s A/ec&ssy. lyg^c^ /s - United States Environmental ... · U.S. ENVIRONMENTAL PROTECT N AGENCY - HWI Sample Mana^ .jcnt Office P.O. Box 81S - Alexandria, Virginia 22313 - 703/...

Call (made by) (raoaivod by - t/ X

Suranary:

/s A/ec&ssy. lyg^c^ /s

REPORT OF TELEPHONE CONVERSATION

Date:

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EPA III-031-74-T

U.S. ENVIRONMENTAL PROTECT. N AGENCY - HWI Sample Mnnag, <cnt OfficeP.O. Box SI?'- Alexandria, Virginia 22313 - 703/ 557-2490/FTS-8-557-2490

INORGANICS ANALYSIS DATA SHEET^ 585-16

LABORATORY NAME

LAB

1.2.3.

5.6.7.3.9.

•

1.2.3.

1.. -2.3.

SAMPLE ID NO.

AluminumChromiumBariumBerylliumCadmiumCobaltCopperIronLead

ArsenicAntimonySeleniumThallium

AmmoniaFluor ideSulfide

Versar SAMPLE NO. MC0093

4657 OC REPORT NO. 4

TASK 1 (Elements to be identified and measured)

ug/114. inn 10. Nickel finiqn. 11. Manganese ?nnan. 12. Zinc mo.2. 13. Boron 70.<5. 1*. Vanadium so.10. 15. Calciunr 5,900.60. 16. Magnesium 4,800.35,000. 17. Sodium 4,800.

<40.


ug/130. 5. Mercury <1.

<20. s. Tin 30.<10. 7. Silver <20.<10.


mg/1 *. Cyanidemg/1 5. pHmg/1 6. TOC

•

ug/1

.

ug/1

mg/1Unitsmg/1

COMMENTS:

&RIOQM8

U.S. ENVIRONMENTAL PROTECT. ,N AGENCY - HW1 Sample Manafc, ,>cnt OfficeP.O. .Box Sl.S - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-B-557-2490

INORGANICS ANALYSIS DATA SHEET585-16

LABORATORY NAME Versar_____ SAMPLE NO. MC00944658

LAB SAMPLE ID NO.__________________ QC REPORT NO.

6. Cobalt__________<1Q._______ . 15. Calcium______6,400.7. Copper_________<20._______ 16. Magnesium____1,100*8. Iron 100. 17. Sodium 2,300.9. Lead <40.

Thallium


ug/1 ug/11. Aluminum________<5n.________ 10. Nickel_______<2Q.__________________2. Chromium_______<IQ._______ 11. Manganese____20.___________________3. Barium__________10._______ 12. Zinc________30_,__________________4. Beryllium________<2,__________[ 13. Boron ______20_._______;____5. Cadmium <5. 1*. Vanadium <10.


ug/1 ' ug/11. Arsenic_________<1Q-_______ 5. Mercury_____<:L'_____________________2. Antimony________<20-_______ 6. Tin________<2Q-_____________3. Selenium <10- 7. Silver <2°-


1. Ammonia_______________mg/1 4. Cyanide_________________mg/1•2. Fluor ide_______________mg/1 5. £H___________________Units3. Sulfide_________________mg/1 6. TOC___________________mg/1

COMMENTS: ' o

flRIOOl»!9

U.S. ENVIRONMENTAL PROTECT N AGENCY - HWI Sarnpjc Manag, »cnt OfficeP.O. Box 81 &- Alexandria, Virginia 22313 - 703/557-2490/FTS-8-557-2490


LABORATORY NAME Versar_________ SAMPLE NO. MC00954659



ug/1 ug/11. Aluminum_______ 11.900._____ 10. Nickel_______40.______________________2. Chromium_____ IQQ.______ 11. Manganese____50. ________________3. Barium_____._____40._______ 12. Zinc_________IQQ.______________*. Beryllium________2._______ 13. Boron _____80.______;____5. Cadmium <5. 1*. Vanadium 90.

Thallium

6. Cobalt___________10._______ 15. Calcium______4,800.___________7. Copper__________40.__________ 16. Magnesium____4,500.________________8. Iron_______________58,100.____ 17. Sodium_______2,200.___________9. Lead_______________<40._______


ug/1 ' ug/11. Arsenic__________£j;___________ 5. Mercury_____^____________2. Antimony_______<2°-_______ 6. Tin_________^_____________3. Selenium <10- 7. Silver <2°-


1. Ammonia_______________________mg/I 4. Cyanide________________mg/1•2. Fluor ide________________mg/1 5. pjj_____________________________________Units3. Sulfide________________mg/1 6. TOC__________________mg/1

COMMENTS: ' ^

ARIOOU20

U.S. ENVIRONMENTAL PROTECT N AGENCY - HWI Sample Mana^ .jcnt OfficeP.O. Box 81S - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-8-557-2490

INORGANICS ANALYSIS DATA SHEET

585-16

LABORATORY NAME Versar___ SAMPLE NO. MC00964660


Thallium


ug/1 ug/11. Aluminum_________123.QQQ.____ 10. Nickel_______120.________________2. Chromium________1.140._____ 11. Manganese____I,QQQ._______________3. Barium___________260._______ 12. Zinc_________770.________________4. Beryllium_________16._______ 13. Boron ______1,000._____:______5. Cadmium_________15._______ 1*. Vanadium_____890._____________________6. Cobalt__________70._______ 15. Calcium______12,500.__________7. Copper__________300.______ 16. Magnesium____33,900._____________8. Iron____________539,000. 17. Sodium_______3,300.__________________9. Lead___________<40.____________


ug/1 ' ug/11. Arsenic_________19°-______ 5. Mercury_____<3--___________________2. Antimony________<20-_______ 6. Tin________<2Q-_____________3. Selenium <10- 7. Silver <2°-


1. Ammonia____________ mg/1 4. Cyanide________________mg/1•2. Fluor ide________________mg/1 5. pjj____________________Units3. Sulfide_____;____________mg/1 6. TOC___________________mg/1

COMMENTS:

RRIOOI+21

U.S. ENVIRONMENTAL PROTECT. N AGENCY - HWI Sample Manag. <cnt OfficeP.O. Box 81 5-- Alexandria, Virginia 22313 - 7Q3/ 557-2490/FTS-8-557-2490

^^ INORGANICS ANALYSIS DATA SHEETB 585-16

LABORATORY NAME

LAB SAMPLE ID NO.

1. Aluminum2. Chromium3. Barium*. Beryllium5. Cadmium6. Cobalt7. Copper8. Iron9. Lead

•1. Arsenic2. Antimony3. Selenium4. Thallium

1. Ammonia-2. Fluoride3. Sulfide

V<PT«?flT"

4661SAMPLE NO. MTQn97

QC REPORT NO. 4


ug/135,900.* 10. Nickel 120.*220.*160.*12.*<5.*60.*40.*125,000.*<40.*

TASK 2 (Elements

ug/150.

<20.<10.<10.

TASK 3 (Elements

mg/1mg/1mg/1

11. Manganese 340.*12. Zinc 655.*13. Boron 135.*1*. Vanadium 290.*15. Calcium 11,800.*16. Magnesium 8,450.*17. Sodium 2,000.*

to be identified and measured)

5. Mercury <J-6. Tin <20.7. Silver <20.


4. Cyanide5. pH6. TOC

ug/1

.

ug/1

mg/IUnitsmg/1

•

COMMENTS:*Mean of 2 determinations.

U.S. ENVIRONMENTAL PROTEC. JN AGENCY - HWI Sample ManaL ncnt OfficeP.O. Box 81S - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-8-557-2490


LABORATORY NAME v^rsar__________ SAMPLE NO.

LAB SAMPLE ID NO. 4662___________ QC REPORT NO.

*. Beryllium________4.________ 13. Boron _____3,460.5, Cadmium <5. 14. Vanadium 80.6. Cobalt 20. 15. Calcium 74,500.7. Copper__________20.________ 16. Magnesium____27,100.8. Iron____________70,100._____ 17. Sodium______93,700.9. Lead <40.

>lj


ug/1 ug/11. Aluminum________16,000._____ 10. Nickel_______180._________________2. Chromium________120._______ 11. Manganese____2,890.______________3. Barium 710. 12. Zinc 270.


ug/1 ' ug/11. Arsenic_________30._______ 5. Mercury____<i.________________2. Antimony_______<20.________ 6. Tin________<2Q_.___________________3. Selenium_______<io. ______. 7. Silver______<20._________________4. Thallium


1. Ammonia______________mg/1 4. Cyanide________________mg/I•2. Fluor ide________________mg/I 5. p_H____________________Units3. Sulfide_________________mg/1 6. TOC___________________mg/1

COMMENTS:

U.S. ENVIRONMENTAL PROTEC. -N AGENCY - HWI SarnpJc ManaL .icnt OfficeP.O. Cox 81.S - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-8-557-2490

INORGANICS ANALYSIS DATA SHEET585-16_______

LABORATORY NAME yeysse___ SAMPLE NO.



ug/1 ug/11. Aluminum________550.______ 10. Nickel_______<20._____________2. Chromium___________<5.________^ 11. Manganese ___'100.__________________3. Barium__________20. 12. Zinc <10.*. Beryllium________<2.________ 13. Boron ______20.5. Cadmium <5. 1 . Vanadium <10.6. Cobalt <10. 15. Calcium 1,200.7. Copper_________<20._______ 16. Magnesium____900.8. Iron_______________6,080._____ 17. Sodium_______2yQQO.9. Lead <40.


ug/1 ' ug/1.1. Arsenic_________<IQ._______ 5. Mercury_____<i.________________2. Antimony__________<20._______ 6. Tin________<20._______________3. Selenium________<1Q_.______. 7. Silver______<20.____________________it. Thallium

TASK 3 (Bements to be identified and measured)

1. Ammonia_______________mg/1 4. Cyanide_________________mg/I-2. Fluoride____;___________mg/1 5. g_H____________________Units3. Sulfide________________mg/1 6. TOC__________________mg/1

COMMENTS: ' ^ o

~.~ X 3

-A

Pace 1 of 1

Tasx I: iismencs zo oe icentinec anc r.easurac _y .ncuc-ive«yCoupled Arson Plasma Spec-rcraezer or comparable alt.err.azefrom Appendix ?

Minimum Reporting Level, ug/1

1. Aluminum 502. Chromium 102. Barium 104. Beryllium 25. Cadmium 56. Cobalt , 107. Copper 208. Iron 209. Lead 40

10. Nickel 2011. Mancanese . 1012. Zinc 1013. Boron . 1014. Vanadium 1015. Calcium 100IS. Magnesium 10017. Sodium 100

Task 2: Elements to be Identified and Measured by Flame/?lameless Atomic Absorption Spectrometer or comparable alternatefrom Appendix F

Minimum Reporting Level, uc/1

1. Arsenic ' 102. Antimonv • 20•3. Selenium 104. Thallium , 10'5. Mercury- " 16. Tin " . 207. 'Silver 20

Taske 3: Inorganic Parameters to be Identified and Measuredby Procedures Specified in Appendix E. and/or Appendix F.


1. Ammonia 1002. Fluoride 2003. Sulfice 504. Cyanide 105. oH within 0.1 oH ur.i.c6. TCC 2,000 " *?

ARIOOU25

U.S. ENVIRONMENTAL PROTECTION AGENCY - HWI Sample Management OfficeP.O. Box 81-8 - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-B-557-2490

^^ INORGANICS ANALYSIS DATA SHEET «, r- on «

9 585~15 an niAGoadLABORATORY NAME

LAB SAMPLE ID NO.

1. Aluminum2. Chromium3. Barium4. Beryllium5. Cadmium6. Cobalt7. Copper8. Iron9. Lead

. fl k_~*

1. Arsenic2. Antimony3. Selenium14. Thallium

1. Ammonia•2. Fluor ide3. Suifide

Versar4643

• SAMPLE NO. MC0078

QC REPORT NO. 4


ug/1 ug/1<50. ' 10. Nickel <20.<10.40.<2.<5.<10.100.120.<40.

TASK 2 (Elements

ug/1<10.<20.<10,<10.

TASK 3 (Oements

mg/1mg/1mg/1

11. Manganese <10.12. Zinc 50.13. Boron 10.1*. Vanadium <10.15. Calcium 8,800.16. Magnesium 6,900.17. Sodium 4,400.


ug/15. Mercury <1;6. Tin <20.7. Silver <20.


4. Cyanide mg/15. pH Units6. TOC . mg/1

COMMENTS:

U.S. ENVIRONMENTAL PROTECTION AGENCY - HWI Sample Management OfficeP.O. Box 818 - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-8-557-2490


LABORATORY NAME Versar___ SAMPLE NO. MC0079


Beryllium________<2.________ 13. Boron ______70.Cadmium <5. 14. Vanadium <10.

6. Cobalt <10. 15. Calcium 6,900.7. Copper__________<20._______ 16. Magnesium____2,090.8. Iron____________17,300.____ 17. Sodium_______6,470.9. Lead <40.

Thallium3. Selenium <10> 7. Silver <2CL


ug/1 ug/11. Aluminum________<50.____' 10. Nickel_______<20. _________________2. Chromium________<10._______ 11. Manganese_____30.____________________3. Barium 40. 12. Zinc <10.


ug/1 ' ug/11. Arsenic_________<^*_______ 5. Mercury_____<-*-'______________________2. Antimony_______<2°-_______ 6. Tin________<2°-___________


I. Ammonia______________mg/1 4. Cyanide________________mg/1-2» Fluor ide________________mg/1 5. gH_____________________Units3. Sulfide________________mg/1 6. TOC__________________mg/1

COMMENTS:

ftR!OOl427

December '979?=ce 1 of 1

Task 1: llemer.cs to oe Identified and measured sy I.ncuctive^yCoupled Argon Plasma Soeczrcmeter or comparable alterr.a-afrom Appendix F

Minimum P.eportinc Level, ug/1

1. Aluminum 502. Chromium 103. Barium 104. Beryllium 25. Cadmium 56. Cobalt 107. Copper 208. Iron 209. Lead 40

10. Nickel 2011. Mancanese 1012. Zinc 1013. Soron . 1014. Vanadium 1015. Calcium 10016. Magnesium 10017. Sodium 100

Task 2: Elements to be Identified and Measured by 'Flame/Flameless Atomic Absorption Spectrometer or comparable alternatefrom Appendix F


1. Arsenic ' 102 . Antimonv - 2 0'3. Selenium 104. Thallium , 10

' 5. Mercurv• 16. Tin * 207. Silver 20

Taske 3: Inorganic Parameters to be Identified and Measuredby Procedures Specified in Appendix E. and/or Appendix ?.

Minimum Reporting Level/ ug/1

1. Ammonia 1002. Fluoride 2003. Sulfide • 504. Cyanide 105. oH within 0.1 ?H units6. TOC 2,000

BR1001*28

. i n .WftdnflfT V^ Qfe\t fcV

U.S. ENVIRONMENTAL PROTECTION AGENCY - HWI Sample Management Office T 1P.O. ftox 818 - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-8-557-2490

INORGANICS ANALYSIS DATA SHEET585-11 fc

LABORATORY NAME

LAB SAMPLE ID NO.

1. Aluminum2. Chromium3. Barium4. Beryllium5. Cadmium6. Cobalt7. Copper8. Iron9. Lead

1. Arsenic2, Antimony3. Selenium4. Thallium

1. Ammonia•2. Fluor ide3. Sulfide

Versar

4497

SAMPLE NO. MC8045

QC REPORT NO. 3


ug/1 ug/1<50. 10. Nickel <20.<10.70.

< 2.< 5.<10.20.<20.<40.

TASK 2 (Elements

ug/1

<20.<10.<10.

TASK 3 (Elements

mg/1mg/1mg/1

11. Manganese 80.12. Zinc 980.13. Boron <10.1*. Vanadium <10.15. Calcium 7,800.16. Magnesium 3,900.17. Sodium 6,300.

to be identified and measured) ^ B

ug/15. Mercury < 1-6. Tin <20.7. Silver <20.


4. Cyanide mg/15. pH Units6. TOC mg/1

-COMMENTS:

p,.(1.5. ENVIRONMENTAL PROTECTION AGENCY - HWI Sample Management Office I 1P.O. Box 818 - Alexandria, Virginia 22313 - 703/ 557-2490/FTS-8-557-2490

^^ INORGANICS ANALYSIS DATA SHEETP 585-11

LABORATORY NAME

LAB SAMPLE ID NO.

I. Aluminum2. Chromium3. Barium*. Beryllium5. Cadmium6. Cobalt7. Copper8. Iron9. Lead

1. Arsenic2. Antimony3. Selenium4. Thallium

1. Ammonia•2. Fluor ide3. Sulfide

Versar SAMPLE NO. MC8044

4496 QC REPORT NO. 3


ug/1200. 10. Nickel 150.<10. 1L150. 12.

< 2- 13.45. i_.m20. 15.

40- 16.1,240. 17.<40.

Manganese 690.Zinc 5,050.Boron < 10.Vanadium < 10.Calcium 82,600.Magnesium 34,500.Sodium 52,200.


ug/1<10. 5. Mercury < 1-<20. 6.<_LO • TT/ *<10.

Tin <20.Silver <20.


mg/1 4. Cyanidemg/1 5.mg/1 6.

PHTOC

ug/1

.

.,

ug/1

mg/1Unitsmg/1

COMMENTS:

ftRiOOU30

U.S. ENVIRONMENTAL PROTECTION AGENCY - HWI Sample Management OfficeP.O. Dox-8.18 - Alexandria, Virginia 22313 - 703/' 557-2490/FTS-8-557-2490 \

INORGANICS ANALYSIS DATA SHEET

LABORATORY NAME Versar • SAMPLE NO. MC8043

LAB SAMPLE ID NO.______4495_________ QC REPORT NO.

4. Beryllium__________< 2._____ 13. Boron _______20.5. Cadmium 3,810. 14. Vanadium6. Cobalt 570. 15. Calcium 51,600.7. Copper____________200._____ lg. Magnesium 26,200.8. Iron____________1/0*0-_____ 17. Sodium_____26,600.9. Lead <4°-

AUS


300. u§/! 600. u§/]1. Aluminum___________________ 10. Nickel_______________________2. Chromium____;________pj_____ 11. Manganese___31,100.__________________3. Barium 80- 12. Zinc 194,000.


ug/1 ' ug/11. Arsenic___________<1Q-_____ 5. Mercury_______<_;!•__________2. Antimony__________<2°-_____ 6. Tin__________<50.*___________3. Selenium____________£______ 7. Silver________<20._______________4. Thallium__________<1Q-_____


1. Ammonia_______________mg/1 4. Cyanide_________________mg/12. Fluor Ide________________mg/1 5. £H____________________Units3. Sulfide____________ mg/1 6. TOC___________________mg/1

COMMENTS:

*Interference, did not allow normal detection limit.

s A/ec&ssy. lyg^c^ /s - United States Environmental ... · U.S. ENVIRONMENTAL PROTECT N AGENCY - HWI Sample Mana^ .jcnt Office P.O. Box 81S - Alexandria, Virginia 22313 - 703/...

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