L C - M S Report Sample Name LY294002-03 : Data File : D:\DATA-LCMS-13\2019\10-19\31\1\LY294002-03.D Injection Date : Thu, 31. Oct. 2019 Inj. Vol. : 5ul Acq Operator : LCMS-13 Location : Vial 31 Acq. Method : D:\data-lcms-13\2019\10-19\31\1\P-05-95-C2.M Method Info. : column:C18;column size:4.6*50mm ;mobile phase:B(ACN) ! A(0.02%NH4Ac); gradient(B%) as Acq.Method above min 2 4 6 mAU -500 0 500 1000 1500 2000 DAD1 A, Sig=214,8 Ref=off (D:\DATA-LCMS-13\2019\10-19\31\1\LY294002-03.D) 3.268 min 2 4 6 mAU 0 200 400 600 800 1000 DAD1 B, Sig=254,16 Ref=off (D:\DATA-LCMS-13\2019\10-19\31\1\LY294002-03.D) 3.265 min 2 4 6 0 500000 1000000 1500000 2000000 2500000 MSD1 TIC, MS File (D:\DATA-LCMS-13\2019\10-19\31\1\LY294002-03.D) MM-ES+APCI, Pos, Scan, Frag: 80 3.299 ========================================================================== Integration Results ========================================================================== Signal 1: DAD1 A, Sig=214,8 Ref=off # R.T. Type Height Height% Width Area Area % ----------------------------------------------------------------- 1 3.268 MF 2921.012 100.000 0.073 12793.646 100.000 ----------------------------------------------------------------- Instrument 1 Thu, 31. Oct. 2019 01:41:21 pm Page 1 of 2