Sub-Appendix C-A Multi-Level Soil Gas Probe Study Geo-Logic Associates, January 2007
MULTI-LEVEL SOIL GAS PROBE STUDY PALOS VERDES LANDFILL LOS ANGELES COUNTY, CA
January 2007
PREPARED FOR: Sanitation Districts of Los Angeles County 1955 Workman Mill Road Whittier, California 90607 PREPARED BY: GeoLogic Associates, Inc. 1831 Commercenter East San Bernardino, California 92408 (909) 383-8728
MULTI-LEVEL SOIL GAS PROBE STUDY PALOS VERDES LANDFILL
LOS ANGELES COUNTY, CALIFORNIA
EXECUTIVE SUMMARY This report describes work that was performed to install and sample six new multi-level soil gas probes at the closed Palos Verdes Landfill in Los Angeles County, California. The probes were constructed on behalf of the County Sanitation Districts of Los Angeles County (LACSD) near and along the northeast boundary of the landfill, including Ernie Howlett Park and South Coast Botanic Garden. The probes were installed for the Five-Year Review being conducted by the Department of Toxic Substances Control. Data obtained from the multi-level soil gas probes will subsequently be used to update the Health Risk Assessment for the landfill.
MULTI-LEVEL SOIL GAS PROBE STUDYPALOSVERDESLAND~L
LOS ANGELES COUNTY, CALIFORNIA
TABLE OF CONTENTS
1.0 INTRODUCTION 11.1 GENERAL 11.2 WORK SCOPE , 1
2.0 SITE BACKGROUND 12.1 HISTORy 22.2 GEOLOGy 22.3 HYDROGEOLOGY 3
3.0. SOIL-PORE GAS PROBE INSTALLATION 33.1 UTILITY CLEARANCE 43.2 DRILLING METHODS 43.3 SOIL SAMPLING : 43.4 PROBE CONSTRUCTION 53.5 GEODETIC SURVEy 73.6 CUTTINGS CONTAINMENT AND DISPOSAL.. 7
4.0 LABORATORY ANALYSES 84.1 GEOTECHNICAL LABORATORY TESTING 84.2 DRILL CUTTINGS ANALYSES 84.3 SOIL GAS ANALYSES , 84.4 QUALITY ASSURANCE / QUALITY CONTROL (QAlQC) SAMPLES 9
5.0 CLOSURE 10
6.0 REFERENCES ~ 11
TABLESTable 1Table 2Table 3Table 4
FIGURESFigure IFigure 2
APPENDICESAPPENDIX AAPPENDIXBAPPENDIXC
Geotechnical Analytical SummaryComposite Drill Cuttings AnalysesSoil Gas Probe Analytical ResultsQAlQC Results
Project Location PlanGas Probe Location Plan
Boring and Soil Gas Probe Completion Summary LogsContinuous-Core PhotographsLaboratory Analytical Results
Geologic Associates
1.0 INTRODUCTION
1.1 GENERAL
This report documents soil-pore gas probe installation, sampling, and analyses that wereperformed by GeoLogic Associates (GLA) in May and June 2006 on behalfofthe CountySanitation Districts of Los Angeles County (SDLAC) at the closed Palos Verdes Landfill(pVLF; Figure 1). Results from the project will be used to update a Health Risk Assessmentsupporting a California Department ofToxic Substances Control Five - Year Review of thePVLF.
As detailed herein, the PVLF soil-pore gas probe installation project was completed inaccordance with project guidance document "Landfill Gas Emissions Assessment Workplan"dated December 12, 2005, and requirements of the California Department of ToxicSubstances Control.
1.2 WORKSCOPE
As will be detailed herein, the PVLF soil-pore gas (SPG) probe installation project wascompleted in accordance with the project's Landfill Gas Emissions Assessment Workplanguidance document and involved the following:
• Obtain utility clearance permits.• Drilling, soil sampling, and gas probe installation.• Sampling and analyses ofprobes.• Preparation of this report.
As shown in Figure 2, there are five alluvial channels that cross the northeast border of thePVLF. Alluvial deposits consist ofporous deposits that represent a potential preferentialpathway for migration of landfill gas. As a path of least resistance, this preferential pathwayhas the greatest potential for offsite gas migration. Accordingly, five multi-level soil gasprobes were installed within these former canyons; and one multi-level probe was installedadjacent to the closest residence to assess potential health risks associated with subsurfacelandfill gas.
All work was completed in accordance with applicable regulations and guidelines, and underthe supervision of a California Professional Geologist.
2.0 SITE BACKGROUND
The PVLF site is located at 25706 Hawthome Boulevard, Rolling Hills Estates, California, inLos Angeles County (Figure I). The Site is separated into three sections by Hawthorne andCrenshaw Boulevards; the Main Site, South Coast Botanic Garden (south of Crenshaw Blvd),and Ernie Howlett Park (north of Hawthorne Blvd). The total area of the landfill isapproximately 295 acres (Figure 2).
Geologic Associates
2.1 HISTORY
Since the early 1900s, mining and quarry operations for diatomaceous earth, sand and gravelwere conducted at and around the Main Site. Mining activities at the PVLF continued untilthe 1950s when operations were discontinued primarily due to resource depletion. The PVLFwas operated under permit by the Sanitation Districts as a sanitary landfill from May 1957through December 1980. From 1964 through 1980, the landfill accepted hazardous wastes inthose areas permitted for these wastes. It is estimated that hazardous wastes made up a smallpercentage (3 to 4 percent) of the total volume of wastes disposed at the PVLF. TheSanitation Districts continues on-going maintenance and monitoring of the site through thepresent.
2.2 GEOLOGY
The PVLF is underlain by metamorphic rocks of Jurassic age, marine and non marinesedimentary rocks deposited in the Miocene epoch, and Holocene-aged alluvial and colluvialdeposits. Bedrock units dip from 20 to 50 degrees to the northwest, with local variation dueto slumping and secondary folding. Alluvium has been deposited in historic surface waterdrainage channels located beneath the PVLF, and in the terrane adjacent to the landfill. Also,much of the area's historic surface drainage systems have been modified by development,resulting in drainages being filled and surface water runoffdiverted into manmade stormdrains.
From oldest to youngest, the geologic units at the site are:
• Jurassic-aged Catalina Schist.• Miocene-aged members of the Monterey Formation (from oldest to youngest):
o Altamira Shale;o Valmonte Diatomite;o Malaga Mudstone.
• Holocene-aged alluvium and colluvium.
Altamira Shale - Although not encountered during the soil gas probe study, the AltamiraShale is the oldest and deepest rock that has been encountered during previous siteinvestigations. The member is composed oftan to gray shale and siltstone and crops out atthe southwestern extreme of Ernie Howlett Park and the Main Site.
Valmonte Diatomite - Underlying a majority of the Main Site, Ernie Howlett Park, and theSouth Coast Botanic Garden, the Valmonte Diatomite is comprised of diatomaceous shale anddiatomite. Prior to land filling on the site, this unit was extensively mined for commercialpurposes. This unit was not identified during the project.
Malaga Mudstone - Underlying approximately two-thirds of the northeastern portion oftheSouth Coast Botanic Garden, and the northeastern half of the Main Site, the Malaga Mudstoneconsists primarily of grayish brown to black mudstone. The Mudstone is a highlypetroliferous unit, and yields the majority ofthe hydrocarbons extracted from the Monterey
2006.0088\PVLF Probe Insl~1l R]ll z.ooe 02106/07 2 Geologic Associates
Formation in the Los Angeles area. The mudstone was encountered at depths ranging from15 to 17 feet in borings VN-2, VN-3, and VN-4.
Alluvium and colluvium - Recent sedimentary deposits are derived from erosion of existingbedrock and previously existing soil. Within the study area, alluvium and colluvium arederived from the Monterey Formation bedrock complex and, as such, consist of diatomaceoussilt and clay with scattered sand-, gravel-, and cobble-sized clasts of siltstone and chert.These deposits are thin and discontinuous throughout the Site: alluvium is confined to historiccanyon drainages and colluvium is found along the base of slopes. These materials wereencountered in every project boring. As discussed in Section 1.2, alluvial drainage channelsprovide a path ofleast resistance; this preferential pathway represents the greatest potentialforoffsite gas migration.
2.3 HYDROGEOLOGY
Bedrock underlying the Palos Verdes Hills is comprised mainly of fine-grained sedimentaryrocks of the Monterey Formation, which are not considered to store and transmit largevolumes of groundwater. Members of this formation generally possess low hydraulicconductivity, although fractured rocks and weathered zones may locally possess greaterhydraulic conductivities. According to the Los Angeles Basin Water Quality Control Plan,the Palos Verdes Site does not overlie an identified regional groundwater basin and, as such,no specific beneficial uses for groundwater have been defined.
Generally, near-surface geologic materials at, and in the vicinity of, the PVLF are composedof alluvium and other unconsolidated sediments and have relatively high hydraulicconductivities, compared with underlying bedrock. As illustrated in Figure 2, prior to landfilling and mining operations, several surface water drainages crossed the landfill, which werejoined by various smaller tributaries that merged into the main drainages along present dayCrenshaw and Hawthorne Boulevards. As described above, alluvium in these historicdrainages provides potential pathways for gas migration from the site. Beneath theunsaturated alluvium, these former drainage channels also create preferential groundwaterpathways from the site. Groundwater was only encountered in one of the six deep boringsdrilled during the project (at a depth of about 42 feet in boring VN-l).
3.0 SOIL-PORE GAS PROBE INSTALLATION
In keeping with the Landfill Gas Emissions Assessment Workplan, GLA drilled and installedsix multi-level soil-pore gas (SPG) probes, and two single-level probes, at six locationsselected by SDLAC (Figure 2). Drilling, sampling, and probe construction activities occurredbetween May 5 and May 12,2006, and were conducted in accordance with a site-specificHealth and Safety Plan (GLA, 2006). The following sections describe the methods andprocedures that were used during SPG installation.
Z006.008S\PVLFProbe In51~11 Rpt r.uec OU06l07 3 Geologic Associates
3.1 UTILITY CLEARANCE
Before field work was begun, GLA obtained utility clearance from Underground ServiceAlert ofCalifomia (USA, phone number: 800-227-2600) for the three SPG probe locationsoutside the footprint of the PVLF. The USA permit numbers and corresponding probelocations are tabulated below:
Utility Clearance SummaryProbe
VN-lVN-5VN-6
Clearance USA PermitRequest Date No.May 1,2006 Al211267May 1,2006 Al211276May 1, 2006 Al211280
Utility clearance for the three probe locations located within the Main Site (VN-2, VN-3, andVN-4) was provided by SDLAC.
3.2 DRILLING METHODS
All drilling and soil sampling activities were performed under the supervision of a CaliforniaProfessional Geologist. Probe drilling and installation was performed by ABC-LiovinDrilling, a state-licensed drilling contractor. Drilling for multi-level probes was completedusing ahollow stem auger (HSA) drill rig and 8-inch diameter augers, and combinationcontinuous coring system and California-modified 2.5-inch diameter split-barrel sampler tocollect relatively undisturbed soil samples. As shown on the boring logs in Appendix A, otherthan boring VN-l which encountered groundwater approximately 42 feet below grade (totaldepth of46.5 feet), each multi-level probe borehole was drilled to a depth of50 feet. Prior todrilling operations and between each location, all drill rig and sampling equipment wereproperly decontaminated using high-pressure wash and steam-cleaning equipment. Ofnote,drilling for the two single-level probes that were installed during the project (VN-l-l ON andVN-4-7) was completed using hand-auger methods to excavate approximate 3-inch diameterboreholes. To minimize noise at locations near residential areas, noise abatement techniques(sound walls) were used to reduce noise during drilling/sampling at locations VN-2, VN-3,and VN-4.
3.3 SOIL SAMPLING
Continuous core and split-spoon soil sampling techniques were completed by repeatedlydrilling a five-foot long, 2.5-inch inside diameter CME continuous core split barrel into theground to retain a core sample. After retrieval of the core tube, a 2.5-inch diameter "drive"sample was collected using a California modified split-spoon sampler.
As shown on the boring logs in Appendix A, geologic logging of the soil samples.wasperformed in accordance with the U.S. Department of the Interior Bureau of Reclamation(USDl-BR) "Engineering Geology Field Manual," and included the following elements:
2006.U088IPYLI? Probe Install Rpt Ldoc OU06f07 4 Geologic Associates
• Borehole designation and location.• Times and dates that drilling/excavation began and ended.• Type of exploratory equipment being utilized, including manufacturer, make, and model
for special modifications.• Name(s) ofgeologist(s) responsible for log description.• Name(s) ofother personnel assisting in the logging.• Description of soils according to the Unified Soil Classification System and description
.ofbedrock materials according to accepted geologic nomenclature.• Systematic descriptions of lithologic and micro-structural changes in strata or soil
horizons, including thickness ofunits as well as the depth and elevation of lithologicchanges.
• Presence of, and depth to, groundwater.• Caving or sloughing conditions in the hole, including depth and elevation.• Sampling interval(s), including depths and elevations.• Unusual color, staining, or odors of chemical or waste origin.• Drilling advancement in feet-per-hour (average) and/or feet-per-minute, noting periods of
difficult or very easy drilling.• Any subsurface structures or unusual features encountered.• Descriptions ofmineral seams and fracture fillings.• Faults, gouge, or shear zones penetrated.• Depth and thickness ofweathering.
The boring logs in Appendix A were prepared in accordance with the Unified SoilClassification System (USCS; ASTM D-2487-93). Soil grain size distribution was estimatedto within approximately 5%, and soils were assigned USCS group names and symbols asoutlined in the USDI's "Engineering Geology Field Manual" (Chapter 3, pages 20 through 22,figures 3-2 through 3-4).
All core samples were carefully stored in core boxes, with the collection location and depthsclearly marked for easy reference. Digital photographs of the core samples were obtained andare presented in Appendix B. Upon completion of each boring, core boxes were stored at alocation approved by SDLAC for the duration of the project.
All 2.5-inch split-spoon soil samples were wrapped in plastic bags, sealed in rigid plasticsleeves, and stored in foam-insulated steel boxes. Select 2.5-inch split-barrel samples weretransported to GLA's soils laboratory in Anaheim, California, for geotechnical testing.
3.4 PROBE CONSTRUCTION
All drilling and probe construction was completed in accordance with procedures summarizedin Department of Water Resources Bulletin No. 74-90 (DWR, 1991) and "Landfill GasEmissions Assessment Workplan" under the supervision of a California ProfessionalGeologist. As indicated on the gas probe completion summary logs that are included with theboring logs in Appendix A, the probes were generally constructed as multi-level (or nested)probes with three discrete soil-vapor tips in each borehole. On May 9, 2006, at multi-levelsoil gas probe VN-I, some minor wood and plastic fragments were encountered from 6 to
2006.0088\PVLFProbe lnsmll Rpt z.doc 02106/07 5 Geologic Associates
12.5 feet below ground surface (bgs). In addition, an active gas collection trench wasencountered from 5 to 12 feet bgs at multi-level soil gas probe VN-4. Neither of theseshallow subsurface zones were deemed suitable for soil gas monitoring; thus, two additionalshallow gas probes were constructed in separate boreholes located closer to the propertyboundary in order to collect representative soil gas samples. These two additional shallowprobes were installed and are designated as VNI-ION and VN4-7. VNl-lON was constructedapproximately 20 feet closer to the property boundary from VNI and VN4-7 was constructedapproximately two feet closer to the property boundary. The initial locations ofVNl andVN4 could not be located closer to the property boundary due to the location of overheadpowerlines and the size of the drill rig required to install deeper probes to 50 feet bgs. Theadditional shallow soil gas probes were installed using a hand auger. As summarized below,one borehole probe was constructed with two probe tips, and two probes were constructedwith a single probe tip:
BoreholeID ProbeID Probe Soil Sample Soil SampleDepth (feet) ill Depth (feet)
VN-I VNI-20 20 VN-1/4 21.5VNI-34 34 VN-1/6 31.5
VN-2 VN2-1J 11 VN-2/2 11.5VN2-29 29 VN-2/6 31.5VN2-41 41 VN-2/8 41.5
VN-3 VN3-13 13 VN-3/2 11.5VN3-23.5 23.5 VN-3/4 21.0VN3-31 31 VN-3/6 31.5
VN-4 VN4-23 23 VN-4/2 21.5VN4-31 31 VN-4/5 31.5
VN-5 VN5-16 16 VN-5/3 16.5VN5-31 31 VN-5/4 31.5
VN5-47.5 47.5 VN-5/7 46.5VN-6 VN6-15 15 VN-6/3 16.5
VN6-29 29 VN-6/5 31.5 .
VN6-41 41 VN-6/7 41.5VNI-ION VNI-ION 10 VN-IN 10.2VN4-7 VN4-7 7 NA NA
Note. Sot! SampleID and Depth information refer to corresponding sol! samples.
Each probe was constructed using color-coded (see probe construction summary logs ororange [shallow], green [intermediate], blue [deepD, 1/4-inch polyethylene tubing, and aporous, 316 stainless steel soil-vapor implant that was installed midway between a typical 2foot thick sand pack. The tubing of each probe was secured with "zip ties" to a I-inch PVCpipe during installation, and each probe implant was separated by at least five feet. The top ofeach tube was secured with gas-tight fitting and labeled to identify the depth at which theprobe was constructed. Following probe installation, the PVC pipe was sealed using hydratedbentonite. All probe materials were virgin, decontaminated and factory sealed upon deliveryto the site. The probe label identification system selected by SDLAC (i.e.- VN6-15)references the respective borehole (VN-6) and the depth at which the probe implant wasinstalled (15 feet bgs). The field geologist selected the appropriate depth for installing theprobes by reviewing geologic conditions to determine the most porous zones with the greatestpotential for gas migration, such as fractures and sand layers, as well as the results of field
2006.0088\PVLlI Probe InSlali Up! 2.doe 02106107 6 Geologic Associates
screening ofcuttings produced during drilling so that the probe tips were installed at theapproximate depths that provided the highest concentrations ofvolatile organic compounds.
As shown on the soil gas probe completion summary logs in Appendix A, filter pack materialconsisted ofinert commercial washed and graded #2112 Monterey sand. The grain size of thefilter pack was designed so that the sand grains were no smaller than adjacent lithologicformation.
Each probe/filter pack interval received an initial dry granular bentonite seal that was at leastone foot thick, and a secondary bentonite grout seal that was delivered using tremmie-pipetechniques to preclude infiltration ofhydrated bentonite grout. Grout was placed in theborehole until the top of the grout was at the design depth of the next filter pack.
Depth soundings were employed to evaluate the thickness and uniformity of the sand packs,granular bentonite seals, and bentonite grout seals to assure that no bridging occured. Eachprobe was finished at the surface with a flush-to-grade, traffic-rated utility vault.
3.5 GEODETIC SURVEY
In accordance with the "Landfill Gas Emissions Assessment Workplan", a CaliforniaRegistered Land Surveyor determined the location and elevation of the top of each newlyinstalled probe vault. The horizontal position was established using NAD83 (1992.9 Epoch).Elevation data (relative to feet above mean seal level [msl]) were measured relative toexisting PVLF control points that were provided by SDLAC. Units ofmeasure were U.S.survey feet, and were determined to an accuracy of 0.01 foot. Probe survey data are includedon the boring and probe completion summary logs, and are tabulated below:
Probe Northtnz Eastina ElevationVN-I 1,747,555.35 6,455,431.05 248.19VN-2 1,746,175.74 6,456,825.76 308.11VN-3 1,746,103.84 6,456,892.09 314.92VN-4 1,745,600.02 6,457,391.38 333.53VN-5 1,744,586.52 6,457,265.82 340.30VN-6 1,743,912.12 6,457,849.57 343.38
VNI-ION 1,747,580.37 6,455,444.79 246.17VN4-7 1,745,603.42 6,457,394.63 333.43
3.6 CUTTINGS CONTAINMENT AND DISPOSAL
Drill cuttings returned to the surface during drilling were contained in steel drums and storedon the top deck of the PVLF. As discussed in Section 4.2, the cuttings were sampled andtested, and found to be uncontaminated. As a result, the cuttings were placed on the landfill'stop deck stockpile, and the steel drums were removed from the site.
2006.0088\PVLF Probe Install Rpt z.occ 02/06/07 7 Geologic Associates
4.0 LABORATORY ANALYSES
The project's analytical laboratory schedule included geotechnical testing of select 2.5-inchsplit-spoon soil samples, composite sampling and analyses ofdrill cuttings, and a baselinemonitoring event of the newly installed gas probes.
4.1 GEOTECHNICAL LABORATORY TESTING
As directed by SDLAC, geotechnical laboratory testing was completed on representative 2.5inch split-spoon samples to evaluate in-situ geotechnical properties of soil adjacent to depths thatprobe tips were installed. Testing was performed at GLA's laboratory in Anaheim, California,and included the following schedule:
TEST ASTMMETHODGrain Density D-854Particle Size with Sieve Analysis D-422Moisture Content D-2216Bulk Drv Density D-2937Total Porosity CalculationWater Filled Porosity CalculationAir Filled Porosity CalculationFraction Organic Carbon Walkley-Black Method
The results of geotechnical laboratory tests are summarized on Table 1. Complete analyticalresults are presented in Appendix C.
4.2 DRILL CUTTINGS ANALYSES
Representative samples of the drill cuttings (i.e., soil removed from each borehole) werecollected and composited at AccuLabs, a California-certified laboratory in the City ofIndustry,CA. Composited samples were tested for total petroleum hydrocarbons, metals, volatile organiccompounds, semi-volatile organic compounds, pesticides, polychlorinated biphenyls, andherbicides. As summarized on Table 2 and shown in Appendix C, no petroleum hydrocarbons,volatile or semi-volatile compounds, or organic compounds were detected in the compositedsamples. Metals testing indicated that the soils were consistent with background levelsdocumented for the site (as presented in the "Remedial Investigation Report", SDLAC, June1995). Based on the analytical test results and as approved by DTSC, the cuttings were added tothe soil stockpile located on the top deck of the landfill.
4.3 SOIL GAS ANALYSES
Soil-pore gas samples were collected from each of the newly installed probes on May 31, 2006,using the following procedures:
2006.0088\P"LF Probe Install Rpt 2.11oc 02106/07 8 Geologic Associates
• A stainless-steel gas sampling pump equipped with a non-lubricated Viton® diaphragmand a maximum no-load flow rate of34.8 liters per minute, was connected to the probetubing/port.
• The probe was evacuated until the total organic compounds concentration (as measuredby an FID in a sampling train) remained constant for at least 30 seconds.
• A soil-pore gas sample was collected in a clean-certified 6-liter Summa canister that wasprovided by the project laboratory (Acculabs).
• Following collection, the sample's Summa canister was labeled with the probeidentification number (i.e.- VNI-20), date and time of collection, sampler's name, andproject specific information.
Gas samples were transported to Acculabs laboratory in the City of Industry, California, usingstandard chain-of-custody procedures. Laboratory analytical results are summarized on Table3, and laboratory certificates of analysis are presented in Appendix C.
According to the PVLF Landfill Gas Emissions Assessment Workplan, the soil gas sampleswere scheduled to be tested for total air contaminants (TAC) using EPA Method TO-15 S1M.because this method can provide lower detection limits (parts per trillion) than other testmethods (parts per billion). However, EPA Compendium Method TO-14 was inadvertentlyselected for TACs analysis for this project. While not in conformance with the PVLF LandfillGas Emissions Assessment Workplan, testing for TACs using EPA Method TO-14 providedrepresentative results. This assessment is based on the fact that TACs were detected insamples from each multi-level probe using EPA Method TO-14. IfEPA Method TO-I5 SlMwould have been selected for this project, the TAC concentrations would have requiredsample dilution, and higher detection limits (parts per billion) would have been reported.Moreover, EPA Method TO-14 provided results for a larger list ofTACs than was originallyproposed.
4.4 QUALITY ASSURANCE I QUALITY CONTROL (QAlQc) SAMPLES
The quality assurance I quality control (QAlQc) program completed during the projectincluded analyses of two duplicate soil gas samples, one travel- blank gas sample (QCTB),and two laboratory method blank gas samples. As shown on Table 4, the travel-blank samplewas analyzed only for volatile organic compounds (EPA Method TO-I4), while the duplicatesamples (VN-DUP I for VN2-11 and VN-DUP2 for VN6-I5) and method blank samples(prepared by the analytical laboratory) were analyzed for both TOC (Method 25) and VOCs(Method TO-14). Comparison of primary and duplicate analytical results indicates goodagreement between sample pairs. Although the compounds detected in each pair of duplicatesamples were not identical, given that the numbers and concentrations of compounds weresimilar in each case, and the fact that the QCTB and method blank results yielded nodetections, it is concluded that proper field and laboratory procedures were employed duringthe project.
2006.01188\PVLFProbe Install Rpl z.doc 02106/07 9 Geologic Associates
5.0 CLOSURE
This report is based on the limited data described above and referenced herein. GeoLogicAssociates should be notified of any conditions that differ from those described herein sincethis may require a re-evaluation of the data, conclusions and recommendations presentedherein.
This report was not prepared for use by other parties and projects other than those named ordescribed above. It may not contain sufficient information for other parties or other purposes.This report was prepared in accordance with generally accepted geotechnical andhydrogeologic practices, and makes no other warranties, either expressed or implied, as to theprofessional data presented in it.
'-lJji!;on...l'lfpp, CRgProject Geologist
2006.00881PVLF Probe Install Rill z.uec 02/06/07 10
Michael D. Reason, CRgSenior Hydrogeologist
Geologic Associates
6.0 REFERENCES
Bureau of Rec1amation, 1998, "Engineering Geology Field Manual," U.S. Department oftheInterior.
California Department of Water Resources, 1991, "California Well Standards", Bulletin No.74-90.
GeoLogic Associates, 2006, "Site Health and Safety Plan, Palos Verdes Landfill, Los AngelesCounty, California," presented to Sanitation Districts of Los Angeles County, May.
Sanitation Districts of Los Angeles County, 1995, "Remedial Investigation Report, LosAngeles County," June.
2006.0088\P\'LF Probe Install Rpl z.ooc 02/06/07 11 Geologic Associates
TABLE 1GEOTECHNICAL ANALYTICAL SUMMARY
MULTI-LEVEL SOIL GAS PROBE STUDYPALOS VERDES LANDFILL
Sample No. (Depth - feet)
VN-1/4 (21.5)
VN-1/6 (31.5)
VN-2/2 (11.5)
VN-2/6 (31.5)
VN-2/8 (41.5)
VN-3/2 (11.5)
VN-3/4 (21.0)
VN-3/6 (31.5)
VN-4/2 (21.5)
VN-4/5 (31.5)
L x D 4" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41"
Soil Type
Brown Gray mottled,
Clayey Silt w. Siltstone
Olive Brown,Silty Clay w.
some F. Sand
Olive rown, Silty Clay
D. Gray, Silty Clay w. Hydrocarbo
n odor
D. Gray, Silty Clay w. Hydrocarbo
n odor
Gray Brown, Silty Clay
Olive Gray, Silty clay
D. Gray, Silty Clay w.
Hydrocarbon odor
Orange Brown
mottled, Clayey Silt
Olive Brown,Clayey Silt w. Siltstone
Frgmts
Wet Weight + Tare (g)
715.4 957.5 869.1 827.0 822.3 815.5 844.1 800.1 868.4 861.1
Tare (g) 178.0 222.5 222.5 222.5 222.5 222.5 222.5 222.5 222.5 222.5
Volume of Sample (cf), V
0.011 0.013 0.013 0.013 0.013 0.013 0.013 0.013 0.013 0.013
Water Content (%)
37.0 27.1 51.1 58.2 57.1 70.2 59.5 67.6 44.5 37.4
Weight of Solid (lbs), Ws
0.865 1.275 0.943 0.842 0.842 0.768 0.859 0.760 0.985 1.025
Dry Density (pcf) 81.5 96.2 71.2 63.5 63.5 57.9 64.8 57.3 74.3 77.3
Specific Gravity, G @ 20o 2.564 2.676 2.798 2.478 2.470 2.513 2.733 2.352 2.672 2.549
Porosity (%), n 49.0 42.4 59.2 58.9 58.8 63.1 62.0 61.0 55.4 51.4
n = 1 - ( W s / G V γ w )γ w = 62.4 pcf
TABLE 1 (CONT'D)GEOTECHNICAL ANALYTICAL SUMMARY
MULTI-LEVEL SOIL GAS PROBE STUDYPALOS VERDES LANDFILL
Sample No. (Depth - feet)
VN-5/3 (16.5)
VN-5/4 (31.5)
VN-5/7 (46.5)
VN-6/3 (16.5)
VN-6/5 (31.5)
VN-6/7 (41.5)
VN-1Na (10.0)
VN-1Nb (10.2)
L x D 5" X 2.41" 5" X 2.41" 4" X 2.41" 5" X 2.41" 5" X 2.41" 5" X 2.41" 2.166"x1.966" 4.556"x1.966"
Soil TypeOlive Brown
mottled, Clayey Silt
Olive Brown mottled,
Clayey Silt
Olive Brown mottled,
Clayey Silt w. trace F.
Sand
Gray Brown, Clayey Silt
L. Orange Brown,
Clayey Silt
L. Orange Brown, Silty
Clay
Grayish Brown, Silty
Clay
Grayish Brown, Silty
Clay
Wet Weight + Tare (g)
880.5 860.5 686.4 844.0 826.5 880.0 172.3 392.1
Tare (g) 222.5 222.5 178.0 222.5 222.5 222.5 0.0 0.0
Volume of Sample (cf), V
0.013 0.013 0.011 0.013 0.013 0.013 0.004 0.008
Water Content (%)
44.7 37.8 35.3 28.1 66.1 46.2 34.9 45.0
Weight of Solid (lbs), Ws
1.003 1.021 0.828 1.070 0.802 0.991 0.282 0.596
Dry Density (pcf) 75.6 77.0 78.1 80.7 60.5 74.8 74.0 74.5
Specific Gravity, G @ 20o
2.664 2.577 2.543 2.517 2.636 2.637 2.524 2.506
Porosity (%), n 54.5 52.1 50.8 48.6 63.2 54.6 53.0 52.3
n = 1 - ( W s / G V γ w )γ w = 62.4 pcf
TABLE 2COMPOSITE DRILL CUTTINGS ANALYSES
MULTI-LEVEL SOIL GAS PROBE STUDYPALOS VERDES LANDFILL
ANALYTE GROUP UNITS COMPOSITE SAMPLE ID Background VN-1 VN-2 VN-3 VN-4 VN-5 VN-6 Data (a)
TOTAL PETROLEUM HYDROCARBONS (EPA 8015M)TPH - Gasoline mg/kg 0.1 0.1 0.1 0.1 0.1 0.1 --TPH - Diesel mg/kg 5 5 5 5 5 5 --
METALS (EPA 6010B)Antimony mg/kg 2.9 3.4 3.5 3.4 3.4 3.3 <0.5 - 5.5Arsenic mg/kg 8.4 7.8 5.2 7.7 10 6.9 0.17 - 58Barium mg/kg 690 140 170 200 440 180 5.59 - 4400Beryllium mg/kg 0.12 0.12 0.12 0.12 0.12 0.12 <0.5 - 2.94Cadmium mg/kg 2.8 1.8 0.032 1.6 2.5 0.032 <0.15 - 18.9Chromium mg/kg 58 57 56 53 57 52 16.2 - 193Chromium (CA-DHS for STLC) mg/L 1.3 0.52 0.52 0.52 0.52 0.52 --Cobalt mg/kg 4.8 6.5 5.9 7.1 6.4 4.7 <1.8 - 24.3Copper mg/kg 29 41 46 39 36 44 --Lead mg/kg 6 3.1 3.5 3.5 3.3 4.4 <2 - 5.31Mercury (EPA 7471A) mg/kg 0.0067 0.13 0.14 0.0067 0.11 0.10 <0.05 - 0.318Molybdenum mg/kg 4.4 8.5 6.5 6.8 7.2 19 <0.86 - 70.6Nickel mg/kg 42 48 29 52 57 24 13.4 - 294Selenium mg/kg 0.89 0.89 7.7 0.89 0.89 0.89 <0.01 - 2.9Silver mg/kg 0.16 0.16 0.16 0.16 0.16 0.16 <1 - 4.25Thallium mg/kg 0.45 0.45 0.45 0.45 0.45 0.45 <0.5 - <0.5Vanadium mg/kg 99 60 49 51 91 55 37.5 - 645Zinc mg/kg 67 78 61 79 77 58 30.8 - 408
ORGANOCHLORINE PESTICIDES & PCBs (EPA 8081A & 8082): NDORGANOCHLORINE HERBICIDES (EPA 8151A): NDVOLATILE ORGANIC COMPOUNDS (EPA 8260B): NDSEMI-VOLATILE ORGANIC COMPOUNDS (EPA 8270C): ND
(a) Background data from RI/FS (SDLAC, 1995).
EPA U.S. Environmental Protection AgencyMDL Method Detection Limitmg/L milligrams per litermg/kg milligrams per kilogram
ND Not DetectedPQL Practical Quantitation LimitTPH Total Petroleum Hydrocarbons
-- Not Established
0.1 Not detected above MDL; value listed is MDL (shaded, left justified).
0.1 Value listed is estimated concentration, between MDL and PQL (shaded, right justified, bold font).
0.1 Value listed is measured concentration (no shading, right justified).
TABLE 3SOIL GAS PROBE ANALYTICAL RESULTSMULTI-LEVEL SOIL GAS PROBE STUDY
PALOS VERDES LANDFILL
ANALYTE UNITS VN1-10N VN1-20 VN1-34 VN2-11 VN2-29 VN2-41 VN3-13 VN3-23.5 VN3-315/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06
FIXED GASES (GEM 500)Carbon Dioxide %V 10.2 20.4 10.8 1.7 0 0 1.5 0.1 0Methane %V 0 0 0 0 0 0 0 0 0.5Nitrogen %V 84.8 79.3 76.8 84.3 79.0 79.4 81.3 79.9 81.9Oxygen %V 5.2 0.2 10.8 14 20.5 20.6 17.2 20.2 17.9Total Organic Compounds ppm 5 450 400 55 90 80 100 >1000 >1000
TOTAL ORGANIC COMPOUNDS (EPA Method 25)TOC Non-Methane ppmV 6.34 4.39 1.23 5.82 7.77 2.67 9.05 9.94 2.23TOC with Methane ppmV 6.34 1160 356 2020 7.77 2.67 9.05 90 2050
VOLATILE ORGANIC COMPOUNDS (EPA Method TO-14)Benzene ppbV 0.98 2.4 6.4 6.6 3.0 9.2 15 7.1 5.1Bromomethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.211,3-Butadiene ppbV 2.1 1.5 17 44 6.6 56 7.3 38 145Carbon tetrachloride ppbV 0.19 0.19 0.19 0.19 0.19 0.19 0.19 0.19 0.19Chlorobenzene ppbV 0.21 2.9 29 0.21 0.21 1.6 19 2.3 1.7Chloroethane ppbV 0.3 0.3 1.8 0.3 0.3 0.3 0.3 0.3 0.3Chloroform ppbV 2.7 0.23 0.23 0.23 0.23 0.23 0.23 0.23 0.23Chloromethane ppbV 0.18 0.18 0.18 2.6 0.18 2.0 0.18 1.8 9.21,2-Dibromoethane ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.181,2-Dichlorobenzene ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.181,3-Dichlorobenzene ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.181,4-Dichlorobenzene ppbV 0.2 0.2 0.2 0.2 2.7 0.2 13 3.5 2.7Dichlorodifluoromethane (Freon-12) ppbV 39 335 296 1.4 0.18 0.18 4.8 2.6 1.91,1-Dichloroethane ppbV 0.21 3.4 244 0.21 0.21 0.21 13 0.21 0.211,2-Dichloroethane ppbV 0.19 0.19 12 0.19 0.19 0.19 0.19 0.19 0.191,1-Dichloroethene ppbV 0.23 0.23 2.5 0.23 0.23 4.5 0.23 1.5 0.23cis-1,2-Dichloroethene ppbV 0.19 0.19 0.19 0.19 0.19 0.19 7.8 3.4 3.11,2-Dichloropropane ppbV 0.17 0.17 3.3 0.17 0.17 0.17 0.17 0.17 0.17cis-1,3-Dichloropropene ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21trans-1,3-Dichloropropene ppbV 0.14 0.14 0.14 0.14 0.14 0.14 0.14 0.14 0.141,2-Dichlorotetrafluoroethane (F-114) ppbV 4.3 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.184-Ethyltoluene ppbV 1.5 0.21 0.21 0.21 0.21 2.1 1.5 1.8 1.6Ethylbenzene ppbV 1.6 1.8 1.8 2.1 2.3 4.0 4.7 3.7 3.0Hexachloro-1,3-butadiene ppbV 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26Methylene chloride ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18Styrene ppbV 1.5 1.8 1.3 0.16 1.5 2.1 1.5 1.7 1.51,1,2,2-Tetrachloroethane ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18Tetrachloroethene (PCE) ppbV 36 31 11 0.21 0.21 0.21 3.4 1.8 0.21Toluene ppbV 8.6 7.6 34 48 51 85 49 96 541,2,4-Trichlorobenzene ppbV 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.261,1,1-Trichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.211,1,2-Trichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21Trichloroethene (TCE) ppbV 2.0 4.1 22 0.21 0.21 0.21 2.1 0.21 0.21Trichlorofluoromethane (Freon-11) ppbV 5.1 116 1.8 1.1 0.2 0.2 0.2 0.2 0.21,1,2-Trichlorotrifluoroethane (F-113) ppbV 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.21,2,4-Trimethylbenzene ppbV 3.8 3.4 2.9 2.4 3.2 4.9 6.1 6.9 6.31,3,5-Trimethylbenzene ppbV 1.4 1.1 1.1 1.3 1.4 2.2 4.3 3.4 3.1Vinyl chloride ppbV 0.17 2.1 121 0.17 0.17 0.17 0.17 3.5 1.7m,p-Xylene ppbV 2.4 2.2 2.2 2.5 3.0 5.5 3.5 4.3 3.7o-Xylene ppbV 2.2 2.4 2.5 2.2 2.2 3.9 5.9 5.4 4.7
EPA U.S. Environmental Protection Agency%V percent by Volume
MDL Method Detection LimitPQL Practical Quantitation Limitppm parts per million
ppmV parts per million by volumeppbV parts per billion by volumeTOC Total Organic Carbon
0.1 Not detected above MDL; value listed is MDL (shaded, left justified).
0.1 Value listed is estimated concentration, between MDL and PQL (shaded, right justified, bold font).
0.1 Value listed is measured concentration (no shading, right justified).
TABLE 3 (CONT'D)SOIL GAS PROBE ANALYTICAL RESULTSMULTI-LEVEL SOIL GAS PROBE STUDY
PALOS VERDES LANDFILL
ANALYTE UNITS VN4-7 VN4-23 VN4-31 VN5-16 VN5-31 VN5-47.5 VN6-15 VN6-29 VN6-415/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06 5/31/06
FIXED GASESCarbon Dioxide %V 0 2.3 1.8 1.9 15.4 29.0 4.8 9.2 76.0Methane %V 0 0.1 0.4 0 0 0.5 0 0 0Nitrogen %V 79.8 81.2 81.0 83.1 80.3 70.1 78.6 79 23.2Oxygen %V 20.2 16.2 16.6 14.9 4.4 0 16.4 11.9 0.7Total Organic Compounds ppm 3 900 >1000 4 19 >1000 3 10 700
TOTAL ORGANIC COMPOUNDS (EPA Method 25)TOC Non-Methane ppmV 1.95 9.45 6.03 9.12 12.7 1.91 4.27 13.8 5.79TOC with Methane ppmV 1.95 599 3080 8460 12.7 6740 4.27 48.9 1520
VOLATILE ORGANIC COMPOUNDS (EPA Method TO-14)Benzene ppbV 0.17 13 92 5.1 4.7 2.0 1.1 4.0 8.5Bromomethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.211,3-Butadiene ppbV 0.26 35 27 3.3 2.3 8.0 0.26 8.9 35Carbon tetrachloride ppbV 0.19 0.19 0.19 0.19 0.19 0.19 0.19 0.19 0.19Chlorobenzene ppbV 0.21 2.3 2.2 0.21 0.21 0.21 0.21 1.2 0.21Chloroethane ppbV 0.3 0.3 0.3 0.3 0.3 0.3 0.3 0.3 0.3Chloroform ppbV 0.23 0.23 0.23 5.1 0.23 0.23 0.23 4.1 0.23Chloromethane ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.181,2-Dibromoethane ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.181,2-Dichlorobenzene ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.181,3-Dichlorobenzene ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.181,4-Dichlorobenzene ppbV 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2Dichlorodifluoromethane (Freon-12) ppbV 0.18 0.18 0.18 4.1 3.0 71 0.18 17 0.181,1-Dichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.211,2-Dichloroethane ppbV 0.19 0.19 0.19 0.19 0.19 0.19 0.19 0.19 0.191,1-Dichloroethene ppbV 0.23 7.8 42 0.23 0.23 6.3 0.23 1.0 0.23cis-1,2-Dichloroethene ppbV 0.19 178 0.19 0.19 0.19 4.1 0.19 1.2 0.191,2-Dichloropropane ppbV 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17cis-1,3-Dichloropropene ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21trans-1,3-Dichloropropene ppbV 0.14 0.14 0.14 0.14 0.14 0.14 0.14 0.14 0.141,2-Dichlorotetrafluoroethane (F-114) ppbV 0.18 0.18 4.3 0.18 0.18 2.7 0.18 0.18 0.184-Ethyltoluene ppbV 0.21 0.21 0.21 6.2 6.4 1.5 0.21 7.4 0.21Ethylbenzene ppbV 0.17 1.5 8.1 6.6 6.8 2.4 0.17 11 0.17Hexachloro-1,3-butadiene ppbV 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26Methylene chloride ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18Styrene ppbV 0.16 0.16 0.16 2.0 2.3 1.7 2.0 2.8 0.161,1,2,2-Tetrachloroethane ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18 0.18Tetrachloroethene (PCE) ppbV 0.21 2.7 1.8 6.3 5.9 193 3.3 19 0.21Toluene ppbV 3.4 8.4 33 51 41 41 0.2 14.1 751,2,4-Trichlorobenzene ppbV 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.261,1,1-Trichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.211,1,2-Trichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21Trichloroethene (TCE) ppbV 0.21 0.21 0.21 0.21 0.21 37 0.21 7.5 0.21Trichlorofluoromethane (Freon-11) ppbV 0.2 0.2 0.2 1.6 1.6 2.6 0.2 3.4 0.21,1,2-Trichlorotrifluoroethane (F-113) ppbV 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.21,2,4-Trimethylbenzene ppbV 0.2 1.4 2.8 5.4 5.6 3.9 1.5 4.0 0.21,3,5-Trimethylbenzene ppbV 0.18 0.18 1.3 4.4 4.6 1.9 0.18 4.8 0.18Vinyl chloride ppbV 0.17 19 310 0.17 0.17 2.8 0.17 0.17 0.17m,p-Xylene ppbV 0.37 1.3 4.1 6.7 7.5 3.1 1.0 7.0 0.37o-Xylene ppbV 0.19 1.1 2.2 11 12 3.0 1.1 13 0.19
EPA U.S. Environmental Protection Agency%V percent by Volume
MDL Method Detection LimitPQL Practical Quantitation Limitppm parts per million
ppmV parts per million by volumeppbV parts per billion by volumeTOC Total Organic Carbon
0.1 Not detected above MDL; value listed is MDL (shaded, left justified).
0.1 Value listed is estimated concentration, between MDL and PQL (shaded, right justified, bold font).
0.1 Value listed is measured concentration (no shading, right justified).
TABLE 4QA/QC RESULTS
MULTI-LEVEL SOIL GAS PROBE STUDYPALOS VERDES LANDFILL
ANALYTE UNITS Duplicate Sample 1 Duplicate Sample 2 QCTB Method MethodVN2-11 VN-DUP1 VN6-15 VN-DUP2 5/31/06 Blank 1 Blank 2
TOTAL ORGANIC COMPOUNDS (EPA Method 25)TOC Non-Methane ppmV 5.82 6.09 4.27 5.38 NA 1 1TOC with Methane ppmV 2020 56.1 4.27 5.38 NA 1 1
VOLATILE ORGANIC COMPOUNDS (EPA Method TO-14)Benzene ppbV 6.6 7.3 1.1 1.5 0.17 0.17 0.17Bromomethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.211,3-Butadiene ppbV 44 33 0.26 2.7 0.26 0.26 0.26Carbon tetrachloride ppbV 0.19 0.19 0.19 0.19 0.19 0.19 0.19Chlorobenzene ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21Chloroethane ppbV 0.3 0.3 0.3 0.3 0.30 0.30 0.30Chloroform ppbV 0.23 0.23 0.23 0.23 0.23 0.23 0.23Chloromethane ppbV 2.6 2.5 0.18 0.18 0.18 0.18 0.181,2-Dibromoethane ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.181,2-Dichlorobenzene ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.181,3-Dichlorobenzene ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.181,4-Dichlorobenzene ppbV 0.2 0.2 0.2 0.2 0.2 0.2 0.2Dichlorodifluoromethane (Freon-12) ppbV 1.4 0.2 0.18 2.2 0.18 0.18 0.181,1-Dichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.211,2-Dichloroethane ppbV 0.19 0.19 0.19 0.19 0.19 0.19 0.191,1-Dichloroethene ppbV 0.23 0.23 0.23 0.23 0.23 0.23 0.23cis-1,2-Dichloroethene ppbV 0.19 0.19 0.19 0.19 0.19 0.19 0.191,2-Dichloropropane ppbV 0.17 0.17 0.17 0.17 0.17 0.17 0.17cis-1,3-Dichloropropene ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21trans-1,3-Dichloropropene ppbV 0.14 0.14 0.14 0.14 0.14 0.14 0.141,2-Dichlorotetrafluoroethane (F-114) ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.184-Ethyltoluene ppbV 0.21 1.6 0.21 0.21 0.21 0.21 0.21Ethylbenzene ppbV 2.1 2.6 0.17 0.17 0.17 0.17 0.17Hexachloro-1,3-butadiene ppbV 0.26 0.26 0.26 0.26 0.26 0.26 0.26Methylene chloride ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18Styrene ppbV 0.16 2.1 2.0 0.16 0.16 0.16 0.161,1,2,2-Tetrachloroethane ppbV 0.18 0.18 0.18 0.18 0.18 0.18 0.18Tetrachloroethene (PCE) ppbV 0.21 0.21 3.3 3.3 0.21 0.21 0.21Toluene ppbV 48 68 0.2 1.6 0.20 0.20 0.201,2,4-Trichlorobenzene ppbV 0.26 0.26 0.26 0.26 0.26 0.26 0.261,1,1-Trichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.211,1,2-Trichloroethane ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21Trichloroethene (TCE) ppbV 0.21 0.21 0.21 0.21 0.21 0.21 0.21Trichlorofluoromethane (Freon-11) ppbV 1.1 0.2 0.2 0.2 0.2 0.2 0.21,1,2-Trichlorotrifluoroethane (F-113) ppbV 0.2 0.2 0.2 0.2 0.2 0.2 0.21,2,4-Trimethylbenzene ppbV 2.4 2.6 1.5 1.5 0.20 0.20 0.201,3,5-Trimethylbenzene ppbV 1.3 1.6 0.18 0.18 0.18 0.18 0.18Vinyl chloride ppbV 0.17 0.17 0.17 0.17 0.17 0.17 0.17m,p-Xylene ppbV 2.5 3.0 1.0 0.37 0.37 0.37 0.37o-Xylene ppbV 2.2 2.4 1.1 0.19 0.19 0.19 0.19
EPA U.S. Environmental Protection AgencyMDL Method Detection LimitppbV parts per billion by volumeppmV parts per million by volumePQL Practical Quantitation Limit
QA/QC Quality Assurance/Quality ControlQCTB Quality Control Trip BlankTOC Total Organic Carbon
0.1 Not detected above MDL; value listed is MDL (shaded, left justified).
0.1 Value listed is estimated concentration, between MDL and PQL (shaded, right justified, bold font
0.1 Value listed is measured concentration (no shading, right justified).
REFERENCE:BASE MAP PROVIDED BY COUNTY SANITATION DISTRICTS OFLOS ANGELES COUNTY; TOPOGRAPHY AS OF 10/08/2002.
EXPLANATION:(;) SINGLE-LEVEL GAS PROBEQ MULTI-LEVEL GAS PROBE
- - - - - - HISTORICAL SURFACE DRAINAGE- - - - LANDFILL BOUNDARY
SCALE: 1"=100'
Geologists, Hydrogeologists, and Engineers
QRAWN BY: DATE: JOB NO.'I\. FEBRlIARY 2001 2006-088
Geologic Associates BORING NO.: VN-1Boring Log PAGE: 1 Of 1
JOB NO.: 2006--0088 DAlE STARlED: 5/09/06 c:w DEP1H: 41.21 feetSITE LOCATION: PAlDS VERDES lANDfIll DAlE FINISHED: 5/09/06 lUrA!. 0EP1H: 46.5 feet
ORlWNG METHOD: CONJ1OUS CORE - HSA ELEVATION: 248.19CONlRAClllR: ABC-UOVIN NORIHING: 1747555.35
LOGGED BY: J. SAPP, CHG E'ASIlNG: 6455431.05
ll!El E' ~~ d1!; z ~gb~~
1Il13 zAD §~ ~ ~~ ~~~l1ME (PfII) RQO ~6a>g Q.z Q.
~1!;!i ~~~ DESCRIP1l0N COMMENTSIll'" ~c ~ 0
9:25 - ML FILL: Hand auger to 5 feet,
- Brown to yellowish brown (IOYR 5/3 10 5/4), weed matting material @ 3well-sorled. fine CLAYEY SILT with minor inches.
- angular rock fragments. roots.-
0 0 0
9:45 26 2.5 1 -...(6'-10') - minor wood and plastic-
-fragments; brass nail.
-
1...(10') - color change to dark grayish brown20 2.5 2 -
- (10YR 4/2).0 76 57
- ...(12.5') - section of fan belt.- ...(14') - dense, color change to mottled light
1 brownish gray and very dark gray (2.5Y 6/218 2.5 3 - and 3/1).'--
95 100 95 ...(14.5') - loose.
'--ML Weathered, mottled, massive, light brownish
gray to yellowish (lYR 6/2 to 5/4), poorly
30 2.5 4 '--indurated SANDY SILT with fine-grained. ...(20') - damp cullings.
I--angular, diatomaceous rock fragments.
57 100 90'--
...(21'-21.5') - coarse SANDY lens.
I-- ...(22') - color commonly yellowish brown(10YR 5/4).
36 2.5 5 I-- r-, ...(24') - thin SILTY SAND lenses.
'-- ML- Very dark grayish brown (IOYR 3/2) 1028 95 71 I-- CL mottled grayish brown (IOYR to 2.5YR 5/2),
'-- well-sorted, fine SANDY SILT to SANDY CLAYwith scattered, angular rock fragments.
58 2.5 6 '-- ...(27'-28') - abundant froctures. ...(30') - pulled bock
I-- auger to 20' bgs, wait for2.5 76 57
'-- ...(32.5'-35') - highly weathered andwater from 11 :30 to 12:00
I-- fractured, iron-oxide staining, angular,but no free water.
cemenled SANDSTONE rock fragments.11 2.5 7 I--
...(37') - very dark grayish brown (10YR 3/2).I--
77 76 48 I-- ...(38'-40') - abundant fractures with
I-- shattered/broken concretions....(40'-41') - fine-grained, cemented
50/6" 2.5 NSR I-- ~ concretion.
I-- ...(40'-43') - very loose, poorly indurated, ...(45') - free water on120 76 14 I-- angular rock fragments. barrel of sample No.8;
I-- ...(44'-44.5') - CLAYEY lens. SWL=41.21' bas 01 13:40.
1/ Notes:
13:00 0 0 0 36 2.5 8 I--
I-- 1. Total depth of boring 46.5 feet.2. Groundwater measured at 41.21 feet below
I-- grade.I-- 3. Dual-nested gas probe constructed in
boring with implants installed at 20 and 34I-- feel below grade.I-- 4. Soil sample numbers 4 and 6 selected for
labarolarv testino.
Tho dala prosented on thl. log I. a .lmpllflcalJan of actual candlllan. oncountered and appllos only al tho location of thl. baringand al tho tim. of drilling. Sub.urfaco condlllon. may diffor al othor location. and may chango with tho pooaago of tlmo.
Geologic Associates BORING NO.: VN-2Boring Log PAGE:: 1 OF 1
JOB NO.: 2006-0088 DATE SfARJED: 5/05/06 /111 DEPlH: HESITE lllCATION: PALOS VERDES lANDRLL DATE RNISHED: 5/05/06 lllTAi. DEPTil: 51.5 feet
DRIWNG IIE1HOD: CONnOUS CORE - HSA ElfVATION: 308.11CONTRACTOR: ABC-UlMN NORTHING: 1746175.74
lOGGED BY: J. SAPP, CIIG EASIlNG: 6456825.76
ll!El 'i! ~ffi'd
~ z ~~I~~I
zllME ~ RQD ~~ :i!i5 ~ ~m ~m~ fi:~
0 .... "'g Q.
~~~~ ~fZ DE5CRIP110N COMMENlSR'" 5l~ ~ c
9:00 Asphalt and bose rock over fill soil. Hand auger to 5 feet.Asphalt over base rock.
I- MI. FII.I.:Pole brown to brown (10YR 6/3 to 5/3). Split spoon hammer
" \well-sorted SANOY SILT with scattered (140 lb., 30" stroke).
32 2.5 1 ~ , diatomaceous/siliceous rock fragments, and
I-rounded granitic GRAVEL and COBBLES.
0 55 36~
SM Pole brown to light yellowish brown (10YR 6/3;
to 6/4). well-sorted, fine SILTY SANa withI-scattered GRAVEL clasts.
1 ,28 2.5 2 I-
~ .a 95 48
I- " ...(12'-13') - fractures.;
~
1 "21 2.5 3 I- WEATHERED MAU.GA MEMBER:
I-Weathered, mottled light olive gray to pole
a 95 48~
olive (5Y 6/2 to 6/3), massive, fine-grainedMUDSTONE with oxidized fracture surfaces.
I- ...(17') - color change to greenish gray9/6" 2.5 4 l- I""
(5/10Y to 5/GY)....(19') - shallow fracture.
a 57 38~
MAU.GA MEMBER:I-
~Drak gray (2.5/10Y) to drok olive groy (5Y3/2), massive, commonly petraliferaus
63 2.5 5 ~MUDSTONE with minor amounts of radiolaria
I-scattered through the rock.
.
0 95 95~
I-...(29') - steep fractures.
50 2.5 6 I- ...(30'-35') - massive.
0 98 76 ~
I-
~
69 2.5 7 ~
0 95 95I-
~...(37'-40') - abundant shallow-dipping
I-- fractures.
92/11" 2.5 8 I-- ...(40') - shallow fractures on 3" - 4"
I--centers and filled with light gray SILTY SAND.
0 95 71I--
I-- ...(43'-45') - fractures dip more steeply thanabove.
73/"" 2.5 9 I--
1/Notes:
a 0 a l- I. Total depth of boring 51 feet.I-- 2. No groundwater encountered.I- 3. Triple-nested gas probe constructed in
12:00 2.5 10boring with implants installed at 11, 29,and 4I feet below grade.
I- 4. Soil sample numbers 2, 6 and 8 selectedfor laboratory testing.
The data presented on this log Is a slmplfficatlon af aclual condlllons encounlored and applies anly at the location of this boringand at the lime af drilling. Subsurface condilians may differ at ather Iocatlans and may change with the po_ge at lime.
Geologic Associates BORING NO.: VN-3Boring Log PAGE: 1 OF 1
. JOB NO.: 2llll6-ooas IlAlE SfARTED: 5/08/06 GIl DEPTH: NESITE UlCA11ON: PALOS VERDES lANDRll IlAlE FINISHED: 5/08/06 TOrA!. DEPTH: 51.5 feel
DRIWNG METHOD: CONnOUS CORE - HSA El£VA11ON: 314.92CONTRACTOR: AIlC-lKl'IIN NORTHING: 1748103.84
LOGGED BY: J. SAPP, CHG E"ASI1NG: 8456892.09
ll1lil 'il ~13ci ;;; z ~gO~~z
FlO!~ ~ ~~ ~~~TIME (PPII) RQD ~:I:
ILO IL
~;;; i ~~e DESCRIPTION COMMENTS~~ a 5l S ~ c
7:15 Asphalt over boserock. Hand auger to 5 feet.
I--- SM FILL:,Gray to olive gray (5Y 5/1 to 5/2), veryI--
I--- , well-sarled, fine-grained SILTY SAND., ...(3') - rounded GRAVEL.
13 2.5 1 I--- , ...(5') - mottled pole yellow (5Y 7/3).
I-- .'517 100 71 ;
I--- ,I--
, ...(8'-10') - poorly indurated, friable.';
119 2.5 2 I--
1146 81I---
14 I-- ...(12'-14.5') - poorly induraled, friable.
I--- ,1
,22 2.5 3 I--- ,.
N/A 86 71I--- WEATHERED MALAGA MEMBER:
I-- Weathered, mottled, dark grayish brown (1OYR4/2), massive, fine-grained MUDSTONE with
23 2.5 4 I-- oxidized fracture surfaces.
I---...(20') - gray to drak gray (5Y 5/1 10 4/1).
6230 86 71 I-- ...(23'-24') - poorly indurated, friable.
MALAGA MEMBER:67 2.5 5 I--- Drak gray (2.5/10Y) to drak olive gray (5Y
I-- 3/2), massive, commonly petroliferous4200 100 62
I--- MUDSTONE with minor amounts of radiolaria
I--scattered through the rock.
...(25'-27.5') - fraclured.
80 2.5 6 I-- ...(29.5') - waxy surfaced, high-angle fracture
I--- filled wilh 2-inch light gray SAND.>6547 90 86 I-- ...(30'-33') - shallow fraclures and
I--- interbedded light gray SANDY lenses.
81/9" 2.5 7 I---
4480 96 95I-- ...(36.5'-38') - poorly induraled.I--- ...(38'-39') - silicic concretion surrounded byI-- olive (5Y 5/3) SILTY SANDSTONE; shallow
90/9"fractures.
2.5 8 I-- ...(41.5'-45') - half-inch, lighl gray, SILTYI--- lenses on 6-inch centers, very shallow Clip.
1917 100 100 I-- ...(46') - 1/8" thick SILT-filled vertlcol joints.I--- ...(50') - several vertical, sleep and shallow No free water in boring.
fractures.50/6" 2.5 9 I---
IINoles:
220 100 86I---
1. Total depth of boring 51.5 feet.I--- 2. No groundwater encountered.I--- 3. Triple-nested gas probe constructed in
boring with implants inslalled 01 13, 23.5,10:20 92 2.5 10 I--- and 31 feet below grade.
I-- 4. Soil sample numbers 2. 4 and 6 selectedfor laboralary lesting.
The data presented on this log Is a simplification of actual conditions encountered and appllee only at the Iocotlan of this boringand at the time of drilling. Subsurface conditions may differ at other Iocotlans and may change with the passage of time.
Geologic AssociatesBoring Log
BORING NO.: VN-4PAGE: 1 OF 1
JOB NO,: 200B-ooBBSITE LOCATION: PAlOS 'IERIlES lANDRU.
DRIlliNG MElHOD: CONTIOUS CORE - HSACONlRACIOR: ABC-UOYIN
LOGGED BY: J. SAPP. CHG
D.\TE SfARTED: 5/08/0BD.\TE RNISHED: 5/10/0B
E1£VATION: 333.53NORIHING: 1745600.02
E'ASI1NG: B457391.J8
r;w IlEPIH: NETOrAL DEPTH: 51.5 feet
DESCRIPTION COMMENlS
13:45 Aspholl/boserock over fill. Hand cuqer to 5 feel.
Asphalt over boserock.
...(5'-12') - encounteredlandfill 90S collectiontrench.
-
!--- ~ SC- FILL:s-!+--+--li~t;{'EI,.' CL Grayish brown (lDYR 5/2), poorly sorted, fine
;:y.;;1'\. CLAYEY SAND to SANDY CLAY with rounded",,::1 "pebble GRAVEL.:t.;;; GP Brown (10YR 5/3). well-sorted, rounded,,,\; coarse COBBLES with minor SANDY CLAY to:>t'~.)~ SANDY SILT,:.y,~, .~ ..~~......~.•~
10-1-1---1-
NSR2.517
N/A N/A N/A
14:15
66/11" 2.5
N/A N/A N/A
2.6 100 95
1.9 86 71
15:10
5/097:15
20.3
7:25e--+---+---1
91.1
7:481---1----1------':
8:15
29
39
50
50/6"
88
50/6"
2.5
2.5
2.5
2.5
2.5
2.5
2
3
4
5
6
7
NSR
--
1W-+
-!--!---
!--
!--!--
!---
!--!--
!---
!--
!--!--
!---
I-I-
I-I--
Grayish brawn (10YR 5/2), poorly sorted, fineCLAYEY SAND to SANDY CLAY with roundedpebble GRAVEL.
WEATHERED MAlAGA MEMBER:Brown to yellowish brown (10YR 5/3 to 5/4),with yellow to olive yellow mottling (5Y 6/8 to7/8), fine-grained MUDSTONE withsubhorizontol bedding..•.(19'-22') - iron-oxide staining onsubhorizontal bedding planes.
...(22'-24') - severely fractured/breccioted,friable....(25') - block-stained near horizontolcontact....(26') - mottled.
MALAGA MEMBER:Drok gray (2.5/10Y) to drok olive gray (5Y3/2), massive, commonly petraliferousMUDSTONE with minor amounts of radiolariascattered through the rock....(31') - light green SANDY lens alongshollow-dipping bedding plane.
...(25') - borehole notplumb, unable to continuecoring, begin collectingdrive samples at 2.5'intervals.
97/10" 2.5
No free woter in boring.
Notes:
...(44') - opproximote 45' bedding plane withlight groy SILTY SAND coating.
/
1. Total depth of boring 51.5 feel.2. No groundwater encountered.3. Dual-nested gos probe constructed in
boring with implants installed at 23 and 31feet below qrode.
4. Soil sample numbers 2 ond 5 selected forloboratory testing.
I-I-
I-I--
I-
I-I-
I--
1--1----1--1I--
9
8
11
12
10
2.5
2.5
2.5
91/9"
50/6"
90/10" 2.5
50/3"
5/1015:25
16:30
The data presented on this log Is a slmpRflcaUon of actual conditions encountered and applies only at ths location of this boringand at the time of drilling, Subsurface conditions may differ at othsr locations and may change with ths paBBOge of time.
Geologic Associates BORING NO.: VN-6BorIng Log PAGE: 1 OF 1
JOB NO.: 2006-0088 DAlE SfARTED: 5/10/06 GW OEPIH: NESIJE 1.OCA11ON: PAlOS VEROES lANOFIU. DAlE FINISHED: 5/10/06 TOTAl. OEPJH: 51.5 feel
ORlLllNG MEIHOO: CONl1OUS CORE - HSA ElfVA11ON: 343.38CONTRACIllR: ABC-I.JC'IIN NORTHING: 174J912.12
LOGGED BY: J, SAPP, CHG E'ASIING: 6457849,57
lli!1il ~
~ffi'd
~~Ii: z ;!; z :!!!~ Ii§
flO !i ~ ~~ ~~~ril~TIME (PPM) RQD :;!6 ...~;!;~ ~ ~fZ DESCRIPTION COMMENTS
Mlli! g ~~ ~ c
7:40I--
, SM- FILL: Hand auger to 5 feet.
I--- , ML Weathered, lighl brownish gray (2.5Y 6/2),
I-- .' well-sarled, fine SILTY SAND to SANDY SILTwith minor amaunls of pebble GRAVEL and
I--- CLAY, with diatomaceous/chalky rock,8:20 38 2,5 1
fragments.I--- "I--
,...(6.5'-9.5') - very loose. poorly consolidated.12 62 15
I--- .I-- ..
134 2.5 2 I--
,a 67 50
I---...(12.5'-14') - very loose, poorly
I-- .' consolidated.I--- ...(13') - rool; block 2-inch lens of organic
1,
material.8:40 35 2.5 3 I--- ...(15') - color change to light yellowish brown
I--,
to light olive brown (2.5Y 6/3 to 5/3).a a aI--- ...(17'-1 s') - cemented, fine-grained ...(17.5') - encountered,I-- concretion. refusual during coring.
37 2.5 NSR I-- ML Dense, very dark grayish brown (lOYR 3/2),
I--- very well-sorled SANDY SILT with CLAY and3.1 33 a I--
scattered debris....(21') - minor gloss shards, paper.
I---...(24') - weathered, mottled.
9:30 26 2.5 4 I--- ML Pole yellow (2.5Y 7/3), very well-sorted, fine
I--CL CLAYEY SILT 10 SILTY CLAY with scattered
a 79 62 iron-oxide stains and poorly consolidatedI--- lenses.I-- ...(26') - high-angle porting, surface is
iron-oxide stained. ...(30'-35') - damp, very31 2.5 5 I-- ...(27'-29') - loose, unconsolidated.I--- ...(29') - color change to primarily light gray
sticky•a 67 48
I-- (2.5Y 7/2) with pole yellowish maUling.I--- ...(33.5') - horizontal surface dipping -45'
and coated with fine SAND veneer.20 2.5 6 I--- ...(34.5') - smail-diameter, block organic
I-- material.a 100 86I---
I-- ...(40'-45') - less consolidated, more oxidizedthan above.
23 2.5 7 I-- ...(42'-43') - very loose, unconsolidated lens.
I--- ...(47.5'-48.5') - friable, with limanile/17 67 57 I-- hematite staining.
I--- ...(49') - 2-inch thick gypsum-filled shearzone filled with punky concretion; color change
26 2.5 8 I--- to brown (7.5YR 5/4).
I---
1/Notes:
a 88 57I--
1. Total depth of boring 51.5 feet.2. No groundwater encountered.
I--- 3. Triple-nested gas probe constructed in
41 2.5 9boring with implants inslalled at 15, 29,
11:20 I--- and 41 feel below grade.I-- 4. Soil sample numbers 3, 5, and 7 selected
for laboratory testing.
The data prosented on thle log Is a slmpliflaatlan of actual conditions encountered and applies only at the location of this boringand at the lime of drillln9. Subsurface conditions may differ at other looalIans and may change with the passage of lime.
Geologic AssociatesBoring Log
BORING NO.: VN 1-1 ONPAGE: 1 Of 1
JOB NO,: 2lllJ6-1lO88SITE LOCAllON: PALOS VERDES lANDAU.
DRIWNG IIE1HOD: HAND AUGERCONIRACfOR: ABC-LKMN
LOGGED BY: J. SAPP, CHG
DATE SfARIED: 5/12/06DATE FINISHED: 5/12/06
ELEVATION: 246.17NORTHING: 1747580.37
E'ASIING: 6455444.79
GIl DEPIH: NETOTAL DEPIH: 11 feet
liME
ll!lilflO 8 e:!
(PPM) ~~ OESCRIP110N COMMENTS
13:55
15:10
I---
I--I---
I--
I--l-
I--I-
1
I--l-
I--1
I--l-
I--I---
I---
I--I---
I--
I--I---
I--I---
I---
I--I---
I--
I--I---
I--I---
I---
I--I---
I---
I---
I--I---
I--
I--I-
.. SM FILL: Hand auger to 11 feet.~ Dark grayish brown (10YR 4/2), poorly sorted.
fine to medium SILTY SAND....(0' -3') - roots.
...(5') - black and gray mottllnq.Damp cultings.
Nates:
1. Total depth of baring 11 feet.2. No graundwaler encountered.3. Single gas probe constructed in boring with
implant installed at 10 feet below grade.4. 50;1 Sample collected from 10 feet for
laboralory testing.
The data presented on this log Is a simplification of actual conditions encountered and applies only ot the location of this boringand ot the time of drilling. Subsurface conditions may differ ot other locations and may change with the passage of time,
Geologic Associates BORING NO.: VN4-7Boring Log PAGE: 1 Of 1
JOB NO.: 2006--llllll1l Il.\TE STARTED: 5/12/06 GIl DEPIH: NESITE LllCAl1ON: PALOS VERDES lANDFIll Il.\TE FINISHED: 5/12/06 TOTAL DEPIH: 10 feel
DRIWNG IolElHOD: HAND AUGER . El.E.VAl1ON: 333.53CONlRACIOR: AIlC-UOVIN NORTHING: 1745603.42
LOGGED BY: J. SAPP, CHG E'ASI1NG: 6457394.63
llifi:l~
~13ciIi: z ;!l; z ;!!
-J liSflO
~~ fQ~~ ~~ ~~~ lil ~TIME (PPM) :i!i'5
0", :il 6 ~!. ~ ~;!l;~~~ DESCRIPTION COMMENTSM'" S Q
10:10I-- Asphalt over baserock. Hand auger to 10 feet.
I--
I-- ~•.SC FILL:CL Grayish brawn (10YR 5/2), poorly sorted, fine
CLAYEY SAND to SANDY CLAY with roundedI-- pebble GRAVEL.
I--ML Pole yellow to light gray (2.5Y 7/3 to 7/2),
I--fine SANDY SILT.
12:301 Notes: ...(10') - unable to retainI--
undisturbed drive sampleI-- 1. Total depth of boring 10 feet. due to soil sampling barrelI-- 2. No groundwater encountered. lodged in boring.I-- 3. Single gas probe constructed in boring with
1 implant installed at 7 feet below grade.I-- 4. No ·soil sample retained from boring.
I----
----
-
I--
I--'--
----
I--I--
I--I--
I--I--
I--I--
I--
I--I--
I--
I--
f--
The data presented on this log Is a slmpllflcaUon of actual conditions encountsred and applies only at the locaUon of this baringand at the time of drilling. Subsurfaco conditions may differ at other locaUons and may change with the poBBOge of time.
GeoLogic Associates
SOIL GAS PROBE COMPLETION SUMMARYWELL NO.:
PAGE: 1 OF 1
VN-1
JOB NO.: 2006-00BBPROJECT: MULTI-LEVEL SOIL GAS PROBE STUOY
LOCATION: PALOS VEROES lANOFlLLINSPECTOR: J. SAPP. CHG
CHECKED BY: M. REASON, CHG
ELEVATION GROUND LEVEl.: 248.09ELEVATION TOP OF VAULT: 248.19
DATE STARTED: 5/09/0BDATE FINISHED: 5/09/06
TOTAL DEPTH: N/A
0--
5-
10-
15-
20-
25-
30-
35-
40--
45--
50--
55-
60-
65-
1111111.1.1.0000 " "
DRILLING SUMMARY: WELL CONSTRUCTION LOG:Start Flnllh
Toiol Deplh: 45 feet Oat. TIm. Oat. Tim.Borehole dlomeler: B" Drilling (Contlnuou. Co,,): 5/r»/rKJ t.25 5/r»/rKJ 13:00Driller: ABC-UOVIN
CME-75Probe Conltructlon: 5/r»/rKJ 13:20 5/r»/rKJ 15:30
Rig:Blleo): N/A
Drilling Fluid: N/A
Prolectlve Cooing: Hollow-stem augers.
WELL CONSTRUCTION DETAILS:
[I] Pipe: 1" dJomotor, flush-ih...ded Sch.80 PJC fflled with bentonite.(From 0.5 ill 35.2 feet.)
o=JTublng: 1/4" dIomotor poIyethyIano -WELL DEVELOPMENT LOG:
Shallow (ORInge) ill 10 foot, Start Flnllh
Intormedlolo (green) ill 2D foot,Oat. Tim. TIm.
Deep (blue) ill 34 feet. Surgo Block
I I IProbe: 316 stoinleos sleoI soli ¥cpo!" Bailinglmplont.(At 20 ond 34 feet.) Pumping
Totol GoUono Removed:
~Bonlonlte W)o-Ben Enviroplug, medium.Chip Soal: (From 11.3 ill 13.5 foot, STABILIZATION TEST DATA:
from 21.1 ill 24 foot, Gallon. pH sp••. Con~ (,../c~ Temp r-F)from 31.1 ill 33 foot ondfrom 35.2 ill 45 feet.)
r 'in] FUler Pock: Common:lol 12/12 tolontoreytypo oond.(From 9 ill 11.3 foot,from 19.1 ill 21.1 foot ondfrom 33 ill 35.2 feet.)
Granular W)o-Ben No. 6.rOOOOOOg~000000000001>000000 Benlonlte (From 4.8 ill 11.5 foot,
Sool: from 17.5 ill 19.1 foot and Comments:from 28.B ill 31.1 feet.) Probe finished at the surface with
~GrOUI Seal: W)o-Bon Grout-Woli. flush-to-grade vault.(From 3 ill 4.6 foot,from 13.5 ill 17.5 foot andfrom 24 ill 2B.8 feet.)
L/:YVI Concrele: From 0 ill 3 feet.
WELL MONITORING OAT A:
~Tim.
I
O••crlptlon
1- I'~-ISWL
~
GeoLogic Associotes
SOIL GAS PROBE COMPLETION SUMMARYWELL NO.:
PAGE: 1 OF 1
VN-2
JOB NO.: 2006-0088PROJECT: MULTI-LEVEL SOIL GAS PROBE STUDY
LOCATION: PALOS VERDES LANDFILLINSPECTOR: J. SAPP, .CHG
CHECKED BY: M. REASON, CHG
ELEVATION GROUND lEVEl.: 308.01ELEVATION TOP OF VAULT: 308.11
DATE STARTED: 5/05/06DATE FINISHED: 5/05/06
TOTAL DEPTH: N/A
0-
5-
10-
15-
20-.-
25-
30--
35-
40-
45-
50-
55-
60-
65-
DRILLING SUMMARY: WELL CONSTRUCTION LOG:start Fin,.h
Totol Depth: 50 feet Date Tim. Oat. Tim.Borehole dlometer: B"
Drilling lContlnuo.. Core): 5/110/00 9:DD 5/110/00 12:00Driller: ABC-UOVIN
CME-75Probe Construction: 5/110/00 13:00 5/110/00 14:36
Rig:Blt(o): N/"
Drilling Fluid: N/A
Protective Cooing: Hollow-stem augers.
WELL CONSTRUCTION DETAILS:
IT] Pipe: 1" d1ametor, flllllh-thnloded Soh.80 PVC fllied with bentonite.(From 0.5 to 43 feel)
[TITublng: 1/4" d1ametor poIysthyIene - WELL DEVELOPMENT LOG:5I101low (OIIInge) to 11 feel,
Start F1nllhIntermediote (gl88ll) to 29 leeI, Oat. Tmo TlmoDeep (b1uo) to 41 feel Surgo Siock
I I IProbe: 316 otolnleoo steel son voperSoilingImplanl
(At 11, 29 end 41 feel) Pumping
~Bontonlte Wyo-Ben Enviroplug, medium. Total Gallono Removed:Chip Soal: (From 2 to 4 feel,
from 7 to S.5 feel,STABILIZATION TEST DATA:from 12 to 14 feel,
from 20.5 to 25.5 feel, Gallona pH spo.. ConcL 1,../ctriJ Tomp (OFtfrom 3D to 34 feel,from 36 to 3B feet andfrom 43 to 50 feel)
I?V?BI Filter Pack: Cornrnerclal 12/12 Montereytype sond.(From 10 to 12 feel,from 2B to 3D feet andfrom 40 to 43 feel)
roooooo;~ Granular Wyo-Ben No. 8.000000000000000000 Sontonlte (From 8.5 to 10 feel, Comments:
Sool: from 25.5 to 2B feet andProbe finished at the surface withfrom 3B to 40 feel)f1ush-to-grade vaull
~ Grout Seal: Wyo-Ben Grout-Well.(From 4 to 7 feel,from 14 to 20.5 feet andfrom 34 to 3B feel)
f:::~~tt:~tl Concrete: From 0 to 2 feel
WELL MONITORING DATA:
~Tlmo
1
D..crJptlon
1- I"'"~'ISWL
B
Geologic Associates
SOIL GAS PROBE COMPLETION SUMMARYWELL NO.:
PAGE: 1 OF 1
VN-3
JOB NO.: 2006-00BBPROJECT: MULTI-lEVEL SOIL GAS PROBE sruDY
LOCATION: PALOS VERDES LANDFILLINSPECTOR: J. SAPP, CHG
CHECKED BY: M. REASON, CHG
ELEVATION GROUND LEVEL: 314.S2ELEVATION TOP OF VAULT: 314.92
DATE STARTED: 5/0S/06DATE FINISHED: 5/'OS/OB
TOTAL DEPTH: N/A
0-
5-
10-
15-
20-
25-
30-
35-
40-
45-
50-
55-
60-
65-
DRILLING SUMMARY: WELL CONSTRUCTION LOG:Start Flnl.h
Total Depth: 50 feot Oat. Tim. Dat. Tim.
Borehole diameter: S" Drilling (Continuo.. Core): 5/1'il/1'18 7:15 5/1'18/1'18 10'.20Driller: ABC-UOVIN
Rig: CME-75Probe Construction: 5/1'18/1'18 10:40 5/1'il/1'18 16:15
Bltto): N/A
Orllllng Fluid: N/A
ProtectlYe Cooing: Hollow-stem augers.
WELL CONSTRUCTION DETAILS:
CD Pipe: 1· diameter, fluoh-thlllCldod Soh.80 PVC fillod with bentonite.(Fn>m 0.5 to 32 feet.)
[TITublng: 1/4· diameter polyethyleno - WELL DEVELOPMENT LOG:Shallow (orange) to 13 fool,
~.rt F'm,'hIntormocfIale (greon) to 23.5 fool, Oat. m. T •
Deep (blue) to 31 feet. Surgo Block
I I IProbe: 316 ""'Inleso sleeI eoII vaporBailingImplant
(At 13, 23.5 and 31 feet.) Pumping
~Bentonite Wyo-Bon £rMn>pIug, modIum.
Total Galiano RemoYed:Chip Seol: (Fn>m 2 to 4 fool,from B to 9.7 fool,from 14.1 to 17 fool, STABILIZATION TEST DATA:from 25 to 26 feel and Gallon. pH Speo. Cond. (lUI/ern) T.mp (OF)from 35 to 47 feet.)
I(XU Filter Pack: Commercial #2/12 Montereytype sand.(Fn>m 12 to 14 fool,from 22.6 to 25 feel andfrom 30 to 32 feet.)
IForoo""o~~, Granular W,ya-Bon No. 8.0000"000000000000 Bentonite (From 9.7 to 12 fool,
5.01: from 21.2 to 22.6 fool,from 28 to 30 feel and Comments:from 32 to 35 feet.)
~Graut Seal: W,ya-Bon Graul-WelL Probe finished at the surface with(From 4 to 8 feel, f1ush-to-grade Yaullfrom 17 to 21.2 feel andfrom 26 to 28 feet.)
t~<;YI Concrete: From °to 2 feet.
Ed Slaugh: From 47 to 50 feet.
WELL MONITORING DATA:
~Time
ID••crlptlon
1- I'~'-IaWL
B
GeoLogic Associates
SOIL GAS PROBE COMPLETION SUMMARYWELL NO.:PAGE: 1 OF 1
VN-4
JOB NO.: 2006-00BBPROJECT: MULTI-LEVEl SOIL GAS PROBE STUDY
LOCATION: PALOS VERDES LANDFILLINSPECTOR: J. SAPP. CHG
CHECKED BY: M. REASON, CHG
ELEVATION GROUND L.EVEl..: 333.43ELEVATION TOP OF VAULT: 333.53
DATE STARTED: 5/0B/06DATE FINISHED: 5/11/06
TOTAL DEPTH: N/A
0--
5-
10-
15-
20--
25-
30-
35--
40--
45-
50-
55-
60--
65-
DRILLING SUMMARY: WELL CONSTRUCTION LOG:Start Flnl,h
Totol Depth: 50 feet Dat. Tim. Dat. Tim.Borehole diameter: B"
Drilling IConllnuoul Corel: 5/lm/11l 13:45 5/10/11l 18:30Driller: ABC-UOVIN
Rig: CME-75Probe Conltructlon: 5/11/11l 7:00 5/11/11l 9:15
Bltlo): NIl.
Drilling Fluid: N/A
Protective Cooing: Hollow-stem ouger.
WELL CONSTRUCTION DETAILS:
[I] Pipe: I" diameter, flush-threaded Sell.60 we filled with benlDnlto.(FIll/Il 0.5 to 32 feeL)
[I] Tubing: 1/4" diameter polyethylene - WELL DEVELOPMENT LOG:ShcDow (orangs) to 23 feet,Deep (blue) to 31 feat. Start FlnJah
Dat. Tim. Time
I I IProbe: 316 aloin""'" ateeI IIOiI vapor Surge Blocklmplonl(At 23 and 31 feat.) Bailing
~Bentonite Wyo-Ben ErMroplug, rnedlum. PumpingChip Seal: (FIll/Il 2 to 3 feet,
from 5.5 to 12 feet, Tatal Gallono Removed:from 15.6 to 19.8 feet,from 24.2 to 25 feet,
STABILIZATION TEST DATA:from 26.8 to 26.6 feet andfrom 32 to 46.5 feat.) Bailon. pH Spe.. Cond. (JIlI/CrN Temp (OF)
n;ij Filter Pack: Commen:lal 12/12 Montereytwo sand.(FIll/Il 14.2 to 15.6 feet,from 22 to 25 feet andfrom 30 to 32 feat.)
I~oooooo~ Granular Wyo-Ben No. 8.0000000000000000 Bentonite (FIll/Il 19.8 to 22 feet and
Seal: from 28.6 to 30 feat.)
I~%%Z1:l Graul Seal Neat, type lilY PortlandComments:" ' (Noal cemenll: cemenl
(Flllm 3 to 5.5 feet and Probe finished at the surface withfrom 12 to 14.2 feat.) f1ush-to-grade vault. Tubing sheathed
~Grout Seal Wyo-Ben Grout-WelL with 1-inch PVC fram 4 to 14 feet
(Bentonite): (Flllm 25 to 26.8 feat.) below rgound surface.
[1(\):1 Concrete: FIll/Il 0 to 2 feat.... "........... ': ..
E54 Slough: Flllm 46.5 to 50 feat.
WELL MONITORING DATA:
~TIme
•
D..crlptlon I,", I-'"~'SWL
B
Geologic Associates
SOIL GAS PROBE COMPLETION SUMMARYWELL NO.:
PAGE: 1 OF 1
VN-5
JOB NO.: 2006-00SSPROJECT: MULTI-LEVEL SOIL GAS PROBE STUDY
LOCATION: PALOS VERDES lANDFlLLINSPECTOR: J. SAPP, CHG
CHECKED BY: M. REASON, CHG
.ELEVATION GROUND LEVEL: 340.20ELEVATION TOP OF VAULT: 340.30
DAlE STARTED: 5/11/06DAlE FlNISHED: 5/11/06
TOTAL DEPTH: N/A.
0-
5-
10-
15-
20-
25-
30--
35-
40-
45-
50-
55-
60-
65-
DRilliNG SUMMARY: WELL CONSTRUCTION LOG:Start Flnl,h
Totol Depth: 50 feet Oaf. Tim. Oat. Tim.
Borehole dlometer: S" Drilling (ContlnuoUl Core): 5/11/08 11:00 5/11/08 15:30Driller: ABC-UOVIN
CME-75Probe Conatructlon: 5/11/08 16:00 5/11/08 18:00
Rig:Slt(.): N/A
Drilling Fluid: N/A
Protectl.e Co.lng: Hollow-stem auger.
WELL CONSTRUCTION DETAILS:
IT] Pipe: 1" diameter, f1U8h-tiIIlloded Soh.80 Pt'C filled with bentonite.(FIllII1 0.5 to 48.5 feeL)
IT] TUbing: 1/4' diameter poIyeIhyIene - WELL DEVELOPMENT LOG:Shallow (orange) to 16 feel. s\:, FlnllhIntermedlate (g....,) to 31 feel. Oat. T • Tim.Deep (blue) to 47.5 feeL
Surge Block
I , IProbe: 316 ""'Inless sIeeI soD YOpor BailingImplant.(At 16, 31 and 47.5 feeL) Pumping
~Bentonite Wyo-Bon Envirnplug, medium. Total Gollon. Remo.ed:Chip Seal: (FIllII1 2.1 to 5.9 feel.
fnHn 10.2 to 12.4 feel. STABILIZATION TEST DATA:fnHn 17 to 21.1 feel.fnHn 32 to 36 feel. Gallon. pH Sp••• C.nd. ("./~ Temp (-F)
fnHn 44.1 to 46.5 feal andfnHn 4B.5 to 50 feeL)
I r! Filter Pack: Commen:IaI 12/12 Montorsytype sond.(FIllII1 14.9 to 17 feel.fnHn 30 to 32 feal andfnHn 46.5 to 48.5 feeL)
II~::::::::~Granular Wyo-Bon No. 8.
Sentanll. (FIllII1 5.9 to 7.5 feel.S.al: fnHn 12.4 to 14.9 feel. Comments:
fnHn 25.3 to 30 feal andProbe finished at the surface withfnHn 41.8 to 44.1 feeL)
~ Grout Seal: Wyo-Bon Groul-W.O. flush-to-grade .ault.
(FIllII1 3 to 4.8 feel.fnHn 13.5 to 17.5 feal andfnHn 24 to 28.8 feeL)
[>(:;/1 Concrete: FIllII1 0 to 2.1 feeL
WELL MONITORING DATA:
~Tim.
1
D..crlptlan
1- I'~~"ISWL
B
Geologic Associotes
SOIL GAS PROBE COMPLETION SUMMARYWELL NO.:
PAGE: 1 OF 1
VN-6
JOB NO.: 2006-00B8PROJECT: MULTI-LEVEL SOIL GAS PROBE STUDY
LOCATION: PALOS VERDES LANDFlLLINSPECTOR: J. SAPP, CHG
CHECKED BY: M. RE'ASON, CHG
ELEVATION GROUND LEVEL: 343.28ELEVATION TOP OF VAULT: 343.38
DATE STARTED: 5/10/06DATE FlNISHED: 51.10/06
TOTAL DEPTH: N/A
0-
5-
10-
15-
20-
25-
30-
35-
40-
45-
50-
55-
60-
65-
DRilliNG SUMMARY: WELL CONSTRUCTION LOG:Start Flnl.h
T0101 Deplh: 50 feet Oaf. Time Oat. Time
Borehole dlomeler: 8" Drilling (Conlln.o.1 Co..): 5/ID/0ll 7:40 5/10/00 11:20Driller: ABC-UOVIN
Rig: CME-75Probe Conelrucllon: 5/10/00 12:00 5/10/00 13:30
BII(e): N/A
Drilling Fluid: N/A
Prolectlve Coelng: Hollow-etem augers.
WELL CONSTRUCTION DETAILS:
CD Pipe: I" diometer, flush-tiIlllGdeel Soh.80 PVC tilled with bentonite.(From 0.5 to 42.5 feet.) WELL DEVELOPMENT LOG:
[TITublng: 1/4" diometer poI)othyIene - !Mart F~hShaDow (onmge) to 15 feet, Date mo T •InterrnedIote (green) to 29 feet, Surge BlockOeep (blue) to 41 feet.
I J IProbe: 316 eIolnleee steel eon YOparBoiling
Implant Pumping(At 15, 29 ond 41 feet.)
Toiol Gollone Removed:
~Benlonlte Wyo-Ben Enviroplug, medium.Chip Seol: (From 2 to Heet, STABILIZATION TEST DATA:
from 35 to 37.6 feet ond Ganon. pH spo.. Cando (pa/cml Tomp (OF)from 42.5 to 50 feet.)
I ?I Filter Pack: Commen:lal #2/12 llonterey.......... type eond•
(From 12.9 to 16.7 feet,from 2B to 30 feet andfrom 40 to 42.5 feet.)
II~~~~:::::~ Granular Wyo-Ben No. B.Benlonlle (From 7.5 to 12.9 feet.
Seal: from 23.5 to 2B feet,from 30 to 32.3 feet and Comments:from 37.6 to 41 feet.)
Probe finished at the surface with~ Groul Seal: Wyo-Ben Grout-Well flush-to-grade vault.
(From 4 to 7.5 feet,from 16.7 to 23.5 feet andfrom 32.3 to 35 feet.)
fYnil Concrete: From 0 to 2 feet.
WELL MONITORING DATA:
~TIm.
•
D••crlpflon
I"" 1--'1SWL
B
GeoLogic Associates WELL NO.: VN1-10NSOIL GAS PROBE COMPLETION SUMMARY
PAGE: 1 OF 1
JOB NO.: 2006-0088 ~ATION GROUND~ 246.07PROJECT: MULTI-lEVEL SOIL GAS PROBE STUDY ~ATION TOP OF VAULT: 246.17LOCATION: PALOS VERDES lANDFlLL DATE STARTED: 5/12/06
INSPECTOR: J. SAPP. CHG DATE FlNISHED: 5/.12/06CHECKED BY: M. RE'ASON. CHG TOTAL DEPTH: N/A
0-- DRILLING SUMMARY: WELL CONSTRUCTION LOG:-\1 ..I:~:~- .e. Start Flnllh
- :··.·.:v·, " '"VI,' Total Oepth: 11 feet Oat. Tim. Oat. Tim.-
~~Borehole diameter: 3"
Drilling (Hand Auger): 5/12/08 13:55 5/12/08 15:10- Driller: ABC-UOVIN5- Probe Con.tructlon: 5/12/08 15:20 5/12/08 16:05- 000000 000000 Rig: CME-75
- g~~g~g iii::: BII(o): N/A--
10- Drilling Fluid: N/A-- Protective Cooing: N/A--
15- WELL CONSTRUCTION DETAILS:----
20-D=]Tublng: 1/4" diameter polyethylene to 10-
feet. WELL DEVELOPMENT LOG:-- ~.rt F~h- Date ma T a
25- I I IProbe: 316 sIalnl... steel BOIl vapor Surge Block- implanl- (At 10 feel) Bailing-- Pumping
30-- I rj Filter Pack: Commercial '2/12 Iofantorey Total Galiano Removed:- type sand.- (From 7.6 to 11 feet.) STABILIZATION TEST DATA:- Gallon. pH Speo. Cond. (pa/CrN Tamp ('FI35--- Ilrrooooooia Granular Wyo-Ben No. 8.00000000
00000000 Bentonite (From 5.B to 7.6 feel)-- 5001:
40---
~Bentonite Wyo-Ben Enviroplug, medium.- Chip 5001: (From 2.5 to 5.8 feet.)-
45-0
- [ ..::\..:1 Comments:- Concrete: From 0 to 2.5 feet.- Probe finished at the surface with- flush-ta-grade vault.
50- •----
55---
WELL MONITORING DATA:--
~ITim. D..crlptlon
O-~~ISWL
~60-
I
----
65-
GeoLogic Associates WELL NO.: VN4-7SOIL GAS PROBE COMPLETION SUMMARY PAGE: 1 OF 1
JOB NO.: 2006-0088 ELEVATION GROUND LEVEL: 333.43PROJECT: MULTI-LEVEL SOIL GAS PROBE STUDY ELEVATION TOP OF VAULT: 333.53
LOCATION: PALOS VERDES LANDFILL DATE STARTED: 5/12/06INSPECTOR: J. SAPP, CHG DATE FINISHED: 5/12/06
CHECKED BY: M. REASON, CHG TOTAL DEPTH: NIl.
0-DRILLING SUMMARY: WELL CONSTRUCTION LOG:
-:", .:;:~- ..~.-.y','. Start Flnl,h
- ~~"'''0:Totol Depth: 11 feet Oat. Tim. Oat. Tim.
- 000000 000000 Borehole dlometer: 3"5/12/00 5/12/00- 000000 000000
Orlller: ABC-UOVINDrilling (Hand Auger): 10:10 12:30000000 000000
000000 000000
5- 000000 000000
5/12/00 5/12/00000000 000000 Probe Construction: 12:50 13:10- ....... ......... Rig: CME-75....... .. ..- ......... .....BII(I): N/"
........-
~-10- Drilling Fluid: NIl.
-- ProtectlYe COllng: NIl.--
15- WELL CONSTRUCTION DETAILS:----
20-[TITublng: 1/4" dIomeler poIyelhyIene to 7-
fest. WELL DEVELOPMENT LOG:-- Start Flnl,h- Data Tim. Tim.
25-I I IProbe: 316 alolnl... aleeI IlCliI YOJlOI' Surge Block- Implant.
- (At 7 fest.) Boiling-- Pumping
30-- IIIIFilter Pock: Commerclol 12/12 IIonlerey Totol Gollonl RemoYed:- type 8Qnd.- (FIllIIl 5.5 to 7.5 fest.) STABILIZATION TEST DATA:-
Temp rF)35- Gallon. pH Speo. tond. (pa/CrN
-- 11:::::::::3 Granular Wyo-Ben No. 6.- Ben'onlte (FIllIIl 3 to 5.5 fest.)- Seal:
40---
~Bentonite Wyo-Ben Eirliroplug. medium.- Chip Seal: (From 1.5 to 3 fest.)-
45--
t::~d::~::::~~::1 Comments:- Concrete: FIllIIl 0 to 1.5 fest.- Probe finished at the surface with-
Ed flush-to-grade vault.50- Slough: FIllIIl 7.5 to 10 feat.
----
55----
WELL MONITORING DATA:--
~Tim. D••crlptlon Carr.
1"""-1OWL
860-
I 1----
65-
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-1 Core Photos
VN-115’ ↓
10 FT
20 FT
VN-15’ ↓
VN-215’ ↓
VN-220’ ↓
20 FT
25 FT
VN-120’ ↓
25 FT 30 FT 33 FT
VN-125’ ↓
28 FT VN-130’ ↓
VN-110’ ↓
Box: 1 of 3 Box: 2 of 3
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-1 Core Photos
VN-140’ ↓
45 FT
33’ ↓
Box: 3 of 335 FT
VN-135’ ↓
VN-25’ ↓
10 FT15 FT
13 FT VN-210’ ↓
VN-215’ ↓
VN-220’ ↓
20 FT
25 FT
Box: 1 of 4 Box: 2 of 4
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-2 Core Photos
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-2 Core Photos
VN-235’ ↓
44 FTVN-230’ ↓
35 FT
30 FT
VN-225’ ↓
28 FT
VN-240’ ↓
45 FT
Box: 3 of 4 Box: 4 of 4
Box: 1 of 3 Box: 2 of 3
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-3 Core Photos
VN-320’ ↓
35 FT
VN-35’ ↓
VN-310’ ↓
10 FT 20 FT
VN-315’ ↓
VN-325’ ↓
VN-330’ ↓
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-3 Core Photos
Picture file for Box 3 of 3 becamecorrupted and is not available.
Box: 3 of 3
VN-415’ ↓
20 FT
Box: 1 of 1
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-4 Core Photos
VN-420’ ↓
25 FT
Box: 1 of 3 Box: 2 of 3
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-5 Core Photos
VN-525’ ↓
35 FT
VN-55’ ↓
VN-515’ ↓
10 FT 25 FT
VN-520’ ↓
VN-530’ ↓
VN-510’ ↓
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-5 Core Photos
Box: 3 of 3
VN-535’ ↓
VN-540’ ↓
VN-545’ ↓
50 FT
VN-615’ ↓
17.5 FT
10 FT
VN-65’ ↓
35 FT50 FT
Box: 1 of 2 Box: 2 of 2
Palos Verdes LandfillMulti-level Soil Gas Probe Study
VN-6 Core Photos
VN-610’ ↓
15 FT
VN-620’ ↓
VN-625’ ↓
28 FT
VN-630’ ↓
VN-635’ ↓
VN-640’ ↓
VN-645’ ↓
AccuLabs, Inc.Air Toxic « Contaminated Soil « Water and Wastewater· Industrial and Hazardous Waste· Chemical Consultation
Date: May 23, 2006
Mr. Mike Reason and Mr. Jason SappGeoLogic Associates1831 Commercenter EastSan Bernardino, CA 92408
RE: Work Order Number: AL-06050004 / Palos Verde LandfillInvoice Number: GLA-OI04Y06-02
Dear Mr. Reason and Mr. Sapp:
Enclosed are the analytical reports and the invoice for the samples received by AccuLabson May 12,2006. The samples are tested for the parameters in accordance with theEPA methods as shown on the chain of custody form.
Thank you for the opportunity to provide analytical tests for your company.
Please feel free to call me at (626) 934-1288 if! can be of further assistance to yourcompany.
Sincerely,
lffHt}1Laboratory Director
15437 E. Proctor Avenue' City of Industry, California 91745 • Mailing Address: P.O. Box 92314' City ofIndustry. California 91745-2314Tel: (626) 934-1288' Fax: (626) 934-1299
~ AccuLabs, Inc. TeL (626) 934-1288 Fax, (626) 934-1299
15437E. Proaor Ave: Cityo[Industry, CA91745
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White - AccompanyLab Reportto Client Canary - Client's Copy Pink - Lab's ChronoFile
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Sign: --============
A I b £lient's P.ONumber: IReceivedby: Company: C.c..lA- b~A"",-,S""--i+--'
Print: ::rltda- H~lAe Date: 'ii/n.! ABBREVIATIONS I___-'7-'-,_b~ Sign: =4}V.lt<,$Y." lime:
CL/tDate: 5).>ft6. I
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Print: Date: _
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Nole: Payment for service is due within 30 days from the date of invoice.Samples will be disposed of after 30 days from the date of issuing the final report.
~ AccuLabs, Inc. TeL (626) 934-1288 Fax: (626) 934-1299
15437E. Proctor Ave. City ofIndustry, CA91745
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Print: Date: DW· Drinking Water WW - Waste Water
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Note: Payment for service is due within 30 days from the date of invoice.Samples will be disposed of after 30 days from the date of issuing the final report. White - Accompany Lab Report to Client Canary - Client's Copy Pink - Lab's Chrono File
~ AccuLabs, Inc. Tel. (626) 934-1288 Fax: (626) 934-1299
15437E. ProclorAve. Cilyoj1nduslry,CA 91745
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(1)(2)(3)(4)(5)(6)(7)(8)
Analytical Results:
TPH as Gasoline by EPA 8015MTPH as Diesel by EPA 8015MTitle 22 Metals by EPA 6010B & EPA 7471AOrganochlorine Pesticides (OCPs) by EPA 8081APolychlorinated Biphenyls (PCBs) by EPA 8082Volatile Organic Compounds by EPA 8260BSemivolatile Organic Compounds by EPA 8270COrganochlorine Herbicides by EPA 8150B
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrialand HazardousWaste. ChemicalConsultation
Project Info Sample Info Report InfoProject ID: 2006.0088 Date Sampled: 5/5,8,9,10&11/08 AccuLabs Batch No: AL-6050004
Sample Site: Palos Verde LF Date Received: 5/12/2006 Date Reported: 5/19/2006Client Name: GeoLoaic Associates SamDie Matrix: Soil ReDortina Units: maiKo
TPH as Gasoline by EPA 8015M
Sample Date Date
Client 10 Lab 10 Batch MOL RL Result OF Prepared Analyzed Qualifiers
VN-1-Composite 06050004-01 6050004 0.1 0.2 NO 1 5/16/06 5/16/06
VN-2-Composite 06050004-02 6050004 0.1 0.2 NO 1 5/16/06 5/16/06
VN-3-Composite 06050004-03 6050004 0.1 0.2 NO 1 5/16/06 5/16/06
VN-4-Composite 06050004-04 6050004 0.1 0.2 NO 1 5/16/06 5/16/06
VN-5-Composite 06050004-05 6050004 0.1 0.2 NO 1 5/16/06 5/16/06
VN-6-Composite 06050004-06 6050004 0.1 0.2 NO 1 5/16/06 5/16/06
NA Method Blank 6050004 0.1 0.2 NO 1 5/16/06 5/16/06
Key: RL =ReportIng Limit J =Trace Cone. Bin MOL and RL M.B. =Method Blank T.B. = Trip Blank F.B. =Field Blank E.B. =Equipment Blank
Client 10
VN-1-Composite
VN-2-Composite
VN-3-Composite
VN-4-Composite
VN-5-Composite
VN-6-Composite
Lab 1006050004-01
06050004-02
06050004-03
06050004-04
06050004-05
06050004-06
Surrogate % Recovery
a,a,a-TFT cc Limit
116 75-125
108 75-125
110 75-125
109 75-125
107 75-125
106 75-125
AccuLabs, Inc.
vl4Ellis Hsue '1Laboratory Director
(4:) AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Date Sampled: 5/5,8,9,10&11 /06 AccuLabs Batch No: AL-6050004
Sample Site: Palos Verde IF Date Received: 5/12/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Sample Matrix: Soil Reporting Units: mg/Kg
TPH as Diesel by EPA 8015M
Sample Date Date
Client 10 Lab 10 Batch MOL RL Result OF Extracted Analyzed Qualifiers
VN-1-Composite 06050004-01 6050004 5 10 NO 1 5/16/06 5/16/06
VN-2-Composite 06050004-02 6050004 5 10 NO 1 5/16/06 5/16/06
VN-3-Composite 06050004-03 6050004 5 10 NO 1 5/16/06 5/16/06
VN-4-Composite 06050004-04 6050004 5 10 NO 1 5/16/06 5/16/06
VN-5-Composite 06050004-05 6050004 5 10 NO 1 5/16/06 5/16/06
VN-6-Composite 06050004-06 6050004 5 10 NO 1 5/16/06 5116/06
NA Method Blank 6050004 5 10 NO 1 5/16/06 5/16/06Key: RL - Reponing limit J = Trace Cone. Bin MOL and RL M.B. - Method Blank T.B. - Trip Blank F.B. = Field Blank E.B. =Equipment Blank
Client 10 Lab 10
VN-1-Composite 06050004-01
VN-2-Composite 06050004-02
VN-3-Composlte 06050004-03
VN-4-Composite 06050004-04
VN-5-Composite 06050004-05
VN-6-Composite 06050004-06
* Note: BFB: Bromofluorobenzene
~~7tLabS, Inc.
~s~~Laboratory Director
Surrogate % Recovery
'BFB QC Limit
101 75-125
114 75-125
117 75-125
114 75-125
113 75-125
106 75-125
~ AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Samalelnfo Reaort InfoProject 10: 2006.0088 Date Sampled: 5/8,9,10 & 11 /2006 AccuLabs Batch No.: AL-06050004
Sample Site: Palos Verde landfill Date Received: 5/12/06 Date Reported: 5/19/06
Client Name: Geologic Associates Sample Matrix: Soil Reporting Units: mg/Kg
Title 22 Metals by EPA 6010B & EPA 7471A (Mercury)
Client ID NA VN-1 Composite VN-2 Composite VN-3 Composite VN-4 Composite VN-5 Composite VN-6 Composite DateAccuLabs ID Method Blank 06050004-01 06050004-02 06050004-03 06050004-04 06050004-05 06050004-06 DF MDL R.L. AnalyzedAntimony ND 2.9 3.4 3.5 3.4 3.4 3.3 1 0.52 2.0 5/18/06Arsenic ND 8.4 7.8 5.2 7.7 10 6.9 1 0.84 1.0 5/18/06Barium ND 690 140 170 200 440 180 1 0.034 1.0 5/18/06
Beryllium ND ND ND ND ND ND ND 1 0.12 1.0 5/18/06Cadmium ND 2.8 1.8 ND 1.6 2.5 ND 1 0.032 1.0 5/18/06Chromium ND 58 57 56 53 57 52 1 0.08 1.0 5/18/06
Cobalt ND 4.8 6.5 5.9 7.1 6.4 4.7 1 0.15 1.0 5118/06Copper ND 29 41 46 39 36 44 1 0.85 2.0 5/18/06
Lead ND 6 3.1 3.5 3.5 3.3 4.4 1 0.3 1.0 5/18/06Molybdenum ND 4.4 8.5 6.5 6.8 7.2 19 1 0.35 1.0 5/18/06
Nickel ND 42 48 29 52 57 24 1 0.14 1.0 5/18/06Selenium ND ND ND 7.7 ND ND ND 1 0.89 1.0 5/18/06
Silver ND ND ND ND ND ND ND 1 0.16 1.0 5/18/06Thallium ND ND ND ND ND ND ND 1 0.45 1.0 5/18/06
Vanadium ND 99 60 49 51 91 55 1 0.051 1.0 5/18/06Zinc ND 67 78 61 79 77 58 1 0.65 1.0 5/18/06
Mercury ND ND 0.13 0.14 ND 0.11 0.10 1 0.0067 0.10 5/18/06
Key: MDL = Method Detection Limit RL = Reportlnq Limit J = Trace Cone. between MDL and RL M.B. = MethodBlank T.B. = Trip Blank F.B. = Field Blank E.B. = EquipmentBlank
AccuLabs, Inc.
til H~~Ellis HsueLaboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial and Hazardous Waste. Chemical Consulation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VN-1 Composite AccuLabs 10: 06050004-01
Sample Site: Palos Verde Landfill Date Sampled: 51912006 Date Reported: 511912006Client Name: Geologic Associates Date Received: 511212006 Reporting Units: uglKg
Client 10: VN-1-1,2,3,4 & 5 Compo Samole Matrix: SoH
Organochlonne Pesticides by EPA 8081AEPA Sample Date Date
Analyte Method Batch MDL RL Result DF Prepared Analyzed Qualifiers4,4,-DDD 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
4,4-DDE 8081A 6050004 0.50 2.0 ND 1 5117106 51181064,4-DDT 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
Aldrin 8081A 6050004 0.50 1.0 ND 1 5117106 5118106alpha-SHC 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
alpha-Chlordane 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
beta-SHC 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
Chlordane 8081A 5050004 5.0 8.5 ND 1 5117106 5118106
delta-SHC 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
Dieldrin 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
DieldrinEndosulfane I 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
Endosulfane Ii 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
Endosulfane suldfate 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
Endrin 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
Endrin aldehyde 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
Endrin ketone 8081A 6050004 0.50 2.0 ND 1 5117106 5118106
gamma-SHC 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
gamma-Chlordane 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
Heptachlor 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
Heptachlor epoxide 8081A 6050004 0.50 1.0 ND 1 5117106 5118106
Methoxychlor 8081A 6050004 0.50 8.5 ND 1 5117106 5118106
Toxaphene 8081A 6050004 50 85.0 ND 1 5117106 5118106Surrogates % Recovery Q.Q..bl!!!!1Tetrachloro-m-xylene 80.0 59-127
Decachlorobiphenyl 81.6 60-109Key; MOL= MethodDetection Umil RL- Reporting Umil J '" TraceCone.betweenMOLand RL M.B. MethOd Blank 'r.s. = TripBlank F.B. FieldBlank E.B.= EquipmenlBlank
AccuLabs, Inc.
7lliE~iS Hsu '1Laboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. weter and Wastewater. Industrialand HazardousWaste. Chemical ccneulancn
Proiect Info ReDortlnfoProject 10: 2006.0088 Sample 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: PalosVerde Landfill Date Sampled: 5/5/2006 Date Reported: 5/19/2006
Client Name: Geologic Associates Date Received: 5112/2006 Reporting Units: ug/KgClient 10: VN-2-1.2.3,4,5 & 6 Compo Sample Matrix: Soil
Organochlorine Pesticides by EPA 8081AEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
4,4,-DDD 8081A 6050004 0.50 2.0 NO 1 5/17106 5/18/06
4,4-DDE 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
4,4-DDT 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Aldrin 8081A 6050004 0.50 1.0 NO 1 5117/06 5/18/06
alpha-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
alpha-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
beta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Chlordane 8081A 6050004 5.0 8.5 NO 1 5/17/06 5/18/06
delta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Dieldrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
DieldrinEndosulfane I 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endosulfane II 8081A 6050004 0.50 2.0 NO 1 5117/06 5/18/06
Endosulfane suldfate 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin aldehyde 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Endrin ketone 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
gamma-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
gamma-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Heptachlor 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Heptachlor epoxide 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Methoxychlor 8081A 6050004 0.50 8.5 NO 1 5/17/06 5/18/06
Toxaphene 8081A 6050004 50 85.0 NO 1 5/17/06 5/18/06Surrogates % Recovery Q.C.JJ.ml.tTetrachloro-m-xytene 79.0 59-127
Decachlorobiphenyl 83.3 60-109Key: MOL =Method Detection Limit RL = Reporting Limit J - Trace Cone. between MOL and RL M.B. - Method Blank T.B. = Trip Blank F.B. - Field Blank E.B. = Equipment Blank
AccuLabs, Inc.
~H7Ellis sue '1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soli. Waler and Wastewater _ Industrial and Hazardous Waste _ Chemical Consulation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VN-3 Composite AccuLabs 10: 06050004-03
Sample Site: Palos Verde Landfill Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-3-1.2.3.4 & 5 Compo Samole Matrix: Soil
Organochlorine Pesticides by EPA 8081AEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers4,4,-DDD 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
4,4-DDE 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
4,4-DDT 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Aldrin 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
alpha-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18106
alpha-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18106
beta-SHC 8081A 5050004 0.50 1.0 NO 1 5/17/06 5/18106
Chlordane 8081A 6050004 5.0 8.5 NO 1 5/17/06 5/18/06
delta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Dieldrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
DieldrinEndosulfane I 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endosulfane II 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endosulfane suldfate 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin aldehyde 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin ketone 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
gamma-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
gamma-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Heptachlor 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Heptachlor epoxide 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Methoxychlor 8081A 6050004 0.50 8.5 NO 1 5/17/06 5/18/06
Toxaphene 8081A 6050004 50 85.0 NO 1 5/17/06 5/18/06Surrogates % Recovery Q.C...1lm.i1Tetrachlcro-m-xylene 73.8 59-127Decachlorobiphenyl 82.8 60-109Key: MOL = Method Detection umn RL = Reporting Umit J - Trace Cone. between MOL and RL M.B. :::: Method Blank T.B. Trip Blank F.B. Field Blank E.B. - Equipment Blank
AccuLabs, Inc.
-W:1~1Ellis HsueLaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrial and HazardousWaste. Chemical Consulation
Protect tnto RepC)rt tntoProject 10: 2006.0088 Sample 10: VN-4 Composite AccuLabs 10: 06050004-04
Sample Site: Palos Verde Landfill Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
ClientlD: VN-4-1,2,3,4,5& 6 Camp. Samole Matrix: Soil
Organochlonne Pesticides by EPA 8081AEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
4,4,-DDD 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
4,4-DDE 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/064,4-DDT 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Aldrin 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06alpha-SHC 8081A 6050004 0.50 1.0 NO 1 5/17106 5/18/06alpha-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06beta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06Chlordane 8081A 6050004 5.0 8.5 NO 1 5/17/06 5/18/06delta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18106
Dieldrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06DieldrinEndosulfane I 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06Endosulfane II 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06Endosulfane suldfate 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06Endrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06Endrin aldehyde 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06Endrin ketone 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06gamma-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06gamma-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18106
Heptachlor 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06Heptachlor epoxide 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06Methoxychlor 8081A 6050004 0.50 8.5 NO 1 5/17/06 5/18/06Toxaphene 8081A 6050004 50 85.0 NO 1 5/17/06 5/18/06SUrrogates % Recovery .QC....!.J.m.!!
Tetrachloro-m-xylene 73.7 59-127Decachloroblphenyl 77.8 60-109Key: MOL = Method Detection Limn RL = Reporting Limit J =Trace Cone. between MOL and RL M.B. =Method Blank T.8. - Trip Blank F.B. = Field Blank E.B. - Equipment Blank
AccuLabs, Inc.
-mH~Ellis Hsue 1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soli. Water and Was1ewater • Industrial and Hazardous Waste. Chemical Consulation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VN-5 Composite AccuLabs 10: 06050004-05
Sample Site: Palos Verde Landfill Date Sampled: 5/1112006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 511212006 Reporting Units: uglKg
Client 10: VN-5-1,2,3,4& 5 Compo Samole Matrix: Soil
Organochlonne Pesticides by EPA 8081AEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
4,4,-DDD 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/064,4-DDE 8081A 6050004 0.50 2.0 NO 1 5/17106 5/18/06
4,4-DDT 8081A 6050004 0.50 2.0 NO 1 5/17106 5/18/06
Aldrin 8081A 6050004 0.50 1.0 NO 1 5/17106 5/18/06
alpha-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
alpha-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
beta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18106
Chlordane 8081A 6050004 5.0 8.5 NO 1 5/17/06 5/18/06
delta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Dieldrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
DieldrinEndosulfane I 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endosulfane II 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endosulfane suldfate 8081A 6060004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Endrin aldehyde 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin ketone 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
gamma-SHC 8081A 6050004 0.60 1.0 NO 1 5/17106 6118/06
gamma-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17106 5/18/06
Heptachlor 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Heptachlor epoxide 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18106
Methoxychlor 8081A 6050004 0.50 8.5 NO 1 5/17/06 5/18106
Toxaphene 8081A 6050004 50 85.0 NO 1 5/17/06 5/18/06
Surrogates % Recovery .Q.Q..!Jm.i!
Tetrachloro-m-xylene 77.7 59-127
Decachlorobiphenyl 84.5 60-109Key: MOL =Method Detection Limit RL = ReportingLimit J Trace Conc. betweenMOL aner RL M.B. = Method Blank T.B. = Trip Blank F.B. = Field Blank E.B. = EquipmentBlank
AccuLabs, Inc.
~{t8~~fLaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consulation
Proiect Info ReoortlnfoProject 10: 2006.0088 Sample 10: VN-6 Composite AccuLabs 10: 06050004-06
Sample Site: Palos Verde Landfill Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-6-1,2,3,4& 5 Camp. Sample Matrix: Soil
Organochlorine Pesticides by EPA 8081AEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
4,4,-DDD 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/064,4-DDE 8081A 6050004 0.50 2.0 NO 1 5/17106 5/18/064,4-DDT 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Aldrin 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18106
alpha-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06alpha-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06beta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06Chlordane 8081A 6050004 5.0 8.5 NO 1 5/17/06 5/18/06delta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06Dieldrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06DieldrinEndosulfane I 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06Endosullane II 8081A 6050004 0.50 2.0 NO 1 5/17106 5/18/06Endosulfane suldfate 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Endrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Endrin aldehyde 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
Endrin ketone 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18106
gamma-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06gamma-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06Heptachlor 8081A 6050004 0.50 1.0 NO 1 5117/06 5/18/06Heptachlor epoxide 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06Methoxychlor 8081A 6050004 0.50 8.5 NO 1 5/17/06 5/18/06Toxaphene 8081A 6050004 50 85.0 NO 1 5/17/06 5/18106
Surrogates % Recovery ~
Tetrachloro-m-xytene 78.7 59-127Decachlorobiphenyl 86.4 60-109Key: MOL::: Method Detection umu Rl::: Reporting umn J::: Trace Cone. between MOL and RL M.B. :::Method Blank T.B. :::Trip Blank F,B. :::Field Blank E.B. :::Equipment Blank
AccuLabs, Inc.
~(~Ellis Hsu vfLaboratory Director
AccuLabs, Inc.Air Toxic • Contaminated Soil. Water and Wastewater • Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-1 Compo AccuLabs 10: 0605004-01
Sample Site: Palos Verde Landfill Date Sampled: 5/9/2006 Date Reported: 5/19/06Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-1-1 ,2,3,4 & 5 Camp. Sample Matrix: Soil
Polychlorinated Biphenyls (PCBs) by EPA 8082
Sample Date Date
Analyle EPA Method MOL RL Result OF Extracted Analyzed Qualifiers
Aroclor-1016 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1221 8082 5 33 NO 1 5/17/06 5/18/06
Aroclor-1232 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1242 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1248 8082 5 16 NO 1 5/17106 5118/06
Aroclor-1254 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1260 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1262 8082 5 16 NO 1 5/17106 5/18/06
Aroclor-1268 8082 5 16 NO 1 5/17/06 5/18/06
Surrogates % Recovery QC Limit
Decachlorobiphenyl 92.3 44-132
Tetrachloro-m-xylene 101 63-130Key: RL = ReportingLimit J:::Trace Cone. Btn MOL and RL M.B. = Method Blank T.e. = Trip Blank F.B. = Field Blank E.B. = EqUipment Blank
AccuLabs, Inc.
~H~t'lEllis HsueLaboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial andHazardous Waste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Sample 10: VN-2 Camp. AccuLabs 10: 0605004-02
Sample Site: Palos Verde Landfill Date Sampled: 5/5/2006 Date Reported: 5/19/06Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-2-1,2,3.4,5&6Compo Samole Matrix: Soil
Polychlorinated Biphenyls (PCBs) by EPA 8082
Sample Date Date
Analyte EPA Method MDL RL Result DF Extracted Analyzed QualifiersAroclor-1016 8082 5 16 ND 1 5/17/06 5/18/06Aroclor-1221 8082 5 33 ND 1 5/17/06 5/18/06Aroclor-1232 8082 5 16 ND 1 5/17/06 5/18/06Aroclor-1242 8082 5 16 ND 1 5/17/06 5/18/06Aroclor-1248 8082 5 16 ND 1 5/17/06 5/18/06Aroclor-1254 8082 5 16 ND 1 5/17/06 5/18/06Aroclor-1260 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1262 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1268 8082 5 16 ND 1 5117/06 5/18/06Surrogates % Recovery OC Limit
Decachlorobiphenyl 89.6 44-132Tetrachloro-m-xylene 94.1 63-130Key: RL = Reporting LImit J = Trace Cone. Bin MOL and Rl M.B. = Method Blank T.e. = Tnp Blank F.B. =FjeldBlank E.B. = EquipmentBlank
AccuLabs, Inc,
Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated SoH. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-3 Camp. AccuLabs 10: 0605004-03
Sample Site: Palos Verde Landfill Date Sampled: 5/8/2006 Date Reported: 5/19106Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/K9
Client 10: VN-3-1,2,3,4,5&6 Compo Samole Matrix: Soil
Polychlorinated Biphenyls (PCBs) by EPA 8082
Sample Date Date
Analyle EPA Method MOL RL Result OF Extracted Analyzed Qualifiers
Aroclor-1016 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1221 8082 5 33 NO 1 5/17/06 5/18/06
Aroclor-1232 8082 5 16 NO 1 5/17106 5/18/06
Aroclor-1242 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1248 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1254 8082 5 16 NO 1 5/17/06 5118106
Aroclor-1260 8082 5 16 NO 1 5/17106 5/18/06
Aroclor-1262 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1268 8082 5 16 NO 1 5/17/06 5/18/06
Surrogates % Recovery QC Limit
Decachlorobiphenyl 95.0 44-132Tetrachlcro-m-xylene 95.8 63-130Key: RL;; Reporting LImIt J =Trace Cone.Bin MOLand RL M.B.;; Method Blank T.B. - Tnp Blank F.B. =Field Blank E.B. - EquipmentBlank
AccuLabs, Inc.
~s:r1Laboratory Director
AccuLabs, Inc.Air Toxic • Contaminated Soll e WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Sample 10: VN-4 Camp. AccuLabs 10: 0605004-04
Sample Site: Palos Verde Landfill Date Sampled: 5/8/2006 Date Reported: 5/19/06Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1 ,2,3,4,5&6 Compo SamDie Matrix: Soil
Polychlorinated Biphenyls (PCBs) by EPA 8082
Sample Date Date
Analyle EPA Method MDL RL Result DF Extracted Analyzed QualifiersAroclor-1016 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1221 8082 5 33 ND 1 5/17/06 5/18/06
Aroclor-1232 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1242 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1248 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1254 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1260 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1262 8082 5 16 ND 1 5/17106 5/18/06
Aroclor-1268 8082 5 16 ND 1 5/17106 5/18/06Surrogates % Recovery QC Limit
Decachlorobiphenyl 96.6 44-132Tetrachloro-m-xylene 95.0 63-130Key: RL - Reportmg limit J - TraceConc. BtnMOLand RL M.B.= Method Blank T.B. '" Top Blank F.B. = FieldBlank E.B. - Equipment Brank
AccuLabs, Inc.
~~~Ellis Hsue '!Laboratory Director
AccuLabs, Inc.Air Toxic • Oontaminatec Soile WaterandWastewater _ Industrial andHazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject ID: 2006.0088 Sample ID: VN-5 Compo AccuLabs ID: 0605004-05
Sample Site: Palos Verde Landfill Date Sampled: 5/11/2006 Date Reported: 5/19/06
Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client ID: VN-5-1,2,3,4 & 5 Compo Samole Matrix: Soil
Polychlorinated Biphenyls (PCBs) by EPA 8082
Sample Date Date
Analyle EPA Method MDL RL Result DF Extracted Analyzed Qualifiers
Aroclor-1016 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1221 8082 5 33 ND 1 5/17/06 5/18/06
Aroclor-1232 8082 5 16 ND 1 5/17/06 5/18/06Aroclor-1242 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1248 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1254 8082 5 16 ND 1 5/17/06 5/18/06
Aroclor-1260 8082 5 16 ND 1 5/17/06 5/18/06Aroclor-1262 8062 5 16 ND 1 5/17/06 5/18/06
Aroclor-1268 8082 5 16 ND 1 5/17/06 5/18/06
Surrogates %Recovery QC Limit
Decachloroblphenyl 94.4 44-132
Tetrachloro-m-xylene 93.8 63-130Key: RL - Reporting Limit J - TraceCone. BInMOLandRl M.B. '"Method Blank 'r.a. '"Tnp Blank F.B. - FieldBlank E.B.= EqUipment Blank
AccuLabs, Inc.
:~H\~Laboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. Water and Wastewater. Industrial andHazardous Waste. Chemical Consultation
Profect Info Sample/nfo Report/nfoProject 10: 2006.0088 Sample 10: VN-6 Camp. AccuLabs 10: 0605004-06
Sample Site: Palos Verde Landfill Date Sampled: 5/10/2006 Date Reported: 5/19/06
Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/KgClient 10: VN-6-1,2,3.4 & 5 Compo Sample Matrix: Soil
Polychlorinated Biphenyls (PCBs) by EPA 8082
Key: RL = Reporting Limit J =Trace Conc. atnMOL and RL M.B. - Method Blank T.B. - Trip Blank F.B. = Fjeld Blank E.B. - EqUipment Blank
Sample Date Date
Analyte EPA Melhod MOL RL Result OF Extracted Analyzed QualifiersAroclor-1016 8082 5 16 NO 1 5/17/06 5/18/06Aroclor-1221 8082 5 33 NO 1 5/17/06 5/18/06Arocior-1232 8082 5 16 NO 1 5/17/06 5/18/06
Arocior-1242 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1248 8082 5 16 NO 1 5/17/06 5/18/06
Arocior-1254 8082 5 16 NO 1 5/17/06 5/18/06Arocior-1260 8082 5 16 NO 1 5/17/06 5/18/06Arocior-1262 8082 5 16 NO 1 5/17/06 5/18/06Aroclor-1268 8082 5 16 NO 1 5117/06 5/18/06
Surrogates % Recovery QC Limit
Decachlorobiphenyl 92.1 44-132Tetrachloro-m-xylene 95.7 63-130
-
AccuLabs, Inc.
·tdtt~JJEllis HsueLaboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial andHazardous Waste. Chemical Consulation
Project Info ReDort/nfoProject 10: 2006.0088 Sample 10: VN-1 Composite AccuLabs 10: 06050004-01
Sample Site: PalosVerde Landfill Date Sampled: 5/9/2006 Date Reported: 5/22/2006plient Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-1-1,2,3,4 & 5 Compo Sample Matrix: Soil
Organochlorine Herbicides by EPA 8151A
EPA Sample Date DateAnalyte Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
2,4,5-T 8151A 6050004 0.444 1.1 NO 1 5/19-20/06 5121/06
2,4-DB 8151A 6050004 0.555 5 NO 1 5/19-20/06 5/21/06
2,4-D 8151A 6050004 0.066 1.2 NO 1 5/19-20/06 5/21/06
Dalapon 8151A 6050004 0.353 0.5 NO 1 5/19-20/06 5/21/06
Dicamba 8151A 6050004 0.518 0.6 NO 1 5/19-20/06 5/21/06
Dichloroprop 8151A 6050004 0.660 0.8 NO 1 5/19-20/06 5/21/06
Dinoseb 8151A 6050004 0.413 1.1 NO 1 5/19-20/06 5/21/06
MCPA 8151A 6050004 86.0 200 NO 1 5/19-20/06 5/21/06
MCPP 8151A 6050004 103 150 NO 1 5/19-20/06 5/21/06
4-Nitrophenol 8151A 6050004 1.89 5 NO 1 5/19-20106 5/21/06
Pentachlorophenol 8151A 6050004 0.0437 1 NO 1 5/19-20/06 5121/06
Silvex 8151A 6050004 0.438 1.2 NO 1 5/19-20/06 5/21/06Surrogate % Recovery Q.C..!Jrni1
2,4-Dichlorophenylacetic acid(DCAA) 107 43-169Key: MOL = Method Detection limit RL ReportingUmit J = TraceCone.between MOLandRL M.B.- MethodBlenk 'r.a. TripBlank F.B. FieldBlank E.B.- Equipment Blank
AccuLabs, Inc,
~4t{Ellis Hsue 1Laboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical ccneulencn
Proiect Info Reoort InfoProject 10: 2006.0088 Sample 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: PalosVerdesLandfill Date Sampled: 5/5/2006 Date Reported: 5/22/2006Client Name: GeoLogicAssociates Date Received: 5/12/2006 Reporting Units: uglKg
Client 10: VN-2-1.2,3,4,5 & 6 Compo Sample Matrix: Soil
Organochlorine Herbicides by EPA 8151A
EPA Sample Date Date
Analyte Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
2,4,5-T 8151A 6050004 0.444 1.1 NO 1 5/19-20/06 5/21/06
2,4-DB 8151A 6050004 0.555 5 NO 1 5/19-20/06 5/21/06
2,4-D 8151A 6050004 0.066 1.2 NO 1 5/19-20/06 5/21/06
Dalapon 8151A 6050004 0.353 0.5 NO 1 5/19-20/06 5/21/06
Dicamba 8151A 6050004 0.518 0.6 NO 1 5/19-20/06 5/21/06
Dichloroprop 8151A 6050004 0.660 0.8 NO 1 5/19-20/06 5/21/08
Dinoseb 8151A 6050004 0.413 1.1 NO 1 5/19-20/06 5/21/06
MCPA 8151A 6050004 86.0 200 NO 1 5/19-20/06 5/21/06
MCPP 8151A 6050004 103 150 NO 1 5/19-20106 5121/06
4-Nitrophenol 8151A 6050004 1.89 5 NO 1 5/19-20/06 5121/06
Pentachlorophenol 8151A 6050004 0.0437 1 NO 1 5/19-20/06 5121/06
Silvex 8151A 6050004 0.438 1.2 NO 1 5/19-20106 5/21/06
Surrogate %Recovery QC Limit
2,4~Oichlorophenylacetic acid(DCAA) 110 43-169Key: MOL = Method Detection Limil RL = Reporting Limit J = TraceCone.between MOLandRL M.B. = Method Blank T.B. = TripBlank F.B. = Field Blank E,B. = Equipment Blank
AccuLabs, Inc.
-ui~Ellis Hsue '1Laboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoli. Water and Wastewater. Industrial and HazardousWaste. Chemical Consulatlon
Project Info Report InfoProject ID: 2006.0088 Sample ID: VN-3 Composite AccuLabs ID: 06050004-03
Sample Site: Palos Verdes Landfill Date Sampled: 5/8/2006 Date Reported: 5/22/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client ID: VN-3-1,2,3,4,5 & 6 Compo SamDie Matrix: Soil
Organochlorine Herbicides by EPA 8151A
EPA Sample Date Date
Analyte Method Batch MOL RL Result OF Extracted Analyzed
2,4,5-T 8151A 6050004 0.444 1.1 NO 1 5/19-20/06 5/21/06
2,4-DB 8151A 6050004 0.555 5 NO 1 5/19-20/06 5/21/06
2,4-D 8151A 6050004 0.066 1.2 NO 1 5/19-20/06 5/21/06
Dalapon 8151A 6050004 0.353 0.5 NO 1 5/19-20/06 5/21/06
Dicamba 8151A 6050004 0.518 0.6 NO 1 5/19-20/06 5/21/06
Dichloroprop 8151A 6050004 0.660 0.8 NO 1 5/19-20106 5/21/06
Dinoseb 8151A 6050004 0.413 1.1 NO 1 5/19-20/06 5121/06
MCPA 8151A 6050004 86.0 200 NO 1 5/19-20106 5/21/06
MCPP 8151A 6050004 103 150 NO 1 5/19-20106 5121/06
4-Nitrophenol 8151A 6050004 1.89 5 NO 1 5/19-20/06 5/21/06
Pentachlorophenol 8151A 6050004 0.0437 1 NO 1 5/19-20/06 5/21/06
Silvex 8151A 6050004 0.438 1.2 NO 1 5/19-20/06 5/21/06
Surrogate % Recovery .Q.Q....!Jml12,4-Dichlorophenylacetic acid(DCAA) 95 43-169Key: MOL = Method Detection Umi! Rl = Reporting umn J =Trace Cone. between MOL and Rl M.B. =Method Blank T.B. - Trip Blank F.B. Field Blank E.B.
AccuLabs, Inc.
~r{1Ellis HsueLaboratory Director
Qualifiers
Equipment Blank
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consulation
Pro/ect Info ReDortlnfoProject 10: 2006.0088 Sample 10: VN-4 Composite AccuLabs 10: 06050004-04
Sample Site: Palos Verdes Landfill Date Sampled: 5/8/2006 Date Reported: 5/22/2006Flient Name: GeoLogic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-1-1,2,3,4,5 & 6 Compo Samole Matrix: Soil
Organochlorine Herbicides by EPA 8151A
EPA Sample Date Date
Analyte Method Batch MOL RL Result OF Extracted Analyzed2,4,5-T 8151A 6050004 0.444 1.1 NO 1 5/19-20/06 5/21/062,4-DB 8151A 6050004 0.555 5 NO 1 5/19-20/06 5/21/062,4-D 8151A 6050004 0.066 1.2 NO 1 5/19-20/06 5/21/06
Dalapon 8151A 6050004 0.353 0.5 NO 1 5/19-20/06 5121/06
Dicamba 8151A 6050004 0.518 0.6 NO 1 5/19-20/06 5/21/06
Dichloroprop 8151A 6050004 0.660 0.8 NO 1 5/19-20/06 5/21/06Dinoseb 8151A 6050004 0.413 1.1 NO 1 5/19-20/06 5/21/06
MCPA 8151A 6050004 86.0 200 NO 1 5/19-20/06 5/21/06MCPP 8151A 6050004 103 150 NO 1 5/19-20/06 5/21/06
4-Nitrophenol 8151A 6050004 1.89 5 NO 1 5/19-20/06 5/21/06
Pentachlorophenol 8151A 6050004 0.0437 1 NO 1 5/19-20/06 5121/06
Silvex 8151A 6050004 0.438 1.2 NO 1 5/19-20106 5/21/06Surrogate % Recovery QC Limit
2,4-Dichlorophenylacetic acid{DCAA) 130 43-169Key: MOL Method Detection Umit RL =Reporting Umil J Trace Cone. between MOL and RL M.S. =Method Blank T.B. - Trip Blank F.B. =Field Blank E.B.
AccuLabs, Inc.
~l~~Laboratory Director
Qualifiers
Equipment Blank
AccuLabs, Inc.Air Toxic. ContaminatedSoH. Water and Wastewater. Industrialand HazardousWaste. Chemical coneulenon
Project Info Report/nfoProject 10: 2006.0088 Sample 10: VN-5 Composite AccuLabs 10: 06050004-05
Sample Site: Palos Verdes Landfill Date Sampled: 5111/2006 Date Reported: 5/22/2006!client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client 10: VN-5-1,2,3,4 & 5 Compo samole Matrix: Soil
Organochlorine Herbicides by EPA 8151A
EPA Sample Date Date
Analyte Method Batch MDL RL Result DF Extracted Analyzed Qualifiers
2,4,5-T 8151A 6050004 0.444 1.1 ND 1 5/19-20/06 5121/06
2,4-DB 8151A 6050004 0.555 5 ND 1 5/19-20/06 5/21/06
2,4-0 8151A 6050004 0.066 1.2 ND 1 5/19-20/06 5/21/06
Dalapon 8151A 6050004 0.353 0.5 ND 1 5/19-20/06 5/21/06
Dicamba 8151A 6050004 0.518 0.6 NO 1 5/19-20/06 5/21/06
Dichloroprop 8151A 6050004 0.660 0.8 NO 1 5/19-20/06 5/21/06
Dinoseb 8151A 6050004 0.413 1.1 NO 1 5/19-20106 5121/06
MCPA 8151A 6050004 86.0 200 NO 1 5/19-20/06 5/21/06
MCPP 8151A 6050004 103 150 NO 1 5/19-20/06 5121/06
4-Nitrophenol 8151A 6050004 1.89 5 NO 1 5/19-20/06 5/21106
Pentachlorophenol 8151A 6050004 0.0437 1 NO 1 5/19-20/06 5/21/06
Silvex 8151A 6050004 0.438 1.2 NO 1 5/19-20/06 5/21/06
Surrogate % Recovery geLimit
2,4-Dlchlorophenylacetic acid(DCAA) 110 43-169Key: MOL = Method Detection Limit RL = Reporting Umit J Trace Cone. between MOL and RL M.B. =Method Blank r.a. = Trip Blank F.B. = Field Blank E.B. - Equipment Blank
AccuLabs, Inc.
1~,t]1Laboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical ccneulancn
Proiect Info ReDortlnfoProject 10: 2006.0088 Sample 10: VN-6 Composite AccuLabs 10: 06050004-06
Sample Site: PalosVerdes landfill Date Sampled: 5/10/2006 Date Reported: 5/22/2006!client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-6-1,2,3,4 & 5 Compo Sam Die Matrix: Soil
Organochlorine Herbicides by EPA 8151A
EPA Sample Date Date
Analyte Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
2,4,5-T 8161A 8050004 0.444 1.1 NO 1 5/19-20106 5121/06
2,4-08 8151A 6050004 0.555 5 NO 1 5/19-20/06 5/21/06
2,4-D 8151A 6050004 0.066 1.2 NO 1 5/19-20/06 5/21/06
Dalapon 8151A 6050004 0.353 0.5 NO 1 5/19-20/06 5/21/06
Dicamba 8151A 6050004 0.518 0.6 NO 1 5/19-20/08 5/21/06
Dichloroprop 8151A 6050004 0.660 0.8 NO 1 5/19-20/06 5121/06
Dinoseb 8151A 6050004 0.413 1.1 NO 1 5/19-20106 5/21/06
MCPA 8151A 6050004 86.0 200 NO 1 5/19-20/06 5/21/06
MCPP 8151A 6050004 103 150 ND 1 5/19-20/06 5/21/06
4-Nitrophenol 8151A 6050004 1.89 5 NO 1 5/19-20/06 5/21/06
Pentachlorophenol 8151A 6050004 0.0437 1 NO 1 5/19-20/06 5/21/06
Silvex 8151A 6050004 0.438 1.2 NO 1 5/19-20/06 5/21/06
Surrogate % Recovery QC Limit
2,4-Dichlorophenylacetic acid(DCAA) 110 43-169Key: MOL'" Method Detection umu RL = Reporting umn J = TraceCone.between MOLandRL M.B.= MethodBlank T.B. - TripBlank F.B. = FieldBlank E.B. - Equipment Blank
AccuLabs, Inc.
~~s~1Laboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial andHazardous Waste _ Chemical Consultation
Proiect Info Samnlelnfo ReDortlnfoProject 10: 2006.0088 Sample 10: VN-1 Compo AccuLabs 10: 06050004-01
Sample Site: Palos Verde IF Date Sampled: 5/9/2006 Date Reported: 5/19/06!client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client 10: VN-1-1.2,3.4 & 5 Composite Samnle Matrix: Soil
Volatile Organic Compounds by EPA 82608 MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
Acetone 82608 6050004 4.92 20 NO 1 5/16/06 5/16/06
Benzene 82608 6050004 0.84 5 NO 1 5/16/06 5/16/06
Bromobenzene 82608 6050004 0.84 5 NO 1 5/16/06 5/16/06
Bromochloromethane 82608 6050004 1.1 5 NO 1 5/16/06 5/16/06
Bromodichloromethane 82608 6050004 0.79 5 NO 1 5/16/06 5/16/06
Bromoform 82608 6050004 0.67 5 NO 1 5/16/06 5/16/06
Bromomelhane 82608 6050004 2.01 5 NO 1 5/16/06 5/16/06
2-Butanone (MEK) 82608 6050004 1.39 10 NO 1 5/16106 5/16/06
n-Butylbenzene 82608 6050004 0.63 5 NO 1 5/16/06 5/16/06
sec-Butylbenzene 82608 6050004 0.98 5 NO 1 5/16/06 5/16/06
tert-Butylbenzene 82608 6050004 0.65 5 NO 1 5116/06 5/16/06
Carbon tetrachloride 82608 6050004 0.70 5 NO 1 5/16/06 5/16/06
Chlorobenzene 82608 6050004 0.72 5 NO 1 5/16106 5/16/06
Chloroethane 82608 6050004 0.73 5 NO 1 5/16/06 5/16/06
2-Chloroethyl vinyl ether (2-CEVE) 82608 6050004 1.77 10 NO 1 5/16/06 5/16/06
Chloroform 82608 6050004 0.70 5 NO 1 5/16106 5/16/06
Chloromethane 82608 6050004 0.91 5 NO 1 5/16/06 5/16/06
2-Chlorotoluene 82608 6050004 0.72 5 NO 1 5/16106 5/16106
4·Chlorotoluene 82608 6050004 0.79 5 NO 1 5/16106 5/16/06
Dibromochloromethane 82608 6050004 0.77 5 NO 1 5/16/06 5/16106
1,2-Dibromo-3-chloropropane 82608 6050004 1.75 5 NO 1 5/16/06 5/16/06
1,2-Dibromoethane 82608 6050004 0.80 5 NO 1 5/16/06 5/16/06
Dibromomethane 82608 6050004 0.91 5 NO 1 5/16/06 5/16/06
1,2-Dichlorobenzene 82608 6050004 0.81 5 NO 1 5/16/06 5/16/06
1,3-Dichlorobenzene 82608 6050004 0.83 5 NO 1 5/16/06 5/16/06
1,4-Dichlorobenzene 82608 6050004 0.44 5 NO 1 5/16/06 5/16/06
Dichlorodifluoromethane(F-12) 82608 6050004 1.72 5 NO 1 5/16/06 5/16/06
t.t-nrctnoroethane 82608 6050004 0.76 5 NO 1 5/16/06 5/16/06
1,2-Dichloroethane 82608 6050004 0.69 5 NO 1 5/16/06 5/16/06
1,1-Dichloroethene 82608 6050004 1.04 5 NO 1 5/16/06 5/16/06
cis-1,2-Dichloroethene 82608 6050004 0.55 5 NO 1 5/16/06 5/16/06
trans-1 ,2-Dichloroethene 82608 6050004 0.55 5 NO 1 5/16/06 5/16/06
1,2-Dichloropropane 82608 6050004 0.88 5 NO 1 5/16/06 5/16/06
t.a-nctaoroprcpane 82608 6050004 0.94 5 NO 1 5/16/06 5/16/06
2,2-Dichloropropane 82608 6050004 0.67 5 NO 1 5/16/06 5/16/06
1,1-Dichloropropene 82608 6050004 0.85 5 NO 1 5/16/06 5/16/06
Ethylbenzene 82608 6050004 0.35 5 NO 1 5/16/06 5/16/06
Hexachlorobutadiene 82608 6050004 0.55 5 NO 1 5116/06 5/16/06
Key: RL - Reporting Limit J - Trace Cone. Bin MoL and RL M.B. = Method Blank T.B. = Trip Blank F.B. = Field Blank c.B. = cquipmentBlank
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Proiect Info Sample Info Report/nfoProject 10: 2006.0088 Sample 10: VN-1 Compo AccuLabs 10: 06050004-01
Sample Site: Palos Verde IF Date Sampled: 5/9/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-1-1,2,3,4 & 5 Composite Sample Matrix: Soil
Volatile Organic Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
2-Hexanone 8260B 6050004 1.56 10 NO 1 5/16/06 5/16/06
!sopropylbenzene 8260B 6050004 0.63 5 NO 1 5/16106 5/16/06
4-lsopropyltoluene 8260B 6050004 0.55 5 NO 1 5/16/06 5/16106
Methylenechloride 8260B 6050004 1.46 10 NO 1 5/16/06 5/16/06
4-Methyl-2-pentanone(MIBK) 8260B 6050004 2.64 10 NO 1 5/16/06 5/16/06
Napthalene 8260B 6050004 0.70 5 NO 1 5/16/06 5/16/06
n-Propylbenzene 8260B 6050004 0.92 5 NO 1 5/16/06 5/16/06
Styrene 8260B 6050004 0.57 5 NO 1 5/16/06 5/16/06
1,1,1,2-Tetrachloroethane 8260B 6050004 0.92 5 NO 1 5/16/06 5/16/06
1,1.zz-renacntoroauiane 8260B 6050004 2.28 5 NO 1 5/16/06 5/16/06
Tetrachloroethene (peE) 8260B 6050004 0.83 5 NO 1 5/16/06 5/16/06
Toluene 8260B 6050004 0.77 5 NO 1 5/16106 5/16/06
1,2,3-Trichlorobenzene 8260B 6050004 0.85 5 NO 1 5/16/06 5/16106
1,2,4-Trichlorobenzene 8260B 6050004 0.74 5 NO 1 5/16/06 5/16/06
1,1,1-Trichloroethane 8260B 6050004 0.99 5 NO 1 5/16/06 5/16/06
1,1,2-Trichloroethane 8260B 6050004 1.31 5 NO 1 5/16/06 5/16/06
Trichloroethene (TCE) 8260B 6050004 1.4 5 NO 1 5/16/06 5/16/06
Trichlorofluoromethane{F-11 ) 8260B 6050004 0.66 5 NO 1 5/16/06 5116/06
1,2,3-Trichloropropane 8260B 6050004 1.97 5 NO 1 5/16/06 5/16/06
1,2,4-Trimethylbenzene 8260B 6050004 0.55 5 NO 1 5/16106 5/16/06
1,3,5-Trlmethylbenzene 8260B 6050004 1.03 5 NO 1 5/16106 5/16/06
Vinyl chloride 8260B 6050004 1.81 5 NO 1 5/16/06 5/16/06
m,p-Xylene 8260B 6050004 1.84 10 NO 1 5/16/06 5/16/06
o-Xylene 8260B 6050004 0.66 5 NO 1 5/16/06 5/16/06
Melhyl-tert-butyl-ether (MTBE) 8260B 6050004 0.95 10 NO 1 5/16/06 5/16/06
tert-Butanol (TBA) 8260B 6050004 5.56 20 NO 1 5/16/06 5/16/06
Diisopropyl ether (DIPE) 8260B 6050004 0.66 5 NO 1 5/16/06 5/16/06
Elhyl-tert-butyl-elher (ETBE) 8260B 6050004 0.64 5 NO 1 5/16106 5/16/06
tert-Amyl methyl ether (TAME) 8260B 6050004 0.55 5 NO 1 5/16/06 5/16106
Surrogate: Dibromofluoromethane (75-125%) 102 %
Surrogate: 1,2-Dichloroethane-d4 (75-125%) 114 %
Surrogate: Toluene-dB (75-125%) 98 %
Surrogate: 4-Bromofluorobenzene (75-125%) 104 %
Key: MOL= Mel. DetectionLml RL = ReportingUmil J =Trace Cone.bin MOLand RL M.B. = Method Blank T.B. =Trip Blank F.B. = Field Blank E.B. = EquipmentBlank
AccuLabs, Inc.
~ri-yJEllis HsueLaboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste_ Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Sample 10: VN-2 Compo Acculabs 10: 06050004-02
Sample Site: Palos Verde IF Date Sampled: 5/5/2006 Date Reported: 5/19/06~lient Name: Geologic Associates Date Received: 511212006 Reporting Units: ug/Kg
Client 10: VN-2-1 ,2,3,4,5&6 Composite samote Matrix: Soil
Volatile Organic Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
Acetone 8260B 6010026 4.92 20 NO 1 5/16/06 5/16/06
Benzene 8260B 6010026 0.84 5 NO 1 5/16/06 5/16/06
Bromobenzene 8260B 6010026 0.84 5 NO 1 5/16/06 5/16/06
Bromochloromethane 8260B 6010026 1.1 5 NO 1 5/16106 5116106
Bromodichloromethane 8260B 6010026 0.79 5 NO 1 5/16/06 5/16/06
Bromoform 8260B 6010026 0.67 5 NO 1 5/16/06 5/16/06
Bromomethane 8260B 6010026 2.01 5 NO 1 5/16/06 5/16/06
z-Butenone (MEK) 8260B 6010026 1.39 10 NO 1 5/16/06 5/16/06
n-Butylbenzene 8260B 6010026 0.63 5 NO 1 5/16/06 5/16/06
sec-Butylbenzene 8260B 6010026 0.98 5 NO 1 5/16/06 5/16/06
tert-Butylbenzene 8260B 6010026 0.85 5 NO 1 5/16/06 5/16/06
Carbontetrachloride 8260B 6010026 0.70 5 NO 1 5/16/06 5/16106
Chlorobenzene 8260B 6010026 0.72 5 NO 1 5/16/06 5/16/06
Chloroethane 8260B 6010026 0.73 5 NO 1 5/16/06 5/16/06
2-Chloroethyl vinyl ether (2-CEVE) 8260B 6010026 1.77 10 NO 1 5/16/06 5/16/06
Chloroform 8260B 6010026 0.70 5 NO 1 5/16/06 5/16/06
Chloromethane 8260B 6010026 0.91 5 NO 1 5/16106 5/16/06
2-Chlorotoluene 8260B 6010026 0.72 5 NO 1 5/16/06 5/16106
4-Chlorotoluene 8260B 6010026 0.79 5 NO 1 5/16/06 5/16/06
Dibromochloromethane 8260B 6010026 0.77 5 NO 1 5/16/06 5/16/06
1,2-Dibromo-3-chloropropane 8260B 6010026 1.75 5 NO 1 5/16/06 5/16/06
1,2-Dibromoethane 8260B 6010026 0.80 5 NO 1 5/16/06 5/16/06
Dibromomethane 8260B 6010026 0.91 5 NO 1 5/16/06 5/16/06
t.z-ructuorobereene 8260B 6010026 0.81 5 NO 1 5/16106 5/16106
1,3-Dichlorobenzene 8260B 6010026 0.83 5 NO 1 5/16/06 5/16/06
1A-Dichlorobenzene 8260B 6010026 0.44 5 NO 1 5/16/06 5/16/06
Dlchlorodifluoromethane(F-12) 8260B 6010026 1.72 5 NO 1 5/16/06 5/16/06
'l.f-Dichloroethane 8260B 6010026 0.76 5 NO 1 5/16/06 5/16/06
1,2-Dichloroethane 8260B 6010026 0.69 5 NO 1 5/16/06 5/16/06
t.t-mctuoroethene 8260B 6010026 1.04 5 NO 1 5/16/06 5/16106
cls-t.z-urctuoroethene 8260B 6010026 0.55 5 NO 1 5/16/06 5/16/06
trans-t ,2-Dichloroethene 8260B 6010026 0.55 5 NO 1 5/16/06 5/16/06
t.z-rncnroroorocane 8260B 6010026 0.88 5 NO 1 5/16/06 5/16/06
t.a-nrchroropropane 8260B 6010026 0.94 5 NO 1 5/16/06 5/16/06
2,2-Dichloropropane 8260B 6010026 0.67 5 NO 1 5/16/06 5/16/06
1,1-Dichloropropene 8260B 6010026 0.85 5 NO 1 5/16/06 5/16106
Ethylbenzene 8260B 6010026 0.35 5 NO 1 5/16106 5/16/06
Hexachlorobutadiene 8260B 6010026 0.55 5 ND 1 5/16/06 5/16106
Key: RL = Reporting Umit J = Trace Cone. Bin MOL and Rl M.B. = Method Blank T.B. = Trip Blank F.B. = Field Blank E.B. = EquipmentBlank
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater _ Industrial and HazardousWaste. Chemical Consultation
Proiect Info Samo/e/nfo Reoort/nfoProject ID: 2006.0088 Sample ID: VN-2 Compo AccuLabs ID: 06050004-02
Sample Site: Palos Verde IF Date Sampled: 5/5/2006 Date Reported: 5119/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: uglKg
Client ID: VN-2-1,2,3,4,5&6 Composite Sample Matrix: Soil
Volatile Organic Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF oareosxtrac Analyzed Qualifiers
z-Hexanone 8260B 6010026 1.56 10 NO 1 5/16106 5/16/06
Isopropylbenzene 8260B 6010026 0.63 5 NO 1 5/16/06 5/16/06
4-lsopropyltoluene 8260B 6010026 0.55 5 NO 1 5/16/06 5/16/06
Methylene chloride 8260B 6010026 1.46 10 NO 1 5116/06 5/16/06
4-Methyl-2-pentanone (MIBK) 8260B 6010026 2.64 10 NO 1 5/16/06 5116/06
Napthalene 8260B 6010026 0.70 5 NO 1 5/16106 5/16/06
n-Propylbenzene 8260B 6010026 0.92 5 NO 1 5/16/06 5/16/06
Styrene 8260B 6010026 0.57 5 NO 1 5/16/06 5/16/06
1,1,1,2-Tetrachloroethane 8260B 6010026 0.92 5 NO 1 5116/06 5/16/06
1,1,2,2-Tetrachloroethane 8260B 6010026 2.28 5 NO 1 5116/06 5/16/06
Tetrachloroethene (peE) 8260B 6010026 0.83 5 NO 1 5/16/06 5/16/06
Toluene 8260B 6010026 0.77 5 NO 1 5/16106 5/16/06
1,2,3-Trichlorobenzene 8260B 6010026 0.85 5 NO 1 5/16/06 5/16/06
1,2,4-Trichlorobenzene 8260B 6010026 0.74 5 NO 1 5/16/06 5/16/06
1,1,1-Trichloroethane 8260B 6010026 0.99 5 NO 1 5116/06 5/16/06
1,1,2-Trichloroethane 8260B 6010026 1.31 5 NO 1 5/16/06 5116/06
Trlchloroethene (TeE) 8260B 6010026 1.4 5 NO 1 5/16106 5116/06
Trichlorofluoromethane(F-11 ) 8260B 6010026 0.66 5 NO 1 5/16106 5116/06
1,2,3-Trichloropropane 8260B 6010026 1.97 5 NO 1 5/16106 5/16/06
1,2,4-Trimethylbenzene 8260B 6010026 0.55 5 NO 1 5/16/06 5/16/06
1,3,5·Trimethylbenzene 8260B 6010026 1.03 5 NO 1 5/16/06 5/16106
Vinyl chloride 8260B 6010026 1.81 5 NO 1 5116/06 5/16/06
m,p-Xylene 8260B 6010026 1.84 10 NO 1 5116/06 5/16/06
o-Xylene 8260B 6010026 0.66 5 NO 1 5/16106 5/16/06
Methyl-tert-butyl-ether(MTBE) 8260B 6010026 0.95 10 NO 1 5/16106 5/16/06
tert-Butanol (TBA) 8260B 6010026 5.56 20 NO 1 5/16/06 5/16/06
Diisopropyl ether (DIPE) 8260B 6010026 0.66 5 NO 1 5/16/06 5/16106
Ethyl-tert-butyl-ether (ETBE) 8260B 6010026 0.64 5 NO 1 5116/06 5/16/06
tert-Amyl methyl ether (TAME) 8260B 6010026 0.55 5 NO 1 5/16/06 5116/06
Surrogate: Dibromofluoromethane (75-125%) 103 %
Surrogate: 1,2-Dichloroethane-d4 (75-125%) 112 %
Surrogate: Toluene-d8 (75-125%) 92 %
Surrogate: 4-Bromofluorobenzene (75-125%) 90 %
Key: MOL=Mel Detection Lmt RL =ReportingUmil J =Trace Cone. bin MOLand RL M.B. =Method Blank T.B. =Trip Blank F.B.=Field Blank E.B. = EquipmentBlank
AccuLabs, lnc.
~~~1laboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrial and HazardousWaste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Sample 10: VN-3 Compo AccuLabs 10: 06050004-03
Sample Site: Palos Verde IF Date Sampled: 5/8/2006 Date Reported: 5/19/06plient Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: uglKg
Client 10: VN-3-1,2,3,4,5&6 Composite samete Matrix: Soil
Volatile Organic Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
Acetone 82606 6010026 4.92 20 NO 1 5/16106 5/16/06
Benzene 82606 6010026 0.84 5 NO 1 5/16/06 5/16/06
Bromobenzene 82606 6010026 0.84 5 NO 1 5/16/06 5/16/06
Bromochloromethane 82606 6010026 1.1 5 NO 1 5/16/06 5/16/06
Bromodichloromethane 82606 6010026 0.79 5 NO 1 5/16/06 5/16/06
Bromoform 82606 6010026 0.67 5 NO 1 5/16/06 5/16/06
Bromomethane 82606 6010026 2.01 5 NO 1 5/16106 5/16/06
2wButanone (MEK) 82606 6010026 1.39 10 NO 1 5/16/06 5/16/06
n-ButyJbenzene 82606 6010026 0.63 5 NO 1 5/16106 5/16106
sec-Butylbenzene 82606 6010026 0.98 5 NO 1 5/16/06 5/16/06
tert-Butylbenzene 82606 6010026 0.85 5 NO 1 5/16/06 5/16/06
Carbon tetrachloride 82606 6010026 0.70 5 NO 1 5/16/06 5/16/06
Chlorobenzene 82606 6010026 0.72 5 NO 1 5/16/06 5/16/06
Chloroethane 82606 6010026 0.73 5 NO 1 5/16/06 5/16/06
2-Chloroethyl vinyl ether (2wCEVE) 82606 6010026 1.77 10 NO 1 5/16106 5/16/06
Chloroform 82606 6010026 0.70 5 NO 1 5/16106 5/16106
Chloromethane 82606 6010026 0.91 5 NO 1 5/16/06 5/16106
2-Chlorotoluene 82606 6010026 0.72 5 NO 1 5/16/06 5/16/06
4-Chlorotoluene 82606 6010026 0.79 5 NO 1 5/16/06 5/16/06
Dibromochloromethane 82606 6010026 0.77 5 NO 1 5/16/06 5/16/06
1,2-Dibromo-3-chloropropane 82606 6010026 1.75 5 NO 1 5/16/06 5/16/06
1,2-Dibromoethane 82606 6010026 0.80 5 NO 1 5/16/06 5/16/06
Dibromomethane 82606 6010026 0.91 5 NO 1 5/16/06 5/16/06
1,2-Dichlorobenzene 82606 6010026 0.81 5 NO 1 5/16/06 5/16/06
1,3-Dichlorobenzene 82606 6010026 0.83 5 NO 1 5/16106 5/16/06
1.e-Dlchlorobenzene 82606 6010026 0.44 5 NO 1 5/16/06 5/16106
Dichlorodifluoromethane(F-12) 82606 6010026 1.72 5 NO 1 5/16/06 5/16/06
1,1-Dichloroethane 82606 6010026 0.76 5 NO 1 5/16/06 5/16/06
1,2-Dichloroethane 82606 6010026 0.69 5 NO 1 5/16/06 5/16/06
1,1-Dichloroethene 82606 6010026 1.04 5 NO 1 5/16/06 5/16/06
cis-1,2-Dichloroethene 82606 6010026 0.55 5 NO 1 5/16/06 5/16/06
trans-1,2-Dichtoroethene 82606 6010026 0.55 5 NO 1 5/16/06 5/16/06
1,2-Dichloropropane 82606 6010026 0.88 5 NO 1 5/16/06 5/16/06
1,3-Dichloropropane 82606 6010026 0.94 5 NO 1 5/16106 5/16/06
2,2-Dichloropropane 82606 6010026 0.67 5 NO 1 5/16106 5/16106
1,1-Dichloropropene 82608 6010026 0.85 5 NO 1 5/16106 5/16/06
Ethylbenzene 82606 6010026 0.35 5 NO 1 5/16/06 5/16106
Hexachlorobutadiene 82606 6010026 0.55 5 NO 1 5/16/06 5/16/06Key: RL - Reporting Umit J - Trace Cone. B10MDl and RL M.B. = Method Blank T.B. =Trip Blank F.B. Fjeld Blank E.B. = Equipment Blank
AccuLabs, Inc.Air Toxic. Contaminated Soli. Water and Wastewater. Industrial and Hazardous Waste _ Chemical Consultation
Proiect Info Samo/e Info ReporllnfoProject ID: 2006.0088 Sample ID: VN-3 Compo Acculabs ID: 06050004-03
Sample Site: Palos Verde IF Date Sampled: 5/8/2006 Date Reported: 5119/06Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: uglKg
Client ID: VN-3-1,2,3,4,5&6 Composite SamDie Matrix: Soil
Volatile Orgamc Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
2-Hexanone 8260B 6010026 1.56 10 NO 1 5/16/06 5/16/06
Isopropylbenzene 8260B 6010026 0.63 5 NO 1 5/16/06 5/16/06
4-1sopropyltoluene 8260B 6010026 0.55 5 NO 1 5/16/06 5/16/06
Methylene chloride 8260B 6010026 1.46 10 NO 1 5/16/06 5/16106
4-Methyl-2-pentanone (MIBK) 8260B 6010026 2.64 10 NO 1 5/16/06 5/16/06
Napthalene 8260B 6010026 0.70 5 NO 1 5/16/06 5/16/06
n-Propylbenzene 8260B 6010026 0.92 5 NO 1 5/16/06 5/16/06
Styrene 8260B 6010026 0.57 5 NO 1 5/16/06 5/16/06
1,1,1,2-Tetrachloroethane 8260B 6010026 0.92 5 NO 1 5/16/06 5/16/06
1,1,2,2-Tetrachloroethane 8260B 6010026 2.28 5 NO 1 5/16/06 5/16/06
Tetrachloroethene (peE) 8260B 6010026 0.83 5 NO 1 5/16/06 5/16/06
Toluene 8260B 6010026 0.77 5 NO 1 5/16/06 5/16/06
j.z.a-rrtctuorcbenzene 8260B 6010026 0.85 5 NO 1 5/16/06 5/16/06
1,2,4-Trichlorobenzene 8260B 6010026 0.74 5 NO 1 5/16/06 5/16/06
1,1,1-Trichloroethane 8260B 6010026 0.99 5 NO 1 5/16/06 5/16/06
1,1,2-Trichloroethane 8260B 6010026 1.31 5 NO 1 5/16106 5/16/06
Trichloroethene (TeE) 8260B 6010026 1.4 5 NO 1 5/16/06 5/16106
Trichlorofluoromethane(F-11) 8260B 6010026 0.66 5 NO 1 5/16/06 5/16/06
1,2,3-Trichloropropane 8260B 6010026 1.97 5 NO 1 5/16/06 5/16/06
1,2,4-Trimethylbenzene 8260B 6010026 0.55 5 NO 1 5/16/06 5/16106
1,3,5-Trimethylbenzene 8260B 6010026 1.03 5 NO 1 5/16/06 5/16/06
Vinyl chloride 8260B 6010026 1.81 5 NO 1 5/16/06 5/16106
m,p-Xylene 8260B 6010026 1.84 10 NO 1 5/16/06 5/16106
o-Xylene 8260B 6010026 0.66 5 NO 1 5/16/06 5/16/06
Metl1yl-tert-butyl-etl1er (MTBE) 8260B 6010026 0.95 10 NO 1 5/16/06 5/16/06
tert-Butanol (TBA) 8260B 6010026 5.56 20 NO 1 5/16/06 5/16/06
Diisopropyl ether (DIPE) 8260B 6010026 0.66 5 NO 1 5/16/06 5/16/06
EtI1yl-tert-butyl-etl1er (ETBE) 8260B 6010026 0.64 5 NO 1 5/16/06 5/16/06
tert-AmyJ methyl ether (TAME) 8260B 6010026 0.55 5 NO 1 2/2/06 2/2/06
Surrogate: Dibromofluoromethane (75-125%) 102 %
Surrogate: 1,2-Dichloroethane-d4 (75-125%) 117 %
Surrogate: Toluene-d8 (75-125%) 87 %
Surrogate: a-Bromoffuorobenzene (75-125%) 93 %
Key; MOL:: Met Detection Lmt Rl:: ReportingUmit J:: Trace Conc. btn MOLand RL M.B. :: Method Blank T.B. = Trip Blank F.B. :: Field Blank E.B. = Equipment Blank
AccuLabs, Inc.
~tb~tlaboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-4 Compo Acculabs 10: 06050004-04
Sample Site: Palos Verde IF Date Sampled: 5/8/2006 Date Reported: 5/19/06Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1.2,3,4,5&6 Composite SamDie Matrix: Soil
Volatile Organrc Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
Acetone 82608 6010026 4.92 20 NO 1 5/16106 5116/06
Benzene 82608 6010026 0.84 5 NO 1 5/16/06 5/16/06
Bromobenzene 82608 6010026 0.84 5 NO 1 5/16/06 5/16/06
Bromochloromethane 82608 6010026 1.1 5 NO 1 5/16/06 5/16/06
Bromodichloromethane 82608 6010026 0.79 5 NO 1 5/16/06 5/16/06
Bromoform 82608 6010026 0.67 5 NO 1 5/16106 5/16/06
Bromomethane 82608 6010026 2.01 5 NO 1 5/16106 5/16/06
2-Butanone (MEK) 82608 6010026 1.39 10 NO 1 5/16/06 5/16/06
n-Butylbenzene 82608 6010026 0.63 5 NO 1 5/16/06 5/16106
sec-Butylbenzene 82608 6010026 0.98 5 NO 1 5/16/06 5/16/06
tert-Butylbenzene 82608 6010026 0.85 5 NO 1 5/16/06 5/16/06
Carbon tetrachloride 82608 6010026 0.70 5 NO 1 5/16/06 5/16/06
Chlorobenzene 82608 6010026 0.72 5 NO 1 5/16/06 5/16/06
Chloroethane 82608 6010026 0.73 5 NO 1 5/16/06 5/16/06
2-Chloroethyl vinyl ether (2-CEVE) 82608 6010026 1.77 10 NO 1 5/16/06 5/16106
Chloroform 82608 6010026 0.70 5 NO 1 5/16/06 5/16/06
Chloromethane 82608 6010026 0.91 5 NO 1 5/16/06 5/16/06
2-Chlorotoluene 82608 6010026 0.72 5 NO 1 5/16106 5/16/06
4-Chlorotoluene 82608 6010026 0.79 5 NO 1 5/16/06 5/16/06
Dibromochloromethane 82608 6010026 0.77 5 NO 1 5/16/06 5/16106
1,2-Dibromo-3-ehloropropane 82608 6010026 1.75 5 ND 1 5/16/06 5/16/06
t.z-rrcromcemene 82608 6010026 0.80 5 NO 1 5/16/06 5/16/06
Dibromomethane 82608 6010026 0.91 5 NO 1 5/16/06 5/16/06
t.z-rucniorobenzene 82608 6010026 0.81 5 NO 1 5/16/06 5/16/06
1,3-Dichlorobenzene 82608 6010026 0.83 5 NO 1 5/16/06 5/16/06
r.a-ntctuorobenzene 82608 6010026 0.44 5 NO 1 5/16/06 5/16106
Dlchlcrodiffuoromethanetf-12) 82608 6010026 1.72 5 NO 1 5/16/06 5/16106
1,1-Dichloroethane 82608 6010026 0.76 5 NO 1 5/16/06 5/16/06
1,2wDichloroethane 82608 6010026 0.69 5 NO 1 5/16/06 5/16/06
1,1-Dichloroethene 82608 6010026 1.04 5 NO 1 5/16/06 5/16/06
cts-t.z-ptchloroethene 82608 6010026 0.55 5 NO 1 5/16/06 5/16/06
trans-t.z-nrctuoroethene 82608 6010026 0.55 5 NO 1 5/16/06 5/16/06
t.z-ruchtoroorooane 82608 6010026 0.88 5 NO 1 5/16106 5/16106
1,3-Dlchforopropane 82608 6010026 0.94 5 ND 1 5/16/06 5/16106
z.z-mctaorcoropane 82608 6010026 0.67 5 NO 1 5/16/06 5/16/06
1,1-Dlchloropropene 82608 6010026 0.85 5 NO 1 5/16/06 5/16/06
Ethylbenzene 82608 6010026 0.35 5 NO 1 5/16/06 5/16/06
Hexachlorobutadiene 82608 6010026 0.55 5 ND 1 5/16/06 5/16/06Key: RL = Reporting Umit J = Trace Cone. Btn MDL and RL M.B. = Method Blank T.B. =Trip Blank F.B. = Field Blank E.B. = Equipment Blank
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consultation
Proiect Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-4 Compo AccuLabs 10: 06050004-04
Sample Site: Palos Verde IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client 10: VN-4-1,2,3,4,5&6 Composite Samole Matrix: Soil
Volatile Organic Compounds by EPA 82608 MethodEPA Sample Date Date
Analyte Method Batch MDL RL Result DF Prepared Analyzed Qualifiers
2-Hexanone 82608 6010026 1.56 10 ND 1 5/16/06 5/16106
Isopropylbenzene 82608 6010026 0.63 5 ND 1 5/16106 5/16/06
4-lsopropyltaluene 82608 6010026 0.55 5 ND 1 5/16/06 5/16/06
Methylene chloride 82608 6010026 1.46 10 ND 1 5/16/06 5/16/06
4-Methyl-2-pentanone (MIBK) 82608 6010026 2.64 10 ND 1 5/16/06 5/16/06
Napthalene 82608 6010026 0.70 5 ND 1 5/16/06 5/16106
n-Propylbenzene 82608 6010026 0.92 5 ND 1 5/16/06 5/16106
Styrene 82608 6010026 0.57 5 ND 1 5/16/06 5116/06
1,1,1,2-Tetrachloroethane 82608 6010026 0.92 5 ND 1 5/16/06 5/16/06
1,1,2,2-Tetrachloroethane 82608 6010026 2.28 5 ND 1 5/16106 5/16/06
Tetrachloroethane (peE) 82608 6010026 0.83 5 ND 1 5/16/06 5/16/06
Toluene 82608 6010026 0.77 5 ND 1 5/16/06 5/16106
1,2,3-Trichlorobenzene 82608 6010026 0.85 5 ND 1 5/16/06 5/16/06
1,2,4-Trichlorobenzene 82608 6010026 0.74 5 ND 1 5/16/06 5/16/06
1,1,1-Trichloroethane 82608 6010026 0.99 5 ND 1 5/16/06 5/16/06
1,1,2-Trichloroethane 82608 6010026 1.31 5 ND 1 5/16/06 5/16/06
Trichloroethene (TCE) 82608 6010026 1.4 5 ND 1 5/16/06 5/16106
Trichlorofluoromethane(F-11 ) 82608 6010026 0.66 5 ND 1 5/16/06 5/16/06
1,2,3-Trichloropropane 82608 6010026 1.97 5 ND 1 5/16/06 5/16/06
1,2,4-Trimethylbenzene 82608 6010026 0.55 5 ND 1 5/16/06 5/16/06
1,3,5-Trimethylbenzene 82608 6010026 1.03 5 ND 1 5/16/06 5/16/06
Vinyl chloride 82608 6010026 1.81 5 ND 1 5/16106 5/16/06
m,p-Xylene 82608 6010026 1.84 10 ND 1 5/16/06 5/16/06
a-Xylene 82608 6010026 0.66 5 ND 1 5/16/06 5/16/06
Methyl-ten-butyl-ether (MTSE) 82608 6010026 0.95 10 ND 1 5/16/06 5/16/06
tart-Butanol (TBA) 82608 6010026 5.56 20 ND 1 5116/06 5/16/06
Diisopropyl ether (DIPE) 82608 6010026 0.66 5 ND 1 5/16/06 5/16/06
Ethyl-tert-butyl-ether (ET8E) 82608 6010026 0.64 5 ND 1 5/16106 5/16/06
tert-Amyl methyl ether (TAME) 82608 6010026 0.55 5 ND 1 5/16/06 5/16/06
Surrogate: Dibromofluoromethane (75-125%) 101 %
Surrogate: 1,2-Dichloroethane-d4 (75-125%) 113 %
Surrogate: 'toluene-de (75-125%) 91 %
Surrogate: 4-Bromofluorobenzene (75-125%) 87 %
Key: MOL. =Mel. Detection L.mt RL. =ReportingUmil J ='rrace ccnc. bin MOL. and RL. M.B. =Method Blank T.B. =Trip Blank F.B. =Field Blank E.B. =EquipmentBlank
AccuLabs, Inc.
~r I~isHrJfilaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrial and HazardousWaste. Chemical Consultation
Proiect Info Sarno/e/nfo Reoon/nfoProject 10: 2006.0088 Sample 10: VN-5 Compo Acculabs 10: 06050004-05
Sample Site: Palos Verde IF Date Sampled: 5/11/2006 Date Reported: 5/19/06~lient Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-5-1,2,3,4 &5 Composite Sample Matrix: Soil
Analyte
Volatile Organic Compounds by EPA 82608 MethodEPA Sample Date
Method Batch MDL RL Result OF PreparedDate
Analyzed QualifiersAcetoneBenzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butytbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether (2-CEVE)
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dlbromochloromethane
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane(F-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cts-t.z-tnctnoroethene
trans-t .z-Dlchloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
6260B 6010026 4.92 20 ND 1 5/16/06
6260B 6010026 0.64 5 ND 1 5/16/06
6260B 6010026 0.64 5 ND 1 5/16/06
6260B 6010026 1.1 5 ND 1 5/16/06
6260B 6010026 0.79 5 ND 1 5/16106
6260B 6010026 0.67 5 ND 1 5/16/06
8260B 6010026 2.01 5 ND 1 5/16/06
8260B 6010026 1.39 10 ND 1 5/16/06
8260B 6010026 0.63 5 ND 1 5/16/06
8260B 6010026 0.98 5 ND 1 5/16106
8260B 6010026 0.85 5 ND 1 5116/06
8260B 6010026 0.70 5 ND 1 5116/06
8260B 6010026 0.72 5 ND 1 5116/06
8260B 6010026 0.73 5 ND 1 5116/06
8260B 6010026 1.77 10 ND 1 5116/06
8250B 6010026 0.70 5 ND 1 5116106
8260B 6010026 0.91 5 ND 1 5116/06
8260B 6010026 0.72 5 ND 1 5116/06
8260B 6010026 0.79 5 ND 1 5116/06
8260B 6010026 0.77 5 ND 1 5116/06
8260B 6010026 1.75 5 ND 1 5116/06
8260B 6010026 0.80 5 ND 1 5116/06
8260B 6010026 0.91 5 ND 1 5116106
8260B 6010026 0.81 5 ND 1 5116106
8260B 6010026 0.83 5 ND 1 5116/06
8260B 6010026 0.44 5 ND 1 5116/06
8260B 6010026 1.72 5 ND 1 5116/06
8260B 6010026 0.76 5 ND 1 5116/06
8260B 6010026 0.69 5 ND 1 5116106
8260B 6010026 1.04 5 ND 1 5116/06
8260B 6010026 0.55 5 ND 1 5116106
8260B 6010026 0.55 5 ND 1 5116/06
8260B 6010026 0.88 5 ND 1 5116/06
8260B 6010026 0.94 5 ND 1 5116/06
8260B 6010026 0.67 5 ND 1 5116/06
8260B 6010026 0.85 5 ND 1 5116/06
8260B 6010026 0.35 5 ND 1 5116/05
8260B 6010026 0.55 5 ND 1 5116/06
5116/06
5116/06
5116106
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116/06
5116106
5116/06
5116/06
5116/06
5116/06
5116/06
5116106
5116/06
5116/06
5116/06
5116/06
5116/06Key: RL'" Reporting Umit J '" Trace Cone.Bin MOLand RL M.B. '" Method Blank T.B. '" Trip Blank F.B.:: Field Blank E.8.:: EquipmentBlank
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste _ Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-5 Compo AccuLabs 10: 06050004-05
Sample Site: Palos Verde IF Date Sampled: 5/11/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: uglKg
Client 10: VN-5-1,2,3,4 &5 Composite SamDie Matrix: Soil
Volatile Organic Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
2-Hexanone 82608 6010026 1.56 10 NO 1 5/16/06 5/16/06
Isopropylbenzene 82608 6010026 0.63 5 NO 1 5/16/06 5/16106
4-lsopropyltoluene 82608 6010026 0.55 5 NO 1 5/16/06 5/16/06
Methylenechloride 82608 6010026 1.46 10 NO 1 5/16/06 5/16106
4-Methyl-2-pentanone(MIBK) 82608 6010026 2.64 10 NO 1 5/16/06 5/16/06
Napthalene 62608 6010026 0.70 5 NO 1 5116/06 5/16/06
n-Propylbenzene 62608 6010026 0.92 5 NO 1 5/16/06 5/16/06
Styrene 82608 6010026 0.57 5 NO 1 5/16/06 5/16/06
1,1,1,2-Tetrachloroethane 82608 6010026 0.92 5 NO 1 5/16/06 5/16/06
1,1,2,2-Tetrachloroethane 82608 6010026 2.28 5 NO 1 5/16106 5/16/06
Tetrachloroethene (peE) 82608 6010026 0.83 5 NO 1 5/16106 5/16/06
Toluene 82608 6010026 0.77 5 NO 1 5/16/06 5/16/06
1,2,3-Trichlorobenzene 82608 6010026 0.85 5 NO 1 5/16/06 5/16/06
1,2,4-Trichlorobenzene 82608 6010026 0.74 5 NO 1 5/16/06 5/16/06
1,1,1-Trichloroethane 82608 6010026 0.99 5 NO 1 5/16/06 5/16106
1.1,2-Trichloroethane 82608 6010026 1.31 5 NO 1 5/16/06 5/16/06
Trichloroethane (TeE) 82608 6010026 1.4 6 NO 1 5/16/06 5/16106
Trichlorofluoromethane(F-11) 82608 6010026 0.66 5 NO 1 5/16/06 5/16106
1,2,3-Trichloropropane 82608 6010026 1.97 5 NO 1 5/16/06 5/16/06
1,2,4-Trimethylbenzene 82608 6010026 0.55 6 NO 1 5/16/06 5/16/06
1,3,5-Trimethylbenzene 82608 6010026 1.03 5 NO 1 5/16/06 5/16/06
Vinyl chloride 82608 6010026 1.81 5 NO 1 5116/06 5/16/06
m,p-Xylene 82608 6010026 1.64 10 NO 1 5/16106 5/16/06
o-Xylene 82608 6010026 0.66 5 NO 1 5/16/06 5/16/06
Methyl-tert-butyl-ether(MTBE) 82608 6010026 0.95 10 NO 1 5/16/06 5/16/06
tert-Butanol (TBA) 82608 6010026 5.56 20 NO 1 5/16/06 5/16/06
Diisopropylether (D1PE) 82608 6010026 0.66 5 NO 1 5/16/06 5/16/06
Ethyl-tert-butyt-ether(ETBE) 82608 6010026 0.64 5 NO 1 5/16/06 5/16/06
tert-Amyl methyl ether (TAME) 82608 6010026 0.55 5 NO 1 5/16/06 5/16/06
Surrogate: Dibromofluoromethane (75-125%) 106 %
Surrogate: 1,2-Dichloroethane-d4 (75-125%) 111 %
Surrogate: Toluene-dB (75-125%) 83 %
Surrogate: 4-Bromofluorobenzene (75-125%) 105 %
Key: MOL=Mel DetectionLmt Rl.- ReportingLimit J =Trace Cone.bin MOl.ana RL M.B. =MelhoclBlank T.B. =Trip Blank F.B.=FieJaBlank E.B. - EquipmentBlank
AccuLabs, Inc.
~~H\AEllis Hsue Tlaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrial and HazardousWaste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-6 Compo Acculabs 10: 06050004-06
Sample Site: Palos Verde LF Date Sampled: 5/10/2006 Date Reported: 5/19/06plient Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN·6-1.2,3.4 &5 Composite Samole Matrix: Soil
Volatile Orgamc Compounds by EPA 82608 MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
Acetone 82608 6010026 4.92 20 NO 1 5/16/06 5/16/06
Benzene 82608 6010026 0.84 5 NO 1 5/16/06 5/16/06
Bromobenzene 82608 6010028 0.84 5 NO 1 5/16106 5/16/06
Brcmochloromethane 82608 6010026 1.1 5 NO 1 5/16/06 5/16/06Bromodichloromethane 82608 6010026 0.79 5 NO 1 5/16/06 5/16/06Bromoform 82608 6010026 0.67 5 NO 1 5/16106 5/16/06
Bromomethane 82608 6010026 2.01 5 NO 1 5/16106 5/16106
z-autanona (MEK) 82608 6010026 1.39 10 NO 1 5/16/06 5/16/06n-Butylbenzene 82608 6010026 0.63 5 NO 1 5/16/06 5/16/06
sec-Butylbenzene 82608 6010026 0.98 5 NO 1 5/16/06 5/16106
tert-Butylbenzene 82608 6010026 0.85 5 NO 1 5/16/06 5/16106
Carbon tetrachloride 82608 6010026 0.70 5 NO 1 5/16/06 5/16/06
Chlorobenzene 82608 6010026 0.72 5 NO 1 5/16/06 5/16/06Chloroethane 82608 6010026 0.73 5 NO 1 5/16/06 5/16/06
2~Chloroethyl vinyl ether (2-CEVE) 82608 6010026 1.77 10 NO 1 5/16/06 5/16/06Chloroform 82608 6010026 0.70 5 NO 1 5/16/06 5/16/06
Chloromethane 82608 6010026 0.91 5 NO 1 5/16/06 5/16/06
2-Chlorotoluene 82608 6010026 0.72 5 NO 1 5/16/06 5/16/064-Chlorotoluene 82608 6010026 0.79 5 NO 1 5/16/06 5/16/06Dibromochloromethane 82608 6010026 0.77 5 NO 1 5/16/06 5/16/06
1,2-Dibromo-3-chloropropane 82608 6010026 1.75 5 NO 1 5/16/06 5/16/06
1,2-Dibromoethane 82608 6010026 0.80 5 NO 1 5/16/06 5/16/06Dibromomethane 82608 6010026 0.91 5 NO 1 5/16/06 5/16/06
1.2-Dichlorobenzene 82608 6010026 0.81 5 NO 1 5/16/06 5/16/06
1,3-Dichlorobenzene 82608 6010026 0.83 5 NO 1 5/16/06 5/16/06
1A-Dichlorobenzene 82608 6010026 0.44 5 NO 1 5/16/06 5/16/06
Dichlorodifluoromethane(F-12) 82608 6010026 1.72 5 NO 1 5/16/06 5/16/06
1,1-Dichloroethane 82608 6010026 0.76 5 NO 1 5/16/06 5/16/06
1,2-Dichloroethane 82608 6010026 0.69 5 NO 1 5/16/06 5/16/061,1-Dichloroethene 82608 6010026 1.04 5 NO 1 5/16/06 5/16/06
cis-1,2-Dichloroethene 82608 6010026 0.55 5 NO 1 5/16/06 5/16/06
trans-1,2-Dichloroethene 82608 6010026 0.55 5 NO 1 5/16/06 5/16/06
1,2-Dichloropropane 82608 6010026 0.88 5 NO 1 5/16/06 5/16/06
1,3-Dichloropropane 82608 6010026 0.94 5 NO 1 5/16/06 5/16/06
2,2-Dichloropropane 82608 6010026 0.67 5 NO 1 5/16/06 5/16/06
'l.f-Dichloropropene 82608 6010026 0.85 5 NO 1 5/16/06 5/16/06
Ethylbenzene 82608 6010026 0.35 5 NO 1 5/16/06 5/16/06
Hexachlorobutadiene 82608 6010026 0.55 5 NO 1 5/16106 5/16106Key: RL =Reporting Umil J =Trace Cone. Bin MOLand RL M.B. - Method Blank T.B. =Trip Blank F.B. =Field Blank E.B. =Equipment Blank
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical ConsultatIon
Project Info SarnD/elnfo ReDortlnfoProject 10: 2006.0088 Sample 10: VN-6 Compo Acculabs 10: 06050004-06
Sample Site: Palos Verde IF Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client 10: VN-6-1,2,3,4 &5 Composite SamDle Matrix: Soil
Volatile Organic Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
2-Hexanone 8260B 6010026 1.56 10 NO 1 5/16/06 5/16/06
Isopropylbenzene 8260B 6010026 0.63 5 NO 1 5/16/06 5/16/06
4-lsopropyltoluene 8260B 6010026 0.55 5 NO 1 5/16106 5/16/06
Methylene chloride 8260B 6010026 1.46 10 NO 1 5/16/06 5/16/06
4-Methyl-2-pentanone (MIBK) 8260B 6010026 2.64 10 NO 1 5/16106 5/16/06
Napthalene 8260B 6010026 0.70 5 NO 1 5/16/06 5/16/06
n-Propylbenzene 8260B 6010026 0.92 5 NO 1 5/16/06 5/16/06
Styrene 8260B 6010026 0.57 5 NO 1 5/16/06 5/16/06
1,1,1,2-Tetrachloroethane 8260B 6010026 0.92 5 NO 1 5/16/06 5/16/06
1,1,2,2-Tetrachloroethane 8260B 6010026 2.28 5 NO 1 5/16/06 5/16/06
Tetrachloroethene (peE) 8260B 6010026 0.83 5 NO 1 5/16/06 5/16/06
Toluene 8260B 6010026 0.77 5 NO 1 5/16/06 5/16/06
1,2,3-Trichlorobenzene 8260B 6010026 0.85 5 NO 1 5/16/06 5/16/06
1,2,4-Trichlorobenzene 8260B 6010026 0.74 5 NO 1 5/16/06 5/16/06
1,1,1-Trichloroethane 8260B 6010026 0.99 5 NO 1 5/16106 5/16/06
1,1,2-Trichloroethane 8260B 6010026 1.31 5 NO 1 5/16/06 5/16/06
Trichloroethene (TeE) 8260B 6010026 1.4 5 NO 1 5/16/06 5/16/06
Trichlorofluoromethane(F-11) 8260B 6010026 0.66 5 NO 1 5/16/06 5/16/06
1,2,3-Trichloropropane 8260B 6010026 1.97 5 NO 1 5/16/06 5/16/06
1,2,4-Trimethylbenzene 8260B 6010026 0.55 5 NO 1 5/16/06 5/16/06
1,3,5-Trimethylbenzene 8260B 6010026 1.03 5 NO 1 5/16/06 5/16/06
Vinyl chloride 8260B 6010026 1.81 5 NO 1 5/16/06 5/16/06
m,p-Xylene 8260B 6010026 1.84 10 NO 1 5/16106 5/16/06
o-Xylene 8260B 6010026 0.66 5 NO 1 5/16/06 5/16/06
Methyl-tart-butyl-ether (MTBE) 8280B 6010026 0.95 10 NO 1 5/16108 5/16/06
tert-Butanol (TBA) 8260B 6010028 5.56 20 NO 1 5/18/08 5/16/06
Diisopropylether (DIPE) 8260B 6010026 0.66 5 NO 1 5/16/06 5/16/08
Ethyl-tert-butyl-ether (ETBE) 8260B 6010028 0.84 5 NO 1 5/16/06 5/16/06
tert-Amyl methyl ether (TAME) 8260B 6010026 0.55 5 NO 1 5/16/06 5/16/06
Surrogate: Dibromofluoromethane (75-125%) 104 %
Surrogate: t.z-mchioroemene-da (75-125%) 118 %
Surrogate: Toluene-dB (75-125%) 100 %
Surrogate: 4-Bromofluorobenzene (75-125%) 113 %
Key: MOL=Mel. cetecucn Lml RL =ReportingUmil J =Trace Cone. bin MDLand RL M.a. =Method Blank T.B. =Trip Blank F.B.=Field Blank E.B.=Equipment Blank
AccuLabs, Inc.
~1 {LfElliSHOLaboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Proiect Info Sarno/e/nfo ReDort/nfoProject ID: 2006.0088 Sample ID: VN-1 Composite AccuLabs ID: 06050004-01
Sample Site: Palos Verdes IF Date Sampled: 5/9/2006 Date Reported: 5/19/2006
Client Name: Geol.oqlc Associates Date Received: 5/1212006 Reporting Units: ug/KgClient ID: VN-1-1,2,3,4,5 Compo Sam ole Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMOLBatchMethod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyle
AcenaphtheneAcenaphthylene
Anthracene
BenzidineBenzo[a]anthraceneBenzo[bjfluoranthene
Benzo[k]f1uorantheneBenzo[a]pyreneBenzo[g,h,ijperylene
Benzoic acidBenzyl alcoholBenzidine ( M )
4-Bromophenyl phenyl ether
Butyl benzylphthalate
Oi-n-butylphthalate
4-Chloroanilinebis(2-Chloroethoxy) methane
bis(2-Chloroethyi) ether
bis(2-Chloroisopropyl)ether
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
ChryseneDibenzoturanOiben[a,hjanthracene
1,2~Dichlorobenzene
1,3-Dichlorobenzene
1A-Dichlorobenzene3,3'-Dichlorbenzidine
2,4-Dichlorophenol
Oiethylphthalate
2,4-0imethylphenol
Oimethylphlhalate
2.4-Dinitrophenol2,4-Dinitrotoluene
2,6-Dinitrotoluene4,6-0initro-2-methylphenol
8270C
8270C
6270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96
100
87
76
100
33
110
37
28
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
37
25
22
2930
45
330
330
330
1600
330
330
330
330
330
1600
660
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
330
1600
330
330
1600
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117106
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrialand HazardousWaste. Chemical Consultation
Date
Analyzed QualifiersRLMOLBatchMethod
Semlvolable Organic Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyle
Proiect Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Sample 10: VN-1 Composite AccuLabs 10: 06050004-01
Sample Site: Palos Verdes IF Date Sampled: 5/9/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-1-1 ,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 3550B.
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
2-Methylnaphlhalene
2-Methylphenol
4·Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso--di-n~propylamine
n-Nitrosodiphenylamine
Di-n-octylphthalate
Di-n-butylphthalate
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorbenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
2426
26
2627
33
27
74
262932
3628
2921
22
41
29170
86
2827
24
342945
27
26
5327
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
330
330
1600
330
330
330
330
330
330
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
NO 1 5117106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118106
5118/06
5118106
5118106
5118106
5118106
5118106
5118106
AccuLabs, Inc.AirToxic. Contaminated Soil. Water and Wastewater _ Industrialand HazardousWaste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject ID: 2006.0088 Sample ID: VN-1 Composite Acculabs ID: 06050004-01
Sample Site: Palos Verdes IF Date Sampled: 5/9/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: uglKg
Client ID: VN-1-1,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-<:l4 54.9 46-105
2,4,6-TribromophenoJ 74.9 46-146
2-Chlorophenol-d4 59.6 48-117
2-Fluorobiphenyl 62.5 54-112
2-Fluorophenol 58.3 45-119
4-Terphenyl-d14 65.5 46-135
Nitrobenzene-d5 56.8 40-116
Phenol-d6 61.8 37-127
Key: MOL'" Method Detection limit Rl= Reporting Limit J= Trace Cone.between MOL and Rl M.B =Method Blank T.B= Trip Blank F.B::Field Blank E.B= Equipment Blank
AccuLabs, Inc.
laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Indusbial and HazardousWaste. ChemicalConsultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sampie 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: Palos Verdes IF Date Sampled: 5/5/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-2-1 ,2,3,4,5&6 Comp. Sampie Matrix: Soil Extraction Method: EPA 35508
Semlvolatlle Orgamc Compounds by EPA 8270C MethodSample Date Oale
Analyle Melhod Balch MOL RL Result OF Extracted Analyzed Qualifiers
Acenaphlhene 8270C 6050004 26 330 NO 1 5/17106 5/18/06
Acenaphlhylene 8270C 6050004 31 330 NO 1 5/17/06 5/18/06
Anthracene 8270C 6050004 28 330 NO 1 5/17106 5/18/06
Benzidine 8270C 6050004 110 1600 NO 1 5/17/06 5/18/06
Benzo[a}anthracene 8270C 6050004 86 330 NO 1 5/17/06 5/18/06
Benzo[bjfluoranlhene 8270C 6050004 96 330 NO 1 5/17/06 5/18/06
Benzo[kjfluoranlhene 8270C 6050004 100 330 NO 1 5/17/06 5/18/06
Benzo[ajpyrene 8270C 6050004 87 330 NO 1 5/17/06 5/18/06
Benzo[9,h,ijperylene 8270C 6050004 76 330 NO 1 5/17/06 5/18/06
Benzoic acid 8270C 6050004 100 1600 NO 1 5/17/06 5/18/06
Benzyl alcohol 8270C 6050004 33 660 NO 1 5/17106 5/18/06
Benzidine ( M ) 8270C 6050004 110 1600 NO 1 5/17106 5/18/06
4-Bromophenyl phenyl elher 8270C 6050004 37 330 NO 1 5/17/06 5/18/06
Butyl benzylphlhalale 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
Oi-n-butylphlhalate 8270C 6050004 24 330 NO 1 5/17/06 5/18/06
4-Chloroaniline 8270C 6050004 28 660 NO 1 5/17/06 5/18/06
bis(2-Chloroelhoxy) methane 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
bis(2-Chloroelhyl) ether 8270C 6050004 24 330 NO 1 5/17/06 5/18/06
bis(2-Chloroisopropyl)elher 8270C 6050004 33 330 NO 1 5/17/06 5/18/06
4-Chloro-3-melhylphenol 8270C 6050004 32 660 NO 1 5/17/06 5/18/06
2-Chloronaphthalene 8270C 6050004 23 330 NO 1 5/17/06 5/18/06
2-Chlorophenol 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
4-Chlorophenyl phenyl ether 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
Chrysene 8270C 6050004 27 330 NO 1 5/17/06 5/18/06
Dibenzofuran 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
Diben[a,h]anthracene 8270C 6050004 76 330 NO 1 5117/06 5/18/06
1,2-Dichlorobenzene 8270C 6050004 24 330 NO 1 5/17/06 5/18/06
1,3-Dichlorobenzene 8270C 6050004 23 330 NO 1 5/17/06 5118/06
1,4-Dichlorobenzene 8270C 6050004 27 330 NO 1 5/17/06 5118/06
3,3'-Dichlorbenzidine 8270C 6050004 260 660 NO 1 5/17106 5/18/06
2,4-0ichlorophenol 8270C 6050004 28 1600 NO 1 5/17106 5/18/06
Oiethylphlhalate 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
2,4-0imelhylphenol 8270C 6050004 37 330 NO 1 5/17/06 5/18/06
Oimelhylphthalate 8270C 6050004 25 330 NO 1 5/17/06 5/18/06
2,4-Dinitrophenol 8270C 6050004 22 1600 NO 1 5/17/06 5/18/06
2,4-Dinitrotoluene 8270C 6050004 29 330 NO 1 5/17/06 5/18/06
2,6-Dinitrotoluene 8270C 6050004 30 330 NO 1 5/17/06 5/18/06
4,6-0inilro-2-melhylphenol 8270C 6050004 45 1600 NO 1 5/17/06 5/18/06
AccuLabs, Inc.Air Toxic • Contaminated Soil. WaterandWastewater elndustrtal andHazardous Waste. Chemical Consultation
Protect Info Samole Info Reoort InfoProject 10: 2006.0088 Sample 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: Palos Verdes LF Date Sam pled: 5/5/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-2-1,2,3,4,5&6 Compo SamDie Matrix: Soil Extraction Melhod: EPA 3550B
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Dale Dale
Analyle Method Balch MDL RL Result DF Extracted Analyzed Qualifiersbis(2-Elhylhexyl)phlhalate 8270C 6050004 24 330 ND 1 5117/06 5/18/06
Fluoranthene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Fluorene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Hexachlorobenzene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Hexachlorobutadiene 8270C 6050004 27 660 ND 1 5/17/06 5/18/06
Hexachlorocyclopentadiene 8270C 6050004 33 660 ND 1 5/17/06 5/18/06
Hexachloroethane 8270C 6050004 27 330 ND 1 5/17/06 5118/06
Indeno[1,2,3-cd]pyrene 8270C 6050004 74 330 ND 1 5/17/05 5/18/06
Isophorone 8270C 6050004 26 330 ND 1 5/17106 5/18/06
2-Methylnaphlhalene 8270C 6050004 29 330 ND 1 5/17/06 5/18/06
2-Methylphenol 8270C 6050004 32 330 ND 1 5/17/06 5/18/06
4-Methylphenol 8270C 6050004 36 330 ND 1 5/17/06 5/18/06
Naphlhalene 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
2-Nitroaniline 8270C 6050004 29 1600 ND 1 5/17/06 5/18/06
3-Nitroaniline 8270C 6050004 21 1600 ND 1 5/17/06 5/18/06
4-Nitroaniline 8270C 6050004 22 1600 ND 1 5/17/06 5/18/06
Nitrobenzene 8270C 6050004 41 330 ND 1 5/17/06 5118/06
2-Nltrophenol 8270C 6050004 29 330 ND 1 5/17/06 5/18/06
4-Nltrophenol 8270C 6050004 170 1600 ND 1 5/17/06 5/18/06
N-Nitroso-<:li-n-propylamine 8270C 6050004 86 330 ND 1 5/17/06 5/18/06
n-Nitrosodiphenylamine 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
Di-n-oclylphlhalale 8270C 6050004 27 330 ND 1 5/17106 5/18/06
Di-n-butylphlhalale 8270C 6050004 24 330 ND 1 5/17/06 5/18/06
Pentachlorophenol 8270C 6050004 34 1600 ND 1 5/17/06 5/18/06
Phenanthrene 8270C 6050004 29 330 ND 1 5/17/06 5/18/06
Phenol 8270C 6050004 45 330 ND 1 5/17/06 5/18/06
Pyrene 8270C 6050004 27 330 ND 1 5/17/06 5/18/06
1,2,4-Trichlorbenzene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
2,4,5-Trichlorophenol 8270C 6050004 53 330 ND 1 5/17/06 5/18/06
2,4,6-Trichlorophenol 8270C 6050004 27 330 ND 1 5/17106 5118/06
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: Palos Verdes IF Date Sampled: 5/5/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-2-1 ,2,3,4,5&6Comp. Sample Matrix: Soil Extraction Method: EPA 36508
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 60.0 46-1052,4,6-Tribromophenol 71.4 46-1462-Chlorophenol-d4 67 48-1172-Fluoroblphenyl 69.7 54-1122-Fluorophenol 64.4 45-1194-Terphenyl-d14 68.6 46-135Nitrobenzene-d5 63.1 40-116Phenol-d5 67.7 37-127Key: MDL= Method Detection Limit RL= Reporting Limit J= Trace Conc.between MDL and RL M.B =Method Blank T.B= Trip Blank F.B=Field Blank E.B= Equipment Blank
AccuLabs, Inc.
~!11Laboratory Director
(~) AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrialand Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-3 Composite AccuLabs 10: 06050004-03
Sample Site: Palos Verdes IF Date Sampled: 6/8/2006 Date Reported: 5119/2006
Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-3-1,2,3,4.5&6Camp. Sample Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMDLBatchMethod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Date
Result DF ExtractedAnalyte
Acenaphthene
Acenaphlhylene
Anthracene
Benzidine
Benzo[a]anthracene
Benzo[b]f1uoranthene
Benzo[k]fJuoranthene
Benzo[ajpyrene
Benzo[g.h,ijperylene
Benzoic acid
Benzyl alcohol
Benzidine ( M )
4-Bromophenyl phenyl ether
Butyl benzylphthalale
Di-n-butylphthalate
4-Chloroaniline
bis(2-Chloroelhoxy) methane
bis(2-Chloroelhyl) ether
bis(2-Chloroisopropyl)elher
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzofuran
Diben[a,hjanthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorbenzidine
2,4-Dichlorophenol
Diethylphthalale
2,4-Dimethylphenol
Dimethylphthalate
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
4,6-Dinitro-2-methylphenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96
100
87
76
100
33
110
37
28
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
37
25
22
29
30
45
330
330
330
1600
330
330
330
330
330
1600
660
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
330
1600
330
330
1600
ND 1 5/17106
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17106
5/18/06
5/18/06
5/18/06
5/18/06
5118106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118106
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consultation
Project Info SamlJle Info RelJort InfoProject 10: 2006.0088 Sample 10: VN-3 Composite Acculabs 10: 06050004-03
Sample Site: Palos Verdes IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geol.oqic Associales Date Received: 5/12/2006 Reporting Units: uglKg
Client 10: VN-3-1,2,3,4,5&6 Camp. Sam ole Matrix: Soil Extraction Method: EPA 35508Semlvolatlle Organic Compounds by EPA 8270C Method
Sample Dale Dale
Analyle Method Batch MDL RL Result DF Extracted Analyzed Qualifiers
bis(2-Ethylhexyl)phthalate 8270C 6050004 24 330 ND 1 5117106 5118106Fluoranthene 8270C 6050004 26 330 ND 1 5117106 5118106
Fluorene 8270C 6050004 26 330 ND 1 5117106 5118106Hexachlorobenzene 8270C 6050004 26 330 NO 1 5117106 5118106
Hexachlorobutadiene 8270C 6050004 27 660 NO 1 5117106 5118106
Hexachlorocyclopentadiene 8270C 6050004 33 660 NO 1 5117106 5118106
Hexachloroethane 8270C 6050004 27 330 ND 1 5117106 5118106Indeno[1,2,3-cd]pyrene 8270C 6050004 74 330 ND 1 5117106 5118106Isophorone 8270C 6050004 26 330 ND 1 5117106 51181062-Melhylnaphthalene 8270C 6050004 29 330 ND 1 5117106 51181062-Methylphenol 8270C 6050004 32 330 ND 1 5117106 51181064-Methylphenol 8270C 6050004 36 330 ND 1 5117106 5118106Naphthalene 8270C 6050004 28 330 ND 1 5117106 51181062-Nitroaniline 8270C 6050004 29 1600 NO 1 5117106 51181063-Nitroaniline 8270C 6050004 21 1600 ND 1 5117106 5118106
4-NitroaniJine 8270C 6050004 22 1600 ND 1 5117106 5/18106
Nitrobenzene 8270C 6050004 41 330 NO 1 5117106 51181062~Nitrophenol 8270C 6050004 29 330 NO 1 5117106 5118106a-Nltrophenol 8270C 6050004 170 1600 ND 1 5117106 5118106N-Nitroso-di-n-propylamine 8270C 6050004 86 330 ND 1 5117106 5118106n-Nitrosodiphenylamine 8270C 6050004 28 330 ND 1 5117106 5118106Oi-n-oclylphthalate 8270C 6050004 27 330 ND 1 5117106 5118106Di-n-bulylphthalate 8270C 6050004 24 330 ND 1 5117106 5118106
Pentachlorophenol 8270C 6050004 34 1600 ND 1 5117106 5118106
Phenanthrene 8270C 6050004 29 330 ND 1 5117106 5118106
Phenol 8270C 6050004 45 330 NO 1 5117106 5118106Pyrene 8270C 6050004 27 330 ND 1 5117106 51181061,2,4-Trichlorbenzene 8270C 6050004 26 330 ND 1 5117106 51181062,4,5-Trichlorophenol 8270C 6050004 53 330 ND 1 5117106 51181062,4,6-Trichlorophenol 8270C 6050004 27 330 ND 1 5117106 5118106
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and HazardousWaste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-3 Composite Acculabs 10: 06050004-03
Sample Site: Palos Verdes IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 511212006 Reporting Units: ug/Kg
Client 10: VN-3-1.2,3,4.5&6 Camp. Sam pie Matrix: Soil Extraction Method: EPA 35508
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 61.9 46-1052,4,6-Tribromophenol 83.9 46-1462-Chlorophenol-d4 69.6 48-1172-Fluorobiphenyl 69.3 54-1122-Fluorophenol 67.2 45-1194-Terphenyl-d14 66.9 46-135Nitrobenzene-d5 63.9 40-116Phenol-d5 72.1 37-127Key: MDl= Method Detection Limit RL= Reporting limit J= Trace Cone-between MOL and RL M.B =Method Blank T.B: Trip Blank F.B=FieldBlank E.B; Equipment Blank
AccuLabs, Inc.
~tJ4~fEllis H~Je .Laboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Date
Analyzed QualifiersRLMDLBalchMethod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample DateResult DF ExtractedAnalyle
Project Info Samole Info ReDortlnfoProject 10: 2006.0088 Sample 10: VN-4 Composite Acculabs 10: 06050004-04
Sample Site: Palos Verdes IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1,2,3,4,5&6 Comp. Sample Matrix: Soil Extraction Method: EPA 3550B.
AcenaphtheneAcenaphlhylene
AnthraceneBenzidineBenza[a]anthraceneBenzo[bjfluoranthene
Benzo[k]f1uorantheneBenzo[a]pyrene
Benzo[g,h,ijperylene
Benzoic acidBenzyl alcoholBenzidine ( M )
4-Bromophenyl phenyl elher
Butyl benzyiphthalale
Di-n-butylphlhalate
4-Chloroanilinebis(2-Chloroelhoxy) methane
bis(2-Chloroelhyl) elher
bis(2-Chloroisopropyl)elher
4-Chloro-3-methylphenol
2-Chloronaphlhalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
DibenzofuranDiben[a,h]anthracene1,2-Dichlorobenzene
1,3-Dichlorobenzene1A-Dichlorobenzene3,3'-Dichlorbenzidine2,4-Dichlorophenol
Diethylphlhalale
2,4-Dimelhylphenol
Dimelhylphlhalale
2,4-Dinitrophenol
2,4-Dinitrotoluene2,6-Dinitrotoluene4,6-Dinltro-2-melhylphenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96
100
87
76
100
33
110
37
28
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
37
25
22
2930
45
330
330
330
1600
330
330
330
330
330
1600
650
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
330
1600
330
330
1600
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5117/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
5/18/06
5/18/06
5118/06
5118/06
5118/06
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5118/06
5/18/06
5/18/06
5118/06
5118/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-4 Composite AccuLabs 10: 06050004-04
Sample Site: Palos Verdes IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1,2,3,4.5&6Camp. Sample Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMDLBatchMelhod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Dale
Result DF ExtractedAnalyle
bis(2-Elhylhexyl)phlhalale
Fluoranthene
Fluorene
Hexachtorobenzene
HexachlorobutadieneHexachlorocyclopentadiene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
2-Melhylnaphlhalene
2-Melhylphenol
4-Melhylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di~n-propylamine
n-Nitrosadiphenylamine
Di-n-oclylphlhalale
Di-n-bulylphlhalale
Pentachlorophenol
Phenanthrene
Phenol
Pyrena
1,2,4-Trichlorbenzene
2,4,5-Trichlorophenol
2,4,6-Trlchlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
36
28
2921
2241
29170
86
28
27
24
34
2945
27
26
53
27
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
3301600
330
330
330
330
1600
330
330
330
330
330
330
ND 1 5/17106
ND 1 5/17106
ND 1 5/17106
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
5118106
5118/06
5/18/06
5/18/06
5118106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.Air Toxic • Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Proiect Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-4 Composite AccuLabs 10: 06050004-04
Sample Site: Palos Verdes LF Oate Sam pled: 5/8/2006 Oate Reported: 5/19/2006Client Name: GeoLogic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1 ,2,3,4,5&6 Camp. Sample Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates %Recovery QC Limits in %1,2-Dichlorobenzene..cf4 65.5 46-1052,4,6-Tribromophenol 82.5 46-1462-Chlorophenol-d4 72.6 48-1172-Fluorobiphenyl 74.0 54-1122-FJuorophenoJ 68.9 45-1194-Terphenyl-d14 68.8 46-135Nitrobenzene-d5 67.3 40-116Phenol-d5 71.6 37-127Key: MOL,:Method Detection limit RL=Reporting Lim·~ J::: TraceConc.belween MOLard RL M.B '= Method Blank T.B::: TripBlank F.B:::Field Blank E.B=Equipment Blank
AccuLabs, Inc.
-E\?&hiLaboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-5 Composile Acculabs 10: 06050004-05
Sample Site: Palos Verdes IF Date Sampled: 5/11/2006 Date Reported: 5/19/2006Client Name: Geologic Associales Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-5-1,2,3,4,5 Comp. Sampie Matrix: Soil Extraction Method: EPA 3550B
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Date Dale
Analyte Method Batch MDL RL Resull DF Extracted Analyzed Qualifiers
Acenaphthene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Acenaphlhylene 8270C 6050004 31 330 ND 1 5/17/06 5/18/06
Anthracene 8270C 6050004 28 330 ND 1 5/17108 5/18/06
Benzidine 8270C 6050004 110 1600 ND 1 5/17/08 5/18/08
Benza[a]anthracene 8270C 6050004 86 330 ND 1 5/17/06 5118/08
Benzo[bjfluoranlhene 8270C 6050004 96 330 ND 1 5/17/06 5/18/06
Benzo[klfluoranlhene 8270C 6050004 100 330 ND 1 5/17/06 5/18/06
Benzolalpyrene 8270C 6050004 87 330 ND 1 5/17/06 5/18/06
Benzo[g,h,ijperylene 8270C 6050004 76 330 ND 1 5/17/06 5/18/06
Benzoic acid 8270C 6050004 100 1600 ND 1 5/17/06 5/18/06
Benzyl alcohol 8270C 6050004 33 660 ND 1 5/17/06 5/18/06
Benzidine ( M ) 8270C 6050004 110 1600 ND 1 5/17/06 5/18/06
4-Bromophenyl phenyl ether 8270C 6050004 37 330 ND 1 5/17106 5/18/06
Butyl benzylphlhalale 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
Di-n-butylphthalate 8270C 6050004 24 330 ND 1 5117/06 5/18/06
4-Chloroaniline 8270C 6050004 28 660 ND 1 5117/06 5/18/06
bis(2-Chloroelhoxy) methane 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
bis(2-Chloroelhyl) ether 8270C 6050004 24 330 ND 1 5/17/06 5/18/06
bis(2-Chloroisopropyl)elher 8270C 6050004 33 330 ND 1 5/17/06 5/18/06
4-Chloro-3-methylphenol 8270C 6050004 32 660 ND 1 5/17/06 5/18/06
2-Chloronaphlhalene 8270C 6050004 23 330 ND 1 5/17/06 5/18/06
2-Chlorophenol 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
4-Chlorophenyl phenyl ether 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Chrysene 8270C 6050004 27 330 ND 1 5/17106 5/18/06
Dibenzofuran 8270C 6050004 26 330 ND 1 5/17/06 5118/06
Diben[a,hjanlhracene 8270C 6050004 76 330 ND 1 5/17/06 5118/06
1,2-Dichlorobenzene 8270C 6050004 24 330 ND 1 5/17/06 5/18/06
1,3-Dichlorobenzene 8270C 6050004 23 330 ND 1 5117/06 5/18/06
1A-Dichlorobenzene 8270C 6050004 27 330 ND 1 5/17106 5/18/06
3,3'-Dichlorbenzidine 8270C 6050004 260 660 ND 1 5/17/06 5/18/06
2,4-Dichlorophenol 8270C 6050004 28 1600 ND 1 5/17/06 5/18/06
Dielhylphlhalate 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
2,4-Dimelhylphenol 8270C 6050004 37 330 ND 1 5/17/06 5/18/06
Dimelhylphlhalale 8270C 6050004 25 330 ND 1 5/17/06 5/18/06
2,4-Dinitrophenol 8270C 6050004 22 1600 ND 1 5/17106 5/18/06
2,4-Dinitrotoluene 8270C 6050004 29 330 ND 1 5117/06 5/18/06
2,6-Dinitrotoluene 8270C 6050004 30 330 ND 1 5/17/06 5/18/06
4,6-Dinltro-2-melhylphenol 8270C 6050004 45 1600 ND 1 5/17106 5/18/06
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sarno/e/nfo Report/nfoProject ID: 2006.0088 Sample ID: VN-5 Composite Acculabs 10: 06050004-05
Sample Site: Palos Verdes IF Date Sampled: 5/11/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client ID: VN-5-1,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMOLBatchMethod
Semlvolatlle Orgamc Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyle
bis(2-Ethylhexyl)phlhalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno[1,2,3-cd)pyrene
Isophorone
2-Methylnaphlhalene
2-Melhylphenol
4-Melhylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline4-Nitroaniline
Nitrobenzene
2-Nilrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
n-Nitrosodiphenylamine
Oi-n-octylphthalate
Oi-n-bulylphthalate
Pentachlorophenol
Phenanthrene
Phenol
Pyrena
1,2,4-Trichlorbenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
8050004
8050004
8050004
8050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
8050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
3628
2921
2241
29170
88
28
27
24
34
2945
27
26
53
27
330
330
330
330
860
860
330
330
330
330
330
330
330
1600
1600
1600
330
330
1800
330
330
330
330
1600
330
330
330
330
330
330
NO 1 5/17/08
NO 1 5/17/08
NO 1 5/17/06
NO 1 5/17/05
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17108
NO 1 5/17/08
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/05
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/08
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17108
NO 1 5/17/08
NO 1 5/17/06
5/18/08
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/05
5/18/05
5/18/06
5/18/06
5118/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/08
5/18/08
5/18/08
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
(~) AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrialand HazardousWaste. Chemical Consultation
Proiect Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-S Composite Acculabs 10: 06050004-05
Sample Site: Palos Verdes IF Date Sampled: 5/11/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-5-1 ,2,3,4,5 Compo Sam ole Matrix: Soil Extraction Method: EPA 35508
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 55.8 46-105
2,4,6-Tribromophenol 76.6 46-1462-Chlorophenol-d4 59.6 48-1172-Fluorobiphenyl 60.6 54-1122-Fluorophenol 58.9 45-1194-Terphenyl-d14 92.6 46-135Nitrobenzene-d5 59.6 40-116
Phenol-d5 60.8 37-127Key: MDL'" Method Detection limit RL= Reporting Limit J= Trace Concbetween MOL and RL M.B =Method Blank T.B= Trip Blank F.B=FieJdBlank E.B: Equipment Blank
AccuLabs, Inc.
-~t±iLaboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. Waterand Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Proiect Info SamD/e/nfo ReDort/nfoProject ID: 2006.0088 Sample ID: VN-6 Composite Acculabs ID: 06050004-06
Sample Site: Palos Verdes IF Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client 10: VN-6-1 ,2,3,4,5 Camp. Samole Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMOLBalchMethod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Dale
Result OF ExtractedAnalyle
Acenaphlhene
Acenaphthylene
Anthracene
Benzidine
Benzo[a]anthracene
Benzo[b]f1uorantheneBenzo[k]f1uorantheneBenzo[ajpyrene
Benzo[g,h,ijperylene
Benzoicacid
Benzyl alcohol
Benzidine ( M )
4-Bromophenyl phenyl ether
Butyl benzylphthalate
Di-n-butylphthalate
4-Chloroaniline
bis(2-Chloroelhoxy) methane
bis(2-Chloroelhyl) ether
bis(2-Chloroisopropyl)ether
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzofuran
Diben[a,h]anthracene1,2-Dichlorobenzene
1,3-Dichlorobenzene
1A-Dichlorobenzene3.3'-Dichlorbenzidine
2,4-0ichlorophenol
Oielhylphlhalate
2,4-0imelhylphenol
Olmelhylphthaiate
2,4-0Inilrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
4,6-0initro-2-melhylphenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96
100
87
76
100
33
110
3728
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
37
25
22
2930
45
330
330
330
1600
330
330
330
330
330
1600
660
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
330
1600
330
330
1600
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17106
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5118/06
5118/06
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5118/06
5118/06
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial andHazardous Waste. Chemical Consultation
Proiect Info SamDlelnfo ReoortlnfoProject 10: 2006.0088 Sample 10: VN-6 Composite Acculabs 10: 06050004-06
Sample Site: Palos Verdes IF Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-6-1 ,2,3,4,5 Compo Samole Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMDLBalchMethod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Date
Result DF ExtractedAnalyle
bis(2-Elhylhexyl)phlhalale
FluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno[1,2,3-cd]pyrene
Isophorone2-Melhylnaphlhalene
2-Melhylphenol
4-Melhylphenol
Naphlhalene
2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-NitrophenolN-Nitroso-di-n-propylaminen-Nitrosodiphenylamine
Di-n-octylphthalate
Di-n-butylphthalate
PentachlorophenolPhenanthrenePhenol
Pyrena1,2,4-Trichlorbenzene
2,4,5-Trlchlorophenol
2,4,6-Trlchlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
36
28
2921
2241
29170
86
28
27
24
34
2945
27
26
53
27
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
330
330
1600
330
330
330
330
330
330
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
(4:) AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial andHazardous Waste. Chemical Consultation
Proiect Info SamDlelnfo ReDortlnfoProject 10: 2006.0088 Sample 10: VN-6 Composite AccuLabs 10: 06050004-06
Sample Site: Palos Verdes IF Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: uglKg
Client 10: VN-6-1 ,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 62.1 46-1052,4,6-Tribromophenol 82.8 46-1462-Chlorophenol-d4 67.8 48-1172-Fluorobiphenyl 66.0 54-1122-Fluorophenol 66.1 45-1194-Terphenyl-d14 102 46-135Nitrobenzene-d5 64.5 40-116Phenol-d5 70.5 37-127Key: MDL- MethodDetection Limit RL= Reporting Limit J- TraceConc.between MOLandRL M.B = Method Blank T,B=Tnp Blank F.B=FleldBlank E.B= EqUipment Blank
AccuLabs, Inc,
~l~Ellis Hsue1laboratory Director
RECEIVED
~ AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultati
GLA-San :Bernardino
Project Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Date Sampled: 5/8,9,10 & 11 /2006 AccuLabs Batch No.: AL-06050004
Sample Site: Palos Verdes Landfill Date Received: 5/12/06 Date Reported: 5/26/06Client Name: Gecl.ootc Associates Sample Matrix: Liquid Extract from Soil Reporting Units: mg/L
Chromium Test by STLC-Wet Extraction (EPA 601 OB & Cal-DHS)
ClientlD NA VN-1 Composite VN-2 Composite VN-3 Composite VN-4 Composite VN-5 Composite VN-6 Composite Date
AccuLabs ID Method Blank 06050004-01 06050004-02 06050004-03 06050004-04 06050004-05 06050004-06 DF MDL R.L. Analyzed
Chromium ND 1.3 ND ND ND ND ND 1 0.52 1.0 5/18/06
Key: MDL =Method Detection Limit RL =Reporting Limit J =Trace Cone. between MDL and RL M.B. =Method Blank T.B. =Trip Blank F.B. =Field Blank E.B. =Equipment Blank
AccuLabs, Inc.
UGLl~t1Ellis H~uJ .Laboratory Director
(1)(2)(3)(4)(5)(6)(7)(8)
QC Summary Reports
<Part I : Method Blank Summary>
TPH as Gasoline by EPA 8015M (within the summary of report)
TPH as Diesel by EPA 8015M (within the summary of report)
Title 22 Metals by EPA 6010B & EPA 7471AOrganochlorine Pesticides (OCPs) by EPA 8081APolychlorinated Biphenyls (PCBs) by EPA 8082Organochlorine Herbicides by EPA 8151AVolatile Organic Compounds by EPA 8260BSemivolatile Organic Compounds by EPA 8270C
AccuLabs, Inc.Air Toxic. ContaminatedSoli. Water and Wastewater. Industrial and HazardousWaste. Chemical ConsulatJon
Project Info Report/nfoProject 10: 2006.0088 Sample 10: Method Blank AccuLabs 10: 06050004-MB
Sample Site: Palos Verde Landfill Date Sampled: NA Date Reported: 5/19/2006Client Name: GeoLogic Associates Date Received: NA Reporting Units: ug/Kg
Client 10: NA sarnole Matrix: Ottawa Sand
Organochlorine Pesticides by EPA 8081AEPA Sample Date Date
Analyte Method Batch MOL RL Result OF Prepared Analyzed Qualifiers
4,4,-DDD 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
4,4-DDE 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
4,4-DDT 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Aldrin 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
alpha-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
alpha-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
beta-SHC 8081A 6050004 0.60 1.0 NO 1 5/17/06 5/18/06
Chlordane 8081A 6050004 5.0 8.5 NO 1 5/17/06 5/18/06
delta-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Dieldrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
DieldrinEndosulfane I 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endosulfane II 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endosulfane suldfate 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin aldehyde 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
Endrin ketone 8081A 6050004 0.50 2.0 NO 1 5/17/06 5/18/06
gamma-SHC 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
gamma-Chlordane 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Heptachlor 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Heptachlor epoxide 8081A 6050004 0.50 1.0 NO 1 5/17/06 5/18/06
Methoxychlor 8081A 6050004 0.50 8.5 NO 1 5/17/06 5/18/06
Toxaphene 8081A 6050004 50 85.0 NO 1 5/17/06 5/18/06
Surrogates % Recovery ~
Tetrachloro-m-xylene 90.7 59-127
Decachlorobiphenyl 91.5 60-109Key: MOL;; Method Detection umn RL;; Reporting urnn J ;; Trace Cone. between MOL and Rl M.B. ;; Method Blank T.B.;; Trip Blank F.B.;; FieldBlank E.B. ;; Equipment Blank
AccuLabs, Inc.
~~j~1Laboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Proiect Info Sample Info Report InfoProject ID: 2006.0088 Sample ID: Method Blank AccuLabs ID: 0605004-MB
Sample Site: PalosVerde Landfill Date Sampled: NA Date Reported: 5/19/06Client Name: GeologicAssociates Date Received: NA Reporting Units: ug/Kg
Client ID: NA Sample Matrix: Ottawa Sand
Polychlorinated Biphenyls (PCBs) by EPA 8082
Sample Date Date
Analyle EPA Method MOL RL Result OF Extracted Analyzed QualifiersAroclor-1016 8082 5 16 NO 1 5/17106 5/18/06
Aroclor-1221 8082 5 33 NO 1 5/17/06 5/18/06
Aroclor-1232 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1242 8082 5 16 NO 1 5/17106 5/18/06
Aroclor-1248 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1254 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1260 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1262 8082 5 16 NO 1 5/17/06 5/18/06
Aroclor-1268 8082 5 16 NO 1 5/17/06 5/18/06
Surrogates %Recovery OC Limit
Decachlorobiphenyl 90.1 44-132
Tetrachloro-m-xylene 93.0 63-130Key: RL = Reporting limit J =TraceCone. BinMOLandRL M.B.= Method Blank T.B. = Tnp Blank F.B.= FieldBlank E.B.= Equipment Blank
AccuLabs, Inc.
~.lj~Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and HazardousWaste _ Chemical Consulation
Proiect Info Renort InfoProject 10: 2006.0088 Sample 10: Method Blank AccuLabs 10: 06050004-MB
Sample Site: PalosVerdes landfill Date Sampled: NA Date Reported: 5/22/2006plient Name: Geologic Associates Date Received: NA Reporting Units: ug/Kg
Client 10: NA Sample Matrix: Ottawa Sand
Organochlorine Herbicides by EPA 8151A
Analyte
2,4,5-T2,4-D82,4-DDalaponDicambaDichloropropDinosebMCPAMCPP4-NitrophenolPentachlorophenolSilvexSurrogate
2,4-DichlorophenyJacetic acid(DCAA)Kay; MDI. Method Detection Umit RL Reporting limit
AccuLabs, Inc.
~-ft0~~Laboratory Director
EPA Sample Date Date
Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
8151A 6050004 0.444 1.1 NO 1 5/19-20/06 5/21/06
8151A 6050004 0.555 5 NO 1 5/19-20/06 5/21/06
8151A 6050004 0.066 1.2 NO 1 5/19-20106 5/21/06
8151A 6050004 0.353 0.5 NO 1 5/19-20106 5/21/06
8151A 6050004 0.518 0.6 NO 1 5/19-20/06 5121/06
8151A 6050004 0.660 0.8 NO 1 5/19-20/06 5/21/06
8151A 6050004 0.413 1.1 NO 1 5/19-20/06 5/21/06
8151A 6050004 86.0 200 NO 1 5/19-20/06 5/21/06
8151A 6050004 103 150 NO 1 5/19-20/06 5/21106
8151A 6050004 1.89 5 NO 1 5/19-20/06 5/21/06
8151A 6050004 0.0437 1 NO 1 5/19-20/06 5/21106
8151A 6050004 0.438 1.2 NO 1 5/19-20/06 5/21/06% Recovery QC Limit
120 43-169J =Trace Cone. between MOL and RL M.B. = Melhod Blank T.B. = Trip Blank F.B. :::Field Blank E.B. = Equipment Blank
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial andHazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: Method Blank AcculabslD: 6050004BlK
Sample Site: Palos Verde IF Date Sampled: NA Date Reported: 5/19/06plient Name: Geologic Associates Date Received: NA Reporting Units: ug/Kg
Client 10: NA SamDle Matrix: Ottawa Sand
DateOF ExtractedAnalyte
Volatile Organic Compounds by EPA 82608 MethodEPA Sample
Method Batch MOL RL Result
DateAnalyzed Qualifiers
Acetone
BenzeneBromobenzene
BromochloromethaneBromodichloromethane
BromoformBromomethane
z-aiearone (MEK)
n-Butylbenzene
see-Butylbenzene
tert-ButylbenzeneCarbon tetrachloride
ChlorobenzeneChloroethane2-Chloroethyl vinyl ether(2-CEVE)
ChloroformChloromethane
2-ChlorotoJuene4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-ehloropropane1,2-DibromoethaneDibromomethane
1,2-Dichlorobenzene1,3-Dichlorobenzene
t.a-nrchlorobenzene
Dichlorodifluoromethane(F-12)1,1-Dichloroethane1,2-Dichloroethane
1,1-Dichloroethenecis-t ,2-Dichloroethene
trans-1,2-Dichloroethene1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane1,1-Dichlorcprcpene
EthylbenzeneHexachlorobutadiene
8260B 6010026 4.92 20 NO82608 6010026 0.84 5 NO
82608 6010026 0.84 5 NO82608 6010026 1.1 5 NO
82608 6010026 0.79 5 NO82608 6010026 0.67 5 NO
82608 6010026 2.01 5 NO82608 6010026 1.39 10 NO
82608 6010026 0.63 5 NO
82608 6010026 0.98 5 NO82608 6010026 0.85 5 NO
82608 6010026 0.70 5 NO82608 6010026 0.72 5 NO
82608 6010026 0.73 5 NO82608 6010026 1.77 10 NO
82608 6010026 0.70 5 NO82608 6010026 0.91 5 NO82608 6010026 0.72 5 NO82608 6010026 0.79 5 NO
82608 6010026 0.77 5 NO82608 6010026 1.75 5 NO
82608 6010026 0.80 5 NO82608 6010026 0.91 5 NO82608 6010026 0.81 5 NO82608 6010026 0.83 5 NO
82608 6010026 0.44 5 NO82608 6010026 1.72 5 NO82608 6010026 0.76 5 NO
82608 6010026 0.69 5 NO82608 6010026 1.04 5 NO
82608 6010026 0.55 5 NO82608 6010026 0.55 5 NO
82608 6010026 0.88 5 NO82608 6010026 0.94 5 NO
82608 6010026 0.67 5 NO
82608 6010026 0.85 5 NO82608 6010026 0.35 5 NO
82608 6010026 0.55 5 NO
1 51161061 5116106
1 51161061 5116106
1 51161061 5116106
1 51161061 5116106
1 5116106
1 51161061 5116106
1 51161061 5116106
1 51161061 51161061 5116106
1 51161061 51161061 5116106
1 51161061 51161061 5116106
1 51161061 5116106
1 5116/061 5116106
1 51161061 5116106
1 51161061 51161061 5116106
1 51161061 5116106
1 5116106
1 51161061 5116106
1 51161061 5116106
5116106
51161065116106
5116106
5116106
51161065116106
51161065116106
5116106
51161065116106
51161065116106
5116106
5116106
51161065116106
511610651161065116106
51161065116106
51161065116106
51161065116106
5116106
5116106
5116106
511610651161065116106
5116106
51161065116106
5116106
5116106Key: RL'" Reporting Urnit J" Trace Cone. Bin MOL and RL M.B." Malhod Blank 'r.a. = Trip Blank F.B. = Field Blank E.B." EquipmentBlank
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste _ Chemical Consultation
Proiect Info Sample Info ReoortlnfoProject 10: 2006.0088 Sample 10: Method Blank AcculabslD: 6050004BlK
Sample Site: Palos Verde IF Date Sampled: NA Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: NA Reporting Units: ug/Kg
Client 10: NA Sample Matrix: Ottawa Sand
Volatile Organic Compounds by EPA 8260B MethodEPA Sample Date Date
Analyte Method Batch MDL RL Result DF Extracted Analyzed Qualifiers
2-Hexanone 8260B 6010026 1.56 10 ND 1 5/16/06 5/16106
Isopropylbenzene 8260B 6010026 0.63 5 ND 1 5/16/06 5/16/06
4-lsopropyltoluene 8260B 6010026 0.55 5 ND 1 5/16/06 5/16/06
Methylene chloride 8260B 6010026 1.46 10 ND 1 5116/06 5116/06
4~Methyl-2-pentanone (MIBK) 8260B 6010026 2.64 10 ND 1 5/16/06 5/16/06
Napthalene 8260B 6010026 0.70 5 ND 1 5/16/06 5/16/06
n-Propylbenzene 8260B 6010026 0.92 5 ND 1 5/16106 5/16/06
Styrene 8260B 6010026 0.57 5 ND 1 5/16/06 5/16106
1,1,1,2-Tetrachloroethane 8260B 6010026 0.92 5 ND 1 5/16/06 5/16/06
1,1,2,2-Tetrachloroethane 8260B 6010026 2.28 5 ND 1 5/16/06 5/16/06
Tetrachloroethene (peE) 8260B 6010026 0.83 5 ND 1 5/16/06 5/16/06
Toluene 8260B 6010026 0.77 5 ND 1 5/16/06 5/16/06
1,2,3-Trichlorobenzene 8260B 6010026 0.85 5 ND 1 5/16/06 5/16/06
1,2,4-Trichlorobenzene 8260B 6010026 0.74 5 ND 1 5/16/06 5116/06
1,1,1-Trichloroethane 8260B 6010026 0.99 5 ND 1 5/16/06 5/16/06
1,1,2-Trichloroethane 8260B 6010026 1.31 5 ND 1 5/16106 5/16/06
Trichloroethane (TeE) 8260B 6010026 1.4 5 ND 1 5/16/06 5/16106
Trichlorofluoromethane(F-11) 8260B 6010026 0.66 5 ND 1 5/16/06 5/16/06
1,2,3~Trichloropropane 8260B 6010026 1.97 5 ND 1 5/16/06 5/16106
1,2,4-Trimethylbenzene 8260B 6010026 0.55 5 ND 1 5/16/06 5/16/06
1,3,5-Trimethylbenzene 8260B 6010026 1.03 5 ND 1 5/16/06 5/16/06
Vinyl chloride 8260B 6010026 1.81 5 ND 1 5/16/06 5/16/06
m,p-Xylene 8260B 6010026 1.84 10 ND 1 5/16/06 5/16/06
o-Xylene 8260B 6010026 0.66 5 ND 1 5/16/06 5/16/06
Methyl-tert-butyl-ether (MTBE) 8260B 6010026 0.95 10 ND 1 5/16106 5/16/06
tert-Butanol (TBA) 8260B 6010026 5.56 20 ND 1 5/16/06 5/16106
Diisopropyl ether (DIPE) 8260B 6010026 0.66 5 ND 1 5/16/06 5/16/06
Ethyl-tert-butyl-ether (ETBE) 8260B 6010026 0.64 5 ND 1 5/16/06 5/16/06
tert-Amyl methyl ether (TAME) 8260B 6010026 0.55 5 ND 1 5/16/06 5/16/06
Surrogate: Dibromofluoromethane (75-125%) 101 %
Surrogate: 1,2-Dichloroethane-d4 (75-125%) 104 %
Surrogate: Toluene-d8 (75-125%) 106 %
Surrogate: 4-Bromofluorobenzene (75-125%) 113 %
Key: MOL'" Mel Detection Lmt RL _ Reporting limit J - Trace Cone.bin MOL and RL M.B. '" Method Blank T.B. '" Trip Blank F.B. '" Field Blank E.B. '" EquipmentBlank
AccuLabs, Inc.
ld' fElh;~~laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrialand HazardousWaste. ChemicalConsultation
Project Info SamDle Info ReDort InfoProject 10: 2006.0088 Sample 10: Method Blank Acculabs 10: 06050004-MB
Sample Site: Palos Verdes IF Date Sampled: NA Date Reported: 5/19/2006
Client Name: Geologic Associates Date Received: NA Reporting Units: ug/KgClient 10: NA Sample Matrix: Ottawa Sand Extraction Method: EPA 3550B
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Date Date
Analyle Method Batch MDL RL Result DF Extracted Analyzed Qualifiers
Acenaphthene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Acenaphthylene 8270C 6050004 31 330 ND 1 5/17/06 5/18/06
Anthracene 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
Benzidine 8270C 6050004 110 1600 ND 1 5/17/06 5/18/06
Benzojajanthracene 8270C 6050004 86 330 ND 1 5117/06 5/18/06
Benzo[b]fIuoranthene 8270C 6050004 96 330 ND 1 5/17/06 5/18/06
Benzo[k]fluoranthene 8270C 6050004 100 330 ND 1 5/17/06 5/18/06
Benzojalpyrene 8270C 6050004 87 330 ND 1 5/17/06 5118/06
Benzo[g,h,ijperylene 8270C 6050004 76 330 ND 1 5/17/06 5/18/06
Benzoic acid 8270C 6050004 100 1600 ND 1 5/17/06 5118/06
Benzyl alcohol 8270C 6050004 33 660 ND 1 5/17/06 5/18/06
Benzidine ( M ) 8270C 6050004 110 1600 ND 1 5/17/06 5118/06
4-Bromophenyl phenyl ether 8270C 6050004 37 330 ND 1 5/17/06 5118/06
Butyl benzylphthalate 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
Di-n-butylphthalate 8270C 6050004 24 330 ND 1 5/17/06 5/18/06
4-Chloroaniline 8270C 6050004 28 660 ND 1 5/17/06 5118/06
bis(2-Chloroethoxy) methane 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
bis(2-Chloroethyl) ether 8270C 6050004 24 330 ND 1 5/17106 5/18/06
bis(2-Chloroisopropyl)ether 8270C 6050004 33 330 ND 1 5/17106 5/18/06
4-Chloro-3-methylphenol 8270C 6050004 32 660 ND 1 5/17/06 5/18/06
2-Chloronaphthalene 8270C 6050004 23 330 ND 1 5/17106 5/18/06
2-Chlorophenol 8270C 6050004 28 330 ND 1 5/17/06 5118/06
4-Chlorophenyl phenyl ether 8270C 6050004 26 330 ND 1 5/17/06 5118/06
Chrysene 8270C 6050004 27 330 ND 1 5/17/06 5/18/06
Dibenzofuran 8270C 6050004 26 330 ND 1 5/17106 5/18/06
Diben[a,hlanthracene 8270C 6050004 76 330 ND 1 5/17106 5/18/06
1,2-Dichlorobenzene 8270C 6050004 24 330 ND 1 5/17106 5/18/06
1,3-Dichlorobenzene 8270C 6050004 23 330 ND 1 5/17/06 5/18/06
1A-Dichlorobenzene 8270C 6050004 27 330 ND 1 5/17/06 5/18/06
3,3'-Dichlorbenzidine 8270C 6050004 260 660 ND 1 5/17/06 5/18/06
2,4-Dichlorophenol 8270C 6050004 28 1600 ND 1 5/17/06 5/18/06
Diethylphthalate 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
2,4-Dimethylphenol 8270C 6050004 37 330 ND 1 5/17/06 5/18/06
Dimethylphthalate 8270C 6050004 25 330 ND 1 5/17/06 5/18/06
2,4-Dinitrophenol 8270C 6050004 22 1600 ND 1 5/17/06 5/18/06
2,4-Dinitrotoluene 8270C 6050004 29 330 ND 1 5/17/06 5/18/06
2,6-Dinitrotoluene 8270C 6050004 30 330 ND 1 5/17106 5/18/06
4,6-Dlnitro-2-methylphenol 8270C 6050004 45 1600 ND 1 5/17106 5118/06
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste _ Chemical Consultation
Project Info SamDJelnfo ReDortlnfoProject 10: 2006.0088 Sample 10: Method Blank Acculabs 10: 06050004-MB
Sample Site: Palos Verdes IF Date Sampled: NA Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: NA SamDie Matrix: Soil Extraction Method: EPA 3550BSemlvolatlle Orgamc Compounds by EPA 8270C Method
Sample Date Date
Analyle Method Batch MDL RL Result DF Extracted Analyzed Qualifiers
bis(2-Ethylhexyljphlhalate 8270C 6050004 24 330 ND 1 5/17/06 5/18/06
Fluoranthene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Fluorene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
Hexachlorobenzene 8270C 6050004 26 330 ND 1 5/17106 5/18/06
Hexachlorobutadiene 8270C 6050004 27 660 ND 1 5/17/06 5/18/06
Hexachlorocyclopentadiene 8270C 6050004 33 660 ND 1 5/17/06 5/18/06
Hexachloroethane 8270C 6050004 27 330 ND 1 5/17/06 5/18/06
Indeno[1,2,3-cd]pyrene 8270C 6050004 74 330 ND 1 5/17/06 5/18/06
Isophorone 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
2-Methylnaphlhalene 8270C 6050004 29 330 ND 1 5/17/06 5/18/06
2-Methylphenol 8270C 6050004 32 330 ND 1 5/17/06 5/18/06
4-Methylphenol 8270C 6050004 36 330 ND 1 5/17/06 5/18/06
Naphthalene 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
2-Nitroaniline 8270C 6050004 29 1600 ND 1 5/17/06 5/18/06
3-Nitroaniline 8270C 6050004 21 1600 ND 1 5/17106 5/18/06
4-Nitroaniline 8270C 6050004 22 1600 ND 1 5/17106 5/18/06
Nitrobenzene 8270C 6050004 41 330 ND 1 5/17/06 5/18/06
2-Nitrophenol 8270C 6050004 29 330 ND 1 5/17/06 5/18/06
4-Nitrophenol 8270C 6050004 170 1600 ND 1 5/17/06 5/18/06
N-Nitroso-cli-n-propylamine 8270C 6050004 86 330 ND 1 5/17/06 5/18/06
n-Nitrosodiphenylamine 8270C 6050004 28 330 ND 1 5/17/06 5/18/06
Di-n-octylphthalate 8270C 6050004 27 330 ND 1 5/17/06 5/18/06
Di-n-butylphthalate 8270C 6050004 24 330 ND 1 5/17/06 5/18/06
Pentachlorophenol 8270C 6050004 34 1600 ND 1 5/17/06 5/18/06
Phenanthrene 8270C 6050004 29 330 ND 1 5/17/06 5/18/06
Phenol 8270C 6050004 45 330 ND 1 5/17106 5/18/06
Pyrena 8270C 6050004 27 330 ND 1 5/17/06 5/18/06
1,2,4-Trichlorbenzene 8270C 6050004 26 330 ND 1 5/17/06 5/18/06
2,4,5-Trichlorophenol 8270C 6050004 53 330 ND 1 5/17/06 5/18/06
2,4,6-Trichlorophenol 8270C 6050004 27 330 ND 1 5/17/06 5/18/06
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject 10: 2006.0088 Sample 10: Method Blank Acculabs 10: 06050004-MB
Sample Site: Palos Verdes IF Date Sampled: NA Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: NA Sample Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 74.2 46-1052,4,6-Tribromophenol 88.5 46-1462-Chlorophenol-d4 76.5 48-1172-Fluorobiphenyl 80.6 54-1122-Fluorophenol 74.7 45-1194-Terphenyl-d14 105 46-135Nitrobenzene-d5 80.6 40-116Phenol-d5 78.5 37-127Key:. MOL= Method Detection Limit RL= Reporting Limit J= Trace Cone.between MOL and RL M.B = Method Blank T.B= Tnp Blank F.B=Fiald Blank E.B= Equipment Blank
AccuLabs, Inc.
ttl"!Laboratory Director
(1)(2)(3)(4)(5)(6)(7)(8)
QC Summary Reports
<Part II : Matrix Spike Summary>
TPH as Gasoline by EPA 80I5MTPH as Diesel by EPA 80I5MTitle 22 Metals by EPA 60IOB & EPA 747IAOrganochlorine Pesticides (OCPs) by EPA 808lAPolychlorinated Biphenyls (PCBs) by EPA 8082Organochlorine Herbicides by EPA 8l5lAVolatile Organic Compounds by EPA 8260BSemivolatile Organic Compounds by EPA 8270C
_(4:,) AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Reoort InfoProject 10: 2006.0088 Date Sampled: 5/5,8,9,10 &11/06 AccuLabs Batch 10: 6050004
Sample Site: Palos Verde landfill Date Received: 5/12/2006 Date Reported: 5/19/06Client Name: GeologicAssociates Sample Matrix: Soil Reoortina Units: ua/Ka (ppb)
Laboratory Control Standard Spike Summary for TPH as Gasoline by EPA 8015M
AL-06050004 Sample Amount Spike Result MS Spike Result MSD DateLCS,LCSD Result Spiked MS % Recovery MSD % Recovery QC limit %RPD QC Limit Analvzed
TPH as Gasoline 0 1000 1037 104 1050 105 70-130 1.2 20 5/16/06Key: MDL= Method Detection limit RL= Reporting limit J= Trace Cone. between MDL and RL M.B. = Method Blank T.B.= Trip Blank F,B.= Field Blank E,B.= Equipment Blank
AccuLabs, Inc.
~[{Ellis Hsue '1Laboratory Director
w AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrialand Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Date Sampled: 5/5,8,9,10 &11/06 AccuLabs Batch 10: 6050004
Sample Site: Palos Verde landfill Date Received: 5/12/2006 Date Reported: 5/19/06Client Name: GeologicAssociates Sample Matrix: Soil Reporting Units: mg/Kg (ppm)
Laboratory Control Standard Spike Summary for TPH as Diesel by EPA 8015M
AL-06050004 Sample Amount Spike Result MS Spike Result MSD DateLCS,LCSD Result Spiked MS % Recovery MSD % Recovery QC Limit % RPD QC Limit Analyzed
TPH asDiesel 0 1000 1127 113 1089 109 70-130 3.4 20 5/16/06Key: MDL= Method Detection Limit RL= Reporting Limit J= Trace Cone. between MDL and RL M.B. =Method Blank T.B.= Trip Blank F.B.= Field Blank E.B.= Equipment Blank
AccuLabs, Inc.
'~(ifyJEllis HsueLaboratory Director
(1) AccuLabs, Inc.Air Toxic. Contamfnated Soil. Wab3Tand Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Renort InfoProject 10: 2006.0088 Date Sampled: 5/5,8,9,10 & 11/06 AccuLabs Batch ID: 6050004
Sample Site: Palos Verde Landfill Date Received: 5/12/06 Date Reported: 5/19/06Client Name: GeoLoQic Associates Sample Matrix: Soil Reportina Units: maiKo
MS/MSD Summary of Title 22 Metals by EPA 6010B & EPA 7471A (Mercury)
Spiked Sample:-------- -._-_.._-
084443-011 for Sample Amount Spike Result MS Spike Result MSD Date
Batch 6050004 Result Spiked 06050004MS % Recovery 06050004MSD % Recovery QC Limit %RPD QC Limit R.L. Analyzed
Antimony 4.39 125 76.7 58 74.7 56 25-108 2.8 25 2.0 5117/06
Arsenic 7.45 125 99.2 73 90.3 66 46-118 10.2 25 1.0 5/17/06
Barium 114 125 198 67 190 61 32-131 10.0 25 1.0 5/17/06
Beryllium 0.2 125 94.7 76 88.0 70 59-104 7.3 25 1.0 5/17/06
Cadmium 0.3 125 93.1 74 85.2 68 63-105 8.9 25 1.0 5117/06
Chromium 54 125 144 72 161 86 49-116 17.2 25 1.0 5/17/06
Cobalt 14 125 105 73 97.3 67 58·104 8.8 25 1.0 5/17106Copper 17 125 119 82 111 76 54-126 8.1 25 2.0 5117/06
Lead 22 125 106 67 97.7 60 31-122 10.4 25 1.0 5117/06
Molybdenum 0 125 97 78 90.3 72 61-104 7.4 25 1.0 5/17/06
Nickel 69 125 155 69 148 63 50-112 8.5 25 1.0 5/17/06
Selenium 0.0 125 87.2 70 80.9 65 53-109 7.5 25 1.0 5117/06
Silver 0.0 125 88.4 71 82.8 66 41-121 6.5 25 1.0 5/17/06
Thallium 0.0 125 85.5 68 76.9 62 54-100 10.6 25 1.0 5/17/06Vanadium 34.3 125 129 76 127 74 59-109 2.1 25 1.0 5/17/06
Zinc 70 125 140 56 125 44 27-131 24.2 25 1.0 5117/06
Mercury 0 0.83 1.04 125 1.04 125 52-163 0.00 25 0.10 5/17/06
Key: MOL =Method Detection Limit RL =Reporting Limit J =Trace Conc. between MOL and RL M.B. =Method Blank T.B. =Trip Blank F.B. =Field Blank E.B. =Equipment Blank
AccuLabs, Inc.
1£1 H~1Ellis HsueLaboratory Director
(±) Accul.abs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Samp/e/nfo Report InfoProject 10: 2006.0088 Date Sampled: 5/5.8.9.10.11/06 AccuLabs Batch 10: 6050004-MS &MSD
Sample Site: PalosVerde Landfill Date Received: 5/12/2006 Date Reported: 5/19/2006
Client Name: GeoLoaic Associates Samole Matrix: Soil Reporting Units: mg/Kg
MS/MSD Summary of Organochlorine Pesticides (EPA Method 8081A)~
Spiked Sample: Sample Amount Spike Result MS Spike Result MSD Date--------"....-._------_.
084439-002 Result Spiked MS % Recovery MSD % Recovery oc Limit %RPD ac Limit R.L. Analyzed
4,4'-DDT 0 16.65 15.55 93.4 16.25 97.6 64-165 4.4 30 2.0 5/18/2006
Aldrin 0 16.65 18.76 113 18.10 109 68-135 3.6 30 1.0 5/18/2006
Dieldrin 0 16.65 18.73 112 18.88 113 48-165 0.8 30 2.0 5/18/2006
Endrin 0 16.65 20.58 124 22.24 134 60-186 7.8 30 2.0 5/18/2006
gamma-BHC 0 16.65 17.51 105 17.01 102 70-134 2.9 30 1.0 5/18/2006
Heptachlor 0 16.65 19.83 119 19.20 115 73·152 3.2 30 1.0 5/18/2006
TCMX (Surrogate) 0 16.65 13.33 80.1 12.57 75.5 60-109 5.9 30 5/18/2006
Dibutyl chlorendate(Surr.) 0 16.65 15.02 90.2 15.59 93.6 59-127 3.7 30 5/18/2006
Key:MDL = MethodDetection Limit RL = ReportingLimit J = Trace Cone. between MDL and RL M.B.= MethodBlankT.B.=Trip Blank F.B.= Field Blank E.B. = EquipmentBlank
.~g~~aps, Inc.
E~HrJ?1Laboratory Director
QiLJ AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consultation
Project Info Sample Info Report InfoProject ID: 2006.0088 Date Sampled: 5/5.8.9.10.11/06 Acculabs Batch ID: 6050004-MS &MSD
Sample Site: Palos Verde Landfill Date Received: 5/12/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Sample Matrix: Soil Reporting Units: mglKg
MS/MSD Summary of Polychlorinated Biphenyls by EPA 8082
Spiked Sal11J'I~:~ Sample Amount Spike Result MS Spike Resuit MSD Date
084456-004 Result Spiked MS % Recovery MSD % Recovery QC Limit %RPD QC Limit R.L. Anaiyzed
Aroclor-1016 0 166.6 155.3 93.2 156.1 93.7 77-106 0.5 30 16 5/18/06
Aroclor-1260 0 166.6 155.5 93.3 157.3 94.4 78-114 1.2 30 16 5/18/06
Tetrachloro-m-xylene 0 16.65 17.25 104 15.52 93.2 63-130 10.6 30 5/18/06Decachlorobiphenyl(S) 0 16.65 14.97 90 16.95 101.8 44-132 12.4 30 5/18/06
Key:MDL = Method Detection Limit RL = Reporting Limit J = Trace Cone. between MDL and RL M.B.= Method Biank T.B.=Trip Blank F.B.= Field Blank E.B. = Equipment Blank
AccuLabs, Inc.
~H~~Jlaboratory Director
QiLJ AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Reoon InfoProject 10: 2006.0088 Date Sampled: 5/5.8.9.10.11/06 AccuLabs Batch 10: 6050004-MS &MSD
Sample Site: Palos Verde landfill Date Received: 5/12/2006 Date Reported: 5/22/2006Client Name: Geologic Associates Sample Matrix: Soil Reportina Units: mg/Kg
MS/MSD Summary of Organochlorine Herbicides by EPA 8151A
Spiked Sample: Sample Amount Spike Result MS Spike Result MSD Date
DT-06-3462 Result Spiked MS % Recovery MSD % Recovery QC Limit %RPD QC Limit R.L. Analyzed
2,4-0 0 100 110 110 106 106 50-180 3.7 30 1.1 5121/06
2,4,5-TP(Silvex) 0 100 98 98 94 94 42-180 4.2 30 1.2 5/21/06
2,4,5-T 0 100 110 110 108 108 68-160 1.8 30 1.2 5/21/06
DCAA (Surrogate) 130 125 5121106
Key:MDL = Method Detection Limit RL = Reporting Limit J = Trace Cone. between MOL and RL M.B.= Method Blank T.B.=Trip Blank F.B.= Field Blank E.B. = Equipment Blank
AccuLabs, Inc.
-uit-k1Ellis Hsuelaboratory Director
w AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Date Sampled: 5/5,8,9,10 &11/06 Acculabs Batch 10: 6050004
Sample Site: Palos Verde landfill Date Received: 5/12/2006 Date Reported: 511912006Client Name: Geologic Associates Sample Matrix: Soil Reporting Units: ug/Kg
Matrix Spike Summary for vae Analysis by EPA 8260B
SpikedSample: Sample Amount Spike Result MS SpikeResult MSD Date
VN-5 16050004-5 Result Spiked MS % Recovery MSD % Recovery QC Limit %RPD ac Limit Analyzed
1,1 -Dichloroethene 0 15 12.8 85.4 12.4 83 70-130 3.3 20 5/16/2006Benzene 0 15 13.6 90.8 12.9 86 70-130 5.7 20 5/16/2006
Trichloroethene 0 15 13.2 87.8 14.2 95 70-130 7.5 20 5/16/2006Toluene 0 15 16.3 109 15.7 104 70-130 4.2 20 5/16/2006
Chlorobenzene 0 15 14.9 99.0 13.6 91 70-130 8.5 20 5/16/2006Key: MDL=Method Detection Limit RL=Reporting Limit J= TraceCone. between MDLand RL M.B. = Method BlankT.B.=Trip Blank F.B.=FieldBlankE.B.=Equipment Blank
~_u~s, Inc.
Ellis ~sb~iLaboratory Director
(~) AccuLabs, Inc.Air TOXIc. Contaminated Soil _Water andWastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report Info
Project 10: 2006.0088 Date Sampled: 5/5,8,9,10 &11/06 Acculabs Batch 10: 6050004
Sample Site: Palos Verde Landfill Date Received: 5/12/2006 Date Reported: 5/19/2006
Client Name: Geologic Asociates Sample Matrix: Soil Reporting Units: ug/Kg
ds bcfs---_ .. ---- - - ... __ ._ .. -- -_. __. __ ._-_.- -- --.--- - - .... - - ._--- .• -- - - -----._.___Sp~ked SamPJ~:.__._ Sample Amount Spike Result MS Spike Result MSD Date
084457-008 Result Spiked MS % Recovery MSD % Recovery QC Limit %RPD QC Limit Analyzed......._-_ .....__.__.".._-, .•..•......~..,,-2580 87.8 59-129 5/17/2006Acenaphthene 0 3300 78.2 2897 12 30
1A-Dichlorobenzene 0 3300 1870 56.7 2154 65.3 41-110 14 30 5/17/20062,4-Dinitrotoluene 0 3300 2742 83.1 3011 91.2 57-139 9.4 30 5/17/2006
N-Nitroso-di-n-propylamine 0 3300 2366 71.7 2662 80.7 41-135 12 30 5/17/2006
Pyrene 0 3300 2729 82.7 3224 97.7 58-138 17 30 5/17/2006
1,2,4-Trichlorbenzene 0 3300 2167 65.7 2419 73.3 45-126 11 30 5/17/2006
4-Chloro-3-methylphenol 0 3300 2638 79.9 2730 82.7 63-135 3.4 30 5/17/2006
2-Chlorophenol 0 3300 2051 62.2 2360 71.5 52-117 14 30 5/17/2006
4-Nitrophenol 0 3300 2251 68.2 2498 75.7 48-137 10 30 5/17/2006
Pentachlorophenol 0 3300 2991 90.6 3375 102 55-146 12 30 5/17/2006
Phenol 0 3300 2191 66.4 2473 74.9 51-122 12 30 5/17/2006
1,2-Diehlorobenzene-d4(S) 0 3300 2000 60.6 2210 67.0 46-105 10 30 5/17/2006
2-Chlorophenol-d4(S) 0 3300 2178 66.0 2423 73.4 48-117 11 30 5/17/2006
2-Fluoropheno-d4(S) 0 3300 2179 66.0 2336 70.8 45-119 7.0 30 5/17/2006
Phenol-d5 (S) 0 3300 2284 69.2 2491 75.5 37-127 8.7 30 511712006
Nitrobenzene-d5 (S) 0 3300 2290 69.4 2498 75.7 40-116 8.7 30 511712006
2-Fluorobiphenyl (S) 0 3300 2497 75.7 2751 83.4 54-112 9.7 30 5/17/2006
2,4,6-Tribromophenol (S) 0 3300 2887 87.5 3051 92.5 46-146 5.5 30 5/17/2006p-Terphenyl-d14 (S) 0 3300 3021 91.5 3575 108 46-135 17 30 5/17/2006
Key: MDL= Method Detection Limit RL = Reporting Limit J «Trace Cone. between MDL and RL M.B. = Method Blank T.B. = Trip Blank F.B. = Field Blank E.B. = Equipment Blank
~~U~~1bS, Inc.
E~~1Laboratory Director
AccuLabs, Inc.Air Toxic» Contaminated Sotl » Water and Wastewater· Industrial and Hazardous Waste· Chemical Consultation
Date: May 26, 2006
Mr. Mike Reasonand Mr. Jason SappGeoLogic Associates1831 Comrnercenter EastSan Bernardino, CA 92408
RE: Work Order Number: AL-06050004 / Palos Verde LandfillInvoice Number: GLA-OI04Y06-03
Dear Mr. Reason and Mr. Sapp:
Enclosed are the STLC report for Chromium and the revised report for SY~C test.Enclosed also was the invoice for the additional request test (STLC for Chromium) for thesamples received by AccuLabs on May 12, 2006.
The samples are tested for the parameters in accordance with the EPA methods as shown onthe chain of custody form.
Thank you for the opportunity to provide analytical tests for your company.
Please feel free to call me at (626) 934-1288 ifI can be of further assistance to yourcompany.
~d;IYrElliSH~fJLaboratory Director
15437 E. Proctol Avenue· City of Industry, California 91745 • Mailing Address: P.O. Box 92314· City of Industry, Caiifornia 91745·2314Tel: (626) 934·1288 • Fax: (626) 934-1299
(1) AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info SamDlelnfo ReDort InfoProject 10: 2006.0088 Date Sampled: 518,9,10 & 11 12006 AccuLabs Batch No.: AL-06050004
Sample Site: Palos Verdes landfill Date Received: 5/12/06 Date Reported: 5/26/06
Client Name: Geologic Associates Sample Matrix: Soil Reporting Units: mg/l
Chromium Test by STLC-Wet Extraction-ICP
Client ID NA VN-1 Composite VN-2 Composite VN-3 Composite VN-4 Composite VN-5 Composite VN-6 Composite Date
Acculebs ID MethodBlank 06050004-01 06050004-02 06050004-03 06050004-04 06050004-05 06050004-06 DF MDl R.L. Analyzed
Chromium NO 1.3 ND ND ND ND ND 20 0.05 1.0 5/26/06
Key: MDl = Method Detection Limit Rl, = Reporting Limit J =Trace Cone. between MDl and Rl M.B.= Method Blank T.B. = Trip Blank F.B. = Field Blank E.B. = Equipment Blank
AccuLabs, Inc.
td~~Ellis H~U~Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-1 Composite Acculabs 10: 06050004-01
Sample Site: Palos Verdes IF Date Sampled: 519/2006 Date Reported: 5/1912006Client Name: Geologic Associates Date Received: 5112/2006 Reporting Units: uglKg
Client 10: VN-1-1 ,2,3,4,5 Camp. Sample Matrix: Soil Extraction Method: EPA 35508Semlvolatlle Organic Compounds by EPA 8270C Method
Sample Date DateAnalyle Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
Acenaphthene 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
Acenaphthylene 8270C 6050004 31 330 NO 1 5/17/06 5/18/06
Anthracene 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
Benzidine 8270C 6050004 110 1600 NO 1 5/17106 5/18/06
Benzo[a]anthracene 8270C 6050004 86 330 NO 1 5/17/06 5/18/06
Benzo[bjfluoranthene 8270C 6050004 96 330 NO 1 5/17/06 5/18/06
Benzo[kjfluoranthene 8270C 6050004 100 330 NO 1 5/17/06 5118/06
Benzo[aJpyrene 8270C 6050004 87 330 NO 1 5117/06 5118/06
Benzo[g,h,ijperylene 8270C 6050004 76 330 NO 1 5/17/06 5/18/06
Benzoic acid 8270C 6050004 100 1600 NO 1 5117/06 5/18/06
Benzyl alcohol 8270C 6050004 33 660 NO 1 5/17/06 5/18/06
Benzidine ( M ) 8270C 6050004 110 1600 NO 1 5/17/06 5/18/06
4-Bromophenyl phenyl ether 8270C 6050004 37 330 NO 1 5/17/06 5/18/06
Butyl benzylphthalate 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
Oi-n-butyiphthalate 8270C 6050004 24 330 NO 1 5/17/06 5/18/06
4-Chloroaniline 8270C 6050004 28 660 NO 1 5/17/06 5/18/06
bis(2-Chloroethoxy) methane 8270C 6050004 26 330 NO 1 5/17/06 5118/06
bis(2-Chloroethyl) ether 8270C 6050004 24 330 NO 1 5117/06 5/18/06
bis(2-Chloroisopropyl)ether 8270C 6050004 33 330 NO 1 5/17/06 5/18/06
4-Chloro-3-methylphenol 8270C 6050004 32 660 NO 1 5/17/06 5/18/06
2-Chloronaphthalene 8270C 6050004 23 330 NO 1 5/17/06 5/18/06
2-Chlorophenol 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
4-Chlorophenyl phenyl ether 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
Chrysene 8270C 6050004 27 330 NO 1 5/17/06 5118/06
Dibenzofuran 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
Dlbenla.hjanthracene 8270C 6050004 76 330 NO 1 5/17/06 5/18/06
1,2-Dichlorobenzene 8270C 6050004 24 330 NO 1 5/17/06 5/18/06
1,3-Dichlorobenzene 8270C 6050004 23 330 NO 1 5/17/06 5/18/06
1,4-Dichlorobenzene 8270C 6050004 27 330 NO 1 5/17/06 5/18/06
3,3'-Dichlorbenzidine 8270C 6050004 260 660 NO 1 5/17/06 5/18/06
2,4-0ichlorophenol 8270C 6050004 28 1600 NO 1 5/17/06 5/18/06
Oiethylphthalate 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
2,4-0imethylphenol 8270C 6050004 37 330 NO 1 5117/06 5/18/06
Oimethylphthalate 8270C 6050004 25 330 NO 1 5/17/06 5/18/06
2,4-Dinitrophenol 8270C 6050004 22 1600 NO 1 5/17/06 5/18/06
2,4~Dinitrotoluene 8270C 6050004 29 330 NO 1 5/17/06 5/18/06
2,6-Dinitrotoluene 8270C 6050004 30 330 NO 1 5/17/06 5/18/06
4,6-0initro-2-methylphenol 8270C 6050004 45 1600 NO 1 5/17/06 5/18/06
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-1 Composite Acculabs 10: 06050004-01
Sample Site: Palos Verdes IF Date Sampled: 5/9/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
ClientlO: VN-1-1,2,3,4,5 Camp. Sample Matrix: Soil Extraction Method: EPA 35508Semlvolatlle Organic Compounds by EPA 8270C Method
Sample Date Date
Analyle Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
bis(2-Ethylhexyl)phthalate 8270C 6050004 24 330 NO 1 5/17/06 5118/06
Fluoranthene 8270C 6050004 26 330 NO 1 5117/06 5/18/06
Fluorene 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
Hexachlorobenzene 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
Hexachlorobutadiene 8270C 6050004 27 660 NO 1 5/17/06 5/18/06
Hexachlorocyclopentadiene 8270C 6050004 33 660 NO 1 5/17/06 5/18/06
Hexachloroethane 8270C 6050004 27 330 NO 1 5/17/06 5/18/06
Indeno[1,2,3-cd]pyrene 8270C 6050004 74 330 NO 1 5/17106 5/18/06
Isophorone 8270C 6050004 26 330 NO 1 5/17/06 5118/06
2-Methylnaphthalene 8270C 6050004 29 330 NO 1 5117/06 5/18/06
2-Methylphenol 8270C 6050004 32 330 NO 1 5/17/06 5/18/06
4-Methylphenol 8270C 6050004 36 330 NO 1 5/17/06 5/18/06
Naphthalene 8270C 6050004 28 330 NO 1 5/17/06 5/18/06
2-Nitroaniline 8270C 6050004 29 1600 NO 1 5/17/06 5/18/06
3-Nitroaniline 8270C 6050004 21 1600 NO 1 5/17/06 5/18/06
4-Nitroanitine 8270C 6050004 22 1600 NO 1 5/17/06 5/18/06
Nitrobenzene 8270C 6050004 41 330 NO 1 5/17/06 5/18/06
2-Nitrophenol 8270C 6050004 29 330 NO 1 5/17/06 5118/06
4-Nitrophenol 8270C 6050004 170 1600 NO 1 5/17/06 5/18/06
N-Nitroso-di-n-propyJamine 8270C 6050004 86 330 NO 1 5/17/06 5118/06
n-Nitrosodiphenylamine 8270C 6050004 28 330 NO 1 5117/06 5/18/06
Oi-n-octylphthalate 8270C 6050004 27 330 NO 1 5/17/06 5/18/06
Oi-n-bulylphthalate 8270C 6050004 24 330 NO 1 5/17/06 5/18/06
Pentachlorophenol 8270C 6050004 34 1600 NO 1 5/17/06 5/18/06
Phenanthrene 8270C 6050004 29 330 NO 1 5/17/06 5/18/06
Phenol 8270C 6050004 45 330 NO 1 5/17106 5/18/06
Pyrena 8270C 6050004 27 330 NO 1 5/17/06 5118/06
1,2,4-Trichlorbenzene 8270C 6050004 26 330 NO 1 5/17/06 5/18/06
2,4,5-Trichlorophenol 8270C 6050004 53 330 NO 1 5/17/06 5/18/06
2,4,6-Trichlorophenol 8270C 6050004 27 330 NO 1 5/17/06 5/18/06
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and HazardousWaste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-1 Composite Acculabs 10: 06050004-01
Sample Site: Palos Verdes IF Date Sampled: 5/9/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-1-1,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 54.9 46-105
2,4,6-Tribromophenol 74.9 46-146
2-Chlorophenol-d4 59.6 48-117
2-Fluorobiphenyl 62.5 54-112
2-Fluorophenol 58.3 45-119
4-Terphenyl-d14 65.5 46-135
Nitrobenzene-d5 56.8 40-116
Phenol-d5 61.8 37-127
Key: MOL= Method Detection Limit RL= Reporting Limit J= Trace Cone.between MOL and RL M.B" Method Blank T.B= Trip Blank F.B=FieJd Blank E.B= Equipment Blank
AccuLabs, Inc.
~~~'fLaboratory Director
AccuLabs, Inc.Air Toxic. Contaminated SoH. Water and Wastewater. Industrialand Hazardous Waste. ChemicalConsultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: Palos Verdes LF Date Sampled: 5/6/2006 Date Reported: 5119/2006Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client 10: VN-2-1,2,3,4.5&6 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Semlvolatlle OrgaOlc Compounds by EPA 8270C MethodSample Oate Oate
Analyle Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
Acenaphthene 8270C 6050004 26 330 NO 1 5117106 5118106
Acenaphlhylene 8270C 6060004 31 330 NO 1 5117106 5118106
Anthracene 8270C 6050004 28 330 NO 1 5117106 5118106
Benzidine 8270C 6050004 110 1600 NO 1 5117106 5118106
Benzo[a]anthracene 8270C 6050004 86 330 NO 1 5117106 5118106
Benzo[b]f1uoranthene 8270C 6050004 96 330 NO 1 5117106 5118106
Benzo[k]f1uoranthene 8270C 6050004 100 330 NO 1 5117106 5118106
Benzo[ajpyrene 8270C 6050004 87 330 NO 1 5117106 5118106
Benzo[Q,h,i]perylene 8270C 6050004 76 330 NO 1 5117106 5118106
Benzoic acid 8270C 6050004 100 1600 NO 1 5117106 5118106
Benzyl alcohol 8270C 6050004 33 660 NO 1 5117106 5118106
Benzidine ( M ) 8270C 6050004 110 1600 NO 1 5117106 5118106
4-Bromophenyl phenyl ether 8270C 6050004 37 330 NO 1 5117106 5118106
Butyl benzylphthalale 8270C 6050004 28 330 NO 1 5117106 5118106
Oi-n-butylphlhalate 8270C 6050004 24 330 NO 1 5117106 5118106
4-Chloroaniline 8270C 6050004 28 660 NO 1 5117106 5118106
bis(2-Chloroelhoxy) methane 8270C 6050004 26 330 NO 1 5117106 5118106
bis(2-Chloroelhyl) ether 8270C 6050004 24 330 NO 1 5117106 5118106
bis(2-ChloroisopropyIJether 8270C 6050004 33 330 NO 1 5117106 5118106
4-Chloro-3-melhylphenol 8270C 6050004 32 660 NO 1 5117106 5118106
2-Chloronaphthalene 8270C 6050004 23 330 NO 1 5117106 5118106
2-Chlorophenol 8270C 6050004 28 330 NO 1 5117106 5118106
4-Chlorophenyl phenyl ether 8270C 6050004 26 330 NO 1 5117106 5118106
Chrysene 8270C 6050004 27 330 NO 1 5117106 5118106
Dibenzofuran 8270C 6050004 26 330 NO 1 5117106 5118106
Diben[a,h]anthracene 8270C 6050004 76 330 NO 1 5117106 5118106
1,2-Dichlorobenzene 8270C 6050004 24 330 NO 1 5117106 5118106
1,3-Dichlorobenzene 8270C 6050004 23 330 NO 1 5117106 5118106
1,4-Dichlorobenzene 8270C 6050004 27 330 NO 1 5117106 5118106
3,3'-Dichlorbenzidine 8270C 6050004 260 660 NO 1 5117106 5118106
2,4-Dichlorophenol 8270C 6050004 28 1600 NO 1 5117106 5118106
Dielhylphthalale 8270C 6050004 28 330 NO 1 5117106 5118106
2,4-0imethylphenol 8270C 6050004 37 330 NO 1 5117106 5118106
Oimethylphthalate 8270C 6050004 25 330 NO 1 5117106 5118106
2,4-0initrophenol 8270C 6050004 22 1600 NO 1 5117106 5118/06
2,4-Dinitrotoluene 8270C 6050004 29 330 NO 1 5117106 5/18106
2,6-Dinitrotoluene 8270C 6050004 30 330 NO 1 5117/06 5118106
4,6-0Inilro-2-methylphenol 8270C 6050004 45 1600 NO 1 5/17106 5118/06
AccuLabs, Inc.Air Toxic • Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: Palos Verdes LF Date Sampled: 5/5/2006 Date Reported: 5/19/2006Client Name: GeoLogic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-2-1.2.3,4,5&6 Camp. Samole Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMDLBatchMethod
Semlvolatde Organic Compounds by EPA 8270C MethodSample DateResult OF ExtractedAnalyle
bis(2-Ethylhexyl)phlhalate
Fluoranthene
FluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone2-Methylnaphlhalene
2-Melhylphenol
4-Melhylphenol
Naphthalene
2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylaminen-Nitrosodiphenylamine
Di-n-octylphthalate
Di-n-butylphthalate
PentachlorophenolPhenanthrenePhenol
Pyrene1,2,4-Trichlorbenzene
2,4,S-Trichlorophenol2,4,6-Trichlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004.
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
36
28
2921
2241
29170
86
28
27
24
34
2945
27
26
53
27
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
330
330
1600
330
330
330
330
330
330
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
5118106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118106
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.Air Toxic • Contaminated Soil- Water and Wastewater. Industrial and Hazardous Waste _ Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-2 Composite AccuLabs 10: 06050004-02
Sample Site: Palos Verdes IF Date Sampled: 5/5/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-2-1.2.3,4.5&6 Comp. Sam ole Matrix: Soil Extraction Method: EPA 35508
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC limits in %
1.2-Dichlorobenzene-d4 60.0 46-1052,4,6~Tribromophenol 71.4 46-1462-Chlorophenol-d4 67 48-1172-FluorobiphenyJ 69.7 54-1122-Fluorophenol 64.4 45-1194-Terphenyl-d14 68.6 46-135Nitrobenzene-d5 63.1 40-116Phenol-d5 67.7 37-127Key: MOL= Method Detection Limit Rl= Reporting limit J= Trace Cone.between MOL and RL M.B '" Method Blank T.B= Trip Blank F.B"'Field Blank f.B= Equipment Blank
AccuLabs, Inc.
w1~Ellis Hsue .;laboratory Director
(~) AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrialand Hazardous Waste. Chemical Consultation
Proiect Info SarnD/e/nfo Report/nfoProject 10: 2006,0088 Sample 10: VN-3 Composite AccuLabs 10: 06050004-03
Sample Site: Palos Verdes LF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-3-1,2,3,4,5&6 Comp, Sample Matrix: Soil Extraction Method: EPA 35508
Date
Analyzed QualifiersRLMDLBatchMethod
SemlVolatlle Organic Compounds by EPA 8270C MethodSample Date
Result DF ExtractedAnalyte
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo[a]anthracene
Benzo[b]f1uoranthene
Benzo[k]f1uoranthene
Benzo[ajpyrene
Benzo[g,h,ijperylene
Benzoic acid
Benzyl alcohol
Benzidine ( M )
4-Bromophenyl phenyl ether
Butyl benzylphthalate
Di-n-bulylphthalate
4-Chloroaniline
bis(2-Chloroethoxy) methane
bis(2-Chloroethyl} ether
bis(2-Chloroisopropyl}ether
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzofuran
Diben[a,hjanthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1A-Dichlorobenzene
3,3'-Dichlorbenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
4,6-Dinitro-2-methylphenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96
100
87
76
100
33
110
37
28
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
37
25
22
2930
45
330
330
330
1600
330
330
330
330
330
1600
660
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
330
1600
330
330
1600
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject ID: 2006.0088 Sample ID: VN-3 Composite Acculabs ID: 06050004-03
Sample Site: Palos Verdes IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client ID: VN-3-1,2,3.4,5&6 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMDLBatchMethod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample DateResult DF ExtractedAnalyle
bis(2-Ethylhexyl)phlhalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
2-Methylnaphlhalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
3-NitroaniJine4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propyramine
n-Nitrosodiphenylamine
Di-n-oetylphlhalale
Di-n-butylphlhalale
Pentachlorophenol
Phenanthrene
Phenol
Pyrene1,2,4-Trichlorbenzene
2,4,5-Trichlorophenol
2.4,6-Trichlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
36
28
2921
2241
29170
86
28
27
24
34
2945
27
26
53
27
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
330
330
1600
330
330
330
330
330
330
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5117/06
ND 1 5117/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17/06
ND 1 5/17106
ND 1 5/17/06
ND 1 5/17/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consultation
Project Info Samp/e/nfo Report/nfoProject ID: 2006.0088 Sample ID: VN-3 Composite AccuLabs ID: 06050004-03
Sample Site: Palos Verdes LF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: GeoLogic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client ID: VN-3-1.2.3.4.5&6 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 61.9 46-105
2,4,6-Tribromophenol 83.9 46-146
2-Chlorophenol-d4 69.6 48-117
2-Fluorobiphenyl 69.3 54-112
2-Fluorophenol 67.2 45-119
4-Terphenyl-d14 66.9 46-135
Nitrobenzene-d5 63.9 40-116
Phenol-d5 72.1 37-127
Key: MOL= Method Detection Limit RL= Reporting limit J= Trace Conc.between MOL and RL M.B =Method Blank T.B; Trip Blank F.B=Fleld Blank E.B= EqUIpment Blank
AccuLabs, Inc.
tek4Ellis Hsue iLaboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Proiect Info SamDlelnfo ReDortlnfoProject 10: 2006.0088 Sample 10: VN-4 Composite Acculabs 10: 06050004-04
Sample Site: Palos Verdes IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1,2,3.4,5&6 Comp. Sample Matrix: Soil Extraction Method: EPA 35508
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Date Date
Analyle Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
Acenaphthene 8270C 6050004 26 330 NO 1 5117106 5118106
Acenaphthylene 8270C 6050004 31 330 NO 1 5117106 5118106
Anthracene 8270C 6050004 28 330 NO 1 5117106 5118106
Benzidine 8270C 6050004 110 1600 NO 1 5117106 5118106
Benzo[a]anthracene 8270C 6050004 86 330 NO 1 5117106 5118106
Benzo[b]f1uoranthene 8270C 6050004 96 330 NO 1 5117106 5118106
Benzo[k]fIuoranthene 8270C 6050004 100 330 NO 1 5117106 5118106
Benzo[a]pyrene 8270C 6050004 87 330 NO 1 5117106 5118106
Benzcjq.h.ijperylene 8270C 6050004 76 330 NO 1 5117106 5118106
Benzoic acid 8270C 6050004 100 1600 NO 1 5117106 5118106
Benzyl alcohol 8270C 6050004 33 660 NO 1 5117106 5118106
Benzidine ( M ) 8270C 6050004 110 1600 NO 1 5117106 5118106
4-Bromophenyl phenyl ether 8270C 6050004 37 330 NO 1 5117106 5118106
Butyl benzylphthalate 8270C 6050004 28 330 NO 1 5117106 5118106
Oi-n-butylphthalate 8270C 6050004 24 330 NO 1 5117106 5118106
4-Chloroaniline 8270C 6050004 28 660 NO 1 5117106 5118106
bis(2-Chloroethoxy) methane 8270C 6050004 26 330 NO 1 5117106 5118106
bis(2-Chloroethyl) ether 8270C 6050004 24 330 NO 1 5117106 5118106
bis(2-Chloroisopropyl)ether 8270C 6050004 33 330 NO 1 5117106 5118106
4-Chloro-3-methylphenol 8270C 6050004 32 660 NO 1 5117106 5118106
2-Chloronaphthalene 8270C 6050004 23 330 NO 1 5117106 5118106
2-Chlorophenol 8270C 6050004 28 330 NO 1 5117106 5118106
4-Chlorophenyl phenyl ether 8270C 6050004 26 330 NO 1 5117106 5118106
Chrysene 8270C 6050004 27 330 NO 1 5117106 5118106
Dibenzofuran 8270C 6050004 26 330 NO 1 5117106 5118106
Oiben[a,hlanthracene 8270C 6050004 76 330 NO 1 5117106 5118106
1,2-Dichlorobenzene 8270C 6050004 24 330 NO 1 5117106 5118106
1,3-Dichlorobenzene 8270C 6050004 23 330 NO 1 5117106 5118106
1,4-Dichlorobenzene 8270C 6050004 27 330 NO 1 5117106 5118106
3,3'-Dichlorbenzidine 8270C 6050004 260 660 NO 1 5117106 5118106
2,4-0ichlorophenol 8270C 6050004 28 1600 NO 1 5117106 5118106
Oiethylphthalate 8270C 6050004 28 330 NO 1 5117106 5118106
2,4-0imethylphenol 8270C 6050004 37 330 NO 1 5117106 5118106
Oimethylphthalale 8270C 6050004 25 330 NO 1 5117106 5118106
2,4-Dinitrophenol 8270C 6050004 22 1600 NO 1 5117106 5118106
2,4-Dinitrotoluene 8270C 6050004 29 330 NO 1 5117106 5118106
2,6-Dinitrotoluene 8270C 6050004 30 330 NO 1 5117106 5118106
4,6-0Initro-2-melhylphenol 8270C 6050004 45 1600 NO 1 5117106 5118106
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Proiect Info SarnD/e/nfo ReDort/nfoProject 10: 2006.0088 Sample 10: VN-4 Composite AccuLabs 10: 06050004-04
Sample Site: Palos Verdes IF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1,2,3,4,5&6 Comp. Samole Matrix: Soil Extraction Method: EPA 35508
Date
Analyzed QualifiersRLMOLBatchMethod
Semlvolatlle Orgamc Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyte
bis(2-Ethylhexyl)phthalate
Fluoranthene
FluoreneHexachlorobenzeneHexachlorobutadleneHexachlorocyclopentadieneHexachloroethaneIndeno[1,2,3-cd]pyrene
Isophorone2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline3-Nitroaniline4-Nitroaniline
Nitrobenzene2-Nitrophenol4-NitrophenolN-Nitroso-di-n-propylamine
n-NitrosodiphenylamineOi-n-oclylphthalate
Di-n-butylphthalate
PentachlorophenolPhenanthrene
Phenol
Pyrena
1,2,4-Trichlorbenzene
2,4,5-TrichlorophenoJ2,4,6-Trichlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
36
28
2921
2241
29170
86
28
27
24
34
2945
27
26
53
27
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
330
330
1600
330
330
330
330
330
330
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-4 Composite AccuLabs 10: 06050004-04
Sample Site: Palos Verdes LF Date Sampled: 5/8/2006 Date Reported: 5/19/2006Client Name: GeoLogic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-4-1 ,2,3,4,5&6 Comp. Sam Die Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 65.5 46-105
2,4,6-Tribromophenol 82.5 46-1462-Chlorophenol-d4 72.6 48-1172-Fluorobiphenyl 74.0 54-1122-FJuorophenoJ 68.9 45-1194-Terphenyl-d14 68.8 46-135Nitrobenzene-d5 67.3 40-116Phenol-d5 71.6 37-127Key: MOL= Method Detection Limit RL= Reporting Limit J= Trace Conc.between MOL and RL M.B '" Method Blank T.B= Trip Blank F.B=FieJdBlank E.B= Equipment Blank
AccuLabs, lnc.
~LIEllis H~-:J~Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Samo/e/nfo Reoort/nfoProject 10: 2006.0088 Sample 10: VN-5 Composite Acculabs 10: 06050004-05
Sample Site: Palos Verdes IF Date Sampled: 5/11/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-5-1,2,3,4,5 Camp. Samole Matrix: Soil Extraction Method: EPA 35508
Date
Analyzed QualifiersRLMOLBatchMethod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyle
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo[a]anthracene
Benzo[b]f1uoranthene
Benzo[k]f1uoranthene
Benzo[ajpyrene
Benzo[g,h,i]perylene
Benzoic acid
Benzyl alcohol
Benzidine ( M )
4-Bromophenyl phenyl ether
Butyl benzylphthalate
Di-n-butylphthalate
4-Chloroaniline
bis(2-Chloroethoxy) methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl)ether
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl elher
Chrysene
Dibenzofuran
Olben[a,hjanthracene
1,2-Dichlorobenzene
1,3-0ichlorobenzene
1A-Dichlorobenzene
3,3'-Dichlorbenzidine
2,4-Dichlorophenol
Oielhylphthalate
2,4-0imethylphenol
Oimethylphthalate
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
4,6-0inllro-2-methylphenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96100
87
76
100
33
110
37
28
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
37
25
22
2930
45
330
330
330
1600
330
330
330
330
330
1600
660
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
330
1600
330
330
1600
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
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5/18/06
5/18/06
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5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
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5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Proiect Info Samo/elnfo Report InfoProject 10: 2006.0088 Sample 10: VN-5 Composite AccuLabs 10: 06050004-05
Sample Site: Palos Verdes LF Date Sampled: 5111/2006 Date Reported: 5119/2006Client Name: GeoLogic Associates Date Received: 5/12/2006 Reporting Units: uglKg
Client 10: VN-5-1,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
DateAnalyzed QualifiersRLMOLBatchMelhod
Semlvolatlle Organic Compounds by EPA 8270C MethodSample DateResult OF ExtractedAnalyte
bis(2-Ethylhexyl)phlhalale
Fluoranthene
FluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadiene
HexachloroethaneIndeno[1,2,3-cd]pyrene
Isophorone2-Melhylnaphlhalene
2-Melhylphenol
4-Melhylphenol
Naphthalene2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-NitrophenolN-Nitroso-di-n-propylaminen-NitrosodiphenylamineDi-n-octylphthalate
Di-n-butylphthalate
PentachlorophenolPhenanthrene
Phenol
Pyrena1,2,4-Trichlorbenzene2,4,5-Trichlorophenol2,4,6-Trichlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
36
28
2921
2241
29170
86
28
27
24
34
2945
27
26
5327
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
330
330
1600
330
330
330
330
330
330
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5/18/06
5118/06
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5/18/06
5118/06
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5/18/06
5/18/06
5/18/06
5/18/06
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrialand HazardousWaste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-5 Composite Acculabs 10: 06050004-05
Sample Site: Palos Verdes IF Date Sampled: 5/11/2006 Date Reported: 5/19/2006Client Name: Geol.ogic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-5-1,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 3550B
Semivolatlle Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %
1,2-Dichlorobenzene-d4 55.8 46-105
2,4,6~Tribromophenol 76.6 46-146
2-Chlorophenol-d4 59.6 48-117
2-Fluorobiphenyl 60.6 54-112
2-Fluorophenol 58.9 45-119
4-Terphenyl-d14 92.6 46-135
Nitrobenzene-d5 59.6 40-116
Phenol-d5 60.8 37-127
Key: MOL= Method Detection Limit RL= Reporting limit J= Trace Conc.between MOL and RL M.B =Method Blank T.B= Trip Blank F.B=Field Blank E.B= Equipment Blank
AccuLabs, Inc.
td~Ellis Hsue 1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Proiect Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: VN-6 Composite Acculabs 10: 06050004-06
Sample Site: Palos Verdes IF Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-6-1,2,3,4,5 Compo SamDle Matrix: Soil Extraction Method: EPA 35508
Date
Analyzed QualifiersRLMOLBatchMethod
SemlYolatlle Organic Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyle
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo[a]anthracene
Benzo[b]f1uoranthene
Benzo[k]f1uoranthene
Benzo[a]pyrene
Benzo[g,h,ijperylene
Benzoic acid
Benzyl alcohol
Benzidine ( M )
4-Bromophenyl phenyi ether
Butyl benzylphlhalate
Oi-n-butylphlhalale
4-Chloroaniline
bis(2-Chloroethoxy) methane
bis(2-Chloroelhyl) ether
bis(2-Chloroisopropyl)ether
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzofuran
Oiben[a,hjanthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorbenzidine
2,4-0ichlorophenol
Oiethylphthalate
2,4-0imethylphenol
Oimethylphthalate
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
4,6-0initro-2-methylphenoi
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96
100
87
76
100
33110
3728
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
3725
22
293045
330
330
330
1600
330
330
330
330
330
1600
660
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
3301600
330
330
1600
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5117/06
5/18/06
5/18/06
5118/06
5118/06
5118/06
5/18/06
5/18/06
5/18/06
5118/06
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5118106
5/18/06
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5118106
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AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
SemlYolatrle Organic Compounds by EPA 8270C Method
Proiect Info SamDie Info ReDort InfoProject 10: 2006.0088 Sample 10: VN-6 Composite Acculabs 10: 06050004-06
Sample Site: Palos Verdes IF Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geol.cqic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: VN-6-1,2,3,4,5 Compo Sample Matrix: Soil Extraction Method: EPA 35508.
Sample Date Oate
Analyle Method Batch MOL RL Result OF Extracted Analyzed Qualifiers
bis(2-EthylhexyIJphthalate 8270C 6050004 24 330 NO 1 5117106 5118106
Fluorantheme 8270C 6050004 26 330 NO 1 5117106 5118106
Fluorene 8270C 6050004 26 330 NO 1 5117106 5118106
Hexachlorobenzene 8270C 6050004 26 330 NO 1 5117106 5118106
Hexachlorobutadiene 8270C 6050004 27 660 NO 1 5117106 5118106
Hexachlorocyclopentadiene 8270C 6050004 33 660 NO 1 5117106 5118106
Hexachloroethane 8270C 6050004 27 330 NO 1 5117/06 5118106
Indeno[1,2,3-cd]pyrene 8270C 6050004 74 330 NO 1 5117106 5118106
Isophorone 8270C 6050004 26 330 NO 1 5117106 5118106
2-Methylnaphthalene 8270C 6050004 29 330 NO 1 5117106 5118106
2-Methylphenol 8270C 6050004 32 330 NO 1 5117106 5118106
4-Methylphenol 8270C 6050004 36 330 NO 1 5/17106 5118106
Naphthalene 8270C 6050004 28 330 NO 1 5117106 5118106
2-Nitroaniline 8270C 6050004 29 1600 NO 1 5117106 5118106
3-Nitroaniline 8270C 6050004 21 1600 NO 1 5117106 5118106
4-Nitroaniline 8270C 6050004 22 1600 NO 1 5117106 5118106
Nitrobenzene 8270C 6050004 41 330 NO 1 5117106 5118106
2-Nitrophenol 8270C 6050004 29 330 NO 1 5117106 5118106
4-Nitrophenol 8270C 6050004 170 1600 NO 1 5117106 5118106
N-Nitroso-di-n-propylamine 8270C 6050004 86 330 NO 1 5117106 5118106
n-Nitrosodiphenylamine 8270C 6050004 28 330 NO 1 5117106 5118106
Ol-n-oclylphthalate 8270C 6050004 27 330 NO 1 5117106 5118106
Ol-n-bulylphthalate 8270C 6050004 24 330 NO 1 5117106 5118106
Pentachlorophenol 8270C 6050004 34 1600 NO 1 5117106 5118106
Phenanthrene 8270C 6050004 29 330 NO 1 5117106 5118106
Phenol 8270C 6050004 45 330 NO 1 5117106 5118106
Pyrene 8270C 6050004 27 330 NO 1 5117106 5118106
1,2,4-Trichlorbenzene 8270C 6050004 26 330 NO 1 5117106 5118106
2,4,5-Trichlorophenol 8270C 6050004 53 330 NO 1 5117106 5118106
2,4,6-Trichlorophenol 8270C 6050004 27 330 NO 1 5117108 5118106
(~) AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Protect Info Sarno/e/nfo Report/nfoProject 10: 2006.0088 Sample 10: VN-6 Composite Acculabs 10: 06050004-06
Sample Site: Palos Verdes IF Date Sampled: 5/10/2006 Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: uglKg
Client 10: VN-6-1,2,3,4,5 Camp. Samole Matrix: Soil Extraction Method: EPA 35508
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in%1,2-Dichlorobenzene-d4 62.1 46-105
2,4,6~Tribromophenol 82.8 46-146
2-Chlorophenol-d4 67.8 48-117
2-Fluorobiphenyl 66.0 54-112
2-Fluorophenol 66.1 45-119
4-Terphenyl-d14 102 46-135
Nitrobenzene-d5 64.5 40-116
Phenol-d5 70.5 37-127
Key: MOL=MethodDetection Limit Rl= Reporting llmll J=TraceConc.between MOLandRL M.B= Method Blank r.B= Tnp Blank F.B=Fleld Blank E.B= Equipment Blank
AccuLabs, Inc.
~~1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: Method Blank Acculabs 10: 06050004-MB
Sample Site: Palos Verdes IF Date Sampled: NA Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: NA Reporting Units: ug/Kg
Client 10: NA Sample Matrix: Ottawa Sand Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMOLBatchMethod
Semlvolatlle Orgamc Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyle
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo[a]anthracene
Benzo[b]f1uoranthene
Benzo[klfluoranthene
Benzo[a]pyrene
Benzo[g,h,ijperylene
Benzoic acid
Benzyl alcohol
Benzidine ( M )
4-Bromophenyl phenyl ether
Butyl benzylphthalate
Oi-n-butylphthalate
4~Chloroaniline
bis(2-Chloroethoxy) methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl)ether
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzofuran
Diben[a,h]anthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1A-Dichlorobenzene
3,3'-Dichlorbenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-0imethylphenol
Dimethylphthalate
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
4,6-Dinitro-2-methylphenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
26
31
28
110
86
96100
87
76
100
33
110
37
28
24
28
26
24
33
32
23
28
26
27
26
76
24
23
27
260
28
28
37
25
22
2930
45
330
330
330
1600
330
330
330
330
330
1600
660
1600
330
330
330
660
330
330
330
660
330
330
330
330
330
330
330
330
330
660
1600
330
330
330
1600
330
330
1600
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
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NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17/06
NO 1 5/17106
NO 1 5/17/06
NO 1 5/17/06
5/18/06
5/18/06
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5/18/06
5/18/06
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5/18/06
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5118/06
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AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater. Industrial andHazardous Waste. Chemical Consultation
Proiect Info Sample Info Report InfoProject 10: 2006.0088 Sample 10: Method Blank Acculabs 10: 06050004-MB
Sample Site: Palos Verdes IF Date Sampled: NA Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/12/2006 Reporting Units: ug/Kg
Client 10: NA Samole Matrix: Soil Extraction Method: EPA 3550B
Date
Analyzed QualifiersRLMOLBatchMethod
Semlvolatlle Orgamc Compounds by EPA 8270C MethodSample Date
Result OF ExtractedAnalyle
bis(2-Ethylhexyl)phthalate
Fluoranthene
FluoreneHexachlorobenzene
HexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno[1,2,3-cd]pyrene
Isophorone2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline3-Nitroaniline4-Nitroaniline
Nitrobenzene2-Nitrophenol
4-NitrophenolN-Nitroso-di-n-propylaminen-NitrosodiphenylamineOi-n-oclylphthalate
Oi-n-butylphthalate
PentachlorophenolPhenanthrenePhenol
Pyrene1,2,4-Trichlorbenzene2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
6050004
24
26
26
26
27
33
27
74
26
2932
3628
2921
2241
29170
86
28
27
24
342945
27
26
5327
330
330
330
330
660
660
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
330
330
1600
330
330
330
330
330
330
NO 1 5/17106
NO 1 5/17106
NO 1 5/17106
ND 1 5/17106
NO 1 5117106
NO 1 5/17106
NO 1 5/17106
ND 1 5/17106
ND 1 5/17106
ND 1 5/17106
ND 1 5/17106
NO 1 5/17106
NO 1 5/17106
NO 1 5/17106
NO 1 5/17106
ND 1 5/17106
ND 1 5/17106
ND 1 5/17106
ND 1 5117106
NO 1 5/17106
NO 1 5/17106
NO 1 5/17106
NO 1 5/17106
NO 1 5/17106
NO 1 5117106
NO 1 5/17106
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NO 1 5/17106
NO 1 5/17106
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5/18106
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5/18106
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AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater. Industrial and HazardousWaste. Chemical Consultation
Proiect Info Samolelnfo ReoortlnfoProject 10: 2006.0088 Sample 10: Method Blank AccuLabs 10: 06050004-MB
Sample Site: Palos Verdes LF Date Sampled: NA Date Reported: 5/19/2006Client Name: Geologic Associates Date Received: 5/1212006 Reporting Units: ug/Kg
Client 10: NA Samole Matrix: Soil Extraction Method: EPA 3550B
Semivolatile Organic Compounds by EPA 8270C Method
Surrogates % Recovery QC Limits in %1,2-Dichlorobenzene-d4 74.2 46-105
2,4,6-Tribromophenol 88.5 46-146
2-Chlorophenol-d4 76.5 48-117
2-Fluorobiphenyl 80.6 54-112
2-FluorophenOI 74.7 45-119
4-Terphenyl-d14 105 46-135
Nitrobenzene--d5 80.6 40-116
Phenol-d5 78.5 37-127
Key: MOL=MethodDetection Limit RL= Reporting Limit J= TraceConc.between MOLand Rl M.B= MethodBlank T.B= TripBlank F.B=Fleld Blank E.B=Equipment Blank
AccuLabs, Inc.
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VN2~11 gas x x VN-DuplVN2-29 Single vault. gas x xVN2-4l gas x xVN3-13 .. gas x x
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Collect duplicates at VN2-11 and VN6-15; label as shown in right-hand column.(1) Contact Ellis Hsue at AccuJabs (626-934-1288) to schedule sample pick-up.Please deliver sample containers to BAS Ontario Field Office prior to May 30, 2006.
M:\SB\mreasonlPalos Verdes\Bottle Order for May 06.x1s PRINTDATE: 5/25/2006
AccuLabs, Inc.Air Toxic » Contaminated Soil » Water and Wastewater· Industrial and Hazardous Waste. Chemical Consultation
Date: June 19, 2006
Mr. Mike ReasonGeoLogic Associates1831 Commercenter EastSan Bernardino, CA 92408
RE: Work Order Number: AL-0606050013 / Palos Verde LandfillInvoice Number: GLA-Y6-004
Dear Mr. Reason:
Enclosed are the analytical reports and the invoice for the samples received by AccuLabson May 31, 2006. The samples are tested for the parameters in accordance with theEPA methods as shown on the chain of custody form.
Thank you for the opportunity to provide analytical tests for your company.
Please feel free to call me at (626) 934-1288 if! can be of further assistance to yourcompany.
Sincerely,
~~BstpLaboratory Director
15437 E. Proctor Avenue· City ofIndustry, California 91745 • Mailing Address: P.O. Box 92314. City ofIndustry, California 91745-2314Tel: (626)934-1288· Fax: (626) 934-1299
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(~) AccuLabs, Inc.Air Toxic. ContaminatedSoH. Water and Wastewater. Industrialand Hazardous Waste. Chemical Consultation
Project Info SarnD/e/nfo ReDon/nfo
Project 10: 2006.0088 Date Sampled: 5/31/2006 Date Reported: 6/13/2006
Sample Site: Palos Verde Landfill Date Received: 5/31/2006 Reporting Units: ppmVClient Name: GeoLogic Associates Samole Matrix: Gas
Total Organic Compounds by EPA 25 MethodTOC TOC
EPA Result-Non Result with Date
Client ID Acculabs 10 Method Batch MDL RL Methane DF Methane Analyzed Qualifiers
VN1-10N 06050013-01 25 6050013 1 5 6.34 6.34 6/6&7/06
VN1-20 06050013-02 25 6050013 1 5 4.39 1160 6/6&7/06 •VN1-34 06050013-03 25 6050013 1 5 1.23 356 6/6&7/06 *
VN2-11 06050013-04 25 6050013 1 5 5.82 2020 6/6&7/06
VN2-29 06050013-05 25 6050013 1 5 7.77 7.77 6/6&7/06
VN2-41 06050013-06 25 6050013 1 5 2.67 2.67 6/6&7/06
VN3-13 06050013-07 25 6050013 1 5 9.05 9.05 6/6&7/06
VN3-23.5 06050013-08 25 6050013 1 5 9.94 90 6/6&7/06
VN3-31 06050013-09 25 6050013 1 5 2.23 2050 6/6&7/06 •VN4-7 06050013-10 25 6050013 1 5 1.95 1.95 6/6&7/06
VN4-23 06050013-11 25 6050013 5 9.45 599 6/6&7/06 *
VN4-31 06050013-12 25 6050013 5 6.03 3080 6/6&7/06
VN5-16 06050013-13 25 6050013 5 9.12 8460 6/6&7/06
VN5-31 06050013-14 25 6050013 5 12.7 12.7 6/6&7/06
VN5-47.5 06050013-15 25 6050013 1 5 1.91 6740 6/6&7/06 •VN6-15 06050013-16 25 6050013 1 5 4.27 4.27 6/6&7/06
VN6-29 06050013-17 25 6050013 1 5 13.8 48.9 6/6&7/06 *
VN6-41 06050013-18 25 6050013 1 5 5.79 1520 6/6&7/06 *
aCTS 06050013-19 25 6050013 5 ND ND 6/6&7/06
VN-DUP1 06050013-20 25 6050013 5 6.09 56.1 6/6&7/06 *
VN-DUP2 06050013-21 25 6050013 5 5.38 5.38 6/6&7/06
NA METHOD BLANK#1 25 6050013 5 ND ND 6/6/06
NA METHOD BLANK#2 25 6050013 5 ND ND 6m06
Key: MOL= Method oeiecncn Urnil RL = ReportingUmlt J = Trace Cone.betweenMOL and RL M.B. = Method Blank T.B. = Trip Blank F.B.;; FIeld Blank E.8. = EquIpmentBlank
* Note: Methane was detected in addition to other non-methane organic compounds
AccuLabs, Inc.
~dJ~~Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soli. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Proiect Info Report InfoProject 10: 2006.0088 Sample 10: VN1-10N AccuLabs 10: 06-05-0013-01
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106
Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbVSamole Matrix: GAS
Volatile Organic Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 0.98 1 6/1/06 611106
Bromornethane 6050013 0.21 0.5 NO 1 611106 611106
1.a-sutaciene 6050013 0.26 0.5 2.1 1 611106 611106
Carbon tetrachloride 6050013 0.19 0.5 NO 1 611106 6/1/06
Chlorobenzene 6050013 0.21 0.5 NO 1 611106 611106
Chloroethane 6050013 0.3 0.5 NO 1 611/06 611106
Chloroform 6050013 0.23 0.5 2.7 1 611106 611106
Chloromethane 6050013 0.18 0.5 NO 1 6/1/06 611106
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 611106 611106
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/1/06 611106
t.a-tnchlorobenzene 6050013 0.18 0.5 NO 1 611106 611106
1,4-Dichlorobenzene 6050013 0.2 0.5 NO 1 611106 611106
Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 39 1 611106 611106
1,1-Dichloroethane 6050013 0.21 0.5 NO 1 611106 611106
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 611106 611/06
1,1-Dichloroethene 6050013 0.23 0.5 NO 1 611106 6/1/06
cls-t.z-Dlchloroethene 6050013 0.19 0.5 NO 1 611106 6/1/06
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 611106 6/1/06
cls-t.SsDichlorcpropene 6050013 0.21 0.5 NO 1 611/06 611/06
trans-1,3-Dichloropropene 6050013 0.14 0.5 NO 1 611106 611106
1,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 4.3 1 6/1/06 611106
4-Ethyltoluene 6050013 0.21 0.5 1.5 1 6/1/06 611106
Ethylbenzene 6050013 0.17 0.5 1.6 1 6/1/06 611106
Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 6/1/06 611106
Methylenechloride 6050013 0.18 2 NO 1 6/1/06 611106
Styrene 6050013 0.16 0.5 1.5 1 611106 611106
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 611106 611106
Tetrachloroethene(peE) 6050013 0.21 0.5 36 1 611106 611106
Toluene 6050013 0.2 0.5 8.6 1 611106 611106
1,2,4-Trichtorobenzene 6050013 0.26 0.5 NO 1 611106 6/1/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 611106 6/1/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 611106 6/1/06
Trichloroethene(TeE) 6050013 0.21 0.5 2.0 1 611106 611106
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 5.1 1 611/06 611106
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 611106 611106
1,2,4-Trimethylbenzene 6050013 0.2 1 3.8 1 611106 611106
1,3,5-Trimethylbenzene 6050013 0.18 1 1.4 1 611106 611106
Vinyl chloride 6050013 0.17 0.5 NO 1 6/1/06 611106
m,p-Xylene 6050013 0.37 1 2.4 1 6/1/06 611106
o-Xylene 6050013 0.19 0.5 2.2 1 6/1/06 611106System Monitoring Compounds(Surrogate) % Recovery QC Limitl%)
4-Bromofluorobenzene 101 80-120Key: MOL;; Method Detection Limit RL;; Reporting Limit J ;; Trace Cone. between MOL and RL M.a.;; Method Blank T.B.;; Trip Blank F.B.;; Field Blenk E.B. ;; Equipment Blank
_~tis.lnc.
Ellis Hsue iLaboratory Director
AccuLabs, Inc.AIr Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste _ Chemical Consultation
Proiect Info ReoortlnfoProject 10: 2006.0088 Sample 10: VN1-20 AccuLabs 10: 06-05-0013-02
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Sample Matrix: GAS
Volatile Organic Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 2.4 1 6/1/06 6/1/06
Bromomethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
1,3-Butadiene 6050013 0.26 0.5 1.5 1 6/1/06 6/1/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/1/06 6/1/06
Chlorobenzene 6050013 0.21 0.5 2.9 1 6/1/06 6/1/06
Chloroethane 6050013 0.3 0.5 NO 1 6/1/06 6/1/06
Chloroform 6050013 0.23 0.5 NO 1 6/1/06 6/1106
Chloromethane 6050013 0.18 0.5 NO 1 6/1/06 6/1/06
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 6/1/06 6/1106
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/1/06 6/1106
1,3-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/1/06 6/1/06
1A-Dichlorobenzene 6050013 0.2 0.5 NO 1 6/1/06 6/1/06
Dichlorodifluoromethane(Freon-12) 6050013 0.18 8 335 4 6/1/06 6/1/06
1,1-Dichloroethane 6050013 0.21 0.5 3.4 1 6/1/06 6/1/06
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 6/1106 6/1/06
1,1-Dichloroethene 6050013 0.23 0.5 NO 1 6/1/06 6/1/06
cis-1,2-Dichtoroethene 6050013 0.19 0.5 NO 1 611/06 611/06
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/1/06 6/1/06
ers-t ,3-Dichloropropene 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
trans-1,3-Dichloropropene 6050013 0.14 0.5 NO 1 6/1/06 6/1/06
1,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 NO 1 6/1/06 6/1/06
4-Ethyltoluene 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
Ethylbenzene 6050013 0.17 0.5 1.8 1 6/1/06 6/1/06
Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 6/1/06 6/1/06
Methylene chloride 6050013 0.18 2 NO 1 6/1/06 6/1/06
Styrene 6050013 0.16 0.5 1.8 1 6/1/06 6/1/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 6/1/06 6/1/06
Tetrachloroethene (PCE) 6050013 0.21 0.5 31 1 6/1/06 6/1/06
Toluene 6050013 0.2 0.5 7.6 1 6/1/06 6/1/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 6/1/06 6/1/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
Trichloroethene (TCE) 6050013 0.21 0.5 4.1 1 6/1/06 6/1/06
Trichlorofluoromethane(Freon-11) 6050013 0.2 4 116 4 6/1/06 6/1/06
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/1106 6/1/06
1,2,4-Trimethylbenzene 6050013 0.2 1 3.4 1 6/1/06 6/1/06
1,3,5-Trimethylbenzene 6050013 0.18 1 1.1 1 6/1106 6/1/06
Vinyl chloride 6050013 0.17 0.5 2.1 1 6/1/06 6/1/06
m,p-Xylene 6050013 0.37 1 2.2 1 6/1/06 6/1/06
a-Xylene 6050013 0.19 0.5 2.4 1 6/1/06 6/1/06
System Monitoring Compounds (Surrogate) % Recovery QCUmitl%)
4-Bromofluorobenzene 102 80-120Key: MOL'" Method Detection Umit RL'" Reporting Umit J =Trace Cone. between MOL and RL M.B. =Method Blank T.B. '" Trip Blank F.B. - Field81ank E.8. '" Equipment Blank
:~~s, Inc.Ellis sue "fLaboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soli. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Proiect Info RelJort InfoProject 10: 2006.0088 Sample 10: VN1-34 AccuLabs 10: 06-05-0013-03
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 6m06Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Sample Matrix: GAS
Volatile Organic Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MDL RL Result DF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 6.4 1 6/1/06 6/1/06
Bromomethane 6050013 0.21 0.5 ND 1 6/1/06 6/1/06
1,3-Butadiene 6050013 0.26 0.5 17 1 6/1/06 6/1/06
Carbon tetrachloride 6050013 0.19 0.5 ND 1 6/1/06 6/1/06
Chiarobenzene 6050013 0.21 0.5 29 1 6/1/06 6/1/06
Chloroethane 6050013 0.3 0.5 1.8 1 6/1/06 6/1/06
Chloroform 6050013 0.23 0.5 NO 1 6/1/06 6/1/06
Chloromethane 6050013 0.18 0.5 ND 1 6/1/06 6/1/06
1,2-Dibromoethane 6050013 0.18 0.5 ND 1 6/1/06 6/1/06
1,2-Dichlorobenzene 6050013 0.18 0.5 ND 1 6/1/06 6/1/06
1,3-Dichlorobenzene 6050013 0.18 0.5 ND 1 6/1/06 6/1/061,4-Dichlorobenzene 6050013 0.2 0.5 ND 1 6/1/06 6/1/06
Dichlorodifluoromethane(Freon-12) 6050013 0.18 8 296 4 6/1/06 6/1/06
1,1-Dichloroethane 6050013 0.21 2 244 4 6/1/06 6/1/06
1,2-0ichloroethane 6050013 0.19 0.5 12 1 6/1/06 611106
1,1-Dichloroethene 6050013 0.23 0.5 2.5 1 6/1/06 6/1/06cis-1,2-Dichloroethene 6050013 0.19 0.5 ND 1 6/1/06 6/1/06
1,2-Dichloropropane 6050013 0.17 0.5 3.3 1 6/1/06 6/1/06
ciS-1,3-Dichloropropene 6050013 0.21 0.5 ND 1 6/1/06 6/1/06
trans-1,3-Dichloropropene 6050013 0.14 0.5 ND 1 6/1/06 6/1/06
1,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 ND 1 6/1/06 6/1/06
4-Ethyltoluene 6050013 0.21 0.5 ND 1 6/1/06 6/1/06
Ethylbenzene 6050013 0.17 0.5 1.8 1 6/1/06 6/1106
Hexachloro-1,3-butadiene 6050013 0.26 0.5 ND 1 6/1/06 6/1/06
Methylenechloride 6050013 0.18 2 ND 1 6/1/06 6/1/06
Styrene 6050013 0.16 0.5 1.3 1 6/1/06 6/1/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 ND 1 6/1/06 6/1/06
Tetrachloroethene (PCE) 6050013 0.21 0.5 11 1 6/1106 6/1/06
Toluene 6050013 0.2 0.5 34 1 6/1/06 6/1/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 ND 1 6/1/06 6/1/06
1,1,1-Trichloroethane 6050013 0.21 0.5 ND 1 6/1/06 6/1/06
1,1,2-Trichloroethane 6050013 0.21 0.5 ND 1 6/1/06 6/1/06
Trichloroethene (TCE) 6050013 0.21 0.5 22 1 6/1/06 6/1/06
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 1.8 1 6/1/06 6/1/06
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 ND 1 6/1/06 6/1/06
1,2,4-Trimethylbenzene 6050013 0.2 1 2.9 1 6/1/06 6/1/06
1,3,5-Trimethylbenzene 6050013 0.18 1 1.1 1 6/1/06 6/1/06
Vinyl chloride 6050013 0.17 2 121 4 6/1/06 6/1/06
m.p-Xylene 6050013 0.37 1 2.2 1 6/1/06 6/1/06
o-Xylene 6050013 0.19 0.5 2.5 1 6/1/06 6/1/06System Monitoring Compounds (Surrogate) % Recovery QC Limit (%l
4-Bromofluorobenzene 107 80-120Key: MDL'" Method Detection Umit RL = Reporting Umil J =Trace Cone. between MOL and RL M.B. = Method Blank T.B. =Trip Blank F.B. = Field Blank E.B. = Equipment Blank
--ifL8bS' Inc.
EIliSRS~1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated SoH. Water and Wastewater. Industrial and Hazardous waste • cnemlcetConsultation
Project Info Report InfoProject 10: 2006.0088 Sample ID: VN2-11 AccuLabs ID: 06-05-0013-04
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Organic Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
8romomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
ChloroformChloromethane
1,2-Dibromoethane
t.z-ructuorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane(Freon-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1 ,3-Dichloropropene
t.z-nrctuorotetramoroemenets-t ta)4·Ethyltolyene
Ethylbenzene
Hexachloro-1 .a-butadtene
Methylene chloride
Styrene
1,1,2,2~Tetrachloroethane
Tetrachloroethane (peE)
Toluene
1,2,4-Trichlorobenzene
1,1, t-Trtchloroethane
1,1,2-Trichloroethane
Trichlorcethene (TCE)
Trichlorofluoromethane(Freon-11 )
1,1,2~'rrtcntorotrtauoroethanets-113)
1,2,4-Trimethylbenzene
t.s.s-rrirrethyibenzeneVinyl chloride
m.p-Xylene
o-Xylene
System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
60500136050013
605001360500136050013
6050013
60500136050013
60500136050013
6050013
60500136050013
60500136050013
60500136050013
6050013605001360500136050013
60500136050013
605001360500136050013
60500136050013
60500136050013
605001360500136050013
6050013
60500136050013
60500136050013
60500136050013
% Recovery
102
0.170.210.260.19
0.210.3
0.23
0.180.18
0.18
0.18
0.20.180.21
0.190.23
0.190.170.21
0.14
0.180.21
0.170.26
0.180.160.18
0.210.2
0.260.21
0.210.21
0.20.2
0.20.18
0.170.37
0.19
0.50.5
0.50.5
0.50.5
0.5
0.50.50.5
0.5
0.5
2
0.50.5
0.50.5
0.50.50.51
0.5
0.50.52
1.6
0.50.5
0.50.5
0.50.50.5
1
1
1
10.51
0.5
6.6 1 611106
NO 1 611106
44 1 611106NO 1 6/1106
NO 1 6/1/06
NO 1 611106
NO 1 6/1/062.6 1 6/1/06
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611/06
1.4 1 611106
NO 1 611106NO 1 611/06
NO 1 611106
NO 1 611106
NO 1 6/1/06
NO 1 611106
NO 1 6/1/06
NO 1 611106
NO 1 611106
2.1 1 611106
NO 1 611106
NO 1 611/06
NO 1 611106
NO 1 611/06
NO 1 61110648 1 611106
NO 1 611106NO 1 611106
NO 1 611106NO 1 611106
1.1 1 6/1/06
NO 1 6/1/06
2.4 1 6/1/06
1.3 1 6/1/06
NO 1 6/1/06
2.5 1 6/1/06
2.2 1 6/1/06ac Limitl%)
80-120
611106
611106
611106
611106
611106
6/1/06
611106
611106
611106
611106611106
6/1/06
6/1/06611106
611106
611106
6/1/06
611106
611106
611106611/06
611106
6/1/06
611106
6/1/06611106
6/1/066/1/066/1/06
611106
611106
611106
611106
611106
6/1/06
611106
611106
611/06
611/06
611106
Key: MOL=Method Detection Umit RL= ReportingLimit J =Trace Cone.betweenMOL and RL M.B. = Method Blank T.B. =Trip Blank F.B. = Field Blank E.B. = Equipment Blank
AccuLabs, Inc.
-:-~tJ~Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste _ Chemical Consultation
Project Info RelJort InfoProject 10: 2006.0088 Sample 10: VN2-29 AccuLabslO: 06-05-0013-05
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Dare Reported: 6~/06Client Name: Geologic Associates Dare Received: 5/31/06 Reporting Units: ppbV
Sample Matrix: GAS
Volatile Organic Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 3.0 1 6/1/06 6/1/06
Bromomethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
1,3-Butadiene 6050013 0.26 0.5 6.6 1 6/1/06 6/1/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/1/06 6/1/06
Chlorobenzene 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
Chloroethane 6050013 0.3 0.5 NO 1 6/1/06 6/1/06
Chloroform 6050013 0.23 0.5 NO 1 6/1106 6/1/06
Chloromethane 6050013 0.18 0.5 NO 1 611106 6/1/06
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 611106 611106
1,2-Dichlorobenzene 6050013 0.16 0.5 NO 1 611106 611106
1,3-Dichlorobenzene 6050013 0.18 0.5 NO 1 611106 6/1/06
1,4-Dichlorobenzene 6050013 0.2 0.5 2.7 1 611106 6/1/06
Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 NO 1 611106 6/1/06
1,1-Dichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
t.z-mcnioroethane 6050013 0.19 0.5 NO 1 6/1/06 611106
'l.f-Dlchloroethene 6050013 0.23 0.5 NO 1 6/1/06 611106
cis-1,2-Dichloroethene 6050013 0.19 0.5 NO 1 6/1/06 611106
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/1/06 611106
cis-1,3-Dichloropropene 6050013 0.21 0.5 NO 1 611106 611106
trans-1,3-Dichloropropene 6050013 0.14 0.5 NO 1 611106 611106
1,2-Dichlorotetrafluoroethane{F-114) 6050013 0.18 1 NO 1 611106 611106
4-Ethylyoluene 6050013 0.21 0.5 NO 1 611106 6/1106
Ethylbenzene 6050013 0.17 0.5 2.3 1 611106 611106
Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 611106 611106
Methylenechloride 6050013 0.18 2 NO 1 611106 6/1/06
Styrene 6050013 0.16 0.5 1.5 1 611106 6/1/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 611106 6/1/06
Tetrachloroethene (peE) 6050013 0.21 0.5 NO 1 611106 6/1/05
Toluene 6050013 0.2 0.5 51 1 611106 611106
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 611/06 611106
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 611106 611106
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 611106
Trichloroethene (TeE) 6050013 0.21 0.5 NO 1 611106 611106
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 NO 1 6/1/06 611106
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 611106 611106
1,2,4-Trimethylbenzene 6050013 0.2 1 3.2 1 6/1/06 611106
1,3,5·Trimethylbenzene 6050013 0.18 1 1.4 1 611106 611106
Vinyl chloride 6050013 0.17 0.5 NO 1 6/1/06 611106
m,p-Xylene 6050013 0.37 1 3.0 1 611106 611106
o-Xylene 6050013 0.19 0.5 2.2 1 6/1/06 611106
System Monitoring Compounds (Surrogate) % Recovery QC Limit(%)
4-Bromofluorobenzene 101 80-120Key: MOL =Method Detection Umil RL =Reporting Limn J =Trace Cone. between MOL and RL M.B. =Method Blank T.B. =Trip Blank F.B. =Field Blank E.B. =Equipment Blank
~LabS' Inc.
- -H~l~Ellis Hsue .Laboratory Director
AccuLabs, Inc.AirToxic. Contaminated Soil. WaterandWastewater _ Industrial andHazardous Waste_ Chemical Consultation
Proiect Info ReoortlnfoProject 10: 2006.0088 Sample 10: VN2-41 AccuLabs 10: 06-05-0013-06
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 6~/06
Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
QualifiersDate
AnalyzedRLMDLBatch
Volatile Orgamc Compounds by EPA TO-14 MethodSample DateResult OF PreparedAnalyte
Benzene
Bromomethanet.a-autadene
Carbon tetrachlorideChlorobenzeneChloroethane
Chloroform
Chloromethaner.z-moromoethane
1,2-Dichlorobenzene1,3-Dichlorobenzene
1,4-DichlorobenzeneDichlorodifluoromethane(Freon-12)
1,1-Dichloroethane1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene1,2-Dichloropropane
cis-1,3-Dichloropropene
irans-t.a-tnchlcropropene
1,2-Dichlorotetrafluoroethane(F-114)4-EthyltolueneEthylbenzene
Hexachloro-1 ,3-butadieneMethylene chloride
Styrene1,1,2,2-TetrachloroethaneTetrachloroethene (peE)
Toluene1,2,4-Trichlorobenzene
1,1,1-Trichloroethane1,1,2-Trichloroethane
Trichloroethene (TCE)Trichlorofluoromethane(Freon-11 )
1,1,2-Trichlorotrifluoroethane(F-113)1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloridem,p-Xylene
o-Xylene
6050013
605001360500136050013
60500136050013
6050013
60500136050013
60500136050013
605001360500136050013
605001360500136050013
6050013
60500136050013
6050013605001360500136050013
605001360500136050013
60500136050013
60500136050013
60500136050013
60500136050013
6050013
60500136050013
60500136050013
0.170.21
0.260.190.21
0.3
0.23
0.180.180.18
0.180.2
0.180.210.190.23
0.19
0.170.21
0.140.180.21
0.170.260.18
0.160.180.21
0.20.26
0.210.21
0.210.2
0.20.2
0.18
0.170.370.19
0.5
0.52
0.5
0.50.5
0.5
0.50.5
0.50.5
0.52
0.50.50.5
0.50.5
0.50.51
0.50.50.5
20.50.5
0.52
0.50.5
0.50.5
11
1
10.51
0.5
9.2 1 6/1/06
ND 1 6/1/0656 4 6/1/06ND 1 6/1/06
1.6 1 6/1/06ND 1 6/1/06
ND 1 6/1/06
2.0 1 6/1/06ND 1 6/1/06ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06ND 1 6/1/06ND 1 6/1/06
ND 1 6/1/064.5 1 6/1/06ND 1 6/1/06
ND 1 6/1/06ND 1 6/1/06
ND 1 6/1/06ND 1 6/1/06
2.1 1 6/1/064.0 1 6/1/06ND 1 6/1/06ND 1 6/1/06
2.1 1 6/1/06ND 1 6/1/06ND 1 6/1/06
85 4 6/1/06ND 1 6/1/06
ND 1 6/1/06ND 1 6/1/06
ND 1 6/1/06ND 1 6/1/06
ND 1 6/1/064.9 1 6/1/06
2.2 1 6/1/06
ND 1 6/1/065.5 1 6/1/063.9 1 6/1/06
6/1/06
6/1/066/1/066/1/06
6/1/066/1/06
6/1/06
6/1/066/1/06
6/1/066/1/06
6/1/066/1/066/1/06
6/1/066/1/066/1/06
6/1/066/1/06
6/1/066/1/066/1/06
6/1/066/1/066/1/06
6/1/066/1/066/1/06
6/1/066/1/06
6/1/066/1/06
6/1/066/1/06
6/1/066/1/06
6/1/06
6/1/066/1/066/1/06
System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
% Recovery
105
QC Limit(%)
80-120Key: MOL= Method Detection Limit RL = Reporting Limit J = TraceCone.between MOLandRL M.B.=Method Blank T.B.=TripBlank F.B.=Field Blank E.B.=Equipment Blank
A~CflLabs, Inc.
'1a H41A/Ellis Hsue \Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and HazardousWaste. Chemical Consultation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VN3-13 AccuLabs 10: 06-05-0013-07
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
SamDle Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Organic Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane(Freon-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
ers-t ,3-Dichloropropene
trans-t ,3-Dichloropropene
1,2-Dichrorotetrafluoroethane(F~114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-1,3-butadiene
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene (TCE)
Trichlorofluoromethanetfreon-11)
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
a-Xylene
60500136050013
60500136050013
60500136050013
6050013
60500136050013
60500136050013
605001360500136050013
60500136050013
6050013605001360500136050013
6050013
6050013605001360500136050013
60500136050013
60500136050013
605001360500136050013
6050013
60500136050013
60500136050013
60500136050013
6050013
0.17
0.21
0.260.190.21
0.3
0.230.18
0.180.18
0.180.2
0.180.21
0.190.230.19
0.170.210.140.18
0.21
0.170.260.180.16
0.180.21
0.20.260.21
0.21
0.210.2
0.20.2
0.180.17
0.370.19
0.50.5
0.5
0.50.50.5
0.5
0.5
0.50.5
0.50.52
0.50.5
0.50.50.50.5
0.51
0.50.5
0.52
0.50.5
0.50.5
0.50.5
0.50.5
1
1
1
1
0.51
0.5
15 1 6/1/06
NO 1 6/1/067.3 1 6/1/06
NO 1 611/0619 1 6/1/06NO 1 6/1/06
NO 1 611106
NO 1 6/1/06NO 1 611/06
NO 1 6/1/06
NO 1 611/0613 1 6/1/064.8 1 611/06
13 1 6/1/06NO 1 6/1/06NO 1 6/1/06
7.8 1 6/1/06NO 1 6/1/06NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06
1.5 1 611/064.7 1 6/1/06NO 1 611/06NO 1 6/1/06
1.5 1 6/1/06NO 1 6/1106
3.4 1 611/0649 1 6/1/06NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06
2.1 1 6/1/06NO 1 611/06
NO 1 6/1/066.1 1 6/1/06
4.3 1 6/1/06NO 1 6/1/06
3.5 1 611/06
5.9 1 611/06
6/1/06
611/06
6/1/066/1/066/1/06
6/1/06611/06
6/1/06
6/1/066/1/06
6/1/066/1/066/1/06
611/066/1/066/1/06
6/1/066/1/066/1/066/1/06
611106
6/1/066/1/066/1106
6/1/066/1/066/1/06
6/1/066/1/06611106
6/1/066/1/06
6/1/06611106
611106
6/1/06
6/1/066/1/06
6/1/06
6/1/06System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
% Recovery
102
QCUmit(%)
80-120Key: MOL", Method Detection Limit RL'" ReportingLimit J '" Trace Cone.be!ween MDLand RL M.B. '" Method Blank T.B. '" Tlip Blank F.B. '" Field Blank E.B. '" EquipmentBlank
~LabS, Inc.
EllisHs~jLaboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and HazardousWaste. Chemical Consultation
Project Info RenortlnfoProject 10: 2006.0088 Sample 10: VN3-23.5 AccuLabs 10: 06-05-0013-08
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
SamDle Matrix: GAS
Volatile Orgamc Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 7.1 1 6/1/06 6/1/06
Bromomethane 6050013 0.21 0.5 NO 1 6/1/06 611/061,3-Butadiene 6050013 0.26 0.5 38 1 6/1/06 6/1/06Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/1/06 6/1/06Chlorobenzene 6050013 0.21 0.5 2.3 1 6/1/06 6/1/06Chloroethane 6050013 0.3 0.5 NO 1 6/1/06 6/1/06
Chloroform 6050013 0.23 0.5 NO 1 6/1/06 6/1/06
Chloromethane 6050013 0.18 0.5 1.8 1 6/1/06 6/1/06
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 6/1/06 6/1106
t.z-mctnorobenzene 6050013 0.18 0.5 NO 1 6/1/06 6/1/061,3-Dlchlorobenzene 6050013 0.18 0.5 NO 1 6/1/06 6/1/061,4-Dichlorobenzene 6050013 0.2 0.5 3.5 1 6/1/06 6/1/06Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 2.6 1 6/1/06 6/1/06
1,1-Dichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 6/1/06 6/1/06
1,1-Dichloroethene 6050013 0.23 0.5 1.5 1 6/1/06 6/1/06
cis-1,2-Dichloroethene 6050013 0.19 0.5 3.4 1 6/1/06 6/1/06
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/1/06 6/1/06crs-t.a-tnctnoropropene 6050013 0.21 0.5 NO 1 6/1/06 6/1/06nans-t.a-tnchtoroprooene 6050013 0.14 0.5 NO 1 6/1/06 6/1/06
1.z-Dlchlorotetranuoroethanets-114) 6050013 0.18 1 NO 1 6/1/06 6/1/064-Ethyltoluene 6050013 0.21 0.5 1.8 1 6/1/06 6/1/06
Ethylbenzene 6050013 0.17 0.5 3.7 1 6/1/06 6/1/06
Hexacbtoro-f.Scbutadiene 6050013 0.26 0.5 NO 1 6/1/06 6/1/06
Methylenechloride 6050013 0.18 2 NO 1 6/1/06 6/1/06
Styrene 6050013 0.16 0.5 1.7 1 6/1/06 6/1/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 6/1/06 611/06Tetrachloroethene (PCE) 6050013 0.21 0.5 1.8 1 6/1/06 6/1/06Toluene 6050013 0.2 2 96 4 6/1/06 6/1/06t.z.e-rnctnorobenzene 6050013 0.26 0.5 NO 1 6/1106 6/1/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1106
Trichloroethene (TCE) 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
Trichloroftuoromethanetfreon-f t ) 6050013 0.2 1 NO 1 6/1/06 6/1106
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/1/06 6/1/061,2,4w Trimethylbenzene 6050013 0.2 1 6.9 1 6/1/06 6/1/06
1,3,5-Trimethylbenzene 6050013 0.18 1 3.4 1 6/1106 6/1/06Vinyl chloride 6050013 0.17 0.5 3.5 1 6/1/06 6/1/06
m.p-Xylene 6050013 0.37 1 4.3 1 6/1/06 6/1/06
o-Xylene 6050013 0.19 0.5 5.4 1 6/1/06 6/1/06
System Monitoring Compounds (Surrogate) % Recovery OCUmitl%)
a-Bromoflucrobenzene 99 80-120Key: MOL = Method Detection limit RL = Reporting limit J =Trace Cone. between MOL and RL M.B. = Method Blank T,B. =Trip Blenk F.B. = Field Blenk E.B. = Equipment Blank
~ A;zgLabS, Inc.
E~sHsB.t1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soli. Water and Wastewater _ Industrial and HazardousWaste. Chemical Consultation
Project Info ReDortlnfoProject 10: 2006.0088 Sample 10: VN3-31 AccuLabs 10: 06-05-0013-09
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
Volatile Orgamc Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed QualifiersBenzene 6050013 0.17 0.5 5.1 1 5/1/05 6/1/05Bromomethane 6050013 0.21 0.5 NO 1 5/1/06 6/1/06
1,3-Butadiene 6050013 0.26 2 145 4 6/1/06 6/1/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/1/06 6/1/06Chlorobenzene 6050013 0.21 0.5 1.7 1 6/1/06 6/1/06
Ohlcroethane 6050013 0.3 0.5 NO 1 6/1/06 6/1/06
Chloroform 6050013 0.23 0.5 NO 1 6/1/06 6/1/06
Chloromethane 6050013 0.18 0.5 9.2 1 6/1/06 611106
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 6/1/06 6111061,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 611106 611106
1,3-0ichlorobenzene 6050013 0.18 0.5 NO 1 611106 6111061A-Dichlorobenzene 6050013 0.2 0.5 2.7 1 611106 6/1/06
Oichlorodifluoromethane(Freoo-12) 6050013 0.18 2 1.9 1 611106 6/1/061,1-Dichloroethane 6050013 0.21 0.5 NO 1 611106 6/1/06
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 611106 6111061,1-Dichloroethene 6050013 0.23 0.5 NO 1 611106 611106
cts-t.z-rxchroroethene 6050013 0.19 0.5 3.1 1 6/1/06 611106
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 611106 611106cis-1,3-Dichloropropene 6050013 0.21 0.5 NO 1 6/1/06 611106trans-1,3-Dichloropropene 6050013 0.14 0.5 NO 1 6/1/06 611106
1,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 NO 1 6/1/06 6111064-Ethyltoluene 6050013 0.21 0.5 1.6 1 6/1/06 611106Ethylbenzene 6050013 0.17 0.5 3.0 1 611106 611106Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 611106 611106
Methylene chloride 6050013 0.18 2 NO 1 611106 611106Styrene 6050013 0.16 0.5 1.5 1 611106 6111061,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 611106 611106
Tetrachloroethene (peE) 6050013 0.21 0.5 NO 1 611106 6/1/06
Toluene 6050013 0.2 0.5 54 1 611106 6/1/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 611106 6/1/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 611106 6/1/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 611106
Trichloroethene (TCE) 6050013 0.21 0.5 NO 1 611106 611106
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 NO 1 6/1/06 611106
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/1/06 611106
1,2,4-Trimethylbenzene 6050013 0.2 1 6.3 1 6/1/06 611106
1,3,5-Trimethylbenzene 6050013 0.18 1 3.1 1 6/1/06 611106
Vinyl chloride 6050013 0.17 0.5 1.7 1 6/1/06 611106
m,p-Xylene 6050013 0.37 1 3.7 1 611106 611106
o-Xylene 6050013 0.19 0.5 4.7 1 6/1/06 611106System Monitoring Compounds (Surrogate) % Recovery DC Limit (%)
4-Bromofluorobenzene 102 80-120Key: MOL'" Method Detection Umit RL'" Reporting Umil J '" Trace Cone. between MOL and RL M.B. '" Method Blank T.B. '" Trip Blank F.B. '" Field Blank E.B. '" Equipment Blank
AccuLabs, Inc.
--uf; tt,t1Ellis HsueLaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. water and Wastewater_ Industrial and HazardousWaste. ChemIcalConsultation
Proiect Info ReoortlnfoProject 10: 2006.0088 Sample 10: VN4-7 AccuLabs 10: 06-05-0013-10
Sample Sileo Palos Verde Landfill Date Sampled: 5/31/06 Dale Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Sample Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Orgamc Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane(Freon-tz)
1,1-Dichloroethane
1,2-Dichloroethane
t.f-Dichloroethene
cis-1,2-0ichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1 ,3-Dichloropropene
1,2~Dichlorotetrafluoroethane(F-114)
a-Ethyltoluene
Ethylbenzene
Hexachloro-1 .a-butaotene
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,4-Trichlorobenzene
1,1,t-Trichlcrcethane
1,1,2-Trichloroethane
Tnchloroethene (TCE)
Trichlorofluoromethane(Freon-11 )
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4~Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
6050013
60500136050013
60500136050013
60500136050013
6050013
60500136050013
6050013
60500136050013
605001360500136050013
605001360500136050013
60500136050013
6050013605001360500136050013
605001360500136050013
605001360500136050013
6050013
60500136050013
60500136050013
6050013
60500136050013
6050013
0.17
0.210.260.19
0.210.3
0.23
0.18
0.180.18
0.180.2
0.18
0.210.190.230.19
0.170.21
0.140.180.21
0.170.260.180.16
0.180.21
0.20.260.21
0.21
0.210.2
0.20.2
0.180.17
0.370.19
0.50.5
0.50.50.5
0.5
0.5
0.50.5
0.5
0.50.5
20.5
0.50.50.50.5
0.50.5
1
0.50.50.5
20.50.5
0.50.50.5
0.50.5
0.5
1
1
1
1
0.5
1
0.5
NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06NO 1 611/06NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06
3.4 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06
6/1/06
6/1/06
6/1/06
6/1/066/1/06
6/1/06611/06
611/06
6/1/066/1/06
6/1/066/1/06
6/1/06
6/1/06
6/1/066/1/066/1/06
6/1/066/1/06
6/1/06
6/1/066/1/066/1/06
6/1/066/1/066/1/06
6/1/06
6/1/066/1/06
6/1/06
6/1/06
6/1/066/1/06
6/1/06
6/1/066/1/06
6/1/066/1/06
6/1/06611/06
System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
% Recovery
98
QC Limit (%)
80-120Key: MOL" Method Detection Umit Rl" ReportingUmit J" Trace Cone.betweenMOland Rl M.B." Method Blank T.B." Trip Blank F.B." Field Blank E.B." EquipmentBlank
AccuLabs, Inc.
-u£8sEllisHsue iLaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Waler and Wastewater. Industrial and HazardousWaste. Chemical Consultation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VN4-23 AccuLabs 10: 06-05-0013-11
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
VolatIle Orgamc Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed QualifiersBenzene 6050013 0.17 0.5 13 1 6/1/06 6/1/06
Bromomethane 6050013 0.21 0.5 NO 1 6/1/06 6/11061,3-Butadiene 6050013 0.26 0.5 35 1 6/1/06 6/1106
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/1/06 6/1/06
Chlorobenzene 6050013 0.21 0.5 2.3 1 6/1/06 6/1/06Chloroethane 6050013 0.3 0.5 NO 1 6/1/06 6/1/06
Chloroform 6050013 0.23 0.5 NO 1 6/1106 6/1/06Chloromethane 6050013 0.18 0.5 NO 1 6/1/06 6/1106
t.z-noromcethane 6050013 0.18 0.5 NO 1 6/1/06 6/1/06
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/1/06 6/1/06
1.a-nctuorceeneene 6050013 0.18 0.5 NO 1 6/1/06 6/1/06't.a-Dichlorobenzene 6050013 0.2 0.5 NO 1 6/1/06 6/1/06
Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 NO 1 6/1/06 6/1/061,1-Dichloroethane 6050013 0.21 0.5 NO 1 6/1106 6/1/06
1.z-Dichlorcethane 6050013 0.19 0.5 NO 1 6/1/06 6/1/061,1-Dichloroethene 6050013 0.23 0.5 7.8 1 6/1/06 6/1/06
cis-1,2-Dichloroethene 6050013 0.19 0.5 178 1 6/1/06 6/1/061,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/1/06 6/1/06
cis-1,3-Dichloropropene 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
trans-1,3-Dichloropropene 6050013 0.14 0.5 NO 1 6/1/06 6/1/061,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 NO 1 6/1/06 6/1/06
4-Ethyltoluene 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
Ethylbenzene 6050013 0.17 0.5 1.5 1 6/1/06 6/1/06Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 6/1/06 6/1/06
Methylenechloride 6050013 0.18 2 NO 1 6/1/06 6/1/06
Styrene 6050013 0.16 0.5 NO 1 6/1/06 6/1/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 6/1/06 6/1/06
Tetrachloroethene(PCE) 6050013 0.21 0.5 2.7 1 6/1/06 6/1/06
Toluene 6050013 0.2 0.5 8.4 1 6/1/06 6/1/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 6/1/06 6/1/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
Trichloroethane(TCE) 6050013 0.21 0.5 NO 1 6/1/06 6/1/06
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 NO 1 6/1/06 6/1106
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/1/06 6/1/06
1,2,4-Trimethylbenzene 6050013 0.2 1 1.4 1 6/1/06 6/1/06
1,3,5-Trimethylbenzene 6050013 0.18 1 NO 1 6/1/06 6/1/06
Vinyl chloride 6050013 0.17 0.5 19 1 6/1/06 6/1/06
m,p-Xylene 6050013 0.37 1 1.3 1 6/1/06 6/1106
a-Xylene 6050013 0.19 0.5 1.1 1 6/1/06 6/1/06
System MonitoringCompounds(Surrogate> % Recoverv ac limit (%)
4-Bramofluorabenzene 100 80-120Key: MOL = Method Detection Limit RL = Reporting Umit J = Trace Cone. between MOL and RL M.B. = Method Blank T.B. =Trip Blank F.B. = Field Blank E.B. = Equipment Blank
~ULabS, Inc.
~ +ttiEllis HsueLaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoil. Water and Wastewater _ Industrial and Hazardous Waste. ChemIcal Consultation
Project Info Reoort InfoProject 10: 2006.0088 Sample 10: VN4-31 AccuLabs 10: 06-05-0013-12
Sample Site: Palos Verde Landfill Date Sampled: 5/31106 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31106 Reporting Units: ppbV
Samole Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Organic Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane(Freon-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-t.SDlchloropropene
1,2-0ichlorotetrafluoroethane(F-114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-1,3-butadiene
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene (TCE)
Trichlorofluoromethane(Freon-11 )
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
60500136050013
60500136050013
60500136050013
6050013
60500136050013
60500136050013
60500136050013
60500136050013
60500136050013
60500136050013
60500136050013
6050013605001360500136050013
605001360500136050013
60500136050013
605001360500136050013
60500136050013
60500136050013
60500136050013
6050013
0.17
0.210.260.19
0.21
0.30.23
0.18
0.180.18
0.180.2
0.18
0.21
0.190.23
0.190.170.21
0.140.18
0.210.170.260.18
0.160.18
0.210.2
0.26
0.210.21
0.210.2
0.20.2
0.18
0.17
0.370.19
50.50.5
0.50.5
0.5
0.50.5
0.50.5
0.50.5
2
0.5
0.50.5
0.50.5
0.50.51
0.50.50.5
2
0.50.5
0.50.5
0.50.50.5
0.51
1
1
1
5
1
0.5
92 10 6/3106
NO 1 6/3/06
27 1 6/3/06
NO 1 6/3/06
2.2 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3106
NO 1 6/3/06
42 1 6/3106
NO 1 6/3/06
NO 1 6/3106
NO 1 6/3106
NO 1 6/3/06
4.3 1 6/3/06
NO 1 6/3/06
8.1 1 6/3106
NO 1 6/3106
NO 1 6/3106
NO 1 6/3/06
NO 1 6/3106
1.8 1 6/3/06
33 1 6/3/06
NO 1 6/3106
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
2.8 1 6/3/06
1.3 1 6/3/06
310 10 6/3/06
4.1 1 6/3/06
2.2 1 6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3106
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3106
6/3/06
6/3/06
System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
% Recovery
102
OC Umit(%)
80-120Key: MOL=Method DetectionUmlt RL =ReportingUmil J =Trace Cone.betweenMOLand RL M,a. =Method Blank T.B. =Trip Blank EB. =Field Blank E.B.=Equipment Blank
~c..rfLabS, lnc.
,<~t-ltJEIliSH~UP 1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info ReoortlnfoProject 10: 2006.0088 Sample 10: VN5-16 AccuLabs 10: 06-05-0013-13
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 6m06Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
samole Matrix: GAS
Volatile Orgamc Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 5.1 1 6/3/06 6/3/06
Bromomethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,3-Butadiene 6050013 0.26 0.5 3.3 1 6/3/06 6/3/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 613/06 6/3/06
Chlorobenzene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Ohloroethane 6050013 0.3 0.5 NO 1 6/3/06 6/3/06
Chloroform 6050013 0.23 0.5 5.1 1 6/3/06 6/3/06
Chloromethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
't.z-mbromoethane 6050013 0.18 0.5 NO 1 613/06 6/3/06
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,3-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1A-Dichlorobenzene 6050013 0.2 0.5 NO 1 6/3/06 6/3/06
Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 4.1 1 6/3/06 6/3/06
1,1-Dichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 6/3/06 6/3/06
1,1-Dichloroethene 6050013 0.23 0.5 NO 1 6/3/06 6/3/06
cis-1,2-Dichloroethene 6050013 0.19 0.5 NO 1 6/3/06 6/3/06
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
cis-1,3-Dichloropropene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
trans-1 ,3-Dichloropropene 6050013 0.14 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 NO 1 6/3/06 6/3/06
4-Ethyltoluene 6050013 0.21 0.5 6.2 1 6/3/06 6/3/06
Ethylbenzene 6050013 0.17 0.5 6.6 1 6/3/06 6/3/06
Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 6/3/06 6/3/06
Methylene chloride 6050013 0.18 2 NO 1 6/3/06 613106
Styrene 6050013 0.16 0.5 2.0 1 6/3/06 6/3/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
Tetrachloroethene (peE) 6050013 0.21 0.5 6.3 1 6/3/06 6/3/06
Toluene 6050013 0.2 0.5 51 1 6/3/06 6/3/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 6/3/06 6/3/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Trlchloroethene (TeE) 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 1.6 1 6/3/06 6/3/06
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/3/06 6/3/06
1,2,4-Trimethylbenzene 6050013 0.2 1 5.4 1 6/3/06 6/3/06
1,3,5-Trimethylbenzene 6050013 0.18 1 4.4 1 6/3/06 6/3/06
Vinyl chloride 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
m,p-Xylene 6050013 0.37 1 6.7 1 6/3/06 6/3/06
o-Xylene 6050013 0.19 0.5 11 1 6/3/06 6/3/06
System Monitoring Compounds (Surrogate) % Recovery QC Limit(%)
4-Bromofluorobenzene 104 80-120Key: MOL =Method Detection Umil RL = Reporting umn J =Trace Cone. between MOL and RL M.B. =Method Blank T.B. =Trip Blank F.B. = Field Blank E.B. = Equipment Blank
~ULabS, Inc.
~ -ds~lE lis HsuLaboratory Di etor
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste _ Chemical Consultation
Proiect Info ReDortlnfoProject 10: 2006.0088 Sample 10: VN5-31 AccuLabs 10: 06-05-0013-14
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Sample Matrix: GAS
Volatile Organic Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 4.7 1 6/3106 613/06
Bromomethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
t.a-suteeene 6050013 0.26 0.5 2.3 1 6/3106 6/3/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/3/06 613/06
Chlorobenzene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Chloroethane 6050013 0.3 0.5 NO 1 6/3/06 6/3/06
Chloroform 6050013 0.23 0.5 NO 1 6/3/06 6/3/06
Chloromethane 6050013 0.18 0.5 NO 1 6/3/06 6/3106
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3106
1,3-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3106
1,4-Dichlorobenzene 6050013 0.2 0.5 NO 1 6/3/06 6/3/06
Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 3.0 1 6/3/06 6/3/06
1,1-Dichloroethane 6050013 0.21 0.5 NO 1 6/3106 6/3/06
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 6/3106 6/3/06
1,1-Dichloroethene 6050013 0.23 0.5 NO 1 6/3/06 6/3/06
cis-t.z-Dlchloroethene 6050013 0.19 0.5 NO 1 6/3106 613/06
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/3/06 613/06
cls-t ,3-Dichloropropene 6050013 0.21 0.5 NO 1 6/3/06 613/06
uans-t.a-oicbiorcoropene 6050013 0.14 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorotetrafluoroethane(F·114) 6050013 0.18 1 NO 1 6/3/06 6/3/06
4·Ethyltoluene 6050013 0.21 0.5 6.4 1 6/3/06 6/3106
Ethylbenzene 6050013 0.17 0.5 6.8 1 6/3/06 6/3106
Hexachloro-1 ,3-butadiene 6050013 0.26 0.5 NO 1 6/3/06 6/3106
Methylene chloride 6050013 0.18 2 NO 1 6/3/06 6/3/06
Styrene 6050013 0.16 0.5 2.3 1 6/3/06 6/3106
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
Tetrachloroethene (PCE) 6050013 0.21 0.5 5.9 1 6/3/06 6/3/06
Toluene 6050013 0.2 0.5 41 1 6/3/06 6/3/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 6/3106 6/3/06
t.t.t-trtchtoroetnane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/3106 6/3/06
Trichloroethene (TCE) 6050013 0.21 0.5 NO 1 6/3/06 613/06
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 1.6 1 6/3106 613/06
1,1,2·Trichlorotrifluoroethane(F·113) 6050013 0.2 1 ND 1 6/3/06 6/3/06
1,2,4-Trimethylbenzene 6050013 0.2 1 5.6 1 6/3/06 6/3/06
1,3,5·Trimethylbenzene 6050013 0.18 1 4.6 1 6/3/06 613/06
Vinyl chloride 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
m,p-Xylene 6050013 0.37 1 7.5 1 6/3/06 6/3/06
o-Xylene 6050013 0.19 0.5 12 1 6/3/06 6/3/06
System Monitoring Compounds (Surrogate) % Recovery QC Limit(%)
4-Sromofluorobenzene 102 80-120Key: MOL" Method Detection Limit RL" Reporting Umit J "Trace Cone. between MOL and RL M.B." Method Blank T.B." Trip Blank F.B." FierdBrank E.B. " Equipment Brank
~a~LabS' Inc.
~IiS s~iLaboratory Director
AccuLabs, Inc.Air Toxic. ContaminatedSoli. Water and Wastewater. Industrial and HazardousWaste. Chemical Consultation
Proiect Info ReoortlnfoProject 10: 2006.0088 Sample 10: VN5-47.5 AccuLabs 10: 06-05-0013-15
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 6/7/06Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Sample Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Orgamc Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
t.a-nlcmorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane(Freon-12)
t.f-Dlchlcroethane
t.z-mctnoroethane1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
cls-t.SDlchloropropene
trans-1,3-Dichloropropene
1,2MDichlorotetrafluoroethane(F-114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-f.Scbutadiene
Methylenechloride
Styrene
1,1,2,2MTetrachloroethane
Tetrachloroethene (peE)
Toluene1,2,4MTrichlorobenzene
t.t.t-rrtcntoroetbane1,1,2-Trichloroethane
Trlchloroethene (TCE)
Trichloroftucrcmethanetrreon-t t)
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4MTrimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
0.17
0.21
0.26
0.19
0.21
0.3
0.23
0.18
0.18
0.18
0.18
0.2
0.18
0.21
0.19
0.23
0.19
0.17
0.21
0.14
0.18
0.21
0.17
0.26
0.18
0.16
0.18
0.21
0.2
0.26
0.21
0.21
0.21
0.2
0.2
0.2
0.18
0.17
0.37
0.19
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
2
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1
0.5
0.5
0.5
20.5
0.5
2
0.5
0.5
0.5
0.5
0.5
1
1
1
1
0.5
1
0.5
2.0 1 6/3/06
NO 1 6/3/06
8.0 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3106
NO 1 6/3/06
NO 1 6/3106
71 1 613/06
NO 1 613106
NO 1 613/06
6.3 1 613/06
4.1 1 613/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
2.7 1 6/3/06
1.5 1 6/3/06
2.4 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
1.7 1 6/3/06
NO 1 6/3/06
193 4 6/3/06
41 1 6/3/06
NO 1 6/3106
NO 1 6/3/06
NO 1 6/3/06
37 1 6/3/06
2.6 1 6/3106
NO 1 6/3/06
3.9 1 6/3106
1.9 1 6/3/06
2.8 1 6/3106
3.1 1 6/3/06
3.0 1 6/3106
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3106
613/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
613/06
6/3106
613106
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
System Monitoring Compounds (Surrogate)
a-Bromoffuorobenzene
% Recovery
104
QC Umitl%)
80-120Key: Mal = Method DetectionUmit Rl= ReportingUmit J = Trace Cone. betweenMaland RL M.B. = Method Blank T.B. = Trip Blank F.B. = Field Blank E.B. = EquipmentBlank
i(~:;nc.
Laboratory Dirbctor
AccuLabs, Inc.Air Toxic. Contaminated Soil. water and Wastewater _ Industrial and Hazardous Waste _ Chemical Consultation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VN6-15 AccuLabs 10: 06-05-0013-16
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
Volatile Orgamc Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 1.1 1 6/3/06 6/3/06
Bromomethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,3wButadiene 6050013 0.26 0.5 NO 1 6/3/06 6/3/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/3/06 6/3/06
Chlorobenzene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Chloroethane 6050013 0.3 0.5 NO 1 613/06 6/3/06
Chloroform 6050013 0.23 0.5 NO 1 6/3/06 6/3/06
Chloromethane 6050013 0.18 0.5 NO 1 613/06 613/06
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,3-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,4-Dichlorobenzene 6050013 0.2 0.5 NO 1 6/3/06 6/3/06
Dichtorodifluoromethane(Freon-12) 6050013 0.18 2 NO 1 6/3/06 613106
1,1-Dichloroethane 6050013 0.21 0.5 NO 1 6/3/06 613106
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 6/3/06 6/3/061,1-Dichloroethene 6050013 0.23 0.5 NO 1 6/3/06 6/3/06
cis-1,2-Dichloroethene 6050013 0.19 0.5 NO 1 6/3/06 6/3/061,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
cis-1,3-Dichloropropene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
trans-1,3-Dichloropropene 6050013 0.14 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 NO 1 6/3/06 6/3/06
4-Ethyltoluene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Ethylbenzene 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 6/3/06 613/06
Methylene chloride 6050013 0.18 2 NO 1 6/3/06 6/3/06
Styrene 6050013 0.16 0.5 2.0 1 6/3/06 613/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
Tetrachloroethene (peE) 6050013 0.21 0.5 3.3 1 6/3/06 6/3/06
Toluene 6050013 0.2 0.5 NO 1 6/3/06 6/3/061,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 6/3/06 6/3/061,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Trichloroethene (TeE) 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Trichtorofluoromethanejfreon-t t ) 6050013 0.2 1 NO 1 6/3/06 6/3/06
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/3/06 6/3/06
1,2,4-Trimethylbenzene 6050013 0.2 1 1.5 1 6/3/06 6/3/06
1,3,5~Trimethylbenzene 6050013 0.18 1 NO 1 6/3/06 6/3/06
Vinyl chloride 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
m,p-Xylene 6050013 0.37 1 1.0 1 6/3/06 6/3/06
o-Xylene 6050013 0.19 0.5 1.1 1 6/3/06 6/3/06
System Monitoring Compounds (Surrogate) % Recovery QC Limit (%)
4-Bromofluorobenzene 101 80-120Key: MOL = Method Detection Limit RL = Reporting Limit J =Trace Cone. between MOL and Rl M.B. =Method Blank T.B. =Trip Blank F.B. =Field Blank E.B. = Equipmant Blank
AccuLabs, Inc.
~lLaboratory Dir elor
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info ReDort InfoProject 10: 2006.0088 Sample 10: VN6-29 AccuLabs 10: 06-05-0013-17
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 6/7/06Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
Volatile Organic Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 4.0 1 6/3/06 6/3/06
Bromomethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1.s-autacsene 6050013 0.26 0.5 8.9 1 6/3/06 6/3/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/3/06 6/3/06
Chlorobenzene 6050013 0.21 0.5 1.2 1 6/3/06 6/3/06
Chloroethane 6050013 0.3 0.5 NO 1 6/3/06 6/3/06
Chloroform 6050013 0.23 0.5 4.1 1 6/3/06 6/3/06
Chloromethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,2-Dibromoethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,3-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1A-Dichlorobenzene 6050013 0.2 0.5 NO 1 6/3/06 613/06
Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 17 1 6/3/06 613/06
1,1-Dichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 6/3/06 6/3/06
1,1-Dichloroethene 6050013 0.23 0.5 1.0 1 6/3/06 6/3/06
cis-1,2-Dichloroethene 6050013 0.19 0.5 1.2 1 6/3/06 6/3/06
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
cts-t ,3-Dichloropropene 6050013 0.21 0.5 NO 1 613/06 6/3/06
trans-1,3-Dichloropropene 6050013 0.14 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 NO 1 6/3/06 6/3/06
4-Ethyltoluene 6050013 0.21 0.5 7.4 1 613/06 6/3/06
Ethylbenzene 6050013 0.17 0.5 11 1 613/06 6/3/06
Hexachloro-1,3-butadiene 6050013 0.26 0.5 NO 1 613/06 6/3/06
Methylenechloride 6050013 0.18 2 NO 1 613/06 6/3/06
Styrene 6050013 0.16 0.5 2.6 1 613/06 6/3/06
1,1,2,2-Tetrachloroethane 6050013 0.18 0.5 NO 1 613/06 6/3/06
Tetrachloroethene(PCE) 6050013 0.21 0.5 19 1 613/06 6/3/06
Toluene 6050013 0.2 0.5 14.1 1 613106 6/3/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 6/3/06 6/3/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,1,2-Trichloroethane 6050013 0.21 0.5 NO 1 613106 6/3/06
Trtchloroethene(TCE) 6050013 0.21 0.5 7.5 1 6/3/06 6/3/06
Trichlorofluoromethane(Freon-11) 6050013 0.2 1 3.4 1 6/3/06 6/3/06
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/3/06 613/06
1,2,4-Trimethylbenzene 6050013 0.2 1 4.0 1 6/3/06 6/3/06
1,3,5-Trimethylbenzene 6050013 0.18 1 4.8 1 6/3/06 6/3/06
Vinyl chloride 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
m,p-Xylene 6050013 0.37 1 7.0 1 6/3/06 613/06
o-Xylene 6050013 0.19 0.5 13 1 6/3/06 6/3/06
System MonitoringCompounds(Surrogate) % Recovery aCUmit(%)
4-Bromofluorobenzene 105 80-120Key: MDL'" Method Detection Limit RL'" Reporting Limit J '" Trace Cone. between MOL and RL M.B. '" Method Blank T.B. '" Trip Blank F.B. '" Field Blank E.B. '" Equipment Blank
~LabS, Inc.
EIliSHS~~Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Waler and Wastewater _ Industrial and Hazardous Waste _ Chemical Consultation
Project Info RelJort InfoProject 10: 2006.0088 Sample 10: VN6-41 AccuLabs 10: 06-05-0013-18
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31106 Reporting Units: ppbV
Samole Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Organic Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chlorofonn
Chloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane{Freon-12}
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
eans-t.a-rncnroropropene
1,2-Dichlorotetrafluoroethane{F-114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-1,3-butadiene
Methylenechloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene (TCE)
Trichlorofluoromethane(Freon-11 )
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
605001360500136050013
6050013
60500136050013
60500136050013
60500136050013
60500136050013
605001360500136050013
60500136050013
60500136050013
605001360500136050013
605001360500136050013
605001360500136050013
60500136050013
605001360500136050013
6050013
60500136050013
6050013
60500136050013
6050013
0.17
0.210.260.19
0.210.3
0.23
0.180.18
0.180.18
0.20.18
0.210.190.23
0.190.17
0.210.140.180.21
0.17
0.260.180.160.18
0.210.2
0.260.21
0.210.210.2
0.2
0.20.18
0.17
0.370.19
0.5
0.50.5
0.50.5
0.5
0.50.5
0.50.5
0.50.5
2
0.50.5
0.50.5
0.50.50.51
0.50.5
0.52
0.5
0.50.5
20.5
0.50.50.5
1
1
1
1
0.5
1
0.5
8.5 1 611106
NO 1 611106
35 1 611106
NO 1 6/1/06
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 6/1/06
NO 1 6/1106
NO 1 6/1/06NO 1 611106
NO 1 6/1/06NO 1 611/06NO 1 6/1/06
NO 1 611106
NO 1 611106
NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06NO 1 6/1/06NO 1 6/1/06
NO 1 6/1/06NO 1 611106
NO 1 6/1/06
75 4 611106
NO 1 611106
NO 1 611106
NO 1 6/1/06NO 1 611106
NO 1 611106
NO 1 611106
NO 1 6/1/06
NO 1 611106
NO 1 611106
NO 1 6/1/06
NO 1 611106
611/06611106
6/1/066/1/06
6/1/066/1/06
6/1/06611106
6/1/066/1/06
6/1/06
611106
611106
611106
611106
611106
611106
611106
611106
611106
611106
611106
611106
611106
611106
611106
6/1106
611106
611106
611106
611/066/1106
611106
611/06
6/1/066/1/06
6/1/06
6/1/066/1/066/1/06
System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
% Recovery
101
DC Limit(%)
80-120Key: MOL"" Method DetectionUmit RL= ReportingUmit J ""rraee cene. between MOLand RL M.B. "" Method Blank T.B. ""Trip Blank F.B. ""Field Blank E.B. "" Equipment Blank
AccuLabs, Inc.
ldsrektiLaboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info Report InfoProject ID: 2006.0088 Sample ID: aCTS AccuLabs ID: 06-05-0013-19
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
Qualifiers
Date
AnalyzedRLMDLBatch
Volatile Organic Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
'l.a-Diohlorobenzene
Dichlorodifluoromethane(Freon-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1 ,3-Dichloropropene
1,2-Dichlorotetrafluoroethane(F-114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-1,3-butadiene
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene (TCE)
Trichlorofluoromethane(Freon-11 )
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
60500136050013
60500136050013
60500136060013
6060013
6050013
606001360500136050013
605001360500136060013
60500136060013
60500136050013
605001360500136050013
6050013605001360500136050013
60500136050013
60500136050013
60500136050013
60500136050013
60500136050013
60500136050013
60500136050013
6050013
0.17
0.210.260.19
0.210.3
0.23
0.18
0.180.18
0.180.20.18
0.210.19
0.230.190.17
0.210.14
0.180.210.170.260.18
0.16
0.180.21
0.20.260.21
0.210.21
0.20.2
0.20.18
0.17
0.37
0.19
0.5
0.50.5
0.50.5
0.50.5
0.5
0.5
0.50.50.5
2
0.5
0.50.50.5
0.50.50.5
1
0.5
0.50.52
0.5
0.50.5
0.50.5
0.50.50.5
1
1
1
1
0.5
1
0.5
NO 1 6/1/06ND 1 611106
ND 1 6/1/06
ND 1 611106
ND 1 611106ND 1 611106ND 1 611106
ND 1 611106ND 1 611106
ND 1 611106ND 1 6/1/06ND 1 611106
ND 1 611106ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 611106ND 1 6/1/06
ND 1 6/1/06
ND 1 611106ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
ND 1 611106
ND 1 6/1/06ND 1 6/1/06
ND 1 611106ND 1 611106
ND 1 6/1/06ND 1 6/1/06
ND 1 6/1/06
ND 1 6/1/06
6/1/06
611106
6111066111066/1/06
611106611106
611106
6111066/1/06
611106611106
6111066/1/06
6111066111066/1/06
611106
611106611106
611106611106611106
6111066/1/06611106
6/1/066/1/06
6111066111066/1/06
6/1/06611106
611106611106
611106611106
611106
611106611106
System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
% Recovery
100
QC Limit(%)
80-120Key: MOL" Method DetectionLimit RL" ReportingLimit J" Trace Cone.betweenMOL and RL M.B." Method Blank T.B." Trip Blank F.B." Field Blank E.B." EquipmentBlank
~~:s,lnc.
Ellis Hsue '-1Laboratory DJector
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous waste • Chemical Consultation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VNDUP-1 AccuLabs 10: 06-05-0013-20
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 617106Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Samole Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Organrc Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1.s-autecneneCarbon tetrachloride
Chtorobenzene
Chloroethane
Chlorofonn
Chloromethane
1,2-Dibromoethane
1.z-mctaorobenzene
t.a-Dlctuorobenzene
1A-Dichlorobenzene
Dichlorodifluoromethane(Freon-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
ers-t,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorotetrafluoroethane(F-114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-t,3-butadiene
Methylenechloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene(PCE)
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene(TCE)
Trichlorofluoromethane(Freon-11 )
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
6050013
60500136050013
60500136050013
60500136050013
6050013
60500136050013
6050013
60500136050013
6050013605001360500136050013
60500136050013
605001360500136050013
605001360500136050013
6050013605001360500136050013
6050013
60500136050013
60500136050013
60500136050013
60500136050013
60500136050013
0.170.21
0.260.19
0.210.3
0.23
0.18
0.180.18
0.180.2
0.180.210.19
0.230.190.17
0.210.140.18
0.210.17
0.260.180.160.18
0.210.2
0.260.21
0.210.21
0.20.2
0.20.18
0.170.37
0.19
0.50.50.5
0.50.5
0.50.5
0.5
0.5
0.60.5
0.52
0.50.50.50.5
0.50.5
0.51
0.5
0.50.52
0.50.50.5
2
0.5
0.50.5
0.51
1
1
10.5
10.5
7.3 1 6/3106
NO 1 6/3/06
33 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
2.5 1 6/3106
NO 1 6/3/06
NO 1 6/3106
NO 1 613/06
NO 1 613106
NO 1 613/06
NO 1 6/3106NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
1.6 1 6/3/06
2.6 1 6/3106
NO 1 6/3/06
NO 1 6/3106
2.1 1 613106
NO 1 613/06
NO 1 613/0668 4 613/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
2.6 1 6/3/06
1.6 1 6/3/06
NO 1 6/3/06
3.0 1 613106
2.4 1 6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6131066/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3106613106613/06
613/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/31066/3/06
6/31066/3/06
6/3/06
6/3/06
System MonitoringCompounds(Surrogate)
4-Bromofluorobenzene
% Recovery
102
QCUmit(%)
80-120Key: MOL; Method DetectionLimit RL =ReportingLimit J =Trace Cone.betweenMOLand RL M.B.=MethodBlank T.B. = Trip Blank F.B.= Field Blank E.B. =EquipmentBlank
~LabS, Inc.
EIiiSHfut,1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
Project Info Report InfoProject 10: 2006.0088 Sample 10: VNDUP-2 AccuLabs 10: 06-05-0013-21
Sample Site: Palos Verde Landfill Date Sampled: 5/31/06 Date Reported: 6m06Client Name: Geologic Associates Date Received: 5/31/06 Reporting Units: ppbV
Sample Matrix: GAS
Qualifiers
DateAnalyzedRLMOLBatch
Volatile Organrc Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dlchlorobenzene
Dichlorodifluoromethane{Freon-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1.z-Dlcbtorcoropane
cis-f.S-Dlchloropropene
trans-1,3-Dichloropropene
1,2-Dichlorotetrafluoroethane(F-114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-1,3-butadiene
Methylenechloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,4-Trichlorobenzene
t.t.f-rrtcbroroethane
1,1,2-Trichloroethane
Trichloroethene (TCE)
Trichlorofluoromethane(Freon-11 )
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m.p-Xylene
o-Xylene
6050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013605001360500136050013
0.170.210.260.190.210.30.230.180.180.180.180.2
0.180.210.190.230.190.170.210.140.180.210.170.260.180.160.180.210.2
0.260.210.210.210.2
0.20.20.180.170.370.19
0.50.50.50.50.50.50.50.50.50.50.50.52
0.50.50.50.50.50.50.51
0.50.50.52
0.50.50.50.50.50.50.50.51
1
1
1
0.51
0.5
1.5 1 6/3/06
NO 1 6/3/06
2.7 1 6/3/06
NO 1 6/3/06
NO 1 6/3106
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3106
2.2 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 613106
NO 1 613/06
NO 1 613106
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
3.3 1 6/3/06
1.6 1 6/3/06
NO 1 6/3/06
NO 1 613106
NO 1 613/06
NO 1 613106
NO 1 613/06
NO 1 613/06
1.5 1 613/06NO 1 613/06
NO 1 6/3/06
NO 1 6/3/06
NO 1 6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
613106
613/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
613106
613106
613/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
613106
613/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
6/3/06
613106
613/06
System Monitoring Compounds (Surrogate)
a-Bromofluorobenzene
% Recovery
107QC Limit (%)
80-120Key: MDL =Method Detection Umit RL = ReportingUmit J =Trace Cone.between MOLand RL M.B.= Method Blank T.B. =Trip Blank F.B. = FieldBlank E.B. = Equipment Blank
~LabS, Inc.
E~iS Hsrek"'"Laboratory DirJctor
QC Data Summary
(1) Vacuum Reading Log ofPre-Certified SummaCanisters
(2) List of Certificates of Summa Canisters with QCData Performed by EPA TO-IS Method
(3) LCS & LCSD Data Summary-TO-14 Test
(4) Method Blank Data
AccuLabs, Inc.Air Toxic. Contaminated Soil » Water and Wastewater· Industrial and Hazardous Waste· Chemical Consultation
List of Vacuum Readings and The Pre-Certified Summa Canisters
for the Provided Twenty-one Units to GLA- Palos Verde Project
AccuLabslD ENTECH Vacumn Readings Date Prepared Measured andCanister ID Serial Number in mm Hg QC Check (Pass/Fail) & Checked Checked by:
AL-015 CS/N-5955 > 30 Psi Yes 1 Pass 5126/2006 JH<Trip Blank>
AL-002 CS/N-5917 < -29.50 Yes 1Pass 5/27/2006 JH
AL-013 CS/N-5946 < -29.50 Yes 1Pass 5/27/2006 JH
AL-014 CS/N-5954 < -29.75 Yes 1Pass 5/27/2006 JH
AL-005 CS/N-5956 < -29.75 Yes 1Pass 5/27/2006 JH
AL-017 CS/N-6124 < -29.85 Yes 1 Pass 5/27/2006 JH
AL-020 CS/N-6602 < -29.75 Yes 1 Pass 5/27/2006 JH
AL-021 CS/N-6603 < -29.50 Yes 1 Pass 5/27/2006 JH
AL-022 CS/N-6605 < -29.50 Yes 1 Pass 5/27/2006 JH
AL-024 CS/N-6607 < -29.75 Yes 1 Pass 5/27/2006 JH
AL-025 CS/N-6608 < -29.50 Yes 1 Pass 5/27/2006 JH
AL-026 CS/N-6609 < -29.85 Yes 1Pass 5/27/2006 JH
AL-027 CS/N-661 0 < -29.50 Yes 1Pass 5/27/2006 JH
AL-028 CS/N-6611 < -29.50 Yes 1Pass 5/27/2006 JH
AL-029 CS/N-6612 < -29.75 Yes 1Pass 5/27/2006 JH
AL-030 CS/N-6613 < -29.75 Yes 1Pass 5/27/2006 JH
AL-033 CS/N-6616 < -29.75 Yes 1 Pass 5/27/2006 JH
AL-034 CS/N-6617 < -29.50 Yes 1 Pass 5/27/2006 JH
AL-038 CS/N-6621 < -29.50 Yes 1 Pass 5/27/2006 JH
AL-041 CS/N-6624 < -29.75 Yes 1 Pass 5/27/2006 JH
AL-043 CS/N-6626 < -29.75 Yes 1 Pass ~ 5/27/2006 JH
Checked out by Judy Hsue, E.E. ' Received by: «:Date:t{vr (11(, Technician, Acculabs, Inc. Date: <;/ty/oC Bryan A. Stirrat & Asso. for GLA
i
15437 E. Proctor Avenue· City ofIndustry, California 91745 • Mailing Address: P.O. Box 92314 • City of Industry, California 91745-2314Tel: (626) 934-1288· Fax: (626) 934-1299
C1b' AccuLabs, Inc.._----------_.._-_.._-_........_---_._._.._-_._.-...'-.-_._..._.__._._.__..._............__................__.........__._..._._._.__.__...._.__._._..._._._...... ............................................._............_... ..................__.................._............__...._..._...
Air Toxic » Contaminated Soil « Water and Wastewater" Industrial and Hazardous Waste· Chemical Consultation
List of Certificate with Analytical Data Performed by TO-15 Test
for the Provided Silonite Summa Canisters to GLA- Palos Verde Project
AccuLabs ID ENTECH Analytical Results Surrogate % Recovery Certificate ( YIN) I Date CertifiedCanister ID Serial Number for All 62 Compounds QC Limit (80-100)% QC Result (Pass/Fail) & Comment
AL-018 CS/N-6126 ND 101.7 Yes I Pass 2/28/2006<Trip Blank>
AL-002 CS/N-5917 ND 97.3 Yes I Pass 2/23/2006
AL-013 CS/N-5946 ND 97.6 Yes I Pass 2/23/2006
AL-014 CS/N-5954 ND 104.3 Yes I Pass 2/28/2006
AL-005 CS/N-5956 ND 103.1 Yes I Pass 2/28/2006
AL-017 CS/N-6124 ND 103.2 Yes I Pass 2/23/2006
AL-020 CS/N-6602 ND 94.4 Yes I Pass 2/23/2006
AL-021 CS/N-6603 ND 101.3 Yes I Pass 2/23/2006
AL-022 CS/N-6605 ND 97.0 Yes I Pass 2/23/2006
AL-024 CS/N-6607 ND 99.7 Yes I Pass 2/23/2006
AL-025 CS/N-6608 ND 98.6 Yes I Pass 2/24/2006
AL-026 CS/N-6609 ND 98.9 Yes I Pass 2/24/2006
AL-027 CS/N-661 0 ND 94.9 Yes I Pass 2/24/2006
AL-028 CS/N-6611 ND 100.3 Yes I Pass 2/24/2006
AL-029 CS/N-6612 ND 99.9 Yes I Pass 2/23/2006
AL-030 CS/N-6613 ND 99.5 Yes I Pass 2/24/2006
AL-033 CS/N-6616 ND 99.2 Yes I Pass 2/23/2006
AL-034 CS/N-6617 ND 101.6 Yes I Pass 2/23/2006
AL-038 CS/N-6621 ND 101.5 Yes I Pass 2/23/2006
AL-041 CS/N-6624 ND 98.3 Yes I Pass 2/23/2006
AL-043 CS/N-6626 ND 103.4 Yes I Pass 2/28/2006
Certified by Crystal Wu. M.S. Received by: 1A'~.~Date:5(~ Senior Chemist. Acculabs, Inc. Date: 'i/ t 110' Bryan A. Stirrat & Asso. for GLA
15437 E. Proctor Avenue· City ofIndustry, California 91745 • Mailing Address: P.O. Box 92314 • City of Industry, California 91745-2314Tel: (626) 934-/288· Fax: (626) 934-/299
~ AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation
Proiect Info Sample Info Report InfoProject 10: 2008.0088 Date Sampled: NA Acculabs Batch 10: 06050013-lCSQC-1
Sample Site: Palos Verde landfill Date Received: NA Date Reported: 6/7106Client Name: Geo-logic Associates Date Analyzed: 611106 Reporting Units: ppbV
Sample Matrix: Gas ElAP Certification r2608
Laboratory Control Standards (LCS/LCSD) Analysis by EPA TO-14
LCS 105: AL-06050013-LCS & LCSD-Set1
Sample Amount LCS LCS LCSD LCSD Date
Test Parameter Result Spiked Result % Recovery Resuit % Recovery QC Limit %RPD QC Limit R.L. Analyzed
1,1,MDichloroethene 0 50 42.21 84 48.21 98 80-120 13 20 0.5 6/1/06
Benzene 0 50 46.84 94 51.19 102 80-120 9 20 0.5 6/1/06
Trichloroelhene(TCE) 0 50 42.15 84 45.17 90 80-120 7 20 0.5 6/1/06
Toluene 0 50 45.35 91 49.09 98 80-120 8 20 0.5 611106
Tetrachloroethene (PCE) 0 50 41.87 84 43.85 88 80-120 5 20 0.5 6/1/06
Chlorobenzene 0 50 46.62 93 49.48 99 80-120 6 20 0.5 6/1/06
Key:MDL= MethodDetection Limit RL= Reporting Limit J= Trace Conc. betweenMOLand RL M.B.= MethodBlank T.B.= Trip Blank F.B.= Field Blank E.B.= EquipmentBlank
AccuLabs, Inc.
~~1Ellis HsueLaboratory Director
AccuLabs, Inc."" I OXIC. L.omammaleo "011 • vvater ana vvastewater • Industrial and Hazardous Waste. Chemical Consultation
Project Info Sample Info Report InfoProject 10: 2008.0088 Date Sampled: NA AccuLabs Batch 10: 06050013-LCSQC-2
Sample Site: Palos Verde Landfill Date Received: NA Date Reported: 617106Client Name: Geo-Logic Associates Date Analyzed: 6/3/06 Reporting Units: ppbV
Sample Matrix: Gas ELAP Certification 12608
~·~~=. _ " n 'i"iWii'-'".~".~••_~-~._-~====~ L ....... ~ __ ~-- "'--""
Laboratory Control Standards (LCS/LCSD) Analysis by EPA TO-14
LCS 105: AL-06050013-LCS & LCSD-Sel2
Sample Amount LCS LCS LCSD LCSD Date
Test Parameter Result Spiked Result % Recovery Result % Recovery QC Limit %RPD QC Limit R.L. Analyzed
1,1,-Dichloroethene 0 50 51.63 103 50.57 101 80-120 2 20 0.5 6/3/06Benzene 0 50 56.03 112 55.23 110 80-120 1 20 0.5 6/3/06
Trichloroethene(TCE) 0 50 49.32 99 49.24 98 80-120 0 20 0.5 6/3/06Toluene 0 50 54.04 108 53.74 107 80-120 1 20 0.5 6/3/06
Tetrachloroethene (PCE) 0 50 48.44 97 48.91 98 80-120 1 20 0.5 6/3/06Chlorobenzene 0 50 51.98 104 51.96 104 80-120 0 20 0.5 6/3/06Key:MDL= Method Detection Limit RL= Reporting Limit J= Trace Cone. betweenMOLand RL M.B.= Method Blank T.B.= Trip Blank F.B.= Field Blank E.B.= EquipmentBlank
AccuLabs, Inc.
~~4rEllisHsue 1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater _ Industrial and Hazardous Waste. Chemical Consultation
-~._----,----------,-------~-----
Proiect Info ReoortlnfoProject 10: 2006.0088 Sample 10: Method Blank #1 AccuLabs 10: MB060601
Sample Site: Palos Verde Landfill Date Sampled: NA Date Reported: 617106Client Name: Geologic Associates Date Received: NA Reporting Units: ppbV
Sample Matrix: GAS
Qualifiers
Date
AnalyzedRLMOLBatch
Volatile Organic Compounds by EPA TO-14 MethodSample Date
Result OF PreparedAnalyte
Benzene
Bromomethane
1,3-Butadiene
Carbon tetrachloride
Chlorobenzene
ChloroethaneChloroform
Chloromethane
1,2-Dibromoethane
1,2-0ichlorobenzene
1.a-mctuorobenzene
1A-Dichlorobenzene
Dichlorodifluoromethane(Freon-12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorotetrafluoroethane(F-114)
4-Ethyltoluene
Ethylbenzene
Hexachloro-1,3-butadiene
Methylene chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene (PCE)
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene (TeE)
Trichlorofluoromethane(Freon-11)
1,1,2-Trichlorotrifluoroethane(F-113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m,p-Xylene
o-Xylene
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
6050013
0.17
0.21
0.26
0.19
0.21
0.3
0.23
0.18
0.18
0.18
0.18
0.2
0.18
0.21
0.19
0.23
0.19
0.17
0.21
0.14
0.18
0.21
0.17
0.26
0.18
0.16
0.18
0.21
0.2
0.26
0.21
0.21
0.21
0.2
0.2
0.2
0.18
0.17
0.37
0.19
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
2
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1
0.5
0.5
0.5
2
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1
1
1
1
0.5
1
0.5
NO 1 611/06
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611/06
NO 1 611106
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 611/06
NO 1 611/06
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 611106
NO 1 6/1/06
NO 1 611106
NO 1 611106
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
NO 1 6/1/06
611/06
611/06
611/06
611106
611/06
6/1/06
611106
6/1/06
611/06
6/1/06
6/1/06
611106
6/1/06
611106
611106
611106
6/1106
611106
611106
611106
611106
611106
611106
611/06
611106
611106
611106
611106
6/1/06
6/1/06
6/1/06
611/06
6/1/06
6/1/06
6/1/06
6/1/06
6/1/06
611106
6/1/06
611106
System Monitoring Compounds (Surrogate)
4-Bromofluorobenzene
% Recovery
99.6
QC Limit(%)
80-120Koy: MDL.=Method Detection umn RL. = ReportingUmit J =Trace Cone.between MOL. and Rl M.B. =Method Blank T.B. - Trip Blank F.B. = Field Blank E.B. = EquipmentBlank
~~abS, Inc.
EIliSHS~1Laboratory Director
AccuLabs, Inc.Air Toxic. Contaminated Soil. Water and Wastewater. Industrial and Hazardous Waste. Chemical Consultation-(:!)--------'-------
Proiect Info Reoort tntoProject 10: 2006.0088 Sample 10: Method Blank #2 AccuLabs 10: MB060603
Sample Site: Palos Verde Landfill Date Sampled: NA Date Reported: 6m06Client Name: Geologic Associates Date Received: NA Reporting Units: ppbV
Samole Matrix: GAS
Volatile Organic Compounds by EPA TO-14 MethodSample Date Date
Analyte Batch MOL RL Result OF Prepared Analyzed Qualifiers
Benzene 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
Bromomethane 6050013 0.21 0.5 NO 1 6/3/06 6/3106
1,3-Butadiene 6050013 0.26 0.5 NO 1 6/3/06 6/3/06
Carbon tetrachloride 6050013 0.19 0.5 NO 1 6/3/06 6/3/06
Chlorobenzene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Chloroethane 6050013 0.3 0.5 NO 1 613/06 6/3/06
Chloroform 6050013 0.23 0.5 NO 1 6/3106 6/3/06
Chloromethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
t.z-noromcethane 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,2-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3106 6/3/06
1,3-Dichlorobenzene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
1,4-Dichlorobenzene 6050013 0.2 0.5 NO 1 6/3/06 6/3106
Dichlorodifluoromethane(Freon-12) 6050013 0.18 2 NO 1 6/3/06 6/3/06
1,1-Dlchloroethane 6050013 0.21 0.5 NO 1 613/06 6/3/06
1,2-Dichloroethane 6050013 0.19 0.5 NO 1 613106 6/3/06
1,1-Dichloroethene 6050013 0.23 0.5 NO 1 6/3/06 6/3/06
cls-t.z-Dichloroethene 6050013 0.19 0.5 NO 1 6/3/06 6/3/06
1,2-Dichloropropane 6050013 0.17 0.5 NO 1 6/3106 6/3/06
ers-t,3-Dichloropropene 6050013 0.21 0.5 NO 1 6/3/06 6/3106
trans-t ,3-Dichloropropene 6050013 0.14 0.5 NO 1 6/3/06 6/3/06
1,2~Dichlorotetrafluoroethane(F-114) 6050013 0.18 1 NO 1 6/3/06 6/3/06
4-Ethyltoluene 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Ethylbenzene 6050013 0.17 0.5 NO 1 6/3106 6/3/06
Hexachloro-1.s-butaorene 6050013 0.26 0.5 NO 1 6/3106 6/3/06
Methylenechloride 6050013 0.18 2 NO 1 6/3/06 6/3/06
Styrene 6050013 0.16 0.5 NO 1 6/3/06 6/3/06
1,1.z.z-tenactuorcemene 6050013 0.18 0.5 NO 1 6/3/06 6/3/06
Tetrachloroethene (PCE) 6050013 0.21 0.5 NO 1 6/3/06 6/3106
Toluene 6050013 0.2 0.5 NO 1 6/3/06 6/3/06
1,2,4-Trichlorobenzene 6050013 0.26 0.5 NO 1 6/3/06 6/3/06
1,1,1-Trichloroethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
1,t.z-rrtcblorcethane 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Trichloroethene(TCE) 6050013 0.21 0.5 NO 1 6/3/06 6/3/06
Trichlorofluoromethane(Freon-11 ) 6050013 0.2 1 NO 1 6/3106 6/3/06
1,1,2-Trichlorotrifluoroethane(F-113) 6050013 0.2 1 NO 1 6/3/06 6/3/06
1,2,4~TrimethyJbenzene 6050013 0.2 1 NO 1 6/3/06 6/3106
1,3,5-Trimethylbenzene 6050013 0.18 1 NO 1 6/3/06 6/3/06
Vinyl chloride 6050013 0.17 0.5 NO 1 6/3/06 6/3/06
m,p-Xylene 6050013 0.37 1 NO 1 6/3/06 6/3/06
o-Xylene 6050013 0.19 0.5 NO 1 613/06 6/3/06
System MonitoringCompounds(Surrogate) % Recovery QC Limit (%)
4-Bromofluorobenzene 103 80-120Key: MOL =Method Detection Umit RL _ Reporting Umit J =Trace Cone. between MOL and RL M.B. =Method Blank T.B. =Trip Blank F.B. = Field Blank E.B. = Equipment Blank
~ULa:s, Inc.
EllisHtt 1Laboratory Director
JOB NAME:
JOB NO.:
Palos Verdes l
2006-088
ORGANIC MATTER - ASTM 02974
DATE:
BY:
5/22/2006
lD
Sample No. VN-1/4 VN-1/6 VN-2/2 VN-2/6
location
Tare (grms) 174.84 174.81 174.78 174.76
Soil (grms)
Wet Soil + Tare
Dry Soil + Tare 196.04 200.21 200.12 200.14
Dry Soil (grms), B 21.2 25.4 25.34 25.38
Water Content (%)
Ashed Soil + Tare (grms) 195.43 199.56 199.22 197.98
Ash (grms), C 20.59 24.75 24.44 23.22
Ash Content (%), 0 97.1 97.4 96.4 91.5
Organic Matter (%) 2.9 2.6 3.6 8.5
Ash Content, % =(C x 100) 1B
Organic Matter, % = 100.0 - D
Geologic Associates
JOB NAME:
JOB NO.:
Palos Verdes l
2006-088
ORGANIC MATTER - ASTM D2974
DATE:
BY:
5/22/2006
lD
Sample No. VN-218 VN-3/2 VN-3/4 VN-3/6
location
Tare (grms) 174.76 174.76 174.78 174.79
Soil (grms)
Wet Soil + Tare
Dry Soil + Tare 200.57 200.24 200.62 196.05
Dry Soil (grms), B 25.81 25.48 25.84 21.26
Water Content (%)
Ashed Soil + Tare (grms) 197.97 199.16 199.8 193.54
Ash (grms), C 23.21 24.4 25.02 18.75
Ash Content (%), D 89.9 95.8 96.8 88.2
Organic Matter (%) 10.1 4.2 3.2 11.8
Ash Content, % = (C x 100) 1B
Organic Matter, % = 100.0 - D
Geologic Associates
JOB NAME:
JOB NO.:
Palos Verdes L
2006-088
ORGANIC MATTER - ASTM D2974
DATE:
BY:
5/22/2006
LD
Sample No. VN-4/2 VN-4/5 VN-5/3 VN-5/4
Location
Tare (grms) 174.76 174.76 174.78 174.76
Soil (grms)
Wet Soil + Tare
Dry Soil + Tare 203.03 200.15 201.69 200.17
Dry Soil (grms), B 28.27 25.39 26.91 25.41
Water Content (%)
Ashed Soil + Tare (grms) 202.1 198.65 200.72 199.25
Ash (grms), C 27.34 23.89 25.94 24.49
Ash Content (%), D 96.7 94.1 96.4 96.4
Organic Matter (%) 3.3 5.9 3.6 3.6
Ash Content, % =(C x 100) I B
Organic Matter, % = 100.0 - D
Geologic Associates
JOB NAME:
JOB NO.:
Palos Verdes L
2006-088
ORGANIC MATTER· ASTM D2974
DATE:
BY:
5/26/2006
LD
Sample No. VN-5/7 VN-6/3 VN-6/5 VN-6/7
Location
Tare (grms) 174.76 174.76 174.79 174.78
Soil (grms)
Wet Soil + Tare
Dry Soil + Tare 201.37 201.02 200.22 201.06
Dry Soil (grms), B 26.61 26.26 25.43 26.28
Water Content (%)
Ashed Soil + Tare (grms) 200.63 200.18 199.17 199.98
Ash (grms), C 25.87 25.42 24.38 25.2
Ash Content (%), D 97.2 96.8 95.9 95.9
Organic Matter (%) 2.8 3.2 4.1 4.1
Ash Content, % =(C x 100) 1B
Organic Matter, % =100.0 - D
GeoLogic Associates
JOB NAME:
JOB NO.:
Palos Verdes l
2006-088
ORGANIC MATTER· ASTM D2974
DATE:
BY:
5/26/2006
lD
Sample No. VN-10/5 VN-11/1
location
Tare (grms) 174.75 174.76
Soil (grms)
Wet Soil + Tare .
Dry Soil + Tare 201.22 200.96
Dry Soil (grms), B 26.47 26.2
Water Content (%)
Ashed Soil + Tare (grms) 200.08 199.83
Ash (grms), C 25.33 25.07
Ash Content (%), D 95.7 95.7
Organic Matter (%) 4.3 4.3
Ash Content, % =(C x 100) 1B
Organic Matter, % = 100.0 - D
Geologic Associates
Client 1Job Name:
SPECIFIC GRAVITY OF SOILS - ASTM D 854-92
Palos Verdes LF Date: 5/22/2006
Job No. 2006-088 By: LD
.Sample No. VN-1/4 VN-1/6 VN-2/2 VN-2/6
WI. of Pycnometer, W p 177.19 179.38 178.27 175.54
WI. of Oven Dry Soil, W s 44.25 49.93 45.06 46.59
WI. of Pycnometer & H20 @T"W, 675.03 677.57 675.91 674.36
Temperature, T 1 24.5 24.5 24.5 17.5
Pycnometer & H20 & Soil @ T" w, 702.33 709.26 705.28 701.81
Temperature, Tx 22.0 21.0 21.0 21.0
WI. of Pycnometer & H20 @ T,. We 675.33 677.98 676.32 674.02
Specific Gravity @ 200e 2.564 2.676 2.798 2.478
We =[(r H 20 @ Tx / r H20 @ T1) X (W, - W p)J + W p
S.G.@200=Ws/(Ws+We-Wb)xK@Tx
Density of Water and Correction Factor K for VariousTemperatures
Temperature, 0 C
16.016.517.017.518.018.519.019.520.020.521.021.522.022.523.023.524.024.525.025.526.0
yH20
0.998970.998890.998800.998710.998620.998530.998430.998330.998230.998120.998020.997910.997800.997680.997570.997450.997320.997200.997070.996940.99681
Factor K1.00071.00071.00061.00051.00041.00031.00021.00011.00000.99990.99980.99970.99960.99950.99930.99920.99910.99900.99880.99870.9986
GeoLogic Associates
Client 1Job Name:
SPECIFIC GRAVITY OF SOILS - ASTM D 854-92
Palos Verdes LF Date: 5/25/2006
Job No. 2006-088 By: LD
Sample No. VN-2/8 VN-3/2 VN-3/4 VN-3/6
WI. of Pycnometer, W p 177.19 179.38 178.27 175.54
WI. of Oven Dry Soil, W s 44.44 42.27 41.72 42.7
WI. of Pycnometer & H20 @ T"
w, 675.03 677.57 675.91 674.36
Temperature, T 1 24.5 24.5 24.5 17.5
Pycnometer & H20 & Soil @ T" W b 701.73 703.27 702.61 698.4
Temperature, T x 22.5 22.5 22.5 22.5
WI. of Pycnometer & H20 @ T" We 675.27 677.81 676.15 673.85
Specific Gravity @ 200 e 2.470 2.513 2.733 2.352
We =[(yH 20@Tx/yH20@T,)x(Wa - Wp)] + WpS.G. @200 =Ws/(Ws + We - Wb)xK@ T,
Density of Water and Correction Factor K for VariousTemperatures
Temperature, 0 C
16.016.517.017.518.018.519.019.520.020.521.021.522.022.523.023.524.024.525.025.526.0
0.998970.998890.998800.998710.998620.998530.998430.998330.998230.998120.998020.997910.997800.997680.997570.997450.997320.997200.997070.996940.99681
FactorK1.00071.00071.00061.00051.00041.00031.00021.00011.00000.99990.99980.99970.99960.99950.99930.99920.99910.99900.99880.99870.9986
GeoLogic Associates
Client 1Job Name:
SPECIFIC GRAVITY OF SOILS - ASTM D 854-92
Palos Verdes LF Date: 5/25/2006
Job No. 2006-088 By: LD
Sample No. VN-4/2 VN-4/5 VN-5/3 VN-5/4
WI. of Pycnometer, W p 177.19 179.38 178.27 175.54
WI. of Oven Dry Soil, W s 42.97 48.06 47.55 45.21
WI. of Pycnometer & H20 @ T"
Wa 675.03 677.57 675.91 674.36
Temperature, T t 24.5 24.5 24.5 17.5
Pycnometer & H20 & Soil @ T" W b 701.99 706.85 705.69 701.35
Temperature, r, 24.0 24.0 24.0 24.0
WI. of Pycnometer & H20 @ T" W, 675.09 677.63 675.97 673.67
Specific Gravity @ 200 e 2.672 2.549 2.664 2.577
We =ttr H 20@ t , / r H20@ T t ) X (Wa - Wp)J + w,8.G.@20 o = Ws/(Ws + We - Wb)xK@ T,
Density of Water and Correction Factor K for VariousTemperatures
Temperature, 0 C
16.016.517.017.518.018.519.019.520.020.521.021.522.022.523.023.524.024.525.025.526.0
r H 20
0.998970.998890.998800.998710.998620.998530.998430.998330.998230.998120.998020.997910.997800.997680.997570.997450.997320.997200.997070.996940.99681
Factor K1.00071.00071.00061.00051.00041.00031.00021.00011.00000.99990.99980.99970.99960.99950.99930.99920.99910.99900.99880.99870.9986
GeoLogic Associates
Client 1Job Name:
SPECIFIC GRAVITY OF SOILS - ASTM D 854-92
Palos Verdes LF Date: 5/26/2006
Job No. 2006-088 By: LD
Sample No. VN-5/7 VN-6/3 VN-6/5 VN-6/7
WI. of Pycnometer, W p 177.19 179.38 178.27 175.54
WI. of Oven Dry Soil, W s 47.04 53.86 42.97 52.3
WI. of Pycnometer & H20 @T" W a 675.03 677.57 675.91 674.36
Temperature, T1 24.5 24.5 24.5 17.5
Pycnometer & H20 & Soil@T" w, 703.77 710.23 702.77 706.27
Temperature, Tx 23.0 23.0 23.0 23.0
WI. of Pycnometer & H20 @T,. W, 675.21 677.75 676.09 673.79
Specific Gravity @ 20°' 2.543 2.517 2.635 2.637
W, = [(r H20 @ Tx / r H20 @ T 1) X (Wa - W p)J + W p
S.G. @20° =Ws/(Ws + W, - W b ) xK@ t ;
Density of Water and Correction Factor K for VariousTemperatures
Temperature, 0 C
16.016.517.017.518.018.519.019.520.020.521.021.522.022.523.023.524.024.525.025.526.0
r H 2 00.998970.998890.998800.998710.998620.998530.998430.998330.998230.998120.998020.997910.997800.997680.997570.997450.997320.997200.997070.996940.99681
Factor K1.00071.00071.00061.00051.00041.00031.00021.00011.00000.99990.99980.99970.99960.99950.99930.99920.99910.99900.99880.99870.9986
GeoLogic Associates
Client 1Job Name:
SPECIFIC GRAVITY OF SOilS - ASTM D 854-92
Palos Verdes IF Date: 5/26/2006
Job No. 2006-088 By: lD
Sample No. VN-10/5 VN-11/1
WI. of Pycnometer, W p 177.19 179.38
WI. of Oven Dry Soil, W s 54.75 48.5
WI. of Pycnometer & H20 @ T" W a 675.03 677.57
Temperature, T 1 24.5 24.5
Pycnometer & H20 & Soil@T" w, 707.92 706.55
Temperature, Tx 26.0 26.0
WI. of Pycnometer & H20 @ Tx, W, 674.84 677.38
Specific Gravity @ 20°0 2.524 2.506
W, = [(r H 20 @ T x / r H20 @T 1) X (W a - W p)] + W p
S.G. @200 = Ws/(Ws + W, - Wb)xK@ T,
Density of Water and Correction Factor K for VariousTemperatures
Temperature, °C
16.016.517.017.518.018.519.019.520.020.521.021.522.022.523.023.524.024.525.025.526.0
r H 20
0.998970.998890.998800.998710.998620.998530.998430.998330.998230.998120.998020.997910.997800.997680.997570.997450.997320.997200.997070.996940.99681
Factor K1.00071.00071.00061.00051.00041.00031.00021.00011.00000.99990.99980.99970.99960.99950.99930.99920.99910.99900.99880.99870.9986
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088
Date 5/25/06
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM D 422
T AVE. = 25.0Kn = 0.94
Time D Temp. dT R R+C KL d (rnrn) R+M % Pass) 30 0.081 25 -1.17 25.1 25.6 0.784336 0.0597 24.43 75.3
40 0.07 25 -1.17 24.6 25.1 0.788706 0.0519 23.93 73.8
1 0.057 25 -1.17 24 24.5 0.793951 0.0425 23.33 71.9
2 0.041 25 -1.17 22.9 23.4 0.803566 0.0310 22.23 68.6
5 0.026 25 -1.17 21.6 22.1 0.81493 0.0199 20.93 64.5
15 0.015 25 -1.17 20.1 20.6 0.828042 0.0117 19.43 59.9
30 0.011 25 -1.17 19.2 19.7 0.835909 0.0086 18.53 57.1
60 0.0074 25 -1.17 18.3 18.8 0.843776 0.00587 17.63 54.4
90 0.0061 25.5 -1.07 17.8 18.3 0.848147 0.00486 17.23 53.1
250 0.0037 26 -0.96 16 16.5 0.863881 0.00300 15.54 47.9
1440 0.0015 23 -1.55 14.2 14.7 0.879615 0.00124 13.15 40.6
100
100100100100100100100100
PalosVerdes LF
Project 1Client Palos Verdes LF
Sample No. VN-10/5By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
1.8 4.75 #4 983.7 2 #10 965 1.19 #16 95
6.9 0.595 #30 939.3 0.297 #50 9015.2 0.15 #100 8420.6 0.075 #200 78
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1125
34.992.661
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088Date 5/25/06
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM D 422
T AVE." 25.0Kn = 0.94
Time D Temp. dT R R+C KL d (mm) R+M % PassI 30 0.081 25 -1.17 24.6 25.1 0.788706 0.0601 23.93 73.4
40 0.07 25 -1.17 23.9 24.4 0.794825 0.0523 23.23 71.2
1 0.057 25 -1.17 23 23.5 0.802692 0.0430 22.33 68.5
2 0.041 25 -1.17 21.6 22.1 0.81493 0.0314 20.93 64.2
5 0.026 25 -1.17 19.9 20.4 0.82979 0.0203 19.23 59.0
15 0.015 25 -1.17 18 18.5 0.846399 0.0119 17.33 53.1
30 0.011 25 -1.17 17 17.5 0.85514 0.0088 16.33 50.1
60 0.0074 25 -1.17 15.9 16.4 0.864755 0.00602 15.23 46.7
90 0.0061 25.5 -1.07 14.9 15.4 0.873497 0.00501 14.33 43.9
250 0.0037 26 -0.96 13.3 13.8 0.887483 0.00309 12.84 39.4
1440 0.0015 23 -1.55 11 11.5 0.907587 0.00128 9.95 30.5
100100100100100100100100
100
PalosVerdes LF
Project 1Client Palos Verdes IFSample No. VN-11/1By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 100
1.5 9.52 3/8" 982.7 4.75 #4 973.9 2 #10 954.7 1.19 #16 956.9 0.595 #30 9210.7 0.297 #50 8816.3 0.15 #100 8121 0.075 #200 76
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
112545
86.207
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in i.sm 3/4in 3/8in .. #30 #100 #200
100 I, ;
,: i,,
i,:! iii I: I I
, :,i, ""
" I,
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, ,I ' . :
e-, 60, I:
,
: 1 1 : ~', IIII , , , ,
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I ic 50 i-..
'"'i--.i.i: ,: i,
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: , : , ,, .'
, , , ...............~ , ,, , : : : :
,
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" .
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, , ' : ' ,
20 , : : ' : .
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, : [_I ...., ,:, , ,
, ,10
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"
, ,'.
0100 10 1 0.1 0.01 0.001
Grain Size (mm)
Boring / SampleInitial Dry
Initiai MoistTest Dry
Test Moist Permeability, K Unified SoilNo.
Density(%)
Density(%) (em/sec)
LL PL PIClass.
Description(pet) (pcf)
VN-11/1
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088
Date 5/19/06
GRAIN SIZE ANALYSIS - ASTM 0 422
23.30.956
T AVE. =
Kn =
Time 0 Temp. dT R R+C KL d (rnrn) R+M % Pass) 30 0.081 23 -1.55 21 21.5 0.820175 0.0635 19.95 55.5
40 0.07 23 -1.55 20 20.5 0.828916 0.0555 18.95 52.7
1 0.057 23 -1.55 19.2 19.7 0.835909 0.0456 18.15 50.5
2 0.041 23 -1.55 18 18.5 0.846399 0.0332 16.95 47.25 0.026 23 -1.55 16.5 17 0.85951 0.0214 15.45 43.015 0.015 23 -1.55 15 15.5 0.872622 0.0125 13.95 38.830 0.011 23 -1.55 14 14.5 0.881364 0.0093 12.95 36.0
60 0.0074 23 -1.55 13 13.5 0.890105 0.00630 11.95 33.290 0.0061 23 -1.55 12.2 12.7 0.897098 0.00523 11.15 31.0
250 0.0037 24 -1.35 10.4 10.9 0.912832 0.00323 9.55 26.6
1440 0.0015 25.5 -1.07 7.3 7.8 0.93993 0.00135 6.73 18.7
100
100100100100100100100100
Palos Verdes LF
Project 1Client Palos Verdes IFSample No. VN-1/4By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 100
13.1 19.1 3/4" 9519.4 12.7 1/2" 9224.8 9.52 3/8" 9030 4.75 #4 88
34.2 2 #10 8738.8 1.19 #16 8544.9 0.595 #30 8251.5 0.297 #50 8073.9 0.15 #100 71106.9 0.075 #200 58
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
135037
255.47
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS C ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.5in 3f4in 3/ain os #30 #100 #200100 , ,
,~: i r , :I, ,, ,
, .. ,, , ,
.
,
90 . , ,: 1
, , ,, ," , : , ,
"
, , , ,80 ,
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+ :0> 70
" 'i• : "<, '~
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.: ; I:, ,
1
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50,
c: " I:,
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u:, ,: , , , , .c , ,
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, , , -~ 40
i:, I ' ~It--+-e
: 1
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: ,,
e , , , ....0- 30
,I , . ' : , '
, ,
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"
: t-...20
Ii' I: , , , , ,,, ,
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10 ,; ; , " .:: ! ' 'I !
,;
, , ,
, ', , "
, , , , , j0100 10 1 0,1 0,01 0,001
Grain Size (mm)
Boring / SampleInitial Dry
Initial MoistTest Dry
Test Moist Permeability, K Unified SoilNo,
Density(%)
Density(%) (em/sec)
LL PL PIClass.
Description(pcf) (pcf)
VN-1/4
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088
Date 5/19/06
GRAIN SIZE ANALYSIS - ASTM D 422
23.3
0.956
T AVE. =
Kn =
Time D Temp. dT R R+C KL d (mm) R+M % Pass) 30 0.081 23 -1.55 21 21.5 0.820175 0.0635 19.95 63.9
40 0.07 23 -1.55 20.5 21 0.824545 0.0552 19.45 62.3
1 0.057 23 -1.55 19.8 20.3 0.830664 0.0453 18.75 60.12 0.041 23 -1.55 18.8 19.3 0.839406 0.0329 17.75 56.95 0.026 23 -1.55 17.5 18 0.850769 0.0211 16.45 52.715 0.015 23 -1.55 15.9 16.4 0.864755 0.0124 14.85 47.630 0.011 23 -1.55 15.1 15.6 0.871748 0.0092 14.05 45.060 0.0074 23 -1.55 14.2 14.7 0.879615 0.00622 13.15 42.190 0.0061 23 -1.55 13.7 14.2 0.883986 0.00516 12.65 40.5250 0.0037 24 -1.35 12.3 12.8 0.896224 0.00317 11.45 36.71440 0.0015 25.5 -1.07 10.1 10.6 0.915455 0.00131 9.53 30.5
100
100
100
100100
100
100100
100
PalosVerdes LF
Project 1Client Palos Verdes LF
Sample No. VN-1/6
By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 ~5.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
0.2 4.75 #4 1000.7 2 #10 1001.8 1.19 #16 99
3.2 0.595 #30 99
4.9 0.297 #50 98
37.8 0.15 #100 86
90 0.075 #200 67
Total Dry Weight
- #4Wet Weight
Water Content- #4Dry Weight
1350
27.1275.37
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
u.s. Standard Sieve Size
3in t.sm 3f4in 3f8in .. #30 #100 #200
100 " , I , ; I , , I~I
, II :, I I
90"~, , , , , !
'.'"
"
, , , ,
" :I I i, , , ,H"
, , , , ,...... ! ...........
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80 " ... :.- .. '\, '
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: ,,
.<: 70,
tn
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i,
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c :: , , I,
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10,
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100 10 1 0.1 0.01 0.001Grain Size (mm)
Boring / Sam pieInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unified SoilNo.
Density(%)
Density(%) (em/sec)
II Pl PIClass.
Description(pcf) (pcf)
VN-1/6
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088
Date 5/19/06
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE. =
Kn =
Time D Temp. dT R R+C KL d (mm R+M % Pass) 30 0.081 23 -1.55 30.8 31.3 0.73451 0.0569 29.75 95.1
40 0.07 23 -1.55 30.4 30.9 0.738007 0.0494 29.35 93.8
1 0.057 23 -1.55 29.8 30.3 0.743252 0.0405 28.75 91.9
2 0.041 23 -1.55 28.8 29.3 0.751993 0.0295 27.75 88.7
5 0.026 23 -1.55 26.9 27.4 0.768601 0.0191 25.85 82.6
15 0.015 23 -1.55 23.7 24.2 0.796573 0.0114 22.65 72.430 0.011 23 -1.55 21.8 22.3 0.813182 0.0086 20.75 66.3
60 0.0074 23 -1.55 19.7 20.2 0.831538 0.00588 18.65 59.6
90 0.0061 23 -1.55 18.4 18.9 0.842902 0.00492 17.35 55.4250 0.0037 24 -1.35 14.8 15.3 0.874371 0.00309 13.95 44.61440 0.0015 25.5 -1.07 3.3 3.8 0.974895 0.00140 2.73 8.7
100
100100100100100100100100
PalosVerdes LF
Project 1Client Palos Verdes LF
Sample No. VN-2/2By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
0.6 4.75 #4 1001.2 2 #10 992 1.19 #16 99
3.2 0.595 #30 994.3 0.297 #50 985.4 0.15 #100 987.1 0.075 #200 97
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
51.1231.63
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S.StandardSieveSize
3in t.sm 3f4in 3f8in #8 #30 #100 #200
100" , I II I • ,
I::l ' I,: T
'. : , i I 'I
, I ,:--'....,90 ' , ... i. ..... ---- ..._.~,
1, , , , <, !, I ,
': !
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80: I 'I • , : I <, ,, , ,
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'" 70
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I 'a100 10 1 0.1 0.0 0.001
GrainSize (mm)
Boring / SampleInitial Dry
Initiai Moist.Test Dry
Test Moist. Permeability, K Unified SoilDensity Density LL PL PI Description
No.(pet)
(%)(pcf)
(%) (em/sec) Class.
VN-2/2
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088
Date 5/19/06
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE. =
Kn =
Time D Temp. dT R R+C KL d (mrn) R+M % Pass) 30 0.081 23 -1.55 30 30.5 0.741503 0.0574 28.95 93.0
40 0.07 23 -1.55 28 28.5 0.758986 0.0508 26.95 86.6
1 0.057 23 -1.55 25 25.5 0.78521 0.0428 23.95 76.9
2 0.041 23 -1.55 22 22.5 0.811434 0.0318 20.95 67.3
5 0.026 23 -1.55 18.5 19 0.842028 0.0209 17.45 56.0
15 0.015 23 -1.55 15.5 16 0.868252 0.0125 14.45 46.430 0.011 23 -1.55 13.8 14.3 0.883112 0.0093 12.75 41.0
60 0.0074 23 -1.55 11.6 12.1 0.902343 0.00638 10.55 33.9
90 0.0061 23 -1.55 10.4 10.9 0.912832 0.00532 9.35 30.0250 0.0037 24 -1.35 8 8.5 0.933811 0.00330 7.15 23.01440 0.0015 25.5 -1.07 4.7 5.2 0.962657 0.00138 4.13 13.3
100100100100100100100100
100
PalosVerdes LF
Project 1Client Palos Verdes LFSample No. VN-2/6By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 1000 4.75 #4 1000 2 #10 1000 1.19 #16 1000 0.595 #30 1000 0.297 #50 100
0.1 0.15 #100 1001.4 0.075 #200 99
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
58.2221.24
GeoLogic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.5in 3f4in 3fSin .. #30 #100 #200100
:1, , , II ':\ i I I,
,I,--,_..:,:
, , , ,,"
, ,'I' I,! : I .
90 , .. ': , ... ,....• , , , , i ,
i ii :
, , , , ,Ji
, , , , , ,80
!
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, , , i : ,, i\. I
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•
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III : :
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~ 50,
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, :I:20 _....
:, ,
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, ,10
'I:', Ii 'i :i I ! i-----~, , , ,
:,',,
,: ,i ',I ,
!0100 10 1 0.1 0.01 0.001
Grain Size (mm)
Boring / SampieInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unitied SoilNo.
Density(%)
Density(%) (em/sec)
II Pl PIClass.
Description(pet) (pet)
VN-2/6
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088Date 5/19/06
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE. =
Kn =
Time D Temp. dT R R+C KL d (mm) R+M % PassI 30 0.081 23 -1.55 30 30.5 0.741503 0.0574 28.95 93.0
40 0.07 23 -1.55 28 28.5 0.758986 0.0508 26.95 86.61 0.057 23 -1.55 25 25.5 0.78521 0.0428 23.95 76.92 0.041 23 -1.55 22 22.5 0.811434 0.0318 20.95 67.3
5 0.026 23 -1.55 18.5 19 0.842028 0.0209 17.45 56.015 0.015 23 -1.55 15 15.5 0.872622 0.0125 13.95 44.830 0.011 23 -1.55 13 13.5 0.890105 0.0094 11.95 38.460 0.0074 23 -1.55 11 11.5 0.907587 0.00642 9.95 32.090 0.0061 23 -1.55 9.9 10.4 0.917203 0.00535 8.85 28.4
250 0.0037 24 -1.35 7.7 8.2 0.936434 0.00331 6.85 22.01440 0.0015 25.5 -1.07 4.7 5.2 0.962657 0.00138 4.13 13.3
100
100100100100100100100100
PalosVerdes LF
Project 1Client Palos Verdes LFSample No. VN-2/8By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 1000 4.75 #4 1000 2 #10 1000 1.19 #16 1000 0.595 #30 1000 0.297 #50 100
0.1 0.15 #100 1001.8 0.075 #200 99
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
57.1222.79
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.5fn 3/4in 3/8in #8 #30 #100 #200
100 , '.:' , ,i' ", : 'i' " i'\' I 1 I'1 1 Ii::; i I : I ~]
90 if'::!, :' " ,',:: , '80 +.,' c 1
t I; :' I :1 I I ' '
!! :: i:':. '!: . '.' :: \ ! I :
I 70 f': , , !I:.. : , ;: " . L! ] •
> ' ::' 1 I I 'I : I 1 : ~! I " ' :
€i 60 ': : ' ' ,,' i ' , ' ''0: '... I il I I I I "Ql 50 I ! I I I I I .......
il: : I : : I I ' : " : I : "'-c: 40 ' ., II ! " ." I , "".
~ I I 'I I !: I I 1
~ 30: :: :. :' : : ' ~_.... 1+1..·1....-7..,-----;--1-----1
20 ~_. __ .::,',' : :: ;,: :: : , ,: ~l . _~.." _• :..: : : i : :: :, !i: i <,1---...
10 : J; I 1 : I I I I I --...
:I I; :: :. ! ' , ! i Io i:: I !~ ~Ii! I I I I I i
100 10 1 0,1 0,01 0,001Grain Size (mm)
B ' / S I InitIal Dry I 't' 1M' t Test Dry T t M ' t P bllit K U lfl d S 'Ionng amp e D lt m ra OIS, D lt es OIS, ermea II y, LL PL PI nile 01 D' t'N ensi Y (0/) ensi Y (0/) ( / ) CI esenp Ion
0, (pef) /0 (pef) /0 em sec ass,
VN-2/8
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088Date 5/19106
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE. =
Kn =
Time D Temp. dT R R+C KL d (mm) R+M % Pass) 30 0.081 23 -1.55 31.5 32 0.728392 0.0564 30.45 97.5
40 0.07 23 -1.55 31 31.5 0.732762 0.0490 29.95 95.91 0.057 23 -1.55 30.2 30.7 0.739755 0.0403 29.15 93.32 0.041 23 -1.55 29 29.5 0.750245 0.0294 27.95 89.55 0.026 23 -1.55 27 27.5 0.767727 0.0191 25.95 83.115 0.015 23 -1.55 23.8 24.3 0.795699 0.0114 22.75 72.830 0.011 23 -1.55 21.5 22 0.815804 0.0086 20.45 65.560 0.0074 23 -1.55 19.3 19.8 0.835035 0.00591 18.25 58.490 0.0061 23 -1.55 17.9 18.4 0.847273 0.00494 16.85 53.9250 0.0037 24 -1.35 14.2 14.7 0.879615 0.00311 13.35 42.71440 0.0015 25.5 -1.07 8.4 8.9 0.930315 0.00133 7.83 25.1
100
100100100100100100100100
PalosVerdes LF
Project I Client Palos Verdes LFSample No. VN-3/2By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
0.1 4.75 #4 1000.7 2 #10 1000.8 1.19 #16 1000.9 0.595 #30 1000.9 0.297 #50 1001.1 0.15 #100 992.2 0.075 #200 99
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
70.2205.64
GeoLogic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 , Job # 2006-088
U.S. Standard Sieve Size
3in 1.5in 3/4in 3/ain #8 #30 #100 #200
100 'i,: I I i ,
':,', ' ,I ' , , 'i, : i,: I~!~
,
i, .90 :, ,', .
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100 10 1 0,1 0,01 0.001Grain Size (mm)
Boring / SampleInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unified SoilDensity Density LL PL PI Description
No.(pcf)
('!o)(pcf)
('!o) (em/sec) Class.
VN-3/2
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088Date 5/19106
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE."
Kn =
Time D Temp. dT R R+C KL d (rnrn) R+M % Pass) 30 0.081 23 -1.55 30.5 31 0.737133 0.0571 29.45 94.6
40 0.07 23 -1.55 29.8 30.3 0.743252 0.0497 28.75 92.3
1 0.057 23 -1.55 28.2 28.7 0.757238 0.0413 27.15 87.22 0.041 23 -1.55 26.2 26.7 0.77472 0.0304 25.15 80.85 0.026 23 -1.55 23.5 24 0.798322 0.0198 22.45 72.115 0.015 23 -1.55 20.4 20.9 0.82542 0.0118 19.35 62.230 0.011 23 -1.55 18.6 19.1 0.841154 0.0088 17.55 56.460 0.0074 23 -1.55 16.2 16.7 0.862133 0.00610 15.15 48.790 0.0061 23 -1.55 15.1 15.6 0.871748 0.00508 14.05 45.1
250 0.0037 24 -1.35 12 12.5 0.898846 0.00318 11.15 35.81440 0.0015 25.5 -1.07 7 7.5 0.942552 0.00135 6.43 20.7
100
100100100100100100100100
PalosVerdes LF
Project I Client Palos Verdes IFSample No. VN-3/4By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 1000 4.75 #4 1000 2 #10 100
0.1 1.19 #16 1000.1 0.595 #30 1000.2 0.297 #50 1000.6 0.15 #100 1002.4 0.075 #200 99
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
59.5219.44
Geologic Associates
Palos Verdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.5in 3/4in 3/8in #8 #30 #100 #200
100 ! I: ;, I: !I :
i II
, , ,
I "I:
I I I ,.., iI I I I I I
90 'I:' I'I:, I , , I I , I
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0100 10 1 0.1 0.01 0.001
Grain Size (mm)
Boring / SampleInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unified SoilDensity Density II Pl PI DescriptionNo.(pcf)
(%)(pef)
(%) (em/sec) Class.
VN-3/4
Geologic Associates
Job # 2005-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088Date 5/19/06
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE. =
Kn =
Time D Temp. dT R R+C KL d (rnrn) R+M % Pass) 30 0.081 23 -1.55 26.8 27.3 0.769476 0.0596 25.75 82.7
40 0.07 23 -1.55 23 23.5 0.802692 0.0537 21.95 70.5
1 0.057 23 -1.55 20 20.5 0.828916 0.0452 18.95 60.9
2 0.041 23 -1.55 16 16.5 0.863881 0.0339 14.95 48.0
5 0.026 23 -1.55 13.5 14 0.885734 0.0220 12.45 40.0
15 0.015 23 -1.55 11 11.5 0.907587 0.0130 9.95 32.0
30 0.011 23 -1.55 9.5 10 0.920699 0.0097 8.45 27.1
60 0.0074 23 -1.55 8.5 9 0.929441 0.00658 7.45 23.9
90 0.0061 23 -1.55 7.8 8.3 0.935559 0.00546 6.75 21.7
250 0.0037 24 -1.35 5.9 6.4 0.952168 0.00337 5.05 16.2
1440 0.0015 25.5 -1.07 3.9 4.4 0.96965 0.00139 3.33 10.7
100
100100100100100100100100
PalosVerdes LF
Project 1Client Palos Verdes LFSample No. VN-3/6By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 1000 4.75 #4 1000 2 #10 1000 1.19 #16 100
0.1 0.595 #30 1000.2 0.297 #50 1000.6 0.15 #100 1002.1 0.075 #200 99
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
67.6208.83
Geologic Associates
Palos Verdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.51n 3/4in 3/8in m3 #30 #100 #200
100 Ii,:,! ',: i, : I,: I, : Ii': : ; , j i I, 1__ I _90 ': ':!' , ' :i i : " , I .! ~ .-! ,'-~
,i:"" ! I , ,80 ,H-L,-C'-i----h---- -"'-'-'--'-',---f-o-f,-f--'---, +---,~__J..+-)-i-'---"-f----+-,--++-h-f--~-H-f---+--'-+
_ ': ' : : i .::,: n IJ: 70 :1 I I I; I I\. __,~ "" ' " , ii' " - *~: '", ' I,:: ,: !\. iiii 60, ill I'" , '\! ,,--- -Q) !:; I I I I 'I I I !,S 50 ,,' '.", ,,-f-'-1-+-+-+'8,..-+.---+i+++,+---U. II' I I I I I 1< ........:'
-:: i i, ' , ,: ! ' , ,,' , , i 1''-~40, "1'..... ,I' -,-~: : : ,:: : I ........ ' '~n, 30 I _ ~~, ': " 't±J20 I "i " , ',' '_, • !_-+-___ ........'~ I _
I I I I i I I I I!! I j
10 ! : ,: .: " ", ::, :: LL' , " :' • --t--o I, I,: , 'I,: i" :, 'i, :1 ' : • iT Tiii I I i I,100 10 1 0,1 0,01 0,001
Grain Size (mm)
B ' / S I Initial Dry I lti 1M' t Test Dry T t M ' t P bilit K U ifl d S 'Ionnq ampe D lt runa OIS, D it es OIS, ermea II y, LL PL PI ru ie 01 D' tlN ensi Y (01) ensi Y (01 ) ( / ) CI escnp Ion
0, (pet) 10 (pcf) 10 em sec ass,
VN-3/6
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088Date 5/19/06
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE. =
Kn =
Time D Temp. dT R R+C KL d (mm R+M % Pass) 30 0.081 23 -1.55 28.8 29.3 0.751993 0.0582 27.75 88.9
40 0.07 23 -1.55 27 27.5 0.787727 0.0514 25.95 83.1
1 0.057 23 -1.55 25 25.5 0.78521 0.0428 23.95 76.7
2 0.041 23 -1.55 23.3 23.8 0.80007 0.0314 22.25 71.3
5 0.026 23 -1.55 21 21.5 0.820175 0.0204 19.95 63.9
15 0.015 23 -1.55 18 18.5 0.846399 0.0121 16.95 54.3
30 0.011 23 -1.55 16.3 16.8 0.861259 0.0091 15.25 48.860 0.0074 23 -1.55 14.3 14.8 0.878741 0.00622 13.25 42.490 0.0061 23 -1.55 13 13.5 0.890105 0.00519 11.95 38.3
250 0.0037 24 -1.35 10 10.5 0.916329 0.00324 9.15 29.31440 0.0015 25.5 -1.07 5.6 6.1 0.95479 0.00137 5.03 16.1
100
100100100100100100100100
PalosVerdes LF
Project 1Client Palos Verdes LFSample No. VN-4/2By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
0.4 4.75 #4 1000.7 2 #10 1001.7 1.19 #16 993.5 0.595 #30 995.5 0.297 #50 987.4 0.15 #100 979 0.075 #200 96
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
44.5242.21
GeoLogic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.5in 3/41n 3/ain #8 #30 #100 #200100 " I ! !, , , , ,
I,, ,
, !, ' t_, , , , , , ,~, ,
90
: :
,:
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: !
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, , , , , <,tn 70
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"
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m 50 _.'+ ". ,c
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, ,
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100 10 1 0.1 0.01 0.001Grain Size (mm)
Boring / SampleInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unified SoliNo.
Density (%) Density(%) (em/sec)
LL PL PIClass.
Description(pet) (pcf)
VN-4/2
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
HYDROMETER
Job No. 2006-088Date 5/19/06
GRAIN SIZE ANALYSIS - ASTM D 422
23.30.956
T AVE. =
Kn =
Time D Temp. dr R R+C KL d (rnrn) R+M % Pass) 30 0.081 23 -1.55 28.5 29 0.754615 0.0584 27.45 87.5
40 0.07 23 -1.55 26.8 27.3 0.769476 0.0515 25.75 82.1
1 0.057 23 -1.55 25 25.5 0.78521 0.0428 23.95 76.3
2 0.041 23 -1.55 22 22.5 0.811434 0.0318 20.95 66.8
5 0.026 23 -1.55 18.4 18.9 0.842902 0.0210 17.35 55.3
15 0.015 23 -1.55 14.2 14.7 . 0.879615 0.0126 13.15 41.9
30 0.011 23 -1.55 12 12.5 0.898846 0.0095 10.95 34.9
60 0.0074 23 -1.55 9.4 9.9 0.921573 0.00652 8.35 26.6
90 0.0061 23 -1.55 8.4 8.9 0.930315 0.00543 7.35 23.4
250 0.0037 24 -1.35 6.7 7.2 0.945175 0.00334 5.85 18.6
1440 0.0015 25.5 -1.07 4.3 4.8 0.966154 0.00139 3.73 11.9
100
100100100100100100100100
PalosVerdes LF
Project 1Client Palos Verdes LFSample No. VN-4/5By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
1.4 4.75 #4 992 2 #10 99
2.4 1.19 #16 993.1 0.595 #30 993.9 0.297 #50 984.8 0.15 #100 986.1 0.075 #200 98
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1350
37.4254.73
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.5in 3f4in 3/8in .. #30 #100 #200100 ;,
;\,1, ! i !I
, , , , ,I"I , I I I
"90I I I ': ! : :
I
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I
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I, 1 I,I , , , , ,I, I
I0100 10 1 0.1 0,01 0.001
Grain Size (mm)
Boring / SampleInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unified SoilDensity Density LL PL PI DescriptionNo,(pcf)
('!o)(pcf)
('!o) (em/sec) Class.
VN-4/5
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088Date 5/25/06
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM D 422
T AVE. = 25.0Kn = 0.94
Time D Temp. dT R R+C KL d (mrn) R+M % Pass) 30 0.081 25 -1.17 29 29.5 0.750245 0.0571 28.33 88.9
40 0.07 25 -1.17 28.6 29.1 0.753741 0.0496 27.93 87.6
1 0.057 25 -1.17 27.8 28.3 0.760734 0.0408 27.13 85.12 0.041 25 -1.17 26.3 26.8 0.773846 0.0298 25.63 80.45 0.026 25 -1.17 24.3 24.8 0.791329 0.0193 23.63 74.1
15 0.015 25 -1.17 22.1' 22.6 0.810559 0.0114 21.43 67.230 0.011 25 -1.17 20.8 21.3 0.821923 0.0085 20.13 63.260 0.0074 25 -1.17 19 19.5 0.837657 0.00583 18.33 57.590 0.0061 25.5 -1.07 18 18.5 0.846399 0.00485 17.43 54.7250 0.0037 26 -0.96 15.1 15.6 0.871748 0.00303 14.64 45.91440 0.0015 23 -1.55 11.3 11.8 0.904965 0.00128 10.25 32.2
100100100100100100100100
100
PalosVerdes LF
Project I Client Palos Verdes IFSample No. VN-5/3By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
2.1 4.75 #4 994 2 #10 98
5.3 1.19 #16 977.9 0.595 #30 9510.2 0.297 #50 9412.6 0.15 #100 9315.9 0.075 #200 91
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1250
44.7172.77
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
.U.S. Standard Sieve Size
3in 1.5in 3/4in 3/8in os #30 #100 #200100
.:,; . ,
':i I " I II
II1Ij I, ,
: : I
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0100 10 1 0.1 0.01 0.001
Grain Size (mm)
Boring / SampleInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unified SoilDensity Density LL PL PI Description
No.(pcf)
(%)(pcf)
(%) (em/sec) Class.
VN-5/3
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088
Date 5/25/06
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM D 422
T AVE. = 25.0Kn = 0.94
Time D Temp. dT R R+C KL d (mm) R+M % Pass) 30 0.081 25 -1.17 28.4 28.9 0.75549 0.0575 27.73 85.9
40 0.07 25 -1.17 27.7 28.2 0.761608 0.0501 27.03 83.81 0.057 25 -1.17 27 27.5 0.767727 0.0411 26.33 81.62 0.041 25 -1.17 25.6 26.1 0.779965 0.0301 24.93 77.35 0.026 25 -1.17 24 24.5 0.793951 0.0194 23.33 72.315 0.015 25 -1.17 21.9 22.4 0.812308 0.0115 21.23 65.830 0.011 25 -1.17 20.8 21.3 0.821923 0.0085 20.13 62.460 0.0074 25 -1.17 19.1 19.6 0.836783 0.00582 18.43 57.190 0.0061 25.5 -1.07 18 18.5 0.846399 0.00485 17.43 54.0250 0.0037 26 -0.96 15.3 15.8 0.87 0.00303 14.84 46.01440 0.0015 23 -1.55 11 11.5 0.907587 0.00128 9.95 30.8
100100100100100100100100
100
PalosVerdes LF
Project 1Client Palos Verdes IFSample No. VN-5/4By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5~' 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 100
1.6 9.52 3/8" 993.3 4.75 #4 986.4 2 #10 968.2 1.19 #16 9511.8 0.595 #30 9315.1 0.297 #50 9218.1 0.15 #100 9021.8 0.075 #200 88
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
125037.8
181.42
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 200&-088
u.s. Standard Sieve Size
'-I-:T;-'T'.·' i "': '-I.-I~Tr!.TTI1l·-\Tn:iI I", j :,' ,I ': ' ; I: : ; ,
I , I , " , l I , , , ", " \ \ I I "
l~r[=~f.·. :T~=~~hl1il=~5~F=:-;~~f[~rI:~:!~·~1 0;0==~l~·2fOO~l~:r~l-~~·l~f~~l f=t·.·#30. #8314'0 31'"
100 _
----;---90 It i: '+l--ii-i-Hi--JiLI-iTid-HTHITJ=[IJI-'180 +1.!:_70 L_
60
50 W+-+-c-f-----+-":-----'---"tT'-'\--i:·40 i-r-t;,-,--,
30 8-H- '--+-++-+'-"'-~iTlll'--r-r20 +-i-iiH+t--~-,-i:-:-!i!TT'10 4-l:,!..LJ+--'--: '!~---;.----; !-nc-;-o
s:0>
~'"III~
~
~
u:ce~~
0.
100 10 1 0.1 0.01 0.001Grain Size (mm)
Boring / Sam pieNo.
Initial DryDensity
(pcf)
Initial Moist.(%)
Test DryDensity
(pet)
Test Moist.(%)
Permeability, K(em/sec)
II Pl PIUnified Soil
Class.Description
VN-5/4
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088Date 5/25106
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM D 422
T AVE. = 25.0Kn = 0.94
Time D Temp. dr R R+C KL d (mm) R+M % Pass) 30 0.081 25 -1.17 22.1 22.6 0.810559 0.0617 21.43 66.6
40 0.07 25 -1.17 21.8 22.3 0.813182 0.0535 21.13 65.6
1 0.057 25 -1.17 21.3 21.8 0.817552 0.0438 20.63 64.1
J 2 0.041 25 -1.17 20.8 21.3 0.821923 0.0317 20.13 62.5
J 5 0.026 25 -1.17 19.3 19.8 0.835035 0.0204 18.63 57.9
J 15 0.015 25 -1.17 17.9 18.4 0.847273 0.0119 17.23 53.5
30 0.011 25 -1.17 16.9 17.4 0.856014 0.0089 16.23 50.460 0.0074 25 -1.17 15.7 16.2 0.866503 0.00603 15.03 46.790 0.0061 25.5 -1.07 14.8 15.3 0.874371 0.00501 14.23 44.2
250 0.0037 26 -0.96 12.4 12.9 0.89535 0.00311 11.94 37.11440 0.0015 23 -1.55 9 9.5 0.92507 0.00130 7.95 24.7
101010100100100100100
100
PalosVerdes LF
Project I Client Palos Verdes IFSample No. VN-5/7By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
1.7 4.75 #4 996.1 2 #10 9716.3 1.19 #16 9138.4 0.595 #30 7945.5 0.297 #50 7552.1 0.15 #100 7259.5 0.075 #200 68
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1250
35.3184.77
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
u.s. Standard Sieve Size
3in 1.5in 314in 318in #. #30 #100 #200100 ,
!, I,:' , i'-----.. II, ! I: I
, ,III I
" ", ,
90 i I:! I: ' ,
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! Io ,100 10 1 0.1 0.01 0.001
Grain Size (mm)
Boring / SampleInitial Dry
Initial Moist.Test Dry
Test Moist. Permeability, K Unified SoilDensity Density LL PL PI Description
No.(pet)
(%)(pcf)
(%) (em/sec) Class.
VN-5/7
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088Date 5/25/06
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM 0422
T AVE. = 25.0Kn = 0.94
Time 0 Temp. dT R R+C KL d (mm) R+Ar % Pass) 30 0.081 25 -1.17 26 26.5 0.776469 0.0591 25.33 79.0
40 0.07 25 -1.17 25.6 26.1 0.779965 0.0513 24.93 77.7
1 0.057 25 -1.17 25 25.5 0.78521 0.0421 24.33 75.9) 2 0.041 25 -1.17 23.9 24.4 0.794825 0.0306 23.23 72.4) 5 0.026 25 -1.17 22.5 23 0.807063 0.0197 21.83 68.1
15 0.015 25 -1.17 20.8 21.3 0.821923 0.0116 20.13 62.830 0.011 25 -1.17 19.6 20.1 0.832413 0.0086 18.93 59.060 0.0074 25 -1.17 18 18.5 0.846399 0.00589 17.33 54.090 0.0061 25.5 -1.07 17 17.5 0.85514 0.00490 16.43 51.2
250 0.0037 26 -0.96 14.6 15.1 0.876119 0.00305 14.14 44.11440 0.0015 23 -1.55 11.1 11.6 0.906713 0.00128 10.05 31.3
100
1010100100100100100100
Palos Verdes LF
Project 1Client Palos Verdes IFSample No. VN-6/3By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 100
3.3 4.75 #4 985.7 2 #10 979.7 1.19 #16 9519.7 0.595 #30 9025.8 0.297 #50 8731 0.15 #100 84
37.1 0.075 #200 81
Total Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
1250
28.1195.16
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422
U.s. Standard Sieve Size
Job # 200&-088
3in 1 Sin 3/4in 3/ain #8 #30 #100 #200100
I,: " i,: l :
,
-+..-U. 1 I .; I I,I -r Ii
, I, I :
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90,I , ._-
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100 10 1 0.1 0.01 0.001Grain Size (mm)
Boring / SampleInitial Dry
Initial Moist.Test Dry
Test Moist. Permeabiiity, Kill I Pl I PI I Unified Soil INo.
Density(%)
Density(%)
Description(pet) (pcf)
(em/sec) Class.
VN-6/3
Geologic Associates
Job # 2006-088
50Dry Weight (g) =
Job No. 2006-088Date 5/25/06
HYDROMETER
GRAIN SIZE ANALYSIS - ASTM D 422
T AVE. = 25.0Kn = 0.94
Time D Temp. dT R R+C KL d (rnm) R+M % Pass) 30 0.081 25 -1.17 30.7 31.2 0.735385 0.0560 30.03 96.2
40 0.07 25 -1.17 30.3 30.8 0.738881 0.0486 29.63 94.9
1 0.057 25 -1.17 29.8 30.3 0.743252 0.0398 29.13 93.32 0.041 25 -1.17 28.8 29.3 0.751993 0.0290 28.13 90.1
5 0.026 25 -1.17 26.8 27.3 0.769476 0.0188 26.13 83.715 0.015 25 -1.17 24.2 24.7 0.792203 0.0112 23.53 75.430 0.011 25 -1.17 22.1 22.6 0.810559 0.0084 21.43 68.7
60 0.0074 25 -1.17 20.1 20.6 0.828042 0.00576 19.43 62.2
90 0.0061 25.5 -1.07 19 19.5 0.837657 0.00480 18.43 59.0250 0.0037 26 -0.96 15.6 16.1 0.867378 0.00302 15.14 48.51440 0.0015 23 -1.55 10.8 11.3 0.909336 0.00128 9.75 31.2
100100100100100100100100
100
PalosVerdes LF
Project / Client Palos Verdes LFSample No. VN-6/5By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 1000 4.75 #4 100
0.4 2 #10 1000.6 1.19 #16 1000.7 0.595 #30 1001 0.297 #50 99
1.6 0.15 #100 . 992.8 0.075 #200 98
Totai Dry Weight- #4Wet Weight
Water Content- #4Dry Weight
125066.1
150.51
GeoLogic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422 Job # 2006-088
U.S. Standard Sieve Size
3in 1.5in 3/4in 3/8in #8 #30 #100 #200
100r"TT,--c---'-~---;-"-----'--"'''-I'''''--''--'--''i''i''"''''''-!=,==;-='lO='==i':::::;<>Q::T'I-,--c--m,ITII-'----'i ':' I I :! : ';~'........ I j 1
90 , ' " ",'" "~ -, I ------,--, I I I I ,I
80 I I I ; I' I I; 1 I-i-+--+-+--+-----iI I! I II : I I I 1
:c :: i I; 1 I I I I I I"" I ' i:
,2' 70 I ' I"! I ' I ' 1- -')'0 , ---,--,--,-----i---~ ':!;I; I'! I ':' ( k>. 60 I I I I I ; 1 !-H-P>I,,'---,--'-__-t-'-__1
'" ,i, ",' " I'~"... I I I I I : I I i I I
~ 50 II I 1 I
u: , , , 'I " , ,I!', ~- , ,!, , I' ,!" " , ' I ','
~ 40 h-': 'I'" !' " " I "~' "'~i----~ , " " ",' , , :8!. 30 i ll ! : ! :
I; ", , "'I', ,!i! ,20 I ! Iii II! I 1 -i-t+t-+-t--:---'--+---1
'! I I i I I I 1 II: ': I I I I : I I I
1: fT,;; ': tl, I, I, I, I ;, ., ; II ',! ' i i ;, I ,-
100 10 1 0,1 0,01 0,001Grain Size {mm}
B ' / S I Inilial Dry I 'I' 1M' 1 Tesl Dry TIM' 1 P bilit K U ifl d S 'Ionng ampe D'I nma OIS, D'I es OIS, ermea II y, LL PL PI ru re 01 D' I'N ensi Y (0/ ) ensI Y (0/ ) ( / ) CI escnp Ion
0, (pet) /0 (pcf) 10 em sec ass,
VN-6/5
Geologic Associales
Job # 2006-088
50
HYDROMETER
Dry Weight (g) =
GRAIN SIZE ANALYSIS - ASTM D 422
Job No. 2006-088Date 5/25/06
T AVE. = 25.0Kn = 0.94
Time D Temp. dT R R+C KL d (mm) R+M % Pass) 30 0.081 25 -1.17 31 31.5 0.732782 0.0558 30.33 97.4
40 0.07 25 -1.17 30.7 31.2 0.735385 0.0484 30.03 98.5
1 0.057 25 -1.17 30.2 30.7 0.739755 0.0396 29.53 94.9
2 0.041 25 -1.17 29.3 29.8 0.747622 0.0288 28.63 92.05 0.026 25 -1.17 27.7 28.2 0.751608 0.0186 27.03 86.815 0.015 25 -1.17 25.1 25.6 0.784336 0.0111 24.43 78.530 0.011 25 -1.17 23.3 23.8 0.80007 0.0083 22.63 72.7
60 0.0074 25 -1.17 21.3 21.8 0.817552 0.00569 20.63 66.3
90 0.0061 25.5 -1.07 20. 20.5 0.828916 0.00475 19.43 62.4
250 0.0037 26 -0.96 16.1 16.6 0.863007 0.00300 15.64 50.2.
1440 0.0015 23 -1.55 11.2 11.7 0.905839 0.00128 10.15 32.6
100100100100100100100100
100
PalosVerdes LF
Project 1Client Palos Verdes LFSample No. VN-6/7
By SE
Sieve Opening Sieve %Weight mm Size Passing
0 76.2 3" 1000 50.8 2" 1000 38.1 1.5" 1000 25.4 1" 1000 19.1 3/4" 1000 12.7 1/2" 1000 9.52 3/8" 1000 4.75 #4 1000 2 #10 100
0.2 1.19 #16 1000.4 0.595 #30 1000.7 0.297 #50 1001 0.15 #100 992 0.075 #200 99
Total Dry Weight 1- #4Wet Weight 250
Water Content 46.2- #4Dry Weight 171
Geologic Associates
PalosVerdes LF GRAIN SIZE ANALYSIS - ASTM D 422
U.S. Standard Sieve Size
Job # 200&-088
3in t.sm 3f4in 3/8in #8 #30 #100 #200
.E'"~'"III~
~
cii:1:~~e,
100 I I ::' • • ',: I,:, 1:11 " I !: J I: -llLW-I-i.-~·:: I~I~\' '-+--L I -mI-Pl90+-!--".L~. _,_+,_+~.J ",: 1-'I' I I ' .••..' '.1 ':I ,~l.'.l '" lTlT
'I:,: i :: :: Ii I: ,'I:' '.;__._.II~_~__U .],.. __:_i_.: .11:: ... , -mil ~80.L~·,~·' ..,·,~~-~~--·,-- I , "11,1"11,: .",1,; IKltl70t..-~.I ·--i-'-.r- ~Iill--~-~-'r+ I
- - : I-IT lij--I!--j"! 'I 'It\···L \ 'I, :1.: 1,'1 I ,.-' ....~, ':: II, 1,_: ---- .. ".--~:!:--;-;----t-r--L--- ;__~:~~-------.-__; :-'---i-~--r--j __ .... __j_ .. _+++-,_.." ' ,, . ,. ':._~:-'--!, : :" " I I I, 1 1 1 "----j I
;.. ': 1:-------:--,-:-1-' II -----.+--.: i .:- III
,: . :: 1:11 ..1,- ~-'----'-~I~;~In-··.'~I; I40 i++-'-I•..•...,.......•.- -r•... ' .. "'''' . '.: '1.: '1"'1--;' i' I '... ~•• fl.. '.1•.. : I•.; I... : ". ' '.' .•.... ' '.' .'. • '. .' • =-i""'.. ','"" , I" I' 1'1' 1'1 'I,', 'i , '.1_' , '1'' II' 'I I, I,: I ,I! ,j I I .L ._'_':--i---'I-------,--,-,,- -T I I' , : '30:':' ~-':'--'" T'·----'I' " , , " • i I . I .: " ttt .20ITI,'i-_j_-~-,i;----1 ..-il--,-I'I+,,!.-,---'I-~;-! "1';."'·", 1-.II'. --'i'H-'I·~·'· I: : : !:; ; .- -- .:----:--' ---~ --'--!.J--{-i-----1----'"~--I-- _:__U __ ?I__; : I !---~-r----i-10 ---I'- .....-~ --'r-- --.- --------p--- -;11 I _.- ~ I: ' ! ' !.r I r : 'I 'I " , I ,i
I r :1 I, t • I ,r I
I r I I 0 01 0.001o 1 0.1 .100 10 Grain Size (mm)
Boring / Sam pieNo.
VN-6/7
Initial DryDensity
(pcf)
Initial Moist.(%)
Test DryDensity
(pet)
Test Moist.(%)
Permeability, K(em/sec)
LL PL PIUnified Soil
Class.Description
Geologic Associates