No. 84-3 · Stack Test &port No. 84-3 James Julian, Inc. Narth East, ... mthod 1005 as . con* in . AMA . TM 83-05, Stack Test Methods . ... 9.07 14~99 . 13.13 \i017 . 4.0 . 10 ...

Stack Test &port No. 84-3

James Julian, Inc. Narth Eas t , Cecil Co.

Fioehg Drum Mix Asphalt P l a n t May 1984

Div i s ion of Stationary Source Ehfor-t Air Managemsnt Mmbistration

Office of Enviranmental Program Department af Health and Mental Hygiene

state of Mary1aI-d

Approved by Ronald E. Lip"&

May 31, 1984

Introduction :

Particula& stack tests were conducted in May, 1984 on the exhaust emissions £ran the Boeing drum mix asphalt plant operated by Jams Julian, Inc, located in North East, C e c i l County. The tests were conducted i n an effor t to determine whether o r not the fac i l i ty was being operated within canpliance of applicable Maryland S t a t e air quality regulations,

The emissions are controlled by a venturi scrubber folluwed by a cyclone depnister, Although the plant is rrawnally rated a t 600 TPH, the tests were conducted a t the n o d production rate of 275 TPH, The capacity of the storage silo (100 tons) necessitated running each test in t w o halves, By starting with an enpty s i l o and having seueral trucJcs standing by, the plant was able to opexate for the required 45 minutes needed to make A m l e traverse. This inc luda the 36 minutes of sampling plus a period to allm the plant to stabilize. During all three tests, the plant was Using virgin material.

This fac i l i ty was tested in mrdance w i t h mthod 1005 as con* in AMA TM 83-05, Stack Test Methods for Stat ionary Souroes, The controlling

- standard for this source is the federal New Source P e r f o m c e Standard of

R e s u l t s :

A sumnary of the results is presented in table 1-1. Canplete results and prirrrary data are contained i n the al?pendix.

Table 1-1. Summary of Particulate Sampling Results For:

84-3 Jamep Julian, Inc. - Ebdng aMn mix asphpl$,,plant I I '

9kbased on front half catch

2oncentsatio:

004

.04

-04

Run ID

5/2/84-1

5/3/84-1

5/3/84-2

Average

Concentration* (grainslscfd)

-092

.025

. 0077

.065

?

Emission Rate*

( lbslhr)

21.5

5 -4

16.9

14.6

r

Production rate (WH)

275

275

275

Isokinetic Variation

(%I

99.8

101.6

102.2

flow rate (scfm dry)

27282

25495

25731

Data

7. C02

3.5

4.6

3.5

Average Stack

temp (OF)

144

143

145

7. Hz0

22.2

22.3

23.4

Gas

7. 02

12.8

13.0

13.0

APPENDIX :

Nomenclature Calculated Resu l t s Data Summaries Laboratory Ana Lyses Primary Data Calibration Data Preliminary Stack Test Survey

~.-.-- - . -.---- . -.---. --~ . - ---.- ... .. .--.. . .. . . . . .

. . page 1 of 2 .- -. - C -

w w STATe - -- - A i r Management Administration

- STACK SAMPLING NOMENCLATURE -- ..

: cross sact ioual area 02 stack a t sample s i t e , ( f t2)

: mole fract ion moisture i n stack gas, (dimensionless)

: concentration of front half catch, (grainalscfd)

: concentration a t 122 C02, front half catch, (grains/scfd)

: concentration a t 50X EA, front half catch, (grainslscfd)

: dry gar meter correction factor, (dimensionless) .- - - : p i t o t tube coeff ic ient , (dimensionless)

: concentration of t o t a l catch, (grains /scf d)

: concentration a t l2Z C02, t o t a l catch, (grainslscfd)

: concentration a t 50X EA, t o t a l catch, (grainslscfd)

: diameter of sampling nozzle i n l e t , (in)

: percent excess a i r Ln stack gas, (Z)

emission r a t e , front ha l f , (lbs/hr) L

: emission ra te , t o t a l , (lbs/hr)

: o r i f i c e meter pressure d i f f e r en t i a l that provides a flow r a t e of .75 ft-3/min a t 7 @ ~ and 29.92 in.Rg,

- (in, H20) - : average o r i f i c e pressure d i f fe ren t ia l , (in. 820)

: percent isokinetic, (X)

: molecular might of stack gas, dry basis , ( lb/ lb mole)

: molecular weight of stack gas, w e t basis , ( l b l l b mole)

: normality of t i t r a n t for S+ sample, (g-eq/l)

': baromarric pressure, (in, Hg)

:average absolute stack pressure, (in, Hg)

- -. page 2 of 2

NOMENCLATURE

Qa lq

Qm

b t d

Qs

Qsoln

Qsatd

Qti

Q t i b

Q t s t d

Qw

b s t d

Tmavg

Tsatrg

s

Wd

w t

8

. - : velocity pressure d i f f e r en t i a l , (in. X20) --

: volume of SO, sample aliquot t i t r a t e d , (ml)

: net dry sample gas volume , (ac f d)

: standard dry gas sample volume, (scfd)

: ac tua l s tack gas volumetric flow r a t e , dry bas i s , (acfm dry)

: t o t a l volume of & sample solut ion, (ml)

: standard stack gas volumetric flow r a t e , dry bas i s , (scfm dry)

z: volume of t i t r a n t required t o neutra l ize S4, sample a l iquot , (ml)

": volume of t i t r a n t required t o neutra l ize blank solut ion, (ml)

: t o t a l standard sample volume, (scf)

: t o t a l volume of water collected, (ml)

: standard vapor volume of water collected, (scf)

: average dry gas meter temperature, (OF)

: average s tack temperature, (OF)

: average veloci ty of stack gas a t sample s i t e , ( f t l sec)

: front half par t icula te catch, (q)

: t o t a l par t i cu la te catch, (mg)

7: sampling t i m e , (min.)

Page 1 of 1

MA~YLAND smm AIR MANAGEMENT ADMINISTRATION

PARTICULATE STACK SAMPLING CALCULATED RESULTS

- Plant JAMES JULIAN ASPHALT, CECIL CO.

Source Asphalt Plant

"Not Applicable

I

I

5/3/84 - 2 1400 - 4 5

38,509

11.771

5/3/84 - 1 947 - 10

37.906

10.883

RUN ID

1. Qmstd

20 Qwstd

42.78 40.20

90 Qe 30604 28709

100 Qsstd 27282 25495

11. Q -092 -025

51.222 , 30 Qtstd

-h

4. Bw

5/2/84 - 1 17139 - 7 1

39.863

11.358

48.789 50.281

.223 ,234

41.39 I I 29143

25731

.077

- 12. Q - -106 ,044

13. %I12 * *

50 Ma 29.256 29.080

I -087

*

6. 4 s 26.745

7. * *

a. v,

26.486

*

*

*

14. Ct12

150 Cdso

* *

* *

16. Ct50

17. Ed

180 Et

19. 1

* *

21.5 5.4

24.8 9.6

99.8 101.6

*

16.9

19.2

102.2

MARYIAND STATE AIR MANAGEMENT ADMINISTRATION

Page 1 of 1

PARTICUTE STACX SAMPLIE DATA SUMMARY

Plant James Julian Asphalt, C e c i l Cbunty

Source Asphalt Plant

-

I

5/3/8 4-2 1400-1545

-84

38.855

80.7

29 -79

0.928

245.3

191.2

217.0

3.5

RUN ID

1. Cp

2. Qm

-2 - 3. Tmaqh

40 Pbar

160 8

I

10. %2= . 11. Tsavg

12. ( A P P , : ~

130 psavg

14. A, :

15. Dn

5/2/84-1 7209-1423

5. &aw 1-01

72

5/3/84-1 942-1130

0.904

13.0

145.2

12.8

144.4

72

-84

40.174

84.7

30.04

13 -0

143.3

72

-84

38.026

79.0

29.87

226.8

60.4

108.0

4.6

60 Qw 236.7

7. Wd 237 -5

0.685

30.02

15.321

0 -239

80 Wt

90 m 2

273.4

3 -5

0.644 0.658

29.85

15 -321

0.239

29.77

15.321

0.239

MYLAND STAT2 B ~ U OF AIR QuMtIm dr NOISE CONTROL

AND BUREAU OF L A B O R A T O n B

Plant Complete

Faci l i ty Tested . BY

Test Date I

Run ID 5 /3 /w0 / I I #

sulfate Acidity

WEIGHT OF PARTICULATE COLUCl'ZD

Probe

F i l t er

Weight Gain (w)

/60, b

&?6 I /

I n i t i a l Weight ( m m )

/3+98/=L -6 7fS 6 43/

-2

~ o t a l Gain, ( m l ) S 3 L . 7 I

- Container

probe 3

Fi l t er b

Volumatric Gain -( Id1

F iru l V o l w (?la)

1rnping;crs

silica g e l b,

Final Ueight nnw)

136 /hoe 3 / 5 9 . 5 5 4 2

Cyclone 35

I n i t h l Volume (Id)

/5/. Bad$ /5/. $6 73

1

q a 4 . d

L/36,7

L/D, 8

Subtotal, (msr;) $32 5 1

/P Water Soluble

~ O P D

/%6, LP05 I /+u.bs a 5

a 9 d . d

438, p 1 /6r 7

I 38a 6

Oranics /5

Acetone Wash J3

Subtotal. ( w ) 35.5' I - - 'L - Total Weight of PaWcukts Collected, (.g) a - - 373,Lf

!

3, + /H $793 /95889/ ?

1%. 546 9 146 ,533 P 41 7

WYLAN'D STAT3 BUREAU OF A I R QUALITY & NOISE CONTROL

AND BUREAU OF WBORATOIUB

- PARTICULATE STACK SAMPLING WBORATOiiY RESULTS

Plont

Facility Tesb5'

Test Date / /

Run ID 4 - / 3 / 8 ~ / C # /

Conkher Final Ueight Init la l Weight ( m m ) ~~)

Cyclone ' 6d /+5 5937 I / Y 6 5947 I a. O i

Weight Gain m ~ ) '

1

Probe 3 b

t5 Filter

30. #\ \

JK 0 I

. . Subtotal. (w) - ;. 7,k I - - " -

TOM eight of Particulate collected, (mg) / @ I 5 3

'l subtotal. (MI 64.4 I

- Acidity Sulfate . 8

I

Probe mg* "9. N"qH I

Filter log. ~neq. X,~H

t

$9, 0' i

/6,4

VOLUME OF MOISTURE COUECTZD

/rfb, 7337

/ & L/53i?,

Water Soluble 43

0ra;mics 6k

/46# 754/7

/46.97/6

/35 53 56 8 s i Acetone Wash /QOO /3559%8

Volumetric Gain -(Id)

$ / d a d

/ 6 4

Final Volux~e Init la l V o l m . (la) (nl)

~ o t a l Gain. (a) -8 I In~intxer~ 4 10, fl

s i l i ca Gel f , a w g

$00~ u &9#0

X A R W STATE BUREAU OF AIR QUALITY & NOISE CONTROL

AND BUREAU OF LABORATO3133

- PARTICULATE STACK SAWLING LABORbTOaY RESULTS

Plant O f w w - a$~Lf&. Facility Tested I

/ / Test Date . 6/3/4q / I I

R u n ID #

probe b /3K@400 /35: 4 9 9 4 7*6 /97. 3w ' * 7/77

,4 /36#$/63 , 9, 7 \

, b 78d Filter

..- WEIGHT OF PARTICULATE COLL3CTXD

subtob~l. ( m ~ ) d s g I

Weight Gain (w)

-- t

Subtotal. (m) / 9 / 1 & 1

- - L

- Total Weight of Particulab Collected, (mg) - * a m

I n i t k l Ueight ( m m )

-

Sulfate Acidity

Contalper

4

23 *b i

1

* 9

) b /4&.D964 Water Soluble

0r~;mics /& / , 9 p , R / / b

Probe mg. mq. N,OH

Fil ter IDg. mq. XaOH

-

Final Weight (ma Ins)

/4d,8744

/39* 8/0 6

Acetone Wash $6 /4i!348*

Final Volurne (dl

I n ~ i m e r s L/ 3540

Silica Gel r / 39%5 !-

1 /4Z 3 453

Init la l Volume Volumatric Gain (a) -(dl

aoalo $ 3 0 ~ 6

379.9 i s 3

i T o t a l Gain. (d) 3+'5 3 I

$1 9

NOTES

NOTES

OFFICE OF ENVIRONMENTAL PROGRAMS AIR MANAGEMENT ADMINISTRATION

STACK SAMPLING DATA

I C

plant J ~ V M C S ~ d ' l ~ d t

I ' Start /#60 Finish / S e 4 . .

Sampling for: D ~ b y t c 4 ' 4 f c- PitobeID 5-1 Cp r 84 Meter Box (i Cm 989 H@ / , I I ~ DGM I D 5 9 3 2 2 1 C Factor -

Filter ID. 47 8 0 Noz. ID , 2 3 9 ,,. Baro. ( in. Hg. ) 23.73 & ZOO'.

Ambient OF 5 8 I-

Psvg: (in. H20) - ,33 IL

(in. ~ g ) -.02+ - Avg. 1 CO? 3.3- ,: o2 13'0 Leak Rate re ,d/ Cal5"Hg.

Post too @2Cllg.

Duct Dimens ions 5 2l' - ~ r e a /j: 321 f t 2

Diameters Upstream 3 Diame tecs Downstream .y% :: Assumed H20 (%) v:

DHMH 1630 38. g5.5

METER BOX CALIBRATION DATA AND CALCULATION FORM

(English units)

Date FG@ 9. 14 Meter box number $41 3 2 2 1

Barometric pressure, pb = 30.23 in Hg Calibrated by ?= J $

a If there i s only one thermometer on t he dry gas meter, record the temperature under td.

AH, in*

H2°

0.5

1.0

1.5

2-0

3*0

4-0

Quality Assurance Ha~dbook 145-2.3A ( f r o n t side)

in. m@i H ~ O

1,793

LB20

1,831 ll857 1957

'i

,966

.?% ,997 ,988 ,'?9 2

AH - 13.6 - - 0.0368

0.0737

0.110

0-147

0-221 :

0.294

Time @I>

min

l3.08

9.07

14~99 13.13 \i017

4.0 10 I,o,558

>

Ori f ice manometer

s e t t i n g (Am,

in. H20

0.5

1.0

vW Pb(td + 460) - - 'i AH

P + 1 (tw + 460)

Temperatures

.90/4, I

0.0317 bX [(t;w+ 460) '12 m@i = P, (td + 460)

h

Wet t e s t m - meter (tJ,

OF

79.5

79,s 79.5

79, y

79,5

79,s

Gas volume

1,771

>,(3 5 30.. 23x 5 4 2 . 7 ) I+6. -I- s 3 4.5) lot 3 22?"j?.L 8 . e o . n x ( 30.34-X f 3 9 , ~ > 10 (3 &,-z 3 X s7o.e)

10. t53 ( 30,38>( 539,s 1 0 1 3 o o 2 3 ~ ~ 7 o * ~ to, S 8 L ( 30: 45)( 5 3 "r l> 10(30 .~ .3 \1571*7 . I p317(43 , . \ c S 3 q l S > 4.13 / t

i o .ySg( 3 0 . 5 2 3 5 3 9 -

.s) 30.1 3 (571,7) L 1 0 J

W e t t e s t meter (Vw),

f t3

-: - 5 s

5

1.5 I 10

Dry gas meter (Vd) 9

f t 3

s,a+t 5.22+

to.628

Dry gas meter -

2.0 10 I )08~53

3.0 10 1 )4.582 11117 (9.13 . 124-

~ v g ' (tdL OF

925

101,7

108.5 110.4 iIo.5

99.3

I n l e t (td 1,

i OF

102.3

104.3 118.3

121 121.7

Outlet (td 1,

o "F

92.7

4 6 98*7

44.7 99.3

Page 1

MARYLAM) STATE BUREAU OF AIR QUALITY & NOISE CQRIXOL

STACX SAMPLIK; PRELPIIMRY SURVEY

I. General Infomat ion: /

Plant JOMS 1 PQspkc~if f

Address I r

Telephone 30 1 - 28 7 - 91 7/ S u m y Date

Source

~ o n t a c t ( s ) :

fi 'GO/ kL T i t l e *

T i t l e Ext.

T i t l e Bxt.

Process Description ( including type, operating schedule, feed canposit ion and

rates , production, rate, maximum rated capacity, and type of fuel) :

Notes :

Page 2

MARYLAND STATE - BAQNC -

PRBLIMINARY SURVEY

Plant ~~~ // //

Source u ,I

, ,

Survey Date 5&/8 ?‘- I I

11. Stack Data:

Material of Construction . . . . . . . . . . . . . . . . . . . . Height of Sample S i t e from Ground Level, ( f t ) . . . . . . . . . . n/ S o Inside Cross Sectional Dimensions a t Test S i t e L . . . . . . . . . 5-3 ( t

. . . . . . . . Inside,Cross - Sectional Area a t Test S i te , ( f t 2 ) .

. . . . . . . . . . . . . . . . . . . . . . . PortUi%gth, ( in) .

. . . Straight Duct Distance Before Test S i t e (stack diameters).

Stra ight Duct Distance After Test S i t e (stack diameters) . . . . . . . . . . . . . . . . . . . . Number of Points t o be Sampled

Point Ident i f icat ion:

MAb(YUND STATE BAQNC

PRrnINARY SURVEY

Iff. Point Location

Plant J L l e s J U / / ~ ~

source ~ i ~ y L & t

survey. Date

Calculated By: Checked By: