(logo: REPUBLIC OF TURKEY, MINISTRY OF HEALTH) REPUBLIC OF TURKEY GOVERNORSHIP OF SAMSUN PROVINCIAL HEALTH DIRACTORATE SAMSUN PUBLIC HEALTH LABORATORY ANALYSIS REPORT F81/SHSL/03 Report Printing Date : 07.09.2020 Address: Adalet Mahallesi Mevlana Cad. No:66 55070 İlkadım / SAMSUN Tel: 03622348950 Fax: 03622303772 This document has been signed with secure electronic signature pursuant to the electronic signature law no. 5070. (logo: TÜRKAK) Test TS EN ISO/IEC *7025 AB-0834-T 1/6 Ref. Date and Number 19.08.2020 / 2672 AB-0834-T Date/Time of Sampling 20.08.2020 / 10:30 Date/Time of Sample Incoming to HSL (Lab) 20.08.2020 / 16:12 2020-1960-1 Protocol No / Sample Barcode No 2020-1960 - 1 / 11161816 CSBYS No 118715 09.20 Report Page Number 6 Person/Company/Entity Sending the Sample ERZİNCAN PROVINCIAL HEALTH DIRECTORATE Sampling Address AKTOPRAK MAHALLESİ ERZURUM CADDESİ NO:91 - ERZİNCAN Sample Monitoring Address KIZILAY İÇECEK SAN. VE TİC. ERZİNCAN BRANCH WATER OPERATION FILLING SITE Sample Incoming Reason INSPECTION MONITORING *CHEMICAL AND MICROBIOLOGICAL ANALYSES Sample Receival Date-Time / Incoming Reason 21.08.2020 - 13:19 Filling Site Sample Group WATER ANALYSES Sample Type / Name / Brand / Manufacturer NATURAL MINERAL WATER --- KIZILAY KIZILAY İÇECEK SANAYİ VE TİCARET A.Ş. Sample Packaging Type/ Label/ Amount Original Package + Glass Bottle LABELED 200cc x 60 Sample Mnf.Date/ Exp.Date/ Batch No / Serial No 20.08.2020 20.11.2021 PN233 0944 Seal Status / Minute-Contract Date/No SEALED ... ... ... Invoiced To KIZILAY İÇECEK SANAYİ VE TİCARET A.Ş. Receipt Date and No / Voucher Date and No ______ . ______ ... Declr. Date-No /Import Pre-Approval Doc. Date-No ____________________________ Condition of the Sample Suitable for Analysis Sample Information ... ... Analysis Start/End Date 21.08.2020 13:20 04.09.2020 13:55 Reporting Date 05.09.2020 14:26 CHEMICAL ANALYSES Analyses Unit Method Limit of Quantification (LOQ) Legislation Limit Result Carbonate mg/L Spectrophotometric # 0 MICROBIOLOGICAL ANALYSES Analyses Unit Method Limit of Quantification (LOQ) Legislation Limit Result *Total germ count at 22 °C cfu/mL TS EN ISO 6222 100 1 Parasite pcs/5 L Internal method 0 0 Pathogen Staphylococ. cfu/100mL AFNOR NFT 90-412 0 0 *Pseudomonas aeruginosa cfu/250mL TS EN ISO 16266 0 0 *Sulfite Reducing Spore- forming Anaerobic Bacteria cfu/50mL TS 8020 EN 26461-2 0 0 *Escherichia coli cfu/250mL TS EN ISO 9308-1 0 0
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(logo: REPUBLIC OF TURKEY, MINISTRY OF HEALTH)
REPUBLIC OF TURKEY GOVERNORSHIP OF SAMSUN PROVINCIAL HEALTH DIRACTORATE SAMSUN PUBLIC HEALTH LABORATORY ANALYSIS REPORT
F81/SHSL/03 Report Printing Date : 07.09.2020 Address: Adalet Mahallesi Mevlana Cad. No:66 55070 İlkadım / SAMSUN Tel: 03622348950 Fax: 03622303772 This document has been signed with secure electronic signature pursuant to the electronic signature law no. 5070.
(logo: TÜRKAK) Test TS EN ISO/IEC *7025
AB-0834-T
1/6
Ref. Date and Number 19.08.2020 / 2672 AB-0834-T Date/Time of Sampling 20.08.2020 / 10:30 Date/Time of Sample Incoming to HSL (Lab) 20.08.2020 / 16:12 2020-1960-1 Protocol No / Sample Barcode No 2020-1960 - 1 / 11161816 CSBYS No 118715 09.20 Report Page Number 6 Person/Company/Entity Sending the Sample ERZİNCAN PROVINCIAL HEALTH DIRECTORATE Sampling Address AKTOPRAK MAHALLESİ ERZURUM CADDESİ NO:91 - ERZİNCAN Sample Monitoring Address KIZILAY İÇECEK SAN. VE TİC. ERZİNCAN BRANCH WATER OPERATION
FILLING SITE Sample Incoming Reason INSPECTION MONITORING *CHEMICAL AND MICROBIOLOGICAL
ANALYSES Sample Receival Date-Time / Incoming Reason 21.08.2020 - 13:19 Filling Site Sample Group WATER ANALYSES Sample Type / Name / Brand / Manufacturer NATURAL MINERAL WATER
--- KIZILAY KIZILAY İÇECEK
SANAYİ VE TİCARET A.Ş.
Sample Packaging Type/ Label/ Amount Original Package + Glass Bottle
LABELED 200cc x 60
Sample Mnf.Date/ Exp.Date/ Batch No / Serial No 20.08.2020 20.11.2021 PN233 0944 Seal Status / Minute-Contract Date/No SEALED ... ... ... Invoiced To KIZILAY İÇECEK SANAYİ VE TİCARET A.Ş. Receipt Date and No / Voucher Date and No ______ . ______ ... Declr. Date-No /Import Pre-Approval Doc. Date-No ____________________________ Condition of the Sample Suitable for Analysis Sample Information ... ... Analysis Start/End Date 21.08.2020 13:20 04.09.2020 13:55 Reporting Date 05.09.2020 14:26
CHEMICAL ANALYSES Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Carbonate mg/L Spectrophotometric # 0 MICROBIOLOGICAL ANALYSES Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
*Total germ count at 22 °C cfu/mL TS EN ISO 6222 100 1 Parasite pcs/5 L Internal method 0 0 Pathogen Staphylococ. cfu/100mL AFNOR NFT 90-412 0 0 *Pseudomonas aeruginosa cfu/250mL TS EN ISO 16266 0 0 *Sulfite Reducing Spore- formingAnaerobic Bacteria
cfu/50mL TS 8020 EN 26461-2 0 0
*Escherichia coli cfu/250mL TS EN ISO 9308-1 0 0
(logo: REPUBLIC OF TURKEY, MINISTRY OF HEALTH)
REPUBLIC OF TURKEY GOVERNORSHIP OF SAMSUN PROVINCIAL HEALTH DIRACTORATE SAMSUN PUBLIC HEALTH LABORATORY ANALYSIS REPORT
F81/SHSL/03 Report Printing Date : 07.09.2020 Address: Adalet Mahallesi Mevlana Cad. No:66 55070 İlkadım / SAMSUN Tel: 03622348950 Fax: 03622303772 This document has been signed with secure electronic signature pursuant to the electronic signature law no. 5070.
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Ref. Date and No 19.08.2020 / 2672 AB-0834-T Date/Time of Sampling 20.08.2020 / 10:30 Date/Time of Sample Incoming to HSL (Lab) 20.08.2020 / 16:12 2020-1960-1 Protocol No / Sample Barcode No 2020-1960 - 1 / 11161816 CSBYS No 118715 09.20 Report Page Number 6
MICROBIOLOGICAL ANALYSES Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Salmonella Spp. cfu/L TS EN ISO 19250 0 Not Found *Total germ count at 37°C cfu/mL TS EN ISO 6222 20 1 *Coliform Bacteria cfu/250mL AFNOR NFT 9308-1 0 0 *Enterococ./ Fecal Streptococ. cfu/250mL TS EN ISO 7899-2 0 0
CHEMICAL ANALYSES Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Turbidity (Physical) Physical conforming Odor (Physical) Physical conforming Sulphur mg/L Spectrophotometric 0 Color (Physical) Physical conforming Taste (Physical) Physical conforming Bicarbonate TITRIMETRIC # 1475 Oxidizability mg/L TITRIMETRIC 2.56 Cyanide Spectrophotometric 0.01 0.07 Not Found Nitrate mg/L TS EN ISO 10304-1 0.15 50 0.25 Magnesium mg/L TS EN ISO 14911 0.1 312 Sulfate mg/L TS EN ISO 10304-1 0.15 1.38 *Phosphate mg/L TS EN ISO 10304-1 0.3 0.31 Sodium mg/L TS EN ISO 14911 0.4 114 Calcium mg/L TS EN ISO 14911 1 47.0 Potassium mg/L TS EN ISO 14911 1 3.92 Chloride mg/L TS EN ISO 10304-1 0.15 150 Nitrite mg/L TS EN ISO 10304-1 0.02 0.1 Not Found Ammonium mg/L TS EN ISO 14911 0.01 0.79 Fluoride mg/L TS EN ISO 10304-1 0.03 5 0.060 *Copper mg/L EPA 200.8 0.002 1 Not Found
(logo: REPUBLIC OF TURKEY, MINISTRY OF HEALTH)
REPUBLIC OF TURKEY GOVERNORSHIP OF SAMSUN PROVINCIAL HEALTH DIRACTORATE SAMSUN PUBLIC HEALTH LABORATORY ANALYSIS REPORT
Address: Adalet Mahallesi Mevlana Cad. No:66 55070 İlkadım / SAMSUN Tel: 03622348950 Fax: 03622303772 This document has been signed with secure electronic signature pursuant to the electronic signature law no. 5070.
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Ref. Date and No 19.08.2020 / 2672 AB-0834-T Date/Time of Sampling 20.08.2020 / 10:30 Date/Time of Sample Incoming to HSL (Lab) 20.08.2020 / 16:12 2020-1960-1 Protocol No / Sample Barcode No 2020-1960 - 1 / 11161816 CSBYS No 118715 09.20 Report Page Number 6
CHEMICAL ANALYSES Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
*Arsenic mg/L EPA 200.8 0.002 0.01 Not Found
*Aluminum mg/L EPA 200.8 2 200 5.53
Borate mg/L EPA 200.8 30 9.16
*Lead mg/L EPA 200.8 0.002 0.01 Not Found
*Cadmium mg/L EPA 200.8 0.002 0.003 Not Found
*Mercury mg/L EPA 200.8 0.00015 0.001 Not Found
*Barium mg/L EPA 200.8 0.002 1 0.032
*Nickel mg/L EPA 200.8 0.002 0.02 Not Found
*Chrome mg/L EPA 200.8 0.002 0.05 0.011
*Antimony mg/L EPA 200.8 0.002 0.005 Not Found
*Manganese mg/L EPA 200.8 0.002 0.5 0.139
*Iron mg/L EPA 200.8 0.002 0.046
*Selenium mg/L EPA 200.8 0.002 0.01 0.007
Organochlorine Compounds Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Alpha-Endosulfan mg/L Internal Method 0.00001 0.0001 Not Found
Total DDT (op-DDT, pp-DDT, pp-DDD, pp-DDE)
mg/L Internal Method 0.00001 0.0001 Not Found
HCB mg/L Internal Method 0.00001 0.0001 Not Found
Dieldrin mg/L Internal Method 0.00001 0.00003 Not Found
Gamma - HCH (Lindane) mg/L Internal Method 0.00001 0.0001 Not Found
Heptachlor Epoxide (Endo) mg/L Internal Method 0.00001 0.00003 Not Found
Alpha-HCH (BCH) mg/L Internal Method 0.00001 0.0001 Not Found F81/SHSL/03 Report Printing Date :07.09.2020
(logo: REPUBLIC OF TURKEY, MINISTRY OF HEALTH)
REPUBLIC OF TURKEY GOVERNORSHIP OF SAMSUN PROVINCIAL HEALTH DIRACTORATE SAMSUN PUBLIC HEALTH LABORATORY ANALYSIS REPORT
F81/SHSL/03 Report Printing Date : 07.09.2020 Address: Adalet Mahallesi Mevlana Cad. No:66 55070 İlkadım / SAMSUN Tel: 03622348950 Fax: 03622303772 This document has been signed with secure electronic signature pursuant to the electronic signature law no. 5070.
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Ref. Date and No 19.08.2020 / 2672 AB-0834-T Date/Time of Sampling 20.08.2020 / 10:30 Date/Time of Sample Incoming to HSL (Lab) 20.08.2020 / 16:12 2020-1960-1 Protocol No / Sample Barcode No 2020-1960 - 1 / 11161816 CSBYS No 118715 09.20 Report Page Number 6
Organochlorine Compounds Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Aldrin mg/L Internal Method 0.00001 0.00003 Not Found
Beta-Endosulfan mg/L Internal Method 0.00001 0.0001 Not Found
Heptachlor mg/L Internal Method 0.00001 0.00003 Not Found
Organophosphorus Compounds Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Azinphos-methyl mg/L Internal Method 0.00001 0.0001 Not Found
Chlorpyriphos-ethyl mg/L Internal Method 0.00001 0.0001 Not Found
Ethion mg/L Internal Method 0.00001 0.0001 Not Found
Parathion-ethyl mg/L Internal Method 0.00001 0.0001 Not Found
Disulfoton mg/L Internal Method 0.00001 0.0001 Not Found
Diazinon mg/L Internal Method 0.00001 0.0001 Not Found
Parathion-methyl mg/L Internal Method 0.00001 0.0001 Not Found
Azinphos-ethyl mg/L Internal Method 0.00001 0.0001 Not Found
Chlorpyripho s -methyl mg/L Internal Method 0.00001 0.0001 Not Found
Demethon (O+S) mg/L Internal Method 0.00001 0.0001 Not Found
Malathion mg/L Internal Method 0.00001 0.0001 Not Found
Carbamates Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Methiocarb mg/L Internal / LCMSMS Not Found
Aldicarb mg/L Internal / LCMSMS Not Found
(logo: REPUBLIC OF TURKEY, MINISTRY OF HEALTH)
REPUBLIC OF TURKEY GOVERNORSHIP OF SAMSUN PROVINCIAL HEALTH DIRACTORATE SAMSUN PUBLIC HEALTH LABORATORY ANALYSIS REPORT
F81/SHSL/03 Report Printing Date : 07.09.2020 Address: Adalet Mahallesi Mevlana Cad. No:66 55070 İlkadım / SAMSUN Tel: 03622348950 Fax: 03622303772 This document has been signed with secure electronic signature pursuant to the electronic signature law no. 5070.
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Ref. Date and No 19.08.2020 / 2672 AB-0834-T Date/Time of Sampling 20.08.2020 / 10:30 Date/Time of Sample Incoming to HSL (Lab) 20.08.2020 / 16:12 2020-1960-1 Protocol No / Sample Barcode No 2020-1960 - 1 / 11161816 CSBYS No 118715 09.20 Report Page Number 6
Carbamates Analyses Unit Method Limit of Quantification
(LOQ) Legislation Limit Result
Aldicarb-sulfoxide mg/L Internal / LCMSMS Not Found
Oxamyl mg/L Internal / LCMSMS Not Found
Carbofuran mg/L Internal / LCMSMS Not Found
Carbaryl mg/L Internal / LCMSMS Not Found
1-Naphtol mg/L Internal / LCMSMS Not Found
Aldicarb-sulfane mg/L Internal / LCMSMS Not Found
Carbofuran-3 -hydroxy mg/L Internal / LCMSMS Not Found
Propoxur mg/L Internal / LCMSMS Not Found
Methomyl mg/L Internal / LCMSMS Not Found Polycyclic Aromatic Hydrocarbons
Analyses Unit Method Limit of Quantification (LOQ)
Legislation Limit Result
*Benzo (b) fluoranthene mg/L Internal / HPLC Not Found
*Benzo (k) fluoranthene mg/L Internal / HPLC Not Found
*Benzo (ghi) perylene mg/L Internal / HPLC Not Found
*Fluoranthene mg/L Internal / HPLC Not Found
*Indeno (1.2.3 -cd) pyrene mg/L Internal / HPLC Not Found
*Benzo (a) pyrene mg/L Internal / HPLC Not Found
(logo: REPUBLIC OF TURKEY, MINISTRY OF HEALTH)
REPUBLIC OF TURKEY GOVERNORSHIP OF SAMSUN PROVINCIAL HEALTH DIRACTORATE SAMSUN PUBLIC HEALTH LABORATORY ANALYSIS REPORT
F81/SHSL/03 Report Printing Date : 07.09.2020 Address: Adalet Mahallesi Mevlana Cad. No:66 55070 İlkadım / SAMSUN Tel: 03622348950 Fax: 03622303772 This document has been signed with secure electronic signature pursuant to the electronic signature law no. 5070.
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Ref. Date and No 19.08.2020 / 2672 AB-0834-T Date/Time of Sampling 20.08.2020 / 10:30 Date/Time of Sample Incoming to HSL (Lab) 20.08.2020 / 16:12 2020-1960-1 Protocol No / Sample Barcode No 2020-1960 - 1 /11161816 CSBYS No 118715 09.20 Report Page Number 6
Evaluation: The results for the tested parameters are conforming as per Regulation on Natural Mineral Waters published in the Offıcial Gazette dated 01.12.2004 no 25657.
Remarks: - The results are evaluated as per Regulation on Natural Mineral Waters published in the Offıcial Gazette dated 01.12.2004 no 25657. - The analysis results written bold are out of the relevant legislation limit. - The sample was no taken by us, but received in accordance with SAMSUN PUBLIC HEALTH LABORATORY Sample Acceptance Criteria, based on the information provided by the customer.- The analyses on special request were performed based on the information provided by the customer, and evaluated for conformity as per the applicable regulation. - The results and opinions in this report apply to the above-mentioned and tested sample in its condition when received. No section of this report can be used separately or partially, and the report cannot be reproduced without the permission of SAMSUN PUBLIC HEALTH LABORATORY. Unsigned reports are invalid. Reports of sample analyses on special request cannot be used for judicial andadministrative procedures and for advertisement purposes. - Extended measurement uncertainties are stated when requested by the customer or required by legal legislations. - TKEDY: Acceptable for consumers or no abnormal change - cfu: Colony forming unit - Tests marked with * are within the scope of accreditation. - When not requested by the customer or required by legal legislations, the analytical results are reported as x. “x” indicates the analytical result. - When the customer requests measurement uncertainty, the analytical results are reported as x=Ux, where x refers to the analytical result and U refers to extended measurement uncertainty. TGHSLDB (Consumer Safety and Public Health Laboratories Department) Decision Rule: - In case the customer requests measurement uncertainty, the result found for the relevant parameter within the confidence interval determined by the laboratory (k=2, 95%) is
considered “non-conforming” if above the upper legislation limit when the measurement uncertainty is added to the result, or if below the lower legislation limit when the measurement uncertainty issubtracted from the result. The results that are within or equal to the specified legislation limits are considered “conforming”.
Water Microbiology Laboratory Function Supervisor Ümran ALBAYRAK Biologist
05.09.2020
Environmental Sciences Laboratory Function Supervisor HASAN ALTAY Food Engineer
05.09.2020 Laboratory Supervisor DUYGU SAVCI Spec. Dr. 05.09.2020