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Organization of an Organic Chemistry Laboratory
16

Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

Dec 17, 2015

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Page 1: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

Organization of

an Organic Chemistry Laboratory

Page 2: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

Organic chemistry laboratories are mainly specified to conduct organic chemistry research

studies, in particular organic synthesis studies.

Page 3: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

Benches & Hoods

Page 4: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

General Glassware and Metal Equipment1- Reaction flasks (Vessels):

Page 5: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

2- Condensers

3- Addition & Separation Funnels

Page 6: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

4- Beakers & Erlenmeyer FlasksThese glass equipments are widely used for diverse aims in organic

synthesis studies.

5- Graduated Cylinders & PipettesThese glass equipments are used to transfer a certain

amount of liquid.

Page 7: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

6- Funnels

7- Reduction & Expansion adapters

Page 8: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

8- Other accessory of synthesis – the metal, plastic and Teflon equipment

Page 9: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

9-Balances

Balances are the starting points of most of the practices in chemistry laboratories. In order to accurately weight and transfer liquid and solid organic compounds, balances are utilized.

Page 10: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

10-FumeHoodFume hoods in organic and pharmaceutical chemistry lab. Studies are routinely used devices since they provide a safe area to work with chemicals. As learned through the safety parameters, chemicals are hazardous and potential risky to work on, therefore, chemistry labs require safe areas that supplies enough ventilation.

Reaction that are generating toxic gases must be run in fume hoods.

Page 11: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

11-Furnaces(Ovens)

ovens are routinely required in organic synthesis studies to dry the solid reagents and particularly reaction products. These instruments are made-up with an electronic system to set-up desired inside temp. Depending, and particularly knowing, the melting point of organic compounds (i.e., having melting point generally higher than 50°C) ovens are used to dry materials.

Page 12: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

12-HeatersHeaters are so important in organic synthesis

studies, because some of the organic reactions require activation energy to reach to transition state and to yield the products. Employing heat is one of

the ways to charge the energy required.

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Page 13: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

13- Setting cold temperature

Because of highly exothermic of some organic reactions, it is quite important to make those reactions at low temperatures. This is also critical to increase reaction yields to prevent the formation of by-products, and more importantly, to safely conduct the experiment without a serious laboratory accident.

Page 14: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

14-Desiccators

Desiccators are instruments to dry solid compounds in organic and pharmaceutical chemistry applications. They are particularly used to remove water residues in solid organic substances. Another advantage of desiccators is that they are also available to dry substances thermally unstable and therefore should not be heated to dry.

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Page 15: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

*Other instruments used in organic chemistry laboratories

there are other instruments employed routinely in organic and pharmaceutical chemistry practices, like UV (Ultraviolet) spectrophotometers, HPLC (High Pressure

Liquid Chromatography) systems, GC (Gas Chromatography) systems, MS (Mass Spectroscopy) systems.

Page 16: Organization of an Organic Chemistry Laboratory. Organic chemistry laboratories are mainly specified to conduct organic chemistry research studies, in.

*Working with gases

Gas state is one of the states of an organic compound and some organic compounds are at gas

state at room temperature. In general, a gas compound is higher in energy due to its higher

entropy. Therefore, much more attention should be paid during working with gases in chemistry practices. The safety rules must be applied,

otherwise, an explosion might occur that can result in severe laboratory accidents.