Vials & Syringes SUPELCO 374 Order: 1.800.325.3010 Technical Service: 1.800.359.3041 Web: www.sigma-aldrich.com/supelco E000815 E000782 E000792 E000817 E000798 E000810 Vials Selecting Vials, Inserts, and Caps Screw Top Vials These standard and large opening vials are available in both clear and amber glass. They come with a variety of closures and septa. Snap-Top Vials For use with snap- ring seals as well as standard aluminum seals. ABC Screw Top Vials These vials have a unique thread design that allows you to screw on the caps, and still use them in a robotic autosampler. LVI Vials These large opening, crimp top vials have a cone- shaped insert. Vial Varieties Crimp Top Vials These standard and large opening vials are used with aluminum seals. The 11mm aluminum seals have 6mm openings. Shell Vials Cylindrical shell vials compatible with plug-style needle closures to make syringe extraction easier. Polypropylene Hole Cap Temp. Limit 135°C Phenolic Solid Cap w/Teflon Temp. Limit 205°C Not Autoclavable Polypropylene Solid Cap w/ Aluminum Temp. Limit 135°C Not Autoclavable Phenolic Hole Cap Temp. Limit 149°C Inserts with Bottom Springs – The unique design allows the insert to be centered in the vial. Inserts with Top Springs – With the unique design, the insert is centered in the neck of the vial. The needle extracts nearly all of the sample. Cone-Shaped Inserts – These economical inserts stand unsupported in the carrier vial. Capacity 0.10-0.20mL. Shell Style Inserts – These economical inserts stand unsupported in the carrier vial. Capacity 0.25-0.35mL. Selecting Screw Top Vials and Components Volume Vial OD x Height Cap Diameter Cap Thread (GCMI Spec.) Septum Diameter 2mL (0.5 drams) 12 x 32mm 12mm 8-425 8mm 4mL (1 dram) 15 x 45mm 13mm 13-425 11mm 7mL (2 drams) 17 x 60mm 15mm 15-425 13mm 15mL (4 drams) 21 x 70mm 18mm 18-400 16mm 22mL (6 drams) 23 x 85mm 20mm 20-400 18mm 40mL (10.7 drams) 29 x 81mm 24mm 24-400 22mm 40mL (10.7 drams) 28 x 98mm 24mm 24-400 22mm Insert Varieties Cap Varieties P000862-9
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VialsSelecting Vials, Inserts, and Caps
Screw Top VialsThese standard andlarge opening vialsare available in bothclear and amberglass. They comewith a variety ofclosures and septa.
Snap-Top VialsFor use with snap-ring seals as well asstandard aluminumseals.
ABC Screw Top VialsThese vials have aunique thread designthat allows you toscrew on the caps,and still use them in arobotic autosampler.
LVI VialsThese largeopening, crimp topvials have a cone-shaped insert.
Vial Varieties
Crimp Top VialsThese standard andlarge opening vialsare used withaluminum seals. The11mm aluminumseals have 6mmopenings.
Shell VialsCylindrical shell vialscompatible withplug-style needleclosures to makesyringe extractioneasier.
Polypropylene Hole CapTemp. Limit 135°C
Phenolic Solid Cap w/TeflonTemp. Limit 205°CNot Autoclavable
Polypropylene Solid Cap w/AluminumTemp. Limit 135°CNot Autoclavable
Phenolic Hole CapTemp. Limit 149°C
Inserts with Bottom Springs –The unique design allows theinsert to be centered in the vial.
Inserts with Top Springs – Withthe unique design, the insert iscentered in the neck of the vial.The needle extracts nearly all ofthe sample.
Cone-Shaped Inserts – Theseeconomical inserts standunsupported in the carrier vial.Capacity 0.10-0.20mL.
Shell Style Inserts – Theseeconomical inserts standunsupported in the carrier vial.Capacity 0.25-0.35mL.
Selecting Screw Top Vials and Components
Volume Vial OD x Height Cap Diameter Cap Thread (GCMI Spec.) Septum Diameter2mL (0.5 drams) 12 x 32mm 12mm 8-425 8mm
4mL (1 dram) 15 x 45mm 13mm 13-425 11mm7mL (2 drams) 17 x 60mm 15mm 15-425 13mm
15mL (4 drams) 21 x 70mm 18mm 18-400 16mm22mL (6 drams) 23 x 85mm 20mm 20-400 18mm
40mL (10.7 drams) 29 x 81mm 24mm 24-400 22mm40mL (10.7 drams) 28 x 98mm 24mm 24-400 22mm
Insert Varieties
Cap Varieties
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VialsABC Autosampler Vials
ABC Vials, Large Opening,Preassembled, 2mLUniversal autosampler vials,can be used as either crimp-top orscrew top. Use with autosamplers thatrequire 12 x 32mm screw top or crimp top vials.VIAL DESCRIPTION QTY. CAT. NO. PRICEPOLYPROPYLENE CAP, PTFE/SILICONE SEPTUM
ABC Vials, Large Openingwith 0.3mL LVI InsertPacks of 100.VIALS CAT. NO. PRICE
Clear glass, no cap 27562-U Clear glass, w/PTFE red rubber cap 27564-U Clear glass, w/PTFE silicone cap 27565-U Clear glass, w/PTFE/silicone/PTFE cap 27566-U Clear glass, w/PTFE lined cap 27567-U Amber glass, no cap 27563-U
Screw Caps with Septa for ABC VialsCAP COLOR QTY. CAT. NO. PRICEPTFE/SILICONE
Clear 100 27326 Clear 1000 27558 PTFE/RED RUBBER
Clear 100 27327 Clear 1000 27559 RED PTFE/SILICONE
Black 100 507393 Red 100 507423 Yellow 100 507466 PTFE/SILICONE/PTFE
Clear 100 27328 Clear 1000 27560-U TAN PTFE/SILICONE
Black 100 507385 Yellow 100 507458 PTFE/SILICONE/PTFE
Barrier (maximum temp. 350°C)Silicone bonded to aluminum. Use in sealingapplications where non-permeability and lowvolatility are required at temperatures above177°C. Affected by many organic solvents(see examples under Silicone).Butyl (maximum temp. 200°C)Use with many organic solvents: acetic acid(<50%), acetonitrile, acetone, alcohols,DMSO, phenol. Not compatible with alkanes,benzene, carbon disulfide, chlorinatedsolvents, cyclohexane.
Red rubber (maximum temp. 100°C)Use with many hydrocarbons, acetonitrile,alcohols, cyclohexane. Not compatible withchlorinated solvents.Silicone (maximum temp. 250°C)Use with acetone, alcohols, DMSO, ether,aqueous samples. Affected by many organicsolvents: acetonitrile, benzene, chloroform,hexane, pyridine, tetrahydrofuran, toluene.Teflon/Rubber (maximum temp. 100°C)Use with most organics (until pierced).Resistant to chlorosilanes.
PTFE/Teflon/Silicone (maximum temp. 250°C)Use with most organics (until pierced). Notrecommended for use with chlorosilanes.PTFE/Thermoseal (maximum temp. 300°C)An improved grade of silicone septa that can beused at higher temperatures. Affected by manyorganic solvents (see examples under Silicone).Viton (maximum temp. 315°C)Resists mineral oil, aliphatic and aromatichydrocarbons, high concentrations of acids, hightemperatures. Not compatible with strong bases,ketones, low molecular weight esters.
Phenolic, solid caps w/PTFE liner 100 27091-U Phenolic, solid capsw/aluminum liner 100 27092-U Phenolic, black, open top 100 27094-U Polypropylene, black, open top 100 27052
1000 24764 Polypropylene, yellow, open top 1000 24765 Top seal, polypropylene,clear, 0.010" 100 27402 Hole cap, black, large opening 100 27401 Top hat, black, w/silicone septa 100 27403-U Top hat, yellow, w/silicone septa 100 27404
White PTFE, 0.010" 100 27281 (for use with solid cap) 1000 27282 INSERTS, SHELL STYLE
0.35mL glass, 6 x 31mm 100 24715 1000 24716
INSERTS, CONICAL
0.05mL glass w/glass flange,6 x 25mm 100 27408 0.25mL glass, 6 x 31mm 100 24717 0.15mL glass w/top spring,6 x 29mm 100 24719 0.20mL glass w/bottom spring,6 x 29mm 100 24721 0.20mL polypropylenew/bottom spring, 6 x 29mm 100 24722 INSERTS FOR STEP VIALS
0.25mL glass w/glass flange 100 27407 0.25mL polypropylenew/plastic flange 100 27409 KIM-BIN WORK STATION
Station with 2000 clear screwtop 2mL (normal opening) vialsw/caps and PTFE/silicone septa 1 27264-U Unfilled station 1 27263
2mL SCREW TOP VIALS – LARGE OPENING (10mm OPENING)12 x 32mmUse with:
Alcott 738Hitachi AS-2000, AS-4000Shimadzu AOC-14/1400, AOC-17, SIL 6B, SIL 9A, SIL 6A(Use white and yellow closures only.)
Varian 8100, 8200Waters Alliance
VialsScrew Top Autosampler Vials
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Polypropylene Limited Volume ShellVials With Starburst Conical Snap Plugs
These polypropylene limited volume shellvials, with uniquely designed conicalinterior, eliminate the need for glass vialsand inserts. No tedious laboratory assemblyis required. These vials work in 48-positionautosamplers.
Precise conical design permits maximumsample evacuation. They are more effective and cost efficientthan standard glass vials and inserts. The starburst design in thesnap plug allows easy penetration.
DESCRIPTION QTY. CAT. NO. PRICE3mL SHELL VIALS, 15 x 45mm
Phenolic, black 100 27120-U Polypropylene, black 100 27053 Polypropylene capw/PTFE/silicone septa, 0.065" 100 27018 13mm black top hat,w/PTFE/silicone septa 100 27439 SOLID CAPS, 13-245
w/PTFE liner 100 27141 w/Aluminum liner 100 27142
Pre-Assembled Vials Kit
Includes each of the following(in packs of 100).
Screw top vials, 15 x 45mm,4mL glass inserts, 0.30mL clear glass,conical springs for 0.30mL conical insertclosures, open top, phenolic, black septa,red PTFE/red rubber
10mL clear glass(23mm x 46mm) 100 27198 20mL clear glass(23mm x 75mm) 100 27199 ROUND BOTTOM
10mL clear glass(22.6mm x 46mm) 100 27294 10mL clear glass(22.6mm x 46mm) 1000 27295 20mL clear glass(22.6mm x 75mm) 100 27296 20mL clear glass(22.6mm x 75mm) 1000 27297 CLOSURES AND ACCESSORIES FOR BOTH 10mL AND 20mL VIALS
Manual SPMESampling StandHolds eight vials whilesupporting the SPME syringefor consistent fiber immersiondepth. Cat. No. 57333-Uaccommodates 4mL vials only;Cat. No. 57357-U accommo-dates 15mL vials. Order the15mL vial puck (Cat. No.57358-U) as a replacementfor the 15mL unit, or to use15mL vials with the 4mL unit.Not for use with automated /HPLC fiber holders.
Heat/Stir PlateFits compactly on the base of the SPME sampling stand. Heatingrange is 40-550°C, stirring range is 60-1200rpm.
40mL Vial HolderUse this aluminum block for heating/stirring during headspaceSPME sampling of odors or other volatiles. Holds six 40mL vials.
DESCRIPTION CAT. NO. PRICESPME sampling stand for 4mL vials 57333-U SPME sampling stand for 15mL vials 57357-U Vial puck for 15mL vials 57358-U 40mL Vial Holder 33313-U Corning heat/stir plate, 120VAC Z262129-1EA Thermometer, 5” 57332
VIALS TAKING 8mm CRIMP SEALSCHROMACOL UNI-VI VIALS, 7 x 30mm, 7 x 32mm
Use with:Agilent / HP (not 1090A) PU 4247Autometric 4100 Shimadzu AOC-14/1400Beckman 501/502/507 SIL 6B/9A/LC-1Dani ALS 86.80 Spark PromisLDC Marathon, Promis Spectra-PhysicsPerkin-Elmer Integral 4000
VIALS TAKING 8mm CRIMP SEALSCHROMACOL VIALS, 6 x 32mm
A convenient way to organize your vials. Available filled withsupplies or unfilled. Cat. No. 27231-U includes 3000 clear large-opening 2mL vials, PTFE/red rubber 11mm septa, and seals. Cat.No. 27264-U includes 2000 clear screw top 2mL vials (standardopening), red PTFE/silicone septa, and black phenolic closures(recommended for Varian and Spectra Physics autosamplers).
DESCRIPTION CAT. NO. PRICEStation with Crimp Top Vials 27231-U Station with Screw Top Vials 27264-U Unfilled Station 27263
11mm Crimp Seals
DESCRIPTION QTY. CAT. NO. PRICECRIMP SEALS, COLOR CODED, 11mm
Open center, PTFE/rubber septum■ 100 27454-U Open center, PTFE/silicone septum■ 100 27455-U Removable center, PTFE red rubber septum■ 100 27228 Tin plate, open center, PTFE/silicone septum■ � 100 27300 Open center, PTFE/white silicone, 2 mil PTFE septum 100 27229 Open center, white PTFE/white silicone, 5 mil PTFE septum 100 27362
1000 27375 Tin plate, open center, PTFE/butyl rubber septum 100 27301-U Open center, Viton septum 36 33146-U Open center, black Viton septum� 100 27245
1000 27246 ALUMINUM CRIMP SEALS, 20mm w/o SEPTA
Open center 100 27227-U Open center 100 27230-U Tear away center 100 27016 Tear away center■ 100 27200 SEPTA, 20mm
Black Viton◆ ◆100 27247 1000 27248-U
PTFE/Teflon faced butyl 100 27201 PTFE/Teflon/rubber 100 27233 PTFE/Teflon (2mil)/silicone (125 mil total) 100 27236 PTFE/Teflon (10mil)/silicone (100 mil total) 100 27237-U Barrier (foil/silicone) 100 27189 PTFE/silicone (60 mil total) 100 27541 PTFE/silicone (125 mil total, 5/120) 100 27361
Cleaned for water sampling according to US EPA 40CFR 136,Guidelines for Establishing Test Procedures for the Analysis ofPollutants. These vials are assembled with open-top screw capsand specially designed septa (10 mils of Teflon facing on 90 milsof silicone). Clear vials are made of Wheaton-33 low extractableborosilicate glass. Amber vials are Wheaton-320 borosilicateglass.
4 oz. 48/400 24 24551-U 8 oz. 58/400 24 24552 16 oz. 63/400 12 24553-U 32 oz. 89/400 12 24554 CLEAR GLASS, TALL, NARROW MOUTH
32 oz. 33/400 12 24550-U AMBER GLASS, SHORT, WIDE MOUTH
4 oz. 38/400 12 24555 8 oz. 45/400 12 24556 16 oz. 53/400 12 24557-U 32 oz. 53/400 12 24558 AMBER GLASS, SHORT, NARROW MOUTH
32 oz. 33/430 12 24559 AMBER GLASS JUG, NARROW MOUTH
80 oz. 38/430 6 24560 128 oz. 38/430 4 24561
VialsPrecleaned Sampling Containers
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Screw Top Vessels with Caps and Septa
CAPACITY OD/HT./DEPTH CAP QTY. CAT. NO. PRICECLEAR GLASS (GRADUATED)
With hole cap0.1mL 16.5 x 32 x 16mm ▲ 15mm 12 33289 0.3mL 16.5 x 34 x 23mm ▲ 15mm 12 33291
1mL 16.5 x 40 x 33mm ▲ 15mm 12 33293 2mL 16.5 x 58 x 48mm ▲ 15mm 12 33295 3mL 20.5 x 42 x 42mm ▲ 20mm 12 33297 5mL 20.5 x 61 x 58mm ▲ 20mm 12 33299
10mL* 24.0 x 72mm ▲ 24mm 12 27479 With solid cap0.1mL 16.5 x 32 x 16mm ▲ 15mm 12 27034 0.3mL 16.5 x 34 x 23mm ▲ 15mm 12 27035
1mL 16.5 x 40 x 33mm ▲ 15mm 12 27036 2mL 16.5 x 58 x 48mm ▲ 15mm 12 27037 3mL 20.5 x 42 x 42mm ▲ 20mm 12 27038-U 5mL 20.5 x 61 x 58mm ▲ 20mm 12 27039
AMBER GLASS
With hole cap1mL 13 x 41mm ■ 13-425 12 27475-U 2mL 20 x 41mm ■ 20-400 12 27476 3mL 20 x 47mm ■ 20-400 12 27477-U 5mL 20 x 62mm ■ 20-400 12 27478-U
▲ Height with cap; depth from septum to bottom of cone.■ Height without cap.* Not graduated.
Micro Reaction Vessels
Cone shaped inside for easy removal of small samples. Heavy wallborosilicate glass. Supplied with Teflon-faced red rubber septumand cap. Can be autoclaved or centrifuged.
For 13mm screw cap 100 27145 For 15mm screw cap 100 27156 For 20mm screw cap 100 27178 For 24mm screw cap 100 27188-U MININERT VALVES
For 13mm screw cap 12 33300 For 15mm screw cap 12 33301 For 18mm screw cap 12 33302 For 20mm screw cap 12 33303 For 24mm screw cap 12 33304 For 20mm crimp top 12 33305 Replacement septa 50 33310-U Septum inserter 1 33311 CRIMP SEALS
For 2mL & 5mL vessels 100 27229 MAGNETIC STIRRING BARS (TRIANGULAR)
For 0.1-2.0mL vessels 6 23226 For 3.0-5.0mL vessels 6 23227
Heat resistant borosilicateglass flasks provide an inertseal when used with a hole capand Teflon silicone septum(included) or a Mininertvalve. Excellent for liquid-liquid extraction oftrihalomethanes from drinkingwater. Also useful for samplecollection, solution prepara-tions, derivatization reactions,extractions, and many otherapplications.
Crimpers and Decappers
DESCRIPTION CAT. NO. PRICE8mm
Hand Crimper 33272-U Pliers-type Decapper 33284 Hand Decapper 33180-U 11mm
Hand Crimper 33195 Hand Crimper, Adjustable 22313-U Pliers-type Decapper 33281 Hand Decapper 33181-U 13mm
Hand Crimper 33279-U Pliers-type Decapper 33282 Hand Decapper 33182-U 20mm
Hand Crimper 33280-U Hand Crimper, Adjustable 22316-U Pliers-type Decapper 33283 Hand Decapper 33183