6545 Nova Drive, Suite 207 Davie, Florida 33317 +1 954.474.7800 / F +1 954.693.8505 Report Type Microstructure & Porosity Project 17-4PH Date 2/28/2017 Customer Sintavia - 17-4PH, Lot 2016000496, Nitrogen Atomized Scope Powder Analysis QF-824.01 REV B Owner: Metallurgist 7/27/2016 PROPRIETARY NOTICE This document contains confidential and propriety information to Sintavia, LLC. The information contained in this document shall not be copied nor shared, disclosed to others, or used for any purposes beyond the specific purpose for which this document was intended without the express written permission of Sintavia, LLC. Page 1 of 5 Sintavia SEM Inspection for Particle Morphology 200X Overall Spherical Shape 750X Overall Spherical Shape
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Report Type Microstructure & Porosity Project 17-4PH Date ...17-4PH Powder with No Etch & Etched (Vilella’s Reagent) 500X. 6545 Nova Drive, Suite 207 Davie, Florida 33317 +1 954.474.7800
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6545 Nova Drive, Suite 207 Davie, Florida 33317 +1 954.474.7800 / F +1 954.693.8505
Report Type Microstructure & Porosity Project 17-4PH Date 2/28/2017
Customer Sintavia - 17-4PH, Lot 2016000496, Nitrogen Atomized
Scope Powder Analysis
QF-824.01 REV B Owner: Metallurgist 7/27/2016
PROPRIETARY NOTICE
This document contains confidential and propriety information to Sintavia, LLC. The information contained in this document shall not be copied nor shared, disclosed to others, or used for any purposes beyond the specific purpose for which this document was intended without the express written permission of Sintavia, LLC.
Page 1 of 5
Sintavia SEM Inspection for Particle Morphology
200X Overall Spherical Shape
750X Overall Spherical Shape
6545 Nova Drive, Suite 207 Davie, Florida 33317 +1 954.474.7800 / F +1 954.693.8505
Report Type Microstructure & Porosity Project 17-4PH Date 2/28/2017
Customer Sintavia - 17-4PH, Lot 2016000496, Nitrogen Atomized
Scope Powder Analysis
QF-824.01 REV B Owner: Metallurgist 7/27/2016
PROPRIETARY NOTICE
This document contains confidential and propriety information to Sintavia, LLC. The information contained in this document shall not be copied nor shared, disclosed to others, or used for any purposes beyond the specific purpose for which this document was intended without the express written permission of Sintavia, LLC.
Page 2 of 5
6545 Nova Drive, Suite 207 Davie, Florida 33317 +1 954.474.7800 / F +1 954.693.8505
Report Type Microstructure & Porosity Project 17-4PH Date 2/28/2017
Customer Sintavia - 17-4PH, Lot 2016000496, Nitrogen Atomized
Scope Powder Analysis
QF-824.01 REV B Owner: Metallurgist 7/27/2016
PROPRIETARY NOTICE
This document contains confidential and propriety information to Sintavia, LLC. The information contained in this document shall not be copied nor shared, disclosed to others, or used for any purposes beyond the specific purpose for which this document was intended without the express written permission of Sintavia, LLC.
Page 3 of 5
Scanning Electron Microscopy (SEM) - Morphology
Powder Particles Are Overall Spherical But Contains Many Irregular Shaped Particles. Scanning Electron Microscopy & Energy Dispersive Spectrum - Semi Quantitative Chemical Analysis
SEM / EDS Chemical Analysis for Sintavia 17-4PH, 1000X
6545 Nova Drive, Suite 207 Davie, Florida 33317 +1 954.474.7800 / F +1 954.693.8505
Report Type Microstructure & Porosity Project 17-4PH Date 2/28/2017
Customer Sintavia - 17-4PH, Lot 2016000496, Nitrogen Atomized
Scope Powder Analysis
QF-824.01 REV B Owner: Metallurgist 7/27/2016
PROPRIETARY NOTICE
This document contains confidential and propriety information to Sintavia, LLC. The information contained in this document shall not be copied nor shared, disclosed to others, or used for any purposes beyond the specific purpose for which this document was intended without the express written permission of Sintavia, LLC.
Page 4 of 5
Sintavia 17-4PH, Powder Lot 2016000496 17-4PH material 17-4PH Powder with No Etch & Etched (Vilella’s Reagent) 200X
Sintavia 17-4PH, Powder Lot 2016000496 17-4PH material 17-4PH Powder with No Etch & Etched (Vilella’s Reagent) 500X
6545 Nova Drive, Suite 207 Davie, Florida 33317 +1 954.474.7800 / F +1 954.693.8505
Report Type Microstructure & Porosity Project 17-4PH Date 2/28/2017
Customer Sintavia - 17-4PH, Lot 2016000496, Nitrogen Atomized
Scope Powder Analysis
QF-824.01 REV B Owner: Metallurgist 7/27/2016
PROPRIETARY NOTICE
This document contains confidential and propriety information to Sintavia, LLC. The information contained in this document shall not be copied nor shared, disclosed to others, or used for any purposes beyond the specific purpose for which this document was intended without the express written permission of Sintavia, LLC.
Page 5 of 5
Various Powder Analysis
The Hall Meter Flow Test (Method 1) was performed on the 17-4PH, Batch 2016000496, per ASTM B213 the powder exhibited a Positive Flow characteristic of 20.76 seconds per 50 grams units during the test.
The Apparent Density using a Hall Flow Meter per ASTM B212, obtained from calculations on the powder was of 3.42 g/cm3 with a constant volume of 25 cm3.
The Tapped Density per ASTM B527, obtained from calculations was 4.44 g/cm3 with a mass powder of 100g and a volume of 25 cm3.
The room where the experiments were conducted exhibits the following characteristics: Temperature is 22° Centigrade and Relative Humidity is at 34%.