Methods in Enzymolog y Volume 27 6 Macromolecula r Crystallograph y Part A EDITED B Y Charles W. Carter, Jr . DEPARTMENT OF BIOCHEMISTRY AND BIOPHYSIC S UNIVERSITY OF NORTH CAROLINA AT CHAPEL HIL L CHAPEL HILL, NORTH CAROLIN A Robert M. Sweet BIOLOGY DEPARTMEN T BROOKHAVEN NATIONAL LABORATOR Y UPTON, NEW YORK
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Methods in Enzymology
Volume 276
MacromolecularCrystallography
Part A
EDITED BY
Charles W. Carter, Jr.DEPARTMENT OF BIOCHEMISTRY AND BIOPHYSICS
UNIVERSITY OF NORTH CAROLINA AT CHAPEL HILL
CHAPEL HILL, NORTH CAROLINA
Robert M. SweetBIOLOGY DEPARTMEN T
BROOKHAVEN NATIONAL LABORATOR Y
UPTON, NEW YORK
CONTRIBUTORS TO VOLUME 276 . . .
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ix
PREFACE ,
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VOLUMES IN SERIES7[vii
Section I. Introduction
1. Recent Transformations in Structural Biology
BRIAN W . MATTHEWS
3
Section II . Crystals
2. Overview of Protein Crystallization Methods
PATRICIA C. WEBER
1 3
3 . Inferences Drawn from Physicochemical Studies of MADELEINE RIES-KAUTF AN DCrystallogenesis and Precrystalline State
ARNAUD DUCRUIX
2 3
4. Membrane Protein Crystallization : Application of LANGZHOU SONG AN DSparse Matrices to the a-Hemolysin Heptamer J . ERIC GOUAUx
6 0
5 . Response Surface Methods for Optimizing and Im- CHARLES W. CARTER, JR.
74proving Reproducibility of Crystal Growth
6. Second Virial Coefficient as Predictor in Protein A . GEORGE,Crystal Growth
Y . CHIANG ,B . Guo,A . ARABSHAHI ,Z. CAI, AN DW . WILLIAM WILSON
10 0
7 . Kinetic Aspects of Macromolecular Crystallization JOSEPH R . Luvr ANDGEORGE T . DETITTA
11 0
8 . Using Cosolvents to Stabilize Protein Conformation Rut SOUSA
13 1for Crystallization
9 . Preparation and Crystallization of RNA : A Sparse CRAIG E . KUNDROT
143Matrix Approach
10 . Dynamic Light Scattering in Evaluating Crystalliza- ADRIAN R . FERRE-D'AMAREbility of Macromolecules
AN DSTEPHEN K . BURLEY
157
11. Two-Dimensional Protein Crystals in Aid of Three- ALED M . EDWARDS ,
Dimensional Protein Crystal Growth
SETH A . DARST ,SALLY A. HEMMING ,
FRANCISCO J. ASTURIAS ,PETER R . DAVID, ANDRooER D . KORNIERG
16 6
12 . Reductive Alkylation of Lysine Residues to Alter IVAN RAYMENT
17 1Crystallization Properties of Protein s
Section III . Data
A. Apparatus and Sources
13. Practical Cryocrystallography
DAVID W . RODGERS
183
14 . Overview of Synchrotron Radiation and Macromo- JOHN R. HELLIWELL