MECHANICAL PROPERTIES UNDER CONSIDERATION • Hardness • Tensile strength • Ductility
MECHANICAL PROPERTIES UNDER CONSIDERATION
• Hardness• Tensile strength• Ductility
COMPOSITION OF ALUMINUM ALLOY LM 25:
Chemical composition
Copper 0.15-0.2
Magnesium 0.20-0.65
Silicon 6.5-7.5
Iron 0.45-0.55
Manganese 0.35
Nickel 0.15
Zinc 0.15
Lead 0.15
Tin 0.05
Titanium 0.05-0.25
Aluminum Remainder
Aluminium casting alloys
• Alloy designations:• (i) Aluminium Association (AA) system.• (ii) Aluminium Association casting Tamper
Designation system.• (iii) American National Standards Institute
(ANSI ): • (iv) The UNS Alloy Designation System
Contd………..
• (v)DIN AND ISO SYSTEM
For example, 6181=AlSi1Mg0.8
Variation of Mechanical properties with percentage composition of constituent element
• Composition Grouping:There are 7 basic groups…….• Aluminum- copper (2xx)• Aluminum- silicon- copper (3xx)• Aluminum-silicon-magnesium (3xx)• Aluminum- silicon (4xx)• Aluminum- magnesium (5xx)• Aluminum- zinc-magnesium (7xx)• Aluminum-tin (8xx)
Aluminum-Copper
Aluminum-Copper have been used extensively in wrought and cast form where strength and toughness are required. These alloy exhibit
strength and hardness at room and elevated temperatures
Alloy of this types are susceptible to solidification cracking and to interdendritic shrinkage.
Copper-containing aluminum alloys are less resistance to corrosion and may be susceptible to
stress-corrosion
Aluminum-Silicon-Copper
• Copper contributes to strengthening and machinability and silicon improves castability and reduces hot shortness
• Al-Si-Cu alloys with less than 5-6% Cu are heat-treatable, if Mg is added then heat-treatment response is enhanced
Aluminum-Silicon-Magnesium
• Excellent properties after heat treatment, high Corrosion resistance, and a low level of thermal expansion
• While not as strong as high-strength Al-Cu and Al-Si-Cu alloys.
Aluminium-Silicon
• Binary aluminium-silicon alloys exhibit excellent fluidity, castability, and corrosion resistance. These alloys display low strength and poor machinability
• The strength, ductility, and castability of hypoeutectic Al-Si alloys can be further improved by modification of Al-Si eutectic through the controlled addition of sodium and/ or strontium
Aluminium-Magnesium
• Single phase binary alloys with moderate to high strength and toughness
• Most important characteristics is the corrosion resistance including exposed to sea-water and marine application
• Excellent weldability , machinability and attractive appearance
• But they require greater control of temperature gradient
• Mg in Al-alloys increases the oxidation rates
Aluminium-Zinc-Magnesium
• Rapid solidification in these alloys can result in microsegretion of magnesium-zinc phases that reduces hardening potential.
• The cost of heat-treatment, high residual stress levels and distortion are avoided
• The castability of Al-Zn-Mg alloys is poor, and good foundry practices are required to minimize hot tearing and shrinkage defects
Aluminium-Tin• Tin is the major alloying element in compositions developed
for bearing application.• Alloys containing 5.0 to 7.0% Sn are broadly used in bearings
and bushing in which low friction, compressive strength, fatigue strength, and resistance to corrosion are important criteria
• Their light weight minimize loads in reciprocating and heat dissipation improves bearing life
• Al and tin are essentially immiscible before and after solidification, tin is present in dispersed form
• Parts may be plastically cold worked to improve compressive yield strength .
Effects of Alloying Elements
(i) Antimony• 0.10%, antimony refines the aluminum-silicon
eutectic.• But a distinctly lamellar eutectic rather than a fine
fibrous structure• It reacts with sodium or strontium to form coarse
intermetallics with adverse effects on castability and metallurgical structure
• Antimony is a heavy metal with potential of toxicity and associated with stibine gas (SbH3) formation
(ii) Beryllium• Additions of a few parts per million beryllium can be
effective in reducing oxidation losses• At higher concentrations (>0.04% ), beryllium affects the
form and composition of iron-containing intermetallics, markedly improving strength and ductility
• Changing the morphology of the insoluble phase from plate to nodular, beryllium changes its composition, rejecting Mg from the Al-Fe-Si complex and thus permitting its full use for hardening purposes
(iii) Bismuth, Lead, and Cadmium • Bi,Pb, and Cd addition improves the
machinability of cast aluminum alloys, at concentrations greater than 0.1%
(iv) Boron
• Boron combines with other metals to form borides, such as AlB2 and TiB2
• Titanium boride forms stable nucleation sites that interact with active grain-refining phases such as TiAl3 for grain refinement
• Metallic borides reduce tool life and form coarse inclusions with detrimental effects on strength and ductility.
• Borides also contribute to sludging, the precipitation of intermetallics from liquid solution in furnaces .
• Boron treatment with Titanium, Vanadium, Zirconium improve purity and conductivity in electrical applications (Rotor).
(v) Sodium • Sodium modifies the Al-Si eutectic. In the
absence of phosphorus, recovered concentration of 0.01% are effective
• Sodium at less than 0.005% is embrittling in Al-Mg alloys
• Sodium is rapidly lost in molten Al through its high vapour pressure
• Sodium increases surface tension and through addition methods can increase hydrogen content
a) Al-13wt%Si phase diagram and Micrograph
b) Al-13wt%Si-0.01%Na phase diagram and micrograph
(vi) Strontium
• Strontium modifies the Al-Si eutectic. In the absence of phosphorus, recovered concentration range of 0.008% to 0.04% are effective
• Lower concentrations are effective with higher solidification rates
• Higher addition levels are associated with casting porosity
(vii) Phosphorus • As AlP3, phosphorus nucleates and refines
primary silicon-phase formation in hypereutectic Al-Si alloys
• it coarsens the eutectic structure in hypereutectic Al-Si alloys and diminishes the effectiveness of common modifiers
(viii) Tin • Tin is effective in improving antifriction
characteristics and is used in bearing applications.it also improves machinability
(ix) Titanium • Titanium is extensively used to refine grain
structure• TiB2 is necessary grain refinement
(x) Chromium• Chromium typically forms the compound
CrAl3, which display extremely limited solid solubility and is therefore useful in suppressing grain-growth tendencies
• It improves corrosion resistance
a) Without grain refinement b) With grain refinement
Effects of Major Alloying Elements
(i) Silicon• Improvement of casting characteristics • Fluidity, hot tear resistance and feeding characteristics• For slow cooling rate processes such as plaster, investment, and sand,
the preferred range is 5 to 7%, for permanent mold 7 to 9%, and for die casting 8 to 12%
• It combines with Mg and forms an intermetallic compound MgSi2
• Al-Si alloys differ from our "standard" phase diagram in that aluminium has zero solid solubility in silicon at any temperature. This means that there is no beta phase and so this phase is "replaced" by pure silicon (you can think of it as a beta phase, which consists only of silicon).
• Therefore, for Al-Si alloys, the eutectic composition is a structure of alpha+Si rather than alpha+beta
Phase Diagram of Al-Si
(ii) Magnesium • Mg is the basic for strength and hardness development in
heat treated Al-Si alloys and is commonly used in more complex Al-Si alloy containing Cu, Ni and some other elements for same purpose
• The intermetallic compound MgSi2 which acts as a hardening phase display a useful solubility limit corresponding to 0.7% Mg, beyond which either no further strengthening occurs or matrix softening take place
• For high strength Al-Si alloys the range for Mg is between 0.4 to 0.07%
Variation of tensile properties with Mg%
2 4 6 80
50
100
150
200
250
300
350
400
450
0.0% Mn, tensile strength0.1% Mn,tensile strength0.5% Mn, tensile strength0.0% Mn,yield stength0.1% Mn, yield strength0.5% Mn, yield strenth
Mg %
Stre
ngth
MPa
Elongation vs Mg percentage for 1.3mm thick plate
2 4 6 80
5
10
15
20
25
30
35
40
0.1% Mn0.5% Mn0.9% Mn
Mg %
Elon
gatio
n (in
2in
)%
(iii) Copper • It improves strength and hardness in the cast and heat treated
conditions• Alloys containing 4 to 5.5% Cu respond most strongly to
thermal treatment • It reduces corrosion resistance and increases stress-corrosion • It reduces hot tear resistance and increases the potential for
interdendritic shrinkage • Aluminum-copper alloy containing 2 to 10% copper, generally
with other addition, forms important families of alloy. Both cast and wrought aluminum-copper alloys responds to solution heat treatment and subsequent aging with increase in strength and hardness and decrease in elongation.
Variation of tensile properties with copper content
(iv) Iron• Iron improves hot-tearing resistance and
decreases the tendency for die sticking or soldering in die casting .
• Increases in iron content decreased ductility• The intermateilic phases FeAl3, FeMnAl6, and
α-AlFeSi. These insoluble phases are responsible for strength, especially at elevated temperature, but also embrittlement of the microstructure
Effect of Iron plus Silicon impurities on Tensile properties of Al
0 0.2 0.4 0.6 0.8 10
20
40
60
80
100
120
Yield strengthTensile strength
Iron + Silicon %
STRE
NGT
H, M
Pa
(v) Manganese
• In the absences of work-hardening, Mn offers no significant in cast Al-alloys
• High-volume fraction of MnAl6 in alloy containing more than 0.5% Mn may beneficially influence internal soundness
Variation of tensile properties of Al-alloy with Mn %
0 0.5 1 1.5 2 2.50
50
100
150
200
250
300
350
400
450
500
Yield strength (Mpa)
Tensile strength (Mpa)
Elongation (x0.1mm)
Mn %
STRE
NGT
H, M
Pa
(vi) Zinc• Zinc offers no significant benefits in aluminium
casting• Addition of Cu and/ or Mg, however, zinc
results in attractive heat-treatable composition
• Up to 3% Zn in die casting compositions allows the use foe lower-grade and wrought alloy scrap
Variation of tensile properties for Al-Mg alloy with Zn
0 1 2 3 4 5 6 7 8 9 100
100
200
300
400
500
600
700
yield strength-1%Mg
Tensile strength-1%Mg
yield strength-3%Mg
Tensile strength-3%Mg
Zn %
STRE
NGT
H, M
Pa
CASTING
• Sand Casting• Sand casting is the simplest method of casting
aluminium. Sand is made into a mould by forming around a wooden "pattern". The pattern is removed, the sand mould assembled and molten metal poured in. The process is chosen for small production runs, for complex shape castings requiring intricate cores or for very large castings
Sand Casting
Gravity Die-Casting
• Castings are produced by pouring molten metal into permanent metal moulds. It is generally made from cast iron. This process produces ‘ Chill Castings’
Gravity Die-Casting
Low Pressure Die-Casting
• This is a repetitive process where identical parts are cast by injecting molten metal under low pressure into metal dies. This process requires complex machinery and is similar to high pressure die-casting
Low Pressure Die-Casting
High Pressure Die- casting
• High pressure die- casting is a repetitive process for casting identical parts by injecting Aluminium into metal moulds at pressures in the order of 1000psi. Complex machinery and expensive tooling is required for this process. It is characterized by very good surface finish and dimensional consistency. The advantage of this system includes fast cycle times and the convenience of melting the metal in the casting machine.
High Pressure Die- casting
Diesel Furnace
• A diesel furnace is a piece of equipment that produces heat by burning diesel. The diesel used to power the furnace can be of petroleum origin. It is used to make casting specimens. We used a K- type thermocouple to measure the temperature. Temperature Range – 0 to 1100 ºC. We also used a multi channel temperature indicator for mesuring casting temperature.
• The highest temperature that can be obtained in a diesel furnace (in workshop) is 950ºC. The temperature required to melt LM 25 alloy was around 700ºC to 750ºC. It took around 20- 25 minutes to melt the material. After that we took it to a crusible(refractory container) and with the help of laddle we poured the molten metal into the mould. It took 2-3 days to solidify the molten metal and the specimen was obtained. The specimen was mad using three dies- sand, graphite and metal.
Prepared Specimen
BHN values comparision- graphite˂ metal˂sand
CASTING SIMULATION USING PROCAST
FIRST ITERATIONCAST SPECIMEN SPECIFICATION. One test bars with dimensions of 12mm diameter, 52mm gage
length. Cast material is LM25. Two circular section of 20 mm diameter and length 20 mm,
test section diameter 12 mm and 52 mm gauge length. Top gate is designed for this iteration.
CASTING DESIGN.
PROCESS PARAMTER SPECIFICATION
Parameter’s Magnitude
Metal velocity 0.1 m/sec
Casting pressure 1 atm (101325 pa )
Ambient temperature 30 deg Celsius
Film coefficient between casting and mould
100 w/m*m*k
Melt temperature 715 deg Celsius
Die Material Sand Silica
Casting metal Al_AlSi7Mg
TET MESH GENERATION
PRECAST INITIALIZED.
CASTING MATERIAL ASSIGN
MOULD MATERIAL ASSIGN
DEFINING RUN PARAMTER
PROCAST SOLVER
FILL TIME
INTERPRETATION OF RESULT
THIS SHOWS THE TIME WHICH IS REQUIRED FOR THE MOLTEN METAL TO REACH AT A PARTICULAR
POINT. WE CAN KNOW AFTER WHAT TIME MOLTEN METAL
WILL REACH AT THE INTERESTED POINT. IT IS USED FOR THE PREDICTION OF CATING YIELD, IF
FILL TIME FOR A POINT IS MORE THAN THE SOLIDIFICATION TIME OF EARLY POINT IN GATEING SYSTEM THEN THAT POINT WILL REMAIN
EMPTY.
FRACTION SOLID AT 70 SEC
INTERPRETATION OF RESULTTHIS RESULT PREDICTES THE MASS
PERCENTAGE OF SOLID.THIS TELL’S HOW MUCH PERCENTAGE
OF SOLID IS PRESENT AT A GIVEN TIME.LINK FOR ANIMATION.
PRESSURE VARIATIONAT 0.51 SEC
INTERPRETATION OF RESULT.
THIS WILL TELL WHAT IS THE PRESSURE AT EACH SECTION AT A GIVEN TIME.
THE VARIATION OF PRESSURE DIRECTLY INFLUSENCE THE GRAIN SIZE AND HENCE MECHANICAL PROPERTIES.
THE GRAIN SIZE CAN PREDICTED FROM THE PRESSURE AT A POINT.
LINK FOR ANIMATION.
MOULD TEMPERATURE AT 190 SEC
INTERPRETATION OF RESULTTHIS PREDICTES THE VARIATION OF MOULD
TEMPERATURE WITH TIME.THE POINTS WHERE THE TEMPERATURE
REACHES HIGH VALUE WHICH CAN CAUSE HARM TO FOUNDRYMAN.
LINK FOR ANIMATION.
AIR ENTRAPMENT AT 0.57 SEC
INTERPRETATION OF RESULT
THIS TELL’S THE ENTRAPED AIR AT A GIVEN TIME
THIS RESULT CAN BE USED TO PREDICT THE LOCATIONS WHERE AIR CAVITY CAN BE PRESENT IN CASTING.
AIR OR GAS VENT’S CAN BE PROVIDED AT SUITABLE LOCATIONS WHERE THIS AIR ENTRAPMENT IS OCCURING.
LINK FOR ANIMATION.
SOLIDIFICATION TIME.
INTERPRETATION OF RESULTIT PREDICT THE SOLIDIFICATION TIME OF
EVERY POINT.THE MAXIMAM SOLIDIFICATION TIME AND
MINIMUM SOLIDIFICATION TIME CAN BE FOUND OUT.
IF THE SOLIDIFICATION TIME OF A POINT IS LESS THAN THE FILL TIME OF A POINT AFTER IT THEN THE RESULTING CASTING WILL HAVE VOIDS.
TEMPERATURE Vs TIME GRAPH.
INTERPRETATION OF RESULTTHIS GRAPH IS PLOTED BETWEEN TEMPERATURE
AND TIME.THIS GRAPH IS FOR NODAL GAP OF 50.EACH CURVE SHOWS THE TEMPARATURE
VARIATION OF A PARTICULAR NODE WITH TIME.THIS GRAPH WILL BE USED TO KNOW THE
TEMPARATURE OF A PARTICULAR NODE.GRAPH TELL THE TEMPARATURE AT EACH POINT
IN CASTING AND MOULD.LINK FOR ANIMATION.
TEMPARATURE VARIATION OF A NODE
INTERPRETATION OF RESULTTHIS GRAPH SHOWS THE VARIATION OF
TEMPARATURE OF A NODE WHICH IS IN CASTING WITH TIME AND HENCE ITS SOLIDIFICATION RATE CAN BE FOUND OUT.
SOLIDIFICATION RATE INFLUENCE THE HARDNESS.
FRACTION SOLID WITH TIME
INTERPRETATION OF RESULT
THIS GRAPH SHOWS THE FRACTION SOLID WITH NODAL GAP OF 50.
IN ASINGLE GRAPH ALL THE POINT IN CASTING ARE PLOTED WITH THERE FRACTION SOLID WITH TIME.
VOID CREATED AFTER SOLIDIFICATION
INTERPRETATION OF RESULT
AFTER THE SOLIDIFICATION OF CASTING THERE WILL BE A VOID AT TOP MOST PORTION.
VOID OCCURRED BECAUSE THE MOLTEN METAL AT TOP SOLIDIFES AT LAST.
THIS CAN BE AVOIDED WITH PROVIDING A SPUR OF SOME EXTRA HEIGHT.
POROSITY
INTERPRETATION OF RESULT
THIS RESULT CAN TELL US ABOUT THE LOCATION WHERE POROSITY WILL OCCUR.
POROSITY IS A MEASURE OF THE VOID SPACES IN MATERIAL, AND IS A FRACTION OF THE VOLUME OF VOIDS OVER THE TOTAL VOLUME, BETWEEN 0 TO 1 OR AS A PERCENTAGE BETWEEN 0 TO 100.
LINK FOR ANIMATION.
CONCLUSION FOR DESIGNTHIS DESIGN WHICH HAVE TOP GATEING SYSTEM
WILL HAVE SHRINKAGE CAVITY, VELOCITY OF MOLTEN METAL WILL CAUSE SAND INCLUSION.
THIS DESIGN HAS DRAWBACKS OF VOID CREATION, SHRINKAGE POROSITY, FILL TIME OF SOME SECTION ARE MORE THAN THE SOLIDIFACTION TIME OF PREVIOUS POINTS.
NOW WE KNOW WHERE CASTING WILL HAVE DEFECTS, SO WE CAN GO FOR A DESIGN WHICH CAN OVER COME IT.
SECOND ITERATION.
SAME CASTING SPECIMEN SPECIFICATION AS FIRST ITERATION.
THE GATING SYSTEM USED IS BOTTOM GATE.
DEISGN OF CASTING.
PROCESS PARAMTER SPECIFICATION
Parameter’s Magnitude
Metal velocity 0.2 m/sec
Casting pressure 10 atm (101325 pa )
Ambient temperature 30 deg Celsius
Film coefficient between casting and mould
20 w/m*m*k
Melt temperature 715 deg Celsius
Die Material REFRACTORY GRAPHITE MOULD.
Casting metal Al_AlSi7Mg
VELOCITY OF MOLTEN METAL
INTERPRETATION OF RESULTTHIS SHOWS THE VELOCITY PROFILE AND ITS
MAGNITUDE AND HENCE THE EFFECT ON MOULD BECAUSE OF MOLTEN METAL FLOW.
FRACTION SOLID AT T=2.58 SEC
INTERPRETATION OF RESULT
AT THE TIME 2.58 SEC THE MOULD IS NOT COMPLETELY FILLED AND TILL THAT TIME ALL THE MOLTEN METAL IS AT SAME POURING TEMPARATURE BECAUSE THE MOULD IS A REFACTORY MATERIAL WITH VERY LESS FILM COEFFICIENT BETWEEN INTERFACE.
VOID CREATION AT TIME 2.58 SEC
INTERPRETATION OF RESULT
SINCE DURING THE TIME OF 2.58 SEC THE MOULD IS NOT COMPLETELY FILLED HENCE THERE WILL BE A VOID AT THAT TIME.
THIS VOID MAY NOT BE THERE IF SIMULATION IS RUNNED FOR MORE TIME.
TEMPARATURE VARIATION
INTERPRETATION OF RESULT
SINCE THE MOULD IS A BAD CONDUCTOR OF HEAT SO THERE WILL BE VERY LESS HEAT TRANSFER TO SURROUNDING AND MOLTEN METAL WILL BE AT TEMPERATURE OF POURING FOR TIME 2.58 SEC.
VARIATION OF TEMPARATURE.
INTERPRETATION OF RESULT
THERE IS VERY LESS TEMPARATURE VARIATION IN BOTH CASTING AND MOULD BECAUSE THE MOULD MATERIAL IS BAD CONDUCTORE OF HEAT.
THIS RESULT IS ONLY TILL TIME 2.58 SEC.
CONCLUSION.SO FAR TILL TIME OF 2.58 SEC THERE IS
PROPER MOULD FILLING.NOTHING CAN BE CONCLUDED FROM
THIS SIMULATION BECAUSE THE TIME OF SIMULATION IS NOT ENOUGH TO FILL THE MOULD COMPLETELY.
BUT THERE IS WASTAGE OF MATERIAL IN SPUR AND ALSO IT IS DIFFICULT TO REMOVE THE RUNNER AND SPUR FROM CASTING.
ITERATION THIRD.
CAST SPECIMEN SPECIFICATION. ONE TEST BARS WITH DIMENSIONS OF 12MM
DIAMETER, 52MM GAGE LENGTH. CAST MATERIAL IS LM25. TWO CIRCULAR SECTION OF 20 MM DIAMETER
AND LENGTH 20 MM, TEST SECTION DIAMETER 12 MM AND 52 MM GAUGE LENGTH.
BRANCHED GATE IS DESIGNED FOR THIS ITERATION.
CASTING DESIGN.
PROCESS PARAMTER SPECIFICATION
Parameter’s Magnitude
Metal velocity 0.3 m/sec
Casting pressure 1 atm (101325 pa )
Ambient temperature 30 deg Celsius
Film coefficient between casting and mould
20 w/m*m*k
Melt temperature 715 deg Celsius
Die Material Refractory graphite
Casting metal Al_AlSi7Mg
TEMPARATURE VARIATION.
AT TIME 30.8 SEC.
AT TIME 30.8 SEC.
AT TIME 160 SEC.
AT TIME 160 SEC.
TEMPATURE Vs TIME
AIR ENTRAPMENT.
FRACTION SOLID AT T= 40 SEC
FRACTION SOLID Vs TIME.
PROSOITY.
SOLIDIFICATION TIME.
FILL TIME.
CONCLUSION.
THIS DESIGN IS BETTER THAN OTHER AS THERE IS UNIFORM SOLIDIFICATION TIME FOR CASTING.
STANDARDIZATION
• We need to standardize the data of LM25 using the instruments available in the campus so that we can compare this data with the enhanced alloy to be produced. Standardization or standardization is the process of developing and agreeing upon technical standards. A standard is a document that establishes uniform engineering or technical specifications, criteria, methods, processes, or practices. Some standards are mandatory while others are voluntary. Voluntary standards are available if one chooses to use them. Some are de facto standards, meaning a norm or requirement which has an informal but dominant status. Some standards are de jure, meaning formal legal requirements. Formal standards organizations, such as the International Organization for Standardization (ISO) or the American National Standards Institute, are independent of the manufacturers of the goods for which they publish standards
Metallographic Specimen Preparation
Specimen Preparation• The first step in specimen preparation is selection and
separation of samples from the bulk material (sampling) is of special importance. If the choice of a sample is not representative of the material, it cannot be corrected later.it is also difficult to compensate later for improper sectioning, because additional ,time consuming corrective steps are necessary to remove the initial damage.
• Sectioning should render a plane surface for the following preparation without causing critical changes in the material
Mounting• Mounting of specimens is usually necessary to allow them
to be handled easily.it also minimizes the amount of damage likely to be caused to the specimen itself.
• The mounting material used should not influence the specimen as a result of chemical reaction or mechanical stresses.it should adhere well to the specimen ,and if the specimen is to be electro polished later in the preparation then the mounting should also be electrically conducting
• A mounted specimen usually has a height half its diameter, to prevent rocking during grinding and polishing. The polishing edges of the mounting specimen should also be rounded to minimize the damage to grinding and polishing discs.
Grinding• Surface layers damaged by cutting must be removed by grinding.
Mounted specimens are ground with rotating discs of abrasive paper, for example wet silicon carbide paper. The coarseness of the paper is indicated by a number: the number of grains of silicon carbide per square inch. So, for example, 180 grit paper is coarser than 1200 grit.
• The grinding procedure involves several stages, using a finer paper (higher number) each time. Each grinding stage removes the scratches from the previous coarser paper. This can be easily achieved by orienting the specimen perpendicular to the previous scratches. Between each grade the specimen is washed thoroughly with soapy water to prevent contamination from coarser grit present on the specimen surface. Typically, the finest grade of paper used is the 1200, and once the only scratches left on the specimen are from this grade
Polishing• Polishing discs are covered with soft cloth impregnated with
abrasive diamond particles and an oily lubricant or water lubricant. Particles of two different grades are used : a coarser polish-typically with diamond particles 6 microns in diameter which should remove the scratches produced from the finest grinding stage, and a finer polish-typically with diamond particles 1 micron in diameter, to produce a smooth surface. Polishing wheel the specimen should be wasted thoroughly with warm soapy water followed by alcohol to prevent contamination of the disc. The drying can be made quicker using a hot air drier.
•Mechanical polishing will always leave a layer of distributed material on the surface of the specimen. Electro polishing or chemical polishing can be used to remove this, leaving an undisturbed surface
Specimen after grinding
HARDNESS TEST• The Brinell hardness test is used to measure the hardness
of the composites. The Brinell hardness test method consist of indenting the test material with a 10 mm diameter hardness steel ball subjected to a load of 500 kg for softer materials. The full load is normally applied for at least 30 seconds. The diameter of the indentation left in the test material is measured with low powered microscope. The average of two reading of the diameter of impression at right angle should be made. Surface on which the indentations is made be smooth and free from dirt or scale. The brinell hardness number is calculated by dividing the load applied by the surface area of the indentation.
Hardness Test Using Brinell Hardness Testing Machine
• BHN =• Where • P is applied load (kg)• D : is diameter of the ball (mm)• d : is diameter of the indentation (mm)
Hardness Test Using Brinell Hardness Testing Machine
TYPES OF MOULD BHN DIAMETER OF INDENTATION (d in mm)
SAND 60 3.213METAL 58 3.267GRAPHITE 56 3.323
OBTAINED RESULTApplied load, P = 500 KgMaterial of Indentor : carbon steelDiameter of Indentor , D = 10mm
Hardness Test Using Brinell Hardness Testing Machine
Universal Measuring Microscope
SURFACE ROUGHNESS
• Surface roughness is measure of the finer surface irregularities in the surface texture. These are results of the manufacturing process employed to create the surface. Surface roughness Ra is rated as the arithmetic average deviation are large, the surface is rough; if they are small the surface is smooth. Roughness is typically considered t be the frequency, short wavelength component of a measured surface.
• The surface roughness of the machined composites is measured by using profilometer
Measurement of surface roughness using surface profilometer.
OBTAINED DATARa is the arithmetic average of the absolute values and Ry is the range of the collected
roughness data points
SAND MOULD GRAVITY MOULD
METAL MOULD
Ra Ry Ra Ry Ra Ry
13.55 75.62 4.04 26.26 7.39 50.16
13.77 76.74 3.65 24 7.91 63.23
11.51 60.35 4.13 23.32 8.84 65.67
9.56 54.67 5.48 30.31 6.91 43.27
10.93 61.68 6.98 38.21 7.46 52.36
12.6 72.68 5.61 34.64 8.48 64.67
11.33 62.21 6.51 41.49 7.73 51.36
13.23 71.24 5.78 31.22 6.68 42.36
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