846 @@A E:Mer07 z$Llar{7 7091n7 RU
n47-s t,2ochloopropane
1.d,s4 1 ,fi)id oopropaE9+*7 2,2oia dopropdne5e5€-€ l,l.Dicfitoropfopenerto€r{r-t cis-l,3{id{o,cplopene
101061423 baEl-.r{idlloilprop€n€
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1614044 Motryltert-butytdlef1oBnG1 4.$dry-2fsnlenone(MBK)7ss2 Medrylene chlodd€01_203 Naphfiaiene
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Thb loboratoq rcpod is ^ot vdlid x'ithocl en audrodZd slg'/tCdre on thc coser page.
. R€portabl€ Dct€crion Limir BRL = Belov Repding Limit Page 94 of 154
Page 680
Samole IdentificationFB-4
sA59803- t 9
Client Proiect #301-88
MatrixBlaDk Water
Collection Date/Time26-Mar-07 00:00
Received21-Mat01
CAS Na Anrb'te(s) Resull Flag Units *RDL Dilutinn PrcpoEd AndDzed Batch Ahdllst
Volrtile Orgrnic Comporndr
Volatle Oraanic Compoqnds bv SW846 82608Prepared by method SW846 5030 Water MSlq}4a5 Sryrene 8RLd!120.5 I,l,1 z-TelrachtoroetEne BRL79'3+t 1,|,2,2-Tdrachlooehane127'18.,t TeFachlooethene10!-€&3 Tofu4]er{1-6 12,3-Tichlorob€nzene120-82-1 1,2J.Trichto.ob€nzefl€71.5s 1,1,1-Trichloo€thane79{lcs 1,.t2-Tdcloo€thane79-01{ Tfuhlooeh€no
Tti*lorcf uoom€hane (Freofl 1 1)9G18-l 1,2,3-Tric$loropropane
1 J,4.Trifii€thytb€nr6ne10&€7-8 1,3,5-Trirclhylbenzefle7F0r-r \4nyt chlodler3o2o7 m,Pxy'ene96-07{ cx/enet09s6:9 Telr-afiydrotLrrana.&7 Ehyl eher90!-!64 Tgd_amylneht€ther67-!e.3 Ehyt t€d+utyl eiher10€.2rI3 Disopmpylelhef7ft54 TBrt.Bulaml / buv alcohol12391-1 j,+uoxan€
16n00'4 1-Br6pn@tobenzene
M7-6-5 TduEne4S
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Ellradalh Tolal Pelrcteun |Mrocarbo(s
Prepared by melhod SW846 3510C
&066.9 casotinE6&7e30' Fuslot#268trfl1.3 Fue{ Oit*168ts&0(|.{ Fu€l0it$6ne800c00 llotorolJilo1ll|)oo AviationFu€l
Unde0tli€d
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SeDivohtle Orgrnic Compoundr by cC
oroanodhdne P€didies SW846 8081 A
Prepa.ed by method SW846 35'l0C
[email protected] At&ingl9.t46 A€HC
BRL
BRT
8RL
BRL
BRL
BHL
BflL
BFL
BFL
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lgl 1.0
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0.25000.2500
This labofstory fepod is t lrt volU xtilhou aa aulhorirzd signaturc od lhe .owr poge
+ ReDo.table Detectioo Limit BRL = Below ReDortins Limit Page 95 of 154
Page 681
Samote Id€ntificationFB.{sA59E0l-19
Client Project #l0r-88
Mari,(Blank water
Collection Date/Time26-Mar4? 00:00
Rec€ived2'l-Mar-07
CAS No- Aaqlytc(s) RetuU FW Aaia *RDL Ditutioa Method Rel. Preparcd Aral$ed Balch Aaelfst
S€mivolNtik Orgrnic CompoundE by cC
Oroanochlodn€ Pe6licides SW8(; en81A
Propared by method SW846 3510C
319.S5 / b-BHC31!ltG8 d€t]c58.s$e g-BHC (Und6ne)5t-1+9 erbrdanen.544 4,4',000 {p,p')?2-55.s {,{ {DE lp,p)s0-2e3 4,4-00T (p,p)6&5l-i Di€ldinS9l-8 Endosulfsn I3913-66{ Edodjfan tl1qt1{t-8 Efth6ultarSuthte72.2G8 Endin7421-9i-4 EdinAldefryde?E-{]r.8 tbpbd{or7243-5 l.(efiorychlor1024.57.3 HeohcnbrEponds
0@1-3t2 Tcr)oph€iesr6,7r€ a.chlo'dane55663+7 g-c-l o.dar|e5C||g1-7G5 Endin Kolone
1@4, 4,4aBetuMtuiplpq4(s4
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Fohd odnaled Eliphsnvh bv SW846 8082
Prepared by melhod SW846 3510C
1267+11-2 PCB 10181110+282 PCB141||11r,1€-5 PCB 123253,16&21-9 PC81242126t2.294 PCg 1244rlqr-6s1 PcE 1254Io06-ne-5 Pc812603rip4?s5 PC8126e111l)Crlr PcB 1268
IMlul 4,+DB.Maflt@r6ptcny(54
M1-21-3 'edllot@Enta(Sn
S€mlvolrlile Organic Compoundf by GCMS
Somivohdle Oroanic Comroun& bv SW8,4{t 8270C
Prepared by method SW846 351 0C
Bn29 Aaen4hh€ne200.96.8 A€nsphq/bne9012{ l.tirsttylnaphfiaJenee 53n Aniline12O.t2.7 Anhr€cene1912.2+9 AlErin€l@{+3 Arotenzen€,DiptEq,ldaine92-87-5 &nzidne5665 0 Benm (a)anhrac€n€
0RlBBI.BFIBRLBRLBNLBFL8RLBBI.BRLBHLBRLBALBFLBBL8RL8RL8Ft8RL8RL
669
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60IN
pC4 025&
lSI 02500
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This lsbodoq rcport is nol vali.t )tilhottt td aadtoded stg'isu.c on dre coecr psge-
' Reportable Detection Limit BRL = Bebw n€po.ring Limit Page 96 of I54
Page 682
Sample ldentificetionFB.4sA5980l-t9
Client Proiect #l 0 t ^88
Matrixtslank Watef
ColLectio[ Date/Time26-Mar-07 00:00
Received27 -MaL07
CAS No. Atutl4a(s) Result Fl"C AniA rnDL Dilution Prcparcd Anab.ed Balch Antllsl
Scmivoletile Orgrnic Compornds b) ffVS
S€fiivolatil€ oroanic Compounds bv SW846 8270C
ftepared by mebod SW846 35'tOC
cr3'a8 &nzo (a)pyrene
at'*z Benzo (b) looranthene191.?r-2 Beozo(g,h,i)peryene2!7-@{ Benzo(k)fluoranhens66-€5{ Benzoic aaid100.5r.6 Bsqlalcot|olnl-9lJ &b(Zdoroehory)mthane111444 t|is(2doroehyi)other3Be$-324 Bis(2dororsopr@yt)ehe.11741.7 tlis(2ahylh€rylphlhatare1016$3 +&qnophenttpfienylelher8@7 Brlyl b€r141 phhatate
8G7't{ Cadezoleis5G7 44htorGlmethytphenol16-.47-€ +Chtoroan ine91.5&7 2{hlcfonaphtiatene9567{ 2{htctrophenol7!0t72.3 4{hlompheflylphenytehe(218{1,s Chrysene5370.3 Diberuo (a,h) anlhracener3a{4-9 oibenzofurans+5G1 lr-Dctiorob€nzene541-73-1 t,3.Uchlorobenzen€1q-.4+t l,4.Dchlorobentene91€+1 3,3.Dichloobentidineja4+2 z,4.Adlotopra.r,ls1-€62 Diethylphhatale131-11.3 Dimehytphhatale10557.9 a4-Ilmdhytphenol*742 Di+botyt phhalale53462-1 4,&Dnitm-2-meihylgenol5t &5 a{-Dnitrophenol121-1+2 a4.Dnitolotuene@2G2 z,6-Dinitrototuens117-8411 0i+odylphttEtat€206-4,1.0 Fluotanften€6&7+7 Fluorensr1&7't-l Hoxadolc,b€nzenett7{&3 HeEct ombdad€nen17.{ HexachloGlclop€nLadien€6t-t2-1 Hemd olwf|ai€19$30-5 h&no(t,23rd)pyreae?&ss1 hophorcne915/{ 2.li,ielhylMphthalon€6.f&7 2.t eitl;/ptje.trj
10&3+4, s,4.|r€hylphenol1n6-41-59r.20.3 Naphfide|es&7rH ?-NibDanihnecr{g€ O{ifoaniline100415 4tftoanilhe
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i Reportable Derectio[ Limi! BRI- = Below Reporting Limit Page 97 of 154
Page 683
Sample ldeptificationFB4
sA59803. t9
Client Proiect #l0 t-88
MatrixBlank Woter
Collectiop Date/Time26-Mar-07 00:0O
Received2'l-Mat47
CAS No. Adalrta(s) Aesull FIoe Unils *RDL Itilaian Me!*4d. ReI, P.qor.d Aitwd Boteh A"stlsl
Semivohaile Orgrnic Compoundi h,y GCMS
Semivolalilo Olanic Cqnpomds bv S$1846 @70C
Prepared by method SW846 3510C
00.9u litobffz€n€
8e7s 2+.litoph€nol
lm{2.7 +tiihophqrol
62-75-9 N.NitGodmett/aftne
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3et.e.o 2-Fhwdiphent4
$7121 z+hfiqlErd
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11&t9i Z4,6TfuMnod1qd
SVOCS bv SW846 8270C SIM
Prepared by method SW8,+6 3510C
81324 Ac€napntEne
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sr2{ 1-tiddrlaghhatene
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h5.9+2 &nzo (b) iuorantEne1e('?+? Benzo lO,h,i) p€D'lme
?07{84 Benzo (k} lluo(anthene218-01.9 Chrysene53-703 oibenzo(Ah)anthric€oe2!6-.4,1{ Fl0oreaffi€ne0&7,7 Fbo|rn€193-3s.5 lnd€flo {1,2,}cdj pyr€ne
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. Report ble Detecrion Limit BRL = Below ReportiEC Lirit Prge 98 ol 154
Page 684
Sample IdentificationFB.{sA59803- l9
Client Proiecr #l 0 t -88
MatrixBtank Watel
Collectiop Date/Time26-Mar-07 00:00
Rcceived2'7 Mar07
CAS Na Aholfta(s) FIoS A"is *RDL Llethod ReJ:, Prcpsred Anabzed Batch A,altst
Totrl Mcl|ls by EPA 6000/7000 Seri€s Merhao!
71.(l{34 Gdnim BffL
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' R€podabie Det€{tion Limir BRL = Below Reporting Limif Page 99 of 154
Page 685
Sahple tdenrificationT84sA59803-20
Client Proiect #301 -88
Matd.rBlank Water
Collection Date/Time26-Mar{7 00:fi)
Received27-M^.-07
CAS No- ,lnolruls) n4sulr FIdS Aai6 'RDL Dilutia^ Llethod netr Prcpared Anallzpd Botch A!@fust
Volrlile Orga[ic Composnds
Volatilo Orcanic C,lllourlds bv SW846 82608
Prepa.ed by oFlhod SW846 5030 Water MS
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Thit lzborotdry rqort h not valld vlrhout aE arahorlz.d sigtdare on the cover page.
' ReporEbl€ Deaection Umit BRL = B€low Reporting Limir Page 100 of 154
Page 686
Samole [dentificationTB-,1sA5980l-20
Client Proiect #301 -88
MatrixBlank Water
Collection Date/Time26-Mar-07 00:00
Reccivcd2l Mar07
CtS No- Analye(s) Result Fhs Ufii/5 *RDL Dilution Ne/ho.I Ret Prepdred AMIWd R.tkh Arulrst
Voltdle OrgNnic CoI[pounds
Volalile orcanic Cornoounds bv SWO46 82608
Prepared by method sw846 5030 watef Ms
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s-€3{ 1,2,4-Tdrnebytbenzene BRL
1N47], 1,3,5-Idne0iylbenzene 8RL
75{l1rl Vinyicnbdde 8RL
133c2s7 m,p-Xytgne 8RL
s-{76 cxylene BRL
109s99 Tetahydrofu€n BRL
@-&t Ehyl eher BRL
9t4{5.€ fed-amylflEdrtt eitrer 8Rl
63?'92a? Etryt tert-buM ether BRLt@20-3 fi+oFopytdher BFL7s5{r Ted.Bubmt/ butylahohol BRL
w 1.0ps,t 1.0ps,4 0.5
trS4 r.0
us4 L0
}lg4 L0
LrS4 1.0
w 1.0
lsn r.0
PSn r.0
!S4 1.0
pS/ 1.0
!S{ 1.0
PSt, 1.0
ps, 1.0
psrl 2.0
rcn 1.0!S4 100
!s4 1.0
w 1.0
rcn 1.0
lsr 1.0
wn 10.0
!S,4 20.0
/0-130 %70-t30 %70-t3a %70130 %
st!846 82608
123€1 1 1,4-0ioxan€
1$@1 +Erdnohbr,bqzene
N?-265 tduene40
170d,474 l,2-Dichlotodlane44
1d655?/ Di'DtrDfluononethane
BRL
92103t10105
Thk laboru.orl rcpod ir not valid drhout ca dathorized l'/ig/|.a ne on the covr page.
* Repo.table Detection Limit BRL = Below Reporting Lim't Page l0 l of 154
Page 687
Volrtil€ Orgrtric Compounds - Quality Control
Barch 7031790 - SW846 503SA Soil {tow tevet)
tu rnEl?909tfi11
Popared & tualF€d: E-itar47
1,1,2'Trid omt ucroehano (Fr€on Il3l
B€nlene
Bomoform
z€ubnone {[GK)I}BIMb€nzena
sec4uMbenz6e
b.t€uryibenrsne
Carbcn di€uffide
Chloroehan€
Chlorolo.m
ChlordrstE'l€
24t{orohtuar6
1,2-DihDm'3{llorcpopane
0lDrcmocilorun€ttane
1 ,2-DiblolnoefEn€ (EoS)
Ddrdndn6!|ano
12{k*rc'obsl?€.r€
| +DinhxobsrzerE
1,+Dicnbrob€nzene
DiiJ orcdinuorurEhane lFreon12)1 .tDicnhosdune1 ,2.oicnbrcefiane
cis.r,2iichho€lh6i€
[en6l ,2.0i*kro€tEn61 2.oidlloropDpans
l.+Didboporan€
22.fid oroFqane
1 , nokhlo(opop€n€
cis-l3-olc orop|lp€ne
t-ar6-l,goicnioloFopen€
Ehy'b€rEene
H€Iadlhrobiadione
2+lqamn€ (lrBKl
lsoproAjbenrsns
UemM b.ttulyl 6h€i
+lr€M2.p€rteione (MIBK)
tlelvens d ofide
flaphhaleoo
Styr€n€
ARL
ARL
SRL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
ARL
ORL
BRL
BRL
8RL
ARLgRt
aRI
aRt
BRL
BRL
BRL
BRL
BRL
BRL
BRI-
8RLgRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
8RL
aRl-
BRL
SRL
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
|lg|IS wst 5.0
|lgtS lrsl 100
|jgfig,^€l 5.0
tJ91S n€l 5.0
|lEAErel 5.0
lo,lg 161 50
IS,tS'Net 5.0
Nfi{gwst 5.0
t'gfig w€l 10.0
|,g4g trl s0.0
lJg/}g vrel 5-0
|lgtS i€r 5.0
UgrSrel t0
ldfq wel 25.0
tgkSv€t 5.0
Igtgu/el 5.0
lgtg u€l 10.0
lgfgvJal 50
UgtS wsr r00
ygtSrd 10
HYtsYrel 50
pstlqw€t 100
trytg$€t 5.0
|Jg/](! €l 5.0
lErS{'€1 s.0
$gldr,€l 50
llg.*S rsl 5.0
pgrs'.vel t0
|Jg/](g wel 10.0
|jg/|(S wet 5.0
|,gtg v€t 5.0
!$49 'r€l 5-0
tlgrs vlel 5 0
Hg*Sr/€l 50
pgA€ wsl 5.0
t€/tgr€l 5-0
pglqwel 5.0
llgA9 wst 5.0
|J{}rtS wet 5.0
lgtg Y/el 5.0
lEl0rdl 5.0
|4^gwal 5.0
llglrS rdt 50.0
|lgfrg wel 5.0
lglqwat 5.0
US"lqwst 5.0
|,g}swd s{1.0
|ldtS $61 50.0
WIS Y/€l 5-0
US4S wal 5I)
tlg/rs l.€| t0
Thit lzbordort rE ort is t ot valid fi'Uhoq an zathori@d sit taUe on lhc co!.t page-
+ R€Forlable Dct$tion Limit BRL = Belorl/ Reponing Limit Peg€ to2 of 154
Page 688
Volatile Organic Compoulrds - Quality Colrtrol
Analyte{s) Resul t Flag Units .RDLSpike
Level
R}DLimit
Source %REC
Result %REC l-imits RPD
Brach 70317m - SW846 5015A Soil oow l€vel)
Elrnl aTlBlZl0€LKl I
PrBpaEd A Analyu€d: 29-Mad7
1,1,1Z.Tslrad orcefiano
1,1 22.T6trachtom€hane
Io[adt|fosf|€ne
l29T*J olod€nz€rE
r Z,{.Tftnbrct€nz€r€
I,1 ,l -Ticiloo€liarE
1,1 ,z-Tichlomshan€
Tdcn|orp€ttene
Tdci,lolbfl uc.onefi an6 (FI€m 1 I )l3$Tridlorqropam
l2+TdnE$y{b6nzene
l3FTdm€trrylbenz€{r€
VirV dlldid€
m*rxyiens
T€t"ltydolu'
E$ryl6t1q
Tsl{r'yl mery eh€r
E ryl hn bulyl st'€r
D-asopmpyl ehe.
TstB',{anol / t{tyl alcofiol
l+DioEra
Sarqab: 1at.,']{,fin'tr,tFnzefleSEt@: f&ate$gfiogelEj 1 2-9itttto@thaned4Sunq&: Dbrurolknw$hane
LCs ('ttsr ?9G8f r
Pre€arcd E Ans4z6d: 29-Mar.{7
l,1p.Trid{ootlff ljorosthan€ (Frcon 1 13)
Bgu€nt
SotuterEEne
Brcnoddlloronsh€ne
&flmfofln
Brqnon€fisn€
2€ulanon€ {LCK)n.8v!&enzena
sec€dll0€nzene
l6|i€tltlib€nrene
Cdtm dsilfde
Csbff bradtflide
Cltbo€ttne
O orolorln
chhromefEn€
2{trldollu€n€
{{hbor{L€n€
r3{ttfi o-3{,hlo0propane
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
BRL
ERL
BRL
BRL
BRL
BRL
BRL
55.258.4
2 0 4
13.7
2 r . 2
20_8' t t .1
18.9
22.9
19.8
20.8
14.4
17.A
11.7
r 8 5
1 7 8
1 9 8
17.S
17.8
2 0 4
20.2
17.8
19.1
16.f
pg4€ wel
pqfig v/et
pgfig s'et
pg,l(g viel
Pglg w€l
|lg]kgwel
lJg]l(s w€l
tiglg w€l
!g4g wel
ISAS wel
lSAg w€l
lSnq v€l
USAS wel
!s/rs v,/el
!s4s vrel
!94(S v€]
!SA! v€t
!A/l(S vJ€i
!Srl! wet
pg^S yret
pdk! yrei
rcI(S lvet
!S4S wel
pg4(S s/€4pg^0 v€l
lSnq vr€lUYlo v€l
pg/](sw€l
!9,t0 e/el
ljg,kg wet
pqi(g w€t
pgr(g w€t
pgts w€t
!S/tg wet
ldkg wet
ldkg wet
llgn(gwel
|.qftg wel
yen(g wst
ygtg rel
trgAs w6l
|lg,tS wel
US.4S YlBl
|/gl}S "€l
NAS vJel
lErg v€t
lsiks wel
!S/rO v€l
5.0
5 0
5 0
5i
5 0
5.0
5.0
5.0
5.0
5 0
5.0
t00
5.0
500
5.0
5-0
5.0
5.0
500
100
fi.050.050.050.0
105 m130flo n-130117 7Fli0fit 7et30
102 7F130
68 1n-175
106 70-1&
104 70-13!
E6 7F130
94 7G130
114 7G130
99 7G130
104 55.3t36
72 U.8-142
E9 7F130
88 7F130
92 7013{)
89 7t!13{
99 7F130
90 711130
89 55_1130
102 7S130
101 70.t3t)
89 7O.tA)
96 70rt0
E4 70131
20.020.02!.4
20.0
20.0
20.0
m.0
200
? 0 0
m.0
m_0
200
20.0
20.0
200
ml
m!20_0
200
20_0
m.0n.0
Thit labo&tnv report ir not t)zld Hithout an aathotiaed siCnalure on tha coyer page
+ Rcportable Detection Limit BRL = Below ReportiDg Limit Page 103 of 154
Page 689
Volatile Organlc Comporlds - Quallfy Control
Analyte{s) Result Flag Units +RDLSpike Source
Level Rcsutt %REC
7.RECLimits
RPDRPD Limit
Bstch 7031790 - swE{5 5035A Soil (hw levet)
l-cs ft6t7!xl86l I
Prcpared f Ana|}.edr 29.lrar{7
|,?OiDoflo€herE {EoA)0ikonlometErB
l,Slldhrob€nrene
1 ,+oid orch.nrElo
Dk$brldfl oo|Dlnehrne (F|9on12)
1,1{id{do€tlans
l20inbm€tuiE
I ,1-oin|o|lefi€rc
cal ,2{knbBfHrs
fans- l.+DirriooetEne
1 ,2-Dii$b!grp,r€I ,}Dkldc.oglpan€
22oichloropopane
1, mtnloroprop€ne
cbr,!Dichbopooerc
trans-l,$Dir]lloroprqene
Efiytotone
2-H€xanone (MBru
€dtyl M.b'dyl 6m€r.l.ii,!ehM"-ps{anon6 (MISK)
lhphfialene
SlyGne
1,1.1J-Tstsrd o@than6
1,122-Tenacltkf,.€tune
l,elTit{o.ob€n4n€
1,1,l.Tri* orEstune
1.12-Tdcild@hsrF
Tridic.o€fro|E
Tritlc|oftrorlno0lano (Fl€on I 1)
1,2, rit{ctropqarF
1,2,+Tttndrylben26ne
l S,STidrshybfilene
m,FXyhm
ox),lor€
T#rht!fil'3n
Et1t.$er
Tsl-€rnyl ir€hyl odl€r
Ehryl tsd-hnyl 6!10r
Ll.boproptlsts
I€d.S{bnd / hn9 dcoM
22.1
23.1
21.5
t7.9
17.8
17.5
17.4
21.7
19.8
18.5
19.7
22.2
22_6
17.8
19.6
22.2
24.3
18.3
17_6
r6.21 7 . 3
1 8 . r
2 1 . 8'14_1
1 8 . 7
18,5
17.9
18.6
19.5
16.4
21.0
20.7
1g-8
18.3
r8.6
23.3
18.6
2 1 5
18-9
18.6
21.1
17.5
20.5
20_3
21A
20.9
204
|Jfl](s'r€r
!f4g w€l
ug,10 rc{
tdIS r€l
ldkg wot
ygtg wol
ugll(gwet
!c/rs Y€l
!s,*s wd
|Jg'tsrcl
tatg rst
tdtq wet
pg/ts n€l
ldrS $,€l
t,grswd
|]gtS ftl
}lg4(g Yrel
WtS t{01
U91S r{sl
lry](s s,srljg,xsw€l
lSfS Y€i
|EErcr
9Snq w€t
tryrE \*01
llgl(s, l
$gkS {€t
rrS,4S risl
!S/rS wBi
|jg/IS net
L€,lq wst
1 919 r,6l
llgkgs/et
!C4(S ur€l
lgthgrel
tidrq r€r
t4I€mt
U9k9 ebt
Ugtg t{€l
|4/kgYr€l
lEIg wsl
!9|q wd
rclVIstpdqfft
U9l0 ict
ldrg $€l
|lgll(0 *€l
!s,to |Id
|lg& wet
pslq wel
4.020020.0n.020020.02()0fi.020.0&i200200m.020.020nn.0N.O
m.o20.0m.020.020.020.0m.0a!20.0200200MT20020.0at.04.020,020-0201m.0fi0m.020.0m-020,020.040.020,0
N.020.0m04nm3m
r10 64.7-13S
6 7F130
r08 7Gr3)
90 7IIt30
80 70130
88 711130
87 31.+157
16 7G1A)
99 7$13)
c 70130
106 70.130
98 71!130
111 7G130
r13 70130
69 70-130
99 7Gr30
11t 701C)
1U 70-130
92 7G13)
88 m.7.14{t
81 70.t4)
86 TGlm
90 7&130
1011 70.130
70 rt6.1t 45
91 7G131)
!2 ?$1X0
90 701!10
93 7El:l(l
9€ 7S130
8C 70-130
t05 7F1m
t04 70-13n
94 7Gl3)
!l2 70.130
9i| 7l!r30
117 7F130
fi6 7F130
9B 56.&1.10
r08 7Gr30
94 TG|A)
9r' 70130
108 TFrm
8g M30
8€ TrIlO
la2 7Gt3)
102 6a$r3)
llxr 70130
118 7tlitr)
l& 7F13I)
tm 7{}1g)
Ihb hhoratoq Epo.t it noa ealid htitho .E attrtodzed dgadfure od lhc cover page.
' Repo.lable Detcction Limit BRL = Bdow Reportiog Limit Pag€ l{X of 154
Page 690
Volatile Organic Compounds - Quality Conarol
Br.ch 70Jt790 - SW846 5015A Soit oow tev€,,
LCS tn61?m-ASt)
Pr€pad I tuuryzoc ?9Mar47
t,+DioIar€
Slr/r,.fa*:a8]olrffifl/.0banzeneSato&la:Tdhng-dsmrylp:l?.tkltotAtM4furogaia: Dfuonlr'jflu onekane
LCS llno f?BlllGBS0l)
Propdsd & turJFed: 2$f.iar{7
I,l2'Tricnlo.obnuo.oohan€ (Freon 1t3)
Anylonbih
EromobdEerE
Eromoctlkrom€hans
8rfilodichtorofl€tlane
Bro,nolorl|r
Emnometlme
2$ibnoiE (IIEX)
ngJtib€nzeft
3ec-8rr!&st:€r€
teGBdylb€m€n€
C€fton dsufte
Grton b,tact{oid€
Chlor(loonzmo
Cl ooohane
Chlo|Elfin
ChldEfiohan€
2{hlorohegle
4.Cilorot{-rd€
1,2-OltronF3d mpropan€
1 2oih{cnosdlar€ (EDB)
0ibEmo|nafEne
1P.Dk r.ob€izar€
1 &0kihob€nz€rE
1 ,+Didlh.$g|z'l€
o{c+hmlff m'un€d|8ne (Freff 1 ?)
1,1.Dd{d€tnd|€
13-Did om€0wo
l.l-Drnl'o60|$e
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feEnS-Dkft.oe$€ne
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I,$mfttEFlpar'€
e2.Did'hoFlpane
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cb-l,&0icnhrqopene
r!ft{,lDdtoraops}e
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Hfled{otobubdien€
2+I aiono (tilBx)
laogopyitqueo€
9 6 2
52.055.349.152.8
r8.6' t 5.1
21.9
22.2
1 7 . 1
20.1
23.6
19.7
20.7
14_2
18.6
1 7 . 7
18.4
1 6 . 3
1 9 3
1S_1
21_1
202
2 1 . 0
18_6
19.2
18.3
2 3 5
20.7
21.1
17.8
1 8 . 8
17.6
22.2
2 1 6
2 t . 2
17.2
20.0
2 1 . 6
21.5
22.O
1 8 . 1
20.6
23.4
230
18.9
1 A 4
16.6'17.3
!g*S v€l
lsas v.€l
ls,frs v€r
us/ts w€l
|lg/(s w€r
l4/kqwet
!gl(g wet
!!r'lq wet
pglq vi€t
Pg&g w€t
lgltrg wet
pg,tq wet
!q q wer
lglq wer
pg,r(s w€l
pg,lq u,el
Mgwel
lgag wer
PS,kl wel
PgtS vrel
us/rq (cl
lsits $€l
PSAS w€l
pg^g \rel
!9&g wel
pg/kq wel
ps4(s wel
pglq w€l
pgag wel
pgkg wel
!s4q w€l
pg,lq wel
Pgfig wel
!9,4q s€L
|l9rlg wel
!g1g wel
!gl{g wet
|al(swet
lSnq r€t
pglq wet
ljdksrct
l4/4(g l^et
llgnq wet
|lg4q $et
l]g(s,,t€r
ljgrts ra
!9(S rct
!s.&s N/€{
ug,'l(S w6l
Spike
2@g0
50.050.050.0
200
20.0
20.0
20.0
20.0
20.0
20.0
al.0
al.0
20.0
20.0
20.0
20.0
200
20.0
200
20.0
20.0
20.0
200
20.0
m.0
x.020.0
20.0
20.0
20.0
20.0
20.0
20.0
al.0
al.0
2n.020.020.020021).020.020020.0200?00m.0200
49 34-t55
tN 70-130lfi lFtms9 fot30106 70.130
93 ?Gt30 9
76 1.17-115 11
1r0 7D130 4
111 7$1fr 7
86 70-1m 0
100 7&130 6
118 70130 3
s8 70-130 1
t0{ 55 }136 0
71 38.V142 r
93 70-130 4
a8 70-1U D
s2 70t30 0
s2 7F1XO 3
96 7F130 3
9€ /G130 6
106 55.91$ 17
101 7trt30 |
10s 7F130 4
93 7G130 4
96 70t30 0
92 7G130 9
1lE 64.7-13!t 7
104 70t30 tl
106 70-130 2
89 7G130 1
94 7G1m 5
88 70-130 0
111 34.4-167 24
108 70n30 0
106 70-130 7
86 70t30 1
100 70130 6
108 70-130 10
108 70-130 3
1t0 7t !130 3
90 7F1gl 1
103 7+r 30 4
117 7l!130 5
115 7t I130 6
9.4 70-130 2
s2 60 7n40 4
83 70t30 2
86 7rlr 30 0
50
25
25
25
25
25
50
50
25
25
25
25
25
25
50
25
25
25
25
25
25
25
50
25
25
25
25
25
25
25
25
25
25
25
25
50
25
25
Thb labonlor! reporl h ,tol rsIU without ofi oatho aed slgwturc on th4 corvr paqe
+ Reportable D€rection Linit BRL: Below Reporting Limit Pag€ 105 of 154
Page 691
Volstil€ Orgadc Compounds - Quslity Control
Analytqs) R€sult Flag Udits
Sour€e %RxC
Result '/.REC Limits.RDLSpik€LEvel
RPD
LimitRPD
Balct 7011790 - SW846 $35A Soil (low l€vel)
LCS 0|lor sltg08sDl|
Repdrd A tuelyzed: 2+1tu{7
4lsoorFyiblu€r|e
lil€dryl E t{tnt e$er
4-l'leM2{€r'tanon€ (M|BK)
tladrtEld|e
n-ADB/ber|zon€
StyrerE
l.|,12'f€t3d ometlane
1,1 22.T€Facnbroefiane
T€fadlff!€fl€rle
Tdueng
| 2,$Tnd otEbenz€ns
l.?+Iddkrob6nz6n6
I,1,1-lri{ih.oeflom
1,l2.Tdttoo€hane
TrElloofl mron€han€ {FGon 11)
l2Cfdflorofropano
1z+TdrEtylbenzono
I,3,$Tdme$ylb€nz€n€
m"pxyl€ns
TehahrtDilrdn
Efiryl €fier
Eftyl l€rt&nyl €$er
orhoprlpy' ehe.
T€darffol / butyl alcoiol
l,+tIoEll€
Sffiryb: +Brwnott?ro,''wrlagfiqg,d,:TdrEtEd
Suttw:1zetu cf/'a !€44s,''.{d4:Ohtun&r1ddwe
B.Lh 7Gr797 - SW846 5030 Wrt€r MS
8E* filr7g?€1xt I
PG9ar€d e Anallz€d 2$l]lafo7
1,l,2'frittooflnufodnarE {Fl€on 113)
B€n2ers
Eroorobclz€ne
Erfirodh|Drned|a E
8rcflodci|ororlEtls'le
€|Urbfuti
8romffn€|lrane
2AnarsrF (MEn
iAlt|t€rErE
s*€tttdEene
l€d-Br4t€rEsrs
C€Itm d€did€
18.9
2 r .822_020.020_51A-218_6r 9 516.6
20.019.718.719.221.9
18.921_2l s l18.023.436.419.521.320.722.324120.91742445055At4&1523
BRL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRI-
ARL
!$s Yrel
|lEtswd
|lg/rS r€l
!E/lq rcl
lEtAlstpglq vlst
Ugrtq wel
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r Rcportabl€ Det€ciioE Umit BRL = B€low Reportiqg Limit Page 106 of 154
Page 692
Volatile Orgsnic Compoutrds - Quality Control
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Page 693
Volatile Orgrtric Compouods - Qurliay Cotrtrol
Analytds) R€iult Flag Units Resuk %REC Limits RPD
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Page 694
\rolatile Organic Compounds - Qualiay Control
Spike Source %REC RPDAnelyt€G) Resutt Flag Units |RDL Levet Result %REC Limils RpD Limit
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+ Reportablc Detection Limit BRL = Below ReDonins Limit Page t09 of lJ4
Page 695
Volitil€ Orgenic Compourds - Qurlity Cotrarol
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Volaaile Orgaric Compounds - eudity Control
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15450.052.850.6
Sourc!: SA5gtigr.ts
18.9
19.4
2 1 . 2
19.3
19.4
45.050.253.5fl.7
BRL
ARL
BRL
BRL
BRL
BRL
204 BRL 93
20.0 BBt 94
20.0 BRL '06
20.0 8RL 9.{
20.0 0.530 9s
504 9l500 10a50.0 16fi.o 101
20.0 BFL 94
20.0 BnL 97
x.0 881 106
m.0 8FL 96
m0 0.530 9,4
fl.o 9050.0 100u.0 t0/flo 101
I
3
0
2
I
30
JO
30
30
30
Bdcl ru | 8gl - SWt46 5030 Soil (ftigh teveli
Elitt a?8t80{u(| |
Pr$€r€d E AnatEedt 2$Mar{7
l.r,2-llt,1o|!'inuomshsrE lFr6n 113)
Adtk'itile
BE dr€
Broorobglrsl€
Saofioclthrfidrans
l,s4g Yiel
tl$,lsrid
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tJqks $,€t
E4(S.r€t
tckglrst
1.0
20.0
1.0
t .0
1.0
1.0
Thk laborutory ,eporl b ao, valid wirhout al aathoi&A sigacrwe on thz .owr page.+ Reportabl€ Detection Limit BRt_ = Betou/ ReDortinp Limit P a s € l l 1 o f l 5 4
Page 697
Volrtil€ Organic Compounds - Qurlity Conarol
Analyte{t Result Fla8 Units +RDLSpike
t€vel
Sourc€
Result %REC
7.RECLimits
RPD
LimitRPD
B.tch 7031830 - SW846 5"030 Soil Otgh level)
Blsnk l-llts lgi|0€LIl I
Pr€paled A Anaryzed: ?$lrai.07
Bomodcilorom€f|a E
Bromoneli€ne
2-8uhnm€ (MEX)
n-&iylb€nzene
se€uttbsnzene
FnAuU1tl6nzgl€
Qrbon dsufide
Calbon Elracnbidg
Chlorogtune
ftbro{tn
Chloroor€hBne
2-Chloololuei€
4{hloobtueno
1 2.oibDmFCctloroprop.ne
1 ,z.0bomoe[larE (ED€]
12Oi:lioron€nzon€
l,SDichlorohsEene
I ,+Dicldorcbenzsle
Dd ondaluoomefiaft (Frsonlz)
1 , l{i{nritoetEn€
1 ,2.oknhrBfsne
1 ,l.Dictdooefi€ne
c,s-r z-oicn|ollehene
lrans-1 2-DiltoroerEn€
I SOid oroprcpan€
|,Sod'hropmpane
22-0lJ oropoAan€
l,l-Uol olopop€{le
c6.1 ,$O.ibropropen€lr8rB-l
"'Djtjl'looF(opEitsEhylEruerc
z+l€raione {MBK)
Mottyi bftutyl €he.
+Meqy''2 pslanone (Mg!
M€tyhlr€ ct odle
StIEie
1 ,l,l2.Tetadtdo€hans1 ,1Pz.I€tac|loroetan€
T.hchlol€fi€n€
l SgTftilorob€rz€nolz&Trirrlorcb.nz€ne
BRL
BRL
BRL
BRL
BRLgRL
ARL
8Rf
BRT
ARL
8RL
BRL
BRL
ARL
ARL
BRL
ARL
sRr-BFT
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
aa|.8Rt-BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
a8l
ARL
8RL
BRL
ARL
ARL
BRL
ARL
ERL
BRI
8Rt-
BRLgRL
BRL
Ugkgwet 1.0
Wk! wst 13
|MS u/€l 2n
|4AS wel 10.0
|jg,tSr€l 1.0
la/rS id 1.0
rc/lqrel 1.0
$ftSxd 5.0
t€,lqrvst 1.0
Ug,ircYrot 1.0
tJgng r{€l 2.0
|J9AS rct l0
|Jg''(g Y€l 2.0
Mgxr€l 10
ltgtS iEl 1.0
ySrq trer 2.0
|{lql€t 1.0
Ig'rqrEt 1.0
$'lqvrd 1-0
l,gilqriel l.o
|EkS |€t 1.0
!S'lq ftl 1-0
t4ftSrd 2-0
lgtSEl 1.0
lgrSlrsl r.0
tlQlq iiot 1.0
l8llq wst 1.0
l4}r9 fit L0
trytg fel 10
lgrqwet lO
|JgkS {'€l 1.0
|JgrS r€l 1.0
|lg4(S i/€l | 0
|lg/tS d 1.0
UdtS ftl 1.0
|lglts $sr 1.0
USrq'iet 10.0
|4ikS wst 1.0
Iglqwel 1-0
|l0,|(0,r4l 1.0
||gtS |!,sl 10.0
tg,l€ 6{ lo0
lgtSv€l 1-0
tiStS rEl 1.0
lgfS |Bl 1.0
l8/lqrEl 1.0
Udlq mt 1.0
EI€ wot 1.0
$lq $st I o
|4/tS s6l 1.0
|lgllq u/€l l-0
ThX hboftloryqo.l it not wld t' haul oa Mthoriatr 6tgnaur. oa the cover page
+ ReporEble Det€ction Limit BRL = B€low RoFrting Limit P.Ee I l2 of 154
Page 698
Volatile Organic Compou||ds - Qurlity Conarol
turalyte(s) Result FlaB Result o/'REC*RDLUnits
SpikeLevet
% RECLimits
RTDLimilRPD
B{hh ?1131830 - SW846 s030 So (high tever)
Blrnk ?6U10+Ufl |
Prcpar€d E Aftla€d: 29-Mar07
1 ,1, l.TfLhlooohan€
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1,+Dioxsne
Si,flcg €: +Brnpthl@&enrene$'r'Wb; Iolugl€4gnt!€ela: | 2.6d{o!@kaia44tu'cgdc: Es,anofrJaronekane
lcs fraracBsl I
PrEpar€d t Anavu€dr 2+Mar{7
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&oflEdrlolt'nelEn€
&omolcrrn
Brofirofis$an€
2€uhno$€ {i{EK)r!8ut*s|rei|€
str-&ryt€nzgp
bfi'4lbe|lzone
Caftofl dsdfdo
Ca,bon bt'ddiorids
Cllorc!€rE€nq
orbstlane
A{oroldm
Cl ordr€hane
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+Ct{orsbtu€ns
| :-Ubroitolchhrclropane
fikllmcf,lo(gnohrn€
lSlXhon'ooUqne (EDB)
Dlro|IronE tan€
l2-Dl$ttotft6i€
tr'}Djdl<beE€ns
1,l-oklrdobdu€n€
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BRL
BRL
BRI
BRL
ARL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
8RL
BRL
BRL
BRL
30.49.0
29.I
18.9
10.8
1 9 . 3
21.9
2 1 8
21.4
22.3
22.2
22.2
13.3
16_5
18.8
20_0
17_B
1 7 . 0
21.3
1 9 8
2 0 9
21.0
21.O
20.7
19.4
21.5
22.2
20_8
21.5
2 1 . 1
20,8
pE4(S w€t
!S.4(S s€l
pS/tS r.€l
WlrSwet
{,gn(gllet
!g4q wst
t'glq wst
p9l(g wel
|lgnq $€l
!S.4(S wel
pg,4(swer
|rg((Sw€t
!g/kg let
lEkg wet
pg,tq wel
pg/l(s wel
rc*S nel
!S^S v€l|ls4srclpgRs Bpt
llgn(S wet
pS/kU vr€l
lgfrS v,/ei
!o.ft! w€1
!g-tS lvel
llg|rS wet
|lg/kq wet
pgn(g wet
trg4q w€t
ygr'kg wet
lqrrq v/el
pg/](g wel
pglq w€l
pg/tg v.€l
|l{/k0 |let
!S.4(S vr6t
!S,4(S Y.€l
|lg,4(S wet
!sl(s wet
US4q wet
tlga(swst
lafigtr€t
!9[(g wel
lSftS vEl
pglq wel
!0Iq €1
p9k9 y€l
Msve!S/tS v€l
u.Df i030.a30.0
200
m 020.0
2DD
20.0
20.0
20.0
20.0
m.0
m.0
NT
20.0
20.0
20.0
20.0
200
m.0m.020.020.0
m.0
20.0
200
20.0
200
20.0
m.0
m.0
7G13470-1U7013070-130
70130
1.77175
7G t30
7D-130
7rI130
70'130
70-t30
7F130
55 3136
3EE-1€
7G130
70130
7S130
7S130
70t30
70lm
55.3t30
7GI31l
7F1311
70-130
70.130
7G130
u.7-t@
7S130
7S130
7G130
18130
7tI130
1.0
1.0
1.0
1.0
1 0
1.0
1.0
l 0
2.0
1 0
1 0 0
1.0
1.0
t 0
i .0
r 0 0
200
1011t)tJ90
96
1 r 0
i09
107
112
1
1 1 1
o2
94
100
89
85
r06
99
r04
t05
105
t04
99
tm1 1 1
1Q4
106
106
104
This labodory rcpod it not volid wirhoul an auhorAe.I sigt alare on th4 cowt page .+ Repodable Detecrion Limir BRL = Below ReDortine Limjr Page l l3 of 154
Page 699
Volatile Orgrtric Compounds - Quality Control
Anallte(s) Resulr Flag Units rRDLSpiketevel RFD
RPDLimit
SourDe %REC
Resul. %REC Limits
Brtcb 70Jl8J0 - SW846 50J0 Soil (tigt l€vel)
LCS fi031030{Sifl
ft+'red e Amvlad: E.Mr.07
fi chlorcdinudsnsha,€ 1F€on 12)
|,1-Oichlorostlan€
t,ADicl ooourane
1 , l-Diciloroefiene
cisl 2-oidbo€tl€ne
lca(F1 2-ClcNor!€dlens1 ,z'DichlorogoparE
|,9Dld{oroFocane
22'0ktlflopoo8ne
l,1-DlfilompmfEne
cb.l,}Dcnh.opmpene
Fais. 1,3'0ir{oroprop6ne
Eu|)lberE€ir€
z+lexsncne (iAK)
lre$yl led.b|tt€fier
4-f re$yl-2-pstande t\rlPro
r|.d|r€J€n€
Styr€ne
1 ,1,1 z-TeFddllorefi€no
1,I,22.Tsted oroe$sne
1 ,2,&T.itlorobs|zsne
1,1,t-TriJ orooharp
1 ,1 ,2.Triciloroehane
Itichho0ldunrhan€ (F|€dr I !i
1 z$Tndrloropopen€
1,2,4.Tirn€htb€.'zene
1 ,3!5Tdm€ryD€r|zsn€
Vinyi chlorid€
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Etryl redaru 6!Fr
oi.isoprDpyl €lr€r
Tst Eobnol / butyl akohol
1,+Oioxan8
Sffiggae: 4-ett&,altDelvErpSw.gate- fotJeia-d8SnryE: | z-DlcftbtfrUl{t'44S unqab: fturqnoltuotfr |Fdane
t C{l t}uo fiBr&F.BsDl I
20.3
20.4
19.5'19.1
19.S
22.0
21.4
t6.6
20.4
20.4
21.O
20.7
18_3
12_7
19.4
191
m.417.7
r9.5
r8.5
17.2
22.7
21_5
20.3
17.9
19.6
r9.2
1S.1
18.3
22.2
21.1
17.9
23_6
20.4
20.7
19.3
41.4
21.4
20.6
2 l . l
1S_8
20.1
18.6
142
178
fr.027.145
|4{q w€t
pglq v,st
|l9l(r$,er
l]9AS $sl
pdrS s,€l
!Slk0 $€l
lgtS r€l
l'9&|,d
ldq r€l
Elq "rd|/grq Yr€t
I9l€ wl
ug/lSwer
|Jgr0 $€r
Qcl wltgwel
,iSA0 Y€l
|4t(srelpdls rd
t8tg'|€1
l4/tg vrel
rc'lq wol
pdLg '|d
|dk0 [$t
|]g^g fr€l
tJg|lS *€l
l4*srcl
UdtS rE!
Igrg ftl
|{lq $sl
EIqt|Et
Etq f.ot
ug,rg eal
ugrcsttMS rsl
afrs rid
ti94g {€l
tjgtSrJd
ugts i/€l
ll(J'rg|'.t
rcI(g r€l
PgkS rct
ustq *st
mlq vrst
|,qkg €l
|dtS $€l
|MS $/€l
WtS it€l
Ugk {sl
|4itS w€{
HIq wel
20_0
m020.0ft.0
.020.0200m!mi20.0m.020.0m.020.020.020_0200m!m.0m.0m 0ru0m.0m.0mn200200mn,0.0fl-020.0N.ON.0N.0m.0200mn10i
from.0,0.0,0.010.0m.0mN$.0$.0$-09.0
34.+r67
fl}130
7tI130
7G130
7G130
7D!30
70130
7G130
70-130
70-130
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70-r30
70-r30
60,7n40
7S130
zllm
7G130
7&131)( j .1n45
7G13I)
70-r3n
7St30
7St30
70i30
7Gt 30
7(}130
7l'131)
70-130
7G130
7Gr30
7G130
70.!30
55.8-r10
7D130
7F130
7F130
7tl1g)
7G13{l
70n3)
70-r3l
65.$t3]
7Gr3l
7Gr30
7(}r30
7F130
3+155
TAtgv,tfr7ttfr70-1fr
lM.
1W
9E
t{t9
sg110107
E
I(E
r0et05
104p
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08
92
4
108
1(E
90
s6
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l116
90
1 1 €
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100
93
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This labrcllrqt .cport h aot vdid nttou! on zaahorizrd sigrrttue on the cover p4ge,
i Reportable Detecliotr Limit BRL = Below Reporting Limit P€ge I 14 of 154
Page 700
Volatile Organic Compounds - Quality Control
Spikc Source %REC RPI)Analt'teG) tusult Flag uoits *RDL Levet Resujr %R_EC Ljrnjrs RpD Lrntr
Batcb 703183'0- SW8{6 s030 Soit (high levet)ft€pgred t Anotyzed: 2$Uarr}7
I,I,2.Idd oroffiuom€f|ane (Freon i 13) 18.0A.elone 10.5A{tyton|,ilo 19.18eorem 2O.tBrmbbenzeno 21.2Broln d oronohane ZO.9BlDmodEhlordn€ftana 21.3&Drnohm 22.2&omorFttans 21.72.Bubrsns (lrEq 13_1ftg{Vb€nzene 16 0s€r-Eutylben:sD 17.sBl{uvbslzffe 19.3Cafta'd6dfid€ 17.sCtbQnbtact{orjds 16 2C orobenzeno 20 4Cflon€tlsrE 18.3c oro{qm 20.0Ct{orom€tEr€ t9.42{hlo|lblLFir€ 19.94{ olbbl!€ie ZO.Ol,2-DihomekfihrDpopafte 19.8tlihtnfttldDnetlane 21.112{ibo@sltan6(EDts) 22.2Oibrcrmmethar€ 2O.2l,2{idllorohsuene 21.11,$Oi**orotffzens 20.31 ,€irhlorotfi:€ne ZO.4D,cflorodiffuoromet|ane (FGonl2J 2O.1l,lohhloroenune .19.6
l2{l* orodlan€ 19.0I,IO*J oroshsn€ t.6cis.l,2{ichboeti€n€ 20.30nns.1l-06tt0efiene 18.6lSoinbroFopano 20_61,3{hhlompmp6ne 21.12loahloropopafl€ 15.41,1€inkn!popei6 19.5del,3-Did{ao0ropsE 2o1trts.13fi:.ltbiop.Wene 20IEltylb€n en€ tS_SHe''gd omb'ladi:ne 17-s2+krdEn€08g 12.7fsoFlpylbenz€i€ 1A7+lso[ro9]ftti€n€ 18 5Mottyl$rt.drtyl.figr 19 8+tf€br2tedanone(Mt8K) 1a.2tils{ryhnschhne 1a.2Naphhel€.t€ 18.6FPrcpy{b€nzs€ 16_2Sryreie z1.gt,1, tJ!7.tred&'o6,ldle Zt_2
!S^S wet
lSlq wel
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rclq wer
ldkg w€t
USAS w€l
p0IU wel
tSAg,Nei
ug^S u€l
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!sa! rcr
lgtg Yiet
t4^g wel
dtS wel
uS,tS wel
lls/ts'rEl
lgfrg Bet
l]ql(gmr
ljs/rsmr
|Jq4q wer
!g/kg wer
!g/kq wer
UdiS v€l
!g/t(g sel
UEtg wel
!9r(S v€l
lgtS vr€i
pgrl(S $slpqtg w€l
I,gn(s q,61
pgtq v,,el
|lg4S wel
lslq $si
iryrs v€i
|Jg4q vl€l
lglS v,/€1
lJg4sv€lglS w€l
ISAS wel
lSfto wel
!s/kS w€tqc2 lgtg lwl
lglS v/et
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lStS rcl
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rrSftg yvst
20_0
20.0
20.0
m.0
2 0 0
200
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n.020.4
N.0
20.0
2!.0
20_0
mn200
20.0
20.0
20.0
200
2{.0
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20.0
20.0
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20.0
20.0
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20.0
20.0
20.0
zl.0
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x.020.020.0
20.0
20.0
20.0
m.020.020.0
2!.0
20.0
m.0
20.0
20.0
m.0m.020.0
n.0
90 ?ctm 4 25
52 1.77175 4 50
96 7D130 0 25
104 7F130 6 25
t06 7G130 3 25
104 70"130 3 25
106 7Gr30 6 25
111 7F130 0
10€ 55.S136 3 50
66 38.&142 0 50
80 70t30 ? 25
90 7GI30 4 25
96 7Gr30 4 25
88 70130 1 25
81 70.130 5 25
102 70t30 4 2s
92 55.3130 7 50
100 701130 4 25
97 7F130 I 25
100 7tr130 5
100 70-130 4 25
99 70-130 0 25
106 64.7-139 2 :O
111 70-130 A 25
t01 7G130 3 25
106 70-1m ? 25
102 7Ft30 4 25
102 7!-130 2 25
100 314.167 2 50
98 70130 4 25
95 7Gr30 3 25
8a 7E-r30 9 25
1@ ?11130 7 25
93 7G130 6 25
103 7G130 7 25
106 7q130 0.9 25
77 TVIU O 25
98 7G130 5 25
100 70130 2 25
104 i[130 1 25
r00 7s130 4 25
8E 60 7.140 4 50
64 70130 0 25
94 7G130 3 25
s2 7D130 4 25
99 7$tfi 3 25
91 16 r.r45 3 50
91 7G130 7 25
94 7G130 2 25
s1 7D130 6 25
r10 7G130 4 25
106 7A-130 2 25
Thh bbofarory Epoft b ,toa rolid tt ho4t 4n aallioriz.j signarurc on the cowr pge
i Repo.table D€tection Limit BRL = Below Reporting Limit Pase I 15 of lt'4
Page 701
Voladle Organic Compounds - Quality Cootrol
Analyte(s) R€sult Flag Units R€suft %REC Li@ts
Brtch ?03lE3O- SW846 5030 Soil (high l€vel)
LCS Dl. ftlB183llBsol I
Pr€paBd I AnatF€d: E-{lr€r{7
|,122-Tst€droaoehane
Ie4.TrU oob€|lzsns
1 , t,l-Tdcnb!€fiane
I ,12.Tridkrc€fune
Tdchlom€h€ne
Tncnlomfluo{unsdEne (F€on I 1)
I ,2,&TichlorcFop€rF
1,2,4-Tdm€ltyt€n:€ne
|,3,tlimemtbeoz€ns
m,Fxyi€ne
Etryl etEr
Tsl.aflryi m€frrryt e$er
E ylbn-bry' €tr€r
Diisopropyl eher
T*r€ubnor / buty' alcofid
l,+Oio€ne
SunoCaia: +&sndtotdenAr,eSu.i.g,,b: folu$848Sunogde: rz-M1htttttdE44Suncpeb: Obtonf/;wtonedltr,rc
Pdt sott ooSlSf,trst)
Pr€par€d & tu$/zed: 29-lrar{7
B€nzsne
Chlorob€rEeno
t ,1-Dichloru€flgl€
Surosda lannniaotdstBtg
Sutqab: | z.Dblhtwtlu,neaSuo.gab. Itbwfrtdo,ttf]lllf,ne
:rtk Splt Ouo ft@1830€ll
hEpared & Analfz€di 2SMarOT
I,l -Dichroroo$sle
Tdcnbo€h€rF
Sunngab:4MtuobqueaeStutq4ab. fdu{,/EJ€tutlg,lg: |2-Dhtk@tata-d4St//ioS,/E: ObqdwwdarE
Sour!8: SA59E1+02
20118.818.918.71E.317.322.120.017.O23.1r9.520.214.240_621-31 9 120.1rg.419_516.01U1903t1.1n0269291
21.021.419_3
21.3g33 t76.1a 4
|lg/tg \tst
pg/kg $€l
!gf0 YJel
lgtg I/€l
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106 7Gi30
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ahnt a7altls4t-K
Prerd€d & Anaiz€d: 3GMar.07
This laboruto.r, ,eport Lr,tol wlid i'dhost aA aaho.lld sigtgturg ot th. @w. poge-
. Reportable Drtcctiotr Limit BRL = Bdow Reportine Lirnir Page I 16 of 154
Page 702
Volttile Organic Compounds - Quality Control
Analytdt Result Flug Uoits
Sourc€
Result %REC*RDLSpike
Levcl
%RECLimits
RPDLiInitRPD
Be.ct 7031875 - SWE46 s030 Soil (high tever)
Blrnt a/txlt?5.Blt(1 I
fir8pdEd I Ane@: m{ar{7
I,l 2.Tdd1lolgtiffuflE€nane (Freo.r I 13)
Adylmrtile
8&ilartsgrofiob€nu€n€
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Brdnobfin
2.eiaio$e (MEX)
n.8]ltb€nzeE
se8lnyD€nzsle
lsd4utyibenzsre
Carton disulfd€
Ca6on htachloide
Chlo.obenzene
Crhhf€oane
Chlo|b{ofln
24lo.obluene
1 2otosneldicropropane
fibronfiJdoomshan€
1 2.Dib.onefiane (EDB)
Dibromomelrane
lSDid oobenzone
l,SDrd orobsusne
i,,!Dichlorcbenzene
Dicfl odfl u.rom€fi ane (Freonl2)
I , Hlcn|oroemano
t,lficl ffrt|ane
I,l.llcilorosllsn€
a!.1 B.Oici,lcro€t1€n€ll8ns. | 2.oicnhro€lh€ne|,2{id oropopdr€
l,goid oropopane
2,a0ddl|o.opmldl€
l,l.Diir orop|op€n€
ct}l &Dichboprop€r€rans.t SDichlqop@€n€EhylDen2ene
z+lsxamne ([,!8K)
Itopropylbsnzsn€
4.lsoolQy'uudt€
M€'lit bn tuty4 etre.
4-Ll€ry1.2.p€lnanone {Mt8X)ti€qy'€n€ chtfide
ibplr$d€n€
SVi6ns
ARL
SRL
8RL
ARL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRL
ARL
ARL
BRL
BRL
BRL
ARL
BRL
BRL
BRL
BRL
ARL
8RL
BRL
SRL
BRL
ARL
ARL
BRL
BRL
SRL
BRL
8RL
ARL
BRL
BRL
BRL
BRL
8RL
ARL
!S.49 wel | 0
!S,4S r,,El ?00
!S.4(S w6l 1.0
pg/|(g rel 1.0
lgrq Bel 1.0
llgn(gler 1.0
llg,1(S {el 1.0
lgnqBet 1.0
|J91(g yret 2.0
Ug,4qwet 10.0
UglS$€l 1.0
pSn(ow€l l0
pS,lq wel 10
pqn(g !,{€1 s 0
|Jg/tS v€l l-0
ll9rg$€l 1.0
lJgrs v/6i 2.0
l]g/tg wol L0
!S.4S Yrel 2.o
!S*S '/rsl 1-0
!c/rs wel 1 0
!S,4(S $el 20
pS,4(S wel 1 .0
US.4(S w€l 1 .0
llg&s rcl 1.0
fStS i.'el 10
!q,4(g l{el L0
!S/kS wet 1.0
US,*S ,'el 2.0
!9,*g u'el 1.0
pc4(q *el 10
|lg,/l(S wet 1.0
!S/kS wet 1.0
lgtg wel 1.0
lqrS wel 10
!q4S l'€l 1.0
p4.ts rel 1.0
pg/IS rcr 1.0
llg,4(S w€t 1.0
rrg4g wet 1.0
l]g.tgslet 1.0
llg,4(S {er 1.0
!S^q rel 10 0
pg4(S ml 1.0
|Jg/rSwd 1.0
ug.tS |€l 1 0
lJ94(S 5/el 10.0
lgtS wel 10.0
llg^9 Y{61 1.0
|lg/tS wet 1.0
lls/}S wd 1.0
Thir bborotor! rcW is ttol toud tttlhosl an sr.thorizel signalure oft te coeet page.
r Reportable Detection Limi( BRL = Below Repodng Limit Page I 17 of 154
Page 703
Volrtile Org|nic Compounds - Qu{lity Control
An"lyt€(t Resuh Flag iRDLUnitsSpiket evel
Source %REC
Resuk %REC LimitsRPD
RPD LifinI
Brtch 701lE75 - SW846 5030 Soll (high level)
BLnt ftool8rtBL(l I
Preparsd & Analyz€d: glusrry
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8RL
BRL
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BRL
BRL
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8RL
BRL
BRL
BRL
8.64.08.5n.7
17.6
12.3
20.0
21.6
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2 1 . 9
21.4
13.8
16.2
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21.1
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19.5
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Uglg wet
|j91(s,,€lgS,lq tt€l
|lgl|(S $€l
|loksY/€l
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ldrg v'!l
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|Jg/](s s€t
WIS v€l
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|lgl{0 w6l
|lgllg v€l
|lg]ftg s€r
|l9*9"{€r
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lgrg wel
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li9x0 wsl
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7G130
7tlr30
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7+130
t.0
t .0
1.0
t 0
t 0
1 !
t_0
1.0
1.0
1.0
1.0
1.0
1.0
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2nr.0! 0 0
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Thh bbordtary ?epoil k ,rot valiil tdlhout 4n a$rtoiql signdatE oa rhc orer poge.
I Reportable D€tection Limit BRL = Below Reponine LiEit Posc I l8 of 154
Page 704
Volatile Orgahic Compounds - Quality Cotrtrol
Analyte(s) Result Flae UniLr *RDI,Source %REC
Result %REC Limils
Spik€t€vel
RPI)
Li 'n i tRID
Betch 70!1t75 - sn846 5010 soit {high levet,
[cs r0g1E7s.ast IPrepaGd & l^aked: 3trMar{7oibrDmod 6one$aner 2oihDmoe$ane Foa)Dib.dnoin€harE
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21.2
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17.1
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20.6
17.4
18,6
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1 8 . 8
1t .6
21.4
20.0
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23.4
20.4
20.4
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198
lgftg wet
!S4q w€t
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$/rq wet
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|Jgeqw€l
tgftg s€l
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Uglq wel
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l&lrg wet
lgftg wel
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ugn(g wet
ug4(g w€t
llgts wel
lgeq Y/et
pgtg wet
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llgfrg ret
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fiAS wsl
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lS.ftS w6l
Ms wel
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llg/kg wel
pg,kg !re1
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1U 64.7-139
1116 70-130
!@ 7Gr30
106 70-t30
106 7G130
103 70-130
100 u4157
t01 7G130
99 ?G130
92 7G130
r07 7G130
r00 7G1n
106 7U130
103 7S130
79 7Gr30
98 7G130
98 7F130
100 70130
101 70130
88 60_7-140
66 70130
96 7Ur30
9{ 7Gr30
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s7 461.115
96 7S130
% 70-1p
E6 7Gt30
112 7[130
108 7q130
r00 7Gt30
87 7G130
93 7G130
94 7G130
94 70130
68 70-130
1m 7Gt30
lm 7Gt30
85 56.&140
117 7&130
102 70-130
1U 70,|30
92 7F130
104 7G130
r09 70n30
92 7G130
107 dt.9130
94 7(}13t)
100 7F130
91 7}t3l)
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20.020.0m020.020.020.0mimlJm020020040m_0m 0mo200
m_0
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20n20.0m!200m 020.0200200n.020.020.020.020.0m.020.020020.020.020.020.0m.020.020.0240200,40 020.020.020.0mnmn2002m
This laboratory eporl Lt noa talid wAhoul aa rqthortzed signaturc on rte corer page
. Reportable Detection Limit BRI = Below Reporting Linit Pag€ l19of 154
Page 705
Volatile Orgaoic Compounds - Quality Control
Analyt4s) Resul( Flag
Source
Resuh %REC.RDLUnits
Spike
Lcvcl
%RECLimits RPD
RPDLimit
Br.ch 7011t75 - SW846 s030 Soll (higb l€v€l)
LCS n03lAr5-A$)
Pr€pa€d & Arl8lyredi 30.Ma(17
1,+Dioffegrnog'&j +entuo&etAsgSu|"Sa/f;fdrdffiSr'jmagatd : t ?-D*lktbha1s44S$rqatE Etthtooffi$ondaE
LCS DUE f|tslE?t8EDl I
Pfspared & rnaFetr 3GMar{7
1,1l.TiJ orotituolefEre(Freofi 1t3)
Eenzene
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Carbon bracircdde
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12.6
21.5
21,6
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21.7
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1 7 4
15.7
20.7
19.2
20.0
20.3
19,1
19.6
20.4
21.7
22.4
20.7
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20.020.020.020.0m.020.0
96 34.155
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EE 7F130
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103 7(}130
108 7Dt30
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This ta.6orot4ry Eltort is not yolid Nirtou an aa[rorte{ siF @tE on tte cover psge.i Rcporbble Detection LiEit BRL: Below Reporting Lioir Page lmof 154
Page 706
Vol,ttil€ Orgardc Compounds - Quality Cortrol
An€lyt€(s) R€sult Flas Units
Source %R-EC
Resuh %RlC Limits.RDLSpike
Level
RPDLimitRPD
B"tch 7031875 - Sw845 5010 Soil (high lcycl)
LCS D'io P6l8?5{SDl I
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100 70,130
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126 7F130
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103 70130
106 7Gt30
110 70n30
107 65.'130
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105 7G130
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96 7t!130
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This labo&tory rcport is not valid ttiahozt an althofized signzaure on lhe coyu page .
' Repodable D€t€ction Limit BRL = Below Reporting Limit Page 12l of 154
Page 707
Voladle Orgrnic Compoutrds - Qudity Control
Analyre{s) Resull Flag
source %P.I.CResulr %REC LimirsUnit5 'RDL
slkeIrvel
RPDLiftitRPD
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Sdtrc!: llA5989lr0l
PrepaJed & AndF€d: elMar{7
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' Reporhbl€ Det€ction Lirnit BRL = Belo{ Reporting Limit Page 122 of 154
Page 708
Volatile Organic Compounds - Qurlity Cortrol
Analyt(s) Result Flag Units
Sourcc %REC
Result o;RIC l-imilsIRDLSpike
Level
R?D.RPD Limn
Brtch 7M)017 - SWE{6 5030 Soil (high ler et,
8l.n* Otxlx)l7.8LI1l
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95 7G13070-130
1U 70t30113 70t30
r30 70130
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r14 70t30
103 70.130
108 7tr130
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112 7tr130
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I Repotuble Deteation Limit BRI- = B€low Reponing Limit PaEe 123 of 154
Page 709
Volatile Organic ComporDds - Qualiay CoDtrol
Bc.ch 7M00r7 - sw846 5030 Soit (high t€vrl)
lcs r70a{x}17{sllft€Fsred & Ar€lyzed: 0A-&r-07
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115 5 n30
1r7 7U130
116 7ur30
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110 64.7n3S'r(6 fll-t3)
106 70-130
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110 70-130
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114 70t 30
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100 ?Gr31
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+ Reportable Detectkm Limit BRL = Below ReportinC Limit Page 124 of 154
Page 710
Volatile Organic Compounds - Quality Control
Spike
Lcvel
%REC
Limits
RPDLimit
Source
Result %REC
Bahh ?0{0017 - SwE{6 s030 Soil (high level)
LCA 0UO017-8611
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109 7q130
111 70 t30
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119 70130
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106 7S130
86 3+155
99 70-1&7F130
101 7&130110 /0-1W
126 7SI30
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112 7013)'112 7G130
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112 70,130
116 70 130
lE s5-$136
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96 70-t30
100 70130
116 7G130
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110 7tlr30
114 55.9tff1
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102 7Cr30
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r04 70-130
112 70.13i
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120 /tr130
112 7S130
120 7S130
128 701t0
12r 7G130
1r1 70t30
r07 ?G130
Thb labonlory rcpod is Aot vdd withtu! en aaho.izel sig,,atwe on the cover page.
' Reportable D€lection Limj( BRL = Below Reporting Limit Pag€ 125 of 154
Page 711
Volatil€ Orgrtric Compounds - Qualify Control
Anal]'te(s) Resulr FlaC Unitj
Spike
Lael
RPD
LimitRPD.RDLSouce o/.REC
Resuk %REC Limits
Batch 70400 17 - SW846 5030 Sotl (high l€vel)
LCS oup fiO300l7{EDl I
Pt€pared t tuslyred @-Apr47
?,z.Dichlooglpars
| ,r-0ldlorwop€rE
cjs.t,}k rlprnp€n€
fsrB-|.lDa oopop€n€
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+lsoF@ylbbe06
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1 ,2,9Tnd o.obenz€ns
1.1 2-Tidlor!6heno
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Tdcfilonfluo.flne$ane (Fieon 1 l)
1 ,a+TdnotitltenzF.r€
1 ,3,tlrime$tbenz€rE
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m,Fxylen9
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DiisoprEpyt €0ter
T€n.Euhnol / bulyl atcohol
Snrq4E : 1 -atl'tio,fl uo robsnArEgnwdg: lolu s4gnogab: | zaic o@lnfie44gfiogaie: oihfit]{r'/ttfiont6dlE,ne
Iltfi sdrc flxat7{srl
PrEpar€d E An€@r (E.1Cr.07
EsEen€
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l,lOk$ttibsdmm
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23.222.922.324.021.520.016.120.119.723.,118.423120.017.3
21.3t9-6m.220.920.522.522.421822_524.120.42 r .621.843.022_422.O24.918.424.221.6
190u.3E23t5x?5
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1t4 7Gr30
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120 7[130
im 7F1g)
lm 60.7-14l)
m 7!1m
100 70.1s
90 TFtCl
117 7u130
94 46. r-145
116 7G130
r00 7G130
86 7S130
116 7Gr30
114 7D13I)
t6 7trr30
98 70.131)
r01 70n3)
1U TGiAl
102 7G130
112 70130
112 70-130
rm ru-14)ll2 56.814n
r20 7Gr30
1$2 70130
1d6 fl)130
10s 7tI130
110 7G1g)
ll2 7G130
flo 7Gr30
124 65+tgl
92 7G130
121 7Gr&)
lm ru.130
fl6 70.130
95 34.155
101 7Flfr97 70-1Ut6 7&1Nfiz 7V130
97 7G130
04 ?&t30
112 7F130g0 7}r3l)
9,1 711130
t8 7FlfitE 7F1g
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pg&g $rt
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lls4s wel
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lElS dry
rErs drylStS dry
lgrS dry
lSIq dry
lclq d'yli9tg dl
20020.0
m.020.020.020.020.020im.020020020.020.020.0m.0a).0m.0a).02n.0m020!a).0m.0&.020.0m_0m 020.020-040.020.020.0mnm-020.0m-0200
2m9.0n.09.0fi0
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2
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Thi6 leborutory eporl h Aal aoli.! wuhou aE oEttonel slgnslt.. oa rte cowr psge-
+ Repodible Det€ction Limit BRL = Below Reporting Limit Page | 26 of | 54
Page 712
Volaaile Organic Compounds - Quality Control
Analyte(s) Resutt Fjap Units *RDLSpike
I*ecl
RPT)Lirnit
Source %REC
R€sult %RDC Limits RID
Brt h 70{0017 - sw846 5030 Soil (high lev€r)
Ilt|I5!t owl)l7.flSl)
Pcpar€d & tuatE€t @'A[r{7
Sutqzb : 1,2-0tibr@lhanees!firyb: oibranoluidnehane
tluh sdt D|Jd 0IX{xI7.xsD1l
Rrpeed & lrl3lnod @-Apr{7
8s!zm€
O oroh€n:€n€
I,lojdroroefrera
Tofuslre
Tri{r cio€tiene
Suto{,d3j4atdnotuottunzeneS/!'.'!€,,b: rotuane48SUN9,&: | 2.tthlro!@thane44Stl'logetr: offiudondhane
Sourcer SA59@h 1
Soulc€r SA5989l 1
21926624222.430.5in.4n.0i29
Mgdtl!S4S dry
llg4S dry
lSAg dry
aM7 wkgdry
lElS dry
!s^s dry
ls^s dry
lgfts dry
ls^s drylglg dry
s0.030.0
1Nfi2
112
0
107
112
102101931 t 0
30
30
30
30
30
7619701W
70n30 14
70t3{ 16
70130 17
7G13! 17
70-130 17
7G13070t307t+t3078t30
aaLg8L
88!
219
sRr
20.0
2DA
2D,D
200
20_0
N.AgJ.a
u au a
Thk lobonlory repo.t k trot vd6 flilhoul on aalhorized signaturc on thz cot'e! page
+ Repodabl€ Det€{tion Limit BRL = Below Reporting l,imit PzEe tZ1 ot 154
Page 713
Exarachble P€troleum llydrocarbons - Quality Cootrol
Aralyt€(s) Result Flag Units Result %REC Linits
Bstch 7031722 - SWt4635l0C
ELnt fl03lm.OLK|l
Pr€pare{: 2$l\ler.07 Ala zed: g)-lrar'07
Ge.olin6
Frd Olf2
Frd Ol14
Ff lOl{6
Molor Ol
thid€nt'fied
Oll€r Ot
ToEl Pstd€(ln tly(loca'taE
C$C36 l,Iphdic tlydocaitEnsgfiqab:lA@dE
LCS tTIBl f4.8Sl)
Pr@r€d: 281i1347 AElyred: 3o-tlar{7
CS{36 Alpiadc Htd&caltans
s/l7,q,ata: l.gtutffiddcaft
Drtch ?03 l?72 - SW846 35508
8E1k O0l17z{Ll(ll
PreFredr ?9 aO7 &e!zed: 3Hi&r{?
Gasdin€
Fueloil#2
Foel Otr t4
F0sl Ol 16
Molor Oil
lli{tglffird
Otrsr Ol
Tolal Pefol€un fi ydrocartoni
CgC36 Afitiatic Hydruc€rbaE
SUqWAE' 14hlotffin
LCS ff€l?n€Slt
Pr€pared: zg{arfi lrulvred: 30lil"r{7
CgC36 Al(ot'a|jc rwoca,to|ls
Swogab:1$ sffica,p
q.ncds fr03lTz-0tPt)
Pla9ar6d: 2$t art Arulf!8d 30.tta{7
Gasdk\e
FLd Ot f2
Fii€l Oil 14
FilelOl 16
Molo.oil
Ur*lstr€d
Ot€r Ct
Tdal Pgtdoon tt(loartort'q}C36 Aiphdic HyfiEbdls
Swrc{aPjl.d1bo(t',de:;dE
lstk Sd6 fr031z2{61)
Pr€Fe(l Z$Mar{7 tudyr€d: C}.t arfl
BRL
BRLgRL
ARL
SRL
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BRL
BRL
BRL
BRL
0.K3
1 . 1
o1ltr5
ow
1.10
o6m
10-t10
sl20tu129
0.05
0.05
005
035
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0.05
0.05
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mc/tnrElnEnsrrnS/lrndlms4mgilmg4i'E]
n'St
ngl
mS/rS w6l
rr4/tg rd
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mdlq w€l
mglq wot
flrS,lq *ol
ngtg |r€l
ngkq w€l
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rng4g ad
mglq wst
ttBtg sd
ndlq fiy
n4h dy
'Igbdv
m94q diy
mc q4v
nrglg dry
n'Srq drl
nglq dry
rnsrq dryJ,aM4 oElqdy
'rElq d]
ts8 l
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BRL
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69.7
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soulEe sa5g?u!20
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25.2
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13.3
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+ R@rtable Der€dion Limit BRL = B.low R€porting Linit P|ge 128 of 154
Page 714
f,xtrrctable Petroleum Hydrocarbons - Quality Control
Annlr€(t Result FIag UniLs
Sourc€
Resul( %REC.RDI,Spike
I rvcl
%RECLimits RPD
RID
Limit
Bitch 703 U?2 - SW846 35508
ll|ttr Sdke t6l?n {St }
PreparEd:2g- O7 Amtzed:30- aF07
CgC36 Arphdic Mro€ddrs&n@: tQ ot(frbdecaE
*o0ir Sdfte D|lo O6trn-mfi )
Pt€{.q'€d: 2g{r',xof ttdyzed: ?fr+"htn7
CSC36 Aliphdii Hyd|m€Ao{ls
tunr8ale: l{/no/off,frdecat a
Brlch 7031773 - SW8-16 35508
8b1t OtslII+aIXt )
Prep8rE(t 29+lar-07 &alyz€d: 3SMar47
GeEdins
Fud Ol S2
Frr€l Ofl {.{
Frrd Oit 16
L.!ob.0r
Unid*!fi€d
O$€r 0l
Totbl PrftlewnUydlrtr,n,t|6
C+C36 Atphalic ttdocado,ls
S.nn@E:laroftxtudecarc
Lcs frtsl7t18lt1t
Pr€pend:2$ ar{7 Ala}rled: 30+4ad7
C!}C36 Alphatc tl!/drc.stom
snncg8l€: t{ll/ofteadearc
lluDfic.ie {mrz+txptl
PeparBd: 29ilar{7 tualr2€C 3O-Mar-07
Gasolir€
Fd or 12
Frrd 0{ 14
FrDlOl t6
Mob. ol
thiienffed
O$s 0l
Totd P€tol6({n tfidocaDons
Cg.c36 Aliptslic Hldroc€rbons
tur'gsb:i'j@arE
t.tk S6lla OoSfIil}{SD
Pr6t€rbd: 291{ar-07 lnalFsdr 3CMar-07
CA{36 Aliphdk l{ydrsbofts
&nr.get6| l4t1bkffidearc
Sourc€: 5A5078&28
1.t9
3.79
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mgt€ dy
OM2 nrdkg d/y
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30 5+150
4+140
26 50150
82 4G140
19.6
19.5
138
1.91
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BRL
BRL
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ERL
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?43
8 5 1
381
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216
5 W
rng/rc v'€rmgnq w€l
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mg/kq wel
m!/kg wel
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nu/kq $€l
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Il)g*g r|€l
rig,lq Yr€l
rigftg v'€l
riqkg w€t
rngil(g ret
mgks dry
ftEIq dry
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ry/rs dtynVrS dryfngkg dry
nW4(S dry
i'S.4S dry
ms/ks drymslq dry
so2 mg,kg dry
hq/l(g drys02 lnsnq dry
mqts drys02 ndrgdry
n 4G140
91 @120
14 60.tn
13.3
t3.3
t3.3
13.3
13J
13.3
t3.3
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L W
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BRL
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BRL
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121
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121
121
4.53
sourcl: sA59807.1 1
1S5
5.49
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23.1
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This laboraory ppod is ttot ralid ntithou an ltho zed si9nat re oa lhz cover page.
* Reportable Detection Limit BRL = Below Reporting Limit Page 129 of 154
Page 715
Semivoladl€ Orgrnic Compounds by GC - Quality Cotrtrol
Analyte(s) ResultSpikekvel RPD
RPDLimitFlag Unirs .R'L
Source %REC
Resuft %REC Limits
Botch 7031738 - Sw845 3545A
Ahnkruti|€{LKl)
Ple9aftit 2&Mar{? Amlyled: zS-M{t{7
PCB r0r6
PCg re1
PCB t232
PC,B 1212.
PCS r2{l
ru 1254PC812fl)
rc812e
Ftr81268
Sunogats' 4,fi eefr totfutphdVl (SlSutogea: Madtudiplwyl(54
t-Gs l7)3t?ti84str)
ft€per€d: 28-Msr{ AtEgzed: 2g+{ad7
PCg 1016
rcB 12mSw'og2re: 1,+0ee6L0tu1plwyl l9t)sanllg'F: Dead1/o.o&prE/l,/ (Sn
LCS Dlo O0l1?!8.8SDl I
Pegated: 2&Mer{7 lrutyred; i,9-{ar.07
PC8 r0r6
PCA 1260
Surogala: 4,4nU)cbt$!WW $t)Sul48eb'0€fldr/Iqd.'fy]tl(Sl
DLfl c.i! a?u}t?itt-c|JPlI
Prepa€d: 28-li4a,{7 A|sfFen: C}ti{ar{
PCB 1016
PC81221
FC81232
Pffi 12!B
PCB 1248
PCB 1254
rcB 12Sl
PCB 1262
rc8 1288
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l'ti-r Solt aruollm,tsl)
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PCA 1016
rcB 1260
suwate. l,l 4E ocwndiptwvt (stSutt.g?b: ,€fl/dtlot@Istft $4
Irtk 30fi. O! OtEtTiE||Sol I
F!paEd::eM€r{7 Analy!6d: ?O r|-{I/
PCA 1016
PCa 1260gnostut4,+l'lffifr,@(Si
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Birch 703 U39 . SW8.l6 3S45A
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606
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Thb Is&orolo.f Rport is not v6lilt nilttoat tn surrotl?att dgrrrtore oE the caver i?qe.. Repfitable Der€crioo Limit BRL = Below R€poding Limit Pa€e | 30 of | 54
Page 716
S€mivolatile Organic Compounds by GC - Quality Control
Analyre(s) Resulr Ftag Units *RDLSpjke
L€vel
RPI)
Limi t
Source %RtrCResult %RfC Limits RPD
Brrch 7031739 - SWE46 3545AElalt floll?i)&8LKt t
Pt€par€di 28-titu-07 A,arfledr 02-Atr{7
attin
.€tlc
b€ricd0frcg-BfE (undanrl
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4.4{DT{p,p')oioldrhEJd.6dhn I
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fi€pladrlor
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LCS ft8t t3+Esil I
Pripdrd 2&Mart Analfredr 02-Apr.07
Alddn
a€HC
b-8HC
d.BHC
g.Bllc {undara)4,4{DD {p,p)4.4{0E hpl4,4{DT (p,pl
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Prqa€d: 28.ai4sr{7 lrarf.€dr oz-Aprfl
Allln
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8RL
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3 1 7526
59.4
53.4
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54.6
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62.4
5 9 6
69.0
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33.4
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33.4
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33,1
33.4
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33.4
66.7
66.7
66.7
66.7
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56.7
6 6 7
66.7
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667
667
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66.7
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ISAS *€l
!g/tg wel
Ilg,tswer
llg,frgwt
pq,rg wer
lgtg w€t
yglq v'st
!g^q wet
lgxg w€r
ug,lq vr€l
p9t9 wel
z2a !SI(S u€l
ps4(s vJel
p0lq w€l
|lgfts,v€lpgksv€t
uolq Y€l
|Jg4(S u/et
W4(S rcl
lElS v€t
lgfrg wel
lErS wel
lJgfrS "elmAS rcl
!S4(S wet
pVlS v'Bl
USAg wel
lls^s wd
!S.tS wel
lSAq v.€l
Ilg/rs r€l
ffi,7
6./
g>150
34150
4G140.{0-140
1&110
rl{l-1,10
4G140
44-140
40.140
1+140
4+ro
4+r40
40.140
4+r40
4o.140
4o.140
&14n
4S1'11)
4G140
40141)
4+140
40.14{)
&1fl3&1fl
4t!14088 T
Thb laborqo,r rcpor. is not vald wirhoo an autho;zed signatte on the cover page-
' Reponable Detection Limit BRL = B€low R€parting Lihit Page l l l of 154
Page 717
S€mivolstlle Organic Compounds by cC - Quality Cortrol
AnalyteG) R€sult Flag Units .R-DLSpik€Level
RPDLimit
Source o/oREC
Result %REc Limits RPD
Batch 70J1739 - SW8463545A
tcs tuo ar(Btn+asol I
P@parod: 28.M.rfi tuallyz€d: m'Apr{7
a-BHC
b+fic
d€Hc
SS|C (Undan€)
4,4'.DDD(p,p)
4,4r0DE (p,p ) .{.DDl b,p'JIlddrin
Endosdta I
Endoeulhn ll
Endoeulbr Slllbb
Enddn
Endnn Aldef'yde
rlspbd'lor
Haphchlor E oxid€
a{hlordane
!q oturc
Endtu t(dns
Surogale: 1,1-DB-ehfluotfiiflEnt (50Swqate: Dacachtotdtpll€nl 6 t
E llc€te fiofl7le.DuPll
t'rEpercd: 28-li.ter{7 &alf.ed: O-Apr1)?
atddn
a{HC
b€Hc
d+tic
gAHC (l-intarF)
4JrDoD(p,Cl
4,4roDE {pp'),4,4r00T(p,p)
Ihdm
Endos'ibn I
Endo6'1hn ll
Eldo6ulhn $/hb
Endin
Endrin Alddld€
fl6phanbr
Maftox(t|kr
Hsdacflor Epoxnd€
sG odane
g4lk|ldane
Edin Kdone
Sl'/f'c4ata: 4,aAS&fl tMW l9rlSu|rogalr; Ibcad o,oah,rs'y' fst
Irrtir sol. mx}|flg{st.}
PEp€r€dz1- ar.07 Anryred: @-Apd}7
Atddn
a€tc
52.254.921.2
5e.456_9
55.363.159.051 356. t59.762.961.360.457.357.365.8u5
Sdrto: SA5l80+ro
BRL
BRL
BRL
BRL
ARL
SRL
BRL
SRL
BRL
BRL
BRL
ARL
BRI-
BRI
BRT-
8RL
BRL
SRL
BRL
ARL
BRL
BRL
9.163.5
ScJrc.: Sl59E0+16
flgtq rcl
ryrc|llZ-2a !$q |st
US,19 wlt
IryIS9,et
Ug*S wd
!9lg nsl
!S,/rS rd
lsrq tirl
pSn(S r€l
|4tq *61
lgrC wet
ilg4(cr{€t
|,grg r'd
|Jgro l's
!S,tg 'd
lElq€pgiqml
|otg wet
Ugto r'd
l,glsud
ars dttlcQdy
tlslq dv
ldlqdv
l'9r9dy
t'g*S try
udh dv!S^ g el
lS)tS dry
R01 m/lq dy
us'fu dy|4lqdryustg4y|lgrs rvAfs dv|lg}g dry
lCtS dryggts dy
usl€ dry
lglq dry
fs'lq drvpgtc fy
llc,tsd,|lgrs fiy
tlgtsdry
3.{31{33.433.433.433.4s.133.433.{l}.433.433433.433.433.433_4frt.4fr|.4*I4
66.7
66.7
€67
647
667
6.7
78
32
80
8E
85
84
a]95
68
n84
s0g.l
92
91
88
65
00g
56
30303l)3)m30
3l
30
30
30
30
3)
30
30
30
30
30
30
40'1{0{&14n
4&14114&1()+1q/uI1lU)
4+140(H40
40-14)
1&11{
4&140
40r40
4{}140
4&140
4GI40
4&!41)
4&110
40140
4Gr40
&1fl3$1fl
3
I
3260I
I
I
{I
0
6
0
2
2
2
1
34t
343
343
343
34.3
171
34.3
31t
343
343
34.3
34.3
34.3
34.3
34.3
34.3
343
343
t7l
34.?
34.3
3,t.3
Bfif,
BRI.
BRt
BRT
8RL
BFL
ML
8FL
8Ft-
8Rr
BBt
8nt
BRL
8RL
ML
BFT
BRT
BRf,
BFtr
BffL
8fl1
88t
30
30
30
30
30
3l
1)
30
t0
30
30
30
m3030fl)
1l
3l)
30
30
30
30
038.5H5
3GtflcItfr
49-7sti.035.0
BRT
EAL
85
71
69.9
s_9
Th:jJ bhtnrory repon it Eot volful l'dlto4 aI uthoized sigttaure on lhe coee, page_
'Repoftble Det€ction Limit BRL= Betow Repodng Limit Prge 132 of 154
Page 718
Semivolrtile Organlc Compounds by GC - Quality Cotrtrol
Spike Source %RgC RPDAnalyte(t Resul( FLag Units +RDt- Levet Resulr %REC Limits RpD Limit
ANlcfr 70Jlflt - Sw816 J5{5A
Irtk SotG O03l 7lI9{S | |
P|Epared: 28{ft r{7 Analyzed: @.fu r.0?
bgrcd+Hcg€HC (tinftna)
4,4 .ooD {p,p')
4,1'.DDE {p.o')
4,{ .DDT (p,p')
Dieklin
EndcdJlan I
Erdc6'/fan ll
Enddrlhn $lhts
Endn
EttukA,dehtd€
H€pladllq
lil€ltErycnbr
H69bdio. E oxile
eo{orddl€
g{t'lodan€
Endrin Kstsne
*rrogab: 4a-Oehbfllndifre (Sr)gnrqala : Dsf,zdlhtc/tpr.fxt'l 6t)
Idt Sdb qjo fntsl73g,llsDl)
ftiparcd: 28-trlar{7 Anat}"edr (2-Apr{7
A('in
a€tlC
b{fic
d{rc
s€tlc (lidarE)
4,4.0O0(p,p)
4,4'-InE 0p)4,1'-ODT (p,p1
0isHin
Efltoodhn I
Endodibn tl
E doerjbr Sdble
Enddn
Endin AHdryde
tl€pEd'ld
tilctFrldrior
H@d'kr Epoxide
a.Chlo{tb1€
$C ddrr€
Brdh lcbn€gn'rg#'l,ligeffiloabtpha (Stgjrmge Docadlb,Dbiorentl (S,
B.rch m31768 - Sw846 3sl{rc
fllrt lt6l?t!+Ll(l I
Piope,cd t Analyred 2gMarfl
Aldin
a.Bllc
tsgHc
Ed/rcr: SA5{qI}t6
54_4
21_3
5 3 5
56.1
56.3
6 8 9
545
58.4
34.4
267
56.5
62_O
57.7
60_3
57.5
56.6
4 5 1
13.6678
Sourcer SASgsFr6
!04(S dry
Pgls dry
lsAs dry
!4ks dry
irq4(g dry
lsns dry
wtg dryps'ts dry
ldrS d,y
lgtS dy
uly(g ory
Msevpsris dy
!9ts dry
lsnq dy
lg,rks drypglq drypqts drypvts drypSl(g dry
lgrs drypges drv
!s/ks dry
|]gISdrylgrs dry
!g,k dry
|ls^o &v
|ls/I(s dry
|lgrs dry
lyrg dryC[j,{7 lgtq dryu7 WAtl
|lgl(sdryorv!7 pg,ftg dry
ps/rs fivpgrs dry
Ugrg dryps4s dry
|jc4(s drvpsrl(g eypglq dvpgts fiv
30-150
30-r50
3Cr50
30,150
3GI50
3&150
3&150
3S150
30150
30t50
3G150
3F150
31I150
ml50
3GI50
3GI50
3S150
3G150
3+1fi3+t50
3{}t5l 2 30
3l-t3l I 30
3G150 4 30
3G150 6 30
30t31 0 30
3G150 5 t0
3G150 4 30
30t50 5 30
30150 6 m
slt50 6 30
3S150 14 30
3S150 5s 30
3!150 9 30
30.150 60 30
3qr50 1 30
30-150 19 30
3tlt50 5 30
3&150 7 50
30t50 2 50
30-150 41 50
fi-t@341fl
61.0
5 0 5
56.7
22.1
5 3 6
5 8 9
58.6
72.5
5 7 9
62_4
5 9 9
464
62_1
44.0
6 3 2
7 0 1
62.6
6 1 7
58.1
69.0
4 1 5N 4
35_0
35_0
35.0
3 5 0
3 5 0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
59_9
60.9
6 9 9
69.9
69.9
69.9
69.9
69.9
6S.9
69.S
69.9
69.9
69.9
69.9
69.9
m.9
69S
69969.9
69.9
69.9
69.9
699
69.9
69-9
699
69.9
69.9
699
699
69.9
699
699
69.9
599
59.9
699
699
693
69.9699
BRL
BHL
8fl1
8fl1
BffL
8RL
88L
BRL
aBt
aat
8AL
88r
BRL
BRL
BBL
BBL
SRL
BFI
78
30
80
99
84
55
3E
B I
w
89
83
06
82
€l
65
6297
BRI-
8FL
BRL
BflI-
8RL
BRL
BRL
8RL
BFL
BRL
BRL
8Br
BRL
BRL
BRT
BBL
BRT
BNL
BRL
BRT
35_0
350
35.0
350
35.0
350
35.0
35.0
35_0
350
x5.0
350
350
35-0
350
350
350
35.0
35.0
35.0
87
72
81
17
84
84
104
83
E9
86
B9
63
90
100
90
88
93
5999
BRLBRLBRL
001m0.010000100
t]d.u9t!crl
Thir ltbo.alo4 repo.l it nol vrlu withotd sE aathoized sigaalure oa the coeer FaEe' Reportable D€t€ction Limit BRL = Below R€porting Limit Page 13! of 154
Page 719
Semivolatile Organic Compounds by GC - Qur[ty CorFol
Spike Sourc€
Brtcb 7031?68 - SW84615l0C
t|mk mtsI76&Bt xrl
PlFarcd & Analyred: A.fiar{7
+8rc
q-BHC (Udan€)
Ctto.dan€
4,4500 (p,p ).1,4'-DDE(p,p')
4,4'.D0T(p,p')
Oiettin
Endosulfin I
Etthsuian ll
Endo$lhn Sulhb
Endin
Erdrh AH€hyd€
Heptadbr
Hepradtcr Epoxide
a-CliodarE
0{hlddansEnddr f,ebn
Stflogabi 4,4-0&&iaitso66Fn€ny' {S4Surrog€,b:Dec?dlorolbhar (St
lcs fn3r 76&8stl
P@9ar€d & Analadi 2+Mad7
Alddn
aftlc
tsBHC
dfatc
s€fic (Uodar€J
4,4LmDh,C)
4daDOE (9,p')
4,4!DDT (p,C)
Di4drn
Endoslhn ll
Enddilan Sdbh
Enddn
hdin Albntd€
HoPlacfla.
H€pbcr'|ol qodd€
a{t{odarc
g{hlord€n6
Endlh Xehn€
Sutog'dd, 4 i4,DB{fffi rot@Wt (54sifiggde: D6cachhtoryl€,]/ M
LtS Dlp t761tS€SDr)
PrEparbd & Ansly6dr2$ arfl
e.BHC
tsBHC
BRL
SRL
BRL
BRL
BRLgRL
BRL
BRL
8RrBRLBRLBRLBRLBRLBRLBRf6Rl-8RLBRLo0r090.0115
0.01320_01120.01240.00470.01200.0r250.01310.0124o.01?30-01280-01300.01050.01060.0123o.01420_01000_01360.01290 01340.0130o01310.0135
0.01400-01m0.0124
d-g|{c 0.m44 z.2a t4
Mlq4|jg,lpcl
u04
!s,!s.l!s,td!s.'lIlgIr,gt|4It4,,1l/g4lE,||/$'l!91t'sl'!dl!s,
|l$4
I9l
u04Z-2" till
!s,4t's4ttqlusl$4us4r44!o1M!9t!s{l|gll4/lm/r|Jgrlcl!s,tgl
{gl
uc/rlyr
0.01m0.01m0 05000.01m0.0100o0lql0.qpo0.0r000.0rm0J1m0.01m0J1000.0im0.01mo.fim0.05000.0rm0I]1000,0100
03100
0i1m
o0tq)
o0r00
0.01m
0.0100
0_0t00
0.0100
0.ma)[email protected] _01000.0tm
0.w0.0w
0.m10o@o)0 0e000.0200'02m0.m000 (P00
[email protected] .(Bm0.m000,02000.@mo(E000.@q)0.02000.(Em0.02mow0,Mn
0lalo
0.0e00
0.@
0.@00
fitil301fl
4Sr401+140i0.140
r(}140
{&14i)
l|()-14{
4{rr40
40t40
4tr140
4$1.41)
4{1"140
{st40
10-r40(}r€r|(!r€
il+rill)
,|{.1{0
rUll,{)
{1}t{1)
4&t{0
4+r4t)4t 14t)
4G1rO
t{l-lr{)
4Gt40
4&140
a5E
66
56
s224
60
62
62
62
64
65
54
62
71
50
68
64
0i1000.0100o0tm0.01m
m6062
6
7
0g
mmm20
Thls laborulory Eport ls @l rdid xirtod aa sathorid signzn E on th. coter pagc.
. R@orlEblc D€t€ctirn Linit BRL = Below R@orting Limit PNBe I 34 of I 54
Page 720
Semivolatile Organic Compounds by GC - Qualitv Control
Analyle(s) Result FtuC Unils *RDLSpike
Iavcl
Source
Resul l %REC
%REC
Limits RPDRPD
Limit
Brrch 7031?68 - SW846 351m
lcs nip fl0C1768{S011
Prepaftd & &Elyzod: ?9- arc7
g-BIIC {tjndai€)4,,1'.DDD [p.o)4,1'.DDE(p,C)
lt-DDJ lp,p)oi€rtin
EndNrf,an I
Endslrtan ll
Eados lan Suthle
Enddn
E{ddn Aldohy{e
H6@{or Epond€
ecl oiddr€
g€hhdan€
Endrin K€tul€g,iqgate. lfiebffindidw! (g)&nqdd Dsa onbiphe!ryl l&)
Brr.h 7031?69. SW846 3510c
Sb aGtTf+BtKt|
Psparsd A Anstlzsji 29-[rar{/
PC8t016
?cB 1221
PCA 1232
Pca1242
PCA 1248
PC8 t254
PCA 12m
ttB 1262
PCA 12mgfiqtu: 4+N-thn(Mobbhefit4 (Sr)Stnf{,ate: D&dtuttwwg (Sn
lcE fl{El ftg{Et)
P.€9er€d & Anelyr€di Anar{7
PCA t0t6
PCA t260
2,45&TC{t .Xyi€n€ (lS)
su/@ 4 4{Eeriuo(objd@ (9)sul@E Dgrad* otktlf,nt gt
LCS D|p ft6l769{S0ll
RspaEd & Andlyzsd: 2*Marfi
PCB 1016
PCB r2m
sr'r{'siE 1,{D9-o@,rL0robiphe,tt gtsuwqE:bttuta@Eort (st
0.01280.01400.013s0.01480 01390 0141o.o1470.01180 0 1 m0 0152D.01430 01200.0't450.01380 01470 01450.01280.0146
BRL
BRL
BRL
BRL
BRL
BRL
6RL
BRL
BRL
0 01300.02lJ0
o.227
i.264
0.0200
0.013{)0.92w
o.224
0.265
0.01300.u00
0.0tm
0.0100
0.0100
0.0'00
0.0020
0.0rq)
0.0tm
0.0100
0.0100
0.0r00
0.01[u
0.0r00
0.0100
0.0100
0.01m
0.0r4
0.02000.02000.0200o_uM0.0m00.02000.02000.02000.02000_02000.02000.02000.02000.02000.02000.02000.02000.0200
40r40
4G140
40,r10
40,10
4G140
40-140
4GI40
4$ t40
40-t40
1+140
40-J40
40r40
40r40
4S140
4+140
4Cr40
40-1404t-140
|.Er|anlslpsl
81t91!s4psl
us4t8ltcsrc/r$4ps4p94
!s4!s4,r94
64
70
70
70
70
59
63
76
72
60
72
69
14
72
u73
6
1 2
6
12
13
1 3
t 5
20
1
6
8
I O
I(]
2Q
202Q
mm20
20
?0
2A
20
n20
20
20
20
20
ts4t's,4us.4psn
!snI9,pgl
tsrps,l
u!/llsr
91
106
1 1 9
651U
$n$l
us,'ll4\!M
!srrcnNIwI
[email protected] {0.02000.02(Xl0 020{)0 0200
0.f200
0.0200
0.021{l
0.0200
0Mn0 w
025{)0.25010.0
ap000.02\m
0 2500.2500.0?{na02w
65t00
90
1md5t00
30-t50*t50
4G140
4o.140
50200
30-15038150
40-110,l{.14{
?0.150301Q
20
20
Thit labo?atory report is nol toltd x'itho.d an aihorize.l sigtt4ture on the coycr page-
r Reportable D€l€ction Lirnit BRL: Below Reponing Limir Page 135 of 154
Page 721
Semivolatile Organic Compounds by GCMS - Qudity Cooarol
Bstch ?031680 - Sw846 35t0C
Bhnt f/(Bl68G8LKl I
Pr€par€d: z8-lrar0T Analyzedi 29Mad7
1. €$yinapnUralen€
A:ob€n eneDih$ykii€dno
Bsuidiie
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Senzo (a) anr||!c€n€
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8glm (a) pyr€m
SdrF {b) nuorafiel|€
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Bffzo (q,i,i) psyl€ns
B€nzo E) fuoaarUteft
B€l@ll)fi|.o he{te
Eenzoh acid
B€n:yl alohol
Eised{o@tbr' nrsdl{llle
8is(2-ctloro€hyI)€het
BE{2{hhntsoproMstlt
Eisl24bylhoxyhhhahr€
a&orEpher'/ p@ etFr
eJ|yl benzyl phtlslalo
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4-ClldD.3.rn€$ylglEnol
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r 000.0500 0500.4001.000.05i)1.m1.00
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|g'l
wluc4tJg,ugltts4
I Lk ,abontory repod is not vabd x,irttu! aa ourtoitd tlgnaura oa {e coter pag..
I Reportable Detection Limit BRL = Below Reponing Limit Page 136of 154
Page 722
Serniyol{tile Orgaric Cornpounds by GCMS - Quatity Controt
Anslyt€G) Result l'lag Units *RDLSourcc %REC
Result %RF-C Limirs
Spike
Level
RPDLimnRPI)
Batch 7ol1680 - SwS46 3510C
Bla|* ftll?168[8tl(l I
P.BparEd: 28{.kr{7 Anatyzed: 29Mar 0?
2,+Dhr@hefid
4+Di 'ro|()lune
2,&Dln{robluste
D4l.ody' phdbiaie
He&d{orobuhdi6ne
&ndf orocyclop€fl Edi€n€
lftl€no (1 2,&cd) pyrene
Indeno (1 ,elcd) pyrene
2. et'tjnaptlbalene
z{,lehylnapt$arene
2-tloWplrend
3,4-ll€ort&h*lol
l@ntabne
l@h$alene
2-Niroeiine
3.Nilroa ine
+Nitoenlin€
4-Nilrophenol
f !.Mtosodinslhylamine
ftNitt€odnntopy'anine
I\&Nifosodiphenytamine
Pyidna
IZ4-Td:t orcherlz€no
2,,1,s-rdnblopn€rbl
2,4,BTrulooohslol
Hexad onburadl€ne
SunrBa/'.24uotudwlgnqde:2.hJ3nbiplgnyl
Eurpg'/e: 2 FltJotophp,r/&.nog6taffl'oben 6rb.d5turq'b] ms0d45glrogda: leg&laaSu/og,it: ledwl.dlgtroge: 21,6-Ttbtd4taol
ARL
ARL
BRL
BRL
BRL
BRL
ARL
BRL
BRI.
BRL
BRL
BRL
BRL
BRL
ERL
BRL
BRL
BRL
8RL
ARL
BRL
BRL
BRL
BRL
BRL
ARL
BRL
8RL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ARL
ARL
ARL
ARL
SRL
BRL
BRL
BRL
433d3Ja2
78.192.492.465.?
!0r!dl
!sntglrgl!c4!snusn!s/!dl!sn!s,4!s,4!94!s,4!qlflsn!Mus.4
!snrrg/|
PEuglWllctl!s4!snpst
!s,4usnNN
H,4
tel
!s,us,4Nt!94
ldl
!91
|Jsn
vups,lps4p91!s,lPCr!!c!tjs'l|lg4
us4tdl
1.00
1.00
1 0 0
1.@
1.m
0 050
0.050
1 0 0
1.00
0.500
1.00
1.00
0.050
0200
1.40
1.00
0.050
1.00
10.0
1.m
0.050
Lm
1.00
1.mI 0 0
1.00
L00
1.00
1.m1.00
1.00
1.00
0.050
1.00
1.00
0.u60
1.00
r_001.0)t m
1_m1.@
1.00
0.500
tw1N
tfrtffi1@tm1N1ffi
83
a96n9292
3t>1N&1U15-1103A-130111103+1iA3G1Ulg1t0
Thb laho.alory rcpot is not told pUhou ad authori<ed signrrwe on the cover psge .
r Reportable Det€ction Limit BRL = Below Reporting Limit Page 137 of 154
Page 723
Semivolstile Organic Compounds by GCMS - Quality Cotrtrol
AnaLyt4s) UnitsResuft Flug .RDLSpikeL€v€l
%RECLimits RPD
RPD
LirDit
Source
Result %REC
Datch 7031680 - SW846 3510C
LCS A031dn}8s|l
PeparBd: 28-lrs.07 Anaryzed: 29-lrar-07
1-l,lehy'nadrtur€ne
Anllln6
lzoba'z€dDiptr€i\trdia.in€
Eendjin€
Senlo (d afirffile
Senzo (a) an$lac€n€
B€nzo (a) pyr*F
BenD {a) pyr€o€
8€r'zo (b) fr./o€ntsns
Eenzo (Dl lEant'€ns
8€trzo (q,hj) pdltene
Bsnm (ghj) pslien€
Bei.o (k) tuo€nheie
0€nzo (k| nuo€nbl€ne
Eenzoic acid
8€nzyl dcolu
&s(2+lidEsnDry)rlethane
Bii{z{ o{E$y')€trer
Biq2d{.tttisopopt)sth€r
tliX2€hyf lsxri)rf 'f 'alab
4-&onEpi$yl phen}1 etr€/
8utyl ben4l FmdabCarbezol€
a{ orF3{nefiyldlenol
4-ChldwdliE
2-ChlororBFffiat€n€
2.Chlora€h€|d
1-Chhrc9i6nyl phsnyl 6her
Ciry$n€
Chrysene
tttdlzo {a,il an$rac€n€
Dbefto (ah) snlvactn€
Dibenzottfdn
1 ,!Olt{c'!Hra€
I,+Oi$lo.obsEene
1 ,6Did orobduone
3,3 Oiddfloh€nzthe
2,4Dld1ldldBlol
OhhrylSr$e
ometryl phfuab
2,+Dinshylph€ml
tl'ntulyl fidElalo4,6Dinire2{ehly'pn€ftd
77.6
77_6
E5.1
85.1
76.5
103
86.2
E6l
174
94.2
104
80_4
80.4
a7_2
a7.2
83.8
E3.8
65.2
8 5 2
7 9 0
7S.0
77.O
76.8
85.5
92.0
61.4
91.2
77.4
90. I
1r2
83_7
8 6 1
79.7
69.4
76.A
86.6
66.6
90.0
90.0
a1.2
75.5
67_0
75.6
.2
75.2
84.0
E4_4
73.1
74.O
!94pg,l
|84p9l
|lMpdl
!s,|B4
1Jc4
ugl
lcl
rgl'rjstTETpgt
lsl!E]!E
wlt4,llalrgs4
!s,la4t44usrru/]rjEl
MMt44usrlrg4!c/l!s,ttgllq4l,clps/rldrMl&tl
t8,lpgl
uslt4l'Mtdl144
ugltl44
1.000.0500.4000 050r.000.05t)1.00100
o0501.00
1.m1.00035002m0-2m0.0500.0500200t mo0r0 05{)0.300L00Lmtsr_001.001.m1.00100r.m1_m1.00
L00
1.mI llo0.050t.m0 0500?001.001_001,001.mi001.m1.m1.mLm
1.m100
1 m100100r00lo0I F
100
1rI)
100
tm1m1m1(r0
100
t00
100
rml0o
100
!00
100
1 m
rfi)
100
lmt00l0{l
tmrtD1fI)100100100tmr001001001m1ql
r00100t00100r00tql
1m100
1m100tmlm
78 111-t10
78 4Gt4t)
E5 {}141)
E5 4$110
m 1ut-118
76 10.110
lm 4Gr40
86 411141)
66 4+140
174 G2m
91 {0.140
r04 40t40
m 40140
80 10.140
87 ,gl1rl0
E? {0-1{t)
B1 40110
84 4lIrO
85 4+r,{)
85 rl+141)
19 1Sl{n
79 €t10
77 30130
n 4+110
E6 4G140
92 (}1{
6t 4Gr4t)
91 {+140
77 48110
90 :l&140
112 ,91140
81 30-13)
EO 1&1,10
m 40.140
6{t 3}r3)
77 &-1{d
E7 (1140
E7 10-t&
9o 4014{'g0 4st40
81 4+140
76 4+1q
67 1&110
76 10-110
s4 4Gt41)
75 l}l3l)
84 4t114{l
84 {l}140
73 3Gr30
63 4S140
74 3$r3o
This labralory rqod k not ralU irllhott al au&.ofiaed signrntE on thz ctw. page.
t Reportable Detection Limi! BRI- = Below Reportine Limir Pagc l3E of 154
Page 724
Semivolatile Organic Compounds by GCMS - Quality Cotrtrol
An8lyt€(s) Resuli F lag
Sourc.e o/;REC
Result %REC LimitsIRDLUnitsSpik€[,evel
RPI]
LnnitRPD
Batch ?0ll6A0 - SW846 3510C
les fl031681]ost IPr€pated: 28{ilar{7 lnalyzed: 29lVaF072,1-Difi'toph€flol
2,+oinitotoluene
2,Sohitotoluone
Di-n{dyl phr'€ble
H€xacnboctdop€nhdienB
Indsno ( 12,3{d) p}r€ns
lndst'o (123.rd) Mene
z-tlebylmphllalene
2-lil€d\inarfii'aren€
2.Llstry{phend
3,4lrefrybienol
l'laplfial€n€
adrtElene
2+ItDanilitE
Sllt€dline
+ilroanithe
2-l,JitrEdlglol
a-Mrogt€noJ
N{.litosodimeliylanoe
l}lffiosodintropYanlne
r[l|iro&ditl€nylamin€
Fflitr'ne
lbxacl o@benzene
l24.ftichloobeo?erl€
2,4,$IriJtoro{ha|ol
2.4,STdt{orodEnd
Hexaciloobutid€rEgnrogd4: 2+tfiotiplpnylg,nqaE2+wt.t4,,W
s/dr'oga&] z+tro@Ialr/S{''{{l'{f.: ltlt/.1(ff/t2dtx,45Suro4€te:Pffi6g]/7os'iF.:TadBMaagl/'i4eh:Tetfi€vaa
st'ttc@:2,a,eT@rpnol
8 9 5
95.2
92.5
94.9
80.2
80.2
79.9
79.9
75.1
74_5
66.2
63.3
u.784.7
9 0 3
8 2 0
8 2 0
71.7
7 9 2
7 8 9
7 8 9
87_3
86.4
102
95.1
77.6
59_6
al.2
42.7
91.5
73.3
76.8
7 6 8
67.9
75_3
75.3
81 '1
75 '1
63.3
79.8
72.6
73.3
63.0
74.5
m 674.3tu71.64.14.1n.9
v94
!94
UE|lgn!s4lsn!s4usnus4pg4
!s4p94
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vt/]'!dltsrr!grME4trs4!E9SrlsnPE!s4!c4!s/]!04!91w]TSI!sr!91ugl
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1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
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0 050
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1.m
Lm1.00
1_00
1.00
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100
100
100
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100
100
100
100
100
100
100
100
100
100
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1m1Ul
100
100
100
100
100
t0l
100
100
100
t00
100
100
100
l m
l m
100
1m
to0
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100
t00
100
1 m
100
100
1U1&1N1N1N1N1001N
90
95
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80
60
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63
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30,13040t404{"1411rl{.140
4G14{
4Iliro
1111411
4G1411
4{f140
4&140,(F140
4tr1it{l
r(}1rll)
rlGI40
{f140,|G1,1{l
4(}140
411,140
1Gi30
,lGl40
rt+t40
4G140
10l,li)
4&t40
4G140
3$130
3+130
40.140
rr0l40
4i}140
3&130
4+140
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4+r40
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40.140
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4{t140
1&110
3G130
3G1:0
3G130
4Gl4{l
fr-t&30-130tr l l0#ti015-110*130*13011110
This lahontory rcpon k ,ot wlu x,ithod M aa{.odzed tigarurc on the cover page -
* Reportable Detecdon Limit BRL = Below Reporting Limir Pase ll9 of 154
Page 725
Semiyolatile Orgrnlc Compoutrds by GCMS - Quality Cortrol
Analyte{t ResuhSpike
t€vel
Source
ResultUnitsFlag %REC Limits
B.rc! 703t774 - SW846 35508
ah oanT4€LKll
Preg€redr 29-lrar-07 Anatfu€d 02-lpr{7
Al.n€u€ft ,oihs{tyHiarng
8€nzllne
S€nm (a) antlacone
8€nro (4 prem
8€izo (b) ftDlentlefle
B€nlo {o,h,i} pdylsr€
B€nzo (r) fluolanh€r€
8€nmic ard
8snzy' ahohol
&s(2{hlol€nlory)m€ftm
Ers{zrl o!4ldr€t
Brl2rht dsoFwl)€ts
Bis{2{hyt'edFmrahte
+BMEpienyl plrsrrl e0€r
Butyl !€n4l d'r'aksC€ftazol€
&CfilorF}IIEtryblEnat
l{1 oroanilin€
z4lorcmC El€ns
2-oioropherEl
4{Horophenyl ptt€frt ef'er
Chrys€ne
Eb€nu o (Ah) antrdr€ne
Dibenzoiran
1 2.Di{ttomb€nzen€
1 ,loir{orob€nzerEl,4oichlorcbenzsrE
3,3 -Did ctrob€rliinn€
2,+D{rn|o.aphenol
Dery d'haH€Dimefiyt ptt'alab
2,+Dimsd'tdErd
tx-n-butyt pnhabb
I,S0hr62{rcfiyhh€nd
2,4lhi[ophrtol
Z+Oirlrottuen6
4StJirilrolot$e
D-r'.odyl ptddab
liored orohiEdkn
ri6|(adblDcrdoponhd€r€
lrd€no (1,2,9d)prone
I dlstryinapt$€hi'e
BRL
ARL
BRI
BRL
BRL
8RL
BRL
BRL
SRL
BRL
BRL
BRL
BRL
BRL
SRL
BRL
BRL
BRI
BRL
SRL
BRL
BRL
ARL
BRLgRf
BRI.
ARL
8RL
BRL
ARL
BRL
BRL
aRtBRL
8Rf
BRL
ARL
SRL
ERL
8RL
8RL
SRLgRL
BRL
ARL
SRL
BRL
BRL
BRL
8Rt-
BRL
|,drg rv€l
lqrg ',v€l
Igr! rd
lglis ]rEt
lErg '|0l
|J!,rS wst
mliC vrgl
UoAS nsl
|lgtg I'sl
|jgrs wd
!Sr(9 wd
lgrg *l
HllqtrT
|4|lqwsl
UCA! r*l
|lgkgY€I
|lErgwd
tlsts wd
!9brcr
l4|t8r€t
l8,lq\$t
|lgkgwel
|lg}S $,€t
|4/lg rrd
!s,4q 'd
|js/rgwl
lSIq I€!
pSnq rct
|9 q vrel
|jgr'|(S s'sl
uErsffil
l8fts,€l
|lgltg $/sl
US*S ftl
Ug/tq $el
tlgtSwel
llgllqwel
|ld?.9lv€l
|lgkS v/et
|]grg v,El
l]grsl'd
|js/rS Td
|afrSmt
Igrq $et
|ldtgwet
|lg,tS s€l
ug]kS tJ€l
ryrs t{€l$Er! llel
|jg,'|(S f,31
|,dhlrei
330
330
3c0
330
3:]0
330
330
3t0
330
330
$0
3]0
33O
3g)
310
330
340
330
330
331)
33{)g[
cto3303303303:)033t)3m33{33030330330sto3303m3(t0330
3303303i!03it033033{)30330330330330
This labarolary .eport is ^ot rolld flitho$ zd a4ahoiud slgrata.e or, the cover pag
' Reportable D€t ctioo Limir BRL = Below ReportinC Linir Pagc I,{}of 154
Page 726
Semivolatile Organic Compounds by GCMS - euality Control
Spike
Level
%RECLimits
RPDLimrt
Source
Result %RECAnallte(s)
Brtch 7031774 , SW846 35508
Bhnr fl€l?+At(l1
Preparcdi 29.fi erfl aEI.!€d: 02-Ap.-07
2.rlshF€phhalone
z. 6trlphen0l
3,4- on4{Fend
tlapfitteg€
2-l{uoal tino
9Nnr!€niln€
4-ruto8nili||e
t{tDbsEErE
2.t{i@l€{rol
+Nitldr€r'ol
ll.l{ibDrrdi'rrdl}lanirE
li-Ntt6.di.nf .opyl€min€
l'l-l'rltEs.dplE|tamin6
PttilitE
I 2,1-Tn:t orobe||,ene
2,4,tTri*'lordrsnd
2,4,&Tdilo@End
S$qtte: 2'flndifaqASrnryE:anffc{,h1rtr,ls/n/ogate l:$tMt2etE45
griogats; feryhql4aS6roge/f.: 2lEltbwnoptPJnol
tcs oBt z+asrl
PreFEd: 2+Md{7 Arulyz€d: 02-Atr-07
ANINE
Afa2fE
Azob€nzedlXph€nyldiazine
B€nzidfls
B€nzD (4 anfFrc€n€
&rEo (4 pfD te
B€nro (b) lud-antEne
B€nm (g,h,i) psyl€ne
Berllo (l) [t o,rlbsrE
BsnDk std
8€Iuyl ebohd
Sq2dforccfroxylm€$ans
8q2d$roiryl)€$er
Sq2dbotrproprtl€fl€r
Sb{2€t}4@)pl'lhatalo
4&DllEdl€ny' ph€nyi otEr
I'Jtl bsnzyl drtahl€Cartazde
BRL
BRL
BRL
BRL
ARL
ARL
ARL
ARL
BRL
BRL
BRL
BRL
BRL
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BRL
BRL
BRL
BRL
BRL
ARL
BRL
ARL
56405t@65fr
6An
4850
5170
4990
5430
7910
6030
BRL
5000
5500
4720
4840
6380
5620
4780
5340
6000
3600
6170
4680
5940
7030
lj0ks wel
!gl(g flel
!9,4(s wel
llg4(Sl{et
!91(g wet
llgn(qwet
|4,l(9 wel
ugtg w€l
l$tg !$l
trll(g w€ty9k9 rrcl
ruL&o nre,
pg/rs v.el
p0/ksv€l
lyrg wet
|'s(s wel
p!,{(s v€l
tig/*S Y'st
!g'rg wel
!S*g wet
lg.rks mt
p$^g wet
|lg,r(swetil{r4(SwstN/kg nettrgkg welp$4q wer
Pgts w€t
tig/kQ wel
PS*S r €l
Ug/Kg rl€l
Pgnq Yrsl
!g&g s€l
pgr(g $€l
!q^s l^€1
tigr(S r€1
ug4q vr€l
P!,lq w€]
P94q r€1
l]9[0 r'€l
ISAS !,€l
Ig4q rcr
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PSIq wel
l|g,kS we1
IS40 w€l
IS4q !rel
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alo
111)
30
330
330
330
330
1320
330
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330
300
330
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330
330
330
330
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330
330
330
330
330
lB0
330
$0
tr|0
330
x30330330$0frto331)3303303m3:10331
6m6n
66,746m6ft
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6670
6i70
6670
6670
6670
6€70
6670
6670
6670
66m
6670
85
98
9962
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78
75
81
1 1 9
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75g2
7t
96
E4
80
90
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9l
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89
106
3U1301rt103013015 t t03+tfrt r t t0
4Gr30
10-130
4+130
4& 130
€-130
10.130
Gt30
40-t30
4G130
4S130
40r30
4&130
cr30
4+r30
4&r30
4&130
4&130
4+130
4Gr30
40130
4&130
RPD
This labontory rcpoft is not t)olid tellhout aa outhori&d s@narare on tha aecr page
' Reporkble Detection Limit BRL = Belo* Reporting Limit Pase lal of 154
Page 727
Semivolatile Organic Compounds by GCMS - Quality Cotrtrol
Analyt€(s, Resull Flas Units *RDLSourc€ %REC
Result o/oREC Limirs
SpikeLevel
RPDLimitRPD
Barct 7031774 - SW846 35508
tcs iro!1744so
PreFarEd: :€.lra {7 Analr2€{: 02-AF-07
4.Chlom+m€$rylphad
a{|lbDanili|E
?{tloDriaphtu|€ne
2-Cnhopfiffd
4o{croplEfiyl dEnyl €ter
Cnrysene
ttb€nzo {a,hJ anfinc€n€
Dib€nzdu"n
1 ,2-Didcrob$zen€1 ,SDiilorobsrz€n€
l.4Dicnbrcbffzsng
3,3,.olrlffobonzidire
2,+Did oopiend
oiotryl Tlitle|oleDii'eftryj pltHare
2,4{iret4#l€nol
D.rlbutyl C'ttalats
4,ADrrdro-2{€hylph€rEl
2,+DitFopn€rDl
2,+0initoltus€
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. R€portable Detecriofl Limit BRL = Below Reirortinc Limit P{ge 142 of 154
Page 728
Semivolatile Organic Compounds by GCMS - euality Control
Soike Sourc€ %RrC RPDAnalyte(s) Resulr Flag Units *RIIL Level Resutt %REC t_imits RpD I_irnir
Barch 703 U74 - SW846 35508
LCS mfi7l+BSll
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Sutt'g8e: leri6nt44Su/ogag : 2,46I tltuornqhald
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ee(?-clloroehory)n€tlane
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59
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285
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285
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285
285
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881
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* Reportable Dekation Limit BRL = Belov,. Reporting Lirdit Page l4 l of 154
Page 729
Semivolatlle Organic Compounds by GCMS - Quelity Cotrarol
A$alyids) Result Flag Unit5 Result '/oREC Limirs RPD
Brtch 703 1?74 - Swt46 35tlB
olllh3le filFlr'4-lXlPll
Prepsr€d 29{ilar{7 lr|a|}r4d: m-}pr{7
Di{{ctyl pht'dah
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ll€Ischlofmtdopenbdiens
lndeno {1,2,}{d) pyene
l -Mot'tlnaphfialeno
2-fi€hylnaphtlal6n6
2.Ilsdrybiend
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ilaoht\rkrs
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4-Nrophenol
N+litorodnn€0tlamiF
f &Mro€di{rFopyiariin€
N- iEosodiphenylamine
I Z{-Tdchlorobenuene
2,rsTdcllomph€rEl
2,4,STidb.ofi€nol
Sunryt,2-FatfienytSrr'/I.oga/.a:z€/btopll€tlf,lSurgga@:Nittuvefted6Slnogab: Phstd$swqattIdit ttl44Sufi Wan : 2,1,e ldbtonophefl I
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9RL
91.0
BRL
BRL
BRL
BRL
BRL
47 -3
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BRL
BRL
ARL
SFL
8RL
BRL
BRL
BRL
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BRL
BRL
BRL
BRL
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130
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. Reportable D€tectioo Umit BRL = B€bw RepGting Limit Page l,{4 of | 54
Page 730
Semivolati le Organic Compounds by GCMS - Quatity Control
SoLrrce
Brfth 7m1fl4 - SW846 35508
tt'th Soll(g f|tslz4{Si) So{rE€r Srf,5gt8,i{ePr€pared 2$Mar1)7 &at!€d: 03-Afl{7
Sr/rogEbi{bD6srzeE{5 S14O&r?o!ebi Pl€dJS 37&Swrr8tu: re$anyl44 SA0gnftgakjl4iniesnophend fi&
fllt|t SE{{. 0rr t'l(Bl7|+l|S0t) Sotirc€: 5A59785.02P€p&€{ 2$li4ar.{7 lnelyzod: m-Apr{7
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* Reportable Detection Limir BRL = Below Reponing Limil Page 145 of 154
Page 731
Total Metals by EPA 6000/70fi1 Series Metbods - Quality Cotrtrol
Analytqt Resul. Flug UnitsSpikeLevcl RPD
RPDLimiilRDL
Soulc€ %REC
Result %REC Limits
Batch 7031810 - OPA20{ySW7000 S€ri.s
Bldrk l?tl3181GBL(Il
Pr€pared: 02.Apr47 AnalFsd: BAp|{)7
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PrEp€r€d: (B-Apr-o7 Analyz€d: 0l rr{7
Batch 7031823 - SW846 3105A
thr 4ru018?3€t(1 I
Pt par€d: 30fftr-07 tualyzed: m-Apr{?
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. t(Eporrrble Deledion Limit BRL = Below RepoftinB Limit PagE 146 of | !,4
Page 732
Total Metals by EPA 6000/7000 Series Methods - eualitv Cooarol
Ana\te(s) Result FlagSourc€ %REC
Result %REC t,imits+RDLUnitsSpike RPD
l,inritRPt)
Brich 7031823 - SW846 3m5A
thllhde fflFlE2!0UP1l
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Pt€pdEd: 3GMar-07 Analyzedr m.Apr 07
lE€d
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ARL
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BRL
So|rtt.: S459652{t
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rngl
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0.500
0.500
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0.500
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0.500
0.500
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BB!
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0.0198
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95
94
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100
108
95
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101
112
99
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93
94
98
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0.559
0.496
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75-125
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75-125 0 E 20
7U125 1 m
7ts125 l0 20
15-125 1 m
75125 4 n
75-125 2 20
7t125 | 20
6q120
* t m
8G120
80120
E0-r20
mrm8GI20
0.466
0 468
0 509
0.495
0.498
0.492
0 468
rnEl
RSn
n1ll
risl
ru/lmq4
m94
Thk labrctory npon is not uolid tr'i*rou a authodzed signalurc oa tha coeer pzge
* Reportable Detectioo Limit BRL = Below Reporting Ljmit Page 147 of 154
Page 733
Totrl Met{ls by EPA 200 Scries Methods - Quallty Control
Ar'alyt(t Result Flag UniG Result %REC Limits RPD
Bstch 7O3t809 - OqA 200 Scries
Bbnk mEl00lS1Kll
P€t€red E Aralyredi lp.Apr'07
Silwr
Sd€dwn
Clxomtum
CadfiiLrn
Aanum
Duoficlb (7lB18llo-OuPll
Pregacd & Aiatzed lP-Ap.{7
Siitv€r
Sel€niun
C{dn'rrn
Chrc[nun
Barinn
lldtL Sdt fr!31809{Glt
Pr€ps€d A Andrzed: e-&r-07
Selenin
tiilr€t
ftrc|nim
cadftiun
Badum
||Etlr S!*c f?|)tl ns2t
PrEFared t Analyzed: {B-Apr-07
SiL€r
S€l€nrum
Clroniufi
Cadnarn
Bari!fl
Pd so*6 flBt|0o-psl)
Plepaled A Adyrsd: @-a$r{?
Sd€nium
sihl"r
L€iTd
Cdnhln
83rium
Rgt|!.|oe fl0318096i81i!
Pt€pat€d & Aftlfled; (2.Apr1)7
S€l€dum
SilvEr
Chontum
L6ad
SRL2.9048_510.8
0.88022692.3
So|jrl!: SA5SE{E{
146
145
145
135
140
t62
147
Sourc€: SlLtglSqX
143
143
144
138.lB6
135
210
S.{ft.. SA598l)3rm
SRL
sRlSRL
BRL
BRL
ARL
ARL
SoUm.: SA5S{I
|TB'l(! {g 0975
|rg4€'d 1.46
trEltg*d 0.7j1
flVlq mt 0jB7
mS/lq *€t 0244
nS,ftS lv€l r-1(;
[E/rg Bt 0.487
nErsd) 2t7
.nEhd' 3.11
mdtsdf r.55
@lq dy 3.11
mdlgdry 0.518
ngrlqdry 1.04
nEro dy 1.04
'idlqdfy 1.69
rndrSdry 1.13
mg^gdy 0.563
rnEhdy 0282
ftg/fg dty 1.68
nry*S dry 0-E 15
rgrqdry 0.563
mgtqdy 1.10
rndkgdrY 164
rrB4{ dry 0-54€
rrytg dry 02f4
fiSlqdry 0.822
mgllqdry 1.64
mE?,! Ot 0148
ndhdry 1.n
idlqdry 1.15
rnfiqdry 0.859
rylq dy tn
mdk! dry 02E6
ng^S dry 0573
nvtgdly 0.573
rn$Ag wot
mgJtg n6t
n'g/q wsl
'ngrg Id
mt32357.1
r04qSrs
2.5
91_5
1.35
8FL
10.1
0.417
4_86
28.3
47.0
8A[
Ll1
123
0.61t
4.3.5
5.06
8 1 1
1.35
8Fl_
n.x436
o4t7
l o l
,t7.0
l t
l 7
4
1
0.4
0t
35
3535353535
152't34
'157
145
r39
rrtS
189
88.0
46.4
44.5
44.5
t4!
1 4 1
1 4 1
141
l,l1
t41
141
137
131
L n
1n
131
137
137
t€
t €
143
1 €
143
t4il
143
7t.r
{1.1
a9_4
4rll
104
lrxl
96
lm86
95
{X
r05
94
90
98
97
s€9!l
1t0
1.00
0.500
0.750
7St3)
7Gl3)
7G130
7$rx)7Dr307&13070.13[
7il1307Sr3070t307F1307F131)7Grfln}r30
8$t158+t1585-1158+r 15&;11585t l58F115
n.+lzi66.!t33-678.$1m.5E].&118.r
103i6
96
s596
95
9!l
fl3
113
98
s
Thb leboratoq fepod b not valLl tt'ilhout a, rr/.horhed sigaatare ol the Eover page.
* Reportrble DetectioD Limit BRI = Below Reponing Limit Page 148 of 154
Page 734
Total Metals by EPA 200 Series Methods - Qualitv Control
Analyt€(s) Resuh Flag UnitsSpike Source
Level RcsultIRDL %REC%RICLimits
RPD
LimitRPD
Bracft 7031809 - EPA 200 Series
Ber.rrrce ttBl80g+Blt)
Prepflld & Ar€rf2edr (E{pr47
Cadniun
Saium
&acli 703182.1 - f,PAl00/S$'7O00 Sede!
Bldrl ftlElla4€Lxt I
Rep6red: 30+ra{7 &'alEed: m,ApFo7
LCS fr61@+Sltl
t"€FEd: I{rar tualyzsd: m,Apr-07
olllc.ts ao€fia€uPl I
PlrF 6A 30-r/|3r{7 tuatyz€d: 0e-Apr,07
Ltrh s{h fimst8z4{st)
R€pdEd 30{r€r{7 AnalF€d: Cr2-Aprfl
Llr SoL Olj! a7|Bl02+{SOt l
Prefercd: Sl ar{7 l.mt ed: 02-Apr.07
P.d 9d|{e flBrg2cPsil
45.833_6235
rngilg wel
mgAg lrel
rngl(g wel
1 m
0.2500.500
80.8-119.482.1n17.982.7t17.3
443
31.E
215
rg2
r06
109
8RL mg/ 0.00020
mg/l 0 00020
mg,4
0.0fr20
mg4
0.m020
0.0 0 8RL
0.00250
S@dr 545980!18
0.00005
S.rilt : SA$a!}tg
o w249
So{rcs: SA508O}19
0 00260
Sourc€: SA59t&19
208Rr
8nLn'g/
75-125 20
Preps€d:3G lr{7lnalyred: o2-Apr{7
€(.1ry 0 00226 05-t 158ff1ngn
Thit laboralory report is ,tot ealid Hithou r taahoriNcd signaturc o^ the coter page.
* Reportable Det€ction Limit BRL = Below Reporting Limit Pag€ 149 of 154
Page 735
SPLP Metals by EPA l3f2 & 6000t000 Seri€s Methods - Qrality CoDtrol
Analylqs, Result UniLs .RDLSpike
Level
%RECLimits
RPD
LimiaFlag
SourceResult %REC RPD
Betch 703lEt)5 - sw6{6 30t0A
ahnl ar(BlqE€u(1)
Prepa@di 3&ller{7 Analyredr m.Apd7
Lead
Sel€niun
Sd$er
Cirorhirn
C€dniun
Ealiltn
rcs fmr!6.4s1.)
Prepared: 3&Mar.07 AEtyz€d: (z.Aprfi
SelBniun
Sllvor
Cadnim
dllonium
Eariun
LCS Ap i7ml8{F8g)l)
Popar€d: gl-lrr{7 edyzed: m-Apr{7
S€lenhJm
Loird
Ciromium
Srh€r
kniun
Badum
u/oti.{. {7(Btg}stxP
Prepared: 30lrar.{7 lr|3 zed: @.Apr.07
Le.ad
Sddiun
SikE
Cdflkrn
Ctronium
8aiu,n
Lrtr Sd. mglftr&Isl)
PrepatEc 3Gl&r{7 An€lyr€d: 02.Ap..07
Sel€nitm
Clvomum
Cadfiim
Sivrt
Bfifun
Lrdr Stff(. ouo tl6lEt6-||SIX)
Ple96r€dr 3Ot ir.{7 lrlarfze": @-AF{?
S€lenlra
L€ad
Chrunitn
Snver
BRL
BRL
BRL
BRL
BRL
BRL
aRt
1 - 1 5
1 . t 8
t . 1 6
0.390
1 . 2 3
1 . 1 4
1 . 1 8
1 . 1 1
1 _ 1 3
1 _ 1 8
1 , 1 9
r . 1 2
| . 1 6
1_19
SdrEe SAltggF{l
flry|ms/|ndlms4rfidl'rgltng'l
aEn
ru4mdl
ac3 ft911
nEl
msnms4
mdl
ntorl
ms4
ORs npl
ndl
n'94
mdl
lrEl
'rql
mdl
'ndl
r'91
n0rns4
'IRil
,ng/r
mdl
rldl
iE4
OMo fitel
mgr
0.0075
0.0r50
0orm
0 0150
0.0125
0.0@5
0.0060
q0150
om75
0.0r50
0,01m
0.0025
0.0r25
0.0050
0.0r50
0.0075
0.0125
0.0100
0-0r50
00@5
0.060
0.@75
ofi$
0.01m
0.0025
0.0125
0.0150
0.dEtl
0.0075
0-0150
0.0150
0i125
0.m5
0nlfi
0.0050
0,0150
om75
0.0125
0.0100
'71.4.16
68.a113
m.2-t01
5 t + t 2 0
81.1-107
81.7t(b
85_r I 19
7,{.+1m68.6113
El.7'1{E
5tt{20
80.2.r01
8l_1, t07
E5.t - ' l9
r25
IA
125
125
125
125
125
125
125
125
t?5
t25
1 A
1 4
125
1 A't?5
l 4
1 E
125
I A
1 E
r25
!2
94
s3
!,tl
9 l
tl4
o.0272BRLBRLBRLARLBRL
0.01.$
Souc.i Sl500G0t
1 . 1 6
1 . 1 6
1 . 1 8
125
t.34
125
So(tEG SJungB-0|
1 - 1 3
1 . t 3
1 3 1
1 . 1 2
ndlfigrnqlmsr
0.1F00
8RL
8HL
8FL
8aI
o0{x00.0126
8FL
8At
BRI-
0.0118
BRL
BFL
0jt06
BRIgRL
oo11g
sFt
u+114
79"}1@
81.7-100
Bt516
82r06
58.$r04
88.$1r,1
D3I(E
54.+114
81.'1m
58.9104
€s90
94
95g,
94
s0€0t6g0
IO
4
3
l0l
4
O B
3
I
3
r8
20
20
m&nn20
n202020mmm
96
9B
94g0
30
107
99
nn20m
Thb ,aborclary Eparl ,s nal relid withou aa aurtofiaEd signaun on th4 cavet pagc-
* Re!'{rtabl€ Det&tion Limit BRL= B€low ReportinB Limit Page l5Oof 154
Page 736
SPLP Metats by EPA l3l2 & 6000/7000 Series Methods - euality Control
Spike Source
B.tch 7031805 - SW846 3010A
tl.trir Solk Urp l700180(;ilS01I
PEgared: ?Olilarfi Andfz€d: Cz-Apr{7
Cadnirn
Banum
Pod Solk lt0glE{Fpsl)
Pr@8rbd: 3$Mar'07 Analyz€d: 02-Apr.{17
I _ 1 5
I _ 1 9
1 . 2 1
Sourcs 545980301
1 . 1 0
1 0 9
1.O1
1-14
1 . 1 2
1 . 1 7
1 - 1 6
0 00233
56.rrr: SA59{iB-07
BRL
So{rc€r SA59{tr(}01
Source SA59E{F01
nElmslms4
0.0150
0.0025
0.0050
0.0150
0.0075
0.0100
0.0025
0 0150
00125
0-0050
125
125
1.25
125
1 E
1.25
125
125
125
125
8Bt
BAt
00r06
88L
BRI-
BRL
BRI-
BBL
0.0118
0.0106
81.?-100
E?.I06
8€.S114
?0_{-1(E
i0.1,107
67 &93.8
75.8-r@
74 t-104
78.2-107
86.$1t8
92
95
96
3
2
3
20
2A
20
S€l€niurn
L6ad
Sil'/€r
CadmiLrn
Chromtum
Baium
Brtch 7031606 - EPA200/SW7000 Series
B|5d( flBl106€LKtl
PtEpsr€d: ${llar47 A|atfred: 02-Apr{7
lCS L031t{E{Slt
Pcpar.d: 30. r.07 tnaryzed: 02.Atr,07
tlrlicf b lt6180F0ruPl I
Prepat€d: 3H{ar.07 kalyz€d: 02,Apr{7
IrtU SE:t. flqI806{S1l
P'€for€d:3c ar.07 lratyzod: 02.AprO7
IriU Slae fu! fioot8(FttsDt )
Prepand: 30.ltla,-07 lnalyzed: o2-Aprq
Pod Sdte ftBl8G+Sll
Pft{aGdr 30{tsr-07 &Eryz€d: 02.Atr{7
mgl
rndl
mea
m94
mg,4
mqn
rn94
88
86
9 1
90
93
92
rngnBRL
nr0I 0.m250
mga SBL
0.0025a ngn 0.00040 0 00250 BRL
So|Jll : EA5S€09{1
0 00228 mM 0.00040 0 o@s0 8nL
Sclrc€: SA50{e01
76.1-111
76.1.111
66.&1100 00?21 mdl 0fi0-40 0.m250 BFL
General Chemistry Parameaers - Quality Collarol
Andvte(t UnitsFlasResultSpike
L€vel LimirsResult %REC
Bract 7031879 - Cetr€ral Preprrrtion
o|btcrt a?tBlETgoupr)Pr€pe€d E AnalFed: 30.Mar-07% SdidE
Sourcs: SA5078G32
79.89 2 6 l 5
ThIs lahorAory reFod Lt aol valid htilhoul aB oathorited sigdaturc on the cowr page-
+ Reportable Detection Limit BRL = Below Reporting Limit Page 15l of 154
Page 737
Noles and Delinitions
*TPH Calculated as
Comp Compl€ted
FP Field Pres€rved
QC I Analyte out ofacc€plance range.
QC2 Afilyte otrt of aEceptance tulge itr QC spike b(ll tro rcponable €ooce ratiotr preser in sample.
QCa The spike recovery is outside acceptable limils for the LCS. The batch was accefrted based upon the MS ard,/or MSDrn€eting the LCS lihirs crireria-
QM2 The RPD and/or percent recovery lior this Qc spike sample cannot be accurately calculated due to the high concetrhatiooofaoalyte irhereot in lhe sample.
QM4 Visual evaluation ofth€ sample indicales th€ RID is above the control limit due to a non.homogeneous sample matrix-
QM7 The spike tecovery was outside a{ceptatrce limib for the MS and,/or MSD. The barch was accept€d based on acceptableLCS recovery-
QM8 The spike recovery exceeded the QC coohol liEits for the MS atrd/or MSD. The batch was accepted based upotracc€ptable PS and/or LCS recovery.
QRI A-oolys€s are not conholled on RPD values ftffn sarDple concentsatio[s less than | 0 times the reporting linil QC batrhacceptsi baed on LCS and/or LCSD eC resultl.
QR2 The RPD result exceeded the QC control limits; however, both percent recoveries werc acceptable. Sample rcsults fo. theQC batch were accepted based on perceDr recoveries and completeDess of eC dar&
QR4 Analys€s are not controlled on R-PD values ftom sarrple mnceotralions less tharr th€ reporting limit. QC batch aco€pr€obased on LCS and,/or LCSD QC iesuls
QR5 RPD oul ofacccptance range.
Rol The ReportiIlg Limit for this analyte has been .ai$ed !o account for matrix ioterf€rence.
S02 The sunogate rcrovcry for this sample caotrot be accurately quaatified due to interfereuce ftom coeluting organiccompounds preseot io th€ sample ext act.
vex2 Field eKtrBcted
VOCS Reporting limits reflect SW846 5030 extraction t€cbnique due to mahix ilrt€rference usitrg Sw846 50354 €xtractiontechnique.
Z-2 Th€ MRL for this allallte bas increased due to the limited sanple yolume provided for analysis-
Z-2a The recovery ofd-BHC was outsid€ oftbe accepbrce raqge duD io a breakdou! ofd-BHC within the spike Eixtl|r.e.The CCC is within acccptable limitg, which d€monstrates rhat t[€ plobled lies wi6 tbe mixture, not the i[strumentatiotl
BRL Below Reporting Limit - Analyr€ NOT DETECTED er or above dle r€porting limit
dry Sarbple resulrs rcported oo a dry weight basis
NR Not Reported
RPD Relative Percent Differeuce
J Deteoted but b€low the Reporthg Litrril aherefore, result is atr estimated cotrce ratioD (CLp J-Flag).
A plus sign (+) io the Method Referetrc€ colunur indicatcs the method is oot accrcdited bv NELAC-
Thk [email protected] rcport B not ldtd to hoa an atthotizel dgnoUre on t*e covcr prge.
' RQortrble D€tectiotr Limit BRL = Below Reporting Limit Page 152 of 154
Page 738
Intemretation of TotaL Petroleum Hvd.ocarbon Report
Petrol€um ideotificatiol! is determined by coEpanng the GC firgerprint obhired liom th€ sample with a libmry ofGC fingerprintsobtained from an Vses ofvarious p€troleum products_ possible hatch categories are as follows:
Casoline - includes regular, unleaded, premium, ecc.Fuel Oil #2 - includes home heating oil, #2 tuel oil, and dieselFuel Oil it4 - includes #4 fuel oilFuel Oil li6 - includes #6 tuel oit and bunker "C', oilMotor Oil - itrcludes virgin and waste aunomobile oilI-ig.oin - idcludes mineral spirits, pettuleum naphtha, vm&p naphthaAviation Fuel - includes kerosene, Jet A turd Jp-4Other Oil - includes lubricating and cutting oil, and silicon oil
At times, fte uddentified petroleum ptoduct is quantified using a calibratior that most closely approximates the distribution ofcompounds ir the sample. When this occun, the result is quaLified as *TpH (Calculated as).
I-aborEtow conhol samDle (LCS): A krown rnatri( spiked with compouod(s) reprcs€ntativc of rhc targer analytes, which is used rodocument laboratory performance.
Matrix Duolicate: An intra-labo.atory splir samplc which is used to document the precision ofa method in a giveD sample matdx-
Mahix Soike: An aliquot ofa sample spiked with a known conceoaation oftarget a1aLyte(s) Thc spiking occurs pnorto samptepreparauml and analysis. A matrix spike is usedto document the bias ofamethod in a sivm samole malrix.
Method Blank: An anallte-free matrix to which all reagents arc added io the same votumes or proportions as [sed in sampleplocessing The method blank should be carried through the oomplete sample prepatation and analyrical procedure- Tbe methodblsnt is used to document contamination resuLting from the analltical process.
Method Detection Limit (MDL): The minimum concentrario! of a substance that carr be measuted and reponed with 997oconfidence that the analyte concentration is greater than zero and is detemined from analysis ofa sample in a given matrix typecontalning th€ analyte,
ReDortable Detection Limil aRDL): The lowest concenration that ca, be reJiably achieved within specified limirs ofFrecisioD andaccuacy durbg routine laboratory operating conditions. For many anatytes the RDL analyte conccntratioo is selected as ihe lowesttron-zero standard in the calibmtion cutve- While the RDL is approximately 5 to l0 times the MDL, the RDL for each sample takesidto account the samPle volumdwcight, exftact/digestate volurne, cleanup procedures and, ifapplicable, dry weight cofiection.Sample RDLS are highly matrixdependenr.
$qpgg@; Ar organic compound *.hich is similar to the trrger anal)4e(s) in chemical composirion and behavior ir the a@lyticalprocess, but which is not normally found in etvirormental samples_ These compounds are spiked into all blanks, standards, aods,arnpl€s prior to eielysis. Percent recovclics are calculated for each surroqate,
Validated by:Hanibal C. Tay€h, Ph.D.Nicole Brown
Thb laborulory.q,orl is not valu w hout an aurtorked sipstarc ol the corfrr page.
* Reportable Det€ction Lirnit BRL = Below Reponing l-imit Prge 153 of 154
Page 739
State Of ComecticutDepartrnent of Environmental Protection
Laboratory Quality Conhol and Quality Assurance Form
' The compoands ando. elemts rcporled tre s W€cifi@lly .qu6red by dE cticnt on dE Chlin of Cudody lnd io sonE cs€s nay nor inctud€ rh€ tuttelyte list d delined in the m€thod
Negotive rcsponses lor A, B and C arc addressad in a ctse narative on the c.rrer page of rtis repo.l
I, lhe tndersigne4 attesl ander lhe pains and pnnallies ofpelaty thol btsed upon t tlt pedonal inqtit! oflhov respottsiblefor oblaining the inron ratian, rhe male.ia! codraidad irr rhis cna{.r'll.,ll re|nn 4 ro ,*e besr of my hnotrledge stut Mietaccatrqu and codplele
ffieHanibal C. Tayeh, Ph-D-Presidetrt/Labo.atory Director
Datei 414/2007
labomtory Name: Specrrum Aoalytical, Inc. - Agawam, MA Project Name aDd Number:
Projecl Location; NHRY M8 Accepbsce Facility - New tlaveb, CT NHRY M8 Acccptarce Facility - New Haven, CTl
This Form Provides cerrifrcations for the followinS dua set:sA5980l{l sA5980l-Ll
sA59E0l{2 SA59E0I-12
SAJ9EO3,03 SA5%01-13
sA59E03-04 SA59E03-|4
sA59803-05 5459803-15
sA59803-.{b SA59E03-16
saJ9803{7 SA5980l_17
SA59E03-0E 5.{5960l-t8
sA59E03-09 SA59E03-19
sA5980l-t0 sA59E03-20
List Sp€cific Analltical Methods Used:
+CI ETPH
EPA200,7
EP!. 245_tn410A,
SM254O G Mdr
SW 8,15 8?608
sw846l l l2
swE46 t]tz60LoB
sv,rE46 l3t2n470A
sw846 60108
swtil6747lA
swE45 808 | A
sw846 8062
sw846 82608
sw8ut6 E270C
sw8{6 E270CIEPA 62J I
voc
Sample Matnces:
SoiYseditunt
Were all samptes received by the laboratory ia a conditiol consisienrwith that describ€d otr the Chain ofCustody documentation for the dataset?
El Yes E No
BWere all QA"IQC procedures required for rhe rpcified analyticalmethod(s) iflcluded in this reDort followed?
El Yes E No
c Were all QC performalce stardards and r€aommeodations forrhespecifi ed methods achieved?
E Y e s E N o
DWere results for all anal)rt€-list coslpouDdv€lemetrts for the specifiedmethod(s) reporcd? E Y e s E N o *
Thit raborulory Epotl ls ,rol volitt xttdro.tt sn asthodzd sigaat'.E oa tht @ee, page.
'Rel'dtable Detection Limit BRL = Beloin Reponing Limit Page 154 of 154