LABORATORY REPORT · 2018. 11. 18. · 12/11/09 Report Number: 12/11/09 Project ID: PSL0747 14682.013 SAMPLE RECEIPT: Samples were received intact, at 1°C, on ice and with chain

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)

454-9303

LABORATORY REPORT

Prepared For: AMEC Geomatrix Consultants, Inc. - AZ - PGAN

8777 E. Via de Ventura, Suite 396

Scottsdale, AZ 85258

Attention: Brian Mcnamara Sampled:

Received:

Issued:

12/11/09

12/11/09

12/30/09 10:13

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report

were performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless

otherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This

report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain(s) of Custody, 3 pages, are

included and are an integral part of this report.

This entire report was reviewed and approved for release.

Project: 14682.013

NELAP #01109CA Arizona DHS#AZ0728

CASE NARRATIVE

MATRIXCLIENT IDLABORATORY ID

PSL0747-01 ABI-60-121109 Soil

PSL0747-02 ABI-70-121109 Soil

PSL0747-03 ABI-80-121109 DUP Soil

PSL0747-04 ABI-80-121109 Soil

PSL0747-05 ABI-90-121109 Soil

PSL0747-06 ABI-97-121109 Water

PSL0747-07 EB001-121109 Water

PSL0747-08 Trip Blank Water

PSL0747-09 EB001-121109 Water

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas

<Page 1 of 44>

SDMS DOCID#1142215


454-9303

AMEC Geomatrix Consultants, Inc. - AZ - PGAN



Attention: Brian Mcnamara

Sampled:

Received:

12/11/09

12/11/09Report Number:

Project ID:

PSL0747

14682.013

SAMPLE RECEIPT: Samples were received intact, at 1°C, on ice and with chain of custody documentation.

Soil samples for volatile analysis were received as Methanol Kits.

HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica

Sample Acceptance Policy unless otherwise noted in the report.

PRESERVATION: Samples requiring preservation were verified prior to sample analysis.

QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers.

L3-Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the

acceptance limits. Analyte not detected, data not impacted.

L4-Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was below

acceptance limits.

S10-Surrogate recovery was above acceptance limits.

N1-Batch P9L1429 -The LCS recovered high and outside of the project specific acceptance limits for

Chloroethane and n-Propylbenzene. The LCSD and MS/MSD also recovered high and outside of the

project specific acceptance limits for Chlorethane. All recoveries were within the laboratory's historical

limits. All associated samples were non-detect for these compounds and therefore should not be impacted.

N1-Batch P9L1429-The LCS/LCSD and MS/MSD recovered low and outside of the project specific

acceptance limits for Vinyl Chloride. The recoveries were within the laboratory's historical limits. The

sample are field methanol extracted soils and therefore could not be re-extracted and re-analyzed.

N1-Batch P9L1638-The LCS/LCSD and MS/MSD recovered high and outside of acceptance limits for

Vinyl Acetate. All associated samples are non-detect for this compound and therefore should not be

impacted.

N1-Batch P9L1638-The surrogate, Toluene-d8, recovered high and outside of the project specific

acceptance limits in the LCS/LCSD. The recoveries were within the laboratory's historical limits. All

surrogate recoveries in the Method Blank, MS/MSD and associated samples were within the project specific

limits. The data should not be impacted.

COMMENTS: Results that fall between the MDL and RL are 'J' flagged.

SUBCONTRACTED: No analyses were subcontracted to an outside laboratory.

Reviewed By:

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas

The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 2 of 44>


454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-06 (ABI-97-121109 - Water)

Reporting Units: ug/l

SW8260B1,1,2,2-Tetrachloroethane P9L1638 1.0 ND E812/16/09 12/16/0910.12

1,1-Dichloroethene SW8260B P9L1638 0.421.0 E412/16/09 12/16/0910.23

SW8260B1,2-Dichloropropane P9L1638 1.0 ND E812/16/09 12/16/0910.15

SW8260B2-Butanone (MEK) P9L1638 5.0 ND E812/16/09 12/16/0911.8

SW8260BAcetone P9L1638 20 ND E812/16/09 12/16/0913.8

SW8260BBenzene P9L1638 1.0 ND E812/16/09 12/16/0910.15

SW8260BCarbon tetrachloride P9L1638 1.0 ND E812/16/09 12/16/0910.19

Chloroform SW8260B P9L1638 1.11.0 12/16/09 12/16/0910.16

SW8260Bcis-1,2-Dichloroethene P9L1638 1.0 ND E812/16/09 12/16/0910.18

SW8260BEthylbenzene P9L1638 1.0 ND E812/16/09 12/16/0910.16

SW8260Bm,p-Xylenes P9L1638 2.0 ND E812/16/09 12/16/0910.35

SW8260BMethylene Chloride P9L1638 2.0 ND E812/16/09 12/16/0910.50

SW8260Bo-Xylene P9L1638 1.0 ND E812/16/09 12/16/0910.19

Tetrachloroethene SW8260B P9L1638 0.531.0 E412/16/09 12/16/0910.23

SW8260BToluene P9L1638 1.0 ND E812/16/09 12/16/0910.35

SW8260Btrans-1,2-Dichloroethene P9L1638 1.0 ND E812/16/09 12/16/0910.22

SW8260BTrichlorofluoromethane P9L1638 1.0 ND E812/16/09 12/16/0910.17

SW8260BVinyl chloride P9L1638 1.0 ND E812/16/09 12/16/0910.24

SW8260B1,1,1-Trichloroethane P9L1638 1.0 ND E812/16/09 12/16/0910.22


SW8260B1,1-Dichloroethane P9L1638 1.0 ND E812/16/09 12/16/0910.17

SW8260B1,1-Dichloropropene P9L1638 1.0 ND E812/16/09 12/16/0910.19

SW8260B1,2,3-Trichlorobenzene P9L1638 2.0 ND E812/16/09 12/16/0910.27

SW8260B1,2,3-Trichloropropane P9L1638 2.0 ND E812/16/09 12/16/0910.31


SW8260B1,2,4-Trimethylbenzene P9L1638 1.0 ND E812/16/09 12/16/0910.13

SW8260B1,2-Dibromoethane (EDB) P9L1638 1.0 ND E812/16/09 12/16/0910.14

SW8260B1,2-Dichlorobenzene P9L1638 1.0 ND E812/16/09 12/16/0910.12







SW8260B2-Chlorotoluene P9L1638 1.0 ND E812/16/09 12/16/0910.17

SW8260B2-Hexanone P9L1638 5.0 ND E812/16/09 12/16/0910.31


SW8260B4-Methyl-2-pentanone (MIBK) P9L1638 5.0 ND E812/16/09 12/16/0910.43

SW8260BBromobenzene P9L1638 1.0 ND E812/16/09 12/16/0910.15

SW8260BBromochloromethane P9L1638 1.0 ND E812/16/09 12/16/0910.20

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-06 (ABI-97-121109 - Water) - cont.


SW8260BBromodichloromethane P9L1638 1.0 ND E812/16/09 12/16/0910.15

SW8260BBromoform P9L1638 1.0 ND E812/16/09 12/16/0910.19

SW8260BBromomethane P9L1638 2.0 ND E812/16/09 12/16/0910.22

SW8260BChlorobenzene P9L1638 1.0 ND E812/16/09 12/16/0910.12

SW8260BChloroethane P9L1638 1.0 ND E812/16/09 12/16/0910.26

SW8260BChloromethane P9L1638 5.0 ND E812/16/09 12/16/0910.20

SW8260Bcis-1,3-Dichloropropene P9L1638 1.0 ND E812/16/09 12/16/0910.17

SW8260BDibromochloromethane P9L1638 1.0 ND E812/16/09 12/16/0910.15

SW8260BDichlorodifluoromethane P9L1638 1.0 ND E812/16/09 12/16/0910.15

SW8260BMethyl-tert-butyl Ether (MTBE) P9L1638 1.0 ND E812/16/09 12/16/0910.18

SW8260Bn-Butylbenzene P9L1638 1.0 ND E812/16/09 12/16/0910.17

SW8260Bn-Propylbenzene P9L1638 1.0 ND E812/16/09 12/16/0910.18

SW8260Bp-Isopropyltoluene P9L1638 1.0 ND E812/16/09 12/16/0910.21

SW8260Bsec-Butylbenzene P9L1638 1.0 ND E812/16/09 12/16/0910.14

SW8260BStyrene P9L1638 1.0 ND E812/16/09 12/16/0910.15

SW8260Btert-Butylbenzene P9L1638 1.0 ND E812/16/09 12/16/0910.17

SW8260Btrans-1,3-Dichloropropene P9L1638 1.0 ND E812/16/09 12/16/0910.097

SW8260BVinyl Acetate P9L1638 1.0 ND E8, L312/16/09 12/16/0910.21

Surrogate: Dibromofluoromethane (80.3-130%) 131 % S10

Surrogate: Toluene-d8 (88.4-111%) 107 %

Surrogate: 4-Bromofluorobenzene (86.5-114%) 106 %

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-06RE1 (ABI-97-121109 - Water) - cont.


Trichloroethene SW8260B P9L1638 29010 12/16/09 12/16/09101.9

Surrogate: Dibromofluoromethane (80.3-130%) 122 %



Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-07 (EB001-121109 - Water)



SW8260B1,1-Dichloroethene P9L1638 1.0 ND E812/16/09 12/16/0910.23



Acetone SW8260B P9L1638 9.220 E412/16/09 12/16/0913.8



Chloroform SW8260B P9L1638 0.201.0 E412/16/09 12/16/0910.16






SW8260BTetrachloroethene P9L1638 1.0 ND E812/16/09 12/16/0910.23



SW8260BTrichloroethene P9L1638 1.0 ND E812/16/09 12/16/0910.19
























Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-07 (EB001-121109 - Water) - cont.




















SW8260BVinyl Acetate P9L1638 1.0 ND L3, E812/16/09 12/16/0910.21




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-08 (Trip Blank - Water)









SW8260BChloroform P9L1638 1.0 ND E812/16/09 12/16/0910.16

































Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-08 (Trip Blank - Water) - cont.
























Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-09 (EB001-121109 - Water)






Acetone SW8260B P9L1638 9.620 E412/16/09 12/16/0913.8




































Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-09 (EB001-121109 - Water) - cont.
























Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

VOLATILE ORGANICS BY GC/MS (EPA 5035/8260B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-01 (ABI-60-121109 - Soil)

Reporting Units: ug/kg

SW8260B1,1,1-Trichloroethane P9L1429 50 ND E812/12/09 12/22/090.92919

SW8260B1,1,2,2-Tetrachloroethane P9L1429 50 ND E812/12/09 12/22/090.92918


SW8260B1,1-Dichloroethane P9L1429 50 ND E812/12/09 12/22/090.92915

SW8260B1,1-Dichloroethene P9L1429 50 ND E812/12/09 12/22/090.92923

SW8260B1,1-Dichloropropene P9L1429 50 ND E812/12/09 12/22/090.92919

SW8260B1,2,3-Trichlorobenzene P9L1429 100 ND E812/12/09 12/22/090.92918

SW8260B1,2,3-Trichloropropane P9L1429 100 ND E812/12/09 12/22/090.92920


SW8260B1,2,4-Trimethylbenzene P9L1429 50 ND E812/12/09 12/22/090.92927

SW8260B1,2-Dibromoethane (EDB) P9L1429 50 ND E812/12/09 12/22/090.92916

SW8260B1,2-Dichlorobenzene P9L1429 50 ND E812/12/09 12/22/090.92921


SW8260B1,2-Dichloropropane P9L1429 50 ND E812/12/09 12/22/090.92919






SW8260B2-Butanone (MEK) P9L1429 250 ND E812/12/09 12/22/090.929200

SW8260B2-Chlorotoluene P9L1429 50 ND E812/12/09 12/22/090.92915

SW8260B2-Hexanone P9L1429 250 ND E812/12/09 12/22/090.929210


SW8260B4-Methyl-2-pentanone (MIBK) P9L1429 250 ND E812/12/09 12/22/090.929170


SW8260BBenzene P9L1429 50 ND E812/12/09 12/22/090.92923

SW8260BBromobenzene P9L1429 50 ND E812/12/09 12/22/090.92918

SW8260BBromochloromethane P9L1429 50 ND E812/12/09 12/22/090.92924

SW8260BBromodichloromethane P9L1429 50 ND E812/12/09 12/22/090.92918

SW8260BBromoform P9L1429 50 ND E812/12/09 12/22/090.92920

SW8260BBromomethane P9L1429 250 ND E812/12/09 12/22/090.9298.3

SW8260BCarbon tetrachloride P9L1429 50 ND E812/12/09 12/22/090.92920

SW8260BChlorobenzene P9L1429 50 ND E812/12/09 12/22/090.92911

SW8260BChloroethane P9L1429 50 ND E812/12/09 12/22/090.92931

SW8260BChloroform P9L1429 50 ND E812/12/09 12/22/090.92924

SW8260BChloromethane P9L1429 250 ND E812/12/09 12/22/090.92926

SW8260Bcis-1,2-Dichloroethene P9L1429 50 ND E812/12/09 12/22/090.92921

SW8260Bcis-1,3-Dichloropropene P9L1429 50 ND E812/12/09 12/22/090.92915

SW8260BDibromochloromethane P9L1429 50 ND E812/12/09 12/22/090.92911

SW8260BDichlorodifluoromethane P9L1429 50 ND E812/12/09 12/22/090.92919

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-01 (ABI-60-121109 - Soil) - cont.


SW8260BEthylbenzene P9L1429 50 ND E812/12/09 12/22/090.92913

SW8260Bm,p-Xylenes P9L1429 100 ND E812/12/09 12/22/090.92934

SW8260BMethylene Chloride P9L1429 100 ND E812/12/09 12/22/090.92932

SW8260BMethyl-tert-butyl Ether (MTBE) P9L1429 50 ND E812/12/09 12/22/090.92917

SW8260Bn-Butylbenzene P9L1429 50 ND E812/12/09 12/22/090.92918

SW8260Bn-Propylbenzene P9L1429 50 ND E812/12/09 12/22/090.92917

SW8260Bo-Xylene P9L1429 50 ND E812/12/09 12/22/090.92916

SW8260Bp-Isopropyltoluene P9L1429 50 ND E812/12/09 12/22/090.92920

SW8260Bsec-Butylbenzene P9L1429 50 ND E812/12/09 12/22/090.92918

SW8260BStyrene P9L1429 50 ND E812/12/09 12/22/090.92912

SW8260Btert-Butylbenzene P9L1429 50 ND E812/12/09 12/22/090.92920

SW8260BTetrachloroethene P9L1429 50 ND E812/12/09 12/22/090.9299.6

SW8260BToluene P9L1429 50 ND E812/12/09 12/22/090.92915

SW8260Btrans-1,2-Dichloroethene P9L1429 50 ND E812/12/09 12/22/090.92918

SW8260Btrans-1,3-Dichloropropene P9L1429 50 ND E812/12/09 12/22/090.92915

SW8260BTrichloroethene P9L1429 50 ND E812/12/09 12/22/090.92921

SW8260BTrichlorofluoromethane P9L1429 50 ND E812/12/09 12/22/090.92932

SW8260BVinyl Acetate P9L1429 50 ND E812/12/09 12/22/090.92926

SW8260BVinyl chloride P9L1429 50 ND E812/12/09 12/22/090.92925




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-03 (ABI-80-121109 DUP - Soil)










































Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0747-03 (ABI-80-121109 DUP - Soil) - cont.
























Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit




































SW8260BChloroethane P9L1429 50 ND N1, E812/12/09 12/18/090.99931







Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit





Methylene Chloride SW8260B P9L1429 38100 E412/12/09 12/18/090.99932



SW8260Bn-Propylbenzene P9L1429 50 ND E8, N112/12/09 12/18/090.99917












SW8260BVinyl Acetate P9L1429 50 ND E8, M212/12/09 12/18/090.99926

SW8260BVinyl chloride P9L1429 50 ND E8, L412/12/09 12/18/090.99925




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit




































SW8260BChloroethane P9L1429 45 ND E8, N112/12/09 12/18/090.89327







Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bn-Propylbenzene P9L1429 45 ND E8, N112/12/09 12/18/090.89315













SW8260BVinyl chloride P9L1429 45 ND E8, L412/12/09 12/18/090.89322




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

SHORT HOLD TIME DETAIL REPORT

Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: ABI-60-121109 (PSL0747-01) - Soil

2 12/11/2009 09:44 12/11/2009 17:17 12/12/2009 12:45 12/22/2009 19:47SW8260B


2 12/11/2009 11:00 12/11/2009 17:17 12/12/2009 12:45 12/22/2009 20:19SW8260B

Sample ID: ABI-80-121109 DUP (PSL0747-03) - Soil

2 12/11/2009 12:30 12/11/2009 17:17 12/12/2009 12:45 12/22/2009 20:50SW8260B


2 12/11/2009 12:25 12/11/2009 17:17 12/12/2009 12:45 12/18/2009 04:49SW8260B


2 12/11/2009 14:00 12/11/2009 17:17 12/12/2009 12:45 12/18/2009 05:21SW8260B

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte


METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: P9L1638 Extracted: 12/16/09

Blank Analyzed: 12/16/2009 (P9L1638-BLK1)

1,1,2,2-Tetrachloroethane ug/l1.0ND 0.12

1,1-Dichloroethene ug/l1.0ND 0.23

1,2-Dichloropropane ug/l1.0ND 0.15

2-Butanone (MEK) ug/l5.0ND 1.8

Acetone ug/l20ND 3.8

Benzene ug/l1.0ND 0.15

Carbon tetrachloride ug/l1.0ND 0.19

Chloroform ug/l1.0ND 0.16

cis-1,2-Dichloroethene ug/l1.0ND 0.18

Ethylbenzene ug/l1.0ND 0.16

m,p-Xylenes ug/l2.0ND 0.35

Methylene Chloride ug/l2.0ND 0.50

o-Xylene ug/l1.0ND 0.19

Tetrachloroethene ug/l1.0ND 0.23

Toluene ug/l1.0ND 0.35

trans-1,2-Dichloroethene ug/l1.0ND 0.22

Trichloroethene ug/l1.0ND 0.19

Trichlorofluoromethane ug/l1.0ND 0.17

Vinyl chloride ug/l1.0ND 0.24

1,1,1-Trichloroethane ug/l1.0ND 0.22


1,1-Dichloroethane ug/l1.0ND 0.17

1,1-Dichloropropene ug/l1.0ND 0.19

1,2,3-Trichlorobenzene ug/l2.0ND 0.27

1,2,3-Trichloropropane ug/l2.0ND 0.31

1,2,4-Trichlorobenzene ug/l1.00.210 E40.18

1,2,4-Trimethylbenzene ug/l1.0ND 0.13

1,2-Dibromoethane (EDB) ug/l1.0ND 0.14

1,2-Dichlorobenzene ug/l1.0ND 0.12







Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene ug/l1.0ND 0.17

2-Hexanone ug/l5.0ND 0.31


4-Methyl-2-pentanone (MIBK) ug/l5.0ND 0.43

Bromobenzene ug/l1.0ND 0.15

Bromochloromethane ug/l1.0ND 0.20

Bromodichloromethane ug/l1.0ND 0.15

Bromoform ug/l1.0ND 0.19

Bromomethane ug/l2.0ND 0.22

Chlorobenzene ug/l1.0ND 0.12

Chloroethane ug/l1.0ND 0.26

Chloromethane ug/l5.0ND 0.20

cis-1,3-Dichloropropene ug/l1.0ND 0.17

Dibromochloromethane ug/l1.0ND 0.15

Dichlorodifluoromethane ug/l1.0ND 0.15

Methyl-tert-butyl Ether (MTBE) ug/l1.0ND 0.18

n-Butylbenzene ug/l1.0ND 0.17

n-Propylbenzene ug/l1.0ND 0.18

p-Isopropyltoluene ug/l1.0ND 0.21

sec-Butylbenzene ug/l1.0ND 0.14

Styrene ug/l1.0ND 0.15

tert-Butylbenzene ug/l1.0ND 0.17

trans-1,3-Dichloropropene ug/l1.0ND 0.097

Vinyl Acetate ug/l1.0ND 0.21

25.0 80.3-130Surrogate: Dibromofluoromethane ug/l29.6 119

25.0 88.4-111Surrogate: Toluene-d8 ug/l26.8 107

25.0 86.5-114Surrogate: 4-Bromofluorobenzene ug/l26.0 104

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/16/2009 (P9L1638-BS1)

1,1,2,2-Tetrachloroethane ug/l1.026.3 70.5-12525.00.12 105

1,1-Dichloroethene ug/l1.023.1 81.7-12225.00.23 92

1,2-Dichloropropane ug/l1.025.9 85-11525.00.15 104

2-Butanone (MEK) ug/l5.028.8 45.6-14125.01.8 115

Acetone ug/l2035.7 22.4-15325.03.8 143

Benzene ug/l1.023.8 80.7-12025.00.15 95

Carbon tetrachloride ug/l1.023.2 82.5-12325.00.19 93

Chloroform ug/l1.024.3 80.7-11925.00.16 97

cis-1,2-Dichloroethene ug/l1.022.4 83.3-11725.00.18 89

Ethylbenzene ug/l1.023.3 85-11525.00.16 93

m,p-Xylenes ug/l2.022.4 85-11525.00.35 90

Methylene Chloride ug/l2.025.1 79.7-11725.00.50 100

o-Xylene ug/l1.022.4 85-11525.00.19 89

Tetrachloroethene ug/l1.023.2 85-11525.00.23 93

Toluene ug/l1.022.7 85-11525.00.35 91

trans-1,2-Dichloroethene ug/l1.024.0 82.3-12025.00.22 96

Trichloroethene ug/l1.023.5 85-11525.00.19 94

Trichlorofluoromethane ug/l1.023.8 84.5-12325.00.17 95

Vinyl chloride ug/l1.024.2 80.9-12725.00.24 97

1,1,1-Trichloroethane ug/l1.023.8 83.2-12025.00.22 95

1,1,2-Trichloroethane ug/l1.023.5 85-11525.00.19 94

1,1-Dichloroethane ug/l1.025.6 78.8-12225.00.17 102

1,1-Dichloropropene ug/l1.024.2 82.3-11925.00.19 97

1,2,3-Trichlorobenzene ug/l2.023.6 60.4-17125.00.27 94

1,2,3-Trichloropropane ug/l2.025.5 76.3-12525.00.31 102

1,2,4-Trichlorobenzene ug/l1.022.7 71-13625.00.18 91

1,2,4-Trimethylbenzene ug/l1.024.2 78.1-12025.00.13 97

1,2-Dibromoethane (EDB) ug/l1.023.2 85-11525.00.14 93

1,2-Dichlorobenzene ug/l1.024.5 85-11525.00.12 98



1,3-Dichlorobenzene ug/l1.024.2 83.9-11425.00.18 97



2,2-Dichloropropane ug/l2.023.1 70.8-12825.00.18 93

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene ug/l1.025.2 78.6-12025.00.17 101

2-Hexanone ug/l5.024.1 58.5-13525.00.31 97


4-Methyl-2-pentanone (MIBK) ug/l5.023.8 72-12925.00.43 95

Bromobenzene ug/l1.025.0 83.3-11625.00.15 100

Bromochloromethane ug/l1.023.8 83-12225.00.20 95

Bromodichloromethane ug/l1.023.6 84-11725.00.15 94

Bromoform ug/l1.021.8 71.9-13125.00.19 87

Bromomethane ug/l2.025.8 56.3-14525.00.22 103

Chlorobenzene ug/l1.023.4 82.5-12325.00.12 94

Chloroethane ug/l1.024.4 69.5-13225.00.26 98

Chloromethane ug/l5.024.0 70.9-12325.00.20 96

cis-1,3-Dichloropropene ug/l1.024.8 85-11525.00.17 99

Dibromochloromethane ug/l1.022.6 83.2-12325.00.15 91

Dichlorodifluoromethane ug/l1.022.0 72.8-13025.00.15 88

Methyl-tert-butyl Ether (MTBE) ug/l1.024.0 81.8-11825.00.18 96

n-Butylbenzene ug/l1.024.0 74-12125.00.17 96

n-Propylbenzene ug/l1.025.5 79.4-12025.00.18 102

p-Isopropyltoluene ug/l1.023.5 75.5-11625.00.21 94

sec-Butylbenzene ug/l1.023.8 76.7-12125.00.14 95

Styrene ug/l1.022.6 85-11525.00.15 90

tert-Butylbenzene ug/l1.023.4 78.9-11725.00.17 94

trans-1,3-Dichloropropene ug/l1.024.6 82.2-12125.00.097 98

Vinyl Acetate ug/l1.040.0 70.5-13425.0 L30.21 160


25.0 88.4-111Surrogate: Toluene-d8 ug/l27.9 N1112


Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Dup Analyzed: 12/16/2009 (P9L1638-BSD1)

1,1,2,2-Tetrachloroethane 25ug/l1.025.5 70.5-12525.00.12 102 3

1,1-Dichloroethene 25ug/l1.024.3 81.7-12225.00.23 97 5

1,2-Dichloropropane 25ug/l1.025.7 85-11525.00.15 103 1

2-Butanone (MEK) 25ug/l5.025.8 45.6-14125.01.8 103 11

Acetone 25ug/l2028.5 22.4-15325.03.8 114 22

Benzene 25ug/l1.024.3 80.7-12025.00.15 97 2

Carbon tetrachloride 25ug/l1.023.7 82.5-12325.00.19 95 2

Chloroform 25ug/l1.024.2 80.7-11925.00.16 97 0

cis-1,2-Dichloroethene 25ug/l1.022.6 83.3-11725.00.18 90 1

Ethylbenzene 25ug/l1.023.2 85-11525.00.16 93 0

m,p-Xylenes 25ug/l2.022.2 85-11525.00.35 89 1

Methylene Chloride 25ug/l2.024.6 79.7-11725.00.50 98 2

o-Xylene 25ug/l1.021.8 85-11525.00.19 87 3

Tetrachloroethene 25ug/l1.022.5 85-11525.00.23 90 3

Toluene 25ug/l1.022.6 85-11525.00.35 90 0

trans-1,2-Dichloroethene 25ug/l1.024.3 82.3-12025.00.22 97 1

Trichloroethene 25ug/l1.024.3 85-11525.00.19 97 3

Trichlorofluoromethane 25ug/l1.024.2 84.5-12325.00.17 97 2

Vinyl chloride 25ug/l1.024.2 80.9-12725.00.24 97 0

1,1,1-Trichloroethane 25ug/l1.024.6 83.2-12025.00.22 98 3

1,1,2-Trichloroethane 25ug/l1.023.4 85-11525.00.19 94 0

1,1-Dichloroethane 25ug/l1.025.7 78.8-12225.00.17 103 1

1,1-Dichloropropene 25ug/l1.024.5 82.3-11925.00.19 98 1

1,2,3-Trichlorobenzene 25ug/l2.022.1 60.4-17125.00.27 89 6

1,2,3-Trichloropropane 25ug/l2.025.4 76.3-12525.00.31 101 1

1,2,4-Trichlorobenzene 25ug/l1.022.4 71-13625.00.18 90 1

1,2,4-Trimethylbenzene 25ug/l1.024.8 78.1-12025.00.13 99 3

1,2-Dibromoethane (EDB) 25ug/l1.023.1 85-11525.00.14 92 0

1,2-Dichlorobenzene 25ug/l1.024.3 85-11525.00.12 97 1



1,3-Dichlorobenzene 25ug/l1.024.0 83.9-11425.00.18 96 1



2,2-Dichloropropane 25ug/l2.023.6 70.8-12825.00.18 94 2

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene 25ug/l1.025.1 78.6-12025.00.17 100 1

2-Hexanone 25ug/l5.022.7 58.5-13525.00.31 91 6


4-Methyl-2-pentanone (MIBK) 25ug/l5.022.9 72-12925.00.43 91 4

Bromobenzene 25ug/l1.024.0 83.3-11625.00.15 96 4

Bromochloromethane 25ug/l1.023.4 83-12225.00.20 94 2

Bromodichloromethane 25ug/l1.023.5 84-11725.00.15 94 0

Bromoform 25ug/l1.021.5 71.9-13125.00.19 86 2

Bromomethane 25ug/l2.025.6 56.3-14525.00.22 102 1

Chlorobenzene 25ug/l1.023.2 82.5-12325.00.12 93 1

Chloroethane 25ug/l1.024.9 69.5-13225.00.26 100 2

Chloromethane 25ug/l5.024.3 70.9-12325.00.20 97 1

cis-1,3-Dichloropropene 25ug/l1.024.2 85-11525.00.17 97 3

Dibromochloromethane 25ug/l1.021.7 83.2-12325.00.15 87 4

Dichlorodifluoromethane 25ug/l1.021.7 72.8-13025.00.15 87 2

Methyl-tert-butyl Ether (MTBE) 25ug/l1.023.2 81.8-11825.00.18 93 3

n-Butylbenzene 25ug/l1.024.2 74-12125.00.17 97 1

n-Propylbenzene 25ug/l1.026.0 79.4-12025.00.18 104 2

p-Isopropyltoluene 25ug/l1.023.2 75.5-11625.00.21 93 1

sec-Butylbenzene 25ug/l1.024.2 76.7-12125.00.14 97 2

Styrene 25ug/l1.022.2 85-11525.00.15 89 2

tert-Butylbenzene 25ug/l1.023.8 78.9-11725.00.17 95 2

trans-1,3-Dichloropropene 25ug/l1.023.7 82.2-12125.00.097 95 4

Vinyl Acetate 25ug/l1.039.1 70.5-13425.0 L30.21 157 2




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Analyzed: 12/16/2009 (P9L1638-MS1) Source: PSL0747-09

1,1,2,2-Tetrachloroethane ug/l1.025.1 70.4-12425.0 ND0.12 101

1,1-Dichloroethene ug/l1.025.2 82.1-12625.0 ND0.23 101

1,2-Dichloropropane ug/l1.026.0 81.1-11625.0 ND0.15 104

2-Butanone (MEK) ug/l5.027.0 41.6-13025.0 ND1.8 108

Acetone ug/l2037.4 19.7-13125.0 9.653.8 111

Benzene ug/l1.024.0 78.4-12725.0 ND0.15 96

Carbon tetrachloride ug/l1.022.9 80.7-12825.0 ND0.19 92

Chloroform ug/l1.025.5 77.6-12225.0 0.1700.16 101

cis-1,2-Dichloroethene ug/l1.023.3 80.1-11925.0 ND0.18 93

Ethylbenzene ug/l1.023.0 83.4-11625.0 ND0.16 92

m,p-Xylenes ug/l2.022.0 70.8-13225.0 ND0.35 88

Methylene Chloride ug/l2.027.1 74.6-11925.0 ND0.50 108

o-Xylene ug/l1.022.1 77.5-12225.0 ND0.19 88

Tetrachloroethene ug/l1.023.0 77.8-11925.0 ND0.23 92

Toluene ug/l1.022.3 83-11825.0 ND0.35 89

trans-1,2-Dichloroethene ug/l1.024.4 81.3-12325.0 ND0.22 98

Trichloroethene ug/l1.023.5 77.3-12025.0 ND0.19 94

Trichlorofluoromethane ug/l1.024.5 82.4-13225.0 ND0.17 98

Vinyl chloride ug/l1.025.4 69.2-14325.0 ND0.24 102

1,1,1-Trichloroethane ug/l1.024.7 81.4-12525.0 ND0.22 99


1,1-Dichloroethane ug/l1.026.9 75.7-12625.0 ND0.17 107

1,1-Dichloropropene ug/l1.023.9 81.4-12325.0 ND0.19 96

1,2,3-Trichlorobenzene ug/l2.021.4 32.3-11725.0 ND0.27 85

1,2,3-Trichloropropane ug/l2.025.5 69.8-12425.0 ND0.31 102


1,2,4-Trimethylbenzene ug/l1.023.3 75.2-12025.0 ND0.13 93

1,2-Dibromoethane (EDB) ug/l1.023.4 76.5-12025.0 ND0.14 93

1,2-Dichlorobenzene ug/l1.023.5 80.6-11425.0 ND0.12 94







Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene ug/l1.023.1 75.2-12225.0 ND0.17 92

2-Hexanone ug/l5.023.6 57.9-11825.0 ND0.31 94


4-Methyl-2-pentanone (MIBK) ug/l5.024.4 65.6-12725.0 ND0.43 97

Bromobenzene ug/l1.023.6 79.4-11625.0 ND0.15 94

Bromochloromethane ug/l1.024.7 75.5-12525.0 ND0.20 99

Bromodichloromethane ug/l1.023.8 78.1-11825.0 ND0.15 95

Bromoform ug/l1.020.9 63.7-12925.0 ND0.19 84

Bromomethane ug/l2.026.8 44.2-15525.0 ND0.22 107

Chlorobenzene ug/l1.023.2 84.6-11025.0 ND0.12 93

Chloroethane ug/l1.026.4 68.9-13625.0 ND0.26 106

Chloromethane ug/l5.025.1 64.1-13525.0 ND0.20 100

cis-1,3-Dichloropropene ug/l1.023.5 78.6-11825.0 ND0.17 94

Dibromochloromethane ug/l1.022.5 75.2-12325.0 ND0.15 90

Dichlorodifluoromethane ug/l1.022.2 71-13825.0 ND0.15 89

Methyl-tert-butyl Ether (MTBE) ug/l1.025.4 68.8-12625.0 ND0.18 101

n-Butylbenzene ug/l1.022.6 70.4-11925.0 ND0.17 91

n-Propylbenzene ug/l1.024.0 76-12425.0 ND0.18 96

p-Isopropyltoluene ug/l1.021.6 67.9-12225.0 ND0.21 86

sec-Butylbenzene ug/l1.022.6 73.7-12525.0 ND0.14 91

Styrene ug/l1.021.9 55-13625.0 ND0.15 88

tert-Butylbenzene ug/l1.022.3 76.8-11925.0 ND0.17 89

trans-1,3-Dichloropropene ug/l1.023.9 72.8-12325.0 ND0.097 96

Vinyl Acetate ug/l1.039.4 50-13925.0 N1ND0.21 158




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Dup Analyzed: 12/16/2009 (P9L1638-MSD1) Source: PSL0747-09

1,1,2,2-Tetrachloroethane 25ug/l1.025.0 70.4-12425.0 ND0.12 100 1

1,1-Dichloroethene 25ug/l1.025.5 82.1-12625.0 ND0.23 102 1

1,2-Dichloropropane 25ug/l1.025.7 81.1-11625.0 ND0.15 103 1

2-Butanone (MEK) 25ug/l5.026.9 41.6-13025.0 ND1.8 108 0

Acetone 25ug/l2035.2 19.7-13125.0 9.653.8 102 6

Benzene 25ug/l1.024.5 78.4-12725.0 ND0.15 98 2

Carbon tetrachloride 25ug/l1.023.5 80.7-12825.0 ND0.19 94 2

Chloroform 25ug/l1.025.2 77.6-12225.0 0.1700.16 100 1

cis-1,2-Dichloroethene 25ug/l1.022.7 80.1-11925.0 ND0.18 91 3

Ethylbenzene 25ug/l1.023.4 83.4-11625.0 ND0.16 94 2

m,p-Xylenes 25ug/l2.022.5 70.8-13225.0 ND0.35 90 2

Methylene Chloride 25ug/l2.026.0 74.6-11925.0 ND0.50 104 4

o-Xylene 25ug/l1.022.5 77.5-12225.0 ND0.19 90 2

Tetrachloroethene 25ug/l1.023.4 77.8-11925.0 ND0.23 94 2

Toluene 25ug/l1.022.8 83-11825.0 ND0.35 91 2

trans-1,2-Dichloroethene 25ug/l1.024.3 81.3-12325.0 ND0.22 97 1

Trichloroethene 25ug/l1.023.9 77.3-12025.0 ND0.19 96 2

Trichlorofluoromethane 25ug/l1.024.7 82.4-13225.0 ND0.17 99 1

Vinyl chloride 25ug/l1.025.1 69.2-14325.0 ND0.24 100 1

1,1,1-Trichloroethane 25ug/l1.025.2 81.4-12525.0 ND0.22 101 2


1,1-Dichloroethane 25ug/l1.026.7 75.7-12625.0 ND0.17 107 1

1,1-Dichloropropene 25ug/l1.024.6 81.4-12325.0 ND0.19 99 3

1,2,3-Trichlorobenzene 25ug/l2.021.6 32.3-11725.0 ND0.27 86 1

1,2,3-Trichloropropane 25ug/l2.025.1 69.8-12425.0 ND0.31 100 2


1,2,4-Trimethylbenzene 25ug/l1.024.0 75.2-12025.0 ND0.13 96 3

1,2-Dibromoethane (EDB) 25ug/l1.023.7 76.5-12025.0 ND0.14 95 1

1,2-Dichlorobenzene 25ug/l1.024.0 80.6-11425.0 ND0.12 96 2







Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene 25ug/l1.023.9 75.2-12225.0 ND0.17 95 3

2-Hexanone 25ug/l5.025.7 57.9-11825.0 ND0.31 103 9


4-Methyl-2-pentanone (MIBK) 25ug/l5.024.2 65.6-12725.0 ND0.43 97 1

Bromobenzene 25ug/l1.024.4 79.4-11625.0 ND0.15 97 3

Bromochloromethane 25ug/l1.024.4 75.5-12525.0 ND0.20 98 1

Bromodichloromethane 25ug/l1.023.8 78.1-11825.0 ND0.15 95 0

Bromoform 25ug/l1.020.1 63.7-12925.0 ND0.19 80 4

Bromomethane 25ug/l2.026.2 44.2-15525.0 ND0.22 105 2

Chlorobenzene 25ug/l1.023.3 84.6-11025.0 ND0.12 93 1

Chloroethane 25ug/l1.026.3 68.9-13625.0 ND0.26 105 0

Chloromethane 25ug/l5.024.7 64.1-13525.0 ND0.20 99 2

cis-1,3-Dichloropropene 25ug/l1.024.2 78.6-11825.0 ND0.17 97 3

Dibromochloromethane 25ug/l1.022.4 75.2-12325.0 ND0.15 89 1

Dichlorodifluoromethane 25ug/l1.021.6 71-13825.0 ND0.15 86 3

Methyl-tert-butyl Ether (MTBE) 25ug/l1.023.6 68.8-12625.0 ND0.18 94 7

n-Butylbenzene 25ug/l1.023.5 70.4-11925.0 ND0.17 94 4

n-Propylbenzene 25ug/l1.025.0 76-12425.0 ND0.18 100 4

p-Isopropyltoluene 25ug/l1.022.8 67.9-12225.0 ND0.21 91 5

sec-Butylbenzene 25ug/l1.023.5 73.7-12525.0 ND0.14 94 4

Styrene 25ug/l1.022.4 55-13625.0 ND0.15 90 2

tert-Butylbenzene 25ug/l1.022.9 76.8-11925.0 ND0.17 92 3

trans-1,3-Dichloropropene 25ug/l1.023.7 72.8-12325.0 ND0.097 95 1

Vinyl Acetate 25ug/l1.038.2 50-13925.0 N1ND0.21 153 3




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane ug/kg50ND 19

1,1,2,2-Tetrachloroethane ug/kg50ND 18


1,1-Dichloroethane ug/kg50ND 15

1,1-Dichloroethene ug/kg50ND 23

1,1-Dichloropropene ug/kg50ND 19

1,2,3-Trichlorobenzene ug/kg100ND 18

1,2,3-Trichloropropane ug/kg100ND 20


1,2,4-Trimethylbenzene ug/kg50ND 27

1,2-Dibromoethane (EDB) ug/kg50ND 16

1,2-Dichlorobenzene ug/kg50ND 21


1,2-Dichloropropane ug/kg50ND 19






2-Butanone (MEK) ug/kg250248 E4200

2-Chlorotoluene ug/kg50ND 15

2-Hexanone ug/kg250ND 210


4-Methyl-2-pentanone (MIBK) ug/kg250ND 170

Acetone ug/kg500ND 330

Benzene ug/kg50ND 23

Bromobenzene ug/kg50ND 18

Bromochloromethane ug/kg50ND 24

Bromodichloromethane ug/kg50ND 18

Bromoform ug/kg50ND 20

Bromomethane ug/kg250ND 8.3

Carbon tetrachloride ug/kg50ND 20

Chlorobenzene ug/kg50ND 11

Chloroethane ug/kg50ND 31

Chloroform ug/kg50ND 24

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chloromethane ug/kg250ND 26

cis-1,2-Dichloroethene ug/kg50ND 21

cis-1,3-Dichloropropene ug/kg50ND 15

Dibromochloromethane ug/kg50ND 11

Dichlorodifluoromethane ug/kg50ND 19

Ethylbenzene ug/kg50ND 13

m,p-Xylenes ug/kg100ND 34

Methylene Chloride ug/kg100ND 32

Methyl-tert-butyl Ether (MTBE) ug/kg50ND 17

n-Butylbenzene ug/kg50ND 18

n-Propylbenzene ug/kg50ND 17

o-Xylene ug/kg50ND 16

p-Isopropyltoluene ug/kg50ND 20

sec-Butylbenzene ug/kg50ND 18

Styrene ug/kg50ND 12

tert-Butylbenzene ug/kg50ND 20

Tetrachloroethene ug/kg50ND 9.6

Toluene ug/kg50ND 15

trans-1,2-Dichloroethene ug/kg50ND 18

trans-1,3-Dichloropropene ug/kg50ND 15

Trichloroethene ug/kg50ND 21

Trichlorofluoromethane ug/kg50ND 32

Vinyl Acetate ug/kg50ND 26

Vinyl chloride ug/kg50ND 25

1250 39.3-132Surrogate: 4-Bromofluorobenzene ug/kg1410 113

1250 44.5-131Surrogate: Dibromofluoromethane ug/kg1520 122

1250 40.4-136Surrogate: Toluene-d8 ug/kg1400 112

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane ug/kg501220 66.4-118125019 98

1,1,2,2-Tetrachloroethane ug/kg501260 69.7-102125018 101

1,1,2-Trichloroethane ug/kg501140 77-105125023 91

1,1-Dichloroethane ug/kg501280 70.1-113125015 102

1,1-Dichloroethene ug/kg501250 53.2-124125023 100

1,1-Dichloropropene ug/kg501260 72-112125019 101

1,2,3-Trichlorobenzene ug/kg1001170 60.4-120125018 94

1,2,3-Trichloropropane ug/kg1001230 68.8-106125020 99


1,2,4-Trimethylbenzene ug/kg501230 77.2-108125027 98

1,2-Dibromoethane (EDB) ug/kg501150 78.3-106125016 92

1,2-Dichlorobenzene ug/kg501220 78.7-107125021 98


1,2-Dichloropropane ug/kg501290 78.8-105125019 103


1,3-Dichlorobenzene ug/kg501220 81-106125012 97




2-Butanone (MEK) ug/kg2501320 39-1481250200 105

2-Chlorotoluene ug/kg501240 76.9-105125015 99

2-Hexanone ug/kg2501210 50.6-1331250210 97


4-Methyl-2-pentanone (MIBK) ug/kg2501100 62.3-1121250170 88

Acetone ug/kg5001340 23.5-1821250330 107

Benzene ug/kg501210 76-107125023 97

Bromobenzene ug/kg501230 78.5-106125018 99

Bromochloromethane ug/kg501120 65.4-129125024 89

Bromodichloromethane ug/kg501110 71.4-111125018 89

Bromoform ug/kg50976 67.3-110125020 78

Bromomethane ug/kg2501160 10-96.412508.3 93

Carbon tetrachloride ug/kg501190 53.7-129125020 95

Chlorobenzene ug/kg501180 82.3-104125011 94

Chloroethane ug/kg501170 10-36.21250 N131 94

Chloroform ug/kg501170 69.8-114125024 94

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chloromethane ug/kg2501050 35-123125026 84

cis-1,2-Dichloroethene ug/kg501100 76.4-108125021 88

cis-1,3-Dichloropropene ug/kg501150 77.3-108125015 92

Dibromochloromethane ug/kg501080 74.5-107125011 87

Dichlorodifluoromethane ug/kg50880 10-134125019 70

Ethylbenzene ug/kg501220 81.6-107125013 98

m,p-Xylenes ug/kg1001160 83.5-107125034 93

Methylene Chloride ug/kg1001240 70.6-105125032 99

Methyl-tert-butyl Ether (MTBE) ug/kg501090 63.1-119125017 87

n-Butylbenzene ug/kg501300 76.8-114125018 104

n-Propylbenzene ug/kg501350 77.7-1071250 N117 108

o-Xylene ug/kg501160 82.8-108125016 93

p-Isopropyltoluene ug/kg501280 79.6-109125020 102

sec-Butylbenzene ug/kg501330 79.5-110125018 106

Styrene ug/kg501140 82.1-111125012 91

tert-Butylbenzene ug/kg501280 78.3-109125020 102

Tetrachloroethene ug/kg501240 80.3-11212509.6 99

Toluene ug/kg501170 81.3-106125015 93

trans-1,2-Dichloroethene ug/kg501200 73.5-110125018 96

trans-1,3-Dichloropropene ug/kg501130 72.4-109125015 91

Trichloroethene ug/kg501200 78.7-107125021 96

Trichlorofluoromethane ug/kg501200 35.3-137125032 96

Vinyl Acetate ug/kg501440 42.2-124125026 116

Vinyl chloride ug/kg50262 46.4-1311250 L425 21




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane 25ug/kg501230 66.4-118125019 99 1

1,1,2,2-Tetrachloroethane 25ug/kg501160 69.7-102125018 93 8

1,1,2-Trichloroethane 25ug/kg501080 77-105125023 86 5

1,1-Dichloroethane 25ug/kg501280 70.1-113125015 102 0

1,1-Dichloroethene 25ug/kg501240 53.2-124125023 99 1

1,1-Dichloropropene 25ug/kg501220 72-112125019 97 4

1,2,3-Trichlorobenzene 25ug/kg1001170 60.4-120125018 94 0

1,2,3-Trichloropropane 25ug/kg1001170 68.8-106125020 94 5


1,2,4-Trimethylbenzene 25ug/kg501260 77.2-108125027 101 2

1,2-Dibromoethane (EDB) 25ug/kg501110 78.3-106125016 89 4

1,2-Dichlorobenzene 25ug/kg501220 78.7-107125021 97 0


1,2-Dichloropropane 25ug/kg501240 78.8-105125019 99 4


1,3-Dichlorobenzene 25ug/kg501190 81-106125012 95 2




2-Butanone (MEK) 25ug/kg2501350 39-1481250200 108 2

2-Chlorotoluene 25ug/kg501230 76.9-105125015 99 1

2-Hexanone 25ug/kg2501110 50.6-1331250210 89 8


4-Methyl-2-pentanone (MIBK) 25ug/kg2501000 62.3-1121250170 80 9

Acetone 25ug/kg5001340 23.5-1821250330 107 0

Benzene 25ug/kg501200 76-107125023 96 1

Bromobenzene 25ug/kg501170 78.5-106125018 93 5

Bromochloromethane 25ug/kg501140 65.4-129125024 91 2

Bromodichloromethane 25ug/kg501080 71.4-111125018 86 3

Bromoform 25ug/kg50922 67.3-110125020 74 6

Bromomethane 25ug/kg2501160 10-96.412508.3 93 0

Carbon tetrachloride 25ug/kg501150 53.7-129125020 92 3

Chlorobenzene 25ug/kg501170 82.3-104125011 94 1

Chloroethane 25ug/kg501170 10-36.21250 N131 94 0

Chloroform 25ug/kg501180 69.8-114125024 95 1

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chloromethane 25ug/kg2501050 35-123125026 84 0

cis-1,2-Dichloroethene 25ug/kg501110 76.4-108125021 89 1

cis-1,3-Dichloropropene 25ug/kg501140 77.3-108125015 92 0

Dibromochloromethane 25ug/kg501040 74.5-107125011 83 4

Dichlorodifluoromethane 25ug/kg50846 10-134125019 68 4

Ethylbenzene 25ug/kg501210 81.6-107125013 96 1

m,p-Xylenes 25ug/kg1001170 83.5-107125034 94 1

Methylene Chloride 25ug/kg1001220 70.6-105125032 98 1

Methyl-tert-butyl Ether (MTBE) 25ug/kg501080 63.1-119125017 86 1

n-Butylbenzene 25ug/kg501300 76.8-114125018 104 0

n-Propylbenzene 25ug/kg501330 77.7-107125017 106 2

o-Xylene 25ug/kg501150 82.8-108125016 92 1

p-Isopropyltoluene 25ug/kg501240 79.6-109125020 99 3

sec-Butylbenzene 25ug/kg501320 79.5-110125018 106 1

Styrene 25ug/kg501130 82.1-111125012 90 1

tert-Butylbenzene 25ug/kg501260 78.3-109125020 100 2

Tetrachloroethene 25ug/kg501200 80.3-11212509.6 96 4

Toluene 25ug/kg501140 81.3-106125015 91 3

trans-1,2-Dichloroethene 25ug/kg501220 73.5-110125018 97 2

trans-1,3-Dichloropropene 25ug/kg501090 72.4-109125015 87 4

Trichloroethene 25ug/kg501180 78.7-107125021 94 2

Trichlorofluoromethane 25ug/kg501170 35.3-137125032 93 3

Vinyl Acetate 25ug/kg501400 42.2-124125026 112 3

Vinyl chloride 25ug/kg50270 46.4-1311250 L425 22 3




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane ug/kg501300 58.2-1151330 ND19 98

1,1,2,2-Tetrachloroethane ug/kg501250 57.5-1081330 ND18 94


1,1-Dichloroethane ug/kg501330 61.8-1101330 ND15 100

1,1-Dichloroethene ug/kg501350 39.2-1231330 ND23 102

1,1-Dichloropropene ug/kg501350 60.6-1111330 ND19 101

1,2,3-Trichlorobenzene ug/kg1001200 39.2-1251330 ND18 90

1,2,3-Trichloropropane ug/kg1001270 59.4-1101330 ND20 96


1,2,4-Trimethylbenzene ug/kg501310 54.6-1201330 ND27 99

1,2-Dibromoethane (EDB) ug/kg501230 64.2-1081330 ND16 93

1,2-Dichlorobenzene ug/kg501270 63.5-1081330 ND21 96


1,2-Dichloropropane ug/kg501280 66.7-1061330 ND19 96


1,3-Dichlorobenzene ug/kg501240 62-1111330 ND12 94




2-Butanone (MEK) ug/kg2501430 34.5-1541330 ND200 107

2-Chlorotoluene ug/kg501290 58.1-1131330 ND15 97

2-Hexanone ug/kg2501300 38.6-1461330 ND210 98


4-Methyl-2-pentanone (MIBK) ug/kg2501140 56.5-1111330 ND170 86

Acetone ug/kg5001470 20.1-1821330 ND330 111

Benzene ug/kg501260 63.6-1081330 ND23 95

Bromobenzene ug/kg501240 64.2-1091330 ND18 93

Bromochloromethane ug/kg501150 60-1231330 ND24 87

Bromodichloromethane ug/kg501160 61.8-1111330 ND18 88

Bromoform ug/kg50986 57.5-1091330 ND20 74

Bromomethane ug/kg2501220 10-93.51330 ND8.3 92

Carbon tetrachloride ug/kg501260 44.5-1231330 ND20 95

Chlorobenzene ug/kg501290 66.9-1071330 ND11 97

Chloroethane ug/kg501250 10.3-34.11330 N1ND31 94

Chloroform ug/kg501230 63.2-1121330 ND24 93

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chloromethane ug/kg2501160 15.3-1231330 ND26 87

cis-1,2-Dichloroethene ug/kg501160 64.1-1081330 ND21 87

cis-1,3-Dichloropropene ug/kg501180 63.3-1101330 ND15 89

Dibromochloromethane ug/kg501120 63-1091330 ND11 84

Dichlorodifluoromethane ug/kg50957 10-1181330 ND19 72

Ethylbenzene ug/kg501350 62.4-1131330 ND13 102

m,p-Xylenes ug/kg1001300 57.7-1181330 ND34 98

Methylene Chloride ug/kg1001260 57.6-1061330 38.032 92

Methyl-tert-butyl Ether (MTBE) ug/kg501120 54.9-1181330 ND17 85

n-Butylbenzene ug/kg501440 47.8-1321330 ND18 108

n-Propylbenzene ug/kg501420 55.8-1171330 ND17 107

o-Xylene ug/kg501270 60.8-1161330 ND16 96

p-Isopropyltoluene ug/kg501350 59-1161330 ND20 102

sec-Butylbenzene ug/kg501430 60.3-1171330 ND18 107

Styrene ug/kg501230 64.5-1151330 ND12 93

tert-Butylbenzene ug/kg501340 60.3-1141330 ND20 101

Tetrachloroethene ug/kg501390 56.7-1301330 ND9.6 104

Toluene ug/kg501210 62.6-1131330 ND15 91

trans-1,2-Dichloroethene ug/kg501290 58.4-1121330 ND18 97

trans-1,3-Dichloropropene ug/kg501170 61.4-1091330 ND15 88

Trichloroethene ug/kg501300 64.9-1101330 ND21 98

Trichlorofluoromethane ug/kg501260 31.8-1261330 ND32 95

Vinyl Acetate ug/kg50ND 10-1271330 M2ND26

Vinyl chloride ug/kg50304 26.1-1301330 N1ND25 23




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane 25ug/kg501270 58.2-1151300 ND19 98 2

1,1,2,2-Tetrachloroethane 25ug/kg501260 57.5-1081300 ND18 97 1


1,1-Dichloroethane 25ug/kg501300 61.8-1101300 ND15 100 2

1,1-Dichloroethene 25ug/kg501320 39.2-1231300 ND23 102 2

1,1-Dichloropropene 25ug/kg501370 60.6-1111300 ND19 105 2

1,2,3-Trichlorobenzene 25ug/kg1001180 39.2-1251300 ND18 91 2

1,2,3-Trichloropropane 25ug/kg1001280 59.4-1101300 ND20 98 1


1,2,4-Trimethylbenzene 25ug/kg501300 54.6-1201300 ND27 100 1

1,2-Dibromoethane (EDB) 25ug/kg501240 64.2-1081300 ND16 96 1

1,2-Dichlorobenzene 25ug/kg501230 63.5-1081300 ND21 95 3


1,2-Dichloropropane 25ug/kg501280 66.7-1061300 ND19 99 0


1,3-Dichlorobenzene 25ug/kg501220 62-1111300 ND12 94 2




2-Butanone (MEK) 25ug/kg2501320 34.5-1541300 ND200 102 7

2-Chlorotoluene 25ug/kg501300 58.1-1131300 ND15 100 1

2-Hexanone 25ug/kg2501290 38.6-1461300 ND210 99 1


4-Methyl-2-pentanone (MIBK) 25ug/kg2501200 56.5-1111300 ND170 93 6

Acetone 25ug/kg5001300 20.1-1821300 ND330 100 12

Benzene 25ug/kg501240 63.6-1081300 ND23 96 1

Bromobenzene 25ug/kg501230 64.2-1091300 ND18 94 1

Bromochloromethane 25ug/kg501140 60-1231300 ND24 88 1

Bromodichloromethane 25ug/kg501140 61.8-1111300 ND18 88 2

Bromoform 25ug/kg50935 57.5-1091300 ND20 72 5

Bromomethane 25ug/kg2501210 10-93.51300 ND8.3 93 1

Carbon tetrachloride 25ug/kg501270 44.5-1231300 ND20 97 1

Chlorobenzene 25ug/kg501230 66.9-1071300 ND11 95 5

Chloroethane 25ug/kg501230 10.3-34.11300 N1ND31 94 2

Chloroform 25ug/kg501180 63.2-1121300 ND24 91 5

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chloromethane 25ug/kg2501120 15.3-1231300 ND26 86 3

cis-1,2-Dichloroethene 25ug/kg501120 64.1-1081300 ND21 86 3

cis-1,3-Dichloropropene 25ug/kg501180 63.3-1101300 ND15 91 0

Dibromochloromethane 25ug/kg501070 63-1091300 ND11 82 4

Dichlorodifluoromethane 25ug/kg50965 10-1181300 ND19 74 1

Ethylbenzene 25ug/kg501300 62.4-1131300 ND13 100 4

m,p-Xylenes 25ug/kg1001250 57.7-1181300 ND34 96 4

Methylene Chloride 25ug/kg1001220 57.6-1061300 38.032 91 3

Methyl-tert-butyl Ether (MTBE) 25ug/kg501090 54.9-1181300 ND17 84 3

n-Butylbenzene 25ug/kg501410 47.8-1321300 ND18 109 2

n-Propylbenzene 25ug/kg501450 55.8-1171300 ND17 111 2

o-Xylene 25ug/kg501220 60.8-1161300 ND16 94 4

p-Isopropyltoluene 25ug/kg501350 59-1161300 ND20 104 0

sec-Butylbenzene 25ug/kg501430 60.3-1171300 ND18 110 0

Styrene 25ug/kg501170 64.5-1151300 ND12 90 5

tert-Butylbenzene 25ug/kg501360 60.3-1141300 ND20 105 2

Tetrachloroethene 25ug/kg501330 56.7-1301300 ND9.6 102 4

Toluene 25ug/kg501190 62.6-1131300 ND15 92 1

trans-1,2-Dichloroethene 25ug/kg501240 58.4-1121300 ND18 95 4

trans-1,3-Dichloropropene 25ug/kg501110 61.4-1091300 ND15 86 5

Trichloroethene 25ug/kg501290 64.9-1101300 ND21 99 1

Trichlorofluoromethane 25ug/kg501250 31.8-1261300 ND32 96 1

Vinyl Acetate 25ug/kg50ND 10-1271300 M2ND26

Vinyl chloride 25ug/kg50294 26.1-1301300 N1ND25 23 3




Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

DATA QUALIFIERS AND DEFINITIONS

E4 Concentration estimated. Analyte was detected below laboratory minimum reporting limit (MRL).

E8 Analyte reported to the MDL per project specification. Target analyte was not detected in the sample.

L3 The associated blank spike recovery was above method acceptance limits.

L4 The associated blank spike recovery was below method acceptance limits.

M2 Matrix spike recovery was low; the associated blank spike recovery was acceptable.

N1 See case narrative.

S10 Surrogate recovery was above laboratory and method acceptance limits. See case narrative.

Relative Percent DifferenceRPD

Analyte NOT DETECTED at or above the reporting limit or MDL, if MDL is specified.ND

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas




454-9303





Sampled:

Received:

12/11/09


Project ID:

PSL0747

14682.013

Certification Summary

Method Matrix Nelac Arizona

TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B

Nevada and NELAP provide analyte specific accreditations. Analyte specific information for TestAmerica may be obtained by contacting

the laboratory or visiting our website at www.testamericainc.com

Project Manager

TestAmerica Phoenix

PSL0747

Tina Paulauskas



Test America THE LEADER IN ENVIRONMENTAL TESTING

TAL-0013-550 (12/08)

Client Name I Address:

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Project Manager: N "Y> 'f; C.ly1 f\1\c. ~~tvf"V\.

Sa~er: . . z::>kb.. \-\ &_.z" t~ 0-f?-... ne..r · ....,

Sample Container Sample Description Matrix Type

A\3\- too- \2..\\oq s \]oA

IA8.l- (D- tz.noq s \IDA A-f?::> l- <60- 12\\09 buP s \loA

CHAIN OF CUSTODY FORM

[ 1 Phoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602). 437-3340 FAX (602) 454-9303 [ 1 Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ 1 Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number: Analysis Required lY ~ ~:l. eJ i 3

Phone Number: CD '-\ '%0 - 3-\ g .,r \ ?- 4 L{ ~0 Fax Number: 0~ L\ 'lo- 34 tr- 1;;14~

# of Sampling Sampling . ~ Cont. Date Time Preservatives

I \2fn/uc1 Dq:t.Jtt- fv\e6t+ X \ '2/tl/r:A fl!OO Meol-} X l '2/uia'i l2~30 f\1\eDt-\. )<._

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Special Instructions

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same day 72 hours R~linquished By: Date/Time: ~LvifcfBy: . Date/Time: 24 hours 5 days

/ 48 hours normal .X Relinquished By: Date/Time: /_ Received in Lab~· Date/Time: Sample lnt];;: (Check) . l { £(_.

1.---- tf rz1 lt!t/r /l:/( intact on Ice [ ·

Note: By relinquishing samples to TestAmerica, client agrees topay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be. disposed of after 30 days.

~

------------------------~--~------------------------~-------------

Test America ·THE LEADER IN ENVIRONMENTAL TESTING

TAL-0013-550 (12/08}

Client Name I Address:


[ ] Phoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ·1 Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number: Analysis Required A1Yl G-c G f-t,lt/1-T €A x. i '-[bg-~~ 6/3 ·~~, \1\C\_Oe..v"~-b.ut\. 9\-e- -sqb '"

· k\e -A?-Project Manager: Phone Number: ~-~v~ 6-.Vl ~N~o-.... l{&J-- 34.g- ).?-l{ t-t sasi~JtA W~t'\P--Y F~r:~qg-- lJ-<{ s- 0~

Sample Descriptio~ Sample Container #of Sampling Sampling Goo Matrix Type Cont. Date Time Preservatives -;;:::>

Ml-Orl.- I.:Li ld1 w \ICJPr 3 l~t/oti N~3D ~ )( p~ :L/) IIL/7 ,_ 0' 50oo\- l?.-l\ oCj vJ '\} () 11 3 P/,t/o«=t I t/~SD liu( i( r- (51

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7~7};L~iJA l.;~;~rr;;: Received By: Date/Time: Turnaround Time:

17~'/7 =-- same day --....... Relinquished By: Date/Time: Received By.: .. ---- Date/Time: 24 hours

_...---·--·---- 48 hours

Relinquished By: Date/Time: .·C-...---~ved-inte~ Date/Time: Sample ln,\ty:

i7 ilif/)q 11r1 intact ~ ,. I

Page of

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I

~ ---=- ~~ ~ (i)~

-#f >---;:: / ~

(Check)

72 hours

5 days

normal _}(" (Check) t 1°( on ice

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

\'


TAL-0013-550 (12/08)

Client Name/ Address:

~ ME C £ .. eowudv1 X g\-e, 3~lo <?I l ~ J7 , \h o.. l::e_ "\fe;AhL {C\.

SeD +s ~"- \ e, -fr-L 0

Project Manager: N ~-.;-; tlVI f'v\c_ ~~tvf?A

Sa~er: ~kR v. &_I!... "l,_:) ~ ne.r

Sample Description v Sample Container

Matrix Type

A8\ -(oo- \2..\\oC.,. s \lOA

Ml-lD- \2\\ 0 q s \{1)-fl

I~ t- <60 -l2\to9 t>u.P s \lOA


[ 1 Phoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602} 437-3340 FAX (602) 454-9303 [ 1 Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520} 807-3803 [ 1 Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (7.02) 798-3621

Project/ PO Number: Analysis Required lY ~ ~:). · CJ i 3

Phone Number: en \{ ~0 - ?M g ;oo-' ~ L{ '-1 0 Fax Number: ·~ ..9.-4 ~(J- 34 ~- j;lL\5' Q~ #of Sampling Sampling . ~ Cont. Date Time Preservatives

I \2ft\/oc1 oq~yq., N\eoH- >< l '2/tt lrf1 il !00 IV\eol4 X l '2/u I If\ l2.~ 30 (\Ae()t-\ ){._

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v

'·

~;o:::t: / ~t~~- I zA~/;~/77: I 7 < "Hece1ve·~ Date/Time: Turnaround Time: (Check)

same day 72 hours

R~linquished By: Date/Time: ~LvffifBy: .Date/Time: 24 hours 5 days

/ 48 hours normal _X Relinquished By: Date/Time:

~-~~din Lab ~tt Date/Time: Sample ln:t;;: (Check) . /-{'L _ rz;J!Ib1 /l:/( intact on 1ce I,

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be_ disposed of after 30 days.

~


454-9303

LABORATORY REPORT




Attention: C. Kirk Craig Sampled:

Received:

Issued:

12/15/09

12/15/09

12/31/09 08:53




report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain of Custody, 1 page, is included and

is an integral part of this report.


Project: 14682.013


CASE NARRATIVE


PSL0871-01 AB4-10-121509 Soil

PSL0871-02 AB4-20-121509 Soil

PSL0871-03 AB4-30-121509 Soil

PSL0871-04 AB4-TB-121509 Water

PSL0871-05 AB4-40-121509 Soil

PSL0871-06 AB4-40-121509 DUP Soil

PSL0871-07 AB4-ERB-121509 Water

PSL0871-08 AB4-50-121509 Soil

PSL0871-09 AB4-60-121509 Soil

PSL0871-10 AB4-70-121509 Soil

PSL0871-11 AB4-80-121509 Soil

Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas

<Page 1 of 47>


454-9303




Attention: C. Kirk Craig

Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

SAMPLE RECEIPT: Samples were received intact, at 0.3°C, on ice and with chain of custody documentation.








N1-Batch P9L1638 - The LCS/LCSD and MS/MSD recovered high and outside of acceptance limits for

Vinyl Acetate. All associated samples are non-detect for this compound and therefore should not be

impacted.

N1-Batch P9L1638 - The surrogate, Toluene-d8, recovered high and outside of the project specific

acceptance limits in the LCS/LCSD. The recoveries were within the laboratory's historical limits. All

surrogate recoveries in the Method Blank, MS/MSD and associated samples were within the project specific

limits. The data should not be impacted.

N1-Batch P9L1626 - The LCS/LCSD and MS/MSD recovered high and outside of the project specific

acceptance limits for Chloroethane. The recoveries were within the laboratory's historical limits. All

associated samples were non-detect for this compound and therefore should not be impacted.

N1a-The RPD exceeded the acceptance limit due to sample matrix effects.



Reviewed By:

Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-04 (AB4-TB-121509 - Water)






Acetone SW8260B P9L1638 5.620 E412/16/09 12/16/0913.8




































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-04 (AB4-TB-121509 - Water) - cont.
























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-07 (AB4-ERB-121509 - Water)






Acetone SW8260B P9L1638 9.920 E412/16/09 12/16/0913.8












Trichloroethene SW8260B P9L1638 0.451.0 E412/16/09 12/16/0910.19
























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-07 (AB4-ERB-121509 - Water) - cont.
























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-01 (AB4-10-121509 - Soil)










































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-01 (AB4-10-121509 - Soil) - cont.
























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit














SW8260BTetrachloroethene P9L1626 56 ND E812/15/09 12/22/091.1211











Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

































SW8260BBromomethane P9L1626 350 ND E812/15/09 12/22/091.4112










Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-06 (AB4-40-121509 DUP - Soil)










































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0871-06 (AB4-40-121509 DUP - Soil) - cont.
























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: AB4-10-121509 (PSL0871-01) - Soil

2 12/15/2009 09:00 12/15/2009 17:27 12/15/2009 09:00 12/22/2009 21:22SW8260B


2 12/15/2009 09:34 12/15/2009 17:27 12/15/2009 09:34 12/22/2009 21:53SW8260B


2 12/15/2009 10:24 12/15/2009 17:27 12/15/2009 10:24 12/22/2009 22:25SW8260B


2 12/15/2009 11:37 12/15/2009 17:27 12/15/2009 11:37 12/22/2009 22:56SW8260B

Sample ID: AB4-40-121509 DUP (PSL0871-06) - Soil

2 12/15/2009 11:37 12/15/2009 17:27 12/15/2009 11:37 12/22/2009 23:27SW8260B


2 12/15/2009 12:38 12/15/2009 17:27 12/15/2009 12:38 12/22/2009 23:59SW8260B


2 12/15/2009 14:30 12/15/2009 17:27 12/15/2009 14:30 12/23/2009 00:30SW8260B


2 12/15/2009 15:20 12/15/2009 17:27 12/15/2009 15:20 12/23/2009 01:02SW8260B


2 12/15/2009 16:20 12/15/2009 17:27 12/15/2009 16:20 12/23/2009 01:33SW8260B

Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.028.8 45.6-14125.01.8 115

Acetone ug/l2035.7 22.4-15325.03.8 143

Benzene ug/l1.023.8 80.7-12025.00.15 95


Chloroform ug/l1.024.3 80.7-11925.00.16 97



m,p-Xylenes ug/l2.022.4 85-11525.00.35 90


o-Xylene ug/l1.022.4 85-11525.00.19 89


Toluene ug/l1.022.7 85-11525.00.35 91





















Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.024.1 58.5-13525.00.31 97






Bromoform ug/l1.021.8 71.9-13125.00.19 87













Styrene ug/l1.022.6 85-11525.00.15 90







Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.025.8 45.6-14125.01.8 103 11

Acetone 25ug/l2028.5 22.4-15325.03.8 114 22

Benzene 25ug/l1.024.3 80.7-12025.00.15 97 2


Chloroform 25ug/l1.024.2 80.7-11925.00.16 97 0



m,p-Xylenes 25ug/l2.022.2 85-11525.00.35 89 1


o-Xylene 25ug/l1.021.8 85-11525.00.19 87 3


Toluene 25ug/l1.022.6 85-11525.00.35 90 0





















Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.022.7 58.5-13525.00.31 91 6






Bromoform 25ug/l1.021.5 71.9-13125.00.19 86 2













Styrene 25ug/l1.022.2 85-11525.00.15 89 2







Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2037.4 19.7-13125.0 9.653.8 111

Benzene ug/l1.024.0 78.4-12725.0 ND0.15 96


Chloroform ug/l1.025.5 77.6-12225.0 0.1700.16 101



m,p-Xylenes ug/l2.022.0 70.8-13225.0 ND0.35 88


o-Xylene ug/l1.022.1 77.5-12225.0 ND0.19 88


Toluene ug/l1.022.3 83-11825.0 ND0.35 89





















Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.023.6 57.9-11825.0 ND0.31 94






Bromoform ug/l1.020.9 63.7-12925.0 ND0.19 84













Styrene ug/l1.021.9 55-13625.0 ND0.15 88







Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone 25ug/l2035.2 19.7-13125.0 9.653.8 102 6

Benzene 25ug/l1.024.5 78.4-12725.0 ND0.15 98 2


Chloroform 25ug/l1.025.2 77.6-12225.0 0.1700.16 100 1



m,p-Xylenes 25ug/l2.022.5 70.8-13225.0 ND0.35 90 2


o-Xylene 25ug/l1.022.5 77.5-12225.0 ND0.19 90 2


Toluene 25ug/l1.022.8 83-11825.0 ND0.35 91 2





















Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.025.7 57.9-11825.0 ND0.31 103 9






Bromoform 25ug/l1.020.1 63.7-12925.0 ND0.19 80 4













Styrene 25ug/l1.022.4 55-13625.0 ND0.15 90 2







Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/21/2009-12/29/2009 (P9L1626-BS1)






















2-Hexanone ug/kg2501260 50.6-1331250210 101



Acetone ug/kg500987 23.5-1821250330 79

Benzene ug/kg501200 76-107125023 96




Bromoform ug/kg501170 67.3-110125020 94





Chloroform ug/kg501110 69.8-114125024 89

Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes ug/kg1001140 83.5-107125034 91




n-Propylbenzene ug/kg501340 77.7-107125017 107

o-Xylene ug/kg501130 82.8-108125016 91



Styrene ug/kg501190 82.1-111125012 95



Toluene ug/kg501150 81.3-106125015 92






Vinyl chloride ug/kg50656 46.4-131125025 52




Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Dup Analyzed: 12/21/2009-12/29/2009 (P9L1626-BSD1)






















2-Hexanone 25ug/kg2501080 50.6-1331250210 87 15



Acetone 25ug/kg5001020 23.5-1821250330 82 3

Benzene 25ug/kg501220 76-107125023 97 1




Bromoform 25ug/kg501100 67.3-110125020 88 7





Chloroform 25ug/kg501150 69.8-114125024 92 4

Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes 25ug/kg1001160 83.5-107125034 92 1





o-Xylene 25ug/kg501130 82.8-108125016 91 0



Styrene 25ug/kg501190 82.1-111125012 95 0



Toluene 25ug/kg501200 81.3-106125015 96 4






Vinyl chloride 25ug/kg50744 46.4-131125025 60 13




Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone ug/kg2501050 38.6-1461240 ND210 84



Acetone ug/kg500952 20.1-1821240 ND330 77

Benzene ug/kg501190 63.6-1081240 ND23 95










Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL










Methylene Chloride ug/kg1001140 57.6-1061240 ND32 92




o-Xylene ug/kg501110 60.8-1161240 ND16 89



Styrene ug/kg501200 64.5-1151240 ND12 97



Toluene ug/kg501140 62.6-1131240 ND15 92





Vinyl Acetate ug/kg50743 10-1271240 ND26 60

Vinyl chloride ug/kg50379 26.1-1301240 ND25 31




Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone 25ug/kg2501120 38.6-1461250 ND210 90 7



Acetone 25ug/kg500927 20.1-1821250 ND330 74 3

Benzene 25ug/kg501190 63.6-1081250 ND23 95 0










Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL










Methylene Chloride 25ug/kg1001110 57.6-1061250 ND32 89 2




o-Xylene 25ug/kg501160 60.8-1161250 ND16 93 5



Styrene 25ug/kg501210 64.5-1151250 ND12 97 1



Toluene 25ug/kg501150 62.6-1131250 ND15 92 1





Vinyl Acetate 25ug/kg50566 10-1271250 N1aND26 45 27

Vinyl chloride 25ug/kg50424 26.1-1301250 ND25 34 11




Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013








Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas




454-9303





Sampled:

Received:

12/15/09


Project ID:

PSL0871

14682.013



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PSL0871

Tina Paulauskas



Test America CHAIN OF CUSTODY FORM

~hoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303

THE LEADER IN ENVIRONMENTAL TESTING [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803

Page _J__ of J [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621 TAL-0013-550 (12/08)

~me/Address: Project/ PO Number: Analysis Required (=:.(1.,:5~

8777 £. 11 1A b£.. v~ · ~ "3""V.l... I '-{6 8 "2. * ~ ~ "3 ~~Mit. A"Z.. 8S'LS~ Project Manager: V(.tAJ,[ G{J..AV(.::;;. Phone Number: '2..... <{ t{

t{,~--"3'-{JC~t .

Sampler:RP~ rvf-t~'-D ere:om~e~'(;~ ... tzj-1. s G psuitt-11 ~ Sample Description Sample Container #of Sampling Sampling

Preservatives 00 Matrix Type Cont. Date Time Special Instructions

Af;l/-JO ... /~/50'1 $0/L- o/OM/ I 1Z/6/a d/00 Mf-01.} / -or ~~- 2.::> -t '1..J5 DC, tl L{ I 'Lf~lo~ DCJ3t..( tl ~ -vz_ A0 c.{- 3D .... L '"2.-~ S" DC:, L-i I I l t'f. ~I e:s:r J02._ y t I v ~3 A0'i- 1{3 -I L.lSD c; (,VAfiR Ll.D..vf · I ''l../ r'>/ c:J:a ~ L l\ lr+ui v ' -n({ A-04- t.fu'" l""LJSD1 5DIL L/oMI I t "2{1 ')I cry ll37 MEot4 ~ "--05 Al3~- 4 o-LL.~so, Du p I l tL l I "2{ t'i/ tFr 1137 L( v ~(p

A-0'-1 --tER.tJ-rz J5o'1 I~ J{JJIA.J 3 '¥•'>/Cfl [ZoS t-\.G I v -or Afbl./- 5D~ l'2...15D-=c S~t... l.£O;W( I 1'/t!/o"j \'2.38. Mw~ v '"b~ IAf!if-b0-12.1 soc; ·c,t 1. I I t7.ftr/dj /L/70 L ( v "()4

MJI-&0 -Jl.~So'j ll t( l t-zftr/oT lcf3o l( / tv.sjMSb -{b

484-70-_ \"150'1 1\. t I I ''it>}Cft t5"2..0 l \ / --L r A13Lf- 9°-t"2.JS'ocr l ( tl I nf,sh, 16e2> L f v -rZ.

~~~~8~ L 7.} bS I ~a9/Time\ l 21 ~ceived By: Date/Time: Turnaround Time: (Check)

'-- _;;::> same day 72 hours

Relinquished By: v Date/Time: ~dBy: Date/Time: 24 hours 5 days

~ 48 hours normal ~ Relinquished By: Date/Time: ~--~Bived in IPAI J- Date/Time: Sam pi~: (Check) {)_'2:>0 \2-/l5}b'1 L/21 intact on ice -~- (_

J



454-9303

LABORATORY REPORT





Received:

Issued:

12/16/09

12/16/09

01/05/10 12:19







Project: 14682.013


CASE NARRATIVE


PSL0952-01 AB4-90-121609 Soil

PSL0952-02 AB4-101-121609 Water


PSL0952-04 AB4-110-121609 Water

PSL0952-05 AB4-110-121609 DUP Water


PSL0952-07 AB4-120-121609 Water

Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas

<Page 1 of 59>


454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

SAMPLE RECEIPT: Samples were received intact, at 0.3°C, on ice and with chain of custody documentation.




PRESERVATION: Samples requiring preservation were verified prior to sample analysis. Results were qualified where the

sample container did not meet the method preservation requirements.




N1-Batch P9L1764 - The LCS/LCSD and MS/MSD recovered high and outside of the project specific

acceptance limits for Chloroethane. The recoveries were within the laboratory's historical acceptance

limits. All associated samples are non-detect for this compound and therefore should not be impacted.

N1-Batch P9L2330 - The LCS/LCSD and MS/MSD recovered high and outside of acceptance limits for

Vinyl Acetate. The LCS/LCSD and MSD recovered high and outside of acceptance limits for Acetone. All

associated samples are non-detect for these compounds and therefore should not be impacted.

N1-Batch P9L2330 - The MSD recovered high and outside of the project specific acceptance limits for

several compounds. The LCS recovered high and outside of project specific acceptance limits for MEK,

2-Hexanone and MTBE. All recoveries were within the laboratory's historical limits. The associated

sample was non-detect for all affected analytes with the exception of MEK. The detect for MEK was

confirmed through re-analysis with QC recoveries within the project specific limits, outside of hold time.

The data should not be significantly impacted.

N1a-pH = 6

N1b-The RPD exceeded the acceptance limit due to sample matrix effects.



Reviewed By:

Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-02 (AB4-101-121609 - Water) Q3, N1a





2-Butanone (MEK) SW8260B P9L2330 7.95.0 N112/23/09 12/23/0911.8

SW8260BAcetone P9L2330 20 ND V1, E812/23/09 12/23/0913.8










Toluene SW8260B P9L2330 0.461.0 E412/23/09 12/23/0910.35


Trichloroethene SW8260B P9L2330 541.0 12/23/09 12/23/0910.19




















2-Hexanone SW8260B P9L2330 1.35.0 E412/23/09 12/23/0910.31




Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-02 (AB4-101-121609 - Water) - cont. Q3, N1a
























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-03 (AB4-TB-121609 - Water)










































Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-03 (AB4-TB-121609 - Water) - cont.




















SW8260BVinyl Acetate P9L2171 1.0 ND E812/21/09 12/21/0910.21




Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-04 (AB4-110-121609 - Water)










































Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-04 (AB4-110-121609 - Water) - cont.
























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-05 (AB4-110-121609 DUP - Water)










































Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-05 (AB4-110-121609 DUP - Water) - cont.
























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-06 (AB4-ERB-121609 - Water)

























1,2,3-Trichlorobenzene SW8260B P9L2242 0.412.0 E412/22/09 12/22/0910.27


1,2,4-Trichlorobenzene SW8260B P9L2242 0.281.0 E412/22/09 12/22/0910.18



1,2-Dichlorobenzene SW8260B P9L2242 0.121.0 E412/22/09 12/22/0910.12












Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-06 (AB4-ERB-121609 - Water) - cont.













n-Butylbenzene SW8260B P9L2242 0.191.0 E412/22/09 12/22/0910.17











Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-07 (AB4-120-121609 - Water)


















Trichloroethene SW8260B P9L2242 9.31.0 12/22/09 12/22/0910.19
























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL0952-07 (AB4-120-121609 - Water) - cont.
























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











































Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)


2 12/16/2009 09:15 12/16/2009 16:45 12/16/2009 09:15 12/23/2009 05:43SW8260B

Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL































1,2-Dichlorobenzene ug/l1.00.130 E40.12





1,4-Dichlorobenzene ug/l1.00.170 E40.16


Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



















n-Butylbenzene ug/l1.00.210 E40.17



sec-Butylbenzene ug/l1.00.140 E40.14



trans-1,3-Dichloropropene ug/l1.00.310 E40.097





Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.020.6 45.6-14125.01.8 82

Acetone ug/l2026.6 22.4-15325.03.8 106

Benzene ug/l1.023.5 80.7-12025.00.15 94


Chloroform ug/l1.021.6 80.7-11925.00.16 86



m,p-Xylenes ug/l2.052.2 85-11550.00.35 104


o-Xylene ug/l1.026.1 85-11525.00.19 105


Toluene ug/l1.024.6 85-11525.00.35 98





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.025.2 58.5-13525.00.31 101






Bromoform ug/l1.021.7 71.9-13125.00.19 87













Styrene ug/l1.025.6 85-11525.00.15 103



Vinyl Acetate ug/l1.020.1 70.5-13425.00.21 80




Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.021.1 45.6-14125.01.8 84 3

Acetone 25ug/l2030.7 22.4-15325.03.8 123 15

Benzene 25ug/l1.023.3 80.7-12025.00.15 93 1


Chloroform 25ug/l1.021.8 80.7-11925.00.16 87 1



m,p-Xylenes 25ug/l2.050.7 85-11550.00.35 101 3


o-Xylene 25ug/l1.025.8 85-11525.00.19 103 1


Toluene 25ug/l1.023.5 85-11525.00.35 94 4





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.024.7 58.5-13525.00.31 99 2






Bromoform 25ug/l1.021.9 71.9-13125.00.19 88 1













Styrene 25ug/l1.025.1 85-11525.00.15 100 2



Vinyl Acetate 25ug/l1.019.2 70.5-13425.00.21 77 5




Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2020.6 19.7-13125.0 ND3.8 82

Benzene ug/l1.025.2 78.4-12725.0 ND0.15 101


Chloroform ug/l1.023.3 77.6-12225.0 ND0.16 93



m,p-Xylenes ug/l2.055.0 70.8-13250.0 ND0.35 110


o-Xylene ug/l1.027.7 77.5-12225.0 ND0.19 111


Toluene ug/l1.026.1 83-11825.0 ND0.35 104


Trichloroethene ug/l1.027.4 77.3-12025.0 0.8300.19 106



















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.023.7 57.9-11825.0 ND0.31 95






Bromoform ug/l1.023.2 63.7-12925.0 ND0.19 93













Styrene ug/l1.026.0 55-13625.0 ND0.15 104



Vinyl Acetate ug/l1.019.7 50-13925.0 ND0.21 79




Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone 25ug/l2019.4 19.7-13125.0 E4ND3.8 77 6

Benzene 25ug/l1.024.0 78.4-12725.0 ND0.15 96 5


Chloroform 25ug/l1.022.0 77.6-12225.0 ND0.16 88 6



m,p-Xylenes 25ug/l2.051.6 70.8-13250.0 ND0.35 103 6


o-Xylene 25ug/l1.026.1 77.5-12225.0 ND0.19 104 6


Toluene 25ug/l1.024.5 83-11825.0 ND0.35 98 6


Trichloroethene 25ug/l1.026.0 77.3-12025.0 0.8300.19 101 5



















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.021.5 57.9-11825.0 ND0.31 86 10






Bromoform 25ug/l1.022.1 63.7-12925.0 ND0.19 88 5













Styrene 25ug/l1.023.8 55-13625.0 ND0.15 95 9



Vinyl Acetate 25ug/l1.018.2 50-13925.0 ND0.21 73 8




Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL

























trans-1,3-Dichloropropene ug/l1.00.320 E40.097





Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.018.6 45.6-14125.01.8 75

Acetone ug/l2021.4 22.4-15325.03.8 85

Benzene ug/l1.024.1 80.7-12025.00.15 96


Chloroform ug/l1.022.2 80.7-11925.00.16 89



m,p-Xylenes ug/l2.052.8 85-11550.00.35 106


o-Xylene ug/l1.026.5 85-11525.00.19 106


Toluene ug/l1.024.8 85-11525.00.35 99





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.023.4 58.5-13525.00.31 93






Bromoform ug/l1.022.0 71.9-13125.00.19 88













Styrene ug/l1.026.2 85-11525.00.15 105







Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.024.2 45.6-14125.0 R61.8 97 26

Acetone 25ug/l2033.8 22.4-15325.0 R63.8 135 45

Benzene 25ug/l1.024.5 80.7-12025.00.15 98 2


Chloroform 25ug/l1.021.0 80.7-11925.00.16 84 5



m,p-Xylenes 25ug/l2.051.2 85-11550.00.35 102 3


o-Xylene 25ug/l1.025.9 85-11525.00.19 103 2


Toluene 25ug/l1.024.1 85-11525.00.35 97 3





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.027.2 58.5-13525.00.31 109 15






Bromoform 25ug/l1.022.7 71.9-13125.00.19 91 3













Styrene 25ug/l1.025.5 85-11525.00.15 102 3







Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2020.7 19.7-13125.0 ND3.8 83

Benzene ug/l1.026.0 78.4-12725.0 ND0.15 104





m,p-Xylenes ug/l2.056.3 70.8-13250.0 ND0.35 113


o-Xylene ug/l1.028.1 77.5-12225.0 ND0.19 112


Toluene ug/l1.026.9 83-11825.0 ND0.35 108





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.022.2 57.9-11825.0 ND0.31 89






Bromoform ug/l1.022.3 63.7-12925.0 ND0.19 89













Styrene ug/l1.020.7 55-13625.0 ND0.15 83







Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone 25ug/l2023.4 19.7-13125.0 ND3.8 94 12

Benzene 25ug/l1.023.8 78.4-12725.0 ND0.15 95 9





m,p-Xylenes 25ug/l2.051.1 70.8-13250.0 ND0.35 102 10


o-Xylene 25ug/l1.025.5 77.5-12225.0 ND0.19 102 10


Toluene 25ug/l1.024.4 83-11825.0 ND0.35 98 10





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.023.4 57.9-11825.0 ND0.31 93 5






Bromoform 25ug/l1.021.0 63.7-12925.0 ND0.19 84 6













Styrene 25ug/l1.018.0 55-13625.0 ND0.15 72 14







Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l20ND V13.8































Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.036.7 45.6-14125.0 N11.8 147

Acetone ug/l2050.0 22.4-15325.0 V1, L33.8 200

Benzene ug/l1.025.4 80.7-12025.00.15 102


Chloroform ug/l1.026.9 80.7-11925.00.16 108



m,p-Xylenes ug/l2.024.3 85-11525.00.35 97


o-Xylene ug/l1.024.0 85-11525.00.19 96


Toluene ug/l1.024.3 85-11525.00.35 97





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.035.6 58.5-13525.0 N10.31 142


4-Methyl-2-pentanone (MIBK) ug/l5.032.7 72-12925.0 N10.43 131




Bromoform ug/l1.021.9 71.9-13125.00.19 88








Methyl-tert-butyl Ether (MTBE) ug/l1.029.6 81.8-11825.0 N10.18 119





Styrene ug/l1.025.5 85-11525.00.15 102







Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.031.5 45.6-14125.01.8 126 15

Acetone 25ug/l2041.9 22.4-15325.0 V1, L33.8 167 18

Benzene 25ug/l1.024.9 80.7-12025.00.15 99 2


Chloroform 25ug/l1.026.8 80.7-11925.00.16 107 0



m,p-Xylenes 25ug/l2.023.4 85-11525.00.35 94 4


o-Xylene 25ug/l1.023.3 85-11525.00.19 93 3


Toluene 25ug/l1.024.4 85-11525.00.35 97 0





















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.029.2 58.5-13525.00.31 117 20






Bromoform 25ug/l1.021.1 71.9-13125.00.19 84 4













Styrene 25ug/l1.024.9 85-11525.00.15 99 2







Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2035.4 19.7-13125.0 V1, N1ND3.8 142

Benzene ug/l1.025.9 78.4-12725.0 ND0.15 103


Chloroform ug/l1.029.1 77.6-12225.0 0.2200.16 116



m,p-Xylenes ug/l2.023.2 70.8-13225.0 ND0.35 93


o-Xylene ug/l1.024.2 77.5-12225.0 ND0.19 97


Toluene ug/l1.024.9 83-11825.0 ND0.35 100















1,2-Dichloroethane ug/l1.035.2 69.4-12925.0 M1ND0.20 141






Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.027.2 57.9-11825.0 ND0.31 109






Bromoform ug/l1.018.6 63.7-12925.0 ND0.19 74







Dichlorodifluoromethane ug/l1.035.0 71-13825.0 M1ND0.15 140






Styrene ug/l1.022.9 55-13625.0 ND0.15 92







Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





1,2-Dichloropropane 25ug/l1.031.3 81.1-11625.0 N1ND0.15 125 10


Acetone 25ug/l2042.9 19.7-13125.0 V1, N1ND3.8 172 19

Benzene 25ug/l1.028.4 78.4-12725.0 ND0.15 114 9


Chloroform 25ug/l1.033.0 77.6-12225.0 M10.2200.16 131 12


Ethylbenzene 25ug/l1.029.3 83.4-11625.0 N1ND0.16 117 10

m,p-Xylenes 25ug/l2.026.1 70.8-13225.0 ND0.35 104 12

Methylene Chloride 25ug/l2.033.9 74.6-11925.0 M1ND0.50 136 13

o-Xylene 25ug/l1.026.3 77.5-12225.0 ND0.19 105 8


Toluene 25ug/l1.026.8 83-11825.0 ND0.35 107 7



Trichlorofluoromethane 25ug/l1.035.7 82.4-13225.0 N1ND0.17 143 9

Vinyl chloride 25ug/l1.037.6 69.2-14325.0 M1ND0.24 150 21

1,1,1-Trichloroethane 25ug/l1.033.2 81.4-12525.0 M1ND0.22 133 14


1,1-Dichloroethane 25ug/l1.034.0 75.7-12625.0 M1ND0.17 136 9








1,2-Dichloroethane 25ug/l1.038.6 69.4-12925.0 M1ND0.20 154 9



1,3-Dichloropropane 25ug/l1.030.9 77.1-11925.0 M1ND0.18 124 14

1,4-Dichlorobenzene 25ug/l1.028.6 81.3-11025.0 N1ND0.16 114 15


Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.030.6 57.9-11825.0 N1ND0.31 122 11





Bromodichloromethane 25ug/l1.030.4 78.1-11825.0 N1ND0.15 122 11

Bromoform 25ug/l1.024.3 63.7-12925.0 N1bND0.19 97 27




Chloromethane 25ug/l5.038.3 64.1-13525.0 M1ND0.20 153 23

cis-1,3-Dichloropropene 25ug/l1.030.4 78.6-11825.0 N1ND0.17 122 13


Dichlorodifluoromethane 25ug/l1.040.6 71-13825.0 M1ND0.15 162 15

Methyl-tert-butyl Ether (MTBE) 25ug/l1.032.4 68.8-12625.0 N1ND0.18 130 11





Styrene 25ug/l1.026.2 55-13625.0 ND0.15 105 13


trans-1,3-Dichloropropene 25ug/l1.031.2 72.8-12325.0 N1ND0.097 125 14





Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






















2-Butanone (MEK) ug/kg250ND 200
















Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone ug/kg2501140 50.6-1331250210 91



Acetone ug/kg5001080 23.5-1821250330 87

Benzene ug/kg501210 76-107125023 97




Bromoform ug/kg501070 67.3-110125020 85





Chloroform ug/kg501170 69.8-114125024 94

Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes ug/kg1001090 83.5-107125034 87





o-Xylene ug/kg501120 82.8-108125016 90



Styrene ug/kg501120 82.1-111125012 90



Toluene ug/kg501130 81.3-106125015 91










Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone 25ug/kg2501260 50.6-1331250210 101 10



Acetone 25ug/kg5001120 23.5-1821250330 90 3

Benzene 25ug/kg501220 76-107125023 98 1




Bromoform 25ug/kg501100 67.3-110125020 88 3





Chloroform 25ug/kg501220 69.8-114125024 97 4

Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes 25ug/kg1001180 83.5-107125034 94 8





o-Xylene 25ug/kg501170 82.8-108125016 94 4



Styrene 25ug/kg501230 82.1-111125012 98 9



Toluene 25ug/kg501180 81.3-106125015 95 4










Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





1,1,2-Trichloroethane ug/kg50986 64.1-1081240 14023 68



















2-Hexanone ug/kg2501130 38.6-1461240 ND210 91



Acetone ug/kg500766 20.1-1821240 ND330 62

Benzene ug/kg50996 63.6-1081240 ND23 80










Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene ug/kg50966 60.8-1161240 ND16 78



Styrene ug/kg501030 64.5-1151240 ND12 83



Toluene ug/kg50999 62.6-1131240 ND15 80










Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





1,1,2-Trichloroethane 25ug/kg50983 64.1-1081240 14023 68 0



















2-Hexanone 25ug/kg250948 38.6-1461240 ND210 76 18



Acetone 25ug/kg500892 20.1-1821240 ND330 72 15

Benzene 25ug/kg501030 63.6-1081240 ND23 83 3










Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene 25ug/kg50981 60.8-1161240 ND16 79 2



Styrene 25ug/kg501040 64.5-1151240 ND12 84 1



Toluene 25ug/kg501020 62.6-1131240 ND15 83 2





Vinyl Acetate 25ug/kg50222 10-1271240 ND26 18 2





Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013





M1 Matrix spike recovery was high; the associated blank spike recovery was acceptable.


Q3 Sample received with improper chemical preservation.

R6 LFB/LFBD RPD exceeded the method acceptance limit. Recovery met acceptance criteria.

V1 CCV recovery was above method acceptance limits. This target analyte was not detected in the sample.



Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




454-9303





Sampled:

Received:

12/16/09


Project ID:

PSL0952

14682.013



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PSL0952

Tina Paulauskas




m_tloenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix; AZ 85040 (602) 437-3340 FAX (602) 454-9303

TAL-0013-550 (12/08) [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Page I of

[ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 THE LEADER IN ENVIRONMENTAL TESTING

L c)W~me~~~~~ Project/ PO Number: Analysis Required

8111 e. v ""'- ~fl. 11 ~n.>llA ~"3<p:(, IL-\~ca?.-. c 1'> sc..o {1'5~v'(, Ac_. ~:52-'S~

Project Manager: KJ/tCC C/l.A.rA.=> Phone Number: I{ 'bD- ':>"! t;, ~ ( '2.. tftt

0 Sampler: R~r ~~L({,LO Fax Number: -.{]

«..{, w - 3-t ~ ~ ( '2.. <t 5 N

Sample Description Sample Container #of Sampling Sampling ro Matrix Type Cont. Date lime Preservatives


IARJtt- yo- I'Liho'"t SOIL lf,Ot~t/ I 1"-lfh/r:Ji D1J5 MJZ.ol-/- v - 0/ Al3t.J-/D 1- J 'lib~ lt)lm'fl. tf,otWI 3 'o/lo/o~ /DSS 1-1 c../ v - 6? ~8'-1- m- ,"L,~oc; e 1 (t I tl v - 63 Af!Jt.J .... ,, o -t 2. J b01 tl ·n 3.. '"it:/C11 t3 '-IS II / ·- DL/ Af!J'-1 -Jio- rz. I (:,oCj' vuP l l I t 3 '1-fu./ CJ=t ~:St.tS It / ~ f!JS Af!fl- fA6 .. ru bo~ t{ II 3 ''Z{Ib/ c::s:r /t..fOO I t / ..__ o& A/Jt-1-11.0 .... t "2.,1 bO '\ tl t.l 3 P-fl'b/o<:r. t5C.f5 Ll v •1--0-

~~~ tL{Uj~~!Timfb c£S Rec~:.. ..n. · Date/Time: Turnaround Time:

~ (Check)

T '------· same day 72 hours Relinquished By: '-J Date/Time:

~ rFfeceived By: Date/Time: 24 hours 5 days

48 hours normal X \

Relinquished By: Date/Time:( IR~,ed·i~ - r~/t~i/&1 J f 5 Sample Integrity: (Check) IJ ... ~oc_ (j intact-~ on ice

\./' J

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on th1s project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.


454-9303

LABORATORY REPORT





Received:

Issued:

12/17/09-12/18/09

12/18/09

01/06/10 14:00




report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain(s) of Custody, 3 pages, are

included and are an integral part of this report.


Project: 14682.013


CASE NARRATIVE


PSL1052-01 AB5-10-121709 Soil

PSL1052-02 AB5-20-121709 Soil

PSL1052-03 AB5-30-121709 Soil

PSL1052-04 AB5-40-121709 Soil

PSL1052-05 AB5-50-121709 Soil

PSL1052-06 AB5-60-121709 Soil

PSL1052-07 AB5-70-121709 Soil

PSL1052-08 AB5-80-121709 Soil



PSL1052-11 AB5-98-121709 Water

PSL1052-12 AB5-110-121709 Water

PSL1052-13 AB5-110-121709 DUP Water


PSL1052-15 AB5-120-121809 Water

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas

<Page 1 of 75>


454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013







L3-Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above

acceptance limits.

N1-The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

N1a-Batch P9L2251 - The Laboratory Control Sample / Laboratory Control Sample Duplicate recovered

high and outside of the project specific acceptance limits for Chloroethane. The Laboratory Control Sample

Duplicate also recovered high and outside of the project specific acceptance limits for

1,2,4-trimethylbenzene, 1,2-dichloropropane, 1,3,5-trimethylbenzene, 1,3-dichlorobenzene,

1,4-dichlorobenzene, cis-1,3-dichloropropene and trans-1,3-dichloropropene. The Matrix Spike / Matrix

Spike Duplicate recovered high and outside of the project specific acceptance limits for Bromomethane and

Chloroethane. All recoveries were within the laboratory's historical limits. All associated samples are

non-detect for these analytes and therefore should not be impacted.

N1a-Batch P9L2251 - The Matrix Spike Duplicate does not provide useful RPD information due to the

varying weights of the methanol kits used for the Matrix Spike / Matrix Spike Duplicate. The Laboratory

Control Sample /Laboratory Control Sample Duplicate provide acceptable precision data for the batch.

N1a-Batch PSL2850 - The Laboratory Control Sample and Matrix Spike / Matrix Spike Duplicate

recovered low and outside of the project specific acceptance limits for Dichorodifluoromethane. The

recoveries were within the laboratory's historical limits. The associated sample was re-analyzed with all QC

within the project specific limits outside of holding time to confirm the initial results. The re-analysis

confirmed no detects for Dichlorodifluoromethane.

N1a-Batch P9L3108 - The Laboratory Control Sample and Matrix Spike recovered high and outside of the

project specific acceptance limits for 1,1,1-Trichloroethane, 1,1-Dichloroethane, 2,2-Dichloropropane,

Carbon tetrachloride and Chloromethane. The Labooratory Control Sample Duplicate and Matrix Spike

recovered high and outside of the project specific acceptance limits for MIBK and

trans-1,3-Dichloropropene. 1,1,1-Trichloroethane and 1,1-Dichloroethane were also high and outside of the

project specific acceptance limits in the Matrix Spike Duplicate. MTBE recovered high and outside of the

project specific acceptance limits in the Laboratory Control Sample Duplicate. All recoveries were within

the laboratory's historical limits. All associated samples are non-detect for these compounds and therefore

are not impacted.



Reviewed By:

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-09 (AB5-ERB-121709 - Water) Sampled: 12/17/09Reporting Units: ug/l





Acetone SW8260B P9L3108 4.720 E412/30/09 12/30/0913.8



Chloroform SW8260B P9L3108 0.201.0 L3, E412/30/09 12/30/0910.16



























SW8260B2,2-Dichloropropane P9L3108 2.0 ND E8, L312/30/09 12/30/0910.18






Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-09 (AB5-ERB-121709 - Water) - cont. Sampled: 12/17/09Reporting Units: ug/l























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-10RE1 (AB5-ERB-121709 - Water) Sampled: 12/17/09Reporting Units: ug/l









































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-10RE1 (AB5-ERB-121709 - Water) - cont. Sampled: 12/17/09Reporting Units: ug/l






















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-11 (AB5-98-121709 - Water) Sampled: 12/17/09Reporting Units: ug/l

SW8260B1,1,2,2-Tetrachloroethane 10A0010 1.0 ND E812/31/09 12/31/0910.12

SW8260B1,1-Dichloroethene 10A0010 1.0 ND E812/31/09 12/31/0910.23

SW8260B1,2-Dichloropropane 10A0010 1.0 ND E812/31/09 12/31/0910.15

2-Butanone (MEK) SW8260B 10A0010 4.15.0 E412/31/09 12/31/0911.8

SW8260BAcetone 10A0010 20 ND E812/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15

SW8260BCarbon tetrachloride 10A0010 1.0 ND E812/31/09 12/31/0910.19

SW8260BChloroform 10A0010 1.0 ND E812/31/09 12/31/0910.16

SW8260Bcis-1,2-Dichloroethene 10A0010 1.0 ND E812/31/09 12/31/0910.18

SW8260BEthylbenzene 10A0010 1.0 ND E812/31/09 12/31/0910.16

SW8260Bm,p-Xylenes 10A0010 2.0 ND E812/31/09 12/31/0910.35

SW8260BMethylene Chloride 10A0010 2.0 ND E812/31/09 12/31/0910.50

SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19

SW8260BTetrachloroethene 10A0010 1.0 ND E812/31/09 12/31/0910.23

Toluene SW8260B 10A0010 0.401.0 E412/31/09 12/31/0910.35

SW8260Btrans-1,2-Dichloroethene 10A0010 1.0 ND E812/31/09 12/31/0910.22

Trichloroethene SW8260B 10A0010 2.01.0 12/31/09 12/31/0910.19

SW8260BTrichlorofluoromethane 10A0010 1.0 ND E812/31/09 12/31/0910.17

SW8260BVinyl chloride 10A0010 1.0 ND E812/31/09 12/31/0910.24

SW8260B1,1,1-Trichloroethane 10A0010 1.0 ND E812/31/09 12/31/0910.22


SW8260B1,1-Dichloroethane 10A0010 1.0 ND E812/31/09 12/31/0910.17

SW8260B1,1-Dichloropropene 10A0010 1.0 ND E812/31/09 12/31/0910.19

SW8260B1,2,3-Trichlorobenzene 10A0010 2.0 ND E812/31/09 12/31/0910.27

SW8260B1,2,3-Trichloropropane 10A0010 2.0 ND E812/31/09 12/31/0910.31


SW8260B1,2,4-Trimethylbenzene 10A0010 1.0 ND E812/31/09 12/31/0910.13

SW8260B1,2-Dibromoethane (EDB) 10A0010 1.0 ND E812/31/09 12/31/0910.14

SW8260B1,2-Dichlorobenzene 10A0010 1.0 ND E812/31/09 12/31/0910.12







SW8260B2-Chlorotoluene 10A0010 1.0 ND E812/31/09 12/31/0910.17

2-Hexanone SW8260B 10A0010 3.25.0 E412/31/09 12/31/0910.31


SW8260B4-Methyl-2-pentanone (MIBK) 10A0010 5.0 ND E812/31/09 12/31/0910.43

SW8260BBromobenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-11 (AB5-98-121709 - Water) - cont. Sampled: 12/17/09Reporting Units: ug/l

SW8260BBromochloromethane 10A0010 1.0 ND E812/31/09 12/31/0910.20

SW8260BBromodichloromethane 10A0010 1.0 ND E812/31/09 12/31/0910.15

SW8260BBromoform 10A0010 1.0 ND E812/31/09 12/31/0910.19

SW8260BBromomethane 10A0010 2.0 ND E812/31/09 12/31/0910.22

SW8260BChlorobenzene 10A0010 1.0 ND E812/31/09 12/31/0910.12

SW8260BChloroethane 10A0010 1.0 ND E812/31/09 12/31/0910.26

SW8260BChloromethane 10A0010 5.0 ND E812/31/09 12/31/0910.20

SW8260Bcis-1,3-Dichloropropene 10A0010 1.0 ND E812/31/09 12/31/0910.17

SW8260BDibromochloromethane 10A0010 1.0 ND E812/31/09 12/31/0910.15

SW8260BDichlorodifluoromethane 10A0010 1.0 ND E812/31/09 12/31/0910.15

SW8260BMethyl-tert-butyl Ether (MTBE) 10A0010 1.0 ND E812/31/09 12/31/0910.18

SW8260Bn-Butylbenzene 10A0010 1.0 ND E812/31/09 12/31/0910.17

SW8260Bn-Propylbenzene 10A0010 1.0 ND E812/31/09 12/31/0910.18

SW8260Bp-Isopropyltoluene 10A0010 1.0 ND E812/31/09 12/31/0910.21

SW8260Bsec-Butylbenzene 10A0010 1.0 ND E812/31/09 12/31/0910.14

SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15

SW8260Btert-Butylbenzene 10A0010 1.0 ND E812/31/09 12/31/0910.17

SW8260Btrans-1,3-Dichloropropene 10A0010 1.0 ND E812/31/09 12/31/0910.097

SW8260BVinyl Acetate 10A0010 1.0 ND E812/31/09 12/31/0910.21




Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











Ethylbenzene SW8260B P9L2850 0.251.0 E412/29/09 12/29/0910.16































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit











SW8260BDichlorodifluoromethane P9L2850 1.0 ND E8, N1a12/29/09 12/29/0910.15



n-Propylbenzene SW8260B P9L2850 0.211.0 E412/29/09 12/29/0910.18






SW8260BVinyl Acetate P9L2850 1.0 ND E8, M212/29/09 12/29/0910.21




Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-13 (AB5-110-121709 DUP - Water) Sampled: 12/17/09Reporting Units: ug/l















Toluene SW8260B P9L2850 0.661.0 E412/29/09 12/29/0910.35


























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-13 (AB5-110-121709 DUP - Water) - cont. Sampled: 12/17/09Reporting Units: ug/l










SW8260BDichlorodifluoromethane P9L2850 1.0 ND E8, N1a12/29/09 12/29/0910.15













Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-14 (AB5-TB-121809 - Water) Sampled: 12/18/09Reporting Units: ug/l



1,2-Dichloropropane SW8260B P9L3108 0.251.0 E412/30/09 12/30/0910.15





SW8260BChloroform P9L3108 1.0 ND E8, L312/30/09 12/30/0910.16

































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-14 (AB5-TB-121809 - Water) - cont. Sampled: 12/18/09Reporting Units: ug/l























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit









SW8260BChloroform P9L3108 1.0 ND E8, L312/30/09 12/30/0910.16

































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-01 (AB5-10-121709 - Soil) Sampled: 12/17/09Reporting Units: ug/kg










SW8260B1,2,4-Trimethylbenzene P9L2251 89 ND V1, E812/17/09 12/28/091.7849










2-Butanone (MEK) SW8260B P9L2251 410450 E412/17/09 12/28/091.78360





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1052-01 (AB5-10-121709 - Soil) - cont. Sampled: 12/17/09Reporting Units: ug/kg























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit














Toluene SW8260B P9L2251 2882 E412/17/09 12/28/091.6425










Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit














Toluene SW8260B P9L2251 3180 E412/17/09 12/28/091.624










Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)


2 12/17/2009 08:10 12/18/2009 13:19 12/17/2009 08:10 12/28/2009 15:30SW8260B


2 12/17/2009 08:42 12/18/2009 13:19 12/17/2009 08:42 12/28/2009 16:02SW8260B


2 12/17/2009 09:30 12/18/2009 13:19 12/17/2009 09:30 12/28/2009 16:33SW8260B


2 12/17/2009 10:25 12/18/2009 13:19 12/17/2009 10:25 12/28/2009 17:04SW8260B


2 12/17/2009 11:20 12/18/2009 13:19 12/17/2009 11:20 12/28/2009 17:36SW8260B


2 12/17/2009 12:34 12/18/2009 13:19 12/17/2009 12:34 12/28/2009 18:07SW8260B


2 12/17/2009 14:00 12/18/2009 13:19 12/17/2009 14:00 12/28/2009 18:38SW8260B


2 12/17/2009 14:50 12/18/2009 13:19 12/17/2009 14:50 12/28/2009 19:09SW8260B

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL

Batch: 10A0010 Extracted: 12/21/09

Blank Analyzed: 12/31/2009 (10A0010-BLK1)




































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/31/2009 (10A0010-BS1)




2-Butanone (MEK) ug/l5.026.3 45.6-14125.01.8 105

Acetone ug/l2030.7 22.4-15325.03.8 123

Benzene ug/l1.024.4 80.7-12025.00.15 98


Chloroform ug/l1.025.9 80.7-11925.00.16 103



m,p-Xylenes ug/l2.023.6 85-11525.00.35 94


o-Xylene ug/l1.024.0 85-11525.00.19 96


Toluene ug/l1.023.5 85-11525.00.35 94





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/31/2009 (10A0010-BS1)


2-Hexanone ug/l5.025.3 58.5-13525.00.31 101






Bromoform ug/l1.024.0 71.9-13125.00.19 96













Styrene ug/l1.025.1 85-11525.00.15 100







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Dup Analyzed: 12/31/2009 (10A0010-BSD1)




2-Butanone (MEK) 25ug/l5.025.4 45.6-14125.01.8 101 3

Acetone 25ug/l2029.6 22.4-15325.03.8 118 3

Benzene 25ug/l1.023.5 80.7-12025.00.15 94 4


Chloroform 25ug/l1.024.1 80.7-11925.00.16 96 7



m,p-Xylenes 25ug/l2.023.6 85-11525.00.35 94 0


o-Xylene 25ug/l1.023.1 85-11525.00.19 93 4


Toluene 25ug/l1.021.3 85-11525.00.35 85 10





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.029.2 58.5-13525.00.31 117 14






Bromoform 25ug/l1.024.6 71.9-13125.00.19 98 2













Styrene 25ug/l1.024.2 85-11525.00.15 97 4







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Analyzed: 12/31/2009 (10A0010-MS1) Source: PSL1085-06




2-Butanone (MEK) ug/l5.029.1 41.6-13025.0 3.821.8 101

Acetone ug/l2048.7 19.7-13125.0 N1a15.23.8 134

Benzene ug/l1.025.0 78.4-12725.0 ND0.15 100





m,p-Xylenes ug/l2.024.6 70.8-13225.0 ND0.35 99


o-Xylene ug/l1.024.0 77.5-12225.0 ND0.19 96


Toluene ug/l1.022.7 83-11825.0 ND0.35 91



Trichlorofluoromethane ug/l1.033.6 82.4-13225.0 N1aND0.17 135


















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.028.0 57.9-11825.0 ND0.31 112






Bromoform ug/l1.022.5 63.7-12925.0 ND0.19 90













Styrene ug/l1.024.6 55-13625.0 ND0.15 98







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Dup Analyzed: 12/31/2009 (10A0010-MSD1) Source: PSL1085-06




2-Butanone (MEK) 25ug/l5.023.9 41.6-13025.0 3.821.8 80 19

Acetone 25ug/l2037.7 19.7-13125.0 15.23.8 90 25

Benzene 25ug/l1.021.8 78.4-12725.0 ND0.15 87 13





m,p-Xylenes 25ug/l2.022.0 70.8-13225.0 ND0.35 88 11


o-Xylene 25ug/l1.022.7 77.5-12225.0 ND0.19 91 5


Toluene 25ug/l1.021.2 83-11825.0 ND0.35 85 7





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.022.1 57.9-11825.0 ND0.31 88 24






Bromoform 25ug/l1.021.0 63.7-12925.0 ND0.19 84 7













Styrene 25ug/l1.023.0 55-13625.0 ND0.15 92 6







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.026.8 45.6-14125.01.8 107

Acetone ug/l2032.6 22.4-15325.03.8 131

Benzene ug/l1.024.2 80.7-12025.00.15 97


Chloroform ug/l1.023.7 80.7-11925.00.16 95



m,p-Xylenes ug/l2.025.3 85-11525.00.35 101


o-Xylene ug/l1.023.8 85-11525.00.19 95


Toluene ug/l1.023.9 85-11525.00.35 95





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.025.0 58.5-13525.00.31 100






Bromoform ug/l1.024.5 71.9-13125.00.19 98













Styrene ug/l1.025.1 85-11525.00.15 100







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.027.3 45.6-14125.01.8 109 2

Acetone 25ug/l2030.9 22.4-15325.03.8 123 6

Benzene 25ug/l1.023.8 80.7-12025.00.15 95 2


Chloroform 25ug/l1.023.2 80.7-11925.00.16 93 2



m,p-Xylenes 25ug/l2.024.0 85-11525.00.35 96 5


o-Xylene 25ug/l1.023.5 85-11525.00.19 94 1


Toluene 25ug/l1.022.4 85-11525.00.35 90 6





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.026.4 58.5-13525.00.31 106 6






Bromoform 25ug/l1.025.9 71.9-13125.00.19 104 6







Dichlorodifluoromethane 25ug/l1.017.1 72.8-13025.0 N1a0.15 68 7






Styrene 25ug/l1.025.0 85-11525.00.15 100 0







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2024.2 19.7-13125.0 ND3.8 97

Benzene ug/l1.023.4 78.4-12725.0 ND0.15 94




Ethylbenzene ug/l1.024.2 83.4-11625.0 0.2500.16 96

m,p-Xylenes ug/l2.023.7 70.8-13225.0 ND0.35 95


o-Xylene ug/l1.023.3 77.5-12225.0 ND0.19 93


Toluene ug/l1.022.8 83-11825.0 ND0.35 91





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.025.8 57.9-11825.0 ND0.31 103






Bromoform ug/l1.025.8 63.7-12925.0 ND0.19 103







Dichlorodifluoromethane ug/l1.016.3 71-13825.0 N1aND0.15 65



n-Propylbenzene ug/l1.026.0 76-12425.0 0.2100.18 103



Styrene ug/l1.014.0 55-13625.0 ND0.15 56



Vinyl Acetate ug/l1.012.1 50-13925.0 M2ND0.21 49




Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone 25ug/l2029.0 19.7-13125.0 ND3.8 116 18

Benzene 25ug/l1.024.2 78.4-12725.0 ND0.15 97 4




Ethylbenzene 25ug/l1.024.6 83.4-11625.0 0.2500.16 97 2

m,p-Xylenes 25ug/l2.024.1 70.8-13225.0 ND0.35 96 2


o-Xylene 25ug/l1.023.7 77.5-12225.0 ND0.19 95 2


Toluene 25ug/l1.023.3 83-11825.0 ND0.35 93 2





















Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.026.7 57.9-11825.0 ND0.31 107 4






Bromoform 25ug/l1.027.4 63.7-12925.0 ND0.19 110 6







Dichlorodifluoromethane 25ug/l1.016.8 71-13825.0 N1aND0.15 67 3



n-Propylbenzene 25ug/l1.026.0 76-12425.0 0.2100.18 103 0



Styrene 25ug/l1.014.1 55-13625.0 ND0.15 56 1







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.027.8 45.6-14125.01.8 111

Acetone ug/l2024.5 22.4-15325.03.8 98

Benzene ug/l1.029.3 80.7-12025.00.15 117

Carbon tetrachloride ug/l1.031.4 82.5-12325.0 N1a0.19 126

Chloroform ug/l1.030.5 80.7-11925.0 L30.16 122



m,p-Xylenes ug/l2.052.6 85-11550.00.35 105


o-Xylene ug/l1.026.8 85-11525.00.19 107


Toluene ug/l1.025.6 85-11525.00.35 102





1,1,1-Trichloroethane ug/l1.030.9 83.2-12025.0 N1a0.22 123


1,1-Dichloroethane ug/l1.031.2 78.8-12225.0 N1a0.17 125













2,2-Dichloropropane ug/l2.034.7 70.8-12825.0 N1a0.18 139

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.024.2 58.5-13525.00.31 97






Bromoform ug/l1.021.6 71.9-13125.00.19 86




Chloromethane ug/l5.030.9 70.9-12325.0 N1a0.20 124









Styrene ug/l1.025.9 85-11525.00.15 104







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.031.3 45.6-14125.01.8 125 12

Acetone 25ug/l2027.6 22.4-15325.03.8 110 12

Benzene 25ug/l1.028.2 80.7-12025.00.15 113 4


Chloroform 25ug/l1.027.1 80.7-11925.00.16 108 12



m,p-Xylenes 25ug/l2.050.6 85-11550.00.35 101 4


o-Xylene 25ug/l1.026.2 85-11525.00.19 105 2


Toluene 25ug/l1.025.1 85-11525.00.35 100 2




















2,2-Dichloropropane 25ug/l2.032.9 70.8-12825.0 L30.18 132 5

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.028.0 58.5-13525.00.31 112 15


4-Methyl-2-pentanone (MIBK) 25ug/l5.032.6 72-12925.0 N1a0.43 130 12




Bromoform 25ug/l1.023.2 71.9-13125.00.19 93 7








Methyl-tert-butyl Ether (MTBE) 25ug/l1.029.9 81.8-11825.0 N1a0.18 120 4





Styrene 25ug/l1.025.6 85-11525.00.15 103 1


trans-1,3-Dichloropropene 25ug/l1.030.5 82.2-12125.0 N1a0.097 122 4





Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2025.2 19.7-13125.0 3.773.8 86

Benzene ug/l1.030.8 78.4-12725.0 ND0.15 123

Carbon tetrachloride ug/l1.033.2 80.7-12825.0 N1aND0.19 133

Chloroform ug/l1.030.1 77.6-12225.0 0.2000.16 119

cis-1,2-Dichloroethene ug/l1.030.8 80.1-11925.0 N1aND0.18 123


m,p-Xylenes ug/l2.054.5 70.8-13250.0 ND0.35 109

Methylene Chloride ug/l2.030.2 74.6-11925.0 N1aND0.50 121

o-Xylene ug/l1.027.7 77.5-12225.0 ND0.19 111


Toluene ug/l1.026.9 83-11825.0 ND0.35 108

trans-1,2-Dichloroethene ug/l1.031.5 81.3-12325.0 N1aND0.22 126




1,1,1-Trichloroethane ug/l1.033.1 81.4-12525.0 N1aND0.22 132


1,1-Dichloroethane ug/l1.033.2 75.7-12625.0 N1aND0.17 133

1,1-Dichloropropene ug/l1.031.1 81.4-12325.0 N1aND0.19 124












2,2-Dichloropropane ug/l2.034.9 66.5-13425.0 N1aND0.18 140

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.027.7 57.9-11825.0 ND0.31 111


4-Methyl-2-pentanone (MIBK) ug/l5.034.3 65.6-12725.0 N1aND0.43 137



Bromodichloromethane ug/l1.029.9 78.1-11825.0 N1aND0.15 120

Bromoform ug/l1.023.2 63.7-12925.0 ND0.19 93




Chloromethane ug/l5.034.5 64.1-13525.0 N1aND0.20 138









Styrene ug/l1.026.5 55-13625.0 ND0.15 106


trans-1,3-Dichloropropene ug/l1.030.9 72.8-12325.0 N1aND0.097 124





Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone 25ug/l2022.9 19.7-13125.0 3.773.8 77 10

Benzene 25ug/l1.029.8 78.4-12725.0 ND0.15 119 3


Chloroform 25ug/l1.029.4 77.6-12225.0 0.2000.16 117 2

cis-1,2-Dichloroethene 25ug/l1.030.3 80.1-11925.0 N1aND0.18 121 2


m,p-Xylenes 25ug/l2.051.9 70.8-13250.0 ND0.35 104 5


o-Xylene 25ug/l1.026.8 77.5-12225.0 ND0.19 107 3


Toluene 25ug/l1.025.8 83-11825.0 ND0.35 103 4

trans-1,2-Dichloroethene 25ug/l1.031.1 81.3-12325.0 N1aND0.22 124 1




1,1,1-Trichloroethane 25ug/l1.031.7 81.4-12525.0 N1aND0.22 127 4


1,1-Dichloroethane 25ug/l1.032.0 75.7-12625.0 N1aND0.17 128 4














Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.025.4 57.9-11825.0 ND0.31 101 9






Bromoform 25ug/l1.022.1 63.7-12925.0 ND0.19 88 5













Styrene 25ug/l1.025.5 55-13625.0 ND0.15 102 4







Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone ug/kg250971 50.6-1331250210 78



Acetone ug/kg500684 23.5-1821250330 55

Benzene ug/kg501220 76-107125023 98




Bromoform ug/kg501110 67.3-110125020 88




Chloroethane ug/kg50894 10-36.21250 N1a31 72

Chloroform ug/kg501220 69.8-114125024 97

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes ug/kg1001280 83.5-107125034 102





o-Xylene ug/kg501240 82.8-108125016 99



Styrene ug/kg501280 82.1-111125012 102



Toluene ug/kg501190 81.3-106125015 95










Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL












1,2,4-Trimethylbenzene 25ug/kg501380 77.2-1081250 N1a27 110 5




1,2-Dichloropropane 25ug/kg501350 78.8-1051250 N1a19 108 4


1,3-Dichlorobenzene 25ug/kg501340 81-1061250 N1a12 107 5


1,4-Dichlorobenzene 25ug/kg501350 80.6-1051250 N1a19 108 7




2-Hexanone 25ug/kg2501100 50.6-1331250210 88 12



Acetone 25ug/kg500852 23.5-1821250330 68 22

Benzene 25ug/kg501280 76-107125023 102 5




Bromoform 25ug/kg501190 67.3-110125020 95 7




Chloroethane 25ug/kg50967 10-36.21250 N1a31 77 8

Chloroform 25ug/kg501320 69.8-114125024 105 8

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





cis-1,3-Dichloropropene 25ug/kg501390 77.3-1081250 N1a15 111 5




m,p-Xylenes 25ug/kg1001310 83.5-107125034 105 3





o-Xylene 25ug/kg501320 82.8-108125016 105 6



Styrene 25ug/kg501380 82.1-111125012 110 7



Toluene 25ug/kg501220 81.3-106125015 98 3


trans-1,3-Dichloropropene 25ug/kg501400 72.4-1091250 N1a15 112 8








Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









1,2,3-Trichlorobenzene ug/kg1301560 39.2-1251610 35.723 95















2-Hexanone ug/kg3201390 38.6-1461610 ND270 86



Acetone ug/kg6401320 20.1-1821610 ND430 82

Benzene ug/kg641560 63.6-1081610 ND30 97





Bromomethane ug/kg3201510 10-93.51610 N1aND11 94



Chloroethane ug/kg641370 10.3-34.11610 N1aND39 85


Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene ug/kg641610 60.8-1161610 ND20 100



Styrene ug/kg641710 64.5-1151610 ND16 106


Tetrachloroethene ug/kg641550 56.7-1301610 ND12 96

Toluene ug/kg641500 62.6-1131610 ND19 93










Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane 25ug/kg972310 58.2-1152430 N1aND38 95 39

1,1,2,2-Tetrachloroethane 25ug/kg972210 57.5-1082430 N1aND34 91 41


1,1-Dichloroethane 25ug/kg972410 61.8-1102430 N1aND29 99 38

1,1-Dichloroethene 25ug/kg972330 39.2-1232430 N1aND45 96 39

1,1-Dichloropropene 25ug/kg972260 60.6-1112430 N1aND38 93 43

1,2,3-Trichlorobenzene 25ug/kg1902380 39.2-1252430 N1a35.735 96 42

1,2,3-Trichloropropane 25ug/kg1902200 59.4-1102430 N1aND38 91 38

1,2,4-Trichlorobenzene 25ug/kg972410 43.5-1182430 N1aND38 99 38

1,2,4-Trimethylbenzene 25ug/kg972610 54.6-1202430 N1aND53 107 43

1,2-Dibromoethane (EDB) 25ug/kg972390 64.2-1082430 N1aND30 99 40

1,2-Dichlorobenzene 25ug/kg972480 63.5-1082430 N1aND41 102 40


1,2-Dichloropropane 25ug/kg972510 66.7-1062430 N1aND37 103 44


1,3-Dichlorobenzene 25ug/kg972500 62-1112430 N1aND24 103 42




2-Butanone (MEK) 25ug/kg4902210 34.5-1542430 N1aND390 91 31

2-Chlorotoluene 25ug/kg972520 58.1-1132430 N1aND29 104 42

2-Hexanone 25ug/kg4902030 38.6-1462430 N1aND410 83 37


4-Methyl-2-pentanone (MIBK) 25ug/kg4902010 56.5-1112430 N1aND330 83 40

Acetone 25ug/kg9701840 20.1-1822430 N1aND640 76 33

Benzene 25ug/kg972410 63.6-1082430 N1aND45 99 43

Bromobenzene 25ug/kg972540 64.2-1092430 N1aND35 105 42

Bromochloromethane 25ug/kg972460 60-1232430 N1aND47 101 40

Bromodichloromethane 25ug/kg972440 61.8-1112430 N1aND35 100 42

Bromoform 25ug/kg972290 57.5-1092430 N1aND39 94 39

Bromomethane 25ug/kg4902270 10-93.52430 N1aND16 94 40

Carbon tetrachloride 25ug/kg972300 44.5-1232430 N1aND39 95 46

Chlorobenzene 25ug/kg972460 66.9-1072430 N1aND22 101 44

Chloroethane 25ug/kg972110 10.3-34.12430 N1aND59 87 43

Chloroform 25ug/kg972440 63.2-1122430 N1aND47 101 38

Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chloromethane 25ug/kg4901980 15.3-1232430 N1aND50 82 40

cis-1,2-Dichloroethene 25ug/kg972320 64.1-1082430 N1aND41 96 37

cis-1,3-Dichloropropene 25ug/kg972530 63.3-1102430 N1aND30 104 43

Dibromochloromethane 25ug/kg972430 63-1092430 N1aND22 100 39

Dichlorodifluoromethane 25ug/kg971680 10-1182430 N1aND37 69 42

Ethylbenzene 25ug/kg972540 62.4-1132430 N1aND25 105 44

m,p-Xylenes 25ug/kg1902460 57.7-1182430 N1aND66 102 41

Methylene Chloride 25ug/kg1902230 57.6-1062430 N1aND61 92 37

Methyl-tert-butyl Ether (MTBE) 25ug/kg972440 54.9-1182430 N1aND34 101 37

n-Butylbenzene 25ug/kg972530 47.8-1322430 N1aND34 104 41

n-Propylbenzene 25ug/kg972660 55.8-1172430 N1aND33 110 43

o-Xylene 25ug/kg972450 60.8-1162430 N1aND31 101 42

p-Isopropyltoluene 25ug/kg972520 59-1162430 N1aND39 104 42

sec-Butylbenzene 25ug/kg972480 60.3-1172430 N1aND34 102 39

Styrene 25ug/kg972470 64.5-1152430 N1aND24 102 37

tert-Butylbenzene 25ug/kg972440 60.3-1142430 N1aND40 100 41

Tetrachloroethene 25ug/kg972500 56.7-1302430 N1aND19 103 47

Toluene 25ug/kg972390 62.6-1132430 N1aND29 99 46

trans-1,2-Dichloroethene 25ug/kg972430 58.4-1122430 N1aND35 100 41

trans-1,3-Dichloropropene 25ug/kg972520 61.4-1092430 N1aND29 104 41

Trichloroethene 25ug/kg972470 64.9-1102430 N1aND41 102 42

Trichlorofluoromethane 25ug/kg972350 31.8-1262430 N1aND61 97 44


Vinyl chloride 25ug/kg971600 26.1-1302430 N1aND48 66 43




Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013










Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




454-9303





Sampled:

Received:

12/17/09-12/18/09


Project ID:

PSL1052

14682.013



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PSL1052

Tina Paulauskas




TAL-0013-550 (12/08)

Client Name I Address:, !Yl, .

N'f'v/i.-e_ G/1.-.oJV'-'~'"' X ~~~ '7 l. t/IA.. ~'L v~M :tl ;!.~6 ~ L c!> \'{"";:> ~Vfl A L.. Bs z...s- 8,

Project Manager:~\ (Z&L, ~f:¥'=.

Sampler:.n,,n..nn ,.--I'V-'·V't' V\ P t~~

Sample Container


tBf'hoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson - 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number:

Phone Number:

l{ '2? o - ~ Cf. --G - /"Z 'i <f Fax Number: '-t&D -')'-/~- l"Z-lf5

Q XI N

#of Sampling Sampling . rtl

Analysis Required

Page I of

Sample Description Matrix Type Cont. Date Time Preservatives W Special Instructions

lA85- Zo ... l"tl701 r t

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l-:\~V'11~~·~-'~ \\.....eij===+~ • v--z__....:::::::,~___:_( "2.--.!.}~1-l';-1:.1 a;:q~=-..:.1 ~L:::::....::·0~S~-~---:---:-1'~-'~'1JL/---~:ft=--·_.:.r.::z..-..Ll.l ?2.~,!! L~~<'f~/.!:."Z~2:::::·D~-----1 same day ___ 72 hours __ _ Relinquis~~ V · / o/"te/Time: . 13.£_<;:~~: v Date/Time: 24 hours

o!'l'f.,#Cf---· --· lL I 1& ( otj I.~ J .·dj ------- 48 hours '

5 days

normal X' Relinquisl ed By: Date/Time: c:eceive:~a~ Sample Integrity: (Check) . ..:A·'

intact ,X' on ice,.X' _ _ ).fa I

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) Will be disposed of after 30 days.

-------- ---- ----------~-~~~--~~~---------~-~~~~~-

IT est America THE LEADER IN ENVIRONMENTAL TESTING

TAL-0013-550 (12/08)

Client Name/Address:


,..flPhoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ 1 Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ 1 Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number: Analysis Required f\ll'ti£L 6/t..:::::. ~'\iLl- '1... B,}/1 fZ_, V ~~ ~(:)fl. I)~ J!-'39(, tt.Jb2.Z..bl:, S~b "{"'f-s\')t'\vrt.. Ac:... B~-z....'S-'6

Project Manager: K.t. ,z.l(__ cJLAt <--=.. Phone Number: 'i '60 - "b '{. 'G- p .. "'-'1 ()

Sampler:RCJQ.N\.:r"F-v~l- Tl.-\...-0 Fax Number: ..[)

t.[, 'f!,o ~ "b '-i. ~ -1 "'Z..-lf ~ ~

Sample Description Sample Container #of Sampling Sampling

Preservatives ('0

Matrix Type Cont. Date Time

AI3S-!h-t'2J'So_<7 lJM't'A 'fOu.,) I ''/tel eli - t+c-t v --l't.l A85- n..u-rz.,Bo~ It rl -6 ~o/18[ 0"{ t Z.. ?u II v ---r ~ ..,

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l3_Cj intact -

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+ MS/MSP

(Check)

72 hours

5 days

normal ~ (Check)

)C ? .. on ice ,it? Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days. ·


THE LEADER IN ENVIRONMENTAL TESTING

~oenix- 4625 E. Cotton Center Blvd., Suite 189,Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

TAL-0013-550 (12/08)

Client Name I Address.A-fr4 . Project/ PO Number: Analysis Required AMt-e__ bfi-.:>f'A x 1>1' 7 t. vtA.. i)-t. v~ ~ :>c:v(:, JYb~t-o~3 5 c.. c> If";> bAvR... A 7.- Bs t.S' 8

Project Manager:~~\. (Z&L, 6r2../¥6 Phone Number:

'-(~o- ?>tt,~-/"Z'i'f 0 Sampler:~~ Pt~~ Fax Number: ~

'-[&D _.)'-f'O- 17.-'-fS N Sample Description Sample Container #of Sampling Sampling

Preservatives d) Matrix Type Cont. Date Time

A/35 -J D- {(.J7C><j 5t>tL '-{O;u./ I 17.fq/fl1 o&o ll1t~ / "--~(!)

AfJ5- 2,o .-J7.l7t:Ff I l lt I l?..frl/ .:s, oeH"Z. I l L/ . () ( -A(3S'-3c .. €'2.ll09 ll ( ( l I <--frz{ Cfl, o93L:; II / -D ? -Af;5- '-{O-I'Zl7CJ't I t. /( I 1 7'n/o~ 1025 I( ~ ~ -ct)c__,

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AfJ) ..r f.RIJ- (2, nocr W/.tTM qo,,f 3 "Z-h7/q J5DL( Wz.[ /"' -t. )1 1-\(35-E~- Ll.. Li TOj t\. ~l 3 ~"2/~7~crr. lbt5 L\ / -I 0 #35- 96=t£..t7CA L\ n 3 L2/t7/c::J1 l7'30 ll / -[ f AtJtS -11 o-l '1. • bO\ Lt !( ~

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f-.tJ5 .. /1 D -17._.1 ~ D'1., bu {) I t ll 3 l'f,'a/oi £005 "' !( 7 --I ~

QQ~h:;;q v-1<_ Date/Time: Received!

·I;Jlkf-- I r;te/Time: Turnaround Time:

( rz-J r ~race -z-z.,0s tz. I e, 1!1 I -z '2tS same day

Relinquis~V · l %te/Time: ~: -v· Date/Time: 24 hours

"""-~ -- ( L !@ (}tj I,'?., ) 6J 48 hours

Relinquished By: I Date/Time:

~ Receivw_?_b~ t7~evR1or ,~q Sample Integrity:

I- ;\ intact X" ' I T

Page I of


·,.

MS/MS{:)

.SltMt Plict?~

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(Check)

72 hours

5 days

normal .::><" (Check) • - _. bt

on ice£____}-&

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) Will be disposed of after 30 days.

I--


454-9303

LABORATORY REPORT





Received:

Issued:

12/18/09-12/19/09

12/19/09

01/06/10 14:35







Project: 14682.013


CASE NARRATIVE



PSL1082-02 AB6-10-121809 Soil

PSL1082-03 AB6-30-121809 Soil

PSL1082-04 AB6-40-121809 Soil


PSL1082-06 AB6-60-121909 Soil

PSL1082-07 AB6-70-121909 Soil

PSL1082-08 AB6-70-121909 DUP Soil

Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas

<Page 1 of 41>


454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013







N1a-The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

N1a-N1a-Batch P9L2251 - The Laboratory Control Sample / Laboratory Control Sample Duplicate

recovered high and outside of the project specific acceptance limits for Chloroethane. The Laboratory

Control Sample Duplicate also recovered high and outside of the project specific acceptance limits for

1,2,4-trimethylbenzene, 1,2-dichloropropane, 1,3,5-trimethylbenzene, 1,3-dichlorobenzene,

1,4-dichlorobenzene, cis-1,3-dichloropropene and trans-1,3-dichloropropene. The Matrix Spike / Matrix

Spike Duplicate recovered high and outside of the project specific acceptance limits for Bromomethane and

Chloroethane. All recoveries were within the laboratory's historical limits. All associated samples are

non-detect for these analytes and therefore should not be impacted.

N1a-Batch P9L2251 - The Matrix Spike Duplicate does not provide useful RPD information due to the

varying weights of the methanol kits used for the Matrix Spike / Matrix Spike Duplicate. The Laboratory

Control Sample /Laboratory Control Sample Duplicate provide acceptable precision data for the batch.



Reviewed By:

Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit





SW8260B2-Butanone (MEK) 10A0010 5.0 ND E812/31/09 12/31/0911.8

Acetone SW8260B 10A0010 5.020 E412/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15


Chloroform SW8260B 10A0010 0.231.0 E412/31/09 12/31/0910.16




Methylene Chloride SW8260B 10A0010 0.522.0 E412/31/09 12/31/0910.50

SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19


Toluene SW8260B 10A0010 0.361.0 E412/31/09 12/31/0910.35


SW8260BTrichloroethene 10A0010 1.0 ND E812/31/09 12/31/0910.19




















SW8260B2-Hexanone 10A0010 5.0 ND E812/31/09 12/31/0910.31




Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15







Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit






SW8260BAcetone 10A0010 20 ND E812/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15







SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19


SW8260BToluene 10A0010 1.0 ND E812/31/09 12/31/0910.35


























Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15







Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit




Methylene Chloride SW8260B P9L2251 47140 E412/19/09 12/29/091.3844




















Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1082-08 (AB6-70-121909 DUP - Soil) Sampled: 12/19/09Reporting Units: ug/kg







1,2,3-Trichlorobenzene SW8260B P9L2251 36130 E412/19/09 12/23/091.3524


































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1082-08 (AB6-70-121909 DUP - Soil) - cont. Sampled: 12/19/09Reporting Units: ug/kg


















SW8260BVinyl Acetate P9L2251 67 ND E8, M212/19/09 12/23/091.3534





Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)


2 12/18/2009 15:30 12/19/2009 11:40 12/18/2009 15:30 12/29/2009 01:37SW8260B


2 12/18/2009 17:05 12/19/2009 11:40 12/18/2009 17:05 12/29/2009 02:08SW8260B


2 12/18/2009 18:00 12/19/2009 11:40 12/18/2009 18:00 12/29/2009 02:39SW8260B


2 12/19/2009 09:50 12/19/2009 11:40 12/19/2009 09:50 12/29/2009 03:10SW8260B


2 12/19/2009 10:50 12/19/2009 11:40 12/19/2009 10:50 12/29/2009 03:42SW8260B

Sample ID: AB6-70-121909 DUP (PSL1082-08) - Soil

2 12/19/2009 10:50 12/19/2009 11:40 12/19/2009 10:50 12/23/2009 01:15SW8260B

Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/31/2009 (10A0010-BS1)




2-Butanone (MEK) ug/l5.026.3 45.6-14125.01.8 105

Acetone ug/l2030.7 22.4-15325.03.8 123

Benzene ug/l1.024.4 80.7-12025.00.15 98


Chloroform ug/l1.025.9 80.7-11925.00.16 103



m,p-Xylenes ug/l2.023.6 85-11525.00.35 94


o-Xylene ug/l1.024.0 85-11525.00.19 96


Toluene ug/l1.023.5 85-11525.00.35 94





















Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/31/2009 (10A0010-BS1)


2-Hexanone ug/l5.025.3 58.5-13525.00.31 101






Bromoform ug/l1.024.0 71.9-13125.00.19 96













Styrene ug/l1.025.1 85-11525.00.15 100







Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.025.4 45.6-14125.01.8 101 3

Acetone 25ug/l2029.6 22.4-15325.03.8 118 3

Benzene 25ug/l1.023.5 80.7-12025.00.15 94 4


Chloroform 25ug/l1.024.1 80.7-11925.00.16 96 7



m,p-Xylenes 25ug/l2.023.6 85-11525.00.35 94 0


o-Xylene 25ug/l1.023.1 85-11525.00.19 93 4


Toluene 25ug/l1.021.3 85-11525.00.35 85 10





















Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.029.2 58.5-13525.00.31 117 14






Bromoform 25ug/l1.024.6 71.9-13125.00.19 98 2













Styrene 25ug/l1.024.2 85-11525.00.15 97 4







Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.029.1 41.6-13025.0 3.821.8 101

Acetone ug/l2048.7 19.7-13125.0 N1a15.23.8 134

Benzene ug/l1.025.0 78.4-12725.0 ND0.15 100





m,p-Xylenes ug/l2.024.6 70.8-13225.0 ND0.35 99


o-Xylene ug/l1.024.0 77.5-12225.0 ND0.19 96


Toluene ug/l1.022.7 83-11825.0 ND0.35 91





















Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.028.0 57.9-11825.0 ND0.31 112






Bromoform ug/l1.022.5 63.7-12925.0 ND0.19 90













Styrene ug/l1.024.6 55-13625.0 ND0.15 98







Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.023.9 41.6-13025.0 3.821.8 80 19

Acetone 25ug/l2037.7 19.7-13125.0 15.23.8 90 25

Benzene 25ug/l1.021.8 78.4-12725.0 ND0.15 87 13





m,p-Xylenes 25ug/l2.022.0 70.8-13225.0 ND0.35 88 11


o-Xylene 25ug/l1.022.7 77.5-12225.0 ND0.19 91 5


Toluene 25ug/l1.021.2 83-11825.0 ND0.35 85 7





















Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.022.1 57.9-11825.0 ND0.31 88 24






Bromoform 25ug/l1.021.0 63.7-12925.0 ND0.19 84 7













Styrene 25ug/l1.023.0 55-13625.0 ND0.15 92 6







Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone ug/kg250971 50.6-1331250210 78



Acetone ug/kg500684 23.5-1821250330 55

Benzene ug/kg501220 76-107125023 98




Bromoform ug/kg501110 67.3-110125020 88





Chloroform ug/kg501220 69.8-114125024 97

Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes ug/kg1001280 83.5-107125034 102





o-Xylene ug/kg501240 82.8-108125016 99



Styrene ug/kg501280 82.1-111125012 102



Toluene ug/kg501190 81.3-106125015 95










Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


















1,3-Dichlorobenzene 25ug/kg501340 81-1061250 N1a12 107 5


1,4-Dichlorobenzene 25ug/kg501350 80.6-1051250 N1a19 108 7




2-Hexanone 25ug/kg2501100 50.6-1331250210 88 12



Acetone 25ug/kg500852 23.5-1821250330 68 22

Benzene 25ug/kg501280 76-107125023 102 5




Bromoform 25ug/kg501190 67.3-110125020 95 7





Chloroform 25ug/kg501320 69.8-114125024 105 8

Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





cis-1,3-Dichloropropene 25ug/kg501390 77.3-1081250 N1a15 111 5




m,p-Xylenes 25ug/kg1001310 83.5-107125034 105 3





o-Xylene 25ug/kg501320 82.8-108125016 105 6



Styrene 25ug/kg501380 82.1-111125012 110 7



Toluene 25ug/kg501220 81.3-106125015 98 3


trans-1,3-Dichloropropene 25ug/kg501400 72.4-1091250 N1a15 112 8








Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









1,2,3-Trichlorobenzene ug/kg1301560 39.2-1251610 35.723 95















2-Hexanone ug/kg3201390 38.6-1461610 ND270 86



Acetone ug/kg6401320 20.1-1821610 ND430 82

Benzene ug/kg641560 63.6-1081610 ND30 97





Bromomethane ug/kg3201510 10-93.51610 N1aND11 94





Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene ug/kg641610 60.8-1161610 ND20 100



Styrene ug/kg641710 64.5-1151610 ND16 106


Tetrachloroethene ug/kg641550 56.7-1301610 ND12 96

Toluene ug/kg641500 62.6-1131610 ND19 93










Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







1,1-Dichloroethene 25ug/kg972330 39.2-1232430 N1aND45 96 39

1,1-Dichloropropene 25ug/kg972260 60.6-1112430 N1aND38 93 43

1,2,3-Trichlorobenzene 25ug/kg1902380 39.2-1252430 N1a35.735 96 42

1,2,3-Trichloropropane 25ug/kg1902200 59.4-1102430 N1aND38 91 38

1,2,4-Trichlorobenzene 25ug/kg972410 43.5-1182430 N1aND38 99 38


1,2-Dibromoethane (EDB) 25ug/kg972390 64.2-1082430 N1aND30 99 40





1,3-Dichlorobenzene 25ug/kg972500 62-1112430 N1aND24 103 42




2-Butanone (MEK) 25ug/kg4902210 34.5-1542430 N1aND390 91 31


2-Hexanone 25ug/kg4902030 38.6-1462430 N1aND410 83 37


4-Methyl-2-pentanone (MIBK) 25ug/kg4902010 56.5-1112430 N1aND330 83 40

Acetone 25ug/kg9701840 20.1-1822430 N1aND640 76 33

Benzene 25ug/kg972410 63.6-1082430 N1aND45 99 43

Bromobenzene 25ug/kg972540 64.2-1092430 N1aND35 105 42

Bromochloromethane 25ug/kg972460 60-1232430 N1aND47 101 40

Bromodichloromethane 25ug/kg972440 61.8-1112430 N1aND35 100 42

Bromoform 25ug/kg972290 57.5-1092430 N1aND39 94 39

Bromomethane 25ug/kg4902270 10-93.52430 N1aND16 94 40

Carbon tetrachloride 25ug/kg972300 44.5-1232430 N1aND39 95 46

Chlorobenzene 25ug/kg972460 66.9-1072430 N1aND22 101 44


Chloroform 25ug/kg972440 63.2-1122430 N1aND47 101 38

Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chloromethane 25ug/kg4901980 15.3-1232430 N1aND50 82 40

cis-1,2-Dichloroethene 25ug/kg972320 64.1-1082430 N1aND41 96 37

cis-1,3-Dichloropropene 25ug/kg972530 63.3-1102430 N1aND30 104 43

Dibromochloromethane 25ug/kg972430 63-1092430 N1aND22 100 39

Dichlorodifluoromethane 25ug/kg971680 10-1182430 N1aND37 69 42

Ethylbenzene 25ug/kg972540 62.4-1132430 N1aND25 105 44

m,p-Xylenes 25ug/kg1902460 57.7-1182430 N1aND66 102 41


Methyl-tert-butyl Ether (MTBE) 25ug/kg972440 54.9-1182430 N1aND34 101 37

n-Butylbenzene 25ug/kg972530 47.8-1322430 N1aND34 104 41

n-Propylbenzene 25ug/kg972660 55.8-1172430 N1aND33 110 43

o-Xylene 25ug/kg972450 60.8-1162430 N1aND31 101 42

p-Isopropyltoluene 25ug/kg972520 59-1162430 N1aND39 104 42

sec-Butylbenzene 25ug/kg972480 60.3-1172430 N1aND34 102 39

Styrene 25ug/kg972470 64.5-1152430 N1aND24 102 37

tert-Butylbenzene 25ug/kg972440 60.3-1142430 N1aND40 100 41

Tetrachloroethene 25ug/kg972500 56.7-1302430 N1aND19 103 47

Toluene 25ug/kg972390 62.6-1132430 N1aND29 99 46

trans-1,2-Dichloroethene 25ug/kg972430 58.4-1122430 N1aND35 100 41

trans-1,3-Dichloropropene 25ug/kg972520 61.4-1092430 N1aND29 104 41

Trichloroethene 25ug/kg972470 64.9-1102430 N1aND41 102 42

Trichlorofluoromethane 25ug/kg972350 31.8-1262430 N1aND61 97 44


Vinyl chloride 25ug/kg971600 26.1-1302430 N1aND48 66 43




Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013








Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1082

14682.013



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PSL1082

Tina Paulauskas



·- ··--·-·-------------·-----~~------- ~-- -------


~enix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ 1 T 1870 W P . R d S "t 59 T AZ 85705 (520) 807 3801 FAX (520) 807 3803 THE LEADER IN ENVIRONMENTAL TESTING ucson- . nnce oa , UJe , ucson, - -

Page / [ 1 Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

of TAL-0013·550 (12/08)

~~ezt~x · Project/ PO Number: Analysis Required

ell'> -t_. 'hA ~ v~ 1:1:. '3"ib l'tbCfiL. 0:::.1:3> $c..>rt-1~ 4'-. ~S'~S~ Project Manager:K_~,~ CAA•b Phone Number:

P:LIDJL '1~ --;)'t~-l Z...'-t i 0 Sampler: R~ fF-VP-IfLY> Fax Number: G...'{._5

't'B0- ~l.{'l:S,- I _ ~ ~

Sample Container #of Sampling Sampling N Sample Description Matrix Type Cont. Date Time Preservatives «) Special_lnstructions

APJb-f:.PJ!;- I 'L I 8D1 6-)A-flt{ t/Otw/ 3 ry,-o~ t3oY ~ ~ ( Dl -:s II"\ ,_(j..o(b~

A~-Jo-t2JiYJ'1 Sot'- 'tD-*/ z.. •7/,tt'ott lS'~ MJt:oU.\. ~- -z ~z AfJh- Jo ... f2.J'6c:f( ; l ( { t 2.. ''ft~Jo=r llo5 J.,l -V "(_ D5 1Af3l:-.-'f0 -17--J &DCf e-l u 3 '2flt>/o"'( lHoe> t I ~ ~ r /l,Ob-77>--1 '2-lcr c~ lV~ 1\ I ''l.f IC:, I tYi o16c::J j-\-G\ / .-c. :') A6~-'=-0-l1..\qO_~ ~1L lfcM\ 3 '2.f,~ICFJ 0~ M£-OLI-\ / u ~ A~-70--(l.l l D'1 I\ "l 3 ZU"ilor; loS.:::. l( 1/ -o 17 Af!h-ID- L< ... £)OC, bqp t\ ll 3 ifaec( D'\ LOS.:> (\ 1/ ---7_) ~

R~~~ J2/t~f~'Time:ll ~s ReceiveL: Date/Time: Turnaround Time: (Check)

~-~ ~~ tt/tt;fc,'l uof same day- 72 hours

~~~~~/~;/Time: rJ '-to Rec~ Date/Time: 24 hours 5 days

48 hours normal

Relinquished By: 'oate/Time:

~ ~ceivedi~- l-2a7?47(f1 ll'-IC

Sampl~grity: (Check) /fJ. /De intact _.. on ice'/_"



454-9303

LABORATORY REPORT




Attention: Kirk Craig Sampled:

Received:

Issued:

12/18/09-12/19/09

12/21/09

01/07/10 12:52







Project: 14682.009


CASE NARRATIVE


PSL1085-01 AB6-80-121909 Soil

PSL1085-02 AB6-90-121909 Water

PSL1085-03 AB6-90-121909 DUP Water



PSL1085-06 AB6-105-121909 Water

Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas

<Page 1 of 37>


454-9303




Attention: Kirk Craig

Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009


Soil samples for Volatile analysis were received as Methanol Kits.





N1a-Batch 10A0010 - The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

N1a-Batch P9L2145 - The Laboratory Control Sample / Laboratory Control Sample Duplicate and Matrix

Spike / Matrix Spike Duplicate recovered high and outside of the project specific acceptance limits for

Chloroethane. The LCSD was also high and outside of the project specific acceptance limits for

n-propylbenzene. The Laboratory Control Sample / Laboratory Control Sample Duplicate recovered low

and outside of the project specific acceptance limits for Vinyl chloride. All recoveries were within the

laboratory's historical limits. The associated samples is non-detect for Chloroethane and n-propylbenzene

and therefore not impacted by the high recoveries. The Matrix Spike / Matrix Spike Duplicate recovered

within the project limits for Vinyl chloride. The associated sample is a methanol extracted soil and

therefore could not be re-extracted, but was re-analyzed for Vinyl chloride and the LCS/LCSD recovered

low and outside of the project specific acceptance limits in the re-analysis.



Reviewed By:

Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit






SW8260BAcetone 10A0010 20 ND E812/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15







SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19


SW8260BToluene 10A0010 1.0 ND E812/31/09 12/31/0910.35


























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1085-03 (AB6-90-121909 DUP - Water) Sampled: 12/19/09Reporting Units: ug/l





SW8260BAcetone 10A0010 20 ND E812/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15







SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19


SW8260BToluene 10A0010 1.0 ND E812/31/09 12/31/0910.35


























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSL1085-03 (AB6-90-121909 DUP - Water) - cont. Sampled: 12/19/09Reporting Units: ug/l
















SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit






Acetone SW8260B 10A0010 7.520 E412/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15







SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19


SW8260BToluene 10A0010 1.0 ND E812/31/09 12/31/0910.35


























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit






SW8260BAcetone 10A0010 20 ND E812/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15







SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19


SW8260BToluene 10A0010 1.0 ND E812/31/09 12/31/0910.35


























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit





2-Butanone (MEK) SW8260B 10A0010 3.85.0 E412/31/09 12/31/0911.8

Acetone SW8260B 10A0010 1520 E412/31/09 12/31/0913.8

SW8260BBenzene 10A0010 1.0 ND E812/31/09 12/31/0910.15







SW8260Bo-Xylene 10A0010 1.0 ND E812/31/09 12/31/0910.19


SW8260BToluene 10A0010 1.0 ND E812/31/09 12/31/0910.35


























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0010 1.0 ND E812/31/09 12/31/0910.15







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit










































Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit
























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)


2 12/18/2009 12:00 12/21/2009 08:35 12/18/2009 12:00 12/24/2009 19:52SW8260B

Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/31/2009 (10A0010-BS1)




2-Butanone (MEK) ug/l5.026.3 45.6-14125.01.8 105

Acetone ug/l2030.7 22.4-15325.03.8 123

Benzene ug/l1.024.4 80.7-12025.00.15 98


Chloroform ug/l1.025.9 80.7-11925.00.16 103



m,p-Xylenes ug/l2.023.6 85-11525.00.35 94


o-Xylene ug/l1.024.0 85-11525.00.19 96


Toluene ug/l1.023.5 85-11525.00.35 94





















Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 12/31/2009 (10A0010-BS1)


2-Hexanone ug/l5.025.3 58.5-13525.00.31 101






Bromoform ug/l1.024.0 71.9-13125.00.19 96













Styrene ug/l1.025.1 85-11525.00.15 100







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.025.4 45.6-14125.01.8 101 3

Acetone 25ug/l2029.6 22.4-15325.03.8 118 3

Benzene 25ug/l1.023.5 80.7-12025.00.15 94 4


Chloroform 25ug/l1.024.1 80.7-11925.00.16 96 7



m,p-Xylenes 25ug/l2.023.6 85-11525.00.35 94 0


o-Xylene 25ug/l1.023.1 85-11525.00.19 93 4


Toluene 25ug/l1.021.3 85-11525.00.35 85 10





















Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.029.2 58.5-13525.00.31 117 14






Bromoform 25ug/l1.024.6 71.9-13125.00.19 98 2













Styrene 25ug/l1.024.2 85-11525.00.15 97 4







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) ug/l5.029.1 41.6-13025.0 3.821.8 101

Acetone ug/l2048.7 19.7-13125.0 N1a15.23.8 134

Benzene ug/l1.025.0 78.4-12725.0 ND0.15 100





m,p-Xylenes ug/l2.024.6 70.8-13225.0 ND0.35 99


o-Xylene ug/l1.024.0 77.5-12225.0 ND0.19 96


Toluene ug/l1.022.7 83-11825.0 ND0.35 91





















Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.028.0 57.9-11825.0 ND0.31 112






Bromoform ug/l1.022.5 63.7-12925.0 ND0.19 90













Styrene ug/l1.024.6 55-13625.0 ND0.15 98







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.023.9 41.6-13025.0 3.821.8 80 19

Acetone 25ug/l2037.7 19.7-13125.0 15.23.8 90 25

Benzene 25ug/l1.021.8 78.4-12725.0 ND0.15 87 13





m,p-Xylenes 25ug/l2.022.0 70.8-13225.0 ND0.35 88 11


o-Xylene 25ug/l1.022.7 77.5-12225.0 ND0.19 91 5


Toluene 25ug/l1.021.2 83-11825.0 ND0.35 85 7





















Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.022.1 57.9-11825.0 ND0.31 88 24






Bromoform 25ug/l1.021.0 63.7-12925.0 ND0.19 84 7













Styrene 25ug/l1.023.0 55-13625.0 ND0.15 92 6







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









1,2,3-Trichlorobenzene ug/kg10020.0 E418










1,3-Dichloropropane ug/kg5040.5 E414



















Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone ug/kg250979 50.6-1331250210 78



Acetone ug/kg5001070 23.5-1821250330 85

Benzene ug/kg501170 76-107125023 93




Bromoform ug/kg50860 67.3-110125020 69





Chloroform ug/kg501120 69.8-114125024 89

Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes ug/kg1001160 83.5-107125034 93





o-Xylene ug/kg501140 82.8-108125016 91



Styrene ug/kg501110 82.1-111125012 89



Toluene ug/kg501110 81.3-106125015 89






Vinyl chloride ug/kg50262 46.4-1311250 N1a25 21




Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone 25ug/kg2501150 50.6-1331250210 92 16



Acetone 25ug/kg5001130 23.5-1821250330 91 6

Benzene 25ug/kg501250 76-107125023 100 7




Bromoform 25ug/kg50989 67.3-110125020 79 14





Chloroform 25ug/kg501150 69.8-114125024 92 3

Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes 25ug/kg1001220 83.5-107125034 97 5




n-Propylbenzene 25ug/kg501350 77.7-1071250 N1a17 108 8

o-Xylene 25ug/kg501180 82.8-108125016 95 4



Styrene 25ug/kg501180 82.1-111125012 94 6



Toluene 25ug/kg501210 81.3-106125015 97 8






Vinyl chloride 25ug/kg50266 46.4-1311250 N1a25 21 2




Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






















2-Butanone (MEK) ug/kg2501190 34.5-1541350 246200 70


2-Hexanone ug/kg2501070 38.6-1461350 ND210 79



Acetone ug/kg500762 20.1-1821350 ND330 57

Benzene ug/kg501200 63.6-1081350 ND23 89










Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene ug/kg501150 60.8-1161350 ND16 86



Styrene ug/kg501260 64.5-1151350 ND12 93



Toluene ug/kg501140 62.6-1131350 ND15 84










Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






















2-Butanone (MEK) 25ug/kg2501050 34.5-1541180 246200 68 13


2-Hexanone 25ug/kg250986 38.6-1461180 ND210 84 8



Acetone 25ug/kg500653 20.1-1821180 ND330 56 15

Benzene 25ug/kg501080 63.6-1081180 ND23 92 10










Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene 25ug/kg501100 60.8-1161180 ND16 94 5



Styrene 25ug/kg501130 64.5-1151180 ND12 96 11



Toluene 25ug/kg501050 62.6-1131180 ND15 89 8










Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009







Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




454-9303





Sampled:

Received:

12/18/09-12/19/09


Project ID:

PSL1085

14682.009



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PSL1085

Tina Paulauskas




TAL-0013-550 (12/08)

. . . CHAIN OF CUSTODY FORM . PS llDC6S -~oenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303

[ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621 {

Page

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ft:/:J .... 3Clt 't) -t, '2.." "( 0 s~~ Fax Number: ~ tl- 't:oC> ... 3 ~ ~ - £ LCf. $

Sample Container #of Sampling Sampling 00

of 1

Sample Description Matrix Type Cont. Date lime Preservatives Special Instructions

IA/bb- so-12.\<tcR so~ "JOM.f b '1.(,'~1 rFt I ZOO MW#4- L -- 0( M$}!USI>

Aeb-qo ~ rz.....J'l99 w~ 'i014/ 3 IZJ"ij_vt 11..~5 ~( / - OJ Mb- ~-rz..£~ o~ J;:;,JP l \. ,t 3 '1.../ lc;,Jl)C, I'Z.\,1S t I / - (k~ A0~-EM3-l?.\ <to'\ u Lt 3 '"tf •-.f.:>; J 32.1 l ( / - 6'-1 J.I.Vmtf'G)IoJ<4/.

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~et~ L 2 .. {.-~~r~~ime: Received By: Date/Time: Turnaround Time: (Check)

.""\ -_'- OB:>) "'"'

same day 72 hours Relinquished By:

...., Date/Time: ~In By:

Date/Time: 24 hours 5 days

48 hours normal .k' '

Relinquished By: Date/Time: l~~LabBy: J Da~1'Time: Sample Integrity: (Check)

iL. Ll o'l oB3S intact )0. on ice X' 5,.8 '-" "'t'


.,.~


454-9303

LABORATORY REPORT





Received:

Issued:

01/04/10

01/04/10

01/19/10 16:22




report shall not be reproduced, except in full, without written permission from TestAmerica.


Project: 14682.013


CASE NARRATIVE


PTA0054-01 AB2-21-01410 Soil

PTA0054-02 AB2-30-01410 Soil

PTA0054-03 AB2-40-01410 Soil

PTA0054-04 AB2-40-01410 Dup Soil

PTA0054-05 AB2-50-01410 Soil

PTA0054-06 AB2-TB-01410 Water

PTA0054-07 AB2-TB-01410 Soil

PTA0054-08 AB2-60-01410 Soil

Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon

<Page 1 of 41>


454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013






R1 SW8260B:The RPD exceeded the acceptance limit for Vinyl Acetate.

N1a SW8260B:Batch 10A0020-The MS and/or MSD were above the acceptance limits for

Bromomethane,1,1-Dichloroethane,1,2-Dichlorobenzene and Methylene Chloride. See Blank Spike (LCS).

N1a SW8260B:Batch 10A0366- The Laboratory Control Sample recovered high and outside of the project

specific acceptance limits for cis-1,3-Dichloropropane and Methylene chloride. The Laboratory Control

Sample also recovered high and outside of the project specific acceptance limits for Methylene chloride.

There were several analytes that recovered high and outside of the project specific acceptance limits in the

Matrix Spike / Matrix Spike Duplicate. All recoveries were within the laboratory's historical limits. All

associated samples are non-detect for the affected compounds and therefore are not impacted.

N1a SW8260B:Batch 10A0020-The Laboratory Control Sample Duplicate recovered low (40%) and

outside of the 46.4-131% project specific acceptance limits for Vinyl chloride. The recovery was within the

laboratory's historical limits. The Laboratory Control Sample and Matrix Spike / Matrix Spike Duplicate

recovered within the project specific acceptance limits.

N1a SW8260B: Batch 10A0020:The following

compounds:n-Propylbenzene,1,1,2,2-Tetrachloroethane,Vinyl Acetate,1,2-Dichloropropane, and

Chloroethane were above 8260(PGA) acceptance limits, but were within laboratory acceptance limits in the

LCS/LCSD and/or MS/MSD.



Reviewed By:

Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-06 (AB2-TB-01410 - Water) Sampled: 01/04/10Reporting Units: ug/l





SW8260BAcetone 10A0366 20 ND E801/14/10 01/14/1013.8

SW8260BBenzene 10A0366 1.0 ND E801/14/10 01/14/1010.15







SW8260Bo-Xylene 10A0366 1.0 ND E801/14/10 01/14/1010.19


SW8260BToluene 10A0366 1.0 ND E801/14/10 01/14/1010.35


























Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-06 (AB2-TB-01410 - Water) - cont. Sampled: 01/04/10Reporting Units: ug/l
















SW8260BStyrene 10A0366 1.0 ND E801/14/10 01/14/1010.15







Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-01 (AB2-21-01410 - Soil) Sampled: 01/04/10Reporting Units: ug/kg

SW8260B1,1,1-Trichloroethane 10A0020 50 ND E801/04/10 01/05/10119

SW8260B1,1,2,2-Tetrachloroethane 10A0020 50 ND E801/04/10 01/05/10118


SW8260B1,1-Dichloroethane 10A0020 50 ND E801/04/10 01/05/10115

SW8260B1,1-Dichloroethene 10A0020 50 ND E801/04/10 01/05/10123

SW8260B1,1-Dichloropropene 10A0020 50 ND E801/04/10 01/05/10119

SW8260B1,2,3-Trichlorobenzene 10A0020 100 ND E801/04/10 01/05/10118

SW8260B1,2,3-Trichloropropane 10A0020 100 ND E801/04/10 01/05/10120


SW8260B1,2,4-Trimethylbenzene 10A0020 50 ND E801/04/10 01/05/10127

SW8260B1,2-Dibromoethane (EDB) 10A0020 50 ND E801/04/10 01/05/10116

SW8260B1,2-Dichlorobenzene 10A0020 50 ND E801/04/10 01/05/10121


SW8260B1,2-Dichloropropane 10A0020 50 ND E801/04/10 01/05/10119






SW8260B2-Butanone (MEK) 10A0020 250 ND E801/04/10 01/05/101200

SW8260B2-Chlorotoluene 10A0020 50 ND E801/04/10 01/05/10115

SW8260B2-Hexanone 10A0020 250 ND E801/04/10 01/05/101210


SW8260B4-Methyl-2-pentanone (MIBK) 10A0020 250 ND E801/04/10 01/05/101170

SW8260BAcetone 10A0020 500 ND E801/04/10 01/05/101330

SW8260BBenzene 10A0020 50 ND E801/04/10 01/05/10123

SW8260BBromobenzene 10A0020 50 ND E801/04/10 01/05/10118

SW8260BBromochloromethane 10A0020 50 ND E801/04/10 01/05/10124

SW8260BBromodichloromethane 10A0020 50 ND E801/04/10 01/05/10118

SW8260BBromoform 10A0020 50 ND E801/04/10 01/05/10120

SW8260BBromomethane 10A0020 250 ND E801/04/10 01/05/1018.3

SW8260BCarbon tetrachloride 10A0020 50 ND E801/04/10 01/05/10120

SW8260BChlorobenzene 10A0020 50 ND E801/04/10 01/05/10111

SW8260BChloroethane 10A0020 50 ND E801/04/10 01/05/10131

SW8260BChloroform 10A0020 50 ND E801/04/10 01/05/10124

SW8260BChloromethane 10A0020 250 ND E801/04/10 01/05/10126

SW8260Bcis-1,2-Dichloroethene 10A0020 50 ND E801/04/10 01/05/10121

SW8260Bcis-1,3-Dichloropropene 10A0020 50 ND E801/04/10 01/05/10115

SW8260BDibromochloromethane 10A0020 50 ND E801/04/10 01/05/10111

SW8260BDichlorodifluoromethane 10A0020 50 ND E801/04/10 01/05/10119

Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-01 (AB2-21-01410 - Soil) - cont. Sampled: 01/04/10Reporting Units: ug/kg

SW8260BEthylbenzene 10A0020 50 ND E801/04/10 01/05/10113

SW8260Bm,p-Xylenes 10A0020 100 ND E801/04/10 01/05/10134

SW8260BMethylene Chloride 10A0020 100 ND E801/04/10 01/05/10132

SW8260BMethyl-tert-butyl Ether (MTBE) 10A0020 50 ND E801/04/10 01/05/10117

SW8260Bn-Butylbenzene 10A0020 50 ND E801/04/10 01/05/10118

SW8260Bn-Propylbenzene 10A0020 50 ND E801/04/10 01/05/10117

SW8260Bo-Xylene 10A0020 50 ND E801/04/10 01/05/10116

SW8260Bp-Isopropyltoluene 10A0020 50 ND E801/04/10 01/05/10120

SW8260Bsec-Butylbenzene 10A0020 50 ND E801/04/10 01/05/10118

SW8260BStyrene 10A0020 50 ND E801/04/10 01/05/10112

SW8260Btert-Butylbenzene 10A0020 50 ND E801/04/10 01/05/10120

SW8260BTetrachloroethene 10A0020 50 ND E801/04/10 01/05/1019.6

SW8260BToluene 10A0020 50 ND E801/04/10 01/05/10115

SW8260Btrans-1,2-Dichloroethene 10A0020 50 ND E801/04/10 01/05/10118

SW8260Btrans-1,3-Dichloropropene 10A0020 50 ND E801/04/10 01/05/10115

SW8260BTrichloroethene 10A0020 50 ND E801/04/10 01/05/10121

SW8260BTrichlorofluoromethane 10A0020 50 ND E801/04/10 01/05/10132

SW8260BVinyl Acetate 10A0020 50 ND V1, E801/04/10 01/05/10126

SW8260BVinyl chloride 10A0020 50 ND E8, N1a01/04/10 01/05/10125




Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0020 500 ND E801/04/10 01/06/101330

SW8260BBenzene 10A0020 50 ND E801/04/10 01/06/10123















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0020 50 ND E801/04/10 01/06/10116



SW8260BStyrene 10A0020 50 ND E801/04/10 01/06/10112



SW8260BToluene 10A0020 50 ND E801/04/10 01/06/10115





SW8260BVinyl Acetate 10A0020 50 ND V1, E801/04/10 01/06/10126





Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0020 500 ND E801/04/10 01/06/101330

SW8260BBenzene 10A0020 50 ND E801/04/10 01/06/10123















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0020 50 ND E801/04/10 01/06/10116



SW8260BStyrene 10A0020 50 ND E801/04/10 01/06/10112



SW8260BToluene 10A0020 50 ND E801/04/10 01/06/10115





SW8260BVinyl Acetate 10A0020 50 ND E801/04/10 01/06/10126





Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-04 (AB2-40-01410 Dup - Soil) Sampled: 01/04/10Reporting Units: ug/kg

























SW8260BAcetone 10A0020 500 ND E801/04/10 01/06/101330

SW8260BBenzene 10A0020 50 ND E801/04/10 01/06/10123















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-04 (AB2-40-01410 Dup - Soil) - cont. Sampled: 01/04/10Reporting Units: ug/kg







SW8260Bo-Xylene 10A0020 50 ND E801/04/10 01/06/10116



SW8260BStyrene 10A0020 50 ND E801/04/10 01/06/10112



SW8260BToluene 10A0020 50 ND E801/04/10 01/06/10115










Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0020 500 ND E801/04/10 01/06/101330

SW8260BBenzene 10A0020 50 ND E801/04/10 01/06/10123















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0020 50 ND E801/04/10 01/06/10116



SW8260BStyrene 10A0020 50 ND E801/04/10 01/06/10112



SW8260BToluene 10A0020 50 ND E801/04/10 01/06/10115










Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-07 (AB2-TB-01410 - Soil) Sampled: 01/04/10Reporting Units: ug/kg

























SW8260BAcetone 10A0020 500 ND E801/04/10 01/06/101330

SW8260BBenzene 10A0020 50 ND E801/04/10 01/06/10123















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0054-07 (AB2-TB-01410 - Soil) - cont. Sampled: 01/04/10Reporting Units: ug/kg







SW8260Bo-Xylene 10A0020 50 ND E801/04/10 01/06/10116



SW8260BStyrene 10A0020 50 ND E801/04/10 01/06/10112



SW8260BToluene 10A0020 50 ND E801/04/10 01/06/10115










Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0020 500 ND E801/04/10 01/06/101330

SW8260BBenzene 10A0020 50 ND E801/04/10 01/06/10123















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0020 50 ND E801/04/10 01/06/10116



SW8260BStyrene 10A0020 50 ND E801/04/10 01/06/10112



SW8260BToluene 10A0020 50 ND E801/04/10 01/06/10115










Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: AB2-21-01410 (PTA0054-01) - Soil

2 01/04/2010 11:55 01/04/2010 17:01 01/04/2010 11:55 01/05/2010 19:37SW8260B


2 01/04/2010 12:45 01/04/2010 17:01 01/04/2010 12:45 01/06/2010 11:51SW8260B


2 01/04/2010 14:05 01/04/2010 17:01 01/04/2010 14:05 01/06/2010 13:01SW8260B

Sample ID: AB2-40-01410 Dup (PTA0054-04) - Soil

2 01/04/2010 14:05 01/04/2010 17:01 01/04/2010 14:05 01/06/2010 13:33SW8260B


2 01/04/2010 15:07 01/04/2010 17:01 01/04/2010 15:07 01/06/2010 14:06SW8260B

Sample ID: AB2-TB-01410 (PTA0054-07) - Soil

2 01/04/2010 15:15 01/04/2010 17:01 01/04/2010 15:15 01/06/2010 14:37SW8260B


2 01/04/2010 16:07 01/04/2010 17:01 01/04/2010 16:07 01/06/2010 15:09SW8260B

Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



































1,3-Dichloropropane ug/l1.00.610 E40.18



Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.01.83 E40.31


























Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/14/2010 (10A0366-BS1)




2-Butanone (MEK) ug/l5.025.5 45.6-14125.01.8 102

Acetone ug/l2024.6 22.4-15325.03.8 98

Benzene ug/l1.025.5 80.7-12025.00.15 102


Chloroform ug/l1.027.9 80.7-11925.00.16 112



m,p-Xylenes ug/l2.024.5 85-11525.00.35 98

Methylene Chloride ug/l2.031.2 79.7-11725.0 N1a0.50 125

o-Xylene ug/l1.024.6 85-11525.00.19 98


Toluene ug/l1.024.5 85-11525.00.35 98





















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/14/2010 (10A0366-BS1)


2-Hexanone ug/l5.021.0 58.5-13525.00.31 84






Bromoform ug/l1.022.3 71.9-13125.00.19 89





cis-1,3-Dichloropropene ug/l1.029.0 85-11525.0 N1a0.17 116








Styrene ug/l1.026.1 85-11525.00.15 105







Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.025.8 45.6-14125.01.8 103 1

Acetone 25ug/l2024.1 22.4-15325.03.8 96 2

Benzene 25ug/l1.025.0 80.7-12025.00.15 100 2


Chloroform 25ug/l1.027.7 80.7-11925.00.16 111 1



m,p-Xylenes 25ug/l2.024.2 85-11525.00.35 97 2

Methylene Chloride 25ug/l2.030.5 79.7-11725.0 N1a0.50 122 2

o-Xylene 25ug/l1.024.5 85-11525.00.19 98 0


Toluene 25ug/l1.023.5 85-11525.00.35 94 4





















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.021.5 58.5-13525.00.31 86 3






Bromoform 25ug/l1.023.2 71.9-13125.00.19 93 4













Styrene 25ug/l1.025.5 85-11525.00.15 102 2







Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Analyzed: 01/14/2010 (10A0366-MS1) Source: PTA0598-01


1,1-Dichloroethene ug/l1.025.8 82.1-12625.0 0.4300.23 101

1,2-Dichloropropane ug/l1.031.2 81.1-11625.0 N1aND0.15 125

2-Butanone (MEK) ug/l5.043.7 41.6-13025.0 M1ND1.8 175

Acetone ug/l2046.4 19.7-13125.0 M1ND3.8 186

Benzene ug/l1.026.0 78.4-12725.0 ND0.15 104

Carbon tetrachloride ug/l1.023.4 80.7-12825.0 0.3100.19 92

Chloroform ug/l1.031.2 77.6-12225.0 0.7000.16 122



m,p-Xylenes ug/l2.023.8 70.8-13225.0 ND0.35 95

Methylene Chloride ug/l2.035.5 74.6-11925.0 N1aND0.50 142

o-Xylene ug/l1.024.5 77.5-12225.0 ND0.19 98


Toluene ug/l1.024.5 83-11825.0 ND0.35 98


Trichloroethene ug/l1.0187 77.3-12025.0 1640.19 89




1,1,2-Trichloroethane ug/l1.034.0 77.5-11825.0 N1aND0.19 136



1,2,3-Trichlorobenzene ug/l2.030.7 32.3-11725.0 N1aND0.27 123




1,2-Dibromoethane (EDB) ug/l1.031.4 76.5-12025.0 M1ND0.14 126


1,2-Dichloroethane ug/l1.038.3 69.4-12925.0 N1aND0.20 153






Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.035.6 57.9-11825.0 N1aND0.31 142


4-Methyl-2-pentanone (MIBK) ug/l5.041.4 65.6-12725.0 M1ND0.43 166


Bromochloromethane ug/l1.034.6 75.5-12525.0 M1ND0.20 138

Bromodichloromethane ug/l1.030.3 78.1-11825.0 N1aND0.15 121

Bromoform ug/l1.027.0 63.7-12925.0 ND0.19 108





cis-1,3-Dichloropropene ug/l1.034.0 78.6-11825.0 N1aND0.17 136

Dibromochloromethane ug/l1.032.3 75.2-12325.0 N1aND0.15 129


Methyl-tert-butyl Ether (MTBE) ug/l1.041.2 68.8-12625.0 M1ND0.18 165





Styrene ug/l1.024.6 55-13625.0 ND0.15 98


trans-1,3-Dichloropropene ug/l1.036.7 72.8-12325.0 N1aND0.097 147

Vinyl Acetate ug/l1.037.4 50-13925.0 N1aND0.21 150




Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Dup Analyzed: 01/14/2010 (10A0366-MSD1) Source: PTA0598-01

1,1,2,2-Tetrachloroethane 25ug/l1.032.5 70.4-12425.0 N1aND0.12 130 6

1,1-Dichloroethene 25ug/l1.028.9 82.1-12625.0 0.4300.23 114 11

1,2-Dichloropropane 25ug/l1.032.9 81.1-11625.0 N1aND0.15 132 5

2-Butanone (MEK) 25ug/l5.046.1 41.6-13025.0 M1ND1.8 184 5

Acetone 25ug/l2050.6 19.7-13125.0 M1ND3.8 202 9

Benzene 25ug/l1.027.5 78.4-12725.0 ND0.15 110 5

Carbon tetrachloride 25ug/l1.026.1 80.7-12825.0 0.3100.19 103 11

Chloroform 25ug/l1.032.1 77.6-12225.0 N1a0.7000.16 126 3



m,p-Xylenes 25ug/l2.025.9 70.8-13225.0 ND0.35 104 9

Methylene Chloride 25ug/l2.036.7 74.6-11925.0 N1aND0.50 147 3

o-Xylene 25ug/l1.025.9 77.5-12225.0 ND0.19 104 6


Toluene 25ug/l1.026.1 83-11825.0 ND0.35 104 6


Trichloroethene 25ug/l1.0190 77.3-12025.0 1640.19 100 2




1,1,2-Trichloroethane 25ug/l1.033.9 77.5-11825.0 N1aND0.19 136 0



1,2,3-Trichlorobenzene 25ug/l2.031.6 32.3-11725.0 N1aND0.27 126 3

1,2,3-Trichloropropane 25ug/l2.034.0 69.8-12425.0 M1ND0.31 136 11



1,2-Dibromoethane (EDB) 25ug/l1.033.1 76.5-12025.0 M1ND0.14 133 5





1,3-Dichloropropane 25ug/l1.031.1 77.1-11925.0 M1ND0.18 125 5



Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.036.2 57.9-11825.0 N1aND0.31 145 2


4-Methyl-2-pentanone (MIBK) 25ug/l5.042.8 65.6-12725.0 M1ND0.43 171 3


Bromochloromethane 25ug/l1.034.4 75.5-12525.0 M1ND0.20 137 1

Bromodichloromethane 25ug/l1.030.9 78.1-11825.0 N1aND0.15 124 2

Bromoform 25ug/l1.028.7 63.7-12925.0 ND0.19 115 6





cis-1,3-Dichloropropene 25ug/l1.034.7 78.6-11825.0 N1aND0.17 139 2

Dibromochloromethane 25ug/l1.033.6 75.2-12325.0 N1aND0.15 134 4


Methyl-tert-butyl Ether (MTBE) 25ug/l1.040.1 68.8-12625.0 M1ND0.18 161 3





Styrene 25ug/l1.026.1 55-13625.0 ND0.15 104 6


trans-1,3-Dichloropropene 25ug/l1.036.5 72.8-12325.0 N1aND0.097 146 0

Vinyl Acetate 25ug/l1.037.2 50-13925.0 N1aND0.21 149 1




Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



















1,3-Dichloropropane ug/kg5035.0 E414



















Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/05/2010-01/07/2010 (10A0020-BS1)


1,1,2,2-Tetrachloroethane ug/kg501350 69.7-1021250 N1a18 108












1,2-Dichloropropane ug/kg501380 78.8-1051250 N1a19 110








2-Hexanone ug/kg2501350 50.6-1331250210 108



Acetone ug/kg5001120 23.5-1821250330 90

Benzene ug/kg501310 76-107125023 105




Bromoform ug/kg501010 67.3-110125020 81





Chloroform ug/kg501200 69.8-114125024 96

Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/05/2010-01/07/2010 (10A0020-BS1)







m,p-Xylenes ug/kg1001250 83.5-107125034 100




n-Propylbenzene ug/kg501350 77.7-1071250 N1a17 108

o-Xylene ug/kg501270 82.8-108125016 101



Styrene ug/kg501290 82.1-111125012 103



Toluene ug/kg501250 81.3-106125015 100





Vinyl Acetate ug/kg501740 42.2-1241250 N1a26 139





Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Dup Analyzed: 01/05/2010-01/07/2010 (10A0020-BSD1)


1,1,2,2-Tetrachloroethane 25ug/kg501370 69.7-1021250 N1a18 109 2


















2-Butanone (MEK) 25ug/kg2501790 39-1481250 R6200 143 44


2-Hexanone 25ug/kg2501220 50.6-1331250210 97 11



Acetone 25ug/kg5001990 23.5-1821250 R6330 160 56

Benzene 25ug/kg501240 76-107125023 100 5




Bromoform 25ug/kg501020 67.3-110125020 81 1





Chloroform 25ug/kg501210 69.8-114125024 97 1

Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes 25ug/kg1001210 83.5-107125034 97 3





o-Xylene 25ug/kg501210 82.8-108125016 97 5



Styrene 25ug/kg501230 82.1-111125012 98 5



Toluene 25ug/kg501190 81.3-106125015 96 5





Vinyl Acetate 25ug/kg501760 42.2-1241250 N1a26 141 1

Vinyl chloride 25ug/kg50504 46.4-1311250 N1a, R125 40 33




Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Analyzed: 01/05/2010-01/07/2010 (10A0020-MS1) Source: PTA0054-01














1,2-Dichloropropane ug/kg501360 66.7-1061250 N1aND19 109








2-Hexanone ug/kg2501140 38.6-1461250 ND210 91



Acetone ug/kg5001690 20.1-1821250 ND330 135

Benzene ug/kg501250 63.6-1081250 ND23 100





Bromomethane ug/kg2501260 10-93.51250 N1aND8.3 100





Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene ug/kg501190 60.8-1161250 ND16 95



Styrene ug/kg501200 64.5-1151250 ND12 96



Toluene ug/kg501190 62.6-1131250 ND15 95










Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Dup Analyzed: 01/05/2010-01/07/2010 (10A0020-MSD1) Source: PTA0054-01






















2-Hexanone 25ug/kg2501440 38.6-1461250 ND210 115 23



Acetone 25ug/kg5002110 20.1-1821250 ND330 169 22

Benzene 25ug/kg501340 63.6-1081250 ND23 107 7





Bromomethane 25ug/kg2501310 10-93.51250 N1aND8.3 105 4





Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene 25ug/kg501280 60.8-1161250 ND16 102 7



Styrene 25ug/kg501280 64.5-1151250 ND12 103 7



Toluene 25ug/kg501280 62.6-1131250 ND15 103 7










Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013






R1 The RPD/RSD exceeded the method acceptance limit.

R6 LFB/LFBD RPD exceeded the method acceptance limit. Recovery met acceptance criteria.




Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303





Sampled:

Received:

01/04/10


Project ID:

PTA0054

14682.013



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PTA0054

Carlene McCutcheon




454-9303

LABORATORY REPORT





Received:

Issued:

01/05/10

01/06/10

01/20/10 16:43







Project: 14682.013


CASE NARRATIVE


PTA0196-01 AB2-70-01510 Soil


PTA0196-03 AB2-ERB-01510 Water

PTA0196-04 AB2-90-01510 Soil

PTA0196-05 AB2-97-01510 Water

PTA0196-06 AB2-111-01510 Water

PTA0196-07 AB2-111-01510 DUP Water

PTA0196-08 AB2-ERB2-01510 DUP Water

Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon

<Page 1 of 41>


454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013






N1a SW8260B:Batch-10A0082:The Laboratory Control Sample / Laboratory Control Sample Duplicate

and Matrix Spike / Matrix Spike Duplicate recovered high and outside the project specific acceptance limits

for Chloroethane. The recoveries were within the laboratory's historical limits. The associated samples are

non-detect for this compound and therefore are not impacted.

R1 SW8260B:Batch -10A10082:The RPD exceeded the acceptance limit for Acetone and Vinyl Chloride

in the MS/MSD. The LCS/LCSD RPD met acceptance criteria.

N1a SW8260B:Batch-10A0141:The MS and/or MSD were above the acceptance limits for Acetone. See

Blank Spike (LCS).



Reviewed By:

Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit






SW8260BAcetone 10A0141 20 ND E801/07/10 01/07/1013.8

SW8260BBenzene 10A0141 1.0 ND E801/07/10 01/07/1010.15







SW8260Bo-Xylene 10A0141 1.0 ND E801/07/10 01/07/1010.19


SW8260BToluene 10A0141 1.0 ND E801/07/10 01/07/1010.35


























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0141 1.0 ND E801/07/10 01/07/1010.15







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-03 (AB2-ERB-01510 - Water) Sampled: 01/05/10Reporting Units: ug/l





Acetone SW8260B 10A0141 5.320 E401/07/10 01/07/1013.8

SW8260BBenzene 10A0141 1.0 ND E801/07/10 01/07/1010.15







SW8260Bo-Xylene 10A0141 1.0 ND E801/07/10 01/07/1010.19


SW8260BToluene 10A0141 1.0 ND E801/07/10 01/07/1010.35


























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-03 (AB2-ERB-01510 - Water) - cont. Sampled: 01/05/10Reporting Units: ug/l
















SW8260BStyrene 10A0141 1.0 ND E801/07/10 01/07/1010.15







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-05 (AB2-97-01510 - Water) Sampled: 01/05/10Reporting Units: ug/l





SW8260BAcetone 10A0141 20 ND E801/07/10 01/07/1013.8

SW8260BBenzene 10A0141 1.0 ND E801/07/10 01/07/1010.15







SW8260Bo-Xylene 10A0141 1.0 ND E801/07/10 01/07/1010.19


SW8260BToluene 10A0141 1.0 ND E801/07/10 01/07/1010.35


























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-05 (AB2-97-01510 - Water) - cont. Sampled: 01/05/10Reporting Units: ug/l
















SW8260BStyrene 10A0141 1.0 ND E801/07/10 01/07/1010.15







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-06 (AB2-111-01510 - Water) Sampled: 01/05/10Reporting Units: ug/l





SW8260BAcetone 10A0141 20 ND E8, M101/07/10 01/07/1013.8

SW8260BBenzene 10A0141 1.0 ND E801/07/10 01/07/1010.15







SW8260Bo-Xylene 10A0141 1.0 ND E801/07/10 01/07/1010.19


SW8260BToluene 10A0141 1.0 ND E801/07/10 01/07/1010.35


Trichloroethene SW8260B 10A0141 871.0 01/07/10 01/07/1010.19
























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-06 (AB2-111-01510 - Water) - cont. Sampled: 01/05/10Reporting Units: ug/l





SW8260BChlorobenzene 10A0141 1.0 ND E8, M101/07/10 01/07/1010.12











SW8260BStyrene 10A0141 1.0 ND E801/07/10 01/07/1010.15







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-07 (AB2-111-01510 DUP - Water) Sampled: 01/05/10Reporting Units: ug/l





SW8260BAcetone 10A0141 20 ND E801/07/10 01/07/1013.8

SW8260BBenzene 10A0141 1.0 ND E801/07/10 01/07/1010.15







SW8260Bo-Xylene 10A0141 1.0 ND E801/07/10 01/07/1010.19


SW8260BToluene 10A0141 1.0 ND E801/07/10 01/07/1010.35


Trichloroethene SW8260B 10A0141 831.0 01/07/10 01/07/1010.19
























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-07 (AB2-111-01510 DUP - Water) - cont. Sampled: 01/05/10Reporting Units: ug/l
















SW8260BStyrene 10A0141 1.0 ND E801/07/10 01/07/1010.15







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-08 (AB2-ERB2-01510 DUP - Water) Sampled: 01/05/10Reporting Units: ug/l





SW8260BAcetone 10A0141 20 ND E801/07/10 01/07/1013.8

SW8260BBenzene 10A0141 1.0 ND E801/07/10 01/07/1010.15







SW8260Bo-Xylene 10A0141 1.0 ND E801/07/10 01/07/1010.19


SW8260BToluene 10A0141 1.0 ND E801/07/10 01/07/1010.35


Trichloroethene SW8260B 10A0141 0.221.0 E401/07/10 01/07/1010.19
























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0196-08 (AB2-ERB2-01510 DUP - Water) - cont. Sampled: 01/05/10Reporting Units: ug/l
















SW8260BStyrene 10A0141 1.0 ND E801/07/10 01/07/1010.15







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


SW8260B1,1,1-Trichloroethane 10A0082 57 ND E801/05/10 01/11/101.1422

SW8260B1,1,2,2-Tetrachloroethane 10A0082 57 ND E801/05/10 01/11/101.1420


SW8260B1,1-Dichloroethane 10A0082 57 ND E801/05/10 01/11/101.1417

SW8260B1,1-Dichloroethene 10A0082 57 ND E801/05/10 01/11/101.1426

SW8260B1,1-Dichloropropene 10A0082 57 ND E801/05/10 01/11/101.1422

SW8260B1,2,3-Trichlorobenzene 10A0082 110 ND E801/05/10 01/11/101.1421

SW8260B1,2,3-Trichloropropane 10A0082 110 ND E801/05/10 01/11/101.1422


SW8260B1,2,4-Trimethylbenzene 10A0082 57 ND E801/05/10 01/11/101.1431

SW8260B1,2-Dibromoethane (EDB) 10A0082 57 ND E801/05/10 01/11/101.1418

SW8260B1,2-Dichlorobenzene 10A0082 57 ND E801/05/10 01/11/101.1424


SW8260B1,2-Dichloropropane 10A0082 57 ND E801/05/10 01/11/101.1422






SW8260B2-Butanone (MEK) 10A0082 280 ND E801/05/10 01/11/101.14230

SW8260B2-Chlorotoluene 10A0082 57 ND E801/05/10 01/11/101.1417

SW8260B2-Hexanone 10A0082 280 ND E801/05/10 01/11/101.14240


SW8260B4-Methyl-2-pentanone (MIBK) 10A0082 280 ND E801/05/10 01/11/101.14190

SW8260BAcetone 10A0082 570 ND E801/05/10 01/11/101.14380

SW8260BBenzene 10A0082 57 ND E801/05/10 01/11/101.1426

SW8260BBromobenzene 10A0082 57 ND E801/05/10 01/11/101.1421

SW8260BBromochloromethane 10A0082 57 ND E801/05/10 01/11/101.1428

SW8260BBromodichloromethane 10A0082 57 ND E801/05/10 01/11/101.1420

SW8260BBromoform 10A0082 57 ND E801/05/10 01/11/101.1423

SW8260BBromomethane 10A0082 280 ND E801/05/10 01/11/101.149.4

SW8260BCarbon tetrachloride 10A0082 57 ND E801/05/10 01/11/101.1423

SW8260BChlorobenzene 10A0082 57 ND E801/05/10 01/11/101.1413

SW8260BChloroethane 10A0082 57 ND E801/05/10 01/11/101.1435

SW8260BChloroform 10A0082 57 ND E801/05/10 01/11/101.1427

SW8260BChloromethane 10A0082 280 ND E801/05/10 01/11/101.1429

SW8260Bcis-1,2-Dichloroethene 10A0082 57 ND E801/05/10 01/11/101.1424

SW8260Bcis-1,3-Dichloropropene 10A0082 57 ND V1, E801/05/10 01/11/101.1417

SW8260BDibromochloromethane 10A0082 57 ND E801/05/10 01/11/101.1413

SW8260BDichlorodifluoromethane 10A0082 57 ND E801/05/10 01/11/101.1421

Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


SW8260BEthylbenzene 10A0082 57 ND E801/05/10 01/11/101.1415

SW8260Bm,p-Xylenes 10A0082 110 ND E801/05/10 01/11/101.1439

Methylene Chloride SW8260B 10A0082 66110 E401/05/10 01/11/101.1436

SW8260BMethyl-tert-butyl Ether (MTBE) 10A0082 57 ND E801/05/10 01/11/101.1420

SW8260Bn-Butylbenzene 10A0082 57 ND E801/05/10 01/11/101.1420

SW8260Bn-Propylbenzene 10A0082 57 ND E801/05/10 01/11/101.1420

SW8260Bo-Xylene 10A0082 57 ND E801/05/10 01/11/101.1418

SW8260Bp-Isopropyltoluene 10A0082 57 ND E801/05/10 01/11/101.1423

SW8260Bsec-Butylbenzene 10A0082 57 ND E801/05/10 01/11/101.1420

SW8260BStyrene 10A0082 57 ND E801/05/10 01/11/101.1414

SW8260Btert-Butylbenzene 10A0082 57 ND E801/05/10 01/11/101.1423


SW8260BToluene 10A0082 57 ND E801/05/10 01/11/101.1417

SW8260Btrans-1,2-Dichloroethene 10A0082 57 ND E801/05/10 01/11/101.1421

SW8260Btrans-1,3-Dichloropropene 10A0082 57 ND V1, E801/05/10 01/11/101.1417

SW8260BTrichloroethene 10A0082 57 ND E801/05/10 01/11/101.1424

SW8260BTrichlorofluoromethane 10A0082 57 ND E801/05/10 01/11/101.1436

SW8260BVinyl Acetate 10A0082 57 ND E801/05/10 01/11/101.1429

SW8260BVinyl chloride 10A0082 57 ND E801/05/10 01/11/101.1428




Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0082 500 ND E801/05/10 01/11/101.09330

SW8260BBenzene 10A0082 50 ND E801/05/10 01/11/101.0923












SW8260Bcis-1,3-Dichloropropene 10A0082 50 ND E801/05/10 01/11/101.0915



Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0082 50 ND E801/05/10 01/11/101.0916



SW8260BStyrene 10A0082 50 ND E801/05/10 01/11/101.0912


SW8260BTetrachloroethene 10A0082 50 ND E801/05/10 01/11/101.099.6

SW8260BToluene 10A0082 50 ND E801/05/10 01/11/101.0915


SW8260Btrans-1,3-Dichloropropene 10A0082 50 ND E801/05/10 01/11/101.0915








Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)


2 01/05/2010 09:28 01/06/2010 12:11 01/05/2010 09:28 01/11/2010 20:23SW8260B


2 01/05/2010 12:00 01/06/2010 12:11 01/05/2010 12:00 01/11/2010 20:55SW8260B

Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/07/2010 (10A0141-BS1)




2-Butanone (MEK) ug/l5.025.2 45.6-14125.01.8 101

Acetone ug/l2028.9 22.4-15325.03.8 116

Benzene ug/l1.023.1 80.7-12025.00.15 92


Chloroform ug/l1.023.6 80.7-11925.00.16 94



m,p-Xylenes ug/l2.025.1 85-11525.00.35 101


o-Xylene ug/l1.024.0 85-11525.00.19 96


Toluene ug/l1.023.0 85-11525.00.35 92





















Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/07/2010 (10A0141-BS1)


2-Hexanone ug/l5.026.9 58.5-13525.00.31 108






Bromoform ug/l1.023.4 71.9-13125.00.19 94













Styrene ug/l1.025.7 85-11525.00.15 103







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.026.6 45.6-14125.01.8 106 5

Acetone 25ug/l2025.8 22.4-15325.03.8 103 11

Benzene 25ug/l1.022.9 80.7-12025.00.15 92 1


Chloroform 25ug/l1.022.7 80.7-11925.00.16 91 4



m,p-Xylenes 25ug/l2.024.1 85-11525.00.35 96 4


o-Xylene 25ug/l1.023.6 85-11525.00.19 95 1


Toluene 25ug/l1.023.5 85-11525.00.35 94 2





















Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.025.1 58.5-13525.00.31 101 7






Bromoform 25ug/l1.024.1 71.9-13125.00.19 97 3













Styrene 25ug/l1.024.6 85-11525.00.15 98 4







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2032.9 19.7-13125.0 N1aND3.8 132

Benzene ug/l1.020.7 78.4-12725.0 ND0.15 83


Chloroform ug/l1.024.7 77.6-12225.0 0.2200.16 98



m,p-Xylenes ug/l2.022.5 70.8-13225.0 ND0.35 90


o-Xylene ug/l1.023.2 77.5-12225.0 ND0.19 93


Toluene ug/l1.022.1 83-11825.0 ND0.35 88


Trichloroethene ug/l1.0111 77.3-12025.0 87.30.19 94



















Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.028.6 57.9-11825.0 ND0.31 115






Bromoform ug/l1.021.8 63.7-12925.0 ND0.19 87













Styrene ug/l1.017.9 55-13625.0 ND0.15 72







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone 25ug/l2031.9 19.7-13125.0 ND3.8 128 3

Benzene 25ug/l1.021.7 78.4-12725.0 ND0.15 87 5


Chloroform 25ug/l1.023.2 77.6-12225.0 0.2200.16 92 6



m,p-Xylenes 25ug/l2.021.7 70.8-13225.0 ND0.35 87 4


o-Xylene 25ug/l1.021.5 77.5-12225.0 ND0.19 86 7


Toluene 25ug/l1.021.5 83-11825.0 ND0.35 86 3


Trichloroethene 25ug/l1.0109 77.3-12025.0 87.30.19 85 2



















Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.027.2 57.9-11825.0 ND0.31 109 5






Bromoform 25ug/l1.022.1 63.7-12925.0 ND0.19 88 1


Chlorobenzene 25ug/l1.020.9 84.6-11025.0 M2ND0.12 84 6











Styrene 25ug/l1.018.1 55-13625.0 ND0.15 72 1







Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






































Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






























Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/07/2010-01/09/2010 (10A0082-BS1)






















2-Hexanone ug/kg250990 50.6-1331250210 79



Acetone ug/kg500983 23.5-1821250330 79

Benzene ug/kg501040 76-107125023 83




Bromoform ug/kg501050 67.3-110125020 84





Chloroform ug/kg501090 69.8-114125024 87

Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/07/2010-01/09/2010 (10A0082-BS1)







m,p-Xylenes ug/kg1001110 83.5-107125034 89





o-Xylene ug/kg501130 82.8-108125016 90



Styrene ug/kg501170 82.1-111125012 94



Toluene ug/kg501100 81.3-106125015 88










Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone 25ug/kg2501090 50.6-1331250210 87 9



Acetone 25ug/kg5001050 23.5-1821250330 84 7

Benzene 25ug/kg501140 76-107125023 91 9




Bromoform 25ug/kg501140 67.3-110125020 91 7





Chloroform 25ug/kg501140 69.8-114125024 91 4

Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL









m,p-Xylenes 25ug/kg1001180 83.5-107125034 95 7





o-Xylene 25ug/kg501090 82.8-108125016 87 3



Styrene 25ug/kg501210 82.1-111125012 97 4



Toluene 25ug/kg501170 81.3-106125015 94 7










Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone ug/kg250938 38.6-1461240 ND210 76



Acetone ug/kg500765 20.1-1821240 ND330 62

Benzene ug/kg501010 63.6-1081240 ND23 81










Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene ug/kg501100 60.8-1161240 ND16 89



Styrene ug/kg501150 64.5-1151240 ND12 93



Toluene ug/kg501080 62.6-1131240 ND15 87










Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL
























2-Hexanone 25ug/kg250977 38.6-1461250 ND210 78 4



Acetone 25ug/kg5001040 20.1-1821250 R1ND330 83 30

Benzene 25ug/kg50967 63.6-1081250 ND23 77 4










Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL














o-Xylene 25ug/kg501030 60.8-1161250 ND16 82 7



Styrene 25ug/kg501090 64.5-1151250 ND12 88 5



Toluene 25ug/kg501020 62.6-1131250 ND15 82 6






Vinyl chloride 25ug/kg50453 26.1-1301250 R1ND25 36 34




Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013







R1 The RPD/RSD exceeded the method acceptance limit.




Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




454-9303





Sampled:

Received:

01/05/10


Project ID:

PTA0196

14682.013



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PTA0196

Carlene McCutcheon




TAL·0013·550 (12/08)

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Sampler: 1<<:::(114'\ T R~te\JO

Sample Description Sample Container Matrix Type

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~hoenix ~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson - 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number: Analysis Required

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Phone Number:

tt"Bo..,. 3~ ~- ~ "G'-f. 'f IJ Fax Number: ·'{) ~~c- ~Vb ._ i?..4 5' N #of Sampling Sampling

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Cont. Date Time

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/ 12 u intact

Page I of I

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(Check)

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normal ~

(Check)

on ice I r) 0 L ( Q , S~l ,

Note: B relin uishing sam les to TestAmerica, client a rees to a to '""' "'"' i""'"' e uested on this chain of cus od form and an Y q P 9 PY q y y additional anal ses erformed on this ro'ect. y p p J -...

Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.


454-9303

LABORATORY REPORT





Received:

Issued:

01/06/10

01/06/10

01/21/10 16:05







Project: 14682.013


CASE NARRATIVE


PTA0235-01 AB3-10-01610 Soil


PTA0235-03 AB3-20-01610 Soil

PTA0235-04 AB3-30-01610 Soil

PTA0235-05 AB3-40-01610 Soil

PTA0235-06 AB3-50-01610 Soil

PTA0235-07 AB3-60-01610 Soil

PTA0235-08 AB3-ERB-01610 Water

PTA0235-09 AB3-70-01610 Soil

PTA0235-10 AB3-90-01610 Soil

PTA0235-11 AB3-90-01610 DUP Soil

PTA0235-12 AB3-TB2-01610 Soil

Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon

<Page 1 of 49>


454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013






N1 SW8260B: Batch-10A0210:The Laboratory Control Sample recovered high and outside of the project

specific acceptance limits for Methylene chloride, cis-1,3-Dichloropropene and MTBE. All recoveries

were within the laboratory's historical limits. All associated samples are non-detect for these compounds

and therefore are not impacted.

N1 SW8260B:Batch-10A0192:The Laboratory Control Sample / Laboratory Control Sample Duplicate

recovered high and outside of the project specific acceptance limits for 1,2-Dichloropropane,

Bromomethane, Chloroethane, cis-1, 3-Dichloropropene, Dibromochloromethane, Methylene chloride and

trans-1, 3-Dichloropropene. The Matrix Spike / Matrix Spike Duplicate recovered high and outside of the

project specific acceptance limits for 1,2-Dichloropropane, Bromomethane, Chloroethane, Methylene

chloride and trans-1, 3-Dichloropropene. The MSD recovered high and outside of the project specific

acceptance limits for 1,2-Dichloropropane and cis-1, 3-Dichloropropene. The Laboratory Control Sample

Duplicate also recovered high and outside of the project specific acceptance limits for 1,4-Dichlorobenzene.

All recoveries were within the laboratory's historical limits. All associated samples are non-detect for these

compounds and therefore should not be impacted.



Reviewed By:

Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit






SW8260BAcetone 10A0210 20 ND E801/09/10 01/09/1013.8

SW8260BBenzene 10A0210 1.0 ND E801/09/10 01/09/1010.15







SW8260Bo-Xylene 10A0210 1.0 ND E801/09/10 01/09/1010.19


SW8260BToluene 10A0210 1.0 ND E801/09/10 01/09/1010.35


























Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

















SW8260BStyrene 10A0210 1.0 ND E801/09/10 01/09/1010.15







Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0235-08 (AB3-ERB-01610 - Water) Sampled: 01/06/10Reporting Units: ug/l





SW8260BAcetone 10A0210 20 ND E801/09/10 01/09/1013.8

SW8260BBenzene 10A0210 1.0 ND E801/09/10 01/09/1010.15







SW8260Bo-Xylene 10A0210 1.0 ND E801/09/10 01/09/1010.19


SW8260BToluene 10A0210 1.0 ND E801/09/10 01/09/1010.35


























Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0235-08 (AB3-ERB-01610 - Water) - cont. Sampled: 01/06/10Reporting Units: ug/l
















SW8260BStyrene 10A0210 1.0 ND E801/09/10 01/09/1010.15







Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0192 450 ND E801/06/10 01/11/100.901300

SW8260BBenzene 10A0192 45 ND E801/06/10 01/11/100.90121















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit




SW8260BMethylene Chloride 10A0192 90 ND E801/06/10 01/11/100.90129




SW8260Bo-Xylene 10A0192 45 ND E801/06/10 01/11/100.90114



SW8260BStyrene 10A0192 45 ND E801/06/10 01/11/100.90111



SW8260BToluene 10A0192 45 ND E801/06/10 01/11/100.90114










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0192 680 ND E801/06/10 01/11/101.36450

SW8260BBenzene 10A0192 68 ND E801/06/10 01/11/101.3631















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0192 68 ND E801/06/10 01/11/101.3621



SW8260BStyrene 10A0192 68 ND E801/06/10 01/11/101.3617



SW8260BToluene 10A0192 68 ND E801/06/10 01/11/101.3620










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit





















2-Butanone (MEK) SW8260B 10A0192 210250 E401/06/10 01/11/101.06200





SW8260BAcetone 10A0192 500 ND E801/06/10 01/11/101.06330

SW8260BBenzene 10A0192 50 ND E801/06/10 01/11/101.0623















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0192 50 ND E801/06/10 01/11/101.0616



SW8260BStyrene 10A0192 50 ND E801/06/10 01/11/101.0612



SW8260BToluene 10A0192 50 ND E801/06/10 01/11/101.0615










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0192 500 ND E801/06/10 01/11/101.01330

SW8260BBenzene 10A0192 50 ND E801/06/10 01/11/101.0123















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0192 50 ND E801/06/10 01/11/101.0116



SW8260BStyrene 10A0192 50 ND E801/06/10 01/11/101.0112



SW8260BToluene 10A0192 50 ND E801/06/10 01/11/101.0115










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0192 500 ND E801/06/10 01/11/101.04330

SW8260BBenzene 10A0192 50 ND E801/06/10 01/11/101.0423












SW8260Bcis-1,3-Dichloropropene 10A0192 50 ND E8, V101/06/10 01/11/101.0415



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0192 50 ND E801/06/10 01/11/101.0416



SW8260BStyrene 10A0192 50 ND E801/06/10 01/11/101.0412



SW8260BToluene 10A0192 50 ND E801/06/10 01/11/101.0415










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0192 500 ND E801/06/10 01/11/101.05330

SW8260BBenzene 10A0192 50 ND E801/06/10 01/11/101.0523












SW8260Bcis-1,3-Dichloropropene 10A0192 50 ND E8, V101/06/10 01/11/101.0515



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0192 50 ND E801/06/10 01/11/101.0516



SW8260BStyrene 10A0192 50 ND E801/06/10 01/11/101.0512



SW8260BToluene 10A0192 50 ND E801/06/10 01/11/101.0515










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0192 500 ND E801/06/10 01/14/101.06330

SW8260BBenzene 10A0192 50 ND E801/06/10 01/14/101.0623















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0192 50 ND E801/06/10 01/14/101.0616



SW8260BStyrene 10A0192 50 ND E801/06/10 01/14/101.0612



SW8260BToluene 10A0192 50 ND E801/06/10 01/14/101.0615










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit


























SW8260BAcetone 10A0192 500 ND E801/06/10 01/14/100.99330

SW8260BBenzene 10A0192 50 ND E801/06/10 01/14/100.9923















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit








SW8260Bo-Xylene 10A0192 50 ND E801/06/10 01/14/100.9916



SW8260BStyrene 10A0192 50 ND E801/06/10 01/14/100.9912



SW8260BToluene 10A0192 50 ND E801/06/10 01/14/100.9915



Trichloroethene SW8260B 10A0192 3350 E401/06/10 01/14/100.9921







Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0235-11 (AB3-90-01610 DUP - Soil) Sampled: 01/06/10Reporting Units: ug/kg

























SW8260BAcetone 10A0192 450 ND E801/06/10 01/14/100.903300

SW8260BBenzene 10A0192 45 ND E801/06/10 01/14/100.90321















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0235-11 (AB3-90-01610 DUP - Soil) - cont. Sampled: 01/06/10Reporting Units: ug/kg







SW8260Bo-Xylene 10A0192 45 ND E801/06/10 01/14/100.90314



SW8260BStyrene 10A0192 45 ND E801/06/10 01/14/100.90311



SW8260BToluene 10A0192 45 ND E801/06/10 01/14/100.90314










Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0235-12 (AB3-TB2-01610 - Soil) Sampled: 01/06/10Reporting Units: ug/kg

















1,3-Dichloropropane SW8260B 10A0192 3250 E401/06/10 01/12/10114








SW8260BAcetone 10A0192 500 ND E801/06/10 01/12/101330

SW8260BBenzene 10A0192 50 ND E801/06/10 01/12/10123















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PTA0235-12 (AB3-TB2-01610 - Soil) - cont. Sampled: 01/06/10Reporting Units: ug/kg







SW8260Bo-Xylene 10A0192 50 ND E801/06/10 01/12/10116



SW8260BStyrene 10A0192 50 ND E801/06/10 01/12/10112



SW8260BToluene 10A0192 50 ND E801/06/10 01/12/10115






SW8260BVinyl chloride 10A0192 50 ND E801/06/10 01/12/10125




Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)


2 01/06/2010 08:45 01/06/2010 17:21 01/06/2010 08:45 01/11/2010 14:29SW8260B


2 01/06/2010 09:25 01/06/2010 17:21 01/06/2010 09:25 01/11/2010 15:01SW8260B


2 01/06/2010 10:19 01/06/2010 17:21 01/06/2010 10:19 01/11/2010 15:33SW8260B


2 01/06/2010 11:10 01/06/2010 17:21 01/06/2010 11:10 01/11/2010 16:06SW8260B


2 01/06/2010 12:22 01/06/2010 17:21 01/06/2010 12:22 01/11/2010 13:57SW8260B


2 01/06/2010 13:15 01/06/2010 17:21 01/06/2010 13:15 01/11/2010 21:28SW8260B


2 01/06/2010 14:12 01/06/2010 17:21 01/06/2010 14:12 01/14/2010 16:15SW8260B


2 01/06/2010 16:20 01/06/2010 17:21 01/06/2010 16:20 01/14/2010 16:46SW8260B

Sample ID: AB3-90-01610 DUP (PTA0235-11) - Soil

2 01/06/2010 16:20 01/06/2010 17:21 01/06/2010 16:20 01/14/2010 17:18SW8260B

Sample ID: AB3-TB2-01610 (PTA0235-12) - Soil

2 01/06/2010 16:30 01/06/2010 17:21 01/06/2010 16:30 01/12/2010 21:14SW8260B

Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



































1,3-Dichloropropane ug/l1.00.680 E40.18



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.01.87 E40.31


























Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/09/2010 (10A0210-BS1)




2-Butanone (MEK) ug/l5.031.2 45.6-14125.01.8 125

Acetone ug/l2030.2 22.4-15325.03.8 121

Benzene ug/l1.025.5 80.7-12025.00.15 102


Chloroform ug/l1.027.7 80.7-11925.00.16 111



m,p-Xylenes ug/l2.025.3 85-11525.00.35 101

Methylene Chloride ug/l2.029.4 79.7-11725.0 N10.50 118

o-Xylene ug/l1.025.1 85-11525.00.19 100


Toluene ug/l1.025.1 85-11525.00.35 100





















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/09/2010 (10A0210-BS1)


2-Hexanone ug/l5.027.4 58.5-13525.00.31 109






Bromoform ug/l1.023.0 71.9-13125.00.19 92





cis-1,3-Dichloropropene ug/l1.029.3 85-11525.0 N10.17 117



Methyl-tert-butyl Ether (MTBE) ug/l1.031.2 81.8-11825.0 N10.18 125





Styrene ug/l1.025.8 85-11525.00.15 103







Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL






2-Butanone (MEK) 25ug/l5.024.7 45.6-14125.01.8 99 23

Acetone 25ug/l2024.8 22.4-15325.03.8 99 19

Benzene 25ug/l1.022.1 80.7-12025.00.15 89 14


Chloroform 25ug/l1.023.3 80.7-11925.00.16 93 17



m,p-Xylenes 25ug/l2.023.0 85-11525.00.35 92 9


o-Xylene 25ug/l1.022.5 85-11525.00.19 90 11


Toluene 25ug/l1.021.8 85-11525.00.35 87 14





















Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.022.9 58.5-13525.00.31 91 18






Bromoform 25ug/l1.021.2 71.9-13125.00.19 85 8













Styrene 25ug/l1.023.3 85-11525.00.15 93 10







Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone ug/l2023.3 19.7-13125.0 ND3.8 93

Benzene ug/l1.022.4 78.4-12725.0 ND0.15 90





m,p-Xylenes ug/l2.022.1 70.8-13225.0 ND0.35 88


o-Xylene ug/l1.021.8 77.5-12225.0 ND0.19 87


Toluene ug/l1.021.8 83-11825.0 ND0.35 87


















1,3-Dichloropropane ug/l1.021.9 77.1-11925.0 0.6800.18 85



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone ug/l5.020.4 57.9-11825.0 1.860.31 74






Bromoform ug/l1.020.7 63.7-12925.0 ND0.19 83







Dichlorodifluoromethane ug/l1.016.9 71-13825.0 M2ND0.15 68






Styrene ug/l1.021.6 55-13625.0 ND0.15 86







Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







Acetone 25ug/l2024.5 19.7-13125.0 ND3.8 98 5

Benzene 25ug/l1.021.9 78.4-12725.0 ND0.15 87 3





m,p-Xylenes 25ug/l2.021.4 70.8-13225.0 ND0.35 86 3


o-Xylene 25ug/l1.021.3 77.5-12225.0 ND0.19 85 2


Toluene 25ug/l1.021.5 83-11825.0 ND0.35 86 1


















1,3-Dichloropropane 25ug/l1.021.4 77.1-11925.0 0.6800.18 83 2



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL




2-Hexanone 25ug/l5.019.3 57.9-11825.0 1.860.31 70 5






Bromoform 25ug/l1.020.3 63.7-12925.0 ND0.19 81 2







Dichlorodifluoromethane 25ug/l1.015.9 71-13825.0 M2ND0.15 64 6






Styrene 25ug/l1.020.8 55-13625.0 ND0.15 83 4







Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane ug/kg25ND 9.7

1,1,2,2-Tetrachloroethane ug/kg25ND 8.9


1,1-Dichloroethane ug/kg25ND 7.5


1,1-Dichloropropene ug/kg25ND 9.7

1,2,3-Trichlorobenzene ug/kg50ND 9.1

1,2,3-Trichloropropane ug/kg50ND 9.9

1,2,4-Trichlorobenzene ug/kg25ND 9.8


1,2-Dibromoethane (EDB) ug/kg25ND 7.8



1,2-Dichloropropane ug/kg25ND 9.6

1,3,5-Trimethylbenzene ug/kg25ND 8.1

1,3-Dichlorobenzene ug/kg25ND 6.2

1,3-Dichloropropane ug/kg2516.0 E46.8

1,4-Dichlorobenzene ug/kg25ND 9.6



2-Chlorotoluene ug/kg25ND 7.5


4-Chlorotoluene ug/kg25ND 9.0




Bromobenzene ug/kg25ND 9.1


Bromodichloromethane ug/kg25ND 9.0



Carbon tetrachloride ug/kg25ND 9.9

Chlorobenzene ug/kg25ND 5.7



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





cis-1,3-Dichloropropene ug/kg25ND V17.6

Dibromochloromethane ug/kg25ND 5.7

Dichlorodifluoromethane ug/kg25ND 9.5

Ethylbenzene ug/kg25ND 6.5



Methyl-tert-butyl Ether (MTBE) ug/kg25ND 8.7

n-Butylbenzene ug/kg25ND 8.8

n-Propylbenzene ug/kg25ND 8.6

o-Xylene ug/kg25ND 7.9


sec-Butylbenzene ug/kg25ND 8.8

Styrene ug/kg25ND 6.1



Toluene ug/kg25ND 7.5

trans-1,2-Dichloroethene ug/kg25ND 9.1

trans-1,3-Dichloropropene ug/kg25ND V17.5








Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/11/2010-01/12/2010 (10A0192-BS1)

1,1,1-Trichloroethane ug/kg25661 66.4-1186259.7 106

1,1,2,2-Tetrachloroethane ug/kg25599 69.7-1026258.9 96


1,1-Dichloroethane ug/kg25682 70.1-1136257.5 109


1,1-Dichloropropene ug/kg25602 72-1126259.7 96

1,2,3-Trichlorobenzene ug/kg50673 60.4-1206259.1 108

1,2,3-Trichloropropane ug/kg50589 68.8-1066259.9 94

1,2,4-Trichlorobenzene ug/kg25696 65.1-1156259.8 111


1,2-Dibromoethane (EDB) ug/kg25638 78.3-1066257.8 102



1,2-Dichloropropane ug/kg25696 78.8-105625 N19.6 111

1,3,5-Trimethylbenzene ug/kg25640 76.7-1096258.1 102

1,3-Dichlorobenzene ug/kg25624 81-1066256.2 100

1,3-Dichloropropane ug/kg25605 76.9-1056256.8 97

1,4-Dichlorobenzene ug/kg25648 80.6-1056259.6 104



2-Chlorotoluene ug/kg25604 76.9-1056257.5 97

2-Hexanone ug/kg120591 50.6-133625100 95

4-Chlorotoluene ug/kg25619 76.7-1086259.0 99


Acetone ug/kg250914 23.5-182625170 146

Benzene ug/kg25622 76-10762511 100

Bromobenzene ug/kg25624 78.5-1066259.1 100


Bromodichloromethane ug/kg25662 71.4-1116259.0 106

Bromoform ug/kg25529 67.3-11062510 85

Bromomethane ug/kg120626 10-96.4625 N14.2 100

Carbon tetrachloride ug/kg25625 53.7-1296259.9 100

Chlorobenzene ug/kg25623 82.3-1046255.7 100


Chloroform ug/kg25681 69.8-11462512 109

Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


LCS Analyzed: 01/11/2010-01/12/2010 (10A0192-BS1)



cis-1,3-Dichloropropene ug/kg25720 77.3-108625 V1, N17.6 115

Dibromochloromethane ug/kg25678 74.5-107625 N15.7 108

Dichlorodifluoromethane ug/kg25448 10-1346259.5 72

Ethylbenzene ug/kg25628 81.6-1076256.5 101

m,p-Xylenes ug/kg50619 83.5-10762517 99

Methylene Chloride ug/kg50733 70.6-105625 N116 117

Methyl-tert-butyl Ether (MTBE) ug/kg25682 63.1-1196258.7 109

n-Butylbenzene ug/kg25636 76.8-1146258.8 102

n-Propylbenzene ug/kg25622 77.7-1076258.6 99

o-Xylene ug/kg25618 82.8-1086257.9 99


sec-Butylbenzene ug/kg25600 79.5-1106258.8 96

Styrene ug/kg25654 82.1-1116256.1 105



Toluene ug/kg25608 81.3-1066257.5 97

trans-1,2-Dichloroethene ug/kg25642 73.5-1106259.1 103

trans-1,3-Dichloropropene ug/kg25720 72.4-109625 V1, N17.5 115








Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane 25ug/kg25654 66.4-1186259.7 105 1

1,1,2,2-Tetrachloroethane 25ug/kg25598 69.7-1026258.9 96 0


1,1-Dichloroethane 25ug/kg25688 70.1-1136257.5 110 1


1,1-Dichloropropene 25ug/kg25603 72-1126259.7 96 0

1,2,3-Trichlorobenzene 25ug/kg50674 60.4-1206259.1 108 0

1,2,3-Trichloropropane 25ug/kg50588 68.8-1066259.9 94 0

1,2,4-Trichlorobenzene 25ug/kg25693 65.1-1156259.8 111 0


1,2-Dibromoethane (EDB) 25ug/kg25621 78.3-1066257.8 99 3



1,2-Dichloropropane 25ug/kg25704 78.8-105625 N19.6 113 1

1,3,5-Trimethylbenzene 25ug/kg25652 76.7-1096258.1 104 2

1,3-Dichlorobenzene 25ug/kg25635 81-1066256.2 102 2

1,3-Dichloropropane 25ug/kg25602 76.9-1056256.8 96 1

1,4-Dichlorobenzene 25ug/kg25664 80.6-105625 N19.6 106 2



2-Chlorotoluene 25ug/kg25619 76.9-1056257.5 99 3

2-Hexanone 25ug/kg120522 50.6-133625100 84 12

4-Chlorotoluene 25ug/kg25642 76.7-1086259.0 103 4


Acetone 25ug/kg250750 23.5-182625170 120 20

Benzene 25ug/kg25622 76-10762511 99 0

Bromobenzene 25ug/kg25644 78.5-1066259.1 103 3


Bromodichloromethane 25ug/kg25666 71.4-1116259.0 107 1

Bromoform 25ug/kg25532 67.3-11062510 85 1

Bromomethane 25ug/kg120610 10-96.4625 N14.2 98 3

Carbon tetrachloride 25ug/kg25621 53.7-1296259.9 99 1

Chlorobenzene 25ug/kg25630 82.3-1046255.7 101 1


Chloroform 25ug/kg25686 69.8-11462512 110 1

Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





cis-1,3-Dichloropropene 25ug/kg25717 77.3-108625 V1, N17.6 115 0

Dibromochloromethane 25ug/kg25676 74.5-107625 N15.7 108 0

Dichlorodifluoromethane 25ug/kg25430 10-1346259.5 69 4

Ethylbenzene 25ug/kg25636 81.6-1076256.5 102 1

m,p-Xylenes 25ug/kg50626 83.5-10762517 100 1

Methylene Chloride 25ug/kg50730 70.6-105625 N116 117 0

Methyl-tert-butyl Ether (MTBE) 25ug/kg25648 63.1-1196258.7 104 5

n-Butylbenzene 25ug/kg25651 76.8-1146258.8 104 2

n-Propylbenzene 25ug/kg25648 77.7-1076258.6 104 4

o-Xylene 25ug/kg25618 82.8-1086257.9 99 0


sec-Butylbenzene 25ug/kg25619 79.5-1106258.8 99 3

Styrene 25ug/kg25656 82.1-1116256.1 105 0



Toluene 25ug/kg25602 81.3-1066257.5 96 1

trans-1,2-Dichloroethene 25ug/kg25646 73.5-1106259.1 103 1

trans-1,3-Dichloropropene 25ug/kg25710 72.4-109625 V1, N17.5 114 1








Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane ug/kg25644 58.2-115625 ND9.7 103

1,1,2,2-Tetrachloroethane ug/kg25563 57.5-108625 ND8.9 90


1,1-Dichloroethane ug/kg25651 61.8-110625 ND7.5 104


1,1-Dichloropropene ug/kg25597 60.6-111625 ND9.7 95

1,2,3-Trichlorobenzene ug/kg50661 39.2-125625 ND9.1 106

1,2,3-Trichloropropane ug/kg50556 59.4-110625 ND9.9 89

1,2,4-Trichlorobenzene ug/kg25703 43.5-118625 ND9.8 113


1,2-Dibromoethane (EDB) ug/kg25582 64.2-108625 ND7.8 93



1,2-Dichloropropane ug/kg25660 66.7-106625 ND9.6 106

1,3,5-Trimethylbenzene ug/kg25648 50.6-123625 ND8.1 104

1,3-Dichlorobenzene ug/kg25625 62-111625 ND6.2 100

1,3-Dichloropropane ug/kg25570 64.8-107625 ND6.8 91

1,4-Dichlorobenzene ug/kg25635 62.4-110625 ND9.6 102


2-Butanone (MEK) ug/kg120689 34.5-154625 226100 74

2-Chlorotoluene ug/kg25612 58.1-113625 ND7.5 98

2-Hexanone ug/kg120507 38.6-146625 ND100 81

4-Chlorotoluene ug/kg25630 60.8-115625 ND9.0 101


Acetone ug/kg250656 20.1-182625 ND170 105

Benzene ug/kg25612 63.6-108625 ND11 98

Bromobenzene ug/kg25600 64.2-109625 ND9.1 96


Bromodichloromethane ug/kg25637 61.8-111625 ND9.0 102


Bromomethane ug/kg120637 10-93.5625 N1ND4.2 102

Carbon tetrachloride ug/kg25622 44.5-123625 ND9.9 100

Chlorobenzene ug/kg25618 66.9-107625 ND5.7 99



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





cis-1,3-Dichloropropene ug/kg25689 63.3-110625 V1ND7.6 110

Dibromochloromethane ug/kg25638 63-109625 ND5.7 102

Dichlorodifluoromethane ug/kg25472 10-118625 ND9.5 76

Ethylbenzene ug/kg25627 62.4-113625 ND6.5 100


Methylene Chloride ug/kg50695 57.6-106625 N1ND16 111

Methyl-tert-butyl Ether (MTBE) ug/kg25612 54.9-118625 ND8.7 98

n-Butylbenzene ug/kg25646 47.8-132625 ND8.8 103

n-Propylbenzene ug/kg25636 55.8-117625 ND8.6 102

o-Xylene ug/kg25606 60.8-116625 ND7.9 97


sec-Butylbenzene ug/kg25610 60.3-117625 ND8.8 98

Styrene ug/kg25637 64.5-115625 ND6.1 102



Toluene ug/kg25594 62.6-113625 ND7.5 95

trans-1,2-Dichloroethene ug/kg25634 58.4-112625 ND9.1 101

trans-1,3-Dichloropropene ug/kg25683 61.4-109625 V1ND7.5 109








Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane 25ug/kg25651 58.2-115625 ND9.7 104 1

1,1,2,2-Tetrachloroethane 25ug/kg25594 57.5-108625 ND8.9 95 5


1,1-Dichloroethane 25ug/kg25674 61.8-110625 ND7.5 108 3


1,1-Dichloropropene 25ug/kg25588 60.6-111625 ND9.7 94 2

1,2,3-Trichlorobenzene 25ug/kg50656 39.2-125625 ND9.1 105 1

1,2,3-Trichloropropane 25ug/kg50588 59.4-110625 ND9.9 94 6

1,2,4-Trichlorobenzene 25ug/kg25674 43.5-118625 ND9.8 108 4


1,2-Dibromoethane (EDB) 25ug/kg25609 64.2-108625 ND7.8 97 5



1,2-Dichloropropane 25ug/kg25668 66.7-106625 N1ND9.6 107 1

1,3,5-Trimethylbenzene 25ug/kg25632 50.6-123625 ND8.1 101 3

1,3-Dichlorobenzene 25ug/kg25612 62-111625 ND6.2 98 2

1,3-Dichloropropane 25ug/kg25573 64.8-107625 ND6.8 92 1

1,4-Dichlorobenzene 25ug/kg25638 62.4-110625 ND9.6 102 1


2-Butanone (MEK) 25ug/kg120732 34.5-154625 226100 81 6

2-Chlorotoluene 25ug/kg25596 58.1-113625 ND7.5 95 2

2-Hexanone 25ug/kg120520 38.6-146625 ND100 83 3

4-Chlorotoluene 25ug/kg25614 60.8-115625 ND9.0 98 2


Acetone 25ug/kg250689 20.1-182625 ND170 110 5

Benzene 25ug/kg25609 63.6-108625 ND11 97 1

Bromobenzene 25ug/kg25620 64.2-109625 ND9.1 99 3


Bromodichloromethane 25ug/kg25645 61.8-111625 ND9.0 103 1


Bromomethane 25ug/kg120624 10-93.5625 N1ND4.2 100 2

Carbon tetrachloride 25ug/kg25608 44.5-123625 ND9.9 97 2

Chlorobenzene 25ug/kg25596 66.9-107625 ND5.7 95 4



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL





cis-1,3-Dichloropropene 25ug/kg25697 63.3-110625 V1, N1ND7.6 112 1

Dibromochloromethane 25ug/kg25644 63-109625 ND5.7 103 1

Dichlorodifluoromethane 25ug/kg25471 10-118625 ND9.5 75 0

Ethylbenzene 25ug/kg25603 62.4-113625 ND6.5 96 4


Methylene Chloride 25ug/kg50713 57.6-106625 N1ND16 114 3

Methyl-tert-butyl Ether (MTBE) 25ug/kg25655 54.9-118625 ND8.7 105 7

n-Butylbenzene 25ug/kg25630 47.8-132625 ND8.8 101 3

n-Propylbenzene 25ug/kg25622 55.8-117625 ND8.6 100 2

o-Xylene 25ug/kg25583 60.8-116625 ND7.9 93 4


sec-Butylbenzene 25ug/kg25594 60.3-117625 ND8.8 95 3

Styrene 25ug/kg25627 64.5-115625 ND6.1 100 2



Toluene 25ug/kg25586 62.6-113625 ND7.5 94 1

trans-1,2-Dichloroethene 25ug/kg25637 58.4-112625 ND9.1 102 0

trans-1,3-Dichloropropene 25ug/kg25702 61.4-109625 V1, N1ND7.5 112 3








Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013









Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




454-9303





Sampled:

Received:

01/06/10


Project ID:

PTA0235

14682.013



TestAmerica Phoenix

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PTA0235

Carlene McCutcheon




TAL-0013-550 (12/08)

Project Manager: i:,.~ C.flA.I(:;.

Sampler: '[email protected] r~~

Sample Description Sample Matrix

A83-IO- 0 I f:>l 0 SoH ...

AG~- ~-Dib~C v.J~

~'3-lt.::> -cJ b to SOIL.

413->-1 o -ol bt-O l(

Ai0'3-L{p-o~ I::. to 'L

AS:3-So-ol b~o J\

P/33-66-61 bt 0 H

Af/3-~e-o\ b~o -b)AM

A03-7o~ o J '=- ~ (:) SOH ..

Af!fJ- yo- e:>l b J o . ll

AB3- ?o- o1 t:.1o buP tl

A6'3-T82.- O\ 6£.'D wAwc.

Relinquished By:

CHAIN OF CljSTODY FORM

~hoenix ~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602} 454-9303 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520} 807-3801 FAX (520) 807-3803

Container Type

L/DM;/ ~A.\

tj,DM-/ li

t t

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L(

l{,CMJl

l(;CM.I I(

ll

40MJI

[ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702} 798-3620 FAX (702} 798-3621

Project/ PO Number:

Phone Number:

"tCCo -'3 "VC- t,Z,.'"'j 't (j -.f)

N Fax Number: Lte:>-o'l'B- n ... 'i5 #of

Cont. Sampling Sampling . 00

Date lime Preservatives

3 Jf b/Jo 6Bt.JS MroJ(.. / l 'h.f K::> 0125 W.c.l /

3 .,,b/ bll octZS MtE..cl7i- / 3 ''biJ 0 Jotc; t.( v 3 l/oh'il> 'J 16 L l / 6 l/b/Jo 17....?.:2.... l f / 3 l/b//0 1315 I I ~ 3 "lbJ~c 132$ b-ki / ":) ~fb/tc l'-!t'L Me.q,.t v 3 'lh/1o /b'LD t I I/ 3 '/b/to lb~ tl v I lf,f,o J{/30 (YleCI-J ,./

Analysis Required

Page of /


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as

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Received By: Date/Time: Turnaround Time: (Check) ·-----? same day 72 hours

Date/Time: Date/Time: 24 hours 5 days

48 hours normal ~ ' Sample Integrity: (Check)

\"7 2~ intact -~ on ice c{J,t L Relinquished By: Date/Time: (_ ~ceiveP~+ j ;{;//~me:

Note: By rehnqu1shmg samples to TestAmenca, client agrees to pay for the serv1ces requested bn th1s cham of c~stody form and any additional analyses performed on th1s project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

: .,

LABORATORY REPORT · 2018. 11. 18. · 12/11/09 Report Number: 12/11/09 Project ID: PSL0747 14682.013 SAMPLE RECEIPT: Samples were received intact, at 1°C, on ice and with chain

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