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Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based Composites Center Chip Frazier T.M. Brooks Professor of Sustainable Biomaterials Director, Wood-Based Composites Center Virginia Tech Blacksburg, Virginia, U.S.A.
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Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

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Page 1: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Industry/University Cooperative Research in North America

The National Science Foundation

The Wood-Based Composites Center

Chip Frazier T.M. Brooks Professor of Sustainable Biomaterials

Director, Wood-Based Composites Center Virginia Tech

Blacksburg, Virginia, U.S.A.

Page 2: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Map: VectorTemplates.com

Page 3: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Our folks

Arauco North America Arclin

Boise Cascade Columbia Forest Products

Fraunhofer WKI Institute for Wood Research Georgia-Pacific Chemicals

Henkel Corporation Momentive Specialty Chemicals

Queensland, Australia Government Solenis

Willamette Valley Company

Page 4: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

The Research Spectrum in North America

The Ivory Tower Academia

The Real World Industry

Principal drivers:

• Federal initiatives • Money, university revenue • Publications • Graduates

• Market forces • Innovation • Money, profits

Page 5: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

The Research Spectrum in North America

The Ivory Tower Academia

The Real World Industry

Positive qualities:

• Public service • Developing students • Long-term focus

• Practical • Rapid & efficient • Accountable

Page 6: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

The Research Spectrum in North America

The Ivory Tower Academia

The Real World Industry

Negative qualities:

• Slow & inefficient • Perhaps poor accountability • Often less practical value

• Short-term focus • Perhaps superficial

Page 7: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Merits & faults are found both in academia & industry…

The Ivory Tower Academia

The Real World Industry

Merits in each may be enhanced through collaboration; faults in each may be neutralized in collaboration.

Page 8: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

In which domain will collaboration occur?

The Ivory Tower Academia

The Real World Industry

Public Domain: • Broad participation • Broad focus

Private Domain: • Limited participation • Limited focus

Page 9: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

The U.S. National Science Foundation

• Independent federal agency created "to promote the progress of science; to advance the national health, prosperity, and welfare; to secure the national defense…"

• Annual budget of $7.2 billion (FY 2014).

• Funding source for 24 percent of all federally supported basic research conducted by U.S. colleges and universities.

Page 10: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

The U.S. National Science Foundation

Industry/University Cooperative Research Centers program- I/UCRC: • Small program, annual budget ~ $15 million (~ 0.2% of the NSF budget).

• Leveraging a small federal investment into a large industrial investment.

• 30+ years of successful operation.

Page 11: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

A little federal funding- a lot of industry funding

NSF $120,000/yr (maximum)

Industry $300,000/yr (minimum)

Official NSF sites

Current sub-contractors

Page 12: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Wood-Based Composites Center, 1 of about 60 I/UCRC’s

Center Leadership Team

Director (VT) Co-Director (OSU)

Managing Director

NSF External Evaluator NSF

Program Director

Partner Universities

OSU VT

NSF Sites

UBC Maine

Members

Industrial Advisory Board

Technical Committee

Executive Committee

Pro

ject 1

Pro

ject 2

Pro

ject 3

Pro

ject n

Page 13: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

WBC Industry Advisory Board

Executive Committee:

• Meet once/year

• Strategic planning

• Establish/oversee Center bylaws

• Review membership costs/benefits

• Review Center mission, objectives

• Review Center metrics

• Manage recruiting initiatives

• Oversee Center finances

Technical Committee:

• Meet twice/year

• Establish/monitor Center research

• Select and oversee research projects

• Provide recommendations/feedback

to the Executive Committee

• Serve as consultant to specific

projects, not all projects.

VP of Check Writing

Director of R&D

Page 14: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

WBC Industry Advisory Board

Executive Committee:

• Meet once/year

• Strategic planning

• Establish/oversee Center bylaws

• Review membership costs/benefits

• Review Center mission, objectives

• Review Center metrics

• Manage recruiting initiatives

• Oversee Center finances

Technical Committee:

• Meet twice/year

• Establish/monitor Center research

• Select and oversee research projects

• Provide recommendations/feedback

to the Executive Committee

• Serve as consultant to specific

projects, not all projects.

VP of Check Writing

Director of R&D

Major objective is to engage each member through multiple contacts.

Page 15: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Members drive the Center

• Members create the research agenda.

• Faculty compete for funds, annually.

• Competition based upon:

Scientific merit

Responsiveness to industry needs.

Responsiveness to industry feedback.

Performance on yearly deliverables.

Page 16: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Members drive the Center

• Membership fees are pooled.

• Faculty submit proposals.

• Members review proposals, and…

Accept

Reject, or

Accept w/ designated changes.

• Members award funding based upon merit.

Page 17: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Research in the public domain

• Ultimately, research results are released to the public.

• Research is precompetitive; tends to focus on broader industry needs.

• Intellectual property is protected.

• This model tends to attract faculty that are committed to industry service.

Page 18: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

What research do we conduct? The research that our members request.

Current/Recent Projects:

• Improving blending efficiency and resin distribution of the rotary drum blending process using discrete element modeling.

• Ranking resins by their effects on durability of wood composites.

• Accelerated weathering for the development of an NDT product durability assessment toolkit.

• Multi-scale accelerated weathering of wood composite materials.

• Checking in maple plywood.

• Wetting and diffusion associated with selected liquid/wood interfaces.

• Multi-scale investigation of adhesive bond durability.

• Investigation of micro‐scale wood/adhesive interaction.

Page 19: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

What research do we conduct? The research that our members request.

Current/Recent Projects (continued):

• Fundamentals of formaldehyde detection and emission determination.

• Filler effects in PF Resoles

• Understanding the differences in bonding characteristics of Douglas-fir and southern yellow pine wood.

• Biogenic formaldehyde emission.

• Adhesion fundamentals in spotted gum (Corymbia sp.).

• Fiber quality in medium density fiberboard production.

Page 20: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Investigation of micro‐scale wood/adhesive interaction

Investigators: Fred Kamke, John Nairn, Lech Muszynski

Goal: • Quantitate the role of adhesive penetration on bond performance.

Approach:

• Develop micron‐scale numerical model to predict bond behavior as affected by adhesive penetration, adhesive modulus, and wood anatomy.

• Characterize 3D adhesive penetration patterns using micro X‐ray computed tomography – basis for numerical model.

• Measure 2D strain of adhesive bonds and compare to model predictions.

Page 21: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Investigation of micro‐scale wood/adhesive interaction

3D micro X‐ray computed tomography

Digital image correlation: 2D strain fields in micro-bonds

3D modeling of stress/strain Including virtual experiments to failure.

Page 22: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Investigation of micro‐scale wood/adhesive interaction

2014 Forest Products Society Wood Award for outstanding graduate student research:

Dr. Jesse Paris R&D Chemist

Willamette Valley Company

Page 23: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Improving blending efficiency and resin distribution of the rotary drum blending process using discrete element modeling.

Investigator: Greg Smith

Goal: • Reduce flake surging and its impact on blender operation

Approach:

• Model flakes as discrete elements.

• Experimentally verify flake motion and surging.

• Use modeling results to help optimize boom placement & function.

Page 24: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Fundamentals of Formaldehyde Detection and Emissions Determination

Investigators: Barbara Cole, Ray Fort, Doug Gardner

Goal: • Determine the amount and sources of formaldehyde in native wood, and

the mechanisms by which it is formed.

Approach:

• Investigate effects of

temperature on native formaldehyde emissions.

wood moisture on native formaldehyde emissions.

• Determine which wood components (lignin, carbohydrates, other) are sources of native formaldehyde.

Page 25: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Filler effects in PF Resoles

Investigator: Chip Frazier

Goal: • Determine effects of filler particle size & filler chemistry on PF resole

penetration and performance.

Approach:

• Fillers: corn cob residue, alder bark, and walnut shell

• Characterize filler

Chemical composition

Surface chemistry & impact on adhesive surface tension.

Impact on adhesive rheology

• Measure performance using mode-I fracture & relate to adhesive penetration.

Page 26: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Filler effects in PF Resoles

10-2

10-1

100

101

102

103

104

103

104

Shear rate (1/s)

Vis

co

sity (m

Pa

s)

A-1

A-2

A-3

Shear rate decreasing

10-2

10-1

100

101

102

103

104

103

104

C-1

C-2

C-3

Shear rate (1/s)

Shear rate decreasing

10-2

10-1

100

101

102

103

104

103

104

Shear rate (1/s)

W-1

W-2

W-3

Shear rate decreasing

103

10410

-210

-110

010

110

210

310

4Shear rate (1/s)

A-1

A-2

A-3

Vis

co

sity (m

Pa

s)

Shear rate increasing

10-2

10-1

100

101

102

103

104

103

104

Shear rate (1/s)

C-1

C-2

C-3

Shear rate increasing

103

10410

-210

-110

010

110

210

310

4

Shear rate (1/s)

W-1

W-2

W-3

Shear rate increasing

Page 27: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Filler effects in PF Resoles

10-2

10-1

100

101

102

103

104

103

104

Shear rate (1/s)

Vis

co

sity (m

Pa

s)

A-1

A-2

A-3

Shear rate decreasing

103

10410

-210

-110

010

110

210

310

4Shear rate (1/s)

A-1

A-2

A-3

Vis

co

sity (m

Pa

s)

Shear rate increasing

0 20 40 60 80 100 120

0

50

100

150

200

Str

ain

%

A-1

Time (sec.)

X

Y

Z

Step 1

ramp-up flow

Step 2

ramp-down flow

X

Y

Z

Detection of liquid-state network structures dependent upon filler type, particle size,

and shear history.

Page 28: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Filler effects in PF Resoles

Filler particle

Filler particle

Filler particle

Colloidal particles: • < 1 micron in size • Dissolved polysaccharides • Dissolved lignin • Associated PF chains • Dissolved extractives

Formulated adhesives exhibit unique liquid-state structures. Determine how liquid-state structures translate to the solid-state bondline.

Non-colloidal particles: • > 1 micron in size

Page 29: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Filler effects in PF Resoles

Mode-I fracture

Lo

ad

, P

Displacement,

a1

P1, a1

Page 30: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Adhesion fundamentals in spotted gum (Corymbia sp.)

Investigator: Chip Frazier

Goal: • Advance fundamental knowledge in the science and technology of

adhesion in Corymbia sp. (spotted gum).

Approach:

• Measure surface chemistry of spotted gum and Gympie messmate (Eucalyptus cloeziana), using contact angle analysis.

• Compare sensitivities to heat-induced surface change.

Page 31: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

The value proposition in the I/UCRC model

Precompetitive Research

Professional Networking

Student Recruiting

Page 32: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

The I/UCRC model & its impact on students

Our students enjoy the greatest benefit:

• Industry-selected, relevant research.

• Regular scrutiny, review by industry professionals.

• Extended industry Interaction.

• Accountability for meeting project deliverables.

• Improved presentation skills.

• Networking.

Page 33: Industry/University Cooperative Research in North America · 2018-08-02 · Industry/University Cooperative Research in North America The National Science Foundation The Wood-Based

Acknowledgements

Arauco North America Arclin

Boise Cascade Columbia Forest Products

Fraunhofer WKI Institute for Wood Research Georgia-Pacific Chemicals

Henkel Corporation Momentive Specialty Chemicals

Queensland, Australia Government Solenis

Willamette Valley Company