OPTIQUAD-M 4050 W · 2018. 5. 4. · VARINLINE® measuring section. The entire system consists of the Analyzer Unit, multifunctional thermal section, Operating Unit and temperature
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Spectroscopic analysis system for the continuous inline measurement of protein, fat and lactose
• Non-contact measurement of protein, fat and lactose content in milk products• For use in dynamic control loops• High precision and long-term stability
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OPTIQUAD-M 4050 W
1 Product features 3
1.1 Inline measurement of protein, fat and lactose in milk products................................... 31.2 Options and variants......................................................................................................... 51.3 Description of the entire system...................................................................................... 71.4 Measuring principle.......................................................................................................... 8
2 Technical data 9
2.1 Technical data - OPTIQUAD.............................................................................................. 92.2 Technical data - temperature sensor ............................................................................ 132.3 Technical data - sampling valve with operating key...................................................... 142.4 Dimensions and weights ................................................................................................ 15
2.4.1 Operating Unit ....................................................................................................................... 152.4.2 Analyzer Unit ......................................................................................................................... 162.4.3 Process connections............................................................................................................. 17
3 Installation 18
3.1 Intended use ................................................................................................................... 183.2 General installation conditions ...................................................................................... 183.3 Installation of the Analyzer Unit..................................................................................... 19
3.3.1 Mechanical load relieving ..................................................................................................... 193.3.2 Installation in horizontal pipelines ....................................................................................... 213.3.3 Installation in vertical pipelines ........................................................................................... 223.3.4 Installation position and horizontal or vertical distances.................................................... 233.3.5 Influence of built-in components ......................................................................................... 243.3.6 Water cooling and air flushing.............................................................................................. 25
3.4 Installation of Operating Unit ......................................................................................... 26
4 Electrical connections 27
4.1 Safety instructions.......................................................................................................... 274.2 Connection diagram ....................................................................................................... 274.3 Power supply .................................................................................................................. 284.4 Configuration of connection terminals for the outputs ................................................. 29
5 Order information 30
5.1 Order code ...................................................................................................................... 30
6 Notes 33
PRODUCT FEATURES 1
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1.1 Inline measurement of protein, fat and lactose in milk products
The innovative OPTIQUAD-M 4050 WOPTIQUAD-M 4050 WOPTIQUAD-M 4050 WOPTIQUAD-M 4050 W is used to measure the protein, fat and lactose in milk products and opens up new possibilities in process optimization.
Unlike conventional bypass devices, measurement takes place directly in the pipeline - without coming into contact with the medium. Analysis is done through an optical window in a standard VARINLINE® measuring section. This enables the OPTIQUAD to provide extremely precise readings every second, enabling much quicker intervention into production.
The advantages are obvious: Measurement is hygienic and there is no need for sampling or sample transport and its associated sources of error. High long-term stability and no need for consumables mean a significant reduction in operating and maintenance costs. Best of all, the OPTIQUAD outshines typical bypass devices with its outstanding price/performance ratio.
Figure 1-1: Analyzer Unit and measuring section
1 Analyzer Unit2 Sampling valve with operating key and temperature sensor
3 VARINLINE® measuring section
1 PRODUCT FEATURES
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Highlights• Inline measurement of protein, fat and lactose in milk products• Non-contact analysis• High precision and long-term stability• For use in dynamic control loops• Eliminates the need for sampling, sample transport and preparation• Eliminates the need for daily cleaning• No costs for chemicals, reagents and cleaning agents• Impressive price/performance ratio
Industries• Dairies• Cheese dairies
Applications• Strategic increase in the protein content of cheese-making milk by adding protein
concentrate as retentate from a UF plant.• Standardization of the fat content in drinking milk production.• Setting a constant ratio of fat to protein. This results in a constant quantity of cheese per
cheese producer, and the avoidance of empty forms in the press system. The increase in the protein content from 0.1% to 0.3%, depending on the type of cheese, results in an increase in yield of 2% to 5%!
• Increased concentration of whey or skim milk to produce protein concentrate.• Production of protein concentrate through evaporation and spray drying.• Measurement and setting of the fat and protein content in the production of UHT milk and
evaporated milk.
PRODUCT FEATURES 1
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1.2 Options and variants
Compact and flexible Operating Unit
Hygienic process connection and easy cleaning
Water cooling and air flushing
The compact Operating Unit is extremely flexible and can be installed anywhere thanks to a serial interface - either in its own stainless steel housing or into a control cabinet on site. The measured values and status information can be read off this unit and output to the automation system. This unit is also used to input laboratory values for recalibration.
The Analyzer Unit is connected to the process without any contact via an optical window in the VARINLINE® measuring section.
The measuring section housing conforms to the FDA. In addition, cleaning is easy using the SIP/CIP method.
The use of water as a coolant is necessary at higher ambient temperatures and when measuring hot media. The OPTIQUAD Analyzer Unit can be optimally cooled that way.
Air can be flushed in to prevent condensation on the optical window.
1 PRODUCT FEATURES
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Optimised sampling and easy recalibration
Less maintenance, more stability
Taking samples and analysing them in the laboratory is typically how the OPTIQUAD is verified.
Thanks to the integrated sampling valve with operating key, sampling campaigns are simple.
The reference values determined in the laboratory are then input into the Operating Unit and recalibration is performed at the touch of a button.
Compared to typical laboratory and bypass devices, no daily recalibrations are necessary when operating the OPTIQUAD. As there are no moving parts, high long-term stability and thus minimal maintenance is achieved. In addition, the optical window remains "automatically" free of any coatings thanks to the cleaning cycles performed by the dairy.
PRODUCT FEATURES 1
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1.3 Description of the entire system
The main components of the OPTIQUAD are the Analyzer Unit and the Operating Unit.
The Analyzer Unit is connected to the VARINLINE® measuring section via the multifunctional thermal section (MFT). In addition, a temperature sensor and a sampling valve with operating key are fitted to the VARINLINE®.
The Operating Unit, which can be shut off, is used for display and parametrisation of the system. In addition the unit delivers readings via up to four 4...20 mA signals as well as four binary signals for status, warning and error messages.
Figure 1-2: Setup of the entire system
1 Operating Unit2 Analyzer Unit3 Quick connections for water cooling and air flushing4 Temperature sensor5 Sampling valve with operating key
6 VARINLINE® measuring section7 Electrical connections8 24 VDC9 4...20 mA current outputs and digital outputs
1 PRODUCT FEATURES
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1.4 Measuring principle
The OPTIQUAD uses several light sources to measure the substances. Depending on the measuring task, up to 4 optical processes and 12 wavelengths are used. They are coupled into the medium via the optical window and measured with appropriate sensor elements, depending on the analytical process. The multitude of raw measured values is fed into a mathematical model which determines the protein and fat content.
Advantages of the measuring principle:• Unique combination of 4 optical measuring processes in one Analyzer Unit• Synchronous measurement of transmission, scattering, fluorescence and refraction• 12 different wavelengths of UV/VIS/NIR/IR, 200 to 4000 nm
1 Analyzer Unit2 Optical window
3 VARINLINE® measuring section
1 Coupling radiation2 Refraction3 Fluorescence, scattering4 Transmission5 Mirror or blind cover6 Medium7 Lens or optical window8 Radiation and reception level
TECHNICAL DATA 2
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2.1 Technical data - OPTIQUAD
Measuring systemMeasuring principle Spectroscopic analysis with up to 4 optical measuring principles (transmission,
scattering, fluorescence and refraction with different wavelengths in the UV to IR range)
Application range Measurement of protein, fat and lactose in milk products
Measuring range Fat: 0...5% (for standardized raw milk and drinking milk)
Protein: 2..5% (for standardized raw milk and drinking milk)
Lactose: 0...1%, 3...5%, 8...12% (for standardized raw milk and drinking milk)
DesignConstruction Non-contact inline measurement in which the OPTIQUAD is adapted to a standard
VARINLINE® measuring section.
The entire system consists of the Analyzer Unit, multifunctional thermal section, Operating Unit and temperature sensor as well the sampling valve with operating key.
Analyzer UnitAnalyzer UnitAnalyzer UnitAnalyzer Unit
Version The Analyzer Unit is installed on a VARINLINE® measuring section via the multifunctional thermal section (MFT).
Disassembling the Analyzer Unit does not result in any interruption in production.
A temperature sensor and a sampling valve with operating key are integrated into the VARINLINE® measuring section.
The hygienic, cleanable sampling valve with integrated operating key allows the precisely timed allocation of the sample to the measurement of the Analyzer Unit and the Operating Unit.
VARINLINE® measuring sections are available for pipelines from DN40 to DN150/PN10 with, for example, welded ends, flange or milk pipe connection (refer to section "Process connections").
Operating UnitOperating UnitOperating UnitOperating Unit
Version Industrial PC with touch screen display, parameterization and calibration built into a stainless steel housing or integrated into a control cabinet on site.
Interfaces 1x RS422 isolated, connection to Analyzer Unit
1x USB 2.0, data removal
Outputs Up to 4 analogue 4...20 mA outputs
Up to 4 digital outputs
Display and user interface 5.7" colour LCD with touch screen and background lighting
QVGA resolution 320x240 pixels, 256 colours, 6 control keys
Operating languages German, English and French
2 TECHNICAL DATA
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OptionsOptionsOptionsOptions
Air flushing Purge air feed line: connects the conditioned compressed air to the Analyzer Unit (MFT) to prevent condensation on the optical window and heat accumulation at high temperatures.
Purge air return: disposal into the environment
Connection: quick connector with 6 mm / 0.24" outer hose diameter
Air pressure: 0.3...0.5 bar / 4.4...7.3 psi (can be set by customer)
Consumption: e.g. 1 l/min at 0.5 bar / 7.3 psi (depending on application)
Cooling Cooling water feed line: cooling water or tap water, deficient in lime, to cool the Analyzer Unit by way of serial connection of the separate water connections for the Analyzer Unit and the MFT.
Cooling water return: drain into open channel or closed circuit.
Connection: quick connector with 10 mm / 0.39" outer hose diameter
Operating pressure: 0.5 bar / 7.3 psi
Consumption: approx. 0.1 l/min (depending on application)
Temperature: +4...+20°C / +39...+68°F recommended
Measuring accuracyReference conditions Measuring accuracy based on the calibration of the measuring device by way of
reference samples and under constant process conditions within a sampling campaign.
Recalibration On site through sampling and input of laboratory values via the Operating Unit. This results in an automatic adjustment of the calibration curve to changed conditions.
Measuring accuracy Standard deviation protein measurement: ≤±0.02%
Standard deviation fat measurement: ≤±0.03%
Standard deviation lactose measurement: ≤±0.1%
Repeatability Standard deviation protein measurement: ≤±0.01%
Standard deviation fat measurement: ≤±0.015%
Standard deviation lactose measurement: ≤±0.05%
Temperature dependency Compensation over the temperature sensor.
Pressure dependency Measurement not affected by pressure.
TECHNICAL DATA 2
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2.4 Dimensions and weights
2.4.1 Operating Unit
Dimensions Weight
[mm] ["] [kg] [lb]
a 370 14.75 8.0 17.6
b 130 5.12
c 290 11.42
2 TECHNICAL DATA
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2.4.2 Analyzer Unit
Entire system
Metric VARINLINE® measuring section, welded ends acc. to DIN 11850
Entire length of the Analyzer Unit including sampling valve and the metric measuring section:739 mm + b1 (mm value from table above) or 29.1" + b1 (" value from table above).
Entire length of the Analyzer Unit including the sampling valve and imperial measuring section:739 mm + b1 (mm value from table above) or 29.1" + b1 (" value from table above).
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3.1 Intended use
OPTIQUAD is a spectroscopic analysis system that uses up to 4 optical processes (transmission, scattering, fluorescence and refraction) and up to 12 wavelengths.
Measurement is done inline, is non-contact, continuous and precise, using no bypass, sampling or moving mechanical parts. The result is wear-free and extremely low-maintenance inline measurement. Recalibration is only necessary at very large time intervals, depending on the application.
The main area of application is in determining the protein, fat and lactose content in milk products.
It is primarily the optical data of the medium that is recorded and the temperature of the medium is measured. From these parameters, stored mathematical formulas and calibration data specific to the application are used to calculate the protein and fat values.
3.2 General installation conditions
The Operating Unit, an industrial PC with touch screen and built into a stainless steel housing, is installed at the customer's site following delivery or, if ordered as an option, the industrial PC with touch screen is integrated into an existing control cabinet on site and then electrically connected.
As a rule, the Analyzer Unit is completely preinstalled and delivered with the VARINLINE® measuring section that was ordered. This complete measuring system must then be installed in the pipeline at the customer's site. Depending on the conditions on site, the following installation positions are possible:
Horizontal pipelines• Standard: horizontal Analyzer Unit (at 90° to the pipeline)• Alternative: for technical reasons, the temperature sensor and the sampling valve with
operating key are installed on separate VARINLINE® measuring sections.
Vertical pipelines• Standard: Analyzer Unit at 90° angle to pipeline• Alternative: for technical reasons, the temperature sensor and the sampling valve with
operating key are installed on separate VARINLINE® measuring sections.• Flow direction from bottom to top
It is recommended to have an intervisibility between the Operating Unit and the Analyzer Unit. This makes sense predominantly in terms of recalibration and potential system checks.
The pressure-bearing parts have been designed and rated for stationary operation taking into account the maximum pressure and temperature.
INSTALLATION 3
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3.3 Installation of the Analyzer Unit
3.3.1 Mechanical load relieving
Especially in the case of pipeline vibrations the Analyzer Unit should be relieved from mechanical loads.
If installed horizontally, the intended mounting ring may be used as needed to mechanically support the Analyzer Unit or to hang it on.
The Analyzer Unit should be installed where easily accessible.
Figure 3-1: Example for mechanical load relieving for horizontal installation
1 Attached to joist, ceiling, beam…2 Threaded rod (can be installed above or below)3 Screwed connection on mounting ring on Analyzer Unit
Materials and tools required for installation are not included in the scope of delivery and must be provided by the customer.
3 INSTALLATION
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If installed vertically, an optional retaining bracket construction may relieve the Analyzer Unit from mechanical loads.
Figure 3-2: Example for mechanical load relieving for vertical installation
1 Secure support strut 1 in the threaded hole in the Analyzer Unit cover with M6 screw.2 Support strut 13 Fasten support strut 1 to support strut 2 with M6 screws.4 Support strut 25 M12 threaded rod6 Fasten support strut 2 to support strut 3 with M12 screw.
Fasten support strut 3 to the threaded shank of the pipe clamps with M12-screws.7 Support strut 38 Fasten two pipe clamps with threaded shank to pipe with M6 screws
INSTALLATION 3
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3.3.2 Installation in horizontal pipelines
In the standard version, the Analyzer Unit, MFT, temperature sensor and sampling valve with operating key are all installed in one unit. The product can flow through the measuring section in both directions.
If, for technical reasons, the sampling valve with operating key has to be installed separately, an additional measuring section is used. The sampling valve with operating key must be installed in the direction of flow of the product and upstream from the Analyzer Unit.
Horizontal installation of Analyzer Unit
Figure 3-3: Example of VARINLINE® measuring section with welded ends
1 Analyzer Unit with MFT2 Pipeline3 Flow direction of medium
4 VARINLINE® measuring section with temperature sensor and sampling valve with operating key
Horizontal installation with additional VARINLINE® measuring section
Figure 3-4: Example of VARINLINE® measuring section with welded ends
1 Analyzer Unit with MFT2 Pipeline3 Flow direction of medium
4 VARINLINE® measuring section with mirror module or blind cover5 Temperature sensor and sampling valve with operating key
3 INSTALLATION
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3.3.3 Installation in vertical pipelines
In the standard version, the Analyzer Unit, MFT, temperature sensor and sampling valve with operating key are all installed in one unit. The product flows through the measuring section from bottom to top.
If, for technical reasons, the sampling valve with operating key has to be installed separately, an additional VARINLINE® measuring section is used. The sampling valve with operating key must be installed in the direction of flow of the product and upstream from the Analyzer Unit.
When using two VARINLINE® measuring sections, the sampling valve with operating key and the Analyzer Unit can be freely positioned on the x-y plane.
Vertical installation of Analyzer Unit
Figure 3-5: Example of VARINLINE® measuring section with welded ends
1 Analyzer Unit with MFT2 Pipeline3 Flow direction of medium
4 VARINLINE® measuring section with temperature sensor and sampling valve with operating key
Vertical installation with additional VARINLINE® measuring section
Figure 3-6: Example of VARINLINE® measuring section with welded ends
1 Analyzer Unit with MFT (can be freely positioned on x-y plane)2 Pipeline3 Flow direction of product
4 VARINLINE® measuring section with mirror module or blind cover
5 VARINLINE® measuring section with temperature sensor and sampling valve with operating key (can be freely posi-tioned on x-y plane)
INSTALLATION 3
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3.3.4 Installation position and horizontal or vertical distances
When installing, choose a location in which the Analyzer Unit is easily accessible. The sampling valve and operating key in particular must be easily accessible.
Since the Analyzer Unit must swing down for the system check, there must be enough space below.
When installing the Analyzer Unit, there must be at least 725 mm / 2.4 ft space left underneath, measured from the middle of the Analyzer Unit.
Figure 3-7: Installation position and horizontal or vertical distances
1 Remove the Analyzer Unit horizontally from the VARINLINE® measuring section2 Minimum horizontal distance: 950 mm / 3.1 ft3 Minimum vertical distance: 725 mm / 2.4 ft4 Analyzer Unit in swung down position
3 INSTALLATION
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3.3.5 Influence of built-in components
Pipe bends, valves, gate valves, pumps and other built-ins can have an influence on the product and thus on the measurement. For this reason, the results must be checked following any change in the production process and, if necessary, recalibrated.
In the event that the product has not been sufficiently homogeneously mixed, a stationary mixer 4 is recommended.
Figure 3-8: Built-in components
1 Valves or gate valves2 Pipe bends3 Pumps
4 Stationary mixer (in the direction of flow upstream from the VARINLINE® measuring section)
INSTALLATION 3
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3.3.6 Water cooling and air flushing
Air can be flushed in to prevent condensation settling on the optical window.
The use of water as a coolant is recommended at high ambient temperatures and when measuring hot media. This allows water to completely flow through the outer jacket of the MFT and the Analyzer Unit to cool it.
Refer to "Technical data" for the exact requirements regarding purge air and cooling water.
Figure 3-9: Water cooling and air flushing
1 Supply of purge air (conditioned compressed air)2 Disposal of purge air into environment3 Supply of cooling water or tap water deficient in lime to Analyzer Unit4 Hose connection between separate water connections for MFT and Analyzer Unit5 Supply of cooling water to MFT water connection6 Disposal of cooling water to open channel or closed circuit
Materials and tools required for installation are not included in the scope of delivery and must be provided by the customer.
3 INSTALLATION
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3.4 Installation of Operating Unit
The Operating Unit is available in the following versions: Industrial PC with touch screen display, parameterization and calibration in a stainless steel housing or installation in a control cabinet on site.
It is recommended to have an intervisibility between the Operating Unit and the Analyzer Unit. This makes sense predominantly in terms of recalibration and potential system checks.
Figure 3-10: Wall mounting of Operating Unit in stainless steel housing
1 Horizontal distance between drill holes: 190 mm / 7.48"2 Vertical distance between drill holes: 210 mm / 8.27"3 Recommended distance to the wall: 5 mm / 0.20"; spacers to be provided by customer4 Assembly bracket (optional)5 When selecting the screws, bear in mind the weight of the Operating Unit!
To guarantee protection category IP65, the Operating Unit may not be installed directly on the wall. We recommend, therefore, the use of spacers 3. They guarantee that the drill holes on the rear wall of the Operating Unit are sealed.
ELECTRICAL CONNECTIONS 4
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4.1 Safety instructions
4.2 Connection diagram
All work on the electrical connections may only be carried out with the power disconnected. Take note of the voltage data on the nameplate!
Observe the national regulations for electrical installations!
Observe without fail the local occupational health and safety regulations. Any work done on the electrical components of the measuring device may only be carried out by properly trained specialists.
Look at the device nameplate to ensure that the device is delivered according to your order. Check for the correct supply voltage printed on the nameplate.
Figure 4-1: Connection diagram Analyzer Unit - Operating Unit
1 Analyzer Unit (head end)2 Operating Unit (inside view)3 Black wire from red / black twisted cable4 Red wire from red / black twisted cable5 Shielding; heat shrink tubing yellow / green6 Black wire from orange / black twisted cable7 Orange wire from orange / black twisted cable8 Black wire from yellow / black twisted cable9 Yellow wire from yellow / black twisted cable
4 ELECTRICAL CONNECTIONS
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4.3 Power supply
24 VDC (tolerance range: 24 VDC (tolerance range: 24 VDC (tolerance range: 24 VDC (tolerance range: ±25%)25%)25%)25%)• The housings of the devices, which are designed to protect the electronic equipment from
dust and moisture, should be kept well closed at all times. Creepage distances and clearances are dimensioned to VDE 0110 and IEC 664 for pollution severity 2. Supply circuits are designed for overvoltage category III and the output circuits for overvoltage category II.
• Fuse protection (IN ≤ 16 A) for the infeed power circuit, as well as a separator (switch, circuit breaker) to isolate the Operating Unit must be provided close to the device. The separator must be marked as the separator for this device.
Preparing the connecting cable
• Use 3 x 1 mm2 copper cable• Strip flexible cable approx. 10 mm / 0.39" and crimp wire end sleeve• Strip fixed lines approx. 10 mm / 0.39" and connect directly
The device must be grounded in accordance with regulations in order to protect personnel against electric shocks.
Figure 4-2: Power supply connection
1 Connection GND 24 VDC-2 Connection 24 VDC+3 Connection green/yellow PE4 Cable assembly can be connected to either of the two electrically equal openings
ELECTRICAL CONNECTIONS 4
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4.4 Configuration of connection terminals for the outputs