MEMORANDUM FROM JANET MUSE, USEPA TO JON … · CAS Chemical Abstracts Service ... Reported by Janet Muse Project: 13-0162, Aberdeen Groundwater Volatile Organics Sample ID: ,4CGSTB011713

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road, Athens, Georgia 30605-2700 D.A.R.T. Id: 13-0162

Project: 13-0162, Aberdeen Groundwater- Reported by Janet Muse

4SESD-ASB

MEMORANDUM

March 1,2013

SUBJECT: FINAL Analytical Report

Project: 13-0162, Aberdeen Groundwater

Superfiind Remedial

FROM: Janet Muse

OCS Chemist

THRU: Sallie Hale, Chief

ASB Organic Chemistry Section

TO: Jon Bomholm

Attached are the final results for the analytical groups listed below. These analyses were performed in accordance with the Analytical Support Branch's (ASB) Laboratory Operations and Quality Assurance Manual (ASB LOQAM) found at www.epa.gov/region4/ses(i/asbsop. Any unique project data quality objectives specified in writing by the data requestor have also been incorporated into the data unless otherwise noted in the Report Narrative. Chemistry data have been verified based on the ASB LOQAM specifications and have been qualified by this laboratory if the applicable quality control criteria were not met. Verification is defined in Section 5.2 of the ASB LOQAM. For a listing of specific data qualifiers and explanations, please refer to the Data Qualifier Definitions included in this report. The reported results are accurate within the limits of the method(s) and are representative only of the samples as received by the laboratory.

Analyses Included in this report: Method Used: Accreditations:

Physical Properties (PHYSP)

Physical Properties Volatile Organics (VOA)

Volatile organic compounds

EPA 200.2 (Soil)

EPA 8260C (Soil)

None

ISO

Page I of 38 E130310 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42

http://www.epa.gov/region4/ses(i/asbsop

LFNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division


Project: 13-0162, Aberdeen Groundwater - Reported by Janet Muse

Sample Disposal Policy

Because of the laboratory's limited space for long term sample storage, our policy is to dispose of samples on a periodic schedule. Please note that within 60 days of this memo, the original samples and all sample extracts and/or sample digestates will be disposed of in accordance with applicable regulations. The 60-day sample disposal policy does not apply to criminal samples which are held until the laboratory is notified by the criminal investigators that case development and litigation are complete.

These samples may be held in the laboratory's custody for a longer period of time if you have a special project need. If you wish for the laboratory to hold samples beyond the 60-day period, please contact our Sample Control Coordinator, Debbie Colquitt, by e-mail at Colquitt.Debbiei'ajepa.gov, and provide a reason for holding samples beyond 60 days

cc: Nardina Turner

Page 2 of 38 El30310 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42




SAMPLES INCLUDED IN THIS REPORT


Sample ID

ACGSTB0I1713

SD-OI

SD-02

SD-902

SD-09

Laboratory ID

EI30310-0I

El 30310-08

EI30310-I0

EI30310-I1

E130310-14

Matrix

Trip Blank- Soil

Sediment

Sediment

Sediment

Sediment

Date Collected

I/17/I3 17:15

1/17/13 15:35

1/17/13 15:05

1/17/13 15:05

1/17/13 14:45

Date Received

1/18/13 11

1/18/13 11

1/18/13 11

1/18/13 11

1/18/13 11

32

32

32

32

32

Page 3 of 38 E130310 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42




DATA QUALIFIER DEFINITIONS

U The analyte was not detected at or above the reporting limit.

0-4 MRL elevated due to interferences.

J The identification of the analyte is acceptable; the reported value is an estimate.

0-2 Result greater than MDL but less than MRL.

QC-1 Analyte concentration low in continuing calibration verification standard

OM-6 Matrix Spike Recovery less than 10%

OR-1 MRL verification recovery less than lower control limits.

ACRONYMS AND ABBREVIATIONS

CAS Chemical Abstracts Service Note: Anaiytes with no known CAS identifiers have been assigned codes beginning with "E". the EPA ID as assigned by the EPA Substance Registry System (www.epa.gov/srs), or beginning with "R4-", a unique identifier assigned by the EPA Region 4 laboratory.

1 SO The tesL i f analyzed after June 26, 2012, is accredited under the EPA Region 4 ASB's ISO/1 EC 17025 accreditation issued by ANSI-ASQ National Accreditation Board/ACLASS. Refer to certificate and scope of accreditation AT-1691.

MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero.

MRL Minimum Reporting Limit - Analyte concentration that corresponds to the lowest demonstrated level of acceptable quantitation. The MRL is sample-specific and accounts for preparation weights and volumes, dilutions, and moisture content of soil/sediments.

TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument software's mass spectral library. A calibration standard has not been analyzed to confirm the compound's identification or the estimated concentration reported.


http://www.epa.gov/srs



Project 13-0162, Aberdeen Groundwater - Reported by Janet Muse


Volatile Organics

Sample ID: .4CGSTB011713

Station ID:

Lab ID: E130310-01

Matrix: Trip Blank - Soil

Date Collected: 1/17/13 17:15

./•/.'/.-' (-nits MRI !. 'ri 'p,ir:M

R4-7I56

630-20-d

71-55-6

79-34-5

76-13-1

79-00-5

75-34-3

75-35-4

563-58-6

87-61-6

96-18-4 ,:

120-82-1

IS-63*! 96-12-8

106-93-4

95-, 0-l

107-06-2

78-,S7-S

108-67-8

541-73-1

142-28-9

106-46-7

594-20-7

67-64-1

|l-43-2

108-86-1

74-97-5

(m- and/or p-)Xylene

I 1 I 2-retrachloroelhane

1,1 l-Trichloroethane

I 1 2 2- .•lraL'lll(lroelhant•

l,l,2-T^chloro-l.2.2-Trifûoroethane

(Frcon 113)

I I 2-rriclil()i(Klhdne

I.l-Dichloroethane

I l-DichloriKilxne (l.l-Dichlori)Lllnli.ne) 1.1-Dichioropropene

1.2.3-'rrichloroben/ene

1,2.3-Trichloropropane

1 -2.4- rncl i lorohen/ene

t,2,4-Trimethylbenzene

1.2-Dibri)mo- i-Chloropropane (DBC P)

L2-Dibromoethane (EDB;

1.2-Dichloroben/ene

t.2-Dichloroethane

l.2-Dich!oropropane

1,3,5-Trimeth'ilbciuei

l.3-Dit:hlort)bi.n/Lne

1,3-Dichloropropani

L4-Dii:hlorobcnzene

2,2-Dichloropropanii

Acetone

Benzene

BroirmbL-nzene

Bromochloromethane

1/18/13

I IS i t I - "(.

I IS 13 15 06

1'18/n no6

I ' l R ' H 1 5 0D

I/I8/I3 15:06

1 IS II I ^ IK,

i ' l 8 / I 3 15 05

I IS n I'i IK,

1 18/13 15 06

1 18/13 i'i 06

1 IS I ! 1 1 IK,

1/18/13 15:06

MS n IS 06

1/18/13 15:00

I IS n IS IK,

1/18/13 15:06

1/18/13 15:06

1,'29/13 1 5 2 5

1,''29/13 15:25

1/2<>''13 15:35

1 / : O T 3 (5:25

1,'29/13 15-25

15 25

I 2') I . IS Z-.

1/29'I3 IS 25

l/29'13 \ i2 ' -

1/29/13 13:25

injiin 15:25

15,25

t.''2«13 15:25

0.87 'PPI

r, a-7 I 18'13 0 . 0 / 15 06

EPA 8260C

1I ' . \ 8:60C

EPA S260C

11'. \ s:()Oc

EPA 8260C

i.i'.-\ s:(iOC

t P A 8250C

11'.-\ «:(,(!(•

EPA 8260C

i:l'.\ ,S26I)C

t P A 8260C

1 P \ S 2 I . { ) ( '

L P \ S 2 6 0 C

1 I' \ 8 : 6 0 C '

E P A 8 2 5 0 C

L P . \ 8260C'

E P A 8 2 6 0 C

l . l ' . \ »2ht](-

E P A 8 2 6 0 C

I I ' A s:<)OC

E P A S 2 6 0 C

I p.\ s:6i)C

EPA 8260C

EP.-\ 8260C

' l ^ y , ' EPA 82500

\ \ ' P 1 P \ S2iilK

EP'\82bOC 1 29 13 15 25

Page 5 of38 E130310 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42




Volatile Organics


Sample ID: ACGSTB011713

Station ID:

Lab ID: E130310-0I

Matrix: Trip Blank - Soil


C4.V

Number

J^..\>*SJ'

AnahttAV-i.

l e i i ' ' -f- o-'-vf.fiA

Results' Qualificrs.Ai^^.^'. Units

-'^.'A^f.^ffithiv.' ' ' A A A A

MRI;''. -•Prep'ared .Inalyied.. Mithod

BromodichloroiTiethane ll; ... _,-.„ t.sr. i'r:,..-:>t.z^-.„^«:: Bromoform

0.87 U

1.7 1.1

; Ug/kg dry

ug/kg dry

0.87 1/18/13 = 1506

, T I/I8/I3 l . l 15 06

7,4:-83£9iVi,; : •--. BroiTtometHaneLv'.-^t •A.''A-'A%'A.-&fti J-Sftv^ ;:s:3:S,lf> P M $ ^ ^ 4 H Z i i i : - 'hÂZii

1/29/13 • ,15 2S

1/29/13 15 25

" • M M m i . 1 5 23

.jEPA 8260C

EPA 8250C w^g»S>f t - j ; - Jg i ' ^» ..':.•;' •--tfSjEPA8260C:.'Kl':-;<^. :A,s-a^' ri\. M.r 1:;fr.-f'f,5..'',

Carbon disulfide

,CarbonTetrachloride ' ' % : : '

Chlorobenzene

.Chloroediane

Chloroform

: Chloro'meth'ane'.-f'-%",-!-J

3.5 U

'o.iiu 0.87 1.1

:•. ^p.Ltl

0.87 11

ug/kg dry

--'Ta-; ug/kg dry-..

ug/kg dry

'ug^'g dry" .•';?.

ug/kg dry

3.5

(TsT

0.87

3.5

0.87

1/18/13 15 06

ITfsTiT" ,.I5J36,-

1/18/13 15 uo

I ' lS / lS 15:06

l/IS/13 15 06

-c.-.-, v'i^|tfS7n;j Uiia »a:;i -mMmmz^w t

CIS-1,2-Dtchloroethene 0.87 IJ ug/kg dry A 0-7 1/18/13 0 . 6 / 15 06

>:t<cis-l-y|pichl6ropi'opene,;-,

Cyclohexane

Dibromochioroniethahe ~.h;.

Dibromomethane

'rt.:!jbichlorodifluoromethane (Freon 12) . ' i i ^ a S ^ & f a i f i i - , : . . , * . . . . . . . . . . . . .

Ethyl Benzene

0.87 IJ

0.87 U

0.87 U

0.87 IJ

ug/kg dry

ug/kg dr>'

ug/kg dry

•' r^tipcg'dr^J.;.

ug/kg dry

"0;8Ii^ -•15 OS ! n 0-7 1/18/13 0 - 8 / 15 06

ITI'STB ' „_.!i*" '

~7PPn i/18/Tr 0 . 0 / IS 06 EPA 8250C

iHexachloroDutadiene!:' ? -'-. ?.-. Wc?W>?-0.87'U:i «^ss35Sirn37ST7;" v r .^tr'y?-?r'i!'?.«••'"«-? '• '/iiiiTv'~T?"i'/io7i'i';''-'"-"' ^::i8*-<'°'''-tsyj<i-\3'-' ^#SffV"8/kg<lfy-; #-:? f0:87- i;4iso6J'X-''. -5''rSEPAi8,26oc r-;#^^

Isopropylbenzene 0.87 U

MethyFAcetate

Ug/kg dry

•upig'dry-:

,-, 0-7 1/18/13 0 . 0 / 15 06 EPA 8250C

Methyl Butyl Ketone

Methyl Ethyl Ketone

MeUiyl Isobutyl Ketone

,1634-.04^;, J ^ w i i i - i _ V 'A.

108-87-2

7^3)9-2" '

104-51-8

[Op-PsK-''.

95-49-8

95-47-6

-y--:|!l_ethvl;.T^Butyl -Ether (MTBE), >" „ •

Methylcyclohexane

Me5iylehe_Chloride-

n-Butylbenzene

n-Propylbenzehe-i'* . f

o-Chlorotoluene

,;. - :o-.Xylene '

Page 6 of 38 EI30310 PHYSP VOA FIN/U. 03 01 13 0942 3/1/13 9:42





Volatile Organics

Sample ID: ,4CGSTB011713

Stat ion ID:

Lab ID: E130310-0I

Matr ix : Trip Blank-Soil


. - ^ , * 5 *5-J • - - • • . > 1 - .

,\uiiibei;-y\^ ••; tAiAfi.iilyte-i.j RhiilMpiuiiiifi'erk-A ' ' ' •••^•.i.^'=f:-ai:*',isti.^'z. i '.'i

'..'\;:.l%kA.*4.

( . • m ' r . a « "

- -' ' '-igU . •'.••>.iA'J:t:'-

l|4<^|.:'s.w«/:.f\/voH(.f<;<^;-;^ Ji'!%'i*s., ',' -;,>'; -.Wr/)oT/M=5l%i,w.q

Siii^ ; •, p-Chlof6tdluehe^^.i;^&|,iv"''•§-'•^•^•l i ' ^ • r ' € ,";\t''J^^^ 'riw&^BMMP :.*?sa/29/i3--' I M ^ I ^ V I L

156-60-5

.r006*l^2?5'ij-" ,-r-/:fl'trf.S •'.Atit

79-01-6 apfi-r——— 75r69-4 ^ i i - J

p-lsopropyltoluene

sec-Biityl6enzene ' K * ^ ' .

Styrene -.'-—r'** ?^:^sr—- ..-^.^..^

tert-Biitylbenzene "Ife., '^."^

Tetrachloroethene (Tetrachloroethylenel

T o l u e n l f ' p J : " T i ^ ^ ^ " ' "Tf l

ffans-1.2-Dichloroethene

0 63 J, 0 - 2

87 U-

87 11

87 U

87 LJ

•i^'^ZWs 87 U:;^$a^ffiJi=^;,

0 87 IJ

. ug/kg dry

ug/kg dr>''

ug/kg dry

ug/kg dry

ug/kg dry

ug/kg dry,

ug/kg dry

0.87 l/lS/13 15 06

.AWi'vorr"^''"'^'iîin '-rffi':?.-^?' 15:06 Ai^kiOii^ Ci. .

0.87

- '.H0f-y: 0 . 8 7 ,

l/lS/13 15 116

1/18/13' 15 06

1/18/13 15 06

"T/fs'/lr; 15'06ls

0.87 1/18/13 15 06

l/2i/n I525'

Fl"'S"lT JJtS:25 1/20/13 15 25

't/29/13 ' ' 15.25

1/29/13 15 25

1/29/13'* 15 25^^

1/2Q/I3 15 25

EPA 8260C

EPA,S260C;.:'.; : -.'g

EPA 8200C

EPA"si60C "

EPA 8260C

{EPA S260C - ' p p *

EPA 8260C

75-01-4

' trans''-r,3-Di,chJoropropen'e^-.;v;^y i-'^.,-;*;^*.^^':-:?.--"!

Trichloroethene (Trichloroethylene)

Trichlorofluoromethane (Ffeqn4.!);"i'

Vinvl chloride

0.87

'vgf;. 1/29/13 i " '^^ 15.-25=1

l 'EPAS2MG-'-U^p^

EPA 8260C

EPA 8250C;-r

EPA 8260C

Tentatively Identified Coinpounds:

^?»^' iT ' •

R4i:0000 .Tentatively'Identified .e6mpouii,ds;a&:' ^?Stt:'S ..iiig/kg drv i20* 1/18/13. •-;,ai/;9/l3 15:06 • S;:frmi3:2S EPAI8260C -

Page 7 of 38 EI30310 PHYSP VOA f W A L 03 01 13 0942 3/1/13 9:42





Physical Properties

Sample ID: ACGSTB011713

Station ID:


Lab ID: E130310-0I

Matrix: Trip Blank-Soil

.CAS, Number- -:• •.-.':• .Atiulyle

'~'*=.hi- '

-:ma»a ii-.f^mB^Mf'ti *•'•''-mesutt&Quiilific'rsAv . . ' -.i Units v •jM'RifSrreiiii7ed': AiialyAizd IMethSd'SP. - - - ,i-!t

f,tmÂ<'A>r-'-.':.- •. •••: "• :,-as'^.'k"> i:-:XX i.. >,;•• "'-ty.^. l-!':A-- • •' .i -f -z--' i-K-'iii^.lr':- - ---•:Li^,:^;^Wxfl;fe"?v;':^.'-.a'.v'-.'i- ;.v-..s--<.tf?fes^^.'j-jt?v-<,r^-•. • • c ^:.-a;gy.jiC«' v^..s:s:

Page 8 of 38 EI303I0 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42

4, -J • H





Volatile Organics

Sample ID: SD-01

Station ID: SW-01


Lab ID: El30310-08

Matrix: Sediment

( i \

Nunil'er -•iHKnte • ' s u l h * •"! I I " r\

R4-7156

630-20-6

71-55-6

79-34-5

76-13-1

79-00-5

75-34-3

75-3.5-4

563-S8-6

87-61-6

96-18-4

120-82-1

95-63-6

96-12-8

106-93-4

95-50-1

107-06-2

78-87-5

Si08-67-8

541-73-1

142-28-9

106-46-7

594-20-7

67-64-1

71-43-2

108-86-1

74-97-5

(m-and/or p-)Xylene

LI.I .2- rctrachloroelhane

1,1.1 -Trichloroethane

1.1.2.2- rctrachloroelhane

t, 1,2-Trichloro-1 2,2-Trifluoroethane (Freon 113)

l.l .2-rnchlorocthane

1,1-Dichloroethane ,,

I, I-Dichloroethene (l.l-Dichlor(>clh\lone) 1,1 -Dichioropropene

1.2.3- Tnchlorobenzcne

1.2.3-I'richloropropane

1.2.4- Irichlorobcn/.cnc

1,2,4-'rrimethy Ibenzcne

1.2-i:)ibronio-3-Chloropropane (DBCP)

t ,2-Dibromoethane (EDB)

1.2-Dichlor(jbcn/cne

l,2-Dichloroethane|

1.2-nichloropropane

1,3.5-Trimeth\ Ibenzene

I .j-Dichltjrohcn/onc

t,3-Dichloropropan!

1.4-Dichlorobcnzene

2,2-Dichloropro]

'\cclonc

Benzene

Bromobcn/cne

Bromochloromethane

ug/kg dry

ug/kg dr\

ug/kg do'

U12 kg dr\

ug/kg dry

ug/kg dr\

Ug/kg diy

ug/'kg dry

ug/kg diy

ug/kg dr\

Ug/kg dry

ug/kg dr\

ug/kg dry

ug'kg dn.

ug/kg dry

ug/kg dp.

Ug/kg dry

ug/kg dry

ug/kg dry

83

4 2

4.2

42

4.2

42

42

4 2

4.2

42

4.2

42

92

8 3

4.2

42

4.2

42

42

42

4.2

42

4.2

no

42

42

42

1 1813 15 09

1 Is 1

1-'18/13 15:09

1 1 S 1 '-]S ll»

1/18/1; 1509

I' IS, 1.1 IS U')

1 /H/ t J 15.09

1 IS 1 1 IS 1,0

1/I8,'13 15:09

I Is 1.' 1 s 110

I/IS/LI 15:09

1 IS j I | S i l . l

I ' l S ' l J 15 09

1 IS M 1 S I IV

1/18/13 15:09

1 1 S 1.1 |S r,o

1/18/13 IS 09

M S 1 ! 1

l i s t ) IS o t

M S I 1

1/18/13 15:09

1 IS 1 I | s llO

1/18/13 15:09

1 IS n

1 18 H 15 09

1 IS n 1 S 1)1)

1/18.13 IS 09

1 29 13 15 51

1 " 1 15 51

1,-'29/13 15:51

2" 1 '. | S .s

1.'29/13 15:51

1 -'1 1.!

1.129/13 15-51

1 2'') \ : |S .M

I.'29/13 15:51

1 2" 13 IS .M

1/29/13 15.51

1 2') M IS Sl

1/29/13 15:31

! 2'' M | S S l

1,-'29/13 15:51

1 2') l.i

1/29/13 15:51

1 2'/ 1 ! 1 1

1 20 H IS 51

1 1 I 1

l/'29/13 15:51

1 2') 1.! IS SI

1,'29/13 i.5:51

1 I'-l L! M M

[ 29/13

1/29/13 15 51

1/20/13 15 51

1PA8250C

I P \ s ^ 6 n [ '

EPA S250C

1 p . \ s ; i . i i t

EPA 8 2 ^

l 'l>.\ S 2 6 0 C

EP./ S260C

i - | ' - \ S2hO(

EPA 8260C

i:P.-\ 82(.0(

EPA 8260C

1 P . \ X.?(.IK

EPA 8260C

I:P.\S;(,IK

EPA S260C

11'.\ x:i)i)c

EPA 8260C

I:P.\ s:(>oi

EFA 8260C

LPA s onc

EPA 8260C

I ' P . \ S 2 6 0 t

EPA S260C

r p \ S2f.n(

LP'\8260C

EP \ S2i,»C

LPA 8260C

Page 9 of 38 El30310 PHYSP VOA FfNAL 03 01 13 0942 3/1/13 9:42





Volatile Organics

Sample ID: SD-01

Stat ion ID: SW-01


L a b I D : E 1 3 0 3 1 0 - 0 8

M a t r i x : Sediment

^llllll T I..- '{, wit\ 0!ii!li!tei-\ Units ^llll Pte{xii-eil •tf Skthod

75-27-4 Bromodichloromethane

75 2i 2 Bromolorni

74-83-9 Bromometh:

75-15-0 Carbon disultlde

56-23-5 Carbon Tetrachloride

108-90-7 t hloiolxn/cnc

7S-00-3 ( hloroelliane

6 7 (-•tl 5 C h l n r t i t o i n i

74-87-3 Chlorometh

156-59-2 CIS-1 2-Dichloroethene

10061-01-5 cis-l,3-Dichloropropene

110-82-^ Csclohcxanc

124-48-1 Dibrtmochloromethane

74-95-3 Dibromomethane

75-71-8 Dichlorodifluoromethane (Freon 12)

100-41-4 Llhyl BcO/'cnc

He.xachlorobutadiei

98-82-8 lsopropvlbon>'cnc

79-20-9 Methyl Acetate

591-78-6 Methyl Butyl ketone

78-93-3 Methvl Ethyl Ketone

108-10-1 .VIctlnl IsobtiKl Ketone

1634-04-4 Methyl T-Butyl Ether (MTBE)

108-87-2 \lethvlcvcloho\ane

75-09-2 Methylene Chloride

104-51-8 n-But\lbcn/cne

il03-65-l n-Propylbenêne

95-49-8 O-L hlorotoliiciie

95-47-6 o-Xylene

l/IS/13 15:09

M S 1 * IS I)»

1/18/13 15:09

1 1 S l i S 0 0

1 18'13 15 09

1/29/11 15:51

1 2') l.i |S sl

i/29/13 15:51

2'J 1 3 IS Sl

129 n IS 5 |

M S I . I M P I ' M 1 ^|

1 18 1! 15 09

I 29 13 I j 51

M S I I ' r | M ' ) M

1 18 11 15 09

M S I , M IK)

1'18/I3 15 09

M S n 1 o )

1 IS'13 15 09

1 I8 ' I3 IS 09

15 09

l/'29 11 13 51

1/29/13 15 51

15 51

1 2) n 1 ^1

1 2 9 ' n

15 51

1 29 n 15 51

1 29-11 15 S|

1 18/13 1/29/13 1509 1551

1 \iMBBK^^m 1509 1551

M s l \ -- \^ l - I M -1

1 18,11 15 09

M S 11 IS IK)

1 18/13 15 09

1 20 11 15 51

1 20 n IS S|

1'29/1< 15 51

M S I , 1 1 IS 110 1 1

1/18/13 15:09

1 2 9 13 1551

11S 1.! 1 11 ISiio 1 M

1-'18/13 15:09

129 '13 1551

M S n 1 ) 1 IS IK) I 1

1/18/IS 13:09

1 19 13 15 SI

1 1 S; H 1 1 IS 1)1) 1 1

l / l S ' i l 1509

1 29 n 1351

EPA 82«)C

I P.A S:i,lK

EPA S260C

PPA 8260C

EPAS260C

I P \ 521 IK

tP\8260C

1 p \ s:(.i)(

LP \ 826fJC

EP\ s:<)(i(

EPA 82B0C

I p \ s:i)()(

IPA8250C

I p \ s:()ii(

r-PAS26IK

i-p\ 8:()0c

EPA 8250C

1 P \ S2()l)(

EPA 8260C

1 P \ 82(ilK

rP\8260C

1 p \ s;<iix

tPA 8260C

1 p \ 8:6u('

EPA 8260C

1 P \ S2i.0('

I P V 8250C

I i'\«.?i,IIC

EPA 8260C

Page 10 of 38 E I 3 0 3 1 0 PHYSP V O A FINAL 03 01 13 0942 3/1/13 9:42





Volatile Organics

Sample ID: SD-01

Station ID: SW-01

Lab ID: E130310-08

Matrix: Sediment


,<t.i I lieiiills OmitiAen 't-IRL M.-rftcd

106-43-4 p-Chlorotoluene.

99-87-6 p-lsoprop\ llolucnc

135-98-8 sec-Butylbenzene: j

100-42-5 SKrcnc

98-06-6 tert-Butylbenzene

127-18-4 rcirachlorocthcnc (letrachlorocths lene)

108-813^ Toluene

15(1-60-5 trans-1.2-DichlorocllK'ne

10()61 -02-6 trans-1,3-Dichloropropei

79-01-6 rnchlorociheno (Trichloroethylene)

75-69-4 Trichlorofluoromethane (Freon 11)

75-01-4 Vinvl chloride

4.2

4.2

4.2

I IS 13 IS 09

1 18/13 15 09

4.2

42

42

42

42

42

42

4.2

4.2

IS ilO

1 18 n 15 09

IS n IS )9

1 18/13 15 09

1 IS 1 1

1 1813 1509

Is 1

1/18/13 15:09

118,13 15:09

1 29 n 15 51

1 29 13 1531

I 19 13 l « s |

I 1 I IS SI

1 29)13 15 SI

1 2 0 1 ' 1551

1/29/13 15.51

1,29/13 1551

EPA 826flC

I PA S2(,I)C

EPA 8260C

i:PAx2(>()t'

1P\S260C

I l> \ S2()IK

tP\8250C

I P \ s'oiit

FPis. 8260C

PI A s:oiic'

EPA 8260C

EPA 8260C

Tentatively Identified Compounds:

R4-0000 Tentatively Identified Compounds 8011 ug/kg dry 80 1/18/13 \mm EPA 8260C

Page 11 of 38 E130310 PHYSP VOA FIN/\L 03 01 13 0942 3/1/13 9:42




Physical Properties


Sample ID: SD-01

Station ID: SW-01

Lab I D : El30310-08

Matrix: Sediment


/:;4,S' Number

'APi. .Ani'ilyti!.;,-:';r.

A^'p^lippAiWA-pResulis fQuul'lflei's

••WfAA . ' :' •}.'.:'i)^-A. , j /,:-.-'- - \- - - ' K ^ : ? ' '

l'nits '-ATlAplRI. Prepared -InaiKed .Method- 'AAA-AA: •

E1642941 "/oSolidsj- i^pmmmmm. »M,: 1/29/13

iA:2\ 1/30/13 ppX r^v-,-Vi--.H..-. 15:23 : EPA'?,QBIwyi:'


UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

Region 4 Science and Ecosystem Support Division

980 College Station Road, Athens, Georgia 30605-2700

D.A.R.T. Id: 13-0162 Project: 13-0162, Aberdeen Groundwater - Reported by Janet Muse


Volatile Organics

Sample ID: SD-02

Station ID: SW-02

Lab ID: E130310-10

Matrix: Sediment







Volatile Organics

Sample ID: SD-02

Station ID: SW-02

Lab ID: E130310-10

Matr ix : Sediment


0 \Stimber AmtlyU" Results Qualifiers Units MRL : Prepared ,,, Aiiitiy.zed .Method

75^27-4 :-. .-Bromodichloromelhane

75-25-2 Brotnoform

74';83-9 ':,-.-. 'Bromomethane.. f..:-.

75-15-0 Carbon disulfide

56-23-^.^-,l:,1-- ^rtxHiTetrachlorid^l^.--,

108-90-7 Chlorobenzene

75-00-3 'H • , Chloroethane ' - V ; /

67-66-3 Chloroform

74-87-3.;;'•• Ch^methane ' •• ? ' ) P '

156-59-2 cis-1.2-Dichloroethene

•10061-01-5 • cis-1 ,®ichtotoptflpene ' ' r t W •i::: ;.;••-•.. -Ammm::: :A. ' ; . . . . . . A - I .

110-82-7 Cyclohexane

124-48-1 ' J :;Dibn}inocK16rpriiethane

74-95-3 Dibromomethane

75-71-8;- Dichlorodifluororhethane (Freon 12)

100-41-4 EthylBenzene

87-68-3 i Hexachlorobutadiene :,: A p i

98-82-8 Isopropylbenzene

79-20-9 . . Metpfl-caftate - '"'-•,

591-78-6 Methyl Butyl Ketone

78-93-3.' ••• 's i ' l^MethyiTîcistone

108-10-1 Methvl Isobuu'l Ketone

WA:

':'':AA

163i^04| | |p j ' ; t ivjoihyl T-Butyl :Ether (MTBE)

Methvlcyclohexane ;yt

108-87-2

75-09-2 'A Methylene Chlonde

104-51-8 n-Butylbenzene

103-65-1 n-tôpyibenzene

95-49-8 o-Chlorotoluene

? ® K 6 ^ i . :.f • , r ; . S o - X y l e n 3 j ^ :

: 0.52 U

1.0 1!

V-ip\j . 2.1 U

] • 0',52 IJ

0.52 11

Z%\ u 0.52 U

' "'oWZ: 0.52 U

o.yiZZJ.i 0.52 U

0.52 U

0.52 Ll

" 0.52 U

0.52 U

'-^0.52 1]

0.52 U

1.0 Ll

1.0 u

0.52 u " " ^ I

0.52 U

, 0 . 5 2 U

0.52 IJ

-ÔMdJ,

0.52 U

a^Hji;

ug/kg dry

ug/kg dry

ug/kg diy

ug/kg dry

ug/kg dry

ttg/kg dry

ug/kg dry

ug/kg dry

ug/kg dry

ug/kg dry

• ug/kg,dty

ug/kg dr>'

!:: ^ P , i^'tig/i^'diy ?v::

ug/kg dry

ug/kg dry • '

tig/kg dry

ug/kg dry

ug/kg dp,'

ug/kg dry

ug/kg dry

,. ug/kg dry

ug/kg dry

M , . - - . M;ug/ifgfijy-'

ug/kg dr\'

ug/kg dry "•;•

ttg/kg dry

ug/kg dry

ug/kg dry

:,,, ug/kg dry

0.52

1.0

\ 2.1

2.1

0.52 ••-

0.52

2.1

0.52

0.52 ;

0.52

0.52

0.52

0.52

0.52

^;^HJ.52,

0.52

;o.52 ;•:

0.52

1.0

1.0

4.1

1.0

0.52

0.52

0.52

0.52

' vflj52 ;

0.52

'''Tallii

1/18/13 15:15

1/18/13 15.1i

l/IS/13 15 15

' l ' / l 8 / i 3 ' 15 15

I /I8.I3 |5 15

1/18/13. 15-15

I / I8/I1 15 15

l / l 8 / i 3 15:15

1/18/13 15 15

l / lS/13 15:15

1/18/13 15.15

1/18/13 15:15

l/IS/13 15 15

:i/l'8/li' -' ' 5 ; ' - ^ I / I8/I3

15 15

''1>1S/T3'', - 15:15?

i.ns/u: i 5 . i i : ' i

1/18/13 15:1} ,

l/l 8; 13 15 15

1/18/13 15:15

l / ia/13 15 IS

1/18/13 1 5 J 5 -

r/18/13 15 15

1/18/13 ,15-15

I / I8 ' I3 15:15

•îjiixi. toSlSii

::\a9l\i-' J, ; . '? ' ! , ' ' • - '

1/29/13 16 17

'':i7isi/iyi^ • ' l 16.17

i ' : « i3 16 17

~ . A m i ; ' * • ' ? ~ 1/29/13 16 17

" \l'2<)'!\3

.'- ' S J ^ 1.29/13 1617

EPA 82600; : ;

EPA 8260C

E P A 8 2 6 0 C ^ ^ P ^ ' '

EPA 8260C

E P A 8 2 6 0 C B S J ; -

EPA 8260C

EPA 8260CftftS;. .:-.2:Mi^::..;::-j.:..

EPA 8260C

| i | ^ | P A 8 2 6 0 ^

p-pP EPA8260C tHAoxiW^ •'•-••: '-• •:im:S:.

.ISii 1/29/13

E P A 8 2 6 0 C 16:17

A'^J. iÊR^8260C-CWi:'

E P A 8 2 5 0 C 1/29'! 3 lo 17

1/29/13 16:17

1;:9/|3 16 17

I'1/29/13 ii l,&17

1/29/11 16 17

1/29/13 ; 16-17

1/29/13 16 17

-T':'I/29/13 j,US:17

I'29/13 16 17

' W 9 / i 3 16-17'.,

1/29/13 16:17

EPA 8260C

EPA 8260C

EPA826iDC

EPA 8250C

EPA426J)C

. . ::..k.. EPA 8260C

EPA82()ix;..

EPA 8260C

EPA8260Ci

EPA 8260C

P P P EPA 8260C

:-EPA8260C

1/29/13 !6:17

EPA 8260C

E P A : 8 2 6 0 C

Page 14 o f 3 8 El30310 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42




D.A.R.T. Id: 13-0162


Project: 13-0162, Aberdeen Groundwate r

Volatile Organics

Sample ID: SD-02

Station ID: SW-02

Lab ID: E130310-10

Matrix: Sediment


6:4 .V Another

106-43-4

99-87-6

135-98-8

100-42-5

98-06-6 :

127-18-4

108-88-3

1 56-60-5

10061-02-6

79-01-6

75-69wlM,,::,

75-01-4

Tentatively

114-0000

, tt!ii>]-!i; R

p-ChlorotoIuene

p-lsoprop\ Itoluene

s e c - B u t y J ^ ^ ^ ^ ^ ^ H H B j ^ ^ ^ ^ ^ ^ ^ H I K ^

Sl\ rcne

tert-Butylbenzene f H | H H H H | | | H H B

Iclrachloroethene (Tctrachloroethv lene)

Toluene -^mm^^mmmm^

trans-1.2-Dichloroc'thene

trans- i ,3-Dichloropropene fl^^^^^^^^^^K

Trichloronuoromethane (Freon It) ^ ^ ^ ^ ^ H P

Vinyl chloride

Identified C o m p o u n d s :

Tentatively Identified Compounds

';suiis i

0.52 1,1

0 52 1 !

0 52 n

0 52 1

0.52 1'

0 52 i

0.52 11

0,52 I

0.52 i 1

f l •^•^ i

0 52 U

0.52 U

10 n

ûAifie^s (:iiits

ug/kg dry

ug/kg dp.'

^ ^ j j j j j j j j j j j j ^ ^ d r y ug/kg dr\

IBHHHR'^s'^''^' ug/kg dry

' ^ H ^ H U K K T ' ^ ^ dry ug/kg dp.'

^ • • • • • • ^ g / k g dry g-2 ug/kg dry

j m ^ ^ S d r y ug/kg dry

ug/kg dry

M R L

0.52

0,52

0.52

0,52

0.52

0,52

0.52

0,52

0.52

0.52

0.52

0.52

10

!'n-p-.i:-. -/

1 18 n 15 |S

M S I , Is

1 IS 13 15 Is

M S I , MM

I'lS 11 15 | s

M S I , M 1-

1 18,13 15 15

M S I , M l>

1 18,13 15 15

1 IS 11 IS IS

1 18 13 15 15

1 18 13 15 15

!/t8/l'3 15 15

1 29 | , If. 17

1 ll r

I 29 13 16 17

1 1 r

1 29 11 l o l 7

1 2 / 1 , 1' n

i/io 13 16 17

1 2 ' 1 ,

r I 20/11 16 17

1/29/13 16 17

thm 15 17 1 29 13 16 17

' V » l \ 3 16-17

if

I P \ 8260C

1 p \ s:i,i)i'

1 P \ 8260C

1 i' \ s2i>oc:

E P y 8 2 f i M H H H |

1 P \ 8 2 6 n r

EPA8260C

r P \ 8 2 6 0 C

EPA 8260C

EPA 8260C

EPA 8260C

EPA S260C

EPA 8260C



980 College Station Road, Athens; Georgia 30605-2700 D.A.R.T. Id: 13-0162


Physical Properties


Sample ID: SD-02

Station ID: SW-02

Lab ID: E130310-10

Matrix: Sediment

Date Collected: 1/17/13

C A 0 ^ ^ • Z ' - - ' Numlter -^pA-fj- ...Aniilyt'e'i 1;

-• ViiJ.Cy ':•%:"- • 'Ar

15:05

''MP<P'P-'' •' P P Z " : "A

: 'i Z < Z i P : \ •• M ';: ; :R'eflilts •• Qiiatifiers

VApp ' '' '•'pp Units 'Pi . -MTiL Prepared

y ^ - f . 4 / ! ' - ' - ' • - • ' M ; ; =. '; ;

'.iîiitlyzed .Methiid. g ^

' " .E! 64294??; - ^ y o Solids'll-,

•::--r~. r j j r | r - 7 - • "" '^Z. '" " ZZ ^ ' - ™ - - ...-fr.-..

. -i'OJi) . 1/29/13 14 21

T'4/3b7i3 :'=.'-• 1,5 2 3

EPA 206.2 -





D.A.R.T. Id: 13-0162


Project: 13-0162, Aberdeen Groundwate r

Volatile Organics

Sample ID: SD-902

Stat ion ID: SW-02

Lab ID: E130310-1I

Mat r ix : Sediment


('4.V,, .,

.'•iilntber . - • ^ • • ^ : ^ ^ ^

Anti/i-tellff

' ' 'i-7';*Ss*c-^r^r . • = •^'•A)[4^-f'-'.'-'.

Re.sults - Quiilifiersj WS':* -' - Unifi MRL "• ••-. Prepared t/ialy-i-d Method i 'if:-

R 4 7 ^ ^ p ^ f n i t a ^ ^ l ^ Y i e n e - ^ f y b i ; ; ^ , '

1.1.1,2-Tetrachloroethane 630-20-6 'hi^^z.:-: . . . .u:

'(?ÎV . E P A ^ 2 ^ S j

71-55;6>a^.>;%K:"l,l{l-TftchloroeUiaiiej ^^.!tg;t^}H ^ i ' v.-''^p a^,.:„.<.'rM.;&.;^:^s£iAU„.'r.a , iT, 7..S!!SSiiti!::.;:::u.:.a..imA&M±JiisA.S,:-AJ... 79-34-5 1.1.2,2-Tetrachloroethane

ug/kg dry'.i":i^?.-r.-0.9,

0.46 U ug/kg drs' 0.46

iu.,ia->-:u;a. f3iSj: ,x:r'/';f-WA>-s¥,-rs-. -,i-r''.'.i.--.'?'t,' -, p,i,S-r,iiA:z...i..,..i:'.si?2iy2;.ii_j>ca.&:ii,».;

1/18/13 15 20

1/29/13 16 43

0.46 IJ ug/kg dry 0.46 1/18/13 15 20

1/29/13 16 43

76rf3?i;=-rj!E r;.tsîtl.2;Trichlor6-'H2.2JTrinuor6ethaneBr5'«;:'-. % A-i ; '•••.^'•.^%--t-9'-''='^^.tf(îlftTi;3i^^'-^^'i:3<S*.^';'''^ ;^y»^K•-:-^ '••'1'--t

EPA 8260C

75-35-4 I, I-Dichloroethene

(I. I-Dichloroethylene)

•563-5S'-i5f ' 'fl^;:l,l-Dichioropropene

87-61-6 1,2.3-Trichlorobenzene

16-18-4 .,li^2;3-Trichioro|romite Sii- ': iSsi-;-,.. ,. ..'.'..*.'-:-.. 120-82-1 1.2.4-Triclilorobenzene

1,2;4|Trirnethylt)enzeiie/

0.46 U tigAigdrv' 0.46 " P ' P p P P EPA 82bOC

0.46 IJ ug/kg dry 0.46 I / I8/I3 15 20

1/29/13 1641

95^3-6 ... , |^: |

96-12-8 l,2-Dibromo-3-Chloropropane(DBCP)'

•mAAAWA-mfr-: "J6^93iP'M*i: 1.2-Dibroftioethane(EDB):/

95-50-1 1.2-Dichlorobenzene

10.46 U

0.46 U

;jb:46 U

0.46 U

0.92 U

0 . 4 6 ^

0.46 IJ

0 . 4 6 ' . W » * s r -

• , f ^ J ^ ^ ^ , ' - u g / k g dry'

ug/kg dry

^ ^ ^ P 5 : T P T - > T * . ^

-.y- 0 . 4 6 ^ ^ ^ ,5.;ci -,<!>; ,6,43

0.46

; - ^ u g / | t g d r y

ug/kg dry ^ " - T ^ > T ^ " - ^ ' " '

• ^ J g ^ d r y

tig/kg dry

itg/kg;dry s,^

I / I8/I3 15 20

n Af. - : ^ " I / I 8 / I 3

0.46 -.f-; 15:20 1/18/13

15 20 0.46

0.46. .M:M 15:20 . ; . i . . :^J&Sd.^.-. . .-

0.92 AA ),A'AAA3Wvy:

0.46 - ;;i5;:o.:

I / I8/I3 15:20

1,2-Dichloropropane

l 0 8 ^ 6 7 l 8 ' ; ; S l T S ^ 3 5 | T r i r n e ^ S i S h ? ' - " " ^ S ; " - ' • • ' aa-fls„.,rri-,.,.-y , --r: fra.t;, '5:r;,' •A f ,mit.r..-X •xi Mx iJz,. V%

EPA8260C

EPA 8,260c

EPA 8250C

EPAS260C

EPA 8260C • • • " • w m f i : : :

EPA 8260<5i(h:: .-, / EaMS',:^

EPA 8260C

„,jilS?!M 1/29/13 16 43

1/29/13 1643

"1/29/13 -16.43

1/29/13 16 43

''WiShr-' ' ^ M u .

1/29/13 10-43

EPA 8260C

''^3|;s'itEPA 8260C':

0.46 Ll EPA 8260C

i/:»/i3-.Ji';

541-73-1 1,3-Dichlorobenzene

l42-2S;?':;.^.*-s|ilU-Dichl'OTOprdpah'el^;rJ';-.;C ^ ^ ^ -'i^ / >

0.46 U ugflcgdry 0.46 'I's'sn P P P E P A 8 2 6 0 C rp j , - , . ^k^nimAÂTmA- -A.

106-46-7 1,4-Dichlorobenzene -rpsff-.. .. ^x.. i,'ii' ^"v—vi!t'':'*r " '20-7-''-'-'-="TT>'-""'7;ni6 594-20-7-:'/*,;:> •,2,2-Djchloropropane4!"i. •

:^M^lM..:.M iisS:,i,-,',: .-, „.. .na^mir^. 67-64-1 Acetone I / I8/I3

15:20 16,43 EPA 8260C

71-43-2^

108-86-1

^ - 9 7 - 5 &i:-: i-

Benzeiie; ^^^"'

Bromobenzene

:':|Brom6cliloromethane

0.46 U ugflcg dry 0.46 "I'/jo" P P n EPA 82bOC

r7T7is/T3;.^j 'm^-^:^mMAZî''%^mp^Z..:-'-mk'i--• j S l ^ S i l I 8 U , J, Q C - I , ug/kg dry IS

QR- l

',0:4(5 U '

0.46 U

'^®;;: ug/kg dry

g g / k g dry

0.46

fo-He-

1/18/13-1

Xi'p: I I/I8/L1

15 20

1/7893" IT; 1 5 : 2 0 - ; : '

' l f«^ -2 ;EPAJ260C-

" p ' P EPA 8250C

. 1 6 43 •E,f;^^8260e

Page 17 of 38 E1303I0 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42





Volatile Organics

Sample ID: SD-902

Stat ion ID: SW-02

Lab ID: E130310-I1

Matr ix : .Sediment


<.'4.V-,

Number .Annh-le-J't-'' .. X: •-'-t-'^-'-- f:;-

si 1 p;. Results- Qualifiers ,-l.:lJnih-. iMRL, "• Prepared'A,AiwJ-tzed Meih'itdX

ii-2rm 75-25-2

Bromodichloromethane.' i-; ^lisa^.ula.î^'ata^':;...-Bromofomi

i i S ; i » 01.46 U : .j ;*ug)Tvg dry'i' 0.46 1/18/13, ;m;!r/29;13 1..i:::2^:ALP^Jfi:^. . . ^ P P * - ^ ^ '

74r'83=9K' *'^"..-..—....;* ^4 ';i^; -'. "^ i"^^^î* '^^^- ' ' i* ;T ' :»> Bromoniethane;j^^K.fe/;r-t'".

75-15-0 Carbon disulfide

5,6-23Bj^;!g/,';;f.^^^^^^|ilmdl^^^^ ^ .A PP^

108-90-7 Chlorobenzene

0 .92 U UgAg dry 0 .92 •""'"'"'^s^^lTSTP^^jî^•-'•••^vJ—r-??r?-r^^'^'•:••"-vjjit^'^-,.Ji*""."./"/'" I'-i—^r*'^,

A^:î^mPMZîAij.'Z-'I}^^^Zz./ ..^:^Z 1.8 U ugrt:gdry I

75-00-3: •trhloroethane," •,:^--JA»iX. f-..-:

67-66-3 Chloroform

Chloromethane'. A':^-%:

j^'lS3pji6^1Mllfe&ii:ll!ig!^ :^^';Z^^'SM% 0.46 U ugrtcgdry 0.46 ",Pô ' [ V A ? EPA 8260C

^zSzl^^^^^MMzMl!mSlEz 0 4 6 U ug/kg dry 0.46 75 :'o "ifi'i EPA 8260C

' T F','??s^-E^-r:-r'r—t-:

:.' ' ' ' .•;!'«l>-.! r

cis-1.2-Dichloroethene

Scisr,l-,3-Dichloropropene-S'^Sp"''' • # ^ ^ ^ ; j : , , • -....^ ;„J.,^2.2Î:^^:i^,

Cyclohexane •--:ss^^:- ^^-r^-' • •• - --•' -T .:?sf: .

Dibrornochlpromethane ,• •'iAfiM

Dibromomethane

Dichldrodifludfoinethane (Freon 12)

Ethyl Benzene .

He.xachIorobutadiefl'e'l-Ci--f|;''i-

j ^ o ^ 6 U : : ; -

0.46 Ll

:P%6\PpZ.

— ^ — . t M:.„Sii:.,siitntii)ifM:,n,!iti:',»iiinViiiri C ~ ' ~- " ^ - ••-^:-* -^ - -

0.46 IJ

98-82-8

•r-is-

ug/kg dry

•ug/kg dry

ug/kg dry

ug/kg dry

ug/kg dry

ug/kg dry

ttg/kg dry

0.46

0.45 '

0.46

0.46

0.46

0.46_

0.46

1/18/13 15-20

• 1/187 i fT 15.20ji

1/18/13 15 20

""1/18/13" t5:20

1 IS/13 15 20

1/18/13 ' 15-20

1/18/13 15 20

1/29/13 1643

•M/29/13

J '*•'?:' 1/29/13 1641

"i/*29/13 1,6.«

1,29/13 16 43

' u'iihr'. 16.43 /

1/29/13 16 43

r^ | |ug/kg^;^ iJ | ( ) .46 ,y ' i^M. ug/kg dry 0.46 1/18/13

15 20

•l.'2< • ; 1 6 : 4 3 ^

1/29/13 16,43

EPA 8260C

EPA «2"a}C,

EPA 8260C

EPA S260"C-;.;j;:"'

EPA 8260C

EPAS260C'*^-,V t^-r- . . - :^H2ai^ • * „ . .

EPA 8260C

BRA8260Gs

EPA 8260C

nfsjwfs Wf( '

591-78-6 Methyl Butyl Ketone

\ • •SlL).92U';.-vr.- ^• '3;^flP^dR^^0!92>f'^ ' 'y^r ;'••;:'- 5? ÊM^^ :.j,...uAMrii:^?:i..^;iC}.". - ,'• ,^Kr-;-,7•W-;â»«i^W^^^^&f.i,a.âM.:.'i,,a!^'A^-j:2.>:ji,°i2^^

0.92 Ll ug/kg dry 0.92 75"2o " I ' P EPA8260C

0.92 U ug/kg dry 0.92 'iv',o P P P EPA8260C

Page 18 o f 3 8 E 1 3 0 3 1 0 P H Y S P V O A F I N / \ L 0 3 01 13 0942 3/1/13 9:42





Volatile Organics

Sample ID: SD-902

Station ID: SW-02


Lab ID: E130310-11

Matrix: Sediment

( ' •1.5

Sii t t thef •(/////¥ fe' Re%uits Quids tiers Uni ts : M R l I'repu.-fd Aimii-'ed M.'lhnd

106-43-4 p-Chlorotoluene

99-87-6 p-1 sopropv Itoluene

135-98-8 sec-Butylbenzene i

100-42-5 Stsrcnc


127-18-4 letraehloroethene (I'etrnchloroetlnlen,

108-88-3 I'oluene

1511-60-5 trans-1.2-Dichloroethcnc

10061 -02-6 trans-1,3- Dich loropropene|

79-01-6 rnehloroethone (Trichlorocthslene)

75-69-4 Trichlorofluoromethane (Freon 11)

75-01-4 Vinvl chloride

ug/kg dry

ug/kg di'y

ug/kg dry

iig kg dr\

Ug/kg dry

uti'kg dr\

Ug/kg dry

ug/kg dr\

ug/kg dry

ug/kg dn,

ug/kg dry

ug/kg dry

0,46

0.46

0.46

1)46

0.46

0 46

0 46

0 to

0.46

0 40

0.46

0.46

1/18/13 1520 EPA 8260C

I p . \ X2i,nc

EPA 8260C

I PA !C()(l(

EPA S260C

PP,\ 82(,(IC

EPA S260C

IPA S250C

EPA 82f>0C

LPA 82506

EPA 8260C

EPA 8260C


R4-0000 Tentatively Identified Compounds 911 ug/kg dry I/30/I3 FPA 8260C






Physical Properties

Sample ID: SD-902

Station ID: SW-02

Lab ID: EI30310-II

Matrix: Sediment

Date Collected: 1/I7/I3 15:05

.yii'mber iiAhply'l'A ' '.:.PI^piA'Ati^}i.-mm'

'APPpLiipPtpaAed:Pptiiilp,edp\MS'wP.p,^ ZM

El 642941 %'Sol ids -ry—*fr-; 86:; :0.0. I.'29/13 14:21

;|/30/13, EPA 200.2


-tl'





Volatile Organics

Sample ID: SD-09

Station ID: SW-09

Lab ID: E130310-14

Matrix: Sediment


I ( 'AS ll, ',1-i'.

R4-7I56

630-20-0

71-55-6

79-34-5

76-13-1

79-00-5

75-34-3

75-.55-4

503-58-6

87-61-6

96-18-4

120-82-1

95-63-6

96-12-8

106-93-4

95-50-1

I07-(fe-2

7S 87 >

108-67-8

541-73-1

142-28-9

106-46-7

67-64-1

71-43-2"

108-86-1

74-97-S


eiiachloroethane

1,1-Trichloroethane

1.2.2- I'eirachloroethane

. 1,2-Trichloro-1.22J-Triflu«ro8thane (Freon 113)

-rrieliloroethane

1-Dichloroethane

Dicliloroelhcne .l~Dichloroelh\lenel l-Dichloropropcne

2 3-1 richloroben/ene

2.3-Ti ichloropropane

1 2 4- Incliloroben/ene

.2,4- frimethylbenzene

1.2-Dihromo-3-Chloropropane (UBCI'l

1,2-Dibromoethane (EDi

1.2-Dichlorobenzene

I 2 Dichloroethane

1 '' Dichloropiopane

1,3,5-1 rimathv Ibenzcne

1,3-Dichlorobcn/ene

1.3-Dichloropropane

Bromobenzene

Bromoch loromethane

1 18 13 15 25

1/18/13 15:25

1/18/r, I5'25

I,' IK, I i IS 25

1/18/13 15.25

I'l 8/13 15:25

I 18,1) is 25

1/I8/I3 15:25

1/18/13 15:25

1/18/13 15:25

1/18/13 15:25

I 18 11 IS 25,

I 18/13 15 25

l.'18'I3 IS 25

1'18/I3 15:25

I/I8/I3 15:25

1/18/13 15:25

I 29/13 17 09

1/29/13 17:09

1/29/13 17:09

1/29/13 1709

1/29/13 1709

1 29/13 17 09

L''29/13 1709

1/29/13 1709

1,'29/13 1709

1'29/13 1709

1 29 11 .^17 09

1/29/11 17 09

I'29/13 1709

1/29/13 1709

1/29/13 1709

I : P , \ S:( ,IK

EPA 8250C

i:p,\ .s;:6n(

EPA 8260C

MM,..:,-.. EPA 8260C






Sample ID: SD-09

Sta t ion ID: SW-09


Volatile Organics

Lab ID: E130310-14

M a t r i x : Sediment

( A S

V«wft/T ' • ' I / , ^ • : : i >

75-27-4

75-25-2

74-83-9

75-15-0

S6-23-*5

los s)(i_-

75-00-3

67-66-3

74-87.

156-59-2

10061-01-5

110-82-7

124-48-I

74-95-3

75-71-8

100-41-4

87-68-3

98-82-8

79-20-9

591-78-6

108-lU-l

1634-04-4

108-87-2

7S-09-2

104-51-8

|03-65-l

95-49-8

95-47-6 1

Bromodichloromethane

Broniolbrm

Bromomethane

Ljtbon disulfide

Carbon fctrachlor

( hlorobcn/i.ne

Chloroethane

Lliloioloini

orometh:

cis-l 2-Dichloroethene

cis-l,3-Dichloropropene

C\clolie\ane

Dibromochloromethane

Dibioinomethaiie

Dtchloroditluoromcthane (Freon "12)

Mh\l Benzene

Hexachlorobutadieiti

Isopropylben/cni

Methyl Acetate

Methvl Biitvl Kelone

Methyl Ethyl Keuine

Metln 1 Isobulvl Kelone

Methyl T-Butyl Ether (MTBE)

Meihslcsclohexane

Methylene CUonde

n-But\ Iben/ene

n-Propylbenzene

o-L'hiorotoluone

0-.Xylene

0 59

12

24

24

0.59

(1 59

2.4

0 59

0 59

0 50

0.59

0,59

0.59

0,59

0.59

0,59

0.59

0.59

1.2

1,2

' 4.7

1,2

0.59

0,59

0.59

0 50

0.59

0 50

0 59

1/18/13 15:25

1 lS-1 i ps 2S

I/18/I3 15:25

M S n IS 25

1/18/13 15,25

M S 1 i

1/18/1.! 15:25

M S n | S

1 18 13 1525

1 IS 1 IS

1 18/13 15 25

1 IS 1 1

1 IS 13 15 25

1 IS 1 1

1 IS 1 IS 75

1/29/13 17.09

1 2'/ 1 s

1,''29/13 1709

1 29 1 s 7 uo

1/29/13 1709

1 2') IS

1,'19/I3 ( 7 0 9

r ^ o 1 : 1

1 ' > 11 1 -09

1 1 1 0

1 29 13 1 7 0 9

1 1 1

1 29 13 1 7 0 )

1 1 1

1 29/13 1 7 0 1

11 1 1 1 1 1 9

1 18 I J 15 25

1 S 1 1

1 18 11 15 »5

1 IS 13 Is 75

1 IS/lJt 1525

1 29/13 1 7 0 9

1 1 1

1 ' > 1 3 17 09

1/29/13 17 09

17 09

M s l 1 1 1 1

1 18 13 I s 25

M S 1 i IS 2S

1/18/13 1525

M S 1 i

1 18 ,1! 15 2S

I M I , 1 2^

1 18 1! 15 25

1 29 13 17 09

1 20 n 1 •' 00

1/29/13 17:09

1 20 11 MHO

1 19.13 17 09

1 2 ) 1 , r . K )

1 29 11 17 09

EPA 82(>0C

LPA s;()l)('

EPA 8260C

I PA s:6oc

EPA 8260C

pp,\ s:()iic

EPA 8260C

II \ s:<)i)C

EP^ 8250C

1 p \8 :oo( '

EPii 8260C

1 P \ 8260C

I PA 8260C

1 I \ 82(>0(.'

EP'\8260C

I i \82r>0('

EPA 8260C

1 I \ 82()OC

FPA 8260C

EPA 8260C

EPA 8260C

1 1 \ « 2 i , I J ( '

tPA 8260C

PPA 8:()0C

EPA S260C

PPA 8:(>0C

EP.V S260C

I P \ 82oO(

EPA 8260r





D.A.R.T.Id: 13-0162 Project: 13-0162, Aberdeen Groundwater- Reported by Janet Muse


Volatile Organics

Sample ID: SD-09

Station ID: SW-09

Lab ID: E130310-14

Matrix: Sediment


infilrtc i f . i ' i ' f . t-ttits Prcpiued ..Uiim-"ed Method

106-43-4 p-Chlorotoluenc

99-87-6 p-Isopropyl toluene

135-98-8 sec-Butylbenzene

100-42-5 Styrene


127-18-4 rclrachloroethene ( Tetrachloroethvlene)

108-88-3 Toluene

156-60-5 trans-1.2-Dichloroetlieni

10061 -02-6 trans-1,3-Dichloropropei

79-01-6 Trichloroethene! Trichloroethylene)

75-69-4 Trichlorofluoromethane (Freon 1

75-01-4 Vinyl chloride

ug/kg dry

ug/kg dp,'

ug/kg dry

ug/kg drv

ug/kg dry

u_;kg diA

ug/kg dry

ug. kg dp.

Ug/kg dry

ug/kg dry

0.59

0,59

0.59

0 ^0

0 59

0 ^0

'*'0 59

0 50

0 59

0.59

0.59

0.59

/IS/13 15:25

i/|8,'13 15:25

1 18 It 15 25

1 18 l> IS 25

1 18/13 15 25

1/18/13 15:25

118 11 15:25

1,'29/13 17,09

l.'29/13 17:09

I 29 11 17 09

I 29 11 1709

1 20 13 17 09

i,'29/t3 1709

1 2')/II 1709

EPA 826()C

I:P.\ S:5nt'

EPA 8260C

EPA 82606

EPA S260C

i'P-\ s''(.in

EPA 8260C

IPA s:(,iii.

EPA 8260C

PP.\ 82506'

EPA 8260C

EPA 8260C


R4-0000 Tentttively Identified Compounds 10 '•r%^llVfi:$' - :>:':f^ div 10 ' ; ' | » ' •' ^ ^ ' %PAli260C






Physical Properties

Sample ID: SD-09

Station ID: SVV-09

Lab ID: EI30310-14

Matrix: Sediment


Nitmber Aiililpe ; | ; ? V A-: :• ^pmf^gmA:-' •' '

•A: : -A .:,AuivA:^tA* . .; :Resim<Oitiifificrs

• - , • • • \ .

Units MRL

•" -'= .-AA. •

. ' p P : •"»; ' • Prepared AnalAzed .Method :m

'•-. = '

61642941;: %'Solids -s i s . ; , , . . • : : • • : ^ -----.•••-•r. - -

jiS'T " ' • P ^ $ ^ Z 1 A A : °/» " 0.0 .l/:9/13iy:f./4;T/30/13 "^c'pi ,,-ir,, ;;'l-t2j;4M»v 15.23.. '2'^?^^,""'-





Volatile Organics (VOA) - Quality Control

US-EPA, Region 4, SESD

.Analyte Result

Reponing

Limit Units

Spike Source

Level Result ' 'oREC

».'oREC

Limits RPD

RPD

Limit Notes

Batch 1301113 - V 5035 VOA Soil and W aste Prep

Blank (1301II3-BLK1) Prepared & Analyzed: 01/29/13

EPA 8260C Dichlorodifluoroinelhane (Freon 12)

Cliloroineihane

Vinyl ijhloride

Bromomethane

Chloroethane

Trichlorotluoromethane (Freon 11)

Acetone

1.1 -Dichloroethene (1,1 -Dichloroethylene)

Methylene Chloride

1.1,2-Trichloro-1.2.2-Trifluoroelh ane

(Freon 113)

Methy! Acetate

Carbon disulfide

trans-1,2-Dichloroethene


1.1-Dichloroethane

Methyl Ethyl Ketone


Bromochloromethane

Chloroform

2.2-Dichloropropane

l,2-Dichloroeth3ne


1,1-Dichioropropene

Cyclohexane

Carbon Tetrachloride

Benzene

Dibromonicthajie

i.2-Dichloropropane



Methylcyclohexane

cis-1,3-Dichloropropene

Melhyl Isobutyl Ketone

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

Toluene

1,3-Dichloropropane


u Ll

U

0.55714

Ll

U

Ll

U

IJ

U

U

U

U

LI

U

U

U

U

U

U

IJ

Ll

U

U

U

U

u u Ll

LI

L'

Ll

U

U

U

Ll

U

U

0,71

0,71

0,71

2.9

2.9

0.71

29

0.71

0.71

0.71

' 1.4

2,9

0,71

0.71

0.71

5.7

0.71

0.71

0.71

0.71

0.71

0.71

0.71

0.71

0.71

0.71

0.71

0,71

0.71

0.71

0.71

0.71

1.4

0.71

0.71

0.71

0.71

0.71

ug/kg wet

" " "

" " " " "

" " " " " " " " " " " " " " " " " " " " " " " "

"

u u u

1-3. <">2.

J

U

u u u u u

u u u u u u u u u u u u u u u u u u u u u u u u u u u u




. Project: 13-0162, Aberdeen Groundwater - Reported by Janet Muse



Methyl Butyl Kelone

1,2-Dibromoethane (EDB)

Tetrachloroethene (Tetrachloroethylene)

1,1.1.2-Tetrachloroethane

Chlorobenzene

Ethyl Benzene

(in- and/or p-)Xylcne

Bromotbrm

Styrene

1.1.2.2-Tetrachloroethane

0-Xylene

1.2.3-Trichloropropane

Isopropylbenzene

Bromobenzene

n-Propylbenzene

o-Chlorotoluene

p-Chlorotoluene

1.3.5-Trimethylbenzene

ten-Butylbenzene

1.2.4-Trimeihylbenzene

sec-Butylbenzene

1,3-DichIorobenzene

1,4-Dichlorobenzene

p-Isopropyltoluene

1.2-Dichloroben2ene

n-Butylbenzene

1.2-Dibromo-3-Chloropropane(DBCP)

1.2,4-Trichlorobenzene

Hexachlorobutadiene

1,2,3-Trichlorobenzene

Tentatively Identified Compounils

u u u IJ

IJ

Ll

U

Ll

U

U

U

IJ

U

U

U

U

U

LI

IJ

U

U

Ll

0,20000

U

U

U

Ll

0.35714

U

0.35714

11

1.4 ug/kg

0.71

0.71

0.71

0.71

0.71

1.4

1.4

0.71

0.71

0.71

0.71

0.71

0.71

0.71

. 0.71

0.71

0,71

0,71

0.71

0,71

0.71

0.71

0,71

0.71

0.71

1,4

0.71

0.71

0.71

i n

.Analyte Result Reporting

Limit Units Spike Source Level Result %REC

".'oREC Limits RPD

RPD Limit Notes

Batch 1301113 - V 5035 VOA Soil and Waste Prep

Bliink(l30ll l3-BLK1) Prepared & Analyzed: 01/29/13 1

u u u u u u u u u u u u u u u u u u u u u u

Q-2. I

u u u u

B-3, (>2.

J

U

B-3.Q-2. J

B

Page 26 of 38 EI303I0 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42






Analyte Result Reporting

Limit , Units Spike Source %REC Level Result "'oREC Limits RPD

RPD Limit Notes


Blank (1301113-BLK2) Prepared: 01/18/13 Analyzed: 01/29/13

EPA 8260C Dichlorodilluoromethane (Freon 12)

Chloromethane

Vinyl chloride

Bromomethane

Chloroethane

Trichlorofluoromethane (Freon 11)

Acetone

1,1-Dichloroethene (1.1-Dichloroethylene)

Methylene Chloride

1,1,2-Trichloro-1,2.2-Trifluoroethanc (Freon 113)

Methyl Acetate

Carbon disulfide

trans-1.2-Dichloroerhene


1,1-Dichloroethane

Methyl Ethyl Ketone

cis-1.2-DichIoroelhene

Bromochloromethane

Chlorolorm

2,2-Dichloropropane

1,2-Dichloroethane

1.1, l-Trichloroethane

1,1-Dichioropropene

Cyclohexane


Benzene

Dibromomethane

1,2-Dichloropropane



Methylcyclohexane

cis-1,3-Dichloropropene

Methyl Isobutyl Ketone

trans-1 ,j-Dichloropropene

L1.2-Trichloroethane

Toluene

L3-Dichloropropane


u u u u u u u u u u

u u u u u u u u u u u u u u u u u u u u u u u u u u u u

0.71

0.71

0.71

2.9

2.9

0,71

29

0.71

0.71

0.71

1,4

2.9

0.71

0.71

0.71

5.7

0,71

0.71

0.71

0.71

0.71

0,71

0.71

0.71

0,71

0.71

0.71

0,71

0.71

0.71

0.71

0.71

L4

0.71

0.71

0.71

0.71

0.71

ug/kg wet







Methyl Butyl Ketone

1.2-Dibromoethane (EDB)


1,1,1,2-Tetrachloroethane

Chlorobenzene

Ethyl Benzene

(in- and/or p-)Xylene

Bromoform

Styrene

1.1,2,2-Tetrachloroethane

o-Xylene

1.2,3-Trichloropropane

Isopropylbenzene

Bromobenzene

n-Propylbenzene

o-Chlorotoluene

p-Chlorotoluene

1.3,5-Triinethylbenzene

tcn-Butylbenzene

1.2,4-Trimethylbenzene

sec-Butylbenzene

1.3-Dichlorobenzene

1.4-Dichlorobenzene

p-lsopropyltoluene

1.2-Dichlorobenzene

n-Butylbenzene

l,2-Dibromo-3-Chloropropane (DBCP)

1,2,4-Trichloroben2ene

Hexachlorobutadiene

1.2.3-Trichlorobenzene

Tentatively Identified Compounds

u u u u u u u

u u u u u u u u u u u u u u u u u u u u u u u u

1.4

0.71

0,71

0,71

0.71

0.71

14

L4

0.71

0.71

0,71

0.71

0,71

0,71

0.71

0,71

0,71

0.71

0.71

0.71

0,71

0,71

0,71

0.71

0.71

0.71

1.4

0.71

0.71

0.71

10

ug/'kg wet

Analyte Result

Reponing

Limit Units

Spike Source %REC

Level ResiJt °oREC Limits RPD

RPD

Limit Notes


Blank (1301II3-BLK2) Prepared: 01/18/13 Analyzed: 01/29/13







.Analyte Result

Reporting

Limit Units

Spike Source

Level Result 'I'oREC

-'oREC

Liinits RPD

RPD

Limit Notes


LCS(130IU3-BSI) Prepared &. Analyzed: 01 /29/13

EPA 8260C Dichlorodifluoromethane (Freon 12)

Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


Acetone

1.1 -Dichloroethene (1.1 -Dichloroethylene)

Methylene Chloride

1.1.2-Trichloro-1.2.2-Trifluoroethane

(Freon 113)

Methyl Acetate

Carbon disulfide

trans-l,2-Dichloroeihene

Methyl T-Butyl Elher (MTBE)

1.1-Di chloroethane

Methyl Ethyl Ketone


Bromochloromethane

Chiorofomi

2,2-DichIoropropane

1.2-Dichloroethane


I.I-Dichloropropene

Cyclohexane


Benzene

Dibromomethane

1.2-Dichloropropane



Methylcyclohexane

cis-1.3-Dichloropropene



1.1,2-Trichloroelhane

Toluene

1,3-Dichloropropane


35.200

28,329

32.457

27,385

30.086

33,114

44,414

30,385

29.671

31,800

56,757

30,414

29.914

28.400

30.343

52,129

28.971

28.986

30.414

27.443

30.729

32.929

30.443

31,100

3-1,400

30,229

28.114

29.457

29.857

29.843

31.914

34.786

55.143

34.229

29.486

31.714

30,429

32.143

0.71 ug/kg

0.71

0.71

2,9

2.9

0.71

29

0.71

0.71

0.71

1,4

2.9

0,71

0,71

0.71

5,7

0.71

0,71

0.71

0.71

0.71

0,71

0.71

0,71

0.71

0.71

0.71

0.71

0.71

0.71

0.71

0.71

1,4

0,71

0.71

0.71

0.71

0.71

wet 28.571

28.571

28.571

28 571

28.571

28,571

57.143

28,571

28,571

28.571

57,143

28,571

28.571

28.571

28.571

57,143

28.571

28.571

28.571

28.571

28.571

, 28.571

28.571

28.571

28.571

28.571

28.571

28.571

28.571

28.571

28.571

28,571

57.143

28.571

28.571

28.571

23.571

28.571

123

09,1

114

95,8

105

116

77.7

106

104

III

9 9 3

106

105

99,4

106

91.2

101

101

106

95.0

108

115

107

109

120

106

98,4

103

104

104

112

122

98.2

120

103

II I

106

112

22.4-184

51.9-146

52.8-145

70.4-159

58 3-147

75,8-142

57,1-127

78,3-131

73.3-119

66.2-137

65.1-140

68.5-135

83.4-123

72.3-142

84.2-120

64,6-136

84.2-122

83,4-125

7S.4-13I

82,5-129

75.4-133

82.3-129

84.7-121

798-132

83.2-130

82.4-122

82.3-129

77,2-128

82.6-128

78 I-I33

80.5-129

86.I-I22

84.4-130

899-125

87,7-116

85-118

85,2-119

87-117

nc-2

Page 29 of 38 El30310 PHYSP VOA FfNAL 03 01 13 0942 3/1/13 9:42






Analyte Result

Reporting

Limit Units

Spike Source

Level Result "iREC

•ioREC

Limits RPD

RPD

Limit Notes


LCS(130III3-BSI) Prepared & Analyzed: 01/29/13 , Methyl Butyl Ketone

1.2-Dibromoethane (EDB)


1,1,1,2-Tetrachloroethanc

Chlorobenzene

Ethyl Benzene

(in- and'or p-)Xylene

Bromoform

StyTene

1.1,2.2-Tetrachloroethane

o-Xylene

1.2,3-Trichloropropane

Isopropylbenzene

Bromobenzene

n-Propylbenzene

o-Chlorotoluene

p-Chlorololuene

L3.5-Trimethylbenzene

tert-Butylbenzene

1,2,4-Trimethylbenzene

sec-Butylbenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

p-Isopropyltoluene

1.2-Dichlorobenzene

n-Butylbenzene

l,2-Dibromo-3-ChIoropropane(DBCP)


Hexachlorobutadiene

1,2.3-Trichlorobenzene

54,257

32,143

32.129

34.400

31.329

33.157

64.557

68.057

31.786

27.986

31.914

28.971

32.486

29.614

33,029

31.700

31,257

32,614

32,786

32.214

33.557

30.557

29,971

32.986

30,243

32,843

66.514

29.786

32.814

29.686

1.4 ug/kg

0,71

0.71

0.71

0.71

0.71

1.4

1.4

0.71

0,71

0.71

0.71

0.71

0,71

0,71

0.71

0,71

0,71

0,71

0.71

0.71

0,71

.0,71

0.71

0.71

0.71

1.4

0.71

0,71

0,71

wet 57.143

28.571

28,571

28.571

28,571

28,571

57.143

57,143

28,571

28.571

28.571

28.571

28.571

28.571

28.571

28.571

28,571

28,571

28,571

28.571

28.571

28.571

28.571

28,571

28.571

28.571

57,143

28.571

28.571

28.571

94.9

112

112

120

no 115

113

119

II I

97.9

112

101

114

104

116

III

IOO

114

115

113

117

107

105

115

106

115

116

104

115

104

83,6-128

86-121

80,8-125

892-124

84-120

83.3-124

86,2-127

79-115

84,4-131

69,2-124

81.2-126

863-1 18

SI.8-125

84,3-118

82.1-123

82,8-121

83,4-123

80,5-124

74.2-126

71.8-135

75.4-123

82.I-I21

81-120

76-123

83-118

78.4-123

68.5-114

65.8-127

60.9-119

57,1-125

OC-2.

OL-2







Analyte, Result

Reporting

Limit Units

Spike Soiu-ce %REC

Level Result %REC Limits ' RPD

RPD

Limit Notes

Batch 1301113 - V 5035 VOA Soil and \Vaste Prep

M a t r i x S p l k e ( 1 3 0 l l l 3 - M S l ) Sou ree •E1303 I0 -14 Prepared: Ol/I.S/13 Analyzed: 01/29/13


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane

Trichlorotluoromethane (Freon 11)

.Acetone

1,1-Dichloroethene (1,1-DichloroethyIene)

Methylene Chloride

1,1,2-Trichloro-1,2,2-Trifluoroethane

(Freon 113)

Methyl Acetate

Carbon disultlde

trans-1,2-Dichloroeihene


l.i-Dichloroethane

Methyl Ethyl Ketone

cis-1,2-Dichloroethene

Bromochloromethane

Chlorotpnn

2.2-Dichloropropane

1,2-Dichloroethane

1.1, l-Trichloroethane

1,1 -Dichioropropene

Cyclohexane

Carbon Tenâchloride

Benzene

Dibromomethane

!,2-Dichloropropane



Methylcyclohexane




1,1.2-TrichIoroethane

Toluene

1,3-Dichloropropane


21.778

21.164

21.719

23.916

30,435

20,704

54.812

20.834

24.412

18.731

40.628

20,149

21.613

23.774

23.975

40,061

22.463

23.243

23.975

21.082

24.625

23.018

20,196

17.101

22.369

22.841

21.767

22,593

21.034

23.066

15.850

25.558

42.021

24554 '

23.196

24.613

23.915

24.01!

0.59 ug/kg dry 23.521

0.59

0.59

2,4

2.4

0.59

24

0,59

0.59

0.59

1.2

2.4

0,59

0.59

0.59

4.7

0.59

0.59

0,59

0.59

0.59

0.59 ,

0.59

0,59

0.59

0,59

0,59

0.59

0.59

0,59

0,59

0.59

1.2

0.59

0.59

0.59

0.59

0,59

23,521

23,521

23.521

23.62 1

23.621

47,242

23.521

23.621

23,621

47.242

23.621

23.621

23.621

23.621

47.242

23.621

23.621

23.621

23.521

23.62 I

23.621

23,621

23.621

23.021

23.621

23.621

23.621

23.621

23.621

23,521

23.621

47.242

23.621

23.621

23.621

23.621

23.621

U

U

U

U

, U

U

57,942

U

U

u •

U

U

U

U

U

9,6077

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

1.1004

U

U

92.2

89,6

92,0

101

129

87.7

NR

88.2

103

79,3

85.0

85.3

91.5

101

102

64.5

95.1

98.4

102

8 9 3

104

97.4

, 85.5

72,4

94.7

96,7

92.2

95.7

89.1

97,7

67.1

108

8 9 0

104

98,2 .

99,5

lOI

102

10-200

16.7-141

25.4-146

10-164

35,3-147

35,8-154

10-137

33.I-I41

35,4-132

35,9-149

10-144

13.9-130

3 1.2-129

54.2-129

46,6-127

10-134

36.8-126

45,7-125

43,5-129

38,3-137

40-127

38,6-137

31,1-128

22.9-144

3I.6-I4I

38-124

39-132

43.4-123

23-125

35,8-129

11,1-140

10-137

10-153

10-139

47.5-123

43.3-I2I

50.1-118

42.5-116

QC-2

OC-I.

OM-6







Reporting

Analyte Result Limit Units

Spike Source %REC

Level Result %REC Liinits RPD

RPD

Limit Notes


Matrix Spike (1301113-MSl) Source: EI30310-14 Prepared: 01/18/13 Analyzed: 01/29/13

Melhyl Butyl Ketone

1,2-Dibromoethane (EDB)


1,1.1,2-Tetrachloroethane

Chlorobenzene

Elhyl Benzene

(m- and/or p-).Xylene

Bromoform

Styrene

1,1,2,2-Tetrachloroethane

o-Xylene

1,2,3-Trichloropropane

Isopropylbenzene

Bromobenzene

n-Propylbenzene

o-Chlorotoluenc

p-Chlorotoluene


ten-Butylbenzene

1.2.4-Trirnethylbenzene

sec-Butylbenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

p-Isopropyltoluene

1.2-Dichlorobenzene

n-Butylbenzene

1.2-Dibromo-3-Chloropropane(DBCP)


Hexachlorobutadiene


39354

23.833

21.176

25,463

i2.003

23.798

45.777

54.162

17.456

23,479

23.042

23.703

25.050

22,310

23.987

23.444

22,511

24,199

23,786

23.822

22.109

20.019

18.596

22.239

19428

19,428

47.017

12,519

13.936

11.362

1.2 ug/ks

0.59

0,59

0.59

0,59

0.59

1.2

1,2

0.59

0.59

0.59

0.59

0.59

0,59

0,59

0,59

0.59

0,59

0.59

0,59

0.59

0.59

0.59

0.59

0,59

0.59

1,2

0.59

0.59

0.59

,dry 47.242

23.621

23.621

23,621

23,621

23.621

47.242

47.242

23,621

23.621

23.621

23.621

23.621

23.621

. 23.621

23.621

23.621

23.621

23.621

23.621

23.621

23.621

23.521

23.621

23.621

23.621

47.242

23.621

23.621

23.621

U

U

u u u u u u

u u u •

u u u u u Ll

u u u u u u

0.74542

U

u U

U

U

U

83.3

101

89,6

108

IS,2

101

96.9

115

73.9

99,4

'17.6

IOO

106

94.5

102

99.3

05.3

102

lOI

101

93,6

84.8

792

91.0

82.3

82.3

99.5

53.0

5 9 0

48.1

10-149

17.7-127

41-116

45.5-125

32,9-115

36,5-118

37,3-120

23,8-110

14,7-1 IS

32,4-121

35.4-119

42-155

12.9-153

3I.9-I28

24.2-142

265-139

28.9-127

31-127

13-153

261-129

24.3-117

20.9-114

17,9-114

24.4-110

16,4-115

15.8-98,9

25.9-111

10-94,4

10-95.9

10-95

OC-2. nM-2







Reporting

.-îi.-ilyte Result Limit Units

Spike Source VoREC

Level Result ôREC Limits RPD

RPD

Limit Notes


Matrix Spike Dup (1301113-MSDl) Source: EI303I0-14 Prepared: 01/18/13 Analyzed: 01/29/13


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


Acetone

1.1 -Dichloroethene (1,1 -Dichloroethylene)

Methylene Chloride

1,1,2-Trichloro-1.2,2-Trifluoroethane (Freon 1 13)

Methyl Acetate

Carbon disulfide

trans-1.2-Dichloroethene


1,1-Dichloroethane

Methyl Elhyl Ketone


Bromochloromethane

Chlorolorm

2,2-Dichloropropane

1,2-Dichloroethane

1,1,1 -Trichloroethane

1,1-Dichioropropene

Cyclohexane


Benzene

Dibromomethane

1,2-Dichloropropane



Methylcyclohexane


Melhyl Isobutyl Ketone

trans-1,3-Dichloropropcne

1,1,2-Trichloroethane

Toluene

1.3-Dichloropropane


Page 33 of 38

18.521

18,645

18.502

21.911

26.510

17.766

61,944

17,754

20,913

16.104

35.900

15.400

18,016

23.312

20.866

38.964

18,906

20,284

21.210

21.186

2 1.602

20,830

17.125

15.106

19.001

19,381

18,716

20.070

17.315

19833

13.835

21.721

41.351

20.343

21.234

20.750

21.412

21.685

0,59 ug/kg dry 23.752

0.59

0.59

2.4

2.4

0,59

24

0,59

0,59

0.59

1,2

2.4

0.59

0.59

0.59

4,8

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0,59

0.59

1.2

0.59

0,59

0,59

0.59

0.59

FINAL 03 01 13 0942

23.752

23.752

23,752

23.752

23,752

47.503

23.752

23.752

23.752

47,503

23.752

23.752

23.752

23.752

47.503

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23,752

23.752

23.752

23.752

47.503

23,752

23.752

23.752

23,752

23.752

U

U

U

Ll

U

U

57 942

U

U

U

U

U

U

U

U

9,6077

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

u u u u

1.1004

u u

78.4

78.5

77.9

92.2

112

74,8

8,43

74.7

88.0

67.8

75.6

6 9 0

75,8

98,1

87.8

61.8

7 9 5

85.4

8 9 3

89.2

90.9

87.7

72.1

53.6

80.0

81.6

78.8

84.5

72.9

83.5

58.2

91.4

87.1

85.6

89,4

82.8

90.1

91.3

10-200

I67- I4 I

25.4-146

10-164

35 3-147

35.8-154

10-137

33.I-I4I

35 4-132

35.9-149

10-144

13.9-130

31.2-129

54.2-129

•16.6-127

10-134

35.8-125

45.7-125

43.5-129

38.3-137

40-127

38.6-137

3I.I-128

22.9-144

3I.5-I4I

38-124

39-132

43.4-123 .

23-125

35.8-129

11.1-140

10-137

10-153

10-139

47.6-123

43.3-121

50.9-118

42.5-116

15.6

12.7

16.0

8.75

13.8

15.3

12.2

16.0

15.4

15.1

12.4

20.5

18.2

1.96

13.9

2.77

17.2

13.5

12.2

0.496

13.1

9.98

16.5

12.4

163

15.4

15.1

11.8

194

15.1

13.6

162

.1.61

18.8

8.83

17.0

ILO

10.2

34.3 OC-2

32.2

33.1

53

33.5

35.4

27.2 OC-I.

QM-5

42.2

44.8

44.2

46.6

42.9

4 7 3

22

52.6

41.2

49

25.7

47.2

46.1

24.4

4 9 2

52.7

53.7

57

52.6

26.6

34.4

47.1

33.6

56

54.2

54.8

41.4

25.9

54.6

26.1

33.6

3/1/13 9:42






Methyl Butyl Ketone

1.2-Dibromoeihane(EDB)


1,1.1,2-Tetrachloroethane

Chlorobenzene

Elhyl Benzene


Bromoform

Styrene

1.1.2,2-Tetrachloroethane

o-X>lene

1.2,j-Trichloropropane

Isopropylbenzene

Bromobenzene

n-Propylbenzene

o-Chlorotoluene

p-Chlorotoluene

1.3.5-Trimethylbenzene .

tert-Butylbenzene


sec-Butyibenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

p-lsopropyltoluene

l.2-Dichloroben2ene

n-Butylbenzene.

L2-Dibromo-3-Chloropropane (DBCP)

1,2.4-Trichloroben2ene

Hexachlorobutadiene

1.2.3-Trichlorobenzene

35.687

20.699

18.158

22.325

17.576

20.165

38.026

50.840

13.028

22.837

19.607

23.110

22.956

18.336

21.460

19999

18.882

21.103

21.412

20.414

19833

15.724

14.880

I976I

15.712

16.538

46.422

9.6550

12.101

8.6931

1.2 ug/kg dry 47.503

0.59

0.59

0.59

0.59

0.59

1.2

1.2

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

0.59

1.2

0.59

0.59

0.59

23.752

23.752

23.752

23.752

23.752

47.503

47.503

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

23.752

47.503

23.752

23.752

23.752

U

U

U

U

U

U

U

U

U

U

U

U

U

U

u u u u u u u u u

0.74542

U

U

U

U

U

U

75.1

87.1

76.4

94.0

74.0

84.9

80.0

107

54.8

96.1

82.5

97.3

95.6

77.2

90.3

84.2

79.5

88.8

"O.l

85.0

83.5

66.2

62.6

80.1

55.1

70.0

97.7

40.6

50.9

36.6

10-149

I7.7-I27

41-116

46.5-125

32.9-115

36.5-118

37.3-120

23.8-110

14.7-118

32.4-121

35.4-119

42-155

12.9-163

3I.9-I28

24.2-142

26.6-139

28.9-127

31-127

13-153

26.1-129

243-117

20.9-114

17.9-114

24.4-110

164-115

16.8-98.9

25.9-111

10-94.4

10-95.9

10-95

9.80

14 1

15.3

13.1

22.4

16.5

18.5

6.33

291

2.77

16.1

2.53

8.72

19.6

I I I

15.9

17.5

13.7

10.5

15.4

10.9

24.0

22.7

11.8

21.2

15.5

1.27

25.8

14.1

26.6

72

40

51.7

62.1

46.5

60.9

62.4

41.5

60.7

42.9

65.4

55.5

74.5

52.8

71.4

793

55.4

74.9

70.8

57.4

71.9

56.4

55.8

72.5

561

595

53

60.3

78.8

54.4

Reporting

Analyte Result Limit Units

Spike Source "i'oREC

Level Result "oREC Limits RPD

RPD

Limit Notes


Matrix Spike Dup (1301113-MSDI) Source: E1303I0-I4 Prepared: 01/18/13 Analyzed; 01/29/13

OC-2







.Analyte Result

Reporting

Limit Units

Spike Source

Level Result ?-oREC

roREC

Limits RPD

RPD

Limit Notes


MRL Verification (1301113-PSl) Prepared & Analyzed: 01/29/13


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


Acetone

1.1 -Dichloroethene (1.1 -Dichloroethylene)

Methylene Chloride

1,1.2-Trichloro-1,2.2-TrinuoroeihiVie (Freon 113)

Methyl Acetate

Carbon disulfide

trans-1.2-Dichloroelhene


1,1-Dichloroethane

Methyl Ethyl Ketone

cis-1.2-DichIoroethene

Bromochloromethane

Chloroform

2,2-Dichloropropane

1,2-Dichioroethane


1.1 -Dichioropropene

Cyclohexane


Benzene

Dibromomethane

1,2-Dichloropropane



iVlethylcyclohexane




1,1.2-Trichloroethane

Toluene

1,3-Dichloropropane

18,829

14.071

16.329

12.771

18,157

17,686

12,143

15.700

15.100

17000

27.714

15,686

15.057

12 186

15.443

25.300

14.871

15.143

15.400

11.186

16.129

15.600

15.329

15.571

17,286

15.171

14.029

14.571

15.043

14.943

15.514

16,214

26.043

15.529

14.729

16.129

15.114

0,71 ug/k

0.71

0.71

2.9

2.9

0,71

29

0.71

0,71

0.71

1,4

2.9

0.71

0,71

0.71

• 5.7

0,71

0,71

0,71

0.71

0.71

0.71

0.71

0.71

0.71

0,71

0.71

0,71

0.71

0,71

0.71

0.71

1.4

0.71

0.71

0.71

0.71

ttivet 14.286

14.286

14.286

14,286

14.286

14.286

28,571

14.286

14.286

14,286

28.571

14.285

14,286

14.285

14.286

28,571

14,286

14,286

14.286

14.286

14,286

14.2S6

14.286

14.286

14,286

14.286

14,286

14.286

14.286

14.286

14.286

14,286

28,571

14.286

14,286

14.286

14,286

132

98.5

114

89,4

127

124

42.5

110

106

119

97,0

no 105

85,3

108

88.5

104

106

108

78.3

113

109

107

109

121

106

98.2

103

105

105

109

114

01.2

109

103

113

106

10-204

31.9-166

42.8-165

50,4-179

48.3-167

55.8-162

47.I-I47

58.3-151

53,3-139

46,2-157

45.1-150

48.5-155

53,4-143

52.3-162

64.2-140

44.6-156

64.2-142

53.4-145

58,4-151

62,5-149

55,4-153

62,3-149

64.7-141

59.8-152

63,2-150

62.4-142

52.3-149

57,2-148

62.6-148

58,1-153

60,5-149

66.1-142

64.4-150

699-145

67.7-136

55-138

65.2-139

OC-2

OC-I. OR-I.

MRL-3. J



980 College Station Road, Athens, Georgia 30605-2700 D.A.R.T.Id: 13-0162




Analyte Resull

Reponing

Limit Units

Spike Source

Level Result "^bREC

%RBC

Limits RPD

RPD

Limit Notes

Batch 1301113 - V 5035 V O A Soil and Wa.ste P r ep

MRL Verification (I30M 13-PSl) Prepared & Analyzed: 01 /29/13


Methyl Butyl Ketone

1.2-Dibromoeth3ne (EDB)

Telrachloroethene (Tetrachloroethylene)

1,1.1,2-TetTachloroeihane

Chlorobenzene

Ethyl Benzene

(m- and'or p-)Xylcne

Bromoform

Styrene

1.1,2.2-Tetrachloroeihane

o-.Xylene

1,2.3-Trichloropropane

Isopropylbenzene

Bromobenzene

n-Propylbenzene

o-Chloroioluene

p-Chlorotoluene


tert-Butylbenzene


sec-Butylbenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

p-Isopropylloluene

l,2-Dichloroben2enc

n-Butylbenzene

1.2-Dibromo-3-Chloropropane (DBCP)

1,2.4-Trichlorobenzene

Hexachlorobutadiene

1.2.3-Trichlorobenzenc

15,514

24.686

15.157

16.000

16.657

15.943

16771

33.014

34.700

15.957

14.271

15.814

14,157

16,343

14,971

16.743

15.957

15.886

15.471

16.400

16,557

16.900

15.286

14.986

16614

15.486

16200

33 185

14.400

16371

14.543

0.71 ug/'kg

1.4

0.71

0.71

0.71

0.71

0.71

1.4

1,4

0.71

0,71

0.71

0.71

0.71

0.71

0.71

0,71

0.71

0,71

0,71

0.71

0.71

0.71

0,71

0.71

0.71

0.71

1.4

0,71

0,71

0.71

wet 14,286

28.571

14,286

14.285

14,280

14,285

14.286

28.571

28.571

14,285

14.285

14.285

14.286

14.286

14.286

14.286

14.286

14.286

14.285

14 285

14.286

14.286

14.286

14.286

14.286

14.286

14.286

28.571

14.285

14.286

14.286

109

86.4

105

112

117

112

117

116

121

112

99.9

III

991

114

105

117

112

II I

115

115

116

118

107

105

116

108

113

115

101

115

102

67-137

63.5-148

56-141

60.8-145

69.2-144

64-140

63.3-144

66.2-147

59-135

64.4-151

492-144

61.2-146

56.3-138

51.8-145

54.3-138

62.1-143

62.8-141

63.4-143

60.5-144

84.2-146

51.8-155

55.4-143

52.1-141

61-140

56-143

63-138

58.4-143

48.5-134

45.8-147

40.9-139

37.1-145

0C-.





Physical Properties (PHYSP) - Quality Control


.Analyte. Reporting

Result Limit Units Spike Source "iREC Level Result %REC Limits RPD

RPD Limit Notes

Batch 1 3 0 1 1 1 8 - M % Solids

Duplicate( l30l l l8-DUPI) Source: E1303I0-14 Prepared: 01/29/13 Analyzed; 01/30/13

EPA 200.2 ".i Solids

Page 37 of 38 EI30310 PHYSP VOA FINAL 03 01 13 0942 3/1/13 9:42




Notes and Definitions for QC Samples

'J The analyte was not detected at or above the reporting limit.

^-^ Level in blank does not impact data quality

J The identillcation of the analyte is acceptable; the reported value is an estimate.

MRL-3 MRL verification for Soil matrix

Q-- Result greater than MDL but less than MRL.

QC-1 Analyte concentration low in continuing calibration verification standard

QC-2 Analyte concentration high in continuing calibration verification standard

QL-2 Laboratory Control Spike Recovery greater than method control limits

QM-2 Matrix Spike Recovery greater than method control limits

QM-6 Matrix Spike Recovery less dian 10%

Ql^"! MRL verification recovery less than lower control limits.

Page38of38 El 30310 PHYSP VOA FfNAL 03 01 13 0942 3/1/13 9:42

MEMORANDUM FROM JANET MUSE, USEPA TO JON … · CAS Chemical Abstracts Service ... Reported by Janet Muse Project: 13-0162, Aberdeen Groundwater Volatile Organics Sample ID: ,4CGSTB011713

Documents