Page 1
10971250007 - l»k. CountyN. Chicago Refiner* & Smclten
!LD 097271563
Superiund/HRS
CERCLAScreening Site
InspectionAnalytical Results
Illinois EnvironmentalProtection AgencyP.O. Box 19276Springfield, IL 62794-9276
EPA Region 5 Records Ctr
229807
Confidential Material May be Enclosed
Printed on Recycled Paper
Page 2
Appendix H
Target Compound List Analytical Results
H-l
CERCLA SSI: North Chicago Refiner* and Smelten - ILD 097271563
Page 3
U:OB7Z715«I
iAMPUNG POUT
VCCAT'LES
i - O
FESTiClOES/PCB**x:rtn« -DOEEn dm4 41 -DOT
vcclor-icn»VOCKX-1254
S6VHVOLW1LES
ncurxa 1 i3-c<*0>nn4>
1NOROAMC*MXTM jm
Annmony
CoppwIf on
MvcuiyNeMI
HI SON. 3AUPLE AWSLrDOi. RESULTS
X119
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1300 a8.X l>aoou6.00U
—•poe)
22.00U4100U42.00 U1100 J
220 00 U220. 00 U210.00 U42000 U(B*)
890 00 U860. OOO850.00 U680.00 U890 00 U300.00 J8900011990 00 U21OOOJ1 80.00 J860 JO U950.00 U980.00 U880.00 W850.001;880.00 U950.00 U960.00 U960 00 U850.00 U
— ...._
(PP«*
111000914.00 UJ740J
90090.701voo BJ
92900021091150828 90
18800.0948.09
4000008900
0.22J2209;
2360.000.84 u*toou
40100 U2810IliOO
X101
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„310. OOJ-_.-"-— ._
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030QOJ-500 OOJ
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14JOO.OO4S.30Jnsov
2MOO380
3650J67800.00
TV. 0012,79 A
9180001190000
U60QO34300.00
07400tW J
130.0023*0.00
3.10 Jftt.OB
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4.9700.00
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91000038000.00338000
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970008tt.09
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1 2700 003410000
4000 OOJ10000.00
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11700.09. .2570 J
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NOTES:U -8 - indUM confound * iJ - ndc«M compound • •
Page 4
Ncrtn cncogo R«rtn«ni I SnVUre:LC 067371583
SAMPLING POINT
VCLA TILES
SSI SEDUgCNT SAMPLE ANALYTICAL RESULTS
1 .2-C'cnk»asth«r» (total)5-3a«non«1 . 1 . t - TncMara«r<ano
E:ryEir»f
4.4'-OC€Enorin44 ' -OOr
gamma-Chioraan*Afaciof-1018Aroctaf- 1 254
SeWIVOLATlLES
P>r»Bjy1
B.3[2 -«ChrjfMod3i-o-octytpntn«iat»
• nd»no(1 .2.3-cd)pyr»n»Benzofg hjl
3enz(a)anthr«c«n»
Arthrac»o«. 2 -methyl9, 1 0-art!yac*r»*on«B8nzo|B]naptho[2.3.0]furanNapr»nal«n», 2-pn«oy<
1 -m«<nry1
INORGANICS .AluminumA/ximonyAnwicSan urnB«rybiumCadmium
CobaKCopp«fIronUnaMagrmun
M«rcuryNek*
SsicnuinSilv«rSodiumVaradiunZ.ncCyvnd*
NOTCS:U - indiutMconxxxnl wai t«M tor but not d*«ttdS - indicAM compound * an Ktimoled valueJ - indwM«« compocnd » an MiimatM vilu*
xi u1 1 -25-91(Sadimw*Background}
25.00 U120OU4.00.1
12 MU190O10002.00J
—(PPO)
20 OOU38-00 U38.00 U36.00 U
20O.COU200.00 U190.00 U240 OOJIPPO)
780.00 U780.00 U700.00 U780.00 U700.00 U7«acou
1300,00300.00 J
140QOOJ12QOOO780.00 U790.00 U540.00 J320.00 J480.00 J400.00 Jt500X0 J450.00 J490 OOJ700.00 U
— —-—- —--
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(ppb)
420000ixaouj8.JCM
90303.00180J
MOCOtXtt38 £&8JDB
710-CO18100.09
306.0047200XO
880.00O^flJ
38.20780, COB
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300OOO0.83 U
(ppm)
X11211-13-91
1100———
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—--(ppb)
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1500.00(PP«»
290 OOJ930.00 J
1 500.0090000
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—4700.00 J
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480JBJ1000. OOJ680 OOJ
—-—
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(ppb)
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1400.0010000.00
815.0037300,00
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42.00880.008--1.9ft
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(ppb)
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(ppb)
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(ppb)
4420.00
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74300X03320400B
304.009044001880.00
377O3XX}370.00
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870.00ISO
(ppm)
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Page 5
Il l inois Envi ronmenta l Protection Agency P.O. Box 19276, Springfield. IL 52794-3273
MEMORANDUM
DATE: February 11,1992
TO: Greg Dunn
FROM: Ron Turpin <Sc Jim Shaw
SUBJECT: Review of Data PackageNorth Chicago Refiners and Smelters
The Division of Laboratories Quality Assurance Section has reviewed theabove referenced data package. The package was for 18 soil samplestaken on November 15,1991, for the target compound list. The sampleswere analyzed at the IEPA laboratories in Springfield (organics) and inChampaign (inorganics). The results are valid as qualified on theattached Forms 1.
attachments
cc John HurleyKarl ReedTom Crause
RECEIVED
FEB131992
Page 6
Illinois Environmental Protection Agency • P.O. Box 19276, Springfield, IL 62T94-9276
MEMORANDUM
DATE: September 1, 1992
TO: Greg Dunn
FROM: Ron Turpin <W f U<V^1
SUBJECT: Erroneous Mercury results reported on N. Chicago Refiners & SmeltersSDG 59.
Attached are corrected Form 1's to replace the original forms for the above referencedsite. Due to a calculation error made by the laboratory, the Mercury results wereincorrect.
Page 7
SAMPLE DATA SUMMARY PACKAGE
J
Page 8
ILLINOIS ENVIRONMENTAL PROTECTION AGENCYSpringfield Organicg Laboratory
825 N. Rut ledgeSpringfield, Illinois S27Q2
217-732-9730
CASE NARRATTVT^
N. Chicago Refiners i Smelters
X101 D199S73X102 D199679X103 D199680X104 D199681X105 D199S66X106 D199667X107 D1996S3X103 D199669X109 D199S7QXliO 1-199571Xlll D199S&2X112 3199623
X114 D199685Xllo ~199636X.11S ^199537X117 Il99f^2'{' • ?.
Flucr-ce.-oene is used as an additional ir.terr.al standard to oalo\
vela- 1_= 3'andard.
•Zair.p'.-Ti wi-h laboratory file ident if ica~ ir.-.s cegir.r.ir.g with ar. A warerun on instrument 5 100 A. Those beginning with a 2 war? run on instru-sr.t
X101 w=.s rerun as X101RE. In XlOl 5urr:gatr3 573 and toluene-dS as wea3 two ~z the three internal standard- were outside acceptable iimit=In X1:J2?_Z both surrogates were still rut cf control as well as ailthree internal standards. This reanalysis ot-plies with the Volatilerequire-ents, feotion III. paragraphs 4.2.2.1.4 and 6.1.1.2 of the2/85 itatenent of Woric.
The Wi.ey Mass Spectral Database in the Chemical Information System.on-line service was searched as an ado it ic.Tal oheok to try tt identisome tf the more signif ioant TICs. N-: r.atrhes were found.
The baseline rise in the 12/02/31 standard had no effect on ouant 1 tat :-.-.
Page 9
^i-i". "i----~i"T. - — ^_~ r. 'S r. r. c CT. ir.u ir. & ~i*icrit«cr. c r ' " 5 r' a.
Although all samples were extracted on 11/15/91, the samples received cr.11/14/91 were extracted by the day shift and those received on 11/15/9:were extracted by the evening shift. Hence- there are two blanks and-wo sets of matrix spikes.
XilS matrix spike FORM III SV-2 ;Pyrene was detected in the original sample at a concentration higherthan that in the matrix spiked samples. This resulted in a net negativerecovery in the matrix spikes on FORM III. This may be due to an unevendistribution of the analyte in the sample container.
X1C2 ; The spectral disagreement of fluoranthene is more than the 2C°Sallowed when compared with the standard spectrum because of a co-elutingTIC in the sample.
X103 ; The spectral disagreement of di-n-butylphthalate is more thar. tr.e2Crs allowed when compared with the standard spectrum because of aoo-eluting TIC in the sample.
X106 ; The spectral disagreement of fluoranthene is more than the 20%allowed when compared with the standard spectrum because of backgroundnoise in the sample.
X10S : The spectral disagreement of ber.zc cb ; fluoranthene , ir.deno( 1, 2 , 2- : d -pyrer.e and ber.ro •;. ghi )pery ler.e is more than the 20Ji all-wed when ccmparec,with the standard spectrum because of background noise in the sample.
XI10 ; The spectral disagreement of n-nitrosodiphenylamine is more th-zr.the 20^ allowed when compared with the standard spectrum because ofbackground noise in the sarr.ple.
X.lll ; The spectral disagreement cf ir.der.c ; 1, 2. 3-od ; pyrer.e ar.o rrr.~o i/.. -p-rryle.-.e is r.:r? Than the 20% allowed when ocr.pared with the £tandardspectrum because of background noise in the sample.
X112 ; The stertral disagreement of fluorene is more thar. the 2'.'"i allcveowhen ccmpared with the standard spectrum brcause 4-ohloropher.yl phenylet.-.er c:-elute* in the standard.The spectra, disagreement of naphthalene, butylbenrylphthslate. benrc =. -pyrer.e. -.n-der.: : 1, 2 . 3-od ; pyrer.e and bsr.zc-'. gr.i . pery ler.e is mere thar. the 21 •.allcwed when compared with the standard spectrum because of a cc-eluf.r.aTIC in the sample.
XI13 : The spectral disagreement of bsr.o:; b : f luorar.thene and ber.o-.'.-: -flu:r*nthene is more than the 2G£ allowed when compared with the standirdspectrum because of background no is? ir. the simple.
XI15 : The spectral disagreement of flucrene is more than the 20% ail eweuwren ccmpared with the standard spectrum because 4-ohlcropher.yl pher.ylether cr-elutes in the standard.The spectr=l disagreement c-f bisi 2-ethylhe>:yl'phthalate is more than tr.s20ti al_:wed when compared with the standard =p»otrur. because ber.scio =.cidco-elutes in the standard.The spectral disagreement of indenc ( 1. 2. 3-cd pyrer.e and bensc'. ghi :?ery ler.is more thar. the 20"4 allowed when compared with the standard speotru:"hecauze cf cackground noise in the sample.
X115 : The spectral disagreement of flucrer.e is more than the 20 - all-ewe:
Page 10
-» — •»-*— —* -• .a * • • .a a * o **W A • ** a *^ '^ a v*^5 - i. 5 r »w~"r--*'-(33 ^ n -**e 3.a.*^a.^.
XI 13 ; There is insufficient space on FORM III EV-TIC for the naj.es ofthe components detected. Most are PCS isomers. See the Library searcheswith the seoivolatiie data or the pesticide results for identification.
Surrogate recoveries on samples X112. Xil5, X115 and XllSMS (Fern 25)were high due to matrix interference in the samples.
Surrogate was not detected (Form SE ; in samples X115, XllSMS and X112MSL1
due to the high amount of PCS causing masking, so recovery was calculate:from the alternative confirmation column.
Matrix spike analytes Aldrin. Dieldrin and DLT were net detected 'Form 2:due to masking by the PCS concentration.
The %r> for 4,4'-DDT was high ;?orT. 9} due to the improper integrationof the peaks in the late runs caused by the rise in the baseline fromthe temperature program". 4,4'-DDT was not detected frr quant itat ion zzno corrective action was taken.
The alpha and gamma-Chlordane found in X1C5 (Fcrm 10; was confirmedby GC/M2 but the specific isomers were not determined.
Celeste Crowley (/ DatePesticide Supervisor
ar/jermannC-'Mi Supervisor
- ^ - , . + ^ i —arf..-. :-:--rley 7aboratory Manager
Date
Page 11
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Page 22
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LEto r:-OF CUSTODY
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Page 26
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Page 28
V- CLJ> "OF CUSTODY
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Page 29
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
EPA SAMPLE NO
X101
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.Q (g/mL)
Level: (low/ned) LOW
% Moisture: not dec. 46
Column: (pack/cap) CAP
Contract: 097l25nnn7
Case No.: REFINE SAS No.: SDG No.: D1996R
Lab Sample ID: D19967H
Lab File ID: Blll9LCMn
Date Received: 11/15/91
Date Analyzed: 11/19/91
Dilution Factor: 1. 0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride.67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene.75-34-3 1, 1-D ichloroethane.
67-66-3 Chloroform107-06-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1,1,1-Tr ichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene.75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene.79-34-5 1,1,2,2108-88-3 Toluene108-90-7 Chlorobenzene_100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total).
19191919142399999919991999999999919199999999
Q
;u;u:u
: u;u:u;u:u;u!U10IU:u:u;o:u:o!u:u:u!U;u:u;u: u10:u:o:u;u
FORM I VGA 000004
Page 30
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE NC
X101
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.Q (g/mL)
Level: (low/Bed) LOW
% Moisture: not dec. 46
Column (pack/cap) CAP
Contract: Q97125QQ07
Case No.: REFINE SAS No.: SDG No.: D19966
Lab Sample ID: D199678
Lab File ID: B1119LC10
Date Received: 11/15/31
Date Analyzed: 11/19/91
Dilution Factor: 1.0
Number TICs found; Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC OOOCOS 1/37
Page 31
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
EPA SAMPLE SC
X102
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/ned) LOW
% Moisture: not dec. 42
Column: (pack/cap) CAP
Contract: Q971250QQ7
Case No.: REFINE SAS No.: SDG No.: D19955
Lab Sample ID: D199679
Lab File ID: B1119LC13
Date Received: 11/15/9!
Date Analyzed: 11/19/31
Dilution Factor: 1.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1,1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroe thane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1, 1,2, 2-Tetrachloroethane_108-83-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
17171717Jf2499999917991799999999917179999999
Q
:u;u:u:u
: u: u;u
:u10;u:u:o!U: u:u;u1U
: u!U:u:u;u1 U:u;u;u
FORM I VOA oooccs
Page 32
IBVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE SO
X102
Lab Code: SPFLD
Matrix: (soil/water) SJUL.
Sample wt/vol:
Level: (low/med)
Contract: Q97125QOQ7 |
Case No.: BJLLLNJL SAS No.: SDG No.: D19966
(g/mL)
% Moisture: not dec. 42
Column (pack/cap) CAP
Lab Sample ID: D199679
Lab File ID: Blll9LC!3
Date Received: 11/15/91
Date Analyzed: 11/19/91
Dilution Factor: 1. 0
Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FOPM I V O A - T I Cnnnnrvi
1/3"
Page 33
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
EPA SAMPLE NO
X103
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 4Q
Column: (pack/cap) CAP
Contract: Q97i?snnn7
Case No.: REFINE SAS No.: SDG No.: D19936
Lab Sample ID: D19968Q
Lab File ID: B1119LC12
Date Received: 11/15/91
Date Analyzed: 11/19/91
Dilution Factor: 1. Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichlo roe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1 ,1 , 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
17171717
88838817881788888888817178883388
Q
UUU;U
! U!D!DIDIUIDID!DIU!UID:o:uIDID:uID:uIDIDIDIDIDIDIUIUIU,'D
FORM I VGA 1/37 ?-
Page 34
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA Contract: 0971250QQ7
EPA SAMPLE S:
X103
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 40
Column (pack/cap) CAP
Lab Sample ID: 0199680
Lab File ID: B1119LC12
Date Received: 11/15/91
Date Analyzed: 11/19/9!
Dilution Factor: 1.0
Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FQBM I V O A - T I C 000011 1 /Q 'i / J
Page 35
LAVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ILLINOIS EPA Contract: 0971250007
a?A SAMPLE NC
X104
Lab Code: SPFLD
Matrix: (soil/water)
Sample wt/vol:
Level: (low/Bed) LOW
Case No.: REFINE SAS No.: SDG No.:
(g/mL)
% Moisture: not dec. 20
Column: (pack/cap) CAP
Lab Sample ID: D199681
Lab File ID: B1119LC1
Date Received: . 11/15/91
Date Analyzed: 11/19/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION DNITS:(ug/L or ug/Rg) UG/KG
74-37-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chlo roe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroethane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-Butanone71-55-6- ---1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride103-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1,2-Trichloroe thane71-43-2 Benzene10061-02-6 trane-1,3-Dichloropropene_75-25-2 Bromoform1 OS-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-13-4 Tetrachloroethene79-34-5 1,1, 2,2-Tetrachloroethane_108-83-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
121212127
6666612661266666666612126666666
Q
!U
uuuuuuuu:u:u;u!U', u;u
UUuu:u:uiu:u
FORM i VOAQOQG12
1/8'
Page 36
12VOLATILE OBGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: Tr.LTNOIS EPAX104
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 20
Column (pack/cap) CAP
Contract: 0971250007
Case No.: REFINE SAS No.: £DG No.: D19966
Lab Sample ID: D199681
Lab File ID: B1119LCM
Date Received: 11/15/91
Date Analyzed: 11/19/91
Dilution Factor: 1.0
Number TICs found: Q_CONCENTRATION UNITS:(ug/L or ug/Kg) UG/RG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I V G A - T I C000013
Page 37
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Nam«: ILLINOIS EPA
EPA SAMPLE NO
X105
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. .. 14
Column: (pack/cap) CAP
Contract: 0971250007
Case No.: REFINE SAS No.: SDG No.: D199SS
Lab Sample ID: D199fififi
Lab File ID: All2f)Ryn4
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Rg) DG•KG
74-37-3 ChJ ore. me thane74-33-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1,2-Dichloroethene (total),67-66-3 Chloroform107-06-2 1,2-Dichloroe thane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cia-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-l,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 l,l,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
12121212666666
12661266666666612126666666
Uu
UuuuU
uU
i U;u!U:u;u:u:u:u
Uuuu
i uiu:u:u:u
FORM I VOA OOG014
Page 38
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDSLab Name: ILLINOIS EPA Contract: Q97125QOQ7
EPA SAMPLE NO
X105
Lab Code: SEILJL Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 14
Column (pack/cap) CAP
Number TICs found: L
Lab Sample ID: D199666
Lab File ID: A112QBK04
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1. Q
CONCENTRATION UNITS:(ug/L or ug/Kg) OG/KG
CAS NUMBER
1. 60-29-3
COMPOUND NAME
ETHYL ETHER
! RT
1 1.65l'
E3T. CONC. ^
9.8 J
FOPM I VOA-TIC 000015
Page 39
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
EPA SAMPLE NO
X106
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5 .
Level: (low/med) LOW
Contract: Q97l25pflfl7
Case No.: REFINE SAS No.: SDG No.: D19966
(g/mL)
Lab Sample ID: D199667
Lab File ID: A112QRKOfi
% Moisture: not dec. 2^
Column: (pack/cap) CAP
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
.7^-87-3 ChloromethaneT4-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2- Bu t anone71-55-6 1,1,1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1, 2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
1313131371377777713771377777777713137777777
:u;u10i ui
i u!U:ui ri
iu:u:u
;u;u;ui ui ui u:u:u;u:u!Ui u;u:oiui u:u;u
FORM I VOA OOOOlo
Page 40
ISVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE N:
X106
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5 .
Level: (low/aed) LOW
Contract: 09712500Q7
Case No.: REFINE SAS No.: SDG No.: D19966
(g/mL)
Lab Sample ID: Dl99fifi7
Lab File ID: A112nBKns
% Moisture: not dec. 24
Column (pack/cap) CAP
Date Received: 11 /I
Date Analyzed: 11/20/91
Dilution Factor: l.Q
Number TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1. 60-29-3
COMPOUND NAME
ETHYL ETHER
RT
1.65
EST. CONC. !
5.4! J1
Q
FORM T VOA-TTH
Page 41
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE SO
Lab Nam«: T T . T . T N Q T S EPAX107
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/ned) LOW
X Moisture: not dec. . 16
Column: (pack/cap) CAP
Contract: Q97i25nnn7 _
Case No.: REFINE SAS No.: SDG No.: D1996S
Lab Sample ID: D1996B3
Lab File ID: A112QBKnfi
Date Received: 11/14/91
Date Analyzed: 11/2Q/91
Dilution Factor: 1. Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Rg) UG/RG
74-87-3 Chlororae thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Kethylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochlorome thane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1, l,2,2-Tetrachloroethane_108-38-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
12121212612666666
12661266666666612126666666
Q
;u;u;u
;u!'J;u
;u
uuU
: u;U;uI U!U:u!Ui U:u!U!U!U:o:u!U
FORM I VOA 00001S
Page 42
IBVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE SC
X107
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 16
Column (pack/cap) CAP
Contract: Q9712SQQQ7
Case No.: REFINE SAS No.: SDG No.: D19968
Lab Sample ID: D199663
Lab File ID: A112Q3K06
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1. 0
Number TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1. 60-29-3
COMPOUND NAME
ETHYL ETHER
l
! RT
1 1.67I
EST. CONC.
6.5
'•*
J
FORM
Page 43
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
EPA SAMPLE NO
X108
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: S.Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 19
Column: (pack/cap) CAP
Contract: Q97i?.snon7_
Case No.: REFINE SAS No.: SDG No.: D19965
Lab Sample ID: D199669
Lab File ID: A1120BK07
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/RG
74-87-3 Chloromethane74-83-9 Bromomethane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochloromethane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachlorc-:-r.ane_108-88-3 Toluene108-90-7 Chlorobenzenel"00-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
1212121261266666612661266666666612126666666
Q
'J;uo:u; uUuu10
uo
au:o;u1U10;u:u
;ui u;u!U10:u
FOPM I VOA 000020 I/
Page 44
ISVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE MO
X108
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5. Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 19
Column (pads/cap) CAP
Contract: 097125QDQ7
Case No.: REFINE SAS No.: SDG No.: D19966
Lab Sample ID: D1996p3
Lab File ID: All20Ryn7
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1. 0
Number TICs found: Q.CONCENTRATION DNITS:(ug/L or ug/Kg) DG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I V O A - T I C 000021 1 / 5'
Page 45
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
L-b Name: n.MNOlS EPAX109
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 16
Column: (pack/cap) CAP
Contract: 097125DQQ7
Case No.: REFINE SAS No.: SDG No.;
Lab Sample ID: Dl996?n
Lab File ID: A1121HK04
Date Received: 11/14/91
Date Analyzed: 11/21/91
Dilution Factor: 1.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG.
74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chlo roe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-C6-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate7 5 - 2 7 - 4 Bromodichlorome thane76-37-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1 , 1 , 2 , 2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
1212121261266666612661266666666612126666666
Q
UUuIU
IU!U:o!U!U!U
!U:u;o10i u:u;u;u;u!U!U10IUIU
uuiuiu
FORM I VOA000022
Page 46
ISVOLATILE ORGANICS ANALYSIS DATA SH2ST
TENTATIVELY IDENTIFIED COMPOUNDS
EPA 3A:l?"_Z S"
Lab Name: n.T.TNQTS EPAX109
Lab Code: SPFLD
Matrix: (soil/water) S_C_1L
Sample wt/vol:
Level: (low/med) LOW
Contract: 0971250007
Case No.: REFINE SAS No.: SDG No.: 019955
D1996TO
(g/mL)
% Moisture: not dec. Lfi.
Column (pack/cap) CAP
Lab Sample ID:
Lab File ID: A11215KQ4
Date Received: 11/14/9:
Date Analyzed: 11/21/91
Dilution Factor: 1.0
Number TICs found: Q_CONCENTRATION UNITS:(ug/L or ug/Kg) DG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. ; £ -
FORM I V O A - T I C
000023
Page 47
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ILLINOIS EPA Contract: Q97i25nnn?
SPA SAMPLE NO
X110
Lab Code: S_P_£LD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 5.Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 22
Column: (pack/cap) CAP
Lab Sample ID: D199671
Lab File ID: A112QBKn9
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION Ur-ITS:(ug/L or ug/Kg) UG/RG
74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1,2-Dichloroethcne (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichloromethane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloro«T.-.ene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2,2-Tetrachloroethane.108-38-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
1313131361366666613661366666666613136666666
1 UU•J:u:u:u:u
u
UU
uu:u:u;u:u!U
U
u:o:u
FORM I VOA000024
1/8'
Page 48
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE N'
X110
Lab Code: SPFLD
Matrix: (soil/water) S_Q_LL
Sample wt/vol: 5,_
Level: (low/med) LOW
, Contract: Q97125QQQ7
Case No.: REFINE SAS No.: SDG No.: 019966
(g/nL)
% Moisture: not dec. 22.
Column (pack/cap) CAP
Number TICs found: Q.
Lab Sample ID: D199671
Lab File ID: A112CER09
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1. 0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC OOC02-?
Page 49
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ILLINOIS EPA Contract: 0971250007
EPA SAMPLE Si
Xlll
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: Dl996n
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 15
Column: (pack/cap) CAP
Lab Sample ID: D1996R7
Lab File ID: B1119r.r!' A
Date Received: 11/15/31
Date Analyzed: 11/19/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
74-87-374-83-975-01-475-00-375-09-267-64-175_15_075-35-475-34-3KdO-^Q-O
67-66-3107-06-278-93-371-55-656-23-5108-05-475-27-473-37-510061-01-579-01-6124-48-179-00-571-43-21 nnfii -.n9-fi---75-25-2108-10-1591-78-6127-18-47Q_-ax_K
108-88-3108-90-7100-41-4100-42-51330-20-7
Chlorome thaneBromome thaneVinyl ChlorideChlo roe thaneMethylene ChlorideAcetoneCarbon Disulf ide1 1-Dichloroe thene1, 1-D ichloroethaneI O — rii/^Kl^^y^rtA^K^n^ / t" n "t* .a 1 i £i/icn.i.OiO*Jiinene v. total iChloroform1 . 2-Dichloroethane2-Butanone1 1 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane
- — 1 2 — Dichloropropane— -— cis-1, 3— Dichloropropene
Trichlo roe thene— — Dibromochloromethane
1 1 2-TrichloroethaneBenzenetrans i , *3 .ui.cn loropropeneBromof orm4-Methy 1-2-Pentanone2-HexanoneTetrachloroethene
i l)£|£ie&racn J-oroeunaneTolueneChlorobenzeneEthyl benzeneStyreneXvlene (total}
1212121225126664661219612666
106666612122666666
:u! U!U:u&U 4\ u!U;u;ui j!U;UI Ut
:u!U:u:u:u\
i ui U!U:u;u!U:uuiu!U:u:u:u', Ui
FORM I VOA
Page 50
LEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLTMQIS EPA Contract: Q9712500Q7
EPA SAMPLE
Xlll
Lab Code: S££LD_ Case No.: R£F_1N£ SAS No. : SDG No.: D19955
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med) LOW
(g/aL)
Lab Sample ID: D199682
Lab File ID: B1119LC14
% Moisture: not dec. 15
Column (pack/cap) CAP
Date Received: 11/15/91
Date Analyzed: 11/19/91
Dilution Factor: 1.Q
Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Rg) UG/RG
CAS NUMBER COMPOUND NAME PT EST. CONC. Q
FORM I VOA-TIC000027
1 /' 3 ?
Page 51
1AVOLATILE CRGANICS ANALYSIS DATA SHEET
L«o Name: ILLINOIS EPA
EPA SAMPLE NO
X112
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec.
Contract: 0971250007
Case No.: REFINE SAS No.: SDG No.: D199SQ
Lab Sample ID: D199683
Lab File ID: B112QLC:J4
Column: (pack/cap) CAP
CAS NO. COMPOUND
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: 1. 0
CONCENTRATION UNITS:(ug/L or ug/Xg) DG/KG
74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1,1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-3utanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroe thane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachloroethane_108-33-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
13131313111366666613661366676666613136666666
Q
;o:o!U;ut
io; o
U000o00ua:ui
iu;u:o
;o!0;u:u!D
FORM I VOA 000028
Page 52
ISVOLATILE CRGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Nan«: ILLINOIS EPA
EPA SAKF1S $
X112
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/ypl: 5.Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 21
Column (pack/cap) CAP
Contract: 0971250007
Case No.: REFINE SAS No.: SDG No.: D19966
Number TICs found:
Lab Sample ID: D199683
Lab File ID: B1120LCC4
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: 1. Q
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KQ
CAS NUMBER
1. 60-29-32.3.4.5.
f
i COMPOUND NAME
1 ETHYL ETHER! UNKNOWN! UNKNOWN1 UNKNOWN! UNKNOWNi
RT
1.8315.4216.1216.6917.92
EST. CONC.
6.7147.2
116. 1
Q
JJJJJ
FOPM I V O A - T I C000029
1/3'
Page 53
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
o Name: ILLINOIS EPA
Lab Code: SPFLD Case No.: REFINE
Matrix: (soil/water) SOIL
Sample wt/vol: 510 Cg/mL) G_
Level: (low/med) LOW
% Moisture: not dec. I5
Column: (pack/cap) CAP
Contract: 0971250007
SAS No.:
EPA SAMPLE N(
X113
SDG No,:
Lab Sample ID: D199634
Lab File ID: Bli2QLr:n
Date Received: 11/15/9"!
Date Analyzed: 11/20/91
Dilution Factor: 1. Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG-
74-87-3 Chloromethane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1, 2-Dichloroethene (total)_67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2- Bu t anone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride103-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-37-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene .124-43-1 Dibromochloromethane79-00-5 1, l, 2-Trichloroethan*71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene__75-2^-2 Bromoform108-10-1 4-Me thy 1-2-Pent anone591-73-6 2-Hexanone127-13-4 Tetrachloroethene79-34-5 1,1, 2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene-100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
121212121612666666
12661266hi
6
68612126666666
Q
UUUU
UU
.11UUUUUU
!U:u1 u:u
1 T;
;U
!UI ri
iuIU
:u:u
FORM I VOA OOO0301/3"
Page 54
ISVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE !>'(
X113
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 15
Column (pack/cap) CAP
Number TICs found:
Contract: 0971250007
Case No.: REFINE SAS No.: SDG No.: D1996S
D199684
3112CLC03
Lab Sample ID:
Lab File ID:
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 000031 1 / :
Page 55
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE SO
I Name: ILLINOIS EPA
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture; not dec. 20
Column: (pack/cap) CAP
_ Contract: 0971250007
Case No.: REFTNE SAS No.:
X114
No.:
Lab Sample ID: D199685
Lab File ID: B112QL(?ns
Date Received: 11/15/91
Date Analyzed: 11/20/9!
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION DNITS:(ug/L or ug/Kg) OG/KG
74-87-3 Chloromethane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroe thane75-9 3-3 2-Butanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichloromethane78-87-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-13-4 Tetrachloroethene79-34-5 1, l,2,2-Tetrachloroethane_103-88-3 Toluene108-90-7 Chlorobenzene100-41-4- Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
121212121012666666126612666666665121 i-L —6666666
Q
oo
Uu
;u:u;u;u:u:u;u:u:u;u;u
;u:u
uuUouu:u
FOPM I VOA000032
1/8
Page 56
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE
X114
Lab Code: 3PFLD
Matrix: (soil/water) S_Q_LL
Sample wt/vol:
Level: (low/med) LQJi
Contract: 0971250007
Case No.'- REFINE SAS No.: SDG No.: D19??6
D199635
(g/mL) B112QLC05
% Moisture: not dec. 20
Column (pack/cap) CAE—
Lab Sample ID:
Lab File ID:
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor-- 1. 0
Number TICs found: Q_CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. i~i.<* i
(
FORM I VGA-TIC
Page 57
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
Lab Code: SPFLD Case No.: REFTN5
Matrix: (soil/water) SOIL
Sample wt/vol: 5.Q (g/mL) G_
Level: (low/med) LOW
Contract: 0971250007
EPA SAMPLE NC
X115
SAS No. : SDG No.: D19956
Lab Sample ID: D
Lab File ID: B112QLCD6
% Moisture: not dec.
Column: (pack/cap) CAP
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: L. 0
CAS NO. COMPOUNDCONCENTRATION DNITS:(ug/L or ug/Kg) DG/KG
74-87-3 Chloromethane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride103-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-l,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Fentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenrene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (totalj
13131313161366656613861366676666613139666666
Q
ID!UIDIDI
ID! DIDi:J: J: o!D:Dii
:D:o;u:D:DID;D:DIDIDID!0iIDiDIDIDIDID
FOPM I VOA 0000341/87 Fe
Page 58
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
-O Name: ILLINOIS EPA
EPA SAMPLE NO
X115
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 21
Column (pack/cap) CAE
Contract: 097125QQQ7
Case No.: REFINE SAS No.: SDG No.: HL3_2££
Lab Sample ID: D199636
Lab File ID: B112QLCQ6
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: 1. 0
Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. ,— i<*
FOPM I VOA-TIC 000035
Page 59
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
EPA SAMPLE :;r
X116
Lab Code: SPFLD
Mat r ix : ( soi l /water) SJ1LL
Sample wt/vol :
Level: ( low/med)
. Contract: Q971250Q07
Case No.: B££IH2. SAS No.: SDG No.: D19956
(g/mL)
% Moisture: not dec. Lfi.
Column: (pack/cap) CAP
Lab Sample ID: D199687
Lab File ID: B1120LC09
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: 1. 0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
74-87-3 Chlorome thane74-83-9 Bromomethane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1 , 1 , 1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochlorome thane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoforo108-10-1 4-Methyl-2-Pentanone591-73-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4--- Ethylbenzene100-42-5 Styrene1330-20-7 Xylene ( to ta l )
12121212
666666
1266
12665.666666
1212
6666666
Q
! U: u: U! Ui
: u: u
: u;":a; u; u; u! U; u;u! U;u:u; u:u:ui ri
i u! U! U! U: u;u:u; u! U
FORM I VOA OOC036
Page 60
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
EPA SAMPLE SO
X116
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.Q (g/mL)
Level: (low/aed) LOW
% Moisture: not dec. 18
Column (pack/cap) CAP
Contract: 097125Qnn7
Case No.: REFINE SAS No.: SDG No.: DI9966
Lab Sample ID: 0199537
Lab File ID: B112QLCQ3
Date Received: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor; 1.0
Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. 3
FOPM I VGA-TIC 000037
Page 61
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
EPA SAMPLE
X117
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
X Moisture: not dec. 24
Column: (pack/cap) CAP
Contract: Q971250Q07
Case No.: REFINE SAS No.: SDG No.: D19986
Lab Sample ID: D199672
Lab File ID: A112QBK1G
Date Received: 11/14/91
Date Analyzed: 11/20/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
74-87-3 Ch lor ome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroethane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cie-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1, 1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
13131313IS247777771377
1377777777713137777777
Q
! U;u!U:ui
ITi U!U;u;u; u
:u!U:uIU;ui u!U:u;uiu;u:u:u!U:ui u:u;u!U;u!U
FORM I VOA
Page 62
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
1 > Name: ILLINOIS EPA
EPA SAMPLE NC
X117
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/ned) LOW
% Moisture: not dec. 24
Column (pack/cap) CAP
Contract: 097125QQQ7
Case No.: REFINE SAS No.: SDG No.: D19966
Lab Sample ID: D199672
Lab File ID: Al12QBE 10
Date Received: 11/14/91
Date Analyzed: 11/2Q/91
Dilution Factor: LJ1
Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I V G A - T I C 1,nnnmo
Page 63
1AVOLATILE OHGANICS ANALYSIS DATA SHEET
EPA SAMPLE NC
Lab Name: ILLINOIS FPA
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOH
% Moisture: not dec. 17
Column: (pack/cap) CAP
Contract: 0971250007
Case No.: BEJLLHi SAS No.: SDG No.
X118
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
A112DRK1
11/14/91
11/20/91
Dilution Factor-- 1. Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) OG/KG
74-87-3 Chlorome thane74-83-9 Bromo me thane75-01-4 Vinyl Chloride75-00-3 Chlo roe thane75-09-2 Kethylene Chloride67-64- 1 Acetone75- 15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66- 3 Chloroform107-06-2 1, 2-DichloroethaneT 3-93-3 2-3utanone71-55-6 1,1, 1-Trichlo roe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1, l,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene10 0-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)
1212121214126666661266126661066666121259666666
uou
u
;ui
i u:u:ui u;uiu:ui
iu;u; u:u;u;u
FORM i VOA
Page 64
IEVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
3 Name: ILLINOIS EPA
SPA SAMPLE SO
X118
Lab Code: SPFLD
Matrix: (soil/water)
Sample wt/vol:
Level: (low/rned; LOW
% Moisture: not dec. 1
Contract: Q97i?5pnn7
Case No.: REFINE SAS No.: SDG No.:
(g/mL)
Lab Sample ID- D199571
Lab File ID: All COBS'
Column pack/cap) CAP
Date Received: 11 -• 14 / 9 1
Date Analyzed: 11/20/9 1
Dilution Factor: 1 . 'J
Nur.ber TICs found:CONCENTRATION UNITS:(ug/L or ug/Rg) UG/KG
CAS NUMBER
1. 60-29-3
COMPOUND NAME
ETHYL ETHER
RT
1.67
EST. CCNC.
8.2
Q
J
FORM I VOA-TIC 000041
Page 65
3IMI VOLATILE ORGAN ICS ANALYSIS 3ATA SHEET
Lab Name: TT.LTNQIS EPAX101
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 31.0 (g/mL)
Level: (low/med) LOW
X Moisture: not dec. 46 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) I pH:
Contract: Q9712500Q7 ;
Case No.: EE£ULB SAS No.: SDG No.: D19966
Lab Sample ID: D199675
Lab File ID: C12Q3W10
7.9
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UQ/XG Q
n i A A A^ qq q _
Q j- c 7 p
541-73-1X >J W T O '
100-51-6xJ w) W v .L
S5-4S-7i AQ CA i1UO DO _
106-44-5* O 1 r .4 7Oil i — On '
67-72-1QO _QR t1
70 =.q i _1 O O3 1a Q ~7 ~ c.Bo- ,'O-0105 57 9 -65-85-0i i 1 qi i120-33-2120-82-191-20-3106-47-887-68-359-50 7-91-57-677 47_4_88-06-295-95 4-
88-74 4 — -131-11-3208-96-8606-20-2 --
— — fneno i.i • / o f*, 1 , i INfftV.— — — Disi . — nj-oroeLnyi j n tnero r < v t v i— z umoropneno± _1 r 3— Dichlorobenzene
— — — 1 T 4— DichlorobenzeneBenzyl Alcohol
- — 1 . 2— Dichlorobenzene ..2 -Methyl phenol
— _ Xi^fO.. r*l^T/-NT»/^-l— T-N'»^/-\T-,»*''iIr*-U^»%— o i s i.~ L/n J, o ro . oopropy - j iT-ner4-Methvlohenol
- — N— Ni t rosw— D i n-Prcp/ . mi neHe xachloro ethaneLl X Li X LJ R 1 1 C 1 1 c
T U— — i sopnorone _. _ _-witrophenol ,
2 t 4 — Dimethyl phenolBenzoic Acid
2 , 4— Dichloropheno 1
Naphthalene
Hexachlorobutadiene
2— Me thy 1 naphthalene
2 4 T 6— Trichlorophenol
2 -N it roan i 1 ineDime thy IphfchalateAc en a ph thy lene2 6— Din i, t ro to luene
1 r\r\l^iUU5 o r\ r\l^UU1 O/^Al^UU12001 OAA1-iUU12001 OPiAl^UU120C1 OA/*"^1^ JU
12001 O/"l Al^UU1 200T or\r\I^UU1 OAP)UUUx200120057001 90O1200120031012001200120012001 ?0012005700i onol^UU
5700120012001200
li r Ti *Ji r Ti Ui r T, U1 ni r T) 1Ui r ii U• r Ti r i
1 T I
( 1 Ui r T, Ui r •)i U
i U' U1 U1 ni >J1 U1 U; J!U;u1 U!U1 U1 VJ
;u', U1 n;u!U!U:u
FORM I SV-1
000042
Page 66
1CSEMIVOLATILE ORGANICS^ANALYSIS DATA SHEET
I? A SAJ1PL3 NO
L,ab Name: T T . r . T N Q T S RPA Contract: 0971250007X101
Code: SPFT.D Case No.: REFINE SAS No.: SDG No.: D1S566
Matrix: (soil/water) SQTL
Sample wt/vol: 31.Q (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 46 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) £_ pH: 7.9
Lab Sample ID: D199679
Lab File ID: C12Q3W10
Date Received: 11/15/9T_
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene34-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol.35-30-6 N-Nitrosodiphenylamine (1).101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol35-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(1.2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene
57001200570057001200120012001200120057005700120012001200570054012001200630500120024001200120012001200120012001200120012001200
Q
:u;u:u;u;u;u;u;u
;u:uI T TI ^
!J:u;u!J!J:u!U;u!U:u:uiu:u!U;u;u:u
(1) - Cannot be separated from Diphenylamine
FORM I SV-2000043
Page 67
IFSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHZZT
TENTATIVELY IDENTIFIED COMPOUNDS
,ah NAm«: ILLINOIS EPA
.a_ Coda: SPFLD Case No. :
Matrix: f Boil/water 1 SOIL
Sample wt/vol: 31.0 (g
Level: (
S Moisture:
Extraction:
3PC Cleanup
Dumber TICs
low/me d) LOW
not dec. 46
(SepF/Cont/Sonc)
: (Y/N) I
found: 20
t
CAS NUMBER I
1.2.3.4.c.
e!•7a
9.10.11.12.13.14.15.16.17.18.19.20.
! UN KNOWN1 UNKNOWN! UN KNOWN1 UNKNOWN; UNKNOWN; UNKNOWN; UN KNOWN: UNKNOWN! UNKNOWN; UNKNOWN; UN KNOWNi UNKNOWNi UNKNOWN; UN KNOWN! UNKNOWNi UNKNOWNi UNKNOWN! UN KNOWN1 UN KNOWN[UNKNOWNl
X101Contract: 0971250007
REFINE SAS No.: SDG No.! m996fi
Lab Samcle ID: D1996^3
/mL) G Lab File ID: C1203W10
Date Received: 11/15/91
dec. Date Extracted: 11/15/91
SOJiC Date Analyzed: 12/03/91
pH: 7.9 Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
COMPOUND NAME
ALIP
ALIP
ALIP
ALIPALIPALIPALIP
ALIPALIP
. HYDROCARBON
. HYDROCARBON
. HYDROCARBON
. HYDROCARBON
. HYDROCARBON
. HYDROCARBON
. HYDROCARBON
. HYDROCARBON
. HYDROCARBON
RT
27.5627.7727.8423.0123.0223.0728.1428.3128.5428.5928.8128.8929.0129.0429.6630.8231.0931.4231.7131.84
EST. CCNC.
1900740960120044024001200180013001100200075016004102200130010005201500780
3 :
jJ ;T
T
J
J
"
**
.J
J
T
u7
JT
7
JJJT
FORM I SV-TIC
000044
Page 68
13SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAKPLZ SC.
Lab Name: TLLINQTS EPAX102
Lau Code: SPFLD
Matrix: (3oil/water) SOIL
Sample wt/vol: 30.6 (g/nxL) G
Level: (low/med) LOW
% Moisture: not dec. 42 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y pH:
Contract: Q9712SQQQ7
Case No.: REPINE SAS No.: SDG No. : D19966
Lab Sample ID: D199679
Lab File ID: C12Q3W11
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 b is (2-Chloroe thy 1) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1, 2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 Ms(2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bi s (2-Chloroethoxy) Methane120-83-2 2, 4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene___:88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2, 6-Dinitrotoluene
110011001100110011001100110011001100110011001100110011001100110054001100110011001100110011001100110011001100540011005400110011001100
FORM I SV-1
Q
;u:u!U!U!U:u;u:u;u;u;u;ui u;u!U:uiu;u;u:u!U:u!U:u;u!U:u!U:u:u:u:u;u
1/87 Re-
000045
Page 69
SEMIVOLATILE ORGANIC3 ANALYSIS DATA SHEET2?A SAM?12 SC
Lab Name: ILLINOIS EPA Contract: 09712SQQO7X102
Lab Code: SPFLD Case No. : REFINE SAS No. :
Matrix: (soil/water) SOIL _
Sample wt/vol: 30-6 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 42 dec.
Extraction: (SepF/Cont/Sonc) SQH£
GPC Cleanup: (Y/N) Y. pH:
SDG No.: 019966
Lab Sample ID: D199679
Lab File ID: C12Q3W11
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) US/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dini tro toluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4 ,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene8'-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 BenzoCg.h , i )Perylene
5400110054005400110011001100110011005400540011001100110054001100110011002601100110022001100110011001100110011001100110011001100
Q
u;u;u;u;u;u:u
:u;u!U:u!U:u:u!U:u!J!U:u;u:u;u;u!U!U:u!U;u:u;u
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 000046
Page 70
IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SPA SAM?L& NO
Lab Name: TLLINQTS EPA Contract: 0971950007X102
Code: SPFLD Case No.: REFTNE SAS No.: SDG No.: D19966
Matrix: (ooil/water) SOIL
Sample wt/vol: 30.6 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 42. dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH: 7.3
Number TICs found: 2Q
Lab Sample ID: D199679
Lab File ID: C12Q3WT1
Date Received: 11/15/31
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3. 100-52-74.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.
l
! COMPOUND NAME
; UNKNOWN; UNKNOWNi BENZALDEHYDE; UNKNOWN; UN KNOWN PHTHALATEI UNKNOWN ALIP. HYDROCARBONI UNKNOWN'.UNKNOWN[UNKNOWN ALIP. HYDROCARBON; UNKNOWN! UNKNOWN! UNKNOWN1 UNKNOWN! UNKNOWN! UNKNOWN1 UNKNOWN! UNKNOWN! UNKNOWN! UN KNOWN[UNKNOWNI
RT
9.5410.2010.5511.0923.7526.7127.1927.5629.6631.4131.5932.9633.6933.7134.6634.7635.3635.8438.2740.17
EST. CONC.
3800440022001400730660530800120012006208900210011006801000270064016001100
; a!BAJ:AJ!J!AJ; j: Jp Ti '-'
;JI T1 •-<
;j;jp Ti w
:J; J!Ju;ji TI u
IJ
!J!
FORM I SV-TIC
000047
Page 71
13SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA £AM?LZ NC
Lab Name: Tr.r.TNQIS EPA Contract: Q97125QQQ7X103
Lab Code: SPFLD Case No. : EEJEIM SAS No . : SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 3.Q.3 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 40 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y pH: 7.8
Lab Sample ID: D19968Q
Lab File ID: C1204W03
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1, 4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether.106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine_67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2 , 4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane_120-33-2 2,4-Dichlorophenol120-32-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2, 4 , 6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene
11001100110011001100110011001100110011001100110011001100110011005300110011001100650110011001100180011001100530011005300110011001100
FORM I SV-1
Q
;u:u;u;u!U;u;ui M, w
!U;u!U:u!U;u:u;u:u;u:u;uu:u;u:ut
:u;uIU;u;uiu;u;u
000048
Page 72
1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SrA SAM? 12
Lab Name: ILLINOIS EPA Contract: Q97125QQQ7X103
Lao Code: SPFLD Case No.: REFTNB SAS No.: SDG No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.3 (g/mL)
Level: (low/med) LOW
X Moisture: not dec. 4p dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) £ pH: 7.B
Lab Sample ID: D19968Q
Lab File ID: C1204WQ3
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitro toluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3*-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Be nzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-33-5 Indeno(l,2,3-cd)Pyrene53-70-3 DibenzC a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene
530011005300530011001100110011001100530053001100110011005300880liOO11001000710110022001100110011001100110011001100110011001100
Q
:u!U1U:u!U!U!U:uI TlI ^<
:u;u:u;u;u;u!J;u:uu;j:u:u;u;u:u:u:u!Uiu:u;uiu
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 OC0049
Page 73
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
ErA 3AM?12 N.
X103
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.3 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 40 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y. pH:
Number TICs found: ,19
Contract: 0971250007
Case No.: REFINE SAS No.: SDG No.: D19966
Lab Sample ID: D199680
Lab File ID: C12Q4WQ3
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: l.Q
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3.4.5.6.7.3.9.10.11.12.13.14.15.IS.17.18.19.
(
[ COMPOUND NAME
1 UNKNOWN ALIP.J UNKNOWN! UNKNOWN1 UN KNOWN; UNKNOWN ALIP.1 UNKNOWNi UNKNOWN; UN KNOWN ALIP.; UN KNOWN1 UNKNOWN ALIP.[UNKNOWN; UNKNOWN! UNKNOWN ALIP.! UN KNOWN! UNKNOWN[UNKNOWN ALIP.[UNKNOWN! UNKNOWN[UNKNOWN ALIP.I
HYDROCARBON
HYDROCARBON
HYDROCARBON
HYDROCARBON
HYDROCARBON
HYDROCARBON
HYDROCARBON
RT
27.8628.0928.1728.4928.7628.9729.3929.6129.9130.4730.7730.9631.4231.6631.7932.5432.9133.5133.74
EST. CONC.
3300100012001800440095080050002200290017001700260080023001300410023003700
i •— .j
; Q
!J!J: Ji Ti tJ
i Ti »-'
, u
: J: j; J: j!J;j;J;j;J!J;j[J;j
FORM I SV-TIC
000050
/o 7 ~ =.- •/ w ' . .2 -
Page 74
SEMIVOLATILE ORGANiCS ARAL*513 DATA SHE2T
Lab Name: Jt.T.TNnrs EPA Contract: Q97125QQQ7X104
Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19956
Matrix: (soil/water) SOIL
Sample vrt/vol: 30.2 (g/mL)
Level: ( low/med) LOW
% Moisture: not dec. 20 dec.
Extraction: ( SepF/Cont/Sonc )
GfJ Cleanup: ( Y / N ) Y. _ pH:
CAS NO. COMPOUND
Lab Sample ID: D199681
Lab File ID: C12Q3W13
8.6
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg)
108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-I'ichlorobenzene95-48-7 2-Methylphenol
60-1 bis(2-Chloroisopropyl)Ethei44-5 4-Methylphenol
621-64-7 N-Nitroso-Di-n-Propylamine_67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane.120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene.106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene_88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene
820820820820820820820820820820820820820820820820400082082082082082082082082082082040008204000820820820
Q
!U!UiU;u;u:u;u:u:u:u!U:u!U:u;u;u!U;u:uIU:u;u:u!UiU;u:u:u•!U!U;u!U
FORM I SV-1 1/87 ?. = •
000051
Page 75
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHZZTS?A SAM?12 .r
Lab Name: ILLINOIS EPAX104
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) £
Level: (low/med) LOW
% Moisture: not dec. 2Q dec.
Extraction: (SepF/Cont/Sonc) S_QUC
GPC Cleanup: (Y/N) X pH: 8.6
Contract: 0971250007
Case No.: EEEIHE SAS No.: SDG No.: D19266
Lab Sample ID: D1996S1
Lab File ID: C12Q3W13
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) US/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol.100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-284-66-27005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene
•2,4-Dinitrotoluene.-Diethylphthalate
•Pentachlorophenol.-Phenanthrene-Anthracene
100-10-6 4-Nitroaniline534-52-1 4, 6-Dinitro-2-Methy 1 phenol.86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-585-01-8120-12-784-74-2 Di-n-Butylphthalate.206-44-0 Fluoranthene129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-0
-Pyrene-Butylbenzylphthalate-3,3'-Dichlorobenzidine.-Benzo(a)Anthracene-Chrysene.bis(2-Ethylhexyl)Phthalate_Di-n-Octyl Phthalate
205-99-2 Benzo(b)Fluoranthene .207-08-9 Benzo (k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno( 1,2,3-cd)Pyrene53-70-3 Dibenzt a, h) Anthracene191-24-2 Benzo( g,h, i )Perylene
4000820400040008208208208208204000400082082082040008208208208201808201600820820820820820820820820820820
Q
;u;u:u;u;u:u;u;u;u;u;u;u!UIU:u:u:uIU!U;j!Uiu!U:u!U!U:u:u:uiu:u:u
(I) - Cannot be separated from Diphenylamine
FORM I SV-2 000052
Page 76
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPAX104
T 5 Code: SPFLD Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 2Q dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y_ pH: 8.6
Number TICs found: I
Contract: 0971250007
SAS No. : SDG No. : D19966
Lab Sample ID: D1996fll
Lab File ID: C12Q3W13
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3.4.5. 100-52-76.7.
1
i COMPOUND NAME
[UNKNOWN ALIP.; UNKNOWN ALIP..UNKNOWN1 UN KNOWN; BENZALDEHYDE; UN KNOWN[UNKNOWN ALIP.i
HYDROCARBONHYDROCARBON
HYDROCARBON
RT
8.428,599.5710.2210.5511.1021.77
EST. CONC.
810710310013001800690570
t
i Q
!JU! BAJ! AJ:J;AJ! J
FORM I SV-TIC
000053
1/87 p.e
Page 77
IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: Tf.r.TNQTS EPA Contract: 097125QQQ7X105
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL.
Sample wt/vol: 30.J
Level: (low/med) LOW
% Moisture: not dec. 14
(g/mL)
dec.
Lab Sample ID: D199666
Lab File ID: C1202W04
Date Received: 11/14/91
Date Extracted: 11/15/91
Extraction: (SepF/Cont/Sonc) SO.UC
GPC Cleanup: (Y/N) Y. pH: 6.6
Date Analyzed: 12/02/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis (2-Chloroethoxy) Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 2, 6-Dinitrotoluene
760760760760760760760760760760760760760760760760370076076076076076076076076076076037007603700760760760
FORM I SV-1
;u;u;u;u!U:u:u;u:u!U; u:u:u:u;u:u;u;u;u;u!U:u;u:u!U:ui u!U!U;u;u:u;u
0000541/5'
Page 78
SEMI VOLATILE ORGAN ICS ANALYSIS DATA SHZST
Lab Name: ILLINOIS EPA Contract: 0971250QQ7X105
> Code: SPFLT) Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (eoil/water) SQTL
Sample wt/vol: 30.1 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 14 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) X pH: 6.6
Lab Sample ID: D19966K
Lab File ID: C12Q2WQ4
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) Q
99-09-283-32-951-28 5100-02-7132-64-9121-14-284-66-27005 72 3 - -86-73-7100-10-6R04_CO_ 1JO^l lj£ 1PC QA (S_
i ni -c.R-'s _.iw i. — sJO — O1 1 R 7d- 11 1O / n — I87 86-5-QC A 1 _fl _.acjui — a —120-12-734-74-2206-44-0129-00-085-68 7 —91-94-1 -56-55-3218-01-9i i 7 — a i 7 .
117-84-0205-99-2207-08 950-32-8193-39-553-70-3 — —191-24-2
3-Ni troanilineAcenaphthene
4-NitrophenolDibenzofuran2 , 4-Dinitro tolueneDiethylphthalate
Fluorene4 -Ni troaniline, D— JJinj.ur'o— £.— ne iny xpneno ±M i. LruBuu ipricny io-uunc ^ j. i
— oromopneny j. — pnen v j.e uner— — Hexach 1 orobenzene __
Pentachlorophenol— r'nenancnrene ... ......AnthraceneDi-n-ButylphthalateFluoranthenePyrene
Benzo( a ) AnthraceneChryaeneV>1a/C> tTi-V<w1 Viavtrl ^PVit-V>a 1 a+-o
Di-n-Octyl Phthalate
Ben2O( k )FluorantheneBenzo( a )PyreneTndeno(l 2 3-cd)Pyrene
— Dibenzfa h)AnthraceneRen2:o(g,h i)Perylene
3700760370037007607607607607603700-3700o / uu7fiO7 er\/ ou7AOf o\l37007fin/ Dv
76076019019076015007607607 (3 AI DVJ
760760760760760760760
i
1 U;U'U;Um!U:u1 ni ^:u;U1 ni Ui n1 n( Ui rii u!UP MI U
!U'U! J! J!U!U:u:ui ni u;U:u;u:u;U!U;Ut
m |
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 000055 1/87 He-
Page 79
IFSEMIVCLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
i?A 5AMP1Z
Lab Name: Tr.LINQIS EPAX105
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 14 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y pH: 6.6
Number TICs found: Q.
Contract: Q971250QQ7
Case No. : REFINE SAS No. : SDG No. : D-19_9_£fi
Lab Sample ID: D199666
Lab File ID: C12Q2WG4
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS(ug/L or ug/Kg)
CAS NUMBER
1.2.3.4.5.6.7.8.
l
i COMPOUND NAME
; UNKNOWNi UNKNOWN! UNKNOWN1 UNKNOWN PHTHALATE1CHLORDANE ISOMERICHLORDANE ISOMER;CHLORDANE ISOMER; UNKNOWN ALIP. HYDROCARBON
RT
9.5410.1911.0723.7526.6927.0127.0933.87
EST. CONC.
14004806105609201000410590
Q
BAJBAJBAJTuJuT
rJ
FORM I SV-TIC
0000561/5-
Page 80
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA Contract: 0971250007X106
Code: SJPFLD Case No.: REPINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL)
Level: (low/med) LOW
Lab Sample ID: D199667
Lab File ID: C12Q2WQR
Moisture: not dec. 24 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y. pH: 6.7
Date Received: 11/14/9 ]_
Date Extracted: 11/15/9]
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1, 3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-43-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol ,__91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene ,606-20-2 2,6-Dinitrotoluene
870870870870870870870870870870870870870870870870420087087087087087087087087087087042008704200870870870
FORM I SV-1
Q
!U!U:u!U!U!U:u;u;u:u!U1U!U!UI U!U:u:u;u:ui u!U;u:u:u!U;u:u:u:u;u;u;u
0000571/87 Re
Page 81
1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: ILLINOIS EPA Contract: 097125QQQ7X106
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30 -Q (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 24 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) £ pH: 6.7
Lab Sample ID: D199667
Lab File ID: C1202W05
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2, 4-Dini trophenol100-02-7 4-Ni trophenol132-64-9 Dibenzofuran121-14-2 2, 4-Dinitrotoluene
70C5-72-3 4-Chlorophenyl-phenyletner_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4, 6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene
206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz(a,h
24-2 Benzo(g,h,:
4200870420042008708708708708704200420087087087042001000870870120011008701700870510870870470410430870870870
Q
u:u:u;u;u:u
;u;ui r Ti ^:u;u!U!Ui
iu;u
:u!U!U!J!UiUiJ!J;j!U:u!U
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 000058
Page 82
IrSEMI VOLATILE ORGANICS" ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS EPA
L Code: SPFLD Case No.: REFINE
X106Contract: 0971250007
SAS No. : SDG No. : D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) Q
Level: (low/med) LOW
% Mois*«ure: not dec. 24 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y. pH: 6.7
Number TICs found: Z
Lab Sample ID: D199667
Lab File ID: C12Q2WQfi
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) US/KG
CAS NUMBER
1.2.3.4.cw .
6.7. 205-82-3
l
! COMPOUND NAME
! UN KNOWN ALIP. HYDROCARBON; UNKNOWN! UNKNOWN! UN KNOWN[UNKNOWN PHTHALATE1 UNKNOWN ALIP. HYDROCARBON! BEN ZO [ J ] FLUORANTHENE
RT
8.599.5510.2011.0923.7733.8934.81
EST. CONC.
52020004906706201300530
l
! Q
: j!BAJ!BAJ: BAJ; J;BJ;j
FORM I SV-TIC 1/87 p.e
000059
Page 83
13SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA 3AT.PL2 NC
Lab Name: T T . T . T N O T S EPA Contract: Q97125QQO7X107
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 16 dec.
Extraction: (SepF/Cont/Sonc) SQ_t!£
GPC Cleanup: (Y/N) X pH: 7.3
Lab Sample ID: D19966S
Lab File ID: C1202WOfi
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis (2-Chloroe thy 1) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1, 4-Bichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis (2-Chloroethoxy) Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 ' 2,6-Dinitrotoluene
790790790790790790790790790790790790790790790790380079079079079079079079079079079038007903800790790790
Q
:u!U;u!U:u!U;u;u;u;u:u!U:u:u1U;u:u;u!U:u:u;u;u:u;u;u;u;u;u:u;u:u;u
FORM I SV-1 1/67
OOC060
Page 84
SEMIVOLATILE ORGAN ICS ANALYSIS DATA 5HZ2T
Lab Name: TT.LINQIS EPA
I C.-de: SPFLD Case No.: REPINE
X107Contract: 0971250007
SAS No.: SDG No.: D199fifi
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 16 dec.
Extraction: (SepF/Cont/Sonc) SQJI£
GPC Cleanup: (Y/N) Y. pH:
CAS NO. COMPOUND
Lab Sample ID: D19966S
Lab File ID: C1202WQ6
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitro toluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenyl ether.86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol.86-30-6 N-Nitrosodiphenylamine (1).101-55-3 4-Bromophenyl-phenyiether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3*-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k) Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indenod, 2,3-cd) Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene
3800790380038007907907907907903800380079079079038007907907907907907901600790790790790790790790790790790
Q
!U!U,'U;u;u;u;u:u:u;u:u:u;u:u;u!U;u:u:u!U:u;u:u;u:u!U;u!U!U:u!U!U
(1)"- Cannot be separated from Diphenylamine
FORM I SV-: 000061 1/S7 ?.e
Page 85
=ah!VOLATILE ORGAN ICS ANALYSIS DATA S"ri2ETTENTATIVELY IDENTIFIED COMPOUNDS
X107Lab Name: TT.LINQTS EPA Contract: Q97125QQQ7
Lab Code: 5PFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. Ifi dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) X pH: 7.3
Number TICs found:
Lab Sample ID: D19966S
Lab File ID: C1202WQ6
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3.4.5.
t
,' COMPOUND NAME
i UNKNOWN ALIP. HYDROCARBON1 UNKNOWN ALIP. HYDROCARBON; UNKNOWN! UNKNOWN[UNKNOWN PHTHALATE
RT
8.428.609.5711.1023.79
EST. CONC. i Q
570 iJ470 ! J2000 ;J610 : j520 ; J
FORM I SV-TIC 1/S7 Rev.
000062
Page 86
SEMIVOLATIL2 ORGANICS ANALYSIS DATA SHEET
Lab Name: TT.LINQIS EPAX108
I Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 13. dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH: 6.9
Contract: Q97125QQQ7 ;
Case No.: REPINE SAS No.: SDG No.: D199fifi
Lab Sample ID: D199669
Lab File ID: C12Q2WQ7
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/~ or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene
810810810810810810810810810810810810810810810810400081081081081081081081081081081040008104000810810810
Q
!U;u!U;u;u;u;u:u;u!U;u!UIU:u;u!U;u;u:u:uIU:u:u!U:u:u:u!U:u:uI U:u:u
FORM I SV-1
000063l/S'
Page 87
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET£rA NO.
Lab Name: ILLINOIS EPAX108
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 19 dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH: 6.9
Contract: Q97125QQQ7
Case No. : REFINE SAS No. : SDG No. :
Lab Sample ID: D199669
Lab File ID: C12Q2WQ7
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) DG/KQ
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran
84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo (b)Fluoranthene207-08-9 Benzo (k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene
24-2 BensoCg.h, i )Perylene
400081040004000810810810810810400040008108108104000930810810120012008101600810600810810500510540430810500
Q
:uIU;u;u;u;u:u:u!U;u:u;u!U!U!Ui
;u!UI
iT!U:u!U!J:u;u
!J:u
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 O00064 1/3" =ev.
Page 88
IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SAMPLE SO.
Lab Name: ILLINOIS EPAX108
. o Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) G
Level: (low/med) LOW
3» Moisture: not dec. 19 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y pH: 6.9
Number TICs found: a
Contract: Q97125QQ07
Case No.: REFINq SAS No.: SDG No.: D19966
Lab Sample ID: D199669
Lab File ID: C12Q2WQ7
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3.4.5.6.7. 205-82-38.
l
i COMPOUND NAME
; UNKNOWN ALIP. HYDROCARBON! UNKNOWN! UN KNOWN1 UNKNOWN[UNKNOWN PHTHALATE! UNKNOWN ALIP. HYDROCARBONi BENZO [ J ] FLUORANTHENEI UNKNOWN ALIP. HYDROCARBONi
RT
8.609.5710.2211.1023.7933.9134.8437.36
EST. CONG.
4401800570620530
1400730850
l
: Q;j!BAJ!BAJ!BAJ!J;j!J!J<
FORM I SV-TIC 1/87
000065
Page 89
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETir A iAXr _£.
Lab Name: ILLINOIS EPAX109
. a Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 16 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) X pH:
Contract: Q97125QQQ7
Case No.: REFINE SAS No.: SDG No.: D19966
Lab Sample ID: D199670
Lab File ID: C1202WOft
7.3
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
108-95-2 Phenol111-44-4 bis(2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether.106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine_67-72-1 Hexachloroethane^98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane_120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene •106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene
790790790790790790790790790790790790790790790790380079079079079079079079079079079038007903800790790790
Q
!U;u;u;u:u!U;u:u!U:u!U;u;u!U:u:uIU;u:u:u:u!U:u;u:u
!U;u:u;u;u!U
FORM I SV-1 1/87 Re-
000066
Page 90
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETirA SArtrLS SO
Lab Name: ILLINOIS EPA Contract: Q97125QQQ7X109
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (aoil/water) SOIL
Sample wt/vcl: 30.0 (g/mL) fi
Level: (low/med) LOW
% Moisture: not dec. Lfi dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y. pH: 7.3
Lab Sample ID: D19967Q
Lab File ID: C1202WQR
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
99-09-2 3-Nitroaniline '83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo (a) Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz(a,h)Anthracene191-24-2 Benso(g,h,i)Perylene
3800790380038007907907907907903800380079079079038007907907907907907901600790790790790790790790790790790
Q
;u:uiu;u!U!U;uiu;u:u;uiUIU:u:u!U:uiU;u:u!U!U:u:u!U:u!U:u!U:u;u!U
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 000067 i//p-7
Page 91
SZHIVOLATILE ORGANICS ANALYSIS DATA STENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: TLLINQIS EPAX109
T i Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 16, dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: ( Y / N ) I pH:
Number TICs found:
Contract: Q97125QOO7
Case No. : REFINE SAS No. : SDG No. : D19966
Lab Sample ID: D199670
Lab File ID: C12Q2WQ8
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
1
CAS NUMBER
1.2.3.4.5.
11
l
! UNKNOWN! UNKNOWN! UNKNOWN! UN KNOWN! UNKNOWN
COMPOUND NAME
ALIP. HYDROCARBON
PHTHALATE
RT
8.609.5710.2211.1023.79
EST. CONC.
5902100870690510
; Q
!JIBAJiBAJ;BAJ;j
FORM I SV-TIC 1/87 P.ev
000068
Page 92
IBIIVOLATILE ORGAfllCS ANALYSIS DATA SHEET
EPA SAMPLE SO,
Lab Name: Tr r .TMQTS EPA Contract: 0971250007X110
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 22. dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y. pH: 7.0
Lab Sample ID: D199671
Lab File ID: C12Q2WQ9
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1, 4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol
65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichiorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene
850850850850850850850850850850850850850850850850410085085085085085085085085085085041008504100850850850
FORM I SV-1
Q
:u:u;u;u;u!U:u!U:u:u;u;u:u:u!U;u:u:u;u!U!U;u:u:u:u:u:u!U:u:u!U!U:u
1/37 Rev,
000069
Page 93
1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SPA SAHFL3 NO,
Lab Name: ILLINOIS RPAX110
o Code: SPFLD
Matrix: (soil/water) SQTL
Sample wt/vol: 30.Q (g/mL) Q
Leve1: (low/med) LOW
% Moisture: not dec. 22 dec.
extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y__ pH: 7.Q
Contract: Q97125QQQ7
Case No.: REFIMg SAS No.: SDG No.: £19966
Lab Sample ID: D199671
Lab File ID: C12Q2WQ9
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) Q
-3-Nitroaniline.-Acenaphthene
99-09-283-32-951-28-5 2,4-Dini trophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-284-66-2
2,4-Dinitrotoluene.Diethylphthalate
72-3 4-Chl or ophenyl-phenyl ether.86-73-7 Fluorene100-10-6
2-1L-Nitroaniline.
-Anthracene-Di-n-Butylphthalate.-Fluoranthene-Pyrene
4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1).101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-0205-99-2207-08-950-32-8193-39-5
•Butylbenzylphthalate-3,3*-Dichlorobenzidine_- Benzo(a)Anthracene-Chrysene-bie(2-]-Di-n-Octyl Phthalate.-Benzo(b)Fluoranthene.-Benzo(k)Fluoranthene.-Benzo(a)Pyrene
53-70-3-191-24-2-
-Indeno(1,2,3-cd)Pyrene.-Dibenz(a,h)Anthracene-Benzo(g,h,i)Perylene
410085041004100850850850850
41004100
85041008508508502101808501700850850850850850850850850850850
!U!U:u:u;u;u:u:u
iu!U;u:u;u!J
iu:u:uiuI M
:u:u:u:u:u:u!U
(1) - Cannot be separated from Diphenylamine
FORM I SV-2000070
1/87 Re-
Page 94
IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE SO
Lab Name: T T.LI NO IS EPAX110
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) Q
Level: (low/med) LOW
X Moisture: not dec. 22 dec.
Extraction: (SepF/Cont/Sonc) SQHC
GPC Cleanup: (Y/N) Y__ pH: 7.Q
Number TICs found: Z
Contract: 0971250007
Case No.: REFtN% SAS No. : SDG No. : D199S6
Lab Sample ID: D19967]
Lab File ID: C1202WQ9
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS(ug/L or ug/Kg)
CAS NUMBER
1.2.3.4.5.6.7.
i COMPOUND NAME
1 UNKNOWN ALIP. HYDROCARBON! UNKNOWN! UNKNOWN[UNKNOWN PHTHALATE1 UN KNOWN! UNKNOWN ALIP. HYDROCARBON.UNKNOWN ALIP. HYDROCARBON
RT
8.609.5910.2423.8033.1933.9437.39
EST. CONC.
4901800670520940800950
rI
! Q
!J!BAJ!BAJ; j!J; j; J
FORM I SV-TIC000071
1/87 Re-
Page 95
IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAhPLS MO.
Lab Name: TT.TJNQIS SPA Contract: Q97125QQQ7Xlll
SDG No.: D19_966. b Code: SPFLD Case No.: REPINff SAS No.:
Matrix: (soil/water) SOIL Lab Sample ID: D199682
Sample wt/vol: 30-7 (g/mL) Q Lab File ID: C1203W14
Level: (low/med) LOW Date Received: 11/15/91
% Moisture: not dec. 15. dec. Date Extracted: 11/15/91
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N)
SQNC
7.2
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl )Ether106---? f 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane_98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenc;65-85-0 Benzoic Acid111-91-1 bia(2-Chloroethoxy)Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol '95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene
760760760760760760760760760760760760760760760760370076076076076076076076076076076037007603700760760760
FORM I SV-1
Q
:u!U!U!U;u!U!U!U:u:u:u:u;u!U!U:uiu:u:u:uiu:u!U:u!U:uiu:u!U!U!U!U!U
000072
Page 96
SSMIVOLATILE ORGANICS ANALYSIS DATA SHZST
Lab Name: TLLINQIS EPA Contract: Q97125QQQ7Xlll
Lab Code: SPFLD Case No.: REPINE SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.7 (g/nxL) G
Level: (low/med) LOW
% Moisture: not dec. 15 dec.
SDG No.: D19966
Lab Sample ID: D199682
Lab File ID: C12Q3W14
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH: 7.2
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene___193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibens(a,h) Anthracene191-24-2 Benzo(g,h, i)Perylene
3700760370037007607607607607603700370076076076037001300300760140012007601500760540760320480450500450760460
Q
:u;u!U:u!U;u;u!U:u;u;u!U!U:u!U
!UiU;u!J:u!J!J!J!J!J!U!J
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 000073 1/87 ?.-•
Page 97
SEMIVOLATILS ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINQIg EPA Contract: Q97125QQQ7Xlll
f b Code: SPFLD Case No.: REFINE SAS No.: SDG No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.7 (g/mL) fi
Level: (low/med) LOW
% Moisture: not dec. 15 dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y pH:
Number TICs found:
Lab Sample ID: D199682
Lab File ID: C1203W14
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/KG
CAS NUMBER
1.2.3.4. 100-52-75.6.7.8. 56-55-39. 192-97-2
l
! COMPOUND NAME
! UNKNOWN ALIP. HYDROCARBONi UNKNOWN! UNKNOWN! BEN Z ALDEHYDE! UNKNOWN! UNKNOWN PHTHALATE; UNKNOWN PHTHALATEiBENZC A] ANTHRACENE!BENZO[E]PYRENE1i
RT
8.429.5510.2210.5511.1023.7730.1730.2134.79
EST. CONC.
420150013004805103807501000580
l
i Q!J:BAJiAJ!J!AJ; J!J: j;j!
FORM I SV-TIC
0000741/87 F.e
Page 98
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETS?A SAJlr
Lab Name: ILLINOIS EPA Contract: 097125QQQ7X112
Case No.: REFINE SAS No.:Lab Code: SPFLD
Matrix: (soil/water) S
Sample wt/vol: 30.2 (g/mL)
Level: (low/mod) LOW
X Moisture: not dec. 21 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) X pH:
SDG No . : P19966
Lab Sample ID: D1996S3
Lab File ID: C12Q3W15
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether,106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane_120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene
830830830830830830830830830830830830830830830830400083083083063083083083029083083040008304000830830830
Q
;u!U:u;u:u:u;u:u:ui u:u:u!U;u;u!U;u:u:u:uu:u:u:uuiu;u!U:u:u;u;u:u
FORM I SV-1 1/37 Re-
000075
Page 99
SEMIVOLATILE ORGANICS ANALYSIS DATA 3KZSTSArtrLS NO,
Lab Name: ILLINOIS EPA Contract: Q97125QQQ7X112
Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D199fifi
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) G _
Level: (low/med) LOW
% Moisture: not dec. 21 dec. _
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y. _ pH:
CAS NO. COMPOUND
Lab Sample ID: D199683
Lab File ID: C12Q3Wlfi
Date Received: 11/15/qi
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: l.Q
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
(1) - Cannot be separated from Diphenylamine
FORM I SV-2
000076
Q
83-32-9C -1 _OO R3 i. 4,0 3 — —
100-02-7
121-14-2
j* k _fpc 70 7 _
100 10 6 -
PC Of) C_
101-55-3--118-74-1P7 PC_K,
85-01-8120-12-784-74-2-206-44-0129-00-085-68 7 — —9i_94_i56-55-3O 1 p A 1 _Q ___
m pi _7
m-84-0205-99-29H7 OP. Q*_u i uo y50-32-8- —193-39-553-70 3 -191-24-2
— N i troan i .L ine _Acenaphthene
T *i — uini tropneno -L .4-Nitrophenol
— — — jjinenzoiuraii2 T 4-Dinitro toluene
— — — T^^+-Vnr1 i**Vs V^ a 1 A +• a— — — ijie tny -LpriLnaxa iie_ .
— r j.uorene4-Ni troani line
Hexachlorobenzene— Pentachlorophenol. ... .
PhenanthreneAnthraceneDi-n-ButylphthalateFluor an thenePyrene
Benzo ( a ) Anthracene
hi s( 9-Ft-hvl hf»w1 tPhthal at-pDi-n-Octvl Phthalate
— — nenzo K ) p luaraniLnerieBenzo ( a ) PyreneIndeno (1,2, 3-cd ) PyreneDibenz(a h)AnthraceneBenzo ( g , h t i )Pery lene
40001500400040009608308308301400400040008308308304000100002000830
1100067002101700830470083083048003500440036008303400
iu
iu;uiu:u;uiu!U;u;u:u!U
IT:u
!J!U!U
iu!U1
iu111
1/87 Rev.
Page 100
IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SA*?L3 NC.
Lab Name: TT.T .TNOTS EPAX112
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) fi
Level: (low/med) LOW
% Moisture: not dec. 21 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y_ PH:
Number TICa found: _12
Contract: 097125QQQ7
Case No.: REFINE SAS No.: SDG No.: TM9966
Lab Sample ID: D199653
Lab File ID: C1203W15
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/03/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3.4.5. 613-12-76.7. 84-65-18. 243-42-59.10.11.12.13.14.15.16.17.18.19.
1
! COMPOUND NAME
! UNKNOWN ALIP. HYDROCARBON'.UNKNOWN ALIP. HYDROCARBON,' UNKNOWN ALIP. HYDROCARBONI UNKNOWN; ANTHRACENE, 2-METHYL-; UNKNOWN ALIP. HYDROCARBON1 9 , 10-ANTHRACENEDIONE;BENZO[B]NAPHTHO[2,3-D]FURAN1 UNKNOWN PNA; UNKNOWN PNAI UNKNOWN PNA[UNKNOWN PNA[UNKNOWN PNA! UNKNOWN PNA[UNKNOWN PNA[UNKNOWN PNA[UNKNOWN PNA! UNKNOWN! UNKNOWN11 ___—_^_— _ _^__^____^_^_^__
RT
11.3211.7513.1523.7924.5925.0225.3627.2927.5927.8728.0228.1428.4629.2229.5129.5929.6429.6429.76
EST. CONC.
140004000110002200150011001900110094027001100110064012001800160015008001500
iItI
I —I —
!J!J!Ju;j;Ji 7, o
;J; J:J;j:J!J!J!J[JU!J;j1
Q
FORM I SV-TIC
0000771/87 Rev.
Page 101
IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SPA SAMP12 HC
Lab Name: TLLINQTS EPA Contract: Q97125QQQ7X113
L j Code: SPFLD Case No.: REFINE SAS No.: SDG No.: E19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) Q
Level: (low/med) LOW
X Moisture: not dec. 15 dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y, pH: 7.6
Lab Sample ID: D1996S4
Lab File ID: C12Q3Wifi
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzole Acid111-91-1 bis(2-Chloroethoxy)Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene
770770770770770770770770770770770770770770770770370077077077077077077077077077077037007703700770770770
Q
!U!U;u!U;u;u!U!U;u;u:u;u;u:u:u:u:u:u:u:u!U!U:u!U!U:u!U:u!U:u:u:u:u
FORM I SV-1 1/87
00007R
Page 102
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETEFA SAMPLE NC .
Lab Name: TT.LTNQTS EPA Contract: Q97125QOQ7X113
Lab Code: SPFLD Case No. : REZLNE SAS No. : SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30-2 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 15 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) X pH: 7.6
Lab Sample ID: D199684
Lab File ID: C12Q3W16
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Die thy Iphtha late7005-72-3 4-Chlorophenyl-phenylether86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol86-30-6 N-Nitrosodiphenylamine (1)101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a )Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo( a )Pyrene •193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene
I_ _ - . _ __ - — i
(1) - Cannot be separated from Diphenylamine
3700770370037007707707707707703700370077077077037003107707703704107701500770190770770210170190770770770
Q
;u!U:u;u!U:u:u:u:u;u;u!U:u!U!U!J:u!U!J!J:u!U:u!J:u:uu!J!J:u;u:u
FORM I SV-2 000079 1/87 Rev.
Page 103
IrSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
£PA SO.
Lab Name: TLLINQTS SPA
1
X113
Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 15 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y_ pH:
Number TICs found: S
Contract: Q97125QQQ7
Case No. : REFINE SAS No. : SDG No. : D19966
Lab Sample ID: D199684
Lab File ID: C12Q3W16
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: l.Q
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3.4. 100-52-75.6.
1
i COMPOUND NAME. _ i _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ____
! UNKNOWN ALIP. HYDROCARBON! UNKNOWN[UNKNOWN! BENZALDEHYDEi UN KNOWN! UNKNOWN ALIP. HYDROCARBONi
RT___ — ___
8.599.5510.2010.5511.1021.75
EST. CONC.
42019001100420710610
i1
: Q!J:BAJ!AJ!J:AJ;Ji
FORM I SV-TIC 1/87 Rev
000080
Page 104
SEKIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: EPAX114
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.8 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 20 dec.
Contract: Q97125QQQ7
Case No.: REFINE SAS No.: SDG No.: D19966
Lab Sample ID: D1996fl5
Lab File ID: C12Q3W17
Extraction:
GPC Cleanup:
CAS NO.
(SepF/Cont/Sonc) SQKC
(Y/N) Y__ pH: 7.5
COMPOUND
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg)
108-95-2 Phenol111-44-4 bis (2-Chloroe thy 1) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylajnine67-72-1 Hexachlo roe thane98-95-3 Nitrobenzene73-59-1 Isophorone38-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene83-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene
800800800800800800800800800800800800800800800800390080080080080080080080080080080039008003900800300800
Q
!U:u:u:u:u:u!U:u:u;u;u:u!U;u!U:u;u;u:u;u:u:u!U:u;u!U:u!U:u:u:u;u;u
FORM I SV-1 i/e?
OQ0081
Page 105
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA Contract: Q97i9finnn7X114
; . Code: SPFLD Case No.: REFINE SAS No.:
Matrix: (soil/water) SQTL
Sample wt/vol: 30.8 (g/mL) G
Level: (low/med) LOW
X Moisture: not dec. 20 dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH:
SDG No.:
Lab Sample ID:
Lab Pile ID: C12Q3WT7
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 ButylbenzylDhthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chryeene117-81-7 biB(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a,h) Anthracene191-24-2 Benzo(g,h,i)Perylene
3900800390039008008008008008003900390080080080039001908008002802808001600800800800800800800800800800800
Q
:u:u:u!U:u:u;u:u;u:u;u!U!U!U!J:u:u!J!J
iu!U:u:u;u;u:u;u!U:u!U
(1) - Cannot be separated from Diphenylamine
FORM I SV-2
000082
Page 106
SEMTVOLATILE ORGANICS ANALYSIS DATA SHZETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: TLLTNQTS EPAX114
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.8 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 20. dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) I pH:
Number TICs found: 18
Contract: Q97125QQ07
Case No.: REFINE SAS No.: SDG No.: D19966
Lab Sample ID: D199685
Lab File ID: C1203W17
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3. 100-52-74.5.6.7.8.9.10.11.12.13.14.15.16.17.18.
i
i COMPOUND NAME
! UNKNOWN! UNKNOWN; BENZALDEHYDE! UNKNOWN ALIP.1 UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.! UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.[UNKNOWN ALIP.! UNKNOWN ALIP.1 UNKNOWN ALIP.[UNKNOWN ALIP.', UN KNOWN ALIP.[UNKNOWN ALIP.1
HYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBON
RT
9.5210.1910.5211.2513.1015.0016.3417.4517.7919.1420.4421.0421.6521.7222.8222.9423.9226.94
EST. CONC.
15006804804907304808003006207105904306401200510550470530
ll
! Q
!BAJ!AJ! Ju: J;ji 7i '-*
i J! J; J: J!J;j;ju;j!Ji -ri wi
FORM I SV-TIC
OOGC831/2"
Page 107
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA
I . Code: SPFLD Case No.: REPINE
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) G_
Level: (low/med) LOW
Contract: Q97125QQQ7
SAS No.:
X115
SDG No.: D19966
Lab Sample ID: 0199686
Lab File ID: C12Q3W18
% Moisture: not dec. 21 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y__ pH:
CAS NO. COMPOUND
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol103-60-1 bis (2-Chloroisopropyl) Ether10S-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline .131-11-3 Diznethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene
830830830830830830830830630830330830830830830830400083083083055083083083032083083040008304000830830830
FORM I SV-1
Q
!U:u!U!U:u!U;u;u:u,u:ui u:u;u!U!U!U:u:u;u;j;u;u:u;J;u;u:u:u:u:u;u;u
1/87 p.e-
000084
Page 108
SZMIVOLATILE ORGAN!CS ANALYSIS DATA SHEET
Lab Name: TLLINQTS KPAX115
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample vrt/vol: 30.2 (g/mL) G
Level: (low/med) LOW
% Moiature: not dec. 21 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) I pH: 7.5
Contract: Q97125QQQ7
Case No. : REFINE SAS No. : SDG No. : D19966
Lab Sample ID: D1996S6
Lab File ID: C12Q3W19
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether.86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4 , 6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-j118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene__85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine.56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhe117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo (b) Fluoranthene207-08-9 Benzo (k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene.53-70-3 Dibenz(a,h)Anthracene_191-24-2 Benzo(g,h, i)Perylene
4000100040004000660830830830100040004000830830830400084001700830930068008301700830390072083040002800370031008303000
Q
u
:u;j!U:u;uii:u:u!U!U:u!U
:ui
\J:u!U:uIT!J!U\J:J
u
(1) - Cannot be separated from Diphenylamine
FORM I SV-2
0000851/8"
Page 109
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ILLINOIS RPAX115
7 b Code: SPFLD
Matrix: (soil/water) SQTL
Sample wt/vol: 30.2 (g/mL) G
Leve1: (low/med) LOW
% Moisture: not dec. 21 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) I pH:
Number TICs found: 20
Contract: Q97125Q007
Case No. : REFTNE SAS No.: SDG No. : D19966
Lab Sample ID: Dl9968fi
Lab File ID: C1203Wifl
Date Received: ll/15/Q^
Date Extracted: 11/15/Q1
Date Analyzed: 12/04/91
Dilution Factor: l.Q
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
1.2.3.4. 613-12-75.6. 612-94-27.8.9.10.11.12.13.14.15.16.17.18.19.20.
! COMPOUND NAME
1 UNKNOWN ALIP. HYDROCARBON1 UNKNOWN[UNKNOWN ALIP. HYDROCARBON; ANTHRACENE, 2-METHYL-; UNKNOWN ALIP. HYDROCARBON; NAPHTHALENE, 2-PHENYL-! UN KNOWN1 UNKNOWN PNA; UN KNOWN ALIP. HYDROCARBON! UNKNOWN; UNKNOWN PNA'.UNKNOWN PNA! UNKNOWN PNA1 UN KNOWN PNAi UNKNOWN PNA'.UNKNOWN PNA! UN KNOWN; UNKNOWN PNA! UN KNOWN! UNKNOWNi
RT
21.7423.7423.9224.5424.9925.2425.3125.9625.9927.2427.5427.8227.9728.1128.3628.4229.4629.5429.6229.71
EST. CONC.
23001500140012001000780120032072098079026001200990650620130013004001100_______^__^__
i Q
!J!J;j!J: J!J, <J1 . j
:J;j, T
. <J; J;J!J!J!J!J;j;j!Ji>
FORM I SV-TIC000086
1/3-
Page 110
IDSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
fir A
Lab Name: TLf.TNQIS EPA Contract: Q97125QQQ7X116
Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30-8 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 18 dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH: 7.4
CAS NO. COMPOUND
Lab Sample ID: D1996B7
Lab File ID: C1204WQ4
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg)
108-95-2 Phenol111-44-4 bis(2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 b is (2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 : 2,6-Dinitrotoluene
780780780780780780780780780780780780780780780780380078078078078078078078078078078038007803800780780780
Q
!U!U;u:uJ U!U:u;u!U:u:u:u:u!U;u;u!U!U!U;u!U:u!U:u!U;u:u!U:u;u:u!U:u
FORM I SV-1
000087
Page 111
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEZT
Lab Name: TLLTNQIS EPAX116
' ) Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.8 (g/mL)
Level: (low/med) LOW
% Moisture: not dec. Lfl dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y. pH:
Contract: Q971253QQ7 ;____
Case No.: REFTNB SAS No. : SDG No. : D19966
Lab Sample ID: D1996R7
Lab File ID: C1204WQ4
7.4
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol_100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitro toluene.84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-]86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 BenzoCk) Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h, i)Perylene
38002003800380018078078076033038003800780780780380028001000780430040007801600780210078078014001300160012007801300
Q
uU;u;u;jIUc,u:u; j:u;u;u:u:u:u
!U
\S;u:u:u:SJU!Ufu
- Cannot be separated from Diphenylamine
FORM I SV-2 00008S 1/3-7 ? • = • - •
Page 112
SIMIVOLATILE OMAN US ANALYSIS 2AIA SHUTTENTATIVELY IDENTIFIED COMPOUNDS
X116Lab Name: TTLTNOTS gPA
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/voi: 30.8 (g/mL) fi
Level: (low/med) LOW
X Moisture: not dec. 18 dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) I pH: 7.4
Number TICs found: 16
Contract: 097125QQQ7 ;
Case No. : REFINE SAS No.: SDG No. :
Lab Sample ID: D199687
Lab File ID: C12Q4W04
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 12/04/91
Dilution Factor: 1.0
CONCENTRATION UNITS(ug/L or ug/Kg)
CAS NUMBER
1.2.3. 100-52-74.5.6. 613-12-77. 610-48-08. 243-42-59.10. 238-84-611.12.13.14.15.16. 2C5-82-3
I
i COMPOUND NAME
! UNKNOWN; UNKNOWN! BENZALDEHYDE! UNKNOWN ALIP. HYDROCARBON! UNKNOWN ALIP. HYDROCARBON! ANTHRACENE , 2-METHYL-; ANTHRACENE, 1-METHYL-;BENZO[B]NAPHTHO[2,3-D]FURANI UNKNOWN PNA! 11H-BENZO[A]FLUORENE! UN KNOWN PNAi UN KNOWN PNA; UN KNOWN PNA! UN KNOWN PNA! UNKNOWN PNA1 BENZO [ J ] FLUORANTHENEtI _____^—^^— — — — — — — — _
RT
9.5010.1710.5221.6521.7224.4524.5427.2227.5227.8127.9728.0729.4429.5230.4134.74
EST. CONG.
93061043046078055070055057017008907005406806501700
ii Q -
; EAJ;AJ!J,'Ji Tt w
, u. T• ««
. TI <-*
; J!JiJ;ji TI •->
IJ
u!J
FORM I SV-TIC
0000891/57 ?.e-
Page 113
IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE MO,
Lab Name: ILLINOIS SPA Contract: 097125QQQ7X117
L^J Code: SPFLD Case No.: R5FTNE SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) G
Level: (low/med) LOW
X Moisture: not dec. 24 dec.
Extr'ttion: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH: B.2
SDG No.: D19966
Lab Sample ID: D199672
Lab File ID: C12Q2W1Q
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KQ Q
108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroiscpropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol '__120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chlorc-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene.88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate •208-96-8 Acenaphthylene606-20-2 '• 2,6-Dinitro toluene
870870870870870870870870870870870870870870£70F. 70420087087087087087087087087087087042008704200870870870
!U!U!U!U!U!U!U:u:ui •
;u:u;u!U:u:u:u!U:u:u:u!U:u:u:u;u;u;u;u:u;u:u
FORM I SV-11/87 Rev.
000090
Page 114
SSMIVOLATILE ORGANI Co ANALYSIS DATA SHEET
Lab Name: TLLINQIS EPA Contract: Q97125QQQ7X117
Lab Code: SPFLD Case No.: REPINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30. Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 24 dec.
Extraction: ( SepF/Cont/Sonc )
GPC Cleanup: (Y/N) X _ pH:
Lab Sample ID: D19967?
Lab File ID: C12Q2W10
S.2
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Xg) UG/KG
99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_36-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene ;120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene_129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h, i)Perylene
1t - _- . - - - - —
(1) - Cannot be separated from Diphenylamine
4200870420042008708708708708704200420087087087042001908703702502508701700870870870870870870870870870870
Q
i U;ui U;u:u!U:u;u;u;u;ui u:u:u!U!J!U:u!JU!U!U:u:u!U:u;u!U:u!U:u!U
FORM I SV-2000091
Page 115
SSMIVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: TLT.TMQTS EPAX117
J > Code: SPFLD
Matrix: (soil/water) SOIL
Sairple wt/vol: 30.Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 24 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) X pH: B.2
Number TICs found: Z
Contract: Q97125QQQ7
Case No.: REZIHE SAS No. : SDG No. : D19966
Lab Sample ID: D199672
Lab File ID: C12Q2WJQ
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CONCENTRATION UNITS(ug/L or ug/Kg)
CAS NUMBER
1.2.3.4. 100-52-75.6.7.
I
i COMPOUND NAME
1 UNKNOWN ALIP. HYDROCARBON[UNKNOWN[UNKNOWN[BENZALDEHYDE1 UNKNOWN[UNKNOWN ALIP. HYDROCARBON[UNKNOWN PHTRALATE
RT
8.579.5410.2010.5511.0921.6723.75
EST. CONC.
53018001000580860570610
; Q
: J[BAJ[BAJ[J[BAJ: J:Ji
FORM I SV-TIC 1/87 Re
000092
Page 116
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPAX118
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 17 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) X pH: B.I
Contract: 09712SOOO7
Case No. : REFINE SAS No. : SDG No.: D19966
Lab Sample ID: D199673
Lab File ID: C1202W1
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: 1.0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroiscpropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis (2-Chloroethoxy) Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene
800800800800800800410800800800sooSCO800800800800390080080080080080080080080080080039008003900800800800
Q
!U;u1U:u!U:uu:u:u:ui r Ti i~:u:u:u:u:u;u;u;u;u!U!U:u:u;u;u:u!U:u;u!U:u!U
FORM I SV-1 1/87 R.ev.
000093
Page 117
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET* ^ A *^ *k ** ' •**•*•*• •» X«A* *i *»
Lab Name: ILLINOIS EPA Contract: Q9712SQQn7xiia
L j Code: SPFLIL Case No.: REFINE SAS No.: SDG No.: D19966
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. LZ dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) X pH:
Lab Sample ID: D1996?a
Lab File ID: C12Q2W11
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: l.Q
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
99-09-2 3-Nitroaniline83-32-9 Acenaphthene__51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol ,132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenyl ether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-39-2 Benzo(b) Fluoranthene207-08-9 Benzo(k) Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a,h)Anthracene191-24-2 Benzo(g,h, i)Perylene
3900800390039008008008008008003900390080080080039008201608009508708001600800410800800340340330300800800
Q
1U;u!U;u:u:u;u;u!U:u;u;u:u;u:uit!J:u\S:u:u:u!J:u;u!Ju!J!J!U:u
(1) - Cannot be separated from Diphenylamine
FORM I SV-2000094
1/8'
Page 118
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: TT.MNQIS KPAxiia
Lab Code: SPFLD Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL)
Level: (low/med) LOW
% Moisture: not dec. 17 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
Number TICs found: 20
Contract: Q97125QOQ7
SAS No.: SDG No.: D1996S
Lab Sample ID: D199673
Lab File ID: C12Q2WH
JLJ.
Date Received: 11/14/91
Date Extracted: 11/15/91
Date Analyzed: 12/02/91
Dilution Factor: l.Q
CONCENTRATION UNITS(ug/L or ug/Kg)
CAS
1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.
NUMBER
26914-33-0
38380-02-841464-51-137680-73-273575-56-125429-29-251908-16-825429-29-256030-56-951908-16-825429-29-2
26601-64-9
-
COMPOUND NAME
UNKNOWNUNKNOWN ALIP. HYDROCARBONUNKNOWN PHTHALATEUNKNOWN ALIP. HYDROCARBON1,1 '-BIPHENYL, TETRACHLORO-UNKNOWN ALIP. HYDROCARBONUNKNOWN ALIP. HYDROCARBON1,1 '-BIPHENYL, 2, 2', 3, 4, 5' -P1,1 '-BIPHENYL, 2, 2', 3' ,4,5-P1,1'-BIPHENYL, 2,2',4,5,5'-P1,1'-BIPHENYL, 2,2',3,5,6-PEl.l'-BIPHENYL, PENTACHLORO-l.l'-BIPHENYL, 2, 2', 3, 4', 5, 5l.l'-BIPHENYL, PENTACHLORO-l.l'-BIPHENYL, 2, 2', 3, 4, 4', 61,1'-BIPHENYL, 2, 2', 3, 4', 5, 51 , 1 '-BIPHENYL, PENTACHLORO-UNKNOWN ALIP. HYDROCARBON1,1 '-BIPHENYL, HEXACHLORO-UNKNOWN ALIP. HYDROCARBON
RT
9.5521.7523.7723.9524.8725.0026.0126.2926.7426.8627.2127.5228.0128.0428.4628.5928.5928.7929.0429.66
- -
EST. CONC.
150015006107005705705207801700700540190084012008705106205501100600
n "*"
!BAJ! <JiJu; J; J, JT
J
!J;Ju; J!J!J ^U;JU!J;Jj
FORM I SV-TIC
000095
1 /PTL/ w '
Page 119
FESTICILE Ir.jANICS ANALYSIS DATA SHEET
V ' iA — o *
L=b Name: ILLINOI a EPA Contract: 0971250007
Lab Code: SPFLB. Case No.: BEEiHE SAS No.: SDG No . : Dl
Matrix: fsoil/water) SOIL
Sample wt/vol: 30.Q (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 46 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y pH: 7.9
Lab Sample ID: Dl9967a
Lab File ID:
Date Received: 11/15/51
Date Extracted: 11/15/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
319-84-6 alpha-BHC319-65-7 beta-BHC319-86-8 delta-BHC58-89-9 gamma-BHC76-44-6 Heptachlcr309-00-2 Aldrin1024-57-3 Hept. epoxide959-93-8 Endcsulfan I6C -£7- 1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endr in33212-65-9 Sndosulfan II72-04-6 4,4'-DDI>1031-O^-? Endcsulfan sulfate.50-29-3 4, 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-9 a Ipha-Ch lordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroc lor-101611104-28-2 Aroclor-122111141-16-5 Aroclor-123253469-21-9 Aroclor-124212672-29-6 Aroc lor-124811097-69-1 Aroc lor-125411096-82-5 Aroc lor-1260
31313131313131316161-> ^C j.
61616161310•313103106303103103103103101700610
Q
:u:u:u:U:u:u•r
:U:U:u.u:U:'J!U;u!U:u:u:u:ui
:u
FORM I PEST 1/87 Rev
000096
Page 120
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
X102Lab Name: ILLINOIS EPA Contract: 0971250007
Lab Code: SPFLD Case N o . : REELilE 3AS N o . : SE*j No.: 1-1 j
Matrix: (soil/water)
Sample wt/vol: 30.1 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 42 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y__ pH: 7.3
CAS NO. COMPOUND
Lab Sample ID: D199673
Lab File ID:
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS:(ug/L or ug/Kg)
*^ « •— - .— , 4 {-*J la-is - b319 65 7-q i o fl C PO 1 .3 O C O
5g_cp_97 r-: ' A-O1 O t *i D
i-~>'">,; P."? "i Ji. t ~— ' ' • -•
959-93-360-57-17 c c Q _1 . -^-j y72-20-833213-65-9-7^-54-Si • j i ,i" ^x O 1 U ' oC ,'\ O Q -j^ J ^3 •;'7'" _ <1 •- P• — H-- •->
53-43:4 -''f-.? -£103-71-- --P 1 /I •! 7/'w i ' J O / H ^o on 1 ^c; oCUU 1 JO £:
12674-11-2-11104-28-2-11141-16-5-CO^CQ_O1 _Q_OO1D3<il;3
12672-29-6-11097-69-1-11096-82-5-
alpha-BHCbeta-BHC
ffamma-BHC
Aldrin
Endosulfan IDie Idr inA A* .nnp"
Endr inEndosulfan II4.4'-DDD
< A* _rir1'T** . 4 L/L'l
"nd^in kp-t-or^a 1 p h a - C '•-. 1 c r T % n e
_,, . ,gamiTia Lnior'aaneT U— — i oxapneneAro'clor-1016Aroc lor- 1221Aroc lor- 1232
Aroc lor- 1248Aroc lor- 1254Aroc lor- 1260
29
:.9'__'->!
L". 929292957575757C.'JO 1
e -7
c;7
290290580280290280280280380570
T 'W
T)
;u1 1.1' rJ:U' r ;
:uTJ:u. r Ti_;
:U. ' T
r •
• : i
1 T.j
:u!U:u:u:u:u:u:u: j:u
FORM I PEST 1/37 Rev.
000097
Page 121
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
L-o Name: ILLINOIS EPA
E?A SAMPLE NO
X103
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 4Q dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y_ pH: 7.8
. Contract: 0971 50007 ;
Case No.: BEZlNJa SAS No.: SDG No.:
Lab Sample ID: D1996BQ
Lab File ID:
Date Received: 11/15/51
Date Extracted: 11/15/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/'L or ug/Kg) U_£ Q
1
319-84-631S-85-7319-86-8f^a AQ QOO Oi? C7
76-44-8-o f \ q n O - 9 -^ C\/~, A c; 7 -3 _iUi-H G / v-< —QCQ QR AJ533 C7~ Q" ' \ p. 7 1C-U 3 ' 17 *•< _ c. K Q _
7 •-, _ O f) M -' _ £. ' J ~ ~
33213-65-9-72-54-81 031-07-8 —50-29-372 43 553494-70-5-cipvo 71 Q_
5103-74-2 —Ann 1 TC. oOUU 1 O!j 4i
12674-11-2-11104-28-2-11141-16-5-53469-21-9-12672 29 611 A 07 J;Q •)IX'^oi— C3 1
1 1 j36-cll-.t, -
aloha-BHCbeta-EHCdelta-BHC
— samma— BH^Heptachlor
— Aldr inHept . epcxideT-< j -i f -r~ tnaosu LL an ir\ • i — Jjieiurin4 A ' nT'C1• 1JL/E. , . , , . , .
— ~EndrinEndosulfan II4.4'-DDDEndosulfan sulfate4.4'-DDTMethoxvchlorEndrin ketone
— alpha— Cnl ordanegairuna— Chlordane
— — ToxapneneAroclor-1016Aroc lor- 1221Aroc lor- 1232Aroc lor- 124TAroclor-12-a
_A *-,/-,/-, 1 /-.v»— 1 ***£ A— — t\L oc ior— L^^t^tAroc lor- 1260
'"' i
2823'"* Q
28232828555555555555552805523028057027028027027017 (,240550
i
:u:u', U:u:u: rj' F T
'U:u:u:u:u:u'U!U:U:u'U!U:U•U:u:u:u
:.]:ui
FOR-X I PEST000098
1/37 Rev.
Page 122
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: ILLINOIS EPA Contract: 0971250007
v • ^ <A . -< t
Lab Code: £££LIL Case N o . : BJEZLNJi 3A3 N c . : 2LG No . : Hii-iE
(g/mL)
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med) LOW
% Moisture: not dec. 20. dec.
Extraction: (SepF/Cont/Sonc) SONG
GPC Cleanup: (Y/N) Y. pH: 8.6
Lab Sample ID: 1199681
Lab File ID:
CAS NO. COMPOUND
Date Received: 11/15/9J.
Date Extracted: 11/15/91
Date Analysed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
1
319 84 6- - -0 1 Q O C, "7oj.y oo iO 1 Q Or? Qj iy oo o58-89-97fi ^1/1 fl - -/ D t t t t~O
303-00-2•> /-i--. -1 c,7 •?J. \J <£ -i -J 1 O —n c o QR Qy 3 y y C O
60-57-1~ •-' c. e; q< _ .J.J y72-20-8^ QO 1 -3 CC, Qooi. 10 DO y7^ = " QI — o -» Oi n "5 1 n7 P _lU>-/ i U( Oc,f- 9Q QOv_/ ^a O — — —
72-43-5cq,jQ.i 7n cOo'ty'n » U O5103-71 9- --c-i 0^ — 7/1 — 9O X U o — / *t — <i —Rnrn ^c._9OUUJ. OO <i
12674-11-211104-28-211141-16-553469-21-912672-29-61 1 DQ7 £Q 1i .Luy / oy i1 1 ("iQrt R9 Cij. iuyo o^i D
alpha-BHC_U04- _ RHP— De L.a Dfiv_ _ .
do 1 +• a PUPe 1 w3 cri^gamma-BHC
Aldr in
— n.nao&ui^an iE ' ie ldr in
— ii d ' _nnr— H , t — L>L>L.
Endrin—Endosul fan I I— A A ' -nnr^— — *i . *4 — UUL
T-t , -| _£ 1 - 4 .
— 4 4 * PlFlT
Methoxvchlor"Endrin ketone
alpha— Chi ordane
xoxapneneAroc lor- 10 16Aroc lor- 1221Aroc lor- 1232Aroc lor- 1242Aroclor-1248
""HTOC -LOr~ 1^3*4
— Av»*-i/-»T/-iv» lOf in— r t r o c ± o i r J.^DU , , . , , .
2121O 1
2121
212141414141414141
21041
210210420210210210210210410410
; U:u:u1 n' U: U' U
:u:u! U:u:u:u:u
:u:u!U:uI U:u:u:u:ui
FORM I PE.-3T 1/87
000099
Page 123
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
.^O Name: ILLINOIS EPA
[FA SAMPLE NO.
X105
Lab Code: SPFLD
Matrix: (soil/water)
Sample wt/vol: 30.5 (g/mL) G.
Level: (low/med) LOW
% Moisture: not dec. 14 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y pH: 6.6
Contract: 0971250007
Case No.: REFINE SAS No.: SDG No.:
Lab Sample ID: D199666
Lab File ID:
Date Received: 11/14/9;\±c*f>
Date Extracted: l l /Lfc/91~f ~ ~
Date Analyzed: 11/29/91
Dilution Factor: 1.00
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
T 1 Q o A CLo 1 3 OS DQ i Q OC, 7
"3 1 L AS fiwj-J OC OJ- p pQ Q
'"'» y 1 a
309-00-2
C, C. Q Q D Q _3 o3 3O a£.•"* R7— •" -D u D ' i70 cc Q( ^. 3D 3
72-20-833213-65 9-T~- ^(A R/ 4. OS — oi f \ o i H7 — A —1 U o 1 wio —
50-29-372 43 5-
5103-71-95103-74-28001-35-212674-11-2111C4-28-211141-16-5
12672-29-611 r~lQ7 AQ 1iuy i oy— i—i i n Q R _ P O _ f ^ _1 1U3D — o£ <J~
a i i-,Ka nwr*aipna r>n\^V\a-(- a — RUfD e t a — on or^e. 1 t- a -TaUPa e i u a — on
Pjjp• r , •,neptacmorAldrinHept . epoxideT-, i i f Ttnuosuiran i . ._r\ • i Jijie lar in. . > nriTT
EndrinEndosulfan II
T-. , -I f 1 JT 4.— tLnaosu 1 1 an suiraL,e4.4 '-DDTMethoxychlor
—Endrin ketonealpha-Chlordaneflamma-ChlordaneToxapheneAroclor-1016Aroc lor- 1221Aroc lor- 1232
•~ ™AlT*OC ior*" J. 4tf£
Aroc lor- 12 48~ f\ \j c i o r ^ -i. ^t o
A 1 1 OC/t— Arocior— IZDU
1 QLJ1 Qlj1 Qi y1 Q1C71 Q13
191 Q
1 QL3•30OOOQOO
3333COOOOflOO
3 '^190
•JOOO130012003901901901901 r\Aiyu190VjO \J
•3Qn
11 f 1, u1 f T, u1 T T
i r i. UI M
:U1 " 1. O. r.
1 M
i r i. U' U:ui ri. U-. r T
' U1 ; T; r ;, Uit
:U:u;u;u\ r T, U
!Ui CTi Ui r T
:
FORM I PEST 1/87 R*-,
000100
Page 124
::;:z ORGANics ANALYSIS DATA SHEET
Lab Name: ILLINOIS £PA
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.6 fg/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 2A dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) Y_ pH: 6.7
Contract: 0971250007
Case No.: REJLL&E 3A.5 No.: SDG No.: Llai
Lab Sample ID: D19S667
Lab File ID:
CAS NO. COMPOUND
Date Received: 11/14/91
Date Extracted: 11/4- /91
Date Analysed: 11/29/91
Dilution Factor: 1. C'."-
CONCENTRATION UNITS:fug/L or ue/Kgl UG/KG £
-213 Q/i £_ _>i^.d 0*1 O —313 35 7--o • Q pc a•J is OO C
58-89-5-7c 44 3"5''*C 1O ""o >-• cr u u _i A - - / 1 _ C , 7 _ Q _tU.in O ' O —Q C, a Q O Q
£(-. c.7 iDU O ' 170 cc, q _' ^ o-j y7^ "/(•• P' ._ ^v o-aoo i o crc, QoO<i. 1 0 DD ir"? P A P
1 r> "3 1 — D 7 3 _I v O i U / O=, r> ^ Q "3DO ^.y ^.- -T~> A~* R' t- T'-' vJ
53494-70-5-5103-71 9-5103-74 28001-35-2 —1 fJR'7 A 11 OliCO ' H 1 J. «i1 1 1 C\A OR — O —l i lwl ^O ~ £,~1 1 1 4 1 — 1 f t R —111H1 — JLO «J~
53469-21-9-12672-29-6-1 1 AQ7_f f Q_ 11 lUj ' — D i 7 i
11096-82-5-
a 1 -.U -j nU("— aipna cnv^beta-BHC
_ j _, i r - _OUp
ear^na-BHCHeota^hlor
— n icir in
— . , f -r— C.P.CIOSU ir an i
4 A ' rifiP— .— — Unarm"C*— -J -. e;* » "T f — —. T Tr,nuoouiia.n 11
- d. A ' TlTlTlj-, . , ,- , .— incJosuiian sullate4 4 • _rir)T. i — uu i.
eurioxYcnj.01Endrin ketonea Ipha-Chlordanegamma -ChlordaneToxaphene
— — — A»**-v/^1^\»«— 1A1 ft— — — rtroc j.or— J.VJ ID^. Av%^is*1^v 1*?T^1— — HrOCJ.Or L££.±.
— — ___ A »>/->/-» 1 /-»» 1OQO— — rtrocj.or izjzAroc lor- 1242Aroclor-1248flv.^l/^1 /-1T»_1 OC</1— — ttroc io r— L^OH . .,Aroc lor- 1260
•~1 •"
.-j /-,
'". O
O *"•
O'"1
* •' VOO
431643434343
110220
43220220440210220210210210180430
: U: C >I T T
:u1 ' J! rJ• -JT.i1 ' 1
: J! U:u:u:ui
;u: U:U:u:u:u:u!U!U!U: J:u
FORM I PEST 1/87 Rev.
000101
Page 125
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
i. _> Name: ILLINOIS EPAX107
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. IS dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: CY/N) Y_ pH: 7.3
Contract: 0971250007
Case N o . : REEIiiE. SAS N o . : SDG N o . :
Lab Sample ID: D199668
Lab File ID:
Received: 11/14/91fil C 6
Date Extracted: ll/ier/91
Date Analysed: 11/30/91
Dilution Factor: 1.00
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
3 1 Q ft A K-.1-3 Ol O
319-85-7•7 1 O PA fl3 1.3 OD O
58-89-97G-44-8309-00-21C24-57-3
'- - - 7 i
72-20-3o '-_•-•• o O C. O•-'K-'ii-i.O — DO 3 —
72-54-81031-07-850-29-370 y l Q _ C . _
53494-70-5--5103-71-9f\ 1 m 7/1 _o _DJ-VJo I <i~ £ —
8001-35-212674-11-2 —11104-28-2 —11141-16-5 —53469-21-9 —12672-29-6 —11097-69-1 —11096-82-5 —
beta-BHC— ae 1 La— nriL.
garrjTJct-S'-'CHpptachlorAldr in
Er<rjc£ul£&-i I
4 A * — r^itr. «t LJJJE.
Endrin
4.4 ' -DDDEndosulfan svilfate4. 4 '-DDT
— ne unoxycn j-or .. ,Endrin ketonealpha-Chlordane
— — ganuna— Cnlordane ., _,„ToxapheneAroc lor- 10 16Aroc lor- 1221Aroc lor- 1232Aroc lor- 1242Aroclor-1248Aroc lor- 1254Aroc lor- 12 60
2020202020
20390.753939393939
20039
200200400200200200200200
20390
i:u:U•u
• L I
:u:u:u •:u:u:u
:u:u:u!U:u:u!U
! J!U1
FORM I PEST 1/37 Rev.
000102
Page 126
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: ILLINOIS EPA Contract: 0971250007
Lab Code: SPFLD Case N o . : REFINE SAS N o . : SDG No.:
( g/mL )
Matr ix : (soi l /water)
Sample wt/vol:
Level: ( low/med) LOW
% Moisture: not dec. 19 dec.
Extraction: (SepF/Cont/Sonc) SOHC .
GPC Cleanup: (Y/N) I pH: 6.9
Lab Sample ID:. D199669
Lab File ID:
Date Received: 11/14/91i4s<^>
Date Extracted: Il/:fc5/9l
Date Analyzed: 11/30/91
Dilution Factor: l.QO
CAS NO. COMPOUNDCONCENTRATION UNITS:fug/L or ug/Kg) UG/KG
319-84-6 alpha-BHC319-85-7 beta-EHC319-86-8 delta-BHC58-89-9 gamma-BHC76-44 -3 Heptachlor309-00-2 Aldrin1024-57-3 Kept, epoxide959-98-8 Endosulfan I60-57-1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endrin33213-65-9 Endosulfan II72-54-8 4,4'-DDD1031-07-8 Endosulfan sulfate50-29-3 4, 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroclor-122111141-16-5 Aroclor-123253469-21-9 Aroclor-124212672-29-6 Aroclor-124811097-69-1 Aroc lor-125411096-82-5 Aroc lor-1260
2121212121
3.212140404040404040
21040
210210410200200200200200190400
!U;U'U:u:u
7; j
:u:u:u:u!U;u!U:u:u:u:u:u:u!U:u:u!U: j:u
Q
FORM I FE3T 1/87 Rev.
000103
Page 127
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
Name: ILLINOIS EPA Contract: 0971250007
EPA SAMPLE S'C.
XI03
Lab Code: SPFLD Case No.: REFIME SAS No.: SDG No. : D199r:n
Matrix: (soil/water) SOIL
Sample wt/vol: 30.4 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 16 dec.
Extraction: fSepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH: 7.3
Lab Sample ID: D19967Q
Lab File ID:
Date Received: 11/14/91ft £<&
Date Extracted: 11/Mr/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CAS NO. COMPOUNDCONCENTRATION ONITS:(ug/L or ug/Kg) UG/KG Q
319-84-6 alpha-BHC319-85-7 beta-EHC319-86-8 delta-BHC58-89-9 gamma-BHC76-44-8 Heptachlor309-00-2 Aldrin1024-57-3 Hept. epoxide959-98-3 Endosulfan I60-57-1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endrin33213-65-9 Endosulfan II72-54-8 4,4'-DDD1031-07-8 Endosulfan sulfate.50-19-3 4, 4'-DDT72-43-5 Me t hoxy c h lor534-94-70-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroclor-122111141-16-5 Aroc lor-123253469-21-9 Aroclor-124212672-29-6 Aroclor-124811097-69-1 Aroc lor-125411096-82-5 Aroclor-1260
20 :u20 ; u20 in2020
202039393939393939
20039
200200400190200190190190110390
:u:u
5' J:u:uu
:u• u
:u:u;u:u!U!U:u:u:u:u:u!J:u
FORM I- PES
O00104Rev.
Page 128
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
X11CLab Name: ILLINOIS EPA Contract: 0971250007
Lab Code: £££LP_ Case No.: BEEIHE SAS No.: SDG No. : Ll^ac-i:
Matrix: (soil/water) SOIL.
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 22 dec.
Extraction: (SepF/Cont/Sonc)
Lab Sample ID: D199671
Lab File ID:
Cleanup:
CAS NO.
(Y/N) PH: 7.Q
COMPOUND
Date Received: 11/14/31
Date Extracted: ll/Jrg/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS:fug/L or ug/Ks) UG. 'KG Q
319-84-60 i Q QC 7J ^ C 7 O O ~ '
319-86-3K O PQ Q"._> OC> 3
76-44-8•3r'd '• , (•• . ••••J U. v w ~1 n^^d ^7 "^- -J. U .i. M Q' o — —QCQ QQ Qy^/cr yo o60-57-17O K C Q _I ^. --/O ^ — ~
7 o _ C1 n A-' «_ -iU OO •; •". 1 "3 (if SvjO^. 1 o Do 3
72-54-81031-07-8e.r\ oq o
72 43-553494-70-55103-71-9c-iA'i 74_9_O .LvJo— / t~ ii—8001-35-212674-11-211104-28-21 1 1 4 1 — 1 f t — c i —J. i XM i — iO~ sJ~ ~ ~
53469-21-919R79-°C1 Ci j d D ' ^ . i . C ' D — — —1 1 fSQ7 (iQ 1X J . U i # / DC? i11096-82-5
--alpha-BHCKof-a RWi"DeT..a — tiri^
--dplta-BHCgciinnici nnVx
— Heritachl cr—A Idr in
— , . . T— i,ndosu i r an i--Dieldrin
4 A ' TiT^t?. 1. — UUC.
— I7*ri/^ /-\ c»i i 1 -f a »-» T T— rLnaosLi .LI an 11- -4 .4 ' -DDD— Endosulfan sulfate
4 A ' _r\r\'r. ** — LiLtL
— Methoxychlor--Endrin ketone— alpha-Chlordane
— gamma — i_>n j. o r aa.ne- -Toxaphene--Aroclor-1016— Aroclor-1221_ — At*r\s\ 1 **•**_ , 1 OQO— — HrOC ± O r — l<iOii--Aroclor-1242, __A*^ /»>^1 r-.vt_1 O.4Q— — n r O C l O r — J.^.^io
A v^— v^v 1 ^VV*—1 O^AnrOC J.or— 1 iDt
--Aroclor-1260
22/-• .->t,
j"*) «*.^_ 4_
22
22222242424242
* O»-t<i.4212
22042
220220440210210210210210420420
:u:u: u' • j' r!
:u:u:u:TJ:u! LT
:u:u:u:J' U!U:u:u:u:u:u:u:u:u:u:uii
FORM I PEST 000105
Page 129
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
Name: ILLINOIS
EPA SAMPLE SO.
Xlll
Lab Code: SPFLD
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/mL
Level: (low/med) LOW
% Moisture: not dec. JLS dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y_ pH: 7.2
Contract: Q971250Q07 I
Case No.: REFINE SAS No.: SDG No.:
Lab Sample ID: D1996R2
Lab File ID:
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analysed: 11/30/9;
Dilution Factor: 1.QQ
CAS NO. COMPOUNDCONCENTRATION UNITS:fug/L or ug/Kg) UG/KG Q
•3 1 Q a A C _>_/ j. y OH o319-85-7319-86-8RR OQ Q_DO OJ i? —
76 44 83C9 00 2- -t n^4 ^7 ^ -L<J t.'i 3 f O
959-98-360 57 172-55-970 ^ n - R/ <i ^.U — OQ T O 1 O CC QOOi.lO DO a —7° ^4 fli ^. CJT O" i"i '^ 1 ("17 P-^O^l U ' Oc f •-> Q T
7"? 43-5-- -c- j , iQ, i 7(-i cDOn3M 1 U O51 r\ o 71 Q _luo / i a —5103-74-28001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
a 1 T-iVia — RPPaipna — Dfio .beta-BHCdelta-BHCff/inuTia BflL-
HeptachlorAldr inHept . epoxideEndosulfan IDie ldr in4 . 4 ' - D D EEndr in
— c.naosu±ran LL4 A ' T\T\T\. i \j\j\jTT -J 1 * 1 * 4.— iinaosunan suirats4 /1 * HTiT
T ** JJLJl
MethoxychlorEndrin Ice tone
i.pna— L^n lorQane _ .gamma— Chi ordaneToxapheneAroc lor -10 16Aroc lor- 1221Aroclor-1232Aroclor-1242Aroc lor- 1248Aroclor-1254Aroc lor- 12 60
202020202020202039393939393939
20039
200200400190200190190190240390
i
:u:u:u;u:u:u:u
:u1U:u:u!U:u!U:u:u:u:u!U!U!U:u:u:u!J!U1
FORM I PEST 1/87 Rev.
OOOlOfi
Page 130
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
E?A = A«?'_;
X112Lab Name: ILLINOIS EPA Contract: 0971250007
Lab Code: SPFLD Case No.: EEEIUE. SAS No.: SDG No.: ri9sgg
Matrix: (soil/water) 20J_L_
Sample wt/vol: 30.0 (g/mL) G
Level: flow/med) LOW
% Moisture: not dec. 21 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y. pH: 7.1
Lab Sample ID: D199633
Lab File ID:
CAS NO. COMPOUND
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 11/30/51
Dilution Factor: 1.00
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
319 84-6T 1 Q_P Ci_7•J±3 CO- /010 PC flO 1 i7 — OO O
58-89-97 C ilJ R —i D *t*t O
309-00-2^ f~;n A Pi 7 "5iU^l'i U ' OQC.Q QA -PI- -333 jo O ~CA R7 1Du O ' 17 •-, c c Qi .i. 33 370 on O' i. — £. U O•;• 0 O 1 1 C R Q^^•J*O DO !3
72-54-31 f. •? 1 c\ 7 -^ — _lUO^. wl o — -c,"s ^Q -^_^ l J i. 3 O70 /iq c.r {. to Oc-3^C|.i 7fi C
5103-71-9C.1 A'5_7/l_'7__O1UO / H ^onn i — ^ 9 —DUU1 — JO 4. —1 OC7/1 1 1 _OX<cD ' 4 1 1. £.
11104-28-211141-16-553469-21-912672-29-611097-69-11 1 D Q f i — fl9 R1J.UC3O — O^i O
-alpha BHC— Viot- a _nup— oe ua — Dno
j_ 1 4. -,_nur— uei ta — DfiL/gamma -BHCHsptacnlorAldr in
— nepu . epoxxCieEndosulfan ITi ' 1 Juie icir ind 4 ' _ r>r>F'i . 4 — UUE,T? Jtncir in
— TT»-i^^^oT»l'^ 'a»-i TT— n.nuosuiran 114 . 4 ' - D D D
4 A ' _nriT. *i ~ L>L> iM 4- U U Tne LnoxvcniorT-. , . .£.no.rin xetonealDha-Chlordane
— gamma— Cnlordane _.rp >— — — loxapneneA-»>«/^1 ^»«_ 1 f"M C— — Kroc J.OT*— lu J.DAroc lor- 1221Aroc lor- 1232Aroclor-1242Aroclor-1248Aroclor-1254
— — — Av^r f - t r^ l^ iv* lOAPl— — — rtrocior _L^-DU, _._
2222
222242424242424242
22042
220220430210210210210210
1500420
i
:u• u!U
! U
;u\ \ i:u'. U:u' U:u:u:u:u!U!U:u:u:u:u!U:ui ut
FORM I PEST 000107 1/S7 Rev.
Page 131
PESTICIDE ORGANICS ANALYSIS DATA SHEETCm o.-„ .r _z.
Name: ILLINOIS EPAX113
Lab Code: £?FLD
Matrix: (soil/water) £.
Sample wt/vol: 30.1 (g/mL) Q
Level: (low/med) LOW
% Moisture: not dec. 15 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) X pH: 7.6
Contract: 0971250007 ;
Case No.: BEEIME SAS No.: SDG No.:
CAS NO. COMPOUND
Lab Sample ID: D
Lab File ID:
Date Received: 11/15/91
Date Extracted: 11/15.'91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Jj
312-54-6 alpha-BHC319-85-7 beta-BHC319-e6-5 deita-BHC55-39-9 gamma-BHC75-44-3 Kept ach lor3CS-00-2 Aldrin1024-57-3 Kept, epoxide95.^-^3-3 Endosulfan I60-57-1 Dieldrin^2-55-9 4, 4'-DDE72-20-6 Endrin33213-65-9 Endosulfan II72-54-3 4.4'-DDD1031-07-8 Endcsulfan sulfate.5C-29-3 4. 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-3 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroc lor-122111141-16-5 Aroc lor-123253469-21-9 Aroc lor-124212672-29-6 Aroc lor-124811097-69-1 Aroclor-125411096-82-5 Aroc lor-1260
202020202020203939393939393920039200200400190200190190190390390
!U:u:u
u: u:u;u:u:u:u'U:u•u:u:U:u:u:u;u!U:u!U:u:u
FORM I PEST 1/3
00010S
Page 132
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
| — , T v -
Lab Name: ILLINOIS EPA Ccr.tract: 0971250007
Lab Code: 3RFLD Case No.: REFINE SAS No.: SDG No.:
Matrix: (soil/water) SOIL
Sample wt/voi: 30.1 (g/mL^ Q
Level: (low/tned) LOW
% Moisture: not dec. 20. dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) X pH: 7.5
CAS NO. COMPOUND
Lab Sample ID: D199635
Lab File ID:
Date Received: 11/15/91
Date Extracted: 11/15/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
319-34-6 alpha-BHC_319-85-7 beta319-36-8 delta-]58-39-9 g a mm a - B K C76-44-3 Heptachlor309-00-2 Aldrin1024-57-3 Hept. epoxide959-98-6 Endcsulfan I60-57- 1 Jieldrin
72-20-6 Endrin33213-65-9 Endosulfan II72-54-8 4.4'- DDD1031-07-8 Endosulfan sulfate.50-29-3 4,4 '-DDT72-43-5 Methoxychlor53494-7C-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroc lor—101611104-28-2 Aroc lor-:11141-16-5 Aroc53469-21-9 Aroc lor-!12672-29-6 Aroclor-1248.
11096-82-5 Aroc lor-:
21212121212121r*i i~ 1
41414141414141
2lL>
41210210420210210210210210410410
:u: u'U:u•u:u:IT;u:u:u:U!'J' U:U:U:U:n;U:u:u!U!U:u:u:u:u:u
FORM I PEST 1/87 Rev
000109
Page 133
IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET
_?A SAMPLE SO
X115Name: ILLINOIS EPA Contract:
Lab Code: SPFLD Case N o . : R££IiiE £AS N o . : SDG No. : I-lrri-
Matrix: (scii/water) SOIL
Sample wt/vol: 3Q.0 ig/mL) Q
Level: flow/med) LOW
% Moisture: not dec. 21 dec.
Extraction: fSepF/Cont/Sonc) SQNC
GPC Cleanup: (Y/N) X pH: 7.5
Lab Sample ID: 0199686
Lab File lli:
Date Received: 11/15/91
Date Extracted: 11/15/9:
Date Analyzed: 11/30/91
Dilution Factor: 1. 0(J
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or us/Kg) UG/KG Q
319-84-6319-35-7•j 1 a a £ po iy — oo c58-89-97 p ,1 ." Qi !D ^l O'ViG r><~> 9•J'Jlr L'U Z1 rv~) ^ c, 7 Q1 L _. 4 - 3 / O —359-33-5---6 -~i c "> 1 _•J O ' i
72 c 5 9T~ '->c ATOO '. 1 CC, Q
•-7 *~- [^ 4 /j
T3--C7-3--50-29-372-43-553494-70-5-5103-71-9--5 1 /-> — 74 •-.
8001-35-2--
11104-28-2-11141-16-5-53469-21-9-12672-29-6-11097-69-1-11096-82-5-
%loha_BHcbeta-BHCd *. 1 4- -, _ TDLJ^e 1 1 a — cn*^samma— BHC
•i i •.i i. >3 r i nr.ez-t. epox. :•?Endcsu l fan Ir- . 1 jL' i. e lar in4 4 ' D*^^"C1 Jtncir inT— - i r* j -r— £.naosu i. j. an 11A A ' riPiFl
"ndosu It" an sul^'ate4 . 4 ' - D D TM^-thoxvchlorEndrin ketonea I'&ha-Ch lordane
— sainina—Cn lordane ,Tox* phene
— Aroc lo r— lOlbAroclor-1221Arcclor- 1232Aroc lor- 12 42Aroc lor- 1248Aroclor- 1254Aroc lor -1260
: 22' O'".
1 •', r>*
.
i .-,,-.
i
f .~> /-\
i ' j •",
4242
: 42! 42
42' 4°1 4 -~j
•1 -
: 42
! 220! 430
! 210: 210! 210: 210
1400! 420I
:u1 U1 rjt r •
(.'.
' f ;
:ui n
:u!U
:u:u
:u; u
FORM I PS.-.'
000110l'.:<7 Rev.
Page 134
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA £AM?LZ SO
Lab N
Lab C
Matri.
Sanpl
Level
% Moi
Extra<
GPC C
ame: ILLINOIS
sde: SPFLD
x: (soil /water
= wt/vol:
: ( low/med )
sture : not dec
EPA
Case No. : REFINE
^ SOIL
30.0 fg/mL) G
LOW
. 18 dec.
Contract: 0971250007
SAS No. : SCO No
Lab S<
Lab F
Date
Date ]
rtion: (SepF/Cont/Sonc) SQNC Date I
leanup: (Y/N) Y. pH: 7.4 Dilut
CONCENTRATECAS NO. COMPOUND fug/L or ug,
319-84-6319-85-7T 1 Q O C QO j. o OO O
7fi 44 R^ |7 n
i no A c,7 "3L\J 4 O ( o
, c- i
•""" =, S. Q. _ O -J J"-? /• O '"V Qi — ; > — O
3? O * "3 C - O._>_.,. O C-_ ir7 •"• r .- o
• O 1 _' ' CC •) OQ J
^"JQJ, 7'" -
5103-71-95103-74-2RAA1 T^ O
12674-11 2 —11104-28-2 —11141-16-5 —C •0,1 CQ O1 Q _•JOHDO < -L CJ
• t • Q-^ SQ i"
11C33-32-5--
alpha-BHrbeta-BHC
T ' U n&ptacn ior— rtiarin— riept . epoxide
T-i , •) ,- Ttnuosuiian i- - r' • e 1 -^ »•• i "•
, . , p." ^^ndr inEnacsultan I j.
T7 1 • •" JT- E.ndos'Li i rar sj-t/ _1 * ""ifiT"- 4 . -i r'L'l
Methoxychlor— Endrin Ketone
alpha-Chlordanegamma-Chlordane
Aroc lor- 10 16Aroc lor- 1221Aroc lor- 1232
A 1 1 " JR
* -^1 1 ° P J
Aroclor-1260
ate
XI 16
£} • QO •- *-,
ample ID: D199687
ile ID:
Received: i.
Extracted : .L
Analyzed: ±.
ion Factor:
3N UNITS:'Kg) UG/'KG
21212121212121
404'J
40
4040
21040210210410200200200200200400400
1/15/91
1/15/91
1/30/91
1.00
Q
i '
;u:u ::u ;;u:u ::u:u• ry
!U"J:un
:u:u:u : ^:u:u :!U ::u ::u:u:u:u:u:u :!Ui i
FORM I FE3TO00111
Page 135
IDRGANIC3 ANALYSIS DATA SHEET
Name: ILLINOIS EPAXI 17
Lab Code: SPFLD
Matrix: fsoil/water) SOIL
Sample wt/vol: 30. 3 (g./mL) Q
Level: (low/med) LOW
% Moisture: not dec. 24 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GPC Cleanup: CY/N) Y_ pH: 8.2
Contract: 0971250007 ;
Case No.: EEZLNE 3AS No.: SDG No.:
Lab Sample ID:
Lab File ID:
CAS NO. COMPOUND
Date Received: 11/14/51i 4 t*
Date Extracted: 11/3-6-/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS:.'ug/L or ug/Kg) UG/KG Q
319-34-6 alpha-BHC31S-85-7 beta-BHC319-36-3 delta-BHC58-39-9 gamma-BHC76-44-8 Heptachlor3C9-CO-2 Aldrir.1024-57-3 Kept, epoxide959-93-8 Er.dosulfar. I60-57-1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endrin33213-65-9 Endosulfan II72-54-8 4,4'-DDD1051-07-8 Endosulfan sulfate.50-29-3 4. 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroc lor-122111141-16-5 Aroc lor-123253469-21-9 Aroc lor-124212672-29-6 Aroclor-124811097-69-1 Aroc lor-125411096-82-5 Aroclor-1260
22 ' 'J22 : U22 !U22 !U22 IU22 | H22 : U22 ' U43 !U43 'U43434343432204322022044083220210210210480430
!U•n'U
•_i:U:U'U:u!U:u1 j!U:u:u:ui
:u
FORM I PEST000112
Page 136
IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: I L L I N O I S
Lab Code: SPFLD
: X116EPA Contract: 0971250007 :
HARP N o . : REFINE SAS N o . : ' SDG Nn • D'SS**.
Matrix: ( soi l /water) S.OIL Lab S<
Sample wt/vol: 30 . 1 ( g / m L ) Q Lab F
Level: ( low/med) LOW Date I
% Moisture: not dec. 17. dec. Date I
Extraction: (SepF/Cont/Sonc ) SONC Date t
GPC Cleanup: ( Y / N ) Y pH: 8.1 Dilut:
CONCENTRATKCAS NO. COMPOUND (ug/L or ug,
i•313 C A fioiy-o^ o -•5 1 Q DC, 7o iy 0.3 '3 1 Q Q A fliy 3D Oc c pa QT ••* * * Q
•3 r\ Q ri f\ oo u y i j u i. —1 o _ 4 57 3C P C ^ £3 Qy v^ y ^ o o
7 o c, c ot-l f- /~l ,*. Q/ ^. ^.Vj O ~
- O R 3,'t;0 A750-29-37? 43-5^ Q ^ O X _-7O — 'SP i n ^ 71 Q — —ClUo t L J
5103-74-2
1007^4 11 o _
1 1 1 / 1 1 1A *^ .
12672-29-6 —i 1 n<37 — AO 1i ivjy / oy i11096-82-5--
- Ko1-n RWP
H o T -h a RWr*
Hept achlcr— MI ur in
— h e p t . epcxide— • J i -r T— ii,ncsosuii&n in « i ^, ,, , n^tr
— ,— fc.nur in— Endosulfari il
. . , r\nr>C1 J T •£ 1 JT i.c.nuosuiian suiia^e4 . 4 ' - D D TMethoxychlorEndrin ketone.
— — a l p h a — Cnl or danegamma-Chlordane
~Toxapnsne— — — rtroc ior— lu ID
A l t O O 1
A 1 1 T3O
A 1 1 O X O— — — — Hrocior— IZHZAroc lor- 1248
Aroc lor- 1260
ample ID: D199S73
Received: 11/14/91I1* C*6
Extracted: 11/J^v'Sl
^nalvzed: 11/30/91
ton Factor: 1.00
JN UNITS:' 'Kg) UG/KG Q
20 : u J" •20 : 'J J"20 : rJj ;20 ^J20 : Uj20 : "J"20 ' UJ"20 ' US40 ' Uj-
260 ! T40 ! UJ-40 ! UJ i40 ;UJ40 'UJ~
200 ! UT40 : ur
200 !UJ200 : UT410 ;uj~200 : ur i200 !UT :200 : ur200 : ur i200 :uJ
12000 : j"400 : ui
t
FORM I
000113
Page 137
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. Chicago Refiners & Smelters
Lab Code: Case No.: SAS No.: SDG No.: —59—
SOW No.: ILM01.0
EPA Sample No. Lab Sample ID
-X102—-X102S-
-B115908-B115908S—-B115908D—-B115909-B115910-B115911-B115912-B115913-B115914-B115975-B115976-B115977-B115978-B115979-B115980
Vere ICP interelement corrections applied?
Were ICP background corrections applied?If yes, were raw data generated beforeapplication of background corrections?
Yes
Yes
No
Comments: -1.0 ML OF 1:1 HCL ADDED TO MICROWAVE DIGESTION PROCEDURE TOIMPROVE ANTIMONY RECOVERY. FIELD SAMPLE 1X111 AMD #X113 WERE INITIALLY-RECEIVED IN BROKEN BOTTLES AND THEN RESAMPLED.-
I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, for otherfr^at the conditions detailed above. Release of the data contained in this. .rdcopy data package has been authorized by the Laboratory Manager or theManager's des(S nee7Ss<* vesX.ified by the following signature.
Signature:Date:
Name:Title:
-ROY FRAZIE1-LAB MGR-
BOOOOOi
Page 138
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERS
Lab Code: Case No, SAS No.:
SOW No.: ILM01.0
SDG No.: —59—
EPA Sample No,
-XI10--XI17--XI18--XI11--XI13-
Lab Sample ID
B115981B115982B115983B116417B116418
Were ICP interelement corrections applied?
Were ICP background corrections applied?If yes, were raw data generated beforeapplication of background corrections?
Yes
Yes
No
Comments: -1.0 ML OF 1:1 HCL ADDED TO MICROWAVE DIGESTION PROCEDURE TOIMPROVE ANTIMONY RECOVERY. FIELD SAMPLE fXlll AND 1X113 WERE INITIALLYRECEIVED IN BROKEN BOTTLES AND THEN RESAMPLED
I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, for otherthat the conditions detailed above. Release of the data contained in thishardcopy data pacfakge has been authorized by the Laboratory Manager or theManager's deslgnee, Jas^ve^rif ied by the following signature.
Signature:Date:
Name:Title:
-ROY FRAZIER--LAB MGR
Rnnnnn-
Page 139
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO
X101
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERY
Matrix ( S<Level ( LoiX Solids:
Color Bef(Color Aft<Comments:
ail ) •j j. i. i .
^aac 11 u.. —
Lab
-56.5-Concentration Units (mg/kg dry weigl
CAS No.
7429-90-57440-36-0
7440-39 3
7440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-1743Q-Q5-4
7439-96-57439-97-67440-09-2
7440-09-77782-49-27440-22-47440-73— 57440-7ft-O
7440-62-27440-fifi-fi
-
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration i C;i
14300 !
45 5 ' '\
°se '5 3 '
56 5 !
57800 •76 fi '1 ° 7 ' E '
R1 fiO '
31500 !fiflfiQ '
0 4 5 0 0 ij
/t7' q« |
t
255051 '
1 i?1 0 ' '
1039 ' B35 ! u!-
27 *5
4970Q ' i -
1 5 U1
1
O1JVJ 11 U . . J3
Qqmnl i~ TT>- nil^Q?^
Date Received: 11/15/9:
Q ; M •
PM _:
E PM "T
E * , pu T"PM
- - . PM
E , ., .. . PM... 7
PM ,1 PMPM
PM
. , OM
•t, „ ,. pM
PM
t PM
E AS JT
-,_ . . PMii PM - -
S F , , . FM Ji
1 mE ! FM T
PM ,
AS1
1 '
! i
_ /^ 1 a T* 1 V A 4* t" T" • _-_ - f* 1 A ft T* - — Artifacts •
FORM I - INSOIL BOOOO i u 3 /X
Page 140
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE SO,
XI 0/2
Lab Name: ILLINOIS EPA CHAMPAIGN LABLab Code: Case No.:Matrix (Soil):Level (Low/Med):X Solids: -62.2-
Contract: N. CHICAGO REFINERS t SMELTERSSAS No.: SDG No.: —59—
Lab Sample ID: —B115908—Date Received: 11/14/91
Concentration Units (mg/kg dry weight):
CAS No. Analyte Concentration
Clarity Before: —Opaque-Clarity After: Clear—
Q
Artifacts:
M
7 4 * ? < } c i O » c ? Aluminum ' 1 fl?^rt ' nu
7440^-^f i -O Ant -i ntrtnv . 1 o n ; rr : p nu Ti '
7 4 4 0 - ? Q - - ^ RAPT urn
7 4 4 O 41 7 : ROT-V! 1 i um
74 4 O — 4 *3 — 9 PoHmiiim
17 fi F * FM
°°Q PM
-1 ^ PM
oa c ' TT nu
7 4 4 0 7 O ? r«.1 r* i um 1^2 00 i ! PM _.
sJ
T
7440 47 -T Phi-omi lira TC n ' nu
7440 4ft 4 fnhn.1 f l -
7 4 4 O — SO — ft PnrmoT*
j°0 0 : PM
ci nn i : DL<
74 TO ftQ fi Tr-nn T ft 000 , PM
7^9q_qo 1 T r-Ad .- - T T f i Q t FM
74*^Q«Q^ — 4. Mocfnooium - - - 1 fi 7 HO......... ' ^M
7400 qc c Montf an*»*>*» i OTrt * nu
7439-97-6 ' Morrurv •
7440 — 0? — ? i Ni r*1r*» 1
744O O1 — 7 ' Pni*««ainm
77f t?— r A Q ^ O ^oloniim - _— _- _-
744O ?? 4 ^il V^T-
74dO-2fl-0 ThAl 1 iu»
1 7/i4n-fiR-f5 7inr \
i
"'"d^if^' E \si en PM
1
3 500 PM
5 0 + p PM
9 0 , , , , : , , , , ' P M .
070 ' P PM
2 -t i ^ E ! FM
Tft O ' PM
>R400 ' i PM ,
1 *? i II ' \SI
I it !
J
J
J
Texture: -PintColor Before: -GrayColor After: -YellowComments: ICP RESULTS TAKEN FROM 5X DILUTION ZINC CHANNEL SATURATION.
FORM I - INSOIL BOOOOO: 3/90
Page 141
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO,
X103
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS i SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):X Solids: -72.3-
Case No.: SAS No.: SDG No.: —59—Lab Sample ID: —B115909—
Date Received: 11/14/91
Concentration Units (mg/kg dry weight):
CAS No. Analyte Concentration C-
Color Before: —BrowiColor After: —YellovComments:
Clarity Before: —Opaque-Clarity After: Clear—
Q M
7429-90-5
7440-^fi-O
7440-Tf t -?
7440-^Q — **
7440-4 1-7
7440-43-9
7440-70-?
7440—47-^
7440-48-4
i 7440-50-fi
7419-89-fi
. 741Q-Q2-1
74TQ-Q5-4
74qq Qf i_S
• 7440-02-2
7440-09-7
77R9-4Q-2
, 7440-22-4
i 744O — 2^-51 744O-28-O
i 7440-fi?-?
• 744O-fif i— fi!
1
i
R^r*vl 1 i urn
C* A rim i nm
Cobalt
r^ntiri^ T*
T *>aH
Ni rlr^l
c \ 1 V*»T*
T^i A Ili iim
7 1 T\f*
. - . - 1 2*50O PM .,07 O ' F PM T1 0 ^ ' \ F * . FM -T
IOC pM j
138 . . PM ;1° ft F ' PM T
i i15800 ' ! PM •'
fl° 0 - •' i PM i
15 0 i ' PM !1°700 PM i31100 i ' PM '-
1000 ! + * FM -T*i ;
1 0000 i PM ,1100 i + PM i
""fr'Sll *** F A^ TOt50 i PM !
150Q PM i
5 7. .- . J_, . + F FM, ^
6 0 PM Io .u inft 1 Q Ft PM
2 fi TI P FM ,301 O ' PM \
** "" *iOO i PM !
1 ° U ' AS--!
i ! i
i i i— Texture:Artifacts:
—Fine-
FORM I - INSOIL B000004 3/90
Page 142
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NC
X104
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERS
Matrix (ScLevel ( LovX Solids:
Color BefcColor Af t<Comments:
^___ ^•> i "M •j / M ^ H } *
-80.2-Concentration Units (mg /k
CAS No.
74297440-^fi-O
7440-38-27440-39-37440-4 1 -7
7440-43-97440-70-27440-47-3 '7440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-27440-09-77782-49-2
7440-22-47440-23-57440-28-07440-62-27440-66-6
Tab ^/imnlf* TD- ^ R 1 1 "5 Q 1 0
Date Received: 11/14/91
Analyte ; Concentration C; Q M
l
C n. 1 c i urn ' . , . . , . 12500i
Poha.lt 1°Pr*nr»r^T* .-,____....£ 0 OO
T cad , . . . . , . , . .2820
Mntf nr*«a i iim •-.- ——. — 01 Of)
Mrintf rin**^** -— — fifiO
PM
0 ' II ' P PM T. \j , u •- i • - — — -JL -— I'M \J
7 F * RM ^
i PM
1 ' ' pu .
1 F PM— .7. ' pu .
0 PM- -
5 ; PM —
i PM! i
pvi
i PM .* nn
McrcurT ' ^-K<T ** ' «• ! * c? T
Nicke l 102
C •• 1 xr**r* ^
Thallium 2
i
7-ir^r* 1 _ - 1 A 9 O n
iI
7
i ' PM
PM-R q p ; PM «r
? R ' PM,- J
PM.. ,t «•
fi U F FM J
0 PM '.u . , , rn ,! ! ' PM- .
O U AS -J1 1
1 11 i
! 1
FORM I - INson.
BOOOOO;/on
Page 143
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO
X105
Lab Name: ILLINOIS EPA CHAMPAIGN LABLab Code: Case No.:Matrix (Soil):Level (Low/Med):X Solids: -85.4-
Contract: N.SAS No.:
CHICAGO REFINERS i SMELTER;SDG No.: —59—ID: —B115976—
Date Received: 11/15/9:
Concentration Units (mg/kg dry weight):
CAS No. Anal7te 1 Concentration Q M' i !
7429744O-?fi — O
! 7440-38-2! 7440-39-3i 7440-41-7i 7440-43-97440-70-2
i 7440-47-^7440-48-4
! 7440-50-8: 7439-89-61 7439-92-1i 7439-95-4i 7439-96-5i 7439-97-6! 7440-02-2I 7440-09-7i 7782-49-2! 7440-22-4! 7440-23-5j 7440-28-0! 7440-62-2i 7440-66-6it
1
Color After: -Colorl*
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
•* Clariljss — Claril
1 1 °flO : PM
110 IT F PM Ti ,_
9\ .,-.-._,.. F * FM J
% ° fi PM ..
0 70 .. ; •• R PM .
° \ F PM 7T
32ROQ PM-1
21 Q . . , , , _ , PM . ,
9 A ,.,._.. R PM.
110 ' ' PM i
9 1 DOO i PM--
1 R 7 + t FM T
20300 i PM~~360 t ' PM !
"7r~~l_9 F - \°i T°fi S PM -
o o K o i PM 1
0 6 ft i W F ' FM "T1 q IT PM . j
oqn TT ! ' PM J
1 0 11 17 j T7W 7
oo 7 ! PM J
1 ? 0 i - PM -11 !
OOP . _ TT A I- <
i i i! i
FORM I - INSOIL B00001I 3/90
Page 144
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO
X106
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -79.8-
Case No. SAS No.: SDG No.: —59—Lab Sample ID: —B115977—
Date Received: 11/15/91
Concentration Units (mg/kg dry weight):
CAS No. Analyte Concentration
Color Before: —BrowiColor After: -Colorless—Comments:
Clarity Before:Clarity After:
—Opaque-Clear—
Q M
1 7429-90-5
7440-36-0
7440 ? ft - 2
' 7440-39-3
7440-41-7' 744O — 41-Q
; 7440-70-21 7440-47-1
7440-48-4
i 7440-50-8' 7439 89 6i 7439-92-1
7439-95-47439-96-5
'
' 7440-02-2
, 7440-OQ-7
• 77R2-49-2
i 7440-22-4
' 7440-21-5
' 7440-28-0
i 7 4 4 O — R7— 21 7440— fifi— fi
i
ii1
Ant" i fflon v
RA T* i vi inR*»T*V! 1 i lira
f* A 1 £* i tm
m
Cobalt
Iron
Lead
Mfl t fTi^Qi n IB
Ni rlr*» 1
Q i 1 V^T*
THA! 1 i nm
7i nr*
191 OO
1°
153i
81 QO°7
9
°o°oo90
6°001 30
o.TJ— •
930ni
3601
550i
' PM - -
0 U P PM T
O p * fM. "^
PM . ->_X0 R PM
5 p , PM . T
• PM ,
1 ' ] PM. . .'
2 E PM i
! PM i
0 t FM - .L PM . ,
i: * pM ..,
35° 1 -r4>2l ' F \^- tJ
•j . PM. j
B.I ... , , PM . J
5O ' W F FM. \J~~^
8 11 ' PM i
U - , , PM— i6 lA F FM tr
5 PM- ..i
PM. -
O TT \C! j
! ii ' \
i iTexture: —Pint
Artifacts:
FORM I - INSOIL BOOOOI2 3/90
Page 145
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO,
X107
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):X Solids: -82.1-
Case No.: SAS No.: SDG No.: —59—Lab Sample ID: —B115978—
Date Received: 11/15/91
Concentration Units (nig/kg dry weight):
1 CAS No.
1 7429-90-57440-36-0
\ 7440-39-37440-41-7
i 7440-43-97440-70-2
I 7440-47-37440-48-47440-50-8
i Analyte Concentration • C i Q M! ' l >
A 1 11 mi mi m . , , .11100 ' PM. .
A nt i mnmr . - - - 140 < U F PM 7
> A T-tmn i c~ Q 4 c * + , T7M T
Rji r ium : - ... • fi^ 6 ' PM ..: 1
Rn-pvl 1 i nm •_ - n 7n ; n ; r>n
1 Q ' t? nu rr1 '
P/il r i i im 2fi20n l nu '
o K r>L«
Pnhn.1 t Q 7 n ' DM
Pnr»n*a i~ 1 1
1T *-,J I 0
•5 i PMi
n ' PM in n * tru-_ * ~^—— i ^ - . ~ ,
74 3 9 --9 5 4 u—,.— _..•:.._ ! 1 Term ' nw
*! A *3 Q Q £ _ £)
7440-02-2j 7440-09-7
7782-49-27440-22-47440-23-5
i 7440-28-0i
7440-66-6
U^—.M.I.-. ^-A^Jo A C*V i T? ' * < ? * ! •
NT rlrr 1 ,. . -. .2
Poi~ n ^i nm __-..-_.. 9SO
QrtH T iivk -_ -_ 41
TVkol 1 i nm
7 1 Til™ ^ *>
ii
r* l •%•*%•! 4- •«» o^h.^j-s-*»«^ •
Color After: -Colorless — Clarity After:
7 ° ! ' PM '•
0 I ' PM . J
051 U W F ! FM ft.
2 0 , ! - l I PM.. J
O il ! PM.— J
11 u ' F ! FM ;T
0 5 ! ' PM ;
n 1 i PM J10 II i A^. - 1
i 1 i |i i i1 i
i Pi r*AYB-m«- AT*^ "i fnr*+ T •
FORM I -SOIL BOOOOI3 3/90
Page 146
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NC
X108
Lab Name: ILLINOIS EPA CHAMPAIGN LABLab Code: Case No.:Matrix (Soil):Level (Low/Med):X Solids: -82.3-
Contract: N.SAS No.:
CHICAGO REFINERS i SMELTERSSDG No.: —59—
Lab Sample ID: —Bl 15979—Date Received: 11/15/91
Concentration Units (mg/kg dry weight):
CAS No. Analyte Concentration
Color Before: —Black-Color After: -Yellow—Comments:
Clarity Before: —Opaque-Clarity After: Clear—
Q M
7429-90-5
7440-36-0
7440-38-2: 7440-39-3
7440-41-7
' 7440-43-97440 70-2
7440-47-37440-48-4
7440-50-8
7439-89-67439-92-17439-95-47439-96-57439-97-67440-02-9
7440-09-7
7782-49-9
7440-22-4
7440-23-5
7440-28-07440-62-27440-fifi-fi
Ant" i monvA r*^#*r> i c*P o r» 4 nm
fTHT*oni 11 m
fohal t
T T*rtn
T.A oH
MAC? no Q i iim
MATtt fAnAQA
MoY*fMi T*V
Mi r*lr«»l
Q A 1 on i 11 IB
Q i 1 VAT*
C oH i HM
Th A 111 tin
7 i r\f+
PvAni HA
11700
130 U '
°5 7179 ;
in • R :
1 6 '1 9^00 '
°9 3?1 fiJ i . D |
389 ! '°150Q i
4*5510*500
1 TS 0 ; i
T^'Sj* 'Tfi 7
"'TiO
1 n1 R II !
?70 11
15 a
^1 O
1 fiOO ! i
i n T Ti
!
°M i
E PM .T
E * .. . pi/, T -• rn- v^PM .
PM
E PM , T1 PM . .
PM !
PM .
puj '
' pu .
* FM .
i PM .
* PM
E \S IT
PM
PM. .
+ F FM J
PM- i
PM — «
E . . . i FM . rr1
PM 1
PM '1 A^ - i1 !1
Texture: —Fine-Artifacts:
FORM I - INRfinnni/i
Page 147
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO,
X109
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERSl_lttU VvUUC •
Matrix ( S<Level ( Loi% Solids:
Color Bef<Color Aft«Comments:
3 il ) •i i ; .j /Mr>rl \ •
uaac; «w • . — -
-88.5-Concentration
CAS No.
7429-90-57440-36-07440-38-27440-39-3
7440-41-77440-43-97440-70-2
7440-47-37440-48-47440-50-87439-89-67439-92-17419-95-47439-96-57439-97-67 4 4 0 — 0 9 — 27440-09-77782-49-27440-22-47440-23-5744O ?ft — f)
7440-62-27440-66-6
— — — — — ijfivj rtu . . — — _
Lab SD
Jnits (mg/kg dry weight
Analyte Concentration i C;1
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
R T 7 0no i!
95 : '6 7 0
19 ' i! 1
0 0 :
19900 '
11 i ! !8 n_ t a : P '
19121100 '- i
298<5fi3QQ ' '
386 '
4^LF<* !°0 ft i
ftOO ! RQ fil1 <? ! II
*50° R
0 69 (A1 7 9
fifiO !o q - 1 ' n
1ii
p 1 n T- i t- ir A^t-oi-' . f l r n r
ouu n<J . . L> J —
Amr>1*» in- Rl 1 S9fiO
ate Received: 11/15/9
) .
Q : M :
PM -^
E . PM. J
E ^ pvf -.TPM - »
PM
E PM "T
PM--
PM . ,
PM '
PM-
PM.«,
t FM- .
PM--
^ PM-
E AS. sT
PM .DM
I rn ,WF FM , L"T
PM -
PM . i
E . i ,. . . FM~ -TT
PM---
P M . (
AC . ,( ;I
;
A r+ \ ^nr*t" •> • . , . .
FORM I - INSOIL BOOOOI5 3/90
Page 148
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO,
X110
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSLittu v^uiac .
Matrix (SLevel ( LoiX Solids:
Color Bef<Color Aft«Comments:
n i M •
w/Mr-rf \ •
v^a^c iiv» • . — • • unu
-77.5-Concentration Units (mg/kg
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97d4n 7O— 9
74/10-47 — 1
7440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-27440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
T ah ^amril ** TH* A I I ^ Q f l l
Date Received: 11/15/91
1 Analyte Concentration C Q M
A 1 11 mi niim < « — . 1 ^ 1 0 0 .i '
nu
A n t - i m n n v , - .. . -—,--14 0 Ui F PM !T
ATQc*ni r • 7 ft i F * FM T
R n T- -i urn ... - - - — « . fl *? 0 I PMnOT.— i I ^ um _ Q 7Q j R PM-.-
r*riHmiiin - -« 10 ° ^ n" ^
f f i l f - i i i m 1 -- (ii?fiO
r*Ki-rtm 1 11 IB . ? 1 Q
Pohftl i- .. - -11 5i
Pf-iTM-kAr °fi Q
TT-rin . -19SQO
T rtnrl . ._._ A Q 0i
MrtntTrtncar: - 929.o<.
fH r-lr*» 1 . . ._«-?? Q
Pnt* A-atti !!• .. ?^f iO .
*? i lTr«%f - « . . 20
^nrlinvi — 4 D 1 .
Thti 1 1 i iim .... --- ,- .- 1 4
VanoH i iim - ?Q 1
7 i nr* .. — — 11?
iPM
PM—
B, „ . pu
..j.,, PM
i i PM
' * FMi tripu1 . rM
t PM3^0 • -rfl °r E A4? J
; pu
. . . . ' P M
1 U WE FM f t .
U * , .. . - i PMU i PM —
U F ! FM J"! TM• PH
U A"? .I
I
!!
sr: -Colorless — Clarity After: —— r* 1 /* nr* - r - - AT'^ ' i 'Ff t i"*^^* — .-. . ..
FORM I - IN BOOOO i 6
Page 149
U.S. EPA - CLP EPA SAMPLE NO,
INORGANIC ANALYSIS DATA SHEET i XI 11i
Lab Name :Lab Code :Matrix (S<Level (Loi% Solids:
-
-
Color BefcColor Aft«Comments:
ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSf- M— • OAO vi~ . on/-> vr_ . en
-,il \ .
•r/Meri \ •L
-89.2-Concentration Units (mg/kg dry we
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-4 1-77440-43-97440-70-27440-47-37440-48-47440-50-874. Q ft Q — fi
741Q-99-1
7439 96-57439-97-67440-02-27440-09-77782-49-27440-22-47440-23-57440-28-07440-69-2
7440-66-6
»r: -Colorl*
Analyte Concentration C
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
i Clarilsss — Claril
Date Received: 11/26/91
i tfhf ) • ....,,
Q : M '
A °fiO PM _
110 TI ' F PM T90' c- * c-w T
1 01 6
1QQfiQO
TO C
fi •? Ft
710
PMPM
E ; PM IT
PM .,
PM ,1 DM }
DLf
. , i Q i on ' PM.°fiS 1 FM-
i i47°nn i PM -fifiO * n"
o- ™5u?
oo'o 1
730 BO g g0 0 TI
17 M101 _ n ,
1 * "
E A<v 1
' PM. -
PM ,
W R. — -• .. FM T
PM...-
PM- -
E_. «.— . 1., FM ^T
PM -
PM M
A<^ 1
'•
ty After: Clear-
FORM I - INSOTT. Rnnnni9
Page 150
U.S. EPA - CLP EPA SAMPLE
INORGANIC ANALYSIS DATA SHEET j XI 12
Lab NameLab CodeMatrix (Level (LX Solids
: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERir>n*,p. Wo • OAC vr- . or\/i »T_ . c n
q0 : l ) .
nu /Mort \ •
: -76.5-Concentration Units (
T nh ^nnrnl r- T F » * R 1 1 S Q 1 1
Date Received: 11/14/91
m tf/lrtf HT*TT w ^ i r f h ' f r ' ^ * _ _, - _
CAS No. Analyte Concentration ' C; Q M
Color BeColor AfComments
' 7/1 9O — Qfi ^ ^ A l u m i n u mI !
1A.A.r\ — Tfi — fl A n t i m n m r
7 A A n Ifl 9 Ayisonio
7il dn^ 1 Q-. T R n y i n m ' .
744O 41-7 Re nr Il ium
1 A. 4D^ A T-- 1 : PaHmi i im
744O 7O ? f j i l r i i im ! .
' 7ddn 47 "\ Ph-romi urn '-
7440-df l -4 Coha.lt -. -
7-140 — fi — A Pfrnn^T*
' 7439-89-6 Iron 17410 12 1 T r>jid ... _ . .
i 74 in .OS d Mnffnr -^ i nm 3
'• 74 on ,. nc c M« nrf An*»-=tn
7^ ' i q^q7_e | Mm~riiT-vi i
7440-0? 9 NT r-k^l1 7/1 .4 n OQ 7 ' P n ^ a O Q i i i m
7700^40^9 ! «:^lAniiiiii
7440 ?2 4 S i lv fT*7440--?^-*? : ^nH i un
7 4 4 O ?ft-O TViJil 1 i iim
744O-fi2-2 VanAHi nm
7 4 4 O fifi-fi 7i nr-
i
ii
40OO , PM
1 4 0 ' i f ' F P M " T
9 *5 - ! ^ F 'f FM f _f
400 PM .- .
3 *5 : 1 PM .
o o p PM--J"
7flOO : ' ' PM -
*57 0 PM
6 1 - - ;. PM —HOO PM
6600 ! PM6 15 : * FM.
7°00 PM .
IRQ ' t PMt ou -» -» <s • T rn
~#4i^'i E : \2 T1° 0 ' PM
fiQO R * PM- - -'
0 *50- -U W F ! FM- -C
1 9 i PM m
pqn R PM- .
1 fi U W F FM IT
9 1 . R PM--
4 1! 70 . . I 1 PM--
U A m A ^ » — .
I
1
ter: —Colorless — Clarity Aftcl T* * f I ^fii* A l ^ ^ T ^ r t l ^ ^ ^ * .... .
FORM I - IN BOOOOOo
Page 151
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
X113
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -74.9-
Case No. SAS No.: SDG No.: —59—Lab Sample ID: —B116418—
Date Received: 11/26/91
Concentration Units (mg/kg dry weight):
CAS No. Analyte Concentration Q M
' 749Q-QO 5
7440-36 0
7440-38-2
' 7440-3Q-3
7440-41-7
• 7440-43-Q
7440-70-7
7440-47-?
7440-48-47440-50-87 4 T q _ Q q _ f i
743q~q2-l7439-95-4
743q-q6-5
7439-97-6744O— O9— 9
7440-09-777R7-4.Q— 9
i7ddn-??-47ddO— 91— **744f i -? f t— O
7440-62-2
744O-6fi-fi1
Ant* i monv
R^Tvl 1 "i 11 m
Cobalt
T,*»Ari
M^T*r*iiT*v\i 4 Irol
C i 1 \r A v*
ThA.1 1 i tin
VAnnH i tin
7i nof^TTATl 1 HA
^ inn !
M O TJ
6 59 ^ 0 '
0 50 R1 6
700OO i '
1 fi \ ' i
7 3 B•57 ° !
1 'I'lOO '
103
1Q°00
\ °7
>^ i i°? 1 i
1 100 '0 5 3 T Io q |
4?0 TI
050 M
1 5 6
210
1 1 T Ii
ii
1 nM
E PM rrE ^t . ' pw *r
PM !
i PM i
E ; PM iT
PM —
PM j
PM --i
PM. . ,
PM
* PM,. -
i PM 't PM -J
E A*? IT
' PM '
PM i
¥ P FM fi.
i PM .
PMi-
4- p PM ^T
PM J
PM !
A- i1 j
ii
Color Before: —BrowiColor After: -Yellow-Comments:
Clarity Before:Clarity After:
—Opaque-Clear—
Texture: —Fine-Artifacts:
FORM I - INSOIL B000020
Page 152
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAHPLE NO
X114
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS &. SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -76.8-
Case No. SAS No.: SDG No.: —59—Lab Sample ID: —B115912—
Date Received: 11/14/91
Concentration Units (mg/kg dry weight):
! CAS No. Analyte1 ;7499—90—5 • Aluminum
7440-36-0 Antimony, 7440-38-2 Arsenic7440-39-3 Barium7440-41 7 Bervllium
' 7440—43—9 Cadmium1
74.40 — 70-2 Calc ium
j 7440-47-3 Chromium7440-48-4 i Cobalt
\ 7440-50-8 ! Copper] 7439-89-6 Iron7439 92-1 Lead7439-95-4 ; Magnesium
j 7439-96-5 Manganese
1 7440-02-2 Nickel
i 7440-09-7 Potassium' 7782-49-2 Selenium
i 7440-22-4 Silver1 7440-23-5 Sodiuml 7440-28-0 Thalliumi 7440-62-2 Vanadium1 7440-66-6 Zinc
1i
!
Concentration C ! Q M
i 3600 * ' PM1 i i110 II F PM
1 9 fi 1 ' F * FM -
°fi fi B PM .
0 50 U PM\
0 99 U i F PM
\ "5*5 00 i PM
U 7 '' \ PM
1 R i H '• PMi
01 ? ! PM!
10300 ' PM '3 ft A * ' PM
9 9 inn ' ou
390 ! t ' PM""^ ~ft~ 5 1 C1 AC
13 3 ^ PMI ic *> A o ' nu '
O SO- *— U F ', FM
2 Q i n ' pM ;
100 u' i PM iU I ; ;
0.. _L_ . *4— F ! FM
107 B ' ! PM '
fl° 0 ! ' PM i
1 1 IT' ' A<n
i!
! i I
Color After: -Colorless — ClarihTT A^^OT** ("* 1 f*fiT* AT"h 1 Af*^ W* __- -
1
T
T
T
[ium
FORM I - IN
Page 153
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO,
X115
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSuau isuuc .
Matrix ( S<Level ( LoiX Solids:
Color Bef<Color Aft*Comments:
D i 1 ) ••r/Mr-H } •
_ T^UCoi-^l—Tn. D 1 1 R Q 1 O
-79.4-Concentration \
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-874^Q-ft<?-fi
7439-92-17439-95-47d^Q-Qfi-57439-97-6744ft— O9-?
744O-OQ 7
77R2-49-2
7440-22-4744O — 91 — *>
7440-28-07440-62-27440-66-6
Date Received: 11/14/9
Jni tn fmsf/lrtf HT*V wf^irfht"^*
1
Analyte Concentration I C Q M! i :
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
11 °Q f ' PM1 • •«
130 ; 17 F PM ,T5 8 i P * FM T
4fl 5 ' PM0 SO ; R PM0 1 : F PM J
74HQO ' PM-,700 pu
1 0 - r R PM ..
qni ' ^M jqo-M ! ' "M ;1 990 t PM !T7°00 : PM .
?70 * PM i4/UO.T37 1P1
-ft 50 at F A<^ ^T1 C ft U [ pu
fifiO B PM '
0 46- »— IT' W F FM..-.fl.
A an n PM_ .
0 70 • 1 F FM .T
76 H PM 1O7f> ; pM. _
1 ^ A*^ - ii
r
jr: -Colorless — ClarihvA-f+jar'* pi rriT" - Art i f firt.n *
FORM I - INSOIL B000006 3/90
Page 154
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NC'
X116
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -78.6-
Case No.: SAS No.: SDG No.: —59—Lab Sample ID: —B115914—
Date Received: 11/14/91
Concentration Units (mg/kg dry weight):
CAS No. Concentration
Color Before: —BrownColor After: —ColorlessComments:
Clarity Before: —Opaque-Clarity After: Clear—
M
7429-90-57440-36-07440 38-2
i 7440-39-37440-41-7
• 7440-43-97440-70-2744O-47 37440-48-4
7440-50-87439-89-67439-92-1
7439-95 4
7439-96-57439-97-67440-02-27440-09-77782-49-27440-22-4
i 7440-23-57440-28-07440-62-27440-66-6
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium0
IronLjG&d
Magnesium
MercuryNickelPotassiumSeleniumSilverSodiumThallium
ZincCyanide
i
T 1 30
onni
1 fi7'
611 1 OO
fMfl
630
28570
n
| ; ' PM. .
O n F PM ,."**1 F * FM . . J^-
8 ! B ' PM !A n i , n ; ' PM. .
6 ' F PM vTPM .. J
8 PM i
1 -0 OL*
DW :
PM ^
' FMt
PM -
t ! PM i0.3** ; L •_T 2J _ J E» * 0 ~
1
5 1
Q
105O9
1
53
a
PM i
B PM !
U i W F FM .. .Q
PM.-4
U ; i PM ..J
n • nu '.1 1
r»Li
.1 U i A°l .-i! 1
ii
Texture: MediumArtifacts:
FORM I - IN BOOOOO^
Page 155
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO,
X117
Lab Name: ILLINOIS EPA CHAMPAIGN LABLab Code: Case No. :Matrix (Soil):Level (Low/Med):X Solids: -78.4-
Contract: N. CHICAGO REFINERS i SMELTERSSAS No.: SDG No.: —59—
Lab Sample ID: —B115982—Date Received: 11/15/91
Concentration Units (mg/kg dry weight):
CAS No. Analyte Concentration Q M
1 7429-90-5
7440-36-07440-38-27440-39-37440-41-77440-43-97440-70-2
7440-47-37440-4K-4744O-5O-R
7439-89-67439-92-17439-95-47439-96-574"lQ_u'7_fi
i 7440-02-27440-09-7
| 7782-49-27440-22-4
1 7440-23-5! 744O— 9 f t — O1 7440-62-2I 7440-66-6ii ..___
!
1 — »^«__- ii • •Ij
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
1 fi°00 I110 ; IT '09 o ! !
? fl 7
5? ft :
S I R i >I f i f t O Q
TRO !
39 0 ' 'R 1 ?nn ' 'fiOfiOG ''
1 T'OO '
SQftO ;
°760 '~ \i1ta I
>Il <=* 'n.4 | i1 07O '
410 ' TT !
8 4 - \
37 iO f i O C
2 fi- . 11
8 ^ . . p '- - 1 Of t^Of l '
11 - TT
[ Ii
' PM ^
E PM \T
S F * PM .T
PM ^j
i PM '
E PM. ,3*
' PM, tn {1 PM -i1 PM !
nM i
' PM. i
t ! FM '1 PM 1
t ! PM i
E i AS TPM I
! 1
! PM J
S f . ! PM ,T
PM i
1 PM
E ^ PM J*rPM
PM
, AC
I A-ii
Art i f act1 a • - -
FORM I - INSOIL
BOOOOI 73/90
Page 156
U.S. EPA - CLP1
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NC
X118
Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS A. SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -80.7-
Case No.: SAS No.: SDG No.: -59—Lab Sample ID: —B115983—
Date Received: 11/15/91
Concentration Units (ing/kg dry weight):
CAS No. Analyte Concentration ! C Q M
1 74?<?-Q0^5 ' A l u m i n u m ' 10800 PM ,
7 4 4 0 ^ T f i — 0 A n f i m o n v —60 4 ' i F PM "*"
7 4 4 0 T f i 2 A r ^ p r i - i « ~ ' . - 1 9 7 - ' - ' ^ F * FM 7*-
7 4 4 O TQ-^1 ' Rj iT-ium . T ? 1 ' i PM
7440 41 7 Ben-I l ium 7 5 : PM
7 4 4 O — 41— 9 r*AHmi iim 1 ft ^ ' ^ ^^
7440-70-2 r j i l r i nm .-.. -19TO n ' n»*I
744O — 47--T PhT^nmi i im ' • S 1 1 ' OXJ
J
744O-4H-4 Pobalt . ... . - - I f l S ' PM
74^9 ft 9 fi Tr-on ^^ f l f l
7419 92 1 ' r*»AH , 479
74?9 9^ — 4 Mntfn^ta-i iim fi^fl
7 A oq 07 c MoT^r^ii'rT "^
1 7440-02-2 Nickel . -.-16
7440-09—7 Pot fl^tai nm 9?
77ft? 49 2 ^o I o n i u m
0 : *'M
0 ' '•• * ' FM
o - ; PMO ' -t PM35.9^ : • . P ,"^KJ? CA i \ F '\<?0 PM
0 R PMoo o t? ' trw
7440 22 4 ' ^-i Ivo-r — . - 2° ° ! nu '
7440--23-5 Sodium 114
7440-2B-0 T h a l l i n n t 2
7440-R2 2 Vann^i i iHi - — ..,5
' 74 4O fifi fi 7i nr- 1 9 4 C
i
0 B ' PM '
fi 6 Vl E ' FM '0 1 i PM
0 ' PM
1 0 U i ' A<?
t '
T
>_
T
T
Color Before: —Black-Color After: -Yellow-Comments:
Clarity Before: —Opaque-Clarity After: Clear-
Texture: -FineArtifacts:
FORM I - IN BOOOOI8