Insert report title here Supplementary Soil Survey for Proposed …eisdocs.dsdip.qld.gov.au/Galilee Coal Project (Northern Export Facility... · 12 December 2012 Cardno 4 L:\Engineer

$Page 1: Insert report title here Supplementary Soil Survey for Proposed …eisdocs.dsdip.qld.gov.au/Galilee Coal Project (Northern Export Facility... · 12 December 2012 Cardno 4 L:\Engineer$
Insert report title here

Insert project name

U23415

Prepared forWaratah Coal

12 December 2012

Supplementary Soil Survey for Proposed Open Cut Area

China First Coal Mine Project

U23415

A p p e n d i c e s | Supplementary Soil Survey for Open Cut Area

179179

WARATAH COAL CHINA FIRST COAL MINE

12 December 2012 Cardno iiL:\Engineer Reports\U23415 Waratah Coal_Mapping-Galilee Basin\Correspondance\U23415_Waratah Coal Report Version 1_ Final.doc

Document Information Prepared for Waratah Coal Project Name China First Coal Mine, Alpha File Reference U23415_Waratah Coal Report Version 1_ Final.doc Job Reference U23415 Date 12 December 2012

Contact Information Cardno QLD Trading as Cardno Ullman & Nolan Geotechnic ABN 57 051 074 992

71 Connors Road, Mackay Qld 47400

Telephone: 07 4952 5255 Facsimile: 07 4952 5455 International: 614+ 07 4952 5255

[email protected]

Document Control Version Date Author Author

InitialsReviewer Reviewer

Initials

0 29.11.12 Andrew Williams AW Karen Gates KEG

1 12.12.12 Michael Large ML Andrew Williams AW

© Cardno 2012. Copyright in the whole and every part of this document belongs to Cardno and may not be used, sold, transferred, copied or reproduced in whole or in part in any manner or form or in or on any media to any person other than by agreement with Cardno.

This document is produced by Cardno solely for the benefit and use by the client in accordance with the terms of the engagement. Cardno does not and shall not assume any responsibility or liability whatsoever to any third party arising out of any use or reliance by any third party on the content of this document.

W A R A T A H C O A L | Galilee Coal Project | Supplementary Environmental Impact Statement – March 2013

180


12 December 2012 Cardno iiiL:\Engineer Reports\U23415 Waratah Coal_Mapping-Galilee Basin\Correspondance\U23415_Waratah Coal Report Version 1_ Final.doc

Executive Summary

Table of Contents Executive Summary iii 1 Letter of Transmittal 4

2 Project Description 5

3 Methodology of Survey 5 3.1 Field Work 5

3.1.1 Physical Testing 6 3.1.2 Chemical Testing 7

4 Acid Sulphate Soils Assessment 7

5 Results and Discussions 7

6 Soil Management Units 8

7 Recommendations 8

Appendices APPENDIX A Descriptive Borehole Logs, Site Photographs and Daily Activity Summary APPENDIX B Physical Test Results APPENDIX C Chemical Test Results

Tables

Table 1 Physical Laboratory Results 6

Figures

Figure 1 Site Location........................................................................................................... 9 Figure 2 Borehole Locations- Glen Innes ............................................................................. 9 Figure 3 Borehole Locations-Kia Ora .................................................................................... 9 Figure 4 Distribution of Soil Management ............................................................................. 9


181181


12 December 2012 Cardno 4 L:\Engineer Reports\U23415 Waratah Coal_Mapping-Galilee Basin\Correspondance\U23415_Waratah Coal Report Version 1_ Final.doc

1 Letter of Transmittal

Contact: Andy Williams

12 December 2012

Waratah Coal Level 7, 380 Queen Street, Brisbane QLD4740

Attention: Natasha McIntosh

plementary Soil Survey Ffor Proposed Open Cut AreaSUPPLEMENTARY SOIL SURVEY FOR PROPOSED OPEN CUT AREA CHINA FIRST COAL MINE

Dear Natasha,

At the request of the client, Waratah Coal; Cardno Ullman & Nolan Geotechnic (CUNG) have undertaken an additional soil survey to assist in the development approval process for the proposed China First Coal Mine near Alpha in Central Queensland.

This request provides the methodology and findings of the survey. The scope and methodology followed herein has dictated by the client’s scope which is understood to adhere to directives from the regulator.

This survey should be construed as preliminary in nature which needs verification by additional work prior to commencement of cut activities.

Thank you for your commission to undertake this investigation. Should you have any queries please do not hesitate to contact the undersigned.

Yours faithfully,

Andrew Williams Principal Engineering Geologist / Project Director MS.Env.Mgmt., BSc.(Hons), Pg.Dip., CGeol for Cardno Ullman & Nolan Geotechnic Email: [email protected]

Cardno Ullman & Nolan Geotechnic Pty Ltd ABN 57 051 074 992

71 Connors Road Mackay Old 4740 Mackay Qld4741Australia Telephone: 07 4952 5255 Facsimile: 07 4952 5455 International: +61 7 4952 5255 [email protected] www.cardno.com.au


182



2 Project Description

The Galilee Coal Project (Northern Export Facility – also known as the China First Coal Mine – hereafter referred to as the ‘the project’ involves the development of the following:

A new coal mine and associated infrastructure located near Alpha in the Galilee Basin, Central Queensland, and

A rail network between the mine and the Abbot Point State Development Area (APSDA)

The project is being developed by Waratah Coal, a privately owned Australian Coal Exploration and Coal development company.

The project comprises a new coal mine located in the Galilee Basin, Queensland, approximately 30 km to the North of Alpha and a new rail line connecting the mine to future coal terminal and stockpiling facilities in the Abbot Point State Development Area (ASPDA) and port loading facilities at the Port of Abbot Point. The Rail line and port components are not part of this current commission.

Waratah Coal proposes to mine 1.4 billion tonnes of raw coal from its existing tenements, Exploration Permit for Coal (EPC) 1040 and part of EPC 1079 (mining lease application 70454). The mine development involves the construction of four 9 million tonnes per annum (Mtpa) underground long-wall coal mines, two 10 Mtpa open cut pits and two coal preparation plants both with raw washing capacity of 28 Mtpa.

The annual Run-of-Mine (ROM) coal production will be 56 Mtpa to produce 40 Mtpa of saleable export highly volatile, low sulphur, steaming coal to international markets. At this scale of operation, the capital expense of $8.3 billion (AUD) to construct the mine and rail infrastructure is economically viable over the life of the project.

The particular part of the project involved in this commission is the Open Cut areas of the Coal Mine near Alpha. Figure 1 shows the location of this site area.

3 Methodology of Survey

The scope of the survey was directed by the client following the scope requested by the regulator for additional soil survey. The survey will not meet usual density of sampling but is meant to be preliminary in nature to be followed by a more detailed later stage prior to excavation of the open pit.

3.1 Field Work

The field survey was conducted between 29th and 30th October to collect additional data on the soils of the project site (proposed open cut area on Kia Ora and Glen Innes Property)(Figure 1). This survey was undertaken over a period of two (2) days; consisted of primary sampling and visual assessments. Visual assessments were conducted continuously across the study area while traversing along the limited access tracks. Where visual assessments indicated a change in soils conditions outside of the pre-selected sampling grid, an additional sample was collected.

Sampling strategies and survey plans were developed in accordance with the Technical Guidelines for the Environmental Management of Exploration and Mining in Queensland – Land Suitability Assessment Techniques (Department of Minerals and Energy, 1995). However the Kia Ora area was restricted to sampling along the linear Monklands road corridor on the eastern boundary. The land holder denied access to Kia Ora on 29th October. Glen Innes property was accessed but sampling was restricted to existing tracks. Primary sampling was conducted at 20 locations within the boundaries of the proposed open cut areas (figure 2). The location of each site was recorded using a global positioning system (GPS) with an accuracy of +/- 10 metres (m), see figure 2.

Using a mechanical auger for holes 1 to 7 and hang auger for 8 to 20, samples holes were excavated to a depth of 100 centimetres (cm), where possible. Soil samples were collected from a minimum of five depths throughout the profile; typically 0 -10cm, 10 – 20cm, 20 – 30cm, 30 – 60cm and 60 – 100cm. Care was taken to ensure clean samples were taken from each of the five depths in order to avoid cross-contamination.


183183



Sampling at evenly spaced intervals across the Bimblebox area of Glen Innes station (Figure 2) allowed for quantitative comparisons between chemical and physical parameters following analysis and best met the data requirements for determining the pre-mining land use suitable in accordance with the technical guidelines with the Environmental Management of Exploration and Mining in Queensland (Department of Minerals and Energy, 1995). The sampling for Kia Ora Station (KO1 & KO7) was restricted as access was denied on the 29th October to the property. The holes were then relocated along Monklands Road in the adjacent road corridor (Figure 3). Although not ideal we feel this still reflects the soil likely to be encountered on Kia Ora.

Each sample was sealed in a clean plastic zip-lock bag. The bags were labelled with the sample site number and depth of sampling. At the completion of the field survey, bagged soil samples were grouped together into similar soil types based on field observations, soil physical characteristics and the topographical and vegetation characteristics of the survey site. This arrangement, coupled with a site map outlining soil sampling location, was used to select several representative samples of each soil type for further analysis of their chemical and physical properties. The selected samples were then packaged for transportation to a National Association of Testing Authorities (NATA) registered laboratory for chemical and physical analysis. Laboratory Testing

3.1.1 Physical Testing

A total of five sampling locations were selected for physical laboratory analysis. Tests carried out by Mackay CUNG laboratory were gradings, Atterberg limits and Emerson class in accordance with AS1289.

The physical laboratory results are summarised in table 1 below and given in Appendix B.

Table 1 – Physical Laboratory Results

Location Depth (m) Material Description

GravelContent

(%)

Sand Content

(%)

Clay & Silt

Content (%)

Liquid Limit (%)

Plastic Limit (%)

Plastic Index(%)

Emerson Class

No.

Bimble Box 07 0.3-0.6 Silty Sand 0 78 22 NO ND NP 2



Monklands Road KO 2 0.3-0.6 Silty Sand 0 79 21 NO ND NP 2

Monklands Road KO 5 0.1-0.2 Silty Sand 0 73 27 NO ND NP 2

NO = Not Obtainable ND = Non Determinable NP = Non Plastic


184



3.1.2 Chemical Testing

Twenty two (22) samples were selected from those collected in the field and submitted to a NATA Certified Laboratory, ALS Environmental Laboratories in Brisbane, for chemical Analysis. Surface and subsurface sample from both the KO and BB areas were tested for:

Conductivity; Chloride Concentration; Soil pH; Cation Exchange Capacity (CEC) with Exchangeable Sodium Percentage (ESP); and The Sodium Absorption Ratio (SAR).

Confirmation from ALS indicates that the samples were received in good condition and with recommended holding times.

The results are given in Appendix C.

4 Acid Sulphate Soils Assessment

State Planning Policy 2/02 – Planning and Managing Development Involving Acid Sulphate Soils (Department of Infrastructure and Planning (DIP), 2002) sets out the State‟s interests concerning development involving acid sulphate soils in low-lying coastal areas. The policy applies only to certain types of development assessments in a strict list of local government areas as outlined in Annex 1 of the policy. Given that the Project falls outside of these areas, an assessment of the risk of acid sulphate soils is not relevant. We note also the soils test results indicated uniform alkaline soils and we consider that acid producing soils are unlikely to be encountered at this site.

5 Results and Discussions

The available analytical data from the Waratah Coal's Galilee Coal Project's "the site” soil profile show the soil to be generally non sodic at the surface with a marked increases in sodicity with depth, exhibiting strongly sodic characteristics. The soil profile is moderately alkaline in nature with the pH ranging from 5.9 to 9.4 pH units, with the majority of the tested pH readings ranging from 6-8 pH units. The soil contains no net acidity. The soil alkalinity directly affects the salinity and exchangeable sodium percentage (ESP), hence the soils are moderate to highly saline, however salt crusts were not observed and may go some way in explaining the high concentrations of chloride and sodium in the soil.

Down the soil profile the ESP in the KO area(for example KO1)increases whilst the Sodium absorption ratio (SAR) decreases. Alternatively in the BB area, BB15 shows both variables to increase down the profile and whilst BB6 reveals a third set of trends with an increasing SAR and a decreasing ESP. This may implicitly reveal a trend of increasing sodium concentration, hence sodicity down the soil profile.

The CEC of the soil generally suggests the soil profile to be largely macro and micro nutrient deficient for agronomic purpose.

No conclusions can be drawn into the soil's viability for optimal plants, based on the analytical data. Analysis of nitrogen, phosphorous and organic carbon must be performed to quantify the topsoil for these purposes. “Preliminary Report on the Geochemical Assessment of the Galilee Coal Project – DRAFT” dated 10 November 2012, was reviewed at the request of the client. Although our survey did not go deep enough to validate its findings, the chemistry of the soil supports the findings of the EGI report.


185185



6 Soil Management Units

Based on field and laboratory assessments, ten soil management units (SMUs) were identified within the Project site. These SMUs were classified as the Britt and Nelson unit. The distribution of these units havebeen mapped and presented in Figure 4. A description of each management unit is provided below.

Britt Soil Management Unit-

Australian soil classification: Brown - Grey Vertosol Topography and Landform Attributed: Landscapes of the Britt SMU consist primarily of gently undulating plains which have been extensively cleared for agriculture, slopes of 0.5 to 1%. Geology Unit: The physio-chemical characteristics of this soil are consistent with the soil’s development in close proximity to Tertiary basaltic geological formations. Native Vegetation: Cleared; Non-remnant. Physical Attributes: The Britt SMU consists primary of a grey to brownish-grey medium clay, with a consistent texture maintained through the profile. Field observations suggest a soil with small and irregular cracking at the surface, indicating a soil that is likely to shrink (dry) swell (wet). The soil is well structured with large (40-80mm), friable peds. A very fine sandy surface layer was present.

7 Recommendations

We have provided the soil mapping areas across the Open Cut area based on limited access, andsurrounding surrogate data survey data. We recommend at a later date we verify our mapping at a later date.

The surface soils down to around 300mm depths seem to have the potential for reuse as topsoil for mine site remediation. This needs to be further confirmed with additional investigation into the nutrients levels of the soils.

We have found that on the basis of our survey, no acid providing soils exist at site and therefore no management is required.

We trust that you find this report of interest and look forward answering any queries and to being of service to Waratah Coal again in the near future.

Additional investigation at a later stage is required to sample and test the soils in full area of Open Cut to meet appropriate regulatory requirements.


186



Figure 1 Site Location Figure 2 Borehole Locations- Glen Innes Figure 3 Borehole Locations-Kia Ora Figure 4 Distribution of Soil Management


187187

188

This page is intentionally left blank.


189



190

191



192


12 December 2012 Cardno 10L:\Engineer Reports\U23415 Waratah Coal_Mapping-Galilee Basin\Correspondance\U23415_Waratah Coal Report Version 1_ Final.doc

APPENDIX A

Descriptive Borehole Logs, Site Photographs and Daily Activity Summary


193193

U23415 Waratah Coal Services – Soils Survey Daily Activites

28th October 2012

Time ActivityMobilise from Mackay to Rockampton

5pm Arrive at Alpha Motel

29th October 2012

Time Activity6.15am Woke up6.45am Breakfast7.00am Met with Jo Chen7.45am Wash down9.00am Finish wash down9.15am Sign of wash down9.45am Toolbox Check9.45am Drive to site10.15am Arrive at site – discussions with landowner who refused entry to land,

discussion with Brisbane and waiting upon instruction11.45am Jo Chen has mechanical car breakdown12.30pm Arrive a Northern Site , chainage 41.712.45pm Start BH11.35pm Start BH22.00pm Start BH32.35pm Start BH43.05pm Start BH53.35pm Start BH64.05pm Start BH74.35pm Finish BH7 and demobilised for the day4.55pm Left Site5.45pm Arrive at motel

30th October 2012

Time Activity6.15am Woke up6.45am Breakfast7.35am Days preparation7.45am Leave for site8.45am Arrive at site, start BH089.25am Start BH0910.06am Start BH1010.36am Start BH1111.25am Start BH1211.55am Start BH1312.30pm Start BH1412.55pm Start BH151.55pm Start BH162.26pm Start BH172.50pm Start BH183.10pm Start BH19


194

3.35pm Start BH204.15pm Left site for motel5.15pm Arrived back at motel

31st October 2012

Time Activity6.15am Woke up7.00am Demobilisation from Alpha Motel to Rockampton and Mackay2pm Arrive in Mackay


195195

0.05

0.28

1.40

L

MD

M

D

M

Silty Sand; black to dark brown, fine grained, with roots and ash, nostructureSandy Silt (loam); brown, fine grained sand, peds up to 30mmMPS 1 LL NP P75 65

Silty Sand; orange-brown, fine grainedMPS 1 LL NP P75 25

occassional red iron staining

Photographs 12 and 13

BB 07 TERMINATED AT 1.40 mSurface Feature: disturbed in cut drain around 200mm below ngl, flat,mature grasses

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency

TESTINGVISUAL SOIL DESCRIPTION

Description(SOIL NAME; plasticity/grain size, colour, particle

shape, secondary components, minor constituents)(ROCK NAME; grain size, colour, minor constituents)

CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel

Contractor : Cardno UNGDrill Rig : Hand AugerMounting : AugerDiameter: 75 mmCoords : 443071.0 m E 7408376.0 m N MGA94

BOREHOLE LOGBorehole No. : BB 07

Sheet : 1 of 1

Hole Commenced : 29.10.12Hole Completed : 29.10.12Logged By : AWChecked By : AWSurface R.L. (m) : 339.00 WSG 84

Client : Waratah CoalProject : Waratah Coal Mapping GalileeBasinJob No : U23415Site : China First Coal MineLocation : Glen Innis - Bimble BoxCH29.3km

Sup

port

Met

hod

& B

it

TestingSampling

DRILLING

very softsoftfirmstiff

very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75

Moisture Visual Description Method Bit SupportConsistency SamplingRollerBlankV bit

TC bitDiamond

Maximum particle sizeLiquid Limit

% passing 75um sieve

CasingMud

Nil

UDNPPBESLABDUPSPLIT

Undisturbed Sample & Size in mmDisturbed Sample

Standard Penetration Test & ResultPocket Penetrometer Value

Bulk SampleEnvironmental Sample

Sample sent to LabDuplicate Sample

Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer

CoreRotary air flush

Vibrocore

CMN

0.5

1.0

338.5

338.0


196

0.28

1.00

MD

M

D

Silty Sand; dark brown, fine grained, with rootlets and organics atsurface (SANDY LOAM)MPS 1 LL NP P75 30

becoming brown, no organics, no structure, peds up to 20mm

Silty Sand; orange-brown, fine grained, (SANDY LOAM), nostructureMPS 0.5 LL NP P75 35

See phtographs 14 and 15

BB 08 TERMINATED AT 1.00 mSurface Feature: flat, mature gums, low strubs and grasses

NAT

B-1

B-2

B-3

0.10m

0.20m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1


Client : Waratah CoalProject : Waratah Coal Mapping GalileeBasinJob No : U23415Site : China First Coal MineLocation : Glen Innis Track - Bimble Box

Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

353.5

353.0


197197

0.80

1.00

MD

M

D

M

Silty Sand; dark brown, fine grained, with rootlets, (Sandy Loam)MPS 2 LL NP P75 30

becoming pale brown, gradational change, no structure and noorganics

Silty Sandy Gravel; dark orange-brown mottled brown and grey,angular, sandstoneMPS 20 LL NP P75 15

See photographs 16 and 17

BB 09 TERMINATED AT 1.00 m

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

349.5

349.0


198

0.45

1.00

L

MD

D

M

D

M

Silty Sand; dark brown, fine grainedMPS 1 LL NP P75 40

becoming pale brown

peds up to 45mm

Silty Clayey Sand; brown mottled pale brown-biege, fine grained,peds up to 40mm with orange-brown staining along fissuresMPS 1 LL NP P75 50

occassional dark red-brown streaks and mottles, iron staining


BB 10 TERMINATED AT 1.00 mSurface Feature: flat, anthills, mature remnant vegetation - trees,shrubsDrainage: to north

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

347.5

347.0


199199

1.00

L

M

D

M

Silty Sand; dark brown, fine grained, , no strucutre (Sandy Loam)MPS 1 LL NP P75 30

becoming pale brown

becoming orange- brownMPS 1 LL NP P75 35


BB 11 TERMINATED AT 1.00 mSurface Feature: flat, mature remnant 150m south of Kia Oraboundary

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

348.5

348.0


200

0.20

0.33

1.00

MD

VD

MD

M

D

Silty Sand; dark brown, fine grained, with rootlets and organics(Sandy Loam)MPS 1 LL NP P75 40Silty Sand, brown, fine grained, no structure or organics, peds size upto 5mm

Silty Sand; brown, fine grained, slightly cementedMPS 1 LL NP P75 45

Clayey Silty Sand; brown, ped size up to 40mm, uncemented, nostructure or organic gradational

becoming orange-brown mottled biege, ped size up to 20mm


BB 12 TERMINATED AT 1.00 mSurface Feature: flat, mature, bimble box grass, shrubs and treesDrainage: to north-east

NAT

B-1

B-2

B-3

0.10m

0.20m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

337.5

337.0


201201

0.09

0.75

MD

D

M

D

Silty Sand; dark brown, with rare gravel, angular (sandy Loam)MPS 10 LL NP P75 30

Silty Gravelly Sand; brown, fine grainedMPS 10 LL NP P75 30

Silty Gravelley Sand, dark brown mottled grey and pale brown,sub-angular to angular sandstone

becoming very hard augering (possibly weathered rock)

Photographs 24 and 25BB 13 TERMINATED AT 0.75 mRefusalSurface Feature: flat, mature, bimblebox remunant trees, shrubs andgrass

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

338.5

338.0


202

0.08

0.70

1.00

L

MD

M

D

M

Silty Sand; dark brown, fine grained, with rootlets and surfaceorganicsMPS 1 LL NP P75 25Silty Sand; brown, fine grained, with rare roots and rare angulargravelsMPS 7 LL 15 P75 30

Silty Sand; brown-grey mottled orange-brown, fine grained, withgravelMPS 10 LL 20 P75


BB 14 TERMINATED AT 1.00 m

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

353.5

353.0


203203

0.12

0.45

1.00

MD

D

M

D

Silty Sand; dark brown, fine grained, with rootlets and organicsMPS 1 LL NP P75 40

Silty Sand; pale brown, fine grainedMPS 0.5 LL NP P75 40

hard, slow augering due to slight cementation

Gravelly Silty Sand; orange-brown mottled grey, fine grained, fine tocoarse grained, angular sandstone gravelMPS 20 LL NP P75 30


BB 15 TERMINATED AT 1.00 mSurface Feature: flat, mature bimle box material trees

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

349.5

349.0


204

0.08

0.38

1.00

LM

Silty Sand; dark brown, fine grained, with organics and rootlets atsurface (Sandy Loam)MPS 1 LL NP P75 15Silty Sand; brown, fine grained, no organics, no structureoccassional pale brown mottling

Silty Sand; orange-brown, fine to medium grained, peds up to20mm, no structure, no organicsMPS 2 LL NP P75 25

occassional pale brown mottling


BB 16 TERMINATED AT 1.00 mSurface Feature: flat, mature trees, shrubs and grasses

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

344.5

344.0


205205

0.07

0.79

L

MDM

Silty Sand; dark brown, fine grained, with organics and rootlets(Sandy Loam) MPS 1 LL 0 P75 30Silty Sand; pale brown, fine grained, no structure, no organicsMPS 2 LL NP P75 35

Gravelley Silty Sand, pale brown, fine to coarse grained gravels,angular (possible weathered rock)MPS 2 LL NP P75 35


BB 17 TERMINATED AT 0.79 mRefusalSurface Feature: gentle slope 2 degrees to east, slightly cementedsands exist along road within 10m of auger hole

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

358.5

358.0


206

1.00

LM

Silty Sand; fine grained, no structure, organics at surface (SandyLoam)

Silty Sand, pale brown, fine graind, gradationalMPS 0.5 LL 20 P75 35

tree roots at 0.5m

becoming orange-brown - powdery

see photographs 34 and 35

BB 18 TERMINATED AT 1.00 mSurface Feature: flat, 3m from trackVegetation: mature trees, shrubs and grassesDrainage: to eastSee phograph 34 and 35

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

344.5

344.0


207207

1.00

L

MD

M

Silty Sand; dark brown, fine grained, (Sandy Loam)Silty Sand, brown, gradation colour change, ped up to 20mm, nostructure, no organics

Becoming light brown


BB 19 TERMINATED AT 1.00 mSurface Feature: flat, matureVegetation: trees and grasses, 4m from track, soft sands on track 50mto west

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

340.5

340.0


208

0.22

1.00

L

M

D

Silty Sand; dark brown, fine grained, ped size up to 30mm, noorganics, no structure (sandy Loam)MPS 1 LL NP P75 35

Silty Sand; orange-brown, fine grained, no organics, no structureMPS 1 LL NP P75 30

becoming gravelley, angular, dark brown sandstone


BB 20 TERMINATED AT 1.00 mSurface Feature: gentle slope 1 degree to north-eastVegetation: mature trees and shrubs and grassesDrainage: to north-east, fire break scraped surface

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

348.5

348.0


209209

0.34

1.00

L - MD

St

VSt

M

D

M

Silty Sand; pale brown, fine grained, slighly clayey, ped size10-30mm, occassional root with occassional black (root staining) withrare gravels (sandy Loam)MPS 10 LL NP P75 40

Silty Clay; green-brown, (VERTOSOL) no structureMPS 1 LL 30 P75 75


KO 01 TERMINATED AT 1.00 mSurface Feature: Disturbed devegetation, very flat, 10m from roadVegetation: grass, sparce small treesDrainage: to south west

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel

Contractor : Cardno UNGDrill Rig : CruiserMounting : AugerDiameter: 75 mmCoords : 448507.0 m E 7419082.0 m N MGA94

BOREHOLE LOGBorehole No. : KO 01

Sheet : 1 of 1

Hole Commenced : 29.10.12Hole Completed : 29.10.12Logged By : AWChecked By : AWSurface R.L. (m) : WSG 84

Client : Waratah CoalProject : Waratah Coal Mapping GalileeBasinJob No : U23415Site : China First Coal MineLocation : Kia Ora - CH41.7km

Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0


210

1.20

L

MD

M

D

M

Silty Sandy loam; brown, fine grained, (Aedian)MPS 2 LL NP P75 30

becoming orange-brownMPS 0.5 LL NP P75 21

See photographs 3 to 5

KO 02 TERMINATED AT 1.20 mSurface Feature: side of road, mature cactus grasses, flat lagooncreek 200m west

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1

Hole Commenced : 29.10.12Hole Completed : 29.10.12Logged By : AWChecked By : AWSurface R.L. (m) : WSG 84


Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0


211211

0.47

1.00

L

St

M

D

M

Silty Sandy loam; pale brown, fine grained, powdery, with rarerootlets, Aeolian, no structureMPS 2 LL NP P75 25

Sandy Silty Clay; brown, with fissures and slicken sides,VERTOSOLMPS 1 LL 20 P75 65


KO 03 TERMINATED AT 1.00 m

NAT

B-1

B-2

B-3

B-4

B-5

B-6

0.10m

0.20m

0.30m

0.47m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

333.5

333.0


212

0.55

1.10

F

D - VD

D

M

Sandy Powdery silt; pale brown, with fine grained sand, trace raregravels and rootlets (LOAM)MPS 10 LL 20 P75 55

no gravels

Silty Sandy Gravel; dark brown, angular, shaped ped up to 20mm(ALLUVIAL)MPS 20 LL NP P75 30

No photographs taken

KO 04 TERMINATED AT 1.10 mSurface Feature: flat immature grass and bush, 10m from roadDrainage: to east grass sparse and anthills

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

331.5

331.0


213213

0.38

1.00

F

St

VSt

D

M

Sandy Silt loam; pale brown, fine grained sand, powdery, noorganics

Silty Clay; green-brown, with rare gravels, angular, with somefissures peds up to 10mm

KO 05 TERMINATED AT 1.00 mSurface Feature: flat, mature gums and shrubs, grasses, 10m fromroad, standing water next to road 30m away

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1



Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

330.5

330.0


214

0.28

1.00

F

M

D

Sandy Silt; pale grey-biege, fine grained sand, sandy loam, ped size20mm , no organics (LOAM)becoming less gravelMPS 4 LL NP P75 60

Silty Clay; dark brown, with pale brown, angular gravels ofSandstone, with fine grained sand, ped size 8mm, no fissures(VERTOSOL)

becoming less gravellyMPS 4 LL 35 P75 65MPS 20 LL 25 P75 60

KO 06 TERMINATED AT 1.00 mSurface Feature: flat, mature gums 15m from roadVegetation: grasses and low bushesDrainage: drains to east

NAT

B-1

B-2

B-3

B-4

B-5

0.10m

0.20m

0.30m

0.60m

STRATA

Gra

phic

Log

Moi

stur

e

Dep

th (m

)

RL

(m W

SG

84)

Cla

ssifi

catio

n

Con

sist

ency




CU

_LIB

_06.

GLB

Log

CU

BO

RE

HO

LE L

OG

U23

415_

LOG

S.G

PJ <

<Dra

win

gFile

>> 2

9/11

/201

2 14

:52

8.3

0.00

3 D

evel

oped

by

Dat

gel



Sheet : 1 of 1


Client : Waratah CoalProject : Waratah Coal Mapping GalileeBasinJob No : U23415Site : China First Coal MineLocation : Kia Ora - Bimble BoxCH31.7km

Sup

port

Met

hod

& B

it

TestingSampling

DRILLING


very stiffhard

very looseloose

medium densedense

very dense

DMW

DryMoistWet

MPSLLP75


TC bitDiamond



CasingMud

Nil

UDNPPBESLABDUPSPLIT





Split Sample

RBVTD

VSSFStVStHVLLMDDVD

AWPHCRV

AugerWashbore

PercussionHammer


Vibrocore

CMN

0.5

1.0

329.5

329.0


215215

WARATAH COAL CHINAS FIRST COAL MINE

22 November 2012 Cardno 9

`

Photo 1 KO 1 – Typical surface features

Photo 2 KO 1 – Soil profile 0.0 – 1.0m


216


22 November 2012 Cardno 10Photo 5 KO 2 - Soil profile on Auger

Photo 3 KO 2 – Typical Surface Features

KO 2 – Soil Profile

Photo 4 KO 2 - Soil Profile0.0 – 1.0m

Photo 3 KO 2 – Typical Surface Features


217217




Photo 7 KO 3 – Soil Profile 0.0 – 1.0m


218






219219






220






221221



Photo 14 BB 8 – Typical surface features

Photo 15 BB 8 – Soil Profile 0.0 – 1.0m


222






223223






224



Photo 20 BB 11 – Typical surface features (Notice ant hills)



225225






226




Photo 25 BB KO 13 – Soil Profile 0.0 – 1.0m


227227






228



Photo 28 BB 15 – Typical surface features (Notice ant hill in the distance)



229229






230






231231






232






233233






234



APPENDIX B

Physical Test Results


235235

ULLMAN & NOLAN UNGR 1 G

Technical Services Pty Ltd (-/12/05)

A.C.N. 103 205 205REPORT ON SOIL CLASSIFICATION

Sheet 1 of 1 Mackay Laboratory

CLIENT: Waratah Coal JOB NO: U23415 LAB REF NO: 12-6901ABC

PROJECT: China First Coal Mine SAMPLED BY: CUNG DATE: 1.11.12

LOCATION: Glenn Innis TESTED BY: DATE: 2.11.12

MATERIAL: Bimble Box 7, Depth 0.30-0.60m CHECKED BY: NJR DATE: 7.11.12

TEST PROCEDURES: AS 1289.3.1.1,3.2.1,3.3.1,3.4.1,3.6.1,3.8.1 CLIENT REF: -2 0 1 0 0 -2 0 0 -2 0 0 -2 0 0 0 -2 0 02 ## 1 ## 0 ## 0 0 ## 0 0 ## 0 # 0 # 0 ##5 0 0 05 ## 0 ##7 0 0 07 ## 0 ##

10 0 0 010 ## 0 ##13 0 0 -213 ## 0 ##19 0 0 019 ## 0 ##27 0 0 -227 ## 0 ##38 0 0 038 ## 0 ##53 0 0 -253 ## 0 ##75 0 0 075 ## clay silt sand gravel cobbles 0 ##

1 0 fine medium coarse fine medium coarse fine medium coarse 0 01 ## ... ... ... ... ... ... ... ... 0 ##

Particle Percent Particle Percent Liquid Plastic Plasticity Linear Soil Particle

Size Passing Size Passing Limit Limit Index Shrinkage Density

(mm) (%) (mm) (%) (%) (%) (%) (%) (g/cm3)150.0 Not Obtainable Non Determinable Non Plastic - -75.0 Classification: Silty Sand

37.5 100 (SP)19.0 100

9.5 100 Emerson Class No. 2 Type of Water: Distilled Temperature of Water: 23°C

4.75 100 Preparation History of Atterberg Limits

2.36 100 Sample : Natural/Air Dried/Oven Accredited No. 910

1.18 92 Sieved: Wet/dry Certificate No. 12-6901A

0.600 80 Date of Issue 7.11.12

0.425 73 Linear Shrinkage Data

0.300 65 Length of Mould (mm) :

0.150 44 Sample: -0.075 22

KC,LH

252

0.00

1

0.00

2

0.00

4

0.00

6

0.00

80.

01

0.02

0.04

0.06

0.6

0.08

0.10

0.07

5

0.15

0

0.30

0

0.42

5

1.0

1.18

2.36

4.75

6.70 9.5

10

13.2

19.0

26.5

37.5

53.0

75.0

150.

0

100

clayfine

silt

medium coarse fine

sand

medium coarse fine

gravel

medium coarsecobbles

0

10

20

30

40

50

60

70

80

90

100

Per

cent

fine

r tha

n si

ze

Particle size - (mm)

A.S. Metric Sieve - (mm)

022 20 0 0 031 27

This document is issued in accordance with NATA's accreditation requirements.

Authorised Signatory ....................................................................


236






PROJECT: China's First Coal Mine SAMPLED BY: CUNG DATE: 1.11.12

LOCATION: Glenn Innis TESTED BY: DATE: 2-6.11.12

MATERIAL: Bimble Box 10, depth 0.10-0.20m CHECKED BY: NJR DATE: 7.11.12

TEST PROCEDURES: AS 1289.3.1.1,3.2.1,3.3.1,3.4.1,3.6.1,2.1.1,3.8.1 CLIENT REF: -2 0 1 0 0 -2 0 0 -2 0 0 -2 0 0 0 -2 0 02 ## 1 ## 0 ## 0 0 ## 0 0 ## 0 # 0 # 0 ##5 0 0 05 ## 0 ##7 0 0 07 ## 0 ##






37.5 100 (SP)19.0 100





0.600 87 Date of Issue 7.11.12



0.150 41 Sample: -0.075 23

KC,LH

252

0.00

1

0.00

2

0.00

4

0.00

6

0.00

80.

01

0.02

0.04

0.06

0.6

0.08

0.10

0.07

5

0.15

0

0.30

0

0.42

5

1.0

1.18

2.36

4.75

6.70 9.5

10

13.2

19.0

26.5

37.5

53.0

75.0

150.

0

100

clayfine

silt

medium coarse fine

sand

medium coarse fine

gravel


0

10

20

30

40

50

60

70

80

90

100

Per

cent

fine

r tha

n si

ze



023 13 0 0 030 34




237237







LOCATION: Glenn Innis TESTED BY: DATE: 2-6.11.12

MATERIAL: Bimble Box 11, Depth 0.20-0.30m CHECKED BY: NJR DATE: 7.11.12







37.5 100 (SP)19.0 100





0.600 93 Date of Issue 7.11.12



0.150 41 Sample: -0.075 21

KC,LH

252

0.00

1

0.00

2

0.00

4

0.00

6

0.00

80.

01

0.02

0.04

0.06

0.6

0.08

0.10

0.07

5

0.15

0

0.30

0

0.42

5

1.0

1.18

2.36

4.75

6.70 9.5

10

13.2

19.0

26.5

37.5

53.0

75.0

150.

0

100

clayfine

silt

medium coarse fine

sand

medium coarse fine

gravel


0

10

20

30

40

50

60

70

80

90

100

Per

cent

fine

r tha

n si

ze



021 7 0 0 034 38




238







LOCATION: Monklands Road TESTED BY: DATE: 2-6.11.12

MATERIAL: KO 2, Depth 0.30-0.60m CHECKED BY: NJR DATE: 7.11.12







37.5 100 (SP)19.0 100





0.600 94 Date of Issue 7.11.12



0.150 41 Sample: -0.075 21

KC,LH

252

0.00

1

0.00

2

0.00

4

0.00

6

0.00

80.

01

0.02

0.04

0.06

0.6

0.08

0.10

0.07

5

0.15

0

0.30

0

0.42

5

1.0

1.18

2.36

4.75

6.70 9.5

10

13.2

19.0

26.5

37.5

53.0

75.0

150.

0

100

clayfine

silt

medium coarse fine

sand

medium coarse fine

gravel


0

10

20

30

40

50

60

70

80

90

100

Per

cent

fine

r tha

n si

ze



021 6 0 0 033 40




239239







LOCATION: Monklands Road TESTED BY: DATE: 2-6.11.12

MATERIAL: KO 5, Depth 0.10-0.20m CHECKED BY: NJR DATE: 7.11.12







37.5 100 (SP)19.0 100





0.600 89 Date of Issue 7.11.12



0.150 42 Sample: -0.075 27

KC,LH

252

0.00

1

0.00

2

0.00

4

0.00

6

0.00

80.

01

0.02

0.04

0.06

0.6

0.08

0.10

0.07

5

0.15

0

0.30

0

0.42

5

1.0

1.18

2.36

4.75

6.70 9.5

10

13.2

19.0

26.5

37.5

53.0

75.0

150.

0

100

clayfine

silt

medium coarse fine

sand

medium coarse fine

gravel


0

10

20

30

40

50

60

70

80

90

100

Per

cent

fine

r tha

n si

ze



027 11 0 0 027 35




240



APPENDIX C

Chemical Test Results


241241

EB

12

29

10

3

Fa

lse

2 2

.00

Tru

e

En

vir

on

men

tal

Div

isio

n

CE

RT

IFIC

AT

E O

F A

NA

LY

SIS

Wo

rk O

rder

:E

B1

22

91

03

Page

:1

of 7

::

Labora

tory

Clie

nt

En

viro

nm

en

tal D

ivis

ion

Brisb

an

eC

AR

DN

O U

LL

MA

N &

NO

LA

N G

EO

TE

CH

NIC

PT

Y L

TD

::

Co

nta

ctC

on

tact

MR

AN

DR

EW

WIL

LIA

MS

Cu

sto

me

r S

erv

ice

s

::

Addre

ssA

ddre

ss7

1 C

ON

NO

RS

RO

AD

MA

CK

AY

QL

D,

AU

ST

RA

LIA

47

40

32

Sh

an

d S

tre

et

Sta

ffo

rd Q

LD

Au

stra

lia 4

05

3

::

E-m

ail

E-m

ail

so

ils@

ca

rdn

o.c

om

.au

Brisb

an

e.E

nvi

ro.S

erv

ice

s@a

lsg

lob

al.co

m

::

Tele

phone

Tele

phone

+6

1 4

95

25

25

5+

61

7 3

24

3 7

22

2

::

Facs

imile

Facs

imile

+6

1 0

7 4

95

25

45

5+

61

7 3

24

3 7

21

8

:P

roje

ctU

23

41

5Q

C L

eve

l:

NE

PM

19

99

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

:O

rder

num

ber

UN

62

67

:C

-O-C

num

ber

----

Date

Sam

ple

s R

ece

ived

:0

5-N

OV

-20

12

Sam

ple

r:

----

Issu

e D

ate

:1

4-N

OV

-20

12

Site

:--

--

22

:N

o. of sa

mple

s re

ceiv

ed

Quote

num

ber

:E

N/0

24

/11

22

:N

o. of sa

mple

s analy

sed

Th

is

rep

ort

su

pe

rse

de

s

an

y p

revi

ou

s re

po

rt(s

) w

ith

this

re

fere

nce

. R

esu

lts

ap

ply

to

th

e

sam

ple

(s)

as

sub

mitt

ed

. A

ll p

ag

es

of

this

re

po

rt

ha

ve

be

en

ch

eck

ed

a

nd

a

pp

rove

d

for

rele

ase

.

Th

is C

ert

ific

ate

of

An

aly

sis

con

tain

s th

e f

ollo

win

g in

form

atio

n:

l

Ge

ne

ral C

om

me

nts

l

An

aly

tica

l Re

su

lts

NA

TA

Acc

redite

d L

abora

tory

825

Acc

redite

d for

com

plia

nce w

ith

ISO

/IE

C 1

7025.

Sig

nato

ries

Th

is

do

cu

me

nt

ha

s b

ee

n

ele

ctro

nic

ally

si

gn

ed

b

y th

e

au

tho

rize

d

sig

na

torie

s in

dic

ate

d

be

low

. E

lect

ron

ic

sig

nin

g

ha

s b

ee

n

carr

ied

ou

t in

co

mp

lian

ce w

ith p

roce

du

res

spe

cifie

d in

21

CF

R P

art

11

.

Sig

na

torie

sA

ccre

dita

tio

n C

ate

go

ryP

osi

tion

Gre

g V

og

el

La

bo

rato

ry M

an

ag

er

Brisb

an

e I

no

rga

nic

s

Kim

McC

ab

eS

en

ior

Ino

rga

nic

Ch

em

ist

Brisb

an

e I

no

rga

nic

s

En

viro

nm

en

tal D

ivis

ion

Brisb

an

e A

BN

84

00

9 9

36

02

9 P

art

of

the

AL

S G

rou

p

A

Ca

mp

be

ll B

roth

ers

Lim

ited

Co

mp

an

y

Ad

dre

ss 3

2 S

ha

nd

Str

ee

t S

taff

ord

QL

D A

ust

ralia

40

53 | P

HO

NE

+

61-7

-3243 7

222 | F

acsim

ile

+

61

-7-3

24

3 7

21

8


242

2 o

f 7

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Gen

era

l C

om

men

ts

The

analy

tical

pro

cedure

s use

d

by

the

Environm

enta

l D

ivis

ion

have

been

deve

loped

from

est

ablis

hed

inte

rnatio

nally

re

cogniz

ed

pro

cedure

s

such

as

those

publis

hed

by

the

US

EP

A,

AP

HA

, A

S

and

NE

PM

. In

house

deve

loped p

roce

dure

s are

em

plo

yed in

the a

bse

nce

of docu

mente

d s

tandard

s or

by

clie

nt re

quest

.

Where

mois

ture

dete

rmin

ation h

as

been p

erf

orm

ed, re

sults

are

report

ed o

n a

dry

weig

ht basi

s.

Where

a r

eport

ed le

ss than (

<)

resu

lt is

hig

her

than the L

OR

, th

is m

ay

be d

ue to p

rim

ary

sam

ple

ext

ract

/dig

est

ate

dilu

tion a

nd/o

r in

suffic

ient sa

mple

for

analy

sis

.

Where

the L

OR

of a r

eport

ed r

esu

lt d

iffe

rs fro

m s

tandard

LO

R, th

is m

ay b

e d

ue to h

igh m

ois

ture

conte

nt, in

suffic

ient sa

mple

(re

duce

d w

eig

ht em

plo

yed)

or

matr

ix in

terf

ere

nce

.

When s

am

plin

g tim

e in

form

atio

n is

not pro

vid

ed b

y th

e c

lient, s

am

plin

g d

ate

s are

show

n w

ithout a tim

e c

om

ponent. In

these

inst

ance

s, the tim

e c

om

ponent has

been a

ssum

ed b

y th

e la

bora

tory

for

pro

cess

ing p

urp

ose

s.

CA

S N

um

ber

= C

AS

regis

try

num

ber

from

data

base m

ain

tain

ed b

y C

hem

ical A

bst

ract

s S

erv

ices.

The C

hem

ical A

bst

ract

s S

erv

ice is

a d

ivis

ion o

f th

e A

merica

n C

hem

ical S

oci

ety

.

LO

R =

Lim

it of re

port

ing

^ =

This

resu

lt is

com

pute

d fro

m in

div

idual a

naly

te d

ete

ctio

ns

at or

above

the le

vel o

f re

port

ing

Key

:


243243

3 o

f 7

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

An

aly

tical R

esu

lts

KO

4 0

.2-0

.3m

KO

3 0

.6-1

.0m

KO

2 0

.6-1

.0m

KO

1 0

.2-0

.3m

KO

1 0

.1-0

.2M

Clie

nt

sam

ple

ID

Sub-M

atr

ix:

SO

IL (

Matr

ix:

SO

IL)

29-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

0C

lien

t sa

mp

ling

da

te /

tim

e

EB

12

29

10

3-0

05

EB

12

29

10

3-0

04

EB

12

29

10

3-0

03

EB

1229103-0

02

EB

1229103-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

EA

002 :

pH

(S

oils)

pH

Valu

e7.1

6.9

6.5

8.2

7.1

pH

Unit

0.1

----

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

So

diu

m A

dso

rpti

on

Rati

o0.8

61.1

60

.39

31

.71

.43

-0.0

1--

--

EA

010:

Co

nd

ucti

vit

y

Ele

ctr

ical C

on

du

cti

vit

y @

25°C

17

16

53

69

19

µS

/cm

1--

--

EA

055:

Mo

istu

re C

on

ten

t

Mo

istu

re C

on

ten

t (d

ried

@ 1

03°C

)7.7

11.9

15

.12

5.9

2.2

%1.0

----

ED

008:

Exch

an

geab

le C

ati

on

s

Exch

an

geab

le C

alc

ium

2.0

1.7

0.7

0.7

2.8

meq/1

00g

0.1

----

Exch

an

geab

le M

ag

nesiu

m3.8

1.2

0.2

1.0

0.6

meq/1

00g

0.1

----

Exch

an

geab

le P

ota

ssiu

m0.1

0.1

<0.1

<0.1

0.2

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

0.5

<0.1

<0.1

0.9

<0.1

meq/1

00g

0.1

----

Cati

on

Exch

an

ge C

ap

acit

y6.5

3.1

1.0

2.6

3.7

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

Perc

en

t8.0

1.6

<0.1

32

.90

.3%

0.1

----

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

Ch

lori

de

<10

10

<10

45

020

mg/k

g10

16887-0

0-6


244

4 o

f 7

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

An

aly

tical R

esu

lts

BB

12 0

.6-1

.0m

BB

12 0

.3-0

.6m

BB

15 0

.2-0

.3m

BB

15-0

.6-1

.0m

KO

5 0

.3-0

.6m

Clie

nt

sam

ple

ID

Sub-M

atr

ix:

SO

IL (

Matr

ix:

SO

IL)

29-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

0C

lien

t sa

mp

ling

da

te /

tim

e

EB

12

29

10

3-0

10

EB

12

29

10

3-0

09

EB

12

29

10

3-0

08

EB

1229103-0

07

EB

1229103-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

EA

002 :

pH

(S

oils)

pH

Valu

e7.5

8.8

5.9

8.4

9.0

pH

Unit

0.1

----

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

So

diu

m A

dso

rpti

on

Rati

o1.4

865.6

0.2

62

.85

18

.7-

0.0

1--

--

EA

010:

Co

nd

ucti

vit

y

Ele

ctr

ical C

on

du

cti

vit

y @

25°C

29

481

542

11

9µ

S/c

m1

----

EA

055:

Mo

istu

re C

on

ten

t

Mo

istu

re C

on

ten

t (d

ried

@ 1

03°C

)8.0

19.8

14

.81

0.5

18

.6%

1.0

----

ED

008:

Exch

an

geab

le C

ati

on

s

Exch

an

geab

le C

alc

ium

5.1

3.1

0.4

1.5

1.7

meq/1

00g

0.1

----

Exch

an

geab

le M

ag

nesiu

m4.1

1.4

0.3

1.0

1.6

meq/1

00g

0.1

----

Exch

an

geab

le P

ota

ssiu

m0.2

<0.1

<0.1

0.1

<0.1

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

0.2

1.1

<0.1

0.5

1.2

meq/1

00g

0.1

----

Cati

on

Exch

an

ge C

ap

acit

y9.6

5.6

0.8

3.2

4.6

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

Perc

en

t2.1

18.8

<0.1

16

.127

.5%

0.1

----

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

Ch

lori

de

20

480

<10

30

80

mg/k

g10

16887-0

0-6


245245

5 o

f 7

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

An

aly

tical R

esu

lts

BB

13 0

.6-0

.75m

BB

09 0

.1-0

.2m

BB

10 0

.3-0

.6m

BB

11 0

.0-0

.1m

BB

07 0

.1-0

.2m

Clie

nt

sam

ple

ID

Sub-M

atr

ix:

SO

IL (

Matr

ix:

SO

IL)

29-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

0C

lien

t sa

mp

ling

da

te /

tim

e

EB

12

29

10

3-0

15

EB

12

29

10

3-0

14

EB

12

29

10

3-0

13

EB

1229103-0

12

EB

1229103-0

11

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

EA

002 :

pH

(S

oils)

pH

Valu

e6.1

6.4

8.4

6.2

7.0

pH

Unit

0.1

----

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

So

diu

m A

dso

rpti

on

Rati

o0.1

70.2

71

6.8

0.8

90

.47

-0.0

1--

--

EA

010:

Co

nd

ucti

vit

y

Ele

ctr

ical C

on

du

cti

vit

y @

25°C

74

16

813

10

µS

/cm

1--

--

EA

055:

Mo

istu

re C

on

ten

t

Mo

istu

re C

on

ten

t (d

ried

@ 1

03°C

)14.8

10.7

11

.21

6.0

13

.0%

1.0

----

ED

008:

Exch

an

geab

le C

ati

on

s

Exch

an

geab

le C

alc

ium

1.1

0.6

1.0

1.4

2.1

meq/1

00g

0.1

----

Exch

an

geab

le M

ag

nesiu

m0.4

0.2

1.6

0.5

1.2

meq/1

00g

0.1

----

Exch

an

geab

le P

ota

ssiu

m<

0.1

<0.1

0.1

0.2

0.2

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

<0.1

<0.1

0.8

<0.1

<0.1

meq/1

00g

0.1

----

Cati

on

Exch

an

ge C

ap

acit

y1.6

0.8

3.6

2.1

3.6

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

Perc

en

t<

0.1

<0.1

23

.7<

0.1

2.2

%0.1

----

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

Ch

lori

de

<10

<10

13

0<

10

<10

mg/k

g10

16887-0

0-6


246

6 o

f 7

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

An

aly

tical R

esu

lts

BB

6 0

.2-0

.3m

BB

20 0

.0-0

.1m

BB

16 0

.6-1

.0m

BB

17 0

.6-1

.0m

BB

19 0

.2-0

.3m

Clie

nt

sam

ple

ID

Sub-M

atr

ix:

SO

IL (

Matr

ix:

SO

IL)

29-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

0C

lien

t sa

mp

ling

da

te /

tim

e

EB

12

29

10

3-0

20

EB

12

29

10

3-0

19

EB

12

29

10

3-0

18

EB

1229103-0

17

EB

1229103-0

16

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

EA

002 :

pH

(S

oils)

pH

Valu

e7.5

6.2

6.1

6.2

6.3

pH

Unit

0.1

----

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

So

diu

m A

dso

rpti

on

Rati

o1.7

44.2

82

.44

1.4

92

.02

-0.0

1--

--

EA

010:

Co

nd

ucti

vit

y

Ele

ctr

ical C

on

du

cti

vit

y @

25°C

31

84

41

7µ

S/c

m1

----

EA

055:

Mo

istu

re C

on

ten

t

Mo

istu

re C

on

ten

t (d

ried

@ 1

03°C

)23.6

1.5

17

.314

.02

.5%

1.0

----

ED

008:

Exch

an

geab

le C

ati

on

s

Exch

an

geab

le C

alc

ium

2.1

1.2

0.6

0.9

1.0

meq/1

00g

0.1

----

Exch

an

geab

le M

ag

nesiu

m2.8

0.4

0.3

0.2

0.7

meq/1

00g

0.1

----

Exch

an

geab

le P

ota

ssiu

m0.3

0.1

<0.1

0.1

0.1

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

0.3

<0.1

<0.1

<0.1

<0.1

meq/1

00g

0.1

----

Cati

on

Exch

an

ge C

ap

acit

y5.5

1.6

1.0

1.2

1.8

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

Perc

en

t6.1

1.1

<0.1

<0.1

4.8

%0.1

----

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

Ch

lori

de

20

<10

<10

<10

20

mg/k

g10

16887-0

0-6


247247

7 o

f 7

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

An

aly

tical R

esu

lts

----

----

----

BB

18 0

.0-0

.1m

BB

6 0

.3-0

.6m

Clie

nt

sam

ple

ID

Sub-M

atr

ix:

SO

IL (

Matr

ix:

SO

IL)

----

----

----

29-O

CT

-2012 1

5:0

029-O

CT

-2012 1

5:0

0C

lien

t sa

mp

ling

da

te /

tim

e

----

----

----

EB

1229103-0

22

EB

1229103-0

21

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

EA

002 :

pH

(S

oils)

pH

Valu

e6.5

9.4

----

----

----

pH

Unit

0.1

----

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

So

diu

m A

dso

rpti

on

Rati

o0.3

035.0

----

----

----

-0.0

1--

--

EA

010:

Co

nd

ucti

vit

y

Ele

ctr

ical C

on

du

cti

vit

y @

25°C

6257

----

----

----

µS

/cm

1--

--

EA

055:

Mo

istu

re C

on

ten

t

Mo

istu

re C

on

ten

t (d

ried

@ 1

03°C

)17.7

17.0

----

----

----

%1.0

----

ED

008:

Exch

an

geab

le C

ati

on

s

Exch

an

geab

le C

alc

ium

1.2

21.7

----

----

----

meq/1

00g

0.1

----

Exch

an

geab

le M

ag

nesiu

m0.2

6.1

----

----

----

meq/1

00g

0.1

----

Exch

an

geab

le P

ota

ssiu

m<

0.1

0.3

----

----

----

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

<0.1

1.1

----

----

----

meq/1

00g

0.1

----

Cati

on

Exch

an

ge C

ap

acit

y1.5

29.2

----

----

----

meq/1

00g

0.1

----

Exch

an

geab

le S

od

ium

Perc

en

t<

0.1

3.7

----

----

----

%0.1

----

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

Ch

lori

de

<10

70

----

----

----

mg/k

g10

16887-0

0-6


248

Fa

lse

En

vir

on

men

tal D

ivis

ion

QU

AL

ITY

CO

NT

RO

L R

EP

OR

TW

ork

Ord

er

:E

B1

22

91

03

Page

:1

of 5

::

Labora

tory

Clie

nt

En

viro

nm

en

tal D

ivis

ion

Brisb

an

eC

AR

DN

O U

LL

MA

N &

NO

LA

N G

EO

TE

CH

NIC

PT

Y L

TD

::

Co

nta

ctC

on

tact

MR

AN

DR

EW

WIL

LIA

MS

Cu

sto

me

r S

erv

ice

s

::

Addre

ssA

ddre

ss7

1 C

ON

NO

RS

RO

AD

MA

CK

AY

QL

D,

AU

ST

RA

LIA

47

40

32

Sh

an

d S

tre

et

Sta

ffo

rd Q

LD

Au

stra

lia 4

05

3

::

E-m

ail

E-m

ail

so

ils@

card

no

.co

m.a

uB

risb

an

e.E

nvi

ro.S

erv

ice

s@a

lsg

lob

al.co

m

::

Tele

phone

Tele

phone

+6

1 4

95

25

25

5+

61

7 3

24

3 7

22

2

::

Facs

imile

Facsi

mile

+6

1 0

7 4

95

25

45

5+

61

7 3

24

3 7

21

8

:P

roje

ctU

23

41

5Q

C L

eve

l:

NE

PM

19

99

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

Site

:--

--

:C

-O-C

num

ber

----

Date

Sam

ple

s R

ece

ived

:0

5-N

OV

-20

12

Sam

ple

r:

----

Issu

e D

ate

:1

4-N

OV

-20

12

:O

rder

num

ber

UN

62

67

22

:N

o. of sa

mple

s re

ceiv

ed

Quote

num

ber

:E

N/0

24

/11

22

:N

o. of sa

mple

s analy

sed

Th

is

rep

ort

su

pe

rse

de

s a

ny

pre

vio

us

rep

ort

(s)

with

th

is

refe

ren

ce

. R

esu

lts

ap

ply

to

th

e

sam

ple

(s)

as

sub

mitt

ed

. A

ll p

ag

es

of

this

re

po

rt

ha

ve

be

en

ch

eck

ed

a

nd

a

pp

rove

d

for

rele

ase

.

Th

is Q

ua

lity C

on

tro

l R

ep

ort

co

nta

ins t

he

fo

llow

ing

in

form

atio

n:

l

Labora

tory

Duplic

ate

(D

UP

) R

eport

; R

ela

tive P

erc

enta

ge D

iffere

nce

(R

PD

) and A

ccepta

nce

Lim

its

l

Meth

od B

lank

(MB

) and L

abora

tory

Contr

ol S

pik

e (

LC

S)

Report

; R

eco

very

and A

ccepta

nce

Lim

its

l

Matr

ix S

pik

e (

MS

) R

eport

; R

eco

very

and A

ccepta

nce

Lim

its

NA

TA

Accr

edited L

abora

tory

825

Acc

redite

d for

com

plia

nce

with

ISO

/IE

C 1

7025.

Sig

nato

ries

Th

is

do

cum

en

t h

as

be

en

e

lect

ron

ica

lly

sig

ne

d

by

the

a

uth

orize

d

sig

na

torie

s in

dic

ate

d

be

low

. E

lect

ron

ic

sig

nin

g

ha

s b

ee

n

ca

rrie

d o

ut

in c

om

plia

nce

with

pro

ced

ure

s sp

eci

fied

in 2

1 C

FR

Pa

rt 1

1.

Sig

na

torie

sA

ccre

dita

tio

n C

ate

go

ryP

osi

tion

Gre

g V

og

el

La

bo

rato

ry M

an

ag

er

Brisb

an

e I

no

rga

nic

s

Kim

McC

ab

eS

en

ior

Ino

rga

nic

Ch

em

ist

Brisb

an

e I

no

rga

nic

s

Ad

dre

ss 3

2 S

ha

nd

Str

ee

t S

taff

ord

QL

D A

ust

ralia

40

53 | P

HO

NE

+

61-7

-3243 7

222 | F

acsim

ile

+

61

-7-3

24

3 7

21

8

En

viro

nm

en

tal D

ivis

ion

Brisb

an

e A

BN

84

00

9 9

36

02

9 P

art

of

the

AL

S G

rou

p

A

Ca

mp

be

ll B

roth

ers

Lim

ited

Co

mp

an

y


249249

2 o

f 5

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Gen

era

l C

om

men

ts

The

analy

tical

pro

cedure

s

used

by

the

Envi

ronm

enta

l D

ivis

ion

have

been

deve

loped

from

est

ablis

hed

inte

rnatio

nally

re

cogniz

ed

pro

cedure

s su

ch

as

those

publis

hed

by

the

US

EP

A,

AP

HA

, A

S

and

NE

PM

. In

house

deve

loped p

roce

dure

s are

em

plo

yed in

the a

bse

nce

of docu

mente

d s

tandard

s or

by

clie

nt re

quest

.

Where

mois

ture

dete

rmin

atio

n h

as

been p

erf

orm

ed, re

sults

are

report

ed o

n a

dry

weig

ht basi

s.

Where

a r

eport

ed le

ss than (

<)

resu

lt is

hig

her

than the L

OR

, th

is m

ay

be d

ue to p

rim

ary

sam

ple

ext

ract

/dig

est

ate

dilu

tion a

nd/o

r in

suffic

ient sa

mple

for

analy

sis.

Where

the L

OR

of a r

eport

ed r

esu

lt d

iffers

fro

m s

tandard

LO

R, th

is m

ay

be d

ue to h

igh m

ois

ture

conte

nt, in

suffic

ient sa

mple

(re

duce

d w

eig

ht em

plo

yed)

or

matr

ix in

terf

ere

nce

.

Anonym

ous =

Refe

rs to s

am

ple

s w

hic

h a

re n

ot sp

ecifi

cally

part

of th

is w

ork

ord

er

but fo

rmed p

art

of th

e Q

C p

roce

ss lo

t

CA

S N

um

ber

= C

AS

regis

try

num

ber

from

data

base

main

tain

ed b

y C

hem

ical A

bst

ract

s S

erv

ices.

The C

hem

ical A

bst

ract

s S

erv

ice is

a d

ivis

ion o

f th

e A

merica

n C

hem

ical S

oci

ety

.

LO

R =

Lim

it of re

port

ing

RP

D =

Rela

tive P

erc

enta

ge D

iffere

nce

# =

Indic

ate

s faile

d Q

C

Key :


250

3 o

f 5

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Lab

ora

tory

Du

plicate

(D

UP

) R

ep

ort

The

qualit

y contr

ol

term

Labora

tory

D

uplic

ate

re

fers

to

a

random

ly

sele

cted

intr

ala

bora

tory

sp

lit.

Labora

tory

duplic

ate

s pro

vide

info

rmatio

n

regard

ing

meth

od

pre

cisi

on

and

sam

ple

hete

rogeneity

. T

he

perm

itted

ranges

for

the

Rela

tive

P

erc

ent

Devi

ation

(RP

D)

of

Labora

tory

D

uplic

ate

s are

sp

eci

fied

in

ALS

M

eth

od

QW

I-E

N/3

8 a

nd

are

dependent

on

the

magnitu

de

of

resu

lts

in

com

pariso

n

to

the

leve

l of

report

ing:

Resu

lt <

10 t

imes

LO

R:-

No L

imit;

Resu

lt betw

een 1

0 a

nd 2

0 tim

es L

OR

:- 0

% -

50%

; R

esu

lt >

20 tim

es

LO

R:-

0%

- 2

0%

.

Sub-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

ca

te (

DU

P)

Re

po

rt

Ori

gin

al

Re

su

ltR

PD

(%

)L

ab

ora

tory

sa

mp

le I

DC

lie

nt

sa

mp

le I

DM

eth

od:

Co

mp

ou

nd

CA

S N

um

be

rL

OR

Un

itD

up

lic

ate

Re

su

ltR

ec

ov

ery

Lim

its

(%

)

EA

002 :

pH

(S

oils)

(Q

C L

ot:

2587414)

EA

002: pH

Valu

e--

--0.1

pH

Unit

6.9

6.7

2.5

0%

- 2

0%

KO

1 0

.1-0

.2M

EB

1229103-0

01

EA

002: pH

Valu

e--

--0.1

pH

Unit

6.4

6.4

0.0

0%

- 2

0%

BB

07 0

.1-0

.2m

EB

1229103-0

11

EA

002 :

pH

(S

oils)

(Q

C L

ot:

2587421)

EA

002: pH

Valu

e--

--0.1

pH

Unit

9.4

9.5

0.0

0%

- 2

0%

BB

6 0

.3-0

.6m

EB

1229103-0

21

EA

010:

Co

nd

ucti

vit

y (Q

C L

ot:

2587415)

EA

010: E

lect

rica

l Conduct

ivity

@ 2

5°C

----

1µ

S/c

m16

17

6.1

0%

- 5

0%

KO

1 0

.1-0

.2M

EB

1229103-0

01

EA

010: E

lect

rica

l Conduct

ivity

@ 2

5°C

----

1µ

S/c

m4

328.6

No L

imit

BB

07 0

.1-0

.2m

EB

1229103-0

11

EA

010:

Co

nd

ucti

vit

y (Q

C L

ot:

2587422)

EA

010: E

lect

rica

l Conduct

ivity

@ 2

5°C

----

1µ

S/c

m257

251

2.4

0%

- 2

0%

BB

6 0

.3-0

.6m

EB

1229103-0

21

EA

055:

Mo

istu

re C

on

ten

t (

QC

Lo

t: 2

587386)

EA

055-1

03: M

ois

ture

Conte

nt (d

ried @

103°C

)--

--1.0

%2.0

2.2

8.0

No L

imit

Anonym

ous

EB

1229036-0

16

EA

055-1

03: M

ois

ture

Conte

nt (d

ried @

103°C

)--

--1.0

%15.1

15.2

1.2

0%

- 5

0%

KO

2 0

.6-1

.0m

EB

1229103-0

03

EA

055:

Mo

istu

re C

on

ten

t (

QC

Lo

t: 2

587387)

EA

055-1

03: M

ois

ture

Conte

nt (d

ried @

103°C

)--

--1.0

%1.5

1.5

0.0

No L

imit

BB

19 0

.2-0

.3m

EB

1229103-0

16

ED

008:

Exch

an

geab

le C

ati

on

s (Q

C L

ot:

2591351)

ED

008: E

xch

angeable

Calc

ium

----

0.1

meq/1

00g

1.7

1.8

7.3

0%

- 5

0%

KO

1 0

.1-0

.2M

EB

1229103-0

01

ED

008: E

xchangeable

Magnesi

um

----

0.1

meq/1

00g

1.2

1.3

0.0

0%

- 5

0%

ED

008: E

xchangeable

Pota

ssiu

m--

--0.1

meq/1

00g

0.1

0.1

0.0

No L

imit

ED

008: E

xchangeable

Sodiu

m--

--0.1

meq/1

00g

<0.1

<0.1

0.0

No L

imit

ED

008: E

xchangeable

Calc

ium

----

0.1

meq/1

00g

1.5

1.4

8.7

0%

- 5

0%

BB

12 0

.3-0

.6m

EB

1229103-0

09

ED

008: E

xchangeable

Magnesi

um

----

0.1

meq/1

00g

1.0

1.0

10.0

0%

- 5

0%

ED

008: E

xchangeable

Pota

ssiu

m--

--0.1

meq/1

00g

0.1

<0.1

0.0

No L

imit

ED

008: E

xchangeable

Sodiu

m--

--0.1

meq/1

00g

0.5

0.5

0.0

No L

imit

ED

008:

Exch

an

geab

le C

ati

on

s (Q

C L

ot:

2591353)

ED

008: E

xch

angeable

Calc

ium

----

0.1

meq/1

00g

21.7

22.0

1.4

0%

- 2

0%

BB

6 0

.3-0

.6m

EB

1229103-0

21

ED

008: E

xchangeable

Magnesi

um

----

0.1

meq/1

00g

6.1

6.1

0.0

0%

- 2

0%

ED

008: E

xchangeable

Pota

ssiu

m--

--0.1

meq/1

00g

0.3

0.3

0.0

No L

imit

ED

008: E

xchangeable

Sodiu

m--

--0.1

meq/1

00g

1.1

1.0

0.0

0%

- 5

0%

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

(Q

C L

ot:

2587416)

ED

045G

: C

hlo

ride

16887-0

0-6

10

mg/k

g10

20

0.0

No L

imit

KO

1 0

.1-0

.2M

EB

1229103-0

01

ED

045G

: C

hlo

ride

16887-0

0-6

10

mg/k

g<

10

<10

0.0

No L

imit

BB

07 0

.1-0

.2m

EB

1229103-0

11

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

(Q

C L

ot:

2587423)

ED

045G

: C

hlo

ride

16887-0

0-6

10

mg/k

g70

60

0.0

No L

imit

BB

6 0

.3-0

.6m

EB

1229103-0

21


251251

4 o

f 5

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

The

qualit

y co

ntr

ol

term

M

eth

od

/ Labora

tory

B

lank

refe

rs

to

an

analy

te

free

matr

ix

to

whic

h

all

reagents

are

added

in

the

sam

e

volu

mes

or

pro

port

ions

as

use

d

in

standard

sa

mple

pre

para

tion.

The

purp

ose

of

this

Q

C

para

mete

r is

to

m

onito

r pote

ntia

l la

bora

tory

co

nta

min

ation.

The

qualit

y co

ntr

ol

term

Labora

tory

C

ontr

ol

Sam

ple

(L

CS

) re

fers

to

a

cert

ified

refe

rence

m

ate

rial,

or

a

know

n

inte

rfere

nce

fr

ee

matr

ix

spik

ed

with

ta

rget

analy

tes.

The p

urp

ose

of th

is Q

C p

ara

mete

r is

to m

onito

r m

eth

od p

reci

sion a

nd a

ccura

cy in

dependent of sa

mple

matr

ix. D

ynam

ic R

eco

very

Lim

its a

re b

ase

d o

n s

tatis

tical e

valu

atio

n o

f pro

cess

ed L

CS

.

Sub-M

atr

ix:

SO

ILM

eth

od

Bla

nk

(M

B)

Re

po

rt

La

bo

rato

ry C

on

tro

l S

pik

e (

LC

S)

Re

po

rt

Sp

ike

Sp

ike

Re

co

ve

ry (

%)

Re

co

ve

ry L

imit

s (

%)

Re

su

ltC

on

ce

ntr

ati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

be

rL

OR

Un

it

EA

002 :

pH

(S

oils)

(Q

CL

ot:

2587414)

EA

002: pH

Valu

e--

--0.1

pH

Unit

----

100

4.0

0 p

H U

nit

102

98

EA

002 :

pH

(S

oils)

(Q

CL

ot:

2587421)

EA

002: pH

Valu

e--

--0.1

pH

Unit

----

100

4.0

0 p

H U

nit

102

98

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

(Q

CL

ot:

2591345)

EA

006: S

odiu

m A

dso

rptio

n R

atio

----

0.0

1<

0.0

5--

----

----

----

--

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

(Q

CL

ot:

2591346)

EA

006: S

odiu

m A

dso

rptio

n R

atio

----

0.0

1<

0.0

5--

----

----

----

--

EA

010:

Co

nd

ucti

vit

y (Q

CL

ot:

2587415)

EA

010: E

lect

rica

l C

onduct

ivity

@ 2

5°C

----

1µ

S/c

m<

1100

1412 µ

S/c

m110

86

EA

010:

Co

nd

ucti

vit

y (Q

CL

ot:

2587422)

EA

010: E

lect

rica

l C

onduct

ivity

@ 2

5°C

----

1µ

S/c

m<

1100

1412 µ

S/c

m110

86

ED

008:

Exch

an

geab

le C

ati

on

s (Q

CL

ot:

2591351)

ED

008: E

xchangeable

Calc

ium

----

0.1

meq/1

00g

<0.1

100

1 m

eq/1

00g

109

91

ED

008: E

xchangeable

Magnesiu

m--

--0.1

meq/1

00g

<0.1

103

1.6

66 m

eq/1

00g

111

87

ED

008: E

xchangeable

Pota

ssi

um

----

0.1

meq/1

00g

<0.1

96.1

0.5

19 m

eq/1

00g

117

79

ED

008: E

xchangeable

Sodiu

m--

--0.1

meq/1

00g

<0.1

106

0.8

70 m

eq/1

00g

125

75

ED

008: C

atio

n E

xchange C

apaci

ty--

--0.1

meq/1

00g

<0.1

102

4.0

55 m

eq/1

00g

116

84

ED

008:

Exch

an

geab

le C

ati

on

s (Q

CL

ot:

2591353)

ED

008: E

xchangeable

Calc

ium

----

0.1

meq/1

00g

<0.1

99.3

1 m

eq/1

00g

109

91

ED

008: E

xchangeable

Magnesiu

m--

--0.1

meq/1

00g

<0.1

102

1.6

66 m

eq/1

00g

111

87

ED

008: E

xchangeable

Pota

ssi

um

----

0.1

meq/1

00g

<0.1

96.3

0.5

19 m

eq/1

00g

117

79

ED

008: E

xchangeable

Sodiu

m--

--0.1

meq/1

00g

<0.1

105

0.8

70 m

eq/1

00g

125

75

ED

008: C

atio

n E

xchange C

apaci

ty--

--0.1

meq/1

00g

<0.1

101

4.0

55 m

eq/1

00g

116

84

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

(Q

CL

ot:

2587416)

ED

045G

: C

hlo

ride

16887-0

0-6

10

mg/k

g<

10

92.7

5000 m

g/k

g115

77

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

(Q

CL

ot:

2587423)

ED

045G

: C

hlo

ride

16887-0

0-6

10

mg/k

g<

10

97.0

5000 m

g/k

g115

77

Matr

ix S

pik

e (

MS

) R

ep

ort

The

qualit

y co

ntr

ol

term

M

atr

ix

Spik

e

(MS

) re

fers

to

an

intr

ala

bora

tory

sp

lit

sam

ple

sp

iked

with

a

repre

senta

tive

set

of

targ

et

analy

tes.

T

he

purp

ose

of

this

Q

C

para

mete

r is

to

m

onito

r pote

ntia

l m

atr

ix

effect

s on

analy

te r

eco

veries.

Sta

tic R

eco

very

Lim

its a

s per

labora

tory

Data

Qualit

y O

bje

ctiv

es

(DQ

Os)

. Id

eal r

eco

very

ranges

state

d m

ay

be w

aiv

ed in

the e

vent of sam

ple

matr

ix in

terf

ere

nce

.

l

No

Matr

ix S

pik

e (

MS

) R

esu

lts a

re r

eq

uir

ed

to

be r

ep

ort

ed

.


252

5 o

f 5

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Matr

ix S

pik

e (

MS

) an

d M

atr

ix S

pik

e D

up

licate

(M

SD

) R

ep

ort

The

qualit

y co

ntr

ol

term

M

atr

ix

Spik

e

(MS

) and

Matr

ix

Spik

e

Duplic

ate

(M

SD

) re

fers

to

in

trala

bora

tory

sp

lit

sam

ple

s sp

iked

with

a

repre

senta

tive

set

of

targ

et

analy

tes.

T

he

purp

ose

of

these

Q

C

para

mete

rs

are

to

monito

r pote

ntia

l matr

ix e

ffect

s on a

naly

te r

ecove

ries.

Sta

tic

Recove

ry L

imits

as

per

labora

tory

Data

Qualit

y O

bje

ctiv

es

(DQ

Os)

. Id

eal r

eco

very

ranges

state

d m

ay

be w

aiv

ed in

the e

vent of sa

mple

matr

ix in

terf

ere

nce

.

l

No

Matr

ix S

pik

e (

MS

) o

r M

atr

ix S

pik

e D

up

licate

(M

SD

) R

esu

lts a

re r

eq

uir

ed

to

be r

ep

ort

ed

.


253253

Tru

e

En

vir

on

men

tal D

ivis

ion

INT

ER

PR

ET

IVE

QU

AL

ITY

CO

NT

RO

L R

EP

OR

TW

ork

Ord

er

:E

B1

22

91

03

Page

:1

of 8

::

Labora

tory

Clie

nt

En

viro

nm

en

tal D

ivis

ion

Brisb

an

eC

AR

DN

O U

LL

MA

N &

NO

LA

N G

EO

TE

CH

NIC

PT

Y L

TD

::

Co

nta

ctC

on

tact

MR

AN

DR

EW

WIL

LIA

MS

Cu

sto

me

r S

erv

ice

s:

:A

ddre

ssA

ddre

ss7

1 C

ON

NO

RS

RO

AD

MA

CK

AY

QL

D,

AU

ST

RA

LIA

47

40

32

Sh

an

d S

tre

et

Sta

ffo

rd Q

LD

Au

stra

lia 4

05

3

::

E-m

ail

E-m

ail

soils

@ca

rdn

o.c

om

.au

Brisb

an

e.E

nvi

ro.S

erv

ice

s@a

lsg

lob

al.co

m:

:T

ele

phone

Tele

phone

+6

1 4

95

25

25

5+

61

7 3

24

3 7

22

2:

:F

acs

imile

Facs

imile

+6

1 0

7 4

95

25

45

5+

61

7 3

24

3 7

21

8

:P

roje

ctU

23

41

5Q

C L

eve

l:N

EP

M 1

99

9

Sch

ed

ule

B(3

) a

nd

AL

S Q

CS

3 r

eq

uire

me

nt

Site

:--

--:

C-O

-C n

um

ber

----

Date

Sam

ple

s R

ece

ived

:0

5-N

OV

-20

12

----

:S

am

ple

rIs

sue D

ate

:1

4-N

OV

-20

12

:O

rder

num

ber

UN

62

67

No. of sa

mple

s re

ceiv

ed

:2

2Q

uote

num

ber

:E

N/0

24

/11

No. of sa

mple

s analy

sed

:2

2

This

report

supers

edes a

ny

pre

vious

report

(s)

with this

refe

rence

. R

esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted. A

ll pages

of th

is r

eport

have

been c

heck

ed a

nd a

ppro

ved for

rele

ase

.

This

Inte

rpre

tive Q

ualit

y C

ontr

ol R

eport

conta

ins

the follo

win

g in

form

atio

n:

l

Analy

sis

Hold

ing T

ime C

om

plia

nce

l

Qualit

y C

ontr

ol P

ara

mete

r F

requency

Com

plia

nce

l

Brief M

eth

od S

um

maries

l

Sum

mary

of O

utli

ers

Ad

dre

ss 3

2 S

ha

nd

Str

ee

t S

taff

ord

QL

D A

ust

ralia

40

53 | P

HO

NE

+

61-7

-3243 7

222 | F

acsim

ile

+

61

-7-3

24

3 7

21

8

En

viro

nm

en

tal D

ivis

ion

Brisb

an

e A

BN

84

00

9 9

36

02

9 P

art

of

the

AL

S G

rou

p

A

Ca

mp

be

ll B

roth

ers

Lim

ited

Co

mp

an

y


254

2 o

f 8

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

The

follo

win

g

report

su

mm

arise

s ext

ract

ion

/ pre

para

tion

and

analy

sis

times

and

com

pare

s w

ith

reco

mm

ended

hold

ing

times.

D

ate

s re

port

ed

repre

sent

first

date

of

ext

ract

ion

or

analy

sis

and

pre

cludes

subse

quent

dilu

tions

and

reru

ns.

In

form

ation

is

als

o

pro

vided

re

the

sam

ple

co

nta

iner

(pre

serv

ativ

e)

from

w

hic

h

the

analy

sis

aliq

uot

was

take

n.

Ela

pse

d

period

to

analy

sis

repre

sents

num

ber

of

days

fr

om

sa

mplin

g

where

no

ext

ract

ion

/ dig

est

ion

is

invo

lved

or

period

from

ext

ractio

n

/ dig

est

ion

where

th

is

is

pre

sent.

For

com

posi

te

sam

ple

s,

sam

plin

g

date

is

ass

um

ed

to

be

that

of

the

old

est

sa

mple

co

ntr

ibutin

g

to

the

com

posi

te.

S

am

ple

date

for

labora

tory

pro

duce

d

leachate

s

is

ass

um

ed

as

the

com

ple

tion

date

of

the

leach

ing

pro

cess

. O

utli

ers

fo

r hold

ing

time

are

base

d

on

US

EP

A

SW

846

, A

PH

A,

AS

and

NE

PM

(1

999

).

A

listin

g

of

bre

ach

es

is

pro

vided

in

the

Sum

mary

of O

utli

ers

.

Hold

ing

times

for

leach

ate

m

eth

ods

(exc

ludin

g

elu

tria

tes)

va

ry

acc

ord

ing

to

the

analy

tes

bein

g

dete

rmin

ed

on

the

resu

lting

solu

tion.

For

non

-vola

tile

analy

tes,

th

e

hold

ing

time

com

plia

nce

ass

ess

ment

com

pare

s th

e

leach

date

w

ith

the

short

est

analy

te

hold

ing

tim

e

for

the

equiv

ale

nt

soil

meth

od.

These

so

il hold

ing

times

are

: O

rganic

s (1

4 d

ays

);

Merc

ury

(2

8 d

ays

) &

oth

er

meta

ls

(180 d

ays

).

A

reco

rded

bre

ach

th

ere

fore

does

not

guara

nte

e

a b

reach

for

all

non-v

ola

tile p

ara

mete

rs.

Matr

ix:

SO

ILE

valu

atio

n: û

= H

old

ing tim

e b

reach

; ü

= W

ithin

hold

ing tim

e.

Analy

sis

Ext

ract

ion / P

repara

tion

Sa

mp

le D

ate

Me

tho

d

Eva

luatio

nD

ue for

analy

sis

Da

te a

na

lys

ed

Eva

luatio

nD

ue for

ext

ract

ion

Da

te e

xtr

ac

ted

Co

nta

ine

r / C

lient S

am

ple

ID

(s)

EA

002 :

pH

(S

oils)

Sn

ap

Lo

ck B

ag

(E

A002)

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

09-N

OV

-2012

05-N

OV

-2012

12

-NO

V-2

01

209-N

OV

-20

12

29-O

CT

-2012

ûû

EA

006:

So

diu

m A

dso

rpti

on

Rati

o (

SA

R)

Sn

ap

Lo

ck B

ag

(E

A006)

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

27-A

PR

-2013

27-A

PR

-2013

14

-NO

V-2

01

214-N

OV

-20

12

29-O

CT

-2012

üü


255255

3 o

f 8

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Matr

ix:

SO

ILE

valu

atio

n: û

= H

old

ing tim

e b

reach

; ü

= W

ithin

hold

ing tim

e.

Analy

sis

Ext

ract

ion / P

repara

tion

Sa

mp

le D

ate

Me

tho

d

Eva

luatio

nD

ue for

analy

sis

Da

te a

na

lys

ed

Eva

luatio

nD

ue for

ext

ract

ion

Da

te e

xtr

ac

ted

Co

nta

ine

r / C

lient S

am

ple

ID

(s)

EA

010:

Co

nd

ucti

vit

y

Sn

ap

Lo

ck B

ag

(E

A010)

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

07-D

EC

-2012

05-N

OV

-2012

12

-NO

V-2

01

209-N

OV

-20

12

29-O

CT

-2012

ûü

EA

055:

Mo

istu

re C

on

ten

t

Sn

ap

Lo

ck B

ag

(E

A055-1

03)

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

12-N

OV

-2012

----

08

-NO

V-2

01

2--

--29-O

CT

-2012

----

ü

ED

008:

Exch

an

geab

le C

ati

on

s

Sn

ap

Lo

ck B

ag

(E

D008)

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

26-N

OV

-2012

26-N

OV

-2012

13

-NO

V-2

01

213-N

OV

-20

12

29-O

CT

-2012

üü


256

4 o

f 8

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Matr

ix:

SO

ILE

valu

atio

n: û

= H

old

ing tim

e b

reach

; ü

= W

ithin

hold

ing tim

e.

Analy

sis

Ext

ract

ion / P

repara

tion

Sa

mp

le D

ate

Me

tho

d

Eva

luatio

nD

ue for

analy

sis

Da

te a

na

lys

ed

Eva

luatio

nD

ue for

ext

ract

ion

Da

te e

xtr

ac

ted

Co

nta

ine

r / C

lient S

am

ple

ID

(s)

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

Sn

ap

Lo

ck B

ag

(E

D045G

)K

O 1

0.1

-0.2

M,

KO

1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

07-D

EC

-2012

05-N

OV

-2012

12

-NO

V-2

01

209-N

OV

-20

12

29-O

CT

-2012

ûü


257257

5 o

f 8

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Qu

ality

Co

ntr

ol P

ara

mete

r F

req

uen

cy C

om

plian

ce

The follo

win

g r

eport

sum

marise

s th

e fre

quency

of la

bora

tory

QC

sam

ple

s analy

sed w

ithin

the a

naly

tical l

ot(

s) in

whic

h the s

ubm

itted s

am

ple

(s)

was(

where

) pro

cess

ed. A

ctual r

ate

should

be g

reate

r th

an o

r equal t

o the

exp

ect

ed r

ate

. A

list

ing o

f bre

aches

is p

rovid

ed in

the S

um

mary

of O

utli

ers

.

Matr

ix:

SO

ILE

valu

atio

n: û

= Q

ualit

y C

ontr

ol f

requency

not w

ithin

speci

ficatio

n ; ü

= Q

ualit

y C

ontr

ol f

requency

with

in s

peci

ficatio

n.

Qu

alit

y C

on

tro

l S

pe

cifica

tio

nQ

ua

lity

Co

ntr

ol S

am

ple

Typ

e

Ex

pe

cte

dQ

CR

eg

ula

rA

ctu

al

Ra

te (

%)

Qu

alit

y C

on

tro

l Sa

mp

le T

ype

Co

un

tE

valu

atio

nA

na

lytica

l Me

tho

ds

Me

tho

d

Labora

tory

Duplic

ate

s (

DU

P)

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

13.6

10.0

322

üC

hlo

ride S

olu

ble

By

Dis

crete

Analy

ser

ED

045G

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

13.6

10.0

322

üE

lect

rica

l Conductiv

ity (

1:5

)E

A010

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

13.6

10.0

322

üE

xchangeable

Catio

ns

with

pre

-tre

atm

ent

ED

008

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

10.0

10.0

330

üM

ois

ture

Conte

nt

EA

055-1

03

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

13.6

10.0

322

üpH

(1:5

)E

A002

Labora

tory

Contr

ol S

am

ple

s (L

CS

)

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

18.2

10.0

422

üC

hlo

ride S

olu

ble

By

Dis

crete

Analy

ser

ED

045G

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

9

.1

5.0

222

üE

lect

rica

l Conductiv

ity (

1:5

)E

A010

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

9

.1

5.0

222

üE

xchangeable

Catio

ns

with

pre

-tre

atm

ent

ED

008

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

9

.1

5.0

222

üpH

(1:5

)E

A002

Meth

od B

lanks

(M

B)

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

9

.1

5.0

222

üC

hlo

ride S

olu

ble

By

Dis

crete

Analy

ser

ED

045G

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

9

.1

5.0

222

üE

lect

rica

l Conductiv

ity (

1:5

)E

A010

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

9

.1

5.0

222

üE

xchangeable

Catio

ns

with

pre

-tre

atm

ent

ED

008

NE

PM

1999 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

9

.1

5.0

222

üS

odiu

m A

dso

rptio

n R

atio

(S

AR

)E

A006


258

6 o

f 8

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Bri

ef

Meth

od

Su

mm

ari

es

The a

naly

tical p

roce

dure

s u

sed b

y th

e E

nvironm

enta

l D

ivis

ion h

ave

been d

eve

loped fro

m e

stablis

hed in

tern

atio

nally

reco

gniz

ed p

roce

dure

s su

ch a

s th

ose

publis

hed b

y th

e U

S E

PA

, A

PH

A, A

S a

nd N

EP

M. In

house

deve

loped p

roce

dure

s are

em

plo

yed in

the a

bse

nce

of docu

mente

d s

tandard

s or

by

clie

nt re

quest

. T

he follo

win

g r

eport

pro

vides

brief desc

riptio

ns

of th

e a

naly

tical p

roce

dure

s em

plo

yed for

resu

lts r

eport

ed in

the

Cert

ifica

te o

f A

naly

sis. S

ourc

es

from

whic

h A

LS

meth

ods h

ave

been d

eve

loped a

re p

rovi

ded w

ithin

the M

eth

od D

esc

riptio

ns.

An

aly

tica

l Me

tho

ds

Me

tho

d D

esc

rip

tion

sM

atr

ixM

eth

od

(AP

HA

21

st e

d.,

45

00

H+

) p

H is

de

term

ine

d o

n s

oil

sam

ple

s a

fte

r a

1:5

so

il/w

ate

r le

ach

. T

his

me

tho

d is

com

plia

nt

with

NE

PM

(1

99

9)

Sch

ed

ule

B(3

) (M

eth

od

10

3)

pH

(1

:5)

EA

002

SO

IL

US

EP

A 6

00

/2 -

78

- 5

4.

Th

e c

on

cen

tra

tion

as

me

q o

f C

a,

Mg

an

d N

a a

re d

ete

rmin

ed

on

sa

tura

ted

so

il b

y w

ate

r

lea

ch.

Re

sults

are

use

d t

o c

alc

ula

te S

AR

.

So

diu

m

Ad

so

rptio

n R

atio

(S

AR

)E

A006

SO

IL

(AP

HA

21

st e

d.,

25

10

) C

on

du

ctiv

ity is

de

term

ine

d o

n s

oil

sam

ple

s u

sin

g a

1:5

so

il/w

ate

r le

ach

. T

his

me

tho

d is

com

plia

nt

with

NE

PM

(1

99

9)

Sch

ed

ule

B(3

) (M

eth

od

10

4)

Ele

ctr

ica

l C

on

du

ctiv

ity (

1:5

)E

A010

SO

IL

A g

ravi

me

tric

pro

ced

ure

ba

sed

on

we

igh

t lo

ss o

ver

a 1

2 h

ou

r d

ryin

g p

erio

d a

t 1

03

-10

5 d

eg

ree

s C

. T

his

me

tho

d is

com

plia

nt

with

NE

PM

(2

01

0 D

raft

) S

che

du

le B

(3)

Se

ctio

n 7

.1 a

nd

Ta

ble

1 (

14

da

y h

old

ing

tim

e).

Mo

istu

re C

on

ten

tE

A055-1

03

SO

IL

Ra

yme

nt

& H

igg

inso

n (

19

92

) M

eth

od

15

A2

. S

olu

ble

sa

lts

are

re

mo

ved

fro

m t

he

sa

mp

le p

rio

r to

an

aly

sis.

C

atio

ns

are

exc

ha

ng

ed

fro

m t

he

sa

mp

le b

y co

nta

ct w

ith A

mm

on

ium

Ch

lorid

e.

Th

ey

are

th

en

qu

an

tita

ted

in

th

e f

ina

l

solu

tion

by

ICP

AE

S a

nd

re

po

rte

d a

s m

eq

/10

0g

of

orig

ina

l so

il. T

his

me

tho

d is

com

plia

nt

with

NE

PM

(1

99

9)

Sch

ed

ule

B(3

) (M

eth

od

30

1)

Exch

an

ge

ab

le C

atio

ns w

ith

pre

-tre

atm

en

tE

D008

SO

IL

Th

e t

hio

cya

na

te io

n is

lib

era

ted

fro

m m

erc

uric

thio

cya

na

te t

hro

ug

h s

eq

ue

stra

tio

n o

f m

erc

ury

by

the

ch

lorid

e io

n t

o

form

no

n-io

nis

ed

me

rcu

ric

chlo

rid

e.in

th

e p

rese

nce

of

ferr

ic io

ns

the

lib

rate

d t

hio

cyn

ate

fo

rms

hig

hly

-co

lou

red

fe

rric

thio

cyn

ate

wh

ich

is m

ea

sure

d a

t 4

80

nm

AP

HA

21

st e

ditio

n 4

50

0-C

l- E

.

Ch

lorid

e S

olu

ble

By

Dis

cre

te A

na

lyse

rE

D045G

SO

IL

Pre

pa

ratio

n M

eth

od

sM

eth

od

De

scrip

tion

sM

atr

ixM

eth

od

US

EP

A 6

00

/2.

So

il is

bo

ug

ht

to s

atu

ratio

n w

ith d

istille

d w

ate

r b

y ca

pili

ary

act

ion

.S

AR

Pre

pE

A006P

RS

OIL

Ra

yme

nt

& H

igg

inso

n (

19

92

) m

eth

od

15

A1

. A

1M

NH

4C

l e

xtra

ctio

n b

y e

nd

ove

r e

nd

tu

mb

ling

at

a r

atio

of

1:2

0.

Th

ere

is n

o p

retr

ea

tme

nt

for

solu

ble

sa

lts.

Ext

ract

s ca

n b

e r

un

by

ICP

fo

r ca

tio

ns.

Exc

ha

ng

ea

ble

Ca

tio

ns

Pre

pa

ratio

n

Me

tho

d

ED

007P

RS

OIL

10

g o

f so

il is

mix

ed

with

50

mL

of

dis

tille

d w

ate

r a

nd

tu

mb

led

en

d o

ver

en

d f

or

1 h

ou

r.

Wa

ter

solu

ble

sa

lts

are

lea

che

d f

rom

th

e s

oil

by

the

co

ntin

uo

us

susp

en

sio

n.

Sa

mp

les

are

se

ttle

d a

nd

th

e w

ate

r filte

red

off

fo

r a

na

lysi

s.

1:5

so

lid /

wa

ter

lea

ch f

or

so

lub

le

an

aly

tes

EN

34

SO

IL


259259

7 o

f 8

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Su

mm

ary

of

Ou

tlie

rs

Ou

tlie

rs :

Qu

ality

Co

ntr

ol S

am

ple

s

The

follo

win

g

report

hig

hlig

hts

outli

ers

fla

gged

in

the

Qualit

y

Contr

ol

(QC

) R

eport

. S

urr

ogate

re

cove

ry

limits

are

st

atic

and

base

d

on

US

EP

A

SW

846 o

r A

LS

-QW

I/E

N/3

8 (

in

the

abse

nce

of

speci

fic

US

EP

A

limits

).

This

report

dis

pla

ys Q

C O

utli

ers

(bre

aches)

only

.

Du

pli

ca

tes

, M

eth

od

Bla

nk

s,

La

bo

rato

ry C

on

tro

l S

am

ple

s a

nd

Ma

trix

Sp

ike

s

l

Fo

r all m

atr

ices, n

o M

eth

od

Bla

nk v

alu

e o

utl

iers

occu

r.

l

Fo

r all m

atr

ices, n

o D

up

licate

ou

tlie

rs o

ccu

r.

l

Fo

r all m

atr

ices, n

o L

ab

ora

tory

Co

ntr

ol o

utl

iers

occu

r.

l

Fo

r all m

atr

ices, n

o M

atr

ix S

pik

e o

utl

iers

occu

r.

Re

gu

lar

Sa

mp

le S

urr

og

ate

s

l

Fo

r all r

eg

ula

r sam

ple

matr

ices, n

o s

urr

og

ate

reco

very

ou

tlie

rs o

ccu

r.

Ou

tlie

rs :

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

This

report

dis

pla

ys H

old

ing T

ime b

reach

es

only

. O

nly

the r

espect

ive E

xtra

ctio

n / P

repara

tion a

nd/o

r A

naly

sis

com

ponent is

/are

dis

pla

yed.

Matr

ix:

SO

IL

Analy

sis

Ext

ract

ion / P

repara

tion

Date

analy

sed

Date

ext

ract

ed

Co

nta

iner

/ C

lien

t S

am

ple

ID

(s)

Da

ys

ov

erd

ue

Da

ys

ov

erd

ue

Due for

ext

ract

ion

Due for

analy

sis

Me

tho

d

EA

002 :

pH

(S

oils)

Sn

ap

Lo

ck B

ag

09-N

OV

-2012

05-N

OV

-2012

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

12-N

OV

-2012

09-N

OV

-2012

43

EA

010:

Co

nd

ucti

vit

y


260

8 o

f 8

:P

age

Work

Ord

er

: :C

lient

EB

1229103

CA

RD

NO

ULLM

AN

& N

OLA

N G

EO

TE

CH

NIC

PT

Y L

TD

U23415

:P

roje

ct

Matr

ix:

SO

IL

Analy

sis

Ext

ract

ion / P

repara

tion

Date

analy

sed

Date

ext

ract

ed

Co

nta

iner

/ C

lien

t S

am

ple

ID

(s)

Da

ys

ov

erd

ue

Da

ys

ov

erd

ue

Due for

ext

ract

ion

Due for

analy

sis

Me

tho

d

EA

010:

Co

nd

ucti

vit

y -

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

Sn

ap

Lo

ck B

ag

----

05-N

OV

-2012

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

----

09-N

OV

-2012

4--

--

ED

045G

: C

hlo

rid

e D

iscre

te a

naly

ser

Sn

ap

Lo

ck B

ag

----

05-N

OV

-2012

KO

1 0

.1-0

.2M

,K

O1 0

.2-0

.3m

,

KO

2 0

.6-1

.0m

,K

O3 0

.6-1

.0m

,

KO

4 0

.2-0

.3m

,K

O5 0

.3-0

.6m

,

BB

15-0

.6-1

.0m

,B

B15 0

.2-0

.3m

,

BB

12 0

.3-0

.6m

,B

B12 0

.6-1

.0m

,

BB

07 0

.1-0

.2m

,B

B11 0

.0-0

.1m

,

BB

10 0

.3-0

.6m

,B

B09 0

.1-0

.2m

,

BB

13 0

.6-0

.75m

,B

B19 0

.2-0

.3m

,

BB

17 0

.6-1

.0m

,B

B16 0

.6-1

.0m

,

BB

20 0

.0-0

.1m

,B

B6 0

.2-0

.3m

,

BB

6 0

.3-0

.6m

,B

B18 0

.0-0

.1m

----

09-N

OV

-2012

4--

--

Ou

tlie

rs :

Fre

qu

en

cy o

f Q

uality

Co

ntr

ol S

am

ple

s

The follo

win

g r

eport

hig

hlig

hts

bre

aches

in the F

requency

of Q

ualit

y C

ontr

ol S

am

ple

s.

l

No

Qu

ality

Co

ntr

ol S

am

ple

Fre

qu

en

cy O

utl

iers

exis

t.


261261

262

This page is intentionally left blank.


Insert report title here Supplementary Soil Survey for Proposed …eisdocs.dsdip.qld.gov.au/Galilee Coal Project (Northern Export Facility... · 12 December 2012 Cardno 4 L:\Engineer

Documents