Perhitungan Penetapan Kadar Abu Simplisiarepository.wima.ac.id/647/7/LAMPIRAN.pdfPerhitungan Penetapan Kadar Abu Simplisia Berat krus kosong: 1. 18,8572 gram 2. 18,8897 gram 3. 19,1592

76

Lampiran 1

Perhitungan Penetapan Susut Pengeringan Simplisia

Hasil Susut PengeringanReplikasi Hasil susut Pengeringan

1 2,20%2 2,40%3 2,00%

Rata-rata 20,23

00,240,220,2

%

Perhitungan Penetapan Kadar Abu Simplisia

Berat krus kosong: 1. 18,8572 gram

2. 18,8897 gram

3. 19,1592 gram

Rata-rata 9687,183

1592,198897,188572,18

gram

Berat krus kosong + abu: 1. 18,9093 gram

2. 18,9422 gram

3. 19,2123 gram

Rata-rata =3

2123,199422,189093,18 = 19,0212 gram

Berat simplisia : 1. 2,0028 gram

2. 2,0032 gram

3. 2,0051 gram

77

Rata-rata =3

0051,20032,20028,2 = 2,0037 gram

Kadar abu

%100SerbukBerat

kosong)krusberatrata-(Rata-abu)kosongkrusBeratrata-(Rata

= %1000037,2

9687,180212,19

= 2,62 %

78

Lampiran 2

Hasil Pengamatan dan Perhitungan Kromatografi Lapis Tipis

Rf =

Pengamatan secara visibel :

Jarak yang ditempuh oleh fase gerak = 8 cm

Rf Beta-karoten (pembanding)

Jarak noda = 6,3 cm Harga Rf = 6,3 / 8 = 0,78

Warna noda = kuning

Rf Jus Umbi Wortel

Jarak noda = 6,3 cm Harga Rf = 6,3 / 8 = 0,78

Warna noda = kuning

Pengamatan secara visible ( flavonoid ) :

*) Pengamatan pada sinar UV 254

*) Jus umbi wortel *) Jus umbi wortelHarga Rf = 0,52 Harga Rf = 0,52

*) umbi wortel (dalam n-hexane) *) Umbi wortel (dalam n-hexane)Harga Rf = 0,52 Harga Rf = 0,52

*) Pembanding rutin *) Pembanding rutinHarga Rf = 0,52 Harga Rf = 0,52

Pengamatan pada sinar UV 366 :

*) Jus umbi wortelHarga Rf = 0,52

*) umbi wortel (dalam n-hexane)Harga Rf = 0,52

*) Pembanding rutinHarga Rf = 0,52

Jarak yang ditempuh oleh zat (cm)

Jarak yang ditempuh oleh fase gerak (cm)

79

Lampiran 3

Perhitungan Anava Rambang Lugas hari ke-0 untuk Pengukuran Kadar Kolesterol

Total Tikus Putih Jantan

Kadar kolesterol total hari ke-0K1 K2 K3 K4 K5 K6 Jumlah

1 70 69 67 63 70 702 64 73 69 78 67 673 63 71 60 65 63 684 73 68 68 60 69 735 66 60 73 74 69 64X 67,2 68,2 67,4 68 67,6 68,4 406,8n 5 5 5 5 5 5 30Ji 336 341 337 340 338 342 2034J²i 112896 116281 113569 115600 114244 116964 689554Y²ij 22650 23355 22803 23354 22880 23438 138480

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5

db (Ey) = db total – db (Py) = 29 – 5 = 24

Jk total = N

JiiJY

2

2 )(= 574,8

Jk (Py) = N

Ji

niJ

22 )(= 5,3

Jk (Ey) = Jk total – Jk (Py) = 574,8 – 5,3 = 569,5

RJK (Py) =)()(

PydbPyJk

= 06,153,5

80

RJK (Ey) =)()(

EydbEyJk

= 729,2324

5,569

Fhitung =)()(

EyRJKPyRJK

= 04467,0729,2306,1

Tabel Anava

SV JK db RJK Fhitung

Perlakuan (Py) 5,3 5 1,06 0,04467

Dalam (Ey) 569,5 24 23,729

Total 574,8 29

Ftabel (p=0,05) = [db antar (5); db dalam (29)] → Ftabel (p=0,05) = 2,54


Jadi Fhitung < Ftabel (p=0,05)

Kesimpulan : Tidak ada perbedaan bermakna antara kelompok kontrol dan kelompok

perlakuan.

81

Lampiran 4

Perhitungan Anava Rambang Lugas Hari ke-8 untuk Pengukuran Kadar kolesterol



1 73 80 82 85 76 812 64 87 82 84 71 693 60 97 79 91 86 724 75 82 75 79 80 735 65 90 89 74 83 66X 67,4 87,2 81,4 82,6 79,2 72,2 470n 5 5 5 5 5 5 30Ji 337 436 407 413 396 361 2350J²i 113569 190096 165649 170569 156816 130321 927020Y²ij 22875 38202 33235 34279 31502 26191 216284

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5

db (Ey) = db total – db (Py) = 24529

Jk total = NJi

iJY2

2 )(= 32200,6667

Jk (Py) = N

Ji

niJ

22 )(= 1320,6667

Jk (Ey) = Jk total – Jk (Py) = 308806667,13206667,32200

RJK (Py) =)()(

PydbPyJk

= 13334,26456667,1320

82

RJK (Ey) =)()(

EydbEyJk

= 6667,128624

30880

Fhitung =)()(

EyRJKPyRJK

= 20528,06667,1286

13334,264

Tabel Anava


Perlakuan (Py) 1320,6667 5 264,13334 0,20528

Dalam (Ey) 30880 24 1286,6667

Total 32200,6667 29



Jadi Fhitung < Ftabel (p=0,05 dan p=0,01)


perlakuan.

83

Lampiran 5

Perhitungan Anava Rambang Lugas Hari ke-15 untuk Pengukuran Kadar Kolesterol



1 87 86 96 92 78 772 92 89 90 94 94 893 84 90 85 96 89 844 77 92 88 89 93 805 88 100 90 80 89 87X 85,6 91,4 89,8 90,2 88,6 83,4 529n 5 5 5 5 5 5 30Ji 428 457 449 451 443 417 2645J²i 183184 208849 201601 203401 196249 173889 6996025Y²ij 36762 41881 40385 40837 39411 34875 234151

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = NJi

iJY2

2 )(=950,1667

Jk (Py) = N

Ji

niJ

22 )(=233,7667

Jk (Ey) = Jk total – Jk (Py) = 4,7167667,2331667,950

RJK (Py) =)()(

PydbPyJk

= 7534,4657667,233

84

RJK (Ey) =)()(

EydbEyJk

= 85,2924

4,716

Fhitung =)()(

EyRJKPyRJK

= 56627,185,29

7534,46

Tabel Anava


Perlakuan (Py) 233,7667 5 46,75334 1,56627

Dalam (Ey) 716,4 24 29,85

Total 950,1667 29



Jadi Fhitung < Ftabel (p=0,05 dan p=0,01)


perlakuan.

85

Lampiran 6




1 80 94 90 94 66 552 60 93 91 80 83 513 63 89 85 93 69 594 74 108 80 88 85 725 60 104 95 89 69 51X 67,4 97,6 88,2 88,8 74,4 57,6 474n 5 5 5 5 5 5 30Ji 337 488 441 444 372 288 2370J²i 113569 238144 194481 197136 138384 82944 964658Y²ij 23045 47886 39031 39550 27992 16892 194396

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = N

JiiJY

2

2 )(=7166

Jk (Py) = N

Ji

niJ

22 )(=5701,6

Jk (Ey) = Jk total – Jk (Py) = 4,14646,57017166

RJK (Py) =)()(

PydbPyJk = 32,1140

56,5701

86

RJK (Ey) =)()(

EydbEyJk

= 0166,6124

4,1464

Fhitung =)()(

EyRJKPyRJK

= 6886,180166,61

32,1140

Tabel Anava


Perlakuan (Py) 5701,6 5 1140,32 18,6886

Dalam (Ey) 1464,4 24 61,0166

Total 7166 29



Jadi Fhitung > Ftabel (p=0,05 dan p=0,01)

Kesimpulan : ada perbedaan bermakna antara kelompok kontrol dan kelompok

perlakuan.

87

Lampiran 7

Tabel Uji HSD

Perlakuan MeanK1 K2 K3 K4 K5 K6

67,4 97,6 88,2 88,8 74,4 57,6K1 67,4 0 - - - - 9,8K2 97,6 0 9,4 8,8 23,2 40K3 88,2 0 13,8 30,6K4 88,8 0 14,4 31,2K5 74,4 0 16,8K6 57,6 0

Perhitungan Statistik HSD

HSD =21

)(2nnERJK

q y

k = 6, Db = 24, q = 4,37, RJK (Ey) = 61,0166 → HSD (5%) =

55

)(237,4

EyRJK15,2652

k = 6, Db = 24, q = 5,37, RJK (Ey) = 61,0166 → HSD (1%) =

55

)(237,5

EyRJK18,7583

88

Derajat Kebermaknaan

Perlakuan Mean HSD 1 % HSD 5% KesimpulanK1 vs K6 9,8 18,758 15,265 TBK2 vs K3 9,4 18,758 15,265 TBK2 vs K4 8,8 18,758 15,265 TBK2 vs K5 23,2 18,758 15,265 SBK2 vs K6 40 18,758 15,265 SBK3 vs K5 3,8 18,758 15,265 TBK3 vs K6 30,6 18,758 15,265 SBK4 vs K5 4,4 18,758 15,265 TBK4 vs K6 31,2 18,758 15,265 SBK5 vs K6 16,8 18,758 15,265 B

Keterangan:K1 : diberi air suling secara oral sebanyak 1 ml/100gBBK2 : diberi larutan propiltiourasil 0,01% dalam aquades sebanyak 1 ml/100gBB

secara oralK3 : diberi larutan propiltiourasil 0,01% dalam aquades dan jus umbi wortel

dengan konsentrasi 80% v/v masing-masing sebanyak 1 ml/100gBB secaraoral

K4 : diberi larutan propiltiourasil 0,01% dalam aquades dan jus umbi worteldengan konsentrasi 90% v/v masing-masing sebanyak 1 ml/100gBB secaraoral

K5 : diberi larutan propiltiourasil 0,01% dalam aquades dan jus umbi worteldengan konsentrasi 100 % v/v masing-masing sebanyak 1 ml/100gBB secaraoral

K6 : diberi larutan propiltiourasil 0,01% dalam aquades dan Gemfibrozil dengandosis 81 mg/kgBB masing-masing sebanyak 1 ml/100gBB secara oral

B : Bermakna, artinya perbedaan bermakna karena selisih dua mean > HSD 5%SB : Sangat Bermakna, artinya perbedaan sangat bermakna karena selisih dua

mean > HSD 1%TB : Tidak Bermakna, artinya perbedaan tidak bermakna karena selisih dua mean

< HSD 5%Vs : Versus

89

Lampiran 8




1 72 90 87 93 58 692 66 106 92 73 66 583 65 103 87 92 74 644 70 105 85 79 86 615 62 105 89 89 69 54X 67 101,8 88 85,2 70,6 61,2n 5 5 5 5 5 5 30Ji 335 509 440 426 353 306 2369J²i 112225 259081 193600 181476 124609 93636 964627Y²ij 22509 51995 38748 36604 25353 18858 194067

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = NJi

iJY2

2 )(=6994,9667

Jk (Py) = NJi

niJ

22 )(=5853,3667

Jk (Ey) = Jk total – Jk (Py) = 6,11413667,58539667,6994

RJK (Py) =)()(

PydbPyJk

= 67334,117053667,5853

90

RJK (Ey) =)()(

EydbEyJk

= 56667,4724

6,1141

Fhitung =)()(

EyRJKPyRJK

= 6112,2456667,4767334,1170

Tabel Anava

SV JK Db RJK Fhitung

Perlakuan (Py) 5853,3667 5 1170,67334 24,6112

Dalam (Ey) 1141,6 24 47,56667

Total 6994,9667 29



Jadi Fhitung > Ftabel (p=0,05 dan p=0,01)

Kesimpulan : ada perbedaan bermakna antara kelompok kontrol dan kelompok

perlakuan.

91

Lampiran 9

Tabel Uji HSD


67 101,8 88 85,2 70,6 61,2K1 67 0 - - - - 5,8K2 101,8 0 13,8 16,6 31,2 40,6K3 88 0 2,8 17,4 26,8K4 85,2 0 14,6 24K5 70,6 0 9,4K6 61,2 0


HSD =21

)(2nnERJK

q y

k = 5, Db = 24, q = 4,37, RJK (Ey) = 47,56667 → HSD (5%) =

478,1355

)(237,4

EyRJK

k = 5, Db = 24, q = 5,29, RJK (Ey) = 47,56667 → HSD (1%) =

563,1655

)(237,5

EyRJK

92


Perlakuan Mean HSD 1 % HSD 5% KesimpulanK1 vs K6 5,8 16,563 13,478 TBK2 vs K3 13,8 16,563 13,478 BK2 vs K4 16,6 16,563 13,478 SBK2 vs K5 31,2 16,563 13,478 SBK2 vs K6 40,6 16,563 13,478 SBK3 vs K4 2,8 16,563 13,478 TBK3 vs K5 17,4 16,563 13,478 SBK3 vs K6 26,8 16,563 13,478 SBK4 vs K5 14,6 16,563 13,478 BK4 vs K6 24 16,563 13,478 SBK5 vs K6 9,4 16,563 13,478 TB

Keterangan:

K1 : diberi air suling secara oral sebanyak 1 ml/100gBBK2 : diberi larutan propiltiourasil 0,01% dalam aquades sebanyak 1 ml/100gBB








< HSD 5%Vs : Versus

93

Lampiran 10

Perhitungan Koefisien Korelasi

X Y XY 2X 2Y

80 13,55 1084 6400 183,6025

90 16,30 1467 8100 265,69

100 30,65 3065 10000 939,4225

X 270 Y 60,5 XY 5616 2X 24500 2Y 1388,715

X = 90 Y = 20,1666

n = 3

2222

YYnXXn

YXXYnr

93113,05,60715,13883270245003

5,602705616322

r

r hitung = 0,93113 , r tabel (p=5%) = 0,997 maka r hitung < r tabel

Kesimpulan: Tidak ada hubungan korelasi yang bermakna antara peningkatan

konsentrasi dengan penurunan kadar kolesterol total.

Keterangan:r : Koefisien KorelasiX : Konsentrasi jus umbi wortel (Daucus carota, L.)Y : Persen penurunan kadar kolesterol total hari ke-29n : Jumlah perlakuan

94

Lampiran 11

Perhitungan Anava Rambang Lugas hari ke-0 untuk Pengukuran Kadar Trigliserid

Tikus Putih Jantan


1 56 62 58 61 60 582 58 61 62 58 55 563 65 58 60 59 62 534 54 60 57 64 59 625 59 56 54 56 54 60X 58,4 59,4 58,2 59,6 58 57,8n 5 5 5 5 5 5 30Ji 292 297 291 298 290 289 1757J²i 85264 88209 84681 88804 84100 83521 514579Y²ij 17122 17665 16973 17798 16866 16753 103177

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = N

JiiJY

2

2 )(= 275,3667

Jk (Py) = N

Ji

niJ

22 )(= 14,1667

Jk (Ey) = Jk total – Jk (Py) = 275,3667-14,1667 = 261,2

RJK (Py) =)()(

PydbPyJk

= 8334,251667,14

95

RJK (Ey) =)()(

EydbEyJk

= 8833,1024

2,261

Fhitung =)()(

EyRJKPyRJK

= 2603,08833,108334,2

Tabel Anava


Perlakuan (Py) 14,1667 5 2,8334 0,2603

Dalam (Ey) 261,2 24 10,883

Total 275,3667 29





perlakuan.

96

Lampiran 12


Tikus Putih Jantan


1 62 66 60 65 64 572 62 60 55 58 65 533 59 58 61 70 58 624 54 59 60 52 54 655 57 56 62 54 60 59X 58,8 59,8 59,6 59,8 60,2 59,2n 5 5 5 5 5 5 30Ji 294 299 298 299 301 296 1787J²i 86436 89401 88804 89401 90601 87616 532259Y²ij 17334 17937 17790 18109 18201 17608 106979

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = N

JiiJY

2

2 )(= 533,3667

Jk (Py) = N

Ji

niJ

22 )(= 6,1667


RJK (Py) =)()(

PydbPyJk

= 23334,15

1667,6

97

RJK (Ey) =)()(

EydbEyJk

= 96667,2124

2,527

Fhitung =)()(

EyRJKPyRJK

= 05614,096667,2123334,1

Tabel Anava


Perlakuan (Py) 6,1667 5 1,23334 0,05614

Dalam (Ey) 527,2 24 21,96667

Total 533,3667 29





perlakuan.

98

Lampiran 13


Tikus Putih Jantan


1 60 65 64 61 65 582 62 67 67 58 57 623 61 58 62 54 58 654 58 62 58 62 63 555 57 65 59 67 62 67X 59,6 63,4 62 60,4 61 61,4n 5 5 5 5 5 5 30Ji 298 317 310 302 305 307 1839J²i 88804 100489 96100 91204 93025 94249 563871Y²ij 17778 20147 19274 18334 18651 18947 113131

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = N

JiiJY

2

2 )(= 400,3

Jk (Py) = NJi

niJ

22 )(= 43,5


RJK (Py) =)()(

PydbPyJk = 7,8

55,43

99

RJK (Ey) =)()(

EydbEyJk

= 8666,1424

8,356

Fhitung =)()(

EyRJKPyRJK

= 5852,08666,14

7,8

Tabel Anava


Perlakuan (Py) 43,5 5 8,7 0,5852

Dalam (Ey) 356,8 24 14,8666

Total 400,3 29





perlakuan.

100

Lampiran 14


Tikus Putih Jantan


1 56 60 60 63 60 622 57 65 62 58 58 573 58 64 62 59 53 544 61 69 65 64 57 525 60 68 64 68 62 58X 58,4 65,2 62,6 62,4 58 56,6n 5 5 5 5 5 5 30Ji 292 326 313 312 290 283 1816J²i 85264 106276 97969 97344 84100 80089 551042Y²ij 17070 21306 19609 19534 16866 16077 110462

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = N

JiiJY

2

2 )(= 533,4667

Jk (Py) = N

Ji

niJ

22 )(= 279,8667

Jk (Ey) = Jk total – Jk (Py) = 533,4667-279,8667=253,6

RJK (Py) =)()(

PydbPyJk

= 97334,5558667,279

101

RJK (Ey) =)()(

EydbEyJk

= 5667,1024

6,253

Fhitung =)()(

EyRJKPyRJK

= 2914,55667,1097334,55

Tabel Anava


Perlakuan (Py) 279,8667 5 55,97334 5,2914

Dalam (Ey) 253,6 24 10,5667

Total 533,4667 29




Kesimpulan : Ada perbedaan bermakna antara kelompok kontrol dan kelompok

perlakuan.

102

Lampiran 15

Tabel Uji HSD


58,4 65,2 62,6 62,4 58 56.6K1 58,4 0 - - - 0,4 1,8K2 65,2 0 2,6 2,8 7,2 8,6K3 62,6 0 0,4 4,6 6K4 62,4 0 4,4 5,8K5 58 0 1,4K6 56,6 0


HSD =21

)(2nnERJK

q y

k = 5, Db = 24, q = 4,37, RJK (Ey) = 10,5667 → HSD (5%) =

3528,655

)(237,4

EyRJK

k = 5, Db = 20, q = 5,37, RJK (Ey) = 10,5667 → HSD (1%) =

8065,755

)(237,5

EyRJK

103


Perlakuan Mean HSD 1 % HSD 5% KesimpulanK1 vs K5 0,4 7,8065 6,3528 TBK1 vs K6 1,8 7,8065 6,3528 TBK2 vs K3 2,6 7,8065 6,3528 TBK2 vs K4 2,8 7,8065 6,3528 TBK2 vs K5 7,2 7,8065 6,3528 BK2 vs K6 8,6 7,8065 6,3528 SBK3 vs K4 0,4 7,8065 6,3528 TBK3 vs K5 4,6 7,8065 6,3528 TBK3 vs K6 6 7,8065 6,3528 TBK4 vs K5 4,4 7,8065 6,3528 TBK4 vs K6 5,8 7,8065 6,3528 TBK5 vs K6 1,4 7,8065 6,3528 TB

Keterangan:









< HSD 5%Vs : Versus

104

Lampiran 16


Tikus Putih Jantan


1 54 61 59 58 58 602 56 64 63 59 53 573 59 67 61 63 57 584 61 68 66 65 57 545 68 69 65 70 60 51X 57,6 65,8 62,8 63 57 56n 5 5 5 5 5 5 30Ji 288 329 314 315 285 280 1811J²i 82944 108241 98596 99225 81225 78400 548631Y²ij 16618 21691 19752 19939 16271 15730 110001

db (total) = N – 1 = 30 – 1 = 29

db (Py) = P – 1 = 6 – 1 = 5


Jk total = N

JiiJY

2

2 )(=676,9667

Jk (Py) = N

Ji

niJ

22 )(= 402,1667


RJK (Py) =)()(

PydbPyJk

= 43334,8051667,402

105

RJK (Ey) =)()(

EydbEyJk

= 45,1124

8,274

Fhitung =)()(

EyRJKPyRJK

= 0247,745,11

43334,80

Tabel Anava


Perlakuan (Py) 402,1667 5 80,43334 7,0247

Dalam (Ey) 274,8 24 11,45

Total 676,9667 29




Kesimpulan : Ada perbedaan bermakna antara kelompok kontrol dan kelompok

perlakuan.

106

Lampiran 17

Tabel Uji HSD


57,6 65,8 62,8 63 57 56K1 57,6 0 - - - 0,6 1,6K2 65,8 0 3 2,8 8,8 9,8K3 62,8 0 - 5,8 6,8K4 63 0 6 7K5 57 0 1K6 56 0


HSD =21

)(2nnERJK

q y

k = 5, Db = 24, q = 4,37, RJK (Ey) = 11,45 → HSD (5%) =

6131,655

)(237,4

EyRJK

k = 5, Db = 24, q = 5,37, RJK (Ey) = 11,45 → HSD (1%) =

1264,855

)(237,5

EyRJK

107


Perlakuan Mean HSD 1 % HSD 5% KesimpulanK1 vs K5 0,6 8,1264 6,6131 TBK1 vs K6 1,6 8,1264 6,6131 TBK2 vs K3 3 8,1264 6,6131 TBK2 vs K4 2,8 8,1264 6,6131 TBK2 vs K5 8,8 8,1264 6,6131 SBK2 vs K6 9,8 8,1264 6,6131 SBK3 vs K5 5,8 8,1264 6,6131 TBK3 vs K6 6,8 8,1264 6,6131 BK4 vs K5 6 8,1264 6,6131 TBK4 vs K6 7 8,1264 6,6131 BK5 vs K6 1 8,1264 6,6131 TB

Keterangan:









< HSD 5%Vs : Versus

108

Lampiran 18

Perhitungan Koefisien Korelasi

X Y XY 2X 2Y

80 4,559 364,72 6400 20,7845

90 4,2553 382,977 8100 18,1076

100 14,8936 1489,36 10000 221,8193

X 270 Y 23,7079 XY 2237,057 2X 24500 2Y 260,7114

X = 90 Y = 7,9026

n = 3

2222

YYnXXn

YXXYnr

8533,07079,237114,2603270245003

7079,23270057,2237322

r

r hitung = 0,8533 , r tabel (p=5%) = 0,997 maka r hitung < r tabel

Kesimpulan: Tidak ada hubungan korelasi yang bermakna antara peningkatan

konsentrasi dengan penurunan kadar kolesterol total.

Keterangan:r : Koefisien KorelasiX : Konsentrasi jus umbi wortel (Daucus carota, L.)Y : Persen penurunan kadar kolesterol total hari ke-29n : Jumlah perlakuan

109

Lampiran 19

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.j5u5015

SUZHOU HENGYI PHARMACEUTIGAL C;;>., LTD.

54 KUNTAI RQAD XINZHEN KUNSHAN JIANGSU CHINA

CERT1FICATE. OF ANALYSIS

PRODUCT PROPYLTHIOURACil PDWDI!''' _\.-,

BATCH /010 C8127l" STANOARD:~;;OOO ) r I "M"'<'!'lG ;>5" ;'-~-RC"C'r-'--------+I-M-~G. u"TE Oe:Cu:20oe I

I QUANTITY 21!KGS !8IP DAlE UEC 22. 200~ i TESTS I SPECIFICATIONS RE~ULTS I

P.05

~ -. -+~~;;;o;;'"~""~~"","';;'~;;;;'n~';;;1tYS"T"'U - --i

l CI-lAIV-CTERl.SncS ().I! ~~YSl o.u l ,* PO.~ I QU,o,UF.i:t -----1/~Ec',m""GiTr-eoeo~~co~ec-~-----.--__i ,

I 1'7·:Ul"C I 21Y 5·22tl,5l:" ,/ POINT

CONFORMED

I i1ElAreO +--.

\ GUSSTNlC;o i

r.OtlFOR..,EO -

CONfor,MED

'-.- -'_.,-'-"-" -~ <!l_ 0~~ ---i

0.011% ,L'OU:-'C'C"C'C,OeDOCA=' C"._-tI ___ -::c'<1t,o. I'"

LA;:"""A;'''';;;;;;-__ I ___ -'·='_''='':·~ .. ''c_·c==cc===:'':'·.:::,. ~ rCONCLUSION CONFORMWITH8~OO\l =- I

REMARK'

mv N~.: 1100704 ., uc NUMBER: MI77\061..':'4a2~ 1. 'CDAn:;;06122U .

f)~TE: 2001.'1/10

• 1vtAt'UI'AC, CRIl' u \)",r" ",UT OVER TI;lr\\-i,Ql(..AIA!"P/;i~~~~1f: t'ROM lVl . nATE. 11M" rn.Jdrli!>CJ l§,,~ fHrt 4 IIJ

•. _ ~9HOU mllG~ ~lJJIjcrulw CO. lTD )l.IA?,UFACi'URER: ~'CZIIOL: HENDY! '"l t..J- -:'

PIIAR.\IACF.FT1('.ALCQ .. LTD. ~y

J

110

Lampiran 20

LEMBAGA ILMU PENGETAHUAN INDONESIA (Indonesian Institue of Sciences)

UPT BALAI KONSERVASI TUMBUHAN KEBUN RAYA PURWODADI (punvodadi Botanic Garden)

JI. Raya Surabaya - Malang Km. 65, Purwodadi - Pasuruan 67163 Telepon : 0341 - 426046 Fu. : 0341 - 426046

e-mail: [email protected]

SURAT KETERANGAN IDENTIFIKASI No. /0.J8IIPU.UPT.031HM12006

Kepala Kebun Raya Purwodadi dengan ini menerangkan bahwa material tanaman

yang dibawa oleh :

FREDY. NRP:2443003039

Mahasiswa Fakultas Fannasi Universitas Katolik Widya Mandala Surabaya, datang di

UPT Balai Konservasi Tumbuhan Kebun Raya Purwodadi pada tanggal 13 Nopember

2006 berdasarkan buku Flora oC Java, karangan C.A. Backer, Vol II (1965) hal 178.

nama ilmiahnya adaJah :

Marga

Jenis

: Daucus

:Daucus carola L.

Adapun menurut buku The Standard Cyclopedia oCUorticultare karangan L.U. Bailey

jilid I ( 1953) halaman 2-4, klasifikasinya adalab sebagai berikut :

Divisio : Spennatophyta

Sub Divisio

Kelas

Ordo / Bangsa

Family / Suku

: Angiospennae

: Dicotyledoneae

: Umbelliflorae

: Umbelliferae (Apiae.ae)

Demikian surat keterangan ini dibuat untuk dapat dipergunakan sebagaimana

mestinya.

Purwodadi, 13 Nopember 2006

111

Lampiran 21

Tabel Uji F

112

Lanjutan

.-Derajit1!tlUn ·untiif ratw'kllldnt 1.,. JebIh bem,

I 2 3 4 5 6 7 • • 10 II 12 14 16 20 24 30 40 JO 15 'ICO 2CO JOG • 32 US 1.30 2.90 2,67 2," ),40 2.32 US 2.1. 2.14 2.10 2.07 2.02 1.'7 1.91 1.16 1.12 1.76 1.74 1.69 1,67 1,64 1.61 1.5' 1.JO 5.34 4.46 3.91 3.66 3.42 3.2S 3.12 3.01 2.94 2.16 Ul 2.10 2.62 2.51 2.42 2.34 2.25 2.20 2.12 2.01 2.02 I." 1,'6 34 U3 3." 2.' 2,65 2.49 2.38 2.30 2.23 2.17 2.12 2.01 US 2.03 I.ts 1.19 1.14 I." 1.14 1.11 1.67 I." 1.61 1.59 1.57

7." 5,29 4.42 3.93 3.61 3.38 3.21 3.01 tt1 2.19 2.12 2.16 2.66 UI 2,41 2.31 2.lO 2.21 2.15 2.01 2,04 1," 1.t4 l.tI 36 4.11 3.26 1.16 2.63 2.48 2.36 2.21 2.21 2.IS 2,10 2,06 2.03 1.19 1.93 1.11 1.12 1.11 1.72 1.69 1.65 1.62 1.59 1.56 I.5S 1.39 5.2S 01 3.19 3.51 3.3S 3.11 3.04 2.94 2.16 2.1' 2.72 2.62 2.54 2.4 2.35 2.26 2.17 tI2 2.04 2.CO 1.94 1.90 1.17

~ 31 4.10 US US 2.62 2046 2.3S 2,26 2.19 2.14 2.09 2.OS 2.02 1.96 1.92 1.85 I." 1.76 1.71 1.61 1.63 UO 1.57 1.54 1.53 II .II 1.35 5.21 4034 1.16 U4 1.32 3.15 3.02 2.91 2.12 2.15 2., 2.S9 2.51 2.40 2.32 2.22 2.14 2.01 tco 1.97 1.90 1.16 1.14

= 1.7~ I.' ~40 4001 3.23 2.14 2.61 2.45 2.34 2.2S UI 1:12 2.07 2.04 2.CO 1.95 1.90 1.14 1.79 1,16 1.61 I.Sf US r.53 1.51 ' .. 7.31 5.11 01 3.13 3,51 3.29 3.12 2.99 2.. U 2.73 2.66 2.56 2.49 2.37 2.29, 2.2d 1M US 1,91 1.'4 1,' 1.14 1.11 ' L2

. >. 4.07 3.22 2.13 2.st 2.44 2.32 2,24 2.17 2.11 2.06 2.02 1.90 1.94 1.19 1.12 1.11 1.73 I. .. 1.64 1.110 1.57 1.54 1.$1 1.49 ' i 7.27 5.15 4.29 1.., 1.4' 3.26 2.10 2.96 2.~ tn 2.10 2.64 2,54 2.46 US 2.26 2.17 ::.01 2.02 M4 l.tI I,., I,., I,~ 1« U6 3.21 2.12 1.51 2.43 2.31 2.23 U6 2.10 2,OS 2.01 I." 1.92 I.. I,ll 1.76 1.72 1.66 :.'" 1.51 I." !.S2 I.JO 1.41 ' :s 7.24 5.12 4,26 3.11 3.46 3.24 3.01 2.94 2.14 2." 2." 2.62 1.52 2.44 2.32 2.24 2.15 2.06 1.09 1.92 1" 1.12 1.11 1,75 .II c J 46 US 3.20 2.11 2.S1 UZ 2.30 2.22 2.14 2.09 2.04 2.03 1.91 l.tI 1.11 1.10 I.1S 1.71 1.65 1.t2 1.57 1.54 UI 1,.1 1.46 ' e 7.21 5.10 124 3.76 3.« 3.22 US 2.92 2.12 2.73 2.66 2.411 2.50 2.42 2.30 2.22 2.13 2.04 I." 1.90 1.16 I," 1.76 I.n ·

141 4.04 3. It 2." 2.56 2.41 2.30 2.21 2.14 2.01 2.03 1.t9 I." 1.90 1.16 1.19 1.74 I.~ 1.64 1.61 1.56 1.53 UO 1.41 1.45 1

t 7.1t 5;0, 4,22 1.7~ 3.42 UI 1.04 2.90 2." 2.71 2.64 2.SI 2.41 2.41') 2.1 :,20 2..11. 2.0. l.96 I.' 1.14 I," 1.73 110 ! :I , ,

' 1 .JO 4.03 3.11 2.19 2." 2.40 2.29 2.20 2.13 2.07 2.02 I." I.ts 1.90 I.IS 1.71 1 ~7~ 1.69 I,'" I." I.s! 1.52 1,41 1.46 1,44 I • 7.11 5.06 4.20 1.72 3.41 3.11 to2 2.. 2.71 2.10 2.62 2." 2.46 2.~ 2.26 2.11 2.10 2.00 1,'4 I." 1.12 1,76 1.71 I." , iss 4.02 3.17 2.71 2." "'1 2.27 . 2.11 2.11 US 2.00 1.91 I.ts I .• 1.13 1.76 1.72 1.67 1,'11'," 1.52 1,50 1.46 I.G 1.41. .II 7.12 5.01 W t .. 3.37 W 2." US t15 2.66 2.59 2.53 2.43 2.35 2.23 2. IS 2.06 I," I.to 1.12 I,,. 1.71 1,66 1.64 , .. i" to) 3. IS 2.76 2,52 U7 2.2S 2,17 2.10 2.04 I." l.ts 1.92 1.16 1.11 1.75 1.70 1.65 U9 L56 I ,so I,'" 1,44 1.41 1,29

! 7.01 4." 4.13 U 3.34 tl2 US 2.12 2.72 2.63 2." 2.JO 2,40 2.32 UJ 2.12 2.03 1.93 1,17 I," 1,74 1," 1,63 1.613

AS t" 3.14 2.75 UI 2.36 2.24 2,15 2.01 2.02 I ~" 1.94 I.to I.'" I." 1.73- 1.61 1.63 I,,, 1.54 1,4' 1.46 1,42 1.29 I.n 7,04 US 4.10 3.62 3.31 3.09 2.93 2.19 2.10 2.61 2.54 2.41 2.37 2.30 2.11 2.09 2,CO 1,90 1.54 1,76 1,71 1,64 I," I,"

70 l," til 2.74 2.50 2.3$ 2.32 2.14 2.07 2.01 I. 91 1.93 1.19 1.14 1.19 1.72 1.61 1.62 1.S6 I.Sl 1,47 1.45 1,40 1.37 1,35 7.01 4.92 UI l," 3.2f 3.01 2/1 2.77 ~.67 2.!' 2.51 2.45 US 2.21 2.15 2.07 I,,. I." 1.12 1.74 1.69 1.62 1,56 I," ,

Ik : ,f 6 I,ll 2.12 1.41 U2 UI t.1~ 11'~IL~II .f~ 1:'.91 I.. 1.11 I," I,,. \,., 1,.0 1,14 t,tt I,d t,41 t,1I I." I,ll , ... til U4 3.56 US 3.04 2.11 2.74 2.64 US 2 .... 2.41 U2 2.24 2.11 2.03 1.94 1.14 1.7, 1.70 1.65 I,n I.S 2 1.41

Sumber: Schefler (1987).

113

Lampiran 22

Tabel Uji HSD (0,05)

I J 4 S 6 7 8 9 10 11

5 U .. ".60 5.12 5.67 6.03 6.33 6.58 6.S0 6,99 7.17 6 U6 ".M ".90 5.30 5.63 5090 6.12 6.32 6,49 6.65 7 5.34 4.16 4.68 5.06 5.36 5.61 5.82 6.00 6.16 6.30 8 U6 4.01 4.53 4.89 5.17 5.40 UO 5.n 5.12 6.05 · 9 UO 3.S~ 4.41 4.76 5.02 5,24 5.45 5.59 5.74 5.87

10 US U8 4.33 US 4.91 5.12 5.50 5.46 5.60 5.72 11 . 3.11 U2 4.26 4.57 4.82 5.05 5.tO 5.55 5.49 5.61 12 5.08 5.n· 4.20 4.51 4.75 4.95 5.12 5.27 5.59 5.51 IS S.06 5.7S 4.15 4.45 4.69 4.88 5.05 5.19 5.32 . 5.4S 14 S.05 5.70 •. 11 •.• 1 •. 64 •. 85 •. 99 5.IS 5.25 S.36 15 S.OI S.67 4.08 4.37 4.59 4.78 4.94 5.08 5.20 5.51 16 5.00 5,65 •. 05 • • SS 4.56 4.74 4.90 5.05 5.15 5,26 17 2.98 3.63 4.02 4.30 4.52 4.71 4.86 499 5.11 5.21 18 2,97 5.61 4.00 4.28 4.49 4.6i •• 82 4,96 5.07 5.17 19 2.96 3.59 3.98 4.25 4.47 4.65 4.79 4.92 5.04 5.14

20 US 5.58 5.96 4.2S 4.45 4.62 4.77 4.90 5.01 5.11 24 t.12 3.53 5.90 4.17 4.37 4.54 4.68 4.81 4.12 ~ .0.1 SO U!' t.49 5.85 4.10 4.50 4.46 4.60 4.72 ~.82 4.12 40 2.£6 3.~< 3.79 4.04 · U3 4.39 4.52 4.63 4.15 4.82 60 US S.40 5.74 S.98 4.16 4.S! 4,44 4.55 US 4.15 . 120 UO U6 S.68 S.92 •. 10 4.24 4.56 4.47 4.56 4.64 «I t.77 5.S! US U8 4.05 4.17 4.29 4.39 4.47 4.55

Catatan bkt DuI A.1fIII o/IfIII_'1cII ,.,1It1ts. ~ ..uk _lUI ...... blI. The Instku" of loIathomatlca1 Statlsllc:&.

Sumber: Schefler (1987).

114

Lampiran 23

Tabel Uji HSD (0,01)

115

Lampiran 24

Tabel Uji r

DEGREES OF 5 • 1 DEGREES OF 5 1 FREEDOM (OF) PERCENT PERCENT FREEDOM (OF) PERCENT PERCENT

1 .997 .. 1.000 204 .388 .496 2 .950 . .990 25 .381 .487 3 .878 .959 26 .374 .478 4 :811 .917 . 27 .367 .470 5 .75·' . 874 28 .361 .463 6 .707 .834 29 .355 .456 7 .666 .798 . 30 .349 .449

. 8 :.632 .765 35 .325 .418 9 .602 :735 ' 40 .304 .393

10 .576 .708 48 .288 .372 11 .553 .684 50 .273 .354 12 .532 .661 60 .250 .325 13 .5104 .6041 70 .232 .302 , 104 .497 .623 80 .217 .283 15 . .,(82 .606 90 .205 ' .267 16 .468 .590 100 .195 .25,( 17 . .456 .575 125 .174' .228 18 .4404 .561 150 .159 .208

, 19 .0433 .5049 200 .138 .181 20 .423 .537 300 .113 .1048

I 21 .4 13 ' • .526 400 .098 .128 22 .404 , .515 500 .088 .115 23 ·.396 .505 1000 .062 .081

" , -

Smnber: Soedigdo & SoedigdQ (1977),

Perhitungan Penetapan Kadar Abu Simplisiarepository.wima.ac.id/647/7/LAMPIRAN.pdfPerhitungan Penetapan Kadar Abu Simplisia Berat krus kosong: 1. 18,8572 gram 2. 18,8897 gram 3. 19,1592

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