to~~aJY File: 18G D.B. 1 ~~~~~~~~~~~~~~~~~~/ Oo 'fj I ~~INDOOR FIRING RANGE' REMEDIAL ACTION REPORT ETELSON AIR FORCE BASE I ~~~~ALASKA J ~~~~~FINAL NOVEMBER 1998 Jacobs Engineering Group Inc. In affiliation with: Anderson Alaska, Inc. Philip Services Corporation Radian International, LLC I ~~~~~~~Shannon & Wilson, Inc. Alaska District Wilder Construction Company Total Environmental Restoration Contract
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to~~aJY File: 18GD.B.
1 ~~~~~~~~~~~~~~~~~~/If Oo 'fj
I ~~INDOOR FIRING RANGE'REMEDIAL ACTION
REPORT
ETELSON AIR FORCE BASEI ~~~~ALASKA
J ~~~~~FINAL
NOVEMBER 1998
Jacobs Engineering Group Inc.
In affiliation with:Anderson Alaska, Inc.Philip Services CorporationRadian International, LLCI ~~~~~~~Shannon & Wilson, Inc.
Alaska District Wilder Construction Company
Total Environmental Restoration Contract
I ~~INDOOR FIRING RANGE
REMEDIAL ACTION
REPORT
EIELSON AIR FORCE BASEALASKA
FINALNOVEMBER 1998
Prepared for: Prepared by:U.S. Army Corps of Engineers Jacobs Engineering Group Inc.I ~ ~~~~~~~~P.O. Box 898 4300 B Street, Suite 600Anchorage. Alaska 99506-0898 Anchorage, Alaska 99503
Total Environmental Restoration ContractContract No. DACA 85-95-D-0018
ii ~~~~~~~~~~~Task Order No. 07
TABLE OF CONTENTS
7 ~~~~SECTION PAGE
ACRONYMS AND ABBREVIATIONS .......................................................... U
3.1 MOBILIZATION AND DEMOBILIZATION.......................................... 3-1
3.2 AIR MONITORING...................................................................... 3-1
3.3 RANGE DECONTAMINATION........................................................3-33.4 FIRING RANGE SAND REMOVAL................................................... 3-5
3.5 LEAD SHOT REMOVAL ............................................................... 3-8
3.6 FIRING RANGE DEMOLITION........................................................ 3-8
3.7 FIRING RANGE CONFIRMATION SAMPLING .................................... 3-8
3.8 PUNCHLIST WORK ITEMS........................................................... 3-114.0 WASTE MANAGEMENT AND DISPOSAL............................................. 4-1
U.S. Army Engineer District, Alaska (USAED) contracted with Jacobs Engineering Group
Inc. (Jacobs) through the Total Environmental Restoration Contract (TERC) to perform a
demolition of an indoor firing range on Eielson Air Force Base (AFB) near Fairbanks, Alaska.
The demolition was performed in accordance with the work plan and associated regulatory
guidan ce regarding shipping and disposal of the firing range sands. The project consisted of
pre-demolition characterization of building surfaces and materials and removing and
disposing or recycling of:
* Approximately 103 tons of firing range sands and 600 pounds of lead bullet fragments;
* Approximately 300 pounds of light ballast;
* Approximately 23,000 pounds of building material debris, including furniture andconcrete;
* Approximately 400 pounds of a target retrieval system and ventilation system blowers;
* One 5-gallon drum of petroleum hydrocarbon contaminated sawdust; and* Approximately 2 tons of steel backstop, armor plating and ducting.
Analytical results of confirmation samples collected following demolition of the indoor firing
range were compared to the established cleanup levels. Analytical results indicated that the
majority of the samples met the criteria for clean closure, while several exceeded the
established criteria. Although exceeding the established cleanup level of 1 O0pg/1ft, the resultsare well below levels that would pose a health risk to humans in an industrial environment
such as the space of the former firing range. Therefore, no further action is recommended to
remediate the indoor firing range.
Remediation of the firing range was curtailed in late-October. 1997 due to inclement weather
conditions. Duhfng the project walk-through conducted at the end of the 1997 field seasonwith USA.ED, U.S. Air Force (USAF), Jacobs, and Brice Environmental Services Corporation
(BESCORP) personnel, a punch list was developed that delineated the work items to be
* ~~~Figure 1-2 identifies the location of Building 2204 relative to Eielson AFB and identifies the
location of the small-arms firing range within Building 2204. The indoor range was located in
the south end of the basement. The firing range and project site layout is presented in
Figure 1-3.
T ~~~The demolition was conducted in accordance with the work plan and consisted of the
following activities:
*Cleaning surfaces exposed to lead dust;
*Removal and disposal of firing range sand and an area of lead bullet fragments;
*Removal of firing range appurtenances, protective armor and sound proofing, selectedducts and utility services, and miscellaneous pieces of furniture;
*Characterization and disposal of a drum of contaminated sawdust;* Re-seeding disturbed areas outside the range and patching holes left in the building walls
caused by the demolition of the range; and
L .~~~ Collecting confirmation soil and wipe samples.
1.2 PROJECT BACKGROUND
The indoor small-arms firing range is believed to have been constructed concurrently with the
remainder of Building 2204. Bullet fragments indicate that 22-caliber and 45-caliber
ammunition were frequently used. Signs posted near the entrance indicate that shotguns could
also have been used in the range; however, lead shot was not observed in the firing range
sands. The firing range was inactive at the time of the demolition and had not been used for
target practice since the mid- to late-1980s. Access to the range was restricted by the354ti SPS/CC (Security Police Squadron), who kept small arms and ammnunition in the vault
adjacent to the firing range.
L B~~~I:EIE1SONMO5M3070WI\W\inuj Etelson Rejportll~ 1-3 AKT-J07-05M307.122.0002Final I1/98
- ~~~~~~~~~~~~NORTH
~23 493 2259
2350 fl ~~~~~~~~~EAST LOOP
2256 2260 2262 2264
GE MAINT. SHOPS
CNTRALAV
F - ~~~ATHLETIC FIELDS -I20
GAS I ~~~~~~DINING HALL
2202~~20
1125~~~~~~~~1
STORAGE 12 1 1- 12 _ _ _ _
BUILDING 2204 LOCATION DETAILEIELSON AFB, ALASKA
LATERAL CLEARANCE LINE
TASK MG4R: JACAD FILE NO: FIGURE $0:0 500 1000 2000 0. BURGESS FI G2-_2 I
I --I DRAWN BY: PROJ. NO:DAESCALE IN FEET aS.B. K. 105M30701. JULY 98
The objective of the demolition was to safely demolish and decontaminate. the basement of
Building 2204 so the building could be re-utilized for storage, offices, Or other purposes. The
cleanup levels associated with this obj ective are presented in Table I1-1I.1
Tablel1-1 Project Cleanup Levels
Item fCleanup Level
Materials removed from the range for reuse or 5 milligram per liter (mg/L) toxicity characteristicdisposal leaching procedure (TCLP) lead
Surfaces and materials remaining in the range 1 00 micrograms pier square toot (pgift2)1
Disposal and treatment of firing range sand and 400 milligram/lkilogranm (mng/kg) total lead
Notfaes: of soil remaining in placeI
'The cleanup level is the most conservative of the three recommended by the U.S. Department of Urban Housing andDevelopment (HUD). The results of the confirmation wipe sampling indicated levels greater than 100 (pg/ft2) to be presentfollowing demolition of the range. Based upon the plan for meuse of the space, the level of lead contamination remaining, andthe threat posed to human health, the cleanup level accepted at the completion of the demolition was raised to a level mareIappropriate for an industrial selling. See Section 3.7 for further details on the results of the confirmation sampling.
To demonstrate. that the majority of the demolished construction materials could be disposed of
at the Fairbanks North Star Borough (FNSB) landfill as non-hazardous wastes, pre-demolition
sampling and analysis were performed on 14-15 and 17 July 1997. XRF screening was
performed on the interior surfaces of the range using a Spectrace 9000 XRF analyzer
- manufactured by TN Technologies of Round Rock, Texas. XRF screening was performed both£ before and after dry vacuuming and/or wet wiping at locations identified for the collection of
composite TCLP samples. The measure of residual lead compared to the pre-decontaminatedI.~~~~~~~~~~~~~
L ~~surface lead measurement was used to provide guidance for selecting the appropniate
decontamination technique. Following XRF screening and surface decontamination, 34 bulk
samples were collected of the various groups of construction materials and sent to ColumbiaV ~~Analytical Services (CAS) in Anchorage, Alaska, for analysis. The bulk samples were reduced
to seven composite samples and analyzed for toxic characterization leaching procedure (TCLP)
B ~~lead analysis using U.S. Environmental Protection Agency (EPA) Methods SW131 1/6010A.
Figure 2-1 shows the location of all the areas screened for surface lead by XRF. Table 2-1
presents the screening location, sample identification numbers, XRF screening results,
pre-composite TCLP sample numbers, and the composite sample numbers into which each
pre-composite sample was reduced. The chain of custody (CoC) forms and the data analytical
g ~~reports associated with these samples are presented in Appendix B.
Material Type Number (mgIL) (mg/kg) Volatile Organics3 (mglkg)
Floor Tiles 1 0.8 NA NAFloor Tiles 2 2.0 NA NAFloor/Ceiling Tiles 3 0.04J NA NACeiling/Wall Tiles 4 0.5 NA NASheetrock/Lumber 5 0.06J NA NAPlywood/Lumber 6 2.8 NA NAFloor Tiles 7 0.8 NA NADrum Contents JE97EIE131US1 .2 ND 0.059J - Ba NA
_______ _____ _ ______ 0.04J - Se
Drum Contents JE97EIE136US NA NA 2J Trichlorofluoromethane12J Methylene chloride2J Benzene4J8 Toluene100 1 .3,5-Trichloropropane1 0J tert-Butylbenzne160 1 ,2,4-Trimethlybenzene.9J 4-isapropyltoluene
Notes:ISample matrix code US refers to Unknown Solid.
2 Drum contents sampled once for TCLP metals and once for volatile organics; therefore two sample numbers were used.Complete analytical data set is presented in Appendix B that includes non-detected results and detection limits.
NA Not AnalyzedB Analyte present in the blank and sampleBa Barium.1 Estimated valueND Not DetectedSe - Selenium
p ~~~mgfkg milligrams per kilogram
The results of the composite samples indicated that the construction materials to be removed
from the range during the demolition would not be classified as a hazardous waste and could be
disposed of at the FNSB landfill. The results of the sawdust analyses indicated that volatile
organic contamination was present at levels dictating disposal as a hazardous waste through the
Eielson AFB Hazardous Material Section and Defense Reutilization and Marketing Organization
2 009 SE Exclusion Zone <3.03 010 1 1 Floor Stairwell <3.03 011 SE Exclusion Zone <3.04 012 1" Floor Stairwell 26.74 013 SE Exclusion Zone <3.05 014 1" Floor Stairwell 36.45 015 SE Exclusion Zone <3.06 016 W Exclusion Zone <3.0
Notes:SE southeastW Westpg/rn3 microgramns per cubic meter
Monitoring stations were set up at five points during the sand removal action to monitor for
airborne lead dust. The air monitoring locations consisted of:
* Two personnel monitors;
* One station downwind of the vacuum truck;
a One station in the stairwell on the first floor directly above the basement; and
* One station setup in the opening of a super sacks while being filled with firing range sand.
Results of the air monitoring activities were reviewed by a Jacobs certified industrial
hygienist~ (CIH) to verify that the Occupational Safety and Health Administration (OSHA)
PELs and the American Conference of Governmental. Industrial Hygienists (ACGIH)
threshold limit value (TLV) of 50 micrograms per cubic meter (pg/rn3) of measured air was
not exceeded and were found to pass the regulatory criteria. One personnel sample collected
during the removal of the sands was found to exceed the PEL for lead dust. As shown in
Table 3-1, Sample No. 005 had a result of 52 pg/rn3 . This result verified the need for workers
to wear respiratory protection during the removal of the firing range sands. As a precaution,
all personnel working in the range during the sand removal action were equipped with
- ~~~half-face respirators. The sand removal activity is discussed in more detail in Section 3.5.
- ~3.3 RANGE DECONTAMINATION
Prior to removal of the firing range sands or any of the construction materials located in the
basement of Building 2204, the range was decontaminated by removal of the surface lead
dust. The surface of the walls, ceilings, floors, ducting, furniture, and other objects were
£ ~~~cleaned with portable dry vacuums equipped with high efficiency particulate air (H[EPA)
* ~~~filters. The work was performed in modified Level C PPE due to the unknown levels of lead
dust that may have become airborne during this activity. To ensure that worker safety was not
-' ~~compromised, air monitoring was also conducted in the range during this activity. A
discussion of the air monitoring activities is presented in Section 3.2.
L ~~~Following dry vacuuming of the range, removal of the wall and ceiling tiles was conducted.
After each layer of building materials was removed from the walls and ceiling, dry vacuuming
was again performed to remove dust that may have migrated beneath the wall and floor
coverings.
The dividing and temporary walls in Rooms 1 through 4 as shown in Figure 1-3 were
J ~~~decontaminated~and removed during this activity. Figure 3-1 presents the final configuration
of the firing range following the completion of the demolition. The materials removed during
this activity were containerized and managed as described in Section 4 of this report.
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7' ~3.4 FIRING RANGE SAND REMOVAL
* ~~~The firing range sands were removed using a super sucker cyclone vacuum truck equipped
with a HEPA filter system. The vacuum truck was set up in the exclusion zone on the south
side of Building 2204. The sands were removed using a 1 00-foot hose run through anopening in the basement wall left by the removal of the ventilation system blowers. The sand
was packaged into one ton super sacks, weighed, and placed on wood pallets in the wastestaging area. Each super sack was marked with a unique sack number, the date, and the
weight.
Characterization of the sand for disposal and/or recycling purposes was performed during theC'
bench-scale treatability study performed during late-1996. The results of the study are
L ~~~presented in the Treatability Study Report, dated May 1997. Management and disposition of~~~ ~the sands is presented in Section 4.2.
The sand removal activity was conducted in modified Level C PPE and was accompanied by
air monitoring activities as described in Section 3.2.
Following the completion of the sand removal activity, a total of six confirmation samples
were collected from the firing range floor and bullet trap area excavations to ensure that lead
contamination exceeding the 400 mg/kg action level had been removed. The samples werecomposited from a total of four locations in the bottom of the excavations and sent to CAS fortotal lead analysis, as shown in Figure 3-2. Table 3-2 presents the results of the soil
confirmation sampling. The CoG forms and analytical data sheets associated with these
- ~~~samples are presented in Appendix B. The sample results indicated that the cleanup, levels
had been achieved and that no further excavation was necessary.
L Notes:mg/kg milligrams per kilogramND non-detect
At the direction of USALF representatives, the excavations left by removal of the firing range
- ~~~sands were backfilled with clean fill and compacted. Approximately 115 cubic yards of fill
material were obtained from the Bear Lake Quarry at Eielson AFB and hauled to the project
site. A Bobcat loader equipped with a muffler to minimize exhaust emissions was used to
place the fill inside the range through the opening left in the east end of the range. A
gasoline-fired compactor was used to compact and level the fill material. The final grade of
r ~~~the basement floor was established by line of sight.
During the removal of the firing range sands, a broken sewer line was uncovered. At the
direction of USAF representatives, the line was not covered with fill so that access could be
maintained for repairs. The fill material required to cover the line was left piled adjacent to
the hole.
P ~~~Air monitoring was conducted during the activity to ensure that a dangerous atmosphere was
not created by use of the compactor. Because the work was performed in a cyclic manner,
alternating the use of the Bobcat and compactor, ample time was provided for air changes in
the basement following use of the compactor. The alternation of the equipment resulted in
achieving the level of carbon dioxide below the PEL of 35 parts per million (ppm).
I \ETELSON\05M30701\WPhFinal Eielsorn Reportl~doc 3-7 AKT-JO1.05M307-J22.0002Final I1/98
3.5 LEAD SHOT REMOVAL
During the removal of the firing range sands, an area of metallic lead contamination
consisting of lead bullet fragments was discovered on the west side of Building 2204, as
shown in Figure 3-2. Prior to removal of the lead fragments, Eielson AFB unexploded
ordinance (UXO) personnel inspected the area and determined that no undischarged. bullets
remained and that the lead could safely be removed. At the direction of USAGE and USAF
representatives, the vacuum truck and rakes were used to remove approximately 590 pounds
of lead bullet fragments. The lead was placed into super sacks and taken to the waste staging
area along with the super sacks of firing range sand. Further discussion of the disposition of
the metallic lead is presented in Section 4.2.
3.6 FIRING RANGE DEMOLITION
Following removal of the firing range sands, the building construction materials in the range
were dry vacuumed as necessary to remove dust generated by the sand removal activity and
removed. These materials consisted of lighting fixtures; wall, floor, and ceiling tiles;
sheetrock; lumber; plywood; ventilation system ducting; and armor plating. The materials
were segregated for disposal depending upon composition. Waste segregating and disposition
activities are presented in Section 4.0.
At the~ completion of the firing range removal action, the heating system blowers were
reconnected to the building electrical circuits to supply heat to the basemeht so that the water
and sewer lines would not freeze.
3.7 FIRING RANGE CONFIRMATION SAMEPLING
Following completion of the decontamination of the firing range and removal of the firing
range sand, construction materials, furniture, and other miscellaneous materials, 27 wipe
confirmation samples were collected in accordance with the work plan. Figure 3-2 shows the
confirmation sample locations, and Table 3-3 presents the results of the confirmation
sampling. Table 3-4 presents the results of the characterization sampling performed on the
I:\EIESON\05M30701\VW~inaI Eielsot Reportldo 3-8 AKT-JO7-05M307-J22-0002Final I 1/98
liner in the waste staging area. Appendix B presents the CoG forms and the analytical data
r ~~~sheets associated with these samples.
Table 3-3 Firing Range Wipe Confirmation Sample Results
Sample ResultsSample Number Sample Location SW 7420 (pg/wlpe)
JE97EIE143SW Field Blank NDJE97EIE144SW Room #1 Floor. 100JE97EIE145SW Room #2 Floor 40JE97EIE146SW Doorway Floor 70JE97EIE147SW . Doorway Floor 50JE97EIE148SW Vault Doorway Floor 50JE97EIE149SW Main Entryway Floor soJE97EIE150SW Duplicate of 149 170JE97EIE151SW Residence Hall Floor Outside Range A-ccess Doo-r 70JE97EIE152SW Room #1 West Wall INDJE97EIE153SW Room #2 West Wall 20JE97EIE154SW Room #3 West Wall 60JE97EIE1 55SW Room #4 West Wall 30JE97EIE1 56SW Room #5 West Wall 340JE97EIE157SW Vault North Wall NDJE97EIE158SW Range East Wall (South of Access Door) 170JE97EIE159SW West Wall of Main Entrance NDJE97EIE160SW Duplicate of 159 NDJE97EIE161SW Firing Range North Wall 140JE97EIE162SW Firing Range South Wall 20JE97EIE163SW Column #4 North Side 40JE97EIE164SW Column #5 South Side 30JE97EIE165SW Column #6 West Side 220JE97EIE166SW Duplicate of 165 120JE97EIE167SW Ceiling Near Column #2 80JE97EIE168SW Ceiling Near Column #5 NDJE97EIE169SW East Side of Metal Ducting in Room 4 220
All the tasks associated with this project could not be completed due to inclement weather
conditions experienced at the end of the 1997 field season. The tasks requiring completion
were noted duiring the final inspection and include the following:
* Vegetation of the former location of two concrete pads;
* Reseeding of an area of lawn used to remove items from the back of the firing range;
* Closure of the openings in the north and south walls of the basement left by the removal ofthe ventilation system and painting of the affected areas on the outside of the building;
* Repair and closure of the trap door at the back of the firing range on the east side ofBuilding 2204 and painting of the affected areas on the outside of the building;
* Removal of a sheet of plywood near the entrance of the range. The plywood was left inplace because it was supporting a sewage line. After Eielson AFB personnel support theline, the plywood will be removed.
On 15 June 1998, BESCORP personnel remobilized to Building 2204 to complete the work
items listed above. Upon completion of these punch list items, USAED and USAF personnel
conducted a final inspection of the project site. USAED and USAF personnel agreed that all
work was satisfactorily completed and that no firther action was required to complete
Final I U98~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
5.0 DATA QUALITY ASSESSMENT
5.1 ANALYTICAL SUMMARY
Sample collection, handling, analysis, and reporting procedures as defined in the Sampling
and Analysis Plan Addendum were followed. Most data acceptance criteria were met, with,
the few exceptions defined in this section. All data are considered usable.
The analytical data was provided by the laboratory in both hardcopy and electronic formats.
One hundred percent of the analytical hardcopy data was reviewed. Fifty percent of theelectronic data was reviewed for completeness and accuracy. The primary laboratory, CAS,
located in Anchorage, Alaska, supported the analytical requirements of the 1997 demolition.
The data review and completeness check was performed by Jacobs. The review process
described in the Sampling and Analysis Plan (SAP) Addendum and the Standard Sampling
Analysis Plan (SSAP) was followed, including a review of summary forms, CoC records, run
logs, and extraction logs.L
Quality Assurance Project Plan (QAPP) laboratory acceptance criteria and EPA National
Functional Guidelines (EPA 1994a~b) criteria were used to assess the data usability. The
Jacobs project chemist performed a completeness check on the hardcopy data and reviewed
the hardcopy and electronic data to evaluate comparability and accuracy. Data qualifications
used to determine usability are based upon EPA 1994a~b.
Appendix B, Analytical Data, is included to supplement this section of the report: This
appendix provides case narratives, cooler receipt forms, a summary of the laboratory
nonconformance issues, a description of laboratory-implemented corrective actions, and
sample conditiob receipt documents. It also contains CoC records, which provide sample
identification information, site locations, method requirements, and sampling dates and
identifies quality assurance/quality control (QAIQC) samples.
Reported data within this package should be considered valid but may be biased
(qualifications noted in the body of this report). The qualifiers used to flag data are defined as
follows:
*"U"-Synonymous with "ND" for non-detect; not detected above the reporting limit(practical quantitation limit); final numerical result becomes the reporting limit flaggedwith "U."
*"J"-Analyte was positively identified, but numerical value of concentration is approximatedue to compromised quality control or inherent inability to analyze the sample (e.g., matrixeffects).
*"U.J-The analyte was not reported above the practical quantitation limit, but the reportedquantitation limit is approximate (due to compromised quality control or inherent inabilityto analyze the sample).
*"UR"-The analyte was not detected above the reporting limit, but sample results wererejected due to significant, deficiencies in quality controls or inherent ability to analyze thesample (e.g., matrix effects).
The qualifiers listed above, or "flags," are hyphenated in the report to reflect the basic
rationale behind the qualification (e.g. "J-S"). The following qualifiers were used in the text
of this report to indicate which QA/QC protocols were not met:
* S-surrogate recovery;
- *~~~ L-lab control sample;
. C-calibration;
. T-instrumnent 1 2-hour tuning criteria;
* M-matrix spike and/or spike duplicate;
1 -internal standard;
*B-method blank;
.H-for holding times; and
E -value exceeds instrument calibration range.
5.2 DATA QUALITY SUMMARY
in general, the overall quality of the data was acceptable. The data quality was determined as
acceptable or estimated. Acceptable data are associated with QC data that meet all QC criteria
or with QC samples that did not meet QC criteria but data quality objectives were not
I:\EIELON05M30701\'W~himui Eielson Reporti dc 5-3 AKCT-07-05NO07-122.0002Final 11/98
affected. Estimated (J) results are considered inaccurate due to a bias created by matrix
interference or QC acceptance criteria which were not met. The EPA National Functional
Guidelines (EPA 1994a~b) were used to evaluate the acceptability of the data.
All CoC sample identification numbers include JE (Jacobs Engineering), BE (Brice
Environmental), 97 (1997), FIB (Eielson AFB), three numbers (individual sample number
starting at 100) and two letters that identify the type of sample collected (i.e., CM=
construction material, US = unknown solid). The term positive results is used to identify all
results that are not considered non-detected (U) and all results refers to both nondetected andpositive results. The term non-defected (U) refers to results that are less than the laboratory
reporting limit and detection limits will, therefore, be qualified or biased.
Details of the evaluation are provided in the following sections by analytical method and
include the associated samples and analytes:
Volatile Organic Compounds (BTEXNV-SW8260A. Overall data quality is acceptable with
the following exceptions:
* The positive result for toluene in sample JE97EIE136US is considered estimated (J-B)because it was also found in the blank.
* The 8260 surrogate recovery in sample JE97EIEl36US was outside normal laboratorycontrol limits because of suspected matrix interference. The sample was re-analyzed, andagain produced results outside control limits. The results from the original analysis arereported.
* The 8260 soil Matrix Spike/Duplicate Matrix Spike (MSIDMS) recoveries of severalanalytes were outside the normal laboratory 9ontrol limits because of matrix interferencescaused by excessive levels of naphthalene. No further corrective action was taken.
* The 8260 soil MSIDMS recovery of naphthalene was not calculated. The analyteconcentration in the sample was significantly higher than the added spike concentration,preventing accurate evaluation of the spike recovery.
As a result of the interferences created by the fuel contamination in the sawdust sample,
surrogate and matrix spike recovery criteria were not met; however data are usable for waste
U.S. Army Corps of Engineers (USACE). 1997 (May). Bench-Scale Treatability Study,Indoor Range Sands, Elelson AEB, Alaska.
U.S. Army Corps of Engineers (USACE). 1997 (August 14). Engineering Evaluation,Indoor Range Sands Treatment and Disposal, Eielson AFB, Alaska.
U.S. Army Corps of Engineers (USACE). 1997 (June 14). Technical Memorandum on Wipeand Soil Sampling of Indoor Firing Range (AOC-3 2), Eielson AFB, Alaska.
U.S. Department of Housing and Urban Development (HUD). 1995 (June). Guidelines forthe evaluation and Control of Lead-Based Paint Hazards in Housing.
Environmental Protection Agency (EPA). 1994a (February). Con tract Laboratory ProgramNational Functional Guidelines for Inorganic Data Review, EPA-540/R-94-o013.
Environmental Protection Agency (EPA). 1 994b (February). Con tract Laboratory ProgramNational Functional Guidelines for Inorganic Data Review, EPA-540/R-94-O012.
Jacobs Engineering. 1997 (July). Work Plan, Eielson AFB, Alaska.
EJ AREA START ~START4 LOCAIION: DPERSONAL STPARRSLS(U/M)
DCLEARANCE ro? tyAR EUT' ~~E OF RSMOVAL fl8NVIRONMENTTOAPE OF RFM~~~~~vAL: ~~TOTALTOARJLOAXI SAJPLIE PMP U BATESAMPLE TYPE iTag Now ni VOLUME wiPE BESULTI (ua/h?)
I I j D~~~1 CLANK- I- - IJ~~~~~~~~E AREA START START
LOCA11,0N: D3PERSONAi.SO I ESII(QM
Tht'S OF REMOVAL: TOTALoTOTA
Please fax results to client as noted above and* ~~~~to.RJ Lee Group. Alaska at 9O7-562-3218.
LEAD ANALYSIS j e ruAAKClienttp &L~'aThe Materials Characteorization Spc 0 j~
-- .4 StdS~~~~~~~~~64NleLsanWoy Anchorage, AK 9951aClient Job # gRJLGAK# g>: f~,t ct, Phone 907-562-4218 fOX 907-562-3218
Job name/location ~ ~ ~ ~ AZ1042400 College Road Fairbanks, AK 997Q9Ordered ~~~~~~~~~~~~Phone 907-452-3974 PCX 907-452-3974
Sampled byvey PAGE .. .. OF . 4Fax Results to LA\51Z - s 'i% AIRBILLO III _________
DAtE TIME RUIUNIQUISKED BY COMPANY RECEIVED BY COMPANY C3 After C1 24 HoL,
Sri i44#~~~~~~~~~~~~~~~~~~~L. ~~~~~HoursC3 Rush Q 0Hu
La BHour Vl72 M
IJLCAK A AMrPLI U PUMPWI OAT" SAMPLE TYPE TVAI FLOW tAll VOUM winE Sntilt (Utailf)
LOCATION: ~ ~ ~ ~~~~~~RE START ~:4 START
1C~~Aoc4 5~~.k.Jvt\ DCLEAYANCE STO *a?, 10 STOP AAR INUtILLS(3 I
rIPE OFREMOVAL: OENVIRNow.ENr TOTAL SI\\TOTAL. Z6 - -7
310G SMLE PUMPe DATS SAMPLE TYPE Mt no fOWm VOL1JMI WIPE AESOUf (UG/Y?)
lit"Itt SAPPP#te SAMPLE TYPE TIM now AEVOLME LTvs: CUG[Fe')I C C AREA S~?TRLOCATION! OPESONAAI 0iini./A
OCLEARANCiE sOr TTOP ARIILS(GM
IYPE OF REMOVAL: CW4VIROI4AEJJT TOTAL TOTAL
Please fox results to client as noted above andto RJ Lee Group, Alaska at 907.562-3218.
COLUMBIA ANALYTICAL SERVICES, INC.
Client: Jacobs Engineering Group, Inc. Service Request No.: A9701018Project: EAFH Firing Range Date Received: October 30, 1997I ~~~Sample Matrix: Solid
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc.(CAS). 'This report contains analytical results for sample(s) designated for Tier ACQE data d'eliverables. Whenappropriate to the method, method blank results have been reported with each analytical test. Additional qualitycontrol analyses reported herein include. Matrix/Duplicate Matrix Spike (MS/DMS), Laboratory/DuplicateLaboratory Control Sample (LCS/DLCS), and Imnital Continuing Calibration Verification Standards (ICV/CCV).
All EPA recommended holding times have been met for analyses in this sample delivery group.
The following difficulties were experienced during analysis of this batch:
Insufficient sample was provided to obtain the required minimum 100 gram sample aliquot necessary to performthe requested TCLP\1 311 extraction. As footnoted, the amount of extraction fluid was adjusted according to theamount of sample provided; 50.1 grams of sample JE97EIE17OLN was extracted into 1000 ml and 44.8 grams ofsample JE97EIEI1I71LN was extracted into 896 ml.
Approved by Date IIIto1q, 0 0 00 1;!
o 00
-
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Columbia Analytical Services, Inc.Cooler Receipt and Preservation From
* ~~~Client: Jacobs Engineering Group, Inc. Work order: A9701018Project: EAFB Firing RangeCooler received on: 10/30/97 and opened on 10/30/9 7 by Sherry Long
Yes No /1 Were custody seals on outside of cooler? RI 0
If yes, how many and where? 2 F & BWere signature and date correct? MXI 0
2 Were custody papers properly filled out (ink, signed, etc .... )? MI 0: 03 Did all bottles arrive in good condition (unbroken, etc .... )? MR 01 54 Were all bottle labels correct (analysis, preservation, etc .... )9 0X 0 0
- ~~~~5 Did all bottle labels and tags agree with custody papers? 177 0 0l6 Were correct bottles used for test indicated? MR 5 57 Were VOA vials checked for absence of air bubbles, and noted? 01 0 MR8 Temperature of cooler upon receipt 5.8 Degrees C
- ~~Explain any discrepancies: ______________________________
Yes No Sample I.D. Rage Vol.- ~~~pH Reagent x
12 NaOH x2 HNO3 X2 H2S04 x
- ~~Yes all samples OKNo =Samples were preserved at lab as listed
Comments:
n
COLUMBIA ANALYTICAL SERVICES, INC.
Client: Jacobs Engineering Group, Inc. Service Request No.: A9700999Project: EAFB Firing Range Date Received: 10/27/97Sample Matrix: Wipe
CASE NARRATIVE
All analyses were perforned consistent with the quality assurance program of Columbia Analytical Services, Inc.(CAS). This report contains analytical results for sample(s) designated for Tier ACOE data deliverables. Whenappropriate to the method, method blank results have been reported with each analytical test. Additional qualitycontrol analyses reported herein include: Laboratory/Duplicate Laboratory Control Sample (LCS/DLCS) and IntialContinuing Calibration Verification Standards (ICV/CCV).
All EPA recommended holding times have been met for analyses in this sample delivery group.
Approved by A"- ateI l/uf17 0 0 00
__JACOBS ENGINEERING GROUP INC A o 009 71GE 4300 B STREET SUITE 600. ANCHORAGE. ALASKA MM035222® I TELEPHONE (9O7I 563-32 FAX 1907) 563.332 CHAIN OF CUSTODY RECORDUSE A BALLPOINT PEN, BLACK INK, AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACK
IWHC'.-.J __ C IS__ t-+LC O M M _ _ _ _ _ _ _ _rb: ~IWSS.J '½I ta (L.JflA _ __A _ _ _ _ L I0 5 0
- _ _6.1 _3_ _tf l i t I oB Y 1_ _ _ _ _ _ _
IREot BY_ _AT T___ REU0411SE m DAT TIM
4~~
a~~~~~~~~~~~~~~~~~~~~~~
RECORD RETURNED BY DATE TIME~~~~~~~~~O~h IM
SlIPPING NUBR
DISTIhBUTIONJ W1411 - PROJECT FRLE /CANARY - LAB REatPT /PME - DATA k4ANAGEMBNT CGQDGOO - Fa , jn c
CZG LI
.4~~~~~~~~~~~~~~~~~~~~~~~~~~0
- JACOBS ENGINEERING GROUP INC ~E 4300 6 STREET. SUITE 600 ANCHORAGE. ALASKA 995035922 -II ®TELEPHONE (907l 5633322 FAX (0 56330CHAIN OF CUSTODY RECORDUSE A BALLPOINT PEN, BLACK INK, AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACK
PRJETNAE LBOMRY"a AD_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _'4 f .- s a A k j
PROJECT NUMBER:H¾ 37~~~~ U -~~~~~~~~~~~ ~ ~ ~~~sast~~~~~~~~~~~~~A
W&S CODE: SUBCONTRACT I D.O. No. ______________ ~,~\ I
w'i~~ RELEAS~~~tt ATEiETURNAROUND TUME " 4 ~ /2___RECE ~~~~~~~DATE TIME REUNOUS14ED BY DATE T
RECORD RETURNED BYDAE TE
SHWPPING NUMBEA:
rASTRUBJIN: WHM - PROJECT FILE ICANARI - LAS RECEIPT PM Pt DATA MANAG8OET I2 GOL ' /EL.{D
'-'
JACOBS ENGINEERING GROUP INC /90/7099c?;Ut®TELEPHONE (9071 563.3322 FAX 107) 563.3320 CANOF CLWDy RECORD
USE A BALLPOINT PEN. BLACK INK, AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACKPROJECT NAME: OT4A153ADot
PSOJCT NUMBER:
WBS CODE: ~~~SUBCONTRACT / 0.0.N.
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_____ _ - It2-~~~~~~~o nf
Columbia Analytical Services, Inc.Cooler Receipt and Preservation From
Client: Jacobs Engineering Group, Inc. Work order: A9700999
Project: EAFB_ Firing Range
Cooler received on' 10/27/97 and opened on 10/27/97 by Sherry Long
Yua No WAI Were custody seals on outside of cooler? MR 01 0
If yes, how many and where? 2 F & B
Were signature and date correct? El 0 02 Were custody papers properly filled out (ink, signed, etc .... )? MR 0 Q1
3 Did all bottles arrive in good condition (unbroken, etc .... )? MR 03 04 Were all bottle labels correct (analysis, preservation, etc .... )? MR 0 05 Did all bottle labels and tags agree with custody papers? r0- 0 0-6 Were correct bottles used for test indicated? MR 01 07 Were VOA vials checked for absence of air bubbles, and noted? 0R 0 08 Temperature of cooler upon receipt 14.7 Degrees C
Explain any discrepancies: ______________________________
Yes No Sample I.D. Reage Vol.
pH Reagent _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
12 NaOH _ _ _ _ _ _ __
2 HNO 3 _ _ _ _ _ _ _ _ _ _ _ _ _
2 H 2 S 04 _ _ _ _ _ _ __ _ _ _ _ _ _ _ _ _ _ _
Yes =all samples OK
No =Samples were preserved at lab as listed
Comments: _ _ _ _ _ _ _ _ __ _ _ _
__________________
000j
COLUMBIA ANALYTICAL SERVICES, MNC.
Client: Jacobs Engineering Group, Inc. Service Request No.: A9700967Project: Eielson Firing Range/05M30701 Date Received: 10/16/97Sample Matrix: Soil
I ~ ~~~~~~~~CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc.(CAS). This report contains analytical results for sample(s) designated for Tier ACOE data dieliverables. Whenappropriate to the method, method blank results have been reported with each analytical test. Additional qualitycontrol analyses reported herein include: Matrix/Duplicate Matrix Spike (MS/DMS), Laboratory/Duplicate
Laboratory Control Sample (LCSIDLCS), and Initial Continuing Calibration Verification Standards (ICV/CCV).
All EPA recommended holding times have been met for analyses in this sample delivery group.
I~ ~~Apoe y t '
__ JACOBS ENGINEERING GROUP INC A I?00 (7~JE 4300 B STREET, SUITE 800, ANCHORAGE. ALASKA 995015922A s TELEPHONE 907) 5813.32 FAX (907) 563-3320 CHAIN OF CUSTDY RECORDUSE A BALLPOINT PEN, BLACK INK, AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACK
PROJECT NAME:c A ? itwcr ADOR~t Snt
PR-OJECT NUMBER: = =-1 go'o
WSB CODE: SUBCONTRACT D .0. NO. 4< gs
CO"Mu& a t a: w-oLAkN IT' 1^. - commonV-f "'
EY.. NI//( DATET6E TU lf4NARO"•VoJ_7AY-N
__ __ ~~~~V)I cltl ; tMOj I_ _ _ _ _
R.ECR RETUREDBY ATE1 TUK 1JNAUN U
DITRBUIO: WT RJC IECW DASRCITE P DAE REUNOUSED B CY DATEE
81w9340 lambma~0
Columbia Analytical Services, Inc.Cooler Receipt and Preservation From
Client: Jacobs Engineering Group, Inc. Work order: A9700967Project: EIEL$ON FIRING RANGE/05M30701Cooler received on: 10/16/97 and opened on 10/16/97 by Sherry Long
Yes NLAI Were custody seals on outside of cooler? MR 0 0
If yes, how many and where? I FrontWere signature and date correct? El 00
2 Were custody papers properly filled out (ink, signed, etc .... )? [RI 03 Did all bottles arrive in good condition (unbroken, etc .... )? FX1 0 014 Were all bottle labels correct (analysis, preservation, etc ...)? 0 05 Did all bottle labels and tags agree with custody papers? Q1 Q6 Were correct bottles used for test indicated? 0 0 0l7 Were VOA vials checked for absence of air bubbles, and noted? 0 0 M
8 Temperature of cooler upon receipt 10.2 Degrees C
Client: Jacobs Engineering Group, Inc. Service Request No.: A9700963Project: .Eielson Firing Range/05M30701 Date Received: 10/15/97
Sample Matrix: SoilI
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc.(CAS). This report contains analytical results for sample(s) designated for Tier ACQE data deliverables. Whenappropriate to the method, method blank results have been reported with each analytical test. Additional qualityIcontrol analyses reported herein include: Matrix/Duplicate Matrix Spike (MS/DMS), Laboratory/DuplicateLaboratory Control Sample (LCS/DLCS), Initial Continuing Calibration Verification Standards (IC V/CC V), andInitial Continuing Calibration Blanks (ICB/CCB).j
All EPA recommended holding times have been met for analyses in this sample delivery group.
Approved by ~- ae~
2 AM;;n
__JACOBS ENGINEERING GROUP INC F¶ W nJE 4300 8 STREET. SUITE 600. ANCHORAGE. ALASKA 99535fl22®TELEPHONE (9071563.3322 PAX (907) 543.32 CHAIN OF CUSTODY RECORD
USE A BALLPOINT PEN. BLACK INK, AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE 1BACK
COLLECTEDS& REy DATE TKIE IURNAROUND Toe u L A E ! v ~ a _ _ _ _ _ _ _ _ _ _ _ _ _
R By ~~~~~~~DATE TWE 11REUNQJ4IED BY DATE TIME
RECORD RETURNED BY DFATE TME
DISTRIBUTION W1411 - PROJECT RLE /CAN4ARY LAB RECEPT PME - DALA IAANAGmqNT / GQUDfrc - FIED
Columbia Analytical Services, Inc.Cooler Receipt and Preservation From
Client: Jacobs Engineering Group, Inc. Work order: A9700963Project: Eielson Firing Range/05M30701Cooler received on: 10/15/97 and opened on 10/15/97 by Sherry Long
Yes No LI Were custody seals on outside of cooler? [El9
If yes. how many and where? 2 F &BWere signature and date correct? 0
2 Were custody papers properly filled out (ink, signed, etc .... )? MI3 Did all bottles arrive in good condition (unbroken, etc .... )? MR 04 Were all bottle labels correct (analysis, preservation, etc .... )? [E 01 0-
5 Did all bottle labels and tags agree with custody papers? 0R C 016 Were correct bottles used for test indicated? MR 9- 97 Were VOA vials checked for absence of air bubbles, and noted? 0 03M8 Temperature of cooler upon receipt . Degrees C
Explain any discrepancies: Cooler to small to insert thermometer, no temp blank. [
Yes No Sample I.D. Reage Vol.
pH Reagent x L12 NaOH x2 HN0 3 X _______
2 H2S0 4 x L
Yes =all samples OK __________
No =Samples were preserved at lab as listed
Commnents:
Ir.
L2
COLUMBIA ANALYTICAL SERVICES, INC.
Client: A97000831I Service Request No.: A9700831Project: - Eielson Range Flow Date Received: 9/16/97Sample Matrix: Soil
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc.(GAS). This report contains analytical results for sample(s) designated for Tier ACQE data deliverables. Whenappropriate to the method, method blank results have been reported with each analytical test. Additional quality contrlanalyses reported herein include: Laboratory Duplicate (DUP) and Matrix Spike (MS).
All EPA recommended holding times have been met for analyses in this sample delivery group.
¶ ~~~The analyses for TS, BOD, and TOG were performed in our Kelso, Washington laboratory. The Service Requestnumber for this work is K97068 18.
Approved by__________9________ / tI7 0 0 0
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Columbia Analytical Services, Inc.Cooler Receipt and Preservation From
Client: Jacobs Engineering Group, Inc. Work order: A970083 1Project: Bielso~n Range FlowCooler received on: 9/16/97 and opened on 9/16/97 by Meghan Kennish
Yu No MLAI Were custody seals on outside of cooler? 0 X 0
If yes, how many and where?
Were signature and date correct? x 0 0
2 Were custody papers properly filled out (ink, signed, etc ... )? x o o3 Did all bottles arrive in good condition (unbroken, etc .... )? x o o
4 Were all bottle labels correct (analysis, preservation, etc .... )? x 0 o5 Did all~bottle labels and tags agree with custody papers? x o o
6 Were correct bottles used for test indicated? x o 0
7 Were VOA vials checked for absence of air bubbles, and noted? o o x
S Temperature of cooler upon receipt 4.9 Degrees C
Explain any discrepancies: ____________________________
Yes = all samples OKNo = Samples were preserved at lab as listed
Comments:
00 00 i
COLUMBIA ANALYTICAL SERVICES, INC.
Client: Jacobs Engineering Group, Inc. Service Request No.: A9700656Project: Eielson Indoor Firing Range (AOC 32) DateReceived: 8/13/97Sample Matrix: Soil
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc.(GAS). This report contains analytical results for sample(s) designated for Tier ACQE data deliverables. When
- ~~~appropriate to the method, method blank results have been reported with each analytical test.
All EPA recommended holding times have been met for analyses in this sample delivery group.
FDA is a high pressure, total dissolution technique that utilizes a combination of acids (HF, HCI, and HN0 3).Refractory samples, sililateous material and most minerals are completely dissolved using this technique.
Approved by 1~0 Cnate-L//<&f -7
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Columbia Analytical Services, Inc.Cooler Receipt and Preservation From
Client: Jacobs Engineering Group, Inc. Work order: A9700656
¶ ~~~Project:Cooler received on: 8/13/97 and opened on 8/13/97 by Sherry Long
YnNo WAI Were custody seals on outside of cooler? 01 MR0
If yes, how many and where?
Were signature and date correct? MR 0 032 Were custody papers property filled out (ink, signed, etc ... )? MX 0 0
., Did all bottles arrive in good condition (unbroken, etc .... )? 5X 1 014 Were all bottle labels correct (analysis, preservation, etc .... )? MX 0 535 Did all bottle labels and tags agree with custody papers? 03 06 were correct bottles used for test indicated? 5 57 Were VOA vials checked for absence of air bubbles, and noted? 0 08 Temperature of cooler upon receipt Ambient Degrees C
Explain any discrepancies: ____________________________
Yes No Sample I.D. Rae Vl
pH Reagent ___ ______
12 NaOH _ _
2. HNO 3 _ __ _ _ _
2 H2 S0 4 ____ __ ________
Yes = all samples OK
No = Samples were preserved at lab as listed
C~ommrents:-
COLUMBIA ANALYTICAL SERVICES, INC.I
Client: Jacobs Engineering Group, Inc. Service Request No.: A9700530Project: Eielson Indoor Firing Range (AOC 32) Date Received: 7/16/97Sample Matrix: Solid
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc.(CAS). This report contains analytical results for sample(s) designated for Tier ACOE-4 data deliverables. Whenappropriate to the method, method blank results have been reported with each analytical test. Additional quality controlIanalyses reported herein include: Matrix/Duplicate Matrix Spike (MS/DMS), Laboratory/Duplicate Laboratory ControlSample (LCS/DLCS), and Initial Continuing Calibration Verification Standards (ICV/CCV).
All EPA recommended holding times have been met for analyses in this sample delivery group.
Approved by 24m TC Date 85$/,9,j 000
I ~JAC0dS ENGINEERING GROUP INC.4170S3 i/[JE 430 B STREET. SUITE 00 ANCHORAGE. ALASKA B9503-5922 I,TELEHNCE (907) 503-3322 FAX (907) 5C3320 CHAIN OF CUSTODY RECORD
USE A BALLPOINT PEN, BLACK INK. AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACK
[ PROJECT NAME: LABORATORY NAME &ADDRESS
WBS CODE: SAJBCONTRACT I 0.0. No.9 , t,,es~ *ir ~ { r
4r rcci~ Ce.J A,&i vs (4w:o4r-ra Cs...s$e* \SA3161COLLECTED & RELEASED BY '~DATE IE ITRNAROUNO TIME
7v y _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 2_
REC I - ~~~~~DATE TIME REUNCUISHED BY DATE TIMEf
RECORO RETURNED BY DATE TWE
SNI)PPW NUMBER: ?H~ -3 g iDtSTIhBU~rflJ: M41E - PROJECT RI.E/ CANARY - LAS RECEIT /PM~ - DAIA ?MNAGa4B6r I GOfLDENROD - FIELD
_JACOBS ENGINEERING GROUP INC.(4 7 5 o3 -JE300 B STREET. SUITE = MNCHRAGE. ALASK.A 9950-5922FElTELEPHONE (907) 5C33 FAX (9710563-3320 CHAIN OF CUSTODY RECORDUSE A BALLPOINT PEN, BLACK INK. AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACK
P&OJECT NAME: (ALA LUMIYLM &R 1 5W ISc.,-ePROJECT NUMBER: 'ii uins L"'S I Wuk Sit VIWES CODS: SUBCONTRACT I .. NM.4~ ~a-t.
1~~ coa~~~cuowt~~~~ 4v . Arhi b A tc e. 7I-3 2-'6
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C~ __j- e0 7 -c m -q_ _ _ _ _ _ _ _ _ _ _
COMMENTS' I
COLTTED & LEASED B~YTUNRNDim
RECEIVED BYE ELNQISEDB DATE TIME
REODRETURNED BY DATE "a____
D~simaullt WH~t - ROJECT /SHIPPIN NUMBER: H r3 ' Z 6D1A3.A PMU~4BET / G flS~iROD
_JACOBS ENGINEERING GROUP INC. Cbe417 •3we43W B STREET. SUITE 6W O4ORAGE. ALASKASOSO3-522CHIOFUSDYR ODmi EI.EP4O (907) 563-3322 FAX (9D7) 563-3320CHIOFUS DYROD
USE A BALLIPOINT PEN, BLACK INK. AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACK
PROJECT NAME: LASORAORY NAME A ADDRESS.
WES CODE: SUBCONTRACT I D.0 .I 4No.14klle" VPl Itj4*;J
RON= ~ ~ o
~~ 4 t~hI~~fl'flAM~~ ~ ~~Q tcA
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4-44 J59?6E I o r ,.1- __
COMMDENS: - -~( 4 P _ _COLUCTED& AEOYr LA11gb gr~TM REUOUN4D nYDAE IM
FREC-ORD RETURNED BY DATE TE
SHIPPIING NUMBER:
D4STIBThIuNa WMIE - PROJECT FILE I CANARY- LAS RECEIPT PMfl - DMAIAM ARAEaiEVT U 0 0 00 (2 0
ft ~JACOBS ENGINEERING GROUP INC.JAE 4300 B STREET. SUITE 600 ANCORAAGE. ALASKlA 99eW5922 t47,70053oit: T~mOJEw)Scan FAX~7)5C3320CHAIN OF CUSTODY RECORDUSE A BALLPOINT PEN. BL.ACK INK, AND PRESS FIRMLY. INSTRUCTIONS ARE ON THE BACK
7 CT NAME: LBRTY AE& ADDrES1:
PROJECT NUMBER:OI t -A Stt
11 ~~WES COOE: SUBCONTRACT I 0.0. NM.
A ~~raa P3~SA M P~~~~~~~~~~~~t _ _ _ _ _ _ _ _ S2 Sal -~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~.
Client: Jacobs Engineering Group Service Request No.: K9705076Project: Eielson Firing Range Date Received: 7/18/97Sample Matrix: Soil, Water
Li ~~~~~~~~~CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc.(CAS). This report contains analytical results for sample(s) designated for Tier 11A data deliverables. WhenI ~ ~~appropriate to the method, method blank results have been reported with each analytical test. Surrogate recoveries havebeen reported for all applicable organic analyses. Additional quality control analyses reported herein include:Matrix/Duplicate Matrix Spike (MS/DMS) and Laboratory Control Sample (LCS).
I ~~~All EPA recommended holding times have been met for analyses in this sample delivery group.
I ~~~The following difficulties were experienced during analysis of this batch:The 8260 surrogate recovery in sample JE97E I E 1 36US was outside normal CAS control limits because of suspectedmatrix interference. The sample was re-analyzed, and again produced results outside control limits. The results of thej ~~~original analysis are reported.
The 8260 soil Matrix Spike/Duplicate Matrix Spike (MS/DMS) recoveries of several analytes were outside the normalGAS co ntrol limits because of matrix interferences caused by excessive levels of Naphthalene. No further corrective
action was taken.
The 8260 soil Matrix Spike/Duplicate Matrix Spike (MS/DMS) recovery of Naphthalene was not calculated. 'TheI ~ ~~analyte concentration in the sample was significantly higher than the added spike concentration, preventing accurateevaluation of the spike recovery.
Columbia Analytical Services, Inc.Cooler Receipt and Preservation From
Client: Jacobs Engineering Group, Inc. Work order: A9700533Project: Ejelson Firing RangeCooler receivedobn: 7/18/97 and-opened on 7/18/97 by Chris Ezell
nc NLA1 Were custody seals on outside of cooler? x o o
If yes, how many and where? 2 f&bWere signature and date correct? x o o
2 Were custody papers properly filled out (ink, signed, etc .... )? x o o3 Did all bottles arrive in good condition (unbroken, etc .... )? x o o
- ~~ ~~~4 Were all bottle labels correct (analysis, preservation, etc .... )? x o o5 Did all bottle labels and tags agree with custody papers? x o o6 Were correct bottles used for test indicated? x o o7 Were VQA vials checked for absence of air bubbles, and noted? x o a8 .Temperature of cooler upon receipt 4.8 Degrees C
Explain any discrepancies: ____________________________
_______ ~Yes No Sample I.D. Reage Vol.
-pH Reagent x12 NaOH x2 HNO3 X
2 H2S04 x
* ~~Yes = all samples OK __ __________
No = Samples were preserved at lab as listed
Comments:
a~~~~~~~~~~~~~~~~~~~~~~I
000 026
!000
r - -~~~~~~~~-LLA~ ~ ~ ~ N~rcc~~~~~~~~~~~~~~~~~~~~
MEMORANDUM FOR ENVIRONMENTAL PROTECTION AGENCY (EPA)ATTENTION: MS. MARY JANE NEARMvANOffice of Environmental Cleanup Unit 441200 Sixth Ave ECL- 113Seattle WA 98101-3180
FROM; 354 CBS/cc2258 Central Ave StelOCEielson APE AK 99702-2299
SUBJECT; Transmitta Letter for Cleanup Level Acceptance at the Indoor Firing Range(Building 2204)
1. I am writing this transmittal letter in response to your conversation with Mr. Jim Me Millan,354 CBS/CEVR, on 8 J'an 98, regarding your deparirnents verbal acceptance of Building 2204,Indoor Firing Range cleanup levels of lead-contaminated sands. Work was completed this pastfield season by Jacobs Engineering Group/Brice Environmental Services Corporation. In theStatement of Work, a target rernediation cleanup goal of 1 00 microgranis/squar foot waschosen. This residential lead cleanup level is designed to primarily protect young children whoplay on floors. The level is based on US Department of Housing and Urban Development's(HUD) 1991 residential cleanup standards. US Department of Housing and Urban Developmentalso established additional cleanup levels for interior window sills of 500 rnicrogramis/squarfoot, and a window trough, exterior concrete/rough surface level of 800 micrograms/square foot.Although the target cleanup level wasn't attained in all sample results, the results were below thesecond and third higher levels, and well within an acceptable range for the rough surfacescleaned. The basement area is an isolated area without a ventilation/air system, so there wouldbe no movement of basement air into any oilier portion of the building.
2. Based on the achieved cleanup levels, anticipated long range usage of that basement facility(archery range), the fact that no inside air is exhausted into the remainder of the building, andverbal acceptance from both the EPA and the Alaska Department of Environmentai* ~~Conservation; Eielson AFB accepts the current cleanup standard and will convey the facilityback to our real property officer for disposition.
SAU L WUU15
12'/12'/97 U9L50 IUO7 452 5018 BRICE INC. -tJACOBS ENGINEERI I4oo3/00312/12-97 FRI 08:51 FAl 19073773367 CEV c .000 2
E)-/ei'e
State of LouisianaDepartment of Environmental Quality K1
fla OVEIRtNFOT R. J5. DALE GIVF.%'s
GOVERNOR A~~~~~~~~~~~~~~~~ECRETAR'r
Rcurn ROCC eitkquestedZ 012 944 686
Dlecember 10, 1997
Mr. Jim McMillanBielson Air Porce BaseFairbanks, AK 99702-2299
RE: Lead Connminated SandSchuylkill ManiaLADOOS8 184 137
Deax Mr. McMillan:
The Louisiana Deparmnent of(Enviro enmtnl Qua lity, Hazardous WseDvso LE-w)Mconideed ourreqestforinfrmaIon regarding rho ability of The Schuylkill Metals Corporationfacility, located in Baton Rouge, Louisiana, to accept sand conlrtiagbld with leadi bullets. This sand,approximately 99 largo bags, was genextmod from the cleanup of a forme fig raC. Schuylkcill isapermined facility and may accept such materials. AS the generator, YOU ane required to properlycharacterize this weane and ship it accordingly. lIfthe material is a hazardous waste it must carry thecode for the constituent~s) responsible for that classilicagion e.g. DO0R for lead. The proper handling
code (recycling) should be included on the manifest.
Should you have any questions concerning this correspondence, please contact Mr. Mike Miller atC504) 765-0272.
Sincerely,
esamC'Aat. ~
James H. Brent, Pk.DAdministrawr P0a:.fl. Fax Note 7671 i
This letter serves as notification of Secretary -Kai D.Midboe'Is f inal decision to issue a hazardous waste operating permitto Schuylkill Metals Corporation located in Baton Roug'e, East EatonRouge Parish, Louisiana. The effective date of tbe final permnit isNovember 1, 1993. This permit will expire an November i, 2003.
Responses to all comments received during the comment periodcan be f ound at the end of the permit in the ResponsivenessSummary.
in accordance with La. RLS. 3012024, the applicant may requestan adjudicatory hearing within thirty (30) days from date ofservice or any person aggrieved by a final decision or order of theSecretary may appeal to the Court of Appeal, First Circuit, if amotion for appeal is filed with the Secretary within thirty (30)days after thet final decision or order is served upon theRespondent. only the specified provisions appealed will besuspended pending an adjudicatory hearing. Al]1 other provisions ofthis permit will become effective on the specified date.
If you have any questions regarding this action, pleasecontact Mr. Scott Guilliams at (504) 765-0272. Thank you for yourattention to this matter..
Assis at Secretary
GAM/fl/j~g
Enclosure
c: Mr. William Gallagher, U.S. EPAMs. Maria Daniel, U.S. EPAMs. Ann Zimmerman, U.S. EPA
WUXISrANA DEPARTMEfNT OF ENVIRONMENTAL. QUALrrY
HAZARDOUS WASTE IS) FACILIT
OPERATDIG PERMIT
pma4JrrEE Schyirviill Metals Cororatiop
nLSMIT NU3SUER LAD008I84137-OP-1
FACILIY West End of Brookiawn DriveLOCATION: Baton Route._Louisi-ana 70807
This permit is issued to the permittee by the Louisiana Deoarizuent of EnvironmentalQuality CLEQ) and the United States Environmaental Protection Agency (USEPA) underthe authority of the Louisiana Hazardous Waste Conral Law R.S. 30:2171 et seq., and theregulations adopted thereunder and by the U.S. Environmental Protection Agency underthe authority of the 1984 Hazardous and Solid Waste Amendments to RCRA CHWA) toSchuykikll Metals Corporation, (hereafter called the permittee), to operate a hazardouswaste treatment and storage CM51) facility located at Baton Rouge, Louisianat, at latitude3a0 35'008" and longitude 31' 14140M.
The permittee must comply with ail terms and conditions of this permit. This permitconsists of the conditions contained herein and the applicable regulations as specified in this
* ~permit. Applicable regulations are those which are in effect on the date of issuance of thispermit.
This permit is based on the assumption that the information provided to LDEQ by thepermittee is accurat. Further, this permit is based in part on the provisions of Sections206, 212, and 224 of the HSWA of 1984, which modify Sections 3004 and 3005 of RCRA.In particular, Section 206 requires corrective action far all releases of hazardous waste orconstituents from any solid waste management unit at a treatment, storage or disposalfacility seeking a p&rmit, regardless of the time at which waste was placed in such wnilt.
7 ~Section 21.2 provides authority to review and modify the permit at any lime. Anyinaccuracies found in the submitted information way be grounds for the termination,modifiation or revocation and reissuance of this permit (-see LAC 33:V-323) and potentia
* ~enforcement action- The permittee must Inform the administrative authority of anydeviation from~ or changes in the information in the applicatian which would affect thePermittee's ability to comply with the applicable regulations or permit conditions.
his permit is effective as of November 1 .199l and shall remain" in effct222n~p~npr 9 n l~,unless revoked and reism ed, modified or terminated In accordance I
kb LAC 33:V.705 of the Louisiana~ Hazardous Waste Regulations.
0~~~~~~~~~~~~~~~~~1 ~~~~ ~ ~ *
Louisiana Department of Environmental Quality
3~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
DEPARTMENT OF THE AIR FORCEPACIFIC AIR FORCES
I g F,2:
MEMORANDUM FOR LOUTISIANA DEPARTMENT OF ENVIRONMENTAL QUALITYATTENTION: MR. MIK.E MILLEROffice of Waste ServicesH-azardous Waste DivisionP 0 Box 8278Baton Rouge LA 90884-2178
FROM: 354 CES/CE-22258 Central Ave Ste 100Eielson AFB AK, 99702-2299
SUBJECT: Transmittal Letter for Movement/Transportation of Firing Range Sands
1. I am writing this transmittal letter in response to your conversation with Mr. Jum Mc Millan
on 5 Dec 97, regarding your departments verbal okay to ship our firing range sands to the
Schuykill Metals Corporation (Exide smelter) in Baton Rouge, LA. These sands will be used as
a flux material for Schuykill's blast furnaces.
r 2. It is our intention to start loading the sands 8 Dec 97. We will have five van loads totaling
approximately 21 0,000 pounds. It is our understanding that the Louisiana Department of
Environmental Quality is forwarding an approval letter, upon directorate signature to Eielson
AFB, for your departments final approval authority in this matter. In lieu of receipt of this letter,
we plan to start shipping the first van load upon completion of loading, and one van load every
subsequent two weeks via Lyndon Transport (Fairbanks shipper).
L ~~3. Thank you for your coopcration and assistance in this matter. For fuither information orquestions, please contact Mr. Jim Mc Millan, 354 CES/CIEVR. 907-377-5209.
g LMllS 6113, RA
OPTIONAL FUHN4 99 (I-0f))
FAX TRANSMITTALIT
r 33 0 Fa.5 j 3NGN 75-0J1-.317-73d0 5092-101 GENERAL SEIRVICES ADMINIS AATION
-"f UJ.I ~l &U~i AJ Q09 DuavIn 't 1'N~- - ' JAC0Ub~' LiNkl.ti\t~l LVJ00 o 2 /0'97 FRI 02:44 PM EXIDE MIETALS GROUP FAX NO, 610 378 0514 P. 0I/O]
Per our telephone copversatian, Excide Corporation wfill accept one -load ofrange sand every tw.o weeks at our Baton Rouge, Louisiana facility This. sand willbe used as a flux li ourbls rac.
S incerely,
T'HOMAS W. KERCHNERAssistant DirectorMetals:Group
645 Penn, Street Reading, PA 19601P.0.. Box 14205 Reading, PA 19612-420S
-- , - .-n±0z - I4. ** UALUUj _ t.ltKI 'C005/006lkAiJ.Vi I A JU .,Lj Lat JA(UD.~ L2%U.\LLRIN,\Uv
DEPARTMENT OF THE AIR FORCEPACIFIC AIR FORCES
7CP"3,J997
MEMORANDUM FOR ENVIRONMENTAL PROTECTION AGEFNCY REGION 7A1TTN: BILL GRESHAM
FROM: 354 CE.S/CC2258 Central Ave Ste 100Eielson AFB AK 99702.22 99
SUBJECT: Lead-Contamninated Sands fromn Indoor Firing Range, Building 2204. HielsonAir Force Base (Eielson)
I. Eieison will be shipping reused materials (firing range sands) to The Exide facility inybur region. An exctensive revjdw was conducted by the Air Force of thte variousalternatives regarding the remnoval and disposal of thre lead-bearing sand, consideringissues of cost, schedule, and liability. The findings determined the most effectiveapproach forthe project was to ship the sand to Exide Corporation's secondary sinelter hidarnhon14blloW., Mi~s'sori.' The material, which was determirid to cedhtain a silicacontent of 80 percent. would replace sands with a similar silica content normally requiredfor use as flux material during the lead-snmelting process.
2. One of our concerns surrounding trrnisporting the firing range sand to a smelter waswhether EPA would clasi$fy the material as ibithr i solid waste, or exempt from being asolid waste undcr 40 CPR 2612.2 The classification issue is importantL because or theexorbitaim cosis associated with hanzadous waste manifested Shipments versus bill orlading shipments from Alaska to the ILower 48. -3Bot Mary Jane Nearman and DaveBartus, EPA-Regioin 10U, assisted us in clarifying ibis issue. Our fiwa deECrIninat ion iNbased art 40 CFR 261.2 (e).(1) which specifies that materials are not solid waste wheni
.~~~theyxcan-be shown Lo-be~reeycled by being.: .
a:l "Uied oi feused a-s ingredierns .i~n:an industvial prdcess to make a prdduct. providcdthe materials ar-e not being reelaimed;" or
b. '~Usedtot-rcus-d as cffective substitumes forcorn~mdrc fi~L'pctts." (probc.Jc51)
3. It is our opinion, based on the silica content of the s11ooting range sand, thaL rht~mdterial qualifies under patt ii of te regulation. During the sirelting process a -.-lux.agerit" (sand) containing-a high percernage. orsilica must be used as part of' the Snottlingprocesk. This nLTerialnmtustbe Purchased by thcsnmelter asan itgredienrifor the sneltingprocess. if niot oxherwisc available. Many firing ranges are comoosed of clean; Washedsands contaninfg liTtle, if any finds in 6rder to niiniriiile dust, generation or rockl in order
*-to minimize ricochets; When hin'g range tands-are6omnpos&d'of. silica minerals:'silica.
comprises the bulk Of the mass of the material, thus making it an ide~J substitute for thccommercially available flux agent. Since the Eielson firing range sands contaiin a silicacontent matching the comxncrcial flux agent, according 1o040 CFR 261.2 Ce) (ii). we willnot require hazardous waste manifesting during shipment to the smelter facility.
4. Support fcr our interpretation that the Eielson firing range sand is exempt froni7hazardous waste manifesting requirements is enclosed in the form of correspondencefrom: (1) EPA Region 4; (2) the state of North Carolina; (3) the state of Washington.Depantment of ECOlu6; and C4) the state of Missouri, Department of Natural Resources.
S. We realize that regardless of the exempti ons in 40 CFR 261.2 (e). the firing ranigesands still must be packaged compliant with DOT regulations governiing dry solids andour transport liability minimized. As suciL we are requiring the sands be loaded intosupersacks With A precautionary required inner liner. Furthermore, we -are also requiringthat the supersacks be shipped in closed truck trailers only. Should you heave anyquestions concerning the transportation of the firing range sands from Eielson. pleasecontact Mr. Mike Raabe, Chief, Installation Restoration Program, (907) 377-1164.
Attachments:1. Lrr,l16 Mar 942. Lu:'29 Mar 95
3.Lf, 15 Jan 974: LTr,-7 Dec 93-
cc:Mfizy .Iane.Nearman, EPA Region 10Dave Bartus. -EPA Region -10.Ron Short, ADECRobin'Moshier. Eiicsoni AFBM1ike R~aabe, Rielson AFB
fax (907) A5P-S0lo Ms. Kim KearneyJacobs Engineering Group, Inc.
554Roo 3' 4300 B Street, Suite 600Ro. Box 76 Anchorage, Alaska 99503
Ringoes. NJ O8&551Tel [908) 806-3655
tax(98)80-393 RE: Bill or Lading Information and Package Labeling
e-ma121: Dear Kim:b@f oarp
opoarnl~crPrior to loading and transporting the Eielson sands from Alaska to Baton Rouge,Louisiana, we need to address information that will go on the bill of lading and on thepackages of sand. I have researched this and enclose my findings andrecommendations. Jacobs must provide final approval, so I recommend that atransportation specialist within your group review my findings as quickly as possiblein order to avoid any delay associated with the disposition of the material.
The silica sand is not a hazardous waste because the material meets the provisions ofI40 CFR 261.2 (e) (ii). Consequently, the Hazardous Waste Manifest Requirements ofthe U.S. Environmental Protection Agency (EPA) specified in 40 CFR Part 262 do norapply.
49 CFR 172.101, Department of Transportation regulations stipulate package labelingand nomenclature forthe bill of lading. Part 172.1 01, Table 1. - Hazardous SubstancesOther Th$n Radionuclide's was reviewed and lead identified on page 240. The tablespecifies that Lead has a reportable quantity (RQ) of 10 pounds (lb.) per package. Thefootnote states that the RQ for this hazardous substance is limited to those pieces ofthe metal having a diameter smaller than 100 micrometers (.004 inches orapproximately 140 mesh).
According la the DOT, a hazardous substance means a material including its mixtures andSolutLiouns that. I) are lIIsted in Pant 172. 101L (2) is in a quantity in one package w hi chequals or exceeds the reportable quantity (RQ) l isted in Pant 172. 101, and, ,(3) when in amixture or.solution exceeds the concentration corresponding to the RQ of the material.
Using high-end treatability study results, lead concentrations were determined to beapproximately 80,370 mglkg for the bullet trap. sand and 3.865 mgg for the range floorsand. Approximately 23 percent of the material recovered from the range was from thetrap irea and 77 percent was from the range floor area. The material from each area wasplaced into supersacks. Upon completion of the removal action, sands were re-distributed because the weight limit for some of the supersacks was exceeded. Uponproject completion 99 supersacks were filled, with an average weight of 2.083 pounds.-
In order to determine if the packages contain material meeting the hazardous substancedesignation listed above, the lead concentration and material quantity from each area wasweight averaged using the treatability study and quantity information listed above. Theaverage quantity of lead was determined to be approximately 47.9 pounds per supersack.
Although the quantity is approximately 47.9 lbs./package, treatability study results haveshown that virtually all of the lead is greater than .004 inc hes in diameter (140 mesh).The treatability study did not examine the minus 140 mesh fraction, however the minus200 mesh was analyzed for rotal lead. The minus 200 mesh fraction was dletermnined to be1.62 percent of the bullet trap sand gradation and contain 69,5316 mg/kg lead, while therange floor sand contained 1.91 percent minus 200 containing 3,750 6 mg/kg leadExtrapolating this data to the bulk soil results in an avenage minus 200 mesh leadcontribution of 0.66 pounds per package. It is not possible for the minus 140 by 200mesh fraction to contain an additional 9.34 pounds of lead, hence the material does notmeet the DOT hazardous substance designation.
If the material had met DOT's definition of a hazardous substance, the following wouldhave been required for the Bill of Lading:
Hazard Class 9UN # 3077
Plackaging Group IllEnvironmentally Hazardous Substance, Solid (N.O.S.) Lead
Each package would have had to be labeled as follows:
UN #3077
Environmentally Hazardous Substance, Solid (N.O.S.) Lead
Because the material does not meet the DOT definition of a hazardous substance, the billof lading only needs to include a description of The material. The material will bedescribed as follows:
"Silica Sand"
Each supersack will be labeled the same.
Sincerely,
Caig Jones
Jniform Straight Bill L3ND3NM) Lading THEr ALL MODEL CAHRIER =MI
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First time pick-up?-tiiJ-No If not, is MSDS or lab sample available? CieuiNo