Rev 2 to Procedure 12 PMP 3150 PCP.001, …xiiiarv Build'ng o eea must be place1 ed intoi a container, b keat from entering are 1 soi's must e. s and must be cleane u d t 1 3.2 No

~ 0

o ~ r I '~

'I I' ~

~ ~ ~ ~ ~ ~ ~ ~ ~ ~

~ ~ ~ ~ ~ 0 ~ ~ ~ ~ ~ ~ 0 ~ ~

~ 4 ~ 0 ~

~ ~ ~ ~ ~

~ ~ ~ ~ ~ ~ 0 ~ ~ ~ ~

4 ~

0 0 ~

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1C

/I

L lt, I'

i

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1NDIAN% tk AMCHIGANPQW R CQMPANYDONALD C. COOK NUCLEAR PLANT

PROCEDURE COVER SHEET

Procedure No.lZ PMP 3150 PCP.001

Revision No.

RADIOACTIYE MASTS PROCESS C0~TROL ~ANNUAL

SCOPE OF REVISION

SIGNATURES

ORIGINAL Rev. 1 REV. 2 Rev. 0

PREPARED BY

QUALiTYASSURAi tC.RE VIE'cV

iNT=RFACING DEBAR i MENTi:EAD CONCURRENC-

DEPARTMEVi T:-BADAPPROVAL

PLANT iVUC'"ARSAFETY COMMITTEE

NT MANAGERAPPROVAL

77

DA:= OF iSSUE

12 PNP 3150 PCP.001

FIST OF EFrc.CTIVZ PAGES

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REVISION NUMBER AND DATE

Revision 2, 02/15/83


















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IIST OF EFFECTIVE PAGES

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AT ACE~:NT IIPage 1 of 1

REVISION %AMER AND DATE



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XZ rm'a>O PCP.001

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KIST OF EF ECTIVE PAGFS

REVISION NUNBER AND DATE

ATTAC21~ IX


ATTAINTX

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ATTAINTXII


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12 P!1P 3150 PCP.001

INDIANA & 5!ICHIGM ELECTRIC COa~PANYDONALD C COOK NUCLZAB P~IT

RADIOACTIVE NASTZ PROCESS CONTROL PROGBAiii

1.0 OBJECTIVE

This manual is to give the necessary d'rections to insurethat all ~lant cenerated adioac"ive wastes are t ansferred,packaged and sh'pped such "hat radioac ive waste sh'=mentand burial regulations are satisfied.

2.0 BE:EBZNCES

2. 1 Code o f Federal Reculations T'ie 49 Pa" s 170-179

2.2 Coce of Federal Regulations Tit'e 10 Parts 19-71, 150

2.3 NRC Radioactive Material License No. 46-13536-01

2.4 State of South Carolina, Radioactive Materials L'censeNo. .097.

2.5 State of ~~iarvland Rad'oac ive Haterials 'License No. i~iD27-001-02.

2.6 Technica'pecifications, Apoendiv A to L'cense No.DPR-58.

2.7 Technical Speci"icaticns, Appendix A to License No.DPR-74.

U.S. Zcologv Incorporated, State or Nevada, Depa" wentor Human Resources, Division of Health, Radioactivei~!aterials License No. 13-11-0043-02.

2.9 U.S. Zcologv incorporated, NRC g Radioact'e i~iaterialsLicense No. 04-03766-01.

2.10 U.S. Fcologv, incor-orated, State o" Nash'gtonRadioac ive i~!aterials L'cense No. (vN-1019-02.

2.11 U.S. =cologv incorporated, NBC, Nashincton License16-19204-01.

Page 1 of 26Rev. 2

p)~ 50 PCS 001

Depar men o

er 345 Division 60 ror"~ative Rules Chapter ' 'or2 ~ 13 Oregon Adminis~raR oactive Materia~ls, Transport Perm'heOregon Raaisirequirement

t, Corpora'tion Radwaste~ear and Developmen o2.14 Hittman Nuc earService NanuaHandl ng

waste Handling Service Manual.2.15 Chem Nuclear Radwaste Han i

vLarge Quantity shi ments orplicatj.on to transpo ". h,."an should be made

2. p . materj.al i~ itic -'g553 o~ Ac No ~ 20'ursuantto the r« - .

41, as amendedi beingo~„"the publj.c Acts oz ~

D rtmen of State, Po i9 of Act No ~St te pire Safety Boar

ded and Sectionspublj.c Acts o368 of ™he Publ Acts2226i and 13521 o " '33. 2226 I 333 ~'n 5 16 109, ~ '

1978, as amended, be'ngled Laws (<michigan

of~ 333 13521 oz he ygichigan Compi eanc ~

.- Publ'c Health) ~

PRZCAUTZONS3.0

uct s wloi or u ~ 'll be pou ed 'nto any- omB ilding loo drains. 'o

and re%ovexiiiarv Build'ng o

e 1 ed into a container,ea must be place ib keat from entering

are1 soi's must e .

d t 1s and must be cleane u

3.2 No package i~ e hz. ment, xn of a hole, aa. ure,

snot must beindic tio

'p." Pa" icular attenh has an o

"ion wi1 b led o .ot Shia eno Qo esid to welds, znsu ng .

1.a kec o "'ed an

wefor shipmen

smashed prior to p acut up or

3.3

3.4

s tr2.c ~ly p

500 allon tanksk Co fo

e' 00 allon and 1 g

red bv H'hland Tanmanu actu ec v prohwaste is s c i

shipment.

o s 1nto se 1 anv open'gsxv mater'ls o" shipment of racioaa package =or srohibited.

Page 2 of 26Rev. 2

0 l2 P< aso PCP.ool

Cq-CK OF> AND INFOP-~AT O.1 S="= S

t I Truck/~"a~ler ~ns~ect.on Check-Or SheetAttachmen

Attachment XX Cement Solidification Verification Log

Cement Haste Solidific tion Data SheetAttachment XXXI

Attachment IV Calculation She " "or Cement Solidi-'cat'ono= Resin

Attachment V

Attac? ..ent VX

Attachment VXX

Haste Management Simple Flow Diagram

Responsx,baal'v

U.S. Ecology, Inc. Radioactive ShippingRecord

At"achment VXXX

Attachment ZX

A'ttachment Z

Chem Nuclear Svstems, Xnc., Rad'oac iveShipping Record

Hashincton Low Level Rad'oact've HasteShipment Ce tif'ationNevada Low Level Radioactive Haste Sh'pmentCe t'fication

Attachment XX Nevada Certi"icationA"tachment XXX Driver Instructions for Maintenance of

Exclusive Use Shipment Controls

Attachment XXXX

Attachment XXV

State Police Not'cat'on Forms

Radioact'e Haste T uckRad'ion/Contamination Survev

Attachment XV South Carol'na Rad'oac ive Haste ShipmentCe t'"ication Form

At"achment XVX South Caro'ina Prior Not'"ication andi~|an'st Form

A achme.. Radioact'e Haste Shipment Not'icationForm

oAt achment X x . aVXX" R. dioact've Haste Shipment Cnecko~ Sheet

At"achment XXX

At achment XX

fZif-l00 LinerF~'e Change Sign-Of" Shee"

A"tachment

Attachment X:<XX

Low Level Has e Box Invento=r

Demineralizer Resin Ca'culation SheetPage 3 or. 6Rev. 2

p II

12 . 3150 PCP.001

5.0 DETAZLS

The plan" waste processing ecuipment (deminera'"ers,evaporators, etc.) a e designed to process wastes in thechemical and physical orms wnich exist in the operatinglant svsiems. Plane admin'strat've procedures dictate the

plant svstem's chemical ooerating oarameters, and routinesampling of these systems insu e that all parameters arekept with'n the ooerat'ng Limits. Other procedures are ineffect wh'ch -"ever." materials wh'ch effect waste systemoaeration from enter'ng these systems.

Zf alternate or additional ecuipment such as filters,demineralizers, incinerators, etc. are reauired or wasteprocessing they will be operated by the ph'osophyestablished in this manual to assure that the ='nal formsmeet all the regulations =or shipoing and bu ial. Pr'or tothe operat'on of anv alternate eau'pment, procedures will bewritten and approved.

A. Licuid Processina And Solid f'cat.onThe waste evaporators are operated by the instruct'onsgiven in one of the ollowing olant procedures:

1 OHP 4021.002.005 Operation of Waste Evaporator

1 OHP 4021.024.002 Pumping of Waste Evaporator Bot oms

12 OHP 4021.022.00S Placing En Serv'ce and Ooeration 0The South Bor'c Acid EvaporatorXncluding System Kine Up As A Was eEvaporator

1 OHP 4021.022.009 "S" Boric Acid. Evaporator CooldownAnd Pump Out o" Evaporator BotiomsOperating As A Wasto Evaporator

The evaporators are operated for the purpose o"reducina the licuid waste act'vity levels such tha"tnese liauids can be released to tne env'ronment at

'f A wwQ Qconcentracions with'n the L~miis oz .0 ~:R ar 20.Licuids wh'ch are within the lira's, can be releasedd'rect'v without urther processing. With thesere'eases being made the total vo'ume of licuids wn'chrecuire solid'"'ca 'on is reduced. This reduct'onso'idif'ed volume makes it possible for fewer shipmentso" " dioac 've,.at ia's and less volume to be bu"'ed.

The ';..'" of vo'ume reduct'on 's depenceni onconcentration of several chemical ana radiochemicaspec's (See Table Z) .

Page 4 o 26Rev. 2

'

s 'I

12 PkiP 3150 PC2.001

Zf the concent ation oz boron is allowed to increaseabove the ''mits of Table Z the concentratescr~s"aI.lize in the evaporator when cooled down forpump-out, creating mechanica3. problems or theevaoorator and pumps. To orevent crvstallization ofevaoorator concentrates the corcentration oz boron iskeot below the limits of Table Z and sodium hvd oxideis added as reauired to maintain an elevated oH toconvert the H3303 to sodium tetraboraze which is much

more soluble than H3303.

330 —:2HaQH 'fa234o7 . H20

The concent at'on of chlorides in the evapora orconcentrates is kept below the 3.'m' of Table Z inorder to orevent materia3. damage to the evaoorator. Z"the concentration is al'owed to 'ncrease above the3.imit of Table Z there is a oossib''itv o" co» osion ofthe evaporator 'nternal surzaces, including tne neatertubes. Zf these tubes are corzoded to the point wherethey wou'd leak, activ'ty would enter the steam system.These tubes wou3.d tnen have to be olugged or replaced.

The ac ivity leve's in the evaporator concen rates a e.monitored as an aid to evaluate the need or shieldedtransoort eauipment.

Samples a e taken pe iod'callv bv Chemical Sect'onpe sonnel during tne batcn evapo"ato ope ation tomain"ain tne evaoorator bottoms within the limits ofTable Z, however, evaporator bottoms maybe prooerlvsolidified for shipping and. bu ial within tne 1'mi"s ofTable ZZ by the use of he procedures given 'n th'sprogram.

Page 5 of 25P.ev. 2

l ~~ ~

I

12 PNP 3150 PCP.001

TABLE INaste Evaporator Normal Oaeratina Limits

BORON, B 20,000 to 30,000 porn as B

CHLORiDES, Cl

Gross Bv total

>9.0

500 ppm

0.2 uci/cc

Page 6 of 26Rev. 2

j12 PNP 3150 PCP.001

r

TABLE IX

Waste Evaporator Concent=ates L'm's For Solid'ica 'on

BORON

CHLORZDES

ACT1VZTY OF

FZSSZON AND

ACTIVATION PRODUCTS

0 » 40,000 ppm

3 - 11

0 - 1000 ppm

0 - 0.0001 Hillicurie/gram Transport Group

0 - 0.005 Millicurie/gram Transport Group

0 — 0.3 ~hi}.lieu 'e/gram Transport Group i"

Page 7 of. 26Rev. 2

~ ~

L ~ I 12 P~G'150 PCP.001

SOLIDlFXCATZO".l BY US. OF C

SYST" 2 DESCRIPTION

The svstems described he»e'n are designed to handle thesolidi ication of liquids, evapora or bottoms and othe"concentrated liauids, spen»csin, o" other miscellaneous wastes.

Nas e eed System

The waste =eed svstem cons'sts o= n electr'c motor drivenpump and waste supply 1'ne to trans"e» waste to the line".The Naste Evapo" d'or Bot"oms S"orage Tank Transfer Pumptakes suction = om the ''cuid waste storage tank and pumpswaste into the 1'ner. Nhen usinc; temporarv concent atesholding tanks, waste is pumped through flexible nosedirectlv to the line" with a portable electr'c pump. Theliner 's "'ied until a pre-se" level is reached as detectedbv a leve'enso" suspended =rom tne liner. (See A3 ttachmentZ1Z)

Cement Feed System

Cement and sodium metasi''cate are put into hoppers and areaugered 'nto he liner. Upon con" cting the licuid waste,the sod'um metasil'cate begins to act, shortening the settime o" the cement. Each 'incr is supplied, wi"h an internalmixing device designed to provide thorough mi..'ng of theen ire line coI tents A m zing mo or moun ed on he top 0the liner prior to the "'ll'ng opera 'o.. 's start d prior tothe add'ion of cement..'1izing cont'nues for approximatelytwentv minutes after add'tion o" the cement and sod'ummetasilicate or until the motor automatically trips off dueto high esistance to mixing.

The cement =eed sys em also has a vent 1'ne tocontro'ementdust. Flexible nose is connected at the loading

=lange. Nhen cement 's augered 'nto tne l'ner from thehoppers a vacuum on th's line d aws o=f the a'" being vented=ron the liner. The a'" is th n conveved to tne vent airr'ter.

Page 8 o 26Rv. 2

12 PtL~ 3150 PCP.001

COLLECTION AND AUAZYS'ZS OF S92lPLES

General Recuirem nts

The PCP shall be used to verify the solidification of atleast one representative test specimen rom at leas everytenth batch.o each tvpe o wet adioactive waste (e.g.evaporator bot"oms, bor''c acid solution).For the purposes of the PCP a batch is defined as the amountin the HZ~ST at the time of sampling p ior to pumping to thesolidifica"ion equipment.

I anv test specimen fails to sol'di y, the batch under testshall be suspended unt'l such time as add'tional testspecimens can be obtained, alternative solid'ficat'onparameters can be determined in acccrcance with the ProcessControl P ocram, anc a subsecuent t;est ve '='essolidi ica" ion. Sol''cation o= the batch mav then beresumed using the alternate solid'ication parametersde termined.

Xf the init'al test specimen from a batch of waste fails toverify solidific tion then representative test specimensshall be collected from each consecutive ba"ch o= tne sametype of waste unt'' three (3) consecutive initial testspecimens demonstrate solidi 'cat'ons. The p"ocess shall bemodified as required to assure so'idi 'c tio~ of subsequentbatches of waste.

For, high activ'tv waste, where the handlinq o= samples couldresult in personnel radiation exposures which areinconsistent with the ALMQ. Principle, representativenonrad'oac"ive samples wil be procuced and tested. Thesesamples should be as close to ne actual wast in. thei"phvs'cal and chemica'roper"'s as possible to ver'fvproper sol'd'cation: parameters.

Pace 9 of 26Rev. 2

~~

\ 12 Pta 3150 PCP.001

Waste So' d ' icat'n Data Sheet Attachment ZZl

A Waste Solid''cat'on Data Sheet will be mainta'ned oreach test sample solidified. Each data sneet vill containpe tinent in ormation on the test samp" e and tne batchnumbers o vastes solidi=ied based on each test sample.

The Waste Sol'di='cation Data Sheet vill conta'n pert'ner.tinformation on the characterist'cs o the test samplesolid'=ied so as to verify,solidification o. the subsecuent10 batches of simila wastes vithout retesting.The Test Sample Data will include, but not be |.imited to,the type o" vaste s'olidified, major radioact've const'tue..tspH, volume o sample, identi"icatior. o= oil 'n samples and

he ratio o f tne sample to the final volume o = hesolidifiec product.

The Waste Solidification Data Shee" will include the batchnumbe , batcn volume, and date solid'f'ed, for each batchsol'd''ed based on the sample described on the test sampledata sheet.

Collec"'o.. Of Samples

Two samples of the batch o" liauid to be solidif'ed shall betaken =or analysis. Sample sizes shall be compat'ble wi"nthe s andard size sample used for the radioact'vity analysisand the second for the chemical ar.alvsis. I theadioactiv'v levels are too high to permit full size

samples to be taken then smal'er samples shall be taken w.'ththe results-corrected accordingly.

Page 10 o 26Pev. 2

12 PMP 3150 PCP.001

TEST SOLEDZPlCnT ON AtcD ACCZPTANC" C2ZT 3EA

Test So'ificationTest Solid-'fications should be conaucted using a 1000ml disposable beaker or similar size container. Mixingshould be accomplished bv s-irr'ng unt''1 a homogeneousmixture is obtained. (Min'mum stirring t'me 5minutes.)

Neasu e 'nto the mixirg vesse'3S ml. of the waste tobe solidified.Measure out 479 grams of (Portland l) cement arc 68.56grams of sodium metasilica"e (anhydrous) and acd thisto the waste to be solidi=ied. The cement and sodiummetasilicate (anhvc ous) must be rom tne same 'ot ofmat ria s wh'ch are to be usec for the solidification.

two lots are to be usea "hen «he tes« mus oe maaewith the evact proportions o= each lot which are to beused in the line".Mix the cement (Por"'anc i) and socium metasi'icate(anhydrous) togethe" and slowlv add this mivture to thetest sample while ' is be'ng st'rred.A ter ten (10) minutes of mixing and a homoceneousmixture is obtained allo~ "he waste to stand for amin'mum of 60 minutes.

Solidi ication Acceatabil'tvThe following criteria defines an acceptable solidifica ionprocess ana process parameters.

The solid'cation is consiaered acceptable, '= uponvisual inspection of the sample, tne waste appea s hati" would hold i"s shape '= removec from the bea'<er andi" resists penet=at'on, anc no more than 0.5. o= thetotal volume o» the beaker is " ee water.

Solidification Unacceat bil'tvIf the waste'ails arv o= the c "e ia set =or h above,t..e so 'a'=icat'on wil be termec u..accep- ble and anew se" of sol'ifica"ion parameters will neea to beestablished.

Tf the test solic'=ication is unaccep"able «hen thesame test p ocedures must be =o'lowec on eachsubsecuent batcn of «he same type of waste untiL three(3) consecut've test samples are so''c'='ec.

Page 1 o 26Rev. 2

12 P5L~ 3150 PCP. 001

Alternate Solidification Parameters

If a test samp3.e ails to provide acceptable solid'ficationof the waste the following procedures should be followed:

Mix eaual volumes of dry cement and water to ensurethat the prob3.em is not a bad batch of cement.

2. Add addi"ional caus 'c solution to the sample to raise.tne pH above 8, i" recu'red.

3. I the.,waste is on'y oart'ally solidified, use lowewaste to cemen" rat'os.Prepare test as ol'ows allowinq at least one hou" =oreach test to so3.idify. If each test doesn't sol'ify,go to the ne..t set o" parameters.

MLSHaste

GHCemen

TZST

G~~(

Sodium NetaS'licate

(Anhvdrous)

Ga13.onsHaste

LIH:-R

BagsCement

BagsSodium MetaSi 'cate

(Anhvd ous)

1. 400 523 75.4 ~ 712 83 11

2. 375 567 82.3 668 88 12

3. 350 592 89.1 623 94 ~ 13

4. 325 624 96.0 - 579 99 14

Packages of cement solid'ed licuid wastes wil3. be held for amin'mum of twenty four (24) hours after solidifications, andver'ication of compliance will be just pr'or to 'oading orshipment and will be documented on Attachment II.Solid'f'cation of ''cuids other tha.. evapora o oo toms maybecome necessary and wi3.3. be done such i:at compliance with allthe aporopr'te regu'ati ns is ve ified pr'or to shipment.

Page '2 of 26Pev. 2

12 Pt& 315 0 PCP . 0 p 1

B. Comaressibles Nastes

All contaminated or, potentially contaminated compressiblewaste will be taken to a designatec area ne r the nvcraulicbaler. The waste vill then be compressed into d ums.

Material wnich wou'd be in nonccmpliance wi"h theappropriate regu'ations wil'ot be placec '.".to a oackagefor baling.A3. drums which have been filled will be documented as tothe number o= the package, cescription of the contents, dateanc init'als o= person =''nc package anc radioactivesurvev data. "-ach package wil'e sealed and stcrec unt'3.loaded =or shipmenz. arc Burial.Prio to 3.oacing, the package must be cnecked bvEnvironmental Sect'on pe sonnel =or anv incic tion c" holesfa''ures or weak spots at the seams, we3.cs or otherwise.

All of the above ope at'ons are per"ormed within the limitsof the olloving procecure:

12 THP 6010 BAD.303 Solic Nas e Hanc3. ng anc D umming

Page 13 of 26.Rev. 2

~glI

12 P."1P 3150 PCP.001

C. Noncomoressible Naste-FiltersAll licuic process type "''ters should be remo:ea by thespeci ic 'ndividual filters change procecure (See AttachmentVX, page 5 of 5) and transoortea to the Drumming Poom. ~ oensure adequate drain tiime for removal of =ree stand'ngliquid, fi3.ters must be drainea as follows:Pilter 'Jte ~1inimum Drain T'me

Reactor Coolant

Seal Nate"Injection

coub le-stage stainlesssteel pleated paper

single-stage s a''sssteel p l.ea "ed nape"

15 minutes

15 minutes(10*)

Spent Fue3. Pit

Soent Fuel P'tSkimmer

coub1e-stage sta''sssteel pleatec pape"

doub le-stage s tain's ssteel pleat d paper

1 3 vill,ilute s

'5 minutes

Refue'ng NaterPurification

double-stage stainlessstee3. pleated oaper

15 mi..utes

Seal Nater Return douhle-stage stain3.esssteel 'pleatec oaoer

15 minutes

CVCS Ton Evchance single-stage stalnl esssteel leated paper

1 5 Pillnu e s(10")

B.A. "=vaooratorConcent atesCondensate

single-stage s ain~esssteel pleatea paper

15 minutes(3 0%)

Boric Acid 30" c'oth wrapoed 15 minutes*"

Naste =vaporator 30" cloth wrappedFeed anc Condensa"e

15 minutes"*

Temporary-ReactorCavity and SpentFuel Pit

20" cloth wrapoed10" cloth w aooea

1 5 minutes (1 Qw)15 minutes (5")

/

Large f'ers or h'ch activity ='lters shou3.d be storec 'nthe d~ thev we~e original'v placed in when removed. P'aceall drums 'n s orage area pe" 12 THP 6010 RAD.303: Sol'cNaste Handl'ng and Druviming.

~ t(lnlmt m craln - me cetermlnea by test ~ ng.~","1ax'mum number o= this t':oe of filter is 8 pe" crum.

For proper documentAt"achment XZ."-'ters not analyz cBarnwell Burial S't

'on required dur'ng =''ter changes, see

or solidifiea can not be shiooec to the

Page 14 o 26Rev. 2

12 P&1P 3150 PCP.001

Miscellaneous-Includina Absolute, and Heaa P'tersAll miscellaneous noncompressible waste must be placed in ametal bov as soon as possible after determination the itemis to be disposed of. No 1'cuid or damp items oz anv kindare- to be placed in metal boves. No metal bov is to besea'ed until 't has been visually inspected bv Env'ronmentalSection personnel, has been numbered and a description othe contents, including approximate ite... si e and amount, 'scompleted on the Low Level Haste Bov Inven"ory, Att chmentXXI.

NOTE: Any box 'which is g eater than 640 cubic feet mustbe placarded on both s'des and 'th ends.

Scintillation VialsNOTE: Insure t:he =ollowing procedure is followed "or

packaging and shipping scintillat'on z'uids.1. Obtain a fif"y-five (55) ga'on waste d w (DOT 17H)

place in the hot lab and label "Po sc'tilla ionvials Only - DO NOT Ship to Barnwel'". Line the drumwith a minimum four (4) mil plastic liner.

2. The final p oduct to absorbent material ratio must notevceed one-to-two.

*3. Place approvimately 3" oz absorbent at he bottom ofthe drum.

4. Place 6" of vials (not to be opened) 'n the container.

S. Place 6" of absorbent in the container.

6. Place 6" oz v'ls in the con a'ne

7. Fil'he remainder of the conta'ne w'th absorbentmate ial.

8. Close container and take to the 587'rumming Poom.

9. Replace w'h new barrel and fol'cw abovelingo

steps =o"

*Approved absorbents1. Diatomaceous Ea" h (Medium G ade)2. Super Pine {Diatomite)3. Speedi Dry4. Hi - Dzy5. Calatom (j>f-P78)6. Ploor Dry 85 Super=inc7. Instant -

Dr'.

Sa e — — Sorb (Pentraso b)Page 15 o" 26Rev. 2

12 P&IP 3150 PCP. 001

D. RESINS

Spen" res'ns are normally trans e ed to tne spent resinstorage tank to await packaging or shipment. The prooerliner ard cask to be used or the resin shipment wil'edetermined by the activitv of the resin to be packaged(At achment ZV) . The cask to be usea ' determined "romthose available =rom Chem-Huclea and Hittman ';Iuclear andDevelooment Co o., in the'r Radwaste Hardl'ng Servicetianuals. Afte the prope" cask is deciaed on and rece'ved.ac the plant (including checking for contam'nation as perproceau"e 12 THP 6040 PER.467 it should be prepared forshipment using 12 THP 6040 PER.470 "Resir. Transfer "-romSoent Res'n Storage Tank To A Cask", 12 THP 6040 PER.467"Cask Handl'ng", ana this Process Control ~Ianual.

The package, when full, will be checked .or free wa eroe ioaica'ly urti'hipoed. he check for free wate"

wil'ncludecewatering for each check. Th's wil'e done bypumping licuia of= the too or crain'na or pullinc suction

rom the bot om. Each di ferent type of package used w llbe tested such that the volume of licuid wnich mav beremain'ng in the package is known o" each dewate"ing methodused. The volume wn'ch could be r maining will alwavs beunder the volume allowed by the NRC, DOT ana Burial Siteregulations at the time of sh'poing.

Zf regulations recu're resin sol'di ication it will be done afterdewate 'ng by use o" tne cement solia'fication ou line wh'chfo''ows and Attachment V.

Collec 'on of Samples

1. Raa' logical oro"ection

1. 1 Comolv wi l aoo 1'ab ' Radia 'on York Permits.

1.2 Tes" samples which usedisposed o= by olac ngsolid'='cation.

actual waste shall be'n the d'sposal 1'ner after

1.3 A Naste So''a'fication Data Sheet will bemainta'ned =or each test sample sol'di ied'. Eachaata shee" will contain pertinent in=orma ion onthe test sample and the batch nu-.her of wastsol'a''='ed basea on each test sample.

Page 16 o f 26Rev. 2

Waste Solidi "icat'cn Dat Sheet

The Waste Sol=: '=ic t'on Data Sheet wil'ontain pertinentinformation on the characteristics oz tne test sample solid'fiedso as to veri y solidif'cat'cn oz subsecuent batches of simi3.arwastes without retesting.

2.

The test sample cata for spent resin w'3.l 'nclude, but notnecessarily be limited to, tne type oz waste solidified,volume of sample and rat'o of sample vo3.ume tc the zina3.volume of the solidi ied product.The waste so i"'cat'on data sheet w''1 'nclude the Ba chNumber, Batch Volume, and Date So3.'d'='ed, =or each batchsolidified based on sample described.

Collection of Samnles

One sample shal3. be taken fo analvs ' The sam+le shal3. becompat'ble with tne st nd r si" sample used =o= the cammaisotopic analysis. 1'f the radioact'v'"y leve's are too hichto permit full size samp'es to be taken, then smallersamples shal3. be taken with the resu3.ts correctedaccordingly. Sample sizes shall be determined by RadiationProtect'on personnel.

2. Samples should be drawn to allow adecuate time to ™omp'etethe recuired testing and veri ica-ion o solidificationprior to the planned waste sol'di"icat'on procedure.

Test Solidification and Access nceCr'te"'.

Waste Cond't'oninc

L.l I large (i.e., oam c using) cuantit'es ofdetergents are presen , the sample should betreated with an anti-foaming agent. The cuant'tyof ant'- oaming agent e u'red shall be recozdedon At"achment ~ ZZ.

Page 1 I of 26Rev. 2

12 PMP 3150 PCP.001

1.2 Zf oil is present in cuantities greater than 1$ byvolume, the oil should either be emoved by

- skimming, or emulsification agents should be used.to break up tne oil. The auantity of anysubstance adcec to the samp3.e for this purposeshall oe recorced on Attaca~ent ZZZ.

Test Sold.dl:Lcat1on

Anv sample to be solidi=iec sha3.3. be pretre tec as.spec'=ied in Sec"ion 1 unde" Test Solidi=ication andAc"eptanc Criteria.

2 ~ Test Solidi='cations snould be conducted using a 1000ml. disposal beaker or similar size cont incr. M'zinashou d be accomplished bv st'ing with an electr'cmixer until a homogeneous mixture 's obtained, but inno case =or less than three (3) minutes.

3. For the test solidif'cations o res'n, measure into twomixing vessels 240 gms o" uncompacted dewa" erec csine ch anc adc 90 ml of water.

4. Measure out the reau'rec quantities o" cemen- andanhydrous sodium metasilicate as shown below. Vo3.umesare =or loose, unccmpactec material.

Grams Cement Grams Anh;c=ous Sociun Metasilic teWaste Sam+le A Sample B S anal A Sa. oleResins

Resins

5.

189 236 19 24

265 346 27 35

Slowlv adc the cement to the test samp e while ''t isbeing mixed.

6. er all o.- the cene -„ is added, slowly ac" theanhycrous sodium metas'licate to the test sanple whilei" is beinc mixed.

7. A"ter suf='c' (3 m'nutes =-=" " a'1 cement andanhyc ous sodium metasi'icate is acced) m'zing soa homogeneous mixture 's obta'nec 3.low the wastestand for a minimum o= 4 hours.

tha0 o

Page 18 o= 26Rev. 2

~ ~'

12 P.'1P'150 PCP.001

Solidificat'on Acceotabi3.itv

The following criteria define an acceptable solidif'cat'onorocess and process parameters:

1. The sample solidiri ations are considered acceptable ithere is no visual o" drainable free water.

~e ~ The sample sol'd''ations e corside ed acceptable i.upon visual inspection tne waste appears that it wouldhold i s shape i= removed from the oeaker and i"resists penet at'on by a rigid stick.

3. The sample so3.idi icatiors establ'sh a range from tneratios o" cemert to waste that will esult in anacceptable oroduct.

Solid' cat'on Ur. cceotabil'vXf the waste, fails any of the cr'teria set =orth in theSection Soliai=ication Acceptability, thesolidi icat'on wil'e termed unacceptable and a newset of sol'a'f'cation parameters wil'eec to be

.establishec under the orocedures in the SectionA3.ternate Sol'cificat'on Parameters.

2. Xf the t st sol'ci icat'on is unacceptable then thesame test procedures mus- be followed on eachsubsequen batch of the same type or waste unt'1 threeconsecutive test samples are sol'd'.'ec.

A.l ernate Sol'di 'c 'on Paramete s

Xf a test samp'e fails to provide acceptable solid''ca ion ofthe waste tne =ollow'nc procedures should be followed:

Mix equa'olumes of c=v cement and water to ensurethat the problem is no a bad batch of cement.

2. X" the waste is only partially sol'ci=ied, use lowewaste to cement and anhycrous sodium metasil'cateratios. Using the recommencec quartities o" cement andanhvd ous socium metas'''cate, re"uce the waste samplevolume to 215 gms anc continue =eauc'nc the samplevolume by 25 gms unti'e acceptabi'ity c=ite"ia aremet.

NOT"S:

l. The weign of annv rous soc=um me"asil'cate 'sthe cement we'g'".t.

10 pe c n" o

e'c for aica"iors,

to loac'nc

~ Packages o cement so'idifi c " s''ns wi'' be hminimum of twenty-four (24) nou"s a=te

so3.'d'eri='a"'onof compl'nce w''e just priorsn'pment anc will be documented on A achment

ancor

Page 19 o 26

12 PMP 3150 PCP.001

E. LOADING

Prior to loading a Truck/Trai3.er Inspection shall be maaeusing check of= sheet Attachment Z. All transport vehiclesarriving on site or shipment o" radioactive waste will havea contamination and radiation survey taken prior to entryinto the Auxiliary Building. If the vehicle will not beentering the Auxiliary Builaing, the survey must beper ormed orior to loaaing. Loaa'ng of a cask onto a truckwill be as oer 12 THP 6040 PER.467 "Cask Handling". Loadingof the cask or truck will be such that the packages w'll beloaded as to minimize the exposure toward the front of thet uck. The Ba nwell, South Carolina burial site recuiresthat mixed (bar els and boxes) shipments of low speci"'cactivity materials on sole use vehicles be arranged so thatall boxes are placed toward the back of the truck. TheBeattv, Nevada buria''te doesn't have this recrui ement andboxes and barrels can be mixed on the truck with the onerequirement being that ba" els be olac d on barrels andboxes be olaced on boxes. All loads must be braced tominimize movement of packages auring normal transoort.After December 31, 1982, all arum shipments to the BarnwellBurial Site wil'e palletized. or shipoea in. ooen top vansor on lat bed traile s.

F. NOTIFZCATZON SCH"DULE

For "Large Quantity" Shipments

Aoolication to transoort a "larg auantitv" "radioact'vematerial shipmen" in M'higan should be maae oursuant to thereauirements o" R29.553 of Act. No. 207 of the Public Actsof 1941, as amended, being 29.3 c of the Mich'gan CompiledLaws (Deoartment of State Police - State Fire Safety hoard)and Section 9 of Ac . No. 380 of the Public Acts of 1965, asamended, and Sect'ons 2226, 2233, and 13521 o= Ac No. 368of the Publ'c Acts of 1978, as amenaed be'ng 3 16.109,333.2226, 333.2233 and 333.13521 of the Michigan Comoi'eaLaws .(Michigan Department of Public Health).

The governor or his designee of each state through which the'a. orementioned shioment will " ave must be given advancenot'cat'on 'n acco"dance with .itle '0-Energy Coae oFederal Regulations. P r- 571.5a.

* A "large cuan'itv" shipment is that which 's greate" than 200curies of Group ZZZ and ZV radionucl'des.

Page 20 of 26Rev. 2

gt

k~ ~ 12 PtiP 3150 PCP. 001

As burial space is recuired

Both the Beatty, Nevada and R'chland, Nashington burialsites do not have volume al'ocation plans. For burial spacecall:Beatty, Nevada - Steve CarpenterU.S. Ecology, Inc.

702-553-2203

Richland, Washington - Vern D. Apple - 509-377-2411U. S. Zcology, Enc.

At least 3 months before shipment

The Ba nwell, South Caro'ina Bu ial Site has~ a volumeallocation plan. Fo" bu ial space and allocat'on numberscall:Barnwell, S. C. - Angie Jones

VAP/PNP Dept. Linda Bragg(CNSX) Lewis Rouse

803-259-3577803-259-3578

Call Hittman Nuclear and Development Corporation ortransportation and scheduled sn'pment date confirmation ancfollow with a lette».HNDC - Chuck Stout - 312-232-6133

At 1 ast 7 days prior to shipment

Notifv the Michigan Department of Public Health of thescheduled date of sh'pment and est'mated curie conten

Mich. Dept. of Public Health - Joe Hennigan 517 3 3Mike McCarty

Prior Not'fication and Man'fest must be sen" to the Sta e o=South Carolina and tne Barnwell Buria'ite to be received72 hours prior to shipment a" iva'.Ve ify that th proposed carr'er has a valid petit totransport radioac"ive mate ials in the S a"e o Oregon.This ver'".cat'on is onlv recuir d when the consignee is theRichland Burial Site.

Pace 21 o" 26Rev. 2

4

12 Pl& 3150 PCP.001

Dav of shinment, nrior to deaar ure

Notify burial site be'ng shipped to. For shipments to theBarnwell Site, the route through South Caro3.ina must begiven.

Barnwell Burial SiteChem-NuclearSystems, Inc.

Beatty Burial SiteU.S. =-coloav, Inc.

Angie Jones - 803-259-3577Linda Bragg - 803-259-3578

Steve Carpente - 702-553-2203

R'chland Burial Site - Ve n D. Apple - 509-377-2411

If there a e anvHanifest "or themust be notiried

charges in "he Prior Hotific tion andBarnwell Site, the State o South Carolinain addit'on to the Burial Site.

State o- S. C. — Virgil AutrvBetty Bethea - 803-758-7806i(im l3ob3.e

Hoti 'cation of the Michigan State Po3.ice must be givenpr'or to shipment. (See Attachment XIII)Michigan State Police - 616-469-1111

SHIP P IitG

All shipping of radioac=ive ma"eria3.s for burial or forother reasons are reauired by procecure to comply with a'lNRC and DOT regulations. All packaging in the above stepsof this proaram are designed to insure compliance wi h allthe appropr 'te regulations. The followina procedu es areused to insure and!or veri y'compliance with theregu3.at'ons.

PNI 33.50 Receipt And Shipmen" 0 Rad'oactive.aterials ~

THI 3150 Receip" And Shipment Of Radioact'vel|ateria's.

12 THP 6010 RAD.304

12 THP 6040 PER.467

Sh'pment 0= Radioact've liateria3.s

Cask Handl'na

Page 22 of 26Rev, 2

12 PIG'150 PCP.Q01

The following will be the orde in which the Radioact'veShipment Records (RSR) are to be completed pr'or to anyforms being distributed to the espective personnel.

1.2.3.

4 ~

5.

Completion of shipp'ng, recordsRP Supervisor for s'gnatureEnvironmental Section =or signature and correctioncheck on RSR forms.Carrier for signatureThree (3) copies o" the Chem Nuclear (RSR), and U.S.Ecology, Inc. (RSR) are to be made.

Distribution As Follows:

The originals of tne Shipping Papers will go to theollow'ng personnel, witn copies also listed:

D. C. COOK NUCLEAP. PLA;JT

State Police Notification FormRadioactive Haste Shipment Notification FormRadioac"ive Has"e Shipmen Checkof SheetTruck/Trailer Inspection Check-0f" SheetOriginal To Env™onmen al Sect'onDemineralizer Resin Calculation SheetOriginal To RP1 Copy To Env'=onmental1 Copy To D iverBARN!'(rLL HASTE SPINAGE~'"NT FAC LITY - RSR

Hhite OriginalCanary OriginalPink Original1 Copy1 Copy1 Cony„

To Dr'verTo Environmental SectionTo DrLvezTo StoresTo RP Sec"ionTo HHDC

STATE OF S. C. PN&H AND CERTIFICATION FORMS

3 Copies

1 Copy

Or'inal1 Copy

South Carolina Prior Not'ica"ion andHan fes »orm to Dr'verSouth Caro'ina Prio" No""='cation andManifest Form to Environmental Sect'onSouth Carol'na Radioactive HasteSh'pment Certif'cat'on Fo"m to Dr'verSouth Carolina Radioac ive HasteSh'pment Cer ification Form toEnv'' ronment:al Section

Page 23 o= 26Rev. 2

12 PNP 3150 PCP.003.

OriginalWhite Or'inalPink Original

«1 Copy2 White DisposaiS'e Copies1 Carrie CopvOrigira3.

U.S. EcoIogv, Inc. {RSR)U.S. Ecology, Inc. (RSR)Nevaaa Low Level Raaioact've WasteShipment Cert'='cat'onDemineraI'ze Resin C iculation SheetNevaca Ce "' 'at'nSouth Caro''na P ior Not = cat'on ana!grani=est Fo mSouth Carol'na Radioact've WasteShipment Cer ''at'n,Radioactive Waste ruck Rad'tion/Contamina"ion Survev

"1 CopyOriginal3 Copies

1 Copy

1 Copy

DRIVER OF TRANSPORT V:-HICLEOrigina'ittman Nuclear & Development Corp.Driver Instructions =or ."maintenance ofExclusive Use Shipment ControlsWashington Low Level Radioactive WasteShipment Certi 'ationBarnwell Waste Hanagement Facil'y (RSP.)Barnwe3.1 'ste Management Fac 1'ty (RSR)Resin Gamma Spectrum P. intout

NOTE: he driver of the transport vehic3.e will be giventwo or more extra placards/placarc holaers forreplacement purposes if znv o= the affixedalacards become Lost or aamagec during transit.For transport vehicles wh'ch the placard holder ispermanent'y a="'xea on all =our (4) siaes, extrapiaca ds will not neec to be given to the d 've".

FiP1IROViii'~i'TAL S»»m~ yOVBarnwell Was e ~management Facility (RSR)State Police Noti=ication FormRadioactive Haste Shipment Not'icat'onFormRac'oactive Waste Sh'pment Checko""SheetRad'ation/Contam'nat'on ruck SurveyResin Garma Spectrum Pr.'ntoutU.S. Ecology, Inc. (RSR)Nevaca Low LeveI Radioactive wasteSh'pment Cer"'='cationNevaca Cert'cationWashington Low Level Racicact've WasteShipment Cert'icat'onSouth Carolira Pr'or Not'=icat'on andFxnifest FormSouth Carol'na Racioactive WasteS>ipmen Ce t'=ica ionT-uck/T=aiie= Inspect'on Check-O=f SheetDeminerai zer Resin Calculation Sheet

Canary Or gznaOriginalOriginalOriginal

~ Copy*Copy

Customer CopvCopy

CopyCopv

Copy

Copy

Or~gznal*Copy

*Only when res' is he'rc shippec. A pagegamraa spec" um p 'ntout anc a Dem'neral'zer Rev. 2Resin calculat'on shee™» -...ust be provicedfor each package contain'rg esii heingshipped.

12 PMP 3150 PCP.001

RADZATZOH PROTECTZON SEC ZON

1 CopyOriginal1 CopyOriginal

Barnwell Waste Management Facility (RSR)Radiation/Contamination Truck SurveyU. S. Ecology, Znc. (RSR)Demineralize Resin Calculation Sneet

TRAZ;IZ';IG

Personnel who routinelv handle and snip rad'oactive waste(see Attac'nment VZ) wil'e trained at least annuallv on thecurrent regulations (see References Section) and the plantinstructions and procedures which app3.y to Naste Handling.

Page 26 o= 26Rev. 2

12 P!Lb 3150 PCP.QQ1Nw'i Cgtf~»%<~ T

Ib1vP+» /mba

SHXP.'K~itT NO.

Pr'or to I.oadinq, "ae ="'o"Ji..c '"ens re "" be e.".amined anddocumented on t!lis checklist =or eac.'". vehicle

"ransportinc'adioactivewaste -rom ".'".e "'t site:

(2}

(3)

tPruc 1» / IP «a q l e «Pl q

RemarksTruck/Tra er "'nee'sRe.".la ksTr iler Sec nc: ra;..eRemarksLoad 'e-wownsRemarks

Z"JEST:ALS

(5) T"uck/Tra.: eRemarksTruck/TraL '

Rema ks

~ Aw«<,o «g

~laca QBQ

Xniti ls ind'cate ins-ection was mace nc = saccent h'e. = '"B...s =„=Bctin sa=e

1Ouilc g COnt- Ct ~ Ltt..aan .'uc - lc DBVB 'Oment.Person Contacted

"s were'oil or loac a«B(3 2-232-6'3)

D tVehicle inspection cri"B ia as =o'lows:

(1) Truck/T"a'ler Ti" s - A mini...um o= 1/'6" "reac, no =ah«icexposed on sicewall, no c .ts o" in ju™ies 'nto ah '.

(2) . uck/.ra'ler bneels - Check =or v's'h'e cracked wneels,loose luc nuts ox''sinq s"uds.

(3) T"ailer Bed anc "." me - Check visuall. =or c=acks ancbreaks. Check ma'.". ra's "or any v's'h'e cracks in ra'sand assoc'a"Bd welcs. On an~. crop =rame tra''e s, tfe drooarea is "'.".e most susceptih e "o crackinc. I" any cracks areobserved in ma'n a'ls, t" ''er shoulc he ce c''..ed andcar Le immecia elv no 'edLoad Tie-Downs - Check cw~'Bany visible cracks. Cables should he

aosL"ioned so "hat cah' co ..o" """ Banc shackles shall be =ree o= c= cks.

cooc coildL i Lon (snould he

ac.". o".".er. Raic'ne s

(5} T uck/ « ' e c. s - C .Bcks o«oQB a on oz nead-lip. s,*+pail J,icf ts I h ake 'n s af Q Q Bcticfia1 sic als.

(6) Truck/ railer P'acarced — Placarding; on =ro..t, sices ancrecui «BQ ~

Paae 1 o 1Rev 2

Cement Snlidification Verific:ation I

Li»er tlo.

LilleL Vol'lrl(Q

Cement lbs. /bag

Sodiwn t4.tasilicate 3bs./bag(hrrhydroo"l

Date Tine

Tirre Start

Conpletion Date

Corrpletion Tina

Cen)ent Lot I/or DaL.e Arrived

Sodium lletasilicate (Nrhydroo') Lot Il/or. D<lte lKcexved

Verification Date

Verification Tine

Verified By

Ship Date

DM'l'. CAIJAPSNMl'l

PBDCFSS) J)l'ii%f1

tN(LSC['I1I.I

0'lMHt ll ll~~O

CGf tQMl'S n>rnms

Sc))rcll.f3('atlc)ll Ver r.ficclLloll

I here))y cerLify tlrat a viural ior'pection of tire tllllX. 1 irrer i)as beer) c:un<br@ted 'rL'east 24 hoursaft:c r Lhe irulicated corr|l)lc)Lion d'ate arrd time air(1 tlr<rt there wn<s rrot any irrdication of freest<rrrdillg) icloid.

Da te

T3 lne

llHIR Sol)ervi sor

Page 1 of )Bev. 2

12 PMP 3150 PCP.001ATTACHMENT ZZIBatch No:Sample iVo:Date:

C=~E~fT YiASTZ SOLIDIFICATION DATA SHE- T OR

(.ype of $Nasze)

Batch No: Sample 3o:

Sample Volume, ml:

H(1) .

Indications o- Oil/Dete gent:

Other !major Constituents:

. Quantity of CementAdded:

Quantity of SodiumMeta. Silicate(Anhydrous)

Cement Lot =../or DateReceived

Sodium Hetas'icat(Anhydrous) Lot -,'./or DateRece'ved

Final Produc" to Haste Ratio:

Product Acc ptahility:

Rad'nuclides P esen":(Zso ones a Concen"rations)

If pH adjustmen is recuired notechemical used, cuan"itv used and pHa=ter adjustment.

Pace 1 o" 1Rev. 2

12 Pr.lP 315'0 PCP. 001A T:-.C.I'~Ah'V

SOLID = IC. TIOif DATA =A"L=S

SUi~'~L~'Z

For head resin, the 'icehsed cask oayload is linitihg for theHV-100 Series 1 aad H'1-100 Se 'es 2. t/eight is hot a linitihgfactor =or the HN-600, H'H-100 Ser'es 3, H~i-100S, ahd HH-200.

222d +~SLl

Ser'es 1

i~?-100Cow~ scI 4 Series 3

Ei-100S:"2<-200 Bl-600

Usable.Volw~ 142 142 142 65

~ABBY. SolL™MieWas'ol. ft~ 120. 3 142 '42 60

~h:<. HasL". Vol.

Hater &dc~ atV~~v. Pasih Vol.gal.

'03. 0

223 ~ 5

QArC ~ v

214. 5

116. 5

223

116. 5 49. 3 53, 4

253.2 106.9 ~15 9

Cam" Ad&1 ft.'agsfatso %dePcvr~ 100.'-. ~cs

52. '

't ~ r 'tr 7

59

5.5

59

3 ~ 3 2.4

2/

2.5

v pRC~ ~v~hLe~1 R/h Coh=c- 12 12 5 800 100

Page 'f 1

Rev ~ 2

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a

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12 PtIP 3l50 PCP.001ATTACI)tlLtf1'X

tA'I~.IVBIZSTBI2 WAPFl

PAXLSS PIJKGBI&) BY SUPLN'ISED BY VEMIIED BY TNQNTHG BYHaste '1'ransport toBo>(-Karrel

Bo:(-Barrel I'illzng

Ba(lloacL'1veCn))te»t-IsotopicBa tinVc)c):age Sc ale(la»(l la))cled

Pac)(age Qualit>yVeri1 i c)c) tion'I'r»c): Ioa(li!)(g

re)(!k a»d Pac):clgeJ»'>f)ect10» a»()Surve)taclloactlvQS)))ppl»g Ih!(X>L(I

Prior t4tifi(')tin»

ContracL )hint.Perse»»el

7lPersonnel

Ihc)lat lo» Prot.C))(J'))ic() 1 'Itic)l.

Cn»LracLVc '1 1'A3»»e lI'..»Virn)U)>: ntalVerso)«)c 1

> Ll > >> \'0> I a>>CD

IL'cl)a»ic

IL)(liat:ion Prot.I 4').so»» '1 /B)VLLO»l)i!»t'c11

B)virorUw'nta l

I>)viro)U)x»L'c)l

BAD.303

BAD.303

BAD.304

IED. 300

rm.30'eP

IBAD.304

))AD.30<) PCP

I CP

BadlaLlon Prot.51>inte»a»ceSu >Qrvi sorB )(Iiatxo» Prot.Haintena»cew)) x.rv1)>or14«)ic)tin» I'rnt:.S))) >erv1 s(>l

lh')( I) cl t1()n Vl OL.S)))>QLv! HOL/Blvi r I'()LSn»l >elB1viro»)» nL'lVers(>) «)cl )..h>V>>O>>l»'>L1>V( rsor«)el/I t) int;.

~>ul >Qlv!snrIt'«Iiatio» PrnL'.Su))erv 1 1 ~) L /I~lvlLO»))lintc)1Bc)()) c)L'10» I'LOL.Su))c'rvls(>) /lb)virO)U)>t »tc) II'h)vl.rn)llN.'»ta I

-Ihc laLlon ProLQctlonhb lnte»anceSu mrvisnr.)taxation ProtectionGut >rvisnr/lb>vi ro)U)> nta 1I'1()iatio» Prot:ectionSI )I>ervisor/I:»vi ron.Vc)l..S(>) )»L:1lta()1 clt'ln»

PL'AL'')lvlrc>)

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CER I.ICATZON

THIS IS TO C=PTIFY THAT I HAV" R-AD AID UtiDERSTA'iD THEREQUIREt'|EtiTS OF LICEtiSE v 1 3 1 1 00 4 3 0 2 ISSUED TiO U ~ S ~ ECOLOGY IItiC. BY THE HEVADA DEPAR. tKNT OF HUa4AN R" SOURC=S FOR TH" RECEIPTAND DISPOSAL OF RADIOACTIVE:QTERIALS AT BEATTY, H VADA~ ASDESCRIBED ZH PARAGRAPHS 5.1.1.3; 5.1.1.4; 5.1.1.5; 5.1.1.6 anc5.4.6.1 OF THr. U.S. "COLOGY, ItiC. SI OPERATIONS ';GQiUAL, AtiD IFURTHER C RTIFY HA ™HE ."WTE. ALS Itl T..IS SHIPt'~'HT ARE IHCOtiFORi~iITY hiTH HOSE REQUIRE~K iTS.

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AUTHORZZ ED S ZGiiATURE

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Page 1 ofRev. 2

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12 --'-' 5oATTACHMENT XXX

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mipmen is to be maintained as an exclus've use shi n t'p

~ ening must be per=ormed by a single consigner having the

exc3.usive use oz the vehicle. Unloading must be done bv theconsignee, and only at the des'nated destinat'on.Repositioning or movement oz anv loaded material vi"houwr'tten permission or the consignor or Hittman Nuclear &

Development Cor orat'on 's prohibit

Page 1 o~ 1Rev. 2

e ~

12 PNP 3150 PCP.001ATTACH."1ENT XZZZ

S.ATE POLICE:TOTZFICATION FORM

A.

B.

C.

CAi~ER':OAF'OLOR

AilD NJHBER OF CAB

COLOR, .'lUHBER, AilDLEiilGTH OF TRAILER

D. ROUTE FROl1 P~~N 'HROUG"NZCHZGAH AiND IilDIA~lA

TYPE AiilD DESCRIPT ONOF COHTAZi'lER

DESCRZPTZO'l 0- SHiP '" lT

G i i~ ZI'1U~4 'RDIAT Oil LOSELZn '~a/1 R AT 6 "-"==-= FRO:-1TRAILER

TOTAL CURIE CCtlT"al OFSHIP< I='.:T

I TZ"+ A."lD DATE OF S'ZP!1EilT

J. COl1PAi~lY ilAL~< I 6 l1 Elec" r ' Co. D. C. Cook P1an

K. YOUR NAi1E

Brxacman, 1i .

Page 1 or 1Rev. 2

r t~

Mer=.

INCOMING SURVEY - FLAT""EO

12 PMP 3150 PCP .001Attachment XIV

"All smears <50 dam and allreaoings c.Z mR/hr, unlessnoted.

3 I6 I

t~~ I1sses ~ ~ eewmea ew e eml'I

ll

Oaie I ecnn iceman

Time Instrument

OUTGOING SURVEY - L" ~GO

I~ El

l

I ~

Carrier

ra i 1 er.-. Oate

Max. Rad. Level (C) Time

Max. Rad. Level (6') Techni ci an

Max. Rad. Level (3') InstrumentPage 1 Of

4

INCOMING SUR1 7 - lA > OR 'Rr':GTOP

12 PMP 3150 PCP .001Attachment XIV

"All smears <50 dpm and .allreadings <.2 mR/hr, unlessnoted'

m~ ~

aIIIa~ a ~~ marl

3 a

Technician

Time Instrument

OUTGO'G SUR>!KY - V"" 0"- -" —">

Q~ «4

1

~ v

Carrier

r a i 1er-.-.'ateMax. Rad. Level (C) T)me

~ Max. Rad. Level (6') Technician

Max. Rad. Level (3') Instrumentage 2 ofexv

12 PHP 3150 PCP .001Attachment X IV

INCOMING SUR>lEY «Al 1 smears <50 dcm and al 1

readincs <.2 mR/hr, unlessnoted.

1 a ~~ ~

1lace ~ e mama's «a a M Lac ~o~M

l

3

D

Oate Technician

Time Ins:rument

OUTGOING SURYA: C„S

f

I

"arrier

'r a i 1 er-.-". Qate

i4!ax. Rad. Level (C)

i'iax. Rad. Level (6')

Time

Technician

Max. Rad. Level (3') InstrumentS

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12 PMP 3150 PCP.(ATTACHMENT XVI:I

Radioac"ive Waste Shipment Check Of Shee"

Prior to Shiament Date

Shipment No.

Prior Notification Forms <tailed

Allacation No.

Recuixement:

Gite Date «n 4 «a«ea.~ 1

At leas seven (7) days pxior to date of shipment

BarbellBeattyRichland

Gtate InitialMichiganSouth Carolina

Pr'or Noti"'cation Eorms e3.ecaaied *(If Flailing Recuireme.." IsNot L4Iet)

Requirement.:

Sita

At least seventy-two {72} hou s pr'ar to arrivalof shipment at tne Buria'ite.

InitialBarbellBeattyRichland

Priox Noti 'cat'on Given (Telephone}

Recuirement:

Gtate

Michigan

Date Init'lAt least seven days pr'ox to date o= shipment.

Shipment Schedule Arranced (Telephane)

Recuirement: When shipping schedule has been determ'ned vithapplicable Bu. ial Site.

niKC Personnel Contacted Date ZaitiaiSh'ment Schedule Arranced (i~lail)

Recuix'ement: On dav of telephone notification.HNDC Personnel "-orms Mailed To (Name)

Pace 1 of 2Rev. 2

>e ca'm1 ~ 12 P??P 3150 PCP.001

ATTACHMENT XVTZZ

Date of Shipment

State Police Hotificat'onRequirement: At least one hour prior to shipment departure.

Date T'me In'"ial

Bur'al Site NotificationRequirement: To be given when shipment depa ts plant s'te.Date Time Pe sonnel Cont cted Site Initial

BarnwellBeattyRichland

State NotificationRequirement: Noti 'cat'on given only i= there is a change in

the PN&?i Form.

Time Pe sonnel Contacted State InitialSouth

Carol'na

Radioactive Sh'ament Record (RSR) Check For Completeness

Requirement. Thorough check of every colure on RSR for properword.'ng and correc info~tion.

Date Time RSR Initial

Vehicle lPackaae Check

Chem-~luc learU.S. =-col.cgy, Inc.

Date Time Vehic'e Tni te al Packace In'i lPlacardedSurveyed

LabeledSe* edSurveyed

Page 2 o 2Rev. 2

12 PMP 3150 PCP ,001Attach))ent X EX

F~t.;=; ='".B(7S2

~aI«o ~ i~A oqaosa I yeso«r'a hh I «efse ~ IQ \ i~ lrq fIC r«a ~r ~ ~ Solo«e~ ASroee'l« ~

S I'a t"= C"'<'~Z":Cl<

l~ os as ~

~I' ~

l

I

I

I~ ~

II

II

I

~ ~ ~«1 '~S l

II

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Io

I

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a.H I «G «a e)ee

all «r ~ I ««a 1 la«o «« ~o««a« I 1 « I ~ ~ oosr «a«e ~

Page 1 of 1

Revs 2

SHEET OF

12 PtG? 3150 PCP. 001ATTACKIEtlT XXIBOX alO.

LCK7 '~ $ %5T"- BZ{ Lga~ZO~Z

bXZE hWKXZ~~SZBL. SOLID ~H OiK'r. ~O MQL~ OR LIQUID FCGNWVKRS.

DES~~i.~CA APP:"QX. SIZE c~~tD &iCLiuZ DAT I D~ITL~

BIRR ~i3Li.S

BCG~~4

CCbM~

3l

CRZ rmPXVKEGnT

Page 1 of 1Rev, 2

"Kt(,

A,

1 ~12 P~iP 3150 PCP.001ATT3CEMENT Zn

CRAG=" SZC.i~

NCTE The t'm ~~~cd bet,am Step 1 and Step 2 aust he great~~t~ or ~1 to '5 minutes.

GP~~WtS car / ~x / av

STEP 1 ~ Pil~-Vente5 and Dta'-.ea (cia~ca '~p) / /place tMs fern cn pap pane" at,"'ch site.

HGZH

SZEP 2: Rerrave =U.", ~~spar" m 587'ru~gRocm and olace in Dn~ (ti~ f'~" " "~mved~ ~~ing) .

NZE: Fil"or rust ".zt have a congruousz'cw of water cm ".g =an it.Xt should only >a c"i~i".g.

Caut'on: Use ev"~acare, wing placi;g ""o"ilt~ into there~sv~g ccu. el toavoid sowaiirqc"nomination.

STZ? 2 mm minus ~33~~ Dra'1 T~s. ~iirutes

5hinte~anc oerscI ml shed cave =own toRP oe scrawl cove~".g tm~ jcb.

BADDZIO'A PKlV~CN

FilterFilte

Drum Nur~

Contact Badiaticn Reading

hCTE: L~ the~t m"ation msu~ tsare ctheater t~an 2200cm/100 ~~ tlat bar=elmus" he deconr ~

un'helevels are lessthan 2200 ca@/100 an~as~ r~rce9,.

3'adiaticn Paaiir.a

Af~ ~let'™go" t~'s si~t, BP s.'"~~" =or~ to ~"~ =re'~~~»Sec~en

Page 1o 1Rev. 2

~C

12 Pt<> 3150 PCP. 001A ~&CHANT XZZZ

DEZKPKZZH 3HZ'MZKZOi' M

iM-54Co-57Co-58Co~0

I-131Cs-134Cs-13oCs-3.37BaLa-1 40Zr-95iW-95So-124

~~~ATZ&lB2f ZAG

(a)HZ~O'.lOF K71RL

CCKMZEQZZC'l

1.00

(b)-./10

0.47I 0.09I U.55

1.32 I

1. 43

0+870.94 I

0 '30.410.420.98 I

(c)DPCSUBE

CCiK. ~GTXGJl(a) x (b)

'ZCP~D.%~Plyw~l PZSZil(a) x (e)

Exnosure C"n~ibutim (c) = Frac"'cn o" total conco~~~tion (a) z -./10 (b)

Bcpasure at. 1 nate ~ 100 n1. sar@le =

Xf reading taken at 3 ft., R/hr a" 1 rat» = R/hr at 3 f". z .836x .836

(B) Resin volte zac~ = ft'n cask x 283.2

x 283.2

x (8)

'3rtm1, acmviM is resin = st at 1 meter x r sin volcan .actor (d)Toz~ ' cx)~~e ~i~MLLLon Ic)

Pe o~ hv

~'e cv

Ci (e)

Dat=

Sh.zm" Hme

Pace 1 of 1Rev. 2

Rev 2 to Procedure 12 PMP 3150 PCP.001, …xiiiarv Build'ng o eea must be place1 ed intoi a container, b keat from entering are 1 soi's must e. s and must be cleane u d t 1 3.2 No

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