H:\Library\Reports\(4150) Site Characterization\2010\Wells Fargo\R10114.01 Photograph 1. View of installed TSB-2. Photograph 3. Installing TSB-3 with the Power Probe 9635. Photograph 5. View of abandoned TSB-2. Photograph 2. View of general Site lithology from TSB-2. Photograph 4. View of installed TSB-1. Photograph 6. View of drummed investigative derived waste stored near the southwestern limits of the property near the entrance gate.
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H:\Library\Reports\(4150) Site Characterization\2010\Wells Fargo\R10114.01
Photograph 1. View of installed TSB-2.
Photograph 3. Installing TSB-3 with the Power Probe 9635.
Photograph 5. View of abandoned TSB-2.
Photograph 2. View of general Site lithology from TSB-2.
Photograph 4. View of installed TSB-1.
Photograph 6. View of drummed investigative derived waste stored near the southwestern limits of the property near the entrance gate.
TGE Resources, Inc.
APPENDIX B
TGE Resources, Inc.
APPENDIX C
30-Dec-2010
TGE Resources Inc.Kristi Barnette
Dear Kristi,
Re: Holiday Place Work Order: 1012696
Fax: (713) 744-5888Tel: (713) 744-5815
6120 West by Northwest Blvd.
Houston, TX 77040Suite 100
ALS Environmental received 10 samples on 21-Dec-2010 02:07 PM for the analyses presented in the following report.
Project ManagerEd B. Fry
Ed B. FryElectronically approved by: Mary K. Knowles
Certificate No: TX: T104704231-10-3
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Results are expressed as "as received" unless otherwise noted. QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
The total number of pages in this report is 54.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ADDRESS 10450 Stancliff Rd, Suite 210 Houston, Texas 77099-4338 | PHONE (281) 530-5656 | FAX (281) 530-5887ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company
Date: 30-Dec-10ALS Environmental
Project: Holiday PlaceClient: TGE Resources Inc.
Work Order: 1012696Work Order Sample Summary
Lab Samp ID Client Sample ID Collection DateTag Number Date ReceivedMatrix Hold1012696-01 TSB2 (1-2) Soil 12/21/2010 07:30 12/21/2010 14:071012696-02 TSB2 (32-33) Soil 12/21/2010 08:00 12/21/2010 14:071012696-03 TSB3 (2-3) Soil 12/21/2010 09:00 12/21/2010 14:071012696-04 TSB3 (29-30) Soil 12/21/2010 09:05 12/21/2010 14:071012696-05 TSB1 (2-3) Soil 12/21/2010 10:15 12/21/2010 14:071012696-06 TSB1 (25-26) Soil 12/21/2010 10:20 12/21/2010 14:071012696-07 TSB1 Water 12/21/2010 10:45 12/21/2010 14:071012696-08 TSB2 Water 12/21/2010 08:45 12/21/2010 14:071012696-09 TSB3 Water 12/21/2010 09:45 12/21/2010 14:071012696-10 Trip Blank Water 12/21/2010 12/21/2010 14:07
SS Page 1 of 1
Date: 30-Dec-10ALS Environmental
Project: Holiday PlaceClient: TGE Resources Inc.
Work Order: 1012696Case Narrative
Batch 48930, TPH, MS/MSD is an unrelated sample.
Batch 48920, Metals, MS/MSD is an unrelated sample.
Batch 48947, Metals, MS/MSD is an unrelated sample.
Batch 48948, Metals, MS/MSD/DUP is an unrelated sample.
Batch R103100, Volatiles, MS/MSD is an unrelated sample.
Batch R103134I, Volatiles, MSD is an unrelated sample.
CN Page 1 of 1
Project: Holiday PlaceSample ID: TSB2 (1-2)Collection Date: 12/21/2010 07:30 AM Matrix: SOIL
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-01
ALS Environmental Date: 30-Dec-10
SDL
TEXAS TPH TX1005 Analyst: SEPrep: TX1005PR / 12/22/10Method:nC6 to nC12 12/28/2010 22:1061 mg/Kg-dry 1U 19>nC12 to nC28 12/28/2010 22:1061 mg/Kg-dry 1U 19>nC28 to nC35 12/28/2010 22:1061 mg/Kg-dry 1U 19Total Petroleum Hydrocarbon 12/28/2010 22:1061 mg/Kg-dry 1U 19 Surr: 2-Fluorobiphenyl 12/28/2010 22:1070-130 %REC 1100
Surr: Trifluoromethyl benzene 12/28/2010 22:1070-130 %REC 1121
MERCURY SW7471A Analyst: JCJPrep: SW7471A / 12/22/10Method:Mercury 12/22/2010 22:044.40 µg/Kg-dry 116.1 0.26
METALS SW6020 Analyst: SKSPrep: SW3050A / 12/23/10Method:Arsenic 12/30/2010 12:380.538 mg/Kg-dry 13.30 0.065Barium 12/30/2010 12:380.538 mg/Kg-dry 1145 0.086Cadmium J 12/30/2010 12:380.538 mg/Kg-dry 10.0676 0.043Chromium 12/30/2010 12:380.538 mg/Kg-dry 114.0 0.054Lead 12/30/2010 12:380.538 mg/Kg-dry 123.7 0.054Selenium 12/30/2010 12:380.538 mg/Kg-dry 10.980 0.27Silver J 12/30/2010 12:380.538 mg/Kg-dry 10.0993 0.043
TCL VOLATILES SW8260 Analyst: WLRMethod:1,1,1-Trichloroethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000621,1,2,2-Tetrachloroethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000621,1,2-Trichlor-1,2,2-trifluoroethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000741,1,2-Trichloroethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000991,1-Dichloroethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000621,1-Dichloroethene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000991,2,4-Trichlorobenzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000871,2-Dibromo-3-chloropropane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00241,2-Dibromoethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000621,2-Dichlorobenzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000621,2-Dichloroethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000621,2-Dichloropropane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000871,3-Dichlorobenzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000621,4-Dichlorobenzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.000622-Butanone 12/28/2010 15:300.012 mg/Kg-dry 1U 0.00242-Hexanone 12/28/2010 15:300.012 mg/Kg-dry 1U 0.00144-Methyl-2-pentanone 12/28/2010 15:300.012 mg/Kg-dry 1U 0.0012Acetone 12/28/2010 15:300.031 mg/Kg-dry 1U 0.0062Benzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Bromodichloromethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062
AR Page 1 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB2 (1-2)Collection Date: 12/21/2010 07:30 AM Matrix: SOIL
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-01
ALS Environmental Date: 30-Dec-10
SDL
Bromoform 12/28/2010 15:300.012 mg/Kg-dry 1U 0.00099Bromomethane 12/28/2010 15:300.012 mg/Kg-dry 1U 0.0012Carbon disulfide 12/28/2010 15:300.012 mg/Kg-dry 1U 0.0012Carbon tetrachloride 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Chlorobenzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Chloroethane 12/28/2010 15:300.012 mg/Kg-dry 1U 0.0012Chloroform 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Chloromethane 12/28/2010 15:300.012 mg/Kg-dry 1U 0.0012cis-1,2-Dichloroethene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00074cis-1,3-Dichloropropene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Cyclohexane n 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Dibromochloromethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00074Dichlorodifluoromethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00099Dichloromethane 12/28/2010 15:300.012 mg/Kg-dry 1U 0.0017Ethylbenzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Isopropylbenzene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062m,p-Xylene 12/28/2010 15:300.012 mg/Kg-dry 1U 0.0012Methyl acetate 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.0015Methyl tert-butyl ether 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Methylcyclohexane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00074o-Xylene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Styrene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Tetrachloroethene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00074Toluene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062trans-1,2-Dichloroethene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062trans-1,3-Dichloropropene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Trichloroethene 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Trichlorofluoromethane 12/28/2010 15:300.0062 mg/Kg-dry 1U 0.00062Vinyl chloride 12/28/2010 15:300.0025 mg/Kg-dry 1U 0.0012Xylenes, Total 12/28/2010 15:300.019 mg/Kg-dry 1U 0.0012 Surr: 1,2-Dichloroethane-d4 12/28/2010 15:3070-128 %REC 198.1
Surr: 4-Bromofluorobenzene 12/28/2010 15:3073-126 %REC 199.9
Surr: Dibromofluoromethane 12/28/2010 15:3071-128 %REC 1103
Surr: Toluene-d8 12/28/2010 15:3073-127 %REC 1101
MOISTURE E160.3 Analyst: SAYMethod:Percent Moisture n 12/28/2010 14:000.0100 wt% 119.2 0.010
PH SW9045B Analyst: JBAMethod:pH 12/28/2010 08:000.100 pH Units 16.98 0.10
AR Page 2 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB3 (2-3)Collection Date: 12/21/2010 09:00 AM Matrix: SOIL
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-03
ALS Environmental Date: 30-Dec-10
SDL
TEXAS TPH TX1005 Analyst: SEPrep: TX1005PR / 12/22/10Method:nC6 to nC12 12/29/2010 00:1465 mg/Kg-dry 1U 21>nC12 to nC28 12/29/2010 00:1465 mg/Kg-dry 1U 21>nC28 to nC35 12/29/2010 00:1465 mg/Kg-dry 1U 21Total Petroleum Hydrocarbon 12/29/2010 00:1465 mg/Kg-dry 1U 21 Surr: 2-Fluorobiphenyl 12/29/2010 00:1470-130 %REC 1102
Surr: Trifluoromethyl benzene 12/29/2010 00:1470-130 %REC 1122
MERCURY SW7471A Analyst: JCJPrep: SW7471A / 12/22/10Method:Mercury 12/22/2010 22:064.54 µg/Kg-dry 112.6 0.27
METALS SW6020 Analyst: SKSPrep: SW3050A / 12/23/10Method:Arsenic 12/30/2010 12:440.651 mg/Kg-dry 14.32 0.078Barium 12/30/2010 12:440.651 mg/Kg-dry 1181 0.10Cadmium J 12/30/2010 12:440.651 mg/Kg-dry 10.230 0.052Chromium 12/30/2010 12:440.651 mg/Kg-dry 121.5 0.065Lead 12/30/2010 12:440.651 mg/Kg-dry 130.6 0.065Selenium 12/30/2010 12:440.651 mg/Kg-dry 11.20 0.33Silver J 12/30/2010 12:440.651 mg/Kg-dry 10.162 0.052
TCL VOLATILES SW8260 Analyst: WLRMethod:1,1,1-Trichloroethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000661,1,2,2-Tetrachloroethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000661,1,2-Trichlor-1,2,2-trifluoroethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000801,1,2-Trichloroethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00111,1-Dichloroethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000661,1-Dichloroethene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00111,2,4-Trichlorobenzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000931,2-Dibromo-3-chloropropane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00251,2-Dibromoethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000661,2-Dichlorobenzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000661,2-Dichloroethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000661,2-Dichloropropane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000931,3-Dichlorobenzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000661,4-Dichlorobenzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.000662-Butanone 12/28/2010 15:580.013 mg/Kg-dry 1U 0.00252-Hexanone 12/28/2010 15:580.013 mg/Kg-dry 1U 0.00154-Methyl-2-pentanone 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0013Acetone 12/28/2010 15:580.033 mg/Kg-dry 1U 0.0066Benzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Bromodichloromethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066
AR Page 3 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB3 (2-3)Collection Date: 12/21/2010 09:00 AM Matrix: SOIL
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-03
ALS Environmental Date: 30-Dec-10
SDL
Bromoform 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0011Bromomethane 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0013Carbon disulfide 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0013Carbon tetrachloride 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Chlorobenzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Chloroethane 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0013Chloroform 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Chloromethane 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0013cis-1,2-Dichloroethene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00080cis-1,3-Dichloropropene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Cyclohexane n 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Dibromochloromethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00080Dichlorodifluoromethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.0011Dichloromethane 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0019Ethylbenzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Isopropylbenzene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066m,p-Xylene 12/28/2010 15:580.013 mg/Kg-dry 1U 0.0013Methyl acetate 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.0016Methyl tert-butyl ether 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Methylcyclohexane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00080o-Xylene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Styrene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Tetrachloroethene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00080Toluene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066trans-1,2-Dichloroethene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066trans-1,3-Dichloropropene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Trichloroethene 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Trichlorofluoromethane 12/28/2010 15:580.0066 mg/Kg-dry 1U 0.00066Vinyl chloride 12/28/2010 15:580.0027 mg/Kg-dry 1U 0.0013Xylenes, Total 12/28/2010 15:580.020 mg/Kg-dry 1U 0.0013 Surr: 1,2-Dichloroethane-d4 12/28/2010 15:5870-128 %REC 197.5
Surr: 4-Bromofluorobenzene 12/28/2010 15:5873-126 %REC 199.1
Surr: Dibromofluoromethane 12/28/2010 15:5871-128 %REC 1100
Surr: Toluene-d8 12/28/2010 15:5873-127 %REC 198.4
MOISTURE E160.3 Analyst: SAYMethod:Percent Moisture n 12/28/2010 14:000.0100 wt% 124.7 0.010
AR Page 4 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB1 (2-3)Collection Date: 12/21/2010 10:15 AM Matrix: SOIL
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-05
ALS Environmental Date: 30-Dec-10
SDL
TEXAS TPH TX1005 Analyst: SEPrep: TX1005PR / 12/22/10Method:nC6 to nC12 12/29/2010 00:4559 mg/Kg-dry 1U 19>nC12 to nC28 12/29/2010 00:4559 mg/Kg-dry 1U 19>nC28 to nC35 12/29/2010 00:4559 mg/Kg-dry 1U 19Total Petroleum Hydrocarbon 12/29/2010 00:4559 mg/Kg-dry 1U 19 Surr: 2-Fluorobiphenyl 12/29/2010 00:4570-130 %REC 199.8
Surr: Trifluoromethyl benzene 12/29/2010 00:4570-130 %REC 1122
MERCURY SW7471A Analyst: JCJPrep: SW7471A / 12/22/10Method:Mercury 12/22/2010 22:084.13 µg/Kg-dry 123.2 0.25
METALS SW6020 Analyst: SKSPrep: SW3050A / 12/23/10Method:Arsenic 12/30/2010 12:500.535 mg/Kg-dry 14.60 0.064Barium 12/30/2010 12:500.535 mg/Kg-dry 1190 0.086Cadmium J 12/30/2010 12:500.535 mg/Kg-dry 10.219 0.043Chromium 12/30/2010 12:500.535 mg/Kg-dry 121.6 0.053Lead 12/30/2010 12:500.535 mg/Kg-dry 161.2 0.053Selenium 12/30/2010 12:500.535 mg/Kg-dry 10.736 0.27Silver J 12/30/2010 12:500.535 mg/Kg-dry 10.120 0.043
TCL VOLATILES SW8260 Analyst: WLRMethod:1,1,1-Trichloroethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000591,1,2,2-Tetrachloroethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000591,1,2-Trichlor-1,2,2-trifluoroethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000711,1,2-Trichloroethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000941,1-Dichloroethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000591,1-Dichloroethene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000941,2,4-Trichlorobenzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000821,2-Dibromo-3-chloropropane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00221,2-Dibromoethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000591,2-Dichlorobenzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000591,2-Dichloroethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000591,2-Dichloropropane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000821,3-Dichlorobenzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000591,4-Dichlorobenzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.000592-Butanone 12/28/2010 16:250.012 mg/Kg-dry 1U 0.00222-Hexanone 12/28/2010 16:250.012 mg/Kg-dry 1U 0.00134-Methyl-2-pentanone 12/28/2010 16:250.012 mg/Kg-dry 1U 0.0012Acetone 12/28/2010 16:250.029 mg/Kg-dry 1U 0.0059Benzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Bromodichloromethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059
AR Page 5 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB1 (2-3)Collection Date: 12/21/2010 10:15 AM Matrix: SOIL
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-05
ALS Environmental Date: 30-Dec-10
SDL
Bromoform 12/28/2010 16:250.012 mg/Kg-dry 1U 0.00094Bromomethane 12/28/2010 16:250.012 mg/Kg-dry 1U 0.0012Carbon disulfide 12/28/2010 16:250.012 mg/Kg-dry 1U 0.0012Carbon tetrachloride 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Chlorobenzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Chloroethane 12/28/2010 16:250.012 mg/Kg-dry 1U 0.0012Chloroform 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Chloromethane 12/28/2010 16:250.012 mg/Kg-dry 1U 0.0012cis-1,2-Dichloroethene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00071cis-1,3-Dichloropropene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Cyclohexane n 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Dibromochloromethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00071Dichlorodifluoromethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00094Dichloromethane 12/28/2010 16:250.012 mg/Kg-dry 1U 0.0016Ethylbenzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Isopropylbenzene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059m,p-Xylene 12/28/2010 16:250.012 mg/Kg-dry 1U 0.0012Methyl acetate 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.0014Methyl tert-butyl ether 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Methylcyclohexane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00071o-Xylene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Styrene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Tetrachloroethene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00071Toluene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059trans-1,2-Dichloroethene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059trans-1,3-Dichloropropene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Trichloroethene 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Trichlorofluoromethane 12/28/2010 16:250.0059 mg/Kg-dry 1U 0.00059Vinyl chloride 12/28/2010 16:250.0024 mg/Kg-dry 1U 0.0012Xylenes, Total 12/28/2010 16:250.018 mg/Kg-dry 1U 0.0012 Surr: 1,2-Dichloroethane-d4 12/28/2010 16:2570-128 %REC 1103
Surr: 4-Bromofluorobenzene 12/28/2010 16:2573-126 %REC 198.3
Surr: Dibromofluoromethane 12/28/2010 16:2571-128 %REC 1101
Surr: Toluene-d8 12/28/2010 16:2573-127 %REC 199.5
MOISTURE E160.3 Analyst: SAYMethod:Percent Moisture n 12/28/2010 14:000.0100 wt% 115.0 0.010
AR Page 6 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB1Collection Date: 12/21/2010 10:45 AM Matrix: WATER
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-07
ALS Environmental Date: 30-Dec-10
SDL
LOW-LEVEL TEXAS TPH TX1005 Analyst: SEPrep: TX1005PR / 12/22/10Method:nC6 to nC12 12/28/2010 18:330.46 mg/L 1U 0.18>nC12 to nC28 12/28/2010 18:330.46 mg/L 1U 0.18>nC28 to nC35 12/28/2010 18:330.46 mg/L 1U 0.18Total Petroleum Hydrocarbon 12/28/2010 18:330.46 mg/L 1U 0.18 Surr: 2-Fluorobiphenyl 12/28/2010 18:3370-130 %REC 193.8
Surr: Trifluoromethyl benzene 12/28/2010 18:3370-130 %REC 1115
DISSOLVED MERCURY SW7470 Analyst: JCJPrep: SW7470 / 12/28/10Method:Mercury 12/28/2010 17:270.000200 mg/L 1U 0.000042
DISSOLVED METALS SW6020 Analyst: ALRPrep: SW3010A / 12/23/10Method:Arsenic J 12/29/2010 06:440.00500 mg/L 10.00134 0.00090Barium 12/29/2010 06:440.00500 mg/L 10.0787 0.00070Cadmium 12/29/2010 06:440.00100 mg/L 1U 0.00060Chromium J 12/29/2010 06:440.00200 mg/L 10.00148 0.00060Lead J 12/29/2010 06:440.00500 mg/L 10.000830 0.00040Selenium 12/29/2010 06:440.00500 mg/L 1U 0.0025Silver 12/29/2010 06:440.00500 mg/L 1U 0.00070
TCL VOLATILES SW8260 Analyst: PCMethod:1,1,1-Trichloroethane 12/24/2010 16:225.0 µg/L 1U 0.501,1,2,2-Tetrachloroethane 12/24/2010 16:225.0 µg/L 1U 0.501,1,2-Trichlor-1,2,2-trifluoroethane 12/24/2010 16:225.0 µg/L 1U 0.601,1,2-Trichloroethane 12/24/2010 16:225.0 µg/L 1U 0.501,1-Dichloroethane 12/24/2010 16:225.0 µg/L 1U 0.501,1-Dichloroethene 12/24/2010 16:225.0 µg/L 1U 0.501,2,4-Trichlorobenzene 12/24/2010 16:225.0 µg/L 1U 0.501,2-Dibromo-3-chloropropane 12/24/2010 16:225.0 µg/L 1U 1.01,2-Dibromoethane 12/24/2010 16:225.0 µg/L 1U 0.501,2-Dichlorobenzene 12/24/2010 16:225.0 µg/L 1U 0.501,2-Dichloroethane 12/24/2010 16:225.0 µg/L 1U 0.501,2-Dichloropropane 12/24/2010 16:225.0 µg/L 1U 0.501,3-Dichlorobenzene 12/24/2010 16:225.0 µg/L 1U 0.501,4-Dichlorobenzene 12/24/2010 16:225.0 µg/L 1U 0.502-Butanone 12/24/2010 16:2210 µg/L 1U 0.802-Hexanone 12/24/2010 16:2210 µg/L 1U 1.04-Methyl-2-pentanone 12/24/2010 16:2210 µg/L 1U 1.0Acetone 12/24/2010 16:2210 µg/L 1U 1.0Benzene 12/24/2010 16:225.0 µg/L 1U 0.50Bromodichloromethane 12/24/2010 16:225.0 µg/L 1U 0.50
AR Page 7 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB1Collection Date: 12/21/2010 10:45 AM Matrix: WATER
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-07
ALS Environmental Date: 30-Dec-10
SDL
Bromoform 12/24/2010 16:225.0 µg/L 1U 0.50Bromomethane 12/24/2010 16:225.0 µg/L 1U 0.90Carbon disulfide 12/24/2010 16:2210 µg/L 1U 1.0Carbon tetrachloride 12/24/2010 16:225.0 µg/L 1U 0.50Chlorobenzene 12/24/2010 16:225.0 µg/L 1U 0.50Chloroethane 12/24/2010 16:225.0 µg/L 1U 0.50Chloroform 12/24/2010 16:225.0 µg/L 1U 0.50Chloromethane 12/24/2010 16:225.0 µg/L 1U 0.50cis-1,2-Dichloroethene 12/24/2010 16:225.0 µg/L 1U 0.50cis-1,3-Dichloropropene 12/24/2010 16:225.0 µg/L 1U 0.50Cyclohexane n 12/24/2010 16:225.0 µg/L 1U 0.60Dibromochloromethane 12/24/2010 16:225.0 µg/L 1U 0.50Dichlorodifluoromethane 12/24/2010 16:225.0 µg/L 1U 0.50Dichloromethane 12/24/2010 16:2210 µg/L 1U 0.50Ethylbenzene 12/24/2010 16:225.0 µg/L 1U 0.50Isopropylbenzene 12/24/2010 16:225.0 µg/L 1U 0.50m,p-Xylene 12/24/2010 16:2210 µg/L 1U 1.0Methyl acetate 12/24/2010 16:225.0 µg/L 1U 0.50Methyl tert-butyl ether 12/24/2010 16:225.0 µg/L 1U 0.50Methylcyclohexane 12/24/2010 16:225.0 µg/L 1U 0.80o-Xylene 12/24/2010 16:225.0 µg/L 1U 0.50Styrene 12/24/2010 16:225.0 µg/L 1U 0.50Tetrachloroethene 12/24/2010 16:225.0 µg/L 1U 0.60Toluene 12/24/2010 16:225.0 µg/L 1U 0.50trans-1,2-Dichloroethene 12/24/2010 16:225.0 µg/L 1U 0.50trans-1,3-Dichloropropene 12/24/2010 16:225.0 µg/L 1U 0.50Trichloroethene 12/24/2010 16:225.0 µg/L 1U 0.50Trichlorofluoromethane 12/24/2010 16:225.0 µg/L 1U 0.50Vinyl chloride 12/24/2010 16:222.0 µg/L 1U 0.50Xylenes, Total 12/24/2010 16:2215 µg/L 1U 1.0 Surr: 1,2-Dichloroethane-d4 12/24/2010 16:2270-125 %REC 1102
Surr: 4-Bromofluorobenzene 12/24/2010 16:2272-125 %REC 196.6
Surr: Dibromofluoromethane 12/24/2010 16:2271-125 %REC 1100
Surr: Toluene-d8 12/24/2010 16:2275-125 %REC 1100
AR Page 8 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB2Collection Date: 12/21/2010 08:45 AM Matrix: WATER
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-08
ALS Environmental Date: 30-Dec-10
SDL
LOW-LEVEL TEXAS TPH TX1005 Analyst: SEPrep: TX1005PR / 12/22/10Method:nC6 to nC12 12/28/2010 19:040.47 mg/L 1U 0.19>nC12 to nC28 12/28/2010 19:040.47 mg/L 1U 0.19>nC28 to nC35 12/28/2010 19:040.47 mg/L 1U 0.19Total Petroleum Hydrocarbon 12/28/2010 19:040.47 mg/L 1U 0.19 Surr: 2-Fluorobiphenyl 12/28/2010 19:0470-130 %REC 1106
Surr: Trifluoromethyl benzene 12/28/2010 19:0470-130 %REC 1129
MERCURY SW7470 Analyst: JCJPrep: SW7470 / 12/28/10Method:Mercury 12/28/2010 19:330.000200 mg/L 1U 0.000042
METALS SW6020 Analyst: ALRPrep: SW3010A / 12/22/10Method:Arsenic 12/24/2010 13:510.00500 mg/L 10.00502 0.00090Barium 12/24/2010 13:510.00500 mg/L 10.618 0.00070Cadmium 12/24/2010 13:510.00200 mg/L 1U 0.00060Chromium 12/24/2010 13:510.00500 mg/L 10.116 0.00060Lead 12/24/2010 13:510.00500 mg/L 10.0250 0.00040Selenium 12/24/2010 13:510.00500 mg/L 1U 0.0025Silver 12/24/2010 13:510.00500 mg/L 1U 0.00070
TCL VOLATILES SW8260 Analyst: PCMethod:1,1,1-Trichloroethane 12/24/2010 16:455.0 µg/L 1U 0.501,1,2,2-Tetrachloroethane 12/24/2010 16:455.0 µg/L 1U 0.501,1,2-Trichlor-1,2,2-trifluoroethane 12/24/2010 16:455.0 µg/L 1U 0.601,1,2-Trichloroethane 12/24/2010 16:455.0 µg/L 1U 0.501,1-Dichloroethane 12/24/2010 16:455.0 µg/L 1U 0.501,1-Dichloroethene 12/24/2010 16:455.0 µg/L 1U 0.501,2,4-Trichlorobenzene 12/24/2010 16:455.0 µg/L 1U 0.501,2-Dibromo-3-chloropropane 12/24/2010 16:455.0 µg/L 1U 1.01,2-Dibromoethane 12/24/2010 16:455.0 µg/L 1U 0.501,2-Dichlorobenzene 12/24/2010 16:455.0 µg/L 1U 0.501,2-Dichloroethane 12/24/2010 16:455.0 µg/L 1U 0.501,2-Dichloropropane 12/24/2010 16:455.0 µg/L 1U 0.501,3-Dichlorobenzene 12/24/2010 16:455.0 µg/L 1U 0.501,4-Dichlorobenzene 12/24/2010 16:455.0 µg/L 1U 0.502-Butanone 12/24/2010 16:4510 µg/L 1U 0.802-Hexanone 12/24/2010 16:4510 µg/L 1U 1.04-Methyl-2-pentanone 12/24/2010 16:4510 µg/L 1U 1.0Acetone 12/24/2010 16:4510 µg/L 1U 1.0Benzene 12/24/2010 16:455.0 µg/L 1U 0.50Bromodichloromethane 12/24/2010 16:455.0 µg/L 1U 0.50
AR Page 9 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB2Collection Date: 12/21/2010 08:45 AM Matrix: WATER
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-08
ALS Environmental Date: 30-Dec-10
SDL
Bromoform 12/24/2010 16:455.0 µg/L 1U 0.50Bromomethane 12/24/2010 16:455.0 µg/L 1U 0.90Carbon disulfide 12/24/2010 16:4510 µg/L 1U 1.0Carbon tetrachloride 12/24/2010 16:455.0 µg/L 1U 0.50Chlorobenzene 12/24/2010 16:455.0 µg/L 1U 0.50Chloroethane 12/24/2010 16:455.0 µg/L 1U 0.50Chloroform 12/24/2010 16:455.0 µg/L 1U 0.50Chloromethane 12/24/2010 16:455.0 µg/L 1U 0.50cis-1,2-Dichloroethene 12/24/2010 16:455.0 µg/L 1U 0.50cis-1,3-Dichloropropene 12/24/2010 16:455.0 µg/L 1U 0.50Cyclohexane n 12/24/2010 16:455.0 µg/L 1U 0.60Dibromochloromethane 12/24/2010 16:455.0 µg/L 1U 0.50Dichlorodifluoromethane 12/24/2010 16:455.0 µg/L 1U 0.50Dichloromethane 12/24/2010 16:4510 µg/L 1U 0.50Ethylbenzene 12/24/2010 16:455.0 µg/L 1U 0.50Isopropylbenzene 12/24/2010 16:455.0 µg/L 1U 0.50m,p-Xylene 12/24/2010 16:4510 µg/L 1U 1.0Methyl acetate 12/24/2010 16:455.0 µg/L 1U 0.50Methyl tert-butyl ether 12/24/2010 16:455.0 µg/L 1U 0.50Methylcyclohexane 12/24/2010 16:455.0 µg/L 1U 0.80o-Xylene 12/24/2010 16:455.0 µg/L 1U 0.50Styrene 12/24/2010 16:455.0 µg/L 1U 0.50Tetrachloroethene 12/24/2010 16:455.0 µg/L 1U 0.60Toluene 12/24/2010 16:455.0 µg/L 1U 0.50trans-1,2-Dichloroethene 12/24/2010 16:455.0 µg/L 1U 0.50trans-1,3-Dichloropropene 12/24/2010 16:455.0 µg/L 1U 0.50Trichloroethene 12/24/2010 16:455.0 µg/L 1U 0.50Trichlorofluoromethane 12/24/2010 16:455.0 µg/L 1U 0.50Vinyl chloride 12/24/2010 16:452.0 µg/L 1U 0.50Xylenes, Total 12/24/2010 16:4515 µg/L 1U 1.0 Surr: 1,2-Dichloroethane-d4 12/24/2010 16:4570-125 %REC 1104
Surr: 4-Bromofluorobenzene 12/24/2010 16:4572-125 %REC 196.2
Surr: Dibromofluoromethane 12/24/2010 16:4571-125 %REC 199.9
Surr: Toluene-d8 12/24/2010 16:4575-125 %REC 1101
AR Page 10 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB3Collection Date: 12/21/2010 09:45 AM Matrix: WATER
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-09
ALS Environmental Date: 30-Dec-10
SDL
LOW-LEVEL TEXAS TPH TX1005 Analyst: SEPrep: TX1005PR / 12/22/10Method:nC6 to nC12 12/28/2010 19:350.48 mg/L 1U 0.19>nC12 to nC28 12/28/2010 19:350.48 mg/L 1U 0.19>nC28 to nC35 12/28/2010 19:350.48 mg/L 1U 0.19Total Petroleum Hydrocarbon 12/28/2010 19:350.48 mg/L 1U 0.19 Surr: 2-Fluorobiphenyl 12/28/2010 19:3570-130 %REC 1103
Surr: Trifluoromethyl benzene 12/28/2010 19:3570-130 %REC 1123
DISSOLVED MERCURY SW7470 Analyst: JCJPrep: SW7470 / 12/28/10Method:Mercury 12/28/2010 17:290.000200 mg/L 1U 0.000042
DISSOLVED METALS SW6020 Analyst: ALRPrep: SW3010A / 12/23/10Method:Arsenic J 12/29/2010 06:500.00500 mg/L 10.00159 0.00090Barium 12/29/2010 06:500.00500 mg/L 10.150 0.00070Cadmium 12/29/2010 06:500.00100 mg/L 1U 0.00060Chromium J 12/29/2010 06:500.00200 mg/L 10.00181 0.00060Lead J 12/29/2010 06:500.00500 mg/L 10.000865 0.00040Selenium 12/29/2010 06:500.00500 mg/L 1U 0.0025Silver 12/29/2010 06:500.00500 mg/L 1U 0.00070
TCL VOLATILES SW8260 Analyst: PCMethod:1,1,1-Trichloroethane 12/24/2010 17:095.0 µg/L 1U 0.501,1,2,2-Tetrachloroethane 12/24/2010 17:095.0 µg/L 1U 0.501,1,2-Trichlor-1,2,2-trifluoroethane 12/24/2010 17:095.0 µg/L 1U 0.601,1,2-Trichloroethane 12/24/2010 17:095.0 µg/L 1U 0.501,1-Dichloroethane 12/24/2010 17:095.0 µg/L 1U 0.501,1-Dichloroethene 12/24/2010 17:095.0 µg/L 1U 0.501,2,4-Trichlorobenzene 12/24/2010 17:095.0 µg/L 1U 0.501,2-Dibromo-3-chloropropane 12/24/2010 17:095.0 µg/L 1U 1.01,2-Dibromoethane 12/24/2010 17:095.0 µg/L 1U 0.501,2-Dichlorobenzene 12/24/2010 17:095.0 µg/L 1U 0.501,2-Dichloroethane 12/24/2010 17:095.0 µg/L 1U 0.501,2-Dichloropropane 12/24/2010 17:095.0 µg/L 1U 0.501,3-Dichlorobenzene 12/24/2010 17:095.0 µg/L 1U 0.501,4-Dichlorobenzene 12/24/2010 17:095.0 µg/L 1U 0.502-Butanone 12/24/2010 17:0910 µg/L 1U 0.802-Hexanone 12/24/2010 17:0910 µg/L 1U 1.04-Methyl-2-pentanone 12/24/2010 17:0910 µg/L 1U 1.0Acetone 12/24/2010 17:0910 µg/L 1U 1.0Benzene 12/24/2010 17:095.0 µg/L 1U 0.50Bromodichloromethane 12/24/2010 17:095.0 µg/L 1U 0.50
AR Page 11 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Project: Holiday PlaceSample ID: TSB3Collection Date: 12/21/2010 09:45 AM Matrix: WATER
Analyses Result Qual Units Date Analyzed MQL
Client: TGE Resources Inc.Work Order: 1012696
Dilution Factor
Lab ID: 1012696-09
ALS Environmental Date: 30-Dec-10
SDL
Bromoform 12/24/2010 17:095.0 µg/L 1U 0.50Bromomethane 12/24/2010 17:095.0 µg/L 1U 0.90Carbon disulfide 12/24/2010 17:0910 µg/L 1U 1.0Carbon tetrachloride 12/24/2010 17:095.0 µg/L 1U 0.50Chlorobenzene 12/24/2010 17:095.0 µg/L 1U 0.50Chloroethane 12/24/2010 17:095.0 µg/L 1U 0.50Chloroform 12/24/2010 17:095.0 µg/L 1U 0.50Chloromethane 12/24/2010 17:095.0 µg/L 1U 0.50cis-1,2-Dichloroethene 12/24/2010 17:095.0 µg/L 1U 0.50cis-1,3-Dichloropropene 12/24/2010 17:095.0 µg/L 1U 0.50Cyclohexane n 12/24/2010 17:095.0 µg/L 1U 0.60Dibromochloromethane 12/24/2010 17:095.0 µg/L 1U 0.50Dichlorodifluoromethane 12/24/2010 17:095.0 µg/L 1U 0.50Dichloromethane 12/24/2010 17:0910 µg/L 1U 0.50Ethylbenzene 12/24/2010 17:095.0 µg/L 1U 0.50Isopropylbenzene 12/24/2010 17:095.0 µg/L 1U 0.50m,p-Xylene 12/24/2010 17:0910 µg/L 1U 1.0Methyl acetate 12/24/2010 17:095.0 µg/L 1U 0.50Methyl tert-butyl ether 12/24/2010 17:095.0 µg/L 1U 0.50Methylcyclohexane 12/24/2010 17:095.0 µg/L 1U 0.80o-Xylene 12/24/2010 17:095.0 µg/L 1U 0.50Styrene 12/24/2010 17:095.0 µg/L 1U 0.50Tetrachloroethene 12/24/2010 17:095.0 µg/L 1U 0.60Toluene 12/24/2010 17:095.0 µg/L 1U 0.50trans-1,2-Dichloroethene 12/24/2010 17:095.0 µg/L 1U 0.50trans-1,3-Dichloropropene 12/24/2010 17:095.0 µg/L 1U 0.50Trichloroethene 12/24/2010 17:095.0 µg/L 1U 0.50Trichlorofluoromethane 12/24/2010 17:095.0 µg/L 1U 0.50Vinyl chloride 12/24/2010 17:092.0 µg/L 1U 0.50Xylenes, Total 12/24/2010 17:0915 µg/L 1U 1.0 Surr: 1,2-Dichloroethane-d4 12/24/2010 17:0970-125 %REC 1103
Surr: 4-Bromofluorobenzene 12/24/2010 17:0972-125 %REC 197.2
Surr: Dibromofluoromethane 12/24/2010 17:0971-125 %REC 198.6
Surr: Toluene-d8 12/24/2010 17:0975-125 %REC 1102
AR Page 12 of 12
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Date: 30-Dec-10ALS Environmental
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48907 Instrument ID FID-10 Method: TX1005
QualRPD Limit
Analysis Date: 12/23/2010 10:53 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2227266
MBLK
Run ID: FID-10_101222B
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: FBLKW1-101222-48907
nC6 to nC12 0.50U>nC12 to nC28 0.50U>nC28 to nC35 0.50UTotal Petroleum Hydrocarbon 0.50U
002.5 Surr: 2-Fluorobiphenyl 93.4 70-13002.336
002.5 Surr: Trifluoromethyl benzene 104 70-13002.594
QualRPD Limit
Analysis Date: 12/23/2010 09:50 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2227264
LCS
Run ID: FID-10_101222B
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: FLCSW1-101222-48907
0025nC6 to nC12 92 75-1250.5022.990025>nC12 to nC28 104 75-1250.5026.1002.5 Surr: 2-Fluorobiphenyl 116 70-13002.893
002.5 Surr: Trifluoromethyl benzene 96.8 70-13002.42
QualRPD Limit
Analysis Date: 12/23/2010 10:21 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2227265
LCSD
Run ID: FID-10_101222B
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: FLCSDW1-101222-48907
22.99025nC6 to nC12 97.6 75-125 200.50 5.9524.426.1025>nC12 to nC28 108 75-125 200.50 3.3126.98
2.89302.5 Surr: 2-Fluorobiphenyl 122 70-130 200 5.193.047
2.4202.5 Surr: Trifluoromethyl benzene 101 70-130 200 4.672.535
QualRPD Limit
Analysis Date: 12/23/2010 11:57 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2227268
MS
Run ID: FID-10_101222B
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012256-01BMS
01.77223.89nC6 to nC12 96.1 75-1250.4824.7400.349823.89>nC12 to nC28 111 75-1250.4826.76002.389 Surr: 2-Fluorobiphenyl 122 70-13002.914
002.389 Surr: Trifluoromethyl benzene 97.8 70-13002.338
QC Page: 1 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48907 Instrument ID FID-10 Method: TX1005
QualRPD Limit
Analysis Date: 12/23/2010 12:28 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2227269
MSD
Run ID: FID-10_101222B
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012256-01BMSD
24.741.77224.19nC6 to nC12 99.9 75-125 200.48 4.7725.9526.760.349824.19>nC12 to nC28 108 75-125 200.48 0.79926.542.91402.419 Surr: 2-Fluorobiphenyl 121 70-130 200 0.6442.932
2.33802.419 Surr: Trifluoromethyl benzene 99.3 70-130 200 2.72.402
The following samples were analyzed in this batch: 1012696-07B 1012696-08B 1012696-09B
QC Page: 2 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48930 Instrument ID FID-13 Method: TX1005
QualRPD Limit
Analysis Date: 12/28/2010 03:11 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2229813
MBLK
Run ID: FID-13_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: FBLKS1-101222-48930
nC6 to nC12 50U>nC12 to nC28 50U>nC28 to nC35 50UTotal Petroleum Hydrocarbon 50U
0025 Surr: 2-Fluorobiphenyl 90.9 70-130022.73
0025 Surr: Trifluoromethyl benzene 94.8 70-130023.69
QualRPD Limit
Analysis Date: 12/28/2010 02:07 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2229811
LCS
Run ID: FID-13_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: FLCSS1-101222-48930
00250nC6 to nC12 90.3 75-12550225.800250>nC12 to nC28 99.5 75-12550248.90025 Surr: 2-Fluorobiphenyl 114 70-130028.5
0025 Surr: Trifluoromethyl benzene 105 70-130026.2
QualRPD Limit
Analysis Date: 12/28/2010 02:39 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2229812
LCSD
Run ID: FID-13_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: FLCSDS1-101222-48930
225.80250nC6 to nC12 89.2 75-125 2050 1.27223248.90250>nC12 to nC28 103 75-125 2050 3.86258.728.5025 Surr: 2-Fluorobiphenyl 106 70-130 200 7.3826.47
26.2025 Surr: Trifluoromethyl benzene 92.7 70-130 200 12.323.16
QualRPD Limit
Analysis Date: 12/29/2010 01:47 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2231185
MS
Run ID: FID-13_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012622-01BMS
096.91246.3nC6 to nC12 120 75-12549392.2S0719246.3>nC12 to nC28 173 75-125491145
0024.63 Surr: 2-Fluorobiphenyl 123 70-130030.27
0024.63 Surr: Trifluoromethyl benzene 99.5 70-130024.51
QC Page: 3 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48930 Instrument ID FID-13 Method: TX1005
QualRPD Limit
Analysis Date: 12/29/2010 02:18 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2231190
MSD
Run ID: FID-13_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012622-01BMSD
392.296.91246.5nC6 to nC12 112 75-125 2049 4.89373.5S1145719246.5>nC12 to nC28 150 75-125 2049 5.051089
30.27024.65 Surr: 2-Fluorobiphenyl 120 70-130 200 2.6329.48
24.51024.65 Surr: Trifluoromethyl benzene 99.1 70-130 200 0.30824.43
The following samples were analyzed in this batch: 1012696-01B 1012696-03B 1012696-05B
QC Page: 4 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48920 Instrument ID ICPMS03 Method: SW6020
QualRPD Limit
Analysis Date: 12/24/2010 11:07 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2229542
MBLK
Run ID: ICPMS03_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: MBLKW5-122210-48920
Arsenic 0.0050UBarium 0.0050UCadmium 0.0020UChromium 0.0050ULead 0.0050USelenium 0.0050USilver 0.0050U
QualRPD Limit
Analysis Date: 12/24/2010 11:12 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2229544
LCS
Run ID: ICPMS03_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: MLCSW5-122210-48920
000.05Arsenic 97 80-1200.00500.04848000.125Barium 96.3 80-1200.00500.1204000.05Cadmium 93.3 80-1200.00200.04664000.05Chromium 91.5 80-1200.00500.04575000.05Lead 91.6 80-1200.00500.04578000.05Selenium 98.3 80-1200.00500.04913000.05Silver 91.7 80-1200.00500.04586
QualRPD Limit
Analysis Date: 12/24/2010 11:38 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2229550
MS
Run ID: ICPMS03_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012710-07CMS
00.0016440.05Arsenic 94 80-1200.00500.04863SEO02.8320.125Barium 122 80-1200.00502.985
00.0010220.05Cadmium 92.7 80-1200.00200.04737000.05Chromium 83.7 80-1200.00500.04183000.05Lead 93.6 80-1200.00500.04682000.05Selenium 90.7 80-1200.00500.04535
S000.05Silver 78.4 80-1200.00500.0392
QC Page: 5 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48920 Instrument ID ICPMS03 Method: SW6020
QualRPD Limit
Analysis Date: 12/24/2010 11:44 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2229551
MSD
Run ID: ICPMS03_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012710-07CMSD
0.048630.0016440.05Arsenic 96 80-120 150.0050 2.040.04963SEO2.9852.8320.125Barium 171 80-120 150.0050 2.023.046
0.047370.0010220.05Cadmium 96.3 80-120 150.0020 3.710.049160.0418300.05Chromium 86.1 80-120 150.0050 2.850.043040.0468200.05Lead 97.2 80-120 150.0050 3.730.04860.0453500.05Selenium 91.6 80-120 150.0050 0.9660.045790.039200.05Silver 83.3 80-120 150.0050 6.110.04167
QualRPD Limit
Analysis Date: 12/24/2010 11:28 AM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2229548
DUP
Run ID: ICPMS03_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012710-07CDUP
J0.00164400Arsenic 0 0-0 250.0050 00.001656J0.00102200Cadmium 0 0-0 250.0020 00.0009859
0.000464200Chromium 0 0-0 250.0050 0U0.000265800Lead 0 0-0 250.0050 0U0.000788400Selenium 0 0-0 250.0050 0U
-0.000064700Silver 0 0-0 250.0050 0U
QualRPD Limit
Analysis Date: 12/28/2010 08:23 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230570
DUP
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 50
Sample ID: 1012710-07CDUP
2.95200Barium 0 0-0 250.25 8.372.714
QualRPD Limit
Analysis Date: 12/24/2010 11:49 AM
Prep Date:
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2229553
PDS
Run ID: ICPMS03_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012710-07CBS
00.0016440.1Arsenic 87.9 75-1250.00500.0895200.0010220.1Cadmium 90 75-1250.00200.09100.00046420.1Chromium 82.6 75-1250.00500.0830300.00026580.1Lead 92.2 75-1250.00500.092500.00078840.1Selenium 87 75-1250.00500.087740-0.00006470.1Silver 75.5 75-1250.00500.07541
QC Page: 6 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48920 Instrument ID ICPMS03 Method: SW6020
QualRPD Limit
Analysis Date: 12/28/2010 08:33 PM
Prep Date:
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230575
PDS
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 50
Sample ID: 1012710-07CBS
02.9525Barium 98.2 75-1250.257.86
Qual %D Limit
Analysis Date: 12/24/2010 11:33 AM
Prep Date:
Analyte Result %REC %D
Units: mg/L
MQL
Client ID: SeqNo: 2229549
SD
Run ID: ICPMS03_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 5
Sample ID: 1012710-07C DIL SX
0.00164400Arsenic 0 0-0 100.025 0U0.00102200Cadmium 0 0-0 100.010 0U
0.000464200Chromium 0 0-0 100.025 0U0.000265800Lead 0 0-0 100.025 0U0.000788400Selenium 0 0-0 100.025 0U
-0.000064700Silver 0 0-0 100.025 0U
Qual %D Limit
Analysis Date: 12/28/2010 08:28 PM
Prep Date:
Analyte Result %REC %D
Units: mg/L
MQL
Client ID: SeqNo: 2230572
SD
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 250
Sample ID: 1012710-07C DIL SX
2.95200Barium 0 0-0 101.2 4.462.82
The following samples were analyzed in this batch: 1012696-08C
QC Page: 7 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48921 Instrument ID HG02 Method: SW7471A
QualRPD Limit
Analysis Date: 12/22/2010 09:14 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2226416
MBLK
Run ID: HG02_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: GBLKS5-122210-48921
Mercury 3.3U
QualRPD Limit
Analysis Date: 12/22/2010 09:16 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2226417
LCS
Run ID: HG02_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: GLCSS5-122210-48921
00333.3Mercury 98.8 85-1153.3329.3
QualRPD Limit
Analysis Date: 12/22/2010 09:22 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2226420
MS
Run ID: HG02_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-04CMS
045.33339.6Mercury 85.3 85-1153.4334.8
QualRPD Limit
Analysis Date: 12/22/2010 09:24 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2226421
MSD
Run ID: HG02_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-04CMSD
334.845.33349.6Mercury 85.6 85-115 203.5 2.93344.8
QualRPD Limit
Analysis Date: 12/22/2010 09:20 PM
Prep Date: 12/22/2010
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2226419
DUP
Run ID: HG02_101222A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-04CDUP
45.3300Mercury 0 203.5 3.8847.12
The following samples were analyzed in this batch: 1012696-01B 1012696-03B 1012696-05B
QC Page: 8 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48947 Instrument ID ICPMS03 Method: SW6020 (Dissolve)
QualRPD Limit
Analysis Date: 12/29/2010 02:34 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2231057
MBLK
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: MBLKW4-122310-48947
Arsenic 0.0050UBarium 0.0050UCadmium 0.0020UChromium 0.0050ULead 0.0050USelenium 0.0050USilver 0.0050U
QualRPD Limit
Analysis Date: 12/29/2010 02:40 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2231058
LCS
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: MLCSW4-122310-48947
000.05Arsenic 95.6 80-1200.00500.0478000.05Barium 107 80-1200.00500.05368000.05Cadmium 98 80-1200.00200.04899000.05Chromium 91.4 80-1200.00500.0457000.05Lead 99.7 80-1200.00500.04985000.05Selenium 97.4 80-1200.00500.04872000.05Silver 97.8 80-1200.00500.0489
QualRPD Limit
Analysis Date: 12/29/2010 03:01 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2231062
MS
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012490-11CMS
00.030710.05Arsenic 104 75-1250.00500.08276SO00.91690.05Barium 159 75-1250.00500.9965
0-0.00019630.05Cadmium 99.8 75-1250.00200.0496900.00022080.05Chromium 95.5 75-1250.00500.0479700.00015870.05Lead 103 75-1250.00500.0516900.00071080.05Selenium 102 75-1250.00500.051530-0.00023540.05Silver 98.9 75-1250.00500.0492
QC Page: 9 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48947 Instrument ID ICPMS03 Method: SW6020 (Dissolve)
QualRPD Limit
Analysis Date: 12/29/2010 03:06 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2231063
MSD
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012490-11CMSD
0.082760.030710.05Arsenic 102 75-125 250.0050 1.230.08175SO0.99650.91690.05Barium 133 75-125 250.0050 1.340.9832
0.04969-0.00019630.05Cadmium 98.9 75-125 250.0020 0.930.049230.047970.00022080.05Chromium 94.2 75-125 250.0050 1.320.047340.051690.00015870.05Lead 102 75-125 250.0050 0.8550.051250.051530.00071080.05Selenium 100 75-125 250.0050 1.170.050930.0492-0.00023540.05Silver 96.8 75-125 250.0050 2.180.04814
QualRPD Limit
Analysis Date: 12/29/2010 02:50 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2231060
DUP
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012490-11CDUP
0.0307100Arsenic 0 0-0 250.0050 0.09770.030680.916900Barium 0 0-0 250.0050 1.190.9279
-0.000196300Cadmium 0 0-0 250.0020 0U0.000220800Chromium 0 0-0 250.0050 0U0.000158700Lead 0 0-0 250.0050 0U0.000710800Selenium 0 0-0 250.0050 0U
-0.000235400Silver 0 0-0 250.0050 0U
QualRPD Limit
Analysis Date: 12/29/2010 03:11 AM
Prep Date:
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2231064
PDS
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012490-11CBS
00.030710.1Arsenic 92.7 75-1250.00500.1234SO00.91690.1Barium 66.5 75-1250.00500.9834
0-0.00019630.1Cadmium 92.4 75-1250.00200.092200.00022080.1Chromium 87.4 75-1250.00500.0876400.00015870.1Lead 94.2 75-1250.00500.0943800.00071080.1Selenium 94.7 75-1250.00500.095410-0.00023540.1Silver 96.9 75-1250.00500.09666
QC Page: 10 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48947 Instrument ID ICPMS03 Method: SW6020 (Dissolve)
Qual %D Limit
Analysis Date: 12/29/2010 02:56 AM
Prep Date:
Analyte Result %REC %D
Units: mg/L
MQL
Client ID: SeqNo: 2231061
SD
Run ID: ICPMS03_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 5
Sample ID: 1012490-11C DIL SX
0.0307100Arsenic 0 0-0 100.025 7.910.028280.916900Barium 0 0-0 100.025 1.30.905
-0.000196300Cadmium 0 0-0 100.010 0U0.000220800Chromium 0 0-0 100.025 0U0.000158700Lead 0 0-0 100.025 0U0.000710800Selenium 0 0-0 100.025 0U
-0.000235400Silver 0 0-0 100.025 0U
The following samples were analyzed in this batch: 1012696-07C 1012696-09C
QC Page: 11 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48948 Instrument ID ICPMS04 Method: SW6020
QualRPD Limit
Analysis Date: 12/30/2010 01:17 PM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2233458
MBLK
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: MBLKS1-122310-48948
Arsenic 0.50UJBarium 0.500.1452
Cadmium 0.50UChromium 0.50ULead 0.50USelenium 0.50USilver 0.50U
QualRPD Limit
Analysis Date: 12/30/2010 01:23 PM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2233459
LCS
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: MLCSS1-122310-48948
0010Arsenic 93 80-1200.509.2960010Barium 101 80-1200.5010.080010Cadmium 99.6 80-1200.509.9570010Chromium 97.3 80-1200.509.7290010Lead 102 80-1200.5010.210010Selenium 92.7 80-1200.509.2670010Silver 98.9 80-1200.509.891
QualRPD Limit
Analysis Date: 12/30/2010 03:17 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2232653
MS
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-04CMS
04.9799.259Arsenic 101 75-1250.4614.36SEO03879.259Barium 1160 75-1250.46493.9
00.0091519.259Cadmium 91.8 75-1250.468.50808.9899.259Chromium 116 75-1250.4619.6908.8919.259Lead 87.5 75-1250.4616.9900.51879.259Selenium 90.9 75-1250.468.9400.023119.259Silver 90.5 75-1250.468.403
QC Page: 12 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48948 Instrument ID ICPMS04 Method: SW6020
QualRPD Limit
Analysis Date: 12/30/2010 03:23 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2232654
MSD
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-04CMSD
14.364.9799.174Arsenic 106 75-125 250.46 2.0614.66SEO493.93879.174Barium 939 75-125 250.46 4.3473.1
8.5080.0091519.174Cadmium 91.6 75-125 250.46 1.138.41219.698.9899.174Chromium 106 75-125 250.46 5.1918.6916.998.8919.174Lead 99.6 75-125 250.46 5.9218.038.940.51879.174Selenium 91.4 75-125 250.46 0.3618.907
8.4030.023119.174Silver 90 75-125 250.46 1.528.276
QualRPD Limit
Analysis Date: 12/30/2010 03:11 AM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2232651
DUP
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-04CDUP
R4.97900Arsenic 0 0-0 250.47 25.36.420.00915100Cadmium 0 0-0 250.47 0U
8.98900Chromium 0 0-0 250.47 1210.138.89100Lead 0 0-0 250.47 17.710.62
0.518700Selenium 0 0-0 250.47 8.510.56480.0231100Silver 0 0-0 250.47 0U
QualRPD Limit
Analysis Date: 12/30/2010 02:40 PM
Prep Date: 12/23/2010
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2233620
DUP
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 100
Sample ID: 1012558-04CDUP
362.600Barium 0 0-0 2547 19.9442.5
QualRPD Limit
Analysis Date: 12/30/2010 03:29 AM
Prep Date:
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2232656
PDS
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-04CBS
04.9799.434Arsenic 94.8 75-1250.4713.9200.0091519.434Cadmium 91.3 75-1250.478.6208.9899.434Chromium 97.9 75-1250.4718.2308.8919.434Lead 90.3 75-1250.4717.4100.51879.434Selenium 94.8 75-1250.479.46500.023119.434Silver 95.8 75-1250.479.062
QC Page: 13 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48948 Instrument ID ICPMS04 Method: SW6020
QualRPD Limit
Analysis Date: 12/30/2010 02:46 PM
Prep Date:
Analyte Result %REC %RPD
Units: mg/Kg
MQL
Client ID: SeqNo: 2233621
PDS
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 100
Sample ID: 1012558-04CBS
0362.6943.4Barium 92.2 75-125471232
Qual %D Limit
Analysis Date: 12/30/2010 03:35 AM
Prep Date:
Analyte Result %REC %D
Units: mg/Kg
MQL
Client ID: SeqNo: 2232658
SD
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 5
Sample ID: 1012558-04C DIL SX
4.97900Arsenic 0 0-0 102.4 2.934.8330.00915100Cadmium 0 0-0 102.4 0U
8.98900Chromium 0 0-0 102.4 1.358.8688.89100Lead 0 0-0 102.4 3.569.208
0.518700Selenium 0 0-0 102.4 0U0.0231100Silver 0 0-0 102.4 0U
Qual %D Limit
Analysis Date: 12/30/2010 02:53 PM
Prep Date:
Analyte Result %REC %D
Units: mg/Kg
MQL
Client ID: SeqNo: 2233623
SD
Run ID: ICPMS04_101229A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 500
Sample ID: 1012558-04C DIL SX
362.600Barium 0 0-0 10240 3.32374.6
The following samples were analyzed in this batch: 1012696-01B 1012696-03B 1012696-05B
QC Page: 14 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48973 Instrument ID Mercury Method: SW7470 (Dissolve)
QualRPD Limit
Analysis Date: 12/28/2010 04:28 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230291
MBLK
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: GBLKW2-122810-48973
Mercury 0.00020U
QualRPD Limit
Analysis Date: 12/28/2010 04:30 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230292
LCS
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: GLCSW2-122810-48973
000.005Mercury 102 80-1200.000200.00511
QualRPD Limit
Analysis Date: 12/28/2010 04:36 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230295
MS
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012234-01CMS
00.0000110.005Mercury 88.2 80-1200.000200.00442
QualRPD Limit
Analysis Date: 12/28/2010 04:43 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230296
MSD
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012234-01CMSD
0.004420.0000110.005Mercury 90.8 80-120 200.00020 2.90.00455
QualRPD Limit
Analysis Date: 12/28/2010 04:34 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230294
DUP
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012234-01CDUP
0.00001100Mercury 0 0-0 200.00020 0U
The following samples were analyzed in this batch: 1012696-07C 1012696-09C
QC Page: 15 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: 48978 Instrument ID Mercury Method: SW7470
QualRPD Limit
Analysis Date: 12/28/2010 06:36 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230331
MBLK
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: GBLKW3-122810-48978
Mercury 0.00020U
QualRPD Limit
Analysis Date: 12/28/2010 06:38 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230332
LCS
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: GLCSW3-122810-48978
000.005Mercury 101 85-1150.000200.00504
QualRPD Limit
Analysis Date: 12/28/2010 06:44 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230336
MS
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-20DMS
00.0000380.005Mercury 100 85-1150.000200.00504
QualRPD Limit
Analysis Date: 12/28/2010 06:46 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230338
MSD
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-20DMSD
0.005040.0000380.005Mercury 103 85-115 200.00020 3.120.0052
QualRPD Limit
Analysis Date: 12/28/2010 06:42 PM
Prep Date: 12/28/2010
Analyte Result %REC %RPD
Units: mg/L
MQL
Client ID: SeqNo: 2230335
DUP
Run ID: MERCURY_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012558-20DDUP
0.00003800Mercury 0 0-0 200.00020 0U
The following samples were analyzed in this batch: 1012696-08C
QC Page: 16 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
QualRPD Limit
Analysis Date: 12/24/2010 12:44 PM
Prep Date:
Analyte Result %REC %RPD
Units: µg/L
MQL
Client ID: SeqNo: 2228356
MBLK
Run ID: VOA2_101224A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: VBLKW-122410-R103100
1,1,1-Trichloroethane 5.0U1,1,2,2-Tetrachloroethane 5.0U1,1,2-Trichlor-1,2,2-trifluoroethane 5.0U1,1,2-Trichloroethane 5.0U1,1-Dichloroethane 5.0U1,1-Dichloroethene 5.0U1,2,4-Trichlorobenzene 5.0U1,2-Dibromo-3-chloropropane 5.0U1,2-Dibromoethane 5.0U1,2-Dichlorobenzene 5.0U1,2-Dichloroethane 5.0U1,2-Dichloropropane 5.0U1,3-Dichlorobenzene 5.0U1,4-Dichlorobenzene 5.0U2-Butanone 10U2-Hexanone 10U4-Methyl-2-pentanone 10UAcetone 10UBenzene 5.0UBromodichloromethane 5.0UBromoform 5.0UBromomethane 5.0UCarbon disulfide 10UCarbon tetrachloride 5.0UChlorobenzene 5.0UChloroethane 5.0UChloroform 5.0UChloromethane 5.0Ucis-1,2-Dichloroethene 5.0Ucis-1,3-Dichloropropene 5.0UCyclohexane 5.0UDibromochloromethane 5.0UDichlorodifluoromethane 5.0UDichloromethane 10UEthylbenzene 5.0UIsopropylbenzene 5.0Um,p-Xylene 10UMethyl acetate 5.0UMethyl tert-butyl ether 5.0UMethylcyclohexane 5.0Uo-Xylene 5.0UStyrene 5.0U
QC Page: 17 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
Tetrachloroethene 5.0UToluene 5.0Utrans-1,2-Dichloroethene 5.0Utrans-1,3-Dichloropropene 5.0UTrichloroethene 5.0UTrichlorofluoromethane 5.0UVinyl chloride 2.0UXylenes, Total 15U
0050 Surr: 1,2-Dichloroethane-d4 104 70-1255.052.18
0050 Surr: 4-Bromofluorobenzene 95.3 72-1255.047.66
0050 Surr: Dibromofluoromethane 100 71-1255.050.18
0050 Surr: Toluene-d8 98.9 75-1255.049.44
QC Page: 18 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
QualRPD Limit
Analysis Date: 12/24/2010 10:53 AM
Prep Date:
Analyte Result %REC %RPD
Units: µg/L
MQL
Client ID: SeqNo: 2228355
LCS
Run ID: VOA2_101224A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: VLCSW-122410-R103100
00501,1,1-Trichloroethane 98.4 80-1205.049.1900501,1,2,2-Tetrachloroethane 94.9 72-1205.047.4500501,1,2-Trichlor-1,2,2-trifluoroethane 92.9 73-1235.046.4500501,1,2-Trichloroethane 95.8 80-1205.047.8800501,1-Dichloroethane 95.9 76-1205.047.9500501,1-Dichloroethene 96.9 73-1245.048.4700501,2,4-Trichlorobenzene 99 80-1205.049.5100501,2-Dibromo-3-chloropropane 95.1 65-1255.047.5600501,2-Dibromoethane 97.4 80-1205.048.6900501,2-Dichlorobenzene 96.7 80-1205.048.3700501,2-Dichloroethane 95.5 78-1205.047.7500501,2-Dichloropropane 96.9 80-1205.048.4600501,3-Dichlorobenzene 95.8 80-1205.047.900501,4-Dichlorobenzene 94.5 80-1205.047.27001002-Butanone 97 58-1321096.96001002-Hexanone 101 61-13010101.1001004-Methyl-2-pentanone 101 65-12710100.900100Acetone 99.8 59-1371099.770050Benzene 95 73-1215.047.50050Bromodichloromethane 100 80-1205.050.150050Bromoform 91.2 79-1205.045.620050Bromomethane 99 66-1375.049.4800100Carbon disulfide 99.1 68-1411099.070050Carbon tetrachloride 89.6 75-1245.044.790050Chlorobenzene 94.5 80-1205.047.240050Chloroethane 94.1 76-1215.047.040050Chloroform 97.1 80-1205.048.550050Chloromethane 99.5 67-1235.049.760050cis-1,2-Dichloroethene 106 78-1205.052.940050cis-1,3-Dichloropropene 104 80-1205.052.120050Cyclohexane 87.2 66-1255.043.60050Dibromochloromethane 101 80-1205.050.310050Dichlorodifluoromethane 91.7 63-1255.045.850050Dichloromethane 97.1 65-1331048.560050Ethylbenzene 98.3 80-1205.049.150050Isopropylbenzene 98.2 80-1205.049.0900100m,p-Xylene 98.2 78-1211098.160050Methyl acetate 94.4 60-1305.047.20050Methyl tert-butyl ether 99.1 73-1215.049.560050Methylcyclohexane 93.4 75-1225.046.70050o-Xylene 98.8 80-1205.049.410050Styrene 99.9 80-1205.049.97
QC Page: 19 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
0050Tetrachloroethene 92.6 79-1205.046.30050Toluene 94.4 80-1205.047.180050trans-1,2-Dichloroethene 95.3 78-1205.047.670050trans-1,3-Dichloropropene 94.3 80-1205.047.170050Trichloroethene 94.5 80-1205.047.250050Trichlorofluoromethane 93 72-1305.046.50050Vinyl chloride 94 70-1272.047.0200150Xylenes, Total 98.4 80-12015147.60050 Surr: 1,2-Dichloroethane-d4 99.7 70-1255.049.86
0050 Surr: 4-Bromofluorobenzene 99.6 72-1255.049.79
0050 Surr: Dibromofluoromethane 101 71-1255.050.44
0050 Surr: Toluene-d8 98.8 75-1255.049.39
QC Page: 20 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
QualRPD Limit
Analysis Date: 12/24/2010 01:56 PM
Prep Date:
Analyte Result %REC %RPD
Units: µg/L
MQL
Client ID: SeqNo: 2228358
MS
Run ID: VOA2_101224A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 5
Sample ID: 1012598-51AMS
002501,1,1-Trichloroethane 90.3 80-12025225.8002501,1,2,2-Tetrachloroethane 91 72-12025227.4002501,1,2-Trichlor-1,2,2-trifluoroethane 76.8 73-12325192.1002501,1,2-Trichloroethane 96.3 80-12025240.7002501,1-Dichloroethane 96.9 76-12025242.1
S0367.32501,1-Dichloroethene 67.1 73-12425535002501,2,4-Trichlorobenzene 91.2 80-12025228002501,2-Dibromo-3-chloropropane 85.6 65-12525214.1002501,2-Dibromoethane 96.1 80-12025240.1002501,2-Dichlorobenzene 96 80-12025239.9002501,2-Dichloroethane 98.8 78-12025247002501,2-Dichloropropane 99.9 80-12025249.9002501,3-Dichlorobenzene 94.7 80-12025236.9002501,4-Dichlorobenzene 93.3 80-12025233.2005002-Butanone 90.5 58-13250452.7005002-Hexanone 90 61-13050450005004-Methyl-2-pentanone 93.5 65-12750467.700500Acetone 88 59-13750440.200250Benzene 94.5 73-12125236.300250Bromodichloromethane 102 80-1202525600250Bromoform 87.6 79-12025218.900250Bromomethane 77.3 66-13725193.300500Carbon disulfide 89.4 68-14150447.100250Carbon tetrachloride 79.1 75-12425197.700250Chlorobenzene 94.7 80-12025236.800250Chloroethane 86.7 76-12125216.700250Chloroform 98.2 80-12025245.400250Chloromethane 92.7 67-12325231.7015.78250cis-1,2-Dichloroethene 107 78-12025282.300250cis-1,3-Dichloropropene 103 80-12025258.100250Cyclohexane 69 66-12525172.500250Dibromochloromethane 102 80-12025255.200250Dichlorodifluoromethane 75.9 63-12525189.700250Dichloromethane 98.7 65-13350246.800250Ethylbenzene 94.4 80-12025235.900250Isopropylbenzene 90.5 80-12025226.400500m,p-Xylene 95.1 78-12150475.400250Methyl acetate 89.6 60-13025224.100250Methyl tert-butyl ether 95.7 73-12125239.3
S00250Methylcyclohexane 69.6 75-12225174.100250o-Xylene 98.9 80-12025247.300250Styrene 99.2 80-12025247.9
QC Page: 21 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
00250Tetrachloroethene 82.8 79-1202520700250Toluene 93.1 80-12025232.700250trans-1,2-Dichloroethene 92.3 78-12025230.800250trans-1,3-Dichloropropene 91.6 80-120252290122.6250Trichloroethene 88.3 80-12025343.200250Trichlorofluoromethane 79.3 72-13025198.400250Vinyl chloride 83.7 70-12710209.300750Xylenes, Total 96.4 80-12075722.700250 Surr: 1,2-Dichloroethane-d4 100 70-12525251
00250 Surr: 4-Bromofluorobenzene 100 72-12525251.2
00250 Surr: Dibromofluoromethane 102 71-12525253.9
00250 Surr: Toluene-d8 99.5 75-12525248.6
QC Page: 22 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
QualRPD Limit
Analysis Date: 12/24/2010 02:19 PM
Prep Date:
Analyte Result %REC %RPD
Units: µg/L
MQL
Client ID: SeqNo: 2228359
MSD
Run ID: VOA2_101224A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 5
Sample ID: 1012598-51AMSD
225.802501,1,1-Trichloroethane 93.6 80-120 2025 3.57234227.402501,1,2,2-Tetrachloroethane 95.2 72-120 2025 4.51237.9
S192.102501,1,2-Trichlor-1,2,2-trifluoroethane 72.9 73-123 2025 5.19182.4240.702501,1,2-Trichloroethane 98.4 80-120 2025 2.21246.1242.102501,1-Dichloroethane 101 76-120 2025 4.2252.5
535367.32501,1-Dichloroethene 77.9 73-124 2025 4.9356222802501,2,4-Trichlorobenzene 90.6 80-120 2025 0.684226.4
214.102501,2-Dibromo-3-chloropropane 91.8 65-125 2025 6.91229.4240.102501,2-Dibromoethane 98.3 80-120 2025 2.32245.8239.902501,2-Dichlorobenzene 98.2 80-120 2025 2.33245.6
24702501,2-Dichloroethane 101 78-120 2025 2.14252.4249.902501,2-Dichloropropane 101 80-120 2025 0.668251.5236.902501,3-Dichlorobenzene 96.9 80-120 2025 2.27242.3233.202501,4-Dichlorobenzene 95.4 80-120 2025 2.26238.6452.705002-Butanone 91.7 58-132 2050 1.3458.6
45005002-Hexanone 94.9 61-130 2050 5.27474.4467.705004-Methyl-2-pentanone 96.5 65-127 2050 3.12482.5440.20500Acetone 91.4 59-137 2050 3.75457.1236.30250Benzene 98.7 73-121 2025 4.31246.7
2560250Bromodichloromethane 105 80-120 2025 2.48262.4218.90250Bromoform 91.9 79-120 2025 4.86229.8
R193.30250Bromomethane 103 66-137 2025 28.6257.8447.10500Carbon disulfide 93.1 68-141 2050 4.05465.5197.70250Carbon tetrachloride 80.4 75-124 2025 1.65201236.80250Chlorobenzene 98.3 80-120 2025 3.67245.7216.70250Chloroethane 91.3 76-121 2025 5.16228.2245.40250Chloroform 102 80-120 2025 3.5254.1231.70250Chloromethane 99.4 67-123 2025 6.98248.4282.315.78250cis-1,2-Dichloroethene 110 78-120 2025 2.98290.8258.10250cis-1,3-Dichloropropene 106 80-120 2025 2.77265.3
S172.50250Cyclohexane 65.9 66-125 2025 4.63164.7255.20250Dibromochloromethane 105 80-120 2025 2.53261.7189.70250Dichlorodifluoromethane 69.4 63-125 2025 8.88173.6246.80250Dichloromethane 102 65-133 2050 2.93254.1235.90250Ethylbenzene 96.6 80-120 2025 2.35241.5226.40250Isopropylbenzene 90.1 80-120 2025 0.551225.1475.40500m,p-Xylene 96.6 78-121 2050 1.55482.8224.10250Methyl acetate 92.2 60-130 2025 2.86230.6239.30250Methyl tert-butyl ether 99.1 73-121 2025 3.46247.7
S174.10250Methylcyclohexane 64.6 75-122 2025 7.51161.5247.30250o-Xylene 99.7 80-120 2025 0.802249.3247.90250Styrene 103 80-120 2025 3.43256.6
QC Page: 23 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103100 Instrument ID VOA2 Method: SW8260
2070250Tetrachloroethene 83.9 79-120 2025 1.33209.8232.70250Toluene 98.2 80-120 2025 5.31245.4230.80250trans-1,2-Dichloroethene 96.4 78-120 2025 4.32241
2290250trans-1,3-Dichloropropene 95.2 80-120 2025 3.86238343.2122.6250Trichloroethene 93.3 80-120 2025 3.6355.8198.40250Trichlorofluoromethane 76.9 72-130 2025 3.09192.3209.30250Vinyl chloride 83.7 70-127 2010 0.0342209.3722.70750Xylenes, Total 97.6 80-120 2075 1.29732.1
2510250 Surr: 1,2-Dichloroethane-d4 99.7 70-125 2025 0.734249.2
251.20250 Surr: 4-Bromofluorobenzene 100 72-125 2025 0.13250.8
253.90250 Surr: Dibromofluoromethane 102 71-125 2025 0.028253.8
248.60250 Surr: Toluene-d8 98.6 75-125 2025 0.891246.4
The following samples were analyzed in this batch: 1012696-07A 1012696-08A 1012696-09A
QC Page: 24 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
QualRPD Limit
Analysis Date: 12/28/2010 09:37 AM
Prep Date:
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2229503
MBLK
Run ID: VOA3_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: VBLKS1-122810-R103134
1,1,1-Trichloroethane 5.0U1,1,2,2-Tetrachloroethane 5.0U1,1,2-Trichlor-1,2,2-trifluoroethane 5.0U1,1,2-Trichloroethane 5.0U1,1-Dichloroethane 5.0U1,1-Dichloroethene 5.0U1,2,4-Trichlorobenzene 5.0U1,2-Dibromo-3-chloropropane 5.0U1,2-Dibromoethane 5.0U1,2-Dichlorobenzene 5.0U1,2-Dichloroethane 5.0U1,2-Dichloropropane 5.0U1,3-Dichlorobenzene 5.0U1,4-Dichlorobenzene 5.0U2-Butanone 10U2-Hexanone 10U4-Methyl-2-pentanone 10UAcetone 20UBenzene 5.0UBromodichloromethane 5.0UBromoform 5.0UBromomethane 10UCarbon disulfide 10UCarbon tetrachloride 5.0UChlorobenzene 5.0UChloroethane 10UChloroform 5.0UChloromethane 10Ucis-1,2-Dichloroethene 5.0Ucis-1,3-Dichloropropene 5.0UCyclohexane 5.0UDibromochloromethane 5.0UDichlorodifluoromethane 5.0UDichloromethane 10UEthylbenzene 5.0UIsopropylbenzene 5.0Um,p-Xylene 10UMethyl acetate 5.0UMethyl tert-butyl ether 5.0UMethylcyclohexane 5.0Uo-Xylene 5.0UStyrene 5.0U
QC Page: 25 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
Tetrachloroethene 5.0UToluene 5.0Utrans-1,2-Dichloroethene 5.0Utrans-1,3-Dichloropropene 5.0UTrichloroethene 5.0UTrichlorofluoromethane 5.0UVinyl chloride 2.0UXylenes, Total 15U
0050 Surr: 1,2-Dichloroethane-d4 97.1 70-128048.57
0050 Surr: 4-Bromofluorobenzene 99.5 73-126049.76
0050 Surr: Dibromofluoromethane 97.2 71-128048.58
0050 Surr: Toluene-d8 99.2 73-127049.61
QC Page: 26 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
QualRPD Limit
Analysis Date: 12/28/2010 08:42 AM
Prep Date:
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2229501
LCS
Run ID: VOA3_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: VLCSS1-122810-R103134
00501,1,1-Trichloroethane 100 79-1245.050.2300501,1,2,2-Tetrachloroethane 114 75-1235.057.1200501,1,2-Trichlor-1,2,2-trifluoroethane 98.5 79-1255.049.2300501,1,2-Trichloroethane 102 79-1205.050.7900501,1-Dichloroethane 108 75-1245.053.7800501,1-Dichloroethene 104 80-1225.051.9600501,2,4-Trichlorobenzene 103 74-1285.051.4800501,2-Dibromo-3-chloropropane 110 66-1295.055.2200501,2-Dibromoethane 112 79-1205.056.2300501,2-Dichlorobenzene 105 79-1205.052.6600501,2-Dichloroethane 97.8 73-1215.048.900501,2-Dichloropropane 100 76-1205.050.1900501,3-Dichlorobenzene 109 79-1205.054.4600501,4-Dichlorobenzene 106 77-1205.052.96001002-Butanone 123 65-13010122.8001002-Hexanone 114 65-13310114.2001004-Methyl-2-pentanone 111 69-13010110.900100Acetone 109 53-14220108.60050Benzene 104 79-1205.052.210050Bromodichloromethane 100 79-1215.050.210050Bromoform 101 74-1225.050.450050Bromomethane 90.4 68-1311045.2200100Carbon disulfide 102 80-12410101.70050Carbon tetrachloride 99.4 74-1265.049.720050Chlorobenzene 106 79-1205.053.250050Chloroethane 92.3 76-1261046.150050Chloroform 109 78-1205.054.70050Chloromethane 95.6 69-1291047.80050cis-1,2-Dichloroethene 107 80-1205.053.440050cis-1,3-Dichloropropene 108 77-1235.053.880050Cyclohexane 91.5 74-1265.045.750050Dibromochloromethane 115 78-1225.057.470050Dichlorodifluoromethane 80.4 57-1405.040.180050Dichloromethane 97.7 70-1231048.870050Ethylbenzene 104 80-1225.052.050050Isopropylbenzene 106 72-1275.05300100m,p-Xylene 104 79-12210104.10050Methyl acetate 109 69-1235.054.260050Methyl tert-butyl ether 110 76-1215.055.130050Methylcyclohexane 108 77-1265.053.990050o-Xylene 105 80-1235.052.490050Styrene 109 78-1245.054.68
QC Page: 27 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
0050Tetrachloroethene 116 80-1215.057.950050Toluene 103 79-1205.051.460050trans-1,2-Dichloroethene 109 79-1225.054.50050trans-1,3-Dichloropropene 111 77-1205.055.590050Trichloroethene 105 80-1215.052.520050Trichlorofluoromethane 98.5 75-1265.049.230050Vinyl chloride 88.1 76-1262.044.0400150Xylenes, Total 104 80-12015156.60050 Surr: 1,2-Dichloroethane-d4 102 70-128051.02
0050 Surr: 4-Bromofluorobenzene 98.5 73-126049.24
0050 Surr: Dibromofluoromethane 102 71-128050.89
0050 Surr: Toluene-d8 101 73-127050.31
QC Page: 28 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
QualRPD Limit
Analysis Date: 12/28/2010 09:10 AM
Prep Date:
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2229502
LCSD
Run ID: VOA3_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: VLCSDS1-122810-R103134
50.230501,1,1-Trichloroethane 93.3 79-124 305.0 7.4246.6457.120501,1,2,2-Tetrachloroethane 104 75-123 305.0 9.6651.8649.230501,1,2-Trichlor-1,2,2-trifluoroethane 94.3 79-125 305.0 4.3347.1550.790501,1,2-Trichloroethane 89.9 79-120 305.0 12.244.9653.780501,1-Dichloroethane 101 75-124 305.0 6.3850.4651.960501,1-Dichloroethene 96.9 80-122 305.0 7.0348.4451.480501,2,4-Trichlorobenzene 99.6 74-128 305.0 3.3649.7855.220501,2-Dibromo-3-chloropropane 98.9 66-129 305.0 11.149.4456.230501,2-Dibromoethane 98.8 79-120 305.0 12.949.4152.660501,2-Dichlorobenzene 97.5 79-120 305.0 7.7148.7548.90501,2-Dichloroethane 92.4 73-121 305.0 5.7146.18
50.190501,2-Dichloropropane 93.2 76-120 305.0 7.4546.5954.460501,3-Dichlorobenzene 98.4 79-120 305.0 10.249.1852.960501,4-Dichlorobenzene 96.4 77-120 305.0 9.3748.22122.801002-Butanone 107 65-130 3010 13.9106.8114.201002-Hexanone 101 65-133 3010 12.3101110.901004-Methyl-2-pentanone 101 69-130 3010 9.09101.3108.60100Acetone 102 53-142 3020 6.47101.852.21050Benzene 95.4 79-120 305.0 9.0547.6950.21050Bromodichloromethane 90.3 79-121 305.0 10.745.1350.45050Bromoform 91.3 74-122 305.0 1045.6345.22050Bromomethane 82.5 68-131 3010 9.1541.27101.70100Carbon disulfide 96.6 80-124 3010 5.1796.5849.72050Carbon tetrachloride 90.9 74-126 305.0 8.9945.4453.25050Chlorobenzene 96.2 79-120 305.0 10.248.146.15050Chloroethane 87.9 76-126 3010 4.9243.9354.7050Chloroform 100 78-120 305.0 8.5450.2247.8050Chloromethane 90.2 69-129 3010 5.7945.11
53.44050cis-1,2-Dichloroethene 98.3 80-120 305.0 8.3949.1453.88050cis-1,3-Dichloropropene 101 77-123 305.0 6.3350.5845.75050Cyclohexane 84 74-126 305.0 8.542.0257.47050Dibromochloromethane 101 78-122 305.0 12.950.4940.18050Dichlorodifluoromethane 95.5 57-140 305.0 17.247.7348.87050Dichloromethane 82.8 70-123 3010 16.641.3852.05050Ethylbenzene 96 80-122 305.0 8.148
53050Isopropylbenzene 96.2 72-127 305.0 9.6748.11104.10100m,p-Xylene 96 79-122 3010 8.195.9954.26050Methyl acetate 102 69-123 305.0 6.4750.8655.13050Methyl tert-butyl ether 99.7 76-121 305.0 1049.8753.99050Methylcyclohexane 99 77-126 305.0 8.749.4952.49050o-Xylene 97.3 80-123 305.0 7.6248.6454.68050Styrene 100 78-124 305.0 8.8250.07
QC Page: 29 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
57.95050Tetrachloroethene 97.9 80-121 305.0 16.948.9451.46050Toluene 93.4 79-120 305.0 9.6946.754.5050trans-1,2-Dichloroethene 102 79-122 305.0 6.8850.88
55.59050trans-1,3-Dichloropropene 99.3 77-120 305.0 11.349.6652.52050Trichloroethene 96.6 80-121 305.0 8.3548.3149.23050Trichlorofluoromethane 94.3 75-126 305.0 4.3347.1544.04050Vinyl chloride 83.1 76-126 302.0 5.8341.54156.60150Xylenes, Total 96.4 80-120 3015 7.94144.651.02050 Surr: 1,2-Dichloroethane-d4 99.7 70-128 300 2.3149.85
49.24050 Surr: 4-Bromofluorobenzene 100 73-126 300 1.6350.05
50.89050 Surr: Dibromofluoromethane 100 71-128 300 1.6950.04
50.31050 Surr: Toluene-d8 98.3 73-127 300 2.349.16
QC Page: 30 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
QualRPD Limit
Analysis Date: 12/28/2010 10:32 AM
Prep Date:
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2229507
MS
Run ID: VOA3_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012649-47AMS
00501,1,1-Trichloroethane 96.2 79-1245.048.0800501,1,2,2-Tetrachloroethane 107 75-1235.053.500501,1,2-Trichlor-1,2,2-trifluoroethane 95.4 79-1255.047.7200501,1,2-Trichloroethane 92.4 79-1205.046.1800501,1-Dichloroethane 100 75-1245.050.1300501,1-Dichloroethene 101 80-1225.050.4500501,2,4-Trichlorobenzene 96.4 74-1285.048.2200501,2-Dibromo-3-chloropropane 99.9 66-1295.049.9500501,2-Dibromoethane 105 79-1205.052.5200501,2-Dichlorobenzene 104 79-1205.051.900501,2-Dichloroethane 96.4 73-1215.048.200501,2-Dichloropropane 96.6 76-1205.048.300501,3-Dichlorobenzene 108 79-1205.054.0900501,4-Dichlorobenzene 105 77-1205.052.57001002-Butanone 97 65-1301097.03001002-Hexanone 94.2 65-1331094.17001004-Methyl-2-pentanone 92.6 69-1301092.6200100Acetone 91.8 53-1422091.790050Benzene 100 79-1205.050.130050Bromodichloromethane 95.8 79-1215.047.90050Bromoform 95.3 74-1225.047.630050Bromomethane 89.8 68-1311044.8800100Carbon disulfide 99.2 80-1241099.160050Carbon tetrachloride 98.2 74-1265.049.090050Chlorobenzene 102 79-1205.051.170050Chloroethane 95.3 76-1261047.660050Chloroform 103 78-1205.051.560050Chloromethane 93.1 69-1291046.570050cis-1,2-Dichloroethene 99.6 80-1205.049.790050cis-1,3-Dichloropropene 108 77-1235.053.970050Cyclohexane 87 74-1265.043.490050Dibromochloromethane 108 78-1225.053.880050Dichlorodifluoromethane 89.6 57-1405.044.780050Dichloromethane 90.2 70-1231045.090050Ethylbenzene 99.2 80-1225.049.620050Isopropylbenzene 102 72-1275.051.0300100m,p-Xylene 99.2 79-1221099.230050Methyl acetate 91.7 69-1235.045.850050Methyl tert-butyl ether 100 76-1215.050.110050Methylcyclohexane 102 77-1265.051.070050o-Xylene 100 80-1235.050.060050Styrene 104 78-1245.052.01
QC Page: 31 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
0050Tetrachloroethene 108 80-1215.053.810050Toluene 97.7 79-1205.048.860050trans-1,2-Dichloroethene 104 79-1225.052.050050trans-1,3-Dichloropropene 106 77-1205.053.170050Trichloroethene 108 80-1215.054.060050Trichlorofluoromethane 95.4 75-1265.047.720050Vinyl chloride 86.6 76-1262.043.2800150Xylenes, Total 99.5 80-12015149.30050 Surr: 1,2-Dichloroethane-d4 100 70-128050.07
0050 Surr: 4-Bromofluorobenzene 96.5 73-126048.27
0050 Surr: Dibromofluoromethane 101 71-128050.32
0050 Surr: Toluene-d8 98.5 73-127049.26
QC Page: 32 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
QualRPD Limit
Analysis Date: 12/28/2010 11:26 AM
Prep Date:
Analyte Result %REC %RPD
Units: µg/Kg
MQL
Client ID: SeqNo: 2229508
MSD
Run ID: VOA3_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012649-47AMSD
48.080501,1,1-Trichloroethane 108 79-124 305.0 11.754.0353.50501,1,2,2-Tetrachloroethane 108 75-123 305.0 1.2154.16
47.720501,1,2-Trichlor-1,2,2-trifluoroethane 106 79-125 305.0 10.753.1546.180501,1,2-Trichloroethane 101 79-120 305.0 8.4750.2750.130501,1-Dichloroethane 116 75-124 305.0 14.958.250.450501,1-Dichloroethene 113 80-122 305.0 11.256.4548.220501,2,4-Trichlorobenzene 107 74-128 305.0 9.9353.2649.950501,2-Dibromo-3-chloropropane 110 66-129 305.0 9.9855.1952.520501,2-Dibromoethane 112 79-120 305.0 6.155.8251.90501,2-Dichlorobenzene 107 79-120 305.0 2.6953.3148.20501,2-Dichloroethane 105 73-121 305.0 8.4352.4448.30501,2-Dichloropropane 105 76-120 305.0 8.7552.72
54.090501,3-Dichlorobenzene 116 79-120 305.0 6.8857.9452.570501,4-Dichlorobenzene 111 77-120 305.0 5.4855.5397.0301002-Butanone 106 65-130 3010 8.64105.894.1701002-Hexanone 102 65-133 3010 8.11102.192.6201004-Methyl-2-pentanone 104 69-130 3010 11.2103.791.790100Acetone 107 53-142 3020 15.310750.13050Benzene 115 79-120 305.0 13.957.647.9050Bromodichloromethane 111 79-121 305.0 14.955.62
47.63050Bromoform 105 74-122 305.0 9.6652.4744.88050Bromomethane 99.5 68-131 3010 10.349.7799.160100Carbon disulfide 110 80-124 3010 10.2109.849.09050Carbon tetrachloride 110 74-126 305.0 11.254.8951.17050Chlorobenzene 114 79-120 305.0 11.257.2347.66050Chloroethane 102 76-126 3010 6.8451.0451.56050Chloroform 116 78-120 305.0 1258.1746.57050Chloromethane 110 69-129 3010 16.755.0749.79050cis-1,2-Dichloroethene 116 80-120 305.0 15.558.1653.97050cis-1,3-Dichloropropene 122 77-123 305.0 12.261.0143.49050Cyclohexane 101 74-126 305.0 1550.5553.88050Dibromochloromethane 116 78-122 305.0 7.0257.844.78050Dichlorodifluoromethane 100 57-140 305.0 11.550.2445.09050Dichloromethane 99 70-123 3010 9.3149.4949.62050Ethylbenzene 114 80-122 305.0 13.957.0451.03050Isopropylbenzene 115 72-127 305.0 12.157.5899.230100m,p-Xylene 114 79-122 3010 13.9114.145.85050Methyl acetate 107 69-123 305.0 15.353.4750.11050Methyl tert-butyl ether 111 76-121 305.0 10.655.7451.07050Methylcyclohexane 123 77-126 305.0 18.561.550.06050o-Xylene 116 80-123 305.0 14.457.8252.01050Styrene 117 78-124 305.0 11.458.28
QC Page: 33 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103134 Instrument ID VOA3 Method: SW8260
S53.81050Tetrachloroethene 123 80-121 305.0 13.661.6848.86050Toluene 111 79-120 305.0 1355.6652.05050trans-1,2-Dichloroethene 116 79-122 305.0 10.958.07
S53.17050trans-1,3-Dichloropropene 120 77-120 305.0 12.560.23S54.06050Trichloroethene 121 80-121 305.0 11.460.57
47.72050Trichlorofluoromethane 106 75-126 305.0 10.753.1443.28050Vinyl chloride 103 76-126 302.0 1751.33149.30150Xylenes, Total 115 80-120 3015 14.1171.950.07050 Surr: 1,2-Dichloroethane-d4 104 70-128 300 3.7151.96
48.27050 Surr: 4-Bromofluorobenzene 100 73-126 300 3.7350.1
50.32050 Surr: Dibromofluoromethane 100 71-128 300 0.16850.23
49.26050 Surr: Toluene-d8 98.5 73-127 300 0.051849.23
The following samples were analyzed in this batch: 1012696-01A 1012696-03A 1012696-05A
QC Page: 34 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103128 Instrument ID WetChem Method: SW9045B
QualRPD Limit
Analysis Date: 12/28/2010 08:00 AM
Prep Date:
Analyte Result %REC %RPD
Units: pH Units
MQL
Client ID: SeqNo: 2229291
LCS
Run ID: WETCHEM_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: WLCS-122810-R103128
006pH 100 90-1100.106.01
QualRPD Limit
Analysis Date: 12/28/2010 08:00 AM
Prep Date:
Analyte Result %REC %RPD
Units: pH Units
MQL
Client ID: SeqNo: 2229296
DUP
Run ID: WETCHEM_101228A
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012689-01BDUP
9.1500pH 0 0-0 200.10 0.2189.17
The following samples were analyzed in this batch: 1012696-01B
QC Page: 35 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
Project: Holiday Place
Client: TGE Resources Inc.Work Order: 1012696
QC BATCH REPORT
Batch ID: R103186 Instrument ID Balance1 Method: E160.3
QualRPD Limit
Analysis Date: 12/28/2010 02:00 PM
Prep Date:
Analyte Result %REC %RPD
Units: wt%
MQL
Client ID: TSB1 (2-3) SeqNo: 2230626
DUP
Run ID: BALANCE1_101228J
SPK ValSPK Ref
ValueRPD Ref
ValueControl
Limit
DF: 1
Sample ID: 1012696-05BDUP
14.9800Percent Moisture 0 0-0 200.010 10.816.69
The following samples were analyzed in this batch: 1012696-01B 1012696-03B 1012696-05B
QC Page: 36 of 36Note: See Qualifiers Page for a list of Qualifiers and their explanation.
ALS Environmental Date: 30-Dec-10
QUALIFIERS, ACRONYMS, UNITSProject: Holiday Place
Client: TGE Resources Inc.
WorkOrder: 1012696
Units Reported Description
Qualifier Description
Acronym Description
Micrograms per Kilogram - Dry weight correctedµg/Kg-dryMicrograms per Literµg/LMilligrams per Kilogram - Dry weight correctedmg/Kg-dryMilligrams per Litermg/L
pH Unitswt%
Value exceeds Regulatory Limit*Not accreditedaAnalyte detected in the associated Method Blank above the Reporting LimitBValue above quantitation rangeEAnalyzed outside of Holding TimeHAnalyte detected below quantitation limitJManually integrated, see raw data for justificationMNot offered for accreditationnNot Detected at the Reporting LimitNDSample amount is > 4 times amount spikedODual Column results percent difference > 40%PRPD above laboratory control limitRSpike Recovery outside laboratory control limitsSAnalyzed but not detected above the MDLU
Detectability Check StudyDCS
Method DuplicateDUP
Laboratory Control SampleLCS
Laboratory Control Sample DuplicateLCSD
Method BlankMBLK
Method Detection LimitMDL
Method Quantitation LimitMQL
Matrix SpikeMS
Matrix Spike DuplicateMSD
Post Digestion SpikePDS
Practical Quantitation LimitPQL
Serial DilutionSD
Sample Detection LimitSDL
Texas Risk Reduction ProgramTRRP
QF Page 1 of 1
ALS Environmental
Sample Receipt Checklist
Client Name: T/GE
Work Order: 1012696
Date/Time Received: 21-Dec-10 14:07
Received by: RDH
Checklist completed byeSignature Date
Reviewed by:DateeSignature
Matrices: WaterCarrier name: ALS.HS
Shipping container/cooler in good condition? Yes No Not Present
Custody seals intact on shipping container/cooler? Yes No Not Present
Custody seals intact on sample bottles? Yes No Not Present
Chain of custody present? Yes No
Chain of custody signed when relinquished and received? Yes No
Chain of custody agrees with sample labels? Yes No
Samples in proper container/bottle? Yes No
Sample containers intact? Yes No
Sufficient sample volume for indicated test? Yes No
All samples received within holding time? Yes No
Container/Temp Blank temperature in compliance? Yes No
Yes No No VOA vials submittedWater - VOA vials have zero headspace?
Water - pH acceptable upon receipt? Yes No N/A
Temperature(s)/Thermometer(s): 2.1c
Login Notes:
002
Cooler(s)/Kit(s): 3886, 3384
21-Dec-10 22-Dec-10 Raymond N Gamboa Ed B. Fry
pH adjusted? Yes No N/ApH adjusted by:
CorrectiveAction:
Comments:
Client Contacted: Date Contacted: Person Contacted:
Contacted By: Regarding:
SRC Page 1 of 1
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