Page 1
1Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
KOKYU ALCOHOL KOGYO CO., LTD.Head Office & Plant Taiei Kogyo Danchi, 641-6 Kichioka, Narita, Chiba
287-0225 JapanTEL : +81-476-73-6020 FAX : +81-476-73-6024
Tokyo Office Kasahara Bldg. 4F, 1-7-7 Nihonbashi Ningyocho, Chuo-ku, Tokyo 103-0013 JapanTEL : +81-3-3667-2801 FAX : +81-3-3667-3980E-mail : [email protected] URL : http://www.hai-global.com/
Raw material approved by ECOCERT GREENLIFE, conform to the ECOCERT Natural and Organic Cosmetics Standard.Nevertheless, for the certification of final cosmetic products containing ECOCERT already approved ingredients, it must be certified individually according to the ECOCERT Cosmetic Standard.
PR21 [RISOCAST DA-L] en_180701Creation date : Oct. 22, 2007 (Revision date : Jul. 01, 2018)
2Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
MATERIAL INFORMATION
INCI nameCAS No.Chinese INCI name
: HYDROGENATED CASTOR OIL DIMER DILINOLEATE: 646054-62-8: 氢化蓖麻油二聚亚油酸酯
RISOCAST DA-L is an ester obtained from dimer acid and hydrogenated castor oil, approved by ECOCERT.
FEATURES SPECIFICATIONS ꞏ REFERENCE
SPECIFICATIONSVegetable-based high viscosity pasty oil
Rich texture
Natural gloss
Good water-absorption capacity
Prevents syneresis and increases hardness
Specification value
Description Pale yellow, pasty solid, faint characteristic odor
Acid value Not more than 6
Saponification value 160 - 210
Iodine value Not more than 8
Hydroxyl value 60 - 90
Color Not more than 10 Gardner
Reference value
Viscosity 900 mPa・s (60 ºC)
REFERENCEand bending strength of lipsticks
Listed on the Inventory of Existing Cosmetic Ingredients in China
Page 2
3Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
REFRACTIVE INDEX AND WATER-ABSORPTION CAPACITY
Measurement conditions
ApparatusLight sourceTemperature
: Abbe Refractometer NAR-2T (ATAGO CO., LTD.): LED lamp (D-line wavelength): 20 °C
REFRACTIVE INDEX
RISOCAST DA-L is a vegetable derived high viscosity oil with high refractive index and good water-absorption capacity
1.0
1.2
1.4
1.6
1.8
2.0
リソカスタ DA L ⽔添ポリイソブン ラノリン
Ref
ract
ive
inde
x
0
100
200
300
RISOCAST DA-L PB18 LANOLIN
Measurement method
(remove the excess water).
RISOCASTDA-L
HYDROGENATED POLYISOBUTENE
(MW : 1000)
LANOLIN RISOCASTDA-L
HYDROGENATED POLYISOBUTENE
(MW : 1000)
LANOLIN
WATER-ABSORPTION CAPACITY
Wat
er-a
bsor
ptio
n ca
paci
ty (
%)
Water-absorption capacity (%) = x 100Weight of water added (g)
Weight of test sample at start (g)
1. 10 g of sample is weighed in a polyethylene container (500 mL).2. Purified water is added little by little and gently mixed (approx. 0.5 mL/min).3. Mixing is stopped when the sample does not absorb water anymore
4. The water-absorption capacity is calculated.
Similar refractive index toHYDROGENATED POLYISOBUTENE
and LANOLIN.
Good water-absorption capacity compared to HYDROGENATED
POLYISOBUTENE and LANOLIN.
The data shows measurement value.
4Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
1
10
100
1000
1 10 100 1000
PB24 PB18 DA-Lラノリン
TEXTURESensory evaluation and viscoelastic measurement
(1) SENSORY EVALUATION (n=4) (2) VISCOELASTIC MEASUREMENT
Texture of RISOCAST DA-L is evaluated by (1) sensory evaluation and (2) viscoelastic measurement (Texture : hardness and spreadability)
HYDROGENATED POLYISOBUTENE (MW : 1350)
HYDROGENATED POLYISOBUTENE (MW : 1000)
RISOCAST DA-LLANOLIN
Shear rate (1/s)
Vis
cosi
ty(P
a・s)
Measurement temperature : 35 ºC
HardSoft
Low spreadability
High spreadability
RISOCAST DA-L
HYDROGENATEDPOLYISOBUTENE
(MW : 1000)
LANOLIN
HYDROGENATEDPOLYISOBUTENE(MW : 1350)
The data shows measurement value.
Page 3
5Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
COMPATIBILITY
Sample MINERAL OIL(HICALL K-230)
ISOTRIDECYL ISONONANOATE
(KAK 139)
DIPENTAERYTHRITYL HEXAISONONANOATE
(HAILUCENT DPIN6)
CAPRYLIC/CAPRIC TRIGLYCERIDE
(TCG-M)
ISOSTEARYL ISOSTEARATE
(ISIS)
OCTYLDODECYLSTEAROYL STEARATE
(RISOCAST ODSHS)
Concentrationof DA-L 10 % 50 % 10 % 50 % 10 % 50 % 10 % 50 % 10 % 50 % 10 % 50 %
State at 80 ºC T N C C C C C C C C C C
State after1 week at 25 ºC N N N T T T N T N T N T
SampleTRIMETHYLOLPROPANE TRIISOSTEARATE
(KAK TTI)
PENTAERYTHRITYL TETRAISOSTEARATE
(KAK PTI)
OCTYLDODECANOL(RISONOL 20SP)
POLYGLYCERYL-2 TRIISOSTEARATE
(RISOREX PGIS23)
POLYGLYCERYL-2 DIISOSTEARATE(RISOREX PGIS22)
DIISOSTEARYL MALATE
(HAIMALATE DIS)
Concentrationof DA-L 10 % 50 % 10 % 50 % 10 % 50 % 10 % 50 % 10 % 50 % 10 % 50 %
State at 80 ºC C C C C C C C C C C C C
State after1 week at 25 ºC T T T T N T T T T T T T
RISOCAST DA-L is mixed with each oil and heated up to 80 ºC for 1 hour The appearance at 80 ºC is visually observed and then re-checked after 1 week at 25 ºC
Abbr. C : Compatible T : Turbid N : Not compatible Typical data
6Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
EFFECT ON SOLID MIXTURESEvaluation of DA-L-wax interaction : application to lipstick
0
0.1
0.2
0.3
0.4
0.5
0.6
10 15 20 25
DA-L
PB-18
PB-24
ラノリン
0
0.5
1.0
1.5
2.0
5 10 15 20
PB24
PB18
DA-L
LANOLIN
SOLID MIXTURES OF SOLID MIXTURES OFMICROCRYSTALLINE WAX AND OIL POLYETHYLENE AND OIL
Concentration ofMICROCRYSTALLINE WAX (%)
Concentration ofPOLYETHYLENE (%)
Har
dnes
s (N
)
Har
dnes
s (N
)
Measurement method of hardness
Compact Table-Top Universal Tester EZ Test 20N (SHIMADZU CORPORATION) : A 1.0 mm diameter needle penetrates into a solid mixture at 10 mm/min. The hardness is the highest result obtained after a penetration of 10 mm (at 25 ºC).
Measurement temperature : 25 ºCMeasurement temperature : 25 ºC
• HYDROGENATED POLYISOBUTENE (MW : 1350) : PB24• HYDROGENATED POLYISOBUTENE (MW : 1000) : PB18
RISOCAST DA-L is mixed with various concentrations of wax in order to measure the hardness of the mixture HYDROGENATED POLYISOBUTENE (commonly used high viscosity oil) and LANOLIN are selected as comparative oils
The data shows measurement value.
Page 4
7Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
EFFECT ON LIPSTICK (1) Comparison with HYDROGENATED POLYISOBUTENE and LANOLIN
The effect of RISOCAST DA-L on lipstick formulations is evaluated RISOCAST DA-L is compared to HYDROGENATED POLYISOBUTENE (commonly used high viscosity oil) and LANOLIN
Product name/Supplier INCI name wt%
Bas
e fo
rmul
atio
n
1.TCG-M(KOKYU ALCOHOL KOGYO CO., LTD.)
CAPRYLIC/CAPRIC TRIGLYCERIDE 48.0
2. High viscosity oil*1 - 25.0
3. HAIMALATE DIS(KOKYU ALCOHOL KOGYO CO., LTD.)
DIISOSTEARYL MALATE 13.0
4. Refined Microcrystalline Wax(NIKKO RICA CORPORATION)
MICROCRYSTALLINE WAX 7.0
5.POLYWAX-500(Baker Hughes Incorporated)
POLYETHYLENE 7.0
Lips
tick
form
ulat
ion
Base formulation 90 %
Pink pigment paste 10 %
Product name/INCI name Abbr. Viscosity*2
(mPaꞏs, 25 ºC)
HYDROGENATED POLYISOBUTENE(MW : 1350)
PB24 75200
RISOCAST DA-L DA-L 26100
LANOLIN LANOLIN 21700
LIPSTICK FORMULATIONS FOR COMPARISON
*2 The viscosity is the one at 10 (1/s) of shear rateby viscoelasticity measurement.
*1 High viscosity oils are used one by one from the list on the right.
The data shows measurement value.
8Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
EFFECT ON LIPSTICK (1) Comparison with HYDROGENATED POLYISOBUTENE and LANOLIN
0
0.1
0.2
0.3
0.4
00.51.01.52.02.53.0
DA-LPB241.0
1.5
2.0
2.5
8
10
12
14
16
Har
dnes
s (N
)
HARDNESS BENDING STRENGTH
Dep
osite
d qu
antit
y of
lips
tick
(mg)
DEPOSITED QUANTITY SMOOTHNESS
LANOLIN
Ben
ding
stre
ngth
(N
)
PB24
DA-L
LANOLIN
Sufficient
Insufficient
MIU
(sm
ooth
ness
)
1 2 3Frequency of application
(reciprocating time)
Measurement temperature : 25 ºC Measurement temperature : 25 ºC
Measurement temperature : 35 ºC Measurement temperature : 35 ºC
: H (high) : M (medium) : L (low)
The data shows measurement value.
DA-LPB24 LANOLIN
DA-LPB24 LANOLIN
Page 5
9Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
SEM IMAGES OF LIPSTICK
Apparatus : SEM JSM-6460LA(JEOL Ltd.)
Accelerating voltage : 5 kVResolution : HV modeMagnification :X 200, X 1000Detector : secondary electron detectorPre-treatment : freeze-fracture,
Osmium evaporation
Product name wt%
TCG-M 48.0
High viscosity oil 25.0
HAIMALATE DIS 13.0
Refined Microcrystalline Wax 7.0
POLYWAX-500 7.0
Measurement conditions
The formulations with different high viscosity oils are observed by SEM to check their crystal size HYDROGENATED POLYISOBUTENE (commonly used high viscosity oil) and LANOLIN are selected as comparative oils Crystal size of RISOCAST DA-L is found finer than the others
PB24 DA-L LANOLIN
X 200
PB24 DA-L LANOLIN
X 1000
10Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
EFFECT ON LIPSTICK (1) Comparison with HYDROGENATED POLYISOBUTENE and LANOLIN
0
500
1000
0 100 2000
500
1000
1500
2000
0 120 240 360
DA-L
Shear rate (1/s)
She
ar s
tres
s (P
a)
Time (s)
She
ar s
tres
s (P
a)
She
ar s
tres
s (P
a)
Time (s)
0
100
200
300
400
500
600
0 60 120 180 240 300 360
PB24
DA-L
LANOLIN
Light
Heavy
Smooth
LANOLIN
PB24
Good adhesion
Presence of “shoulder”
Height of stress value
Texture by viscoelasticity
Viscosity(mPaꞏs, 25 ºC)
PB24 YES MediumEven coverage and medium adhesion 75200
DA-L YES MediumEven coverage and medium adhesion 26100
LANOLIN NO Low Smooth and light texture 21700
: H (heavy) : M (medium) : L (light)
Hysteresis loop is observedduring the 1st cycle
Stress changes during the 3 cycles
Stress changes during the 3 cycles (enlarged view)
TEXTURE EVALUATION BY VISCOELASTIC MEASUREMENTSENSORY EVALUATION (n=6)
The data shows measurement value.
Page 6
11Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
EFFECT ON LIPSTICK (1) Conclusion
Texture by viscoelasticity Hardness
Bending strength
Deposited quantity
HYDROGENATED POLYISOBUTENE(MW : 1350)
M
M M M
RISOCAST DA-L M H M
LANOLIN L M M M
Characteristics of lipstick with RISOCAST DA-L :
Increases bending strength with good adhesion Similar lipstick texture to the one with HYDROGENATED POLYISOBUTENE (PB24)
: H (heavy/high) : M (medium) : L (light/low)
12Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
EFFECT ON LIPSTICK (2) In combination with various oils
Product name/INCI name Abbr. Viscosity
(mPaꞏs, 25 ºC)
KAK PTI(PENTAERYTHRITYL TETRAISOSTEARATE)
PTI 309
KAK TTI(TRIMETHYLOLPROPANE TRIISOSTEARATE)
TTI 205
KAK DADIP-R(DIISOPROPYL DIMER DILINOLEATE)
DADIP 111
RISOCAST ODSHS(OCTYLDODECYL STEAROYL STEARATE)
ODSHS 96
RISOCAST IOHS(ETHYLHEXYL HYDROXYSTEARATE)
IOHS 55
RISONOL 20SP(OCTYLDODECANOL)
20SP 49
TCG-M(CAPRYLIC/CAPRIC TRIGLYCERIDE)
TCG 26
KAK 139(ISOTRIDECYL ISONONANOATE)
139 11
Product name/Supplier INCI name wt%
Bas
e fo
rmul
atio
n
1. Liquid oil* - 48.0
2. RISOCAST DA-L(KOKYU ALCOHOL KOGYO CO., LTD.)
HYDROGENATED CASTOR OIL DIMER DILINOLEATE 25.0
3.HAIMALATE DIS(KOKYU ALCOHOL KOGYO CO., LTD.)
DIISOSTEARYL MALATE 13.0
4.Refined Microcrystalline Wax(NIKKO RICA CORPORATION)
MICROCRYSTALLINE WAX 7.0
5.POLYWAX-500(Baker Hughes Incorporated)
POLYETHYLENE 7.0
Lips
tick
form
ulat
ion
Base formulation 90 %
Pink pigment paste 10 %
*Liquid oils are used one by one from the list on the right.
The effect of liquid oils used in combination with RISOCAST DA-L is checked by evaluation of the following formulations
LIPSTICK FORMULATIONS FOR COMPARISON The data shows measurement value.
Page 7
13Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
EFFECT ON LIPSTICK (2) In combination with various oils
0
0.1
0.2
0.3
0.4
00.51.01.52.02.53.0
ODSHS
PTI
PTITTIDADIPODSHSIOHS20SPTCG139
0
0.5
1.0
1.5
2.0
2.5
0
4
8
12
16
DADIP
20SP 139TCGTTI IOHS ODSHS
PTI DADIP
20SP 139TCGTTI IOHS
ODSHS
PTI DADIP
20SP 139TCGTTI IOHS
HARDNESS BENDING STRENGTH
DEPOSITED QUANTITY SMOOTHNESS
Measurement temperature : 25 ºC Measurement temperature : 25 ºC
Measurement temperature : 35 ºC Measurement temperature : 35 ºC
Har
dnes
s (N
)D
epos
ited
quan
tity
of li
pstic
k (m
g)
Ben
ding
stre
ngth
(N
)
Sufficient
Insufficient
MIU
(sm
ooth
ness
)
1 2 3Frequency of application
(reciprocating time)
: H (high) : M (medium) : L (low)
The data shows measurement value.
14Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
EFFECT ON LIPSTICK (2) In combination with various oils
Presence of “shoulder”
Height of stress value Texture by viscoelasticity Viscosity
(mPaꞏs, 25 ºC)
PTI YES High Heavy texture and good adhesion 309
TTI YES High Heavy texture and good adhesion 205
DADIP YES High Heavy texture and good adhesion 111
ODSHS YES Medium Even coverage and medium adhesion 96
IOHS YES Medium Even coverage and medium adhesion 55
20SP YES Medium Even coverage and medium adhesion 49
TCG YES Medium Even coverage and medium adhesion 26
139 NO Low Smooth and light texture 11
0
500
1000
0 100 2000
500
1000
1500
2000
0 120 240 3600
100
200
300
400
500
600
0 60 120 180 240 300 360
PTI TTI DADIP ODSHS IOHS 20SP TCG 139
ODSHS
TCG
139
DADIP
PTI
20SP
TTI
IOHS
Light
Heavy
Smooth Good adhesion
Measurement temperature : 35 ºC
Shear rate (1/s)
She
ar s
tres
s (P
a)
Time (s)
She
ar s
tres
s (P
a)
She
ar s
tres
s (P
a)
Time (s)
: H (heavy) : M (medium) : L (light)
Hysteresis loop is observedduring the 1st cycle
Stress changes during the 3 cycles
Stress changes during the 3 cycles (enlarged view)
TEXTURE EVALUATION BY VISCOELASTIC MEASUREMENTSENSORY EVALUATION (n=6)
The data shows measurement value.
Page 8
15Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
RISOCAST DA-L could be combined with various oils for lipsticks to obtain the following effects :
EFFECT ON LIPSTICK (2) In combination with various oils : conclusion
Texture by viscoelasticity Hardness
Bending strength
Deposited quantity
KAK PTI
H
M H MKAK TTI M M M
KAK DADIP-R M H L
RISOCAST ODSHS
M
L M MRISOCAST IOHS L L MRISONOL 20SP M L MTCG-M M H LKAK 139 L M M L
KAK DADIP-R and KAK PTI KAK PTI, KAK DADIP-R and TCG-M RISOCAST ODSHS, KAK TTI and RISOCAST IOHS KAK PTI, KAK TTI and KAK DADIP-R KAK 139
To increase hardness To increase bending strength To increase deposited quantity To add good adhesion To add smooth spreadability
: H (heavy/high) : M (medium) : L (light/low)
16Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
EFFECT ON LIP GLOSSComparison with HYDROGENATED POLYISOBUTENE (PB)
Product name/Supplier INCI name wt%
1. High viscosity oil* - 40.0
2. RISOREX PGIS22(KOKYU ALCOHOL KOGYO CO., LTD.)
POLYGLYCERYL-2 DIISOSTEARATE 30.0
3. HAIMALATE DIS(KOKYU ALCOHOL KOGYO CO., LTD.) DIISOSTEARYL MALATE 14.0
4. KAK PTI(KOKYU ALCOHOL KOGYO CO., LTD.)
PENTAERYTHRITYL TETRAISOSTEARATE 8.7
5. Rheopearl KL2(Chiba Flour Milling Co., Ltd.) DEXTRIN PALMITATE 5.0
6. Hi-Mic-1090(NIPPON SEIRO CO., LTD) MICROCRYSTALLINE WAX 2.0
7. Pink pigment paste - 0.2
8. d-δ-TOCOPHEROL(Tama Biochemical Co., Ltd.) TOCOPHEROL 0.1
Product name/INCI name Abbr.
RISOCAST DA-L DA-L
HYDROGENATED POLYISOBUTENE(MW : 1000)
PB18
LIP GLOSS FORMULATIONS FOR COMPARISON
(1) Mix 1 - 8 into a suitable container and heat up. (2) Stir until completely melted and well dispersed, and de-aerate.(3) Cool down.
Process
The effect of RISOCAST DA-L on lip gloss formulations is evaluated RISOCAST DA-L is compared to HYDROGENATED POLYISOBUTENE (commonly used high viscosity oil)
*High viscosity oils are used one by one from the list on the right.
Page 9
17Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
EFFECT ON LIP GLOSSComparison with PB : sensory evaluation and viscoelastic measurement
0
200
400
600
800
1000
1200
0 60 120 180 240 300 360 420
DA-L
PB18500 2.5
PB18
DA-L
0.1
1
10
100
1000
0.1 1 10 100 1000
DA-L
PB18
DA-L
Measurement temperature : 35 ºC Measurement temperature : 35 ºC
Time (s)
She
ar s
tres
s(P
a)
Shear rate (1/s)
Vis
cosi
ty(P
a・s)
: Good adhesion/Rich type : Smooth/Light type
Rich
Light
SmoothGoodadhesion
Results of sensory evaluation and viscoelastic measurement for lip gloss are shown in this slide
Lip gloss with RISOCAST DA-L is richer and smoother than PB18
The data shows measurement value.
18Copyright © 2007 KOKYU ALCOHOL KOGYO CO., LTD. All rights reserved.
CHARACTERISTICSConclusion
BASIC CHARACTERISTICS
EFFECT ON LIPSTICK FORMULATIONS
EFFECT ON LIP GLOSS FORMULATIONS
• Vegetable-based (approved by ECOCERT) high viscosity pasty oil with rich texture• Natural gloss and good water-absorption capacity • Good compatibility with various oils at high temperature
Recommended applications : lipstick, lip gloss and skin cream
• Improves bending strength compared to HYDROGENATED POLYISOBUTENE (PB24) and LANOLINE• Even coverage and medium adhesion
• Light texture and smooth spreadability compared to HYDROGENATED POLYISOBUTENE (PB18)
Page 10
19
The formulations given in this leaflet can be freely changed, applied and commercialized. However, KOKYU ALCOHOL KOGYO CO., LTD.assumes no responsibility for any liability or damage which may arise directly or indirectly in connection with the use of such formulations. Accordingly, please exercise all due caution in respect of intellectual property rights, safety and other matters when using the formulations.
KOKYU ALCOHOL KOGYO CO., LTD. R&D Division
All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
20All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
LIPSTICK Lab code : LS-AJ1NA
Product name INCI name wt% Supplier
1. RISOCAST DA-LHYDROGENATED CASTOR OIL DIMER DILINOLEATE 29.9 KOKYU ALCOHOL KOGYO CO., LTD.
2. NPDC NEOPENTYL GLYCOL DICAPRATE 20.0 KOKYU ALCOHOL KOGYO CO., LTD.
3. KAK DADIP-R DIISOPROPYL DIMER DILINOLEATE 20.0 KOKYU ALCOHOL KOGYO CO., LTD.
4. AJK-IS3613*ISOSTEARIC ACID, DIBUTYL LAUROYL GLUTAMIDE,DIBUTYL ETHYLHEXANOYL GLUTAMIDE 10.0 KOKYU ALCOHOL KOGYO CO., LTD.
5. Refined Microcrystalline Wax MICROCRYSTALLINE WAX 10.0 NIKKO RICA CORPORATION
6. Pink pigment paste - 10.0 -
7. d-δ-TOCOPHEROL TOCOPHEROL 0.1 Tama Biochemical Co., Ltd.
Stability : Ongoing
*
Process (1) Mix 1 - 7 into a suitable container and heat up.
(2) Stir until completely melted and well dispersed, and de-aerate.
(3) Pour into lipstick molds and cool down.
*AJK-IS3613 is a mixture of ISOSTEARIC ACID EX : ISOSTEARIC ACID (KOKYU ALCOHOL KOGYO CO., LTD.) 64 %, GP-1 : DIBUTYL LAUROYL GLUTAMIDE (AJINOMOTO CO., INC.) 27 %,EB-21 : DIBUTYL ETHYLHEXANOYL GLUTAMIDE (AJINOMOTO CO., INC.) 9 %.
This lipstick with MICROCRYSTALLINE WAX and AJK-IS3613 which are used as a solidification agents gives light and smooth texture effect. AJK-IS3613 features lightening oily texture.
Page 11
21All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
LIPSTICK : LONG-LASTING TYPE
Combining pigments and coloring agents makes long-lasting lipsticks.
Adding RISOCAST DA-L, it smoothly applies and gives good adhesion.
Lab code : LS-D3NA-PL
Product name INCI name wt% Supplier
1. HAILUCENT DPIN6 DIPENTAERYTHRITYL HEXAISONONANOATE 25.0 KOKYU ALCOHOL KOGYO CO., LTD.
2. TCG-M CAPRYLIC/CAPRIC TRIGLYCERIDE 22.5 KOKYU ALCOHOL KOGYO CO., LTD.
3. RISOCAST DA-LHYDROGENATED CASTOR OIL DIMER DILINOLEATE 17.1 KOKYU ALCOHOL KOGYO CO., LTD.
4. Pink pigment paste - 10.0 -
5. HAIMALATE DIS DIISOSTEARYL MALATE 9.0 KOKYU ALCOHOL KOGYO CO., LTD.
6. RISOREX PGIS23 POLYGLYCERYL-2 TRIISOSTEARATE 4.5 KOKYU ALCOHOL KOGYO CO., LTD.
7. Refined Microcrystalline Wax MICROCRYSTALLINE WAX 4.5 NIKKO RICA CORPORATION
8. CERESIN#810 CERESIN 3.6 NIKKO RICA CORPORATION
9. POLYWAX-500 POLYETHYLENE 2.7 Baker Hughes Incorporated
10. CANDELILLA WAX Super refine EUPHORBIA CERIFERA (CANDELILLA) WAX 0.9 Watahan Trading Co., Ltd.
11. D & C Red No.27 RED 27 (CI 45410) 0.1 KISHI KASEI CO., LTD.
12. d-δ-TOCOPHEROL TOCOPHEROL 0.1 Tama Biochemical Co., Ltd.
(1) Mix 1 - 12 into a suitable container and heat up.
(2) Stir until completely melted and well dispersed, and de-aerate.
(3) Pour into lipstick molds and cool down.
Process
Stability : The stability has been confirmed at 25 ºC and 45 ºC for 3 months and by cycle test (5 ºC ↔ 25 ºC ↔ 45 ºC, 5 cycles).
Just after application Tissue off after 30 minutes
Long lastinglipstick
Normal typelipstick
22All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
This lipstick containing RISOCAST DA-L, RISOCAST ODSHS and TCG-M provides even coverage and medium adhesion.
LIPSTICK : MEDIUM TYPE Lab code : LST-12NA
Product name INCI name wt% Supplier
1. RISOCAST DA-LHYDROGENATED CASTOR OILDIMER DILINOLEATE 22.0 KOKYU ALCOHOL KOGYO CO., LTD.
2. RISOCAST ODSHS OCTYLDODECYL STEAROYL STEARATE 21.1 KOKYU ALCOHOL KOGYO CO., LTD.
3. TCG-M CAPRYLIC/CAPRIC TRIGLYCERIDE 21.1 KOKYU ALCOHOL KOGYO CO., LTD.
4. HAIMALATE DIS DIISOSTEARYL MALATE 13.1 KOKYU ALCOHOL KOGYO CO., LTD.
5. Pink pigment paste - 10.0 -
6. POLYWAX-500 POLYETHYLENE 4.8 Baker Hughes Incorporated
7. Refined Microcrystalline Wax MICROCRYSTALLINE WAX 4.2 NIKKO RICA CORPORATION
8. CANDELILLA WAX Super refine EUPHORBIA CERIFERA (CANDELILLA) WAX 3.6 Watahan Trading Co., Ltd.
9. d-δ-TOCOPHEROL TOCOPHEROL 0.1 Tama Biochemical Co., Ltd.
(1) Mix 1 - 9 into a suitable container and heat up.
(2) Stir until completely melted and well dispersed, and de-aerate.
(3) Pour into lipstick molds and cool down.
Process Stability : The stability has been confirmed at 25 ºC and 45 ºC for 3 months and by cycle test (5 ºC ↔ 25 ºC ↔ 45 ºC, 5 cycles).
Page 12
23All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
This is a light and smooth texture lip gloss with RISOCAST DA-L.
RISOCAST DA-L gives natural glossy effect and prevents from looseness.
LIP GLOSS : LIGHT TYPE Lab code : LG-DA50NA
Product name INCI name wt% Supplier
1. RISOREX PGIS22 POLYGLYCERYL-2 DIISOSTEARATE 55.0 KOKYU ALCOHOL KOGYO CO., LTD.
2. KAK PTI PENTAERYTHRITYL TETRAISOSTEARATE 19.0 KOKYU ALCOHOL KOGYO CO., LTD.
3. HAILUCENT DPIN6 DIPENTAERYTHRITYL HEXAISONONANOATE 10.7 KOKYU ALCOHOL KOGYO CO., LTD.
4. RISOCAST DA-LHYDROGENATED CASTOR OIL DIMER DILINOLEATE 10.0 KOKYU ALCOHOL KOGYO CO., LTD.
5. Rheopearl KL2 DEXTRIN PALMITATE 4.0 Chiba Flour Milling Co., Ltd.
6. Hi-Mic-1090 MICROCRYSTALLINE WAX 1.0 NIPPON SEIRO CO., LTD.
7. Pink pigment paste - 0.2 -
8. d-δ-TOCOPHEROL TOCOPHEROL 0.1 Tama Biochemical Co., Ltd.
(1) Mix 1 - 8 into a suitable container and heat up.
(2) Stir until completely melted and well dispersed, and de-aerate.
(3) Cool down.
Process Stability : The stability has been confirmed at 25 ºC and 45 ºC for 3 months and by cycle test (5 ºC ↔ 25 ºC ↔ 45 ºC, 5 cycles).
24All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
This night cream takes advantage of rich texture of RISOCAST DA-L.
It gives rich texture on the skin after applying on.
NIGHT CREAM : DA-L Lab code : SDJ-032/1
Process
Product name INCI name wt% Supplier
Oil
phas
e
1. RISOCAST DA-LHYDROGENATED CASTOR OIL DIMER DILINOLEATE 7.00 KOKYU ALCOHOL KOGYO CO., LTD.
2. TCG-M CAPRYLIC/CAPRIC TRIGLYCERIDE 5.00 KOKYU ALCOHOL KOGYO CO., LTD.
3. NPDIN NEOPENTYL GLYCOL DIISONONANOATE 5.00 KOKYU ALCOHOL KOGYO CO., LTD.
4. CETOSTEARYL ALCOHOL CETEARYL ALCOHOL 3.90 KOKYU ALCOHOL KOGYO CO., LTD.
Wat
er p
hase
5. HAISUGARCANE BG BUTYLENE GLYCOL 3.00 KOKYU ALCOHOL KOGYO CO., LTD.
6. DIOL PD PENTYLENE GLYCOL 3.00 KOKYU ALCOHOL KOGYO CO., LTD.
7. TEGO CARE CG 90 CETEARYL GLUCOSIDE 1.00 Evonik Industries AG
8. ARISTOFLEX AVCAMMONIUM ACRYLOYLDIMETHYLTAURATE/VP COPOLYMER 0.05 Clariant International Ltd.
9. SATIAXANE CX911 XANTHAN GUM 0.05 LASERSON SA
10. Purified water WATER 72.00 -
Stability : The stability has been confirmed at 25 ºC and 45 ºC for 3 months and by cycle test (5 ºC ↔ 25 ºC ↔ 45 ºC, 5 cycles).
pH : 6.5
(1) Mix 5, 6, 8 and 9 in a suitable container at RT.
(2) Add 7 - 10 and heat up to 75 ºC to obtain semi-transparent liquid without stirring.
(3) Mix 1 - 4 and heat up to 75 ºC.
(4) Heat up (2) to 75 ºC and pour (1) into (2) (1000 rpm, 8 min).
(5) Heat up (3) to 75 ºC and pour into (4) (1500 rpm, 5 min).
(6) Homogenize at 1500 rpm and cool down to RT.
Page 13
25All other company or product names are trademarks or registered trademarks of their respective companies or organizations.
This oil balm takes advantage of rich texture of RISOCAST DA-L.
It gives no unpleasant stickiness and smoothly melts on the skin.
FACE OIL BALM Lab code : FOB-3YK
(1) Mix 1 - 5 into a suitable container.
(2) Heat up to 90 ºC and stir until completely melted.
(3) Cool down to RT.
Process
Product name INCI name wt% Supplier
1. TCG-M CAPRYLIC/CAPRIC TRIGLYCERIDE 40.0 KOKYU ALCOHOL KOGYO CO., LTD.
2. NEOLIGHT 180P ISOSTEARYL NEOPENTANOATE 25.0 KOKYU ALCOHOL KOGYO CO., LTD.
3. KAK TTO TRIMETHYLOLPROPANE TRIETHYLHEXANOATE 25.0 KOKYU ALCOHOL KOGYO CO., LTD.
4. RISOCAST DA-L HYDROGENATED CASTOR OIL DIMER DILINOLEATE 5.0 KOKYU ALCOHOL KOGYO CO., LTD.
5. POLYWAX-500 POLYETHYLENE 5.0 Baker Hughes Incorporated
Stability : The stability has been confirmed at 25 ºC and 45 ºC for 3 months and by cycle test (5 ºC ↔ 25 ºC ↔ 45 ºC, 5 cycles).