Inorganic Membranes Proceedings of the 9th International Conference on Inorganic Membranes Lillehammer, Norway ]une 25-29, 2006 TECHNISCHE INFORMATIONSBIBLIOTHEK UNIVERSITATSBIBLIOTHEK HANNOVER Editors R. Bredesen and H. Raeder TIB/UB Hannover 126 170 592 89
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Inorganic Membranes
Proceedings of the 9thInternational Conference on
Inorganic Membranes
Lillehammer, Norway]une 25-29, 2006
TECHNISCHEINFORMATIONSBIBLIOTHEK
UNIVERSITATSBIBLIOTHEKHANNOVER
EditorsR. Bredesen and H. Raeder
TIB/UB Hannover126 170 592
89
Proc. 9th Int. Conf. on Inorganic Membranes, Lillehammer - Norway, June 25-29 2006
Table of contents
Preface 7
Table of contents 11
Plenary lectures 27
Pd-Based Hydrogen Separation Membranes - Status and Prospective.. 28
YiHuaMa
Microporous Silica-based Membranes - Present Status and Prospect.... 38
Masashi Asaeda
Proton Conducting Ceramic Membranes and Hydrogen Devices 48
Hiroyasu Iwahara
Oral lectures 57
Characterization of V-6Ni-5Co Membranes for Hydrogen Separation... 58
Stephen N. Paglieri, Yongqiang Wang, Thomas ]. Venhaus, Hain Oona, Ronny C.Snow, Blake P. Nolen, Robert E. Buxbaum, Kurt S. Rothenberger, Bret H. Howard,and Richard P. Killmeyer
High Flux Pd Membranes Deposited on Stainless Steel Supports byElectroless Plating 65
Sabina K. Cade, Matthew K. Keeling, Daniel K. Steele, ]. Douglas Way, Paul M.Thoen
Preparation of well-defined thin YSZ and SSZ membranes with a narrowpore size distribution 69
/. Shi, K. Shqau, R. Revur, S. Sengupta, J.R. Schorr and H. Verweij
Filtration of aerosols as a method to close membrane defects 74
B.J. Bladergroen, F. Meyer, V.M. Linkov
Nanoporous alumina membranes grown electrochemically: fabricationand modification by metal deposition 78
M. Butera, R. Inguanta, C. Sunseri and S. Piazza
Preparation of YSZ ultrafiltration membrane with larger pore size usinginorganic salts as the precursor 82
Dense Ceramic-Metal Composite Membranes for HydrogenSeparation 86
U. (Balu) Balachandran, T. H. Lee, L. Chen, S. } . Song, and S. E. Dorris
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Proc. 9th Int. Conf. on Inorganic Membranes, Lillehammer - Norway, June 25-29 2006
Thermally Stable Composite Palladium Membranes HavingIntermediate Porous Metal Intermetallic Diffusion Barrier LayersFormed by Bi-Metal Multi-Layer Deposition 92
Ivan P. Mardilovich, ErikE. Engwall and YiHuaMa
Pd and Pd/Ag composite membranes prepared by the electroless platingtechnique: preparation, characterization and interpretation of the H2transport mechanism 96
A. Bottino, G. Capannelli, A. Comite, R. Di Felice, M. Broglia, P. Pinacci
Sol-gel process assisted by supercritical CO2 for nanophase YSZconductive ceramic oxides synthesis 100
Mass transport through zeolite membranes: investigating frameworkpolarity 256
/. Kuhn, J. Gross, J.C. Jansen, P.]. Jansens
New Proton Conducting Materials for Fuel Cells and HydrogenSeparation Membranes 260
Truls Norby, Reidar Haugsrud, Nalini Vajeeston
Oxygen and Hydrogen Separation Using Perovskite Hollow Fiber andZeolite Membranes in Comparison with Organic Membranes 268
Jiirgen Cam, Haihui Wang, Thomas Schiestel, Manfred Noack, Roland Dittmeyer,
Steffen Werth
Formation Mechanism of Microwave Synthesized LTA ZeoliteMembranes and the Thermal/Non-thermal Effects 273
Weishen Yang, Yanshuo Li
Preparation of b-oriented MFI films on the stainless-steel supports 279
A. Avhale, G.T.P. Mabande, W. Schwieger, T. Stief, R. Dittmeyer, S. Ghosh, Z. Lai,
M. Tsapatsis
Preparation of Silicalite Membranes on Large-Scale MonolithSupport 282
Kenji Suzuki, Miyuki Yabuki, Shinji Nakamura, Toshihiro Tomita and ShuichiYoshida
A new generation of zeolite membranes 286
Anita Buekenhoudt, Frans Servaes, Kenny Wyns, Alexander Aerts, ]ohan Martensand Pierre Jacobs
Zeolite membrane for CO2 removal: Operating at high pressure 290
Victor Sebastian, Izumi Kumakiri, Rune Bredesen and Miguel Menendez
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Proc. 9th Int. Conf. on Inorganic Membranes, Lillehammer - Norway, June 25-29 2006
Effect of Microporous Amorphous Silica Structure on Gas PermeationProperties Studied with Molecular Dynamics Simulation 294
Tomohisa Yoshioka, Akinori Yasumoto, Kohei Kishi, Toshinori Tsuru and MasashiAsaeda
A Contribution of Mass Transport Resistance of Ceramic Supports to theOverall Mass Transport Resistance of Composite Membranes MFI typezeolite-cc-alumina 299
V. Kotek, A. Zikdnovd, P. Hrabdnek, K. Kovandovd, L. Brabec, M. Kocifik, V. Fila,V. Navara, M. Lhotka, B. Bernauer, O. Solcovd, P. Uchytil, P. Mikuldsek, H.Jirdnkovd, P. Velikovskd
Solvent membrane layer interaction for transport through oxide ceramicscoated clay alumina support 303
G C Sahoo, S N Roy and S Bandyopadhyay
Ceramic Hollow Fibre Membranes for Separation and Reaction 307
K. Li and Xiaoyao Tan
Ceramic hollow fiber membranes for oxygen production and conversionof methane 313
Haihui Wang, Thomas Schiestel, Cristina Tablet, Jiirgen Cam
Synthesis of Long-term Acid-stable Zeolite Membranes and theirApplication to Dehydration of Acetic Acid and EsterificationReaction 319
Hidetoshi Kita, Xiansen Li, Tatsuya Nagamatsu and Kazuhim Tanaka
Mass-transport in a methylated silica membrane during pervaporationand vapour permeation - Experimental and modelling approach 325
Frans de Bruijn, Joachim Grofl, Zarko Olujic, Peter Jansens, Freek Kapteijn
Separation of bio ethanol by pervaporation with hydrophobic ZSM-5membranes 329
Hannes Richter, Marcus Weyd, Gundula Fischer, Petra Puhlfiirfl, IngolfVoigt
Dehydrations behavior of MFI zeolite membrane for various kinds ofsolvents 333
Carbon membranes on porous ceramic capillaries for membraneextraction 368
I. Voigt, U. Pippardt, G. Fischer, Th. Raiser, J. R. Herguijuela
Cation diffusion in LaCoO3 371
Marian Palcut, Kjell Wiik and Tor Grande
Ceramic membrane bio reactor for Industrial Waste Water Treatment - ACase Study 375
/. Guibaud, S. Paranthoen, A. Balaire
Ceramic Processing of Oxygen Permeable Membranes and their Testingunder Conditions for the Synthesis Gas Production 378
Jiirgen Boer, Wolfgang Burckhardt and Lutz Kiesel
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Proc. 9th Int. Conf. on Inorganic Membranes, Lillehammer - Norway, June 25-29 2006
Characterization and Hydrogen Interaction Studies on Cobalt-DopedAmorphous Silica Composite Materials for High-Temperature HydrogenSeparation Membranes 382
Influence of processing conditions on the microstructure and function of(Bao.5Sro.5)(Feo.8Zno.2)03-5 membranes 503
Julia Martynczuk, Haihui Wang, Mirko Arnold and Armin Feldhoff
Investigation of performance of ceramic ultrafiltration membrane inrelation with speciation and membrane solutes interactions - applicationto removal of salts and textile dyes in liquid effluents 507
H.Loukili
Investigations to the permeation properties for gases on molecular sievemembranes of types: LTA, FAU, ZSM-5 511
M. Noack, P. Kolsch, A. Dittmar, G. Georgi, M. Stohr
Mechanical and Gas Permeation Properties of Porous AluminaCapillary 516
Ryuji Kojima, Koji Sato and Yuji Iwamoto
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Proc. 9th Int. Conf. on Inorganic Membranes, Lillehammer - Norway, June 25-29 2006
Microporous carbon membranes synthesized from tertiary amines/RFresin composites 519
Yong-Rong Dong, Norikazu Nishiyama, Yasuyuki Egashira and Korekazu Ueyama
Microporous ZrO2 Film Preparation by Chemical Vapor Deposition... 524
S. Mathur, E. Hemmer, S. Barth, J. Altmayer, N. Donia, N. Lecerf, I. Kumakiri andR. Bredesen
Microstructural Characterization of Self-Supported Pd/Ag Membranesfor Hydrogen Separation 528
Wakshum Mekonnen, Randi Holmestad, John C. Walmsley, Bjernar Arstad, AstridMejdell, Hallgeir Klette, Hilde Venvik and Rune Bredesen
Microwave-synthesized MFI membranes reproducibility and permeationbehaviour at high temperature 532
Julius Motuzas, Raminta Mikutaviciute, Richard D. Noble, Zigmuntas J.Beresnevicius, Anne Julbe
Mineral-based ceramic membranes for environmental applications .... 536Guangyao Meng, Yingchao Dong, Xiangjun Ren, Xuebin Zhang, Jiakui Yang,Dingkun Peng, Xingqin Liu
Modelling of stationary permeation of binary species through silicalite-1membranes 539
Oxygen Permeation through a Bh.5Yo.3Smo.203-Lao.8Sro.2Mn03-& dual-phaseComposite Membrane 570
Xiusheng Wu, Chunli Yang, Chusheng Chen, and Wei Liu
Partial Oxidation and Selective Hydrogenation in Catalytic MembraneReactors 575
Jiirgen Cam, Haihui Wang, Alexandra Kleinert, Thomas Schiestel, Peter Kolsch,Aurel Wolf, Rainhard Schomdcker, Andrea Schmidt, Roland Dittmeyer, DanielUrbanczyk, Steffen Werth
Partial Oxidation of Methane with Fuel Cell Type Reactor Using LaGaO3Type Membrane 579
Tomohiko Tagawa, Yoshinori Terao, Hiroshi Yamada and Makoto Inomatat
Pd Alloy Membranes with a New Configuration Prepared by aCombined Organic/inorganic Process 583
Himyuki Suda, Jianhua Tong, Kenji Haraya
Pd Coating of Ni-Nb-Zr Glassy Alloy Membrane and Its HydrogenPermeation Characteristics 587