Industrial-chemistry (1).pdf

Year Sem. Course Code Paper Title Theory/Practical Credits

Certificate in Materials and Techniques in Chemical Industries

1 I B190101T

B190102P

B190201T

Fundamentals of Industrial Chemistry Theory

Practical

Theory

4

2

4

Basic Analytical Methods

Material Science and Techniques in Chemical Industries

II

B190202P Materialistic Analysis Practical 2

4

2

Diploma in Industrial Instrumentation and Chemical Analysis

B190301T 2 III Process Instrumentation and Industrial Chemical Analysis

Industrial Chemical and Instrumental Analysis

Theory

B190302P Practical

IV

V

B190401T

B190402P

Process Chemistry Theory

Practical

4

2 Qualitative and Synthetic Methods

B. Sc. in Industrial Chemistry

Industrial Chemicals

Pollution, its Management and Industrial Theory Economics

3 B190501T

B190502T

Theory 4

4

B190503P

B190504R

Industrial Chemicals and Pollution Management

Research Project

Practical 2

3 Project

VI Polymer Science (01)*

B190601T

B190602T

Synthetic Polymer

Polymerization Techniques and

Characterization

Theory

Theory

4

4

B190603P

B190604R

Synthesis and Analysis of Polymers

Research Project

Practical

Project

2

3

Pharmaceutical Chemistry (02)*

Pharmaceutical and Phytochemicals

Medicinal Chemistry and Toxicology

Experimental Pharmaceutical Chemistry

Research Project

B190605T

B190606T

B190607P

B190608R

Theory

Theory

Practical

Project

4

4

2

3

Agrochemicals (03)*

B190609T

B190610T

B190611P

B190612R

General and Halogenated Insecticides

Fungicides and Herbicides

Analysis of Agrochemicals

Research Project

Theory

Theory

Practical

Project

4

4

2

3

*01, 02 & 03 for the elective papers Polymer Chemistry, Pharmaceutical Chemistry & Agrochemicals

respectively in semester-VI.

3

Purpose of the programme:

Industrial chemistry has assisted in the discovery and development of new and improved synthetic fibres, paints,

adhesives, drugs, cosmetics, electronic components, lubricants and thousands of other products, and improved processes

for oil refining and petrochemical processing that saves energy and reduces pollution. The purpose of the undergraduate

Industrial Chemistry programme at the university and college level is to provide the key knowledge base, laboratory

resources and industrial knowledge to prepare students for careers as professionals in various industries and research

institutions. This program is designed to prepare students with the lab experience necessary to build a career in chemistry

along with the theoretical underpinnings and supporting knowledge needed to advance in such a career.

Program’s outcomes:

1. Students will have a firm foundation in the fundamentals and application of current chemical and scientific

theories including those in analytical, inorganic, organic and physical chemistry and various industrialprocesses.

2. Students will be able to design and carry out scientific experiments as well as accurately record and analyze the

results of such experiments.

3. Students will be skilled in problem solving, critical thinking and analytical reasoning as applied to scientific

problems.

4. Students will be able to explore new areas of research in both chemistry and allied fields of science and

technology.

5. Students will become aware of the role of industrial chemistry in our society. They will be able to use this

knowledge on account of ethical behavior in issues faced by chemists in industries for example safe handling of

chemicals, environmental issues and key issues faced by our society in energy, health and medicine.

6. Students will be able to explain why industrial chemistry is an integral activity for addressing social, economic,

and environmental problems.

7. Students will be able to function as a member of an interdisciplinary problem solving team.

8. Chemical industries in India and throughout the entire world are using increasingly sophisticated chemical

procedures and instrumentation. Consequently, industrial leaders are becoming more concerned about health

hazards and safety factors. These companies need chemists and chemical professionals that are experienced and

able to implement new techniques to minimise the industrial pollution.

9. Graduates in Industrial Chemistry may find jobs in various industries like chemical, plastics, pharmaceutical,

environmental, paint, food, automobile, petroleum and personal care products.

4

PROGRAM SPECIFIC OUTCOMES (PSOS)

Certificate in Materials and Techniques in Chemical Industries

First

Year

Certificate in Materials and Techniques in Chemical Industries will give the student a basic knowledge of

all the fundamental principles of chemistry like chemical calculations, thermodynamics, chemical

equilibrium, liquid crystals, solid state, Atomic structures, Periodic properties of more than 111 elements,

Metallurgical operations, various concepts of acid and acids, bases, redox reactions, fundamentals of organic

chemistry and catalysis. This course also provides practical knowledge of good laboratories practice (GLP)

and various basic analytical methods as well as basic knowledge of advanced materials, ceramics, surface

chemistry, crystallization, X-ray powder diffraction, distillation, evaporation, absorption, filtration,

extraction, drying and purification of organic compounds. Student will be also able to do to qualitative and

quantitative analysis in the laboratory.

This certificate course will definitely help to students to get basic knowledge of industrial chemistry on

account of chemical and pharmaceutical industries by which they can get better placement in the

government and private sector services particularly in the field of food safety, health sector, chemical

industries etc.

Second

Year

Diploma in Industrial Instrumentation and Chemical Analysis

Diploma in Industrial Instrumentation and Chemical Analysis will provide the theoretical as well

as practical knowledge of instrumental methods of analysis such as chromatography, instruments

used in measuring of temperature, pressure, liquid levels, and modern spectroscopic methods. This

course also provides sound knowledge of industrial analysis, effluent treatment waste water

management, testing of materials, analysis of water, analysis of industrial chemicals and various

chemical processes in chemical industries. The knowledge of various instruments, spectroscopic

tools and separation technique will make the students skilled to work in industries. Students of

diploma course will achieve the skills required to succeed in the various chemical industry like

cement industries, agro product, paint industries, rubber industries, petrochemical industries, food

processing industries, pollution monitoring and control agencies etc. Students would get the

exposures of a breadth of experimental techniques using modern instrumentation. Monitoring of

environmental pollution problems of atmospheric sciences, water chemistry and soil chemistry and

design processes that meet the specified needs with appropriate consideration for the public health

and safety, and the cultural, societal, and environmental considerations.

Third

Year

B. Sc. in Industrial Chemistry

Degree in Industrial Chemistry aims to introduce very important aspects of modern day course curriculum,

namely, instrumental instrumentation, chemical analysis, pollution monitoring, industrial chemicals, process

chemistry and various physical processes. Fifth semester of this program provide the basic theoretical and

experimental knowledge of pollution management, industrial chemical pollution management and it’s

economics. Final semester of this program provide specialization in Pharmaceutical chemistry or Polymer

chemistry or Agrochemicals.

Upon completion of a degree, industrial chemistry students are able to employ critical thinking and

scientific inquiry in the performance, design, interpretation and documentation of laboratory

experiments, at a level suitable to succeed at an entry-level position in chemical industry or a

chemistry graduate program.

Various research institutions and industry people in the pharmaceuticals, polymers, petroleum

agrochemicals and fertilizer industry sectors will definitely give value to this course.

5

Subject: Chemistry Total

Credits of

the Year Sem. Units Practical

Paper

Units Research

Project Theory

Paper subject

1. Indian ancient chemistry and fundamentals of

chemical calculations

2. Atomic structure and Periodic properties

1. Good laboratory practices, Nil Basic Analytical Methods Calibration of thermometer and

burette

Fundamentals of

Industrial

Chemistry

3. Chemical bonding, acids and bases 2. Simple laboratory techniques I 4+2 = 6 4. Organic compounds and nomenclature

5. Fundamentals of organic chemistry and catalysis 3. Viscosity and Surface tension of liquids

6. Liquid crystal s and solid state

7. Metallurgical operations, metals and alloys 4. Preparation of standard solutions

8. Heat, thermodynamics and chemical equilibrium

1. Advanced materials and material balance

2. Surface chemistry and ceramics

3. Utilities in chemical industry

Materialistic Analysis 1. Analysis of solution

2. Extraction process

3. Refractometer

Nil

Nil

1

Material Science

and Techniques 4. Crystallization

II in Chemical 4+2 = 6 5. X-ray powder diffraction and pharmaceuticals

6. Distillation, evaporation and absorption

7. Filtration, extraction and drying

8. Purification of organic compounds

1. Chromatography

Industries

4. Chromatography

Industrial Chemical and Instrumental Analysis

1. Instrumental methods of analysis

2. Temperature measuring instruments Process

Instrumentation

and Industrial

Chemical

3. Pressure measuring instruments

4. Liquid level measuring instruments

5. Industrial analysis

6. Modern instrumental methods of analysis

7. Spectroscopic methods

8. Effluent treatment and waste water management

1. Nitration

2. Material testing

3. Water analysis


1. Analysis of fuel

2. Chemical process

III 4+2 = 6

Analysis

2 Qualitative and Synthetic Methods

Nil

2. Halogenation

3. Sulphonation

Process 4. Oxidation IV Chemistry 5. Hydrogenations

6. Alkylation

3. Synthesis of common industrial compounds

4+2 = 6

7. Esterification and hydrolysis

8. Amination

4. Limit tests

6

1. Industrial gases

2. Petroleum refining process

1. Qualitative and quantitative analysis

Research Project

3. Industrial Chemicals

Carbon based chemicals and industrial catalysts

4. Pulp and paper industry

5. Surfactants, Soaps, Detergents and Cosmetics 6. Surfactants, soaps, detergents and cosmetics

7. Cane sugar industry

8. Manufacture of chemicals

1. Pollutants, their statutory limits and air pollution

2. Water Pollution

2. Synthesis of organic compound


4+4+2 +3

=13 V

Industrial Chemicals and

Pollution Management Pollution, its 3. Pesticide Pollution

Management 4. Solid and gaseous wastes

and

Economics

Industrial 5. Industrial economics A 4. Gravimetric and volumetric estimations 6. Industrial economics B

7. Industrial economics C

8. Choice of technology and quality control

3 Polymer Chemistry (01)

1. The science of large molecules

2. Types & general classification of polymers

3. Molecular weight and molecular weight distribution

4. Polymer solutions

Synthesis and Analysis of 1. Preparation of representative Research

Project Polymers polymers

5. Polymer structure and morphology

6. Synthesis, properties and applications of the following Thermosetting polymers

7. Synthesis, properties and applications of the following Thermoplastics polymers

2. Determination of saponification

value, viscosity of PMMA and

hydroxyl value of a resin

Synthetic

Polymer

VI

8. Synthesis, properties and applications of Specific polymers

4+4+2 +3

=13

1. Rheology and mechanical properties of polymers

2. Degradation of polymers

3. Material testing

3. Polymerization techniques

4. Plastic technology

5. Fiber technology

Polymerization

Techniques and

Characterization 4. Determination of molecular

weights of the polymers by

viscosity measurements and Tg

value of phosphate glasses

6. Elastomer technology

7. Additives

8. Compounding

7

Or Pharmaceutical Chemistry (02)

1. Pharmaceutical industry and pharmacopoeias 1. Demonstration of various

pharmaceutical packaging

Research Project

2. Various types of pharmaceutical excipients

3. Evaluation of crude drugs materials and quality control tests

of some materials Experimental

Pharmaceutical Chemistry Pharmaceutical

and

Phytochemicals

2.

Active ingredient analysis 4. Surgical dressing, sutures, ligatures

5. Chemical constitution of plants

6. Phytochemicals

7. Various isolation procedures for active ingredients

8. Pharmaceutical quality control and packaging materials

3. 4+4+2 +3

=13 Evaluation of crude drugs

1. Pharmacology drugs classification

2. Introduction to medicinal chemistry

3. Drug metabolism

4. Principles of Toxicology

5. Microbial fermentation

6. Process of manufacture of the following bulk drugs

7. Biotransformation processes

8. Enzyme systems

Medicinal

Chemistry and

Toxicology

4.

Microbiological testing

Or Agrochemicals (03)

General and Halogenated

Insecticides

1. Types of pest and pesticides

2. Inorganic insecticides

3. Insecticides of plant origin

4. Organ phosphorus insecticides:

5. Organothiophosphorus insecticides

6. Carbamate insecticides

7. Chemical and Biofertilizers

8. Chlorinated hydrocarbons

1. Fungicides

Analysis of Agrochemicals 1. Isolation and estimation of active

ingredients

Research Project

2. Preparation of selected pesticide

formulations

4+4+2 +3

=13 Fungicides and Herbicides 2. Organomercuric compounds

3. Dithiocarbamates

3. Estimation of pesticide residues in

food articles 4. Miscellaneous fungicides

5. Herbicides 4. Isolation of nicotine

6. Fumigants, rodenticides and nematicides

7. Plant growth regulators

8. Formulation of pesticides

8

Total

Credits of

the

COURSE SUBJECT: INDUSTRIAL CHEMISTRY

Year Sem.

I

Prerequisite for

paper

Elective For Major Subject

Paper Title Hours per

Semester subject

Certificate in

Materials and

Techniques in

Chemical

Yes Fundamentals of Industrial

Chemistry Theory-1 Chemistry in 12th 60

60

4

2

Zoo/Bot./Physics/Math/Comp Sci

Basic Analytical Methods Opted Sem-I, Yes Practical-1

Theory Paper-1 Zoo/Bot./Physics/Math/Comp Sci Industries

Material

Techniques

Industries

Science

in

and

Chemical

Passed Sem-I Yes Theoty-1 Zoo/Bot./Physics/Math/Comp Sci 60 4

II

Opted Sem-II, Theory Paper-1

Passed Sem-II

Yes Pracical-2

Theoty-1

Pracical-2

Theoty-1

Practical-2

Theory-1

Theory-2

Practical-3

Materialistic Analysis 60

60

60

60

2

4

2

4

2

4

4

2

3

Zoo/Bot./Physics/Math/Comp Sci.

Diploma in

Industrial

Instrumentation

and Chemical

Analysis

Process Instrumentation and Industrial Chemical Analysis

Industrial Chemical and

Instrumental Analysis

Yes Zoo/Bot./Physics/Math/Comp Sci.

III

IV

Opted Sem-III,

Theory Ppaer-1

Yes


Process Chemistry Passed Sem-III Yes Zoo/Bot./Physics/Math/Comp Sci.

Qualitative and Synthetic Methods

Industrial Chemicals

Opted Sem-IV, Theory Ppaer-1

Passed Sem-IV

Yes 60

60


Yes Zoo/Bot./Physics/Math/Comp Sci. Degree in

Industrial

Chemistry

Pollution, its Management and Industrial Economics

Industrial Chemicals and Pollution Management

Passed Sem-IV Yes 60

60

45

Zoo/Bot./Physics/Math/Comp Sci. V

Opted Sem-V Theory Papers-1 &2

Opted Sem-V

Theory Papers-1 &2

Yes Zoo/Bot./Physics/Math.

…………………… Research

Project ………….

Polymer Chemistry (01)

Synthetic Polymer Passed Sem-V Yes Theory-1

Theory-2

60 4 Zoo/Bot./Physics/Math

VI Polymerization Techniques and

Characterization

Passed Sem-V Yes

Zoo/Bot./Physics/Math/Comp Sci. 60

60

4

2 Practical-3 Synthesis and Analysis of Opted Sem-VI(01) Yes

9

Polymers Theory Papers-1 &2 Zoo/Bot./Physics/Math/Comp Sci. (along with theory paper 1 and paper 2)

…………………… Research Project

…………………….. Opted Sem-VI(01) Theory Papers-1 &2

45 3

Pharmaceutical Chemistry (02)

Pharmaceutical and Phytochemicals

Medicinal Chemistry and Toxicology

Passed Sem-V Yes Theory-1

Theory-2

60

60

4

4

Zoo/Bot./Physics/Math

Passed Sem-V Yes Zoo/Bot./Physics/Math/Comp Sci.

Yes

Zoo/Bot./Physics/Math/Comp Sci. (along with theory paper 1 and paper 2)

……………………

Or Experimental Pharmaceutical Opted Sem-VI(02)

Theory Papers-1 &2 Practical-3 Chemistry 60

45

2

3 Research Project

…………………….. Opted Sem-VI(02) Theory Papers-1 &2

Agrochemicals (03)

General and Halogenated Insecticides

Fungicides and Herbicides

Passed Sem-V Yes Zoo/Bot./Physics/Math

Yes

Theory-1

Theory-2

60

60

4

4 Passed Sem-V

Or Zoo/Bot./Physics/Math/Comp Sci.

Analysis of Agrochemicals

………………….

Opted Sem-VI(03)

Theory Papers-1 &2

Yes Practical-3 Zoo/Bot./Physics/Math/Comp Sci.

(along with theory paper 1 and paper 2)

……………………

60

45

2

3 Research Project

Opted Sem-VI(03) Theory Papers-1 &2

10

11

Semester-I

Paper-1 (Theory)

Course Title: Fundamentals of Industrial Chemistry

Programme:

Certificate in Year: First Semester: First

Materials and Techniques in Chemical Industries

Paper-1: Theory Subject: Industrial Chemistry

Fundamentals of Industrial Chemistry Course Code: B190101T Course Title:

Course outcomes:

There is nothing more fundamental to chemistry than the chemical bond. Chemical bonding is the language of

logic for chemists. Chemical bonding enables scientists to take the more than 100 elements of the periodic table

and combine them in myriad ways to form chemical compounds and materials. Periodic trends, arising from the

arrangement of the periodic table, provide chemists with an invaluable tool to quickly predict an element's

properties. These trends exist because of the similar atomic structure of the elements within their respective

group families or periods, and because of the periodic nature of the elements. Reaction mechanism gives the

fundamental knowledge of carrying out an organic reaction in a step-by-step manner. This course will provide a

broad foundation in chemistry that stresses scientific reasoning and analytical problem solving with a molecular

perspective. Students will gain an understanding of chemical calculations, molecular atomic structures, periodic

properties, chemical bonding, acids-bases, nomenclature of organic compounds, catalysis, fundamental of

organic reactions, knowledge of liquid crystals, solid state, Heat, thermodynamics and chemical equilibrium,

metallurgical operations, metals and alloys.

Credits: 4 Compulsory

Max. Marks: 25+75=100 Min. Passing Marks:

Total No. of Lectures: 60h

Topics No. of

Unit

I

Lectures

Fundamentals of chemical calculations:

Atomic weight, molecular weight, equivalent weight, mole concept, percentage yield,

molarity, molality, normality, Mole Fraction. 06h

08h

Chemical bonding:

Concept of hybridization, hybrid orbitals and molecular geometry, valence shell electron pair

repulsion theory (VSEPR), shapes of the following simple molecules and ions containing lone

II pairs and bond pairs of electrons: H O, NH , SF , 2 3 6 - - 2- +

SF , ClF , I , ClF and SO and H O , molecular orbital theory (MOT), molecular orbital 4 3 3 2 4 3

diagrams bond orders of mononuclear and heteronuclear diatomic molecules and ions (N , O , 2 2

CO, NO, and their ions)

Nomenclature and Catalysis:

Classification, generic and trade names of organic and inorganic chemical’s.

Catalysis- Introduction, types, basic principles, mechanism, factors affecting the performance,

enzyme catalyzed reactions, rate model, industrially important reactions.

III 08h

11

12

Fundamentals of organic chemistry:

A Brief introduction of Cleavage of bonds (homolysis and heterolysis), reaction intermediates

(carbocation, carbanion and free radicals), electrophiles and nucleophiles, aromaticity: IV benzenoids and Hückel’s rule, inductive effect, electrometric effects, mesomeric effect, 08h

resonance, hyperconjugation and stearic effect, tautomerism, isomerism, elementary ideas of

stereochemistry (geometrical and optical).

Liquid crystal and solid state:

Classification and molecular arrangements, liquid state, density, diffusion, viscosity,

evaporation, surface tension, effect of temperature and pressure on surface tension,

Crystal lattices, laws of crystallography, crystal systems, unit cell, space lattice.

V 08h

VI Inorganic Materials of Industrial Importance: Availability, Structure and their use

of Alumina, Silicates, Clays, Mica, Carbon, Zeolites. 06h

08h

Metallurgical Operations, metals and alloys: Pulverization, calcination, roasting, smelting, refining, principles of extraction of metals,

extraction of iron and copper from their ores. VII

Important metals and alloys; mechanical and chemical properties of lead, nickel, iron, titanium

,Tin and their alloys and applications.

Heat, thermodynamics and chemical equilibrium:

VIII A brief introduction of heat capacity of pure gases and gaseous mixtures at constant pressures,

enthalpy changes, entropy, thermodynamic laws, processes and functions, free energy,

thermodynamic criteria and equilibrium constant, effect of temperature and pressure on

equilibrium constants in gaseous system (formation of ammonia).

08h

Suggested Readings:

1. Lee, J.D. Concise Inorganic Chemistry, Pearson Education (2010).

2. J. E. Huheey, E. A. Keiter, R. L. Keiter, O.K. Medhi, Inorganic Chemistry, Principles of Structure and

Reactivity, Pearson Education (2006).

3. Douglas, B.E. and Mc Daniel, D.H., Concepts & Models of Inorganic Chemistry, Oxford (1970).

4. Shriver, D.D. & P. Atkins, Inorganic Chemistry 2nd Ed., Oxford University Press, (1994).

5. Singh J.,Yadav L.D.S., Advanced Organic Chemistry, Pragati Edition.

6. Carey, F. A., Guiliano, R. M.Organic Chemistry, Eighth edition, McGraw Hill Education (2012).

7. Loudon, G. M. Organic Chemistry, Fourth edition, Oxford University Press (2008).

8. Clayden, J., Greeves, N. &Warren, S. Organic Chemistry, 2nd edition, Oxford University Press (2012).

9. Graham Solomons, T.W., Fryhle, C. B. Organic Chemistry, John Wiley & Sons, Inc.

Sykes, P. A guidebook to Mechanism in Organic Chemistry, Pearson Education (2003).

10. Atkins, P. W. & Paula, J. de Atkin’s Physical Chemistry Ed., Oxford University Press 13 (2006).

11. Ball, D. W. Physical Chemistry Thomson Press, India (2007).

12. Castellan, G. W. Physical Chemistry 4th Ed. Narosa (2004).

13. G. M. Barrow: Physical Chemistry Tata McGraw‐Hill (2007).

14. G. W. Castellan: Physical Chemistry 4th Edn. Narosa (2004)

Note: For the promotion of Hindi language, course books published in Hindi may be prescribed by the

University

Suggested online links:

1. https://swayam.gov.in/

2. https://nptel.ac.in/courses/112/104/112104113/

3. https://onlinecourses.nptel.ac.in/noc19_ph14/preview 4. http://heecontent.upsdc.gov.in/Home.aspx

12

13

5. https://cbpbu.ac.in/userfiles/file/2020/STUDY_MAT/CHEM/liquid%20crystal.pdf

6. https://www2.chemistry.msu.edu/faculty/reusch/VirtTxtJml/intro1.htm

7. https://nptel.ac.in/courses/104/103/104103071/#

8. https://ncert.nic.in/textbook.php?kech1=0-7

This course is compulsory for the students of following subjects: Chemistry in 12th Class

Suggested Continuous Evaluation Methods: Students can be evaluated on the basis of score obtained in a mid-term exam, together with the performance of other activities which can include short exams, in-class or

on-line tests, home assignments, group discussions or oral presentations, among others . Or

Assessment and presentation of Assignment/ Research Orientation assignment

04 tests (Objective): Max marks of each test = 10 (Average of all 04 tests)

Overall performance throughout the semester, discipline, participation in different activities.

(10 marks)

(10 marks)

(05 marks)

Course prerequisites: To study this course, a student must have had the subject chemistry in class/12th.

Suggested equivalent online courses: ………………………………………………………………………………………………..

Further Suggestions: ………………………………………………………………………………………………..

13

14

Semester-I

Paper-2 (Practical)

Course Title: Basic Analytical Methods

Programme:

Certificate in


Year: First Semester: First

Paper-2: Practical Subject: Industrial Chemistry

Course Code: B190102P Course Title: Basic Analytical Methods

Course outcomes:

Upon successful completion of this lab course students should be able to know about good laboratory

practice (GLP), calibration apparatus, preparation of standard solutions, solutions of various concentrations,

estimation of components through volumetric analysis, determination of viscosity, surface tension of liquids

and simple laboratory techniques.



Total No. of Practical classes: 60h

No. of Unit

I

Topics Lectures

Good laboratory practices, Calibration of thermometer and burette 05h

10h Determination of:

II Calorific Value of Solid Fuel

Enthalpy of Neutralisation of a Acid and Base

Viscosity and Surface Tension of liquids:

Determination of relative viscosity of a liquid with water and determination of % composition

III of an unknown solution. 15h

30h

Determination of the surface tension of an organic liquid and determination of % composition

of an unknown mixture.

Preparation of standard solutions:

1. Preparation of standard solution of K Cr O . To find out the concentration of unknown 2 2 7

K Cr O solution using Na S O solution as anintermediate. 2 2 7 2 2 3

IV 2. Preparation of standard solution of copper sulphate. To find out the concentration of

unknown copper sulphate solution using Na S O solution as anintermediate. 2 2 3

3. Preparation of standard KMnO4 and ferrous ammonium sulphate solution. To find out the

strength of unknown ferrous ammonium sulphate solution using as an intermediate

Suggested Readings:

1. Saxena Ruchi, Srivastava Alok Kumar, “Read & Do Practical Chemistry”, Kitab Mahal, New Delhi, India (2016).

2. Skoog D. A., West.D.M and Holler .F.J., “Analytical Chemistry: An Introduction”, 7th edition,

Saunders college publishing, Philadelphia (2010).

3. G. Larry Hargis, “Analytical Chemistry: Principles and Techniques” Pearson© (1988)


University.


1. https://www.labster.com/chemistry-virtual-labs/

2. https://www.vlab.co.in/broad-area-chemical-sciences

3. http://chemcollective.org/vlabs

This course can be opted as an elective by the students of following subjects: Chemistry in 12th

Class

14

15

Suggested Continuous Evaluation Methods:

Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)

Course prerequisites: To study this course, a student must have had the chemistry in 12 th Class



15

16

Semester-II

Paper-1 (Theory)

Course Title: Material Science and Techniques in Chemical Industries

Programme:

Certificate in Materials and

Techniques in Chemical Industries

Year: First Semester: Second


Course Title: Material Science and Techniques in Chemical Industries Course Code: B190201T

Course outcomes:

Currently, tremendous progress has been made in development of advanced materials for their environmental

applications and knowledge has been accumulated of the effects of these advanced materials on and their

applications in the environment security, recycling and reuse of raw materials and treatment agents, economic

benefits, and potential problems to our society. Upon completion of this theory course students would gain

knowledge of various materials, surface chemistry and interfacial phenomena, catalysis, metals and alloys,

cement, ceramics and corrosion, polymer, glass, advanced materials and material balance, material balance

without chemical reactions, material balance involving chemical reactions.




Topics No. of

Unit

I

Lectures

Advanced materials and Material balance:

A brief introduction of Nanomaterials, superconductors, biomaterials and fullerenes

Material balance without chemical reactions: Flow diagram for material balance and

material balance calculations for distillation, absorption, evaporation, extraction filtration,

crystallization.

Material balance involving chemical reactions: Concepts of stoichiometric equations,

limiting reactant, excess reactant, percent excess, conversion, yield, selectivity and liquid

09h

08h II

phase reaction, gas phase reaction with or without recycle or bypass.

Utilities in chemical industry:

(i) A brief idea about water, steam and air, Boiler-types, and theire used in chemical

industries.

(ii) A brief idea about fans, blowers, compressors and vacuum pumps, reciprocating pumps,

gear pumps, centrifugal pumps, ejectors used in chemical industries.

Distillation, evaporation:

III 08h

09h

(i) Distillation- Introduction, principle, equipments and their applications of simple,

fractional, steam, vacuum. IV

(ii) Evaporation- Introduction, principle, equipments and their applications of short tube

evaporator, and forced circulation evaporators. Falling film evaporators.

Filtration, extraction:

(i) Filtration- Introduction, principle, equipments and their applications of plate and frame

press filters rotary drum filter, bed filter and centrifuges.

(ii) Extraction- Introduction, principle, equipments and their applications of spray column, V 06h

08h

packed Column, soxhlet extractor, liquid-liquid extraction, acid-base extraction.

VI Absorption and Drying:

(i) Absorption- Introduction, principle, equipments and their applications of Tray (Plate)

towers for absorption, packed towers for absorption.

16

16

(ii) Drying- Introduction, principle, equipments, Purpose of drying, and their applications of equipment- tray dryer, rotary dryer, flask dryer, fluid bed dryer, drum dryer, spray dryer.

VII Crystallization: 08h

04h

Introduction, Equilibrium solubility, nucleation and super saturation, equipment and their

application of tank crystallizer, evaporator crystallizer and circulating liquid evaporator

crystallizer.

VIII Surface chemistry and ceramics: (i) Surface chemistry- Adsorption isotherm, sols, gels, emulsions, micelles, aerosol, effect of

surfactants.

(ii) Ceramics- Introduction of ceramics, types, manufacturing processes and applications of

ceramics.

17

17

Suggested Readings:

1. W. D. Bowen, H. K. Kingery, D.R. Uhlmann, Introduction to Ceramics, Wiley Publishers, New

Delhi (1976)

2. J. A. Kent, J. A. (ed), Riegel’s Handbook of Industrial Chemistry, CBS Publishers, NewDelhi.(1997)

3. G. Cao, Nanostructures and Nanomaterials: Synthesis, Properties & Applications by Guozhong Cao,

Imperial college Press, London (2004).

4. W. D. Callister Jr., D. G. Rethwisch Materials Science and Engineering: An Introduction , John Wiley

& Sons (2018) .

5. E. R. Riegel, Industrial Chemistry, Van Nostrand Reinhold Company; 7th Revised edition (1974) .

6. F. H. Northern, Elements of Ceramics, Addision Weslay Publishing Corp (1952).

7. K H. Büchel, H-H. Moretto, D. Werner, Industrial Inorganic Chemistry, Wiley (2008)

8. W.L.F. Armarego W.L.F. Armarego C. Chai, Purification of Laboratory Chemicals, Elsevier (2009)

9. W. L. Mc. Cabe, J. C. Smith & Parriet Unit Operators of Chemical Engineering, Mc. Graw Hill

Book Company Singapore, 7th edition (2017)


University



2. https://onlinecourses.nptel.ac.in/noc21_cy45/preview

3. https://nptel.ac.in/content/storage2/courses/102103047/PDF/mod4.pdf

4. https://onlinecourses.nptel.ac.in/noc19_ch31/preview


6. https://authors.library.caltech.edu/25034/10/BPOCchapter9.pdf (purification)

chemistry-europe.onlinelibrary.wiley.com/journal/23656549

7. https://onlinelibrary.wiley.com/iucr/itc/Ha/ch7o5v0001/ch7o5.pdf

8. https://link.springer.com/content/pdf/10.1007/s41745-017-0026-4.pdf

file:///C:/Users/dell/Downloads/144_Sample-Chapter.pdf

9. https://www.slideshare.net/knowledge1995/material-balance-for-multiple-units-without-chemical-

equation

This course is compulsory for the students of following subjects: Chemistry in 12th Class

Assessment and presentation of Assignment/ Research Orientation assignment

04 tests (Objective): Max marks of each test = 10 (Average of all 04 tests)

Overall performance throughout the semester, discipline, participation in different activities.

(10 marks)

(10 marks)

(05 marks)

Course prerequisites: To study this course, a student must have had the subject chemistry in clas12th.

Suggested equivalent online courses:

………………………………………………………………………………………………..


17

18

Semester-II

Paper-2 (Practical)

Course Title: Materialistic Analysis

Programme:

Certificate in


Year: First Semester: Second

Paper 2: Practical Subject: Industrial Chemistry

Course Title: Materialistic Analysis Course Code: B190202P

Course outcomes:

Upon completion of this lab course students would gain knowledge of preparing solutions of various

concentrations, determination of concentrations, extraction of compounds from solutions, determination of

refractive index of materials, molar refractivity and specific reactivity of solutions and chromatographic

separations. These techniques and methods are very useful tools in various chemical industries such as

pharmaceuticals, petroleum, food and materials.


Max. Marks: 25+75 =100 Min. Passing Marks:

Total No. of Practical classes: 60h

Topics No. of

Unit

I

Lectures

Analysis of Solution

Molecular weight determination by depression in freezing point and elevation in boiling 10h

10h

points.

Extraction process: Phase diagram, partition coefficient.

To find out the partition coefficient of – II

Iodine between CCl4 and water

Acetic acid between water and benzene.

Preparation of Inorganic Salts :

Potash Alum, Mohar’s Salt, Purssian blue, Tetramine Copper Sulphate. III

IV

20h

20h

Chromatography: Column, paper, thin layer

To separate and identify the amino acids by ascending paper chromatography.

To separate and identify the organic compound by the use of thin layer chromatography.

Separation of a mixture of organic compound by column chromatography.

Suggested Readings:

1. A.I. Vogel, A.R. Tatchell, B.S. Furnis ,A.J. Hannaford, P.W.G. Smith, Vogel's Textbook of Practical

Organic chemistry (1989)

2. B.S. Furniss, A.J. Hannaford, P.W.G. Smith, A.R. Tatchell,. Vogel's Textbook of Practical Organic

Chemistry, 5e, Pearson (2003).

3. V. D. Athawale, P. Mathur, Experimental Physical Chemistry, New Age International (P) Ltd.

4. G. Svehla, Vogel's Qualitative Inorganic Analysis, 7e Pearson (2008).

5. G.D. Christian, Analytical Chemistry, 6th Ed. John Wiley & Sons, New York (2004).

6. Harris, D.C., Exploring Chemical Analysis, 9th Ed. New York, W.H. Freeman (2016).


1. https://fac.ksu.edu.sa/sites/default/files/vogel_-_practical_organic_chemistry_5th_edition.pdf

2. http://faculty.chas.uni.edu/~manfredi/860-121/ORG%20LAB%20MAN%20S08.pdf 3. https://www.ipinnovative.com/media/open-access-books/Practical_Lab_Manua l_of_

18

19

Pharmaceutical_Organic_Chemistry_-1_ Low.pdf

4. https://gtu.ge/Agro-Lib/Vogels_TEXTBOOK_OF_QUANTITATIVE_CHEMICAL_ANALYSIS_

5th_ed -_G_H_Jeffery.MsuCity.pdf


Class

Suggested Continuous Evaluation Methods: Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)




19

20

Semester-III

Paper-1 (Theory)

Course Title: Process Instrumentation and Industrial Chemical Analysis

Programme: Semester: Third

Diploma in Industrial Instrumentation

and Chemical Analysis

Year: Second


Course Title: Process Instrumentation and Industrial Chemical Analysis Course Code: B190301T

Course outcomes:

On successful completion of students will gain the knowledge of important topics of industrial chemistry

such as chromatography, thermal instrumentations, pressure measuring devices, liquid level measuring

instruments, Industrial analysis, Modern instrumental analysis, spectroscopic methods, Effluent treatment,

and waste water management.


Max. Marks: 25+75 = 100 Min. Passing Marks:


Topics No. of

Unit

I

Lectures

Chromatography:

Principles, methods and applications of paper chromatography, TLC, GLC, HPLC, GLC and 10h GPC.

Temperature measuring instruments:

II Glass thermometers, bimetallic thermometer, pressure spring thermometer, vapour field 07h

07h

thermometers, resistance thermometers and radiation pyrometers.

Pressure measuring instruments:

III Manometers, barometers, bourdan pressure gauge; below type, diaphragm type pressure

gauges, macleod gauges, pirani gauges etc.

Liquid level measuring instruments:

Direct-indirect level measurements, float type liquid level gauge, ultrasonic level gauges;

bubbler system, viscosity (Ostwald viscometer), surface tension (stalagmometer) and density

(pycnometer) measurement.

IV

V

8h

Industrial analysis:

Sampling procedures, sampling of bulk materials, techniques of sampling solids, liquids

and gases, collecting and processing of data, particle size determination, rheological

properties of liquids, plastics and their analysis.

10h

Modern instrumental methods of analysis:

VI pH and conductivity measurements with special reference to water and soil analysis, optical 4h

6h

rotation of chiral compound, spectrophotometer.

Spectroscopic methods: (theories applications to simple organic molecules)

VII UV-visible spectroscopy, Infra Red spectroscopy, Raman spectroscopy, NMR Spectroscopy,

Mass spectroscopy.

Effluent treatment, waste water management:

Principles and equipment for aerobic, anaerobic treatment like i) Anaerobic high-rate

treatment of industrial wastewater and its reuse in industries; ii) UASB reactors; iii) EGSB

reactors; iv) EGSB/IC reactors; and v) Industrial treatment examples.

Adsorption, filtration, sedimentation, bag filters, electrostatic precipitator, sewage treatment

plants (STPs)

VIII 8h

20

21

Suggested Readings:

1. Metcalf and Eddy, Wastewater Engineering Publisher - McGraw-Hill (2013) .

2. H.S. Peavy, D.R. Rowe and G. Tchobanoglous; Environmental Engineering Publisher - McGraw-Hill

(2015)

3. M. M. Benjamin, D. F. Lawler, Water Quality Engineering: Physical / Chemical Treatment Processes

by La - John Wiley & Sons (2013).

4. V. Ranade V. Bhandari Industrial Wastewater Treatment, Recycling and Reuse, Elsevier (2014)

5. Reynolds P. Richard, Unit Operations and Processes in Environmental Engineering) by T.D.

Publisher-CL Engineering (1996).

6. Khopkar, S.M. Basic Concepts of Analytical Chemistry. New Age International Publisher (2009).

7. Christian, G.D. Analytical Chemistry, 6th Ed. John Wiley & Sons, New York (2004).

8. Harris, D.C.: Exploring Chemical Analysis, 9th Ed. New York, W.H. Freeman (2016).

9. Pavia, D. L. et al. Introduction to Spectroscopy, 5th Ed. Cengage Learning India Ed.

10. Willard, H.H. et al.: Instrumental Methods of Analysis, 7th Ed. Wardsworth Publishing Company,

Belmont, California, USA (1988).


1. https://www.mooc-list.com/tags/physical-chemistry

2. https://www.coursera.org/learn/physical-chemistry

3. https://ocw.mit.edu/courses/chemistry/5-61-physical-chemistry-fall-2017/

4. http://heecontent.upsdc.gov.in/Home.aspx




This course can be opted as an elective by the students of following subjects: Chemistry in 12 th

Class

Suggested Continuous Evaluation Methods: Students can be evaluated on the basis of score

obtained in a mid-term exam, together with the performance of other activities which can include

short exams, in-class or on-line tests, home assignments, group discussions or oral presentations,

among others . Or

Assessment and presentation of Assignment

04 Unit tests (Objective): Max marks of each unit test = 10 (average of all 04 unit tests)

(10 marks)

(10 marks)

Overall performance throughout the semester (Discipline, participation in different activities)

(05 marks)

Course prerequisites: To study this course, a student must have had the chemistry in class 12th



21

22

Semester-III

Paper-2 (Practical)

Course Title: Industrial Chemical and Instrumental Analysis Programme:

Diploma in

Industrial Instrumentation and

Chemical Analysis

Semester: Third Year: Second


Course Code: B190302P Course Title: Industrial Chemical and Instrumental Analysis

Course outcomes:

Students gain knowledge and skill related to this paper are as follows-

Instrumental methods of analysis, Material testing, Water analysis, Use of transducers for measuring flow

control and Flow measuring devices- floats.




Topics No. of

Unit

I

Lectures

Instrumental methods of analysis:

Use of colorimeter, flame photometer, pH meter, potentiometer, conductometer. 15h

15h Material testing:

II Testing of plastics/rubber, Young’s modulus, optical, thermal, mechanical and electrical

properties.

Water analysis: III 10h

20h

Solid content, hardness, COD and other tests as per industrial specifications.


IV Analysis of common raw materials as per the industrial specifications such as phenol, aniline, formaldehyde, hydrogen peroxide, acetone, etc.

Suggested Readings:

1. G. D .Christian, Analytical Chemistry, 6th Ed. John Wiley & Sons, New York (2004).

2. D.C. Harris, Exploring Chemical Analysis, 9th Ed. New York, W.H. Freeman (2016).

3. E. Stocchi, Industrial Chemistry, Vol -I, Ellis Horwood Ltd. UK. (1990).

4. J. A .Kent, (ed) Riegel’s Handbook of Industrial Chemistry, CBS Publishers, New Delhi, (1997).

5. Pani, B. Textbook of Environmental Chemistry, I.K. International Publishing House, (2017).

6. A. K .De, Environmental Chemistry, New Age International Pvt, Ltd, New Delhi (2012).

7. S. M .Khopkar,., Environmental Pollution Analysis, New Age International Publishe (2010)

8. B. D. Khosla,.; V. C. Garg,. &A. Gulati, Senior Practical Physical Chemistry, R. Chand &

Co., New Delhi (2011).

9. C. W. Garland,.Nibler, J. W. & Shoemaker, D. P. Experiments in Physical Chemistry 8th Ed.;

McGraw-Hill: New York (2003).

10. A. M. Halpern,. & McBane, G. C. Experimental Physical Chemistry 3rd Ed.; W.H. Freeman &

Co.: New York (2003


Class


Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)

22

23




23

24

Semester-IV

Paper-1 (Theory)

Course Title: Process Chemistry

Programme:

Diploma in


Chemical Analysis

Semester: Fourth Year: Second


Course Title: Process Chemistry Course Code: B190401T

Course outcomes:

Upon completion of this course the students will have the knowledge and skills regarding various chemical

process of organic chemistry such as nitration, sulphonation, halogenation, oxidation, hydrogenation,

alkylation, ammination, esterification and hydrolysis. These organic chemical processes are important tools to

synthesis of important pharmaceuticals or drug molecules and other industrially important organic compounds.




Topics No. of

Unit

I

Lectures

Nitration:

Introduction, nitrating agents, mechanism and nitration of paraffin 08h hydrocarbons - benzene to nitrobenzene and m-dinitrobenzene, chlorobenzene to o- & p-

nitrochlorobenzenes, acetanilide to p-nitro acetanilide and toluene.

Halogenation:

Introduction, reagents for halogenations, halogenations of aromatics – II 08h

08h

side chain and nuclear halogenations, commercial manufacture of chlorobenzene, chloral,

monochloroacetic acid and chloromethanes.

Sulphonation:

Introduction, sulphonating

sulphonation, mechanism of sulphonation, commercial sulphonation of

naphthalene, alkyl benzene.

agents, chemical and physical factors in III benzene,

Oxidation:

Introduction, types of oxidation reactions, oxidizing agents, mechanism of IV oxidation of naphthalene, phthalamide and anthracene, liquid phase oxidation and vapour

phase oxidation, commercial manufacture of benzoic acid, maleic anhydride, phthalic anhydride, acetaldehyde, acetic acid.

08h

06h

Hydrogenations:

Introduction, thermodynamics of hydrogenation reactions, catalysts for hydrogenation

reactions, hydrogenation of vegetable oils, manufacture of methanol from carbon monoxide

and hydrogen, catalytic reforming.

V

Alkylation:

Introduction, types of alkylation, alkylating agents, thermodynamics and mechanism of

alkylation reactions, manufacture of phenyl ethyl alcohol and alkyl benzenes (for detergent

manufacture).

VI 06h

08h

Esterification and Hydrolysis:

Introduction, esterification reactions by organic acids, commercial manufacture of ethyl

acetate, vinyl acetate, cellulose acetate. VII

Introduction, hydrolyzing agents, mechanism of hydrolysis.

24

25

Amination:

By reduction: Introduction, methods of reduction, metal and acid, catalytic sulfide,

VIII electrolytic, metal and alkali sulfites, metal hydrides, sodium metal, conc. caustic oxidation- 08h

reduction, commercial manufacture of aniline, m-nitroaniline, p-aminophenol. By aminolysis: Introduction, aminating agents, factors affecting.

Suggested Readings:

1. R. N. Morrison & R. N. Boyd, Organic Chemistry, Dorling Kindersley (India) Pvt. Ltd. (Pearson

Education).

2. P. A. Sykes, Guidebook to Mechanism in Organic Chemistry, Pearson Education (2003).

3. F. A. Carey, Guiliano, R. M.Organic Chemistry, Eighth edition, McGraw Hill Education (2012).

4. G. M. Loudo , Organic Chemistry, Fourth edition, Oxford University Press, 2008. 5. J. Clayden, N. Greeves & S. Warren, Organic Chemistry, 2nd edition, Oxford University Press (2012).

6. T.W. Graham Solomons & C. B. Fryhle, Organic Chemistry, John Wiley & Sons, Inc.

7. J. G. Smith, Organic Chemistry, Tata McGraw-Hill Publishing Company Limited.

8. J. March, Advanced Organic Chemistry, Fourth edition, Wiley.

9. Alok Kumar Srivastava, “Organic Chemistry-II”, Mahaveer Publication, Dibrugarh, Assam,

India (2021). Note: For the promotion of Hindi language, course books published in Hindi may be prescribed by the

University


1. http://heecontent.upsdc.gov.in/Home.aspx

2. https://www2.chemistry.msu.edu/faculty/reusch/VirtTxtJml/intro1.htm

3. https://nptel.ac.in/courses/104/103/104103071/#

4. https://swayam.gov.in/

This course can be opted as an elective by the students of following subjects: Chemistry in 12th Class

Suggested Continuous Evaluation Methods: Students can be evaluated on the basis of score obtained

in a mid-term exam, together with the performance of other activities which can include short

exams, in-class or on-line tests, home assignments, group discussions or oral presentations, among

others . Or


04 Unit tests (Objective): Max marks of each unit test

(10 marks)

(10 marks) = 10 (average of all 04 unit tests)


(05 marks)




25

26

Semester-IV

Paper-2 (Practical)

Course Title: Qualitative and Synthetic Methods

Programme:

Diploma in


Chemical Analysis

Semester: Fourth Year: Second


Course Title: Qualitative and Synthetic Methods Course Code: B190402P

Course outcomes:

Students gain knowledge and skill related to this paper are as follows.

Utilities in chemical industry, distillation, evaporation and absorption, filtration and extraction, drying,

crystallization and polymorphism, Fluid Flow, Heat Transfer.




Topics No. of

Unit

I

Lectures

Analysis of fuel 05h

20h

Determination of flash point, ignition point of liquids and smoke point of a fuel.

Chemical process – One or two examples of each of the following unit processes.

II Nitration, sulphonation, friedel-crafts reaction, esterification, hydrolysis, oxidation,

halogenations, chlorosulphonation, reduction and amination.

Synthesis of common industrial compounds: Each step reaction monitor by TLC. III 4-Bromo aniline, 3-Nitroaniline, Sulphanilamide, 4-Amino benzoic acid, 4-Nitro

benzoicacid, Dihalobenzenes, Nitrohalobenzenes. 20h

15h Limit tests

IV Limit tests for chlorine, arsenic and heavy metals – Pb, As, Hg, Fe and ash content.

Suggested Readings:

1. A.I. Vogel, A.R. Tatchell, B.S. Furnis , A.J. Hannaford, P.W.G. Smith, Vogel's Textbook of Practical

Organic chemistry (1989).

2. B.S. Furniss, A.J. Hannaford, P.W.G. Smith, A.R. Tatchell,. Vogel's Textbook of Practical Organic


3. Organic Chemistry, Prentice-Hall, 5th edition (1996).

4. Mann, F.G. & Saunders, B.C. Practical Organic Chemistry Orient-Longman (1960). 5. Harris, D.C.Exploring Chemical Analysis, 9th Ed. New York, W.H. Freeman (2016).

6. Khopkar, S.M. Basic Concepts of Analytical Chemistry. New Age International Publisher (2009).

7. Svehla, G. Vogel’s Qualitative Inorganic Analysis, Pearson Education (2012).

8. Mendham, J. Vogel’s Quantitative Chemical Analysis, Pearson (2009).

Suggestive digital platforms web links:

1. https://www.labster.com/chemistry-virtual-labs/

2. https://www.vlab.co.in/broad-area-chemical-sciences

3. http://chemcollective.org/vlabs


Class

26

27


Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)

Course prerequisites: To study this course, a student must have Opted Sem-V Theory Ppaer-1 &2



27

28

Semester-V

Paper-1 (Theory)

Course Title: Industrial Chemicals

Programme:

Degree in Semester: Fifth Year: Third

Industrial Chemistry


Course Title: Industrial Chemicals Course Code: B190501T

Course outcomes:

The chemical industry comprises the companies that produce industrial chemicals. Central to the modern world

economy, it converts raw materials into more than 70,000 different products. On successful completion of this

course students will gain the knowledge and skills related to various industrial gases, petroleum refining

process, carbon based chemicals and industrial catalysts, pulp and paper industry, surfactants, soaps, detergents

and cosmetics, cane sugar industry, manufacture of heavy organic chemicals, heavy inorganic chemicals, fine

chemicals.




Topics No. of

Unit

I

Lectures

Industrial gases:

Manufacture, uses and economics of N , O , H , CO . 03h

05h

2 2 2 2

Petroleum refining process:

II Introduction, distillation, octane number, additives, hydro treating, cracking, reforming,

alkylation and polymerization, separation of natural gas (methane production).

Carbon based chemicals and industrial catalysts:

Manufacture, properties and uses of methanol, formaldehyde, acetic acid, chloro fluoro carbons

and fluoro carbons.

Industrial catalysts like raney nickel, other forms of nickel, palladium and supported palladium,

copper chromate, vanadium and platinum based catalyst, aluminium alkoxides, titanium

tetrachloride and titanium dioxide.

III

IV

V

10h

05h Pulp and paper industry:

Manufacture of pulp and paper and their uses.

Surfactants, soaps, detergents and cosmetics:

(i) Introduction, cationic and anionic surfactants, straight chain detergent intermediates linear

alcohol sulphates (AS), linear alcohol ethoxy sulphates(AES) and linear alkyl benzene

sulfonates (LAS), amphoterics and detergent builders

(ii) Definition and characteristics of cream, hair dyes, tooth paste, talcum powder, sun tan

lotion, perfumes and essential oils.

10h

07h

Cane sugar industry:

Manufacture of white crystalline sugar, extraction of the juice, clarification (lime defection

process, by sulphate ion and by carbonation), evaporation, crystallization and refining of

sugar, uses of bagasse.

VI

Manufacture of heavy organic and inorganic chemicals: (with respect to raw material,

production process, quality control, hazards and safety, effluent management)

A. Heavy organic chemicals:

VII Fischer-tropsch synthesis, applications and uses of zeolites as catalyst, propyl alcohol, 1,4- 12h

butanediol, vinyl chloride, pyridines, picolines, phthalic anhydrides, glycerol, sorbitol,

chloroform, ethanolamine.

B. Heavy inorganic chemicals:

28

29

Ammonium phosphates, carbon blacks, manufacture of graphite and carbon, calcium carbide, silicon carbide, sodium thiosulphate, borax and boric acid.

Manufacture of fine chemicals: (with respect to Raw material, Production process, Quality

control, Hazards and safety, Effluent management)

Sodium borohydrate, lithium aluminium hydride, sodium ethoxide, paracetamol, indigo,

vat dyes. Essential oils, surfactants and emulsifying agents, coloring agents- manufacture

of some natural and synthetic colors. Flavouring agents – fragrance and food additives. Biochemical reagents – ninhydrin, tetrazolium blue, 1,2-naphthaquinone-4-sulphonate.

VIII 08h

Suggested Readings:

1. B. K. Sharma, Industrial Chemistry, GOEL Publishing House (2000).

2. M. Fahim, T. Al-Sahhaf, A. Elkilani, Fundamentals of Petroleum Refining, 1st edition, Elsevier Science

(2010).

3. Pesticide Calcer Publication, P. B. Pandey.

4. Principle Industrial Chemistry, C. A. Clausion, G. C.Mattson, Wiley (1978).

5. W. L. Mc. Cabe, J. C. Smith & Parriet ,Unit Operators of Chemical Engineering, Mc. Graw Hill Book

Company Singapore (2017).

6. A. F. Mills. Heat Transfer, CRC Press, (1992).

7. K.W. Britt, Handbook of pulp and paper technology Book on Pulp & Paper Industries, 2Ed (2004).










others . Or


04 Unit tests (Objective): Max marks of each unit test = 10

(average of all 04 unit tests)

(10 marks)

(10 marks)


(05 marks)




29

30

Semester-V

Paper-2 (Theory)

Course Title: Pollution, its Management and Industrial Economics

Programme:

Degree in


Year: Third Semester: Fifth


Course Title: Pollution, its Management and Industrial Economics Course Code: B190502T

Course outcomes:

Students gain knowledge and skills related to this paper are as follows.

Pollutants, their statutory limits and air pollution, water pollution, pesticide pollution, solid & gaseous wastes,

factors involved in project cost estimation, capital formation, methods of determining depreciation, some

aspects of marketing, pricing policy, profitability criteria, entrepreneurship, choice of technology and quality

control.



Total No. of Lectures: 60 h

Topics No. of

Unit

I

Lectures

Pollutants, their statutory limits and air pollution:

Definition and classification of pollutants, primary and secondary pollutants, pollution

evaluation methods, sources and classification of air pollution, major air pollutants and their

health impacts, phenomenon of acid rain, photo chemical smog and ozone depletion,

composition of fly-ash, pollution control equipment/techniques.

Water pollution:

Types of water pollution, organic and inorganic pollutants, point and nonpoint sources of

water pollution, estimation of chlorine in water, measurement of BOD & COD, techniques for

removal of waste from water.

08h

08h II

Pesticide pollution:

Classification of chemical pesticides, examples of organochlorines and organophosphates,

III persistent organic pollutants (POPs) and their half-lives, environmental effects of pesticides, 08h

soil and water contamination and its impact, bioaccumulation of pesticides and pesticide

contamination in food.

Solid & gaseous wastes:

Removal of solid contaminants of wastes- coagulation, sedimentation, flocculation, solid waste

IV disposal, incineration, fuel pelletization, soil conditioning 10h

06h

Adsorption, catalytic/non catalytic conversion, recovery of important gases, CO , SO , NO etc.

electrostatic precipitation and bag filters. 2 2

Soil economics A: Factors involved in project cost estimation, methods employed for the

estimation of capital investment, capital formation, elements of cost accounting, interest and

investment costs, time value of money equivalence. V

Soil economics B:Methods of determining depreciation, some aspects of marketing, pricing

VI policy, profitability criteria, economics of selecting alternatives, variation of cost with capacity, 06h

06h

08h

break-even point, optimum batch sizes, production scheduling etc.

Soil economics C: Need, scope and characteristics of entrepreneurship, special schemes for

technical entrepreneurs development (STED), exposure to demand based, resource based,

service based, import substitute and export promotion industries, criteria for principles of

products selection and developments.

VII

Choice of technology and quality control:

Plant and equipments, techno-economic feasibility of the projects, plant layout and process VIII

30

31

planning for the project.

Quality control, quality assurance and testing of the product, packaging, advertising and after

sales service.

Suggested Readings:

1. R.K. Trivedy, N.S. Raman, Industrial Pollution and Environmental Management, Scientific Publishers

Journals (2002).

2. M. Brusseau, I. Pepper, C. Gerba, Environmental and Pollution Science, Third Edition, Elsevier

Science (2019).

3. H. S. Rathore, L.L.L. Nollet, Pesticides: Evaluation of Environmental Pollution, CRC Press (2012).

4. B. K. Sharma, Industrial Chemistry (including Chemical Engineering), GOEL Publishing House(2000).

5. P. F. Rad, Project Estimating & Cost Management, Berrett Kochler Publisher (2001).







6. https://nptel.ac.in/content/storage2/courses/120108004/module1/lecture1.pdf





others . Or



(10 marks)

(10 marks)


(05 marks)




31

32

Semester-V

Paper-3 (Practical)

Course Title: Industrial chemicals and pollution management

Programme:

Degree in Year: Third Semester: Fifth



Course Code: B190503P Course Title: Industrial chemicals and pollution management

Course outcomes:


Determination of Flash and Fire point, Determination of (i) acid value- gum, and resin, (ii) iodine number-

linseed oil, castor oil (iii) saponification value - coconut oil, Synthesis of organic compound: Paracetamol,

Aspirin, Oils of winter green and Urea formaldehyde resin, Analysis of common raw materials as per the

industrial specifications such as phenol, aniline, formaldehyde, hydrogen peroxide, acetone, Gravimetric and

volumetric estimations.




Topics No. of

Unit

I

Lectures

Qualitative and quantitative analysis:

Determination of flash and fire point

Determination of (i) acid value- gum and resin (ii) iodine number- linseed oil, castor oil (iii) saponification value - coconut oil.

Synthesis of organic compound: Each step reaction monitor by TLC. Paracetamol, Aspirin, oils of winter green and urea formaldehyde resin.


10h

10h II

III Analysis of common raw materials as per the industrial specifications such as phenol, aniline, formaldehyde, hydrogen peroxide, acetone, etc.

IV Gravimetric and volumetric estimations.

20h

20h

Suggested Readings:

1. Ruchi Saxena, Alok Kumar Srivastava, “Read & Do Practical Chemistry”, Kitab Mahal, New Delhi, India, 2016.

7. A.I. Vogel, A.R. Tatchell, B.S. Furnis , A.J. Hannaford, P.W.G. Smith, Vogel's Textbook of Practical

Organic chemistry (1989)

2. B.S. Furniss, A.J. Hannaford, P.W.G. Smith, A.R. Tatchell, Vogel's Textbook of Practical Organic

Chemistry, 5e, Pearson (2003)s


Class. Suggested Continuous Evaluation Methods:

Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)

Course prerequisites: To study this course, a student must have Opted Sem-V Theory Ppaer-1 &2



32

33

Semester-VI

Paper-1 (Theory)

Course Title: Synthetic Polymer

Programme:

Degree in Semester: Six Year: Third



Course Title: Synthetic Polymer Course Code: B190601T

Course outcomes:


The science of large molecules, types & general classification of polymers, molecular weight and molecular

weight distribution, polymer solutions, structure and morphology, synthesis, properties and applications of the

following thermosetting polymers, thermoplastics polymers, conducting polymers, light emitting polymers and

biodegradable polymers. This course mainly includes study of polymers synthesis, polymer properties, polymer

processing, polymer testing, polymer degradation, polymer reaction, composites and applications. The course

is career oriented and can provide various opportunities in the field of polymers.

Credits: 4 Elective



Topics No. of

Unit

I

Lectures

The science of large molecules:

Brief history, general definitions, basic chemistry and nomenclature of polymers, brief history

of macromolecular science, general characteristics of polymers in comparison with

common organic compounds. Types & general classification of polymers:

Natural and synthetic polymers, organic & inorganic polymers, thermoplastics &

05h

07h

thermosetting polymers, homo, hetero and copolymers, necessity of copolymers and

II copolymerization, block and graft copolymers, conducting polymers, biopolymers.

Addition, condensation, free radical, ionic (anionic and cationic) and coordination

polymerization, kinetics and mechanism of addition, condensation and ionic polymerization

reactions.

Molecular weight and molecular weight distribution:

III Number, weight & viscosity average molecular weights of polymers, methods of determining molecular weights, significance of molecular weight distribution.

05h

05h

Polymer solutions, structure and morphology:

IV Criteria of polymer solubility, solubility parameters, fractionation of polymers with special

reference to gel permeation chromatography.

Polymer structure and morphology:

A brief idea of microstructure of polymers based on chemical and geometrical structures,

V intermolecular forces and chemical bonding in polymers, linear, branched and cross linked 08h

polymers, stereoregular polymers, crystallinity in polymers, effect of crystallinity on the

properties of the polymers, factors affecting the crystallinity.

Synthesis, properties and applications of the following Thermosetting polymers:

Unsaturated polyesters: Fibre reinforced plastics (FRP), Polyurethanes, Phenol-formaldehyde,

VI urea-formaldehyde, melamine-formaldehyde, Polycarbonates, Alkyl resins and amino resins, Epoxy resins – grades and curing process and its importance with mechanism, Silicones. Elastomers – polyisoprene, polybutadiene and neoprene.

08h

11h Synthesis, properties and applications of the following Thermoplastics polymers:

VII Polyethylene – HDP, LDP, LLDP. Polyvinyl chloride, PTFE (Teflon).

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34

Polystyrene – SBR, ABS, SAN.

Vinyl polymers – PVA, PVB.

Polyacetals, Polyamides – nylon-6, nylon-66

Polyethers and Polyesters – terephthalates (PET). Cellulosic polymers.

Acryclic Plastics- PMMA

Synthesis, properties and application of specific polymers:

1. Conducting polymers: Polyacetylene (PAc), Polyaniline (PANI), Polythiophene (PTh)

2. Light emitting polymers: Polyparaphenylene (PPP), Polyparaphenylenevinylene (PPPV),

Polyfluorene (PF). VIII 11h

3. Biodegradable polymers: Polyglycolic acid (PGA),Polyhydroxybutyrate (PHB),

Polyhydroxybutyrate-co-valerate (PHBV)

Suggested Readings:

1. U. R. Gowariker, N.V. Vishwanathan and J. Shreedhar, Polymer Science by, New Age International

Publishers, New Delhi (1987).

2. H. G. Elias, an introduction to polymer science, Wiley (1997).

3. An Introduction to polymer science and Technology, N. B. Singh, S. S. Das, New age Internal

Publisher, New Delhi (2017).

4. P. Chandrasekhar Conducting Polymers, Fundamentals and Applications, Springer (2013).

5. A. Lendlein, A. Sisson, Handbook of Biodegradable Polymers: Isolation, Synthesis, Characterization

and Applications, Wiley‐VCH (2011).

6. A. J. Domb, J. Kost, D.d Wiseman, Handbook of Biodegradable Polymers, CRC Press (2019).

7. Handbook of Thermoset Plastics, 4th Edition, Hanna Dodiuk, Elsevier (2021).

8. F.W. Billmeyer, Textbook of polymer Science, John Wiley &Sons, New York (1984).



2. https://nptel.ac.in/content/storage2/courses/104103071/pdf/mod16.pdf







others .Or


04 Unit tests (Objective): Max marks of each unit test = 10

(average of all 04 unit tests)

(10 marks)

(10 marks)


(05 marks)

Course prerequisites: To study this course, a student must have had the chemistry in class 12 th



34

35

Semester-VI

Paper-2 (Theory)

Course Title: Polymerization Techniques and Characterization

Programme:

Degree in Year: Third Semester: Six

Subject: Industrial Chemistry

Course Title: Polymerization Techniques and Characterization


Paper-2: Theory

Course Code: B190602T

Course outcomes:

This course mainly includes study of polymers synthesis, polymer properties, polymer processing, polymer

testing, polymer degradation, polymer reaction, composites and applications. This course is career oriented and

can provide various opportunities in the field of polymers. After successful completion of this paper, students

will gain knowledge and skills related to this paper is as follows-

Rheology and mechanical properties of polymers, degradation of polymers, polymerization techniques, plastic

technology, fiber technology, elastomer technology, additives and compounding.

Credits: 4 Elective



Topics No. of

Unit

I

Lectures

Rheology and mechanical properties of polymers:

Viscous flow, rubber elasticity, visco elasticity, glassy state and the glass transition

temperature, (GTT) factors affecting glass transition temperature, optical, electrical and thermal properties of polymers.

10h

Degradation of polymers: II Degradation of polymers by thermal, oxidative, mechanical and chemical methods, random 07h

07h

degradation and chain depolymerization.

Polymerization techniques:

A general idea of bulk, solution, suspension, emulsion, polymerization processes. III

Plastic technology:

General concept of plastics; A brief idea of compression molding, injection molding, extrusion

IV and blow molding techniques, thermoforming and foaming, casting, extrusion, fiber spinning,

coating and calendaring, vulcanization of elastomers, reinforcing (fiber reinforced plastics -

FRP).

10h

Fiber technology: V General concept of fibers; A brief idea of textile and fabric properties, fiber spinning (wet, dry 08h

and melt spinning)

Elastomer technology:

General concept of elastomers; Vulcanization of elastomers, and its chemistry. VI 08h

07h Additives:

VII A general idea of fillers, plasticizers, antioxidants, colourants, fire retardants, thermal

stabilizers.

Compounding:

A general idea compounding ingredients etc. VIII 03h

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36

Suggested Readings:

1. Joel R. Fried, Polymer Science &Technology, Pearson Prentice Hall; 3rd edition (2014).

2. B. K. Sharma, Polymer Chemistry,. Krishna Prakashan Media (2020).

3. D. J. Williams, Polymer Science & Engineering, Prentice Hall Inc (1971).

4. J.A. Brydson. Plastics Material, A. Brydson, Vth Edition, Butter Worth Heinemonn (1989).

5. G. Odian, Principle of Polymerization, Godian IInd edition, John Wieley & Sons (2004).


1. https://www.digimat.in/nptel/courses/video/103103139/L20.html


3. https://www.youtube.com/watch?v=GltrPpUJS9Q






exams, in-class or on-line tests, home assignments, group discussions or oral presentations, among others .Or



(10 marks)

(10 marks)


(05 marks)




36

37

Semester-VI

Paper-3 (Practical)

Course Title: Synthesis and Analysis of Polymers

Programme:




Course Title: Synthesis and Analysis of Polymers Course Code: B190603P

Course outcomes:


Preparation of representative polymers such as bulk polymerization like polystyrene, PMMA Nylon and polysulphide rubber, solution polymerization like phenol formaldehyde, urea formaldehyde, determination of (i) saponification value - polyester (ii) viscosity of PMMA (iii) hydroxyl value of a resin, testing of plastics/rubber, Young’s modulus, optical, thermal, mechanical and electrical properties, determination of molecular weights of the polymers by viscosity measurements and T value of phosphate glasses. g

Credits: 2 Elective

Max. Marks: 25+75 Min. Passing Marks:


Topics No. of

Unit

I

Lectures

Preparation of representative polymers:

Bulk polymerization: Polystyrene, PMMA Nylon and polysulphide rubber

Solution polymerization: Phenol formaldehyde, urea formaldehyde

Determination of (i) saponification value - polyester (ii) viscosity of PMMA (iii) hydroxyl value of a resin.

15h

15h II

Material testing:

III Testing of plastics/rubber, Young’s modulus, optical, thermal, mechanical and electrical 15h

15h

properties.

Determination of molecular weights of the polymers by viscosity measurements and Tg value

of phosphate glasses. IV

Suggested Readings:

1. J. B. Rabek, Experimental methods In Polymer Chemistry, Wiley–Blackwell (1980).

2. D. G. Hundiwale, Experiments In Polymer Science Paperback, New Age International Private

Limited; First edition (2008).

3. T. Tanaka, Experimental Methods in Polymer Science, Academic Press (1999).


Class


Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)

Course prerequisites: To study this course, a student must have Opted Sem-VI Theory Ppaer-1 &2



37

38

Semester-VI

Paper-1 (Theory)

Course Title: Pharmaceutical and Phytochemicals Programme:




Course Title: Pharmaceutical and Phytochemicals Course Code: B190605T

Course outcomes:

After successful completion of this course, students will gain the knowledge and skills related to this paper

are as follows-

Pharmaceutical industry and pharmacopoeias, various types of pharmaceutical excipients, evaluation of crude

drugs, surgical dressing, sutures, ligatures, phytochemicals, chemical constitution of plants, various isolation

procedures for active ingredients, pharmaceutical quality control and packaging materials

Credits: 4 Elective



Topics No. of

Unit

I

Lectures

Pharmaceutical industry and Pharmacopoeias:

Historical background and development of pharmaceutical industry in India in brief,

development of Indian pharmacopoeia and introduction to B.P., U.S.P., E.P., N.F. and other

important pharmacopoeias, introduction to various types of formulations and roots of

administration, aseptic conditions, need for sterilization, various methods of sterilization.

Various types of pharmaceutical excipients:

Chemistry, process of manufacture and quality specifications – Glidants, lubricants, diluents,

preservatives, antioxidants, emulsifying agents, coating agents, binders, colouring agents,

flavouring agents, gelatin and other additives, sorbitol, mannitol, viscosity builders etc.

Evaluation of crude drugs:

06h

06h II

Moisture contents, extractive value, volatile oil content, foreign organic matter, quantitative

III microscopic exercises including of starch, leaf content (palisade ratio, stomatal number, vein 10h islet number and vein termination number) and crude fiber content, various isolation procedures for active ingredients.

Surgical dressing, sutures, ligatures- with respect to the process, equipments used for manufacture, methods of sterlization and quality control.

IV 06h

Phytochemicals:

V Introduction to plant classification and crude drugs, cultivation, collection, preparation for the 08h

market and storage of medicinal plants.

Chemical constitution of plants: including carbohydrates, amino acids, proteins, fats, waxes,

volatile oils, terpenoids, steriods, saponins, flavonoids, tannins, glycosides, alkaloids.

Various isolation procedures for active ingredients:

VI 08h

08h VII With example for alkaloid, e.g., vincaalkaloids, reserpine; one for steriods- sapogenin,

diosgenin, diagroh.

Pharmaceutical quality control and packaging materials:

Sterility testing, pyrogenic testing, glass testing, bulk density of powders, etc. (other than the

analytical methods covered under core subject), ancillary materials, packaging machinery,

quality control of packaging materials.

VIII 08h

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39

Suggested Readings:

1. L. Patrick. L. Graham, An Introduction to Medicinal Chemistry, OUP Oxford; 4th edition (2009).

2. C. O. Wilson, O. Gisvold & R. F. Doerge, Textbook of Organic Medicinal and Pharmaceutical

Chemistry, Lippincott Williams and Wilkins; 8th edition (1982).

3. W. O. Foye, T. L. Lemice and D. A. Williams Principles of Medicinal Chemistry (2019).

4. D J. Abraham, M. Myers, Burger's Medicinal Chemistry, Drug Discovery and Development (1-8

volume), Wiley (2021).

5. G.L. Patrick, An Introduction to Medicinal Chemistry, Oxford; Fifth edition (2013).

6. John T. Arnason, Rachel Mata, John T. Romeo, Phytochemistry of Medicinal Plants, Springer (2019).



2. https://nptel.ac.in/noc/courses/noc20/SEM1/noc20-cy16/

3. https://nptel.ac.in/LocalChapter/statistics/2537

This course can be opted as an elective by the students of following subjects: Chemistry in 12 th Class






(10 marks)

(10 marks)


(05 marks)




39

40

Semester-VI

Paper-2 (Theory)

Course Title: Medicinal Chemistry and Toxicology Programme:

Degree in


Year: Third Semester: Six


Course Title: Medicinal Chemistry and Toxicology

Paper-2: Theory


Course outcomes:

Medicinal chemistry provides pharmacy students with a thorough understanding of drug mechanisms of action,

acid-base and physicochemical properties, and absorption, distribution, metabolism, excretion, and toxicity

profiles. Students gain knowledge and skills related to this paper is as follows. pharmacology drugs

classification, Introduction to medicinal chemistry, drug metabolism, principles of toxicology,

Biotransformation processes and Enzymes

Credits: 4 Elective



Topics No. of

Unit

I

Lectures

Pharmacology and Drugs classification:

Pharmacology classification and therapeutic classification with example, history of the CSA,

DEA and FDA, drugs & cosmetics act, schedule of drugs 1 to 5, concept of drug master file

(DMF), infringing and non-infringing process concept, introduction of patent and its filing process in brief.

08h

Introduction to medicinal chemistry:

History and development of medicinal chemistry, physicochemical properties in relation to

biological action, ionization, solubility, partition coefficient, hydrogen bonding, protein binding, chelation, bioisosterism, optical and geometrical isomerism..

II 08h

06h

06h

Drug metabolism:

III Drug metabolism principles- phase I and phase II, factors affecting drug metabolism including

stereo chemical aspects.

Principles of Toxicology:

Definition of poison, general principles of treatment of poisoning with particular reference to

barbiturates, opioids, organophosphorous and atropine poisoning, heavy metals and heavy metal

antagonists.

Microbial fermentation:

General principle of fermentation processes and product processing, brief idea of micro-

organisms, their structure, growth and usefulness, enzyme systems useful for transformation

microbial products.

IV

V 06h

Process of manufacture of the following bulk drugs:

(i) Sulpha drugs- Sulphaguadine, Sulphamethoxazole

(ii) Antimicrobial- Chloraamphenicol, Furazolidine, Mercurochrome, Isoniazid, Na- PAS

(iii) Antalgesic- anti inflammatory- Salicylic acid and its derivatives, Ibuprofen, Mefenamic

acid.

(iv) Steroidal hormones- Progesterone, Testosterone, Methyl testosterone

(v) Vitamins- Vitamin-A, Vitamin-B6, Vitamin-C.

(vi) Barbiturates- Pentobarbital

VI 16h

(vii) Blockers- Propranolol, Atenolol

(viii) Cardiocascular agent- Methyl dopa

(ix) Antihistamines- Chloropheneramine maleate.

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41

(x)Antibiotics drugs – Penicillin-G, semi synthetic penicillin, Rifamycin,Tetracycline,

and Vitamin-B12.

(xi) Antimalarial drugs. Anticancerous drugs. AntiAIDS vaccines.

Biotransformation processes- for prednisolone, 11-hydroxylation in steroids, enzyme

catalyzed transformation, manufacture of ephidrine.

Enzyme systems - useful for transformation, microbial products, enzyme catalyzed

transformation - manufacture of ephedrine.

VII 05h

05h VIII

Suggested Readings:

1. M.E. Wolff, Burgers Medicinal Chemistry and Drug Discovery Wiley–Blackwell; 5th edition(1997).

2. W. David, Pharmaceutical Chemistry, Elsevier-Health U.K. (2011).

3. C. Donald, Essential of Pharmaceutical Chemistry, Pharmaceutical press, London (2012).

4. L. Patrick. L. Graham, An Introduction to Medicinal Chemistry, OUP Oxford; 4th edition (2009).

5. C. O. Wilson, O. Gisvold & R. F. Doerge. Textbook of Organic Medicinal and Pharmaceutical

Chemistry, Lippincott Williams and Wilkins; 8th edition (1982).

6. W. O. Foye, T. L. Lemice and D. A. Williams Principles of Medicinal Chemistry (2019).

7. D J. Abraham, M. Myers, Burger's Medicinal Chemistry, Drug Discovery and Development (1-8

volume), Wiley (2021).

8. G.L. Patrick, An Introduction to Medicinal Chemistry, Oxford; Fifth edition (2013).

9. John T. Arnason, Rachel Mata, John T. Romeo, Phytochemistry of Medicinal Plants, Springer (2019).



2. https://nptel.ac.in/noc/courses/noc20/SEM1/noc20-cy16/

3. https://nptel.ac.in/LocalChapter/statistics/2537/



6. https://chemistry-europe.onlinelibrary.wiley.com/journal/23656549

7. https://www.griffith.edu.au/study/courses/principles-of-toxicology-2021PHM#trimester-1-gold-coast-

campus







(10 marks)

(10 marks)


(05 marks)




41

42

Semester-VI

Paper-3(Practical)

Course Title: Experimental Pharmaceutical Chemistry Programme:




Course Title: Experimental Pharmaceutical Chemistry Course Code: B190607P

Course outcomes:

Students gain knowledge and skills related to this paper is as follows.

Demonstration of various pharmaceutical packaging materials, quality control tests of some materials-

aluminium strips, cartons, glass bottles, active ingredient analysis of few types of formulations representing

different methods of analysis- acidmetry, alkametry, nonaqueous complexometry, potentiometry, etc.,

evaluation of crude drugs, microbiological testing.

Credits: 2 Elective



Topics No. of

Unit

I

Lectures

Demonstration of various pharmaceutical packaging materials and quality control tests of some materials- aluminium strips, cartons, glass bottles. 10h

Active ingredient analysis of few types of formulations representing different methods of analysis- acidmetry, alkametry, nonaqueous complexometry, potentiometry, etc.

Evaluation of crude drugs- microscopic examination- determination and identification of starch granules, calcium oxalate.

Microbiological testing- Determination of MIC of some antibacterial and antifungal drugs by zone/cup plate methods.

III

IV

V

10 h

20 h

20h

Suggested Readings:

1. Dickson, Experiments in Pharmaceutical Chemistry, CRC Press (2014).

2. S. K. Dwivedi, Practical Lab Manual of Pharmaceutical Organic Chemistry – I, IP, innovative

publication pvt ltd (2014).

3. C. Kokare Pharm. Biotechnology Experiments & Techniques - Pharmaceutical Biotechnology -

Experiments and Techniques Fifth Edition, Nirali Prakashan (2019).

This course can be opted as an elective by the students of following subjects: Chemistry in 12 th

Class


Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)

Course prerequisites: To study this course, a student must have Opted Sem-VI Theory Ppaer-1 &2



42

43

Semester-VI

Paper-1 (Theory)

Course Title: General & Halogenated Insecticides

Programme:

Degree in




Course Title: General & Halogenated Insecticides

Paper-1 Theory


Course outcomes:

Agrochemicals are used for preventing the deterioration of crops from insects and pest infestation and disease.

The global agrochemicals market report offers the latest trends, growth factors, industry competitiveness,

investment opportunities and detailed profile of the top players for the market during the forecast period. The

global agrochemicals market is segmented by product type (fertilizers, pesticides, adjuvants, and plant growth

regulators), application (crop-based and non-crop based) and geography.


Types of pest and pesticides, Inorganic insecticides, Insecticides of plant origin, Organophosphorus

insecticides, Organothiophosphorus insecticides, Carbamate insecticides, Chemical and Biofertilizers,

Chlorinated hydrocarbons

Credits: 4 Elective



Topics No. of

Unit

I

Lectures

Types of pest and pesticides:

Stomach poison, contact poisons systemic poisons, fumigants. Effect of pesticides on soil and 07h environment.

Inorganic insecticides:

Arsenic insecticides, Paris green, Fluoro insecticides. II 04h

04h Insecticides of plant origin:

Nicotine, Nornicotine, Pyrethroids, Rotenoids, Anabasin, Aliethrin III

Organophosphorus insecticides:

IV Phosphoric acid derivatives- Dimecron, dichlorovos, naled, phosphinon, etc. SAR in the

class. 05h

12h

Organothiophosphorus insecticides:

Thiophosphoric acid derivatives- Parathion, Methyl parathion, Thiophos, Demetron,

V Chlorthion, Paraoxon, etc.

Dithiophosphoric acid derivatives- Melathion, Dimethoate, Thiocron, Formathion,

Mecarbam, etc.

Carbamate insecticides:

Carbaryl, Isolan, Mesurol, Zactran, Demetram, Pyrolan, Baygon, mode of action.

Chemical and Biofertilizers:

Introduction, Types of fertilizer, direct application fertilizers, mixed fertilizers (nitrogen,

phosphorus and potassium sources, ammoniation), controlled release fertilizers and

biofertilizers, liquid vs solid fertilizers, biopesticides.

VI 08h

08h VII

Chlorinated hydrocarbons:

DDT, DDD, Nestran, Dilan, Perthan, Dimite, Chlorobenzilate, Sulphenex, Ovotran, Aramite,

DFDT, SAR in the class and mode of action, BHC, Chlodane, Heptachlor, Aldrin, Dieldrin,

endrin, Faodrin, Endosulfan, SAR in the class and mode of action.

VIII 12h

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44

Suggested Readings:

1. Knowles, Alan (Ed.) “Chemistry and Technology of Agrochemical formulations” Springer Netherland

(1998)

2. J. P. Kumar and S. Bharat “ Soil fertility, Fertilizers and Agrochemicals, Daya Publishing House(2016)

3. H. Ohkawa, H. Miyagawa, P. W. Lee Pesticide Chemistry: Crop Protection, Public Health,

Environmental Safety, Wiley (2007).

4. R. Pohanish, Sittig's Handbook of Pesticides and Agricultural Chemicals, Elsevier Science (2014)

5. D. Adams Insecticides and Pesticides: Techniques for Crop Protection, Larsen and Keller Education

(2017).

6. B. L. Bohmont, The standard pesticide user's guide (revised). Prentice Hall: Princeton, NJ (1990).

7. G.W. Ware, The Pesticide Book, 4th ed; W.H. Freeman: Fresno, CA (1994).




3. chemistry-europe.onlinelibrary.wiley.com/journal/23656549

4. https://www.youtube.com/watch?v=qspUM9tV5WY


6. https://onlinecourses.swayam2.ac.in/cec20_bt13/preview

7. https://www.mooc-

list.com/tags/agrochemicals? cf_chl_jschl_tk =pmd_5O5PKDKzkF2LT66i4kE9EjwggvWfiWI2mhh

8Q7oAYwA-1631360062-0-gqNtZGzNAeWjcnBszQjR







(10 marks)

(10 marks)


(05 marks)




44

45

Semester-VI

Paper-2 (Theory)

Course Title: Fungicides and Herbicides

Programme:

Degree in




Course Title: Fungicides and Herbicides

Paper-2: Theory


Course outcomes:

Fungicides, herbicides and insecticides are all pesticides used in plant protection. Herbicides are a broad class

of pesticides that are used to remove nuisance plants, such as grasses and weeds that may compromise the

growth and yield of desired crops that are in close proximity. After successful completion of this paper,

Students gain knowledge and skills related to this paper are as follows-

Fungicides, organomercuric compounds, dithiocarbamates, miscellaneous fungicides, herbicides, fumigants,

rodenticides, nematicides, plant growth regulators, formulation of pesticides.

Credits: 4 Elective



Topics No. of

Unit

I

Lectures

Fungicides:

Introduction, Sulphur, lime sulphur, copper sulphate, bordeaux mixture, bordeaux paste,

bordeaux paint, burgundy mixture, copper oxychloride, cuprous oxide, mercurous chloride.

Organomercuric compounds:

08h

II Ethyl mercuric chloride, ceresan-M, panagen, agalol, uspulan, puratized, germisan; mode of 08h

06h

action, agrosan GN.

Dithiocarbamates: III

IV

Ziram, ferbam, thiram, nabam, zineb, maneb, captan, hinosan, vapam, etc.; mode of action.

Miscellaneous fungicides:

Dithanon, diclone, captan, polpet, diflolatan, mesulfan, brestan, dodine, glyodin, methyrimol, 08h

06h

08h

terrazole.

Herbicides:

V Introduciton, heterocyclic nitrogen herbicides: 2,4-D; 2,4-DB; 2,4-DES; MCPB; 2,4,5-I,

Monujron, fenuron, TCA, paraquat. Fumigants: HCN, CS2, ethylene halides, durofume, methyl halides.

VI Rodenticides: Zice phosphide, warfarin Nematicides: DD mixture, aldicarb, fensulfothion

Plant growth regulators:

VII Introduction, gibberilic acids, indole acetic and butyric acids, naphthalene acetic acid, cycocil, 08h mode of action.

Formulation of pesticides:

VIII Dry formulations- Dusts, grannules, wettable powders, seed disinfectants, liquid formulations- 08h

emulsions, suspensions, etc., aerosols and sprays.

45

46

Suggested Readings:

1. P. N. Nene, Y. L. Thapliyal , Fungicides in Plant Disease Control, Medtech (2017).

2. H. Panda,The Complete Technology Book on Pesticides, Insecticides, Fungicides and Herbicides with

Formulae & Processes, National Institute of Industrial Research (2003).

3. Knowles, Alan (Ed.) “Chemistry and Technology of Agrochemical formulations” Springer Netherland

(1998)

4. J. P. Kumar and S. Bharat “Soil fertility, Fertilizers and Agrochemicals, Daya Publishing House(2016).

5. C.T. Lacal, Plant growth regulators, Arcler Education Inc (2017).

6. E. E. Fletcher, R. C. Kirkwood, Herbicides and Plant Growth Regulators, Methuen (1981).

7. C.L .Foy, C. L. (ed.) Adjuvants for Agrichemicals, CRC Press, Boca Raton, FL. (1992).







(10 marks)

(10 marks)


(05 marks)




46

47

Semester-VI

Paper-3 (Practical)

Course Title: Analysis of Agrochemicals Programme:




Course Title: Analysis of Agrochemicals Course Code: B190611P

Course outcomes:


Isolation and estimation of active ingredients of commercially available insecticide formulations,

preparation of selected pesticide formulations in the form of dusts, emulsions, sprays, estimation of

pesticide residues in food articles, study of the degradation of pesticides in soil in the presence of

sunlight and moisture, determination of pesticide contents in the soil, isolation of nicotine from tobacco or

tea leaves/ wastes.

Credits: 2 Elective



Topics No. of

Unit

I

Lectures

Isolation and estimation of active ingredients of commercially available insecticide formulations. 12h

12h II Preparation of selected pesticide formulations in the form of dusts, emulsions, sprays.

III Estimation of pesticide residues in food articles. 12h

24h IV Isolation of nicotine from tobacco leaves/ wastes or Tea leave

Suggested Readings:

1. B. S. Furniss, A.J. Hannaford, P.W. G. Smith, A.R. Tatchell, Vogel's Textbook of Practical Organic


2. Lab manual 11, FSSAI Manual of methods of analysis of foods

https://old.fssai.gov.in/Portals/0/Pdf/Draft_Manuals/PESTICIDE_RESIDUE.pdf

3. D. A. Knowles, Chemistry and technology of agricultural formulations. Kluwer Academic, London

(1998).

4. S. Ippolito, J. R Mendieta, Formulations of Agrochemicals, Scitus Academics Llc (2020).

5. A. Knowles, Chemistry and Technology of Agrochemical Formulations, Springer, 1998.



Viva voce

Mock test

Overall performance

(10 marks)

(10 marks)

(05marks)

Course prerequisites: To study this course, a student must have Opted Sem-VI Theory Ppaer-1 &2 ( General & Halogenated Insecticides and Fungicides and Herbicides)S



47

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